BQS OBSP Determination:
1-NAPHTHOL
METHOD: 2033 , TESTIDCODE: 49295GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 24% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 65% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 24% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 37% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 56% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 59% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 54% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 45% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 41% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 45% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 13% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 32% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 50% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 24% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 15% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 39% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 44% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 25% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 38% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 42% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 29% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 62% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 49% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 62% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 55% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 71% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 33% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 33% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 78% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 96% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 179% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 92% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 131% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 72% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 119% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 122% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 98% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 40% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 50% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 44% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 49% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 40% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 14% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 39% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 20% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 63% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 21% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 73% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 26% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 43% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 57% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 17% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 58% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 39% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 18% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 31% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 66% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 76% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 28% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 13% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 36% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 24% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 36% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 19% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 39% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 40% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 93% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 96% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 99% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 157% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 124% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 124% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 123% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 146% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 138% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 156% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 91% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 168% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 64% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 67% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 54% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 76% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 62% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 29% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 56% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 60% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 38% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 41% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 59% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 36% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 78% Analysis Date = 01/17/17 Pct Recovery = 48% Analysis Date = 01/07/17 Pct Recovery = 48% Analysis Date = 01/07/17 Pct Recovery = 48% Analysis Date = 12/27/16 Pct Recovery = 48% Analysis Date = 12/27/16 Pct Recovery = 48% Analysis Date = 12/16/16 Pct Recovery = 47% Analysis Date = 12/16/16 Pct Recovery = 47% Analysis Date = 12/05/16 Pct Recovery = 47% Analysis Date = 12/05/16 Pct Recovery = 47% Analysis Date = 11/24/16 Pct Recovery = 47% Analysis Date = 11/24/16 Pct Recovery = 47% Analysis Date = 11/13/16 Pct Recovery = 47% Analysis Date = 11/13/16 Pct Recovery = 47% Analysis Date = 11/03/16 Pct Recovery = 46% Analysis Date = 11/03/16 Pct Recovery = 46% Analysis Date = 10/23/16 Pct Recovery = 46% Analysis Date = 10/23/16 Pct Recovery = 46% Analysis Date = 10/12/16 Pct Recovery = 46% Analysis Date = 10/12/16 Pct Recovery = 46% Analysis Date = 10/01/16 Pct Recovery = 46% Analysis Date = 10/01/16 Pct Recovery = 46% Analysis Date = 09/20/16 Pct Recovery = 46% Analysis Date = 09/20/16 Pct Recovery = 46% Analysis Date = 09/09/16 Pct Recovery = 45% Analysis Date = 09/09/16 Pct Recovery = 45% Analysis Date = 08/29/16 Pct Recovery = 45% Analysis Date = 08/29/16 Pct Recovery = 45% Analysis Date = 08/19/16 Pct Recovery = 45% Analysis Date = 08/19/16 Pct Recovery = 45% Analysis Date = 08/08/16 Pct Recovery = 45% Analysis Date = 08/08/16 Pct Recovery = 45% Analysis Date = 07/28/16 Pct Recovery = 44% Analysis Date = 07/28/16 Pct Recovery = 44% Analysis Date = 07/17/16 Pct Recovery = 44% Analysis Date = 07/17/16 Pct Recovery = 44% Analysis Date = 07/06/16 Pct Recovery = 44% Analysis Date = 07/06/16 Pct Recovery = 44% Analysis Date = 06/25/16 Pct Recovery = 44% Analysis Date = 06/25/16 Pct Recovery = 44% Analysis Date = 06/14/16 Pct Recovery = 43% Analysis Date = 06/14/16 Pct Recovery = 43% Analysis Date = 06/04/16 Pct Recovery = 43% Analysis Date = 06/04/16 Pct Recovery = 43% Analysis Date = 05/24/16 Pct Recovery = 43% Analysis Date = 05/24/16 Pct Recovery = 43% Analysis Date = 05/13/16 Pct Recovery = 43% Analysis Date = 05/13/16 Pct Recovery = 43% Analysis Date = 05/02/16 Pct Recovery = 42% Analysis Date = 05/02/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/21/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 03/31/16 Pct Recovery = 42% Analysis Date = 03/31/16 Pct Recovery = 42% Analysis Date = 03/20/16 Pct Recovery = 41% Analysis Date = 03/20/16 Pct Recovery = 41% Analysis Date = 03/09/16 Pct Recovery = 41% Analysis Date = 03/09/16 Pct Recovery = 41% Analysis Date = 02/27/16 Pct Recovery = 41% Analysis Date = 02/27/16 Pct Recovery = 41% Analysis Date = 02/16/16 Pct Recovery = 41% Analysis Date = 02/16/16 Pct Recovery = 41% Analysis Date = 02/05/16 Pct Recovery = 41% Analysis Date = 02/05/16 Pct Recovery = 41% Analysis Date = 01/25/16 Pct Recovery = 40% Analysis Date = 01/25/16 Pct Recovery = 40% Analysis Date = 01/15/16 Pct Recovery = 40% Analysis Date = 01/15/16 Pct Recovery = 40% Analysis Date = 01/04/16 Pct Recovery = 40% Analysis Date = 01/04/16 Pct Recovery = 40% Analysis Date = 12/24/15 Pct Recovery = 40% Analysis Date = 12/24/15 Pct Recovery = 40% Analysis Date = 12/13/15 Pct Recovery = 40% Analysis Date = 12/13/15 Pct Recovery = 40% Analysis Date = 12/02/15 Pct Recovery = 39% Analysis Date = 12/02/15 Pct Recovery = 39% Analysis Date = 11/21/15 Pct Recovery = 39% Analysis Date = 11/21/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 10/31/15 Pct Recovery = 39% Analysis Date = 10/31/15 Pct Recovery = 39% Analysis Date = 10/20/15 Pct Recovery = 39% Analysis Date = 10/20/15 Pct Recovery = 39% Analysis Date = 10/09/15 Pct Recovery = 38% Analysis Date = 10/09/15 Pct Recovery = 38% Analysis Date = 09/28/15 Pct Recovery = 38% Analysis Date = 09/28/15 Pct Recovery = 38% Analysis Date = 09/17/15 Pct Recovery = 38% Analysis Date = 09/17/15 Pct Recovery = 38% Analysis Date = 09/06/15 Pct Recovery = 38% Analysis Date = 09/06/15 Pct Recovery = 38% Analysis Date = 08/27/15 Pct Recovery = 38% Analysis Date = 08/27/15 Pct Recovery = 38% Analysis Date = 08/16/15 Pct Recovery = 37% Analysis Date = 08/16/15 Pct Recovery = 37% Analysis Date = 08/05/15 Pct Recovery = 37% Analysis Date = 08/05/15 Pct Recovery = 37% Analysis Date = 07/25/15 Pct Recovery = 37% Analysis Date = 07/25/15 Pct Recovery = 37% Analysis Date = 07/14/15 Pct Recovery = 37% Analysis Date = 07/14/15 Pct Recovery = 37% Analysis Date = 07/03/15 Pct Recovery = 37% Analysis Date = 07/03/15 Pct Recovery = 37% Analysis Date = 06/22/15 Pct Recovery = 36% Analysis Date = 06/22/15 Pct Recovery = 36% Analysis Date = 06/12/15 Pct Recovery = 36% Analysis Date = 06/12/15 Pct Recovery = 36% Analysis Date = 06/01/15 Pct Recovery = 36% Analysis Date = 06/01/15 Pct Recovery = 36% Analysis Date = 05/21/15 Pct Recovery = 36% Analysis Date = 05/21/15 Pct Recovery = 36% Analysis Date = 05/10/15 Pct Recovery = 36% Analysis Date = 05/10/15 Pct Recovery = 36% Analysis Date = 04/29/15 Pct Recovery = 36% Analysis Date = 04/29/15 Pct Recovery = 36% Analysis Date = 04/18/15 Pct Recovery = 36% Analysis Date = 04/18/15 Pct Recovery = 36% Analysis Date = 04/07/15 Pct Recovery = 36% Analysis Date = 04/07/15 Pct Recovery = 36% Analysis Date = 03/28/15 Pct Recovery = 36% Analysis Date = 03/28/15 Pct Recovery = 36% Analysis Date = 03/17/15 Pct Recovery = 36% Analysis Date = 03/17/15 Pct Recovery = 36% Analysis Date = 03/06/15 Pct Recovery = 36% Analysis Date = 03/06/15 Pct Recovery = 36% Analysis Date = 02/23/15 Pct Recovery = 36% Analysis Date = 02/23/15 Pct Recovery = 36% Analysis Date = 02/12/15 Pct Recovery = 36% Analysis Date = 02/12/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 01/22/15 Pct Recovery = 36% Analysis Date = 01/22/15 Pct Recovery = 36% Analysis Date = 01/11/15 Pct Recovery = 36% Analysis Date = 01/11/15 Pct Recovery = 36% Analysis Date = 12/31/14 Pct Recovery = 36% Analysis Date = 12/31/14 Pct Recovery = 36% Analysis Date = 12/20/14 Pct Recovery = 37% Analysis Date = 12/20/14 Pct Recovery = 37% Analysis Date = 12/09/14 Pct Recovery = 37% Analysis Date = 12/09/14 Pct Recovery = 37% Analysis Date = 11/28/14 Pct Recovery = 37% Analysis Date = 11/28/14 Pct Recovery = 37% Analysis Date = 11/17/14 Pct Recovery = 37% Analysis Date = 11/17/14 Pct Recovery = 37% Analysis Date = 11/07/14 Pct Recovery = 37% Analysis Date = 11/07/14 Pct Recovery = 37% Analysis Date = 10/27/14 Pct Recovery = 37% Analysis Date = 10/27/14 Pct Recovery = 37% Analysis Date = 10/16/14 Pct Recovery = 37% Analysis Date = 10/16/14 Pct Recovery = 37% Analysis Date = 10/05/14 Pct Recovery = 37% Analysis Date = 10/05/14 Pct Recovery = 37% Analysis Date = 09/24/14 Pct Recovery = 37% Analysis Date = 09/24/14 Pct Recovery = 37% Analysis Date = 09/13/14 Pct Recovery = 38% Analysis Date = 09/13/14 Pct Recovery = 38% Analysis Date = 09/02/14 Pct Recovery = 38% Analysis Date = 09/02/14 Pct Recovery = 38% Analysis Date = 08/23/14 Pct Recovery = 38% Analysis Date = 08/23/14 Pct Recovery = 38% Analysis Date = 08/12/14 Pct Recovery = 38% Analysis Date = 08/12/14 Pct Recovery = 38% Analysis Date = 08/01/14 Pct Recovery = 39% Analysis Date = 08/01/14 Pct Recovery = 39% Analysis Date = 07/21/14 Pct Recovery = 39% Analysis Date = 07/21/14 Pct Recovery = 39% Analysis Date = 07/10/14 Pct Recovery = 39% Analysis Date = 07/10/14 Pct Recovery = 39% Analysis Date = 06/29/14 Pct Recovery = 39% Analysis Date = 06/29/14 Pct Recovery = 39% Analysis Date = 06/19/14 Pct Recovery = 39% Analysis Date = 06/19/14 Pct Recovery = 39% Analysis Date = 06/08/14 Pct Recovery = 40% Analysis Date = 06/08/14 Pct Recovery = 40% Analysis Date = 05/28/14 Pct Recovery = 40% Analysis Date = 05/28/14 Pct Recovery = 40% Analysis Date = 05/17/14 Pct Recovery = 40% Analysis Date = 05/17/14 Pct Recovery = 40% Analysis Date = 05/06/14 Pct Recovery = 41% Analysis Date = 05/06/14 Pct Recovery = 41% Analysis Date = 04/25/14 Pct Recovery = 41% Analysis Date = 04/25/14 Pct Recovery = 41% Analysis Date = 04/14/14 Pct Recovery = 41% Analysis Date = 04/14/14 Pct Recovery = 41% Analysis Date = 04/04/14 Pct Recovery = 41% Analysis Date = 04/04/14 Pct Recovery = 41% Analysis Date = 03/24/14 Pct Recovery = 42% Analysis Date = 03/24/14 Pct Recovery = 42% Analysis Date = 03/13/14 Pct Recovery = 42% Analysis Date = 03/13/14 Pct Recovery = 42% Analysis Date = 03/02/14 Pct Recovery = 42% Analysis Date = 03/02/14 Pct Recovery = 42% Analysis Date = 02/19/14 Pct Recovery = 42% Analysis Date = 02/19/14 Pct Recovery = 42% Analysis Date = 02/08/14 Pct Recovery = 43% Analysis Date = 02/08/14 Pct Recovery = 43% Analysis Date = 01/28/14 Pct Recovery = 43% Analysis Date = 01/28/14 Pct Recovery = 43% Analysis Date = 01/18/14 Pct Recovery = 43% Analysis Date = 01/18/14 Pct Recovery = 43% Analysis Date = 01/07/14 Pct Recovery = 44% Analysis Date = 01/07/14 Pct Recovery = 44% Analysis Date = 12/27/13 Pct Recovery = 44% Analysis Date = 12/27/13 Pct Recovery = 44% Analysis Date = 12/16/13 Pct Recovery = 44% Analysis Date = 12/16/13 Pct Recovery = 44% Analysis Date = 12/05/13 Pct Recovery = 44% Analysis Date = 12/05/13 Pct Recovery = 44% Analysis Date = 11/24/13 Pct Recovery = 45% Analysis Date = 11/24/13 Pct Recovery = 45% Analysis Date = 11/14/13 Pct Recovery = 45% Analysis Date = 11/14/13 Pct Recovery = 45% Analysis Date = 11/03/13 Pct Recovery = 45% Analysis Date = 11/03/13 Pct Recovery = 45% Analysis Date = 10/23/13 Pct Recovery = 46% Analysis Date = 10/23/13 Pct Recovery = 46% Analysis Date = 10/12/13 Pct Recovery = 46% Analysis Date = 10/12/13 Pct Recovery = 46% Analysis Date = 10/01/13 Pct Recovery = 47% Analysis Date = 10/01/13 Pct Recovery = 47% Analysis Date = 09/20/13 Pct Recovery = 47% Analysis Date = 09/20/13 Pct Recovery = 47% Analysis Date = 09/09/13 Pct Recovery = 47% Analysis Date = 09/09/13 Pct Recovery = 47% Analysis Date = 08/30/13 Pct Recovery = 48% Analysis Date = 08/30/13 Pct Recovery = 48% Analysis Date = 08/19/13 Pct Recovery = 48% Analysis Date = 08/19/13 Pct Recovery = 48% Analysis Date = 08/08/13 Pct Recovery = 49% Analysis Date = 08/08/13 Pct Recovery = 49% Analysis Date = 07/28/13 Pct Recovery = 49% Analysis Date = 07/28/13 Pct Recovery = 49% Analysis Date = 07/17/13 Pct Recovery = 50% Analysis Date = 07/17/13 Pct Recovery = 50% Analysis Date = 07/06/13 Pct Recovery = 50% Analysis Date = 07/06/13 Pct Recovery = 50% Analysis Date = 06/25/13 Pct Recovery = 51% Analysis Date = 06/25/13 Pct Recovery = 51% Analysis Date = 06/15/13 Pct Recovery = 52% Analysis Date = 06/15/13 Pct Recovery = 52% Analysis Date = 06/04/13 Pct Recovery = 52% Analysis Date = 06/04/13 Pct Recovery = 52% Analysis Date = 05/24/13 Pct Recovery = 53% Analysis Date = 05/24/13 Pct Recovery = 53% Analysis Date = 05/13/13 Pct Recovery = 53% Analysis Date = 05/13/13 Pct Recovery = 53% Analysis Date = 05/02/13 Pct Recovery = 54% Analysis Date = 05/02/13 Pct Recovery = 54% Analysis Date = 04/21/13 Pct Recovery = 55% Analysis Date = 04/21/13 Pct Recovery = 55% Analysis Date = 04/11/13 Pct Recovery = 55% Analysis Date = 04/11/13 Pct Recovery = 55% Analysis Date = 03/31/13 Pct Recovery = 56% Analysis Date = 03/31/13 Pct Recovery = 56% Analysis Date = 03/20/13 Pct Recovery = 56% Analysis Date = 03/20/13 Pct Recovery = 56% Analysis Date = 03/09/13 Pct Recovery = 57% Analysis Date = 03/09/13 Pct Recovery = 57% Analysis Date = 02/26/13 Pct Recovery = 58% Analysis Date = 02/26/13 Pct Recovery = 58% Analysis Date = 02/15/13 Pct Recovery = 59% Analysis Date = 02/15/13 Pct Recovery = 59% Analysis Date = 02/04/13 Pct Recovery = 60% Analysis Date = 02/04/13 Pct Recovery = 60% Analysis Date = 01/25/13 Pct Recovery = 61% Analysis Date = 01/25/13 Pct Recovery = 61% Analysis Date = 01/14/13 Pct Recovery = 62% Analysis Date = 01/14/13 Pct Recovery = 62% Analysis Date = 01/03/13 Pct Recovery = 63% Analysis Date = 01/03/13 Pct Recovery = 63% Analysis Date = 12/23/12 Pct Recovery = 64% Analysis Date = 12/23/12 Pct Recovery = 64% Analysis Date = 12/12/12 Pct Recovery = 65% Analysis Date = 12/12/12 Pct Recovery = 65% Analysis Date = 12/01/12 Pct Recovery = 66% Analysis Date = 12/01/12 Pct Recovery = 66% Analysis Date = 11/20/12 Pct Recovery = 67% Analysis Date = 11/20/12 Pct Recovery = 67% Analysis Date = 11/10/12 Pct Recovery = 68% Analysis Date = 11/10/12 Pct Recovery = 68% Analysis Date = 10/30/12 Pct Recovery = 69% Analysis Date = 10/30/12 Pct Recovery = 69% Analysis Date = 10/19/12 Pct Recovery = 70% Analysis Date = 10/19/12 Pct Recovery = 70% Analysis Date = 10/08/12 Pct Recovery = 71% Analysis Date = 10/08/12 Pct Recovery = 71% Analysis Date = 09/27/12 Pct Recovery = 72% Analysis Date = 09/27/12 Pct Recovery = 72% Analysis Date = 09/16/12 Pct Recovery = 73% Analysis Date = 09/16/12 Pct Recovery = 73% Analysis Date = 09/06/12 Pct Recovery = 74% Analysis Date = 09/06/12 Pct Recovery = 74% Analysis Date = 08/26/12 Pct Recovery = 75% Analysis Date = 08/26/12 Pct Recovery = 75% Analysis Date = 08/15/12 Pct Recovery = 76% Analysis Date = 08/15/12 Pct Recovery = 76% Analysis Date = 08/04/12 Pct Recovery = 77% Analysis Date = 08/04/12 Pct Recovery = 77% Analysis Date = 07/24/12 Pct Recovery = 78% Analysis Date = 07/24/12 Pct Recovery = 78% Analysis Date = 07/13/12 Pct Recovery = 79% Analysis Date = 07/13/12 Pct Recovery = 79% Analysis Date = 07/02/12 Pct Recovery = 80% Analysis Date = 07/02/12 Pct Recovery = 80% Analysis Date = 06/22/12 Pct Recovery = 81% Analysis Date = 06/22/12 Pct Recovery = 81% Analysis Date = 06/11/12 Pct Recovery = 82% Analysis Date = 06/11/12 Pct Recovery = 82% Analysis Date = 05/31/12 Pct Recovery = 83% Analysis Date = 05/31/12 Pct Recovery = 83% Analysis Date = 05/20/12 Pct Recovery = 84% Analysis Date = 05/20/12 Pct Recovery = 84% Analysis Date = 05/09/12 Pct Recovery = 85% Analysis Date = 05/09/12 Pct Recovery = 85% Analysis Date = 04/28/12 Pct Recovery = 86% Analysis Date = 04/28/12 Pct Recovery = 86% Analysis Date = 04/17/12 Pct Recovery = 87% Analysis Date = 04/17/12 Pct Recovery = 87% Analysis Date = 04/07/12 Pct Recovery = 88% Analysis Date = 04/07/12 Pct Recovery = 88% Analysis Date = 03/27/12 Pct Recovery = 89% Analysis Date = 03/27/12 Pct Recovery = 89% Analysis Date = 03/16/12 Pct Recovery = 90% Analysis Date = 03/16/12 Pct Recovery = 90% Analysis Date = 03/05/12 Pct Recovery = 91% Analysis Date = 03/05/12 Pct Recovery = 91% Analysis Date = 02/23/12 Pct Recovery = 92% Analysis Date = 02/23/12 Pct Recovery = 92% Analysis Date = 02/12/12 Pct Recovery = 93% Analysis Date = 02/12/12 Pct Recovery = 93% Analysis Date = 02/02/12 Pct Recovery = 94% Analysis Date = 02/02/12 Pct Recovery = 94% Analysis Date = 01/22/12 Pct Recovery = 95% Analysis Date = 01/22/12 Pct Recovery = 95% Analysis Date = 01/11/12 Pct Recovery = 96% Analysis Date = 01/11/12 Pct Recovery = 96% Analysis Date = 12/31/11 Pct Recovery = 97% Analysis Date = 12/31/11 Pct Recovery = 97% Analysis Date = 12/20/11 Pct Recovery = 98% Analysis Date = 12/20/11 Pct Recovery = 98% Analysis Date = 12/09/11 Pct Recovery = 99% Analysis Date = 12/09/11 Pct Recovery = 99% Analysis Date = 11/28/11 Pct Recovery = 100% Analysis Date = 11/28/11 Pct Recovery = 100% Analysis Date = 11/18/11 Pct Recovery = 101% Analysis Date = 11/18/11 Pct Recovery = 101% Analysis Date = 11/07/11 Pct Recovery = 102% Analysis Date = 11/07/11 Pct Recovery = 102% Analysis Date = 10/27/11 Pct Recovery = 103% Analysis Date = 10/27/11 Pct Recovery = 103% Analysis Date = 10/16/11 Pct Recovery = 104% Analysis Date = 10/16/11 Pct Recovery = 104% Analysis Date = 10/05/11 Pct Recovery = 105% Analysis Date = 10/05/11 Pct Recovery = 105% Analysis Date = 09/24/11 Pct Recovery = 106% Analysis Date = 09/24/11 Pct Recovery = 106% Analysis Date = 09/13/11 Pct Recovery = 107% Analysis Date = 09/13/11 Pct Recovery = 107% Analysis Date = 09/03/11 Pct Recovery = 108% Analysis Date = 09/03/11 Pct Recovery = 108% Analysis Date = 08/23/11 Pct Recovery = 109% Analysis Date = 08/23/11 Pct Recovery = 109% Analysis Date = 08/12/11 Pct Recovery = 110% Analysis Date = 08/12/11 Pct Recovery = 110% Analysis Date = 08/01/11 Pct Recovery = 111% Analysis Date = 08/01/11 Pct Recovery = 111% Analysis Date = 07/21/11 Pct Recovery = 112% Analysis Date = 07/21/11 Pct Recovery = 112% Analysis Date = 07/10/11 Pct Recovery = 113% Analysis Date = 07/10/11 Pct Recovery = 113% Analysis Date = 06/30/11 Pct Recovery = 114% Analysis Date = 06/30/11 Pct Recovery = 114% Analysis Date = 06/19/11 Pct Recovery = 115% Analysis Date = 06/19/11 Pct Recovery = 115% Analysis Date = 06/08/11 Pct Recovery = 116% Analysis Date = 06/08/11 Pct Recovery = 116% Analysis Date = 05/28/11 Pct Recovery = 117% Analysis Date = 05/28/11 Pct Recovery = 117% Analysis Date = 05/17/11 Pct Recovery = 118% Analysis Date = 05/17/11 Pct Recovery = 118% Analysis Date = 05/06/11 Pct Recovery = 120% Analysis Date = 05/06/11 Pct Recovery = 120% Analysis Date = 04/25/11 Pct Recovery = 121% Analysis Date = 04/25/11 Pct Recovery = 121% Analysis Date = 04/15/11 Pct Recovery = 122% Analysis Date = 04/15/11 Pct Recovery = 122% Analysis Date = 04/04/11 Pct Recovery = 123% Analysis Date = 04/04/11 Pct Recovery = 123% Analysis Date = 03/24/11 Pct Recovery = 124% Analysis Date = 03/24/11 Pct Recovery = 124% Analysis Date = 03/13/11 Pct Recovery = 125% Analysis Date = 03/13/11 Pct Recovery = 125% Analysis Date = 03/02/11 Pct Recovery = 126% Analysis Date = 03/02/11 Pct Recovery = 126% Analysis Date = 02/19/11 Pct Recovery = 127% Analysis Date = 02/19/11 Pct Recovery = 127% Analysis Date = 02/09/11 Pct Recovery = 128% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1-NAPHTHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 8 49% 16% 48% 17%
>= Reporting Level 87 62% 39% 50% 30%
Total 95 61% 38% 50% 29%

Sample Statistics
1-NAPHTHOL

Characteristic N % % Basis
Plotted 95 100% Spiked
Estimated Values 95 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 95 .  
False Negatives 0 0% 0 out of 95
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

BQS OBSP Determination:
2,6-DIETHYLANILINE
METHOD: 2033 , TESTIDCODE: 82660GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 79% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 69% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 93% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 122% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 122% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 108% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 82% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 99% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 114% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 92% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 87% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 82% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 88% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 105% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 141% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 97% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 29% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 90% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 91% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 103% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 97% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 97% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 107% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 87% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 106% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 77% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 105% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 88% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 92% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 103% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 91% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 87% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 107% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 86% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 59% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 57% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 60% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 56% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 93% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 107% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 140% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 141% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 84% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 98% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 92% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 89% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 62% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 96% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 113% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 96% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 90% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 100% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 94% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 86% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 114% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 103% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 78% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 80% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 90% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 90% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 57% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 73% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 44% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 54% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 94% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 103% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 84% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 95% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 112% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 100% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 93% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 116% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 117% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 98% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 89% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 108% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 113% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 119% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 94% Analysis Date = 01/18/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 12/27/16 Pct Recovery = 88% Analysis Date = 12/27/16 Pct Recovery = 88% Analysis Date = 12/16/16 Pct Recovery = 88% Analysis Date = 12/16/16 Pct Recovery = 88% Analysis Date = 12/05/16 Pct Recovery = 88% Analysis Date = 12/05/16 Pct Recovery = 88% Analysis Date = 11/24/16 Pct Recovery = 88% Analysis Date = 11/24/16 Pct Recovery = 88% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/10/16 Pct Recovery = 87% Analysis Date = 09/10/16 Pct Recovery = 87% Analysis Date = 08/30/16 Pct Recovery = 87% Analysis Date = 08/30/16 Pct Recovery = 87% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 85% Analysis Date = 06/15/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/03/16 Pct Recovery = 85% Analysis Date = 05/03/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/11/16 Pct Recovery = 85% Analysis Date = 04/11/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 83% Analysis Date = 01/26/16 Pct Recovery = 83% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 82% Analysis Date = 10/21/15 Pct Recovery = 82% Analysis Date = 10/10/15 Pct Recovery = 82% Analysis Date = 10/10/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/29/15 Pct Recovery = 82% Analysis Date = 09/18/15 Pct Recovery = 82% Analysis Date = 09/18/15 Pct Recovery = 82% Analysis Date = 09/08/15 Pct Recovery = 82% Analysis Date = 09/08/15 Pct Recovery = 82% Analysis Date = 08/28/15 Pct Recovery = 82% Analysis Date = 08/28/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/17/15 Pct Recovery = 82% Analysis Date = 08/06/15 Pct Recovery = 82% Analysis Date = 08/06/15 Pct Recovery = 82% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/15/15 Pct Recovery = 81% Analysis Date = 07/15/15 Pct Recovery = 81% Analysis Date = 07/05/15 Pct Recovery = 81% Analysis Date = 07/05/15 Pct Recovery = 81% Analysis Date = 06/24/15 Pct Recovery = 81% Analysis Date = 06/24/15 Pct Recovery = 81% Analysis Date = 06/13/15 Pct Recovery = 81% Analysis Date = 06/13/15 Pct Recovery = 81% Analysis Date = 06/02/15 Pct Recovery = 81% Analysis Date = 06/02/15 Pct Recovery = 81% Analysis Date = 05/22/15 Pct Recovery = 81% Analysis Date = 05/22/15 Pct Recovery = 81% Analysis Date = 05/11/15 Pct Recovery = 81% Analysis Date = 05/11/15 Pct Recovery = 81% Analysis Date = 05/01/15 Pct Recovery = 81% Analysis Date = 05/01/15 Pct Recovery = 81% Analysis Date = 04/20/15 Pct Recovery = 81% Analysis Date = 04/20/15 Pct Recovery = 81% Analysis Date = 04/09/15 Pct Recovery = 81% Analysis Date = 04/09/15 Pct Recovery = 81% Analysis Date = 03/29/15 Pct Recovery = 81% Analysis Date = 03/29/15 Pct Recovery = 81% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/08/15 Pct Recovery = 80% Analysis Date = 03/08/15 Pct Recovery = 80% Analysis Date = 02/25/15 Pct Recovery = 80% Analysis Date = 02/25/15 Pct Recovery = 80% Analysis Date = 02/14/15 Pct Recovery = 80% Analysis Date = 02/14/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/12/15 Pct Recovery = 81% Analysis Date = 01/12/15 Pct Recovery = 81% Analysis Date = 01/02/15 Pct Recovery = 81% Analysis Date = 01/02/15 Pct Recovery = 81% Analysis Date = 12/22/14 Pct Recovery = 81% Analysis Date = 12/22/14 Pct Recovery = 81% Analysis Date = 12/11/14 Pct Recovery = 81% Analysis Date = 12/11/14 Pct Recovery = 81% Analysis Date = 11/30/14 Pct Recovery = 82% Analysis Date = 11/30/14 Pct Recovery = 82% Analysis Date = 11/19/14 Pct Recovery = 82% Analysis Date = 11/19/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 10/29/14 Pct Recovery = 83% Analysis Date = 10/29/14 Pct Recovery = 83% Analysis Date = 10/18/14 Pct Recovery = 83% Analysis Date = 10/18/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 84% Analysis Date = 09/26/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 84% Analysis Date = 08/25/14 Pct Recovery = 84% Analysis Date = 08/25/14 Pct Recovery = 84% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/03/14 Pct Recovery = 85% Analysis Date = 08/03/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 87% Analysis Date = 07/02/14 Pct Recovery = 87% Analysis Date = 06/21/14 Pct Recovery = 87% Analysis Date = 06/21/14 Pct Recovery = 87% Analysis Date = 06/10/14 Pct Recovery = 87% Analysis Date = 06/10/14 Pct Recovery = 87% Analysis Date = 05/30/14 Pct Recovery = 88% Analysis Date = 05/30/14 Pct Recovery = 88% Analysis Date = 05/19/14 Pct Recovery = 88% Analysis Date = 05/19/14 Pct Recovery = 88% Analysis Date = 05/08/14 Pct Recovery = 89% Analysis Date = 05/08/14 Pct Recovery = 89% Analysis Date = 04/28/14 Pct Recovery = 89% Analysis Date = 04/28/14 Pct Recovery = 89% Analysis Date = 04/17/14 Pct Recovery = 89% Analysis Date = 04/17/14 Pct Recovery = 89% Analysis Date = 04/06/14 Pct Recovery = 90% Analysis Date = 04/06/14 Pct Recovery = 90% Analysis Date = 03/26/14 Pct Recovery = 90% Analysis Date = 03/26/14 Pct Recovery = 90% Analysis Date = 03/15/14 Pct Recovery = 90% Analysis Date = 03/15/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 91% Analysis Date = 03/04/14 Pct Recovery = 91% Analysis Date = 02/22/14 Pct Recovery = 91% Analysis Date = 02/22/14 Pct Recovery = 91% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 01/31/14 Pct Recovery = 92% Analysis Date = 01/31/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/09/14 Pct Recovery = 93% Analysis Date = 01/09/14 Pct Recovery = 93% Analysis Date = 12/30/13 Pct Recovery = 93% Analysis Date = 12/30/13 Pct Recovery = 93% Analysis Date = 12/19/13 Pct Recovery = 93% Analysis Date = 12/19/13 Pct Recovery = 93% Analysis Date = 12/08/13 Pct Recovery = 94% Analysis Date = 12/08/13 Pct Recovery = 94% Analysis Date = 11/27/13 Pct Recovery = 94% Analysis Date = 11/27/13 Pct Recovery = 94% Analysis Date = 11/16/13 Pct Recovery = 94% Analysis Date = 11/16/13 Pct Recovery = 94% Analysis Date = 11/05/13 Pct Recovery = 95% Analysis Date = 11/05/13 Pct Recovery = 95% Analysis Date = 10/26/13 Pct Recovery = 95% Analysis Date = 10/26/13 Pct Recovery = 95% Analysis Date = 10/15/13 Pct Recovery = 95% Analysis Date = 10/15/13 Pct Recovery = 95% Analysis Date = 10/04/13 Pct Recovery = 95% Analysis Date = 10/04/13 Pct Recovery = 95% Analysis Date = 09/23/13 Pct Recovery = 95% Analysis Date = 09/23/13 Pct Recovery = 95% Analysis Date = 09/12/13 Pct Recovery = 95% Analysis Date = 09/12/13 Pct Recovery = 95% Analysis Date = 09/01/13 Pct Recovery = 95% Analysis Date = 09/01/13 Pct Recovery = 95% Analysis Date = 08/22/13 Pct Recovery = 96% Analysis Date = 08/22/13 Pct Recovery = 96% Analysis Date = 08/11/13 Pct Recovery = 96% Analysis Date = 08/11/13 Pct Recovery = 96% Analysis Date = 07/31/13 Pct Recovery = 96% Analysis Date = 07/31/13 Pct Recovery = 96% Analysis Date = 07/20/13 Pct Recovery = 96% Analysis Date = 07/20/13 Pct Recovery = 96% Analysis Date = 07/09/13 Pct Recovery = 96% Analysis Date = 07/09/13 Pct Recovery = 96% Analysis Date = 06/29/13 Pct Recovery = 96% Analysis Date = 06/29/13 Pct Recovery = 96% Analysis Date = 06/18/13 Pct Recovery = 96% Analysis Date = 06/18/13 Pct Recovery = 96% Analysis Date = 06/07/13 Pct Recovery = 97% Analysis Date = 06/07/13 Pct Recovery = 97% Analysis Date = 05/27/13 Pct Recovery = 97% Analysis Date = 05/27/13 Pct Recovery = 97% Analysis Date = 05/16/13 Pct Recovery = 97% Analysis Date = 05/16/13 Pct Recovery = 97% Analysis Date = 05/05/13 Pct Recovery = 97% Analysis Date = 05/05/13 Pct Recovery = 97% Analysis Date = 04/25/13 Pct Recovery = 97% Analysis Date = 04/25/13 Pct Recovery = 97% Analysis Date = 04/14/13 Pct Recovery = 97% Analysis Date = 04/14/13 Pct Recovery = 97% Analysis Date = 04/03/13 Pct Recovery = 97% Analysis Date = 04/03/13 Pct Recovery = 97% Analysis Date = 03/23/13 Pct Recovery = 98% Analysis Date = 03/23/13 Pct Recovery = 98% Analysis Date = 03/12/13 Pct Recovery = 98% Analysis Date = 03/12/13 Pct Recovery = 98% Analysis Date = 03/01/13 Pct Recovery = 97% Analysis Date = 03/01/13 Pct Recovery = 97% Analysis Date = 02/19/13 Pct Recovery = 97% Analysis Date = 02/19/13 Pct Recovery = 97% Analysis Date = 02/08/13 Pct Recovery = 97% Analysis Date = 02/08/13 Pct Recovery = 97% Analysis Date = 01/28/13 Pct Recovery = 97% Analysis Date = 01/28/13 Pct Recovery = 97% Analysis Date = 01/17/13 Pct Recovery = 97% Analysis Date = 01/17/13 Pct Recovery = 97% Analysis Date = 01/06/13 Pct Recovery = 97% Analysis Date = 01/06/13 Pct Recovery = 97% Analysis Date = 12/26/12 Pct Recovery = 97% Analysis Date = 12/26/12 Pct Recovery = 97% Analysis Date = 12/16/12 Pct Recovery = 97% Analysis Date = 12/16/12 Pct Recovery = 97% Analysis Date = 12/05/12 Pct Recovery = 97% Analysis Date = 12/05/12 Pct Recovery = 97% Analysis Date = 11/24/12 Pct Recovery = 97% Analysis Date = 11/24/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 97% Analysis Date = 11/02/12 Pct Recovery = 97% Analysis Date = 11/02/12 Pct Recovery = 97% Analysis Date = 10/23/12 Pct Recovery = 97% Analysis Date = 10/23/12 Pct Recovery = 97% Analysis Date = 10/12/12 Pct Recovery = 97% Analysis Date = 10/12/12 Pct Recovery = 97% Analysis Date = 10/01/12 Pct Recovery = 97% Analysis Date = 10/01/12 Pct Recovery = 97% Analysis Date = 09/20/12 Pct Recovery = 97% Analysis Date = 09/20/12 Pct Recovery = 97% Analysis Date = 09/09/12 Pct Recovery = 97% Analysis Date = 09/09/12 Pct Recovery = 97% Analysis Date = 08/29/12 Pct Recovery = 97% Analysis Date = 08/29/12 Pct Recovery = 97% Analysis Date = 08/19/12 Pct Recovery = 97% Analysis Date = 08/19/12 Pct Recovery = 97% Analysis Date = 08/08/12 Pct Recovery = 97% Analysis Date = 08/08/12 Pct Recovery = 97% Analysis Date = 07/28/12 Pct Recovery = 97% Analysis Date = 07/28/12 Pct Recovery = 97% Analysis Date = 07/17/12 Pct Recovery = 97% Analysis Date = 07/17/12 Pct Recovery = 97% Analysis Date = 07/06/12 Pct Recovery = 98% Analysis Date = 07/06/12 Pct Recovery = 98% Analysis Date = 06/25/12 Pct Recovery = 98% Analysis Date = 06/25/12 Pct Recovery = 98% Analysis Date = 06/15/12 Pct Recovery = 98% Analysis Date = 06/15/12 Pct Recovery = 98% Analysis Date = 06/04/12 Pct Recovery = 98% Analysis Date = 06/04/12 Pct Recovery = 98% Analysis Date = 05/24/12 Pct Recovery = 98% Analysis Date = 05/24/12 Pct Recovery = 98% Analysis Date = 05/13/12 Pct Recovery = 98% Analysis Date = 05/13/12 Pct Recovery = 98% Analysis Date = 05/02/12 Pct Recovery = 98% Analysis Date = 05/02/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 98% Analysis Date = 03/20/12 Pct Recovery = 98% Analysis Date = 03/20/12 Pct Recovery = 98% Analysis Date = 03/09/12 Pct Recovery = 99% Analysis Date = 03/09/12 Pct Recovery = 99% Analysis Date = 02/27/12 Pct Recovery = 99% Analysis Date = 02/27/12 Pct Recovery = 99% Analysis Date = 02/17/12 Pct Recovery = 99% Analysis Date = 02/17/12 Pct Recovery = 99% Analysis Date = 02/06/12 Pct Recovery = 99% Analysis Date = 02/06/12 Pct Recovery = 99% Analysis Date = 01/26/12 Pct Recovery = 99% Analysis Date = 01/26/12 Pct Recovery = 99% Analysis Date = 01/15/12 Pct Recovery = 99% Analysis Date = 01/15/12 Pct Recovery = 99% Analysis Date = 01/04/12 Pct Recovery = 99% Analysis Date = 01/04/12 Pct Recovery = 99% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/14/11 Pct Recovery = 100% Analysis Date = 12/14/11 Pct Recovery = 100% Analysis Date = 12/03/11 Pct Recovery = 100% Analysis Date = 12/03/11 Pct Recovery = 100% Analysis Date = 11/22/11 Pct Recovery = 100% Analysis Date = 11/22/11 Pct Recovery = 100% Analysis Date = 11/11/11 Pct Recovery = 100% Analysis Date = 11/11/11 Pct Recovery = 100% Analysis Date = 10/31/11 Pct Recovery = 100% Analysis Date = 10/31/11 Pct Recovery = 100% Analysis Date = 10/20/11 Pct Recovery = 101% Analysis Date = 10/20/11 Pct Recovery = 101% Analysis Date = 10/10/11 Pct Recovery = 101% Analysis Date = 10/10/11 Pct Recovery = 101% Analysis Date = 09/29/11 Pct Recovery = 101% Analysis Date = 09/29/11 Pct Recovery = 101% Analysis Date = 09/18/11 Pct Recovery = 101% Analysis Date = 09/18/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 08/27/11 Pct Recovery = 101% Analysis Date = 08/27/11 Pct Recovery = 101% Analysis Date = 08/17/11 Pct Recovery = 102% Analysis Date = 08/17/11 Pct Recovery = 102% Analysis Date = 08/06/11 Pct Recovery = 102% Analysis Date = 08/06/11 Pct Recovery = 102% Analysis Date = 07/26/11 Pct Recovery = 102% Analysis Date = 07/26/11 Pct Recovery = 102% Analysis Date = 07/15/11 Pct Recovery = 102% Analysis Date = 07/15/11 Pct Recovery = 102% Analysis Date = 07/04/11 Pct Recovery = 102% Analysis Date = 07/04/11 Pct Recovery = 102% Analysis Date = 06/23/11 Pct Recovery = 102% Analysis Date = 06/23/11 Pct Recovery = 102% Analysis Date = 06/13/11 Pct Recovery = 103% Analysis Date = 06/13/11 Pct Recovery = 103% Analysis Date = 06/02/11 Pct Recovery = 103% Analysis Date = 06/02/11 Pct Recovery = 103% Analysis Date = 05/22/11 Pct Recovery = 103% Analysis Date = 05/22/11 Pct Recovery = 103% Analysis Date = 05/11/11 Pct Recovery = 103% Analysis Date = 05/11/11 Pct Recovery = 103% Analysis Date = 04/30/11 Pct Recovery = 103% Analysis Date = 04/30/11 Pct Recovery = 103% Analysis Date = 04/19/11 Pct Recovery = 104% Analysis Date = 04/19/11 Pct Recovery = 104% Analysis Date = 04/09/11 Pct Recovery = 104% Analysis Date = 04/09/11 Pct Recovery = 104% Analysis Date = 03/29/11 Pct Recovery = 104% Analysis Date = 03/29/11 Pct Recovery = 104% Analysis Date = 03/18/11 Pct Recovery = 104% Analysis Date = 03/18/11 Pct Recovery = 104% Analysis Date = 03/07/11 Pct Recovery = 104% Analysis Date = 03/07/11 Pct Recovery = 104% Analysis Date = 02/24/11 Pct Recovery = 105% Analysis Date = 02/24/11 Pct Recovery = 105% Analysis Date = 02/14/11 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,6-DIETHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 92% 19% 93% 14%
Total 94 92% 19% 93% 14%

Sample Statistics
2,6-DIETHYLANILINE

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
2-CHLORO-2,6-DIETHYLACETANILIDE
METHOD: 2033 , TESTIDCODE: 61618GCM39
Open Data Set

Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 79% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 103% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 84% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 88% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 105% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 105% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 92% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 107% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 113% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 122% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 90% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 102% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 90% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 95% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 104% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 101% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 97% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 132% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 96% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 93% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 107% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 86% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 98% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 117% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 84% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 116% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 84% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 70% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 85% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 90% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 109% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 105% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 100% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 96% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 109% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 102% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 100% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 119% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 127% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 77% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 116% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 109% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 126% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 115% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 111% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 117% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 109% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 122% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 105% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 112% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 81% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 95% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 88% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 91% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 113% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 86% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 102% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 121% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/09/16 Pct Recovery = 86% Analysis Date = 12/09/16 Pct Recovery = 86% Analysis Date = 11/28/16 Pct Recovery = 86% Analysis Date = 11/28/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/07/16 Pct Recovery = 87% Analysis Date = 11/07/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/16/16 Pct Recovery = 87% Analysis Date = 10/16/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/03/16 Pct Recovery = 88% Analysis Date = 09/03/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 07/23/16 Pct Recovery = 88% Analysis Date = 07/23/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/01/16 Pct Recovery = 89% Analysis Date = 07/01/16 Pct Recovery = 89% Analysis Date = 06/20/16 Pct Recovery = 89% Analysis Date = 06/20/16 Pct Recovery = 89% Analysis Date = 06/10/16 Pct Recovery = 89% Analysis Date = 06/10/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/19/16 Pct Recovery = 89% Analysis Date = 05/19/16 Pct Recovery = 89% Analysis Date = 05/09/16 Pct Recovery = 89% Analysis Date = 05/09/16 Pct Recovery = 89% Analysis Date = 04/28/16 Pct Recovery = 90% Analysis Date = 04/28/16 Pct Recovery = 90% Analysis Date = 04/17/16 Pct Recovery = 90% Analysis Date = 04/17/16 Pct Recovery = 90% Analysis Date = 04/06/16 Pct Recovery = 90% Analysis Date = 04/06/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 90% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 91% Analysis Date = 02/02/16 Pct Recovery = 91% Analysis Date = 02/02/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 91% Analysis Date = 01/12/16 Pct Recovery = 91% Analysis Date = 01/12/16 Pct Recovery = 91% Analysis Date = 01/01/16 Pct Recovery = 91% Analysis Date = 01/01/16 Pct Recovery = 91% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/21/15 Pct Recovery = 92% Analysis Date = 12/11/15 Pct Recovery = 92% Analysis Date = 12/11/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/30/15 Pct Recovery = 92% Analysis Date = 11/19/15 Pct Recovery = 92% Analysis Date = 11/19/15 Pct Recovery = 92% Analysis Date = 11/09/15 Pct Recovery = 92% Analysis Date = 11/09/15 Pct Recovery = 92% Analysis Date = 10/29/15 Pct Recovery = 92% Analysis Date = 10/29/15 Pct Recovery = 92% Analysis Date = 10/18/15 Pct Recovery = 93% Analysis Date = 10/18/15 Pct Recovery = 93% Analysis Date = 10/07/15 Pct Recovery = 93% Analysis Date = 10/07/15 Pct Recovery = 93% Analysis Date = 09/27/15 Pct Recovery = 93% Analysis Date = 09/27/15 Pct Recovery = 93% Analysis Date = 09/16/15 Pct Recovery = 93% Analysis Date = 09/16/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 09/05/15 Pct Recovery = 93% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/26/15 Pct Recovery = 94% Analysis Date = 08/15/15 Pct Recovery = 94% Analysis Date = 08/15/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 08/04/15 Pct Recovery = 94% Analysis Date = 07/24/15 Pct Recovery = 94% Analysis Date = 07/24/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/03/15 Pct Recovery = 94% Analysis Date = 07/03/15 Pct Recovery = 94% Analysis Date = 06/22/15 Pct Recovery = 95% Analysis Date = 06/22/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/01/15 Pct Recovery = 95% Analysis Date = 06/01/15 Pct Recovery = 95% Analysis Date = 05/21/15 Pct Recovery = 95% Analysis Date = 05/21/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 05/10/15 Pct Recovery = 95% Analysis Date = 04/30/15 Pct Recovery = 96% Analysis Date = 04/30/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/08/15 Pct Recovery = 96% Analysis Date = 04/08/15 Pct Recovery = 96% Analysis Date = 03/29/15 Pct Recovery = 96% Analysis Date = 03/29/15 Pct Recovery = 96% Analysis Date = 03/18/15 Pct Recovery = 96% Analysis Date = 03/18/15 Pct Recovery = 96% Analysis Date = 03/07/15 Pct Recovery = 96% Analysis Date = 03/07/15 Pct Recovery = 96% Analysis Date = 02/24/15 Pct Recovery = 97% Analysis Date = 02/24/15 Pct Recovery = 97% Analysis Date = 02/14/15 Pct Recovery = 97% Analysis Date = 02/14/15 Pct Recovery = 97% Analysis Date = 02/03/15 Pct Recovery = 97% Analysis Date = 02/03/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/23/15 Pct Recovery = 97% Analysis Date = 01/13/15 Pct Recovery = 98% Analysis Date = 01/13/15 Pct Recovery = 98% Analysis Date = 01/02/15 Pct Recovery = 98% Analysis Date = 01/02/15 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/22/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/12/14 Pct Recovery = 98% Analysis Date = 12/01/14 Pct Recovery = 99% Analysis Date = 12/01/14 Pct Recovery = 99% Analysis Date = 11/20/14 Pct Recovery = 99% Analysis Date = 11/20/14 Pct Recovery = 99% Analysis Date = 11/09/14 Pct Recovery = 99% Analysis Date = 11/09/14 Pct Recovery = 99% Analysis Date = 10/30/14 Pct Recovery = 99% Analysis Date = 10/30/14 Pct Recovery = 99% Analysis Date = 10/19/14 Pct Recovery = 100% Analysis Date = 10/19/14 Pct Recovery = 100% Analysis Date = 10/08/14 Pct Recovery = 100% Analysis Date = 10/08/14 Pct Recovery = 100% Analysis Date = 09/28/14 Pct Recovery = 100% Analysis Date = 09/28/14 Pct Recovery = 100% Analysis Date = 09/17/14 Pct Recovery = 100% Analysis Date = 09/17/14 Pct Recovery = 100% Analysis Date = 09/06/14 Pct Recovery = 101% Analysis Date = 09/06/14 Pct Recovery = 101% Analysis Date = 08/26/14 Pct Recovery = 101% Analysis Date = 08/26/14 Pct Recovery = 101% Analysis Date = 08/16/14 Pct Recovery = 101% Analysis Date = 08/16/14 Pct Recovery = 101% Analysis Date = 08/05/14 Pct Recovery = 101% Analysis Date = 08/05/14 Pct Recovery = 101% Analysis Date = 07/25/14 Pct Recovery = 102% Analysis Date = 07/25/14 Pct Recovery = 102% Analysis Date = 07/15/14 Pct Recovery = 102% Analysis Date = 07/15/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 06/23/14 Pct Recovery = 102% Analysis Date = 06/23/14 Pct Recovery = 102% Analysis Date = 06/12/14 Pct Recovery = 102% Analysis Date = 06/12/14 Pct Recovery = 102% Analysis Date = 06/02/14 Pct Recovery = 102% Analysis Date = 06/02/14 Pct Recovery = 102% Analysis Date = 05/22/14 Pct Recovery = 102% Analysis Date = 05/22/14 Pct Recovery = 102% Analysis Date = 05/11/14 Pct Recovery = 102% Analysis Date = 05/11/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Analysis Date = 04/20/14 Pct Recovery = 102% Analysis Date = 04/20/14 Pct Recovery = 102% Analysis Date = 04/09/14 Pct Recovery = 102% Analysis Date = 04/09/14 Pct Recovery = 102% Analysis Date = 03/29/14 Pct Recovery = 102% Analysis Date = 03/29/14 Pct Recovery = 102% Analysis Date = 03/19/14 Pct Recovery = 102% Analysis Date = 03/19/14 Pct Recovery = 102% Analysis Date = 03/08/14 Pct Recovery = 102% Analysis Date = 03/08/14 Pct Recovery = 102% Analysis Date = 02/25/14 Pct Recovery = 102% Analysis Date = 02/25/14 Pct Recovery = 102% Analysis Date = 02/15/14 Pct Recovery = 102% Analysis Date = 02/15/14 Pct Recovery = 102% Analysis Date = 02/04/14 Pct Recovery = 102% Analysis Date = 02/04/14 Pct Recovery = 102% Analysis Date = 01/24/14 Pct Recovery = 102% Analysis Date = 01/24/14 Pct Recovery = 102% Analysis Date = 01/13/14 Pct Recovery = 102% Analysis Date = 01/13/14 Pct Recovery = 102% Analysis Date = 01/03/14 Pct Recovery = 102% Analysis Date = 01/03/14 Pct Recovery = 102% Analysis Date = 12/23/13 Pct Recovery = 102% Analysis Date = 12/23/13 Pct Recovery = 102% Analysis Date = 12/12/13 Pct Recovery = 102% Analysis Date = 12/12/13 Pct Recovery = 102% Analysis Date = 12/02/13 Pct Recovery = 102% Analysis Date = 12/02/13 Pct Recovery = 102% Analysis Date = 11/21/13 Pct Recovery = 102% Analysis Date = 11/21/13 Pct Recovery = 102% Analysis Date = 11/10/13 Pct Recovery = 102% Analysis Date = 11/10/13 Pct Recovery = 102% Analysis Date = 10/31/13 Pct Recovery = 102% Analysis Date = 10/31/13 Pct Recovery = 102% Analysis Date = 10/20/13 Pct Recovery = 102% Analysis Date = 10/20/13 Pct Recovery = 102% Analysis Date = 10/09/13 Pct Recovery = 102% Analysis Date = 10/09/13 Pct Recovery = 102% Analysis Date = 09/28/13 Pct Recovery = 102% Analysis Date = 09/28/13 Pct Recovery = 102% Analysis Date = 09/18/13 Pct Recovery = 102% Analysis Date = 09/18/13 Pct Recovery = 102% Analysis Date = 09/07/13 Pct Recovery = 102% Analysis Date = 09/07/13 Pct Recovery = 102% Analysis Date = 08/27/13 Pct Recovery = 102% Analysis Date = 08/27/13 Pct Recovery = 102% Analysis Date = 08/17/13 Pct Recovery = 102% Analysis Date = 08/17/13 Pct Recovery = 102% Analysis Date = 08/06/13 Pct Recovery = 102% Analysis Date = 08/06/13 Pct Recovery = 102% Analysis Date = 07/26/13 Pct Recovery = 102% Analysis Date = 07/26/13 Pct Recovery = 102% Analysis Date = 07/15/13 Pct Recovery = 102% Analysis Date = 07/15/13 Pct Recovery = 102% Analysis Date = 07/05/13 Pct Recovery = 102% Analysis Date = 07/05/13 Pct Recovery = 102% Analysis Date = 06/24/13 Pct Recovery = 102% Analysis Date = 06/24/13 Pct Recovery = 102% Analysis Date = 06/13/13 Pct Recovery = 102% Analysis Date = 06/13/13 Pct Recovery = 102% Analysis Date = 06/03/13 Pct Recovery = 102% Analysis Date = 06/03/13 Pct Recovery = 102% Analysis Date = 05/23/13 Pct Recovery = 102% Analysis Date = 05/23/13 Pct Recovery = 102% Analysis Date = 05/12/13 Pct Recovery = 102% Analysis Date = 05/12/13 Pct Recovery = 102% Analysis Date = 05/01/13 Pct Recovery = 102% Analysis Date = 05/01/13 Pct Recovery = 102% Analysis Date = 04/21/13 Pct Recovery = 102% Analysis Date = 04/21/13 Pct Recovery = 102% Analysis Date = 04/10/13 Pct Recovery = 102% Analysis Date = 04/10/13 Pct Recovery = 102% Analysis Date = 03/30/13 Pct Recovery = 102% Analysis Date = 03/30/13 Pct Recovery = 102% Analysis Date = 03/20/13 Pct Recovery = 102% Analysis Date = 03/20/13 Pct Recovery = 102% Analysis Date = 03/09/13 Pct Recovery = 102% Analysis Date = 03/09/13 Pct Recovery = 102% Analysis Date = 02/26/13 Pct Recovery = 102% Analysis Date = 02/26/13 Pct Recovery = 102% Analysis Date = 02/15/13 Pct Recovery = 102% Analysis Date = 02/15/13 Pct Recovery = 102% Analysis Date = 02/05/13 Pct Recovery = 102% Analysis Date = 02/05/13 Pct Recovery = 102% Analysis Date = 01/25/13 Pct Recovery = 103% Analysis Date = 01/25/13 Pct Recovery = 103% Analysis Date = 01/14/13 Pct Recovery = 103% Analysis Date = 01/14/13 Pct Recovery = 103% Analysis Date = 01/04/13 Pct Recovery = 103% Analysis Date = 01/04/13 Pct Recovery = 103% Analysis Date = 12/24/12 Pct Recovery = 103% Analysis Date = 12/24/12 Pct Recovery = 103% Analysis Date = 12/13/12 Pct Recovery = 103% Analysis Date = 12/13/12 Pct Recovery = 103% Analysis Date = 12/03/12 Pct Recovery = 103% Analysis Date = 12/03/12 Pct Recovery = 103% Analysis Date = 11/22/12 Pct Recovery = 103% Analysis Date = 11/22/12 Pct Recovery = 103% Analysis Date = 11/11/12 Pct Recovery = 103% Analysis Date = 11/11/12 Pct Recovery = 103% Analysis Date = 10/31/12 Pct Recovery = 103% Analysis Date = 10/31/12 Pct Recovery = 103% Analysis Date = 10/21/12 Pct Recovery = 103% Analysis Date = 10/21/12 Pct Recovery = 103% Analysis Date = 10/10/12 Pct Recovery = 103% Analysis Date = 10/10/12 Pct Recovery = 103% Analysis Date = 09/29/12 Pct Recovery = 103% Analysis Date = 09/29/12 Pct Recovery = 103% Analysis Date = 09/19/12 Pct Recovery = 103% Analysis Date = 09/19/12 Pct Recovery = 103% Analysis Date = 09/08/12 Pct Recovery = 102% Analysis Date = 09/08/12 Pct Recovery = 102% Analysis Date = 08/28/12 Pct Recovery = 102% Analysis Date = 08/28/12 Pct Recovery = 102% Analysis Date = 08/17/12 Pct Recovery = 102% Analysis Date = 08/17/12 Pct Recovery = 102% Analysis Date = 08/07/12 Pct Recovery = 102% Analysis Date = 08/07/12 Pct Recovery = 102% Analysis Date = 07/27/12 Pct Recovery = 102% Analysis Date = 07/27/12 Pct Recovery = 102% Analysis Date = 07/16/12 Pct Recovery = 102% Analysis Date = 07/16/12 Pct Recovery = 102% Analysis Date = 07/06/12 Pct Recovery = 102% Analysis Date = 07/06/12 Pct Recovery = 102% Analysis Date = 06/25/12 Pct Recovery = 102% Analysis Date = 06/25/12 Pct Recovery = 102% Analysis Date = 06/14/12 Pct Recovery = 102% Analysis Date = 06/14/12 Pct Recovery = 102% Analysis Date = 06/03/12 Pct Recovery = 101% Analysis Date = 06/03/12 Pct Recovery = 101% Analysis Date = 05/24/12 Pct Recovery = 101% Analysis Date = 05/24/12 Pct Recovery = 101% Analysis Date = 05/13/12 Pct Recovery = 101% Analysis Date = 05/13/12 Pct Recovery = 101% Analysis Date = 05/02/12 Pct Recovery = 101% Analysis Date = 05/02/12 Pct Recovery = 101% Analysis Date = 04/22/12 Pct Recovery = 101% Analysis Date = 04/22/12 Pct Recovery = 101% Analysis Date = 04/11/12 Pct Recovery = 101% Analysis Date = 04/11/12 Pct Recovery = 101% Analysis Date = 03/31/12 Pct Recovery = 101% Analysis Date = 03/31/12 Pct Recovery = 101% Analysis Date = 03/20/12 Pct Recovery = 101% Analysis Date = 03/20/12 Pct Recovery = 101% Analysis Date = 03/10/12 Pct Recovery = 101% Analysis Date = 03/10/12 Pct Recovery = 101% Analysis Date = 02/28/12 Pct Recovery = 101% Analysis Date = 02/28/12 Pct Recovery = 101% Analysis Date = 02/17/12 Pct Recovery = 101% Analysis Date = 02/17/12 Pct Recovery = 101% Analysis Date = 02/07/12 Pct Recovery = 101% Analysis Date = 02/07/12 Pct Recovery = 101% Analysis Date = 01/27/12 Pct Recovery = 100% Analysis Date = 01/27/12 Pct Recovery = 100% Analysis Date = 01/16/12 Pct Recovery = 100% Analysis Date = 01/16/12 Pct Recovery = 100% Analysis Date = 01/06/12 Pct Recovery = 100% Analysis Date = 01/06/12 Pct Recovery = 100% Analysis Date = 12/26/11 Pct Recovery = 100% Analysis Date = 12/26/11 Pct Recovery = 100% Analysis Date = 12/15/11 Pct Recovery = 100% Analysis Date = 12/15/11 Pct Recovery = 100% Analysis Date = 12/04/11 Pct Recovery = 100% Analysis Date = 12/04/11 Pct Recovery = 100% Analysis Date = 11/24/11 Pct Recovery = 100% Analysis Date = 11/24/11 Pct Recovery = 100% Analysis Date = 11/13/11 Pct Recovery = 100% Analysis Date = 11/13/11 Pct Recovery = 100% Analysis Date = 11/02/11 Pct Recovery = 100% Analysis Date = 11/02/11 Pct Recovery = 100% Analysis Date = 10/23/11 Pct Recovery = 100% Analysis Date = 10/23/11 Pct Recovery = 100% Analysis Date = 10/12/11 Pct Recovery = 100% Analysis Date = 10/12/11 Pct Recovery = 100% Analysis Date = 10/01/11 Pct Recovery = 100% Analysis Date = 10/01/11 Pct Recovery = 100% Analysis Date = 09/20/11 Pct Recovery = 100% Analysis Date = 09/20/11 Pct Recovery = 100% Analysis Date = 09/10/11 Pct Recovery = 99% Analysis Date = 09/10/11 Pct Recovery = 99% Analysis Date = 08/30/11 Pct Recovery = 99% Analysis Date = 08/30/11 Pct Recovery = 99% Analysis Date = 08/19/11 Pct Recovery = 99% Analysis Date = 08/19/11 Pct Recovery = 99% Analysis Date = 08/09/11 Pct Recovery = 99% Analysis Date = 08/09/11 Pct Recovery = 99% Analysis Date = 07/29/11 Pct Recovery = 99% Analysis Date = 07/29/11 Pct Recovery = 99% Analysis Date = 07/18/11 Pct Recovery = 99% Analysis Date = 07/18/11 Pct Recovery = 99% Analysis Date = 07/07/11 Pct Recovery = 99% Analysis Date = 07/07/11 Pct Recovery = 99% Analysis Date = 06/27/11 Pct Recovery = 99% Analysis Date = 06/27/11 Pct Recovery = 99% Analysis Date = 06/16/11 Pct Recovery = 99% Analysis Date = 06/16/11 Pct Recovery = 99% Analysis Date = 06/05/11 Pct Recovery = 99% Analysis Date = 06/05/11 Pct Recovery = 99% Analysis Date = 05/26/11 Pct Recovery = 99% Analysis Date = 05/26/11 Pct Recovery = 99% Analysis Date = 05/15/11 Pct Recovery = 99% Analysis Date = 05/15/11 Pct Recovery = 99% Analysis Date = 05/04/11 Pct Recovery = 98% Analysis Date = 05/04/11 Pct Recovery = 98% Analysis Date = 04/23/11 Pct Recovery = 98% Analysis Date = 04/23/11 Pct Recovery = 98% Analysis Date = 04/13/11 Pct Recovery = 98% Analysis Date = 04/13/11 Pct Recovery = 98% Analysis Date = 04/02/11 Pct Recovery = 98% Analysis Date = 04/02/11 Pct Recovery = 98% Analysis Date = 03/22/11 Pct Recovery = 98% Analysis Date = 03/22/11 Pct Recovery = 98% Analysis Date = 03/12/11 Pct Recovery = 98% Analysis Date = 03/12/11 Pct Recovery = 98% Analysis Date = 03/01/11 Pct Recovery = 98% Analysis Date = 03/01/11 Pct Recovery = 98% Analysis Date = 02/18/11 Pct Recovery = 98% Analysis Date = 02/18/11 Pct Recovery = 98% Analysis Date = 02/08/11 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 99% 15% 100% 17%
Total 67 99% 15% 100% 17%

Sample Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Characteristic N % % Basis
Plotted 67 99% Spiked
Estimated Values 2 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 68 .  
False Negatives 0 0% 0 out of 68
Not Spiked 101 .  
False Positives 1 1% 1 out of 101

BQS OBSP Determination:
2-ETHYL-6-METHYLANILINE
METHOD: 2033 , TESTIDCODE: 61620GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 74% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 93% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 108% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 109% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 100% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 99% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 77% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 92% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 119% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 88% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 85% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 74% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 85% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 92% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 89% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 91% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 91% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 83% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 96% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 104% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 92% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 87% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 119% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 72% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 82% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 81% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 80% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 102% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 55% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 82% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 124% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 116% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 84% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 89% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 97% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 83% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 106% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 68% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 95% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 102% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 92% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 103% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 101% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 104% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 112% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 92% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 105% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 92% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 103% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 101% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 94% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 73% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 97% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 94% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 30% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 01/17/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 12/27/16 Pct Recovery = 83% Analysis Date = 12/27/16 Pct Recovery = 83% Analysis Date = 12/16/16 Pct Recovery = 83% Analysis Date = 12/16/16 Pct Recovery = 83% Analysis Date = 12/05/16 Pct Recovery = 83% Analysis Date = 12/05/16 Pct Recovery = 83% Analysis Date = 11/24/16 Pct Recovery = 83% Analysis Date = 11/24/16 Pct Recovery = 83% Analysis Date = 11/14/16 Pct Recovery = 82% Analysis Date = 11/14/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 10/23/16 Pct Recovery = 82% Analysis Date = 10/23/16 Pct Recovery = 82% Analysis Date = 10/12/16 Pct Recovery = 82% Analysis Date = 10/12/16 Pct Recovery = 82% Analysis Date = 10/01/16 Pct Recovery = 82% Analysis Date = 10/01/16 Pct Recovery = 82% Analysis Date = 09/21/16 Pct Recovery = 82% Analysis Date = 09/21/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 08/30/16 Pct Recovery = 82% Analysis Date = 08/30/16 Pct Recovery = 82% Analysis Date = 08/19/16 Pct Recovery = 82% Analysis Date = 08/19/16 Pct Recovery = 82% Analysis Date = 08/08/16 Pct Recovery = 82% Analysis Date = 08/08/16 Pct Recovery = 82% Analysis Date = 07/29/16 Pct Recovery = 82% Analysis Date = 07/29/16 Pct Recovery = 82% Analysis Date = 07/18/16 Pct Recovery = 82% Analysis Date = 07/18/16 Pct Recovery = 82% Analysis Date = 07/07/16 Pct Recovery = 82% Analysis Date = 07/07/16 Pct Recovery = 82% Analysis Date = 06/26/16 Pct Recovery = 82% Analysis Date = 06/26/16 Pct Recovery = 82% Analysis Date = 06/15/16 Pct Recovery = 82% Analysis Date = 06/15/16 Pct Recovery = 82% Analysis Date = 06/05/16 Pct Recovery = 82% Analysis Date = 06/05/16 Pct Recovery = 82% Analysis Date = 05/25/16 Pct Recovery = 82% Analysis Date = 05/25/16 Pct Recovery = 82% Analysis Date = 05/14/16 Pct Recovery = 82% Analysis Date = 05/14/16 Pct Recovery = 82% Analysis Date = 05/03/16 Pct Recovery = 82% Analysis Date = 05/03/16 Pct Recovery = 82% Analysis Date = 04/22/16 Pct Recovery = 82% Analysis Date = 04/22/16 Pct Recovery = 82% Analysis Date = 04/12/16 Pct Recovery = 82% Analysis Date = 04/12/16 Pct Recovery = 82% Analysis Date = 04/01/16 Pct Recovery = 82% Analysis Date = 04/01/16 Pct Recovery = 82% Analysis Date = 03/21/16 Pct Recovery = 82% Analysis Date = 03/21/16 Pct Recovery = 82% Analysis Date = 03/10/16 Pct Recovery = 82% Analysis Date = 03/10/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 82% Analysis Date = 01/27/16 Pct Recovery = 82% Analysis Date = 01/27/16 Pct Recovery = 82% Analysis Date = 01/16/16 Pct Recovery = 82% Analysis Date = 01/16/16 Pct Recovery = 82% Analysis Date = 01/05/16 Pct Recovery = 82% Analysis Date = 01/05/16 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/26/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/15/15 Pct Recovery = 82% Analysis Date = 12/04/15 Pct Recovery = 82% Analysis Date = 12/04/15 Pct Recovery = 82% Analysis Date = 11/23/15 Pct Recovery = 82% Analysis Date = 11/23/15 Pct Recovery = 82% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/02/15 Pct Recovery = 83% Analysis Date = 11/02/15 Pct Recovery = 83% Analysis Date = 10/22/15 Pct Recovery = 83% Analysis Date = 10/22/15 Pct Recovery = 83% Analysis Date = 10/11/15 Pct Recovery = 83% Analysis Date = 10/11/15 Pct Recovery = 83% Analysis Date = 09/30/15 Pct Recovery = 83% Analysis Date = 09/30/15 Pct Recovery = 83% Analysis Date = 09/19/15 Pct Recovery = 83% Analysis Date = 09/19/15 Pct Recovery = 83% Analysis Date = 09/09/15 Pct Recovery = 83% Analysis Date = 09/09/15 Pct Recovery = 83% Analysis Date = 08/29/15 Pct Recovery = 83% Analysis Date = 08/29/15 Pct Recovery = 83% Analysis Date = 08/18/15 Pct Recovery = 83% Analysis Date = 08/18/15 Pct Recovery = 83% Analysis Date = 08/07/15 Pct Recovery = 83% Analysis Date = 08/07/15 Pct Recovery = 83% Analysis Date = 07/27/15 Pct Recovery = 83% Analysis Date = 07/27/15 Pct Recovery = 83% Analysis Date = 07/17/15 Pct Recovery = 84% Analysis Date = 07/17/15 Pct Recovery = 84% Analysis Date = 07/06/15 Pct Recovery = 84% Analysis Date = 07/06/15 Pct Recovery = 84% Analysis Date = 06/25/15 Pct Recovery = 84% Analysis Date = 06/25/15 Pct Recovery = 84% Analysis Date = 06/14/15 Pct Recovery = 84% Analysis Date = 06/14/15 Pct Recovery = 84% Analysis Date = 06/03/15 Pct Recovery = 84% Analysis Date = 06/03/15 Pct Recovery = 84% Analysis Date = 05/24/15 Pct Recovery = 85% Analysis Date = 05/24/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 85% Analysis Date = 05/13/15 Pct Recovery = 85% Analysis Date = 05/02/15 Pct Recovery = 85% Analysis Date = 05/02/15 Pct Recovery = 85% Analysis Date = 04/21/15 Pct Recovery = 85% Analysis Date = 04/21/15 Pct Recovery = 85% Analysis Date = 04/10/15 Pct Recovery = 85% Analysis Date = 04/10/15 Pct Recovery = 85% Analysis Date = 03/31/15 Pct Recovery = 86% Analysis Date = 03/31/15 Pct Recovery = 86% Analysis Date = 03/20/15 Pct Recovery = 86% Analysis Date = 03/20/15 Pct Recovery = 86% Analysis Date = 03/09/15 Pct Recovery = 86% Analysis Date = 03/09/15 Pct Recovery = 86% Analysis Date = 02/26/15 Pct Recovery = 86% Analysis Date = 02/26/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/15/15 Pct Recovery = 86% Analysis Date = 02/05/15 Pct Recovery = 87% Analysis Date = 02/05/15 Pct Recovery = 87% Analysis Date = 01/25/15 Pct Recovery = 87% Analysis Date = 01/25/15 Pct Recovery = 87% Analysis Date = 01/14/15 Pct Recovery = 87% Analysis Date = 01/14/15 Pct Recovery = 87% Analysis Date = 01/03/15 Pct Recovery = 87% Analysis Date = 01/03/15 Pct Recovery = 87% Analysis Date = 12/23/14 Pct Recovery = 87% Analysis Date = 12/23/14 Pct Recovery = 87% Analysis Date = 12/13/14 Pct Recovery = 87% Analysis Date = 12/13/14 Pct Recovery = 87% Analysis Date = 12/02/14 Pct Recovery = 88% Analysis Date = 12/02/14 Pct Recovery = 88% Analysis Date = 11/21/14 Pct Recovery = 88% Analysis Date = 11/21/14 Pct Recovery = 88% Analysis Date = 11/10/14 Pct Recovery = 88% Analysis Date = 11/10/14 Pct Recovery = 88% Analysis Date = 10/30/14 Pct Recovery = 88% Analysis Date = 10/30/14 Pct Recovery = 88% Analysis Date = 10/20/14 Pct Recovery = 88% Analysis Date = 10/20/14 Pct Recovery = 88% Analysis Date = 10/09/14 Pct Recovery = 89% Analysis Date = 10/09/14 Pct Recovery = 89% Analysis Date = 09/28/14 Pct Recovery = 90% Analysis Date = 09/28/14 Pct Recovery = 90% Analysis Date = 09/17/14 Pct Recovery = 90% Analysis Date = 09/17/14 Pct Recovery = 90% Analysis Date = 09/06/14 Pct Recovery = 91% Analysis Date = 09/06/14 Pct Recovery = 91% Analysis Date = 08/27/14 Pct Recovery = 91% Analysis Date = 08/27/14 Pct Recovery = 91% Analysis Date = 08/16/14 Pct Recovery = 92% Analysis Date = 08/16/14 Pct Recovery = 92% Analysis Date = 08/05/14 Pct Recovery = 92% Analysis Date = 08/05/14 Pct Recovery = 92% Analysis Date = 07/25/14 Pct Recovery = 93% Analysis Date = 07/25/14 Pct Recovery = 93% Analysis Date = 07/14/14 Pct Recovery = 93% Analysis Date = 07/14/14 Pct Recovery = 93% Analysis Date = 07/04/14 Pct Recovery = 93% Analysis Date = 07/04/14 Pct Recovery = 93% Analysis Date = 06/23/14 Pct Recovery = 94% Analysis Date = 06/23/14 Pct Recovery = 94% Analysis Date = 06/12/14 Pct Recovery = 94% Analysis Date = 06/12/14 Pct Recovery = 94% Analysis Date = 06/01/14 Pct Recovery = 94% Analysis Date = 06/01/14 Pct Recovery = 94% Analysis Date = 05/21/14 Pct Recovery = 95% Analysis Date = 05/21/14 Pct Recovery = 95% Analysis Date = 05/11/14 Pct Recovery = 95% Analysis Date = 05/11/14 Pct Recovery = 95% Analysis Date = 04/30/14 Pct Recovery = 95% Analysis Date = 04/30/14 Pct Recovery = 95% Analysis Date = 04/19/14 Pct Recovery = 95% Analysis Date = 04/19/14 Pct Recovery = 95% Analysis Date = 04/08/14 Pct Recovery = 95% Analysis Date = 04/08/14 Pct Recovery = 95% Analysis Date = 03/28/14 Pct Recovery = 95% Analysis Date = 03/28/14 Pct Recovery = 95% Analysis Date = 03/18/14 Pct Recovery = 95% Analysis Date = 03/18/14 Pct Recovery = 95% Analysis Date = 03/07/14 Pct Recovery = 95% Analysis Date = 03/07/14 Pct Recovery = 95% Analysis Date = 02/24/14 Pct Recovery = 95% Analysis Date = 02/24/14 Pct Recovery = 95% Analysis Date = 02/13/14 Pct Recovery = 95% Analysis Date = 02/13/14 Pct Recovery = 95% Analysis Date = 02/02/14 Pct Recovery = 95% Analysis Date = 02/02/14 Pct Recovery = 95% Analysis Date = 01/23/14 Pct Recovery = 95% Analysis Date = 01/23/14 Pct Recovery = 95% Analysis Date = 01/12/14 Pct Recovery = 95% Analysis Date = 01/12/14 Pct Recovery = 95% Analysis Date = 01/01/14 Pct Recovery = 95% Analysis Date = 01/01/14 Pct Recovery = 95% Analysis Date = 12/21/13 Pct Recovery = 95% Analysis Date = 12/21/13 Pct Recovery = 95% Analysis Date = 12/10/13 Pct Recovery = 95% Analysis Date = 12/10/13 Pct Recovery = 95% Analysis Date = 11/30/13 Pct Recovery = 95% Analysis Date = 11/30/13 Pct Recovery = 95% Analysis Date = 11/19/13 Pct Recovery = 95% Analysis Date = 11/19/13 Pct Recovery = 95% Analysis Date = 11/08/13 Pct Recovery = 95% Analysis Date = 11/08/13 Pct Recovery = 95% Analysis Date = 10/28/13 Pct Recovery = 95% Analysis Date = 10/28/13 Pct Recovery = 95% Analysis Date = 10/17/13 Pct Recovery = 95% Analysis Date = 10/17/13 Pct Recovery = 95% Analysis Date = 10/07/13 Pct Recovery = 95% Analysis Date = 10/07/13 Pct Recovery = 95% Analysis Date = 09/26/13 Pct Recovery = 95% Analysis Date = 09/26/13 Pct Recovery = 95% Analysis Date = 09/15/13 Pct Recovery = 95% Analysis Date = 09/15/13 Pct Recovery = 95% Analysis Date = 09/04/13 Pct Recovery = 95% Analysis Date = 09/04/13 Pct Recovery = 95% Analysis Date = 08/24/13 Pct Recovery = 95% Analysis Date = 08/24/13 Pct Recovery = 95% Analysis Date = 08/14/13 Pct Recovery = 95% Analysis Date = 08/14/13 Pct Recovery = 95% Analysis Date = 08/03/13 Pct Recovery = 95% Analysis Date = 08/03/13 Pct Recovery = 95% Analysis Date = 07/23/13 Pct Recovery = 95% Analysis Date = 07/23/13 Pct Recovery = 95% Analysis Date = 07/12/13 Pct Recovery = 94% Analysis Date = 07/12/13 Pct Recovery = 94% Analysis Date = 07/01/13 Pct Recovery = 94% Analysis Date = 07/01/13 Pct Recovery = 94% Analysis Date = 06/21/13 Pct Recovery = 94% Analysis Date = 06/21/13 Pct Recovery = 94% Analysis Date = 06/10/13 Pct Recovery = 94% Analysis Date = 06/10/13 Pct Recovery = 94% Analysis Date = 05/30/13 Pct Recovery = 94% Analysis Date = 05/30/13 Pct Recovery = 94% Analysis Date = 05/19/13 Pct Recovery = 94% Analysis Date = 05/19/13 Pct Recovery = 94% Analysis Date = 05/08/13 Pct Recovery = 94% Analysis Date = 05/08/13 Pct Recovery = 94% Analysis Date = 04/28/13 Pct Recovery = 94% Analysis Date = 04/28/13 Pct Recovery = 94% Analysis Date = 04/17/13 Pct Recovery = 94% Analysis Date = 04/17/13 Pct Recovery = 94% Analysis Date = 04/06/13 Pct Recovery = 94% Analysis Date = 04/06/13 Pct Recovery = 94% Analysis Date = 03/26/13 Pct Recovery = 94% Analysis Date = 03/26/13 Pct Recovery = 94% Analysis Date = 03/15/13 Pct Recovery = 94% Analysis Date = 03/15/13 Pct Recovery = 94% Analysis Date = 03/05/13 Pct Recovery = 94% Analysis Date = 03/05/13 Pct Recovery = 94% Analysis Date = 02/22/13 Pct Recovery = 94% Analysis Date = 02/22/13 Pct Recovery = 94% Analysis Date = 02/11/13 Pct Recovery = 94% Analysis Date = 02/11/13 Pct Recovery = 94% Analysis Date = 01/31/13 Pct Recovery = 94% Analysis Date = 01/31/13 Pct Recovery = 94% Analysis Date = 01/20/13 Pct Recovery = 94% Analysis Date = 01/20/13 Pct Recovery = 94% Analysis Date = 01/10/13 Pct Recovery = 94% Analysis Date = 01/10/13 Pct Recovery = 94% Analysis Date = 12/30/12 Pct Recovery = 94% Analysis Date = 12/30/12 Pct Recovery = 94% Analysis Date = 12/19/12 Pct Recovery = 94% Analysis Date = 12/19/12 Pct Recovery = 94% Analysis Date = 12/08/12 Pct Recovery = 94% Analysis Date = 12/08/12 Pct Recovery = 94% Analysis Date = 11/27/12 Pct Recovery = 94% Analysis Date = 11/27/12 Pct Recovery = 94% Analysis Date = 11/17/12 Pct Recovery = 94% Analysis Date = 11/17/12 Pct Recovery = 94% Analysis Date = 11/06/12 Pct Recovery = 94% Analysis Date = 11/06/12 Pct Recovery = 94% Analysis Date = 10/26/12 Pct Recovery = 94% Analysis Date = 10/26/12 Pct Recovery = 94% Analysis Date = 10/15/12 Pct Recovery = 94% Analysis Date = 10/15/12 Pct Recovery = 94% Analysis Date = 10/04/12 Pct Recovery = 94% Analysis Date = 10/04/12 Pct Recovery = 94% Analysis Date = 09/24/12 Pct Recovery = 94% Analysis Date = 09/24/12 Pct Recovery = 94% Analysis Date = 09/13/12 Pct Recovery = 94% Analysis Date = 09/13/12 Pct Recovery = 94% Analysis Date = 09/02/12 Pct Recovery = 94% Analysis Date = 09/02/12 Pct Recovery = 94% Analysis Date = 08/22/12 Pct Recovery = 94% Analysis Date = 08/22/12 Pct Recovery = 94% Analysis Date = 08/11/12 Pct Recovery = 94% Analysis Date = 08/11/12 Pct Recovery = 94% Analysis Date = 08/01/12 Pct Recovery = 94% Analysis Date = 08/01/12 Pct Recovery = 94% Analysis Date = 07/21/12 Pct Recovery = 94% Analysis Date = 07/21/12 Pct Recovery = 94% Analysis Date = 07/10/12 Pct Recovery = 94% Analysis Date = 07/10/12 Pct Recovery = 94% Analysis Date = 06/29/12 Pct Recovery = 94% Analysis Date = 06/29/12 Pct Recovery = 94% Analysis Date = 06/18/12 Pct Recovery = 94% Analysis Date = 06/18/12 Pct Recovery = 94% Analysis Date = 06/08/12 Pct Recovery = 94% Analysis Date = 06/08/12 Pct Recovery = 94% Analysis Date = 05/28/12 Pct Recovery = 94% Analysis Date = 05/28/12 Pct Recovery = 94% Analysis Date = 05/17/12 Pct Recovery = 94% Analysis Date = 05/17/12 Pct Recovery = 94% Analysis Date = 05/06/12 Pct Recovery = 94% Analysis Date = 05/06/12 Pct Recovery = 94% Analysis Date = 04/25/12 Pct Recovery = 94% Analysis Date = 04/25/12 Pct Recovery = 94% Analysis Date = 04/15/12 Pct Recovery = 94% Analysis Date = 04/15/12 Pct Recovery = 94% Analysis Date = 04/04/12 Pct Recovery = 94% Analysis Date = 04/04/12 Pct Recovery = 94% Analysis Date = 03/24/12 Pct Recovery = 95% Analysis Date = 03/24/12 Pct Recovery = 95% Analysis Date = 03/13/12 Pct Recovery = 95% Analysis Date = 03/13/12 Pct Recovery = 95% Analysis Date = 03/02/12 Pct Recovery = 95% Analysis Date = 03/02/12 Pct Recovery = 95% Analysis Date = 02/21/12 Pct Recovery = 95% Analysis Date = 02/21/12 Pct Recovery = 95% Analysis Date = 02/10/12 Pct Recovery = 95% Analysis Date = 02/10/12 Pct Recovery = 95% Analysis Date = 01/30/12 Pct Recovery = 95% Analysis Date = 01/30/12 Pct Recovery = 95% Analysis Date = 01/19/12 Pct Recovery = 95% Analysis Date = 01/19/12 Pct Recovery = 95% Analysis Date = 01/08/12 Pct Recovery = 95% Analysis Date = 01/08/12 Pct Recovery = 95% Analysis Date = 12/29/11 Pct Recovery = 95% Analysis Date = 12/29/11 Pct Recovery = 95% Analysis Date = 12/18/11 Pct Recovery = 95% Analysis Date = 12/18/11 Pct Recovery = 95% Analysis Date = 12/07/11 Pct Recovery = 95% Analysis Date = 12/07/11 Pct Recovery = 95% Analysis Date = 11/26/11 Pct Recovery = 95% Analysis Date = 11/26/11 Pct Recovery = 95% Analysis Date = 11/15/11 Pct Recovery = 95% Analysis Date = 11/15/11 Pct Recovery = 95% Analysis Date = 11/05/11 Pct Recovery = 95% Analysis Date = 11/05/11 Pct Recovery = 95% Analysis Date = 10/25/11 Pct Recovery = 95% Analysis Date = 10/25/11 Pct Recovery = 95% Analysis Date = 10/14/11 Pct Recovery = 95% Analysis Date = 10/14/11 Pct Recovery = 95% Analysis Date = 10/03/11 Pct Recovery = 95% Analysis Date = 10/03/11 Pct Recovery = 95% Analysis Date = 09/22/11 Pct Recovery = 95% Analysis Date = 09/22/11 Pct Recovery = 95% Analysis Date = 09/12/11 Pct Recovery = 95% Analysis Date = 09/12/11 Pct Recovery = 95% Analysis Date = 09/01/11 Pct Recovery = 96% Analysis Date = 09/01/11 Pct Recovery = 96% Analysis Date = 08/21/11 Pct Recovery = 96% Analysis Date = 08/21/11 Pct Recovery = 96% Analysis Date = 08/10/11 Pct Recovery = 96% Analysis Date = 08/10/11 Pct Recovery = 96% Analysis Date = 07/30/11 Pct Recovery = 96% Analysis Date = 07/30/11 Pct Recovery = 96% Analysis Date = 07/20/11 Pct Recovery = 96% Analysis Date = 07/20/11 Pct Recovery = 96% Analysis Date = 07/09/11 Pct Recovery = 96% Analysis Date = 07/09/11 Pct Recovery = 96% Analysis Date = 06/28/11 Pct Recovery = 96% Analysis Date = 06/28/11 Pct Recovery = 96% Analysis Date = 06/17/11 Pct Recovery = 96% Analysis Date = 06/17/11 Pct Recovery = 96% Analysis Date = 06/06/11 Pct Recovery = 96% Analysis Date = 06/06/11 Pct Recovery = 96% Analysis Date = 05/27/11 Pct Recovery = 96% Analysis Date = 05/27/11 Pct Recovery = 96% Analysis Date = 05/16/11 Pct Recovery = 96% Analysis Date = 05/16/11 Pct Recovery = 96% Analysis Date = 05/05/11 Pct Recovery = 96% Analysis Date = 05/05/11 Pct Recovery = 96% Analysis Date = 04/24/11 Pct Recovery = 96% Analysis Date = 04/24/11 Pct Recovery = 96% Analysis Date = 04/13/11 Pct Recovery = 97% Analysis Date = 04/13/11 Pct Recovery = 97% Analysis Date = 04/03/11 Pct Recovery = 97% Analysis Date = 04/03/11 Pct Recovery = 97% Analysis Date = 03/23/11 Pct Recovery = 97% Analysis Date = 03/23/11 Pct Recovery = 97% Analysis Date = 03/12/11 Pct Recovery = 97% Analysis Date = 03/12/11 Pct Recovery = 97% Analysis Date = 03/01/11 Pct Recovery = 97% Analysis Date = 03/01/11 Pct Recovery = 97% Analysis Date = 02/19/11 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-ETHYL-6-METHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 90% 15% 92% 13%
Total 69 90% 15% 92% 13%

Sample Statistics
2-ETHYL-6-METHYLANILINE

Characteristic N % % Basis
Plotted 69 99% Spiked
Estimated Values 69 99% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 70 .  
False Negatives 1 1% 1 out of 70
Not Spiked 92 .  
False Positives 0 0% 0 out of 92

BQS OBSP Determination:
3,4-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61625GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 59% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 59% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 87% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 79% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 82% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 84% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 78% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 88% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 77% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 87% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 77% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 69% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 80% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 77% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 78% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 85% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 94% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 71% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 72% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 79% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 76% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 68% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 77% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 95% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 81% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 88% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 83% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 65% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 73% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 77% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 84% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 69% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 69% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 90% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 85% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 60% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 51% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 91% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 54% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 72% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 57% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 57% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 67% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 85% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 72% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 70% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 66% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 81% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 75% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 83% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 101% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 66% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 88% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 75% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 93% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 73% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 82% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 62% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 61% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 83% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 77% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 94% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 100% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 91% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 74% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 79% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 65% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 74% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 64% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 59% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 77% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 67% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 58% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 88% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 45% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 76% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 58% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 58% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 68% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/07/16 Pct Recovery = 71% Analysis Date = 11/07/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/16/16 Pct Recovery = 71% Analysis Date = 10/16/16 Pct Recovery = 71% Analysis Date = 10/06/16 Pct Recovery = 71% Analysis Date = 10/06/16 Pct Recovery = 71% Analysis Date = 09/25/16 Pct Recovery = 70% Analysis Date = 09/25/16 Pct Recovery = 70% Analysis Date = 09/14/16 Pct Recovery = 70% Analysis Date = 09/14/16 Pct Recovery = 70% Analysis Date = 09/04/16 Pct Recovery = 70% Analysis Date = 09/04/16 Pct Recovery = 70% Analysis Date = 08/24/16 Pct Recovery = 70% Analysis Date = 08/24/16 Pct Recovery = 70% Analysis Date = 08/13/16 Pct Recovery = 70% Analysis Date = 08/13/16 Pct Recovery = 70% Analysis Date = 08/03/16 Pct Recovery = 70% Analysis Date = 08/03/16 Pct Recovery = 70% Analysis Date = 07/23/16 Pct Recovery = 70% Analysis Date = 07/23/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/02/16 Pct Recovery = 70% Analysis Date = 07/02/16 Pct Recovery = 70% Analysis Date = 06/21/16 Pct Recovery = 70% Analysis Date = 06/21/16 Pct Recovery = 70% Analysis Date = 06/10/16 Pct Recovery = 70% Analysis Date = 06/10/16 Pct Recovery = 70% Analysis Date = 05/31/16 Pct Recovery = 70% Analysis Date = 05/31/16 Pct Recovery = 70% Analysis Date = 05/20/16 Pct Recovery = 69% Analysis Date = 05/20/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 04/29/16 Pct Recovery = 69% Analysis Date = 04/29/16 Pct Recovery = 69% Analysis Date = 04/18/16 Pct Recovery = 69% Analysis Date = 04/18/16 Pct Recovery = 69% Analysis Date = 04/07/16 Pct Recovery = 69% Analysis Date = 04/07/16 Pct Recovery = 69% Analysis Date = 03/28/16 Pct Recovery = 69% Analysis Date = 03/28/16 Pct Recovery = 69% Analysis Date = 03/17/16 Pct Recovery = 69% Analysis Date = 03/17/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 02/24/16 Pct Recovery = 69% Analysis Date = 02/24/16 Pct Recovery = 69% Analysis Date = 02/14/16 Pct Recovery = 69% Analysis Date = 02/14/16 Pct Recovery = 69% Analysis Date = 02/03/16 Pct Recovery = 69% Analysis Date = 02/03/16 Pct Recovery = 69% Analysis Date = 01/23/16 Pct Recovery = 69% Analysis Date = 01/23/16 Pct Recovery = 69% Analysis Date = 01/13/16 Pct Recovery = 69% Analysis Date = 01/13/16 Pct Recovery = 69% Analysis Date = 01/02/16 Pct Recovery = 69% Analysis Date = 01/02/16 Pct Recovery = 69% Analysis Date = 12/22/15 Pct Recovery = 68% Analysis Date = 12/22/15 Pct Recovery = 68% Analysis Date = 12/12/15 Pct Recovery = 68% Analysis Date = 12/12/15 Pct Recovery = 68% Analysis Date = 12/01/15 Pct Recovery = 68% Analysis Date = 12/01/15 Pct Recovery = 68% Analysis Date = 11/20/15 Pct Recovery = 68% Analysis Date = 11/20/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 68% Analysis Date = 10/30/15 Pct Recovery = 68% Analysis Date = 10/30/15 Pct Recovery = 68% Analysis Date = 10/19/15 Pct Recovery = 68% Analysis Date = 10/19/15 Pct Recovery = 68% Analysis Date = 10/09/15 Pct Recovery = 68% Analysis Date = 10/09/15 Pct Recovery = 68% Analysis Date = 09/28/15 Pct Recovery = 68% Analysis Date = 09/28/15 Pct Recovery = 68% Analysis Date = 09/17/15 Pct Recovery = 68% Analysis Date = 09/17/15 Pct Recovery = 68% Analysis Date = 09/07/15 Pct Recovery = 68% Analysis Date = 09/07/15 Pct Recovery = 68% Analysis Date = 08/27/15 Pct Recovery = 68% Analysis Date = 08/27/15 Pct Recovery = 68% Analysis Date = 08/16/15 Pct Recovery = 68% Analysis Date = 08/16/15 Pct Recovery = 68% Analysis Date = 08/06/15 Pct Recovery = 68% Analysis Date = 08/06/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/26/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/15/15 Pct Recovery = 68% Analysis Date = 07/05/15 Pct Recovery = 68% Analysis Date = 07/05/15 Pct Recovery = 68% Analysis Date = 06/24/15 Pct Recovery = 68% Analysis Date = 06/24/15 Pct Recovery = 68% Analysis Date = 06/13/15 Pct Recovery = 68% Analysis Date = 06/13/15 Pct Recovery = 68% Analysis Date = 06/02/15 Pct Recovery = 68% Analysis Date = 06/02/15 Pct Recovery = 68% Analysis Date = 05/23/15 Pct Recovery = 68% Analysis Date = 05/23/15 Pct Recovery = 68% Analysis Date = 05/12/15 Pct Recovery = 68% Analysis Date = 05/12/15 Pct Recovery = 68% Analysis Date = 05/01/15 Pct Recovery = 68% Analysis Date = 05/01/15 Pct Recovery = 68% Analysis Date = 04/21/15 Pct Recovery = 68% Analysis Date = 04/21/15 Pct Recovery = 68% Analysis Date = 04/10/15 Pct Recovery = 67% Analysis Date = 04/10/15 Pct Recovery = 67% Analysis Date = 03/30/15 Pct Recovery = 67% Analysis Date = 03/30/15 Pct Recovery = 67% Analysis Date = 03/20/15 Pct Recovery = 67% Analysis Date = 03/20/15 Pct Recovery = 67% Analysis Date = 03/09/15 Pct Recovery = 67% Analysis Date = 03/09/15 Pct Recovery = 67% Analysis Date = 02/26/15 Pct Recovery = 67% Analysis Date = 02/26/15 Pct Recovery = 67% Analysis Date = 02/16/15 Pct Recovery = 67% Analysis Date = 02/16/15 Pct Recovery = 67% Analysis Date = 02/05/15 Pct Recovery = 67% Analysis Date = 02/05/15 Pct Recovery = 67% Analysis Date = 01/25/15 Pct Recovery = 67% Analysis Date = 01/25/15 Pct Recovery = 67% Analysis Date = 01/15/15 Pct Recovery = 68% Analysis Date = 01/15/15 Pct Recovery = 68% Analysis Date = 01/04/15 Pct Recovery = 68% Analysis Date = 01/04/15 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/03/14 Pct Recovery = 68% Analysis Date = 12/03/14 Pct Recovery = 68% Analysis Date = 11/22/14 Pct Recovery = 68% Analysis Date = 11/22/14 Pct Recovery = 68% Analysis Date = 11/12/14 Pct Recovery = 68% Analysis Date = 11/12/14 Pct Recovery = 68% Analysis Date = 11/01/14 Pct Recovery = 69% Analysis Date = 11/01/14 Pct Recovery = 69% Analysis Date = 10/21/14 Pct Recovery = 69% Analysis Date = 10/21/14 Pct Recovery = 69% Analysis Date = 10/11/14 Pct Recovery = 69% Analysis Date = 10/11/14 Pct Recovery = 69% Analysis Date = 09/30/14 Pct Recovery = 69% Analysis Date = 09/30/14 Pct Recovery = 69% Analysis Date = 09/19/14 Pct Recovery = 69% Analysis Date = 09/19/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 09/08/14 Pct Recovery = 69% Analysis Date = 08/29/14 Pct Recovery = 69% Analysis Date = 08/29/14 Pct Recovery = 69% Analysis Date = 08/18/14 Pct Recovery = 70% Analysis Date = 08/18/14 Pct Recovery = 70% Analysis Date = 08/07/14 Pct Recovery = 70% Analysis Date = 08/07/14 Pct Recovery = 70% Analysis Date = 07/28/14 Pct Recovery = 70% Analysis Date = 07/28/14 Pct Recovery = 70% Analysis Date = 07/17/14 Pct Recovery = 71% Analysis Date = 07/17/14 Pct Recovery = 71% Analysis Date = 07/06/14 Pct Recovery = 71% Analysis Date = 07/06/14 Pct Recovery = 71% Analysis Date = 06/26/14 Pct Recovery = 71% Analysis Date = 06/26/14 Pct Recovery = 71% Analysis Date = 06/15/14 Pct Recovery = 71% Analysis Date = 06/15/14 Pct Recovery = 71% Analysis Date = 06/04/14 Pct Recovery = 72% Analysis Date = 06/04/14 Pct Recovery = 72% Analysis Date = 05/25/14 Pct Recovery = 72% Analysis Date = 05/25/14 Pct Recovery = 72% Analysis Date = 05/14/14 Pct Recovery = 72% Analysis Date = 05/14/14 Pct Recovery = 72% Analysis Date = 05/03/14 Pct Recovery = 73% Analysis Date = 05/03/14 Pct Recovery = 73% Analysis Date = 04/23/14 Pct Recovery = 73% Analysis Date = 04/23/14 Pct Recovery = 73% Analysis Date = 04/12/14 Pct Recovery = 73% Analysis Date = 04/12/14 Pct Recovery = 73% Analysis Date = 04/01/14 Pct Recovery = 73% Analysis Date = 04/01/14 Pct Recovery = 73% Analysis Date = 03/22/14 Pct Recovery = 74% Analysis Date = 03/22/14 Pct Recovery = 74% Analysis Date = 03/11/14 Pct Recovery = 74% Analysis Date = 03/11/14 Pct Recovery = 74% Analysis Date = 02/28/14 Pct Recovery = 74% Analysis Date = 02/28/14 Pct Recovery = 74% Analysis Date = 02/18/14 Pct Recovery = 74% Analysis Date = 02/18/14 Pct Recovery = 74% Analysis Date = 02/07/14 Pct Recovery = 75% Analysis Date = 02/07/14 Pct Recovery = 75% Analysis Date = 01/27/14 Pct Recovery = 75% Analysis Date = 01/27/14 Pct Recovery = 75% Analysis Date = 01/17/14 Pct Recovery = 75% Analysis Date = 01/17/14 Pct Recovery = 75% Analysis Date = 01/06/14 Pct Recovery = 75% Analysis Date = 01/06/14 Pct Recovery = 75% Analysis Date = 12/26/13 Pct Recovery = 76% Analysis Date = 12/26/13 Pct Recovery = 76% Analysis Date = 12/15/13 Pct Recovery = 76% Analysis Date = 12/15/13 Pct Recovery = 76% Analysis Date = 12/05/13 Pct Recovery = 76% Analysis Date = 12/05/13 Pct Recovery = 76% Analysis Date = 11/24/13 Pct Recovery = 76% Analysis Date = 11/24/13 Pct Recovery = 76% Analysis Date = 11/13/13 Pct Recovery = 77% Analysis Date = 11/13/13 Pct Recovery = 77% Analysis Date = 11/03/13 Pct Recovery = 77% Analysis Date = 11/03/13 Pct Recovery = 77% Analysis Date = 10/23/13 Pct Recovery = 77% Analysis Date = 10/23/13 Pct Recovery = 77% Analysis Date = 10/12/13 Pct Recovery = 77% Analysis Date = 10/12/13 Pct Recovery = 77% Analysis Date = 10/02/13 Pct Recovery = 77% Analysis Date = 10/02/13 Pct Recovery = 77% Analysis Date = 09/21/13 Pct Recovery = 77% Analysis Date = 09/21/13 Pct Recovery = 77% Analysis Date = 09/10/13 Pct Recovery = 78% Analysis Date = 09/10/13 Pct Recovery = 78% Analysis Date = 08/31/13 Pct Recovery = 78% Analysis Date = 08/31/13 Pct Recovery = 78% Analysis Date = 08/20/13 Pct Recovery = 78% Analysis Date = 08/20/13 Pct Recovery = 78% Analysis Date = 08/09/13 Pct Recovery = 78% Analysis Date = 08/09/13 Pct Recovery = 78% Analysis Date = 07/30/13 Pct Recovery = 78% Analysis Date = 07/30/13 Pct Recovery = 78% Analysis Date = 07/19/13 Pct Recovery = 78% Analysis Date = 07/19/13 Pct Recovery = 78% Analysis Date = 07/08/13 Pct Recovery = 78% Analysis Date = 07/08/13 Pct Recovery = 78% Analysis Date = 06/28/13 Pct Recovery = 78% Analysis Date = 06/28/13 Pct Recovery = 78% Analysis Date = 06/17/13 Pct Recovery = 79% Analysis Date = 06/17/13 Pct Recovery = 79% Analysis Date = 06/06/13 Pct Recovery = 79% Analysis Date = 06/06/13 Pct Recovery = 79% Analysis Date = 05/27/13 Pct Recovery = 79% Analysis Date = 05/27/13 Pct Recovery = 79% Analysis Date = 05/16/13 Pct Recovery = 79% Analysis Date = 05/16/13 Pct Recovery = 79% Analysis Date = 05/05/13 Pct Recovery = 79% Analysis Date = 05/05/13 Pct Recovery = 79% Analysis Date = 04/25/13 Pct Recovery = 79% Analysis Date = 04/25/13 Pct Recovery = 79% Analysis Date = 04/14/13 Pct Recovery = 79% Analysis Date = 04/14/13 Pct Recovery = 79% Analysis Date = 04/03/13 Pct Recovery = 79% Analysis Date = 04/03/13 Pct Recovery = 79% Analysis Date = 03/23/13 Pct Recovery = 80% Analysis Date = 03/23/13 Pct Recovery = 80% Analysis Date = 03/13/13 Pct Recovery = 80% Analysis Date = 03/13/13 Pct Recovery = 80% Analysis Date = 03/02/13 Pct Recovery = 80% Analysis Date = 03/02/13 Pct Recovery = 80% Analysis Date = 02/19/13 Pct Recovery = 80% Analysis Date = 02/19/13 Pct Recovery = 80% Analysis Date = 02/09/13 Pct Recovery = 80% Analysis Date = 02/09/13 Pct Recovery = 80% Analysis Date = 01/29/13 Pct Recovery = 80% Analysis Date = 01/29/13 Pct Recovery = 80% Analysis Date = 01/18/13 Pct Recovery = 80% Analysis Date = 01/18/13 Pct Recovery = 80% Analysis Date = 01/08/13 Pct Recovery = 80% Analysis Date = 01/08/13 Pct Recovery = 80% Analysis Date = 12/28/12 Pct Recovery = 80% Analysis Date = 12/28/12 Pct Recovery = 80% Analysis Date = 12/17/12 Pct Recovery = 80% Analysis Date = 12/17/12 Pct Recovery = 80% Analysis Date = 12/07/12 Pct Recovery = 80% Analysis Date = 12/07/12 Pct Recovery = 80% Analysis Date = 11/26/12 Pct Recovery = 80% Analysis Date = 11/26/12 Pct Recovery = 80% Analysis Date = 11/15/12 Pct Recovery = 80% Analysis Date = 11/15/12 Pct Recovery = 80% Analysis Date = 11/05/12 Pct Recovery = 80% Analysis Date = 11/05/12 Pct Recovery = 80% Analysis Date = 10/25/12 Pct Recovery = 80% Analysis Date = 10/25/12 Pct Recovery = 80% Analysis Date = 10/14/12 Pct Recovery = 80% Analysis Date = 10/14/12 Pct Recovery = 80% Analysis Date = 10/04/12 Pct Recovery = 80% Analysis Date = 10/04/12 Pct Recovery = 80% Analysis Date = 09/23/12 Pct Recovery = 80% Analysis Date = 09/23/12 Pct Recovery = 80% Analysis Date = 09/12/12 Pct Recovery = 80% Analysis Date = 09/12/12 Pct Recovery = 80% Analysis Date = 09/02/12 Pct Recovery = 80% Analysis Date = 09/02/12 Pct Recovery = 80% Analysis Date = 08/22/12 Pct Recovery = 80% Analysis Date = 08/22/12 Pct Recovery = 80% Analysis Date = 08/11/12 Pct Recovery = 80% Analysis Date = 08/11/12 Pct Recovery = 80% Analysis Date = 08/01/12 Pct Recovery = 80% Analysis Date = 08/01/12 Pct Recovery = 80% Analysis Date = 07/21/12 Pct Recovery = 80% Analysis Date = 07/21/12 Pct Recovery = 80% Analysis Date = 07/10/12 Pct Recovery = 80% Analysis Date = 07/10/12 Pct Recovery = 80% Analysis Date = 06/29/12 Pct Recovery = 80% Analysis Date = 06/29/12 Pct Recovery = 80% Analysis Date = 06/19/12 Pct Recovery = 80% Analysis Date = 06/19/12 Pct Recovery = 80% Analysis Date = 06/08/12 Pct Recovery = 80% Analysis Date = 06/08/12 Pct Recovery = 80% Analysis Date = 05/28/12 Pct Recovery = 80% Analysis Date = 05/28/12 Pct Recovery = 80% Analysis Date = 05/18/12 Pct Recovery = 80% Analysis Date = 05/18/12 Pct Recovery = 80% Analysis Date = 05/07/12 Pct Recovery = 80% Analysis Date = 05/07/12 Pct Recovery = 80% Analysis Date = 04/26/12 Pct Recovery = 80% Analysis Date = 04/26/12 Pct Recovery = 80% Analysis Date = 04/16/12 Pct Recovery = 80% Analysis Date = 04/16/12 Pct Recovery = 80% Analysis Date = 04/05/12 Pct Recovery = 80% Analysis Date = 04/05/12 Pct Recovery = 80% Analysis Date = 03/25/12 Pct Recovery = 80% Analysis Date = 03/25/12 Pct Recovery = 80% Analysis Date = 03/15/12 Pct Recovery = 80% Analysis Date = 03/15/12 Pct Recovery = 80% Analysis Date = 03/04/12 Pct Recovery = 80% Analysis Date = 03/04/12 Pct Recovery = 80% Analysis Date = 02/22/12 Pct Recovery = 80% Analysis Date = 02/22/12 Pct Recovery = 80% Analysis Date = 02/12/12 Pct Recovery = 80% Analysis Date = 02/12/12 Pct Recovery = 80% Analysis Date = 02/01/12 Pct Recovery = 80% Analysis Date = 02/01/12 Pct Recovery = 80% Analysis Date = 01/21/12 Pct Recovery = 80% Analysis Date = 01/21/12 Pct Recovery = 80% Analysis Date = 01/11/12 Pct Recovery = 80% Analysis Date = 01/11/12 Pct Recovery = 80% Analysis Date = 12/31/11 Pct Recovery = 80% Analysis Date = 12/31/11 Pct Recovery = 80% Analysis Date = 12/20/11 Pct Recovery = 80% Analysis Date = 12/20/11 Pct Recovery = 80% Analysis Date = 12/10/11 Pct Recovery = 80% Analysis Date = 12/10/11 Pct Recovery = 80% Analysis Date = 11/29/11 Pct Recovery = 80% Analysis Date = 11/29/11 Pct Recovery = 80% Analysis Date = 11/18/11 Pct Recovery = 80% Analysis Date = 11/18/11 Pct Recovery = 80% Analysis Date = 11/08/11 Pct Recovery = 80% Analysis Date = 11/08/11 Pct Recovery = 80% Analysis Date = 10/28/11 Pct Recovery = 80% Analysis Date = 10/28/11 Pct Recovery = 80% Analysis Date = 10/17/11 Pct Recovery = 80% Analysis Date = 10/17/11 Pct Recovery = 80% Analysis Date = 10/06/11 Pct Recovery = 80% Analysis Date = 10/06/11 Pct Recovery = 80% Analysis Date = 09/26/11 Pct Recovery = 80% Analysis Date = 09/26/11 Pct Recovery = 80% Analysis Date = 09/15/11 Pct Recovery = 80% Analysis Date = 09/15/11 Pct Recovery = 80% Analysis Date = 09/04/11 Pct Recovery = 80% Analysis Date = 09/04/11 Pct Recovery = 80% Analysis Date = 08/25/11 Pct Recovery = 80% Analysis Date = 08/25/11 Pct Recovery = 80% Analysis Date = 08/14/11 Pct Recovery = 80% Analysis Date = 08/14/11 Pct Recovery = 80% Analysis Date = 08/03/11 Pct Recovery = 80% Analysis Date = 08/03/11 Pct Recovery = 80% Analysis Date = 07/24/11 Pct Recovery = 80% Analysis Date = 07/24/11 Pct Recovery = 80% Analysis Date = 07/13/11 Pct Recovery = 80% Analysis Date = 07/13/11 Pct Recovery = 80% Analysis Date = 07/02/11 Pct Recovery = 80% Analysis Date = 07/02/11 Pct Recovery = 80% Analysis Date = 06/22/11 Pct Recovery = 80% Analysis Date = 06/22/11 Pct Recovery = 80% Analysis Date = 06/11/11 Pct Recovery = 80% Analysis Date = 06/11/11 Pct Recovery = 80% Analysis Date = 05/31/11 Pct Recovery = 80% Analysis Date = 05/31/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/10/11 Pct Recovery = 80% Analysis Date = 05/10/11 Pct Recovery = 80% Analysis Date = 04/29/11 Pct Recovery = 80% Analysis Date = 04/29/11 Pct Recovery = 80% Analysis Date = 04/19/11 Pct Recovery = 80% Analysis Date = 04/19/11 Pct Recovery = 80% Analysis Date = 04/08/11 Pct Recovery = 80% Analysis Date = 04/08/11 Pct Recovery = 80% Analysis Date = 03/28/11 Pct Recovery = 80% Analysis Date = 03/28/11 Pct Recovery = 80% Analysis Date = 03/18/11 Pct Recovery = 80% Analysis Date = 03/18/11 Pct Recovery = 80% Analysis Date = 03/07/11 Pct Recovery = 80% Analysis Date = 03/07/11 Pct Recovery = 80% Analysis Date = 02/24/11 Pct Recovery = 80% Analysis Date = 02/24/11 Pct Recovery = 80% Analysis Date = 02/14/11 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,4-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 75% 12% 75% 12%
Total 94 75% 12% 75% 12%

Sample Statistics
3,4-DICHLOROANILINE

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 94 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
3,5-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61627GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 76% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 48% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 95% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 89% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 82% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 96% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 89% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 98% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 86% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 90% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 95% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 85% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 98% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 77% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 90% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 94% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 87% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 101% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 90% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 89% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 71% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 88% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 94% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 79% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 88% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 103% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 79% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 91% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 90% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 102% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 86% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 94% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 93% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 96% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 94% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 89% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 101% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 73% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 73% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 104% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 93% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 69% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 81% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 83% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 97% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 92% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 83% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 90% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 102% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 97% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 101% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 98% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 79% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 90% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 93% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 114% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 100% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 85% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 84% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 83% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 95% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 72% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 79% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 74% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 93% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 98% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 62% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 96% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 94% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 83% Analysis Date = 01/18/17 Pct Recovery = 85% Analysis Date = 01/07/17 Pct Recovery = 85% Analysis Date = 01/07/17 Pct Recovery = 85% Analysis Date = 12/27/16 Pct Recovery = 85% Analysis Date = 12/27/16 Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/03/16 Pct Recovery = 85% Analysis Date = 11/03/16 Pct Recovery = 85% Analysis Date = 10/23/16 Pct Recovery = 85% Analysis Date = 10/23/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/19/16 Pct Recovery = 84% Analysis Date = 08/19/16 Pct Recovery = 84% Analysis Date = 08/08/16 Pct Recovery = 84% Analysis Date = 08/08/16 Pct Recovery = 84% Analysis Date = 07/28/16 Pct Recovery = 84% Analysis Date = 07/28/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 07/07/16 Pct Recovery = 84% Analysis Date = 06/26/16 Pct Recovery = 84% Analysis Date = 06/26/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 84% Analysis Date = 05/03/16 Pct Recovery = 84% Analysis Date = 05/03/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 84% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/18/15 Pct Recovery = 83% Analysis Date = 09/18/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 06/24/15 Pct Recovery = 83% Analysis Date = 06/24/15 Pct Recovery = 83% Analysis Date = 06/13/15 Pct Recovery = 83% Analysis Date = 06/13/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 05/22/15 Pct Recovery = 83% Analysis Date = 05/22/15 Pct Recovery = 83% Analysis Date = 05/11/15 Pct Recovery = 83% Analysis Date = 05/11/15 Pct Recovery = 83% Analysis Date = 05/01/15 Pct Recovery = 83% Analysis Date = 05/01/15 Pct Recovery = 83% Analysis Date = 04/20/15 Pct Recovery = 83% Analysis Date = 04/20/15 Pct Recovery = 83% Analysis Date = 04/09/15 Pct Recovery = 83% Analysis Date = 04/09/15 Pct Recovery = 83% Analysis Date = 03/29/15 Pct Recovery = 83% Analysis Date = 03/29/15 Pct Recovery = 83% Analysis Date = 03/18/15 Pct Recovery = 83% Analysis Date = 03/18/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 02/25/15 Pct Recovery = 83% Analysis Date = 02/25/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/12/15 Pct Recovery = 83% Analysis Date = 01/12/15 Pct Recovery = 83% Analysis Date = 01/02/15 Pct Recovery = 83% Analysis Date = 01/02/15 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 11/30/14 Pct Recovery = 83% Analysis Date = 11/30/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/08/14 Pct Recovery = 83% Analysis Date = 11/08/14 Pct Recovery = 83% Analysis Date = 10/29/14 Pct Recovery = 83% Analysis Date = 10/29/14 Pct Recovery = 83% Analysis Date = 10/18/14 Pct Recovery = 83% Analysis Date = 10/18/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/15/14 Pct Recovery = 83% Analysis Date = 09/15/14 Pct Recovery = 83% Analysis Date = 09/05/14 Pct Recovery = 83% Analysis Date = 09/05/14 Pct Recovery = 83% Analysis Date = 08/25/14 Pct Recovery = 83% Analysis Date = 08/25/14 Pct Recovery = 83% Analysis Date = 08/14/14 Pct Recovery = 83% Analysis Date = 08/14/14 Pct Recovery = 83% Analysis Date = 08/03/14 Pct Recovery = 83% Analysis Date = 08/03/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/23/14 Pct Recovery = 83% Analysis Date = 07/12/14 Pct Recovery = 83% Analysis Date = 07/12/14 Pct Recovery = 83% Analysis Date = 07/02/14 Pct Recovery = 84% Analysis Date = 07/02/14 Pct Recovery = 84% Analysis Date = 06/21/14 Pct Recovery = 84% Analysis Date = 06/21/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 06/10/14 Pct Recovery = 84% Analysis Date = 05/30/14 Pct Recovery = 84% Analysis Date = 05/30/14 Pct Recovery = 84% Analysis Date = 05/19/14 Pct Recovery = 84% Analysis Date = 05/19/14 Pct Recovery = 84% Analysis Date = 05/08/14 Pct Recovery = 84% Analysis Date = 05/08/14 Pct Recovery = 84% Analysis Date = 04/28/14 Pct Recovery = 84% Analysis Date = 04/28/14 Pct Recovery = 84% Analysis Date = 04/17/14 Pct Recovery = 85% Analysis Date = 04/17/14 Pct Recovery = 85% Analysis Date = 04/06/14 Pct Recovery = 85% Analysis Date = 04/06/14 Pct Recovery = 85% Analysis Date = 03/26/14 Pct Recovery = 85% Analysis Date = 03/26/14 Pct Recovery = 85% Analysis Date = 03/15/14 Pct Recovery = 85% Analysis Date = 03/15/14 Pct Recovery = 85% Analysis Date = 03/04/14 Pct Recovery = 85% Analysis Date = 03/04/14 Pct Recovery = 85% Analysis Date = 02/22/14 Pct Recovery = 85% Analysis Date = 02/22/14 Pct Recovery = 85% Analysis Date = 02/11/14 Pct Recovery = 85% Analysis Date = 02/11/14 Pct Recovery = 85% Analysis Date = 01/31/14 Pct Recovery = 86% Analysis Date = 01/31/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/09/14 Pct Recovery = 86% Analysis Date = 01/09/14 Pct Recovery = 86% Analysis Date = 12/30/13 Pct Recovery = 86% Analysis Date = 12/30/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/08/13 Pct Recovery = 86% Analysis Date = 12/08/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/16/13 Pct Recovery = 87% Analysis Date = 11/16/13 Pct Recovery = 87% Analysis Date = 11/05/13 Pct Recovery = 87% Analysis Date = 11/05/13 Pct Recovery = 87% Analysis Date = 10/26/13 Pct Recovery = 87% Analysis Date = 10/26/13 Pct Recovery = 87% Analysis Date = 10/15/13 Pct Recovery = 87% Analysis Date = 10/15/13 Pct Recovery = 87% Analysis Date = 10/04/13 Pct Recovery = 87% Analysis Date = 10/04/13 Pct Recovery = 87% Analysis Date = 09/23/13 Pct Recovery = 87% Analysis Date = 09/23/13 Pct Recovery = 87% Analysis Date = 09/12/13 Pct Recovery = 87% Analysis Date = 09/12/13 Pct Recovery = 87% Analysis Date = 09/01/13 Pct Recovery = 87% Analysis Date = 09/01/13 Pct Recovery = 87% Analysis Date = 08/22/13 Pct Recovery = 87% Analysis Date = 08/22/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 88% Analysis Date = 08/11/13 Pct Recovery = 88% Analysis Date = 07/31/13 Pct Recovery = 88% Analysis Date = 07/31/13 Pct Recovery = 88% Analysis Date = 07/20/13 Pct Recovery = 88% Analysis Date = 07/20/13 Pct Recovery = 88% Analysis Date = 07/09/13 Pct Recovery = 88% Analysis Date = 07/09/13 Pct Recovery = 88% Analysis Date = 06/29/13 Pct Recovery = 88% Analysis Date = 06/29/13 Pct Recovery = 88% Analysis Date = 06/18/13 Pct Recovery = 88% Analysis Date = 06/18/13 Pct Recovery = 88% Analysis Date = 06/07/13 Pct Recovery = 88% Analysis Date = 06/07/13 Pct Recovery = 88% Analysis Date = 05/27/13 Pct Recovery = 88% Analysis Date = 05/27/13 Pct Recovery = 88% Analysis Date = 05/16/13 Pct Recovery = 88% Analysis Date = 05/16/13 Pct Recovery = 88% Analysis Date = 05/05/13 Pct Recovery = 88% Analysis Date = 05/05/13 Pct Recovery = 88% Analysis Date = 04/25/13 Pct Recovery = 89% Analysis Date = 04/25/13 Pct Recovery = 89% Analysis Date = 04/14/13 Pct Recovery = 89% Analysis Date = 04/14/13 Pct Recovery = 89% Analysis Date = 04/03/13 Pct Recovery = 89% Analysis Date = 04/03/13 Pct Recovery = 89% Analysis Date = 03/23/13 Pct Recovery = 89% Analysis Date = 03/23/13 Pct Recovery = 89% Analysis Date = 03/12/13 Pct Recovery = 89% Analysis Date = 03/12/13 Pct Recovery = 89% Analysis Date = 03/01/13 Pct Recovery = 89% Analysis Date = 03/01/13 Pct Recovery = 89% Analysis Date = 02/19/13 Pct Recovery = 89% Analysis Date = 02/19/13 Pct Recovery = 89% Analysis Date = 02/08/13 Pct Recovery = 89% Analysis Date = 02/08/13 Pct Recovery = 89% Analysis Date = 01/28/13 Pct Recovery = 89% Analysis Date = 01/28/13 Pct Recovery = 89% Analysis Date = 01/17/13 Pct Recovery = 89% Analysis Date = 01/17/13 Pct Recovery = 89% Analysis Date = 01/06/13 Pct Recovery = 89% Analysis Date = 01/06/13 Pct Recovery = 89% Analysis Date = 12/26/12 Pct Recovery = 89% Analysis Date = 12/26/12 Pct Recovery = 89% Analysis Date = 12/16/12 Pct Recovery = 90% Analysis Date = 12/16/12 Pct Recovery = 90% Analysis Date = 12/05/12 Pct Recovery = 90% Analysis Date = 12/05/12 Pct Recovery = 90% Analysis Date = 11/24/12 Pct Recovery = 90% Analysis Date = 11/24/12 Pct Recovery = 90% Analysis Date = 11/13/12 Pct Recovery = 90% Analysis Date = 11/13/12 Pct Recovery = 90% Analysis Date = 11/02/12 Pct Recovery = 90% Analysis Date = 11/02/12 Pct Recovery = 90% Analysis Date = 10/23/12 Pct Recovery = 90% Analysis Date = 10/23/12 Pct Recovery = 90% Analysis Date = 10/12/12 Pct Recovery = 90% Analysis Date = 10/12/12 Pct Recovery = 90% Analysis Date = 10/01/12 Pct Recovery = 90% Analysis Date = 10/01/12 Pct Recovery = 90% Analysis Date = 09/20/12 Pct Recovery = 90% Analysis Date = 09/20/12 Pct Recovery = 90% Analysis Date = 09/09/12 Pct Recovery = 90% Analysis Date = 09/09/12 Pct Recovery = 90% Analysis Date = 08/29/12 Pct Recovery = 90% Analysis Date = 08/29/12 Pct Recovery = 90% Analysis Date = 08/19/12 Pct Recovery = 90% Analysis Date = 08/19/12 Pct Recovery = 90% Analysis Date = 08/08/12 Pct Recovery = 90% Analysis Date = 08/08/12 Pct Recovery = 90% Analysis Date = 07/28/12 Pct Recovery = 90% Analysis Date = 07/28/12 Pct Recovery = 90% Analysis Date = 07/17/12 Pct Recovery = 91% Analysis Date = 07/17/12 Pct Recovery = 91% Analysis Date = 07/06/12 Pct Recovery = 91% Analysis Date = 07/06/12 Pct Recovery = 91% Analysis Date = 06/25/12 Pct Recovery = 91% Analysis Date = 06/25/12 Pct Recovery = 91% Analysis Date = 06/15/12 Pct Recovery = 91% Analysis Date = 06/15/12 Pct Recovery = 91% Analysis Date = 06/04/12 Pct Recovery = 91% Analysis Date = 06/04/12 Pct Recovery = 91% Analysis Date = 05/24/12 Pct Recovery = 91% Analysis Date = 05/24/12 Pct Recovery = 91% Analysis Date = 05/13/12 Pct Recovery = 91% Analysis Date = 05/13/12 Pct Recovery = 91% Analysis Date = 05/02/12 Pct Recovery = 91% Analysis Date = 05/02/12 Pct Recovery = 91% Analysis Date = 04/22/12 Pct Recovery = 91% Analysis Date = 04/22/12 Pct Recovery = 91% Analysis Date = 04/11/12 Pct Recovery = 91% Analysis Date = 04/11/12 Pct Recovery = 91% Analysis Date = 03/31/12 Pct Recovery = 92% Analysis Date = 03/31/12 Pct Recovery = 92% Analysis Date = 03/20/12 Pct Recovery = 92% Analysis Date = 03/20/12 Pct Recovery = 92% Analysis Date = 03/09/12 Pct Recovery = 92% Analysis Date = 03/09/12 Pct Recovery = 92% Analysis Date = 02/27/12 Pct Recovery = 92% Analysis Date = 02/27/12 Pct Recovery = 92% Analysis Date = 02/17/12 Pct Recovery = 92% Analysis Date = 02/17/12 Pct Recovery = 92% Analysis Date = 02/06/12 Pct Recovery = 92% Analysis Date = 02/06/12 Pct Recovery = 92% Analysis Date = 01/26/12 Pct Recovery = 92% Analysis Date = 01/26/12 Pct Recovery = 92% Analysis Date = 01/15/12 Pct Recovery = 92% Analysis Date = 01/15/12 Pct Recovery = 92% Analysis Date = 01/04/12 Pct Recovery = 93% Analysis Date = 01/04/12 Pct Recovery = 93% Analysis Date = 12/24/11 Pct Recovery = 93% Analysis Date = 12/24/11 Pct Recovery = 93% Analysis Date = 12/14/11 Pct Recovery = 93% Analysis Date = 12/14/11 Pct Recovery = 93% Analysis Date = 12/03/11 Pct Recovery = 93% Analysis Date = 12/03/11 Pct Recovery = 93% Analysis Date = 11/22/11 Pct Recovery = 93% Analysis Date = 11/22/11 Pct Recovery = 93% Analysis Date = 11/11/11 Pct Recovery = 93% Analysis Date = 11/11/11 Pct Recovery = 93% Analysis Date = 10/31/11 Pct Recovery = 93% Analysis Date = 10/31/11 Pct Recovery = 93% Analysis Date = 10/20/11 Pct Recovery = 93% Analysis Date = 10/20/11 Pct Recovery = 93% Analysis Date = 10/10/11 Pct Recovery = 94% Analysis Date = 10/10/11 Pct Recovery = 94% Analysis Date = 09/29/11 Pct Recovery = 94% Analysis Date = 09/29/11 Pct Recovery = 94% Analysis Date = 09/18/11 Pct Recovery = 94% Analysis Date = 09/18/11 Pct Recovery = 94% Analysis Date = 09/07/11 Pct Recovery = 94% Analysis Date = 09/07/11 Pct Recovery = 94% Analysis Date = 08/27/11 Pct Recovery = 94% Analysis Date = 08/27/11 Pct Recovery = 94% Analysis Date = 08/17/11 Pct Recovery = 94% Analysis Date = 08/17/11 Pct Recovery = 94% Analysis Date = 08/06/11 Pct Recovery = 94% Analysis Date = 08/06/11 Pct Recovery = 94% Analysis Date = 07/26/11 Pct Recovery = 94% Analysis Date = 07/26/11 Pct Recovery = 94% Analysis Date = 07/15/11 Pct Recovery = 94% Analysis Date = 07/15/11 Pct Recovery = 94% Analysis Date = 07/04/11 Pct Recovery = 95% Analysis Date = 07/04/11 Pct Recovery = 95% Analysis Date = 06/23/11 Pct Recovery = 95% Analysis Date = 06/23/11 Pct Recovery = 95% Analysis Date = 06/13/11 Pct Recovery = 95% Analysis Date = 06/13/11 Pct Recovery = 95% Analysis Date = 06/02/11 Pct Recovery = 95% Analysis Date = 06/02/11 Pct Recovery = 95% Analysis Date = 05/22/11 Pct Recovery = 95% Analysis Date = 05/22/11 Pct Recovery = 95% Analysis Date = 05/11/11 Pct Recovery = 95% Analysis Date = 05/11/11 Pct Recovery = 95% Analysis Date = 04/30/11 Pct Recovery = 95% Analysis Date = 04/30/11 Pct Recovery = 95% Analysis Date = 04/19/11 Pct Recovery = 95% Analysis Date = 04/19/11 Pct Recovery = 95% Analysis Date = 04/09/11 Pct Recovery = 96% Analysis Date = 04/09/11 Pct Recovery = 96% Analysis Date = 03/29/11 Pct Recovery = 96% Analysis Date = 03/29/11 Pct Recovery = 96% Analysis Date = 03/18/11 Pct Recovery = 96% Analysis Date = 03/18/11 Pct Recovery = 96% Analysis Date = 03/07/11 Pct Recovery = 96% Analysis Date = 03/07/11 Pct Recovery = 96% Analysis Date = 02/24/11 Pct Recovery = 96% Analysis Date = 02/24/11 Pct Recovery = 96% Analysis Date = 02/14/11 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,5-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 90 88% 11% 90% 11%
Total 90 88% 11% 90% 11%

Sample Statistics
3,5-DICHLOROANILINE

Characteristic N % % Basis
Plotted 90 96% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 94 .  
False Negatives 3 3% 3 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
4-CHLORO-2-METHYLPHENOL
METHOD: 2033 , TESTIDCODE: 61633GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 49% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 49% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 73% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 46% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 60% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 64% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 60% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 79% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 66% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 62% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 73% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 75% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 69% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 60% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 50% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 72% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 49% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 73% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 64% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 45% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 39% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 58% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 61% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 70% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 61% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 69% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 78% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 65% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 66% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 62% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 89% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 76% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 74% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 81% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 64% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 55% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 77% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 61% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 34% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 51% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 55% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 45% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 55% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 58% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 75% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 83% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 82% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 50% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 45% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 66% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 58% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 43% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 83% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 76% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 66% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 69% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 73% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 76% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 46% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 59% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 61% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 77% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 59% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 66% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 82% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 90% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 59% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 85% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 45% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 67% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 68% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 75% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 62% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 62% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 52% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 68% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 55% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 55% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 68% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 56% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 74% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 46% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 45% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 62% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 01/18/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 12/27/16 Pct Recovery = 55% Analysis Date = 12/27/16 Pct Recovery = 55% Analysis Date = 12/16/16 Pct Recovery = 55% Analysis Date = 12/16/16 Pct Recovery = 55% Analysis Date = 12/05/16 Pct Recovery = 55% Analysis Date = 12/05/16 Pct Recovery = 55% Analysis Date = 11/24/16 Pct Recovery = 55% Analysis Date = 11/24/16 Pct Recovery = 55% Analysis Date = 11/14/16 Pct Recovery = 55% Analysis Date = 11/14/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 10/23/16 Pct Recovery = 55% Analysis Date = 10/23/16 Pct Recovery = 55% Analysis Date = 10/12/16 Pct Recovery = 55% Analysis Date = 10/12/16 Pct Recovery = 55% Analysis Date = 10/01/16 Pct Recovery = 55% Analysis Date = 10/01/16 Pct Recovery = 55% Analysis Date = 09/20/16 Pct Recovery = 55% Analysis Date = 09/20/16 Pct Recovery = 55% Analysis Date = 09/10/16 Pct Recovery = 55% Analysis Date = 09/10/16 Pct Recovery = 55% Analysis Date = 08/30/16 Pct Recovery = 55% Analysis Date = 08/30/16 Pct Recovery = 55% Analysis Date = 08/19/16 Pct Recovery = 55% Analysis Date = 08/19/16 Pct Recovery = 55% Analysis Date = 08/08/16 Pct Recovery = 55% Analysis Date = 08/08/16 Pct Recovery = 55% Analysis Date = 07/28/16 Pct Recovery = 55% Analysis Date = 07/28/16 Pct Recovery = 55% Analysis Date = 07/17/16 Pct Recovery = 56% Analysis Date = 07/17/16 Pct Recovery = 56% Analysis Date = 07/07/16 Pct Recovery = 56% Analysis Date = 07/07/16 Pct Recovery = 56% Analysis Date = 06/26/16 Pct Recovery = 56% Analysis Date = 06/26/16 Pct Recovery = 56% Analysis Date = 06/15/16 Pct Recovery = 56% Analysis Date = 06/15/16 Pct Recovery = 56% Analysis Date = 06/04/16 Pct Recovery = 56% Analysis Date = 06/04/16 Pct Recovery = 56% Analysis Date = 05/24/16 Pct Recovery = 56% Analysis Date = 05/24/16 Pct Recovery = 56% Analysis Date = 05/14/16 Pct Recovery = 56% Analysis Date = 05/14/16 Pct Recovery = 56% Analysis Date = 05/03/16 Pct Recovery = 56% Analysis Date = 05/03/16 Pct Recovery = 56% Analysis Date = 04/22/16 Pct Recovery = 56% Analysis Date = 04/22/16 Pct Recovery = 56% Analysis Date = 04/11/16 Pct Recovery = 56% Analysis Date = 04/11/16 Pct Recovery = 56% Analysis Date = 03/31/16 Pct Recovery = 56% Analysis Date = 03/31/16 Pct Recovery = 56% Analysis Date = 03/20/16 Pct Recovery = 56% Analysis Date = 03/20/16 Pct Recovery = 56% Analysis Date = 03/10/16 Pct Recovery = 56% Analysis Date = 03/10/16 Pct Recovery = 56% Analysis Date = 02/28/16 Pct Recovery = 56% Analysis Date = 02/28/16 Pct Recovery = 56% Analysis Date = 02/17/16 Pct Recovery = 56% Analysis Date = 02/17/16 Pct Recovery = 56% Analysis Date = 02/06/16 Pct Recovery = 56% Analysis Date = 02/06/16 Pct Recovery = 56% Analysis Date = 01/26/16 Pct Recovery = 56% Analysis Date = 01/26/16 Pct Recovery = 56% Analysis Date = 01/15/16 Pct Recovery = 56% Analysis Date = 01/15/16 Pct Recovery = 56% Analysis Date = 01/05/16 Pct Recovery = 56% Analysis Date = 01/05/16 Pct Recovery = 56% Analysis Date = 12/25/15 Pct Recovery = 57% Analysis Date = 12/25/15 Pct Recovery = 57% Analysis Date = 12/14/15 Pct Recovery = 57% Analysis Date = 12/14/15 Pct Recovery = 57% Analysis Date = 12/03/15 Pct Recovery = 57% Analysis Date = 12/03/15 Pct Recovery = 57% Analysis Date = 11/22/15 Pct Recovery = 57% Analysis Date = 11/22/15 Pct Recovery = 57% Analysis Date = 11/12/15 Pct Recovery = 57% Analysis Date = 11/12/15 Pct Recovery = 57% Analysis Date = 11/01/15 Pct Recovery = 57% Analysis Date = 11/01/15 Pct Recovery = 57% Analysis Date = 10/21/15 Pct Recovery = 57% Analysis Date = 10/21/15 Pct Recovery = 57% Analysis Date = 10/10/15 Pct Recovery = 57% Analysis Date = 10/10/15 Pct Recovery = 57% Analysis Date = 09/29/15 Pct Recovery = 57% Analysis Date = 09/29/15 Pct Recovery = 57% Analysis Date = 09/18/15 Pct Recovery = 57% Analysis Date = 09/18/15 Pct Recovery = 57% Analysis Date = 09/08/15 Pct Recovery = 57% Analysis Date = 09/08/15 Pct Recovery = 57% Analysis Date = 08/28/15 Pct Recovery = 57% Analysis Date = 08/28/15 Pct Recovery = 57% Analysis Date = 08/17/15 Pct Recovery = 57% Analysis Date = 08/17/15 Pct Recovery = 57% Analysis Date = 08/06/15 Pct Recovery = 57% Analysis Date = 08/06/15 Pct Recovery = 57% Analysis Date = 07/26/15 Pct Recovery = 57% Analysis Date = 07/26/15 Pct Recovery = 57% Analysis Date = 07/15/15 Pct Recovery = 57% Analysis Date = 07/15/15 Pct Recovery = 57% Analysis Date = 07/05/15 Pct Recovery = 58% Analysis Date = 07/05/15 Pct Recovery = 58% Analysis Date = 06/24/15 Pct Recovery = 58% Analysis Date = 06/24/15 Pct Recovery = 58% Analysis Date = 06/13/15 Pct Recovery = 58% Analysis Date = 06/13/15 Pct Recovery = 58% Analysis Date = 06/02/15 Pct Recovery = 58% Analysis Date = 06/02/15 Pct Recovery = 58% Analysis Date = 05/22/15 Pct Recovery = 58% Analysis Date = 05/22/15 Pct Recovery = 58% Analysis Date = 05/11/15 Pct Recovery = 58% Analysis Date = 05/11/15 Pct Recovery = 58% Analysis Date = 05/01/15 Pct Recovery = 58% Analysis Date = 05/01/15 Pct Recovery = 58% Analysis Date = 04/20/15 Pct Recovery = 58% Analysis Date = 04/20/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 58% Analysis Date = 04/09/15 Pct Recovery = 58% Analysis Date = 03/29/15 Pct Recovery = 58% Analysis Date = 03/29/15 Pct Recovery = 58% Analysis Date = 03/18/15 Pct Recovery = 58% Analysis Date = 03/18/15 Pct Recovery = 58% Analysis Date = 03/08/15 Pct Recovery = 58% Analysis Date = 03/08/15 Pct Recovery = 58% Analysis Date = 02/25/15 Pct Recovery = 59% Analysis Date = 02/25/15 Pct Recovery = 59% Analysis Date = 02/14/15 Pct Recovery = 59% Analysis Date = 02/14/15 Pct Recovery = 59% Analysis Date = 02/03/15 Pct Recovery = 59% Analysis Date = 02/03/15 Pct Recovery = 59% Analysis Date = 01/23/15 Pct Recovery = 59% Analysis Date = 01/23/15 Pct Recovery = 59% Analysis Date = 01/12/15 Pct Recovery = 59% Analysis Date = 01/12/15 Pct Recovery = 59% Analysis Date = 01/02/15 Pct Recovery = 59% Analysis Date = 01/02/15 Pct Recovery = 59% Analysis Date = 12/22/14 Pct Recovery = 59% Analysis Date = 12/22/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 11/30/14 Pct Recovery = 60% Analysis Date = 11/30/14 Pct Recovery = 60% Analysis Date = 11/19/14 Pct Recovery = 60% Analysis Date = 11/19/14 Pct Recovery = 60% Analysis Date = 11/08/14 Pct Recovery = 60% Analysis Date = 11/08/14 Pct Recovery = 60% Analysis Date = 10/29/14 Pct Recovery = 60% Analysis Date = 10/29/14 Pct Recovery = 60% Analysis Date = 10/18/14 Pct Recovery = 60% Analysis Date = 10/18/14 Pct Recovery = 60% Analysis Date = 10/07/14 Pct Recovery = 60% Analysis Date = 10/07/14 Pct Recovery = 60% Analysis Date = 09/26/14 Pct Recovery = 61% Analysis Date = 09/26/14 Pct Recovery = 61% Analysis Date = 09/15/14 Pct Recovery = 61% Analysis Date = 09/15/14 Pct Recovery = 61% Analysis Date = 09/05/14 Pct Recovery = 61% Analysis Date = 09/05/14 Pct Recovery = 61% Analysis Date = 08/25/14 Pct Recovery = 61% Analysis Date = 08/25/14 Pct Recovery = 61% Analysis Date = 08/14/14 Pct Recovery = 61% Analysis Date = 08/14/14 Pct Recovery = 61% Analysis Date = 08/03/14 Pct Recovery = 61% Analysis Date = 08/03/14 Pct Recovery = 61% Analysis Date = 07/23/14 Pct Recovery = 62% Analysis Date = 07/23/14 Pct Recovery = 62% Analysis Date = 07/12/14 Pct Recovery = 62% Analysis Date = 07/12/14 Pct Recovery = 62% Analysis Date = 07/02/14 Pct Recovery = 62% Analysis Date = 07/02/14 Pct Recovery = 62% Analysis Date = 06/21/14 Pct Recovery = 62% Analysis Date = 06/21/14 Pct Recovery = 62% Analysis Date = 06/10/14 Pct Recovery = 62% Analysis Date = 06/10/14 Pct Recovery = 62% Analysis Date = 05/30/14 Pct Recovery = 62% Analysis Date = 05/30/14 Pct Recovery = 62% Analysis Date = 05/19/14 Pct Recovery = 63% Analysis Date = 05/19/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 04/28/14 Pct Recovery = 63% Analysis Date = 04/28/14 Pct Recovery = 63% Analysis Date = 04/17/14 Pct Recovery = 63% Analysis Date = 04/17/14 Pct Recovery = 63% Analysis Date = 04/06/14 Pct Recovery = 63% Analysis Date = 04/06/14 Pct Recovery = 63% Analysis Date = 03/26/14 Pct Recovery = 63% Analysis Date = 03/26/14 Pct Recovery = 63% Analysis Date = 03/15/14 Pct Recovery = 64% Analysis Date = 03/15/14 Pct Recovery = 64% Analysis Date = 03/04/14 Pct Recovery = 64% Analysis Date = 03/04/14 Pct Recovery = 64% Analysis Date = 02/22/14 Pct Recovery = 64% Analysis Date = 02/22/14 Pct Recovery = 64% Analysis Date = 02/11/14 Pct Recovery = 64% Analysis Date = 02/11/14 Pct Recovery = 64% Analysis Date = 01/31/14 Pct Recovery = 64% Analysis Date = 01/31/14 Pct Recovery = 64% Analysis Date = 01/20/14 Pct Recovery = 64% Analysis Date = 01/20/14 Pct Recovery = 64% Analysis Date = 01/09/14 Pct Recovery = 65% Analysis Date = 01/09/14 Pct Recovery = 65% Analysis Date = 12/30/13 Pct Recovery = 65% Analysis Date = 12/30/13 Pct Recovery = 65% Analysis Date = 12/19/13 Pct Recovery = 65% Analysis Date = 12/19/13 Pct Recovery = 65% Analysis Date = 12/08/13 Pct Recovery = 65% Analysis Date = 12/08/13 Pct Recovery = 65% Analysis Date = 11/27/13 Pct Recovery = 65% Analysis Date = 11/27/13 Pct Recovery = 65% Analysis Date = 11/16/13 Pct Recovery = 66% Analysis Date = 11/16/13 Pct Recovery = 66% Analysis Date = 11/05/13 Pct Recovery = 66% Analysis Date = 11/05/13 Pct Recovery = 66% Analysis Date = 10/26/13 Pct Recovery = 66% Analysis Date = 10/26/13 Pct Recovery = 66% Analysis Date = 10/15/13 Pct Recovery = 66% Analysis Date = 10/15/13 Pct Recovery = 66% Analysis Date = 10/04/13 Pct Recovery = 66% Analysis Date = 10/04/13 Pct Recovery = 66% Analysis Date = 09/23/13 Pct Recovery = 66% Analysis Date = 09/23/13 Pct Recovery = 66% Analysis Date = 09/12/13 Pct Recovery = 66% Analysis Date = 09/12/13 Pct Recovery = 66% Analysis Date = 09/01/13 Pct Recovery = 66% Analysis Date = 09/01/13 Pct Recovery = 66% Analysis Date = 08/22/13 Pct Recovery = 66% Analysis Date = 08/22/13 Pct Recovery = 66% Analysis Date = 08/11/13 Pct Recovery = 67% Analysis Date = 08/11/13 Pct Recovery = 67% Analysis Date = 07/31/13 Pct Recovery = 67% Analysis Date = 07/31/13 Pct Recovery = 67% Analysis Date = 07/20/13 Pct Recovery = 67% Analysis Date = 07/20/13 Pct Recovery = 67% Analysis Date = 07/09/13 Pct Recovery = 67% Analysis Date = 07/09/13 Pct Recovery = 67% Analysis Date = 06/29/13 Pct Recovery = 67% Analysis Date = 06/29/13 Pct Recovery = 67% Analysis Date = 06/18/13 Pct Recovery = 67% Analysis Date = 06/18/13 Pct Recovery = 67% Analysis Date = 06/07/13 Pct Recovery = 67% Analysis Date = 06/07/13 Pct Recovery = 67% Analysis Date = 05/27/13 Pct Recovery = 67% Analysis Date = 05/27/13 Pct Recovery = 67% Analysis Date = 05/16/13 Pct Recovery = 67% Analysis Date = 05/16/13 Pct Recovery = 67% Analysis Date = 05/05/13 Pct Recovery = 67% Analysis Date = 05/05/13 Pct Recovery = 67% Analysis Date = 04/25/13 Pct Recovery = 67% Analysis Date = 04/25/13 Pct Recovery = 67% Analysis Date = 04/14/13 Pct Recovery = 67% Analysis Date = 04/14/13 Pct Recovery = 67% Analysis Date = 04/03/13 Pct Recovery = 67% Analysis Date = 04/03/13 Pct Recovery = 67% Analysis Date = 03/23/13 Pct Recovery = 68% Analysis Date = 03/23/13 Pct Recovery = 68% Analysis Date = 03/12/13 Pct Recovery = 68% Analysis Date = 03/12/13 Pct Recovery = 68% Analysis Date = 03/01/13 Pct Recovery = 67% Analysis Date = 03/01/13 Pct Recovery = 67% Analysis Date = 02/19/13 Pct Recovery = 67% Analysis Date = 02/19/13 Pct Recovery = 67% Analysis Date = 02/08/13 Pct Recovery = 67% Analysis Date = 02/08/13 Pct Recovery = 67% Analysis Date = 01/28/13 Pct Recovery = 67% Analysis Date = 01/28/13 Pct Recovery = 67% Analysis Date = 01/17/13 Pct Recovery = 67% Analysis Date = 01/17/13 Pct Recovery = 67% Analysis Date = 01/06/13 Pct Recovery = 67% Analysis Date = 01/06/13 Pct Recovery = 67% Analysis Date = 12/26/12 Pct Recovery = 67% Analysis Date = 12/26/12 Pct Recovery = 67% Analysis Date = 12/16/12 Pct Recovery = 67% Analysis Date = 12/16/12 Pct Recovery = 67% Analysis Date = 12/05/12 Pct Recovery = 67% Analysis Date = 12/05/12 Pct Recovery = 67% Analysis Date = 11/24/12 Pct Recovery = 67% Analysis Date = 11/24/12 Pct Recovery = 67% Analysis Date = 11/13/12 Pct Recovery = 67% Analysis Date = 11/13/12 Pct Recovery = 67% Analysis Date = 11/02/12 Pct Recovery = 67% Analysis Date = 11/02/12 Pct Recovery = 67% Analysis Date = 10/23/12 Pct Recovery = 67% Analysis Date = 10/23/12 Pct Recovery = 67% Analysis Date = 10/12/12 Pct Recovery = 67% Analysis Date = 10/12/12 Pct Recovery = 67% Analysis Date = 10/01/12 Pct Recovery = 67% Analysis Date = 10/01/12 Pct Recovery = 67% Analysis Date = 09/20/12 Pct Recovery = 67% Analysis Date = 09/20/12 Pct Recovery = 67% Analysis Date = 09/09/12 Pct Recovery = 67% Analysis Date = 09/09/12 Pct Recovery = 67% Analysis Date = 08/29/12 Pct Recovery = 67% Analysis Date = 08/29/12 Pct Recovery = 67% Analysis Date = 08/19/12 Pct Recovery = 67% Analysis Date = 08/19/12 Pct Recovery = 67% Analysis Date = 08/08/12 Pct Recovery = 67% Analysis Date = 08/08/12 Pct Recovery = 67% Analysis Date = 07/28/12 Pct Recovery = 67% Analysis Date = 07/28/12 Pct Recovery = 67% Analysis Date = 07/17/12 Pct Recovery = 67% Analysis Date = 07/17/12 Pct Recovery = 67% Analysis Date = 07/06/12 Pct Recovery = 67% Analysis Date = 07/06/12 Pct Recovery = 67% Analysis Date = 06/25/12 Pct Recovery = 67% Analysis Date = 06/25/12 Pct Recovery = 67% Analysis Date = 06/15/12 Pct Recovery = 67% Analysis Date = 06/15/12 Pct Recovery = 67% Analysis Date = 06/04/12 Pct Recovery = 67% Analysis Date = 06/04/12 Pct Recovery = 67% Analysis Date = 05/24/12 Pct Recovery = 67% Analysis Date = 05/24/12 Pct Recovery = 67% Analysis Date = 05/13/12 Pct Recovery = 67% Analysis Date = 05/13/12 Pct Recovery = 67% Analysis Date = 05/02/12 Pct Recovery = 67% Analysis Date = 05/02/12 Pct Recovery = 67% Analysis Date = 04/22/12 Pct Recovery = 67% Analysis Date = 04/22/12 Pct Recovery = 67% Analysis Date = 04/11/12 Pct Recovery = 67% Analysis Date = 04/11/12 Pct Recovery = 67% Analysis Date = 03/31/12 Pct Recovery = 67% Analysis Date = 03/31/12 Pct Recovery = 67% Analysis Date = 03/20/12 Pct Recovery = 67% Analysis Date = 03/20/12 Pct Recovery = 67% Analysis Date = 03/09/12 Pct Recovery = 67% Analysis Date = 03/09/12 Pct Recovery = 67% Analysis Date = 02/27/12 Pct Recovery = 67% Analysis Date = 02/27/12 Pct Recovery = 67% Analysis Date = 02/17/12 Pct Recovery = 67% Analysis Date = 02/17/12 Pct Recovery = 67% Analysis Date = 02/06/12 Pct Recovery = 67% Analysis Date = 02/06/12 Pct Recovery = 67% Analysis Date = 01/26/12 Pct Recovery = 68% Analysis Date = 01/26/12 Pct Recovery = 68% Analysis Date = 01/15/12 Pct Recovery = 68% Analysis Date = 01/15/12 Pct Recovery = 68% Analysis Date = 01/04/12 Pct Recovery = 68% Analysis Date = 01/04/12 Pct Recovery = 68% Analysis Date = 12/24/11 Pct Recovery = 68% Analysis Date = 12/24/11 Pct Recovery = 68% Analysis Date = 12/14/11 Pct Recovery = 68% Analysis Date = 12/14/11 Pct Recovery = 68% Analysis Date = 12/03/11 Pct Recovery = 68% Analysis Date = 12/03/11 Pct Recovery = 68% Analysis Date = 11/22/11 Pct Recovery = 68% Analysis Date = 11/22/11 Pct Recovery = 68% Analysis Date = 11/11/11 Pct Recovery = 68% Analysis Date = 11/11/11 Pct Recovery = 68% Analysis Date = 10/31/11 Pct Recovery = 68% Analysis Date = 10/31/11 Pct Recovery = 68% Analysis Date = 10/20/11 Pct Recovery = 68% Analysis Date = 10/20/11 Pct Recovery = 68% Analysis Date = 10/10/11 Pct Recovery = 68% Analysis Date = 10/10/11 Pct Recovery = 68% Analysis Date = 09/29/11 Pct Recovery = 68% Analysis Date = 09/29/11 Pct Recovery = 68% Analysis Date = 09/18/11 Pct Recovery = 68% Analysis Date = 09/18/11 Pct Recovery = 68% Analysis Date = 09/07/11 Pct Recovery = 68% Analysis Date = 09/07/11 Pct Recovery = 68% Analysis Date = 08/27/11 Pct Recovery = 68% Analysis Date = 08/27/11 Pct Recovery = 68% Analysis Date = 08/17/11 Pct Recovery = 68% Analysis Date = 08/17/11 Pct Recovery = 68% Analysis Date = 08/06/11 Pct Recovery = 68% Analysis Date = 08/06/11 Pct Recovery = 68% Analysis Date = 07/26/11 Pct Recovery = 68% Analysis Date = 07/26/11 Pct Recovery = 68% Analysis Date = 07/15/11 Pct Recovery = 69% Analysis Date = 07/15/11 Pct Recovery = 69% Analysis Date = 07/04/11 Pct Recovery = 69% Analysis Date = 07/04/11 Pct Recovery = 69% Analysis Date = 06/23/11 Pct Recovery = 69% Analysis Date = 06/23/11 Pct Recovery = 69% Analysis Date = 06/13/11 Pct Recovery = 69% Analysis Date = 06/13/11 Pct Recovery = 69% Analysis Date = 06/02/11 Pct Recovery = 69% Analysis Date = 06/02/11 Pct Recovery = 69% Analysis Date = 05/22/11 Pct Recovery = 69% Analysis Date = 05/22/11 Pct Recovery = 69% Analysis Date = 05/11/11 Pct Recovery = 69% Analysis Date = 05/11/11 Pct Recovery = 69% Analysis Date = 04/30/11 Pct Recovery = 69% Analysis Date = 04/30/11 Pct Recovery = 69% Analysis Date = 04/19/11 Pct Recovery = 69% Analysis Date = 04/19/11 Pct Recovery = 69% Analysis Date = 04/09/11 Pct Recovery = 69% Analysis Date = 04/09/11 Pct Recovery = 69% Analysis Date = 03/29/11 Pct Recovery = 69% Analysis Date = 03/29/11 Pct Recovery = 69% Analysis Date = 03/18/11 Pct Recovery = 69% Analysis Date = 03/18/11 Pct Recovery = 69% Analysis Date = 03/07/11 Pct Recovery = 69% Analysis Date = 03/07/11 Pct Recovery = 69% Analysis Date = 02/24/11 Pct Recovery = 70% Analysis Date = 02/24/11 Pct Recovery = 70% Analysis Date = 02/14/11 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLORO-2-METHYLPHENOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 64% 12% 64% 13%
Total 94 64% 12% 64% 13%

Sample Statistics
4-CHLORO-2-METHYLPHENOL

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 94 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
ACETOCHLOR
METHOD: 2033 , TESTIDCODE: 49260GCM33
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 77% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 92% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 82% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 88% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 96% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 78% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 83% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 76% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 91% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 93% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 108% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 72% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 114% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 91% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 105% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 109% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 100% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 99% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 83% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 83% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 90% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 78% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 84% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 82% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 80% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 86% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 110% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 58% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 58% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 74% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 99% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 79% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 90% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 83% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 101% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 118% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 112% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 106% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 99% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 110% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 79% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 88% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 96% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 127% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 99% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 93% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 70% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 121% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 95% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 93% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 104% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 111% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 74% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 63% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 89% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 101% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 63% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 67% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 63% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 74% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 100% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 88% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 83% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 101% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 87% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 109% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 98% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 67% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 78% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 77% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 79% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 85% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 94% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 81% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 83% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 100% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 105% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 135% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 99% Analysis Date = 01/17/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 12/27/16 Pct Recovery = 95% Analysis Date = 12/27/16 Pct Recovery = 95% Analysis Date = 12/16/16 Pct Recovery = 95% Analysis Date = 12/16/16 Pct Recovery = 95% Analysis Date = 12/05/16 Pct Recovery = 94% Analysis Date = 12/05/16 Pct Recovery = 94% Analysis Date = 11/24/16 Pct Recovery = 94% Analysis Date = 11/24/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 11/03/16 Pct Recovery = 94% Analysis Date = 10/23/16 Pct Recovery = 94% Analysis Date = 10/23/16 Pct Recovery = 94% Analysis Date = 10/12/16 Pct Recovery = 94% Analysis Date = 10/12/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/09/16 Pct Recovery = 93% Analysis Date = 09/09/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 07/28/16 Pct Recovery = 92% Analysis Date = 07/28/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 91% Analysis Date = 06/14/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/02/16 Pct Recovery = 91% Analysis Date = 05/02/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 03/30/16 Pct Recovery = 90% Analysis Date = 03/30/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 02/27/16 Pct Recovery = 90% Analysis Date = 02/27/16 Pct Recovery = 90% Analysis Date = 02/16/16 Pct Recovery = 89% Analysis Date = 02/16/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 89% Analysis Date = 01/25/16 Pct Recovery = 89% Analysis Date = 01/25/16 Pct Recovery = 89% Analysis Date = 01/14/16 Pct Recovery = 89% Analysis Date = 01/14/16 Pct Recovery = 89% Analysis Date = 01/04/16 Pct Recovery = 89% Analysis Date = 01/04/16 Pct Recovery = 89% Analysis Date = 12/24/15 Pct Recovery = 88% Analysis Date = 12/24/15 Pct Recovery = 88% Analysis Date = 12/13/15 Pct Recovery = 88% Analysis Date = 12/13/15 Pct Recovery = 88% Analysis Date = 12/02/15 Pct Recovery = 88% Analysis Date = 12/02/15 Pct Recovery = 88% Analysis Date = 11/21/15 Pct Recovery = 88% Analysis Date = 11/21/15 Pct Recovery = 88% Analysis Date = 11/10/15 Pct Recovery = 88% Analysis Date = 11/10/15 Pct Recovery = 88% Analysis Date = 10/30/15 Pct Recovery = 87% Analysis Date = 10/30/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/09/15 Pct Recovery = 87% Analysis Date = 10/09/15 Pct Recovery = 87% Analysis Date = 09/28/15 Pct Recovery = 87% Analysis Date = 09/28/15 Pct Recovery = 87% Analysis Date = 09/17/15 Pct Recovery = 87% Analysis Date = 09/17/15 Pct Recovery = 87% Analysis Date = 09/06/15 Pct Recovery = 86% Analysis Date = 09/06/15 Pct Recovery = 86% Analysis Date = 08/26/15 Pct Recovery = 86% Analysis Date = 08/26/15 Pct Recovery = 86% Analysis Date = 08/15/15 Pct Recovery = 86% Analysis Date = 08/15/15 Pct Recovery = 86% Analysis Date = 08/05/15 Pct Recovery = 86% Analysis Date = 08/05/15 Pct Recovery = 86% Analysis Date = 07/25/15 Pct Recovery = 86% Analysis Date = 07/25/15 Pct Recovery = 86% Analysis Date = 07/14/15 Pct Recovery = 85% Analysis Date = 07/14/15 Pct Recovery = 85% Analysis Date = 07/03/15 Pct Recovery = 85% Analysis Date = 07/03/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 85% Analysis Date = 06/11/15 Pct Recovery = 85% Analysis Date = 06/11/15 Pct Recovery = 85% Analysis Date = 05/31/15 Pct Recovery = 85% Analysis Date = 05/31/15 Pct Recovery = 85% Analysis Date = 05/21/15 Pct Recovery = 85% Analysis Date = 05/21/15 Pct Recovery = 85% Analysis Date = 05/10/15 Pct Recovery = 84% Analysis Date = 05/10/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/18/15 Pct Recovery = 84% Analysis Date = 04/18/15 Pct Recovery = 84% Analysis Date = 04/07/15 Pct Recovery = 84% Analysis Date = 04/07/15 Pct Recovery = 84% Analysis Date = 03/27/15 Pct Recovery = 84% Analysis Date = 03/27/15 Pct Recovery = 84% Analysis Date = 03/16/15 Pct Recovery = 84% Analysis Date = 03/16/15 Pct Recovery = 84% Analysis Date = 03/06/15 Pct Recovery = 84% Analysis Date = 03/06/15 Pct Recovery = 84% Analysis Date = 02/23/15 Pct Recovery = 84% Analysis Date = 02/23/15 Pct Recovery = 84% Analysis Date = 02/12/15 Pct Recovery = 84% Analysis Date = 02/12/15 Pct Recovery = 84% Analysis Date = 02/01/15 Pct Recovery = 84% Analysis Date = 02/01/15 Pct Recovery = 84% Analysis Date = 01/21/15 Pct Recovery = 84% Analysis Date = 01/21/15 Pct Recovery = 84% Analysis Date = 01/10/15 Pct Recovery = 84% Analysis Date = 01/10/15 Pct Recovery = 84% Analysis Date = 12/31/14 Pct Recovery = 84% Analysis Date = 12/31/14 Pct Recovery = 84% Analysis Date = 12/20/14 Pct Recovery = 84% Analysis Date = 12/20/14 Pct Recovery = 84% Analysis Date = 12/09/14 Pct Recovery = 84% Analysis Date = 12/09/14 Pct Recovery = 84% Analysis Date = 11/28/14 Pct Recovery = 84% Analysis Date = 11/28/14 Pct Recovery = 84% Analysis Date = 11/17/14 Pct Recovery = 84% Analysis Date = 11/17/14 Pct Recovery = 84% Analysis Date = 11/06/14 Pct Recovery = 84% Analysis Date = 11/06/14 Pct Recovery = 84% Analysis Date = 10/26/14 Pct Recovery = 84% Analysis Date = 10/26/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/16/14 Pct Recovery = 84% Analysis Date = 10/05/14 Pct Recovery = 84% Analysis Date = 10/05/14 Pct Recovery = 84% Analysis Date = 09/24/14 Pct Recovery = 84% Analysis Date = 09/24/14 Pct Recovery = 84% Analysis Date = 09/13/14 Pct Recovery = 84% Analysis Date = 09/13/14 Pct Recovery = 84% Analysis Date = 09/02/14 Pct Recovery = 84% Analysis Date = 09/02/14 Pct Recovery = 84% Analysis Date = 08/22/14 Pct Recovery = 84% Analysis Date = 08/22/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/11/14 Pct Recovery = 84% Analysis Date = 08/01/14 Pct Recovery = 84% Analysis Date = 08/01/14 Pct Recovery = 84% Analysis Date = 07/21/14 Pct Recovery = 84% Analysis Date = 07/21/14 Pct Recovery = 84% Analysis Date = 07/10/14 Pct Recovery = 84% Analysis Date = 07/10/14 Pct Recovery = 84% Analysis Date = 06/29/14 Pct Recovery = 84% Analysis Date = 06/29/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 05/27/14 Pct Recovery = 84% Analysis Date = 05/27/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/06/14 Pct Recovery = 84% Analysis Date = 05/06/14 Pct Recovery = 84% Analysis Date = 04/25/14 Pct Recovery = 85% Analysis Date = 04/25/14 Pct Recovery = 85% Analysis Date = 04/14/14 Pct Recovery = 85% Analysis Date = 04/14/14 Pct Recovery = 85% Analysis Date = 04/03/14 Pct Recovery = 85% Analysis Date = 04/03/14 Pct Recovery = 85% Analysis Date = 03/23/14 Pct Recovery = 85% Analysis Date = 03/23/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 85% Analysis Date = 03/02/14 Pct Recovery = 85% Analysis Date = 03/02/14 Pct Recovery = 85% Analysis Date = 02/19/14 Pct Recovery = 85% Analysis Date = 02/19/14 Pct Recovery = 85% Analysis Date = 02/08/14 Pct Recovery = 85% Analysis Date = 02/08/14 Pct Recovery = 85% Analysis Date = 01/28/14 Pct Recovery = 85% Analysis Date = 01/28/14 Pct Recovery = 85% Analysis Date = 01/17/14 Pct Recovery = 85% Analysis Date = 01/17/14 Pct Recovery = 85% Analysis Date = 01/06/14 Pct Recovery = 85% Analysis Date = 01/06/14 Pct Recovery = 85% Analysis Date = 12/26/13 Pct Recovery = 85% Analysis Date = 12/26/13 Pct Recovery = 85% Analysis Date = 12/16/13 Pct Recovery = 85% Analysis Date = 12/16/13 Pct Recovery = 85% Analysis Date = 12/05/13 Pct Recovery = 85% Analysis Date = 12/05/13 Pct Recovery = 85% Analysis Date = 11/24/13 Pct Recovery = 86% Analysis Date = 11/24/13 Pct Recovery = 86% Analysis Date = 11/13/13 Pct Recovery = 86% Analysis Date = 11/13/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 86% Analysis Date = 10/22/13 Pct Recovery = 86% Analysis Date = 10/22/13 Pct Recovery = 86% Analysis Date = 10/11/13 Pct Recovery = 86% Analysis Date = 10/11/13 Pct Recovery = 86% Analysis Date = 10/01/13 Pct Recovery = 86% Analysis Date = 10/01/13 Pct Recovery = 86% Analysis Date = 09/20/13 Pct Recovery = 87% Analysis Date = 09/20/13 Pct Recovery = 87% Analysis Date = 09/09/13 Pct Recovery = 87% Analysis Date = 09/09/13 Pct Recovery = 87% Analysis Date = 08/29/13 Pct Recovery = 87% Analysis Date = 08/29/13 Pct Recovery = 87% Analysis Date = 08/18/13 Pct Recovery = 87% Analysis Date = 08/18/13 Pct Recovery = 87% Analysis Date = 08/07/13 Pct Recovery = 88% Analysis Date = 08/07/13 Pct Recovery = 88% Analysis Date = 07/27/13 Pct Recovery = 88% Analysis Date = 07/27/13 Pct Recovery = 88% Analysis Date = 07/17/13 Pct Recovery = 88% Analysis Date = 07/17/13 Pct Recovery = 88% Analysis Date = 07/06/13 Pct Recovery = 88% Analysis Date = 07/06/13 Pct Recovery = 88% Analysis Date = 06/25/13 Pct Recovery = 88% Analysis Date = 06/25/13 Pct Recovery = 88% Analysis Date = 06/14/13 Pct Recovery = 89% Analysis Date = 06/14/13 Pct Recovery = 89% Analysis Date = 06/03/13 Pct Recovery = 89% Analysis Date = 06/03/13 Pct Recovery = 89% Analysis Date = 05/23/13 Pct Recovery = 89% Analysis Date = 05/23/13 Pct Recovery = 89% Analysis Date = 05/12/13 Pct Recovery = 89% Analysis Date = 05/12/13 Pct Recovery = 89% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 04/21/13 Pct Recovery = 90% Analysis Date = 04/21/13 Pct Recovery = 90% Analysis Date = 04/10/13 Pct Recovery = 90% Analysis Date = 04/10/13 Pct Recovery = 90% Analysis Date = 03/30/13 Pct Recovery = 90% Analysis Date = 03/30/13 Pct Recovery = 90% Analysis Date = 03/19/13 Pct Recovery = 90% Analysis Date = 03/19/13 Pct Recovery = 90% Analysis Date = 03/08/13 Pct Recovery = 91% Analysis Date = 03/08/13 Pct Recovery = 91% Analysis Date = 02/25/13 Pct Recovery = 91% Analysis Date = 02/25/13 Pct Recovery = 91% Analysis Date = 02/15/13 Pct Recovery = 91% Analysis Date = 02/15/13 Pct Recovery = 91% Analysis Date = 02/04/13 Pct Recovery = 91% Analysis Date = 02/04/13 Pct Recovery = 91% Analysis Date = 01/24/13 Pct Recovery = 91% Analysis Date = 01/24/13 Pct Recovery = 91% Analysis Date = 01/13/13 Pct Recovery = 92% Analysis Date = 01/13/13 Pct Recovery = 92% Analysis Date = 01/02/13 Pct Recovery = 92% Analysis Date = 01/02/13 Pct Recovery = 92% Analysis Date = 12/22/12 Pct Recovery = 92% Analysis Date = 12/22/12 Pct Recovery = 92% Analysis Date = 12/12/12 Pct Recovery = 92% Analysis Date = 12/12/12 Pct Recovery = 92% Analysis Date = 12/01/12 Pct Recovery = 92% Analysis Date = 12/01/12 Pct Recovery = 92% Analysis Date = 11/20/12 Pct Recovery = 92% Analysis Date = 11/20/12 Pct Recovery = 92% Analysis Date = 11/09/12 Pct Recovery = 92% Analysis Date = 11/09/12 Pct Recovery = 92% Analysis Date = 10/29/12 Pct Recovery = 92% Analysis Date = 10/29/12 Pct Recovery = 92% Analysis Date = 10/18/12 Pct Recovery = 92% Analysis Date = 10/18/12 Pct Recovery = 92% Analysis Date = 10/07/12 Pct Recovery = 93% Analysis Date = 10/07/12 Pct Recovery = 93% Analysis Date = 09/27/12 Pct Recovery = 93% Analysis Date = 09/27/12 Pct Recovery = 93% Analysis Date = 09/16/12 Pct Recovery = 93% Analysis Date = 09/16/12 Pct Recovery = 93% Analysis Date = 09/05/12 Pct Recovery = 93% Analysis Date = 09/05/12 Pct Recovery = 93% Analysis Date = 08/25/12 Pct Recovery = 93% Analysis Date = 08/25/12 Pct Recovery = 93% Analysis Date = 08/14/12 Pct Recovery = 93% Analysis Date = 08/14/12 Pct Recovery = 93% Analysis Date = 08/03/12 Pct Recovery = 93% Analysis Date = 08/03/12 Pct Recovery = 93% Analysis Date = 07/23/12 Pct Recovery = 93% Analysis Date = 07/23/12 Pct Recovery = 93% Analysis Date = 07/13/12 Pct Recovery = 93% Analysis Date = 07/13/12 Pct Recovery = 93% Analysis Date = 07/02/12 Pct Recovery = 93% Analysis Date = 07/02/12 Pct Recovery = 93% Analysis Date = 06/21/12 Pct Recovery = 93% Analysis Date = 06/21/12 Pct Recovery = 93% Analysis Date = 06/10/12 Pct Recovery = 93% Analysis Date = 06/10/12 Pct Recovery = 93% Analysis Date = 05/30/12 Pct Recovery = 93% Analysis Date = 05/30/12 Pct Recovery = 93% Analysis Date = 05/19/12 Pct Recovery = 93% Analysis Date = 05/19/12 Pct Recovery = 93% Analysis Date = 05/08/12 Pct Recovery = 93% Analysis Date = 05/08/12 Pct Recovery = 93% Analysis Date = 04/28/12 Pct Recovery = 93% Analysis Date = 04/28/12 Pct Recovery = 93% Analysis Date = 04/17/12 Pct Recovery = 93% Analysis Date = 04/17/12 Pct Recovery = 93% Analysis Date = 04/06/12 Pct Recovery = 93% Analysis Date = 04/06/12 Pct Recovery = 93% Analysis Date = 03/26/12 Pct Recovery = 93% Analysis Date = 03/26/12 Pct Recovery = 93% Analysis Date = 03/15/12 Pct Recovery = 93% Analysis Date = 03/15/12 Pct Recovery = 93% Analysis Date = 03/04/12 Pct Recovery = 93% Analysis Date = 03/04/12 Pct Recovery = 93% Analysis Date = 02/22/12 Pct Recovery = 93% Analysis Date = 02/22/12 Pct Recovery = 93% Analysis Date = 02/12/12 Pct Recovery = 93% Analysis Date = 02/12/12 Pct Recovery = 93% Analysis Date = 02/01/12 Pct Recovery = 93% Analysis Date = 02/01/12 Pct Recovery = 93% Analysis Date = 01/21/12 Pct Recovery = 93% Analysis Date = 01/21/12 Pct Recovery = 93% Analysis Date = 01/10/12 Pct Recovery = 93% Analysis Date = 01/10/12 Pct Recovery = 93% Analysis Date = 12/30/11 Pct Recovery = 93% Analysis Date = 12/30/11 Pct Recovery = 93% Analysis Date = 12/19/11 Pct Recovery = 93% Analysis Date = 12/19/11 Pct Recovery = 93% Analysis Date = 12/08/11 Pct Recovery = 93% Analysis Date = 12/08/11 Pct Recovery = 93% Analysis Date = 11/28/11 Pct Recovery = 93% Analysis Date = 11/28/11 Pct Recovery = 93% Analysis Date = 11/17/11 Pct Recovery = 93% Analysis Date = 11/17/11 Pct Recovery = 93% Analysis Date = 11/06/11 Pct Recovery = 93% Analysis Date = 11/06/11 Pct Recovery = 93% Analysis Date = 10/26/11 Pct Recovery = 93% Analysis Date = 10/26/11 Pct Recovery = 93% Analysis Date = 10/15/11 Pct Recovery = 93% Analysis Date = 10/15/11 Pct Recovery = 93% Analysis Date = 10/04/11 Pct Recovery = 93% Analysis Date = 10/04/11 Pct Recovery = 93% Analysis Date = 09/23/11 Pct Recovery = 93% Analysis Date = 09/23/11 Pct Recovery = 93% Analysis Date = 09/13/11 Pct Recovery = 93% Analysis Date = 09/13/11 Pct Recovery = 93% Analysis Date = 09/02/11 Pct Recovery = 94% Analysis Date = 09/02/11 Pct Recovery = 94% Analysis Date = 08/22/11 Pct Recovery = 94% Analysis Date = 08/22/11 Pct Recovery = 94% Analysis Date = 08/11/11 Pct Recovery = 94% Analysis Date = 08/11/11 Pct Recovery = 94% Analysis Date = 07/31/11 Pct Recovery = 94% Analysis Date = 07/31/11 Pct Recovery = 94% Analysis Date = 07/20/11 Pct Recovery = 94% Analysis Date = 07/20/11 Pct Recovery = 94% Analysis Date = 07/09/11 Pct Recovery = 94% Analysis Date = 07/09/11 Pct Recovery = 94% Analysis Date = 06/29/11 Pct Recovery = 94% Analysis Date = 06/29/11 Pct Recovery = 94% Analysis Date = 06/18/11 Pct Recovery = 94% Analysis Date = 06/18/11 Pct Recovery = 94% Analysis Date = 06/07/11 Pct Recovery = 94% Analysis Date = 06/07/11 Pct Recovery = 94% Analysis Date = 05/27/11 Pct Recovery = 94% Analysis Date = 05/27/11 Pct Recovery = 94% Analysis Date = 05/16/11 Pct Recovery = 94% Analysis Date = 05/16/11 Pct Recovery = 94% Analysis Date = 05/05/11 Pct Recovery = 94% Analysis Date = 05/05/11 Pct Recovery = 94% Analysis Date = 04/24/11 Pct Recovery = 94% Analysis Date = 04/24/11 Pct Recovery = 94% Analysis Date = 04/14/11 Pct Recovery = 94% Analysis Date = 04/14/11 Pct Recovery = 94% Analysis Date = 04/03/11 Pct Recovery = 94% Analysis Date = 04/03/11 Pct Recovery = 94% Analysis Date = 03/23/11 Pct Recovery = 94% Analysis Date = 03/23/11 Pct Recovery = 94% Analysis Date = 03/12/11 Pct Recovery = 94% Analysis Date = 03/12/11 Pct Recovery = 94% Analysis Date = 03/01/11 Pct Recovery = 94% Analysis Date = 03/01/11 Pct Recovery = 94% Analysis Date = 02/18/11 Pct Recovery = 94% Analysis Date = 02/18/11 Pct Recovery = 94% Analysis Date = 02/08/11 Pct Recovery = 94% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 95 89% 16% 88% 16%
Total 95 89% 16% 88% 16%

Sample Statistics
ACETOCHLOR

Characteristic N % % Basis
Plotted 95 100% Spiked
Estimated Values 6 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 95 .  
False Negatives 0 0% 0 out of 95
Not Spiked 74 .  
False Positives 1 1% 1 out of 74

BQS OBSP Determination:
ALACHLOR
METHOD: 2033 , TESTIDCODE: 46342GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 84% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 98% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 86% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 93% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 95% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 89% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 92% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 95% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 89% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 69% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 93% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 116% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 76% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 86% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 89% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 85% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 93% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 98% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 84% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 102% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 113% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 77% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 93% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 78% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 80% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 88% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 93% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 99% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 86% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 107% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 73% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 110% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 86% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 82% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 84% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 131% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 109% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 80% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 76% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 97% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 107% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 99% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 81% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 73% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 91% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 89% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 93% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 111% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 69% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 69% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 82% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 110% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 89% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 102% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 106% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 87% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 100% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 83% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 76% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 81% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 82% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 90% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 89% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 102% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 88% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 101% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 99% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 113% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 120% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 119% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 126% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 130% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 106% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 104% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 124% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 105% Analysis Date = 12/20/16 Pct Recovery = 87% Analysis Date = 12/09/16 Pct Recovery = 87% Analysis Date = 12/09/16 Pct Recovery = 87% Analysis Date = 11/28/16 Pct Recovery = 87% Analysis Date = 11/28/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/07/16 Pct Recovery = 87% Analysis Date = 11/07/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/16/16 Pct Recovery = 87% Analysis Date = 10/16/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 10/06/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/04/16 Pct Recovery = 88% Analysis Date = 09/04/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/13/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 08/03/16 Pct Recovery = 88% Analysis Date = 07/23/16 Pct Recovery = 88% Analysis Date = 07/23/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/12/16 Pct Recovery = 88% Analysis Date = 07/02/16 Pct Recovery = 88% Analysis Date = 07/02/16 Pct Recovery = 88% Analysis Date = 06/21/16 Pct Recovery = 88% Analysis Date = 06/21/16 Pct Recovery = 88% Analysis Date = 06/10/16 Pct Recovery = 88% Analysis Date = 06/10/16 Pct Recovery = 88% Analysis Date = 05/31/16 Pct Recovery = 88% Analysis Date = 05/31/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/18/16 Pct Recovery = 88% Analysis Date = 04/18/16 Pct Recovery = 88% Analysis Date = 04/07/16 Pct Recovery = 88% Analysis Date = 04/07/16 Pct Recovery = 88% Analysis Date = 03/28/16 Pct Recovery = 88% Analysis Date = 03/28/16 Pct Recovery = 88% Analysis Date = 03/17/16 Pct Recovery = 88% Analysis Date = 03/17/16 Pct Recovery = 88% Analysis Date = 03/06/16 Pct Recovery = 88% Analysis Date = 03/06/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/14/16 Pct Recovery = 89% Analysis Date = 02/14/16 Pct Recovery = 89% Analysis Date = 02/03/16 Pct Recovery = 89% Analysis Date = 02/03/16 Pct Recovery = 89% Analysis Date = 01/23/16 Pct Recovery = 89% Analysis Date = 01/23/16 Pct Recovery = 89% Analysis Date = 01/13/16 Pct Recovery = 89% Analysis Date = 01/13/16 Pct Recovery = 89% Analysis Date = 01/02/16 Pct Recovery = 89% Analysis Date = 01/02/16 Pct Recovery = 89% Analysis Date = 12/22/15 Pct Recovery = 89% Analysis Date = 12/22/15 Pct Recovery = 89% Analysis Date = 12/12/15 Pct Recovery = 89% Analysis Date = 12/12/15 Pct Recovery = 89% Analysis Date = 12/01/15 Pct Recovery = 89% Analysis Date = 12/01/15 Pct Recovery = 89% Analysis Date = 11/20/15 Pct Recovery = 89% Analysis Date = 11/20/15 Pct Recovery = 89% Analysis Date = 11/10/15 Pct Recovery = 89% Analysis Date = 11/10/15 Pct Recovery = 89% Analysis Date = 10/30/15 Pct Recovery = 89% Analysis Date = 10/30/15 Pct Recovery = 89% Analysis Date = 10/19/15 Pct Recovery = 89% Analysis Date = 10/19/15 Pct Recovery = 89% Analysis Date = 10/09/15 Pct Recovery = 89% Analysis Date = 10/09/15 Pct Recovery = 89% Analysis Date = 09/28/15 Pct Recovery = 89% Analysis Date = 09/28/15 Pct Recovery = 89% Analysis Date = 09/17/15 Pct Recovery = 89% Analysis Date = 09/17/15 Pct Recovery = 89% Analysis Date = 09/07/15 Pct Recovery = 89% Analysis Date = 09/07/15 Pct Recovery = 89% Analysis Date = 08/27/15 Pct Recovery = 89% Analysis Date = 08/27/15 Pct Recovery = 89% Analysis Date = 08/16/15 Pct Recovery = 89% Analysis Date = 08/16/15 Pct Recovery = 89% Analysis Date = 08/06/15 Pct Recovery = 89% Analysis Date = 08/06/15 Pct Recovery = 89% Analysis Date = 07/26/15 Pct Recovery = 89% Analysis Date = 07/26/15 Pct Recovery = 89% Analysis Date = 07/15/15 Pct Recovery = 89% Analysis Date = 07/15/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 07/05/15 Pct Recovery = 89% Analysis Date = 06/24/15 Pct Recovery = 89% Analysis Date = 06/24/15 Pct Recovery = 89% Analysis Date = 06/13/15 Pct Recovery = 90% Analysis Date = 06/13/15 Pct Recovery = 90% Analysis Date = 06/02/15 Pct Recovery = 90% Analysis Date = 06/02/15 Pct Recovery = 90% Analysis Date = 05/23/15 Pct Recovery = 90% Analysis Date = 05/23/15 Pct Recovery = 90% Analysis Date = 05/12/15 Pct Recovery = 90% Analysis Date = 05/12/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 04/21/15 Pct Recovery = 90% Analysis Date = 04/21/15 Pct Recovery = 90% Analysis Date = 04/10/15 Pct Recovery = 90% Analysis Date = 04/10/15 Pct Recovery = 90% Analysis Date = 03/30/15 Pct Recovery = 90% Analysis Date = 03/30/15 Pct Recovery = 90% Analysis Date = 03/20/15 Pct Recovery = 90% Analysis Date = 03/20/15 Pct Recovery = 90% Analysis Date = 03/09/15 Pct Recovery = 90% Analysis Date = 03/09/15 Pct Recovery = 90% Analysis Date = 02/26/15 Pct Recovery = 90% Analysis Date = 02/26/15 Pct Recovery = 90% Analysis Date = 02/16/15 Pct Recovery = 91% Analysis Date = 02/16/15 Pct Recovery = 91% Analysis Date = 02/05/15 Pct Recovery = 91% Analysis Date = 02/05/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/15/15 Pct Recovery = 91% Analysis Date = 01/15/15 Pct Recovery = 91% Analysis Date = 01/04/15 Pct Recovery = 91% Analysis Date = 01/04/15 Pct Recovery = 91% Analysis Date = 12/24/14 Pct Recovery = 91% Analysis Date = 12/24/14 Pct Recovery = 91% Analysis Date = 12/14/14 Pct Recovery = 91% Analysis Date = 12/14/14 Pct Recovery = 91% Analysis Date = 12/03/14 Pct Recovery = 92% Analysis Date = 12/03/14 Pct Recovery = 92% Analysis Date = 11/22/14 Pct Recovery = 92% Analysis Date = 11/22/14 Pct Recovery = 92% Analysis Date = 11/12/14 Pct Recovery = 92% Analysis Date = 11/12/14 Pct Recovery = 92% Analysis Date = 11/01/14 Pct Recovery = 92% Analysis Date = 11/01/14 Pct Recovery = 92% Analysis Date = 10/21/14 Pct Recovery = 92% Analysis Date = 10/21/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 10/11/14 Pct Recovery = 92% Analysis Date = 09/30/14 Pct Recovery = 92% Analysis Date = 09/30/14 Pct Recovery = 92% Analysis Date = 09/19/14 Pct Recovery = 93% Analysis Date = 09/19/14 Pct Recovery = 93% Analysis Date = 09/08/14 Pct Recovery = 93% Analysis Date = 09/08/14 Pct Recovery = 93% Analysis Date = 08/29/14 Pct Recovery = 93% Analysis Date = 08/29/14 Pct Recovery = 93% Analysis Date = 08/18/14 Pct Recovery = 93% Analysis Date = 08/18/14 Pct Recovery = 93% Analysis Date = 08/07/14 Pct Recovery = 93% Analysis Date = 08/07/14 Pct Recovery = 93% Analysis Date = 07/28/14 Pct Recovery = 93% Analysis Date = 07/28/14 Pct Recovery = 93% Analysis Date = 07/17/14 Pct Recovery = 93% Analysis Date = 07/17/14 Pct Recovery = 93% Analysis Date = 07/06/14 Pct Recovery = 93% Analysis Date = 07/06/14 Pct Recovery = 93% Analysis Date = 06/26/14 Pct Recovery = 93% Analysis Date = 06/26/14 Pct Recovery = 93% Analysis Date = 06/15/14 Pct Recovery = 94% Analysis Date = 06/15/14 Pct Recovery = 94% Analysis Date = 06/04/14 Pct Recovery = 94% Analysis Date = 06/04/14 Pct Recovery = 94% Analysis Date = 05/25/14 Pct Recovery = 94% Analysis Date = 05/25/14 Pct Recovery = 94% Analysis Date = 05/14/14 Pct Recovery = 94% Analysis Date = 05/14/14 Pct Recovery = 94% Analysis Date = 05/03/14 Pct Recovery = 94% Analysis Date = 05/03/14 Pct Recovery = 94% Analysis Date = 04/23/14 Pct Recovery = 94% Analysis Date = 04/23/14 Pct Recovery = 94% Analysis Date = 04/12/14 Pct Recovery = 94% Analysis Date = 04/12/14 Pct Recovery = 94% Analysis Date = 04/01/14 Pct Recovery = 94% Analysis Date = 04/01/14 Pct Recovery = 94% Analysis Date = 03/22/14 Pct Recovery = 94% Analysis Date = 03/22/14 Pct Recovery = 94% Analysis Date = 03/11/14 Pct Recovery = 94% Analysis Date = 03/11/14 Pct Recovery = 94% Analysis Date = 02/28/14 Pct Recovery = 94% Analysis Date = 02/28/14 Pct Recovery = 94% Analysis Date = 02/18/14 Pct Recovery = 95% Analysis Date = 02/18/14 Pct Recovery = 95% Analysis Date = 02/07/14 Pct Recovery = 95% Analysis Date = 02/07/14 Pct Recovery = 95% Analysis Date = 01/27/14 Pct Recovery = 95% Analysis Date = 01/27/14 Pct Recovery = 95% Analysis Date = 01/17/14 Pct Recovery = 95% Analysis Date = 01/17/14 Pct Recovery = 95% Analysis Date = 01/06/14 Pct Recovery = 95% Analysis Date = 01/06/14 Pct Recovery = 95% Analysis Date = 12/26/13 Pct Recovery = 95% Analysis Date = 12/26/13 Pct Recovery = 95% Analysis Date = 12/15/13 Pct Recovery = 95% Analysis Date = 12/15/13 Pct Recovery = 95% Analysis Date = 12/05/13 Pct Recovery = 95% Analysis Date = 12/05/13 Pct Recovery = 95% Analysis Date = 11/24/13 Pct Recovery = 95% Analysis Date = 11/24/13 Pct Recovery = 95% Analysis Date = 11/13/13 Pct Recovery = 96% Analysis Date = 11/13/13 Pct Recovery = 96% Analysis Date = 11/03/13 Pct Recovery = 96% Analysis Date = 11/03/13 Pct Recovery = 96% Analysis Date = 10/23/13 Pct Recovery = 96% Analysis Date = 10/23/13 Pct Recovery = 96% Analysis Date = 10/12/13 Pct Recovery = 96% Analysis Date = 10/12/13 Pct Recovery = 96% Analysis Date = 10/02/13 Pct Recovery = 96% Analysis Date = 10/02/13 Pct Recovery = 96% Analysis Date = 09/21/13 Pct Recovery = 96% Analysis Date = 09/21/13 Pct Recovery = 96% Analysis Date = 09/10/13 Pct Recovery = 96% Analysis Date = 09/10/13 Pct Recovery = 96% Analysis Date = 08/31/13 Pct Recovery = 96% Analysis Date = 08/31/13 Pct Recovery = 96% Analysis Date = 08/20/13 Pct Recovery = 96% Analysis Date = 08/20/13 Pct Recovery = 96% Analysis Date = 08/09/13 Pct Recovery = 96% Analysis Date = 08/09/13 Pct Recovery = 96% Analysis Date = 07/30/13 Pct Recovery = 96% Analysis Date = 07/30/13 Pct Recovery = 96% Analysis Date = 07/19/13 Pct Recovery = 96% Analysis Date = 07/19/13 Pct Recovery = 96% Analysis Date = 07/08/13 Pct Recovery = 96% Analysis Date = 07/08/13 Pct Recovery = 96% Analysis Date = 06/28/13 Pct Recovery = 96% Analysis Date = 06/28/13 Pct Recovery = 96% Analysis Date = 06/17/13 Pct Recovery = 96% Analysis Date = 06/17/13 Pct Recovery = 96% Analysis Date = 06/06/13 Pct Recovery = 96% Analysis Date = 06/06/13 Pct Recovery = 96% Analysis Date = 05/27/13 Pct Recovery = 96% Analysis Date = 05/27/13 Pct Recovery = 96% Analysis Date = 05/16/13 Pct Recovery = 96% Analysis Date = 05/16/13 Pct Recovery = 96% Analysis Date = 05/05/13 Pct Recovery = 96% Analysis Date = 05/05/13 Pct Recovery = 96% Analysis Date = 04/25/13 Pct Recovery = 96% Analysis Date = 04/25/13 Pct Recovery = 96% Analysis Date = 04/14/13 Pct Recovery = 96% Analysis Date = 04/14/13 Pct Recovery = 96% Analysis Date = 04/03/13 Pct Recovery = 96% Analysis Date = 04/03/13 Pct Recovery = 96% Analysis Date = 03/23/13 Pct Recovery = 96% Analysis Date = 03/23/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/02/13 Pct Recovery = 95% Analysis Date = 03/02/13 Pct Recovery = 95% Analysis Date = 02/19/13 Pct Recovery = 95% Analysis Date = 02/19/13 Pct Recovery = 95% Analysis Date = 02/09/13 Pct Recovery = 95% Analysis Date = 02/09/13 Pct Recovery = 95% Analysis Date = 01/29/13 Pct Recovery = 95% Analysis Date = 01/29/13 Pct Recovery = 95% Analysis Date = 01/18/13 Pct Recovery = 95% Analysis Date = 01/18/13 Pct Recovery = 95% Analysis Date = 01/08/13 Pct Recovery = 94% Analysis Date = 01/08/13 Pct Recovery = 94% Analysis Date = 12/28/12 Pct Recovery = 94% Analysis Date = 12/28/12 Pct Recovery = 94% Analysis Date = 12/17/12 Pct Recovery = 94% Analysis Date = 12/17/12 Pct Recovery = 94% Analysis Date = 12/07/12 Pct Recovery = 94% Analysis Date = 12/07/12 Pct Recovery = 94% Analysis Date = 11/26/12 Pct Recovery = 94% Analysis Date = 11/26/12 Pct Recovery = 94% Analysis Date = 11/15/12 Pct Recovery = 93% Analysis Date = 11/15/12 Pct Recovery = 93% Analysis Date = 11/05/12 Pct Recovery = 93% Analysis Date = 11/05/12 Pct Recovery = 93% Analysis Date = 10/25/12 Pct Recovery = 93% Analysis Date = 10/25/12 Pct Recovery = 93% Analysis Date = 10/14/12 Pct Recovery = 93% Analysis Date = 10/14/12 Pct Recovery = 93% Analysis Date = 10/04/12 Pct Recovery = 93% Analysis Date = 10/04/12 Pct Recovery = 93% Analysis Date = 09/23/12 Pct Recovery = 93% Analysis Date = 09/23/12 Pct Recovery = 93% Analysis Date = 09/12/12 Pct Recovery = 93% Analysis Date = 09/12/12 Pct Recovery = 93% Analysis Date = 09/02/12 Pct Recovery = 93% Analysis Date = 09/02/12 Pct Recovery = 93% Analysis Date = 08/22/12 Pct Recovery = 93% Analysis Date = 08/22/12 Pct Recovery = 93% Analysis Date = 08/11/12 Pct Recovery = 93% Analysis Date = 08/11/12 Pct Recovery = 93% Analysis Date = 08/01/12 Pct Recovery = 93% Analysis Date = 08/01/12 Pct Recovery = 93% Analysis Date = 07/21/12 Pct Recovery = 93% Analysis Date = 07/21/12 Pct Recovery = 93% Analysis Date = 07/10/12 Pct Recovery = 93% Analysis Date = 07/10/12 Pct Recovery = 93% Analysis Date = 06/29/12 Pct Recovery = 93% Analysis Date = 06/29/12 Pct Recovery = 93% Analysis Date = 06/19/12 Pct Recovery = 93% Analysis Date = 06/19/12 Pct Recovery = 93% Analysis Date = 06/08/12 Pct Recovery = 93% Analysis Date = 06/08/12 Pct Recovery = 93% Analysis Date = 05/28/12 Pct Recovery = 93% Analysis Date = 05/28/12 Pct Recovery = 93% Analysis Date = 05/18/12 Pct Recovery = 92% Analysis Date = 05/18/12 Pct Recovery = 92% Analysis Date = 05/07/12 Pct Recovery = 92% Analysis Date = 05/07/12 Pct Recovery = 92% Analysis Date = 04/26/12 Pct Recovery = 92% Analysis Date = 04/26/12 Pct Recovery = 92% Analysis Date = 04/16/12 Pct Recovery = 92% Analysis Date = 04/16/12 Pct Recovery = 92% Analysis Date = 04/05/12 Pct Recovery = 92% Analysis Date = 04/05/12 Pct Recovery = 92% Analysis Date = 03/25/12 Pct Recovery = 92% Analysis Date = 03/25/12 Pct Recovery = 92% Analysis Date = 03/15/12 Pct Recovery = 92% Analysis Date = 03/15/12 Pct Recovery = 92% Analysis Date = 03/04/12 Pct Recovery = 92% Analysis Date = 03/04/12 Pct Recovery = 92% Analysis Date = 02/22/12 Pct Recovery = 92% Analysis Date = 02/22/12 Pct Recovery = 92% Analysis Date = 02/12/12 Pct Recovery = 92% Analysis Date = 02/12/12 Pct Recovery = 92% Analysis Date = 02/01/12 Pct Recovery = 92% Analysis Date = 02/01/12 Pct Recovery = 92% Analysis Date = 01/21/12 Pct Recovery = 92% Analysis Date = 01/21/12 Pct Recovery = 92% Analysis Date = 01/11/12 Pct Recovery = 92% Analysis Date = 01/11/12 Pct Recovery = 92% Analysis Date = 12/31/11 Pct Recovery = 92% Analysis Date = 12/31/11 Pct Recovery = 92% Analysis Date = 12/20/11 Pct Recovery = 92% Analysis Date = 12/20/11 Pct Recovery = 92% Analysis Date = 12/10/11 Pct Recovery = 92% Analysis Date = 12/10/11 Pct Recovery = 92% Analysis Date = 11/29/11 Pct Recovery = 92% Analysis Date = 11/29/11 Pct Recovery = 92% Analysis Date = 11/18/11 Pct Recovery = 92% Analysis Date = 11/18/11 Pct Recovery = 92% Analysis Date = 11/08/11 Pct Recovery = 92% Analysis Date = 11/08/11 Pct Recovery = 92% Analysis Date = 10/28/11 Pct Recovery = 92% Analysis Date = 10/28/11 Pct Recovery = 92% Analysis Date = 10/17/11 Pct Recovery = 92% Analysis Date = 10/17/11 Pct Recovery = 92% Analysis Date = 10/06/11 Pct Recovery = 92% Analysis Date = 10/06/11 Pct Recovery = 92% Analysis Date = 09/26/11 Pct Recovery = 92% Analysis Date = 09/26/11 Pct Recovery = 92% Analysis Date = 09/15/11 Pct Recovery = 92% Analysis Date = 09/15/11 Pct Recovery = 92% Analysis Date = 09/04/11 Pct Recovery = 92% Analysis Date = 09/04/11 Pct Recovery = 92% Analysis Date = 08/25/11 Pct Recovery = 92% Analysis Date = 08/25/11 Pct Recovery = 92% Analysis Date = 08/14/11 Pct Recovery = 92% Analysis Date = 08/14/11 Pct Recovery = 92% Analysis Date = 08/03/11 Pct Recovery = 92% Analysis Date = 08/03/11 Pct Recovery = 92% Analysis Date = 07/24/11 Pct Recovery = 92% Analysis Date = 07/24/11 Pct Recovery = 92% Analysis Date = 07/13/11 Pct Recovery = 92% Analysis Date = 07/13/11 Pct Recovery = 92% Analysis Date = 07/02/11 Pct Recovery = 92% Analysis Date = 07/02/11 Pct Recovery = 92% Analysis Date = 06/22/11 Pct Recovery = 92% Analysis Date = 06/22/11 Pct Recovery = 92% Analysis Date = 06/11/11 Pct Recovery = 92% Analysis Date = 06/11/11 Pct Recovery = 92% Analysis Date = 05/31/11 Pct Recovery = 92% Analysis Date = 05/31/11 Pct Recovery = 92% Analysis Date = 05/21/11 Pct Recovery = 92% Analysis Date = 05/21/11 Pct Recovery = 92% Analysis Date = 05/10/11 Pct Recovery = 92% Analysis Date = 05/10/11 Pct Recovery = 92% Analysis Date = 04/29/11 Pct Recovery = 92% Analysis Date = 04/29/11 Pct Recovery = 92% Analysis Date = 04/19/11 Pct Recovery = 92% Analysis Date = 04/19/11 Pct Recovery = 92% Analysis Date = 04/08/11 Pct Recovery = 92% Analysis Date = 04/08/11 Pct Recovery = 92% Analysis Date = 03/28/11 Pct Recovery = 92% Analysis Date = 03/28/11 Pct Recovery = 92% Analysis Date = 03/18/11 Pct Recovery = 92% Analysis Date = 03/18/11 Pct Recovery = 92% Analysis Date = 03/07/11 Pct Recovery = 93% Analysis Date = 03/07/11 Pct Recovery = 93% Analysis Date = 02/24/11 Pct Recovery = 93% Analysis Date = 02/24/11 Pct Recovery = 93% Analysis Date = 02/14/11 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 92% 14% 90% 13%
Total 94 92% 14% 90% 13%

Sample Statistics
ALACHLOR

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
ALPHA-ENDOSULFAN (ENDOSULFAN I)
METHOD: 2033 , TESTIDCODE: 34362GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 84% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 93% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 86% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 87% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 81% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 90% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 88% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 85% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 64% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 108% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 100% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 80% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 98% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 86% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 67% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 68% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 75% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 101% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 73% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 66% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 77% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 76% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 109% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 83% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 97% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 83% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 81% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 86% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 97% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 68% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 115% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 79% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 108% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 84% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 105% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 85% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 86% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 90% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 97% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 79% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 51% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 87% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 107% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 135% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 95% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 96% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 104% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 94% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 82% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 84% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 96% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 102% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 100% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 86% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 83% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 64% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 91% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 100% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 64% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 130% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 81% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 92% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 97% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 96% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 86% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 74% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 90% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 84% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 126% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 106% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 90% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 110% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 101% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 94% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 92% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 102% Analysis Date = 01/18/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/16/16 Pct Recovery = 90% Analysis Date = 12/16/16 Pct Recovery = 90% Analysis Date = 12/05/16 Pct Recovery = 90% Analysis Date = 12/05/16 Pct Recovery = 90% Analysis Date = 11/24/16 Pct Recovery = 90% Analysis Date = 11/24/16 Pct Recovery = 90% Analysis Date = 11/14/16 Pct Recovery = 90% Analysis Date = 11/14/16 Pct Recovery = 90% Analysis Date = 11/03/16 Pct Recovery = 90% Analysis Date = 11/03/16 Pct Recovery = 90% Analysis Date = 10/23/16 Pct Recovery = 90% Analysis Date = 10/23/16 Pct Recovery = 90% Analysis Date = 10/12/16 Pct Recovery = 89% Analysis Date = 10/12/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 05/24/16 Pct Recovery = 89% Analysis Date = 05/24/16 Pct Recovery = 89% Analysis Date = 05/14/16 Pct Recovery = 89% Analysis Date = 05/14/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/11/16 Pct Recovery = 89% Analysis Date = 04/11/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 89% Analysis Date = 03/20/16 Pct Recovery = 89% Analysis Date = 03/20/16 Pct Recovery = 89% Analysis Date = 03/10/16 Pct Recovery = 89% Analysis Date = 03/10/16 Pct Recovery = 89% Analysis Date = 02/28/16 Pct Recovery = 89% Analysis Date = 02/28/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 89% Analysis Date = 02/17/16 Pct Recovery = 89% Analysis Date = 02/06/16 Pct Recovery = 89% Analysis Date = 02/06/16 Pct Recovery = 89% Analysis Date = 01/26/16 Pct Recovery = 89% Analysis Date = 01/26/16 Pct Recovery = 89% Analysis Date = 01/15/16 Pct Recovery = 89% Analysis Date = 01/15/16 Pct Recovery = 89% Analysis Date = 01/05/16 Pct Recovery = 89% Analysis Date = 01/05/16 Pct Recovery = 89% Analysis Date = 12/25/15 Pct Recovery = 89% Analysis Date = 12/25/15 Pct Recovery = 89% Analysis Date = 12/14/15 Pct Recovery = 89% Analysis Date = 12/14/15 Pct Recovery = 89% Analysis Date = 12/03/15 Pct Recovery = 89% Analysis Date = 12/03/15 Pct Recovery = 89% Analysis Date = 11/22/15 Pct Recovery = 89% Analysis Date = 11/22/15 Pct Recovery = 89% Analysis Date = 11/12/15 Pct Recovery = 89% Analysis Date = 11/12/15 Pct Recovery = 89% Analysis Date = 11/01/15 Pct Recovery = 89% Analysis Date = 11/01/15 Pct Recovery = 89% Analysis Date = 10/21/15 Pct Recovery = 89% Analysis Date = 10/21/15 Pct Recovery = 89% Analysis Date = 10/10/15 Pct Recovery = 88% Analysis Date = 10/10/15 Pct Recovery = 88% Analysis Date = 09/29/15 Pct Recovery = 88% Analysis Date = 09/29/15 Pct Recovery = 88% Analysis Date = 09/18/15 Pct Recovery = 88% Analysis Date = 09/18/15 Pct Recovery = 88% Analysis Date = 09/08/15 Pct Recovery = 88% Analysis Date = 09/08/15 Pct Recovery = 88% Analysis Date = 08/28/15 Pct Recovery = 88% Analysis Date = 08/28/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/17/15 Pct Recovery = 88% Analysis Date = 08/06/15 Pct Recovery = 88% Analysis Date = 08/06/15 Pct Recovery = 88% Analysis Date = 07/26/15 Pct Recovery = 88% Analysis Date = 07/26/15 Pct Recovery = 88% Analysis Date = 07/15/15 Pct Recovery = 88% Analysis Date = 07/15/15 Pct Recovery = 88% Analysis Date = 07/05/15 Pct Recovery = 88% Analysis Date = 07/05/15 Pct Recovery = 88% Analysis Date = 06/24/15 Pct Recovery = 88% Analysis Date = 06/24/15 Pct Recovery = 88% Analysis Date = 06/13/15 Pct Recovery = 88% Analysis Date = 06/13/15 Pct Recovery = 88% Analysis Date = 06/02/15 Pct Recovery = 88% Analysis Date = 06/02/15 Pct Recovery = 88% Analysis Date = 05/22/15 Pct Recovery = 88% Analysis Date = 05/22/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 04/20/15 Pct Recovery = 88% Analysis Date = 04/20/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 03/29/15 Pct Recovery = 88% Analysis Date = 03/29/15 Pct Recovery = 88% Analysis Date = 03/18/15 Pct Recovery = 88% Analysis Date = 03/18/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 02/25/15 Pct Recovery = 88% Analysis Date = 02/25/15 Pct Recovery = 88% Analysis Date = 02/14/15 Pct Recovery = 88% Analysis Date = 02/14/15 Pct Recovery = 88% Analysis Date = 02/03/15 Pct Recovery = 88% Analysis Date = 02/03/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/12/15 Pct Recovery = 88% Analysis Date = 01/12/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/11/14 Pct Recovery = 89% Analysis Date = 12/11/14 Pct Recovery = 89% Analysis Date = 11/30/14 Pct Recovery = 89% Analysis Date = 11/30/14 Pct Recovery = 89% Analysis Date = 11/19/14 Pct Recovery = 89% Analysis Date = 11/19/14 Pct Recovery = 89% Analysis Date = 11/08/14 Pct Recovery = 89% Analysis Date = 11/08/14 Pct Recovery = 89% Analysis Date = 10/29/14 Pct Recovery = 89% Analysis Date = 10/29/14 Pct Recovery = 89% Analysis Date = 10/18/14 Pct Recovery = 89% Analysis Date = 10/18/14 Pct Recovery = 89% Analysis Date = 10/07/14 Pct Recovery = 89% Analysis Date = 10/07/14 Pct Recovery = 89% Analysis Date = 09/26/14 Pct Recovery = 89% Analysis Date = 09/26/14 Pct Recovery = 89% Analysis Date = 09/15/14 Pct Recovery = 89% Analysis Date = 09/15/14 Pct Recovery = 89% Analysis Date = 09/05/14 Pct Recovery = 89% Analysis Date = 09/05/14 Pct Recovery = 89% Analysis Date = 08/25/14 Pct Recovery = 89% Analysis Date = 08/25/14 Pct Recovery = 89% Analysis Date = 08/14/14 Pct Recovery = 89% Analysis Date = 08/14/14 Pct Recovery = 89% Analysis Date = 08/03/14 Pct Recovery = 89% Analysis Date = 08/03/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/12/14 Pct Recovery = 89% Analysis Date = 07/12/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 89% Analysis Date = 06/21/14 Pct Recovery = 89% Analysis Date = 06/21/14 Pct Recovery = 89% Analysis Date = 06/10/14 Pct Recovery = 89% Analysis Date = 06/10/14 Pct Recovery = 89% Analysis Date = 05/30/14 Pct Recovery = 89% Analysis Date = 05/30/14 Pct Recovery = 89% Analysis Date = 05/19/14 Pct Recovery = 89% Analysis Date = 05/19/14 Pct Recovery = 89% Analysis Date = 05/08/14 Pct Recovery = 89% Analysis Date = 05/08/14 Pct Recovery = 89% Analysis Date = 04/28/14 Pct Recovery = 89% Analysis Date = 04/28/14 Pct Recovery = 89% Analysis Date = 04/17/14 Pct Recovery = 89% Analysis Date = 04/17/14 Pct Recovery = 89% Analysis Date = 04/06/14 Pct Recovery = 89% Analysis Date = 04/06/14 Pct Recovery = 89% Analysis Date = 03/26/14 Pct Recovery = 89% Analysis Date = 03/26/14 Pct Recovery = 89% Analysis Date = 03/15/14 Pct Recovery = 89% Analysis Date = 03/15/14 Pct Recovery = 89% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 02/22/14 Pct Recovery = 89% Analysis Date = 02/22/14 Pct Recovery = 89% Analysis Date = 02/11/14 Pct Recovery = 89% Analysis Date = 02/11/14 Pct Recovery = 89% Analysis Date = 01/31/14 Pct Recovery = 89% Analysis Date = 01/31/14 Pct Recovery = 89% Analysis Date = 01/20/14 Pct Recovery = 89% Analysis Date = 01/20/14 Pct Recovery = 89% Analysis Date = 01/09/14 Pct Recovery = 89% Analysis Date = 01/09/14 Pct Recovery = 89% Analysis Date = 12/30/13 Pct Recovery = 89% Analysis Date = 12/30/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/08/13 Pct Recovery = 89% Analysis Date = 12/08/13 Pct Recovery = 89% Analysis Date = 11/27/13 Pct Recovery = 89% Analysis Date = 11/27/13 Pct Recovery = 89% Analysis Date = 11/16/13 Pct Recovery = 89% Analysis Date = 11/16/13 Pct Recovery = 89% Analysis Date = 11/05/13 Pct Recovery = 89% Analysis Date = 11/05/13 Pct Recovery = 89% Analysis Date = 10/26/13 Pct Recovery = 89% Analysis Date = 10/26/13 Pct Recovery = 89% Analysis Date = 10/15/13 Pct Recovery = 89% Analysis Date = 10/15/13 Pct Recovery = 89% Analysis Date = 10/04/13 Pct Recovery = 89% Analysis Date = 10/04/13 Pct Recovery = 89% Analysis Date = 09/23/13 Pct Recovery = 89% Analysis Date = 09/23/13 Pct Recovery = 89% Analysis Date = 09/12/13 Pct Recovery = 89% Analysis Date = 09/12/13 Pct Recovery = 89% Analysis Date = 09/01/13 Pct Recovery = 89% Analysis Date = 09/01/13 Pct Recovery = 89% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/11/13 Pct Recovery = 89% Analysis Date = 08/11/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/09/13 Pct Recovery = 89% Analysis Date = 07/09/13 Pct Recovery = 89% Analysis Date = 06/29/13 Pct Recovery = 89% Analysis Date = 06/29/13 Pct Recovery = 89% Analysis Date = 06/18/13 Pct Recovery = 89% Analysis Date = 06/18/13 Pct Recovery = 89% Analysis Date = 06/07/13 Pct Recovery = 89% Analysis Date = 06/07/13 Pct Recovery = 89% Analysis Date = 05/27/13 Pct Recovery = 89% Analysis Date = 05/27/13 Pct Recovery = 89% Analysis Date = 05/16/13 Pct Recovery = 89% Analysis Date = 05/16/13 Pct Recovery = 89% Analysis Date = 05/05/13 Pct Recovery = 89% Analysis Date = 05/05/13 Pct Recovery = 89% Analysis Date = 04/25/13 Pct Recovery = 89% Analysis Date = 04/25/13 Pct Recovery = 89% Analysis Date = 04/14/13 Pct Recovery = 89% Analysis Date = 04/14/13 Pct Recovery = 89% Analysis Date = 04/03/13 Pct Recovery = 89% Analysis Date = 04/03/13 Pct Recovery = 89% Analysis Date = 03/23/13 Pct Recovery = 89% Analysis Date = 03/23/13 Pct Recovery = 89% Analysis Date = 03/12/13 Pct Recovery = 89% Analysis Date = 03/12/13 Pct Recovery = 89% Analysis Date = 03/01/13 Pct Recovery = 89% Analysis Date = 03/01/13 Pct Recovery = 89% Analysis Date = 02/19/13 Pct Recovery = 89% Analysis Date = 02/19/13 Pct Recovery = 89% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 88% Analysis Date = 10/12/12 Pct Recovery = 89% Analysis Date = 10/12/12 Pct Recovery = 89% Analysis Date = 10/01/12 Pct Recovery = 89% Analysis Date = 10/01/12 Pct Recovery = 89% Analysis Date = 09/20/12 Pct Recovery = 89% Analysis Date = 09/20/12 Pct Recovery = 89% Analysis Date = 09/09/12 Pct Recovery = 89% Analysis Date = 09/09/12 Pct Recovery = 89% Analysis Date = 08/29/12 Pct Recovery = 89% Analysis Date = 08/29/12 Pct Recovery = 89% Analysis Date = 08/19/12 Pct Recovery = 89% Analysis Date = 08/19/12 Pct Recovery = 89% Analysis Date = 08/08/12 Pct Recovery = 89% Analysis Date = 08/08/12 Pct Recovery = 89% Analysis Date = 07/28/12 Pct Recovery = 89% Analysis Date = 07/28/12 Pct Recovery = 89% Analysis Date = 07/17/12 Pct Recovery = 89% Analysis Date = 07/17/12 Pct Recovery = 89% Analysis Date = 07/06/12 Pct Recovery = 89% Analysis Date = 07/06/12 Pct Recovery = 89% Analysis Date = 06/25/12 Pct Recovery = 89% Analysis Date = 06/25/12 Pct Recovery = 89% Analysis Date = 06/15/12 Pct Recovery = 89% Analysis Date = 06/15/12 Pct Recovery = 89% Analysis Date = 06/04/12 Pct Recovery = 89% Analysis Date = 06/04/12 Pct Recovery = 89% Analysis Date = 05/24/12 Pct Recovery = 89% Analysis Date = 05/24/12 Pct Recovery = 89% Analysis Date = 05/13/12 Pct Recovery = 89% Analysis Date = 05/13/12 Pct Recovery = 89% Analysis Date = 05/02/12 Pct Recovery = 89% Analysis Date = 05/02/12 Pct Recovery = 89% Analysis Date = 04/22/12 Pct Recovery = 89% Analysis Date = 04/22/12 Pct Recovery = 89% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/09/12 Pct Recovery = 89% Analysis Date = 03/09/12 Pct Recovery = 89% Analysis Date = 02/27/12 Pct Recovery = 89% Analysis Date = 02/27/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/06/12 Pct Recovery = 90% Analysis Date = 02/06/12 Pct Recovery = 90% Analysis Date = 01/26/12 Pct Recovery = 90% Analysis Date = 01/26/12 Pct Recovery = 90% Analysis Date = 01/15/12 Pct Recovery = 90% Analysis Date = 01/15/12 Pct Recovery = 90% Analysis Date = 01/04/12 Pct Recovery = 90% Analysis Date = 01/04/12 Pct Recovery = 90% Analysis Date = 12/24/11 Pct Recovery = 90% Analysis Date = 12/24/11 Pct Recovery = 90% Analysis Date = 12/14/11 Pct Recovery = 90% Analysis Date = 12/14/11 Pct Recovery = 90% Analysis Date = 12/03/11 Pct Recovery = 90% Analysis Date = 12/03/11 Pct Recovery = 90% Analysis Date = 11/22/11 Pct Recovery = 90% Analysis Date = 11/22/11 Pct Recovery = 90% Analysis Date = 11/11/11 Pct Recovery = 90% Analysis Date = 11/11/11 Pct Recovery = 90% Analysis Date = 10/31/11 Pct Recovery = 90% Analysis Date = 10/31/11 Pct Recovery = 90% Analysis Date = 10/20/11 Pct Recovery = 90% Analysis Date = 10/20/11 Pct Recovery = 90% Analysis Date = 10/10/11 Pct Recovery = 90% Analysis Date = 10/10/11 Pct Recovery = 90% Analysis Date = 09/29/11 Pct Recovery = 90% Analysis Date = 09/29/11 Pct Recovery = 90% Analysis Date = 09/18/11 Pct Recovery = 91% Analysis Date = 09/18/11 Pct Recovery = 91% Analysis Date = 09/07/11 Pct Recovery = 91% Analysis Date = 09/07/11 Pct Recovery = 91% Analysis Date = 08/27/11 Pct Recovery = 91% Analysis Date = 08/27/11 Pct Recovery = 91% Analysis Date = 08/17/11 Pct Recovery = 91% Analysis Date = 08/17/11 Pct Recovery = 91% Analysis Date = 08/06/11 Pct Recovery = 91% Analysis Date = 08/06/11 Pct Recovery = 91% Analysis Date = 07/26/11 Pct Recovery = 91% Analysis Date = 07/26/11 Pct Recovery = 91% Analysis Date = 07/15/11 Pct Recovery = 91% Analysis Date = 07/15/11 Pct Recovery = 91% Analysis Date = 07/04/11 Pct Recovery = 91% Analysis Date = 07/04/11 Pct Recovery = 91% Analysis Date = 06/23/11 Pct Recovery = 91% Analysis Date = 06/23/11 Pct Recovery = 91% Analysis Date = 06/13/11 Pct Recovery = 91% Analysis Date = 06/13/11 Pct Recovery = 91% Analysis Date = 06/02/11 Pct Recovery = 91% Analysis Date = 06/02/11 Pct Recovery = 91% Analysis Date = 05/22/11 Pct Recovery = 91% Analysis Date = 05/22/11 Pct Recovery = 91% Analysis Date = 05/11/11 Pct Recovery = 92% Analysis Date = 05/11/11 Pct Recovery = 92% Analysis Date = 04/30/11 Pct Recovery = 92% Analysis Date = 04/30/11 Pct Recovery = 92% Analysis Date = 04/19/11 Pct Recovery = 92% Analysis Date = 04/19/11 Pct Recovery = 92% Analysis Date = 04/09/11 Pct Recovery = 92% Analysis Date = 04/09/11 Pct Recovery = 92% Analysis Date = 03/29/11 Pct Recovery = 92% Analysis Date = 03/29/11 Pct Recovery = 92% Analysis Date = 03/18/11 Pct Recovery = 92% Analysis Date = 03/18/11 Pct Recovery = 92% Analysis Date = 03/07/11 Pct Recovery = 92% Analysis Date = 03/07/11 Pct Recovery = 92% Analysis Date = 02/24/11 Pct Recovery = 92% Analysis Date = 02/24/11 Pct Recovery = 92% Analysis Date = 02/14/11 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 95% 6% 93% 8%
>= Reporting Level 90 89% 14% 87% 12%
Total 96 89% 14% 88% 12%

Sample Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Characteristic N % % Basis
Plotted 96 100% Spiked
Estimated Values 4 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 96 .  
False Negatives 0 0% 0 out of 96
Not Spiked 73 .  
False Positives 0 0% 0 out of 73

BQS OBSP Determination:
ATRAZINE
METHOD: 2033 , TESTIDCODE: 39632GCM35
Open Data Set

Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 104% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 97% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 98% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 93% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 97% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 90% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 95% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 95% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 101% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 106% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 101% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 104% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 107% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 87% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 107% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 110% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 105% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 108% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 108% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 87% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 92% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 98% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 90% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 80% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 86% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 93% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 105% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 96% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 111% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 105% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 87% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 124% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 116% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 67% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 109% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 82% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 100% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 83% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 96% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 113% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 68% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 80% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 92% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 111% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 94% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 99% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 102% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 78% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 101% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 84% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 107% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 116% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 80% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 94% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 78% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 74% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 99% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 104% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 70% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 81% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 105% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 99% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 106% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 88% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 78% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 72% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 75% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 82% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 93% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 85% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 82% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 82% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 98% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 84% Analysis Date = 11/28/16 Pct Recovery = 84% Analysis Date = 11/28/16 Pct Recovery = 84% Analysis Date = 11/17/16 Pct Recovery = 84% Analysis Date = 11/17/16 Pct Recovery = 84% Analysis Date = 11/07/16 Pct Recovery = 84% Analysis Date = 11/07/16 Pct Recovery = 84% Analysis Date = 10/27/16 Pct Recovery = 84% Analysis Date = 10/27/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/06/16 Pct Recovery = 84% Analysis Date = 10/06/16 Pct Recovery = 84% Analysis Date = 09/25/16 Pct Recovery = 84% Analysis Date = 09/25/16 Pct Recovery = 84% Analysis Date = 09/14/16 Pct Recovery = 84% Analysis Date = 09/14/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 08/24/16 Pct Recovery = 84% Analysis Date = 08/24/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/13/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 07/23/16 Pct Recovery = 84% Analysis Date = 07/23/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/02/16 Pct Recovery = 84% Analysis Date = 07/02/16 Pct Recovery = 84% Analysis Date = 06/21/16 Pct Recovery = 84% Analysis Date = 06/21/16 Pct Recovery = 84% Analysis Date = 06/10/16 Pct Recovery = 84% Analysis Date = 06/10/16 Pct Recovery = 84% Analysis Date = 05/31/16 Pct Recovery = 84% Analysis Date = 05/31/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 84% Analysis Date = 05/20/16 Pct Recovery = 84% Analysis Date = 05/09/16 Pct Recovery = 84% Analysis Date = 05/09/16 Pct Recovery = 84% Analysis Date = 04/29/16 Pct Recovery = 84% Analysis Date = 04/29/16 Pct Recovery = 84% Analysis Date = 04/18/16 Pct Recovery = 84% Analysis Date = 04/18/16 Pct Recovery = 84% Analysis Date = 04/07/16 Pct Recovery = 84% Analysis Date = 04/07/16 Pct Recovery = 84% Analysis Date = 03/28/16 Pct Recovery = 84% Analysis Date = 03/28/16 Pct Recovery = 84% Analysis Date = 03/17/16 Pct Recovery = 84% Analysis Date = 03/17/16 Pct Recovery = 84% Analysis Date = 03/06/16 Pct Recovery = 84% Analysis Date = 03/06/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/14/16 Pct Recovery = 84% Analysis Date = 02/14/16 Pct Recovery = 84% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 02/03/16 Pct Recovery = 84% Analysis Date = 01/23/16 Pct Recovery = 84% Analysis Date = 01/23/16 Pct Recovery = 84% Analysis Date = 01/13/16 Pct Recovery = 84% Analysis Date = 01/13/16 Pct Recovery = 84% Analysis Date = 01/02/16 Pct Recovery = 84% Analysis Date = 01/02/16 Pct Recovery = 84% Analysis Date = 12/22/15 Pct Recovery = 84% Analysis Date = 12/22/15 Pct Recovery = 84% Analysis Date = 12/12/15 Pct Recovery = 84% Analysis Date = 12/12/15 Pct Recovery = 84% Analysis Date = 12/01/15 Pct Recovery = 84% Analysis Date = 12/01/15 Pct Recovery = 84% Analysis Date = 11/20/15 Pct Recovery = 84% Analysis Date = 11/20/15 Pct Recovery = 84% Analysis Date = 11/10/15 Pct Recovery = 84% Analysis Date = 11/10/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/19/15 Pct Recovery = 84% Analysis Date = 10/19/15 Pct Recovery = 84% Analysis Date = 10/09/15 Pct Recovery = 84% Analysis Date = 10/09/15 Pct Recovery = 84% Analysis Date = 09/28/15 Pct Recovery = 84% Analysis Date = 09/28/15 Pct Recovery = 84% Analysis Date = 09/17/15 Pct Recovery = 84% Analysis Date = 09/17/15 Pct Recovery = 84% Analysis Date = 09/07/15 Pct Recovery = 84% Analysis Date = 09/07/15 Pct Recovery = 84% Analysis Date = 08/27/15 Pct Recovery = 84% Analysis Date = 08/27/15 Pct Recovery = 84% Analysis Date = 08/16/15 Pct Recovery = 84% Analysis Date = 08/16/15 Pct Recovery = 84% Analysis Date = 08/06/15 Pct Recovery = 84% Analysis Date = 08/06/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/26/15 Pct Recovery = 84% Analysis Date = 07/15/15 Pct Recovery = 84% Analysis Date = 07/15/15 Pct Recovery = 84% Analysis Date = 07/05/15 Pct Recovery = 84% Analysis Date = 07/05/15 Pct Recovery = 84% Analysis Date = 06/24/15 Pct Recovery = 84% Analysis Date = 06/24/15 Pct Recovery = 84% Analysis Date = 06/13/15 Pct Recovery = 84% Analysis Date = 06/13/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 06/02/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/23/15 Pct Recovery = 84% Analysis Date = 05/12/15 Pct Recovery = 84% Analysis Date = 05/12/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 05/01/15 Pct Recovery = 84% Analysis Date = 04/21/15 Pct Recovery = 84% Analysis Date = 04/21/15 Pct Recovery = 84% Analysis Date = 04/10/15 Pct Recovery = 84% Analysis Date = 04/10/15 Pct Recovery = 84% Analysis Date = 03/30/15 Pct Recovery = 84% Analysis Date = 03/30/15 Pct Recovery = 84% Analysis Date = 03/20/15 Pct Recovery = 84% Analysis Date = 03/20/15 Pct Recovery = 84% Analysis Date = 03/09/15 Pct Recovery = 85% Analysis Date = 03/09/15 Pct Recovery = 85% Analysis Date = 02/26/15 Pct Recovery = 85% Analysis Date = 02/26/15 Pct Recovery = 85% Analysis Date = 02/16/15 Pct Recovery = 85% Analysis Date = 02/16/15 Pct Recovery = 85% Analysis Date = 02/05/15 Pct Recovery = 85% Analysis Date = 02/05/15 Pct Recovery = 85% Analysis Date = 01/25/15 Pct Recovery = 85% Analysis Date = 01/25/15 Pct Recovery = 85% Analysis Date = 01/15/15 Pct Recovery = 85% Analysis Date = 01/15/15 Pct Recovery = 85% Analysis Date = 01/04/15 Pct Recovery = 85% Analysis Date = 01/04/15 Pct Recovery = 85% Analysis Date = 12/24/14 Pct Recovery = 85% Analysis Date = 12/24/14 Pct Recovery = 85% Analysis Date = 12/14/14 Pct Recovery = 85% Analysis Date = 12/14/14 Pct Recovery = 85% Analysis Date = 12/03/14 Pct Recovery = 86% Analysis Date = 12/03/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/12/14 Pct Recovery = 86% Analysis Date = 11/12/14 Pct Recovery = 86% Analysis Date = 11/01/14 Pct Recovery = 86% Analysis Date = 11/01/14 Pct Recovery = 86% Analysis Date = 10/21/14 Pct Recovery = 86% Analysis Date = 10/21/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 10/11/14 Pct Recovery = 86% Analysis Date = 09/30/14 Pct Recovery = 87% Analysis Date = 09/30/14 Pct Recovery = 87% Analysis Date = 09/19/14 Pct Recovery = 87% Analysis Date = 09/19/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 09/08/14 Pct Recovery = 87% Analysis Date = 08/29/14 Pct Recovery = 87% Analysis Date = 08/29/14 Pct Recovery = 87% Analysis Date = 08/18/14 Pct Recovery = 87% Analysis Date = 08/18/14 Pct Recovery = 87% Analysis Date = 08/07/14 Pct Recovery = 88% Analysis Date = 08/07/14 Pct Recovery = 88% Analysis Date = 07/28/14 Pct Recovery = 88% Analysis Date = 07/28/14 Pct Recovery = 88% Analysis Date = 07/17/14 Pct Recovery = 88% Analysis Date = 07/17/14 Pct Recovery = 88% Analysis Date = 07/06/14 Pct Recovery = 88% Analysis Date = 07/06/14 Pct Recovery = 88% Analysis Date = 06/26/14 Pct Recovery = 89% Analysis Date = 06/26/14 Pct Recovery = 89% Analysis Date = 06/15/14 Pct Recovery = 89% Analysis Date = 06/15/14 Pct Recovery = 89% Analysis Date = 06/04/14 Pct Recovery = 89% Analysis Date = 06/04/14 Pct Recovery = 89% Analysis Date = 05/25/14 Pct Recovery = 89% Analysis Date = 05/25/14 Pct Recovery = 89% Analysis Date = 05/14/14 Pct Recovery = 89% Analysis Date = 05/14/14 Pct Recovery = 89% Analysis Date = 05/03/14 Pct Recovery = 90% Analysis Date = 05/03/14 Pct Recovery = 90% Analysis Date = 04/23/14 Pct Recovery = 90% Analysis Date = 04/23/14 Pct Recovery = 90% Analysis Date = 04/12/14 Pct Recovery = 90% Analysis Date = 04/12/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 04/01/14 Pct Recovery = 90% Analysis Date = 03/22/14 Pct Recovery = 90% Analysis Date = 03/22/14 Pct Recovery = 90% Analysis Date = 03/11/14 Pct Recovery = 91% Analysis Date = 03/11/14 Pct Recovery = 91% Analysis Date = 02/28/14 Pct Recovery = 91% Analysis Date = 02/28/14 Pct Recovery = 91% Analysis Date = 02/18/14 Pct Recovery = 91% Analysis Date = 02/18/14 Pct Recovery = 91% Analysis Date = 02/07/14 Pct Recovery = 91% Analysis Date = 02/07/14 Pct Recovery = 91% Analysis Date = 01/27/14 Pct Recovery = 91% Analysis Date = 01/27/14 Pct Recovery = 91% Analysis Date = 01/17/14 Pct Recovery = 92% Analysis Date = 01/17/14 Pct Recovery = 92% Analysis Date = 01/06/14 Pct Recovery = 92% Analysis Date = 01/06/14 Pct Recovery = 92% Analysis Date = 12/26/13 Pct Recovery = 92% Analysis Date = 12/26/13 Pct Recovery = 92% Analysis Date = 12/15/13 Pct Recovery = 92% Analysis Date = 12/15/13 Pct Recovery = 92% Analysis Date = 12/05/13 Pct Recovery = 93% Analysis Date = 12/05/13 Pct Recovery = 93% Analysis Date = 11/24/13 Pct Recovery = 93% Analysis Date = 11/24/13 Pct Recovery = 93% Analysis Date = 11/13/13 Pct Recovery = 93% Analysis Date = 11/13/13 Pct Recovery = 93% Analysis Date = 11/03/13 Pct Recovery = 93% Analysis Date = 11/03/13 Pct Recovery = 93% Analysis Date = 10/23/13 Pct Recovery = 94% Analysis Date = 10/23/13 Pct Recovery = 94% Analysis Date = 10/12/13 Pct Recovery = 94% Analysis Date = 10/12/13 Pct Recovery = 94% Analysis Date = 10/02/13 Pct Recovery = 94% Analysis Date = 10/02/13 Pct Recovery = 94% Analysis Date = 09/21/13 Pct Recovery = 94% Analysis Date = 09/21/13 Pct Recovery = 94% Analysis Date = 09/10/13 Pct Recovery = 94% Analysis Date = 09/10/13 Pct Recovery = 94% Analysis Date = 08/31/13 Pct Recovery = 94% Analysis Date = 08/31/13 Pct Recovery = 94% Analysis Date = 08/20/13 Pct Recovery = 94% Analysis Date = 08/20/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 07/30/13 Pct Recovery = 95% Analysis Date = 07/30/13 Pct Recovery = 95% Analysis Date = 07/19/13 Pct Recovery = 95% Analysis Date = 07/19/13 Pct Recovery = 95% Analysis Date = 07/08/13 Pct Recovery = 95% Analysis Date = 07/08/13 Pct Recovery = 95% Analysis Date = 06/28/13 Pct Recovery = 95% Analysis Date = 06/28/13 Pct Recovery = 95% Analysis Date = 06/17/13 Pct Recovery = 95% Analysis Date = 06/17/13 Pct Recovery = 95% Analysis Date = 06/06/13 Pct Recovery = 95% Analysis Date = 06/06/13 Pct Recovery = 95% Analysis Date = 05/27/13 Pct Recovery = 95% Analysis Date = 05/27/13 Pct Recovery = 95% Analysis Date = 05/16/13 Pct Recovery = 95% Analysis Date = 05/16/13 Pct Recovery = 95% Analysis Date = 05/05/13 Pct Recovery = 96% Analysis Date = 05/05/13 Pct Recovery = 96% Analysis Date = 04/25/13 Pct Recovery = 96% Analysis Date = 04/25/13 Pct Recovery = 96% Analysis Date = 04/14/13 Pct Recovery = 96% Analysis Date = 04/14/13 Pct Recovery = 96% Analysis Date = 04/03/13 Pct Recovery = 96% Analysis Date = 04/03/13 Pct Recovery = 96% Analysis Date = 03/23/13 Pct Recovery = 96% Analysis Date = 03/23/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/02/13 Pct Recovery = 96% Analysis Date = 03/02/13 Pct Recovery = 96% Analysis Date = 02/19/13 Pct Recovery = 96% Analysis Date = 02/19/13 Pct Recovery = 96% Analysis Date = 02/09/13 Pct Recovery = 96% Analysis Date = 02/09/13 Pct Recovery = 96% Analysis Date = 01/29/13 Pct Recovery = 96% Analysis Date = 01/29/13 Pct Recovery = 96% Analysis Date = 01/18/13 Pct Recovery = 96% Analysis Date = 01/18/13 Pct Recovery = 96% Analysis Date = 01/08/13 Pct Recovery = 96% Analysis Date = 01/08/13 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 96% Analysis Date = 11/15/12 Pct Recovery = 96% Analysis Date = 11/15/12 Pct Recovery = 96% Analysis Date = 11/05/12 Pct Recovery = 96% Analysis Date = 11/05/12 Pct Recovery = 96% Analysis Date = 10/25/12 Pct Recovery = 96% Analysis Date = 10/25/12 Pct Recovery = 96% Analysis Date = 10/14/12 Pct Recovery = 96% Analysis Date = 10/14/12 Pct Recovery = 96% Analysis Date = 10/04/12 Pct Recovery = 96% Analysis Date = 10/04/12 Pct Recovery = 96% Analysis Date = 09/23/12 Pct Recovery = 96% Analysis Date = 09/23/12 Pct Recovery = 96% Analysis Date = 09/12/12 Pct Recovery = 96% Analysis Date = 09/12/12 Pct Recovery = 96% Analysis Date = 09/02/12 Pct Recovery = 96% Analysis Date = 09/02/12 Pct Recovery = 96% Analysis Date = 08/22/12 Pct Recovery = 96% Analysis Date = 08/22/12 Pct Recovery = 96% Analysis Date = 08/11/12 Pct Recovery = 96% Analysis Date = 08/11/12 Pct Recovery = 96% Analysis Date = 08/01/12 Pct Recovery = 96% Analysis Date = 08/01/12 Pct Recovery = 96% Analysis Date = 07/21/12 Pct Recovery = 96% Analysis Date = 07/21/12 Pct Recovery = 96% Analysis Date = 07/10/12 Pct Recovery = 96% Analysis Date = 07/10/12 Pct Recovery = 96% Analysis Date = 06/29/12 Pct Recovery = 97% Analysis Date = 06/29/12 Pct Recovery = 97% Analysis Date = 06/19/12 Pct Recovery = 97% Analysis Date = 06/19/12 Pct Recovery = 97% Analysis Date = 06/08/12 Pct Recovery = 97% Analysis Date = 06/08/12 Pct Recovery = 97% Analysis Date = 05/28/12 Pct Recovery = 97% Analysis Date = 05/28/12 Pct Recovery = 97% Analysis Date = 05/18/12 Pct Recovery = 97% Analysis Date = 05/18/12 Pct Recovery = 97% Analysis Date = 05/07/12 Pct Recovery = 97% Analysis Date = 05/07/12 Pct Recovery = 97% Analysis Date = 04/26/12 Pct Recovery = 97% Analysis Date = 04/26/12 Pct Recovery = 97% Analysis Date = 04/16/12 Pct Recovery = 97% Analysis Date = 04/16/12 Pct Recovery = 97% Analysis Date = 04/05/12 Pct Recovery = 97% Analysis Date = 04/05/12 Pct Recovery = 97% Analysis Date = 03/25/12 Pct Recovery = 97% Analysis Date = 03/25/12 Pct Recovery = 97% Analysis Date = 03/15/12 Pct Recovery = 97% Analysis Date = 03/15/12 Pct Recovery = 97% Analysis Date = 03/04/12 Pct Recovery = 97% Analysis Date = 03/04/12 Pct Recovery = 97% Analysis Date = 02/22/12 Pct Recovery = 97% Analysis Date = 02/22/12 Pct Recovery = 97% Analysis Date = 02/12/12 Pct Recovery = 97% Analysis Date = 02/12/12 Pct Recovery = 97% Analysis Date = 02/01/12 Pct Recovery = 97% Analysis Date = 02/01/12 Pct Recovery = 97% Analysis Date = 01/21/12 Pct Recovery = 97% Analysis Date = 01/21/12 Pct Recovery = 97% Analysis Date = 01/11/12 Pct Recovery = 97% Analysis Date = 01/11/12 Pct Recovery = 97% Analysis Date = 12/31/11 Pct Recovery = 97% Analysis Date = 12/31/11 Pct Recovery = 97% Analysis Date = 12/20/11 Pct Recovery = 98% Analysis Date = 12/20/11 Pct Recovery = 98% Analysis Date = 12/10/11 Pct Recovery = 98% Analysis Date = 12/10/11 Pct Recovery = 98% Analysis Date = 11/29/11 Pct Recovery = 98% Analysis Date = 11/29/11 Pct Recovery = 98% Analysis Date = 11/18/11 Pct Recovery = 98% Analysis Date = 11/18/11 Pct Recovery = 98% Analysis Date = 11/08/11 Pct Recovery = 98% Analysis Date = 11/08/11 Pct Recovery = 98% Analysis Date = 10/28/11 Pct Recovery = 98% Analysis Date = 10/28/11 Pct Recovery = 98% Analysis Date = 10/17/11 Pct Recovery = 98% Analysis Date = 10/17/11 Pct Recovery = 98% Analysis Date = 10/06/11 Pct Recovery = 98% Analysis Date = 10/06/11 Pct Recovery = 98% Analysis Date = 09/26/11 Pct Recovery = 98% Analysis Date = 09/26/11 Pct Recovery = 98% Analysis Date = 09/15/11 Pct Recovery = 98% Analysis Date = 09/15/11 Pct Recovery = 98% Analysis Date = 09/04/11 Pct Recovery = 98% Analysis Date = 09/04/11 Pct Recovery = 98% Analysis Date = 08/25/11 Pct Recovery = 98% Analysis Date = 08/25/11 Pct Recovery = 98% Analysis Date = 08/14/11 Pct Recovery = 98% Analysis Date = 08/14/11 Pct Recovery = 98% Analysis Date = 08/03/11 Pct Recovery = 99% Analysis Date = 08/03/11 Pct Recovery = 99% Analysis Date = 07/24/11 Pct Recovery = 99% Analysis Date = 07/24/11 Pct Recovery = 99% Analysis Date = 07/13/11 Pct Recovery = 99% Analysis Date = 07/13/11 Pct Recovery = 99% Analysis Date = 07/02/11 Pct Recovery = 99% Analysis Date = 07/02/11 Pct Recovery = 99% Analysis Date = 06/22/11 Pct Recovery = 99% Analysis Date = 06/22/11 Pct Recovery = 99% Analysis Date = 06/11/11 Pct Recovery = 99% Analysis Date = 06/11/11 Pct Recovery = 99% Analysis Date = 05/31/11 Pct Recovery = 99% Analysis Date = 05/31/11 Pct Recovery = 99% Analysis Date = 05/21/11 Pct Recovery = 99% Analysis Date = 05/21/11 Pct Recovery = 99% Analysis Date = 05/10/11 Pct Recovery = 99% Analysis Date = 05/10/11 Pct Recovery = 99% Analysis Date = 04/29/11 Pct Recovery = 99% Analysis Date = 04/29/11 Pct Recovery = 99% Analysis Date = 04/19/11 Pct Recovery = 99% Analysis Date = 04/19/11 Pct Recovery = 99% Analysis Date = 04/08/11 Pct Recovery = 100% Analysis Date = 04/08/11 Pct Recovery = 100% Analysis Date = 03/28/11 Pct Recovery = 100% Analysis Date = 03/28/11 Pct Recovery = 100% Analysis Date = 03/18/11 Pct Recovery = 100% Analysis Date = 03/18/11 Pct Recovery = 100% Analysis Date = 03/07/11 Pct Recovery = 100% Analysis Date = 03/07/11 Pct Recovery = 100% Analysis Date = 02/24/11 Pct Recovery = 100% Analysis Date = 02/24/11 Pct Recovery = 100% Analysis Date = 02/14/11 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 92% 13% 92% 15%
Total 94 92% 13% 92% 15%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 3 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
AZINPHOS-METHYL
METHOD: 2033 , TESTIDCODE: 82686GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 96% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 57% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 60% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 89% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 86% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 83% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 81% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 78% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 57% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 76% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 57% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 74% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 64% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 79% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 53% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 43% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 63% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 75% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 55% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 61% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 103% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 78% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 38% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 56% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 95% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 66% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 50% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 87% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 72% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 71% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 81% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 56% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 85% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 41% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 71% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 80% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 46% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 55% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 64% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 61% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 53% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 98% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 108% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 64% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 52% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 113% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 94% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 73% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 77% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 45% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 59% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 63% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 63% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 53% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 75% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 108% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 98% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 90% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 82% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 94% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 64% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 94% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 92% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 75% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 77% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 75% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 50% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 64% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 47% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 103% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 124% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 74% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 99% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 94% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 90% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 84% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 62% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 125% Analysis Date = 01/17/17 Pct Recovery = 68% Analysis Date = 01/07/17 Pct Recovery = 68% Analysis Date = 01/07/17 Pct Recovery = 68% Analysis Date = 12/27/16 Pct Recovery = 68% Analysis Date = 12/27/16 Pct Recovery = 68% Analysis Date = 12/16/16 Pct Recovery = 68% Analysis Date = 12/16/16 Pct Recovery = 68% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 11/24/16 Pct Recovery = 67% Analysis Date = 11/24/16 Pct Recovery = 67% Analysis Date = 11/13/16 Pct Recovery = 67% Analysis Date = 11/13/16 Pct Recovery = 67% Analysis Date = 11/03/16 Pct Recovery = 67% Analysis Date = 11/03/16 Pct Recovery = 67% Analysis Date = 10/23/16 Pct Recovery = 67% Analysis Date = 10/23/16 Pct Recovery = 67% Analysis Date = 10/12/16 Pct Recovery = 67% Analysis Date = 10/12/16 Pct Recovery = 67% Analysis Date = 10/01/16 Pct Recovery = 67% Analysis Date = 10/01/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/09/16 Pct Recovery = 67% Analysis Date = 09/09/16 Pct Recovery = 67% Analysis Date = 08/29/16 Pct Recovery = 66% Analysis Date = 08/29/16 Pct Recovery = 66% Analysis Date = 08/19/16 Pct Recovery = 66% Analysis Date = 08/19/16 Pct Recovery = 66% Analysis Date = 08/08/16 Pct Recovery = 66% Analysis Date = 08/08/16 Pct Recovery = 66% Analysis Date = 07/28/16 Pct Recovery = 66% Analysis Date = 07/28/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 66% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/02/16 Pct Recovery = 65% Analysis Date = 05/02/16 Pct Recovery = 65% Analysis Date = 04/21/16 Pct Recovery = 65% Analysis Date = 04/21/16 Pct Recovery = 65% Analysis Date = 04/10/16 Pct Recovery = 65% Analysis Date = 04/10/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/20/16 Pct Recovery = 65% Analysis Date = 03/20/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/16/16 Pct Recovery = 65% Analysis Date = 02/16/16 Pct Recovery = 65% Analysis Date = 02/05/16 Pct Recovery = 64% Analysis Date = 02/05/16 Pct Recovery = 64% Analysis Date = 01/25/16 Pct Recovery = 64% Analysis Date = 01/25/16 Pct Recovery = 64% Analysis Date = 01/15/16 Pct Recovery = 64% Analysis Date = 01/15/16 Pct Recovery = 64% Analysis Date = 01/04/16 Pct Recovery = 64% Analysis Date = 01/04/16 Pct Recovery = 64% Analysis Date = 12/24/15 Pct Recovery = 64% Analysis Date = 12/24/15 Pct Recovery = 64% Analysis Date = 12/13/15 Pct Recovery = 64% Analysis Date = 12/13/15 Pct Recovery = 64% Analysis Date = 12/02/15 Pct Recovery = 64% Analysis Date = 12/02/15 Pct Recovery = 64% Analysis Date = 11/21/15 Pct Recovery = 64% Analysis Date = 11/21/15 Pct Recovery = 64% Analysis Date = 11/10/15 Pct Recovery = 64% Analysis Date = 11/10/15 Pct Recovery = 64% Analysis Date = 10/31/15 Pct Recovery = 64% Analysis Date = 10/31/15 Pct Recovery = 64% Analysis Date = 10/20/15 Pct Recovery = 64% Analysis Date = 10/20/15 Pct Recovery = 64% Analysis Date = 10/09/15 Pct Recovery = 64% Analysis Date = 10/09/15 Pct Recovery = 64% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/17/15 Pct Recovery = 63% Analysis Date = 09/17/15 Pct Recovery = 63% Analysis Date = 09/06/15 Pct Recovery = 63% Analysis Date = 09/06/15 Pct Recovery = 63% Analysis Date = 08/27/15 Pct Recovery = 63% Analysis Date = 08/27/15 Pct Recovery = 63% Analysis Date = 08/16/15 Pct Recovery = 63% Analysis Date = 08/16/15 Pct Recovery = 63% Analysis Date = 08/05/15 Pct Recovery = 63% Analysis Date = 08/05/15 Pct Recovery = 63% Analysis Date = 07/25/15 Pct Recovery = 63% Analysis Date = 07/25/15 Pct Recovery = 63% Analysis Date = 07/14/15 Pct Recovery = 63% Analysis Date = 07/14/15 Pct Recovery = 63% Analysis Date = 07/03/15 Pct Recovery = 63% Analysis Date = 07/03/15 Pct Recovery = 63% Analysis Date = 06/22/15 Pct Recovery = 63% Analysis Date = 06/22/15 Pct Recovery = 63% Analysis Date = 06/12/15 Pct Recovery = 63% Analysis Date = 06/12/15 Pct Recovery = 63% Analysis Date = 06/01/15 Pct Recovery = 63% Analysis Date = 06/01/15 Pct Recovery = 63% Analysis Date = 05/21/15 Pct Recovery = 63% Analysis Date = 05/21/15 Pct Recovery = 63% Analysis Date = 05/10/15 Pct Recovery = 62% Analysis Date = 05/10/15 Pct Recovery = 62% Analysis Date = 04/29/15 Pct Recovery = 62% Analysis Date = 04/29/15 Pct Recovery = 62% Analysis Date = 04/18/15 Pct Recovery = 62% Analysis Date = 04/18/15 Pct Recovery = 62% Analysis Date = 04/07/15 Pct Recovery = 62% Analysis Date = 04/07/15 Pct Recovery = 62% Analysis Date = 03/28/15 Pct Recovery = 62% Analysis Date = 03/28/15 Pct Recovery = 62% Analysis Date = 03/17/15 Pct Recovery = 62% Analysis Date = 03/17/15 Pct Recovery = 62% Analysis Date = 03/06/15 Pct Recovery = 62% Analysis Date = 03/06/15 Pct Recovery = 62% Analysis Date = 02/23/15 Pct Recovery = 62% Analysis Date = 02/23/15 Pct Recovery = 62% Analysis Date = 02/12/15 Pct Recovery = 62% Analysis Date = 02/12/15 Pct Recovery = 62% Analysis Date = 02/01/15 Pct Recovery = 62% Analysis Date = 02/01/15 Pct Recovery = 62% Analysis Date = 01/22/15 Pct Recovery = 62% Analysis Date = 01/22/15 Pct Recovery = 62% Analysis Date = 01/11/15 Pct Recovery = 63% Analysis Date = 01/11/15 Pct Recovery = 63% Analysis Date = 12/31/14 Pct Recovery = 63% Analysis Date = 12/31/14 Pct Recovery = 63% Analysis Date = 12/20/14 Pct Recovery = 63% Analysis Date = 12/20/14 Pct Recovery = 63% Analysis Date = 12/09/14 Pct Recovery = 63% Analysis Date = 12/09/14 Pct Recovery = 63% Analysis Date = 11/28/14 Pct Recovery = 63% Analysis Date = 11/28/14 Pct Recovery = 63% Analysis Date = 11/17/14 Pct Recovery = 64% Analysis Date = 11/17/14 Pct Recovery = 64% Analysis Date = 11/07/14 Pct Recovery = 64% Analysis Date = 11/07/14 Pct Recovery = 64% Analysis Date = 10/27/14 Pct Recovery = 64% Analysis Date = 10/27/14 Pct Recovery = 64% Analysis Date = 10/16/14 Pct Recovery = 64% Analysis Date = 10/16/14 Pct Recovery = 64% Analysis Date = 10/05/14 Pct Recovery = 64% Analysis Date = 10/05/14 Pct Recovery = 64% Analysis Date = 09/24/14 Pct Recovery = 65% Analysis Date = 09/24/14 Pct Recovery = 65% Analysis Date = 09/13/14 Pct Recovery = 65% Analysis Date = 09/13/14 Pct Recovery = 65% Analysis Date = 09/02/14 Pct Recovery = 65% Analysis Date = 09/02/14 Pct Recovery = 65% Analysis Date = 08/23/14 Pct Recovery = 65% Analysis Date = 08/23/14 Pct Recovery = 65% Analysis Date = 08/12/14 Pct Recovery = 65% Analysis Date = 08/12/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 66% Analysis Date = 08/01/14 Pct Recovery = 66% Analysis Date = 07/21/14 Pct Recovery = 66% Analysis Date = 07/21/14 Pct Recovery = 66% Analysis Date = 07/10/14 Pct Recovery = 66% Analysis Date = 07/10/14 Pct Recovery = 66% Analysis Date = 06/29/14 Pct Recovery = 66% Analysis Date = 06/29/14 Pct Recovery = 66% Analysis Date = 06/19/14 Pct Recovery = 66% Analysis Date = 06/19/14 Pct Recovery = 66% Analysis Date = 06/08/14 Pct Recovery = 67% Analysis Date = 06/08/14 Pct Recovery = 67% Analysis Date = 05/28/14 Pct Recovery = 67% Analysis Date = 05/28/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Analysis Date = 05/06/14 Pct Recovery = 67% Analysis Date = 05/06/14 Pct Recovery = 67% Analysis Date = 04/25/14 Pct Recovery = 68% Analysis Date = 04/25/14 Pct Recovery = 68% Analysis Date = 04/14/14 Pct Recovery = 68% Analysis Date = 04/14/14 Pct Recovery = 68% Analysis Date = 04/04/14 Pct Recovery = 68% Analysis Date = 04/04/14 Pct Recovery = 68% Analysis Date = 03/24/14 Pct Recovery = 69% Analysis Date = 03/24/14 Pct Recovery = 69% Analysis Date = 03/13/14 Pct Recovery = 69% Analysis Date = 03/13/14 Pct Recovery = 69% Analysis Date = 03/02/14 Pct Recovery = 69% Analysis Date = 03/02/14 Pct Recovery = 69% Analysis Date = 02/19/14 Pct Recovery = 69% Analysis Date = 02/19/14 Pct Recovery = 69% Analysis Date = 02/08/14 Pct Recovery = 70% Analysis Date = 02/08/14 Pct Recovery = 70% Analysis Date = 01/28/14 Pct Recovery = 70% Analysis Date = 01/28/14 Pct Recovery = 70% Analysis Date = 01/18/14 Pct Recovery = 70% Analysis Date = 01/18/14 Pct Recovery = 70% Analysis Date = 01/07/14 Pct Recovery = 71% Analysis Date = 01/07/14 Pct Recovery = 71% Analysis Date = 12/27/13 Pct Recovery = 71% Analysis Date = 12/27/13 Pct Recovery = 71% Analysis Date = 12/16/13 Pct Recovery = 71% Analysis Date = 12/16/13 Pct Recovery = 71% Analysis Date = 12/05/13 Pct Recovery = 72% Analysis Date = 12/05/13 Pct Recovery = 72% Analysis Date = 11/24/13 Pct Recovery = 72% Analysis Date = 11/24/13 Pct Recovery = 72% Analysis Date = 11/14/13 Pct Recovery = 72% Analysis Date = 11/14/13 Pct Recovery = 72% Analysis Date = 11/03/13 Pct Recovery = 73% Analysis Date = 11/03/13 Pct Recovery = 73% Analysis Date = 10/23/13 Pct Recovery = 73% Analysis Date = 10/23/13 Pct Recovery = 73% Analysis Date = 10/12/13 Pct Recovery = 74% Analysis Date = 10/12/13 Pct Recovery = 74% Analysis Date = 10/01/13 Pct Recovery = 74% Analysis Date = 10/01/13 Pct Recovery = 74% Analysis Date = 09/20/13 Pct Recovery = 74% Analysis Date = 09/20/13 Pct Recovery = 74% Analysis Date = 09/09/13 Pct Recovery = 75% Analysis Date = 09/09/13 Pct Recovery = 75% Analysis Date = 08/30/13 Pct Recovery = 75% Analysis Date = 08/30/13 Pct Recovery = 75% Analysis Date = 08/19/13 Pct Recovery = 76% Analysis Date = 08/19/13 Pct Recovery = 76% Analysis Date = 08/08/13 Pct Recovery = 76% Analysis Date = 08/08/13 Pct Recovery = 76% Analysis Date = 07/28/13 Pct Recovery = 76% Analysis Date = 07/28/13 Pct Recovery = 76% Analysis Date = 07/17/13 Pct Recovery = 77% Analysis Date = 07/17/13 Pct Recovery = 77% Analysis Date = 07/06/13 Pct Recovery = 77% Analysis Date = 07/06/13 Pct Recovery = 77% Analysis Date = 06/25/13 Pct Recovery = 78% Analysis Date = 06/25/13 Pct Recovery = 78% Analysis Date = 06/15/13 Pct Recovery = 78% Analysis Date = 06/15/13 Pct Recovery = 78% Analysis Date = 06/04/13 Pct Recovery = 78% Analysis Date = 06/04/13 Pct Recovery = 78% Analysis Date = 05/24/13 Pct Recovery = 79% Analysis Date = 05/24/13 Pct Recovery = 79% Analysis Date = 05/13/13 Pct Recovery = 79% Analysis Date = 05/13/13 Pct Recovery = 79% Analysis Date = 05/02/13 Pct Recovery = 80% Analysis Date = 05/02/13 Pct Recovery = 80% Analysis Date = 04/21/13 Pct Recovery = 80% Analysis Date = 04/21/13 Pct Recovery = 80% Analysis Date = 04/11/13 Pct Recovery = 80% Analysis Date = 04/11/13 Pct Recovery = 80% Analysis Date = 03/31/13 Pct Recovery = 81% Analysis Date = 03/31/13 Pct Recovery = 81% Analysis Date = 03/20/13 Pct Recovery = 81% Analysis Date = 03/20/13 Pct Recovery = 81% Analysis Date = 03/09/13 Pct Recovery = 81% Analysis Date = 03/09/13 Pct Recovery = 81% Analysis Date = 02/26/13 Pct Recovery = 81% Analysis Date = 02/26/13 Pct Recovery = 81% Analysis Date = 02/15/13 Pct Recovery = 82% Analysis Date = 02/15/13 Pct Recovery = 82% Analysis Date = 02/04/13 Pct Recovery = 82% Analysis Date = 02/04/13 Pct Recovery = 82% Analysis Date = 01/25/13 Pct Recovery = 82% Analysis Date = 01/25/13 Pct Recovery = 82% Analysis Date = 01/14/13 Pct Recovery = 82% Analysis Date = 01/14/13 Pct Recovery = 82% Analysis Date = 01/03/13 Pct Recovery = 82% Analysis Date = 01/03/13 Pct Recovery = 82% Analysis Date = 12/23/12 Pct Recovery = 82% Analysis Date = 12/23/12 Pct Recovery = 82% Analysis Date = 12/12/12 Pct Recovery = 82% Analysis Date = 12/12/12 Pct Recovery = 82% Analysis Date = 12/01/12 Pct Recovery = 82% Analysis Date = 12/01/12 Pct Recovery = 82% Analysis Date = 11/20/12 Pct Recovery = 82% Analysis Date = 11/20/12 Pct Recovery = 82% Analysis Date = 11/10/12 Pct Recovery = 82% Analysis Date = 11/10/12 Pct Recovery = 82% Analysis Date = 10/30/12 Pct Recovery = 82% Analysis Date = 10/30/12 Pct Recovery = 82% Analysis Date = 10/19/12 Pct Recovery = 82% Analysis Date = 10/19/12 Pct Recovery = 82% Analysis Date = 10/08/12 Pct Recovery = 82% Analysis Date = 10/08/12 Pct Recovery = 82% Analysis Date = 09/27/12 Pct Recovery = 82% Analysis Date = 09/27/12 Pct Recovery = 82% Analysis Date = 09/16/12 Pct Recovery = 82% Analysis Date = 09/16/12 Pct Recovery = 82% Analysis Date = 09/06/12 Pct Recovery = 82% Analysis Date = 09/06/12 Pct Recovery = 82% Analysis Date = 08/26/12 Pct Recovery = 82% Analysis Date = 08/26/12 Pct Recovery = 82% Analysis Date = 08/15/12 Pct Recovery = 82% Analysis Date = 08/15/12 Pct Recovery = 82% Analysis Date = 08/04/12 Pct Recovery = 82% Analysis Date = 08/04/12 Pct Recovery = 82% Analysis Date = 07/24/12 Pct Recovery = 82% Analysis Date = 07/24/12 Pct Recovery = 82% Analysis Date = 07/13/12 Pct Recovery = 82% Analysis Date = 07/13/12 Pct Recovery = 82% Analysis Date = 07/02/12 Pct Recovery = 82% Analysis Date = 07/02/12 Pct Recovery = 82% Analysis Date = 06/22/12 Pct Recovery = 81% Analysis Date = 06/22/12 Pct Recovery = 81% Analysis Date = 06/11/12 Pct Recovery = 81% Analysis Date = 06/11/12 Pct Recovery = 81% Analysis Date = 05/31/12 Pct Recovery = 81% Analysis Date = 05/31/12 Pct Recovery = 81% Analysis Date = 05/20/12 Pct Recovery = 81% Analysis Date = 05/20/12 Pct Recovery = 81% Analysis Date = 05/09/12 Pct Recovery = 81% Analysis Date = 05/09/12 Pct Recovery = 81% Analysis Date = 04/28/12 Pct Recovery = 81% Analysis Date = 04/28/12 Pct Recovery = 81% Analysis Date = 04/17/12 Pct Recovery = 81% Analysis Date = 04/17/12 Pct Recovery = 81% Analysis Date = 04/07/12 Pct Recovery = 81% Analysis Date = 04/07/12 Pct Recovery = 81% Analysis Date = 03/27/12 Pct Recovery = 81% Analysis Date = 03/27/12 Pct Recovery = 81% Analysis Date = 03/16/12 Pct Recovery = 81% Analysis Date = 03/16/12 Pct Recovery = 81% Analysis Date = 03/05/12 Pct Recovery = 81% Analysis Date = 03/05/12 Pct Recovery = 81% Analysis Date = 02/23/12 Pct Recovery = 81% Analysis Date = 02/23/12 Pct Recovery = 81% Analysis Date = 02/12/12 Pct Recovery = 81% Analysis Date = 02/12/12 Pct Recovery = 81% Analysis Date = 02/02/12 Pct Recovery = 81% Analysis Date = 02/02/12 Pct Recovery = 81% Analysis Date = 01/22/12 Pct Recovery = 81% Analysis Date = 01/22/12 Pct Recovery = 81% Analysis Date = 01/11/12 Pct Recovery = 81% Analysis Date = 01/11/12 Pct Recovery = 81% Analysis Date = 12/31/11 Pct Recovery = 81% Analysis Date = 12/31/11 Pct Recovery = 81% Analysis Date = 12/20/11 Pct Recovery = 81% Analysis Date = 12/20/11 Pct Recovery = 81% Analysis Date = 12/09/11 Pct Recovery = 81% Analysis Date = 12/09/11 Pct Recovery = 81% Analysis Date = 11/28/11 Pct Recovery = 81% Analysis Date = 11/28/11 Pct Recovery = 81% Analysis Date = 11/18/11 Pct Recovery = 81% Analysis Date = 11/18/11 Pct Recovery = 81% Analysis Date = 11/07/11 Pct Recovery = 81% Analysis Date = 11/07/11 Pct Recovery = 81% Analysis Date = 10/27/11 Pct Recovery = 81% Analysis Date = 10/27/11 Pct Recovery = 81% Analysis Date = 10/16/11 Pct Recovery = 81% Analysis Date = 10/16/11 Pct Recovery = 81% Analysis Date = 10/05/11 Pct Recovery = 81% Analysis Date = 10/05/11 Pct Recovery = 81% Analysis Date = 09/24/11 Pct Recovery = 81% Analysis Date = 09/24/11 Pct Recovery = 81% Analysis Date = 09/13/11 Pct Recovery = 81% Analysis Date = 09/13/11 Pct Recovery = 81% Analysis Date = 09/03/11 Pct Recovery = 81% Analysis Date = 09/03/11 Pct Recovery = 81% Analysis Date = 08/23/11 Pct Recovery = 81% Analysis Date = 08/23/11 Pct Recovery = 81% Analysis Date = 08/12/11 Pct Recovery = 81% Analysis Date = 08/12/11 Pct Recovery = 81% Analysis Date = 08/01/11 Pct Recovery = 81% Analysis Date = 08/01/11 Pct Recovery = 81% Analysis Date = 07/21/11 Pct Recovery = 81% Analysis Date = 07/21/11 Pct Recovery = 81% Analysis Date = 07/10/11 Pct Recovery = 81% Analysis Date = 07/10/11 Pct Recovery = 81% Analysis Date = 06/30/11 Pct Recovery = 81% Analysis Date = 06/30/11 Pct Recovery = 81% Analysis Date = 06/19/11 Pct Recovery = 81% Analysis Date = 06/19/11 Pct Recovery = 81% Analysis Date = 06/08/11 Pct Recovery = 81% Analysis Date = 06/08/11 Pct Recovery = 81% Analysis Date = 05/28/11 Pct Recovery = 81% Analysis Date = 05/28/11 Pct Recovery = 81% Analysis Date = 05/17/11 Pct Recovery = 81% Analysis Date = 05/17/11 Pct Recovery = 81% Analysis Date = 05/06/11 Pct Recovery = 81% Analysis Date = 05/06/11 Pct Recovery = 81% Analysis Date = 04/25/11 Pct Recovery = 81% Analysis Date = 04/25/11 Pct Recovery = 81% Analysis Date = 04/15/11 Pct Recovery = 81% Analysis Date = 04/15/11 Pct Recovery = 81% Analysis Date = 04/04/11 Pct Recovery = 80% Analysis Date = 04/04/11 Pct Recovery = 80% Analysis Date = 03/24/11 Pct Recovery = 80% Analysis Date = 03/24/11 Pct Recovery = 80% Analysis Date = 03/13/11 Pct Recovery = 80% Analysis Date = 03/13/11 Pct Recovery = 80% Analysis Date = 03/02/11 Pct Recovery = 80% Analysis Date = 03/02/11 Pct Recovery = 80% Analysis Date = 02/19/11 Pct Recovery = 80% Analysis Date = 02/19/11 Pct Recovery = 80% Analysis Date = 02/09/11 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 92% 19% 91% 11%
>= Reporting Level 86 71% 18% 66% 17%
Total 93 73% 19% 71% 20%

Sample Statistics
AZINPHOS-METHYL

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 93 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 0 0% 0 out of 76

BQS OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2033 , TESTIDCODE: 61635GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 72% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 29% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 64% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 58% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 64% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 56% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 88% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 63% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 64% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 52% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 87% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 64% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 66% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 65% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 27% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 54% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 50% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 80% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 74% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 40% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 65% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 54% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 28% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 172% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 74% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 79% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 106% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 70% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 39% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 78% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 91% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 113% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 92% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 99% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 113% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 54% Analysis Date = 08/26/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 82% Analysis Date = 08/17/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 07/28/16 Pct Recovery = 82% Analysis Date = 07/28/16 Pct Recovery = 82% Analysis Date = 07/18/16 Pct Recovery = 81% Analysis Date = 07/18/16 Pct Recovery = 81% Analysis Date = 07/09/16 Pct Recovery = 81% Analysis Date = 07/09/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/19/16 Pct Recovery = 80% Analysis Date = 06/19/16 Pct Recovery = 80% Analysis Date = 06/09/16 Pct Recovery = 80% Analysis Date = 06/09/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/21/16 Pct Recovery = 78% Analysis Date = 04/21/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/02/16 Pct Recovery = 78% Analysis Date = 04/02/16 Pct Recovery = 78% Analysis Date = 03/23/16 Pct Recovery = 77% Analysis Date = 03/23/16 Pct Recovery = 77% Analysis Date = 03/13/16 Pct Recovery = 77% Analysis Date = 03/13/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 76% Analysis Date = 02/23/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/05/16 Pct Recovery = 75% Analysis Date = 01/05/16 Pct Recovery = 75% Analysis Date = 12/26/15 Pct Recovery = 74% Analysis Date = 12/26/15 Pct Recovery = 74% Analysis Date = 12/16/15 Pct Recovery = 74% Analysis Date = 12/16/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 72% Analysis Date = 10/28/15 Pct Recovery = 72% Analysis Date = 10/19/15 Pct Recovery = 72% Analysis Date = 10/19/15 Pct Recovery = 72% Analysis Date = 10/09/15 Pct Recovery = 72% Analysis Date = 10/09/15 Pct Recovery = 72% Analysis Date = 09/29/15 Pct Recovery = 71% Analysis Date = 09/29/15 Pct Recovery = 71% Analysis Date = 09/19/15 Pct Recovery = 71% Analysis Date = 09/19/15 Pct Recovery = 71% Analysis Date = 09/09/15 Pct Recovery = 71% Analysis Date = 09/09/15 Pct Recovery = 71% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/11/15 Pct Recovery = 70% Analysis Date = 08/11/15 Pct Recovery = 70% Analysis Date = 08/01/15 Pct Recovery = 69% Analysis Date = 08/01/15 Pct Recovery = 69% Analysis Date = 07/23/15 Pct Recovery = 69% Analysis Date = 07/23/15 Pct Recovery = 69% Analysis Date = 07/13/15 Pct Recovery = 69% Analysis Date = 07/13/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 69% Analysis Date = 06/23/15 Pct Recovery = 68% Analysis Date = 06/23/15 Pct Recovery = 68% Analysis Date = 06/13/15 Pct Recovery = 68% Analysis Date = 06/13/15 Pct Recovery = 68% Analysis Date = 06/04/15 Pct Recovery = 68% Analysis Date = 06/04/15 Pct Recovery = 68% Analysis Date = 05/25/15 Pct Recovery = 67% Analysis Date = 05/25/15 Pct Recovery = 67% Analysis Date = 05/15/15 Pct Recovery = 67% Analysis Date = 05/15/15 Pct Recovery = 67% Analysis Date = 05/05/15 Pct Recovery = 67% Analysis Date = 05/05/15 Pct Recovery = 67% Analysis Date = 04/25/15 Pct Recovery = 67% Analysis Date = 04/25/15 Pct Recovery = 67% Analysis Date = 04/16/15 Pct Recovery = 67% Analysis Date = 04/16/15 Pct Recovery = 67% Analysis Date = 04/06/15 Pct Recovery = 66% Analysis Date = 04/06/15 Pct Recovery = 66% Analysis Date = 03/27/15 Pct Recovery = 66% Analysis Date = 03/27/15 Pct Recovery = 66% Analysis Date = 03/17/15 Pct Recovery = 66% Analysis Date = 03/17/15 Pct Recovery = 66% Analysis Date = 03/08/15 Pct Recovery = 66% Analysis Date = 03/08/15 Pct Recovery = 66% Analysis Date = 02/26/15 Pct Recovery = 65% Analysis Date = 02/26/15 Pct Recovery = 65% Analysis Date = 02/16/15 Pct Recovery = 65% Analysis Date = 02/16/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 65% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/10/14 Pct Recovery = 64% Analysis Date = 12/10/14 Pct Recovery = 64% Analysis Date = 11/30/14 Pct Recovery = 64% Analysis Date = 11/30/14 Pct Recovery = 64% Analysis Date = 11/20/14 Pct Recovery = 63% Analysis Date = 11/20/14 Pct Recovery = 63% Analysis Date = 11/10/14 Pct Recovery = 63% Analysis Date = 11/10/14 Pct Recovery = 63% Analysis Date = 10/31/14 Pct Recovery = 63% Analysis Date = 10/31/14 Pct Recovery = 63% Analysis Date = 10/22/14 Pct Recovery = 63% Analysis Date = 10/22/14 Pct Recovery = 63% Analysis Date = 10/12/14 Pct Recovery = 63% Analysis Date = 10/12/14 Pct Recovery = 63% Analysis Date = 10/02/14 Pct Recovery = 62% Analysis Date = 10/02/14 Pct Recovery = 62% Analysis Date = 09/22/14 Pct Recovery = 62% Analysis Date = 09/22/14 Pct Recovery = 62% Analysis Date = 09/13/14 Pct Recovery = 62% Analysis Date = 09/13/14 Pct Recovery = 62% Analysis Date = 09/03/14 Pct Recovery = 62% Analysis Date = 09/03/14 Pct Recovery = 62% Analysis Date = 08/24/14 Pct Recovery = 61% Analysis Date = 08/24/14 Pct Recovery = 61% Analysis Date = 08/14/14 Pct Recovery = 61% Analysis Date = 08/14/14 Pct Recovery = 61% Analysis Date = 08/04/14 Pct Recovery = 61% Analysis Date = 08/04/14 Pct Recovery = 61% Analysis Date = 07/26/14 Pct Recovery = 61% Analysis Date = 07/26/14 Pct Recovery = 61% Analysis Date = 07/16/14 Pct Recovery = 61% Analysis Date = 07/16/14 Pct Recovery = 61% Analysis Date = 07/06/14 Pct Recovery = 60% Analysis Date = 07/06/14 Pct Recovery = 60% Analysis Date = 06/26/14 Pct Recovery = 60% Analysis Date = 06/26/14 Pct Recovery = 60% Analysis Date = 06/17/14 Pct Recovery = 61% Analysis Date = 06/17/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 04/29/14 Pct Recovery = 63% Analysis Date = 04/29/14 Pct Recovery = 63% Analysis Date = 04/19/14 Pct Recovery = 64% Analysis Date = 04/19/14 Pct Recovery = 64% Analysis Date = 04/09/14 Pct Recovery = 64% Analysis Date = 04/09/14 Pct Recovery = 64% Analysis Date = 03/30/14 Pct Recovery = 64% Analysis Date = 03/30/14 Pct Recovery = 64% Analysis Date = 03/21/14 Pct Recovery = 65% Analysis Date = 03/21/14 Pct Recovery = 65% Analysis Date = 03/11/14 Pct Recovery = 65% Analysis Date = 03/11/14 Pct Recovery = 65% Analysis Date = 03/01/14 Pct Recovery = 66% Analysis Date = 03/01/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 66% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 01/31/14 Pct Recovery = 67% Analysis Date = 01/31/14 Pct Recovery = 67% Analysis Date = 01/21/14 Pct Recovery = 68% Analysis Date = 01/21/14 Pct Recovery = 68% Analysis Date = 01/11/14 Pct Recovery = 68% Analysis Date = 01/11/14 Pct Recovery = 68% Analysis Date = 01/01/14 Pct Recovery = 69% Analysis Date = 01/01/14 Pct Recovery = 69% Analysis Date = 12/22/13 Pct Recovery = 69% Analysis Date = 12/22/13 Pct Recovery = 69% Analysis Date = 12/13/13 Pct Recovery = 70% Analysis Date = 12/13/13 Pct Recovery = 70% Analysis Date = 12/03/13 Pct Recovery = 70% Analysis Date = 12/03/13 Pct Recovery = 70% Analysis Date = 11/23/13 Pct Recovery = 71% Analysis Date = 11/23/13 Pct Recovery = 71% Analysis Date = 11/13/13 Pct Recovery = 71% Analysis Date = 11/13/13 Pct Recovery = 71% Analysis Date = 11/04/13 Pct Recovery = 71% Analysis Date = 11/04/13 Pct Recovery = 71% Analysis Date = 10/25/13 Pct Recovery = 72% Analysis Date = 10/25/13 Pct Recovery = 72% Analysis Date = 10/15/13 Pct Recovery = 72% Analysis Date = 10/15/13 Pct Recovery = 72% Analysis Date = 10/05/13 Pct Recovery = 72% Analysis Date = 10/05/13 Pct Recovery = 72% Analysis Date = 09/25/13 Pct Recovery = 72% Analysis Date = 09/25/13 Pct Recovery = 72% Analysis Date = 09/16/13 Pct Recovery = 72% Analysis Date = 09/16/13 Pct Recovery = 72% Analysis Date = 09/06/13 Pct Recovery = 72% Analysis Date = 09/06/13 Pct Recovery = 72% Analysis Date = 08/27/13 Pct Recovery = 71% Analysis Date = 08/27/13 Pct Recovery = 71% Analysis Date = 08/17/13 Pct Recovery = 71% Analysis Date = 08/17/13 Pct Recovery = 71% Analysis Date = 08/08/13 Pct Recovery = 71% Analysis Date = 08/08/13 Pct Recovery = 71% Analysis Date = 07/29/13 Pct Recovery = 71% Analysis Date = 07/29/13 Pct Recovery = 71% Analysis Date = 07/19/13 Pct Recovery = 71% Analysis Date = 07/19/13 Pct Recovery = 71% Analysis Date = 07/09/13 Pct Recovery = 71% Analysis Date = 07/09/13 Pct Recovery = 71% Analysis Date = 06/29/13 Pct Recovery = 71% Analysis Date = 06/29/13 Pct Recovery = 71% Analysis Date = 06/20/13 Pct Recovery = 70% Analysis Date = 06/20/13 Pct Recovery = 70% Analysis Date = 06/10/13 Pct Recovery = 70% Analysis Date = 06/10/13 Pct Recovery = 70% Analysis Date = 05/31/13 Pct Recovery = 70% Analysis Date = 05/31/13 Pct Recovery = 70% Analysis Date = 05/21/13 Pct Recovery = 70% Analysis Date = 05/21/13 Pct Recovery = 70% Analysis Date = 05/12/13 Pct Recovery = 70% Analysis Date = 05/12/13 Pct Recovery = 70% Analysis Date = 05/02/13 Pct Recovery = 70% Analysis Date = 05/02/13 Pct Recovery = 70% Analysis Date = 04/22/13 Pct Recovery = 70% Analysis Date = 04/22/13 Pct Recovery = 70% Analysis Date = 04/12/13 Pct Recovery = 69% Analysis Date = 04/12/13 Pct Recovery = 69% Analysis Date = 04/02/13 Pct Recovery = 69% Analysis Date = 04/02/13 Pct Recovery = 69% Analysis Date = 03/24/13 Pct Recovery = 69% Analysis Date = 03/24/13 Pct Recovery = 69% Analysis Date = 03/14/13 Pct Recovery = 69% Analysis Date = 03/14/13 Pct Recovery = 69% Analysis Date = 03/04/13 Pct Recovery = 69% Analysis Date = 03/04/13 Pct Recovery = 69% Analysis Date = 02/22/13 Pct Recovery = 70% Analysis Date = 02/22/13 Pct Recovery = 70% Analysis Date = 02/13/13 Pct Recovery = 70% Analysis Date = 02/13/13 Pct Recovery = 70% Analysis Date = 02/03/13 Pct Recovery = 71% Analysis Date = 02/03/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 71% Analysis Date = 01/14/13 Pct Recovery = 71% Analysis Date = 01/14/13 Pct Recovery = 71% Analysis Date = 01/04/13 Pct Recovery = 72% Analysis Date = 01/04/13 Pct Recovery = 72% Analysis Date = 12/26/12 Pct Recovery = 73% Analysis Date = 12/26/12 Pct Recovery = 73% Analysis Date = 12/16/12 Pct Recovery = 74% Analysis Date = 12/16/12 Pct Recovery = 74% Analysis Date = 12/06/12 Pct Recovery = 74% Analysis Date = 12/06/12 Pct Recovery = 74% Analysis Date = 11/26/12 Pct Recovery = 75% Analysis Date = 11/26/12 Pct Recovery = 75% Analysis Date = 11/17/12 Pct Recovery = 76% Analysis Date = 11/17/12 Pct Recovery = 76% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 10/28/12 Pct Recovery = 78% Analysis Date = 10/28/12 Pct Recovery = 78% Analysis Date = 10/18/12 Pct Recovery = 79% Analysis Date = 10/18/12 Pct Recovery = 79% Analysis Date = 10/08/12 Pct Recovery = 80% Analysis Date = 10/08/12 Pct Recovery = 80% Analysis Date = 09/29/12 Pct Recovery = 81% Analysis Date = 09/29/12 Pct Recovery = 81% Analysis Date = 09/19/12 Pct Recovery = 82% Analysis Date = 09/19/12 Pct Recovery = 82% Analysis Date = 09/09/12 Pct Recovery = 83% Analysis Date = 09/09/12 Pct Recovery = 83% Analysis Date = 08/30/12 Pct Recovery = 84% Analysis Date = 08/30/12 Pct Recovery = 84% Analysis Date = 08/20/12 Pct Recovery = 84% Analysis Date = 08/20/12 Pct Recovery = 84% Analysis Date = 08/11/12 Pct Recovery = 84% Analysis Date = 08/11/12 Pct Recovery = 84% Analysis Date = 08/01/12 Pct Recovery = 85% Analysis Date = 08/01/12 Pct Recovery = 85% Analysis Date = 07/22/12 Pct Recovery = 85% Analysis Date = 07/22/12 Pct Recovery = 85% Analysis Date = 07/12/12 Pct Recovery = 85% Analysis Date = 07/12/12 Pct Recovery = 85% Analysis Date = 07/03/12 Pct Recovery = 85% Analysis Date = 07/03/12 Pct Recovery = 85% Analysis Date = 06/23/12 Pct Recovery = 85% Analysis Date = 06/23/12 Pct Recovery = 85% Analysis Date = 06/13/12 Pct Recovery = 85% Analysis Date = 06/13/12 Pct Recovery = 85% Analysis Date = 06/03/12 Pct Recovery = 85% Analysis Date = 06/03/12 Pct Recovery = 85% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/15/12 Pct Recovery = 86% Analysis Date = 05/15/12 Pct Recovery = 86% Analysis Date = 05/05/12 Pct Recovery = 86% Analysis Date = 05/05/12 Pct Recovery = 86% Analysis Date = 04/25/12 Pct Recovery = 86% Analysis Date = 04/25/12 Pct Recovery = 86% Analysis Date = 04/15/12 Pct Recovery = 86% Analysis Date = 04/15/12 Pct Recovery = 86% Analysis Date = 04/06/12 Pct Recovery = 86% Analysis Date = 04/06/12 Pct Recovery = 86% Analysis Date = 03/27/12 Pct Recovery = 87% Analysis Date = 03/27/12 Pct Recovery = 87% Analysis Date = 03/17/12 Pct Recovery = 87% Analysis Date = 03/17/12 Pct Recovery = 87% Analysis Date = 03/07/12 Pct Recovery = 87% Analysis Date = 03/07/12 Pct Recovery = 87% Analysis Date = 02/26/12 Pct Recovery = 87% Analysis Date = 02/26/12 Pct Recovery = 87% Analysis Date = 02/17/12 Pct Recovery = 87% Analysis Date = 02/17/12 Pct Recovery = 87% Analysis Date = 02/07/12 Pct Recovery = 87% Analysis Date = 02/07/12 Pct Recovery = 87% Analysis Date = 01/28/12 Pct Recovery = 87% Analysis Date = 01/28/12 Pct Recovery = 87% Analysis Date = 01/18/12 Pct Recovery = 88% Analysis Date = 01/18/12 Pct Recovery = 88% Analysis Date = 01/09/12 Pct Recovery = 88% Analysis Date = 01/09/12 Pct Recovery = 88% Analysis Date = 12/30/11 Pct Recovery = 88% Analysis Date = 12/30/11 Pct Recovery = 88% Analysis Date = 12/20/11 Pct Recovery = 88% Analysis Date = 12/20/11 Pct Recovery = 88% Analysis Date = 12/10/11 Pct Recovery = 88% Analysis Date = 12/10/11 Pct Recovery = 88% Analysis Date = 11/30/11 Pct Recovery = 88% Analysis Date = 11/30/11 Pct Recovery = 88% Analysis Date = 11/21/11 Pct Recovery = 88% Analysis Date = 11/21/11 Pct Recovery = 88% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 11/01/11 Pct Recovery = 89% Analysis Date = 11/01/11 Pct Recovery = 89% Analysis Date = 10/22/11 Pct Recovery = 89% Analysis Date = 10/22/11 Pct Recovery = 89% Analysis Date = 10/13/11 Pct Recovery = 89% Analysis Date = 10/13/11 Pct Recovery = 89% Analysis Date = 10/03/11 Pct Recovery = 89% Analysis Date = 10/03/11 Pct Recovery = 89% Analysis Date = 09/23/11 Pct Recovery = 89% Analysis Date = 09/23/11 Pct Recovery = 89% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/03/11 Pct Recovery = 90% Analysis Date = 09/03/11 Pct Recovery = 90% Analysis Date = 08/25/11 Pct Recovery = 90% Analysis Date = 08/25/11 Pct Recovery = 90% Analysis Date = 08/15/11 Pct Recovery = 90% Analysis Date = 08/15/11 Pct Recovery = 90% Analysis Date = 08/05/11 Pct Recovery = 90% Analysis Date = 08/05/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/17/11 Pct Recovery = 90% Analysis Date = 07/17/11 Pct Recovery = 90% Analysis Date = 07/07/11 Pct Recovery = 91% Analysis Date = 07/07/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/17/11 Pct Recovery = 91% Analysis Date = 06/17/11 Pct Recovery = 91% Analysis Date = 06/07/11 Pct Recovery = 91% Analysis Date = 06/07/11 Pct Recovery = 91% Analysis Date = 05/29/11 Pct Recovery = 91% Analysis Date = 05/29/11 Pct Recovery = 91% Analysis Date = 05/19/11 Pct Recovery = 91% Analysis Date = 05/19/11 Pct Recovery = 91% Analysis Date = 05/09/11 Pct Recovery = 91% Analysis Date = 05/09/11 Pct Recovery = 91% Analysis Date = 04/29/11 Pct Recovery = 92% Analysis Date = 04/29/11 Pct Recovery = 92% Analysis Date = 04/20/11 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL-OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 45 71% 25% 65% 16%
Total 45 71% 25% 65% 16%

Sample Statistics
AZINPHOS-METHYL-OXON

Characteristic N % % Basis
Plotted 45 78% Spiked
Estimated Values 45 78% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 58 .  
False Negatives 12 21% 12 out of 58
Not Spiked 111 .  
False Positives 1 1% 1 out of 110

BQS OBSP Determination:
BENFLURALIN
METHOD: 2033 , TESTIDCODE: 82673GCM35
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 59% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 82% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 62% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 66% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 87% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 71% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 84% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 101% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 79% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 83% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 66% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 58% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 76% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 79% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 51% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 86% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 74% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 111% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 72% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 60% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 69% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 87% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 53% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 77% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 83% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 76% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 64% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 86% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 66% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 77% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 88% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 106% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 80% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 78% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 97% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 78% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 85% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 78% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 89% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 96% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 83% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 79% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 87% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 71% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 68% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 68% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 73% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 111% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 87% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 56% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 81% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 78% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 62% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 69% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 74% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 80% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 81% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 103% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 64% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 80% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 55% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 106% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 97% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 65% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 89% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 97% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 97% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 90% Analysis Date = 12/19/16 Pct Recovery = 65% Analysis Date = 12/09/16 Pct Recovery = 65% Analysis Date = 12/09/16 Pct Recovery = 65% Analysis Date = 11/28/16 Pct Recovery = 65% Analysis Date = 11/28/16 Pct Recovery = 65% Analysis Date = 11/17/16 Pct Recovery = 65% Analysis Date = 11/17/16 Pct Recovery = 65% Analysis Date = 11/07/16 Pct Recovery = 66% Analysis Date = 11/07/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/27/16 Pct Recovery = 66% Analysis Date = 10/16/16 Pct Recovery = 66% Analysis Date = 10/16/16 Pct Recovery = 66% Analysis Date = 10/06/16 Pct Recovery = 66% Analysis Date = 10/06/16 Pct Recovery = 66% Analysis Date = 09/25/16 Pct Recovery = 66% Analysis Date = 09/25/16 Pct Recovery = 66% Analysis Date = 09/14/16 Pct Recovery = 66% Analysis Date = 09/14/16 Pct Recovery = 66% Analysis Date = 09/03/16 Pct Recovery = 66% Analysis Date = 09/03/16 Pct Recovery = 66% Analysis Date = 08/24/16 Pct Recovery = 66% Analysis Date = 08/24/16 Pct Recovery = 66% Analysis Date = 08/13/16 Pct Recovery = 66% Analysis Date = 08/13/16 Pct Recovery = 66% Analysis Date = 08/02/16 Pct Recovery = 66% Analysis Date = 08/02/16 Pct Recovery = 66% Analysis Date = 07/23/16 Pct Recovery = 67% Analysis Date = 07/23/16 Pct Recovery = 67% Analysis Date = 07/12/16 Pct Recovery = 67% Analysis Date = 07/12/16 Pct Recovery = 67% Analysis Date = 07/01/16 Pct Recovery = 67% Analysis Date = 07/01/16 Pct Recovery = 67% Analysis Date = 06/20/16 Pct Recovery = 67% Analysis Date = 06/20/16 Pct Recovery = 67% Analysis Date = 06/10/16 Pct Recovery = 67% Analysis Date = 06/10/16 Pct Recovery = 67% Analysis Date = 05/30/16 Pct Recovery = 67% Analysis Date = 05/30/16 Pct Recovery = 67% Analysis Date = 05/19/16 Pct Recovery = 67% Analysis Date = 05/19/16 Pct Recovery = 67% Analysis Date = 05/09/16 Pct Recovery = 67% Analysis Date = 05/09/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/06/16 Pct Recovery = 67% Analysis Date = 04/06/16 Pct Recovery = 67% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 68% Analysis Date = 02/24/16 Pct Recovery = 68% Analysis Date = 02/24/16 Pct Recovery = 68% Analysis Date = 02/13/16 Pct Recovery = 68% Analysis Date = 02/13/16 Pct Recovery = 68% Analysis Date = 02/02/16 Pct Recovery = 68% Analysis Date = 02/02/16 Pct Recovery = 68% Analysis Date = 01/22/16 Pct Recovery = 68% Analysis Date = 01/22/16 Pct Recovery = 68% Analysis Date = 01/12/16 Pct Recovery = 68% Analysis Date = 01/12/16 Pct Recovery = 68% Analysis Date = 01/01/16 Pct Recovery = 68% Analysis Date = 01/01/16 Pct Recovery = 68% Analysis Date = 12/21/15 Pct Recovery = 68% Analysis Date = 12/21/15 Pct Recovery = 68% Analysis Date = 12/11/15 Pct Recovery = 68% Analysis Date = 12/11/15 Pct Recovery = 68% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/19/15 Pct Recovery = 69% Analysis Date = 11/19/15 Pct Recovery = 69% Analysis Date = 11/09/15 Pct Recovery = 69% Analysis Date = 11/09/15 Pct Recovery = 69% Analysis Date = 10/29/15 Pct Recovery = 69% Analysis Date = 10/29/15 Pct Recovery = 69% Analysis Date = 10/18/15 Pct Recovery = 69% Analysis Date = 10/18/15 Pct Recovery = 69% Analysis Date = 10/07/15 Pct Recovery = 69% Analysis Date = 10/07/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/05/15 Pct Recovery = 69% Analysis Date = 09/05/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 70% Analysis Date = 08/04/15 Pct Recovery = 70% Analysis Date = 07/24/15 Pct Recovery = 70% Analysis Date = 07/24/15 Pct Recovery = 70% Analysis Date = 07/14/15 Pct Recovery = 70% Analysis Date = 07/14/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 06/22/15 Pct Recovery = 70% Analysis Date = 06/22/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/12/15 Pct Recovery = 70% Analysis Date = 06/01/15 Pct Recovery = 70% Analysis Date = 06/01/15 Pct Recovery = 70% Analysis Date = 05/21/15 Pct Recovery = 70% Analysis Date = 05/21/15 Pct Recovery = 70% Analysis Date = 05/10/15 Pct Recovery = 70% Analysis Date = 05/10/15 Pct Recovery = 70% Analysis Date = 04/30/15 Pct Recovery = 70% Analysis Date = 04/30/15 Pct Recovery = 70% Analysis Date = 04/19/15 Pct Recovery = 70% Analysis Date = 04/19/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 71% Analysis Date = 04/08/15 Pct Recovery = 71% Analysis Date = 03/29/15 Pct Recovery = 71% Analysis Date = 03/29/15 Pct Recovery = 71% Analysis Date = 03/18/15 Pct Recovery = 71% Analysis Date = 03/18/15 Pct Recovery = 71% Analysis Date = 03/07/15 Pct Recovery = 71% Analysis Date = 03/07/15 Pct Recovery = 71% Analysis Date = 02/24/15 Pct Recovery = 71% Analysis Date = 02/24/15 Pct Recovery = 71% Analysis Date = 02/14/15 Pct Recovery = 71% Analysis Date = 02/14/15 Pct Recovery = 71% Analysis Date = 02/03/15 Pct Recovery = 71% Analysis Date = 02/03/15 Pct Recovery = 71% Analysis Date = 01/23/15 Pct Recovery = 71% Analysis Date = 01/23/15 Pct Recovery = 71% Analysis Date = 01/13/15 Pct Recovery = 71% Analysis Date = 01/13/15 Pct Recovery = 71% Analysis Date = 01/02/15 Pct Recovery = 72% Analysis Date = 01/02/15 Pct Recovery = 72% Analysis Date = 12/22/14 Pct Recovery = 72% Analysis Date = 12/22/14 Pct Recovery = 72% Analysis Date = 12/12/14 Pct Recovery = 72% Analysis Date = 12/12/14 Pct Recovery = 72% Analysis Date = 12/01/14 Pct Recovery = 72% Analysis Date = 12/01/14 Pct Recovery = 72% Analysis Date = 11/20/14 Pct Recovery = 72% Analysis Date = 11/20/14 Pct Recovery = 72% Analysis Date = 11/09/14 Pct Recovery = 72% Analysis Date = 11/09/14 Pct Recovery = 72% Analysis Date = 10/30/14 Pct Recovery = 72% Analysis Date = 10/30/14 Pct Recovery = 72% Analysis Date = 10/19/14 Pct Recovery = 72% Analysis Date = 10/19/14 Pct Recovery = 72% Analysis Date = 10/08/14 Pct Recovery = 72% Analysis Date = 10/08/14 Pct Recovery = 72% Analysis Date = 09/28/14 Pct Recovery = 73% Analysis Date = 09/28/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/17/14 Pct Recovery = 73% Analysis Date = 09/06/14 Pct Recovery = 73% Analysis Date = 09/06/14 Pct Recovery = 73% Analysis Date = 08/26/14 Pct Recovery = 73% Analysis Date = 08/26/14 Pct Recovery = 73% Analysis Date = 08/16/14 Pct Recovery = 73% Analysis Date = 08/16/14 Pct Recovery = 73% Analysis Date = 08/05/14 Pct Recovery = 73% Analysis Date = 08/05/14 Pct Recovery = 73% Analysis Date = 07/25/14 Pct Recovery = 73% Analysis Date = 07/25/14 Pct Recovery = 73% Analysis Date = 07/15/14 Pct Recovery = 73% Analysis Date = 07/15/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 07/04/14 Pct Recovery = 73% Analysis Date = 06/23/14 Pct Recovery = 73% Analysis Date = 06/23/14 Pct Recovery = 73% Analysis Date = 06/12/14 Pct Recovery = 73% Analysis Date = 06/12/14 Pct Recovery = 73% Analysis Date = 06/02/14 Pct Recovery = 74% Analysis Date = 06/02/14 Pct Recovery = 74% Analysis Date = 05/22/14 Pct Recovery = 74% Analysis Date = 05/22/14 Pct Recovery = 74% Analysis Date = 05/11/14 Pct Recovery = 74% Analysis Date = 05/11/14 Pct Recovery = 74% Analysis Date = 05/01/14 Pct Recovery = 74% Analysis Date = 05/01/14 Pct Recovery = 74% Analysis Date = 04/20/14 Pct Recovery = 74% Analysis Date = 04/20/14 Pct Recovery = 74% Analysis Date = 04/09/14 Pct Recovery = 74% Analysis Date = 04/09/14 Pct Recovery = 74% Analysis Date = 03/29/14 Pct Recovery = 74% Analysis Date = 03/29/14 Pct Recovery = 74% Analysis Date = 03/19/14 Pct Recovery = 74% Analysis Date = 03/19/14 Pct Recovery = 74% Analysis Date = 03/08/14 Pct Recovery = 74% Analysis Date = 03/08/14 Pct Recovery = 74% Analysis Date = 02/25/14 Pct Recovery = 74% Analysis Date = 02/25/14 Pct Recovery = 74% Analysis Date = 02/15/14 Pct Recovery = 74% Analysis Date = 02/15/14 Pct Recovery = 74% Analysis Date = 02/04/14 Pct Recovery = 75% Analysis Date = 02/04/14 Pct Recovery = 75% Analysis Date = 01/24/14 Pct Recovery = 75% Analysis Date = 01/24/14 Pct Recovery = 75% Analysis Date = 01/13/14 Pct Recovery = 75% Analysis Date = 01/13/14 Pct Recovery = 75% Analysis Date = 01/03/14 Pct Recovery = 75% Analysis Date = 01/03/14 Pct Recovery = 75% Analysis Date = 12/23/13 Pct Recovery = 75% Analysis Date = 12/23/13 Pct Recovery = 75% Analysis Date = 12/12/13 Pct Recovery = 75% Analysis Date = 12/12/13 Pct Recovery = 75% Analysis Date = 12/02/13 Pct Recovery = 75% Analysis Date = 12/02/13 Pct Recovery = 75% Analysis Date = 11/21/13 Pct Recovery = 75% Analysis Date = 11/21/13 Pct Recovery = 75% Analysis Date = 11/10/13 Pct Recovery = 76% Analysis Date = 11/10/13 Pct Recovery = 76% Analysis Date = 10/31/13 Pct Recovery = 76% Analysis Date = 10/31/13 Pct Recovery = 76% Analysis Date = 10/20/13 Pct Recovery = 76% Analysis Date = 10/20/13 Pct Recovery = 76% Analysis Date = 10/09/13 Pct Recovery = 76% Analysis Date = 10/09/13 Pct Recovery = 76% Analysis Date = 09/28/13 Pct Recovery = 76% Analysis Date = 09/28/13 Pct Recovery = 76% Analysis Date = 09/18/13 Pct Recovery = 76% Analysis Date = 09/18/13 Pct Recovery = 76% Analysis Date = 09/07/13 Pct Recovery = 77% Analysis Date = 09/07/13 Pct Recovery = 77% Analysis Date = 08/27/13 Pct Recovery = 77% Analysis Date = 08/27/13 Pct Recovery = 77% Analysis Date = 08/17/13 Pct Recovery = 77% Analysis Date = 08/17/13 Pct Recovery = 77% Analysis Date = 08/06/13 Pct Recovery = 77% Analysis Date = 08/06/13 Pct Recovery = 77% Analysis Date = 07/26/13 Pct Recovery = 77% Analysis Date = 07/26/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 78% Analysis Date = 07/15/13 Pct Recovery = 78% Analysis Date = 07/05/13 Pct Recovery = 78% Analysis Date = 07/05/13 Pct Recovery = 78% Analysis Date = 06/24/13 Pct Recovery = 78% Analysis Date = 06/24/13 Pct Recovery = 78% Analysis Date = 06/13/13 Pct Recovery = 78% Analysis Date = 06/13/13 Pct Recovery = 78% Analysis Date = 06/03/13 Pct Recovery = 78% Analysis Date = 06/03/13 Pct Recovery = 78% Analysis Date = 05/23/13 Pct Recovery = 79% Analysis Date = 05/23/13 Pct Recovery = 79% Analysis Date = 05/12/13 Pct Recovery = 79% Analysis Date = 05/12/13 Pct Recovery = 79% Analysis Date = 05/01/13 Pct Recovery = 79% Analysis Date = 05/01/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/10/13 Pct Recovery = 79% Analysis Date = 04/10/13 Pct Recovery = 79% Analysis Date = 03/30/13 Pct Recovery = 80% Analysis Date = 03/30/13 Pct Recovery = 80% Analysis Date = 03/20/13 Pct Recovery = 80% Analysis Date = 03/20/13 Pct Recovery = 80% Analysis Date = 03/09/13 Pct Recovery = 80% Analysis Date = 03/09/13 Pct Recovery = 80% Analysis Date = 02/26/13 Pct Recovery = 80% Analysis Date = 02/26/13 Pct Recovery = 80% Analysis Date = 02/15/13 Pct Recovery = 80% Analysis Date = 02/15/13 Pct Recovery = 80% Analysis Date = 02/05/13 Pct Recovery = 81% Analysis Date = 02/05/13 Pct Recovery = 81% Analysis Date = 01/25/13 Pct Recovery = 81% Analysis Date = 01/25/13 Pct Recovery = 81% Analysis Date = 01/14/13 Pct Recovery = 81% Analysis Date = 01/14/13 Pct Recovery = 81% Analysis Date = 01/04/13 Pct Recovery = 81% Analysis Date = 01/04/13 Pct Recovery = 81% Analysis Date = 12/24/12 Pct Recovery = 81% Analysis Date = 12/24/12 Pct Recovery = 81% Analysis Date = 12/13/12 Pct Recovery = 81% Analysis Date = 12/13/12 Pct Recovery = 81% Analysis Date = 12/03/12 Pct Recovery = 82% Analysis Date = 12/03/12 Pct Recovery = 82% Analysis Date = 11/22/12 Pct Recovery = 82% Analysis Date = 11/22/12 Pct Recovery = 82% Analysis Date = 11/11/12 Pct Recovery = 82% Analysis Date = 11/11/12 Pct Recovery = 82% Analysis Date = 10/31/12 Pct Recovery = 82% Analysis Date = 10/31/12 Pct Recovery = 82% Analysis Date = 10/21/12 Pct Recovery = 82% Analysis Date = 10/21/12 Pct Recovery = 82% Analysis Date = 10/10/12 Pct Recovery = 82% Analysis Date = 10/10/12 Pct Recovery = 82% Analysis Date = 09/29/12 Pct Recovery = 82% Analysis Date = 09/29/12 Pct Recovery = 82% Analysis Date = 09/19/12 Pct Recovery = 83% Analysis Date = 09/19/12 Pct Recovery = 83% Analysis Date = 09/08/12 Pct Recovery = 83% Analysis Date = 09/08/12 Pct Recovery = 83% Analysis Date = 08/28/12 Pct Recovery = 83% Analysis Date = 08/28/12 Pct Recovery = 83% Analysis Date = 08/17/12 Pct Recovery = 83% Analysis Date = 08/17/12 Pct Recovery = 83% Analysis Date = 08/07/12 Pct Recovery = 83% Analysis Date = 08/07/12 Pct Recovery = 83% Analysis Date = 07/27/12 Pct Recovery = 83% Analysis Date = 07/27/12 Pct Recovery = 83% Analysis Date = 07/16/12 Pct Recovery = 83% Analysis Date = 07/16/12 Pct Recovery = 83% Analysis Date = 07/06/12 Pct Recovery = 83% Analysis Date = 07/06/12 Pct Recovery = 83% Analysis Date = 06/25/12 Pct Recovery = 83% Analysis Date = 06/25/12 Pct Recovery = 83% Analysis Date = 06/14/12 Pct Recovery = 83% Analysis Date = 06/14/12 Pct Recovery = 83% Analysis Date = 06/03/12 Pct Recovery = 83% Analysis Date = 06/03/12 Pct Recovery = 83% Analysis Date = 05/24/12 Pct Recovery = 83% Analysis Date = 05/24/12 Pct Recovery = 83% Analysis Date = 05/13/12 Pct Recovery = 84% Analysis Date = 05/13/12 Pct Recovery = 84% Analysis Date = 05/02/12 Pct Recovery = 84% Analysis Date = 05/02/12 Pct Recovery = 84% Analysis Date = 04/22/12 Pct Recovery = 84% Analysis Date = 04/22/12 Pct Recovery = 84% Analysis Date = 04/11/12 Pct Recovery = 84% Analysis Date = 04/11/12 Pct Recovery = 84% Analysis Date = 03/31/12 Pct Recovery = 84% Analysis Date = 03/31/12 Pct Recovery = 84% Analysis Date = 03/20/12 Pct Recovery = 84% Analysis Date = 03/20/12 Pct Recovery = 84% Analysis Date = 03/10/12 Pct Recovery = 84% Analysis Date = 03/10/12 Pct Recovery = 84% Analysis Date = 02/28/12 Pct Recovery = 84% Analysis Date = 02/28/12 Pct Recovery = 84% Analysis Date = 02/17/12 Pct Recovery = 84% Analysis Date = 02/17/12 Pct Recovery = 84% Analysis Date = 02/07/12 Pct Recovery = 84% Analysis Date = 02/07/12 Pct Recovery = 84% Analysis Date = 01/27/12 Pct Recovery = 84% Analysis Date = 01/27/12 Pct Recovery = 84% Analysis Date = 01/16/12 Pct Recovery = 84% Analysis Date = 01/16/12 Pct Recovery = 84% Analysis Date = 01/06/12 Pct Recovery = 84% Analysis Date = 01/06/12 Pct Recovery = 84% Analysis Date = 12/26/11 Pct Recovery = 85% Analysis Date = 12/26/11 Pct Recovery = 85% Analysis Date = 12/15/11 Pct Recovery = 85% Analysis Date = 12/15/11 Pct Recovery = 85% Analysis Date = 12/04/11 Pct Recovery = 85% Analysis Date = 12/04/11 Pct Recovery = 85% Analysis Date = 11/24/11 Pct Recovery = 85% Analysis Date = 11/24/11 Pct Recovery = 85% Analysis Date = 11/13/11 Pct Recovery = 85% Analysis Date = 11/13/11 Pct Recovery = 85% Analysis Date = 11/02/11 Pct Recovery = 85% Analysis Date = 11/02/11 Pct Recovery = 85% Analysis Date = 10/23/11 Pct Recovery = 85% Analysis Date = 10/23/11 Pct Recovery = 85% Analysis Date = 10/12/11 Pct Recovery = 85% Analysis Date = 10/12/11 Pct Recovery = 85% Analysis Date = 10/01/11 Pct Recovery = 85% Analysis Date = 10/01/11 Pct Recovery = 85% Analysis Date = 09/20/11 Pct Recovery = 85% Analysis Date = 09/20/11 Pct Recovery = 85% Analysis Date = 09/10/11 Pct Recovery = 85% Analysis Date = 09/10/11 Pct Recovery = 85% Analysis Date = 08/30/11 Pct Recovery = 85% Analysis Date = 08/30/11 Pct Recovery = 85% Analysis Date = 08/19/11 Pct Recovery = 85% Analysis Date = 08/19/11 Pct Recovery = 85% Analysis Date = 08/09/11 Pct Recovery = 85% Analysis Date = 08/09/11 Pct Recovery = 85% Analysis Date = 07/29/11 Pct Recovery = 85% Analysis Date = 07/29/11 Pct Recovery = 85% Analysis Date = 07/18/11 Pct Recovery = 86% Analysis Date = 07/18/11 Pct Recovery = 86% Analysis Date = 07/07/11 Pct Recovery = 86% Analysis Date = 07/07/11 Pct Recovery = 86% Analysis Date = 06/27/11 Pct Recovery = 86% Analysis Date = 06/27/11 Pct Recovery = 86% Analysis Date = 06/16/11 Pct Recovery = 86% Analysis Date = 06/16/11 Pct Recovery = 86% Analysis Date = 06/05/11 Pct Recovery = 86% Analysis Date = 06/05/11 Pct Recovery = 86% Analysis Date = 05/26/11 Pct Recovery = 86% Analysis Date = 05/26/11 Pct Recovery = 86% Analysis Date = 05/15/11 Pct Recovery = 86% Analysis Date = 05/15/11 Pct Recovery = 86% Analysis Date = 05/04/11 Pct Recovery = 86% Analysis Date = 05/04/11 Pct Recovery = 86% Analysis Date = 04/23/11 Pct Recovery = 86% Analysis Date = 04/23/11 Pct Recovery = 86% Analysis Date = 04/13/11 Pct Recovery = 86% Analysis Date = 04/13/11 Pct Recovery = 86% Analysis Date = 04/02/11 Pct Recovery = 86% Analysis Date = 04/02/11 Pct Recovery = 86% Analysis Date = 03/22/11 Pct Recovery = 86% Analysis Date = 03/22/11 Pct Recovery = 86% Analysis Date = 03/12/11 Pct Recovery = 86% Analysis Date = 03/12/11 Pct Recovery = 86% Analysis Date = 03/01/11 Pct Recovery = 86% Analysis Date = 03/01/11 Pct Recovery = 86% Analysis Date = 02/18/11 Pct Recovery = 86% Analysis Date = 02/18/11 Pct Recovery = 86% Analysis Date = 02/08/11 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENFLURALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 77% 14% 77% 15%
Total 87 77% 14% 77% 15%

Sample Statistics
BENFLURALIN

Characteristic N % % Basis
Plotted 87 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 0 0% 0 out of 87
Not Spiked 82 .  
False Positives 1 1% 1 out of 82

BQS OBSP Determination:
CARBARYL
METHOD: 2033 , TESTIDCODE: 82680GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 102% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 99% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 99% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 36% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 89% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 82% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 70% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 51% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 115% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 72% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 103% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 94% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 76% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 98% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 53% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 73% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 94% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 81% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 82% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 96% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 80% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 70% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 97% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 67% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 73% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 96% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 88% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 69% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 74% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 58% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 59% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 86% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 53% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 95% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 60% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 62% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 67% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 93% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 81% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 82% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 95% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 50% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 57% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 66% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 78% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 69% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 60% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 53% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 54% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 85% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 91% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 106% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 81% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 90% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 72% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 68% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 89% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 70% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 75% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 58% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 78% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 69% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 64% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 53% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 44% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 74% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 43% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 112% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 79% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 70% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 73% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 123% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 114% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 86% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 115% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 86% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 117% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 94% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 96% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 117% Analysis Date = 01/17/17 Pct Recovery = 61% Analysis Date = 01/07/17 Pct Recovery = 62% Analysis Date = 01/07/17 Pct Recovery = 62% Analysis Date = 12/27/16 Pct Recovery = 62% Analysis Date = 12/27/16 Pct Recovery = 62% Analysis Date = 12/16/16 Pct Recovery = 62% Analysis Date = 12/16/16 Pct Recovery = 62% Analysis Date = 12/05/16 Pct Recovery = 62% Analysis Date = 12/05/16 Pct Recovery = 62% Analysis Date = 11/24/16 Pct Recovery = 62% Analysis Date = 11/24/16 Pct Recovery = 62% Analysis Date = 11/13/16 Pct Recovery = 62% Analysis Date = 11/13/16 Pct Recovery = 62% Analysis Date = 11/03/16 Pct Recovery = 62% Analysis Date = 11/03/16 Pct Recovery = 62% Analysis Date = 10/23/16 Pct Recovery = 62% Analysis Date = 10/23/16 Pct Recovery = 62% Analysis Date = 10/12/16 Pct Recovery = 63% Analysis Date = 10/12/16 Pct Recovery = 63% Analysis Date = 10/01/16 Pct Recovery = 63% Analysis Date = 10/01/16 Pct Recovery = 63% Analysis Date = 09/20/16 Pct Recovery = 63% Analysis Date = 09/20/16 Pct Recovery = 63% Analysis Date = 09/09/16 Pct Recovery = 63% Analysis Date = 09/09/16 Pct Recovery = 63% Analysis Date = 08/29/16 Pct Recovery = 63% Analysis Date = 08/29/16 Pct Recovery = 63% Analysis Date = 08/19/16 Pct Recovery = 63% Analysis Date = 08/19/16 Pct Recovery = 63% Analysis Date = 08/08/16 Pct Recovery = 63% Analysis Date = 08/08/16 Pct Recovery = 63% Analysis Date = 07/28/16 Pct Recovery = 63% Analysis Date = 07/28/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/06/16 Pct Recovery = 64% Analysis Date = 07/06/16 Pct Recovery = 64% Analysis Date = 06/25/16 Pct Recovery = 64% Analysis Date = 06/25/16 Pct Recovery = 64% Analysis Date = 06/14/16 Pct Recovery = 64% Analysis Date = 06/14/16 Pct Recovery = 64% Analysis Date = 06/04/16 Pct Recovery = 64% Analysis Date = 06/04/16 Pct Recovery = 64% Analysis Date = 05/24/16 Pct Recovery = 64% Analysis Date = 05/24/16 Pct Recovery = 64% Analysis Date = 05/13/16 Pct Recovery = 64% Analysis Date = 05/13/16 Pct Recovery = 64% Analysis Date = 05/02/16 Pct Recovery = 64% Analysis Date = 05/02/16 Pct Recovery = 64% Analysis Date = 04/21/16 Pct Recovery = 65% Analysis Date = 04/21/16 Pct Recovery = 65% Analysis Date = 04/10/16 Pct Recovery = 65% Analysis Date = 04/10/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/20/16 Pct Recovery = 65% Analysis Date = 03/20/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/16/16 Pct Recovery = 65% Analysis Date = 02/16/16 Pct Recovery = 65% Analysis Date = 02/05/16 Pct Recovery = 65% Analysis Date = 02/05/16 Pct Recovery = 65% Analysis Date = 01/25/16 Pct Recovery = 66% Analysis Date = 01/25/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/04/16 Pct Recovery = 66% Analysis Date = 01/04/16 Pct Recovery = 66% Analysis Date = 12/24/15 Pct Recovery = 66% Analysis Date = 12/24/15 Pct Recovery = 66% Analysis Date = 12/13/15 Pct Recovery = 66% Analysis Date = 12/13/15 Pct Recovery = 66% Analysis Date = 12/02/15 Pct Recovery = 66% Analysis Date = 12/02/15 Pct Recovery = 66% Analysis Date = 11/21/15 Pct Recovery = 66% Analysis Date = 11/21/15 Pct Recovery = 66% Analysis Date = 11/10/15 Pct Recovery = 66% Analysis Date = 11/10/15 Pct Recovery = 66% Analysis Date = 10/31/15 Pct Recovery = 67% Analysis Date = 10/31/15 Pct Recovery = 67% Analysis Date = 10/20/15 Pct Recovery = 67% Analysis Date = 10/20/15 Pct Recovery = 67% Analysis Date = 10/09/15 Pct Recovery = 67% Analysis Date = 10/09/15 Pct Recovery = 67% Analysis Date = 09/28/15 Pct Recovery = 67% Analysis Date = 09/28/15 Pct Recovery = 67% Analysis Date = 09/17/15 Pct Recovery = 67% Analysis Date = 09/17/15 Pct Recovery = 67% Analysis Date = 09/06/15 Pct Recovery = 67% Analysis Date = 09/06/15 Pct Recovery = 67% Analysis Date = 08/27/15 Pct Recovery = 67% Analysis Date = 08/27/15 Pct Recovery = 67% Analysis Date = 08/16/15 Pct Recovery = 67% Analysis Date = 08/16/15 Pct Recovery = 67% Analysis Date = 08/05/15 Pct Recovery = 68% Analysis Date = 08/05/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/14/15 Pct Recovery = 68% Analysis Date = 07/14/15 Pct Recovery = 68% Analysis Date = 07/03/15 Pct Recovery = 68% Analysis Date = 07/03/15 Pct Recovery = 68% Analysis Date = 06/22/15 Pct Recovery = 68% Analysis Date = 06/22/15 Pct Recovery = 68% Analysis Date = 06/12/15 Pct Recovery = 68% Analysis Date = 06/12/15 Pct Recovery = 68% Analysis Date = 06/01/15 Pct Recovery = 68% Analysis Date = 06/01/15 Pct Recovery = 68% Analysis Date = 05/21/15 Pct Recovery = 68% Analysis Date = 05/21/15 Pct Recovery = 68% Analysis Date = 05/10/15 Pct Recovery = 69% Analysis Date = 05/10/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/07/15 Pct Recovery = 70% Analysis Date = 04/07/15 Pct Recovery = 70% Analysis Date = 03/28/15 Pct Recovery = 70% Analysis Date = 03/28/15 Pct Recovery = 70% Analysis Date = 03/17/15 Pct Recovery = 70% Analysis Date = 03/17/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 02/23/15 Pct Recovery = 71% Analysis Date = 02/23/15 Pct Recovery = 71% Analysis Date = 02/12/15 Pct Recovery = 71% Analysis Date = 02/12/15 Pct Recovery = 71% Analysis Date = 02/01/15 Pct Recovery = 71% Analysis Date = 02/01/15 Pct Recovery = 71% Analysis Date = 01/22/15 Pct Recovery = 72% Analysis Date = 01/22/15 Pct Recovery = 72% Analysis Date = 01/11/15 Pct Recovery = 72% Analysis Date = 01/11/15 Pct Recovery = 72% Analysis Date = 12/31/14 Pct Recovery = 72% Analysis Date = 12/31/14 Pct Recovery = 72% Analysis Date = 12/20/14 Pct Recovery = 72% Analysis Date = 12/20/14 Pct Recovery = 72% Analysis Date = 12/09/14 Pct Recovery = 73% Analysis Date = 12/09/14 Pct Recovery = 73% Analysis Date = 11/28/14 Pct Recovery = 73% Analysis Date = 11/28/14 Pct Recovery = 73% Analysis Date = 11/17/14 Pct Recovery = 73% Analysis Date = 11/17/14 Pct Recovery = 73% Analysis Date = 11/07/14 Pct Recovery = 74% Analysis Date = 11/07/14 Pct Recovery = 74% Analysis Date = 10/27/14 Pct Recovery = 74% Analysis Date = 10/27/14 Pct Recovery = 74% Analysis Date = 10/16/14 Pct Recovery = 74% Analysis Date = 10/16/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 09/24/14 Pct Recovery = 75% Analysis Date = 09/24/14 Pct Recovery = 75% Analysis Date = 09/13/14 Pct Recovery = 75% Analysis Date = 09/13/14 Pct Recovery = 75% Analysis Date = 09/02/14 Pct Recovery = 75% Analysis Date = 09/02/14 Pct Recovery = 75% Analysis Date = 08/23/14 Pct Recovery = 76% Analysis Date = 08/23/14 Pct Recovery = 76% Analysis Date = 08/12/14 Pct Recovery = 76% Analysis Date = 08/12/14 Pct Recovery = 76% Analysis Date = 08/01/14 Pct Recovery = 76% Analysis Date = 08/01/14 Pct Recovery = 76% Analysis Date = 07/21/14 Pct Recovery = 76% Analysis Date = 07/21/14 Pct Recovery = 76% Analysis Date = 07/10/14 Pct Recovery = 77% Analysis Date = 07/10/14 Pct Recovery = 77% Analysis Date = 06/29/14 Pct Recovery = 77% Analysis Date = 06/29/14 Pct Recovery = 77% Analysis Date = 06/19/14 Pct Recovery = 77% Analysis Date = 06/19/14 Pct Recovery = 77% Analysis Date = 06/08/14 Pct Recovery = 77% Analysis Date = 06/08/14 Pct Recovery = 77% Analysis Date = 05/28/14 Pct Recovery = 78% Analysis Date = 05/28/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/06/14 Pct Recovery = 78% Analysis Date = 05/06/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/14/14 Pct Recovery = 79% Analysis Date = 04/14/14 Pct Recovery = 79% Analysis Date = 04/04/14 Pct Recovery = 79% Analysis Date = 04/04/14 Pct Recovery = 79% Analysis Date = 03/24/14 Pct Recovery = 79% Analysis Date = 03/24/14 Pct Recovery = 79% Analysis Date = 03/13/14 Pct Recovery = 79% Analysis Date = 03/13/14 Pct Recovery = 79% Analysis Date = 03/02/14 Pct Recovery = 80% Analysis Date = 03/02/14 Pct Recovery = 80% Analysis Date = 02/19/14 Pct Recovery = 80% Analysis Date = 02/19/14 Pct Recovery = 80% Analysis Date = 02/08/14 Pct Recovery = 80% Analysis Date = 02/08/14 Pct Recovery = 80% Analysis Date = 01/28/14 Pct Recovery = 81% Analysis Date = 01/28/14 Pct Recovery = 81% Analysis Date = 01/18/14 Pct Recovery = 81% Analysis Date = 01/18/14 Pct Recovery = 81% Analysis Date = 01/07/14 Pct Recovery = 81% Analysis Date = 01/07/14 Pct Recovery = 81% Analysis Date = 12/27/13 Pct Recovery = 81% Analysis Date = 12/27/13 Pct Recovery = 81% Analysis Date = 12/16/13 Pct Recovery = 82% Analysis Date = 12/16/13 Pct Recovery = 82% Analysis Date = 12/05/13 Pct Recovery = 82% Analysis Date = 12/05/13 Pct Recovery = 82% Analysis Date = 11/24/13 Pct Recovery = 82% Analysis Date = 11/24/13 Pct Recovery = 82% Analysis Date = 11/14/13 Pct Recovery = 83% Analysis Date = 11/14/13 Pct Recovery = 83% Analysis Date = 11/03/13 Pct Recovery = 83% Analysis Date = 11/03/13 Pct Recovery = 83% Analysis Date = 10/23/13 Pct Recovery = 83% Analysis Date = 10/23/13 Pct Recovery = 83% Analysis Date = 10/12/13 Pct Recovery = 84% Analysis Date = 10/12/13 Pct Recovery = 84% Analysis Date = 10/01/13 Pct Recovery = 84% Analysis Date = 10/01/13 Pct Recovery = 84% Analysis Date = 09/20/13 Pct Recovery = 84% Analysis Date = 09/20/13 Pct Recovery = 84% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 08/30/13 Pct Recovery = 85% Analysis Date = 08/30/13 Pct Recovery = 85% Analysis Date = 08/19/13 Pct Recovery = 85% Analysis Date = 08/19/13 Pct Recovery = 85% Analysis Date = 08/08/13 Pct Recovery = 86% Analysis Date = 08/08/13 Pct Recovery = 86% Analysis Date = 07/28/13 Pct Recovery = 86% Analysis Date = 07/28/13 Pct Recovery = 86% Analysis Date = 07/17/13 Pct Recovery = 86% Analysis Date = 07/17/13 Pct Recovery = 86% Analysis Date = 07/06/13 Pct Recovery = 86% Analysis Date = 07/06/13 Pct Recovery = 86% Analysis Date = 06/25/13 Pct Recovery = 87% Analysis Date = 06/25/13 Pct Recovery = 87% Analysis Date = 06/15/13 Pct Recovery = 87% Analysis Date = 06/15/13 Pct Recovery = 87% Analysis Date = 06/04/13 Pct Recovery = 87% Analysis Date = 06/04/13 Pct Recovery = 87% Analysis Date = 05/24/13 Pct Recovery = 88% Analysis Date = 05/24/13 Pct Recovery = 88% Analysis Date = 05/13/13 Pct Recovery = 88% Analysis Date = 05/13/13 Pct Recovery = 88% Analysis Date = 05/02/13 Pct Recovery = 88% Analysis Date = 05/02/13 Pct Recovery = 88% Analysis Date = 04/21/13 Pct Recovery = 88% Analysis Date = 04/21/13 Pct Recovery = 88% Analysis Date = 04/11/13 Pct Recovery = 89% Analysis Date = 04/11/13 Pct Recovery = 89% Analysis Date = 03/31/13 Pct Recovery = 89% Analysis Date = 03/31/13 Pct Recovery = 89% Analysis Date = 03/20/13 Pct Recovery = 89% Analysis Date = 03/20/13 Pct Recovery = 89% Analysis Date = 03/09/13 Pct Recovery = 89% Analysis Date = 03/09/13 Pct Recovery = 89% Analysis Date = 02/26/13 Pct Recovery = 89% Analysis Date = 02/26/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 01/25/13 Pct Recovery = 89% Analysis Date = 01/25/13 Pct Recovery = 89% Analysis Date = 01/14/13 Pct Recovery = 89% Analysis Date = 01/14/13 Pct Recovery = 89% Analysis Date = 01/03/13 Pct Recovery = 89% Analysis Date = 01/03/13 Pct Recovery = 89% Analysis Date = 12/23/12 Pct Recovery = 89% Analysis Date = 12/23/12 Pct Recovery = 89% Analysis Date = 12/12/12 Pct Recovery = 89% Analysis Date = 12/12/12 Pct Recovery = 89% Analysis Date = 12/01/12 Pct Recovery = 89% Analysis Date = 12/01/12 Pct Recovery = 89% Analysis Date = 11/20/12 Pct Recovery = 89% Analysis Date = 11/20/12 Pct Recovery = 89% Analysis Date = 11/10/12 Pct Recovery = 89% Analysis Date = 11/10/12 Pct Recovery = 89% Analysis Date = 10/30/12 Pct Recovery = 89% Analysis Date = 10/30/12 Pct Recovery = 89% Analysis Date = 10/19/12 Pct Recovery = 89% Analysis Date = 10/19/12 Pct Recovery = 89% Analysis Date = 10/08/12 Pct Recovery = 89% Analysis Date = 10/08/12 Pct Recovery = 89% Analysis Date = 09/27/12 Pct Recovery = 89% Analysis Date = 09/27/12 Pct Recovery = 89% Analysis Date = 09/16/12 Pct Recovery = 89% Analysis Date = 09/16/12 Pct Recovery = 89% Analysis Date = 09/06/12 Pct Recovery = 89% Analysis Date = 09/06/12 Pct Recovery = 89% Analysis Date = 08/26/12 Pct Recovery = 88% Analysis Date = 08/26/12 Pct Recovery = 88% Analysis Date = 08/15/12 Pct Recovery = 88% Analysis Date = 08/15/12 Pct Recovery = 88% Analysis Date = 08/04/12 Pct Recovery = 88% Analysis Date = 08/04/12 Pct Recovery = 88% Analysis Date = 07/24/12 Pct Recovery = 88% Analysis Date = 07/24/12 Pct Recovery = 88% Analysis Date = 07/13/12 Pct Recovery = 88% Analysis Date = 07/13/12 Pct Recovery = 88% Analysis Date = 07/02/12 Pct Recovery = 88% Analysis Date = 07/02/12 Pct Recovery = 88% Analysis Date = 06/22/12 Pct Recovery = 88% Analysis Date = 06/22/12 Pct Recovery = 88% Analysis Date = 06/11/12 Pct Recovery = 88% Analysis Date = 06/11/12 Pct Recovery = 88% Analysis Date = 05/31/12 Pct Recovery = 88% Analysis Date = 05/31/12 Pct Recovery = 88% Analysis Date = 05/20/12 Pct Recovery = 88% Analysis Date = 05/20/12 Pct Recovery = 88% Analysis Date = 05/09/12 Pct Recovery = 87% Analysis Date = 05/09/12 Pct Recovery = 87% Analysis Date = 04/28/12 Pct Recovery = 87% Analysis Date = 04/28/12 Pct Recovery = 87% Analysis Date = 04/17/12 Pct Recovery = 87% Analysis Date = 04/17/12 Pct Recovery = 87% Analysis Date = 04/07/12 Pct Recovery = 87% Analysis Date = 04/07/12 Pct Recovery = 87% Analysis Date = 03/27/12 Pct Recovery = 87% Analysis Date = 03/27/12 Pct Recovery = 87% Analysis Date = 03/16/12 Pct Recovery = 87% Analysis Date = 03/16/12 Pct Recovery = 87% Analysis Date = 03/05/12 Pct Recovery = 87% Analysis Date = 03/05/12 Pct Recovery = 87% Analysis Date = 02/23/12 Pct Recovery = 87% Analysis Date = 02/23/12 Pct Recovery = 87% Analysis Date = 02/12/12 Pct Recovery = 87% Analysis Date = 02/12/12 Pct Recovery = 87% Analysis Date = 02/02/12 Pct Recovery = 87% Analysis Date = 02/02/12 Pct Recovery = 87% Analysis Date = 01/22/12 Pct Recovery = 87% Analysis Date = 01/22/12 Pct Recovery = 87% Analysis Date = 01/11/12 Pct Recovery = 87% Analysis Date = 01/11/12 Pct Recovery = 87% Analysis Date = 12/31/11 Pct Recovery = 87% Analysis Date = 12/31/11 Pct Recovery = 87% Analysis Date = 12/20/11 Pct Recovery = 87% Analysis Date = 12/20/11 Pct Recovery = 87% Analysis Date = 12/09/11 Pct Recovery = 87% Analysis Date = 12/09/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 86% Analysis Date = 11/28/11 Pct Recovery = 86% Analysis Date = 11/18/11 Pct Recovery = 86% Analysis Date = 11/18/11 Pct Recovery = 86% Analysis Date = 11/07/11 Pct Recovery = 86% Analysis Date = 11/07/11 Pct Recovery = 86% Analysis Date = 10/27/11 Pct Recovery = 86% Analysis Date = 10/27/11 Pct Recovery = 86% Analysis Date = 10/16/11 Pct Recovery = 86% Analysis Date = 10/16/11 Pct Recovery = 86% Analysis Date = 10/05/11 Pct Recovery = 86% Analysis Date = 10/05/11 Pct Recovery = 86% Analysis Date = 09/24/11 Pct Recovery = 86% Analysis Date = 09/24/11 Pct Recovery = 86% Analysis Date = 09/13/11 Pct Recovery = 86% Analysis Date = 09/13/11 Pct Recovery = 86% Analysis Date = 09/03/11 Pct Recovery = 86% Analysis Date = 09/03/11 Pct Recovery = 86% Analysis Date = 08/23/11 Pct Recovery = 86% Analysis Date = 08/23/11 Pct Recovery = 86% Analysis Date = 08/12/11 Pct Recovery = 86% Analysis Date = 08/12/11 Pct Recovery = 86% Analysis Date = 08/01/11 Pct Recovery = 85% Analysis Date = 08/01/11 Pct Recovery = 85% Analysis Date = 07/21/11 Pct Recovery = 85% Analysis Date = 07/21/11 Pct Recovery = 85% Analysis Date = 07/10/11 Pct Recovery = 85% Analysis Date = 07/10/11 Pct Recovery = 85% Analysis Date = 06/30/11 Pct Recovery = 85% Analysis Date = 06/30/11 Pct Recovery = 85% Analysis Date = 06/19/11 Pct Recovery = 85% Analysis Date = 06/19/11 Pct Recovery = 85% Analysis Date = 06/08/11 Pct Recovery = 85% Analysis Date = 06/08/11 Pct Recovery = 85% Analysis Date = 05/28/11 Pct Recovery = 85% Analysis Date = 05/28/11 Pct Recovery = 85% Analysis Date = 05/17/11 Pct Recovery = 85% Analysis Date = 05/17/11 Pct Recovery = 85% Analysis Date = 05/06/11 Pct Recovery = 85% Analysis Date = 05/06/11 Pct Recovery = 85% Analysis Date = 04/25/11 Pct Recovery = 85% Analysis Date = 04/25/11 Pct Recovery = 85% Analysis Date = 04/15/11 Pct Recovery = 84% Analysis Date = 04/15/11 Pct Recovery = 84% Analysis Date = 04/04/11 Pct Recovery = 84% Analysis Date = 04/04/11 Pct Recovery = 84% Analysis Date = 03/24/11 Pct Recovery = 84% Analysis Date = 03/24/11 Pct Recovery = 84% Analysis Date = 03/13/11 Pct Recovery = 84% Analysis Date = 03/13/11 Pct Recovery = 84% Analysis Date = 03/02/11 Pct Recovery = 84% Analysis Date = 03/02/11 Pct Recovery = 84% Analysis Date = 02/19/11 Pct Recovery = 84% Analysis Date = 02/19/11 Pct Recovery = 84% Analysis Date = 02/09/11 Pct Recovery = 84% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBARYL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 117% . 117% 0%
>= Reporting Level 94 78% 18% 79% 19%
Total 95 79% 19% 79% 20%

Sample Statistics
CARBARYL

Characteristic N % % Basis
Plotted 95 100% Spiked
Estimated Values 95 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 95 .  
False Negatives 0 0% 0 out of 95
Not Spiked 74 .  
False Positives 3 4% 3 out of 74

BQS OBSP Determination:
CARBOFURAN
METHOD: 2033 , TESTIDCODE: 82674GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 96% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 82% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 93% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 98% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 78% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 32% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 77% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 102% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 87% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 77% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 81% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 109% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 43% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 70% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 97% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 38% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 96% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 68% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 69% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 111% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 94% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 84% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 108% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 99% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 109% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 94% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 47% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 100% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 75% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 64% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 83% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 83% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 125% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 65% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 97% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 80% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 101% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 83% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 83% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 68% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 84% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 95% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 81% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 106% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 83% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 74% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 94% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 127% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 144% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 82% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 92% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 116% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 113% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 102% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 100% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 115% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 114% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 114% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 101% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 106% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 133% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 111% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 113% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 108% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 115% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 97% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 91% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 107% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 124% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 86% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 64% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 67% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 76% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 66% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 106% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 109% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 88% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 107% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 138% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/07/16 Pct Recovery = 71% Analysis Date = 11/07/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/16/16 Pct Recovery = 71% Analysis Date = 10/16/16 Pct Recovery = 71% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 09/25/16 Pct Recovery = 72% Analysis Date = 09/25/16 Pct Recovery = 72% Analysis Date = 09/14/16 Pct Recovery = 72% Analysis Date = 09/14/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/13/16 Pct Recovery = 72% Analysis Date = 08/13/16 Pct Recovery = 72% Analysis Date = 08/02/16 Pct Recovery = 72% Analysis Date = 08/02/16 Pct Recovery = 72% Analysis Date = 07/23/16 Pct Recovery = 72% Analysis Date = 07/23/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 72% Analysis Date = 06/21/16 Pct Recovery = 72% Analysis Date = 06/21/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 05/30/16 Pct Recovery = 72% Analysis Date = 05/30/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/09/16 Pct Recovery = 72% Analysis Date = 05/09/16 Pct Recovery = 72% Analysis Date = 04/28/16 Pct Recovery = 72% Analysis Date = 04/28/16 Pct Recovery = 72% Analysis Date = 04/17/16 Pct Recovery = 72% Analysis Date = 04/17/16 Pct Recovery = 72% Analysis Date = 04/07/16 Pct Recovery = 72% Analysis Date = 04/07/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 72% Analysis Date = 03/05/16 Pct Recovery = 72% Analysis Date = 03/05/16 Pct Recovery = 72% Analysis Date = 02/24/16 Pct Recovery = 72% Analysis Date = 02/24/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 72% Analysis Date = 02/02/16 Pct Recovery = 72% Analysis Date = 02/02/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 72% Analysis Date = 01/23/16 Pct Recovery = 72% Analysis Date = 01/12/16 Pct Recovery = 73% Analysis Date = 01/12/16 Pct Recovery = 73% Analysis Date = 01/01/16 Pct Recovery = 73% Analysis Date = 01/01/16 Pct Recovery = 73% Analysis Date = 12/22/15 Pct Recovery = 73% Analysis Date = 12/22/15 Pct Recovery = 73% Analysis Date = 12/11/15 Pct Recovery = 73% Analysis Date = 12/11/15 Pct Recovery = 73% Analysis Date = 11/30/15 Pct Recovery = 73% Analysis Date = 11/30/15 Pct Recovery = 73% Analysis Date = 11/19/15 Pct Recovery = 73% Analysis Date = 11/19/15 Pct Recovery = 73% Analysis Date = 11/09/15 Pct Recovery = 73% Analysis Date = 11/09/15 Pct Recovery = 73% Analysis Date = 10/29/15 Pct Recovery = 73% Analysis Date = 10/29/15 Pct Recovery = 73% Analysis Date = 10/18/15 Pct Recovery = 73% Analysis Date = 10/18/15 Pct Recovery = 73% Analysis Date = 10/08/15 Pct Recovery = 73% Analysis Date = 10/08/15 Pct Recovery = 73% Analysis Date = 09/27/15 Pct Recovery = 73% Analysis Date = 09/27/15 Pct Recovery = 73% Analysis Date = 09/16/15 Pct Recovery = 73% Analysis Date = 09/16/15 Pct Recovery = 73% Analysis Date = 09/05/15 Pct Recovery = 74% Analysis Date = 09/05/15 Pct Recovery = 74% Analysis Date = 08/26/15 Pct Recovery = 74% Analysis Date = 08/26/15 Pct Recovery = 74% Analysis Date = 08/15/15 Pct Recovery = 74% Analysis Date = 08/15/15 Pct Recovery = 74% Analysis Date = 08/04/15 Pct Recovery = 74% Analysis Date = 08/04/15 Pct Recovery = 74% Analysis Date = 07/25/15 Pct Recovery = 74% Analysis Date = 07/25/15 Pct Recovery = 74% Analysis Date = 07/14/15 Pct Recovery = 74% Analysis Date = 07/14/15 Pct Recovery = 74% Analysis Date = 07/03/15 Pct Recovery = 74% Analysis Date = 07/03/15 Pct Recovery = 74% Analysis Date = 06/23/15 Pct Recovery = 74% Analysis Date = 06/23/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/12/15 Pct Recovery = 74% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 05/21/15 Pct Recovery = 75% Analysis Date = 05/21/15 Pct Recovery = 75% Analysis Date = 05/11/15 Pct Recovery = 75% Analysis Date = 05/11/15 Pct Recovery = 75% Analysis Date = 04/30/15 Pct Recovery = 75% Analysis Date = 04/30/15 Pct Recovery = 75% Analysis Date = 04/19/15 Pct Recovery = 75% Analysis Date = 04/19/15 Pct Recovery = 75% Analysis Date = 04/09/15 Pct Recovery = 75% Analysis Date = 04/09/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/29/15 Pct Recovery = 75% Analysis Date = 03/18/15 Pct Recovery = 75% Analysis Date = 03/18/15 Pct Recovery = 75% Analysis Date = 03/07/15 Pct Recovery = 75% Analysis Date = 03/07/15 Pct Recovery = 75% Analysis Date = 02/25/15 Pct Recovery = 76% Analysis Date = 02/25/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/03/15 Pct Recovery = 76% Analysis Date = 02/03/15 Pct Recovery = 76% Analysis Date = 01/24/15 Pct Recovery = 76% Analysis Date = 01/24/15 Pct Recovery = 76% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/02/15 Pct Recovery = 77% Analysis Date = 01/02/15 Pct Recovery = 77% Analysis Date = 12/23/14 Pct Recovery = 77% Analysis Date = 12/23/14 Pct Recovery = 77% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/01/14 Pct Recovery = 78% Analysis Date = 12/01/14 Pct Recovery = 78% Analysis Date = 11/20/14 Pct Recovery = 78% Analysis Date = 11/20/14 Pct Recovery = 78% Analysis Date = 11/10/14 Pct Recovery = 79% Analysis Date = 11/10/14 Pct Recovery = 79% Analysis Date = 10/30/14 Pct Recovery = 79% Analysis Date = 10/30/14 Pct Recovery = 79% Analysis Date = 10/19/14 Pct Recovery = 79% Analysis Date = 10/19/14 Pct Recovery = 79% Analysis Date = 10/09/14 Pct Recovery = 80% Analysis Date = 10/09/14 Pct Recovery = 80% Analysis Date = 09/28/14 Pct Recovery = 80% Analysis Date = 09/28/14 Pct Recovery = 80% Analysis Date = 09/17/14 Pct Recovery = 80% Analysis Date = 09/17/14 Pct Recovery = 80% Analysis Date = 09/07/14 Pct Recovery = 81% Analysis Date = 09/07/14 Pct Recovery = 81% Analysis Date = 08/27/14 Pct Recovery = 81% Analysis Date = 08/27/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/05/14 Pct Recovery = 82% Analysis Date = 08/05/14 Pct Recovery = 82% Analysis Date = 07/26/14 Pct Recovery = 82% Analysis Date = 07/26/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 07/04/14 Pct Recovery = 83% Analysis Date = 06/24/14 Pct Recovery = 83% Analysis Date = 06/24/14 Pct Recovery = 83% Analysis Date = 06/13/14 Pct Recovery = 83% Analysis Date = 06/13/14 Pct Recovery = 83% Analysis Date = 06/02/14 Pct Recovery = 84% Analysis Date = 06/02/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/01/14 Pct Recovery = 85% Analysis Date = 05/01/14 Pct Recovery = 85% Analysis Date = 04/20/14 Pct Recovery = 85% Analysis Date = 04/20/14 Pct Recovery = 85% Analysis Date = 04/10/14 Pct Recovery = 86% Analysis Date = 04/10/14 Pct Recovery = 86% Analysis Date = 03/30/14 Pct Recovery = 86% Analysis Date = 03/30/14 Pct Recovery = 86% Analysis Date = 03/19/14 Pct Recovery = 86% Analysis Date = 03/19/14 Pct Recovery = 86% Analysis Date = 03/09/14 Pct Recovery = 87% Analysis Date = 03/09/14 Pct Recovery = 87% Analysis Date = 02/26/14 Pct Recovery = 87% Analysis Date = 02/26/14 Pct Recovery = 87% Analysis Date = 02/15/14 Pct Recovery = 88% Analysis Date = 02/15/14 Pct Recovery = 88% Analysis Date = 02/04/14 Pct Recovery = 88% Analysis Date = 02/04/14 Pct Recovery = 88% Analysis Date = 01/25/14 Pct Recovery = 88% Analysis Date = 01/25/14 Pct Recovery = 88% Analysis Date = 01/14/14 Pct Recovery = 89% Analysis Date = 01/14/14 Pct Recovery = 89% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/13/13 Pct Recovery = 90% Analysis Date = 12/13/13 Pct Recovery = 90% Analysis Date = 12/02/13 Pct Recovery = 90% Analysis Date = 12/02/13 Pct Recovery = 90% Analysis Date = 11/21/13 Pct Recovery = 90% Analysis Date = 11/21/13 Pct Recovery = 90% Analysis Date = 11/11/13 Pct Recovery = 91% Analysis Date = 11/11/13 Pct Recovery = 91% Analysis Date = 10/31/13 Pct Recovery = 91% Analysis Date = 10/31/13 Pct Recovery = 91% Analysis Date = 10/20/13 Pct Recovery = 92% Analysis Date = 10/20/13 Pct Recovery = 92% Analysis Date = 10/10/13 Pct Recovery = 92% Analysis Date = 10/10/13 Pct Recovery = 92% Analysis Date = 09/29/13 Pct Recovery = 92% Analysis Date = 09/29/13 Pct Recovery = 92% Analysis Date = 09/18/13 Pct Recovery = 93% Analysis Date = 09/18/13 Pct Recovery = 93% Analysis Date = 09/08/13 Pct Recovery = 93% Analysis Date = 09/08/13 Pct Recovery = 93% Analysis Date = 08/28/13 Pct Recovery = 93% Analysis Date = 08/28/13 Pct Recovery = 93% Analysis Date = 08/17/13 Pct Recovery = 94% Analysis Date = 08/17/13 Pct Recovery = 94% Analysis Date = 08/06/13 Pct Recovery = 94% Analysis Date = 08/06/13 Pct Recovery = 94% Analysis Date = 07/27/13 Pct Recovery = 94% Analysis Date = 07/27/13 Pct Recovery = 94% Analysis Date = 07/16/13 Pct Recovery = 95% Analysis Date = 07/16/13 Pct Recovery = 95% Analysis Date = 07/05/13 Pct Recovery = 95% Analysis Date = 07/05/13 Pct Recovery = 95% Analysis Date = 06/25/13 Pct Recovery = 96% Analysis Date = 06/25/13 Pct Recovery = 96% Analysis Date = 06/14/13 Pct Recovery = 96% Analysis Date = 06/14/13 Pct Recovery = 96% Analysis Date = 06/03/13 Pct Recovery = 96% Analysis Date = 06/03/13 Pct Recovery = 96% Analysis Date = 05/23/13 Pct Recovery = 97% Analysis Date = 05/23/13 Pct Recovery = 97% Analysis Date = 05/13/13 Pct Recovery = 97% Analysis Date = 05/13/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 04/21/13 Pct Recovery = 98% Analysis Date = 04/21/13 Pct Recovery = 98% Analysis Date = 04/11/13 Pct Recovery = 98% Analysis Date = 04/11/13 Pct Recovery = 98% Analysis Date = 03/31/13 Pct Recovery = 98% Analysis Date = 03/31/13 Pct Recovery = 98% Analysis Date = 03/20/13 Pct Recovery = 99% Analysis Date = 03/20/13 Pct Recovery = 99% Analysis Date = 03/10/13 Pct Recovery = 99% Analysis Date = 03/10/13 Pct Recovery = 99% Analysis Date = 02/27/13 Pct Recovery = 99% Analysis Date = 02/27/13 Pct Recovery = 99% Analysis Date = 02/16/13 Pct Recovery = 99% Analysis Date = 02/16/13 Pct Recovery = 99% Analysis Date = 02/05/13 Pct Recovery = 100% Analysis Date = 02/05/13 Pct Recovery = 100% Analysis Date = 01/26/13 Pct Recovery = 100% Analysis Date = 01/26/13 Pct Recovery = 100% Analysis Date = 01/15/13 Pct Recovery = 100% Analysis Date = 01/15/13 Pct Recovery = 100% Analysis Date = 01/04/13 Pct Recovery = 100% Analysis Date = 01/04/13 Pct Recovery = 100% Analysis Date = 12/25/12 Pct Recovery = 100% Analysis Date = 12/25/12 Pct Recovery = 100% Analysis Date = 12/14/12 Pct Recovery = 101% Analysis Date = 12/14/12 Pct Recovery = 101% Analysis Date = 12/03/12 Pct Recovery = 101% Analysis Date = 12/03/12 Pct Recovery = 101% Analysis Date = 11/23/12 Pct Recovery = 101% Analysis Date = 11/23/12 Pct Recovery = 101% Analysis Date = 11/12/12 Pct Recovery = 101% Analysis Date = 11/12/12 Pct Recovery = 101% Analysis Date = 11/01/12 Pct Recovery = 101% Analysis Date = 11/01/12 Pct Recovery = 101% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/11/12 Pct Recovery = 101% Analysis Date = 10/11/12 Pct Recovery = 101% Analysis Date = 09/30/12 Pct Recovery = 102% Analysis Date = 09/30/12 Pct Recovery = 102% Analysis Date = 09/19/12 Pct Recovery = 102% Analysis Date = 09/19/12 Pct Recovery = 102% Analysis Date = 09/09/12 Pct Recovery = 102% Analysis Date = 09/09/12 Pct Recovery = 102% Analysis Date = 08/29/12 Pct Recovery = 102% Analysis Date = 08/29/12 Pct Recovery = 102% Analysis Date = 08/18/12 Pct Recovery = 102% Analysis Date = 08/18/12 Pct Recovery = 102% Analysis Date = 08/07/12 Pct Recovery = 102% Analysis Date = 08/07/12 Pct Recovery = 102% Analysis Date = 07/28/12 Pct Recovery = 102% Analysis Date = 07/28/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/06/12 Pct Recovery = 102% Analysis Date = 07/06/12 Pct Recovery = 102% Analysis Date = 06/26/12 Pct Recovery = 102% Analysis Date = 06/26/12 Pct Recovery = 102% Analysis Date = 06/15/12 Pct Recovery = 102% Analysis Date = 06/15/12 Pct Recovery = 102% Analysis Date = 06/04/12 Pct Recovery = 103% Analysis Date = 06/04/12 Pct Recovery = 103% Analysis Date = 05/25/12 Pct Recovery = 103% Analysis Date = 05/25/12 Pct Recovery = 103% Analysis Date = 05/14/12 Pct Recovery = 103% Analysis Date = 05/14/12 Pct Recovery = 103% Analysis Date = 05/03/12 Pct Recovery = 103% Analysis Date = 05/03/12 Pct Recovery = 103% Analysis Date = 04/22/12 Pct Recovery = 103% Analysis Date = 04/22/12 Pct Recovery = 103% Analysis Date = 04/12/12 Pct Recovery = 103% Analysis Date = 04/12/12 Pct Recovery = 103% Analysis Date = 04/01/12 Pct Recovery = 103% Analysis Date = 04/01/12 Pct Recovery = 103% Analysis Date = 03/21/12 Pct Recovery = 103% Analysis Date = 03/21/12 Pct Recovery = 103% Analysis Date = 03/11/12 Pct Recovery = 104% Analysis Date = 03/11/12 Pct Recovery = 104% Analysis Date = 02/29/12 Pct Recovery = 104% Analysis Date = 02/29/12 Pct Recovery = 104% Analysis Date = 02/18/12 Pct Recovery = 104% Analysis Date = 02/18/12 Pct Recovery = 104% Analysis Date = 02/07/12 Pct Recovery = 104% Analysis Date = 02/07/12 Pct Recovery = 104% Analysis Date = 01/28/12 Pct Recovery = 104% Analysis Date = 01/28/12 Pct Recovery = 104% Analysis Date = 01/17/12 Pct Recovery = 104% Analysis Date = 01/17/12 Pct Recovery = 104% Analysis Date = 01/06/12 Pct Recovery = 104% Analysis Date = 01/06/12 Pct Recovery = 104% Analysis Date = 12/27/11 Pct Recovery = 105% Analysis Date = 12/27/11 Pct Recovery = 105% Analysis Date = 12/16/11 Pct Recovery = 105% Analysis Date = 12/16/11 Pct Recovery = 105% Analysis Date = 12/05/11 Pct Recovery = 105% Analysis Date = 12/05/11 Pct Recovery = 105% Analysis Date = 11/25/11 Pct Recovery = 105% Analysis Date = 11/25/11 Pct Recovery = 105% Analysis Date = 11/14/11 Pct Recovery = 105% Analysis Date = 11/14/11 Pct Recovery = 105% Analysis Date = 11/03/11 Pct Recovery = 105% Analysis Date = 11/03/11 Pct Recovery = 105% Analysis Date = 10/23/11 Pct Recovery = 105% Analysis Date = 10/23/11 Pct Recovery = 105% Analysis Date = 10/13/11 Pct Recovery = 105% Analysis Date = 10/13/11 Pct Recovery = 105% Analysis Date = 10/02/11 Pct Recovery = 106% Analysis Date = 10/02/11 Pct Recovery = 106% Analysis Date = 09/21/11 Pct Recovery = 106% Analysis Date = 09/21/11 Pct Recovery = 106% Analysis Date = 09/11/11 Pct Recovery = 106% Analysis Date = 09/11/11 Pct Recovery = 106% Analysis Date = 08/31/11 Pct Recovery = 106% Analysis Date = 08/31/11 Pct Recovery = 106% Analysis Date = 08/20/11 Pct Recovery = 106% Analysis Date = 08/20/11 Pct Recovery = 106% Analysis Date = 08/09/11 Pct Recovery = 106% Analysis Date = 08/09/11 Pct Recovery = 106% Analysis Date = 07/30/11 Pct Recovery = 106% Analysis Date = 07/30/11 Pct Recovery = 106% Analysis Date = 07/19/11 Pct Recovery = 106% Analysis Date = 07/19/11 Pct Recovery = 106% Analysis Date = 07/08/11 Pct Recovery = 106% Analysis Date = 07/08/11 Pct Recovery = 106% Analysis Date = 06/28/11 Pct Recovery = 107% Analysis Date = 06/28/11 Pct Recovery = 107% Analysis Date = 06/17/11 Pct Recovery = 107% Analysis Date = 06/17/11 Pct Recovery = 107% Analysis Date = 06/06/11 Pct Recovery = 107% Analysis Date = 06/06/11 Pct Recovery = 107% Analysis Date = 05/27/11 Pct Recovery = 107% Analysis Date = 05/27/11 Pct Recovery = 107% Analysis Date = 05/16/11 Pct Recovery = 107% Analysis Date = 05/16/11 Pct Recovery = 107% Analysis Date = 05/05/11 Pct Recovery = 107% Analysis Date = 05/05/11 Pct Recovery = 107% Analysis Date = 04/24/11 Pct Recovery = 107% Analysis Date = 04/24/11 Pct Recovery = 107% Analysis Date = 04/14/11 Pct Recovery = 107% Analysis Date = 04/14/11 Pct Recovery = 107% Analysis Date = 04/03/11 Pct Recovery = 107% Analysis Date = 04/03/11 Pct Recovery = 107% Analysis Date = 03/23/11 Pct Recovery = 107% Analysis Date = 03/23/11 Pct Recovery = 107% Analysis Date = 03/13/11 Pct Recovery = 108% Analysis Date = 03/13/11 Pct Recovery = 108% Analysis Date = 03/02/11 Pct Recovery = 108% Analysis Date = 03/02/11 Pct Recovery = 108% Analysis Date = 02/19/11 Pct Recovery = 108% Analysis Date = 02/19/11 Pct Recovery = 108% Analysis Date = 02/09/11 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBOFURAN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 138% . 138% 0%
>= Reporting Level 92 89% 21% 91% 23%
Total 93 90% 21% 91% 23%

Sample Statistics
CARBOFURAN

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 93 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 0 0% 0 out of 76

BQS OBSP Determination:
CHLORPYRIFOS
METHOD: 2033 , TESTIDCODE: 38933GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 95% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 88% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 93% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 91% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 77% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 98% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 85% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 81% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 92% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 112% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 84% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 87% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 72% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 79% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 67% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 71% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 90% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 90% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 73% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 77% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 93% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 61% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 88% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 75% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 93% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 83% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 84% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 71% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 83% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 93% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 89% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 123% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 103% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 79% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 75% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 133% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 101% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 70% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 78% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 85% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 77% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 90% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 78% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 80% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 68% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 78% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 65% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 65% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 71% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 87% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 71% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 72% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 60% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 64% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 89% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 102% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 86% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 96% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 86% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 108% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 102% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 95% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 95% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 53% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 96% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 87% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 79% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 93% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 76% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 48% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 74% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 68% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 71% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 89% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 112% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 78% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 60% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 86% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 102% Analysis Date = 01/18/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 77% Analysis Date = 12/27/16 Pct Recovery = 77% Analysis Date = 12/27/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 77% Analysis Date = 12/05/16 Pct Recovery = 77% Analysis Date = 12/05/16 Pct Recovery = 77% Analysis Date = 11/24/16 Pct Recovery = 77% Analysis Date = 11/24/16 Pct Recovery = 77% Analysis Date = 11/14/16 Pct Recovery = 77% Analysis Date = 11/14/16 Pct Recovery = 77% Analysis Date = 11/03/16 Pct Recovery = 77% Analysis Date = 11/03/16 Pct Recovery = 77% Analysis Date = 10/23/16 Pct Recovery = 77% Analysis Date = 10/23/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/01/16 Pct Recovery = 77% Analysis Date = 10/01/16 Pct Recovery = 77% Analysis Date = 09/20/16 Pct Recovery = 77% Analysis Date = 09/20/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 77% Analysis Date = 08/19/16 Pct Recovery = 77% Analysis Date = 08/19/16 Pct Recovery = 77% Analysis Date = 08/08/16 Pct Recovery = 77% Analysis Date = 08/08/16 Pct Recovery = 77% Analysis Date = 07/28/16 Pct Recovery = 77% Analysis Date = 07/28/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 07/07/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/26/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 05/24/16 Pct Recovery = 77% Analysis Date = 05/24/16 Pct Recovery = 77% Analysis Date = 05/14/16 Pct Recovery = 77% Analysis Date = 05/14/16 Pct Recovery = 77% Analysis Date = 05/03/16 Pct Recovery = 77% Analysis Date = 05/03/16 Pct Recovery = 77% Analysis Date = 04/22/16 Pct Recovery = 77% Analysis Date = 04/22/16 Pct Recovery = 77% Analysis Date = 04/11/16 Pct Recovery = 77% Analysis Date = 04/11/16 Pct Recovery = 77% Analysis Date = 03/31/16 Pct Recovery = 77% Analysis Date = 03/31/16 Pct Recovery = 77% Analysis Date = 03/20/16 Pct Recovery = 77% Analysis Date = 03/20/16 Pct Recovery = 77% Analysis Date = 03/10/16 Pct Recovery = 77% Analysis Date = 03/10/16 Pct Recovery = 77% Analysis Date = 02/28/16 Pct Recovery = 77% Analysis Date = 02/28/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/06/16 Pct Recovery = 77% Analysis Date = 02/06/16 Pct Recovery = 77% Analysis Date = 01/26/16 Pct Recovery = 77% Analysis Date = 01/26/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/14/15 Pct Recovery = 77% Analysis Date = 12/14/15 Pct Recovery = 77% Analysis Date = 12/03/15 Pct Recovery = 77% Analysis Date = 12/03/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/01/15 Pct Recovery = 77% Analysis Date = 11/01/15 Pct Recovery = 77% Analysis Date = 10/21/15 Pct Recovery = 77% Analysis Date = 10/21/15 Pct Recovery = 77% Analysis Date = 10/10/15 Pct Recovery = 77% Analysis Date = 10/10/15 Pct Recovery = 77% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/18/15 Pct Recovery = 77% Analysis Date = 09/18/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 08/28/15 Pct Recovery = 77% Analysis Date = 08/28/15 Pct Recovery = 77% Analysis Date = 08/17/15 Pct Recovery = 77% Analysis Date = 08/17/15 Pct Recovery = 77% Analysis Date = 08/06/15 Pct Recovery = 77% Analysis Date = 08/06/15 Pct Recovery = 77% Analysis Date = 07/26/15 Pct Recovery = 77% Analysis Date = 07/26/15 Pct Recovery = 77% Analysis Date = 07/15/15 Pct Recovery = 77% Analysis Date = 07/15/15 Pct Recovery = 77% Analysis Date = 07/05/15 Pct Recovery = 77% Analysis Date = 07/05/15 Pct Recovery = 77% Analysis Date = 06/24/15 Pct Recovery = 77% Analysis Date = 06/24/15 Pct Recovery = 77% Analysis Date = 06/13/15 Pct Recovery = 77% Analysis Date = 06/13/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 06/02/15 Pct Recovery = 77% Analysis Date = 05/22/15 Pct Recovery = 78% Analysis Date = 05/22/15 Pct Recovery = 78% Analysis Date = 05/11/15 Pct Recovery = 78% Analysis Date = 05/11/15 Pct Recovery = 78% Analysis Date = 05/01/15 Pct Recovery = 78% Analysis Date = 05/01/15 Pct Recovery = 78% Analysis Date = 04/20/15 Pct Recovery = 78% Analysis Date = 04/20/15 Pct Recovery = 78% Analysis Date = 04/09/15 Pct Recovery = 78% Analysis Date = 04/09/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/29/15 Pct Recovery = 78% Analysis Date = 03/18/15 Pct Recovery = 78% Analysis Date = 03/18/15 Pct Recovery = 78% Analysis Date = 03/08/15 Pct Recovery = 78% Analysis Date = 03/08/15 Pct Recovery = 78% Analysis Date = 02/25/15 Pct Recovery = 78% Analysis Date = 02/25/15 Pct Recovery = 78% Analysis Date = 02/14/15 Pct Recovery = 78% Analysis Date = 02/14/15 Pct Recovery = 78% Analysis Date = 02/03/15 Pct Recovery = 78% Analysis Date = 02/03/15 Pct Recovery = 78% Analysis Date = 01/23/15 Pct Recovery = 78% Analysis Date = 01/23/15 Pct Recovery = 78% Analysis Date = 01/12/15 Pct Recovery = 78% Analysis Date = 01/12/15 Pct Recovery = 78% Analysis Date = 01/02/15 Pct Recovery = 79% Analysis Date = 01/02/15 Pct Recovery = 79% Analysis Date = 12/22/14 Pct Recovery = 79% Analysis Date = 12/22/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 12/11/14 Pct Recovery = 79% Analysis Date = 11/30/14 Pct Recovery = 79% Analysis Date = 11/30/14 Pct Recovery = 79% Analysis Date = 11/19/14 Pct Recovery = 80% Analysis Date = 11/19/14 Pct Recovery = 80% Analysis Date = 11/08/14 Pct Recovery = 80% Analysis Date = 11/08/14 Pct Recovery = 80% Analysis Date = 10/29/14 Pct Recovery = 80% Analysis Date = 10/29/14 Pct Recovery = 80% Analysis Date = 10/18/14 Pct Recovery = 81% Analysis Date = 10/18/14 Pct Recovery = 81% Analysis Date = 10/07/14 Pct Recovery = 81% Analysis Date = 10/07/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/26/14 Pct Recovery = 81% Analysis Date = 09/15/14 Pct Recovery = 81% Analysis Date = 09/15/14 Pct Recovery = 81% Analysis Date = 09/05/14 Pct Recovery = 82% Analysis Date = 09/05/14 Pct Recovery = 82% Analysis Date = 08/25/14 Pct Recovery = 82% Analysis Date = 08/25/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/14/14 Pct Recovery = 82% Analysis Date = 08/03/14 Pct Recovery = 82% Analysis Date = 08/03/14 Pct Recovery = 82% Analysis Date = 07/23/14 Pct Recovery = 82% Analysis Date = 07/23/14 Pct Recovery = 82% Analysis Date = 07/12/14 Pct Recovery = 83% Analysis Date = 07/12/14 Pct Recovery = 83% Analysis Date = 07/02/14 Pct Recovery = 83% Analysis Date = 07/02/14 Pct Recovery = 83% Analysis Date = 06/21/14 Pct Recovery = 83% Analysis Date = 06/21/14 Pct Recovery = 83% Analysis Date = 06/10/14 Pct Recovery = 83% Analysis Date = 06/10/14 Pct Recovery = 83% Analysis Date = 05/30/14 Pct Recovery = 83% Analysis Date = 05/30/14 Pct Recovery = 83% Analysis Date = 05/19/14 Pct Recovery = 84% Analysis Date = 05/19/14 Pct Recovery = 84% Analysis Date = 05/08/14 Pct Recovery = 84% Analysis Date = 05/08/14 Pct Recovery = 84% Analysis Date = 04/28/14 Pct Recovery = 84% Analysis Date = 04/28/14 Pct Recovery = 84% Analysis Date = 04/17/14 Pct Recovery = 84% Analysis Date = 04/17/14 Pct Recovery = 84% Analysis Date = 04/06/14 Pct Recovery = 84% Analysis Date = 04/06/14 Pct Recovery = 84% Analysis Date = 03/26/14 Pct Recovery = 85% Analysis Date = 03/26/14 Pct Recovery = 85% Analysis Date = 03/15/14 Pct Recovery = 85% Analysis Date = 03/15/14 Pct Recovery = 85% Analysis Date = 03/04/14 Pct Recovery = 85% Analysis Date = 03/04/14 Pct Recovery = 85% Analysis Date = 02/22/14 Pct Recovery = 85% Analysis Date = 02/22/14 Pct Recovery = 85% Analysis Date = 02/11/14 Pct Recovery = 85% Analysis Date = 02/11/14 Pct Recovery = 85% Analysis Date = 01/31/14 Pct Recovery = 85% Analysis Date = 01/31/14 Pct Recovery = 85% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/09/14 Pct Recovery = 86% Analysis Date = 01/09/14 Pct Recovery = 86% Analysis Date = 12/30/13 Pct Recovery = 86% Analysis Date = 12/30/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/08/13 Pct Recovery = 86% Analysis Date = 12/08/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/16/13 Pct Recovery = 87% Analysis Date = 11/16/13 Pct Recovery = 87% Analysis Date = 11/05/13 Pct Recovery = 87% Analysis Date = 11/05/13 Pct Recovery = 87% Analysis Date = 10/26/13 Pct Recovery = 87% Analysis Date = 10/26/13 Pct Recovery = 87% Analysis Date = 10/15/13 Pct Recovery = 87% Analysis Date = 10/15/13 Pct Recovery = 87% Analysis Date = 10/04/13 Pct Recovery = 87% Analysis Date = 10/04/13 Pct Recovery = 87% Analysis Date = 09/23/13 Pct Recovery = 87% Analysis Date = 09/23/13 Pct Recovery = 87% Analysis Date = 09/12/13 Pct Recovery = 87% Analysis Date = 09/12/13 Pct Recovery = 87% Analysis Date = 09/01/13 Pct Recovery = 87% Analysis Date = 09/01/13 Pct Recovery = 87% Analysis Date = 08/22/13 Pct Recovery = 87% Analysis Date = 08/22/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/20/13 Pct Recovery = 87% Analysis Date = 07/20/13 Pct Recovery = 87% Analysis Date = 07/09/13 Pct Recovery = 87% Analysis Date = 07/09/13 Pct Recovery = 87% Analysis Date = 06/29/13 Pct Recovery = 87% Analysis Date = 06/29/13 Pct Recovery = 87% Analysis Date = 06/18/13 Pct Recovery = 87% Analysis Date = 06/18/13 Pct Recovery = 87% Analysis Date = 06/07/13 Pct Recovery = 87% Analysis Date = 06/07/13 Pct Recovery = 87% Analysis Date = 05/27/13 Pct Recovery = 87% Analysis Date = 05/27/13 Pct Recovery = 87% Analysis Date = 05/16/13 Pct Recovery = 87% Analysis Date = 05/16/13 Pct Recovery = 87% Analysis Date = 05/05/13 Pct Recovery = 87% Analysis Date = 05/05/13 Pct Recovery = 87% Analysis Date = 04/25/13 Pct Recovery = 87% Analysis Date = 04/25/13 Pct Recovery = 87% Analysis Date = 04/14/13 Pct Recovery = 87% Analysis Date = 04/14/13 Pct Recovery = 87% Analysis Date = 04/03/13 Pct Recovery = 87% Analysis Date = 04/03/13 Pct Recovery = 87% Analysis Date = 03/23/13 Pct Recovery = 87% Analysis Date = 03/23/13 Pct Recovery = 87% Analysis Date = 03/12/13 Pct Recovery = 87% Analysis Date = 03/12/13 Pct Recovery = 87% Analysis Date = 03/01/13 Pct Recovery = 86% Analysis Date = 03/01/13 Pct Recovery = 86% Analysis Date = 02/19/13 Pct Recovery = 86% Analysis Date = 02/19/13 Pct Recovery = 86% Analysis Date = 02/08/13 Pct Recovery = 86% Analysis Date = 02/08/13 Pct Recovery = 86% Analysis Date = 01/28/13 Pct Recovery = 86% Analysis Date = 01/28/13 Pct Recovery = 86% Analysis Date = 01/17/13 Pct Recovery = 86% Analysis Date = 01/17/13 Pct Recovery = 86% Analysis Date = 01/06/13 Pct Recovery = 85% Analysis Date = 01/06/13 Pct Recovery = 85% Analysis Date = 12/26/12 Pct Recovery = 85% Analysis Date = 12/26/12 Pct Recovery = 85% Analysis Date = 12/16/12 Pct Recovery = 85% Analysis Date = 12/16/12 Pct Recovery = 85% Analysis Date = 12/05/12 Pct Recovery = 85% Analysis Date = 12/05/12 Pct Recovery = 85% Analysis Date = 11/24/12 Pct Recovery = 85% Analysis Date = 11/24/12 Pct Recovery = 85% Analysis Date = 11/13/12 Pct Recovery = 84% Analysis Date = 11/13/12 Pct Recovery = 84% Analysis Date = 11/02/12 Pct Recovery = 84% Analysis Date = 11/02/12 Pct Recovery = 84% Analysis Date = 10/23/12 Pct Recovery = 84% Analysis Date = 10/23/12 Pct Recovery = 84% Analysis Date = 10/12/12 Pct Recovery = 84% Analysis Date = 10/12/12 Pct Recovery = 84% Analysis Date = 10/01/12 Pct Recovery = 84% Analysis Date = 10/01/12 Pct Recovery = 84% Analysis Date = 09/20/12 Pct Recovery = 84% Analysis Date = 09/20/12 Pct Recovery = 84% Analysis Date = 09/09/12 Pct Recovery = 84% Analysis Date = 09/09/12 Pct Recovery = 84% Analysis Date = 08/29/12 Pct Recovery = 84% Analysis Date = 08/29/12 Pct Recovery = 84% Analysis Date = 08/19/12 Pct Recovery = 83% Analysis Date = 08/19/12 Pct Recovery = 83% Analysis Date = 08/08/12 Pct Recovery = 83% Analysis Date = 08/08/12 Pct Recovery = 83% Analysis Date = 07/28/12 Pct Recovery = 83% Analysis Date = 07/28/12 Pct Recovery = 83% Analysis Date = 07/17/12 Pct Recovery = 83% Analysis Date = 07/17/12 Pct Recovery = 83% Analysis Date = 07/06/12 Pct Recovery = 83% Analysis Date = 07/06/12 Pct Recovery = 83% Analysis Date = 06/25/12 Pct Recovery = 83% Analysis Date = 06/25/12 Pct Recovery = 83% Analysis Date = 06/15/12 Pct Recovery = 83% Analysis Date = 06/15/12 Pct Recovery = 83% Analysis Date = 06/04/12 Pct Recovery = 83% Analysis Date = 06/04/12 Pct Recovery = 83% Analysis Date = 05/24/12 Pct Recovery = 83% Analysis Date = 05/24/12 Pct Recovery = 83% Analysis Date = 05/13/12 Pct Recovery = 83% Analysis Date = 05/13/12 Pct Recovery = 83% Analysis Date = 05/02/12 Pct Recovery = 83% Analysis Date = 05/02/12 Pct Recovery = 83% Analysis Date = 04/22/12 Pct Recovery = 82% Analysis Date = 04/22/12 Pct Recovery = 82% Analysis Date = 04/11/12 Pct Recovery = 82% Analysis Date = 04/11/12 Pct Recovery = 82% Analysis Date = 03/31/12 Pct Recovery = 82% Analysis Date = 03/31/12 Pct Recovery = 82% Analysis Date = 03/20/12 Pct Recovery = 82% Analysis Date = 03/20/12 Pct Recovery = 82% Analysis Date = 03/09/12 Pct Recovery = 82% Analysis Date = 03/09/12 Pct Recovery = 82% Analysis Date = 02/27/12 Pct Recovery = 82% Analysis Date = 02/27/12 Pct Recovery = 82% Analysis Date = 02/17/12 Pct Recovery = 82% Analysis Date = 02/17/12 Pct Recovery = 82% Analysis Date = 02/06/12 Pct Recovery = 82% Analysis Date = 02/06/12 Pct Recovery = 82% Analysis Date = 01/26/12 Pct Recovery = 82% Analysis Date = 01/26/12 Pct Recovery = 82% Analysis Date = 01/15/12 Pct Recovery = 82% Analysis Date = 01/15/12 Pct Recovery = 82% Analysis Date = 01/04/12 Pct Recovery = 82% Analysis Date = 01/04/12 Pct Recovery = 82% Analysis Date = 12/24/11 Pct Recovery = 82% Analysis Date = 12/24/11 Pct Recovery = 82% Analysis Date = 12/14/11 Pct Recovery = 82% Analysis Date = 12/14/11 Pct Recovery = 82% Analysis Date = 12/03/11 Pct Recovery = 82% Analysis Date = 12/03/11 Pct Recovery = 82% Analysis Date = 11/22/11 Pct Recovery = 82% Analysis Date = 11/22/11 Pct Recovery = 82% Analysis Date = 11/11/11 Pct Recovery = 82% Analysis Date = 11/11/11 Pct Recovery = 82% Analysis Date = 10/31/11 Pct Recovery = 81% Analysis Date = 10/31/11 Pct Recovery = 81% Analysis Date = 10/20/11 Pct Recovery = 81% Analysis Date = 10/20/11 Pct Recovery = 81% Analysis Date = 10/10/11 Pct Recovery = 81% Analysis Date = 10/10/11 Pct Recovery = 81% Analysis Date = 09/29/11 Pct Recovery = 81% Analysis Date = 09/29/11 Pct Recovery = 81% Analysis Date = 09/18/11 Pct Recovery = 81% Analysis Date = 09/18/11 Pct Recovery = 81% Analysis Date = 09/07/11 Pct Recovery = 81% Analysis Date = 09/07/11 Pct Recovery = 81% Analysis Date = 08/27/11 Pct Recovery = 81% Analysis Date = 08/27/11 Pct Recovery = 81% Analysis Date = 08/17/11 Pct Recovery = 81% Analysis Date = 08/17/11 Pct Recovery = 81% Analysis Date = 08/06/11 Pct Recovery = 81% Analysis Date = 08/06/11 Pct Recovery = 81% Analysis Date = 07/26/11 Pct Recovery = 81% Analysis Date = 07/26/11 Pct Recovery = 81% Analysis Date = 07/15/11 Pct Recovery = 81% Analysis Date = 07/15/11 Pct Recovery = 81% Analysis Date = 07/04/11 Pct Recovery = 81% Analysis Date = 07/04/11 Pct Recovery = 81% Analysis Date = 06/23/11 Pct Recovery = 81% Analysis Date = 06/23/11 Pct Recovery = 81% Analysis Date = 06/13/11 Pct Recovery = 81% Analysis Date = 06/13/11 Pct Recovery = 81% Analysis Date = 06/02/11 Pct Recovery = 81% Analysis Date = 06/02/11 Pct Recovery = 81% Analysis Date = 05/22/11 Pct Recovery = 81% Analysis Date = 05/22/11 Pct Recovery = 81% Analysis Date = 05/11/11 Pct Recovery = 81% Analysis Date = 05/11/11 Pct Recovery = 81% Analysis Date = 04/30/11 Pct Recovery = 81% Analysis Date = 04/30/11 Pct Recovery = 81% Analysis Date = 04/19/11 Pct Recovery = 81% Analysis Date = 04/19/11 Pct Recovery = 81% Analysis Date = 04/09/11 Pct Recovery = 81% Analysis Date = 04/09/11 Pct Recovery = 81% Analysis Date = 03/29/11 Pct Recovery = 81% Analysis Date = 03/29/11 Pct Recovery = 81% Analysis Date = 03/18/11 Pct Recovery = 81% Analysis Date = 03/18/11 Pct Recovery = 81% Analysis Date = 03/07/11 Pct Recovery = 80% Analysis Date = 03/07/11 Pct Recovery = 80% Analysis Date = 02/24/11 Pct Recovery = 80% Analysis Date = 02/24/11 Pct Recovery = 80% Analysis Date = 02/14/11 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 95 82% 15% 81% 14%
Total 95 82% 15% 81% 14%

Sample Statistics
CHLORPYRIFOS

Characteristic N % % Basis
Plotted 95 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 95 .  
False Negatives 0 0% 0 out of 95
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

BQS OBSP Determination:
CHLORPYRIFOS, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61636GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 65% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 14% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 40% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 28% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 34% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 50% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 31% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 62% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 24% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 41% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 29% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 18% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 38% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 59% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 39% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 54% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 32% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 33% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 40% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 30% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 29% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 30% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 20% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 21% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 40% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 45% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 46% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 28% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 23% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 46% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 45% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 39% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 30% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 31% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 63% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 54% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 50% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 46% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 11% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 38% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 25% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 43% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 44% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 36% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 45% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 53% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 58% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 33% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 63% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 66% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 29% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 56% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 28% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 20% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 72% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 13% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 27% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 81% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 21% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 25% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 76% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 28% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 81% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 86% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 122% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 96% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 41% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 75% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 61% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 95% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 73% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 102% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 89% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 57% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 72% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 36% Analysis Date = 01/17/17 Pct Recovery = 52% Analysis Date = 01/07/17 Pct Recovery = 52% Analysis Date = 01/07/17 Pct Recovery = 52% Analysis Date = 12/27/16 Pct Recovery = 52% Analysis Date = 12/27/16 Pct Recovery = 52% Analysis Date = 12/16/16 Pct Recovery = 51% Analysis Date = 12/16/16 Pct Recovery = 51% Analysis Date = 12/05/16 Pct Recovery = 51% Analysis Date = 12/05/16 Pct Recovery = 51% Analysis Date = 11/24/16 Pct Recovery = 51% Analysis Date = 11/24/16 Pct Recovery = 51% Analysis Date = 11/13/16 Pct Recovery = 50% Analysis Date = 11/13/16 Pct Recovery = 50% Analysis Date = 11/03/16 Pct Recovery = 50% Analysis Date = 11/03/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/23/16 Pct Recovery = 50% Analysis Date = 10/12/16 Pct Recovery = 50% Analysis Date = 10/12/16 Pct Recovery = 50% Analysis Date = 10/01/16 Pct Recovery = 49% Analysis Date = 10/01/16 Pct Recovery = 49% Analysis Date = 09/20/16 Pct Recovery = 49% Analysis Date = 09/20/16 Pct Recovery = 49% Analysis Date = 09/09/16 Pct Recovery = 49% Analysis Date = 09/09/16 Pct Recovery = 49% Analysis Date = 08/29/16 Pct Recovery = 49% Analysis Date = 08/29/16 Pct Recovery = 49% Analysis Date = 08/19/16 Pct Recovery = 48% Analysis Date = 08/19/16 Pct Recovery = 48% Analysis Date = 08/08/16 Pct Recovery = 48% Analysis Date = 08/08/16 Pct Recovery = 48% Analysis Date = 07/28/16 Pct Recovery = 48% Analysis Date = 07/28/16 Pct Recovery = 48% Analysis Date = 07/17/16 Pct Recovery = 47% Analysis Date = 07/17/16 Pct Recovery = 47% Analysis Date = 07/06/16 Pct Recovery = 47% Analysis Date = 07/06/16 Pct Recovery = 47% Analysis Date = 06/25/16 Pct Recovery = 47% Analysis Date = 06/25/16 Pct Recovery = 47% Analysis Date = 06/14/16 Pct Recovery = 47% Analysis Date = 06/14/16 Pct Recovery = 47% Analysis Date = 06/04/16 Pct Recovery = 46% Analysis Date = 06/04/16 Pct Recovery = 46% Analysis Date = 05/24/16 Pct Recovery = 46% Analysis Date = 05/24/16 Pct Recovery = 46% Analysis Date = 05/13/16 Pct Recovery = 46% Analysis Date = 05/13/16 Pct Recovery = 46% Analysis Date = 05/02/16 Pct Recovery = 45% Analysis Date = 05/02/16 Pct Recovery = 45% Analysis Date = 04/21/16 Pct Recovery = 45% Analysis Date = 04/21/16 Pct Recovery = 45% Analysis Date = 04/10/16 Pct Recovery = 45% Analysis Date = 04/10/16 Pct Recovery = 45% Analysis Date = 03/31/16 Pct Recovery = 45% Analysis Date = 03/31/16 Pct Recovery = 45% Analysis Date = 03/20/16 Pct Recovery = 44% Analysis Date = 03/20/16 Pct Recovery = 44% Analysis Date = 03/09/16 Pct Recovery = 44% Analysis Date = 03/09/16 Pct Recovery = 44% Analysis Date = 02/27/16 Pct Recovery = 44% Analysis Date = 02/27/16 Pct Recovery = 44% Analysis Date = 02/16/16 Pct Recovery = 44% Analysis Date = 02/16/16 Pct Recovery = 44% Analysis Date = 02/05/16 Pct Recovery = 44% Analysis Date = 02/05/16 Pct Recovery = 44% Analysis Date = 01/25/16 Pct Recovery = 43% Analysis Date = 01/25/16 Pct Recovery = 43% Analysis Date = 01/15/16 Pct Recovery = 43% Analysis Date = 01/15/16 Pct Recovery = 43% Analysis Date = 01/04/16 Pct Recovery = 43% Analysis Date = 01/04/16 Pct Recovery = 43% Analysis Date = 12/24/15 Pct Recovery = 43% Analysis Date = 12/24/15 Pct Recovery = 43% Analysis Date = 12/13/15 Pct Recovery = 42% Analysis Date = 12/13/15 Pct Recovery = 42% Analysis Date = 12/02/15 Pct Recovery = 42% Analysis Date = 12/02/15 Pct Recovery = 42% Analysis Date = 11/21/15 Pct Recovery = 42% Analysis Date = 11/21/15 Pct Recovery = 42% Analysis Date = 11/10/15 Pct Recovery = 42% Analysis Date = 11/10/15 Pct Recovery = 42% Analysis Date = 10/31/15 Pct Recovery = 42% Analysis Date = 10/31/15 Pct Recovery = 42% Analysis Date = 10/20/15 Pct Recovery = 41% Analysis Date = 10/20/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 09/28/15 Pct Recovery = 41% Analysis Date = 09/28/15 Pct Recovery = 41% Analysis Date = 09/17/15 Pct Recovery = 41% Analysis Date = 09/17/15 Pct Recovery = 41% Analysis Date = 09/06/15 Pct Recovery = 40% Analysis Date = 09/06/15 Pct Recovery = 40% Analysis Date = 08/27/15 Pct Recovery = 40% Analysis Date = 08/27/15 Pct Recovery = 40% Analysis Date = 08/16/15 Pct Recovery = 40% Analysis Date = 08/16/15 Pct Recovery = 40% Analysis Date = 08/05/15 Pct Recovery = 40% Analysis Date = 08/05/15 Pct Recovery = 40% Analysis Date = 07/25/15 Pct Recovery = 39% Analysis Date = 07/25/15 Pct Recovery = 39% Analysis Date = 07/14/15 Pct Recovery = 39% Analysis Date = 07/14/15 Pct Recovery = 39% Analysis Date = 07/03/15 Pct Recovery = 39% Analysis Date = 07/03/15 Pct Recovery = 39% Analysis Date = 06/22/15 Pct Recovery = 39% Analysis Date = 06/22/15 Pct Recovery = 39% Analysis Date = 06/12/15 Pct Recovery = 38% Analysis Date = 06/12/15 Pct Recovery = 38% Analysis Date = 06/01/15 Pct Recovery = 38% Analysis Date = 06/01/15 Pct Recovery = 38% Analysis Date = 05/21/15 Pct Recovery = 38% Analysis Date = 05/21/15 Pct Recovery = 38% Analysis Date = 05/10/15 Pct Recovery = 37% Analysis Date = 05/10/15 Pct Recovery = 37% Analysis Date = 04/29/15 Pct Recovery = 37% Analysis Date = 04/29/15 Pct Recovery = 37% Analysis Date = 04/18/15 Pct Recovery = 37% Analysis Date = 04/18/15 Pct Recovery = 37% Analysis Date = 04/07/15 Pct Recovery = 37% Analysis Date = 04/07/15 Pct Recovery = 37% Analysis Date = 03/28/15 Pct Recovery = 37% Analysis Date = 03/28/15 Pct Recovery = 37% Analysis Date = 03/17/15 Pct Recovery = 37% Analysis Date = 03/17/15 Pct Recovery = 37% Analysis Date = 03/06/15 Pct Recovery = 37% Analysis Date = 03/06/15 Pct Recovery = 37% Analysis Date = 02/23/15 Pct Recovery = 36% Analysis Date = 02/23/15 Pct Recovery = 36% Analysis Date = 02/12/15 Pct Recovery = 36% Analysis Date = 02/12/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 01/22/15 Pct Recovery = 36% Analysis Date = 01/22/15 Pct Recovery = 36% Analysis Date = 01/11/15 Pct Recovery = 36% Analysis Date = 01/11/15 Pct Recovery = 36% Analysis Date = 12/31/14 Pct Recovery = 36% Analysis Date = 12/31/14 Pct Recovery = 36% Analysis Date = 12/20/14 Pct Recovery = 36% Analysis Date = 12/20/14 Pct Recovery = 36% Analysis Date = 12/09/14 Pct Recovery = 35% Analysis Date = 12/09/14 Pct Recovery = 35% Analysis Date = 11/28/14 Pct Recovery = 35% Analysis Date = 11/28/14 Pct Recovery = 35% Analysis Date = 11/17/14 Pct Recovery = 35% Analysis Date = 11/17/14 Pct Recovery = 35% Analysis Date = 11/07/14 Pct Recovery = 35% Analysis Date = 11/07/14 Pct Recovery = 35% Analysis Date = 10/27/14 Pct Recovery = 35% Analysis Date = 10/27/14 Pct Recovery = 35% Analysis Date = 10/16/14 Pct Recovery = 35% Analysis Date = 10/16/14 Pct Recovery = 35% Analysis Date = 10/05/14 Pct Recovery = 35% Analysis Date = 10/05/14 Pct Recovery = 35% Analysis Date = 09/24/14 Pct Recovery = 35% Analysis Date = 09/24/14 Pct Recovery = 35% Analysis Date = 09/13/14 Pct Recovery = 35% Analysis Date = 09/13/14 Pct Recovery = 35% Analysis Date = 09/02/14 Pct Recovery = 35% Analysis Date = 09/02/14 Pct Recovery = 35% Analysis Date = 08/23/14 Pct Recovery = 36% Analysis Date = 08/23/14 Pct Recovery = 36% Analysis Date = 08/12/14 Pct Recovery = 36% Analysis Date = 08/12/14 Pct Recovery = 36% Analysis Date = 08/01/14 Pct Recovery = 36% Analysis Date = 08/01/14 Pct Recovery = 36% Analysis Date = 07/21/14 Pct Recovery = 36% Analysis Date = 07/21/14 Pct Recovery = 36% Analysis Date = 07/10/14 Pct Recovery = 36% Analysis Date = 07/10/14 Pct Recovery = 36% Analysis Date = 06/29/14 Pct Recovery = 36% Analysis Date = 06/29/14 Pct Recovery = 36% Analysis Date = 06/19/14 Pct Recovery = 36% Analysis Date = 06/19/14 Pct Recovery = 36% Analysis Date = 06/08/14 Pct Recovery = 36% Analysis Date = 06/08/14 Pct Recovery = 36% Analysis Date = 05/28/14 Pct Recovery = 36% Analysis Date = 05/28/14 Pct Recovery = 36% Analysis Date = 05/17/14 Pct Recovery = 36% Analysis Date = 05/17/14 Pct Recovery = 36% Analysis Date = 05/06/14 Pct Recovery = 36% Analysis Date = 05/06/14 Pct Recovery = 36% Analysis Date = 04/25/14 Pct Recovery = 37% Analysis Date = 04/25/14 Pct Recovery = 37% Analysis Date = 04/14/14 Pct Recovery = 37% Analysis Date = 04/14/14 Pct Recovery = 37% Analysis Date = 04/04/14 Pct Recovery = 37% Analysis Date = 04/04/14 Pct Recovery = 37% Analysis Date = 03/24/14 Pct Recovery = 37% Analysis Date = 03/24/14 Pct Recovery = 37% Analysis Date = 03/13/14 Pct Recovery = 37% Analysis Date = 03/13/14 Pct Recovery = 37% Analysis Date = 03/02/14 Pct Recovery = 37% Analysis Date = 03/02/14 Pct Recovery = 37% Analysis Date = 02/19/14 Pct Recovery = 37% Analysis Date = 02/19/14 Pct Recovery = 37% Analysis Date = 02/08/14 Pct Recovery = 38% Analysis Date = 02/08/14 Pct Recovery = 38% Analysis Date = 01/28/14 Pct Recovery = 38% Analysis Date = 01/28/14 Pct Recovery = 38% Analysis Date = 01/18/14 Pct Recovery = 38% Analysis Date = 01/18/14 Pct Recovery = 38% Analysis Date = 01/07/14 Pct Recovery = 38% Analysis Date = 01/07/14 Pct Recovery = 38% Analysis Date = 12/27/13 Pct Recovery = 39% Analysis Date = 12/27/13 Pct Recovery = 39% Analysis Date = 12/16/13 Pct Recovery = 39% Analysis Date = 12/16/13 Pct Recovery = 39% Analysis Date = 12/05/13 Pct Recovery = 39% Analysis Date = 12/05/13 Pct Recovery = 39% Analysis Date = 11/24/13 Pct Recovery = 40% Analysis Date = 11/24/13 Pct Recovery = 40% Analysis Date = 11/14/13 Pct Recovery = 40% Analysis Date = 11/14/13 Pct Recovery = 40% Analysis Date = 11/03/13 Pct Recovery = 40% Analysis Date = 11/03/13 Pct Recovery = 40% Analysis Date = 10/23/13 Pct Recovery = 41% Analysis Date = 10/23/13 Pct Recovery = 41% Analysis Date = 10/12/13 Pct Recovery = 41% Analysis Date = 10/12/13 Pct Recovery = 41% Analysis Date = 10/01/13 Pct Recovery = 41% Analysis Date = 10/01/13 Pct Recovery = 41% Analysis Date = 09/20/13 Pct Recovery = 42% Analysis Date = 09/20/13 Pct Recovery = 42% Analysis Date = 09/09/13 Pct Recovery = 42% Analysis Date = 09/09/13 Pct Recovery = 42% Analysis Date = 08/30/13 Pct Recovery = 42% Analysis Date = 08/30/13 Pct Recovery = 42% Analysis Date = 08/19/13 Pct Recovery = 43% Analysis Date = 08/19/13 Pct Recovery = 43% Analysis Date = 08/08/13 Pct Recovery = 43% Analysis Date = 08/08/13 Pct Recovery = 43% Analysis Date = 07/28/13 Pct Recovery = 43% Analysis Date = 07/28/13 Pct Recovery = 43% Analysis Date = 07/17/13 Pct Recovery = 44% Analysis Date = 07/17/13 Pct Recovery = 44% Analysis Date = 07/06/13 Pct Recovery = 44% Analysis Date = 07/06/13 Pct Recovery = 44% Analysis Date = 06/25/13 Pct Recovery = 45% Analysis Date = 06/25/13 Pct Recovery = 45% Analysis Date = 06/15/13 Pct Recovery = 45% Analysis Date = 06/15/13 Pct Recovery = 45% Analysis Date = 06/04/13 Pct Recovery = 46% Analysis Date = 06/04/13 Pct Recovery = 46% Analysis Date = 05/24/13 Pct Recovery = 46% Analysis Date = 05/24/13 Pct Recovery = 46% Analysis Date = 05/13/13 Pct Recovery = 46% Analysis Date = 05/13/13 Pct Recovery = 46% Analysis Date = 05/02/13 Pct Recovery = 47% Analysis Date = 05/02/13 Pct Recovery = 47% Analysis Date = 04/21/13 Pct Recovery = 47% Analysis Date = 04/21/13 Pct Recovery = 47% Analysis Date = 04/11/13 Pct Recovery = 48% Analysis Date = 04/11/13 Pct Recovery = 48% Analysis Date = 03/31/13 Pct Recovery = 48% Analysis Date = 03/31/13 Pct Recovery = 48% Analysis Date = 03/20/13 Pct Recovery = 49% Analysis Date = 03/20/13 Pct Recovery = 49% Analysis Date = 03/09/13 Pct Recovery = 49% Analysis Date = 03/09/13 Pct Recovery = 49% Analysis Date = 02/26/13 Pct Recovery = 50% Analysis Date = 02/26/13 Pct Recovery = 50% Analysis Date = 02/15/13 Pct Recovery = 50% Analysis Date = 02/15/13 Pct Recovery = 50% Analysis Date = 02/04/13 Pct Recovery = 50% Analysis Date = 02/04/13 Pct Recovery = 50% Analysis Date = 01/25/13 Pct Recovery = 51% Analysis Date = 01/25/13 Pct Recovery = 51% Analysis Date = 01/14/13 Pct Recovery = 51% Analysis Date = 01/14/13 Pct Recovery = 51% Analysis Date = 01/03/13 Pct Recovery = 51% Analysis Date = 01/03/13 Pct Recovery = 51% Analysis Date = 12/23/12 Pct Recovery = 52% Analysis Date = 12/23/12 Pct Recovery = 52% Analysis Date = 12/12/12 Pct Recovery = 52% Analysis Date = 12/12/12 Pct Recovery = 52% Analysis Date = 12/01/12 Pct Recovery = 52% Analysis Date = 12/01/12 Pct Recovery = 52% Analysis Date = 11/20/12 Pct Recovery = 53% Analysis Date = 11/20/12 Pct Recovery = 53% Analysis Date = 11/10/12 Pct Recovery = 53% Analysis Date = 11/10/12 Pct Recovery = 53% Analysis Date = 10/30/12 Pct Recovery = 53% Analysis Date = 10/30/12 Pct Recovery = 53% Analysis Date = 10/19/12 Pct Recovery = 53% Analysis Date = 10/19/12 Pct Recovery = 53% Analysis Date = 10/08/12 Pct Recovery = 54% Analysis Date = 10/08/12 Pct Recovery = 54% Analysis Date = 09/27/12 Pct Recovery = 54% Analysis Date = 09/27/12 Pct Recovery = 54% Analysis Date = 09/16/12 Pct Recovery = 54% Analysis Date = 09/16/12 Pct Recovery = 54% Analysis Date = 09/06/12 Pct Recovery = 55% Analysis Date = 09/06/12 Pct Recovery = 55% Analysis Date = 08/26/12 Pct Recovery = 55% Analysis Date = 08/26/12 Pct Recovery = 55% Analysis Date = 08/15/12 Pct Recovery = 55% Analysis Date = 08/15/12 Pct Recovery = 55% Analysis Date = 08/04/12 Pct Recovery = 56% Analysis Date = 08/04/12 Pct Recovery = 56% Analysis Date = 07/24/12 Pct Recovery = 56% Analysis Date = 07/24/12 Pct Recovery = 56% Analysis Date = 07/13/12 Pct Recovery = 56% Analysis Date = 07/13/12 Pct Recovery = 56% Analysis Date = 07/02/12 Pct Recovery = 57% Analysis Date = 07/02/12 Pct Recovery = 57% Analysis Date = 06/22/12 Pct Recovery = 57% Analysis Date = 06/22/12 Pct Recovery = 57% Analysis Date = 06/11/12 Pct Recovery = 57% Analysis Date = 06/11/12 Pct Recovery = 57% Analysis Date = 05/31/12 Pct Recovery = 58% Analysis Date = 05/31/12 Pct Recovery = 58% Analysis Date = 05/20/12 Pct Recovery = 58% Analysis Date = 05/20/12 Pct Recovery = 58% Analysis Date = 05/09/12 Pct Recovery = 58% Analysis Date = 05/09/12 Pct Recovery = 58% Analysis Date = 04/28/12 Pct Recovery = 58% Analysis Date = 04/28/12 Pct Recovery = 58% Analysis Date = 04/17/12 Pct Recovery = 59% Analysis Date = 04/17/12 Pct Recovery = 59% Analysis Date = 04/07/12 Pct Recovery = 59% Analysis Date = 04/07/12 Pct Recovery = 59% Analysis Date = 03/27/12 Pct Recovery = 59% Analysis Date = 03/27/12 Pct Recovery = 59% Analysis Date = 03/16/12 Pct Recovery = 60% Analysis Date = 03/16/12 Pct Recovery = 60% Analysis Date = 03/05/12 Pct Recovery = 60% Analysis Date = 03/05/12 Pct Recovery = 60% Analysis Date = 02/23/12 Pct Recovery = 60% Analysis Date = 02/23/12 Pct Recovery = 60% Analysis Date = 02/12/12 Pct Recovery = 61% Analysis Date = 02/12/12 Pct Recovery = 61% Analysis Date = 02/02/12 Pct Recovery = 61% Analysis Date = 02/02/12 Pct Recovery = 61% Analysis Date = 01/22/12 Pct Recovery = 61% Analysis Date = 01/22/12 Pct Recovery = 61% Analysis Date = 01/11/12 Pct Recovery = 62% Analysis Date = 01/11/12 Pct Recovery = 62% Analysis Date = 12/31/11 Pct Recovery = 62% Analysis Date = 12/31/11 Pct Recovery = 62% Analysis Date = 12/20/11 Pct Recovery = 62% Analysis Date = 12/20/11 Pct Recovery = 62% Analysis Date = 12/09/11 Pct Recovery = 63% Analysis Date = 12/09/11 Pct Recovery = 63% Analysis Date = 11/28/11 Pct Recovery = 63% Analysis Date = 11/28/11 Pct Recovery = 63% Analysis Date = 11/18/11 Pct Recovery = 63% Analysis Date = 11/18/11 Pct Recovery = 63% Analysis Date = 11/07/11 Pct Recovery = 64% Analysis Date = 11/07/11 Pct Recovery = 64% Analysis Date = 10/27/11 Pct Recovery = 64% Analysis Date = 10/27/11 Pct Recovery = 64% Analysis Date = 10/16/11 Pct Recovery = 64% Analysis Date = 10/16/11 Pct Recovery = 64% Analysis Date = 10/05/11 Pct Recovery = 64% Analysis Date = 10/05/11 Pct Recovery = 64% Analysis Date = 09/24/11 Pct Recovery = 65% Analysis Date = 09/24/11 Pct Recovery = 65% Analysis Date = 09/13/11 Pct Recovery = 65% Analysis Date = 09/13/11 Pct Recovery = 65% Analysis Date = 09/03/11 Pct Recovery = 65% Analysis Date = 09/03/11 Pct Recovery = 65% Analysis Date = 08/23/11 Pct Recovery = 66% Analysis Date = 08/23/11 Pct Recovery = 66% Analysis Date = 08/12/11 Pct Recovery = 66% Analysis Date = 08/12/11 Pct Recovery = 66% Analysis Date = 08/01/11 Pct Recovery = 66% Analysis Date = 08/01/11 Pct Recovery = 66% Analysis Date = 07/21/11 Pct Recovery = 66% Analysis Date = 07/21/11 Pct Recovery = 66% Analysis Date = 07/10/11 Pct Recovery = 67% Analysis Date = 07/10/11 Pct Recovery = 67% Analysis Date = 06/30/11 Pct Recovery = 67% Analysis Date = 06/30/11 Pct Recovery = 67% Analysis Date = 06/19/11 Pct Recovery = 67% Analysis Date = 06/19/11 Pct Recovery = 67% Analysis Date = 06/08/11 Pct Recovery = 67% Analysis Date = 06/08/11 Pct Recovery = 67% Analysis Date = 05/28/11 Pct Recovery = 68% Analysis Date = 05/28/11 Pct Recovery = 68% Analysis Date = 05/17/11 Pct Recovery = 68% Analysis Date = 05/17/11 Pct Recovery = 68% Analysis Date = 05/06/11 Pct Recovery = 68% Analysis Date = 05/06/11 Pct Recovery = 68% Analysis Date = 04/25/11 Pct Recovery = 68% Analysis Date = 04/25/11 Pct Recovery = 68% Analysis Date = 04/15/11 Pct Recovery = 69% Analysis Date = 04/15/11 Pct Recovery = 69% Analysis Date = 04/04/11 Pct Recovery = 69% Analysis Date = 04/04/11 Pct Recovery = 69% Analysis Date = 03/24/11 Pct Recovery = 69% Analysis Date = 03/24/11 Pct Recovery = 69% Analysis Date = 03/13/11 Pct Recovery = 69% Analysis Date = 03/13/11 Pct Recovery = 69% Analysis Date = 03/02/11 Pct Recovery = 70% Analysis Date = 03/02/11 Pct Recovery = 70% Analysis Date = 02/19/11 Pct Recovery = 70% Analysis Date = 02/19/11 Pct Recovery = 70% Analysis Date = 02/09/11 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS, OXYGEN ANALOG

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 72% 23% 73% 24%
>= Reporting Level 72 45% 22% 40% 22%
Total 78 47% 23% 41% 23%

Sample Statistics
CHLORPYRIFOS, OXYGEN ANALOG

Characteristic N % % Basis
Plotted 78 94% Spiked
Estimated Values 78 94% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 83 .  
False Negatives 5 6% 5 out of 83
Not Spiked 76 .  
False Positives 1 1% 1 out of 76

BQS OBSP Determination:
CIS-PERMETHRIN
METHOD: 2033 , TESTIDCODE: 82687GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 50% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 58% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 55% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 63% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 115% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 56% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 60% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 37% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 91% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 51% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 46% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 54% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 55% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 95% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 72% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 69% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 56% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 73% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 48% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 67% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 74% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 56% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 53% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 48% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 71% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 78% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 49% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 46% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 95% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 41% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 52% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 73% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 66% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 54% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 42% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 38% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 78% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 89% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 54% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 66% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 92% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 78% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 90% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 70% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 56% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 70% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 61% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 51% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 63% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 49% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 58% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 40% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 53% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 93% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 86% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 49% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 85% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 50% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 77% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 85% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 74% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 34% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 78% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 76% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 66% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 74% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 76% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 72% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 80% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 105% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 76% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 81% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 54% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 67% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 139% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 90% Analysis Date = 01/17/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 12/27/16 Pct Recovery = 72% Analysis Date = 12/27/16 Pct Recovery = 72% Analysis Date = 12/16/16 Pct Recovery = 72% Analysis Date = 12/16/16 Pct Recovery = 72% Analysis Date = 12/05/16 Pct Recovery = 72% Analysis Date = 12/05/16 Pct Recovery = 72% Analysis Date = 11/24/16 Pct Recovery = 71% Analysis Date = 11/24/16 Pct Recovery = 71% Analysis Date = 11/13/16 Pct Recovery = 71% Analysis Date = 11/13/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/12/16 Pct Recovery = 71% Analysis Date = 10/12/16 Pct Recovery = 71% Analysis Date = 10/01/16 Pct Recovery = 71% Analysis Date = 10/01/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/09/16 Pct Recovery = 71% Analysis Date = 09/09/16 Pct Recovery = 71% Analysis Date = 08/29/16 Pct Recovery = 71% Analysis Date = 08/29/16 Pct Recovery = 71% Analysis Date = 08/19/16 Pct Recovery = 71% Analysis Date = 08/19/16 Pct Recovery = 71% Analysis Date = 08/08/16 Pct Recovery = 71% Analysis Date = 08/08/16 Pct Recovery = 71% Analysis Date = 07/28/16 Pct Recovery = 71% Analysis Date = 07/28/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/06/16 Pct Recovery = 71% Analysis Date = 07/06/16 Pct Recovery = 71% Analysis Date = 06/25/16 Pct Recovery = 71% Analysis Date = 06/25/16 Pct Recovery = 71% Analysis Date = 06/14/16 Pct Recovery = 71% Analysis Date = 06/14/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/13/16 Pct Recovery = 71% Analysis Date = 05/13/16 Pct Recovery = 71% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 04/21/16 Pct Recovery = 70% Analysis Date = 04/21/16 Pct Recovery = 70% Analysis Date = 04/10/16 Pct Recovery = 70% Analysis Date = 04/10/16 Pct Recovery = 70% Analysis Date = 03/30/16 Pct Recovery = 70% Analysis Date = 03/30/16 Pct Recovery = 70% Analysis Date = 03/20/16 Pct Recovery = 70% Analysis Date = 03/20/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 70% Analysis Date = 02/27/16 Pct Recovery = 70% Analysis Date = 02/27/16 Pct Recovery = 70% Analysis Date = 02/16/16 Pct Recovery = 70% Analysis Date = 02/16/16 Pct Recovery = 70% Analysis Date = 02/05/16 Pct Recovery = 70% Analysis Date = 02/05/16 Pct Recovery = 70% Analysis Date = 01/25/16 Pct Recovery = 70% Analysis Date = 01/25/16 Pct Recovery = 70% Analysis Date = 01/14/16 Pct Recovery = 70% Analysis Date = 01/14/16 Pct Recovery = 70% Analysis Date = 01/04/16 Pct Recovery = 70% Analysis Date = 01/04/16 Pct Recovery = 70% Analysis Date = 12/24/15 Pct Recovery = 70% Analysis Date = 12/24/15 Pct Recovery = 70% Analysis Date = 12/13/15 Pct Recovery = 69% Analysis Date = 12/13/15 Pct Recovery = 69% Analysis Date = 12/02/15 Pct Recovery = 69% Analysis Date = 12/02/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/21/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 11/10/15 Pct Recovery = 69% Analysis Date = 10/30/15 Pct Recovery = 69% Analysis Date = 10/30/15 Pct Recovery = 69% Analysis Date = 10/20/15 Pct Recovery = 69% Analysis Date = 10/20/15 Pct Recovery = 69% Analysis Date = 10/09/15 Pct Recovery = 69% Analysis Date = 10/09/15 Pct Recovery = 69% Analysis Date = 09/28/15 Pct Recovery = 69% Analysis Date = 09/28/15 Pct Recovery = 69% Analysis Date = 09/17/15 Pct Recovery = 69% Analysis Date = 09/17/15 Pct Recovery = 69% Analysis Date = 09/06/15 Pct Recovery = 69% Analysis Date = 09/06/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 68% Analysis Date = 08/15/15 Pct Recovery = 68% Analysis Date = 08/05/15 Pct Recovery = 68% Analysis Date = 08/05/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/25/15 Pct Recovery = 68% Analysis Date = 07/14/15 Pct Recovery = 68% Analysis Date = 07/14/15 Pct Recovery = 68% Analysis Date = 07/03/15 Pct Recovery = 68% Analysis Date = 07/03/15 Pct Recovery = 68% Analysis Date = 06/22/15 Pct Recovery = 68% Analysis Date = 06/22/15 Pct Recovery = 68% Analysis Date = 06/11/15 Pct Recovery = 68% Analysis Date = 06/11/15 Pct Recovery = 68% Analysis Date = 05/31/15 Pct Recovery = 68% Analysis Date = 05/31/15 Pct Recovery = 68% Analysis Date = 05/21/15 Pct Recovery = 68% Analysis Date = 05/21/15 Pct Recovery = 68% Analysis Date = 05/10/15 Pct Recovery = 68% Analysis Date = 05/10/15 Pct Recovery = 68% Analysis Date = 04/29/15 Pct Recovery = 68% Analysis Date = 04/29/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 68% Analysis Date = 04/18/15 Pct Recovery = 68% Analysis Date = 04/07/15 Pct Recovery = 67% Analysis Date = 04/07/15 Pct Recovery = 67% Analysis Date = 03/27/15 Pct Recovery = 67% Analysis Date = 03/27/15 Pct Recovery = 67% Analysis Date = 03/16/15 Pct Recovery = 67% Analysis Date = 03/16/15 Pct Recovery = 67% Analysis Date = 03/06/15 Pct Recovery = 67% Analysis Date = 03/06/15 Pct Recovery = 67% Analysis Date = 02/23/15 Pct Recovery = 67% Analysis Date = 02/23/15 Pct Recovery = 67% Analysis Date = 02/12/15 Pct Recovery = 67% Analysis Date = 02/12/15 Pct Recovery = 67% Analysis Date = 02/01/15 Pct Recovery = 67% Analysis Date = 02/01/15 Pct Recovery = 67% Analysis Date = 01/21/15 Pct Recovery = 67% Analysis Date = 01/21/15 Pct Recovery = 67% Analysis Date = 01/10/15 Pct Recovery = 67% Analysis Date = 01/10/15 Pct Recovery = 67% Analysis Date = 12/31/14 Pct Recovery = 67% Analysis Date = 12/31/14 Pct Recovery = 67% Analysis Date = 12/20/14 Pct Recovery = 67% Analysis Date = 12/20/14 Pct Recovery = 67% Analysis Date = 12/09/14 Pct Recovery = 67% Analysis Date = 12/09/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/28/14 Pct Recovery = 67% Analysis Date = 11/17/14 Pct Recovery = 66% Analysis Date = 11/17/14 Pct Recovery = 66% Analysis Date = 11/06/14 Pct Recovery = 66% Analysis Date = 11/06/14 Pct Recovery = 66% Analysis Date = 10/26/14 Pct Recovery = 66% Analysis Date = 10/26/14 Pct Recovery = 66% Analysis Date = 10/16/14 Pct Recovery = 66% Analysis Date = 10/16/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 09/24/14 Pct Recovery = 66% Analysis Date = 09/24/14 Pct Recovery = 66% Analysis Date = 09/13/14 Pct Recovery = 66% Analysis Date = 09/13/14 Pct Recovery = 66% Analysis Date = 09/02/14 Pct Recovery = 66% Analysis Date = 09/02/14 Pct Recovery = 66% Analysis Date = 08/22/14 Pct Recovery = 66% Analysis Date = 08/22/14 Pct Recovery = 66% Analysis Date = 08/11/14 Pct Recovery = 66% Analysis Date = 08/11/14 Pct Recovery = 66% Analysis Date = 08/01/14 Pct Recovery = 66% Analysis Date = 08/01/14 Pct Recovery = 66% Analysis Date = 07/21/14 Pct Recovery = 66% Analysis Date = 07/21/14 Pct Recovery = 66% Analysis Date = 07/10/14 Pct Recovery = 65% Analysis Date = 07/10/14 Pct Recovery = 65% Analysis Date = 06/29/14 Pct Recovery = 65% Analysis Date = 06/29/14 Pct Recovery = 65% Analysis Date = 06/18/14 Pct Recovery = 65% Analysis Date = 06/18/14 Pct Recovery = 65% Analysis Date = 06/07/14 Pct Recovery = 65% Analysis Date = 06/07/14 Pct Recovery = 65% Analysis Date = 05/27/14 Pct Recovery = 65% Analysis Date = 05/27/14 Pct Recovery = 65% Analysis Date = 05/17/14 Pct Recovery = 65% Analysis Date = 05/17/14 Pct Recovery = 65% Analysis Date = 05/06/14 Pct Recovery = 64% Analysis Date = 05/06/14 Pct Recovery = 64% Analysis Date = 04/25/14 Pct Recovery = 64% Analysis Date = 04/25/14 Pct Recovery = 64% Analysis Date = 04/14/14 Pct Recovery = 64% Analysis Date = 04/14/14 Pct Recovery = 64% Analysis Date = 04/03/14 Pct Recovery = 64% Analysis Date = 04/03/14 Pct Recovery = 64% Analysis Date = 03/23/14 Pct Recovery = 64% Analysis Date = 03/23/14 Pct Recovery = 64% Analysis Date = 03/12/14 Pct Recovery = 64% Analysis Date = 03/12/14 Pct Recovery = 64% Analysis Date = 03/02/14 Pct Recovery = 64% Analysis Date = 03/02/14 Pct Recovery = 64% Analysis Date = 02/19/14 Pct Recovery = 64% Analysis Date = 02/19/14 Pct Recovery = 64% Analysis Date = 02/08/14 Pct Recovery = 64% Analysis Date = 02/08/14 Pct Recovery = 64% Analysis Date = 01/28/14 Pct Recovery = 64% Analysis Date = 01/28/14 Pct Recovery = 64% Analysis Date = 01/17/14 Pct Recovery = 63% Analysis Date = 01/17/14 Pct Recovery = 63% Analysis Date = 01/06/14 Pct Recovery = 63% Analysis Date = 01/06/14 Pct Recovery = 63% Analysis Date = 12/26/13 Pct Recovery = 63% Analysis Date = 12/26/13 Pct Recovery = 63% Analysis Date = 12/16/13 Pct Recovery = 63% Analysis Date = 12/16/13 Pct Recovery = 63% Analysis Date = 12/05/13 Pct Recovery = 63% Analysis Date = 12/05/13 Pct Recovery = 63% Analysis Date = 11/24/13 Pct Recovery = 63% Analysis Date = 11/24/13 Pct Recovery = 63% Analysis Date = 11/13/13 Pct Recovery = 63% Analysis Date = 11/13/13 Pct Recovery = 63% Analysis Date = 11/02/13 Pct Recovery = 63% Analysis Date = 11/02/13 Pct Recovery = 63% Analysis Date = 10/22/13 Pct Recovery = 63% Analysis Date = 10/22/13 Pct Recovery = 63% Analysis Date = 10/11/13 Pct Recovery = 63% Analysis Date = 10/11/13 Pct Recovery = 63% Analysis Date = 10/01/13 Pct Recovery = 63% Analysis Date = 10/01/13 Pct Recovery = 63% Analysis Date = 09/20/13 Pct Recovery = 63% Analysis Date = 09/20/13 Pct Recovery = 63% Analysis Date = 09/09/13 Pct Recovery = 63% Analysis Date = 09/09/13 Pct Recovery = 63% Analysis Date = 08/29/13 Pct Recovery = 63% Analysis Date = 08/29/13 Pct Recovery = 63% Analysis Date = 08/18/13 Pct Recovery = 63% Analysis Date = 08/18/13 Pct Recovery = 63% Analysis Date = 08/07/13 Pct Recovery = 64% Analysis Date = 08/07/13 Pct Recovery = 64% Analysis Date = 07/27/13 Pct Recovery = 64% Analysis Date = 07/27/13 Pct Recovery = 64% Analysis Date = 07/17/13 Pct Recovery = 64% Analysis Date = 07/17/13 Pct Recovery = 64% Analysis Date = 07/06/13 Pct Recovery = 64% Analysis Date = 07/06/13 Pct Recovery = 64% Analysis Date = 06/25/13 Pct Recovery = 64% Analysis Date = 06/25/13 Pct Recovery = 64% Analysis Date = 06/14/13 Pct Recovery = 64% Analysis Date = 06/14/13 Pct Recovery = 64% Analysis Date = 06/03/13 Pct Recovery = 64% Analysis Date = 06/03/13 Pct Recovery = 64% Analysis Date = 05/23/13 Pct Recovery = 64% Analysis Date = 05/23/13 Pct Recovery = 64% Analysis Date = 05/12/13 Pct Recovery = 64% Analysis Date = 05/12/13 Pct Recovery = 64% Analysis Date = 05/02/13 Pct Recovery = 64% Analysis Date = 05/02/13 Pct Recovery = 64% Analysis Date = 04/21/13 Pct Recovery = 64% Analysis Date = 04/21/13 Pct Recovery = 64% Analysis Date = 04/10/13 Pct Recovery = 65% Analysis Date = 04/10/13 Pct Recovery = 65% Analysis Date = 03/30/13 Pct Recovery = 65% Analysis Date = 03/30/13 Pct Recovery = 65% Analysis Date = 03/19/13 Pct Recovery = 65% Analysis Date = 03/19/13 Pct Recovery = 65% Analysis Date = 03/08/13 Pct Recovery = 65% Analysis Date = 03/08/13 Pct Recovery = 65% Analysis Date = 02/25/13 Pct Recovery = 65% Analysis Date = 02/25/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 65% Analysis Date = 02/04/13 Pct Recovery = 65% Analysis Date = 02/04/13 Pct Recovery = 65% Analysis Date = 01/24/13 Pct Recovery = 65% Analysis Date = 01/24/13 Pct Recovery = 65% Analysis Date = 01/13/13 Pct Recovery = 66% Analysis Date = 01/13/13 Pct Recovery = 66% Analysis Date = 01/02/13 Pct Recovery = 66% Analysis Date = 01/02/13 Pct Recovery = 66% Analysis Date = 12/22/12 Pct Recovery = 66% Analysis Date = 12/22/12 Pct Recovery = 66% Analysis Date = 12/12/12 Pct Recovery = 66% Analysis Date = 12/12/12 Pct Recovery = 66% Analysis Date = 12/01/12 Pct Recovery = 66% Analysis Date = 12/01/12 Pct Recovery = 66% Analysis Date = 11/20/12 Pct Recovery = 66% Analysis Date = 11/20/12 Pct Recovery = 66% Analysis Date = 11/09/12 Pct Recovery = 66% Analysis Date = 11/09/12 Pct Recovery = 66% Analysis Date = 10/29/12 Pct Recovery = 66% Analysis Date = 10/29/12 Pct Recovery = 66% Analysis Date = 10/18/12 Pct Recovery = 66% Analysis Date = 10/18/12 Pct Recovery = 66% Analysis Date = 10/07/12 Pct Recovery = 66% Analysis Date = 10/07/12 Pct Recovery = 66% Analysis Date = 09/27/12 Pct Recovery = 66% Analysis Date = 09/27/12 Pct Recovery = 66% Analysis Date = 09/16/12 Pct Recovery = 66% Analysis Date = 09/16/12 Pct Recovery = 66% Analysis Date = 09/05/12 Pct Recovery = 66% Analysis Date = 09/05/12 Pct Recovery = 66% Analysis Date = 08/25/12 Pct Recovery = 67% Analysis Date = 08/25/12 Pct Recovery = 67% Analysis Date = 08/14/12 Pct Recovery = 67% Analysis Date = 08/14/12 Pct Recovery = 67% Analysis Date = 08/03/12 Pct Recovery = 67% Analysis Date = 08/03/12 Pct Recovery = 67% Analysis Date = 07/23/12 Pct Recovery = 67% Analysis Date = 07/23/12 Pct Recovery = 67% Analysis Date = 07/13/12 Pct Recovery = 67% Analysis Date = 07/13/12 Pct Recovery = 67% Analysis Date = 07/02/12 Pct Recovery = 67% Analysis Date = 07/02/12 Pct Recovery = 67% Analysis Date = 06/21/12 Pct Recovery = 67% Analysis Date = 06/21/12 Pct Recovery = 67% Analysis Date = 06/10/12 Pct Recovery = 67% Analysis Date = 06/10/12 Pct Recovery = 67% Analysis Date = 05/30/12 Pct Recovery = 67% Analysis Date = 05/30/12 Pct Recovery = 67% Analysis Date = 05/19/12 Pct Recovery = 68% Analysis Date = 05/19/12 Pct Recovery = 68% Analysis Date = 05/08/12 Pct Recovery = 68% Analysis Date = 05/08/12 Pct Recovery = 68% Analysis Date = 04/28/12 Pct Recovery = 68% Analysis Date = 04/28/12 Pct Recovery = 68% Analysis Date = 04/17/12 Pct Recovery = 68% Analysis Date = 04/17/12 Pct Recovery = 68% Analysis Date = 04/06/12 Pct Recovery = 68% Analysis Date = 04/06/12 Pct Recovery = 68% Analysis Date = 03/26/12 Pct Recovery = 68% Analysis Date = 03/26/12 Pct Recovery = 68% Analysis Date = 03/15/12 Pct Recovery = 68% Analysis Date = 03/15/12 Pct Recovery = 68% Analysis Date = 03/04/12 Pct Recovery = 68% Analysis Date = 03/04/12 Pct Recovery = 68% Analysis Date = 02/22/12 Pct Recovery = 69% Analysis Date = 02/22/12 Pct Recovery = 69% Analysis Date = 02/12/12 Pct Recovery = 69% Analysis Date = 02/12/12 Pct Recovery = 69% Analysis Date = 02/01/12 Pct Recovery = 69% Analysis Date = 02/01/12 Pct Recovery = 69% Analysis Date = 01/21/12 Pct Recovery = 69% Analysis Date = 01/21/12 Pct Recovery = 69% Analysis Date = 01/10/12 Pct Recovery = 69% Analysis Date = 01/10/12 Pct Recovery = 69% Analysis Date = 12/30/11 Pct Recovery = 69% Analysis Date = 12/30/11 Pct Recovery = 69% Analysis Date = 12/19/11 Pct Recovery = 69% Analysis Date = 12/19/11 Pct Recovery = 69% Analysis Date = 12/08/11 Pct Recovery = 69% Analysis Date = 12/08/11 Pct Recovery = 69% Analysis Date = 11/28/11 Pct Recovery = 70% Analysis Date = 11/28/11 Pct Recovery = 70% Analysis Date = 11/17/11 Pct Recovery = 70% Analysis Date = 11/17/11 Pct Recovery = 70% Analysis Date = 11/06/11 Pct Recovery = 70% Analysis Date = 11/06/11 Pct Recovery = 70% Analysis Date = 10/26/11 Pct Recovery = 70% Analysis Date = 10/26/11 Pct Recovery = 70% Analysis Date = 10/15/11 Pct Recovery = 70% Analysis Date = 10/15/11 Pct Recovery = 70% Analysis Date = 10/04/11 Pct Recovery = 70% Analysis Date = 10/04/11 Pct Recovery = 70% Analysis Date = 09/23/11 Pct Recovery = 70% Analysis Date = 09/23/11 Pct Recovery = 70% Analysis Date = 09/13/11 Pct Recovery = 70% Analysis Date = 09/13/11 Pct Recovery = 70% Analysis Date = 09/02/11 Pct Recovery = 71% Analysis Date = 09/02/11 Pct Recovery = 71% Analysis Date = 08/22/11 Pct Recovery = 71% Analysis Date = 08/22/11 Pct Recovery = 71% Analysis Date = 08/11/11 Pct Recovery = 71% Analysis Date = 08/11/11 Pct Recovery = 71% Analysis Date = 07/31/11 Pct Recovery = 71% Analysis Date = 07/31/11 Pct Recovery = 71% Analysis Date = 07/20/11 Pct Recovery = 71% Analysis Date = 07/20/11 Pct Recovery = 71% Analysis Date = 07/09/11 Pct Recovery = 71% Analysis Date = 07/09/11 Pct Recovery = 71% Analysis Date = 06/29/11 Pct Recovery = 71% Analysis Date = 06/29/11 Pct Recovery = 71% Analysis Date = 06/18/11 Pct Recovery = 71% Analysis Date = 06/18/11 Pct Recovery = 71% Analysis Date = 06/07/11 Pct Recovery = 71% Analysis Date = 06/07/11 Pct Recovery = 71% Analysis Date = 05/27/11 Pct Recovery = 72% Analysis Date = 05/27/11 Pct Recovery = 72% Analysis Date = 05/16/11 Pct Recovery = 72% Analysis Date = 05/16/11 Pct Recovery = 72% Analysis Date = 05/05/11 Pct Recovery = 72% Analysis Date = 05/05/11 Pct Recovery = 72% Analysis Date = 04/24/11 Pct Recovery = 72% Analysis Date = 04/24/11 Pct Recovery = 72% Analysis Date = 04/14/11 Pct Recovery = 72% Analysis Date = 04/14/11 Pct Recovery = 72% Analysis Date = 04/03/11 Pct Recovery = 72% Analysis Date = 04/03/11 Pct Recovery = 72% Analysis Date = 03/23/11 Pct Recovery = 72% Analysis Date = 03/23/11 Pct Recovery = 72% Analysis Date = 03/12/11 Pct Recovery = 72% Analysis Date = 03/12/11 Pct Recovery = 72% Analysis Date = 03/01/11 Pct Recovery = 73% Analysis Date = 03/01/11 Pct Recovery = 73% Analysis Date = 02/18/11 Pct Recovery = 73% Analysis Date = 02/18/11 Pct Recovery = 73% Analysis Date = 02/08/11 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-PERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 68% 18% 67% 18%
Total 89 68% 18% 67% 18%

Sample Statistics
CIS-PERMETHRIN

Characteristic N % % Basis
Plotted 89 100% Spiked
Estimated Values 4 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 89 .  
False Negatives 0 0% 0 out of 89
Not Spiked 80 .  
False Positives 0 0% 0 out of 80

BQS OBSP Determination:
CYANAZINE
METHOD: 2033 , TESTIDCODE: 04041GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 106% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 111% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 91% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 97% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 102% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 82% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 107% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 67% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 47% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 96% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 68% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 123% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 79% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 101% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 85% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 23% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 77% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 97% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 76% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 67% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 102% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 101% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 25% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 75% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 71% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 99% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 88% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 119% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 99% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 84% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 98% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 104% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 91% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 103% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 108% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 92% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 106% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 90% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 109% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 93% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 94% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 97% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 96% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 67% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 78% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 92% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 77% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 117% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 120% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 26% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 52% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 108% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 114% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 107% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 58% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 56% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 64% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 75% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 76% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 92% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 81% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 49% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 76% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 129% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 102% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 107% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 107% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 91% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 77% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 87% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 142% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 154% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 136% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 88% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 114% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 102% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 107% Analysis Date = 12/20/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/17/16 Pct Recovery = 74% Analysis Date = 11/17/16 Pct Recovery = 74% Analysis Date = 11/07/16 Pct Recovery = 74% Analysis Date = 11/07/16 Pct Recovery = 74% Analysis Date = 10/27/16 Pct Recovery = 74% Analysis Date = 10/27/16 Pct Recovery = 74% Analysis Date = 10/16/16 Pct Recovery = 74% Analysis Date = 10/16/16 Pct Recovery = 74% Analysis Date = 10/06/16 Pct Recovery = 74% Analysis Date = 10/06/16 Pct Recovery = 74% Analysis Date = 09/25/16 Pct Recovery = 74% Analysis Date = 09/25/16 Pct Recovery = 74% Analysis Date = 09/14/16 Pct Recovery = 74% Analysis Date = 09/14/16 Pct Recovery = 74% Analysis Date = 09/03/16 Pct Recovery = 74% Analysis Date = 09/03/16 Pct Recovery = 74% Analysis Date = 08/24/16 Pct Recovery = 74% Analysis Date = 08/24/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 74% Analysis Date = 05/09/16 Pct Recovery = 74% Analysis Date = 05/09/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 74% Analysis Date = 04/17/16 Pct Recovery = 75% Analysis Date = 04/17/16 Pct Recovery = 75% Analysis Date = 04/07/16 Pct Recovery = 75% Analysis Date = 04/07/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/16/16 Pct Recovery = 75% Analysis Date = 03/16/16 Pct Recovery = 75% Analysis Date = 03/05/16 Pct Recovery = 75% Analysis Date = 03/05/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 75% Analysis Date = 02/02/16 Pct Recovery = 75% Analysis Date = 02/02/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/12/16 Pct Recovery = 75% Analysis Date = 01/12/16 Pct Recovery = 75% Analysis Date = 01/01/16 Pct Recovery = 75% Analysis Date = 01/01/16 Pct Recovery = 75% Analysis Date = 12/22/15 Pct Recovery = 75% Analysis Date = 12/22/15 Pct Recovery = 75% Analysis Date = 12/11/15 Pct Recovery = 75% Analysis Date = 12/11/15 Pct Recovery = 75% Analysis Date = 11/30/15 Pct Recovery = 75% Analysis Date = 11/30/15 Pct Recovery = 75% Analysis Date = 11/19/15 Pct Recovery = 75% Analysis Date = 11/19/15 Pct Recovery = 75% Analysis Date = 11/09/15 Pct Recovery = 75% Analysis Date = 11/09/15 Pct Recovery = 75% Analysis Date = 10/29/15 Pct Recovery = 75% Analysis Date = 10/29/15 Pct Recovery = 75% Analysis Date = 10/18/15 Pct Recovery = 75% Analysis Date = 10/18/15 Pct Recovery = 75% Analysis Date = 10/08/15 Pct Recovery = 75% Analysis Date = 10/08/15 Pct Recovery = 75% Analysis Date = 09/27/15 Pct Recovery = 75% Analysis Date = 09/27/15 Pct Recovery = 75% Analysis Date = 09/16/15 Pct Recovery = 75% Analysis Date = 09/16/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/15/15 Pct Recovery = 75% Analysis Date = 08/15/15 Pct Recovery = 75% Analysis Date = 08/04/15 Pct Recovery = 75% Analysis Date = 08/04/15 Pct Recovery = 75% Analysis Date = 07/25/15 Pct Recovery = 75% Analysis Date = 07/25/15 Pct Recovery = 75% Analysis Date = 07/14/15 Pct Recovery = 75% Analysis Date = 07/14/15 Pct Recovery = 75% Analysis Date = 07/03/15 Pct Recovery = 75% Analysis Date = 07/03/15 Pct Recovery = 75% Analysis Date = 06/23/15 Pct Recovery = 75% Analysis Date = 06/23/15 Pct Recovery = 75% Analysis Date = 06/12/15 Pct Recovery = 75% Analysis Date = 06/12/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 05/21/15 Pct Recovery = 75% Analysis Date = 05/21/15 Pct Recovery = 75% Analysis Date = 05/11/15 Pct Recovery = 76% Analysis Date = 05/11/15 Pct Recovery = 76% Analysis Date = 04/30/15 Pct Recovery = 76% Analysis Date = 04/30/15 Pct Recovery = 76% Analysis Date = 04/19/15 Pct Recovery = 76% Analysis Date = 04/19/15 Pct Recovery = 76% Analysis Date = 04/09/15 Pct Recovery = 76% Analysis Date = 04/09/15 Pct Recovery = 76% Analysis Date = 03/29/15 Pct Recovery = 76% Analysis Date = 03/29/15 Pct Recovery = 76% Analysis Date = 03/18/15 Pct Recovery = 76% Analysis Date = 03/18/15 Pct Recovery = 76% Analysis Date = 03/07/15 Pct Recovery = 76% Analysis Date = 03/07/15 Pct Recovery = 76% Analysis Date = 02/25/15 Pct Recovery = 76% Analysis Date = 02/25/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/14/15 Pct Recovery = 76% Analysis Date = 02/03/15 Pct Recovery = 76% Analysis Date = 02/03/15 Pct Recovery = 76% Analysis Date = 01/24/15 Pct Recovery = 76% Analysis Date = 01/24/15 Pct Recovery = 76% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/13/15 Pct Recovery = 77% Analysis Date = 01/02/15 Pct Recovery = 77% Analysis Date = 01/02/15 Pct Recovery = 77% Analysis Date = 12/23/14 Pct Recovery = 77% Analysis Date = 12/23/14 Pct Recovery = 77% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/12/14 Pct Recovery = 78% Analysis Date = 12/01/14 Pct Recovery = 78% Analysis Date = 12/01/14 Pct Recovery = 78% Analysis Date = 11/20/14 Pct Recovery = 78% Analysis Date = 11/20/14 Pct Recovery = 78% Analysis Date = 11/10/14 Pct Recovery = 78% Analysis Date = 11/10/14 Pct Recovery = 78% Analysis Date = 10/30/14 Pct Recovery = 79% Analysis Date = 10/30/14 Pct Recovery = 79% Analysis Date = 10/19/14 Pct Recovery = 79% Analysis Date = 10/19/14 Pct Recovery = 79% Analysis Date = 10/09/14 Pct Recovery = 79% Analysis Date = 10/09/14 Pct Recovery = 79% Analysis Date = 09/28/14 Pct Recovery = 79% Analysis Date = 09/28/14 Pct Recovery = 79% Analysis Date = 09/17/14 Pct Recovery = 80% Analysis Date = 09/17/14 Pct Recovery = 80% Analysis Date = 09/07/14 Pct Recovery = 80% Analysis Date = 09/07/14 Pct Recovery = 80% Analysis Date = 08/27/14 Pct Recovery = 80% Analysis Date = 08/27/14 Pct Recovery = 80% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/05/14 Pct Recovery = 81% Analysis Date = 08/05/14 Pct Recovery = 81% Analysis Date = 07/26/14 Pct Recovery = 81% Analysis Date = 07/26/14 Pct Recovery = 81% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/04/14 Pct Recovery = 82% Analysis Date = 07/04/14 Pct Recovery = 82% Analysis Date = 06/24/14 Pct Recovery = 82% Analysis Date = 06/24/14 Pct Recovery = 82% Analysis Date = 06/13/14 Pct Recovery = 83% Analysis Date = 06/13/14 Pct Recovery = 83% Analysis Date = 06/02/14 Pct Recovery = 83% Analysis Date = 06/02/14 Pct Recovery = 83% Analysis Date = 05/22/14 Pct Recovery = 83% Analysis Date = 05/22/14 Pct Recovery = 83% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/12/14 Pct Recovery = 84% Analysis Date = 05/01/14 Pct Recovery = 84% Analysis Date = 05/01/14 Pct Recovery = 84% Analysis Date = 04/20/14 Pct Recovery = 84% Analysis Date = 04/20/14 Pct Recovery = 84% Analysis Date = 04/10/14 Pct Recovery = 85% Analysis Date = 04/10/14 Pct Recovery = 85% Analysis Date = 03/30/14 Pct Recovery = 85% Analysis Date = 03/30/14 Pct Recovery = 85% Analysis Date = 03/19/14 Pct Recovery = 86% Analysis Date = 03/19/14 Pct Recovery = 86% Analysis Date = 03/09/14 Pct Recovery = 86% Analysis Date = 03/09/14 Pct Recovery = 86% Analysis Date = 02/26/14 Pct Recovery = 86% Analysis Date = 02/26/14 Pct Recovery = 86% Analysis Date = 02/15/14 Pct Recovery = 87% Analysis Date = 02/15/14 Pct Recovery = 87% Analysis Date = 02/04/14 Pct Recovery = 87% Analysis Date = 02/04/14 Pct Recovery = 87% Analysis Date = 01/25/14 Pct Recovery = 87% Analysis Date = 01/25/14 Pct Recovery = 87% Analysis Date = 01/14/14 Pct Recovery = 88% Analysis Date = 01/14/14 Pct Recovery = 88% Analysis Date = 01/03/14 Pct Recovery = 88% Analysis Date = 01/03/14 Pct Recovery = 88% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/24/13 Pct Recovery = 89% Analysis Date = 12/13/13 Pct Recovery = 89% Analysis Date = 12/13/13 Pct Recovery = 89% Analysis Date = 12/02/13 Pct Recovery = 90% Analysis Date = 12/02/13 Pct Recovery = 90% Analysis Date = 11/21/13 Pct Recovery = 90% Analysis Date = 11/21/13 Pct Recovery = 90% Analysis Date = 11/11/13 Pct Recovery = 91% Analysis Date = 11/11/13 Pct Recovery = 91% Analysis Date = 10/31/13 Pct Recovery = 91% Analysis Date = 10/31/13 Pct Recovery = 91% Analysis Date = 10/20/13 Pct Recovery = 92% Analysis Date = 10/20/13 Pct Recovery = 92% Analysis Date = 10/10/13 Pct Recovery = 92% Analysis Date = 10/10/13 Pct Recovery = 92% Analysis Date = 09/29/13 Pct Recovery = 93% Analysis Date = 09/29/13 Pct Recovery = 93% Analysis Date = 09/18/13 Pct Recovery = 93% Analysis Date = 09/18/13 Pct Recovery = 93% Analysis Date = 09/08/13 Pct Recovery = 94% Analysis Date = 09/08/13 Pct Recovery = 94% Analysis Date = 08/28/13 Pct Recovery = 94% Analysis Date = 08/28/13 Pct Recovery = 94% Analysis Date = 08/17/13 Pct Recovery = 95% Analysis Date = 08/17/13 Pct Recovery = 95% Analysis Date = 08/06/13 Pct Recovery = 95% Analysis Date = 08/06/13 Pct Recovery = 95% Analysis Date = 07/27/13 Pct Recovery = 96% Analysis Date = 07/27/13 Pct Recovery = 96% Analysis Date = 07/16/13 Pct Recovery = 96% Analysis Date = 07/16/13 Pct Recovery = 96% Analysis Date = 07/05/13 Pct Recovery = 97% Analysis Date = 07/05/13 Pct Recovery = 97% Analysis Date = 06/25/13 Pct Recovery = 97% Analysis Date = 06/25/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 98% Analysis Date = 06/14/13 Pct Recovery = 98% Analysis Date = 06/03/13 Pct Recovery = 98% Analysis Date = 06/03/13 Pct Recovery = 98% Analysis Date = 05/23/13 Pct Recovery = 99% Analysis Date = 05/23/13 Pct Recovery = 99% Analysis Date = 05/13/13 Pct Recovery = 99% Analysis Date = 05/13/13 Pct Recovery = 99% Analysis Date = 05/02/13 Pct Recovery = 100% Analysis Date = 05/02/13 Pct Recovery = 100% Analysis Date = 04/21/13 Pct Recovery = 100% Analysis Date = 04/21/13 Pct Recovery = 100% Analysis Date = 04/11/13 Pct Recovery = 101% Analysis Date = 04/11/13 Pct Recovery = 101% Analysis Date = 03/31/13 Pct Recovery = 101% Analysis Date = 03/31/13 Pct Recovery = 101% Analysis Date = 03/20/13 Pct Recovery = 102% Analysis Date = 03/20/13 Pct Recovery = 102% Analysis Date = 03/10/13 Pct Recovery = 102% Analysis Date = 03/10/13 Pct Recovery = 102% Analysis Date = 02/27/13 Pct Recovery = 102% Analysis Date = 02/27/13 Pct Recovery = 102% Analysis Date = 02/16/13 Pct Recovery = 102% Analysis Date = 02/16/13 Pct Recovery = 102% Analysis Date = 02/05/13 Pct Recovery = 102% Analysis Date = 02/05/13 Pct Recovery = 102% Analysis Date = 01/26/13 Pct Recovery = 102% Analysis Date = 01/26/13 Pct Recovery = 102% Analysis Date = 01/15/13 Pct Recovery = 102% Analysis Date = 01/15/13 Pct Recovery = 102% Analysis Date = 01/04/13 Pct Recovery = 102% Analysis Date = 01/04/13 Pct Recovery = 102% Analysis Date = 12/25/12 Pct Recovery = 102% Analysis Date = 12/25/12 Pct Recovery = 102% Analysis Date = 12/14/12 Pct Recovery = 102% Analysis Date = 12/14/12 Pct Recovery = 102% Analysis Date = 12/03/12 Pct Recovery = 102% Analysis Date = 12/03/12 Pct Recovery = 102% Analysis Date = 11/23/12 Pct Recovery = 102% Analysis Date = 11/23/12 Pct Recovery = 102% Analysis Date = 11/12/12 Pct Recovery = 102% Analysis Date = 11/12/12 Pct Recovery = 102% Analysis Date = 11/01/12 Pct Recovery = 102% Analysis Date = 11/01/12 Pct Recovery = 102% Analysis Date = 10/21/12 Pct Recovery = 102% Analysis Date = 10/21/12 Pct Recovery = 102% Analysis Date = 10/11/12 Pct Recovery = 102% Analysis Date = 10/11/12 Pct Recovery = 102% Analysis Date = 09/30/12 Pct Recovery = 101% Analysis Date = 09/30/12 Pct Recovery = 101% Analysis Date = 09/19/12 Pct Recovery = 101% Analysis Date = 09/19/12 Pct Recovery = 101% Analysis Date = 09/09/12 Pct Recovery = 101% Analysis Date = 09/09/12 Pct Recovery = 101% Analysis Date = 08/29/12 Pct Recovery = 101% Analysis Date = 08/29/12 Pct Recovery = 101% Analysis Date = 08/18/12 Pct Recovery = 101% Analysis Date = 08/18/12 Pct Recovery = 101% Analysis Date = 08/07/12 Pct Recovery = 101% Analysis Date = 08/07/12 Pct Recovery = 101% Analysis Date = 07/28/12 Pct Recovery = 100% Analysis Date = 07/28/12 Pct Recovery = 100% Analysis Date = 07/17/12 Pct Recovery = 100% Analysis Date = 07/17/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 06/26/12 Pct Recovery = 100% Analysis Date = 06/26/12 Pct Recovery = 100% Analysis Date = 06/15/12 Pct Recovery = 100% Analysis Date = 06/15/12 Pct Recovery = 100% Analysis Date = 06/04/12 Pct Recovery = 100% Analysis Date = 06/04/12 Pct Recovery = 100% Analysis Date = 05/25/12 Pct Recovery = 99% Analysis Date = 05/25/12 Pct Recovery = 99% Analysis Date = 05/14/12 Pct Recovery = 99% Analysis Date = 05/14/12 Pct Recovery = 99% Analysis Date = 05/03/12 Pct Recovery = 99% Analysis Date = 05/03/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 99% Analysis Date = 04/12/12 Pct Recovery = 99% Analysis Date = 04/12/12 Pct Recovery = 99% Analysis Date = 04/01/12 Pct Recovery = 99% Analysis Date = 04/01/12 Pct Recovery = 99% Analysis Date = 03/21/12 Pct Recovery = 99% Analysis Date = 03/21/12 Pct Recovery = 99% Analysis Date = 03/11/12 Pct Recovery = 98% Analysis Date = 03/11/12 Pct Recovery = 98% Analysis Date = 02/29/12 Pct Recovery = 98% Analysis Date = 02/29/12 Pct Recovery = 98% Analysis Date = 02/18/12 Pct Recovery = 98% Analysis Date = 02/18/12 Pct Recovery = 98% Analysis Date = 02/07/12 Pct Recovery = 98% Analysis Date = 02/07/12 Pct Recovery = 98% Analysis Date = 01/28/12 Pct Recovery = 98% Analysis Date = 01/28/12 Pct Recovery = 98% Analysis Date = 01/17/12 Pct Recovery = 98% Analysis Date = 01/17/12 Pct Recovery = 98% Analysis Date = 01/06/12 Pct Recovery = 97% Analysis Date = 01/06/12 Pct Recovery = 97% Analysis Date = 12/27/11 Pct Recovery = 97% Analysis Date = 12/27/11 Pct Recovery = 97% Analysis Date = 12/16/11 Pct Recovery = 97% Analysis Date = 12/16/11 Pct Recovery = 97% Analysis Date = 12/05/11 Pct Recovery = 97% Analysis Date = 12/05/11 Pct Recovery = 97% Analysis Date = 11/25/11 Pct Recovery = 97% Analysis Date = 11/25/11 Pct Recovery = 97% Analysis Date = 11/14/11 Pct Recovery = 97% Analysis Date = 11/14/11 Pct Recovery = 97% Analysis Date = 11/03/11 Pct Recovery = 96% Analysis Date = 11/03/11 Pct Recovery = 96% Analysis Date = 10/23/11 Pct Recovery = 96% Analysis Date = 10/23/11 Pct Recovery = 96% Analysis Date = 10/13/11 Pct Recovery = 96% Analysis Date = 10/13/11 Pct Recovery = 96% Analysis Date = 10/02/11 Pct Recovery = 96% Analysis Date = 10/02/11 Pct Recovery = 96% Analysis Date = 09/21/11 Pct Recovery = 96% Analysis Date = 09/21/11 Pct Recovery = 96% Analysis Date = 09/11/11 Pct Recovery = 96% Analysis Date = 09/11/11 Pct Recovery = 96% Analysis Date = 08/31/11 Pct Recovery = 95% Analysis Date = 08/31/11 Pct Recovery = 95% Analysis Date = 08/20/11 Pct Recovery = 95% Analysis Date = 08/20/11 Pct Recovery = 95% Analysis Date = 08/09/11 Pct Recovery = 95% Analysis Date = 08/09/11 Pct Recovery = 95% Analysis Date = 07/30/11 Pct Recovery = 95% Analysis Date = 07/30/11 Pct Recovery = 95% Analysis Date = 07/19/11 Pct Recovery = 95% Analysis Date = 07/19/11 Pct Recovery = 95% Analysis Date = 07/08/11 Pct Recovery = 94% Analysis Date = 07/08/11 Pct Recovery = 94% Analysis Date = 06/28/11 Pct Recovery = 94% Analysis Date = 06/28/11 Pct Recovery = 94% Analysis Date = 06/17/11 Pct Recovery = 94% Analysis Date = 06/17/11 Pct Recovery = 94% Analysis Date = 06/06/11 Pct Recovery = 94% Analysis Date = 06/06/11 Pct Recovery = 94% Analysis Date = 05/27/11 Pct Recovery = 94% Analysis Date = 05/27/11 Pct Recovery = 94% Analysis Date = 05/16/11 Pct Recovery = 93% Analysis Date = 05/16/11 Pct Recovery = 93% Analysis Date = 05/05/11 Pct Recovery = 93% Analysis Date = 05/05/11 Pct Recovery = 93% Analysis Date = 04/24/11 Pct Recovery = 93% Analysis Date = 04/24/11 Pct Recovery = 93% Analysis Date = 04/14/11 Pct Recovery = 93% Analysis Date = 04/14/11 Pct Recovery = 93% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 03/23/11 Pct Recovery = 92% Analysis Date = 03/23/11 Pct Recovery = 92% Analysis Date = 03/13/11 Pct Recovery = 92% Analysis Date = 03/13/11 Pct Recovery = 92% Analysis Date = 03/02/11 Pct Recovery = 92% Analysis Date = 03/02/11 Pct Recovery = 92% Analysis Date = 02/19/11 Pct Recovery = 92% Analysis Date = 02/19/11 Pct Recovery = 92% Analysis Date = 02/09/11 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYANAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 88% 23% 89% 21%
Total 94 88% 23% 89% 21%

Sample Statistics
CYANAZINE

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 3 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
CYFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61585GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 12% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 59% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 78% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 14% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 23% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 77% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 66% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 55% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 89% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 56% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 61% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 92% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 56% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 89% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 47% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 80% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 61% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 78% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 68% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 73% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 79% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 94% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 20% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 25% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 64% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 91% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 77% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 33% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 42% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 39% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 85% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 67% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 109% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 135% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 139% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 117% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 92% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 97% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 66% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 88% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 61% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 109% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 74% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 68% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 42% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 93% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 103% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 67% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 67% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 58% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 61% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 32% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 26% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Analysis Date = 01/17/17 Pct Recovery = 71% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 12/27/16 Pct Recovery = 72% Analysis Date = 12/27/16 Pct Recovery = 72% Analysis Date = 12/16/16 Pct Recovery = 72% Analysis Date = 12/16/16 Pct Recovery = 72% Analysis Date = 12/05/16 Pct Recovery = 72% Analysis Date = 12/05/16 Pct Recovery = 72% Analysis Date = 11/24/16 Pct Recovery = 72% Analysis Date = 11/24/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/03/16 Pct Recovery = 72% Analysis Date = 11/03/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/09/16 Pct Recovery = 72% Analysis Date = 09/09/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/19/16 Pct Recovery = 72% Analysis Date = 08/19/16 Pct Recovery = 72% Analysis Date = 08/08/16 Pct Recovery = 72% Analysis Date = 08/08/16 Pct Recovery = 72% Analysis Date = 07/28/16 Pct Recovery = 72% Analysis Date = 07/28/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/06/16 Pct Recovery = 72% Analysis Date = 07/06/16 Pct Recovery = 72% Analysis Date = 06/25/16 Pct Recovery = 72% Analysis Date = 06/25/16 Pct Recovery = 72% Analysis Date = 06/14/16 Pct Recovery = 72% Analysis Date = 06/14/16 Pct Recovery = 72% Analysis Date = 06/04/16 Pct Recovery = 72% Analysis Date = 06/04/16 Pct Recovery = 72% Analysis Date = 05/24/16 Pct Recovery = 72% Analysis Date = 05/24/16 Pct Recovery = 72% Analysis Date = 05/13/16 Pct Recovery = 72% Analysis Date = 05/13/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 03/30/16 Pct Recovery = 72% Analysis Date = 03/30/16 Pct Recovery = 72% Analysis Date = 03/20/16 Pct Recovery = 72% Analysis Date = 03/20/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 03/09/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/27/16 Pct Recovery = 72% Analysis Date = 02/16/16 Pct Recovery = 72% Analysis Date = 02/16/16 Pct Recovery = 72% Analysis Date = 02/05/16 Pct Recovery = 72% Analysis Date = 02/05/16 Pct Recovery = 72% Analysis Date = 01/25/16 Pct Recovery = 72% Analysis Date = 01/25/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 72% Analysis Date = 01/04/16 Pct Recovery = 72% Analysis Date = 01/04/16 Pct Recovery = 72% Analysis Date = 12/24/15 Pct Recovery = 72% Analysis Date = 12/24/15 Pct Recovery = 72% Analysis Date = 12/13/15 Pct Recovery = 72% Analysis Date = 12/13/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/10/15 Pct Recovery = 72% Analysis Date = 11/10/15 Pct Recovery = 72% Analysis Date = 10/30/15 Pct Recovery = 72% Analysis Date = 10/30/15 Pct Recovery = 72% Analysis Date = 10/20/15 Pct Recovery = 72% Analysis Date = 10/20/15 Pct Recovery = 72% Analysis Date = 10/09/15 Pct Recovery = 72% Analysis Date = 10/09/15 Pct Recovery = 72% Analysis Date = 09/28/15 Pct Recovery = 72% Analysis Date = 09/28/15 Pct Recovery = 72% Analysis Date = 09/17/15 Pct Recovery = 72% Analysis Date = 09/17/15 Pct Recovery = 72% Analysis Date = 09/06/15 Pct Recovery = 72% Analysis Date = 09/06/15 Pct Recovery = 72% Analysis Date = 08/26/15 Pct Recovery = 72% Analysis Date = 08/26/15 Pct Recovery = 72% Analysis Date = 08/15/15 Pct Recovery = 72% Analysis Date = 08/15/15 Pct Recovery = 72% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 08/05/15 Pct Recovery = 73% Analysis Date = 07/25/15 Pct Recovery = 73% Analysis Date = 07/25/15 Pct Recovery = 73% Analysis Date = 07/14/15 Pct Recovery = 73% Analysis Date = 07/14/15 Pct Recovery = 73% Analysis Date = 07/03/15 Pct Recovery = 73% Analysis Date = 07/03/15 Pct Recovery = 73% Analysis Date = 06/22/15 Pct Recovery = 73% Analysis Date = 06/22/15 Pct Recovery = 73% Analysis Date = 06/11/15 Pct Recovery = 73% Analysis Date = 06/11/15 Pct Recovery = 73% Analysis Date = 05/31/15 Pct Recovery = 73% Analysis Date = 05/31/15 Pct Recovery = 73% Analysis Date = 05/21/15 Pct Recovery = 73% Analysis Date = 05/21/15 Pct Recovery = 73% Analysis Date = 05/10/15 Pct Recovery = 73% Analysis Date = 05/10/15 Pct Recovery = 73% Analysis Date = 04/29/15 Pct Recovery = 73% Analysis Date = 04/29/15 Pct Recovery = 73% Analysis Date = 04/18/15 Pct Recovery = 73% Analysis Date = 04/18/15 Pct Recovery = 73% Analysis Date = 04/07/15 Pct Recovery = 73% Analysis Date = 04/07/15 Pct Recovery = 73% Analysis Date = 03/27/15 Pct Recovery = 73% Analysis Date = 03/27/15 Pct Recovery = 73% Analysis Date = 03/16/15 Pct Recovery = 73% Analysis Date = 03/16/15 Pct Recovery = 73% Analysis Date = 03/06/15 Pct Recovery = 73% Analysis Date = 03/06/15 Pct Recovery = 73% Analysis Date = 02/23/15 Pct Recovery = 73% Analysis Date = 02/23/15 Pct Recovery = 73% Analysis Date = 02/12/15 Pct Recovery = 73% Analysis Date = 02/12/15 Pct Recovery = 73% Analysis Date = 02/01/15 Pct Recovery = 74% Analysis Date = 02/01/15 Pct Recovery = 74% Analysis Date = 01/21/15 Pct Recovery = 74% Analysis Date = 01/21/15 Pct Recovery = 74% Analysis Date = 01/10/15 Pct Recovery = 74% Analysis Date = 01/10/15 Pct Recovery = 74% Analysis Date = 12/31/14 Pct Recovery = 75% Analysis Date = 12/31/14 Pct Recovery = 75% Analysis Date = 12/20/14 Pct Recovery = 75% Analysis Date = 12/20/14 Pct Recovery = 75% Analysis Date = 12/09/14 Pct Recovery = 75% Analysis Date = 12/09/14 Pct Recovery = 75% Analysis Date = 11/28/14 Pct Recovery = 75% Analysis Date = 11/28/14 Pct Recovery = 75% Analysis Date = 11/17/14 Pct Recovery = 76% Analysis Date = 11/17/14 Pct Recovery = 76% Analysis Date = 11/06/14 Pct Recovery = 76% Analysis Date = 11/06/14 Pct Recovery = 76% Analysis Date = 10/26/14 Pct Recovery = 76% Analysis Date = 10/26/14 Pct Recovery = 76% Analysis Date = 10/16/14 Pct Recovery = 77% Analysis Date = 10/16/14 Pct Recovery = 77% Analysis Date = 10/05/14 Pct Recovery = 77% Analysis Date = 10/05/14 Pct Recovery = 77% Analysis Date = 09/24/14 Pct Recovery = 77% Analysis Date = 09/24/14 Pct Recovery = 77% Analysis Date = 09/13/14 Pct Recovery = 78% Analysis Date = 09/13/14 Pct Recovery = 78% Analysis Date = 09/02/14 Pct Recovery = 78% Analysis Date = 09/02/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 78% Analysis Date = 08/22/14 Pct Recovery = 78% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/10/14 Pct Recovery = 80% Analysis Date = 07/10/14 Pct Recovery = 80% Analysis Date = 06/29/14 Pct Recovery = 80% Analysis Date = 06/29/14 Pct Recovery = 80% Analysis Date = 06/18/14 Pct Recovery = 80% Analysis Date = 06/18/14 Pct Recovery = 80% Analysis Date = 06/07/14 Pct Recovery = 80% Analysis Date = 06/07/14 Pct Recovery = 80% Analysis Date = 05/27/14 Pct Recovery = 81% Analysis Date = 05/27/14 Pct Recovery = 81% Analysis Date = 05/17/14 Pct Recovery = 81% Analysis Date = 05/17/14 Pct Recovery = 81% Analysis Date = 05/06/14 Pct Recovery = 81% Analysis Date = 05/06/14 Pct Recovery = 81% Analysis Date = 04/25/14 Pct Recovery = 81% Analysis Date = 04/25/14 Pct Recovery = 81% Analysis Date = 04/14/14 Pct Recovery = 81% Analysis Date = 04/14/14 Pct Recovery = 81% Analysis Date = 04/03/14 Pct Recovery = 81% Analysis Date = 04/03/14 Pct Recovery = 81% Analysis Date = 03/23/14 Pct Recovery = 81% Analysis Date = 03/23/14 Pct Recovery = 81% Analysis Date = 03/12/14 Pct Recovery = 81% Analysis Date = 03/12/14 Pct Recovery = 81% Analysis Date = 03/02/14 Pct Recovery = 81% Analysis Date = 03/02/14 Pct Recovery = 81% Analysis Date = 02/19/14 Pct Recovery = 81% Analysis Date = 02/19/14 Pct Recovery = 81% Analysis Date = 02/08/14 Pct Recovery = 81% Analysis Date = 02/08/14 Pct Recovery = 81% Analysis Date = 01/28/14 Pct Recovery = 81% Analysis Date = 01/28/14 Pct Recovery = 81% Analysis Date = 01/17/14 Pct Recovery = 81% Analysis Date = 01/17/14 Pct Recovery = 81% Analysis Date = 01/06/14 Pct Recovery = 81% Analysis Date = 01/06/14 Pct Recovery = 81% Analysis Date = 12/26/13 Pct Recovery = 80% Analysis Date = 12/26/13 Pct Recovery = 80% Analysis Date = 12/16/13 Pct Recovery = 79% Analysis Date = 12/16/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 11/24/13 Pct Recovery = 78% Analysis Date = 11/24/13 Pct Recovery = 78% Analysis Date = 11/13/13 Pct Recovery = 78% Analysis Date = 11/13/13 Pct Recovery = 78% Analysis Date = 11/02/13 Pct Recovery = 77% Analysis Date = 11/02/13 Pct Recovery = 77% Analysis Date = 10/22/13 Pct Recovery = 77% Analysis Date = 10/22/13 Pct Recovery = 77% Analysis Date = 10/11/13 Pct Recovery = 76% Analysis Date = 10/11/13 Pct Recovery = 76% Analysis Date = 10/01/13 Pct Recovery = 76% Analysis Date = 10/01/13 Pct Recovery = 76% Analysis Date = 09/20/13 Pct Recovery = 75% Analysis Date = 09/20/13 Pct Recovery = 75% Analysis Date = 09/09/13 Pct Recovery = 74% Analysis Date = 09/09/13 Pct Recovery = 74% Analysis Date = 08/29/13 Pct Recovery = 74% Analysis Date = 08/29/13 Pct Recovery = 74% Analysis Date = 08/18/13 Pct Recovery = 73% Analysis Date = 08/18/13 Pct Recovery = 73% Analysis Date = 08/07/13 Pct Recovery = 73% Analysis Date = 08/07/13 Pct Recovery = 73% Analysis Date = 07/27/13 Pct Recovery = 72% Analysis Date = 07/27/13 Pct Recovery = 72% Analysis Date = 07/17/13 Pct Recovery = 72% Analysis Date = 07/17/13 Pct Recovery = 72% Analysis Date = 07/06/13 Pct Recovery = 71% Analysis Date = 07/06/13 Pct Recovery = 71% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/14/13 Pct Recovery = 70% Analysis Date = 06/14/13 Pct Recovery = 70% Analysis Date = 06/03/13 Pct Recovery = 70% Analysis Date = 06/03/13 Pct Recovery = 70% Analysis Date = 05/23/13 Pct Recovery = 69% Analysis Date = 05/23/13 Pct Recovery = 69% Analysis Date = 05/12/13 Pct Recovery = 69% Analysis Date = 05/12/13 Pct Recovery = 69% Analysis Date = 05/02/13 Pct Recovery = 68% Analysis Date = 05/02/13 Pct Recovery = 68% Analysis Date = 04/21/13 Pct Recovery = 68% Analysis Date = 04/21/13 Pct Recovery = 68% Analysis Date = 04/10/13 Pct Recovery = 67% Analysis Date = 04/10/13 Pct Recovery = 67% Analysis Date = 03/30/13 Pct Recovery = 67% Analysis Date = 03/30/13 Pct Recovery = 67% Analysis Date = 03/19/13 Pct Recovery = 66% Analysis Date = 03/19/13 Pct Recovery = 66% Analysis Date = 03/08/13 Pct Recovery = 66% Analysis Date = 03/08/13 Pct Recovery = 66% Analysis Date = 02/25/13 Pct Recovery = 65% Analysis Date = 02/25/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 65% Analysis Date = 02/04/13 Pct Recovery = 64% Analysis Date = 02/04/13 Pct Recovery = 64% Analysis Date = 01/24/13 Pct Recovery = 63% Analysis Date = 01/24/13 Pct Recovery = 63% Analysis Date = 01/13/13 Pct Recovery = 63% Analysis Date = 01/13/13 Pct Recovery = 63% Analysis Date = 01/02/13 Pct Recovery = 62% Analysis Date = 01/02/13 Pct Recovery = 62% Analysis Date = 12/22/12 Pct Recovery = 62% Analysis Date = 12/22/12 Pct Recovery = 62% Analysis Date = 12/12/12 Pct Recovery = 61% Analysis Date = 12/12/12 Pct Recovery = 61% Analysis Date = 12/01/12 Pct Recovery = 61% Analysis Date = 12/01/12 Pct Recovery = 61% Analysis Date = 11/20/12 Pct Recovery = 60% Analysis Date = 11/20/12 Pct Recovery = 60% Analysis Date = 11/09/12 Pct Recovery = 60% Analysis Date = 11/09/12 Pct Recovery = 60% Analysis Date = 10/29/12 Pct Recovery = 59% Analysis Date = 10/29/12 Pct Recovery = 59% Analysis Date = 10/18/12 Pct Recovery = 59% Analysis Date = 10/18/12 Pct Recovery = 59% Analysis Date = 10/07/12 Pct Recovery = 59% Analysis Date = 10/07/12 Pct Recovery = 59% Analysis Date = 09/27/12 Pct Recovery = 59% Analysis Date = 09/27/12 Pct Recovery = 59% Analysis Date = 09/16/12 Pct Recovery = 59% Analysis Date = 09/16/12 Pct Recovery = 59% Analysis Date = 09/05/12 Pct Recovery = 59% Analysis Date = 09/05/12 Pct Recovery = 59% Analysis Date = 08/25/12 Pct Recovery = 59% Analysis Date = 08/25/12 Pct Recovery = 59% Analysis Date = 08/14/12 Pct Recovery = 59% Analysis Date = 08/14/12 Pct Recovery = 59% Analysis Date = 08/03/12 Pct Recovery = 59% Analysis Date = 08/03/12 Pct Recovery = 59% Analysis Date = 07/23/12 Pct Recovery = 59% Analysis Date = 07/23/12 Pct Recovery = 59% Analysis Date = 07/13/12 Pct Recovery = 59% Analysis Date = 07/13/12 Pct Recovery = 59% Analysis Date = 07/02/12 Pct Recovery = 59% Analysis Date = 07/02/12 Pct Recovery = 59% Analysis Date = 06/21/12 Pct Recovery = 59% Analysis Date = 06/21/12 Pct Recovery = 59% Analysis Date = 06/10/12 Pct Recovery = 59% Analysis Date = 06/10/12 Pct Recovery = 59% Analysis Date = 05/30/12 Pct Recovery = 59% Analysis Date = 05/30/12 Pct Recovery = 59% Analysis Date = 05/19/12 Pct Recovery = 59% Analysis Date = 05/19/12 Pct Recovery = 59% Analysis Date = 05/08/12 Pct Recovery = 59% Analysis Date = 05/08/12 Pct Recovery = 59% Analysis Date = 04/28/12 Pct Recovery = 59% Analysis Date = 04/28/12 Pct Recovery = 59% Analysis Date = 04/17/12 Pct Recovery = 59% Analysis Date = 04/17/12 Pct Recovery = 59% Analysis Date = 04/06/12 Pct Recovery = 59% Analysis Date = 04/06/12 Pct Recovery = 59% Analysis Date = 03/26/12 Pct Recovery = 59% Analysis Date = 03/26/12 Pct Recovery = 59% Analysis Date = 03/15/12 Pct Recovery = 59% Analysis Date = 03/15/12 Pct Recovery = 59% Analysis Date = 03/04/12 Pct Recovery = 59% Analysis Date = 03/04/12 Pct Recovery = 59% Analysis Date = 02/22/12 Pct Recovery = 59% Analysis Date = 02/22/12 Pct Recovery = 59% Analysis Date = 02/12/12 Pct Recovery = 59% Analysis Date = 02/12/12 Pct Recovery = 59% Analysis Date = 02/01/12 Pct Recovery = 59% Analysis Date = 02/01/12 Pct Recovery = 59% Analysis Date = 01/21/12 Pct Recovery = 59% Analysis Date = 01/21/12 Pct Recovery = 59% Analysis Date = 01/10/12 Pct Recovery = 59% Analysis Date = 01/10/12 Pct Recovery = 59% Analysis Date = 12/30/11 Pct Recovery = 59% Analysis Date = 12/30/11 Pct Recovery = 59% Analysis Date = 12/19/11 Pct Recovery = 59% Analysis Date = 12/19/11 Pct Recovery = 59% Analysis Date = 12/08/11 Pct Recovery = 59% Analysis Date = 12/08/11 Pct Recovery = 59% Analysis Date = 11/28/11 Pct Recovery = 59% Analysis Date = 11/28/11 Pct Recovery = 59% Analysis Date = 11/17/11 Pct Recovery = 59% Analysis Date = 11/17/11 Pct Recovery = 59% Analysis Date = 11/06/11 Pct Recovery = 59% Analysis Date = 11/06/11 Pct Recovery = 59% Analysis Date = 10/26/11 Pct Recovery = 59% Analysis Date = 10/26/11 Pct Recovery = 59% Analysis Date = 10/15/11 Pct Recovery = 59% Analysis Date = 10/15/11 Pct Recovery = 59% Analysis Date = 10/04/11 Pct Recovery = 59% Analysis Date = 10/04/11 Pct Recovery = 59% Analysis Date = 09/23/11 Pct Recovery = 59% Analysis Date = 09/23/11 Pct Recovery = 59% Analysis Date = 09/13/11 Pct Recovery = 59% Analysis Date = 09/13/11 Pct Recovery = 59% Analysis Date = 09/02/11 Pct Recovery = 59% Analysis Date = 09/02/11 Pct Recovery = 59% Analysis Date = 08/22/11 Pct Recovery = 59% Analysis Date = 08/22/11 Pct Recovery = 59% Analysis Date = 08/11/11 Pct Recovery = 59% Analysis Date = 08/11/11 Pct Recovery = 59% Analysis Date = 07/31/11 Pct Recovery = 59% Analysis Date = 07/31/11 Pct Recovery = 59% Analysis Date = 07/20/11 Pct Recovery = 59% Analysis Date = 07/20/11 Pct Recovery = 59% Analysis Date = 07/09/11 Pct Recovery = 59% Analysis Date = 07/09/11 Pct Recovery = 59% Analysis Date = 06/29/11 Pct Recovery = 59% Analysis Date = 06/29/11 Pct Recovery = 59% Analysis Date = 06/18/11 Pct Recovery = 59% Analysis Date = 06/18/11 Pct Recovery = 59% Analysis Date = 06/07/11 Pct Recovery = 59% Analysis Date = 06/07/11 Pct Recovery = 59% Analysis Date = 05/27/11 Pct Recovery = 60% Analysis Date = 05/27/11 Pct Recovery = 60% Analysis Date = 05/16/11 Pct Recovery = 60% Analysis Date = 05/16/11 Pct Recovery = 60% Analysis Date = 05/05/11 Pct Recovery = 60% Analysis Date = 05/05/11 Pct Recovery = 60% Analysis Date = 04/24/11 Pct Recovery = 60% Analysis Date = 04/24/11 Pct Recovery = 60% Analysis Date = 04/14/11 Pct Recovery = 60% Analysis Date = 04/14/11 Pct Recovery = 60% Analysis Date = 04/03/11 Pct Recovery = 60% Analysis Date = 04/03/11 Pct Recovery = 60% Analysis Date = 03/23/11 Pct Recovery = 60% Analysis Date = 03/23/11 Pct Recovery = 60% Analysis Date = 03/12/11 Pct Recovery = 60% Analysis Date = 03/12/11 Pct Recovery = 60% Analysis Date = 03/01/11 Pct Recovery = 60% Analysis Date = 03/01/11 Pct Recovery = 60% Analysis Date = 02/18/11 Pct Recovery = 60% Analysis Date = 02/18/11 Pct Recovery = 60% Analysis Date = 02/08/11 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYFLUTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 70% 26% 68% 22%
Total 67 70% 26% 68% 22%

Sample Statistics
CYFLUTHRIN

Characteristic N % % Basis
Plotted 67 89% Spiked
Estimated Values 67 89% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 75 .  
False Negatives 8 11% 8 out of 75
Not Spiked 83 .  
False Positives 1 1% 1 out of 83

BQS OBSP Determination:
CYHALOTHRIN
METHOD: 2033 , TESTIDCODE: 61595GCM39
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 37% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 51% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 80% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 40% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 47% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 51% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 53% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 48% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 26% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 9% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 53% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 40% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 25% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 71% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 54% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 55% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 53% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 65% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 58% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 65% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 53% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 62% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 67% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 64% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 40% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 55% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 64% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 48% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 35% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 73% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 56% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 104% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 71% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 66% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 64% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 44% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 75% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 21% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 22% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 57% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 83% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 89% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 50% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 54% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 38% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 48% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 87% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 57% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 57% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 51% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 60% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 55% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 90% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 70% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 29% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 61% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 57% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 58% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 49% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 88% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 51% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 51% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 64% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 57% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 24% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 68% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 75% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 61% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 88% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 58% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 13% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 46% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 43% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 95% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 9% Analysis Date = 12/19/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 11/28/16 Pct Recovery = 70% Analysis Date = 11/28/16 Pct Recovery = 70% Analysis Date = 11/17/16 Pct Recovery = 70% Analysis Date = 11/17/16 Pct Recovery = 70% Analysis Date = 11/07/16 Pct Recovery = 69% Analysis Date = 11/07/16 Pct Recovery = 69% Analysis Date = 10/27/16 Pct Recovery = 69% Analysis Date = 10/27/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 09/25/16 Pct Recovery = 69% Analysis Date = 09/25/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/03/16 Pct Recovery = 69% Analysis Date = 09/03/16 Pct Recovery = 69% Analysis Date = 08/24/16 Pct Recovery = 69% Analysis Date = 08/24/16 Pct Recovery = 69% Analysis Date = 08/13/16 Pct Recovery = 69% Analysis Date = 08/13/16 Pct Recovery = 69% Analysis Date = 08/02/16 Pct Recovery = 69% Analysis Date = 08/02/16 Pct Recovery = 69% Analysis Date = 07/23/16 Pct Recovery = 69% Analysis Date = 07/23/16 Pct Recovery = 69% Analysis Date = 07/12/16 Pct Recovery = 68% Analysis Date = 07/12/16 Pct Recovery = 68% Analysis Date = 07/01/16 Pct Recovery = 68% Analysis Date = 07/01/16 Pct Recovery = 68% Analysis Date = 06/20/16 Pct Recovery = 68% Analysis Date = 06/20/16 Pct Recovery = 68% Analysis Date = 06/10/16 Pct Recovery = 68% Analysis Date = 06/10/16 Pct Recovery = 68% Analysis Date = 05/30/16 Pct Recovery = 68% Analysis Date = 05/30/16 Pct Recovery = 68% Analysis Date = 05/19/16 Pct Recovery = 68% Analysis Date = 05/19/16 Pct Recovery = 68% Analysis Date = 05/09/16 Pct Recovery = 68% Analysis Date = 05/09/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/17/16 Pct Recovery = 68% Analysis Date = 04/17/16 Pct Recovery = 68% Analysis Date = 04/06/16 Pct Recovery = 68% Analysis Date = 04/06/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/16/16 Pct Recovery = 67% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 02/24/16 Pct Recovery = 67% Analysis Date = 02/24/16 Pct Recovery = 67% Analysis Date = 02/13/16 Pct Recovery = 67% Analysis Date = 02/13/16 Pct Recovery = 67% Analysis Date = 02/02/16 Pct Recovery = 67% Analysis Date = 02/02/16 Pct Recovery = 67% Analysis Date = 01/22/16 Pct Recovery = 67% Analysis Date = 01/22/16 Pct Recovery = 67% Analysis Date = 01/12/16 Pct Recovery = 67% Analysis Date = 01/12/16 Pct Recovery = 67% Analysis Date = 01/01/16 Pct Recovery = 67% Analysis Date = 01/01/16 Pct Recovery = 67% Analysis Date = 12/21/15 Pct Recovery = 67% Analysis Date = 12/21/15 Pct Recovery = 67% Analysis Date = 12/11/15 Pct Recovery = 67% Analysis Date = 12/11/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 66% Analysis Date = 11/30/15 Pct Recovery = 66% Analysis Date = 11/19/15 Pct Recovery = 66% Analysis Date = 11/19/15 Pct Recovery = 66% Analysis Date = 11/09/15 Pct Recovery = 66% Analysis Date = 11/09/15 Pct Recovery = 66% Analysis Date = 10/29/15 Pct Recovery = 66% Analysis Date = 10/29/15 Pct Recovery = 66% Analysis Date = 10/18/15 Pct Recovery = 66% Analysis Date = 10/18/15 Pct Recovery = 66% Analysis Date = 10/07/15 Pct Recovery = 66% Analysis Date = 10/07/15 Pct Recovery = 66% Analysis Date = 09/27/15 Pct Recovery = 66% Analysis Date = 09/27/15 Pct Recovery = 66% Analysis Date = 09/16/15 Pct Recovery = 66% Analysis Date = 09/16/15 Pct Recovery = 66% Analysis Date = 09/05/15 Pct Recovery = 65% Analysis Date = 09/05/15 Pct Recovery = 65% Analysis Date = 08/26/15 Pct Recovery = 65% Analysis Date = 08/26/15 Pct Recovery = 65% Analysis Date = 08/15/15 Pct Recovery = 65% Analysis Date = 08/15/15 Pct Recovery = 65% Analysis Date = 08/04/15 Pct Recovery = 65% Analysis Date = 08/04/15 Pct Recovery = 65% Analysis Date = 07/24/15 Pct Recovery = 65% Analysis Date = 07/24/15 Pct Recovery = 65% Analysis Date = 07/14/15 Pct Recovery = 65% Analysis Date = 07/14/15 Pct Recovery = 65% Analysis Date = 07/03/15 Pct Recovery = 65% Analysis Date = 07/03/15 Pct Recovery = 65% Analysis Date = 06/22/15 Pct Recovery = 65% Analysis Date = 06/22/15 Pct Recovery = 65% Analysis Date = 06/12/15 Pct Recovery = 64% Analysis Date = 06/12/15 Pct Recovery = 64% Analysis Date = 06/01/15 Pct Recovery = 64% Analysis Date = 06/01/15 Pct Recovery = 64% Analysis Date = 05/21/15 Pct Recovery = 64% Analysis Date = 05/21/15 Pct Recovery = 64% Analysis Date = 05/10/15 Pct Recovery = 64% Analysis Date = 05/10/15 Pct Recovery = 64% Analysis Date = 04/30/15 Pct Recovery = 64% Analysis Date = 04/30/15 Pct Recovery = 64% Analysis Date = 04/19/15 Pct Recovery = 64% Analysis Date = 04/19/15 Pct Recovery = 64% Analysis Date = 04/08/15 Pct Recovery = 64% Analysis Date = 04/08/15 Pct Recovery = 64% Analysis Date = 03/29/15 Pct Recovery = 64% Analysis Date = 03/29/15 Pct Recovery = 64% Analysis Date = 03/18/15 Pct Recovery = 63% Analysis Date = 03/18/15 Pct Recovery = 63% Analysis Date = 03/07/15 Pct Recovery = 63% Analysis Date = 03/07/15 Pct Recovery = 63% Analysis Date = 02/24/15 Pct Recovery = 63% Analysis Date = 02/24/15 Pct Recovery = 63% Analysis Date = 02/14/15 Pct Recovery = 63% Analysis Date = 02/14/15 Pct Recovery = 63% Analysis Date = 02/03/15 Pct Recovery = 63% Analysis Date = 02/03/15 Pct Recovery = 63% Analysis Date = 01/23/15 Pct Recovery = 63% Analysis Date = 01/23/15 Pct Recovery = 63% Analysis Date = 01/13/15 Pct Recovery = 63% Analysis Date = 01/13/15 Pct Recovery = 63% Analysis Date = 01/02/15 Pct Recovery = 63% Analysis Date = 01/02/15 Pct Recovery = 63% Analysis Date = 12/22/14 Pct Recovery = 62% Analysis Date = 12/22/14 Pct Recovery = 62% Analysis Date = 12/12/14 Pct Recovery = 62% Analysis Date = 12/12/14 Pct Recovery = 62% Analysis Date = 12/01/14 Pct Recovery = 62% Analysis Date = 12/01/14 Pct Recovery = 62% Analysis Date = 11/20/14 Pct Recovery = 62% Analysis Date = 11/20/14 Pct Recovery = 62% Analysis Date = 11/09/14 Pct Recovery = 62% Analysis Date = 11/09/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/19/14 Pct Recovery = 62% Analysis Date = 10/19/14 Pct Recovery = 62% Analysis Date = 10/08/14 Pct Recovery = 62% Analysis Date = 10/08/14 Pct Recovery = 62% Analysis Date = 09/28/14 Pct Recovery = 62% Analysis Date = 09/28/14 Pct Recovery = 62% Analysis Date = 09/17/14 Pct Recovery = 62% Analysis Date = 09/17/14 Pct Recovery = 62% Analysis Date = 09/06/14 Pct Recovery = 61% Analysis Date = 09/06/14 Pct Recovery = 61% Analysis Date = 08/26/14 Pct Recovery = 61% Analysis Date = 08/26/14 Pct Recovery = 61% Analysis Date = 08/16/14 Pct Recovery = 61% Analysis Date = 08/16/14 Pct Recovery = 61% Analysis Date = 08/05/14 Pct Recovery = 61% Analysis Date = 08/05/14 Pct Recovery = 61% Analysis Date = 07/25/14 Pct Recovery = 61% Analysis Date = 07/25/14 Pct Recovery = 61% Analysis Date = 07/15/14 Pct Recovery = 61% Analysis Date = 07/15/14 Pct Recovery = 61% Analysis Date = 07/04/14 Pct Recovery = 60% Analysis Date = 07/04/14 Pct Recovery = 60% Analysis Date = 06/23/14 Pct Recovery = 60% Analysis Date = 06/23/14 Pct Recovery = 60% Analysis Date = 06/12/14 Pct Recovery = 60% Analysis Date = 06/12/14 Pct Recovery = 60% Analysis Date = 06/02/14 Pct Recovery = 60% Analysis Date = 06/02/14 Pct Recovery = 60% Analysis Date = 05/22/14 Pct Recovery = 60% Analysis Date = 05/22/14 Pct Recovery = 60% Analysis Date = 05/11/14 Pct Recovery = 59% Analysis Date = 05/11/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 04/20/14 Pct Recovery = 59% Analysis Date = 04/20/14 Pct Recovery = 59% Analysis Date = 04/09/14 Pct Recovery = 59% Analysis Date = 04/09/14 Pct Recovery = 59% Analysis Date = 03/29/14 Pct Recovery = 59% Analysis Date = 03/29/14 Pct Recovery = 59% Analysis Date = 03/19/14 Pct Recovery = 58% Analysis Date = 03/19/14 Pct Recovery = 58% Analysis Date = 03/08/14 Pct Recovery = 58% Analysis Date = 03/08/14 Pct Recovery = 58% Analysis Date = 02/25/14 Pct Recovery = 58% Analysis Date = 02/25/14 Pct Recovery = 58% Analysis Date = 02/15/14 Pct Recovery = 58% Analysis Date = 02/15/14 Pct Recovery = 58% Analysis Date = 02/04/14 Pct Recovery = 58% Analysis Date = 02/04/14 Pct Recovery = 58% Analysis Date = 01/24/14 Pct Recovery = 57% Analysis Date = 01/24/14 Pct Recovery = 57% Analysis Date = 01/13/14 Pct Recovery = 57% Analysis Date = 01/13/14 Pct Recovery = 57% Analysis Date = 01/03/14 Pct Recovery = 57% Analysis Date = 01/03/14 Pct Recovery = 57% Analysis Date = 12/23/13 Pct Recovery = 57% Analysis Date = 12/23/13 Pct Recovery = 57% Analysis Date = 12/12/13 Pct Recovery = 57% Analysis Date = 12/12/13 Pct Recovery = 57% Analysis Date = 12/02/13 Pct Recovery = 57% Analysis Date = 12/02/13 Pct Recovery = 57% Analysis Date = 11/21/13 Pct Recovery = 57% Analysis Date = 11/21/13 Pct Recovery = 57% Analysis Date = 11/10/13 Pct Recovery = 57% Analysis Date = 11/10/13 Pct Recovery = 57% Analysis Date = 10/31/13 Pct Recovery = 57% Analysis Date = 10/31/13 Pct Recovery = 57% Analysis Date = 10/20/13 Pct Recovery = 57% Analysis Date = 10/20/13 Pct Recovery = 57% Analysis Date = 10/09/13 Pct Recovery = 57% Analysis Date = 10/09/13 Pct Recovery = 57% Analysis Date = 09/28/13 Pct Recovery = 57% Analysis Date = 09/28/13 Pct Recovery = 57% Analysis Date = 09/18/13 Pct Recovery = 57% Analysis Date = 09/18/13 Pct Recovery = 57% Analysis Date = 09/07/13 Pct Recovery = 57% Analysis Date = 09/07/13 Pct Recovery = 57% Analysis Date = 08/27/13 Pct Recovery = 57% Analysis Date = 08/27/13 Pct Recovery = 57% Analysis Date = 08/17/13 Pct Recovery = 57% Analysis Date = 08/17/13 Pct Recovery = 57% Analysis Date = 08/06/13 Pct Recovery = 57% Analysis Date = 08/06/13 Pct Recovery = 57% Analysis Date = 07/26/13 Pct Recovery = 57% Analysis Date = 07/26/13 Pct Recovery = 57% Analysis Date = 07/15/13 Pct Recovery = 57% Analysis Date = 07/15/13 Pct Recovery = 57% Analysis Date = 07/05/13 Pct Recovery = 57% Analysis Date = 07/05/13 Pct Recovery = 57% Analysis Date = 06/24/13 Pct Recovery = 57% Analysis Date = 06/24/13 Pct Recovery = 57% Analysis Date = 06/13/13 Pct Recovery = 56% Analysis Date = 06/13/13 Pct Recovery = 56% Analysis Date = 06/03/13 Pct Recovery = 56% Analysis Date = 06/03/13 Pct Recovery = 56% Analysis Date = 05/23/13 Pct Recovery = 56% Analysis Date = 05/23/13 Pct Recovery = 56% Analysis Date = 05/12/13 Pct Recovery = 56% Analysis Date = 05/12/13 Pct Recovery = 56% Analysis Date = 05/01/13 Pct Recovery = 56% Analysis Date = 05/01/13 Pct Recovery = 56% Analysis Date = 04/21/13 Pct Recovery = 56% Analysis Date = 04/21/13 Pct Recovery = 56% Analysis Date = 04/10/13 Pct Recovery = 56% Analysis Date = 04/10/13 Pct Recovery = 56% Analysis Date = 03/30/13 Pct Recovery = 56% Analysis Date = 03/30/13 Pct Recovery = 56% Analysis Date = 03/20/13 Pct Recovery = 56% Analysis Date = 03/20/13 Pct Recovery = 56% Analysis Date = 03/09/13 Pct Recovery = 56% Analysis Date = 03/09/13 Pct Recovery = 56% Analysis Date = 02/26/13 Pct Recovery = 56% Analysis Date = 02/26/13 Pct Recovery = 56% Analysis Date = 02/15/13 Pct Recovery = 56% Analysis Date = 02/15/13 Pct Recovery = 56% Analysis Date = 02/05/13 Pct Recovery = 56% Analysis Date = 02/05/13 Pct Recovery = 56% Analysis Date = 01/25/13 Pct Recovery = 55% Analysis Date = 01/25/13 Pct Recovery = 55% Analysis Date = 01/14/13 Pct Recovery = 55% Analysis Date = 01/14/13 Pct Recovery = 55% Analysis Date = 01/04/13 Pct Recovery = 55% Analysis Date = 01/04/13 Pct Recovery = 55% Analysis Date = 12/24/12 Pct Recovery = 55% Analysis Date = 12/24/12 Pct Recovery = 55% Analysis Date = 12/13/12 Pct Recovery = 55% Analysis Date = 12/13/12 Pct Recovery = 55% Analysis Date = 12/03/12 Pct Recovery = 55% Analysis Date = 12/03/12 Pct Recovery = 55% Analysis Date = 11/22/12 Pct Recovery = 55% Analysis Date = 11/22/12 Pct Recovery = 55% Analysis Date = 11/11/12 Pct Recovery = 54% Analysis Date = 11/11/12 Pct Recovery = 54% Analysis Date = 10/31/12 Pct Recovery = 54% Analysis Date = 10/31/12 Pct Recovery = 54% Analysis Date = 10/21/12 Pct Recovery = 54% Analysis Date = 10/21/12 Pct Recovery = 54% Analysis Date = 10/10/12 Pct Recovery = 54% Analysis Date = 10/10/12 Pct Recovery = 54% Analysis Date = 09/29/12 Pct Recovery = 54% Analysis Date = 09/29/12 Pct Recovery = 54% Analysis Date = 09/19/12 Pct Recovery = 54% Analysis Date = 09/19/12 Pct Recovery = 54% Analysis Date = 09/08/12 Pct Recovery = 53% Analysis Date = 09/08/12 Pct Recovery = 53% Analysis Date = 08/28/12 Pct Recovery = 53% Analysis Date = 08/28/12 Pct Recovery = 53% Analysis Date = 08/17/12 Pct Recovery = 53% Analysis Date = 08/17/12 Pct Recovery = 53% Analysis Date = 08/07/12 Pct Recovery = 53% Analysis Date = 08/07/12 Pct Recovery = 53% Analysis Date = 07/27/12 Pct Recovery = 53% Analysis Date = 07/27/12 Pct Recovery = 53% Analysis Date = 07/16/12 Pct Recovery = 53% Analysis Date = 07/16/12 Pct Recovery = 53% Analysis Date = 07/06/12 Pct Recovery = 53% Analysis Date = 07/06/12 Pct Recovery = 53% Analysis Date = 06/25/12 Pct Recovery = 52% Analysis Date = 06/25/12 Pct Recovery = 52% Analysis Date = 06/14/12 Pct Recovery = 52% Analysis Date = 06/14/12 Pct Recovery = 52% Analysis Date = 06/03/12 Pct Recovery = 52% Analysis Date = 06/03/12 Pct Recovery = 52% Analysis Date = 05/24/12 Pct Recovery = 52% Analysis Date = 05/24/12 Pct Recovery = 52% Analysis Date = 05/13/12 Pct Recovery = 52% Analysis Date = 05/13/12 Pct Recovery = 52% Analysis Date = 05/02/12 Pct Recovery = 51% Analysis Date = 05/02/12 Pct Recovery = 51% Analysis Date = 04/22/12 Pct Recovery = 51% Analysis Date = 04/22/12 Pct Recovery = 51% Analysis Date = 04/11/12 Pct Recovery = 51% Analysis Date = 04/11/12 Pct Recovery = 51% Analysis Date = 03/31/12 Pct Recovery = 51% Analysis Date = 03/31/12 Pct Recovery = 51% Analysis Date = 03/20/12 Pct Recovery = 51% Analysis Date = 03/20/12 Pct Recovery = 51% Analysis Date = 03/10/12 Pct Recovery = 51% Analysis Date = 03/10/12 Pct Recovery = 51% Analysis Date = 02/28/12 Pct Recovery = 50% Analysis Date = 02/28/12 Pct Recovery = 50% Analysis Date = 02/17/12 Pct Recovery = 50% Analysis Date = 02/17/12 Pct Recovery = 50% Analysis Date = 02/07/12 Pct Recovery = 50% Analysis Date = 02/07/12 Pct Recovery = 50% Analysis Date = 01/27/12 Pct Recovery = 50% Analysis Date = 01/27/12 Pct Recovery = 50% Analysis Date = 01/16/12 Pct Recovery = 50% Analysis Date = 01/16/12 Pct Recovery = 50% Analysis Date = 01/06/12 Pct Recovery = 49% Analysis Date = 01/06/12 Pct Recovery = 49% Analysis Date = 12/26/11 Pct Recovery = 49% Analysis Date = 12/26/11 Pct Recovery = 49% Analysis Date = 12/15/11 Pct Recovery = 49% Analysis Date = 12/15/11 Pct Recovery = 49% Analysis Date = 12/04/11 Pct Recovery = 49% Analysis Date = 12/04/11 Pct Recovery = 49% Analysis Date = 11/24/11 Pct Recovery = 49% Analysis Date = 11/24/11 Pct Recovery = 49% Analysis Date = 11/13/11 Pct Recovery = 48% Analysis Date = 11/13/11 Pct Recovery = 48% Analysis Date = 11/02/11 Pct Recovery = 48% Analysis Date = 11/02/11 Pct Recovery = 48% Analysis Date = 10/23/11 Pct Recovery = 48% Analysis Date = 10/23/11 Pct Recovery = 48% Analysis Date = 10/12/11 Pct Recovery = 48% Analysis Date = 10/12/11 Pct Recovery = 48% Analysis Date = 10/01/11 Pct Recovery = 48% Analysis Date = 10/01/11 Pct Recovery = 48% Analysis Date = 09/20/11 Pct Recovery = 47% Analysis Date = 09/20/11 Pct Recovery = 47% Analysis Date = 09/10/11 Pct Recovery = 47% Analysis Date = 09/10/11 Pct Recovery = 47% Analysis Date = 08/30/11 Pct Recovery = 47% Analysis Date = 08/30/11 Pct Recovery = 47% Analysis Date = 08/19/11 Pct Recovery = 47% Analysis Date = 08/19/11 Pct Recovery = 47% Analysis Date = 08/09/11 Pct Recovery = 47% Analysis Date = 08/09/11 Pct Recovery = 47% Analysis Date = 07/29/11 Pct Recovery = 46% Analysis Date = 07/29/11 Pct Recovery = 46% Analysis Date = 07/18/11 Pct Recovery = 46% Analysis Date = 07/18/11 Pct Recovery = 46% Analysis Date = 07/07/11 Pct Recovery = 46% Analysis Date = 07/07/11 Pct Recovery = 46% Analysis Date = 06/27/11 Pct Recovery = 46% Analysis Date = 06/27/11 Pct Recovery = 46% Analysis Date = 06/16/11 Pct Recovery = 46% Analysis Date = 06/16/11 Pct Recovery = 46% Analysis Date = 06/05/11 Pct Recovery = 45% Analysis Date = 06/05/11 Pct Recovery = 45% Analysis Date = 05/26/11 Pct Recovery = 45% Analysis Date = 05/26/11 Pct Recovery = 45% Analysis Date = 05/15/11 Pct Recovery = 45% Analysis Date = 05/15/11 Pct Recovery = 45% Analysis Date = 05/04/11 Pct Recovery = 45% Analysis Date = 05/04/11 Pct Recovery = 45% Analysis Date = 04/23/11 Pct Recovery = 45% Analysis Date = 04/23/11 Pct Recovery = 45% Analysis Date = 04/13/11 Pct Recovery = 45% Analysis Date = 04/13/11 Pct Recovery = 45% Analysis Date = 04/02/11 Pct Recovery = 44% Analysis Date = 04/02/11 Pct Recovery = 44% Analysis Date = 03/22/11 Pct Recovery = 44% Analysis Date = 03/22/11 Pct Recovery = 44% Analysis Date = 03/12/11 Pct Recovery = 44% Analysis Date = 03/12/11 Pct Recovery = 44% Analysis Date = 03/01/11 Pct Recovery = 44% Analysis Date = 03/01/11 Pct Recovery = 44% Analysis Date = 02/18/11 Pct Recovery = 44% Analysis Date = 02/18/11 Pct Recovery = 44% Analysis Date = 02/08/11 Pct Recovery = 43% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYHALOTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 90 57% 19% 57% 15%
Total 90 57% 19% 57% 15%

Sample Statistics
CYHALOTHRIN

Characteristic N % % Basis
Plotted 90 97% Spiked
Estimated Values 90 97% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 3 3% 3 out of 93
Not Spiked 76 .  
False Positives 0 0% 0 out of 76

BQS OBSP Determination:
CYPERMETHRIN
METHOD: 2033 , TESTIDCODE: 61586GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 45% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 57% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 54% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 58% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 46% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 48% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 50% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 60% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 51% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 73% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 59% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 46% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 61% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 78% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 92% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 66% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 72% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 59% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 72% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 71% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 68% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 60% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 44% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 79% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 64% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 60% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 51% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 42% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 53% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 57% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 52% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 56% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 51% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 74% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 92% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 45% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 62% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 70% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 39% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 85% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 40% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 42% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 84% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 65% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 59% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 115% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 105% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 43% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 102% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 75% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 68% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 115% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 63% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 63% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 65% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 73% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 67% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 63% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 94% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 75% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 69% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 69% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 74% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 68% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 52% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 61% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 63% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 115% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 48% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 81% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 99% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 82% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 57% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 88% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 104% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 88% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 66% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 64% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 72% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 65% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 97% Analysis Date = 01/17/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/05/16 Pct Recovery = 75% Analysis Date = 12/05/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/03/16 Pct Recovery = 75% Analysis Date = 11/03/16 Pct Recovery = 75% Analysis Date = 10/23/16 Pct Recovery = 75% Analysis Date = 10/23/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 74% Analysis Date = 10/12/16 Pct Recovery = 74% Analysis Date = 10/01/16 Pct Recovery = 74% Analysis Date = 10/01/16 Pct Recovery = 74% Analysis Date = 09/20/16 Pct Recovery = 74% Analysis Date = 09/20/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 74% Analysis Date = 08/19/16 Pct Recovery = 74% Analysis Date = 08/19/16 Pct Recovery = 74% Analysis Date = 08/08/16 Pct Recovery = 74% Analysis Date = 08/08/16 Pct Recovery = 74% Analysis Date = 07/28/16 Pct Recovery = 74% Analysis Date = 07/28/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/17/16 Pct Recovery = 74% Analysis Date = 07/06/16 Pct Recovery = 74% Analysis Date = 07/06/16 Pct Recovery = 74% Analysis Date = 06/25/16 Pct Recovery = 74% Analysis Date = 06/25/16 Pct Recovery = 74% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 04/21/16 Pct Recovery = 73% Analysis Date = 04/21/16 Pct Recovery = 73% Analysis Date = 04/10/16 Pct Recovery = 73% Analysis Date = 04/10/16 Pct Recovery = 73% Analysis Date = 03/30/16 Pct Recovery = 73% Analysis Date = 03/30/16 Pct Recovery = 73% Analysis Date = 03/20/16 Pct Recovery = 73% Analysis Date = 03/20/16 Pct Recovery = 73% Analysis Date = 03/09/16 Pct Recovery = 73% Analysis Date = 03/09/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/16/16 Pct Recovery = 73% Analysis Date = 02/16/16 Pct Recovery = 73% Analysis Date = 02/05/16 Pct Recovery = 72% Analysis Date = 02/05/16 Pct Recovery = 72% Analysis Date = 01/25/16 Pct Recovery = 72% Analysis Date = 01/25/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 72% Analysis Date = 01/14/16 Pct Recovery = 72% Analysis Date = 01/04/16 Pct Recovery = 72% Analysis Date = 01/04/16 Pct Recovery = 72% Analysis Date = 12/24/15 Pct Recovery = 72% Analysis Date = 12/24/15 Pct Recovery = 72% Analysis Date = 12/13/15 Pct Recovery = 72% Analysis Date = 12/13/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/21/15 Pct Recovery = 72% Analysis Date = 11/10/15 Pct Recovery = 72% Analysis Date = 11/10/15 Pct Recovery = 72% Analysis Date = 10/30/15 Pct Recovery = 71% Analysis Date = 10/30/15 Pct Recovery = 71% Analysis Date = 10/20/15 Pct Recovery = 71% Analysis Date = 10/20/15 Pct Recovery = 71% Analysis Date = 10/09/15 Pct Recovery = 71% Analysis Date = 10/09/15 Pct Recovery = 71% Analysis Date = 09/28/15 Pct Recovery = 71% Analysis Date = 09/28/15 Pct Recovery = 71% Analysis Date = 09/17/15 Pct Recovery = 71% Analysis Date = 09/17/15 Pct Recovery = 71% Analysis Date = 09/06/15 Pct Recovery = 71% Analysis Date = 09/06/15 Pct Recovery = 71% Analysis Date = 08/26/15 Pct Recovery = 71% Analysis Date = 08/26/15 Pct Recovery = 71% Analysis Date = 08/15/15 Pct Recovery = 71% Analysis Date = 08/15/15 Pct Recovery = 71% Analysis Date = 08/05/15 Pct Recovery = 71% Analysis Date = 08/05/15 Pct Recovery = 71% Analysis Date = 07/25/15 Pct Recovery = 70% Analysis Date = 07/25/15 Pct Recovery = 70% Analysis Date = 07/14/15 Pct Recovery = 70% Analysis Date = 07/14/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 06/22/15 Pct Recovery = 70% Analysis Date = 06/22/15 Pct Recovery = 70% Analysis Date = 06/11/15 Pct Recovery = 70% Analysis Date = 06/11/15 Pct Recovery = 70% Analysis Date = 05/31/15 Pct Recovery = 70% Analysis Date = 05/31/15 Pct Recovery = 70% Analysis Date = 05/21/15 Pct Recovery = 70% Analysis Date = 05/21/15 Pct Recovery = 70% Analysis Date = 05/10/15 Pct Recovery = 70% Analysis Date = 05/10/15 Pct Recovery = 70% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/29/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/18/15 Pct Recovery = 69% Analysis Date = 04/07/15 Pct Recovery = 69% Analysis Date = 04/07/15 Pct Recovery = 69% Analysis Date = 03/27/15 Pct Recovery = 69% Analysis Date = 03/27/15 Pct Recovery = 69% Analysis Date = 03/16/15 Pct Recovery = 69% Analysis Date = 03/16/15 Pct Recovery = 69% Analysis Date = 03/06/15 Pct Recovery = 69% Analysis Date = 03/06/15 Pct Recovery = 69% Analysis Date = 02/23/15 Pct Recovery = 69% Analysis Date = 02/23/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/01/15 Pct Recovery = 69% Analysis Date = 02/01/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/10/15 Pct Recovery = 68% Analysis Date = 01/10/15 Pct Recovery = 68% Analysis Date = 12/31/14 Pct Recovery = 68% Analysis Date = 12/31/14 Pct Recovery = 68% Analysis Date = 12/20/14 Pct Recovery = 68% Analysis Date = 12/20/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 11/28/14 Pct Recovery = 68% Analysis Date = 11/28/14 Pct Recovery = 68% Analysis Date = 11/17/14 Pct Recovery = 68% Analysis Date = 11/17/14 Pct Recovery = 68% Analysis Date = 11/06/14 Pct Recovery = 68% Analysis Date = 11/06/14 Pct Recovery = 68% Analysis Date = 10/26/14 Pct Recovery = 68% Analysis Date = 10/26/14 Pct Recovery = 68% Analysis Date = 10/16/14 Pct Recovery = 68% Analysis Date = 10/16/14 Pct Recovery = 68% Analysis Date = 10/05/14 Pct Recovery = 68% Analysis Date = 10/05/14 Pct Recovery = 68% Analysis Date = 09/24/14 Pct Recovery = 68% Analysis Date = 09/24/14 Pct Recovery = 68% Analysis Date = 09/13/14 Pct Recovery = 68% Analysis Date = 09/13/14 Pct Recovery = 68% Analysis Date = 09/02/14 Pct Recovery = 68% Analysis Date = 09/02/14 Pct Recovery = 68% Analysis Date = 08/22/14 Pct Recovery = 68% Analysis Date = 08/22/14 Pct Recovery = 68% Analysis Date = 08/11/14 Pct Recovery = 68% Analysis Date = 08/11/14 Pct Recovery = 68% Analysis Date = 08/01/14 Pct Recovery = 68% Analysis Date = 08/01/14 Pct Recovery = 68% Analysis Date = 07/21/14 Pct Recovery = 68% Analysis Date = 07/21/14 Pct Recovery = 68% Analysis Date = 07/10/14 Pct Recovery = 68% Analysis Date = 07/10/14 Pct Recovery = 68% Analysis Date = 06/29/14 Pct Recovery = 67% Analysis Date = 06/29/14 Pct Recovery = 67% Analysis Date = 06/18/14 Pct Recovery = 67% Analysis Date = 06/18/14 Pct Recovery = 67% Analysis Date = 06/07/14 Pct Recovery = 67% Analysis Date = 06/07/14 Pct Recovery = 67% Analysis Date = 05/27/14 Pct Recovery = 67% Analysis Date = 05/27/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Analysis Date = 05/06/14 Pct Recovery = 67% Analysis Date = 05/06/14 Pct Recovery = 67% Analysis Date = 04/25/14 Pct Recovery = 66% Analysis Date = 04/25/14 Pct Recovery = 66% Analysis Date = 04/14/14 Pct Recovery = 66% Analysis Date = 04/14/14 Pct Recovery = 66% Analysis Date = 04/03/14 Pct Recovery = 66% Analysis Date = 04/03/14 Pct Recovery = 66% Analysis Date = 03/23/14 Pct Recovery = 66% Analysis Date = 03/23/14 Pct Recovery = 66% Analysis Date = 03/12/14 Pct Recovery = 66% Analysis Date = 03/12/14 Pct Recovery = 66% Analysis Date = 03/02/14 Pct Recovery = 66% Analysis Date = 03/02/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 65% Analysis Date = 02/19/14 Pct Recovery = 65% Analysis Date = 02/08/14 Pct Recovery = 65% Analysis Date = 02/08/14 Pct Recovery = 65% Analysis Date = 01/28/14 Pct Recovery = 65% Analysis Date = 01/28/14 Pct Recovery = 65% Analysis Date = 01/17/14 Pct Recovery = 65% Analysis Date = 01/17/14 Pct Recovery = 65% Analysis Date = 01/06/14 Pct Recovery = 65% Analysis Date = 01/06/14 Pct Recovery = 65% Analysis Date = 12/26/13 Pct Recovery = 65% Analysis Date = 12/26/13 Pct Recovery = 65% Analysis Date = 12/16/13 Pct Recovery = 65% Analysis Date = 12/16/13 Pct Recovery = 65% Analysis Date = 12/05/13 Pct Recovery = 64% Analysis Date = 12/05/13 Pct Recovery = 64% Analysis Date = 11/24/13 Pct Recovery = 64% Analysis Date = 11/24/13 Pct Recovery = 64% Analysis Date = 11/13/13 Pct Recovery = 64% Analysis Date = 11/13/13 Pct Recovery = 64% Analysis Date = 11/02/13 Pct Recovery = 64% Analysis Date = 11/02/13 Pct Recovery = 64% Analysis Date = 10/22/13 Pct Recovery = 64% Analysis Date = 10/22/13 Pct Recovery = 64% Analysis Date = 10/11/13 Pct Recovery = 64% Analysis Date = 10/11/13 Pct Recovery = 64% Analysis Date = 10/01/13 Pct Recovery = 64% Analysis Date = 10/01/13 Pct Recovery = 64% Analysis Date = 09/20/13 Pct Recovery = 64% Analysis Date = 09/20/13 Pct Recovery = 64% Analysis Date = 09/09/13 Pct Recovery = 64% Analysis Date = 09/09/13 Pct Recovery = 64% Analysis Date = 08/29/13 Pct Recovery = 64% Analysis Date = 08/29/13 Pct Recovery = 64% Analysis Date = 08/18/13 Pct Recovery = 64% Analysis Date = 08/18/13 Pct Recovery = 64% Analysis Date = 08/07/13 Pct Recovery = 64% Analysis Date = 08/07/13 Pct Recovery = 64% Analysis Date = 07/27/13 Pct Recovery = 64% Analysis Date = 07/27/13 Pct Recovery = 64% Analysis Date = 07/17/13 Pct Recovery = 64% Analysis Date = 07/17/13 Pct Recovery = 64% Analysis Date = 07/06/13 Pct Recovery = 64% Analysis Date = 07/06/13 Pct Recovery = 64% Analysis Date = 06/25/13 Pct Recovery = 64% Analysis Date = 06/25/13 Pct Recovery = 64% Analysis Date = 06/14/13 Pct Recovery = 64% Analysis Date = 06/14/13 Pct Recovery = 64% Analysis Date = 06/03/13 Pct Recovery = 64% Analysis Date = 06/03/13 Pct Recovery = 64% Analysis Date = 05/23/13 Pct Recovery = 64% Analysis Date = 05/23/13 Pct Recovery = 64% Analysis Date = 05/12/13 Pct Recovery = 64% Analysis Date = 05/12/13 Pct Recovery = 64% Analysis Date = 05/02/13 Pct Recovery = 64% Analysis Date = 05/02/13 Pct Recovery = 64% Analysis Date = 04/21/13 Pct Recovery = 64% Analysis Date = 04/21/13 Pct Recovery = 64% Analysis Date = 04/10/13 Pct Recovery = 64% Analysis Date = 04/10/13 Pct Recovery = 64% Analysis Date = 03/30/13 Pct Recovery = 64% Analysis Date = 03/30/13 Pct Recovery = 64% Analysis Date = 03/19/13 Pct Recovery = 64% Analysis Date = 03/19/13 Pct Recovery = 64% Analysis Date = 03/08/13 Pct Recovery = 64% Analysis Date = 03/08/13 Pct Recovery = 64% Analysis Date = 02/25/13 Pct Recovery = 64% Analysis Date = 02/25/13 Pct Recovery = 64% Analysis Date = 02/15/13 Pct Recovery = 64% Analysis Date = 02/15/13 Pct Recovery = 64% Analysis Date = 02/04/13 Pct Recovery = 64% Analysis Date = 02/04/13 Pct Recovery = 64% Analysis Date = 01/24/13 Pct Recovery = 64% Analysis Date = 01/24/13 Pct Recovery = 64% Analysis Date = 01/13/13 Pct Recovery = 64% Analysis Date = 01/13/13 Pct Recovery = 64% Analysis Date = 01/02/13 Pct Recovery = 64% Analysis Date = 01/02/13 Pct Recovery = 64% Analysis Date = 12/22/12 Pct Recovery = 64% Analysis Date = 12/22/12 Pct Recovery = 64% Analysis Date = 12/12/12 Pct Recovery = 64% Analysis Date = 12/12/12 Pct Recovery = 64% Analysis Date = 12/01/12 Pct Recovery = 64% Analysis Date = 12/01/12 Pct Recovery = 64% Analysis Date = 11/20/12 Pct Recovery = 64% Analysis Date = 11/20/12 Pct Recovery = 64% Analysis Date = 11/09/12 Pct Recovery = 64% Analysis Date = 11/09/12 Pct Recovery = 64% Analysis Date = 10/29/12 Pct Recovery = 64% Analysis Date = 10/29/12 Pct Recovery = 64% Analysis Date = 10/18/12 Pct Recovery = 64% Analysis Date = 10/18/12 Pct Recovery = 64% Analysis Date = 10/07/12 Pct Recovery = 64% Analysis Date = 10/07/12 Pct Recovery = 64% Analysis Date = 09/27/12 Pct Recovery = 64% Analysis Date = 09/27/12 Pct Recovery = 64% Analysis Date = 09/16/12 Pct Recovery = 64% Analysis Date = 09/16/12 Pct Recovery = 64% Analysis Date = 09/05/12 Pct Recovery = 64% Analysis Date = 09/05/12 Pct Recovery = 64% Analysis Date = 08/25/12 Pct Recovery = 64% Analysis Date = 08/25/12 Pct Recovery = 64% Analysis Date = 08/14/12 Pct Recovery = 64% Analysis Date = 08/14/12 Pct Recovery = 64% Analysis Date = 08/03/12 Pct Recovery = 64% Analysis Date = 08/03/12 Pct Recovery = 64% Analysis Date = 07/23/12 Pct Recovery = 64% Analysis Date = 07/23/12 Pct Recovery = 64% Analysis Date = 07/13/12 Pct Recovery = 64% Analysis Date = 07/13/12 Pct Recovery = 64% Analysis Date = 07/02/12 Pct Recovery = 64% Analysis Date = 07/02/12 Pct Recovery = 64% Analysis Date = 06/21/12 Pct Recovery = 64% Analysis Date = 06/21/12 Pct Recovery = 64% Analysis Date = 06/10/12 Pct Recovery = 64% Analysis Date = 06/10/12 Pct Recovery = 64% Analysis Date = 05/30/12 Pct Recovery = 65% Analysis Date = 05/30/12 Pct Recovery = 65% Analysis Date = 05/19/12 Pct Recovery = 65% Analysis Date = 05/19/12 Pct Recovery = 65% Analysis Date = 05/08/12 Pct Recovery = 65% Analysis Date = 05/08/12 Pct Recovery = 65% Analysis Date = 04/28/12 Pct Recovery = 65% Analysis Date = 04/28/12 Pct Recovery = 65% Analysis Date = 04/17/12 Pct Recovery = 65% Analysis Date = 04/17/12 Pct Recovery = 65% Analysis Date = 04/06/12 Pct Recovery = 65% Analysis Date = 04/06/12 Pct Recovery = 65% Analysis Date = 03/26/12 Pct Recovery = 66% Analysis Date = 03/26/12 Pct Recovery = 66% Analysis Date = 03/15/12 Pct Recovery = 66% Analysis Date = 03/15/12 Pct Recovery = 66% Analysis Date = 03/04/12 Pct Recovery = 66% Analysis Date = 03/04/12 Pct Recovery = 66% Analysis Date = 02/22/12 Pct Recovery = 66% Analysis Date = 02/22/12 Pct Recovery = 66% Analysis Date = 02/12/12 Pct Recovery = 66% Analysis Date = 02/12/12 Pct Recovery = 66% Analysis Date = 02/01/12 Pct Recovery = 67% Analysis Date = 02/01/12 Pct Recovery = 67% Analysis Date = 01/21/12 Pct Recovery = 67% Analysis Date = 01/21/12 Pct Recovery = 67% Analysis Date = 01/10/12 Pct Recovery = 67% Analysis Date = 01/10/12 Pct Recovery = 67% Analysis Date = 12/30/11 Pct Recovery = 67% Analysis Date = 12/30/11 Pct Recovery = 67% Analysis Date = 12/19/11 Pct Recovery = 67% Analysis Date = 12/19/11 Pct Recovery = 67% Analysis Date = 12/08/11 Pct Recovery = 67% Analysis Date = 12/08/11 Pct Recovery = 67% Analysis Date = 11/28/11 Pct Recovery = 68% Analysis Date = 11/28/11 Pct Recovery = 68% Analysis Date = 11/17/11 Pct Recovery = 68% Analysis Date = 11/17/11 Pct Recovery = 68% Analysis Date = 11/06/11 Pct Recovery = 68% Analysis Date = 11/06/11 Pct Recovery = 68% Analysis Date = 10/26/11 Pct Recovery = 68% Analysis Date = 10/26/11 Pct Recovery = 68% Analysis Date = 10/15/11 Pct Recovery = 68% Analysis Date = 10/15/11 Pct Recovery = 68% Analysis Date = 10/04/11 Pct Recovery = 69% Analysis Date = 10/04/11 Pct Recovery = 69% Analysis Date = 09/23/11 Pct Recovery = 69% Analysis Date = 09/23/11 Pct Recovery = 69% Analysis Date = 09/13/11 Pct Recovery = 69% Analysis Date = 09/13/11 Pct Recovery = 69% Analysis Date = 09/02/11 Pct Recovery = 69% Analysis Date = 09/02/11 Pct Recovery = 69% Analysis Date = 08/22/11 Pct Recovery = 69% Analysis Date = 08/22/11 Pct Recovery = 69% Analysis Date = 08/11/11 Pct Recovery = 69% Analysis Date = 08/11/11 Pct Recovery = 69% Analysis Date = 07/31/11 Pct Recovery = 70% Analysis Date = 07/31/11 Pct Recovery = 70% Analysis Date = 07/20/11 Pct Recovery = 70% Analysis Date = 07/20/11 Pct Recovery = 70% Analysis Date = 07/09/11 Pct Recovery = 70% Analysis Date = 07/09/11 Pct Recovery = 70% Analysis Date = 06/29/11 Pct Recovery = 70% Analysis Date = 06/29/11 Pct Recovery = 70% Analysis Date = 06/18/11 Pct Recovery = 70% Analysis Date = 06/18/11 Pct Recovery = 70% Analysis Date = 06/07/11 Pct Recovery = 71% Analysis Date = 06/07/11 Pct Recovery = 71% Analysis Date = 05/27/11 Pct Recovery = 71% Analysis Date = 05/27/11 Pct Recovery = 71% Analysis Date = 05/16/11 Pct Recovery = 71% Analysis Date = 05/16/11 Pct Recovery = 71% Analysis Date = 05/05/11 Pct Recovery = 71% Analysis Date = 05/05/11 Pct Recovery = 71% Analysis Date = 04/24/11 Pct Recovery = 71% Analysis Date = 04/24/11 Pct Recovery = 71% Analysis Date = 04/14/11 Pct Recovery = 72% Analysis Date = 04/14/11 Pct Recovery = 72% Analysis Date = 04/03/11 Pct Recovery = 72% Analysis Date = 04/03/11 Pct Recovery = 72% Analysis Date = 03/23/11 Pct Recovery = 72% Analysis Date = 03/23/11 Pct Recovery = 72% Analysis Date = 03/12/11 Pct Recovery = 72% Analysis Date = 03/12/11 Pct Recovery = 72% Analysis Date = 03/01/11 Pct Recovery = 72% Analysis Date = 03/01/11 Pct Recovery = 72% Analysis Date = 02/18/11 Pct Recovery = 73% Analysis Date = 02/18/11 Pct Recovery = 73% Analysis Date = 02/08/11 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYPERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 93 68% 18% 65% 14%
Total 93 68% 18% 65% 14%

Sample Statistics
CYPERMETHRIN

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 93 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 1 1% 1 out of 76

BQS OBSP Determination:
DACTHAL
METHOD: 2033 , TESTIDCODE: 82682GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 98% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 110% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 99% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 105% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 95% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 99% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 95% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 100% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 93% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 89% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 101% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 98% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 89% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 93% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 95% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 98% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 82% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 100% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 112% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 111% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 126% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 99% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 125% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 78% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 122% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 80% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 88% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 108% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 103% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 102% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 107% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 109% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 81% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 100% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 118% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 92% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 91% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 105% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 135% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 97% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 97% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 107% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 112% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 110% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 89% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 99% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 98% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 109% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 92% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 97% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 117% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 76% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 75% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 89% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 106% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 93% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 96% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 106% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 93% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 106% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 102% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 117% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 93% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 80% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 93% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 75% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 93% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 103% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 103% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 113% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 103% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 122% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 118% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 100% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 102% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 103% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 95% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 120% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 106% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 98% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 97% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/09/16 Pct Recovery = 91% Analysis Date = 12/09/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 92% Analysis Date = 10/27/16 Pct Recovery = 92% Analysis Date = 10/16/16 Pct Recovery = 92% Analysis Date = 10/16/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/25/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/04/16 Pct Recovery = 92% Analysis Date = 09/04/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 92% Analysis Date = 08/24/16 Pct Recovery = 92% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/13/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 08/03/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/02/16 Pct Recovery = 93% Analysis Date = 07/02/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/10/16 Pct Recovery = 93% Analysis Date = 06/10/16 Pct Recovery = 93% Analysis Date = 05/31/16 Pct Recovery = 94% Analysis Date = 05/31/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/18/16 Pct Recovery = 94% Analysis Date = 04/18/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 95% Analysis Date = 03/06/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/24/16 Pct Recovery = 95% Analysis Date = 02/14/16 Pct Recovery = 95% Analysis Date = 02/14/16 Pct Recovery = 95% Analysis Date = 02/03/16 Pct Recovery = 95% Analysis Date = 02/03/16 Pct Recovery = 95% Analysis Date = 01/23/16 Pct Recovery = 95% Analysis Date = 01/23/16 Pct Recovery = 95% Analysis Date = 01/13/16 Pct Recovery = 95% Analysis Date = 01/13/16 Pct Recovery = 95% Analysis Date = 01/02/16 Pct Recovery = 95% Analysis Date = 01/02/16 Pct Recovery = 95% Analysis Date = 12/22/15 Pct Recovery = 96% Analysis Date = 12/22/15 Pct Recovery = 96% Analysis Date = 12/12/15 Pct Recovery = 96% Analysis Date = 12/12/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 96% Analysis Date = 11/20/15 Pct Recovery = 96% Analysis Date = 11/20/15 Pct Recovery = 96% Analysis Date = 11/10/15 Pct Recovery = 96% Analysis Date = 11/10/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/30/15 Pct Recovery = 96% Analysis Date = 10/19/15 Pct Recovery = 96% Analysis Date = 10/19/15 Pct Recovery = 96% Analysis Date = 10/09/15 Pct Recovery = 96% Analysis Date = 10/09/15 Pct Recovery = 96% Analysis Date = 09/28/15 Pct Recovery = 96% Analysis Date = 09/28/15 Pct Recovery = 96% Analysis Date = 09/17/15 Pct Recovery = 97% Analysis Date = 09/17/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 09/07/15 Pct Recovery = 97% Analysis Date = 08/27/15 Pct Recovery = 97% Analysis Date = 08/27/15 Pct Recovery = 97% Analysis Date = 08/16/15 Pct Recovery = 97% Analysis Date = 08/16/15 Pct Recovery = 97% Analysis Date = 08/06/15 Pct Recovery = 97% Analysis Date = 08/06/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/26/15 Pct Recovery = 97% Analysis Date = 07/15/15 Pct Recovery = 98% Analysis Date = 07/15/15 Pct Recovery = 98% Analysis Date = 07/05/15 Pct Recovery = 98% Analysis Date = 07/05/15 Pct Recovery = 98% Analysis Date = 06/24/15 Pct Recovery = 98% Analysis Date = 06/24/15 Pct Recovery = 98% Analysis Date = 06/13/15 Pct Recovery = 98% Analysis Date = 06/13/15 Pct Recovery = 98% Analysis Date = 06/02/15 Pct Recovery = 98% Analysis Date = 06/02/15 Pct Recovery = 98% Analysis Date = 05/23/15 Pct Recovery = 98% Analysis Date = 05/23/15 Pct Recovery = 98% Analysis Date = 05/12/15 Pct Recovery = 99% Analysis Date = 05/12/15 Pct Recovery = 99% Analysis Date = 05/01/15 Pct Recovery = 99% Analysis Date = 05/01/15 Pct Recovery = 99% Analysis Date = 04/21/15 Pct Recovery = 99% Analysis Date = 04/21/15 Pct Recovery = 99% Analysis Date = 04/10/15 Pct Recovery = 99% Analysis Date = 04/10/15 Pct Recovery = 99% Analysis Date = 03/30/15 Pct Recovery = 99% Analysis Date = 03/30/15 Pct Recovery = 99% Analysis Date = 03/20/15 Pct Recovery = 99% Analysis Date = 03/20/15 Pct Recovery = 99% Analysis Date = 03/09/15 Pct Recovery = 99% Analysis Date = 03/09/15 Pct Recovery = 99% Analysis Date = 02/26/15 Pct Recovery = 100% Analysis Date = 02/26/15 Pct Recovery = 100% Analysis Date = 02/16/15 Pct Recovery = 100% Analysis Date = 02/16/15 Pct Recovery = 100% Analysis Date = 02/05/15 Pct Recovery = 100% Analysis Date = 02/05/15 Pct Recovery = 100% Analysis Date = 01/25/15 Pct Recovery = 100% Analysis Date = 01/25/15 Pct Recovery = 100% Analysis Date = 01/15/15 Pct Recovery = 100% Analysis Date = 01/15/15 Pct Recovery = 100% Analysis Date = 01/04/15 Pct Recovery = 100% Analysis Date = 01/04/15 Pct Recovery = 100% Analysis Date = 12/24/14 Pct Recovery = 100% Analysis Date = 12/24/14 Pct Recovery = 100% Analysis Date = 12/14/14 Pct Recovery = 101% Analysis Date = 12/14/14 Pct Recovery = 101% Analysis Date = 12/03/14 Pct Recovery = 101% Analysis Date = 12/03/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/22/14 Pct Recovery = 101% Analysis Date = 11/12/14 Pct Recovery = 101% Analysis Date = 11/12/14 Pct Recovery = 101% Analysis Date = 11/01/14 Pct Recovery = 101% Analysis Date = 11/01/14 Pct Recovery = 101% Analysis Date = 10/21/14 Pct Recovery = 101% Analysis Date = 10/21/14 Pct Recovery = 101% Analysis Date = 10/11/14 Pct Recovery = 101% Analysis Date = 10/11/14 Pct Recovery = 101% Analysis Date = 09/30/14 Pct Recovery = 101% Analysis Date = 09/30/14 Pct Recovery = 101% Analysis Date = 09/19/14 Pct Recovery = 101% Analysis Date = 09/19/14 Pct Recovery = 101% Analysis Date = 09/08/14 Pct Recovery = 102% Analysis Date = 09/08/14 Pct Recovery = 102% Analysis Date = 08/29/14 Pct Recovery = 102% Analysis Date = 08/29/14 Pct Recovery = 102% Analysis Date = 08/18/14 Pct Recovery = 102% Analysis Date = 08/18/14 Pct Recovery = 102% Analysis Date = 08/07/14 Pct Recovery = 102% Analysis Date = 08/07/14 Pct Recovery = 102% Analysis Date = 07/28/14 Pct Recovery = 102% Analysis Date = 07/28/14 Pct Recovery = 102% Analysis Date = 07/17/14 Pct Recovery = 102% Analysis Date = 07/17/14 Pct Recovery = 102% Analysis Date = 07/06/14 Pct Recovery = 102% Analysis Date = 07/06/14 Pct Recovery = 102% Analysis Date = 06/26/14 Pct Recovery = 102% Analysis Date = 06/26/14 Pct Recovery = 102% Analysis Date = 06/15/14 Pct Recovery = 102% Analysis Date = 06/15/14 Pct Recovery = 102% Analysis Date = 06/04/14 Pct Recovery = 102% Analysis Date = 06/04/14 Pct Recovery = 102% Analysis Date = 05/25/14 Pct Recovery = 103% Analysis Date = 05/25/14 Pct Recovery = 103% Analysis Date = 05/14/14 Pct Recovery = 103% Analysis Date = 05/14/14 Pct Recovery = 103% Analysis Date = 05/03/14 Pct Recovery = 103% Analysis Date = 05/03/14 Pct Recovery = 103% Analysis Date = 04/23/14 Pct Recovery = 103% Analysis Date = 04/23/14 Pct Recovery = 103% Analysis Date = 04/12/14 Pct Recovery = 103% Analysis Date = 04/12/14 Pct Recovery = 103% Analysis Date = 04/01/14 Pct Recovery = 103% Analysis Date = 04/01/14 Pct Recovery = 103% Analysis Date = 03/22/14 Pct Recovery = 103% Analysis Date = 03/22/14 Pct Recovery = 103% Analysis Date = 03/11/14 Pct Recovery = 103% Analysis Date = 03/11/14 Pct Recovery = 103% Analysis Date = 02/28/14 Pct Recovery = 103% Analysis Date = 02/28/14 Pct Recovery = 103% Analysis Date = 02/18/14 Pct Recovery = 103% Analysis Date = 02/18/14 Pct Recovery = 103% Analysis Date = 02/07/14 Pct Recovery = 103% Analysis Date = 02/07/14 Pct Recovery = 103% Analysis Date = 01/27/14 Pct Recovery = 103% Analysis Date = 01/27/14 Pct Recovery = 103% Analysis Date = 01/17/14 Pct Recovery = 103% Analysis Date = 01/17/14 Pct Recovery = 103% Analysis Date = 01/06/14 Pct Recovery = 103% Analysis Date = 01/06/14 Pct Recovery = 103% Analysis Date = 12/26/13 Pct Recovery = 103% Analysis Date = 12/26/13 Pct Recovery = 103% Analysis Date = 12/15/13 Pct Recovery = 103% Analysis Date = 12/15/13 Pct Recovery = 103% Analysis Date = 12/05/13 Pct Recovery = 103% Analysis Date = 12/05/13 Pct Recovery = 103% Analysis Date = 11/24/13 Pct Recovery = 103% Analysis Date = 11/24/13 Pct Recovery = 103% Analysis Date = 11/13/13 Pct Recovery = 103% Analysis Date = 11/13/13 Pct Recovery = 103% Analysis Date = 11/03/13 Pct Recovery = 103% Analysis Date = 11/03/13 Pct Recovery = 103% Analysis Date = 10/23/13 Pct Recovery = 103% Analysis Date = 10/23/13 Pct Recovery = 103% Analysis Date = 10/12/13 Pct Recovery = 103% Analysis Date = 10/12/13 Pct Recovery = 103% Analysis Date = 10/02/13 Pct Recovery = 103% Analysis Date = 10/02/13 Pct Recovery = 103% Analysis Date = 09/21/13 Pct Recovery = 103% Analysis Date = 09/21/13 Pct Recovery = 103% Analysis Date = 09/10/13 Pct Recovery = 103% Analysis Date = 09/10/13 Pct Recovery = 103% Analysis Date = 08/31/13 Pct Recovery = 103% Analysis Date = 08/31/13 Pct Recovery = 103% Analysis Date = 08/20/13 Pct Recovery = 103% Analysis Date = 08/20/13 Pct Recovery = 103% Analysis Date = 08/09/13 Pct Recovery = 102% Analysis Date = 08/09/13 Pct Recovery = 102% Analysis Date = 07/30/13 Pct Recovery = 102% Analysis Date = 07/30/13 Pct Recovery = 102% Analysis Date = 07/19/13 Pct Recovery = 102% Analysis Date = 07/19/13 Pct Recovery = 102% Analysis Date = 07/08/13 Pct Recovery = 102% Analysis Date = 07/08/13 Pct Recovery = 102% Analysis Date = 06/28/13 Pct Recovery = 102% Analysis Date = 06/28/13 Pct Recovery = 102% Analysis Date = 06/17/13 Pct Recovery = 102% Analysis Date = 06/17/13 Pct Recovery = 102% Analysis Date = 06/06/13 Pct Recovery = 102% Analysis Date = 06/06/13 Pct Recovery = 102% Analysis Date = 05/27/13 Pct Recovery = 102% Analysis Date = 05/27/13 Pct Recovery = 102% Analysis Date = 05/16/13 Pct Recovery = 102% Analysis Date = 05/16/13 Pct Recovery = 102% Analysis Date = 05/05/13 Pct Recovery = 101% Analysis Date = 05/05/13 Pct Recovery = 101% Analysis Date = 04/25/13 Pct Recovery = 101% Analysis Date = 04/25/13 Pct Recovery = 101% Analysis Date = 04/14/13 Pct Recovery = 101% Analysis Date = 04/14/13 Pct Recovery = 101% Analysis Date = 04/03/13 Pct Recovery = 101% Analysis Date = 04/03/13 Pct Recovery = 101% Analysis Date = 03/23/13 Pct Recovery = 101% Analysis Date = 03/23/13 Pct Recovery = 101% Analysis Date = 03/13/13 Pct Recovery = 101% Analysis Date = 03/13/13 Pct Recovery = 101% Analysis Date = 03/02/13 Pct Recovery = 101% Analysis Date = 03/02/13 Pct Recovery = 101% Analysis Date = 02/19/13 Pct Recovery = 100% Analysis Date = 02/19/13 Pct Recovery = 100% Analysis Date = 02/09/13 Pct Recovery = 100% Analysis Date = 02/09/13 Pct Recovery = 100% Analysis Date = 01/29/13 Pct Recovery = 100% Analysis Date = 01/29/13 Pct Recovery = 100% Analysis Date = 01/18/13 Pct Recovery = 100% Analysis Date = 01/18/13 Pct Recovery = 100% Analysis Date = 01/08/13 Pct Recovery = 100% Analysis Date = 01/08/13 Pct Recovery = 100% Analysis Date = 12/28/12 Pct Recovery = 99% Analysis Date = 12/28/12 Pct Recovery = 99% Analysis Date = 12/17/12 Pct Recovery = 99% Analysis Date = 12/17/12 Pct Recovery = 99% Analysis Date = 12/07/12 Pct Recovery = 99% Analysis Date = 12/07/12 Pct Recovery = 99% Analysis Date = 11/26/12 Pct Recovery = 99% Analysis Date = 11/26/12 Pct Recovery = 99% Analysis Date = 11/15/12 Pct Recovery = 99% Analysis Date = 11/15/12 Pct Recovery = 99% Analysis Date = 11/05/12 Pct Recovery = 99% Analysis Date = 11/05/12 Pct Recovery = 99% Analysis Date = 10/25/12 Pct Recovery = 99% Analysis Date = 10/25/12 Pct Recovery = 99% Analysis Date = 10/14/12 Pct Recovery = 99% Analysis Date = 10/14/12 Pct Recovery = 99% Analysis Date = 10/04/12 Pct Recovery = 99% Analysis Date = 10/04/12 Pct Recovery = 99% Analysis Date = 09/23/12 Pct Recovery = 98% Analysis Date = 09/23/12 Pct Recovery = 98% Analysis Date = 09/12/12 Pct Recovery = 98% Analysis Date = 09/12/12 Pct Recovery = 98% Analysis Date = 09/02/12 Pct Recovery = 98% Analysis Date = 09/02/12 Pct Recovery = 98% Analysis Date = 08/22/12 Pct Recovery = 98% Analysis Date = 08/22/12 Pct Recovery = 98% Analysis Date = 08/11/12 Pct Recovery = 98% Analysis Date = 08/11/12 Pct Recovery = 98% Analysis Date = 08/01/12 Pct Recovery = 98% Analysis Date = 08/01/12 Pct Recovery = 98% Analysis Date = 07/21/12 Pct Recovery = 98% Analysis Date = 07/21/12 Pct Recovery = 98% Analysis Date = 07/10/12 Pct Recovery = 98% Analysis Date = 07/10/12 Pct Recovery = 98% Analysis Date = 06/29/12 Pct Recovery = 98% Analysis Date = 06/29/12 Pct Recovery = 98% Analysis Date = 06/19/12 Pct Recovery = 98% Analysis Date = 06/19/12 Pct Recovery = 98% Analysis Date = 06/08/12 Pct Recovery = 98% Analysis Date = 06/08/12 Pct Recovery = 98% Analysis Date = 05/28/12 Pct Recovery = 98% Analysis Date = 05/28/12 Pct Recovery = 98% Analysis Date = 05/18/12 Pct Recovery = 98% Analysis Date = 05/18/12 Pct Recovery = 98% Analysis Date = 05/07/12 Pct Recovery = 98% Analysis Date = 05/07/12 Pct Recovery = 98% Analysis Date = 04/26/12 Pct Recovery = 98% Analysis Date = 04/26/12 Pct Recovery = 98% Analysis Date = 04/16/12 Pct Recovery = 98% Analysis Date = 04/16/12 Pct Recovery = 98% Analysis Date = 04/05/12 Pct Recovery = 98% Analysis Date = 04/05/12 Pct Recovery = 98% Analysis Date = 03/25/12 Pct Recovery = 98% Analysis Date = 03/25/12 Pct Recovery = 98% Analysis Date = 03/15/12 Pct Recovery = 98% Analysis Date = 03/15/12 Pct Recovery = 98% Analysis Date = 03/04/12 Pct Recovery = 98% Analysis Date = 03/04/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/12/12 Pct Recovery = 98% Analysis Date = 02/12/12 Pct Recovery = 98% Analysis Date = 02/01/12 Pct Recovery = 98% Analysis Date = 02/01/12 Pct Recovery = 98% Analysis Date = 01/21/12 Pct Recovery = 98% Analysis Date = 01/21/12 Pct Recovery = 98% Analysis Date = 01/11/12 Pct Recovery = 98% Analysis Date = 01/11/12 Pct Recovery = 98% Analysis Date = 12/31/11 Pct Recovery = 98% Analysis Date = 12/31/11 Pct Recovery = 98% Analysis Date = 12/20/11 Pct Recovery = 98% Analysis Date = 12/20/11 Pct Recovery = 98% Analysis Date = 12/10/11 Pct Recovery = 98% Analysis Date = 12/10/11 Pct Recovery = 98% Analysis Date = 11/29/11 Pct Recovery = 98% Analysis Date = 11/29/11 Pct Recovery = 98% Analysis Date = 11/18/11 Pct Recovery = 98% Analysis Date = 11/18/11 Pct Recovery = 98% Analysis Date = 11/08/11 Pct Recovery = 98% Analysis Date = 11/08/11 Pct Recovery = 98% Analysis Date = 10/28/11 Pct Recovery = 98% Analysis Date = 10/28/11 Pct Recovery = 98% Analysis Date = 10/17/11 Pct Recovery = 98% Analysis Date = 10/17/11 Pct Recovery = 98% Analysis Date = 10/06/11 Pct Recovery = 98% Analysis Date = 10/06/11 Pct Recovery = 98% Analysis Date = 09/26/11 Pct Recovery = 98% Analysis Date = 09/26/11 Pct Recovery = 98% Analysis Date = 09/15/11 Pct Recovery = 98% Analysis Date = 09/15/11 Pct Recovery = 98% Analysis Date = 09/04/11 Pct Recovery = 98% Analysis Date = 09/04/11 Pct Recovery = 98% Analysis Date = 08/25/11 Pct Recovery = 98% Analysis Date = 08/25/11 Pct Recovery = 98% Analysis Date = 08/14/11 Pct Recovery = 99% Analysis Date = 08/14/11 Pct Recovery = 99% Analysis Date = 08/03/11 Pct Recovery = 99% Analysis Date = 08/03/11 Pct Recovery = 99% Analysis Date = 07/24/11 Pct Recovery = 99% Analysis Date = 07/24/11 Pct Recovery = 99% Analysis Date = 07/13/11 Pct Recovery = 99% Analysis Date = 07/13/11 Pct Recovery = 99% Analysis Date = 07/02/11 Pct Recovery = 99% Analysis Date = 07/02/11 Pct Recovery = 99% Analysis Date = 06/22/11 Pct Recovery = 99% Analysis Date = 06/22/11 Pct Recovery = 99% Analysis Date = 06/11/11 Pct Recovery = 99% Analysis Date = 06/11/11 Pct Recovery = 99% Analysis Date = 05/31/11 Pct Recovery = 99% Analysis Date = 05/31/11 Pct Recovery = 99% Analysis Date = 05/21/11 Pct Recovery = 99% Analysis Date = 05/21/11 Pct Recovery = 99% Analysis Date = 05/10/11 Pct Recovery = 99% Analysis Date = 05/10/11 Pct Recovery = 99% Analysis Date = 04/29/11 Pct Recovery = 99% Analysis Date = 04/29/11 Pct Recovery = 99% Analysis Date = 04/19/11 Pct Recovery = 99% Analysis Date = 04/19/11 Pct Recovery = 99% Analysis Date = 04/08/11 Pct Recovery = 99% Analysis Date = 04/08/11 Pct Recovery = 99% Analysis Date = 03/28/11 Pct Recovery = 99% Analysis Date = 03/28/11 Pct Recovery = 99% Analysis Date = 03/18/11 Pct Recovery = 99% Analysis Date = 03/18/11 Pct Recovery = 99% Analysis Date = 03/07/11 Pct Recovery = 99% Analysis Date = 03/07/11 Pct Recovery = 99% Analysis Date = 02/24/11 Pct Recovery = 99% Analysis Date = 02/24/11 Pct Recovery = 99% Analysis Date = 02/14/11 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DACTHAL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 99% 12% 98% 10%
Total 94 99% 12% 98% 10%

Sample Statistics
DACTHAL

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
DEETHYLATRAZINE
METHOD: 2033 , TESTIDCODE: 04040GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 37% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 43% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 68% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 36% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 65% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 28% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 36% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 44% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 84% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 102% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 52% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 33% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 38% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 98% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 97% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 50% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 38% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 47% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 57% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 55% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 44% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 53% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 33% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 109% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 116% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 107% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 112% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 17% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 62% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 51% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 83% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 81% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 60% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 85% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 16% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 37% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 38% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 35% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 32% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 36% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 49% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 56% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 47% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 44% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 50% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 51% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 50% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 112% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 85% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 124% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 133% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 145% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 106% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 58% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 62% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 131% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 114% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 110% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 72% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 139% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 135% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 110% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 130% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 55% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 52% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 52% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 54% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 50% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 51% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 37% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 51% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 63% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 58% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 80% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 78% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 51% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 58% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 61% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 88% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 69% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 62% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 64% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 61% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 54% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 69% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 64% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 73% Analysis Date = 01/17/17 Pct Recovery = 56% Analysis Date = 01/07/17 Pct Recovery = 56% Analysis Date = 01/07/17 Pct Recovery = 56% Analysis Date = 12/27/16 Pct Recovery = 56% Analysis Date = 12/27/16 Pct Recovery = 56% Analysis Date = 12/16/16 Pct Recovery = 56% Analysis Date = 12/16/16 Pct Recovery = 56% Analysis Date = 12/05/16 Pct Recovery = 56% Analysis Date = 12/05/16 Pct Recovery = 56% Analysis Date = 11/24/16 Pct Recovery = 56% Analysis Date = 11/24/16 Pct Recovery = 56% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 10/23/16 Pct Recovery = 55% Analysis Date = 10/23/16 Pct Recovery = 55% Analysis Date = 10/12/16 Pct Recovery = 55% Analysis Date = 10/12/16 Pct Recovery = 55% Analysis Date = 10/01/16 Pct Recovery = 55% Analysis Date = 10/01/16 Pct Recovery = 55% Analysis Date = 09/20/16 Pct Recovery = 55% Analysis Date = 09/20/16 Pct Recovery = 55% Analysis Date = 09/09/16 Pct Recovery = 55% Analysis Date = 09/09/16 Pct Recovery = 55% Analysis Date = 08/29/16 Pct Recovery = 55% Analysis Date = 08/29/16 Pct Recovery = 55% Analysis Date = 08/19/16 Pct Recovery = 54% Analysis Date = 08/19/16 Pct Recovery = 54% Analysis Date = 08/08/16 Pct Recovery = 54% Analysis Date = 08/08/16 Pct Recovery = 54% Analysis Date = 07/28/16 Pct Recovery = 54% Analysis Date = 07/28/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 06/25/16 Pct Recovery = 54% Analysis Date = 06/25/16 Pct Recovery = 54% Analysis Date = 06/14/16 Pct Recovery = 54% Analysis Date = 06/14/16 Pct Recovery = 54% Analysis Date = 06/04/16 Pct Recovery = 54% Analysis Date = 06/04/16 Pct Recovery = 54% Analysis Date = 05/24/16 Pct Recovery = 53% Analysis Date = 05/24/16 Pct Recovery = 53% Analysis Date = 05/13/16 Pct Recovery = 53% Analysis Date = 05/13/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 04/21/16 Pct Recovery = 53% Analysis Date = 04/21/16 Pct Recovery = 53% Analysis Date = 04/10/16 Pct Recovery = 53% Analysis Date = 04/10/16 Pct Recovery = 53% Analysis Date = 03/30/16 Pct Recovery = 53% Analysis Date = 03/30/16 Pct Recovery = 53% Analysis Date = 03/20/16 Pct Recovery = 53% Analysis Date = 03/20/16 Pct Recovery = 53% Analysis Date = 03/09/16 Pct Recovery = 53% Analysis Date = 03/09/16 Pct Recovery = 53% Analysis Date = 02/27/16 Pct Recovery = 52% Analysis Date = 02/27/16 Pct Recovery = 52% Analysis Date = 02/16/16 Pct Recovery = 52% Analysis Date = 02/16/16 Pct Recovery = 52% Analysis Date = 02/05/16 Pct Recovery = 52% Analysis Date = 02/05/16 Pct Recovery = 52% Analysis Date = 01/25/16 Pct Recovery = 52% Analysis Date = 01/25/16 Pct Recovery = 52% Analysis Date = 01/14/16 Pct Recovery = 52% Analysis Date = 01/14/16 Pct Recovery = 52% Analysis Date = 01/04/16 Pct Recovery = 52% Analysis Date = 01/04/16 Pct Recovery = 52% Analysis Date = 12/24/15 Pct Recovery = 52% Analysis Date = 12/24/15 Pct Recovery = 52% Analysis Date = 12/13/15 Pct Recovery = 52% Analysis Date = 12/13/15 Pct Recovery = 52% Analysis Date = 12/02/15 Pct Recovery = 51% Analysis Date = 12/02/15 Pct Recovery = 51% Analysis Date = 11/21/15 Pct Recovery = 51% Analysis Date = 11/21/15 Pct Recovery = 51% Analysis Date = 11/10/15 Pct Recovery = 51% Analysis Date = 11/10/15 Pct Recovery = 51% Analysis Date = 10/30/15 Pct Recovery = 51% Analysis Date = 10/30/15 Pct Recovery = 51% Analysis Date = 10/20/15 Pct Recovery = 51% Analysis Date = 10/20/15 Pct Recovery = 51% Analysis Date = 10/09/15 Pct Recovery = 51% Analysis Date = 10/09/15 Pct Recovery = 51% Analysis Date = 09/28/15 Pct Recovery = 51% Analysis Date = 09/28/15 Pct Recovery = 51% Analysis Date = 09/17/15 Pct Recovery = 51% Analysis Date = 09/17/15 Pct Recovery = 51% Analysis Date = 09/06/15 Pct Recovery = 50% Analysis Date = 09/06/15 Pct Recovery = 50% Analysis Date = 08/26/15 Pct Recovery = 50% Analysis Date = 08/26/15 Pct Recovery = 50% Analysis Date = 08/15/15 Pct Recovery = 50% Analysis Date = 08/15/15 Pct Recovery = 50% Analysis Date = 08/05/15 Pct Recovery = 50% Analysis Date = 08/05/15 Pct Recovery = 50% Analysis Date = 07/25/15 Pct Recovery = 50% Analysis Date = 07/25/15 Pct Recovery = 50% Analysis Date = 07/14/15 Pct Recovery = 50% Analysis Date = 07/14/15 Pct Recovery = 50% Analysis Date = 07/03/15 Pct Recovery = 50% Analysis Date = 07/03/15 Pct Recovery = 50% Analysis Date = 06/22/15 Pct Recovery = 50% Analysis Date = 06/22/15 Pct Recovery = 50% Analysis Date = 06/11/15 Pct Recovery = 49% Analysis Date = 06/11/15 Pct Recovery = 49% Analysis Date = 05/31/15 Pct Recovery = 49% Analysis Date = 05/31/15 Pct Recovery = 49% Analysis Date = 05/21/15 Pct Recovery = 49% Analysis Date = 05/21/15 Pct Recovery = 49% Analysis Date = 05/10/15 Pct Recovery = 49% Analysis Date = 05/10/15 Pct Recovery = 49% Analysis Date = 04/29/15 Pct Recovery = 49% Analysis Date = 04/29/15 Pct Recovery = 49% Analysis Date = 04/18/15 Pct Recovery = 49% Analysis Date = 04/18/15 Pct Recovery = 49% Analysis Date = 04/07/15 Pct Recovery = 49% Analysis Date = 04/07/15 Pct Recovery = 49% Analysis Date = 03/27/15 Pct Recovery = 49% Analysis Date = 03/27/15 Pct Recovery = 49% Analysis Date = 03/16/15 Pct Recovery = 49% Analysis Date = 03/16/15 Pct Recovery = 49% Analysis Date = 03/06/15 Pct Recovery = 48% Analysis Date = 03/06/15 Pct Recovery = 48% Analysis Date = 02/23/15 Pct Recovery = 48% Analysis Date = 02/23/15 Pct Recovery = 48% Analysis Date = 02/12/15 Pct Recovery = 48% Analysis Date = 02/12/15 Pct Recovery = 48% Analysis Date = 02/01/15 Pct Recovery = 48% Analysis Date = 02/01/15 Pct Recovery = 48% Analysis Date = 01/21/15 Pct Recovery = 48% Analysis Date = 01/21/15 Pct Recovery = 48% Analysis Date = 01/10/15 Pct Recovery = 48% Analysis Date = 01/10/15 Pct Recovery = 48% Analysis Date = 12/31/14 Pct Recovery = 48% Analysis Date = 12/31/14 Pct Recovery = 48% Analysis Date = 12/20/14 Pct Recovery = 48% Analysis Date = 12/20/14 Pct Recovery = 48% Analysis Date = 12/09/14 Pct Recovery = 48% Analysis Date = 12/09/14 Pct Recovery = 48% Analysis Date = 11/28/14 Pct Recovery = 48% Analysis Date = 11/28/14 Pct Recovery = 48% Analysis Date = 11/17/14 Pct Recovery = 48% Analysis Date = 11/17/14 Pct Recovery = 48% Analysis Date = 11/06/14 Pct Recovery = 48% Analysis Date = 11/06/14 Pct Recovery = 48% Analysis Date = 10/26/14 Pct Recovery = 48% Analysis Date = 10/26/14 Pct Recovery = 48% Analysis Date = 10/16/14 Pct Recovery = 49% Analysis Date = 10/16/14 Pct Recovery = 49% Analysis Date = 10/05/14 Pct Recovery = 49% Analysis Date = 10/05/14 Pct Recovery = 49% Analysis Date = 09/24/14 Pct Recovery = 49% Analysis Date = 09/24/14 Pct Recovery = 49% Analysis Date = 09/13/14 Pct Recovery = 49% Analysis Date = 09/13/14 Pct Recovery = 49% Analysis Date = 09/02/14 Pct Recovery = 49% Analysis Date = 09/02/14 Pct Recovery = 49% Analysis Date = 08/22/14 Pct Recovery = 49% Analysis Date = 08/22/14 Pct Recovery = 49% Analysis Date = 08/11/14 Pct Recovery = 49% Analysis Date = 08/11/14 Pct Recovery = 49% Analysis Date = 08/01/14 Pct Recovery = 49% Analysis Date = 08/01/14 Pct Recovery = 49% Analysis Date = 07/21/14 Pct Recovery = 49% Analysis Date = 07/21/14 Pct Recovery = 49% Analysis Date = 07/10/14 Pct Recovery = 49% Analysis Date = 07/10/14 Pct Recovery = 49% Analysis Date = 06/29/14 Pct Recovery = 49% Analysis Date = 06/29/14 Pct Recovery = 49% Analysis Date = 06/18/14 Pct Recovery = 49% Analysis Date = 06/18/14 Pct Recovery = 49% Analysis Date = 06/07/14 Pct Recovery = 49% Analysis Date = 06/07/14 Pct Recovery = 49% Analysis Date = 05/27/14 Pct Recovery = 50% Analysis Date = 05/27/14 Pct Recovery = 50% Analysis Date = 05/17/14 Pct Recovery = 50% Analysis Date = 05/17/14 Pct Recovery = 50% Analysis Date = 05/06/14 Pct Recovery = 50% Analysis Date = 05/06/14 Pct Recovery = 50% Analysis Date = 04/25/14 Pct Recovery = 50% Analysis Date = 04/25/14 Pct Recovery = 50% Analysis Date = 04/14/14 Pct Recovery = 51% Analysis Date = 04/14/14 Pct Recovery = 51% Analysis Date = 04/03/14 Pct Recovery = 51% Analysis Date = 04/03/14 Pct Recovery = 51% Analysis Date = 03/23/14 Pct Recovery = 51% Analysis Date = 03/23/14 Pct Recovery = 51% Analysis Date = 03/12/14 Pct Recovery = 51% Analysis Date = 03/12/14 Pct Recovery = 51% Analysis Date = 03/02/14 Pct Recovery = 51% Analysis Date = 03/02/14 Pct Recovery = 51% Analysis Date = 02/19/14 Pct Recovery = 52% Analysis Date = 02/19/14 Pct Recovery = 52% Analysis Date = 02/08/14 Pct Recovery = 52% Analysis Date = 02/08/14 Pct Recovery = 52% Analysis Date = 01/28/14 Pct Recovery = 52% Analysis Date = 01/28/14 Pct Recovery = 52% Analysis Date = 01/17/14 Pct Recovery = 52% Analysis Date = 01/17/14 Pct Recovery = 52% Analysis Date = 01/06/14 Pct Recovery = 53% Analysis Date = 01/06/14 Pct Recovery = 53% Analysis Date = 12/26/13 Pct Recovery = 53% Analysis Date = 12/26/13 Pct Recovery = 53% Analysis Date = 12/16/13 Pct Recovery = 53% Analysis Date = 12/16/13 Pct Recovery = 53% Analysis Date = 12/05/13 Pct Recovery = 53% Analysis Date = 12/05/13 Pct Recovery = 53% Analysis Date = 11/24/13 Pct Recovery = 53% Analysis Date = 11/24/13 Pct Recovery = 53% Analysis Date = 11/13/13 Pct Recovery = 54% Analysis Date = 11/13/13 Pct Recovery = 54% Analysis Date = 11/02/13 Pct Recovery = 54% Analysis Date = 11/02/13 Pct Recovery = 54% Analysis Date = 10/22/13 Pct Recovery = 54% Analysis Date = 10/22/13 Pct Recovery = 54% Analysis Date = 10/11/13 Pct Recovery = 55% Analysis Date = 10/11/13 Pct Recovery = 55% Analysis Date = 10/01/13 Pct Recovery = 55% Analysis Date = 10/01/13 Pct Recovery = 55% Analysis Date = 09/20/13 Pct Recovery = 56% Analysis Date = 09/20/13 Pct Recovery = 56% Analysis Date = 09/09/13 Pct Recovery = 56% Analysis Date = 09/09/13 Pct Recovery = 56% Analysis Date = 08/29/13 Pct Recovery = 57% Analysis Date = 08/29/13 Pct Recovery = 57% Analysis Date = 08/18/13 Pct Recovery = 57% Analysis Date = 08/18/13 Pct Recovery = 57% Analysis Date = 08/07/13 Pct Recovery = 57% Analysis Date = 08/07/13 Pct Recovery = 57% Analysis Date = 07/27/13 Pct Recovery = 58% Analysis Date = 07/27/13 Pct Recovery = 58% Analysis Date = 07/17/13 Pct Recovery = 58% Analysis Date = 07/17/13 Pct Recovery = 58% Analysis Date = 07/06/13 Pct Recovery = 59% Analysis Date = 07/06/13 Pct Recovery = 59% Analysis Date = 06/25/13 Pct Recovery = 59% Analysis Date = 06/25/13 Pct Recovery = 59% Analysis Date = 06/14/13 Pct Recovery = 59% Analysis Date = 06/14/13 Pct Recovery = 59% Analysis Date = 06/03/13 Pct Recovery = 60% Analysis Date = 06/03/13 Pct Recovery = 60% Analysis Date = 05/23/13 Pct Recovery = 60% Analysis Date = 05/23/13 Pct Recovery = 60% Analysis Date = 05/12/13 Pct Recovery = 61% Analysis Date = 05/12/13 Pct Recovery = 61% Analysis Date = 05/02/13 Pct Recovery = 61% Analysis Date = 05/02/13 Pct Recovery = 61% Analysis Date = 04/21/13 Pct Recovery = 61% Analysis Date = 04/21/13 Pct Recovery = 61% Analysis Date = 04/10/13 Pct Recovery = 62% Analysis Date = 04/10/13 Pct Recovery = 62% Analysis Date = 03/30/13 Pct Recovery = 62% Analysis Date = 03/30/13 Pct Recovery = 62% Analysis Date = 03/19/13 Pct Recovery = 63% Analysis Date = 03/19/13 Pct Recovery = 63% Analysis Date = 03/08/13 Pct Recovery = 64% Analysis Date = 03/08/13 Pct Recovery = 64% Analysis Date = 02/25/13 Pct Recovery = 65% Analysis Date = 02/25/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 66% Analysis Date = 02/15/13 Pct Recovery = 66% Analysis Date = 02/04/13 Pct Recovery = 67% Analysis Date = 02/04/13 Pct Recovery = 67% Analysis Date = 01/24/13 Pct Recovery = 68% Analysis Date = 01/24/13 Pct Recovery = 68% Analysis Date = 01/13/13 Pct Recovery = 68% Analysis Date = 01/13/13 Pct Recovery = 68% Analysis Date = 01/02/13 Pct Recovery = 69% Analysis Date = 01/02/13 Pct Recovery = 69% Analysis Date = 12/22/12 Pct Recovery = 70% Analysis Date = 12/22/12 Pct Recovery = 70% Analysis Date = 12/12/12 Pct Recovery = 71% Analysis Date = 12/12/12 Pct Recovery = 71% Analysis Date = 12/01/12 Pct Recovery = 72% Analysis Date = 12/01/12 Pct Recovery = 72% Analysis Date = 11/20/12 Pct Recovery = 73% Analysis Date = 11/20/12 Pct Recovery = 73% Analysis Date = 11/09/12 Pct Recovery = 73% Analysis Date = 11/09/12 Pct Recovery = 73% Analysis Date = 10/29/12 Pct Recovery = 74% Analysis Date = 10/29/12 Pct Recovery = 74% Analysis Date = 10/18/12 Pct Recovery = 75% Analysis Date = 10/18/12 Pct Recovery = 75% Analysis Date = 10/07/12 Pct Recovery = 76% Analysis Date = 10/07/12 Pct Recovery = 76% Analysis Date = 09/27/12 Pct Recovery = 77% Analysis Date = 09/27/12 Pct Recovery = 77% Analysis Date = 09/16/12 Pct Recovery = 78% Analysis Date = 09/16/12 Pct Recovery = 78% Analysis Date = 09/05/12 Pct Recovery = 78% Analysis Date = 09/05/12 Pct Recovery = 78% Analysis Date = 08/25/12 Pct Recovery = 79% Analysis Date = 08/25/12 Pct Recovery = 79% Analysis Date = 08/14/12 Pct Recovery = 80% Analysis Date = 08/14/12 Pct Recovery = 80% Analysis Date = 08/03/12 Pct Recovery = 81% Analysis Date = 08/03/12 Pct Recovery = 81% Analysis Date = 07/23/12 Pct Recovery = 82% Analysis Date = 07/23/12 Pct Recovery = 82% Analysis Date = 07/13/12 Pct Recovery = 83% Analysis Date = 07/13/12 Pct Recovery = 83% Analysis Date = 07/02/12 Pct Recovery = 83% Analysis Date = 07/02/12 Pct Recovery = 83% Analysis Date = 06/21/12 Pct Recovery = 84% Analysis Date = 06/21/12 Pct Recovery = 84% Analysis Date = 06/10/12 Pct Recovery = 85% Analysis Date = 06/10/12 Pct Recovery = 85% Analysis Date = 05/30/12 Pct Recovery = 86% Analysis Date = 05/30/12 Pct Recovery = 86% Analysis Date = 05/19/12 Pct Recovery = 87% Analysis Date = 05/19/12 Pct Recovery = 87% Analysis Date = 05/08/12 Pct Recovery = 87% Analysis Date = 05/08/12 Pct Recovery = 87% Analysis Date = 04/28/12 Pct Recovery = 88% Analysis Date = 04/28/12 Pct Recovery = 88% Analysis Date = 04/17/12 Pct Recovery = 89% Analysis Date = 04/17/12 Pct Recovery = 89% Analysis Date = 04/06/12 Pct Recovery = 90% Analysis Date = 04/06/12 Pct Recovery = 90% Analysis Date = 03/26/12 Pct Recovery = 90% Analysis Date = 03/26/12 Pct Recovery = 90% Analysis Date = 03/15/12 Pct Recovery = 91% Analysis Date = 03/15/12 Pct Recovery = 91% Analysis Date = 03/04/12 Pct Recovery = 92% Analysis Date = 03/04/12 Pct Recovery = 92% Analysis Date = 02/22/12 Pct Recovery = 93% Analysis Date = 02/22/12 Pct Recovery = 93% Analysis Date = 02/12/12 Pct Recovery = 94% Analysis Date = 02/12/12 Pct Recovery = 94% Analysis Date = 02/01/12 Pct Recovery = 94% Analysis Date = 02/01/12 Pct Recovery = 94% Analysis Date = 01/21/12 Pct Recovery = 95% Analysis Date = 01/21/12 Pct Recovery = 95% Analysis Date = 01/10/12 Pct Recovery = 96% Analysis Date = 01/10/12 Pct Recovery = 96% Analysis Date = 12/30/11 Pct Recovery = 97% Analysis Date = 12/30/11 Pct Recovery = 97% Analysis Date = 12/19/11 Pct Recovery = 97% Analysis Date = 12/19/11 Pct Recovery = 97% Analysis Date = 12/08/11 Pct Recovery = 98% Analysis Date = 12/08/11 Pct Recovery = 98% Analysis Date = 11/28/11 Pct Recovery = 99% Analysis Date = 11/28/11 Pct Recovery = 99% Analysis Date = 11/17/11 Pct Recovery = 100% Analysis Date = 11/17/11 Pct Recovery = 100% Analysis Date = 11/06/11 Pct Recovery = 101% Analysis Date = 11/06/11 Pct Recovery = 101% Analysis Date = 10/26/11 Pct Recovery = 102% Analysis Date = 10/26/11 Pct Recovery = 102% Analysis Date = 10/15/11 Pct Recovery = 103% Analysis Date = 10/15/11 Pct Recovery = 103% Analysis Date = 10/04/11 Pct Recovery = 103% Analysis Date = 10/04/11 Pct Recovery = 103% Analysis Date = 09/23/11 Pct Recovery = 104% Analysis Date = 09/23/11 Pct Recovery = 104% Analysis Date = 09/13/11 Pct Recovery = 105% Analysis Date = 09/13/11 Pct Recovery = 105% Analysis Date = 09/02/11 Pct Recovery = 106% Analysis Date = 09/02/11 Pct Recovery = 106% Analysis Date = 08/22/11 Pct Recovery = 107% Analysis Date = 08/22/11 Pct Recovery = 107% Analysis Date = 08/11/11 Pct Recovery = 108% Analysis Date = 08/11/11 Pct Recovery = 108% Analysis Date = 07/31/11 Pct Recovery = 108% Analysis Date = 07/31/11 Pct Recovery = 108% Analysis Date = 07/20/11 Pct Recovery = 109% Analysis Date = 07/20/11 Pct Recovery = 109% Analysis Date = 07/09/11 Pct Recovery = 110% Analysis Date = 07/09/11 Pct Recovery = 110% Analysis Date = 06/29/11 Pct Recovery = 111% Analysis Date = 06/29/11 Pct Recovery = 111% Analysis Date = 06/18/11 Pct Recovery = 112% Analysis Date = 06/18/11 Pct Recovery = 112% Analysis Date = 06/07/11 Pct Recovery = 113% Analysis Date = 06/07/11 Pct Recovery = 113% Analysis Date = 05/27/11 Pct Recovery = 114% Analysis Date = 05/27/11 Pct Recovery = 114% Analysis Date = 05/16/11 Pct Recovery = 114% Analysis Date = 05/16/11 Pct Recovery = 114% Analysis Date = 05/05/11 Pct Recovery = 115% Analysis Date = 05/05/11 Pct Recovery = 115% Analysis Date = 04/24/11 Pct Recovery = 116% Analysis Date = 04/24/11 Pct Recovery = 116% Analysis Date = 04/14/11 Pct Recovery = 117% Analysis Date = 04/14/11 Pct Recovery = 117% Analysis Date = 04/03/11 Pct Recovery = 118% Analysis Date = 04/03/11 Pct Recovery = 118% Analysis Date = 03/23/11 Pct Recovery = 119% Analysis Date = 03/23/11 Pct Recovery = 119% Analysis Date = 03/12/11 Pct Recovery = 119% Analysis Date = 03/12/11 Pct Recovery = 119% Analysis Date = 03/01/11 Pct Recovery = 120% Analysis Date = 03/01/11 Pct Recovery = 120% Analysis Date = 02/18/11 Pct Recovery = 121% Analysis Date = 02/18/11 Pct Recovery = 121% Analysis Date = 02/08/11 Pct Recovery = 122% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEETHYLATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 93 67% 30% 58% 25%
Total 93 67% 30% 58% 25%

Sample Statistics
DEETHYLATRAZINE

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 93 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 1 1% 1 out of 76

BQS OBSP Determination:
DESULFINYLFIPRONIL
METHOD: 2033 , TESTIDCODE: 62170GCM29
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 81% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 99% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 66% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 82% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 72% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 135% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 83% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 94% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 91% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 91% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 70% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 65% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 100% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 64% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 66% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 70% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 63% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 110% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 64% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 61% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 70% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 73% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 67% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 81% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 58% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 99% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 83% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 80% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 98% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 107% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 72% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 84% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 79% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 57% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 67% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 92% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 61% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 73% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 78% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 57% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 83% Analysis Date = 09/09/16 Pct Recovery = 83% Analysis Date = 09/09/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/20/16 Pct Recovery = 83% Analysis Date = 08/20/16 Pct Recovery = 83% Analysis Date = 08/10/16 Pct Recovery = 82% Analysis Date = 08/10/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/10/16 Pct Recovery = 82% Analysis Date = 07/10/16 Pct Recovery = 82% Analysis Date = 06/30/16 Pct Recovery = 82% Analysis Date = 06/30/16 Pct Recovery = 82% Analysis Date = 06/20/16 Pct Recovery = 81% Analysis Date = 06/20/16 Pct Recovery = 81% Analysis Date = 06/10/16 Pct Recovery = 81% Analysis Date = 06/10/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/20/16 Pct Recovery = 80% Analysis Date = 03/20/16 Pct Recovery = 80% Analysis Date = 03/10/16 Pct Recovery = 80% Analysis Date = 03/10/16 Pct Recovery = 80% Analysis Date = 02/29/16 Pct Recovery = 80% Analysis Date = 02/29/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 01/29/16 Pct Recovery = 79% Analysis Date = 01/29/16 Pct Recovery = 79% Analysis Date = 01/19/16 Pct Recovery = 79% Analysis Date = 01/19/16 Pct Recovery = 79% Analysis Date = 01/09/16 Pct Recovery = 79% Analysis Date = 01/09/16 Pct Recovery = 79% Analysis Date = 12/29/15 Pct Recovery = 79% Analysis Date = 12/29/15 Pct Recovery = 79% Analysis Date = 12/19/15 Pct Recovery = 79% Analysis Date = 12/19/15 Pct Recovery = 79% Analysis Date = 12/09/15 Pct Recovery = 78% Analysis Date = 12/09/15 Pct Recovery = 78% Analysis Date = 11/29/15 Pct Recovery = 78% Analysis Date = 11/29/15 Pct Recovery = 78% Analysis Date = 11/19/15 Pct Recovery = 78% Analysis Date = 11/19/15 Pct Recovery = 78% Analysis Date = 11/08/15 Pct Recovery = 78% Analysis Date = 11/08/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 78% Analysis Date = 10/09/15 Pct Recovery = 78% Analysis Date = 10/09/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/18/15 Pct Recovery = 77% Analysis Date = 09/18/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 77% Analysis Date = 08/09/15 Pct Recovery = 77% Analysis Date = 08/09/15 Pct Recovery = 77% Analysis Date = 07/29/15 Pct Recovery = 77% Analysis Date = 07/29/15 Pct Recovery = 77% Analysis Date = 07/19/15 Pct Recovery = 77% Analysis Date = 07/19/15 Pct Recovery = 77% Analysis Date = 07/09/15 Pct Recovery = 77% Analysis Date = 07/09/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/08/15 Pct Recovery = 77% Analysis Date = 06/08/15 Pct Recovery = 77% Analysis Date = 05/29/15 Pct Recovery = 77% Analysis Date = 05/29/15 Pct Recovery = 77% Analysis Date = 05/19/15 Pct Recovery = 77% Analysis Date = 05/19/15 Pct Recovery = 77% Analysis Date = 05/09/15 Pct Recovery = 77% Analysis Date = 05/09/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 77% Analysis Date = 04/18/15 Pct Recovery = 77% Analysis Date = 04/18/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/19/15 Pct Recovery = 77% Analysis Date = 03/19/15 Pct Recovery = 77% Analysis Date = 03/09/15 Pct Recovery = 77% Analysis Date = 03/09/15 Pct Recovery = 77% Analysis Date = 02/26/15 Pct Recovery = 77% Analysis Date = 02/26/15 Pct Recovery = 77% Analysis Date = 02/16/15 Pct Recovery = 77% Analysis Date = 02/16/15 Pct Recovery = 77% Analysis Date = 02/06/15 Pct Recovery = 77% Analysis Date = 02/06/15 Pct Recovery = 77% Analysis Date = 01/27/15 Pct Recovery = 77% Analysis Date = 01/27/15 Pct Recovery = 77% Analysis Date = 01/17/15 Pct Recovery = 77% Analysis Date = 01/17/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/17/14 Pct Recovery = 77% Analysis Date = 12/17/14 Pct Recovery = 77% Analysis Date = 12/07/14 Pct Recovery = 77% Analysis Date = 12/07/14 Pct Recovery = 77% Analysis Date = 11/27/14 Pct Recovery = 77% Analysis Date = 11/27/14 Pct Recovery = 77% Analysis Date = 11/16/14 Pct Recovery = 77% Analysis Date = 11/16/14 Pct Recovery = 77% Analysis Date = 11/06/14 Pct Recovery = 77% Analysis Date = 11/06/14 Pct Recovery = 77% Analysis Date = 10/27/14 Pct Recovery = 77% Analysis Date = 10/27/14 Pct Recovery = 77% Analysis Date = 10/17/14 Pct Recovery = 77% Analysis Date = 10/17/14 Pct Recovery = 77% Analysis Date = 10/07/14 Pct Recovery = 77% Analysis Date = 10/07/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/16/14 Pct Recovery = 77% Analysis Date = 09/16/14 Pct Recovery = 77% Analysis Date = 09/06/14 Pct Recovery = 77% Analysis Date = 09/06/14 Pct Recovery = 77% Analysis Date = 08/27/14 Pct Recovery = 77% Analysis Date = 08/27/14 Pct Recovery = 77% Analysis Date = 08/17/14 Pct Recovery = 77% Analysis Date = 08/17/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 07/27/14 Pct Recovery = 77% Analysis Date = 07/27/14 Pct Recovery = 77% Analysis Date = 07/17/14 Pct Recovery = 77% Analysis Date = 07/17/14 Pct Recovery = 77% Analysis Date = 07/07/14 Pct Recovery = 77% Analysis Date = 07/07/14 Pct Recovery = 77% Analysis Date = 06/27/14 Pct Recovery = 77% Analysis Date = 06/27/14 Pct Recovery = 77% Analysis Date = 06/16/14 Pct Recovery = 77% Analysis Date = 06/16/14 Pct Recovery = 77% Analysis Date = 06/06/14 Pct Recovery = 77% Analysis Date = 06/06/14 Pct Recovery = 77% Analysis Date = 05/27/14 Pct Recovery = 77% Analysis Date = 05/27/14 Pct Recovery = 77% Analysis Date = 05/17/14 Pct Recovery = 77% Analysis Date = 05/17/14 Pct Recovery = 77% Analysis Date = 05/07/14 Pct Recovery = 77% Analysis Date = 05/07/14 Pct Recovery = 77% Analysis Date = 04/26/14 Pct Recovery = 77% Analysis Date = 04/26/14 Pct Recovery = 77% Analysis Date = 04/16/14 Pct Recovery = 77% Analysis Date = 04/16/14 Pct Recovery = 77% Analysis Date = 04/06/14 Pct Recovery = 78% Analysis Date = 04/06/14 Pct Recovery = 78% Analysis Date = 03/27/14 Pct Recovery = 78% Analysis Date = 03/27/14 Pct Recovery = 78% Analysis Date = 03/17/14 Pct Recovery = 78% Analysis Date = 03/17/14 Pct Recovery = 78% Analysis Date = 03/06/14 Pct Recovery = 78% Analysis Date = 03/06/14 Pct Recovery = 78% Analysis Date = 02/24/14 Pct Recovery = 78% Analysis Date = 02/24/14 Pct Recovery = 78% Analysis Date = 02/14/14 Pct Recovery = 78% Analysis Date = 02/14/14 Pct Recovery = 78% Analysis Date = 02/04/14 Pct Recovery = 78% Analysis Date = 02/04/14 Pct Recovery = 78% Analysis Date = 01/25/14 Pct Recovery = 78% Analysis Date = 01/25/14 Pct Recovery = 78% Analysis Date = 01/14/14 Pct Recovery = 78% Analysis Date = 01/14/14 Pct Recovery = 78% Analysis Date = 01/04/14 Pct Recovery = 78% Analysis Date = 01/04/14 Pct Recovery = 78% Analysis Date = 12/25/13 Pct Recovery = 78% Analysis Date = 12/25/13 Pct Recovery = 78% Analysis Date = 12/15/13 Pct Recovery = 78% Analysis Date = 12/15/13 Pct Recovery = 78% Analysis Date = 12/05/13 Pct Recovery = 78% Analysis Date = 12/05/13 Pct Recovery = 78% Analysis Date = 11/24/13 Pct Recovery = 78% Analysis Date = 11/24/13 Pct Recovery = 78% Analysis Date = 11/14/13 Pct Recovery = 79% Analysis Date = 11/14/13 Pct Recovery = 79% Analysis Date = 11/04/13 Pct Recovery = 79% Analysis Date = 11/04/13 Pct Recovery = 79% Analysis Date = 10/25/13 Pct Recovery = 79% Analysis Date = 10/25/13 Pct Recovery = 79% Analysis Date = 10/15/13 Pct Recovery = 79% Analysis Date = 10/15/13 Pct Recovery = 79% Analysis Date = 10/04/13 Pct Recovery = 79% Analysis Date = 10/04/13 Pct Recovery = 79% Analysis Date = 09/24/13 Pct Recovery = 79% Analysis Date = 09/24/13 Pct Recovery = 79% Analysis Date = 09/14/13 Pct Recovery = 79% Analysis Date = 09/14/13 Pct Recovery = 79% Analysis Date = 09/04/13 Pct Recovery = 79% Analysis Date = 09/04/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/14/13 Pct Recovery = 79% Analysis Date = 08/14/13 Pct Recovery = 79% Analysis Date = 08/04/13 Pct Recovery = 79% Analysis Date = 08/04/13 Pct Recovery = 79% Analysis Date = 07/25/13 Pct Recovery = 79% Analysis Date = 07/25/13 Pct Recovery = 79% Analysis Date = 07/15/13 Pct Recovery = 79% Analysis Date = 07/15/13 Pct Recovery = 79% Analysis Date = 07/05/13 Pct Recovery = 80% Analysis Date = 07/05/13 Pct Recovery = 80% Analysis Date = 06/24/13 Pct Recovery = 80% Analysis Date = 06/24/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/04/13 Pct Recovery = 80% Analysis Date = 06/04/13 Pct Recovery = 80% Analysis Date = 05/25/13 Pct Recovery = 80% Analysis Date = 05/25/13 Pct Recovery = 80% Analysis Date = 05/15/13 Pct Recovery = 80% Analysis Date = 05/15/13 Pct Recovery = 80% Analysis Date = 05/04/13 Pct Recovery = 80% Analysis Date = 05/04/13 Pct Recovery = 80% Analysis Date = 04/24/13 Pct Recovery = 80% Analysis Date = 04/24/13 Pct Recovery = 80% Analysis Date = 04/14/13 Pct Recovery = 80% Analysis Date = 04/14/13 Pct Recovery = 80% Analysis Date = 04/04/13 Pct Recovery = 80% Analysis Date = 04/04/13 Pct Recovery = 80% Analysis Date = 03/25/13 Pct Recovery = 80% Analysis Date = 03/25/13 Pct Recovery = 80% Analysis Date = 03/14/13 Pct Recovery = 80% Analysis Date = 03/14/13 Pct Recovery = 80% Analysis Date = 03/04/13 Pct Recovery = 80% Analysis Date = 03/04/13 Pct Recovery = 80% Analysis Date = 02/22/13 Pct Recovery = 80% Analysis Date = 02/22/13 Pct Recovery = 80% Analysis Date = 02/12/13 Pct Recovery = 81% Analysis Date = 02/12/13 Pct Recovery = 81% Analysis Date = 02/02/13 Pct Recovery = 81% Analysis Date = 02/02/13 Pct Recovery = 81% Analysis Date = 01/22/13 Pct Recovery = 81% Analysis Date = 01/22/13 Pct Recovery = 81% Analysis Date = 01/12/13 Pct Recovery = 81% Analysis Date = 01/12/13 Pct Recovery = 81% Analysis Date = 01/02/13 Pct Recovery = 81% Analysis Date = 01/02/13 Pct Recovery = 81% Analysis Date = 12/23/12 Pct Recovery = 81% Analysis Date = 12/23/12 Pct Recovery = 81% Analysis Date = 12/13/12 Pct Recovery = 81% Analysis Date = 12/13/12 Pct Recovery = 81% Analysis Date = 12/02/12 Pct Recovery = 81% Analysis Date = 12/02/12 Pct Recovery = 81% Analysis Date = 11/22/12 Pct Recovery = 81% Analysis Date = 11/22/12 Pct Recovery = 81% Analysis Date = 11/12/12 Pct Recovery = 81% Analysis Date = 11/12/12 Pct Recovery = 81% Analysis Date = 11/02/12 Pct Recovery = 81% Analysis Date = 11/02/12 Pct Recovery = 81% Analysis Date = 10/23/12 Pct Recovery = 81% Analysis Date = 10/23/12 Pct Recovery = 81% Analysis Date = 10/12/12 Pct Recovery = 81% Analysis Date = 10/12/12 Pct Recovery = 81% Analysis Date = 10/02/12 Pct Recovery = 81% Analysis Date = 10/02/12 Pct Recovery = 81% Analysis Date = 09/22/12 Pct Recovery = 81% Analysis Date = 09/22/12 Pct Recovery = 81% Analysis Date = 09/12/12 Pct Recovery = 81% Analysis Date = 09/12/12 Pct Recovery = 81% Analysis Date = 09/02/12 Pct Recovery = 81% Analysis Date = 09/02/12 Pct Recovery = 81% Analysis Date = 08/22/12 Pct Recovery = 81% Analysis Date = 08/22/12 Pct Recovery = 81% Analysis Date = 08/12/12 Pct Recovery = 81% Analysis Date = 08/12/12 Pct Recovery = 81% Analysis Date = 08/02/12 Pct Recovery = 81% Analysis Date = 08/02/12 Pct Recovery = 81% Analysis Date = 07/23/12 Pct Recovery = 80% Analysis Date = 07/23/12 Pct Recovery = 80% Analysis Date = 07/13/12 Pct Recovery = 80% Analysis Date = 07/13/12 Pct Recovery = 80% Analysis Date = 07/02/12 Pct Recovery = 80% Analysis Date = 07/02/12 Pct Recovery = 80% Analysis Date = 06/22/12 Pct Recovery = 80% Analysis Date = 06/22/12 Pct Recovery = 80% Analysis Date = 06/12/12 Pct Recovery = 80% Analysis Date = 06/12/12 Pct Recovery = 80% Analysis Date = 06/02/12 Pct Recovery = 80% Analysis Date = 06/02/12 Pct Recovery = 80% Analysis Date = 05/23/12 Pct Recovery = 80% Analysis Date = 05/23/12 Pct Recovery = 80% Analysis Date = 05/12/12 Pct Recovery = 80% Analysis Date = 05/12/12 Pct Recovery = 80% Analysis Date = 05/02/12 Pct Recovery = 80% Analysis Date = 05/02/12 Pct Recovery = 80% Analysis Date = 04/22/12 Pct Recovery = 80% Analysis Date = 04/22/12 Pct Recovery = 80% Analysis Date = 04/12/12 Pct Recovery = 80% Analysis Date = 04/12/12 Pct Recovery = 80% Analysis Date = 04/02/12 Pct Recovery = 80% Analysis Date = 04/02/12 Pct Recovery = 80% Analysis Date = 03/22/12 Pct Recovery = 80% Analysis Date = 03/22/12 Pct Recovery = 80% Analysis Date = 03/12/12 Pct Recovery = 80% Analysis Date = 03/12/12 Pct Recovery = 80% Analysis Date = 03/02/12 Pct Recovery = 80% Analysis Date = 03/02/12 Pct Recovery = 80% Analysis Date = 02/21/12 Pct Recovery = 80% Analysis Date = 02/21/12 Pct Recovery = 80% Analysis Date = 02/11/12 Pct Recovery = 80% Analysis Date = 02/11/12 Pct Recovery = 80% Analysis Date = 01/31/12 Pct Recovery = 80% Analysis Date = 01/31/12 Pct Recovery = 80% Analysis Date = 01/21/12 Pct Recovery = 80% Analysis Date = 01/21/12 Pct Recovery = 80% Analysis Date = 01/11/12 Pct Recovery = 80% Analysis Date = 01/11/12 Pct Recovery = 80% Analysis Date = 01/01/12 Pct Recovery = 80% Analysis Date = 01/01/12 Pct Recovery = 80% Analysis Date = 12/22/11 Pct Recovery = 80% Analysis Date = 12/22/11 Pct Recovery = 80% Analysis Date = 12/11/11 Pct Recovery = 80% Analysis Date = 12/11/11 Pct Recovery = 80% Analysis Date = 12/01/11 Pct Recovery = 80% Analysis Date = 12/01/11 Pct Recovery = 80% Analysis Date = 11/21/11 Pct Recovery = 80% Analysis Date = 11/21/11 Pct Recovery = 80% Analysis Date = 11/11/11 Pct Recovery = 80% Analysis Date = 11/11/11 Pct Recovery = 80% Analysis Date = 11/01/11 Pct Recovery = 80% Analysis Date = 11/01/11 Pct Recovery = 80% Analysis Date = 10/21/11 Pct Recovery = 80% Analysis Date = 10/21/11 Pct Recovery = 80% Analysis Date = 10/11/11 Pct Recovery = 80% Analysis Date = 10/11/11 Pct Recovery = 80% Analysis Date = 10/01/11 Pct Recovery = 80% Analysis Date = 10/01/11 Pct Recovery = 80% Analysis Date = 09/21/11 Pct Recovery = 80% Analysis Date = 09/21/11 Pct Recovery = 80% Analysis Date = 09/11/11 Pct Recovery = 80% Analysis Date = 09/11/11 Pct Recovery = 80% Analysis Date = 08/31/11 Pct Recovery = 80% Analysis Date = 08/31/11 Pct Recovery = 80% Analysis Date = 08/21/11 Pct Recovery = 80% Analysis Date = 08/21/11 Pct Recovery = 80% Analysis Date = 08/11/11 Pct Recovery = 80% Analysis Date = 08/11/11 Pct Recovery = 80% Analysis Date = 08/01/11 Pct Recovery = 80% Analysis Date = 08/01/11 Pct Recovery = 80% Analysis Date = 07/22/11 Pct Recovery = 80% Analysis Date = 07/22/11 Pct Recovery = 80% Analysis Date = 07/11/11 Pct Recovery = 80% Analysis Date = 07/11/11 Pct Recovery = 80% Analysis Date = 07/01/11 Pct Recovery = 80% Analysis Date = 07/01/11 Pct Recovery = 80% Analysis Date = 06/21/11 Pct Recovery = 80% Analysis Date = 06/21/11 Pct Recovery = 80% Analysis Date = 06/11/11 Pct Recovery = 80% Analysis Date = 06/11/11 Pct Recovery = 80% Analysis Date = 06/01/11 Pct Recovery = 80% Analysis Date = 06/01/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/11/11 Pct Recovery = 79% Analysis Date = 05/11/11 Pct Recovery = 79% Analysis Date = 05/01/11 Pct Recovery = 79% Analysis Date = 05/01/11 Pct Recovery = 79% Analysis Date = 04/21/11 Pct Recovery = 79% Analysis Date = 04/21/11 Pct Recovery = 79% Analysis Date = 04/11/11 Pct Recovery = 79% Analysis Date = 04/11/11 Pct Recovery = 79% Analysis Date = 03/31/11 Pct Recovery = 79% Analysis Date = 03/31/11 Pct Recovery = 79% Analysis Date = 03/21/11 Pct Recovery = 79% Analysis Date = 03/21/11 Pct Recovery = 79% Analysis Date = 03/11/11 Pct Recovery = 79% Analysis Date = 03/11/11 Pct Recovery = 79% Analysis Date = 03/01/11 Pct Recovery = 79% Analysis Date = 03/01/11 Pct Recovery = 79% Analysis Date = 02/19/11 Pct Recovery = 79% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 55 79% 15% 76% 15%
Total 55 79% 15% 76% 15%

Sample Statistics
DESULFINYLFIPRONIL

Characteristic N % % Basis
Plotted 55 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 55 .  
False Negatives 0 0% 0 out of 55
Not Spiked 114 .  
False Positives 1 1% 1 out of 114

BQS OBSP Determination:
DESULFINYLFIPRONIL AMIDE
METHOD: 2033 , TESTIDCODE: 62169GCM29
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 2% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 73% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 11% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 144% Analysis Date = 02/08/16 Pct Recovery = 11% Analysis Date = 01/30/16 Pct Recovery = 6% Analysis Date = 01/30/16 Pct Recovery = 6% Analysis Date = 01/21/16 Pct Recovery = 2% Analysis Date = 01/21/16 Pct Recovery = 2% Analysis Date = 01/12/16 Pct Recovery = 2% Analysis Date = 01/12/16 Pct Recovery = 2% Analysis Date = 01/03/16 Pct Recovery = 2% Analysis Date = 01/03/16 Pct Recovery = 2% Analysis Date = 12/25/15 Pct Recovery = 3% Analysis Date = 12/25/15 Pct Recovery = 3% Analysis Date = 12/16/15 Pct Recovery = 3% Analysis Date = 12/16/15 Pct Recovery = 3% Analysis Date = 12/07/15 Pct Recovery = 3% Analysis Date = 12/07/15 Pct Recovery = 3% Analysis Date = 11/28/15 Pct Recovery = 4% Analysis Date = 11/28/15 Pct Recovery = 4% Analysis Date = 11/19/15 Pct Recovery = 4% Analysis Date = 11/19/15 Pct Recovery = 4% Analysis Date = 11/10/15 Pct Recovery = 5% Analysis Date = 11/10/15 Pct Recovery = 5% Analysis Date = 11/01/15 Pct Recovery = 5% Analysis Date = 11/01/15 Pct Recovery = 5% Analysis Date = 10/23/15 Pct Recovery = 5% Analysis Date = 10/23/15 Pct Recovery = 5% Analysis Date = 10/14/15 Pct Recovery = 6% Analysis Date = 10/14/15 Pct Recovery = 6% Analysis Date = 10/05/15 Pct Recovery = 6% Analysis Date = 10/05/15 Pct Recovery = 6% Analysis Date = 09/26/15 Pct Recovery = 6% Analysis Date = 09/26/15 Pct Recovery = 6% Analysis Date = 09/17/15 Pct Recovery = 7% Analysis Date = 09/17/15 Pct Recovery = 7% Analysis Date = 09/08/15 Pct Recovery = 7% Analysis Date = 09/08/15 Pct Recovery = 7% Analysis Date = 08/30/15 Pct Recovery = 8% Analysis Date = 08/30/15 Pct Recovery = 8% Analysis Date = 08/21/15 Pct Recovery = 8% Analysis Date = 08/21/15 Pct Recovery = 8% Analysis Date = 08/12/15 Pct Recovery = 8% Analysis Date = 08/12/15 Pct Recovery = 8% Analysis Date = 08/03/15 Pct Recovery = 9% Analysis Date = 08/03/15 Pct Recovery = 9% Analysis Date = 07/25/15 Pct Recovery = 9% Analysis Date = 07/25/15 Pct Recovery = 9% Analysis Date = 07/16/15 Pct Recovery = 9% Analysis Date = 07/16/15 Pct Recovery = 9% Analysis Date = 07/07/15 Pct Recovery = 10% Analysis Date = 07/07/15 Pct Recovery = 10% Analysis Date = 06/28/15 Pct Recovery = 10% Analysis Date = 06/28/15 Pct Recovery = 10% Analysis Date = 06/19/15 Pct Recovery = 11% Analysis Date = 06/19/15 Pct Recovery = 11% Analysis Date = 06/10/15 Pct Recovery = 11% Analysis Date = 06/10/15 Pct Recovery = 11% Analysis Date = 06/01/15 Pct Recovery = 11% Analysis Date = 06/01/15 Pct Recovery = 11% Analysis Date = 05/23/15 Pct Recovery = 12% Analysis Date = 05/23/15 Pct Recovery = 12% Analysis Date = 05/14/15 Pct Recovery = 12% Analysis Date = 05/14/15 Pct Recovery = 12% Analysis Date = 05/05/15 Pct Recovery = 12% Analysis Date = 05/05/15 Pct Recovery = 12% Analysis Date = 04/26/15 Pct Recovery = 13% Analysis Date = 04/26/15 Pct Recovery = 13% Analysis Date = 04/17/15 Pct Recovery = 13% Analysis Date = 04/17/15 Pct Recovery = 13% Analysis Date = 04/08/15 Pct Recovery = 14% Analysis Date = 04/08/15 Pct Recovery = 14% Analysis Date = 03/30/15 Pct Recovery = 14% Analysis Date = 03/30/15 Pct Recovery = 14% Analysis Date = 03/21/15 Pct Recovery = 14% Analysis Date = 03/21/15 Pct Recovery = 14% Analysis Date = 03/12/15 Pct Recovery = 15% Analysis Date = 03/12/15 Pct Recovery = 15% Analysis Date = 03/03/15 Pct Recovery = 15% Analysis Date = 03/03/15 Pct Recovery = 15% Analysis Date = 02/22/15 Pct Recovery = 16% Analysis Date = 02/22/15 Pct Recovery = 16% Analysis Date = 02/13/15 Pct Recovery = 16% Analysis Date = 02/13/15 Pct Recovery = 16% Analysis Date = 02/04/15 Pct Recovery = 16% Analysis Date = 02/04/15 Pct Recovery = 16% Analysis Date = 01/26/15 Pct Recovery = 17% Analysis Date = 01/26/15 Pct Recovery = 17% Analysis Date = 01/17/15 Pct Recovery = 17% Analysis Date = 01/17/15 Pct Recovery = 17% Analysis Date = 01/08/15 Pct Recovery = 17% Analysis Date = 01/08/15 Pct Recovery = 17% Analysis Date = 12/30/14 Pct Recovery = 18% Analysis Date = 12/30/14 Pct Recovery = 18% Analysis Date = 12/21/14 Pct Recovery = 18% Analysis Date = 12/21/14 Pct Recovery = 18% Analysis Date = 12/12/14 Pct Recovery = 19% Analysis Date = 12/12/14 Pct Recovery = 19% Analysis Date = 12/03/14 Pct Recovery = 19% Analysis Date = 12/03/14 Pct Recovery = 19% Analysis Date = 11/24/14 Pct Recovery = 19% Analysis Date = 11/24/14 Pct Recovery = 19% Analysis Date = 11/15/14 Pct Recovery = 20% Analysis Date = 11/15/14 Pct Recovery = 20% Analysis Date = 11/06/14 Pct Recovery = 20% Analysis Date = 11/06/14 Pct Recovery = 20% Analysis Date = 10/28/14 Pct Recovery = 20% Analysis Date = 10/28/14 Pct Recovery = 20% Analysis Date = 10/19/14 Pct Recovery = 21% Analysis Date = 10/19/14 Pct Recovery = 21% Analysis Date = 10/10/14 Pct Recovery = 21% Analysis Date = 10/10/14 Pct Recovery = 21% Analysis Date = 10/01/14 Pct Recovery = 22% Analysis Date = 10/01/14 Pct Recovery = 22% Analysis Date = 09/22/14 Pct Recovery = 22% Analysis Date = 09/22/14 Pct Recovery = 22% Analysis Date = 09/13/14 Pct Recovery = 22% Analysis Date = 09/13/14 Pct Recovery = 22% Analysis Date = 09/04/14 Pct Recovery = 23% Analysis Date = 09/04/14 Pct Recovery = 23% Analysis Date = 08/26/14 Pct Recovery = 23% Analysis Date = 08/26/14 Pct Recovery = 23% Analysis Date = 08/17/14 Pct Recovery = 23% Analysis Date = 08/17/14 Pct Recovery = 23% Analysis Date = 08/08/14 Pct Recovery = 24% Analysis Date = 08/08/14 Pct Recovery = 24% Analysis Date = 07/30/14 Pct Recovery = 24% Analysis Date = 07/30/14 Pct Recovery = 24% Analysis Date = 07/21/14 Pct Recovery = 25% Analysis Date = 07/21/14 Pct Recovery = 25% Analysis Date = 07/12/14 Pct Recovery = 25% Analysis Date = 07/12/14 Pct Recovery = 25% Analysis Date = 07/03/14 Pct Recovery = 25% Analysis Date = 07/03/14 Pct Recovery = 25% Analysis Date = 06/24/14 Pct Recovery = 26% Analysis Date = 06/24/14 Pct Recovery = 26% Analysis Date = 06/15/14 Pct Recovery = 26% Analysis Date = 06/15/14 Pct Recovery = 26% Analysis Date = 06/06/14 Pct Recovery = 27% Analysis Date = 06/06/14 Pct Recovery = 27% Analysis Date = 05/28/14 Pct Recovery = 27% Analysis Date = 05/28/14 Pct Recovery = 27% Analysis Date = 05/19/14 Pct Recovery = 27% Analysis Date = 05/19/14 Pct Recovery = 27% Analysis Date = 05/10/14 Pct Recovery = 28% Analysis Date = 05/10/14 Pct Recovery = 28% Analysis Date = 05/01/14 Pct Recovery = 28% Analysis Date = 05/01/14 Pct Recovery = 28% Analysis Date = 04/22/14 Pct Recovery = 28% Analysis Date = 04/22/14 Pct Recovery = 28% Analysis Date = 04/13/14 Pct Recovery = 29% Analysis Date = 04/13/14 Pct Recovery = 29% Analysis Date = 04/04/14 Pct Recovery = 29% Analysis Date = 04/04/14 Pct Recovery = 29% Analysis Date = 03/26/14 Pct Recovery = 30% Analysis Date = 03/26/14 Pct Recovery = 30% Analysis Date = 03/17/14 Pct Recovery = 30% Analysis Date = 03/17/14 Pct Recovery = 30% Analysis Date = 03/08/14 Pct Recovery = 30% Analysis Date = 03/08/14 Pct Recovery = 30% Analysis Date = 02/27/14 Pct Recovery = 31% Analysis Date = 02/27/14 Pct Recovery = 31% Analysis Date = 02/18/14 Pct Recovery = 31% Analysis Date = 02/18/14 Pct Recovery = 31% Analysis Date = 02/09/14 Pct Recovery = 31% Analysis Date = 02/09/14 Pct Recovery = 31% Analysis Date = 01/31/14 Pct Recovery = 32% Analysis Date = 01/31/14 Pct Recovery = 32% Analysis Date = 01/22/14 Pct Recovery = 32% Analysis Date = 01/22/14 Pct Recovery = 32% Analysis Date = 01/13/14 Pct Recovery = 33% Analysis Date = 01/13/14 Pct Recovery = 33% Analysis Date = 01/04/14 Pct Recovery = 33% Analysis Date = 01/04/14 Pct Recovery = 33% Analysis Date = 12/26/13 Pct Recovery = 33% Analysis Date = 12/26/13 Pct Recovery = 33% Analysis Date = 12/17/13 Pct Recovery = 34% Analysis Date = 12/17/13 Pct Recovery = 34% Analysis Date = 12/08/13 Pct Recovery = 34% Analysis Date = 12/08/13 Pct Recovery = 34% Analysis Date = 11/29/13 Pct Recovery = 34% Analysis Date = 11/29/13 Pct Recovery = 34% Analysis Date = 11/20/13 Pct Recovery = 35% Analysis Date = 11/20/13 Pct Recovery = 35% Analysis Date = 11/11/13 Pct Recovery = 35% Analysis Date = 11/11/13 Pct Recovery = 35% Analysis Date = 11/02/13 Pct Recovery = 36% Analysis Date = 11/02/13 Pct Recovery = 36% Analysis Date = 10/24/13 Pct Recovery = 36% Analysis Date = 10/24/13 Pct Recovery = 36% Analysis Date = 10/15/13 Pct Recovery = 36% Analysis Date = 10/15/13 Pct Recovery = 36% Analysis Date = 10/06/13 Pct Recovery = 37% Analysis Date = 10/06/13 Pct Recovery = 37% Analysis Date = 09/27/13 Pct Recovery = 37% Analysis Date = 09/27/13 Pct Recovery = 37% Analysis Date = 09/18/13 Pct Recovery = 37% Analysis Date = 09/18/13 Pct Recovery = 37% Analysis Date = 09/09/13 Pct Recovery = 38% Analysis Date = 09/09/13 Pct Recovery = 38% Analysis Date = 08/31/13 Pct Recovery = 38% Analysis Date = 08/31/13 Pct Recovery = 38% Analysis Date = 08/21/13 Pct Recovery = 39% Analysis Date = 08/21/13 Pct Recovery = 39% Analysis Date = 08/12/13 Pct Recovery = 39% Analysis Date = 08/12/13 Pct Recovery = 39% Analysis Date = 08/03/13 Pct Recovery = 39% Analysis Date = 08/03/13 Pct Recovery = 39% Analysis Date = 07/25/13 Pct Recovery = 40% Analysis Date = 07/25/13 Pct Recovery = 40% Analysis Date = 07/16/13 Pct Recovery = 40% Analysis Date = 07/16/13 Pct Recovery = 40% Analysis Date = 07/07/13 Pct Recovery = 41% Analysis Date = 07/07/13 Pct Recovery = 41% Analysis Date = 06/28/13 Pct Recovery = 41% Analysis Date = 06/28/13 Pct Recovery = 41% Analysis Date = 06/19/13 Pct Recovery = 41% Analysis Date = 06/19/13 Pct Recovery = 41% Analysis Date = 06/10/13 Pct Recovery = 42% Analysis Date = 06/10/13 Pct Recovery = 42% Analysis Date = 06/01/13 Pct Recovery = 42% Analysis Date = 06/01/13 Pct Recovery = 42% Analysis Date = 05/23/13 Pct Recovery = 42% Analysis Date = 05/23/13 Pct Recovery = 42% Analysis Date = 05/14/13 Pct Recovery = 43% Analysis Date = 05/14/13 Pct Recovery = 43% Analysis Date = 05/05/13 Pct Recovery = 43% Analysis Date = 05/05/13 Pct Recovery = 43% Analysis Date = 04/26/13 Pct Recovery = 44% Analysis Date = 04/26/13 Pct Recovery = 44% Analysis Date = 04/17/13 Pct Recovery = 44% Analysis Date = 04/17/13 Pct Recovery = 44% Analysis Date = 04/08/13 Pct Recovery = 44% Analysis Date = 04/08/13 Pct Recovery = 44% Analysis Date = 03/30/13 Pct Recovery = 45% Analysis Date = 03/30/13 Pct Recovery = 45% Analysis Date = 03/21/13 Pct Recovery = 45% Analysis Date = 03/21/13 Pct Recovery = 45% Analysis Date = 03/12/13 Pct Recovery = 45% Analysis Date = 03/12/13 Pct Recovery = 45% Analysis Date = 03/03/13 Pct Recovery = 46% Analysis Date = 03/03/13 Pct Recovery = 46% Analysis Date = 02/22/13 Pct Recovery = 46% Analysis Date = 02/22/13 Pct Recovery = 46% Analysis Date = 02/13/13 Pct Recovery = 47% Analysis Date = 02/13/13 Pct Recovery = 47% Analysis Date = 02/04/13 Pct Recovery = 47% Analysis Date = 02/04/13 Pct Recovery = 47% Analysis Date = 01/26/13 Pct Recovery = 47% Analysis Date = 01/26/13 Pct Recovery = 47% Analysis Date = 01/17/13 Pct Recovery = 48% Analysis Date = 01/17/13 Pct Recovery = 48% Analysis Date = 01/08/13 Pct Recovery = 48% Analysis Date = 01/08/13 Pct Recovery = 48% Analysis Date = 12/30/12 Pct Recovery = 48% Analysis Date = 12/30/12 Pct Recovery = 48% Analysis Date = 12/21/12 Pct Recovery = 49% Analysis Date = 12/21/12 Pct Recovery = 49% Analysis Date = 12/12/12 Pct Recovery = 49% Analysis Date = 12/12/12 Pct Recovery = 49% Analysis Date = 12/03/12 Pct Recovery = 50% Analysis Date = 12/03/12 Pct Recovery = 50% Analysis Date = 11/24/12 Pct Recovery = 50% Analysis Date = 11/24/12 Pct Recovery = 50% Analysis Date = 11/15/12 Pct Recovery = 50% Analysis Date = 11/15/12 Pct Recovery = 50% Analysis Date = 11/06/12 Pct Recovery = 51% Analysis Date = 11/06/12 Pct Recovery = 51% Analysis Date = 10/28/12 Pct Recovery = 51% Analysis Date = 10/28/12 Pct Recovery = 51% Analysis Date = 10/19/12 Pct Recovery = 52% Analysis Date = 10/19/12 Pct Recovery = 52% Analysis Date = 10/10/12 Pct Recovery = 52% Analysis Date = 10/10/12 Pct Recovery = 52% Analysis Date = 10/01/12 Pct Recovery = 52% Analysis Date = 10/01/12 Pct Recovery = 52% Analysis Date = 09/22/12 Pct Recovery = 53% Analysis Date = 09/22/12 Pct Recovery = 53% Analysis Date = 09/13/12 Pct Recovery = 53% Analysis Date = 09/13/12 Pct Recovery = 53% Analysis Date = 09/04/12 Pct Recovery = 53% Analysis Date = 09/04/12 Pct Recovery = 53% Analysis Date = 08/26/12 Pct Recovery = 54% Analysis Date = 08/26/12 Pct Recovery = 54% Analysis Date = 08/17/12 Pct Recovery = 54% Analysis Date = 08/17/12 Pct Recovery = 54% Analysis Date = 08/08/12 Pct Recovery = 55% Analysis Date = 08/08/12 Pct Recovery = 55% Analysis Date = 07/30/12 Pct Recovery = 55% Analysis Date = 07/30/12 Pct Recovery = 55% Analysis Date = 07/21/12 Pct Recovery = 55% Analysis Date = 07/21/12 Pct Recovery = 55% Analysis Date = 07/12/12 Pct Recovery = 56% Analysis Date = 07/12/12 Pct Recovery = 56% Analysis Date = 07/03/12 Pct Recovery = 56% Analysis Date = 07/03/12 Pct Recovery = 56% Analysis Date = 06/24/12 Pct Recovery = 56% Analysis Date = 06/24/12 Pct Recovery = 56% Analysis Date = 06/15/12 Pct Recovery = 57% Analysis Date = 06/15/12 Pct Recovery = 57% Analysis Date = 06/06/12 Pct Recovery = 57% Analysis Date = 06/06/12 Pct Recovery = 57% Analysis Date = 05/28/12 Pct Recovery = 58% Analysis Date = 05/28/12 Pct Recovery = 58% Analysis Date = 05/19/12 Pct Recovery = 58% Analysis Date = 05/19/12 Pct Recovery = 58% Analysis Date = 05/10/12 Pct Recovery = 58% Analysis Date = 05/10/12 Pct Recovery = 58% Analysis Date = 05/01/12 Pct Recovery = 59% Analysis Date = 05/01/12 Pct Recovery = 59% Analysis Date = 04/22/12 Pct Recovery = 59% Analysis Date = 04/22/12 Pct Recovery = 59% Analysis Date = 04/13/12 Pct Recovery = 59% Analysis Date = 04/13/12 Pct Recovery = 59% Analysis Date = 04/04/12 Pct Recovery = 60% Analysis Date = 04/04/12 Pct Recovery = 60% Analysis Date = 03/26/12 Pct Recovery = 60% Analysis Date = 03/26/12 Pct Recovery = 60% Analysis Date = 03/17/12 Pct Recovery = 61% Analysis Date = 03/17/12 Pct Recovery = 61% Analysis Date = 03/08/12 Pct Recovery = 61% Analysis Date = 03/08/12 Pct Recovery = 61% Analysis Date = 02/28/12 Pct Recovery = 61% Analysis Date = 02/28/12 Pct Recovery = 61% Analysis Date = 02/19/12 Pct Recovery = 62% Analysis Date = 02/19/12 Pct Recovery = 62% Analysis Date = 02/10/12 Pct Recovery = 62% Analysis Date = 02/10/12 Pct Recovery = 62% Analysis Date = 02/01/12 Pct Recovery = 62% Analysis Date = 02/01/12 Pct Recovery = 62% Analysis Date = 01/23/12 Pct Recovery = 63% Analysis Date = 01/23/12 Pct Recovery = 63% Analysis Date = 01/14/12 Pct Recovery = 63% Analysis Date = 01/14/12 Pct Recovery = 63% Analysis Date = 01/05/12 Pct Recovery = 64% Analysis Date = 01/05/12 Pct Recovery = 64% Analysis Date = 12/27/11 Pct Recovery = 64% Analysis Date = 12/27/11 Pct Recovery = 64% Analysis Date = 12/18/11 Pct Recovery = 64% Analysis Date = 12/18/11 Pct Recovery = 64% Analysis Date = 12/09/11 Pct Recovery = 65% Analysis Date = 12/09/11 Pct Recovery = 65% Analysis Date = 11/30/11 Pct Recovery = 65% Analysis Date = 11/30/11 Pct Recovery = 65% Analysis Date = 11/21/11 Pct Recovery = 66% Analysis Date = 11/21/11 Pct Recovery = 66% Analysis Date = 11/12/11 Pct Recovery = 66% Analysis Date = 11/12/11 Pct Recovery = 66% Analysis Date = 11/03/11 Pct Recovery = 66% Analysis Date = 11/03/11 Pct Recovery = 66% Analysis Date = 10/25/11 Pct Recovery = 67% Analysis Date = 10/25/11 Pct Recovery = 67% Analysis Date = 10/16/11 Pct Recovery = 67% Analysis Date = 10/16/11 Pct Recovery = 67% Analysis Date = 10/07/11 Pct Recovery = 67% Analysis Date = 10/07/11 Pct Recovery = 67% Analysis Date = 09/28/11 Pct Recovery = 68% Analysis Date = 09/28/11 Pct Recovery = 68% Analysis Date = 09/19/11 Pct Recovery = 68% Analysis Date = 09/19/11 Pct Recovery = 68% Analysis Date = 09/10/11 Pct Recovery = 69% Analysis Date = 09/10/11 Pct Recovery = 69% Analysis Date = 09/01/11 Pct Recovery = 69% Analysis Date = 09/01/11 Pct Recovery = 69% Analysis Date = 08/23/11 Pct Recovery = 69% Analysis Date = 08/23/11 Pct Recovery = 69% Analysis Date = 08/14/11 Pct Recovery = 70% Analysis Date = 08/14/11 Pct Recovery = 70% Analysis Date = 08/05/11 Pct Recovery = 70% Analysis Date = 08/05/11 Pct Recovery = 70% Analysis Date = 07/27/11 Pct Recovery = 70% Analysis Date = 07/27/11 Pct Recovery = 70% Analysis Date = 07/18/11 Pct Recovery = 71% Analysis Date = 07/18/11 Pct Recovery = 71% Analysis Date = 07/09/11 Pct Recovery = 71% Analysis Date = 07/09/11 Pct Recovery = 71% Analysis Date = 06/30/11 Pct Recovery = 72% Analysis Date = 06/30/11 Pct Recovery = 72% Analysis Date = 06/21/11 Pct Recovery = 72% Analysis Date = 06/21/11 Pct Recovery = 72% Analysis Date = 06/12/11 Pct Recovery = 72% Analysis Date = 06/12/11 Pct Recovery = 72% Analysis Date = 06/03/11 Pct Recovery = 72% Analysis Date = 06/03/11 Pct Recovery = 72% Analysis Date = 05/25/11 Pct Recovery = 72% Analysis Date = 05/25/11 Pct Recovery = 72% Analysis Date = 05/16/11 Pct Recovery = 73% Analysis Date = 05/16/11 Pct Recovery = 73% Analysis Date = 05/07/11 Pct Recovery = 73% Analysis Date = 05/07/11 Pct Recovery = 73% Analysis Date = 04/28/11 Pct Recovery = 73% Analysis Date = 04/28/11 Pct Recovery = 73% Analysis Date = 04/19/11 Pct Recovery = 75% Analysis Date = 04/19/11 Pct Recovery = 75% Analysis Date = 04/10/11 Pct Recovery = 88% Analysis Date = 04/10/11 Pct Recovery = 88% Analysis Date = 04/01/11 Pct Recovery = 102% Analysis Date = 04/01/11 Pct Recovery = 102% Analysis Date = 03/23/11 Pct Recovery = 116% Analysis Date = 03/23/11 Pct Recovery = 116% Analysis Date = 03/14/11 Pct Recovery = 130% Analysis Date = 03/14/11 Pct Recovery = 130% Analysis Date = 03/05/11 Pct Recovery = 144% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL AMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 144% . 144% 0%
>= Reporting Level 4 39% 39% 41% 49%
Total 5 60% 57% 72% 46%

Sample Statistics
DESULFINYLFIPRONIL AMIDE

Characteristic N % % Basis
Plotted 5 50% Spiked
Estimated Values 5 50% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 10 .  
False Negatives 5 50% 5 out of 10
Not Spiked 159 .  
False Positives 0 0% 0 out of 159

BQS OBSP Determination:
DIAZINON
METHOD: 2033 , TESTIDCODE: 39572GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 88% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 105% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 95% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 92% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 100% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 87% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 98% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 108% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 100% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 97% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 108% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 102% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 92% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 92% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 99% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 92% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 91% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 97% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 87% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 99% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 103% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 108% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 89% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 101% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 118% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 91% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 98% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 98% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 100% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 109% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 113% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 123% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 102% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 72% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 76% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 91% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 121% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 85% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 99% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 88% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 98% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 107% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 83% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 89% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 87% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 112% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 99% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 99% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 108% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 80% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 75% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 77% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 64% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 93% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 93% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 92% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 74% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 81% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 99% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 95% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 111% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 96% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 91% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 102% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 97% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 104% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 111% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 115% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 107% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 111% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 82% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 77% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 92% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 73% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 83% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 93% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 100% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 100% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 108% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 106% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 78% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 103% Analysis Date = 01/18/17 Pct Recovery = 101% Analysis Date = 01/07/17 Pct Recovery = 101% Analysis Date = 01/07/17 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 101% Analysis Date = 12/16/16 Pct Recovery = 100% Analysis Date = 12/16/16 Pct Recovery = 100% Analysis Date = 12/05/16 Pct Recovery = 100% Analysis Date = 12/05/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 100% Analysis Date = 11/14/16 Pct Recovery = 100% Analysis Date = 11/14/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 10/23/16 Pct Recovery = 99% Analysis Date = 10/23/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/20/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 09/10/16 Pct Recovery = 98% Analysis Date = 08/30/16 Pct Recovery = 98% Analysis Date = 08/30/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 97% Analysis Date = 08/08/16 Pct Recovery = 97% Analysis Date = 07/28/16 Pct Recovery = 97% Analysis Date = 07/28/16 Pct Recovery = 97% Analysis Date = 07/17/16 Pct Recovery = 97% Analysis Date = 07/17/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/15/16 Pct Recovery = 96% Analysis Date = 06/15/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/03/16 Pct Recovery = 95% Analysis Date = 05/03/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/11/16 Pct Recovery = 95% Analysis Date = 04/11/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/20/16 Pct Recovery = 94% Analysis Date = 03/20/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 02/28/16 Pct Recovery = 94% Analysis Date = 02/28/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/06/16 Pct Recovery = 94% Analysis Date = 02/06/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 93% Analysis Date = 01/26/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/05/16 Pct Recovery = 93% Analysis Date = 01/05/16 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 12/03/15 Pct Recovery = 92% Analysis Date = 11/22/15 Pct Recovery = 92% Analysis Date = 11/22/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 09/29/15 Pct Recovery = 91% Analysis Date = 09/29/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 91% Analysis Date = 08/06/15 Pct Recovery = 90% Analysis Date = 08/06/15 Pct Recovery = 90% Analysis Date = 07/26/15 Pct Recovery = 90% Analysis Date = 07/26/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/15/15 Pct Recovery = 90% Analysis Date = 07/05/15 Pct Recovery = 90% Analysis Date = 07/05/15 Pct Recovery = 90% Analysis Date = 06/24/15 Pct Recovery = 90% Analysis Date = 06/24/15 Pct Recovery = 90% Analysis Date = 06/13/15 Pct Recovery = 89% Analysis Date = 06/13/15 Pct Recovery = 89% Analysis Date = 06/02/15 Pct Recovery = 89% Analysis Date = 06/02/15 Pct Recovery = 89% Analysis Date = 05/22/15 Pct Recovery = 89% Analysis Date = 05/22/15 Pct Recovery = 89% Analysis Date = 05/11/15 Pct Recovery = 89% Analysis Date = 05/11/15 Pct Recovery = 89% Analysis Date = 05/01/15 Pct Recovery = 89% Analysis Date = 05/01/15 Pct Recovery = 89% Analysis Date = 04/20/15 Pct Recovery = 88% Analysis Date = 04/20/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 03/29/15 Pct Recovery = 88% Analysis Date = 03/29/15 Pct Recovery = 88% Analysis Date = 03/18/15 Pct Recovery = 88% Analysis Date = 03/18/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 02/25/15 Pct Recovery = 88% Analysis Date = 02/25/15 Pct Recovery = 88% Analysis Date = 02/14/15 Pct Recovery = 88% Analysis Date = 02/14/15 Pct Recovery = 88% Analysis Date = 02/03/15 Pct Recovery = 88% Analysis Date = 02/03/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/12/15 Pct Recovery = 88% Analysis Date = 01/12/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 11/30/14 Pct Recovery = 88% Analysis Date = 11/30/14 Pct Recovery = 88% Analysis Date = 11/19/14 Pct Recovery = 88% Analysis Date = 11/19/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 10/29/14 Pct Recovery = 88% Analysis Date = 10/29/14 Pct Recovery = 88% Analysis Date = 10/18/14 Pct Recovery = 88% Analysis Date = 10/18/14 Pct Recovery = 88% Analysis Date = 10/07/14 Pct Recovery = 88% Analysis Date = 10/07/14 Pct Recovery = 88% Analysis Date = 09/26/14 Pct Recovery = 88% Analysis Date = 09/26/14 Pct Recovery = 88% Analysis Date = 09/15/14 Pct Recovery = 88% Analysis Date = 09/15/14 Pct Recovery = 88% Analysis Date = 09/05/14 Pct Recovery = 88% Analysis Date = 09/05/14 Pct Recovery = 88% Analysis Date = 08/25/14 Pct Recovery = 88% Analysis Date = 08/25/14 Pct Recovery = 88% Analysis Date = 08/14/14 Pct Recovery = 89% Analysis Date = 08/14/14 Pct Recovery = 89% Analysis Date = 08/03/14 Pct Recovery = 89% Analysis Date = 08/03/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/12/14 Pct Recovery = 89% Analysis Date = 07/12/14 Pct Recovery = 89% Analysis Date = 07/02/14 Pct Recovery = 90% Analysis Date = 07/02/14 Pct Recovery = 90% Analysis Date = 06/21/14 Pct Recovery = 90% Analysis Date = 06/21/14 Pct Recovery = 90% Analysis Date = 06/10/14 Pct Recovery = 90% Analysis Date = 06/10/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/19/14 Pct Recovery = 91% Analysis Date = 05/19/14 Pct Recovery = 91% Analysis Date = 05/08/14 Pct Recovery = 91% Analysis Date = 05/08/14 Pct Recovery = 91% Analysis Date = 04/28/14 Pct Recovery = 91% Analysis Date = 04/28/14 Pct Recovery = 91% Analysis Date = 04/17/14 Pct Recovery = 91% Analysis Date = 04/17/14 Pct Recovery = 91% Analysis Date = 04/06/14 Pct Recovery = 92% Analysis Date = 04/06/14 Pct Recovery = 92% Analysis Date = 03/26/14 Pct Recovery = 92% Analysis Date = 03/26/14 Pct Recovery = 92% Analysis Date = 03/15/14 Pct Recovery = 92% Analysis Date = 03/15/14 Pct Recovery = 92% Analysis Date = 03/04/14 Pct Recovery = 92% Analysis Date = 03/04/14 Pct Recovery = 92% Analysis Date = 02/22/14 Pct Recovery = 93% Analysis Date = 02/22/14 Pct Recovery = 93% Analysis Date = 02/11/14 Pct Recovery = 93% Analysis Date = 02/11/14 Pct Recovery = 93% Analysis Date = 01/31/14 Pct Recovery = 93% Analysis Date = 01/31/14 Pct Recovery = 93% Analysis Date = 01/20/14 Pct Recovery = 93% Analysis Date = 01/20/14 Pct Recovery = 93% Analysis Date = 01/09/14 Pct Recovery = 94% Analysis Date = 01/09/14 Pct Recovery = 94% Analysis Date = 12/30/13 Pct Recovery = 94% Analysis Date = 12/30/13 Pct Recovery = 94% Analysis Date = 12/19/13 Pct Recovery = 94% Analysis Date = 12/19/13 Pct Recovery = 94% Analysis Date = 12/08/13 Pct Recovery = 95% Analysis Date = 12/08/13 Pct Recovery = 95% Analysis Date = 11/27/13 Pct Recovery = 95% Analysis Date = 11/27/13 Pct Recovery = 95% Analysis Date = 11/16/13 Pct Recovery = 95% Analysis Date = 11/16/13 Pct Recovery = 95% Analysis Date = 11/05/13 Pct Recovery = 95% Analysis Date = 11/05/13 Pct Recovery = 95% Analysis Date = 10/26/13 Pct Recovery = 95% Analysis Date = 10/26/13 Pct Recovery = 95% Analysis Date = 10/15/13 Pct Recovery = 96% Analysis Date = 10/15/13 Pct Recovery = 96% Analysis Date = 10/04/13 Pct Recovery = 96% Analysis Date = 10/04/13 Pct Recovery = 96% Analysis Date = 09/23/13 Pct Recovery = 96% Analysis Date = 09/23/13 Pct Recovery = 96% Analysis Date = 09/12/13 Pct Recovery = 96% Analysis Date = 09/12/13 Pct Recovery = 96% Analysis Date = 09/01/13 Pct Recovery = 96% Analysis Date = 09/01/13 Pct Recovery = 96% Analysis Date = 08/22/13 Pct Recovery = 97% Analysis Date = 08/22/13 Pct Recovery = 97% Analysis Date = 08/11/13 Pct Recovery = 97% Analysis Date = 08/11/13 Pct Recovery = 97% Analysis Date = 07/31/13 Pct Recovery = 97% Analysis Date = 07/31/13 Pct Recovery = 97% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/20/13 Pct Recovery = 97% Analysis Date = 07/09/13 Pct Recovery = 97% Analysis Date = 07/09/13 Pct Recovery = 97% Analysis Date = 06/29/13 Pct Recovery = 97% Analysis Date = 06/29/13 Pct Recovery = 97% Analysis Date = 06/18/13 Pct Recovery = 98% Analysis Date = 06/18/13 Pct Recovery = 98% Analysis Date = 06/07/13 Pct Recovery = 98% Analysis Date = 06/07/13 Pct Recovery = 98% Analysis Date = 05/27/13 Pct Recovery = 98% Analysis Date = 05/27/13 Pct Recovery = 98% Analysis Date = 05/16/13 Pct Recovery = 98% Analysis Date = 05/16/13 Pct Recovery = 98% Analysis Date = 05/05/13 Pct Recovery = 98% Analysis Date = 05/05/13 Pct Recovery = 98% Analysis Date = 04/25/13 Pct Recovery = 98% Analysis Date = 04/25/13 Pct Recovery = 98% Analysis Date = 04/14/13 Pct Recovery = 98% Analysis Date = 04/14/13 Pct Recovery = 98% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 03/23/13 Pct Recovery = 99% Analysis Date = 03/23/13 Pct Recovery = 99% Analysis Date = 03/12/13 Pct Recovery = 99% Analysis Date = 03/12/13 Pct Recovery = 99% Analysis Date = 03/01/13 Pct Recovery = 99% Analysis Date = 03/01/13 Pct Recovery = 99% Analysis Date = 02/19/13 Pct Recovery = 99% Analysis Date = 02/19/13 Pct Recovery = 99% Analysis Date = 02/08/13 Pct Recovery = 99% Analysis Date = 02/08/13 Pct Recovery = 99% Analysis Date = 01/28/13 Pct Recovery = 99% Analysis Date = 01/28/13 Pct Recovery = 99% Analysis Date = 01/17/13 Pct Recovery = 99% Analysis Date = 01/17/13 Pct Recovery = 99% Analysis Date = 01/06/13 Pct Recovery = 99% Analysis Date = 01/06/13 Pct Recovery = 99% Analysis Date = 12/26/12 Pct Recovery = 99% Analysis Date = 12/26/12 Pct Recovery = 99% Analysis Date = 12/16/12 Pct Recovery = 99% Analysis Date = 12/16/12 Pct Recovery = 99% Analysis Date = 12/05/12 Pct Recovery = 99% Analysis Date = 12/05/12 Pct Recovery = 99% Analysis Date = 11/24/12 Pct Recovery = 99% Analysis Date = 11/24/12 Pct Recovery = 99% Analysis Date = 11/13/12 Pct Recovery = 99% Analysis Date = 11/13/12 Pct Recovery = 99% Analysis Date = 11/02/12 Pct Recovery = 99% Analysis Date = 11/02/12 Pct Recovery = 99% Analysis Date = 10/23/12 Pct Recovery = 99% Analysis Date = 10/23/12 Pct Recovery = 99% Analysis Date = 10/12/12 Pct Recovery = 99% Analysis Date = 10/12/12 Pct Recovery = 99% Analysis Date = 10/01/12 Pct Recovery = 99% Analysis Date = 10/01/12 Pct Recovery = 99% Analysis Date = 09/20/12 Pct Recovery = 99% Analysis Date = 09/20/12 Pct Recovery = 99% Analysis Date = 09/09/12 Pct Recovery = 99% Analysis Date = 09/09/12 Pct Recovery = 99% Analysis Date = 08/29/12 Pct Recovery = 99% Analysis Date = 08/29/12 Pct Recovery = 99% Analysis Date = 08/19/12 Pct Recovery = 99% Analysis Date = 08/19/12 Pct Recovery = 99% Analysis Date = 08/08/12 Pct Recovery = 99% Analysis Date = 08/08/12 Pct Recovery = 99% Analysis Date = 07/28/12 Pct Recovery = 99% Analysis Date = 07/28/12 Pct Recovery = 99% Analysis Date = 07/17/12 Pct Recovery = 99% Analysis Date = 07/17/12 Pct Recovery = 99% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 06/25/12 Pct Recovery = 100% Analysis Date = 06/25/12 Pct Recovery = 100% Analysis Date = 06/15/12 Pct Recovery = 100% Analysis Date = 06/15/12 Pct Recovery = 100% Analysis Date = 06/04/12 Pct Recovery = 100% Analysis Date = 06/04/12 Pct Recovery = 100% Analysis Date = 05/24/12 Pct Recovery = 100% Analysis Date = 05/24/12 Pct Recovery = 100% Analysis Date = 05/13/12 Pct Recovery = 100% Analysis Date = 05/13/12 Pct Recovery = 100% Analysis Date = 05/02/12 Pct Recovery = 100% Analysis Date = 05/02/12 Pct Recovery = 100% Analysis Date = 04/22/12 Pct Recovery = 100% Analysis Date = 04/22/12 Pct Recovery = 100% Analysis Date = 04/11/12 Pct Recovery = 100% Analysis Date = 04/11/12 Pct Recovery = 100% Analysis Date = 03/31/12 Pct Recovery = 100% Analysis Date = 03/31/12 Pct Recovery = 100% Analysis Date = 03/20/12 Pct Recovery = 100% Analysis Date = 03/20/12 Pct Recovery = 100% Analysis Date = 03/09/12 Pct Recovery = 100% Analysis Date = 03/09/12 Pct Recovery = 100% Analysis Date = 02/27/12 Pct Recovery = 100% Analysis Date = 02/27/12 Pct Recovery = 100% Analysis Date = 02/17/12 Pct Recovery = 100% Analysis Date = 02/17/12 Pct Recovery = 100% Analysis Date = 02/06/12 Pct Recovery = 100% Analysis Date = 02/06/12 Pct Recovery = 100% Analysis Date = 01/26/12 Pct Recovery = 100% Analysis Date = 01/26/12 Pct Recovery = 100% Analysis Date = 01/15/12 Pct Recovery = 100% Analysis Date = 01/15/12 Pct Recovery = 100% Analysis Date = 01/04/12 Pct Recovery = 100% Analysis Date = 01/04/12 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/14/11 Pct Recovery = 101% Analysis Date = 12/14/11 Pct Recovery = 101% Analysis Date = 12/03/11 Pct Recovery = 101% Analysis Date = 12/03/11 Pct Recovery = 101% Analysis Date = 11/22/11 Pct Recovery = 101% Analysis Date = 11/22/11 Pct Recovery = 101% Analysis Date = 11/11/11 Pct Recovery = 101% Analysis Date = 11/11/11 Pct Recovery = 101% Analysis Date = 10/31/11 Pct Recovery = 101% Analysis Date = 10/31/11 Pct Recovery = 101% Analysis Date = 10/20/11 Pct Recovery = 101% Analysis Date = 10/20/11 Pct Recovery = 101% Analysis Date = 10/10/11 Pct Recovery = 101% Analysis Date = 10/10/11 Pct Recovery = 101% Analysis Date = 09/29/11 Pct Recovery = 101% Analysis Date = 09/29/11 Pct Recovery = 101% Analysis Date = 09/18/11 Pct Recovery = 101% Analysis Date = 09/18/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 08/27/11 Pct Recovery = 101% Analysis Date = 08/27/11 Pct Recovery = 101% Analysis Date = 08/17/11 Pct Recovery = 101% Analysis Date = 08/17/11 Pct Recovery = 101% Analysis Date = 08/06/11 Pct Recovery = 101% Analysis Date = 08/06/11 Pct Recovery = 101% Analysis Date = 07/26/11 Pct Recovery = 101% Analysis Date = 07/26/11 Pct Recovery = 101% Analysis Date = 07/15/11 Pct Recovery = 102% Analysis Date = 07/15/11 Pct Recovery = 102% Analysis Date = 07/04/11 Pct Recovery = 102% Analysis Date = 07/04/11 Pct Recovery = 102% Analysis Date = 06/23/11 Pct Recovery = 102% Analysis Date = 06/23/11 Pct Recovery = 102% Analysis Date = 06/13/11 Pct Recovery = 102% Analysis Date = 06/13/11 Pct Recovery = 102% Analysis Date = 06/02/11 Pct Recovery = 102% Analysis Date = 06/02/11 Pct Recovery = 102% Analysis Date = 05/22/11 Pct Recovery = 102% Analysis Date = 05/22/11 Pct Recovery = 102% Analysis Date = 05/11/11 Pct Recovery = 102% Analysis Date = 05/11/11 Pct Recovery = 102% Analysis Date = 04/30/11 Pct Recovery = 102% Analysis Date = 04/30/11 Pct Recovery = 102% Analysis Date = 04/19/11 Pct Recovery = 102% Analysis Date = 04/19/11 Pct Recovery = 102% Analysis Date = 04/09/11 Pct Recovery = 102% Analysis Date = 04/09/11 Pct Recovery = 102% Analysis Date = 03/29/11 Pct Recovery = 102% Analysis Date = 03/29/11 Pct Recovery = 102% Analysis Date = 03/18/11 Pct Recovery = 102% Analysis Date = 03/18/11 Pct Recovery = 102% Analysis Date = 03/07/11 Pct Recovery = 103% Analysis Date = 03/07/11 Pct Recovery = 103% Analysis Date = 02/24/11 Pct Recovery = 103% Analysis Date = 02/24/11 Pct Recovery = 103% Analysis Date = 02/14/11 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 96 96% 12% 97% 11%
Total 96 96% 12% 97% 11%

Sample Statistics
DIAZINON

Characteristic N % % Basis
Plotted 96 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 96 .  
False Negatives 0 0% 0 out of 96
Not Spiked 73 .  
False Positives 3 4% 3 out of 73

BQS OBSP Determination:
DIAZINON, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61638GCM14
Open Data Set

Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 86% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 69% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 111% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 84% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 83% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 89% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 59% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 79% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 84% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 92% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 51% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 81% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 84% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 62% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 78% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 84% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 70% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 88% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 126% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 88% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 126% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 96% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 98% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 94% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 89% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 92% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 85% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 109% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 100% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 83% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 82% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 82% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 74% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 88% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 112% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 76% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 69% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 74% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 67% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 71% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 96% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 95% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 130% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 121% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 81% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 103% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 111% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 105% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 74% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 102% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 79% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 114% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 155% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 144% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 119% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 152% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 102% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 106% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 144% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 132% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 114% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 164% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 147% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 148% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 140% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 124% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 80% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 81% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 84% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 117% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 97% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 94% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 109% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 132% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 77% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 196% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 156% Analysis Date = 12/20/16 Pct Recovery = 116% Analysis Date = 12/09/16 Pct Recovery = 116% Analysis Date = 12/09/16 Pct Recovery = 116% Analysis Date = 11/28/16 Pct Recovery = 115% Analysis Date = 11/28/16 Pct Recovery = 115% Analysis Date = 11/17/16 Pct Recovery = 115% Analysis Date = 11/17/16 Pct Recovery = 115% Analysis Date = 11/07/16 Pct Recovery = 115% Analysis Date = 11/07/16 Pct Recovery = 115% Analysis Date = 10/27/16 Pct Recovery = 115% Analysis Date = 10/27/16 Pct Recovery = 115% Analysis Date = 10/16/16 Pct Recovery = 115% Analysis Date = 10/16/16 Pct Recovery = 115% Analysis Date = 10/06/16 Pct Recovery = 115% Analysis Date = 10/06/16 Pct Recovery = 115% Analysis Date = 09/25/16 Pct Recovery = 114% Analysis Date = 09/25/16 Pct Recovery = 114% Analysis Date = 09/14/16 Pct Recovery = 114% Analysis Date = 09/14/16 Pct Recovery = 114% Analysis Date = 09/04/16 Pct Recovery = 114% Analysis Date = 09/04/16 Pct Recovery = 114% Analysis Date = 08/24/16 Pct Recovery = 114% Analysis Date = 08/24/16 Pct Recovery = 114% Analysis Date = 08/13/16 Pct Recovery = 114% Analysis Date = 08/13/16 Pct Recovery = 114% Analysis Date = 08/03/16 Pct Recovery = 113% Analysis Date = 08/03/16 Pct Recovery = 113% Analysis Date = 07/23/16 Pct Recovery = 113% Analysis Date = 07/23/16 Pct Recovery = 113% Analysis Date = 07/12/16 Pct Recovery = 113% Analysis Date = 07/12/16 Pct Recovery = 113% Analysis Date = 07/02/16 Pct Recovery = 113% Analysis Date = 07/02/16 Pct Recovery = 113% Analysis Date = 06/21/16 Pct Recovery = 113% Analysis Date = 06/21/16 Pct Recovery = 113% Analysis Date = 06/10/16 Pct Recovery = 113% Analysis Date = 06/10/16 Pct Recovery = 113% Analysis Date = 05/31/16 Pct Recovery = 112% Analysis Date = 05/31/16 Pct Recovery = 112% Analysis Date = 05/20/16 Pct Recovery = 112% Analysis Date = 05/20/16 Pct Recovery = 112% Analysis Date = 05/09/16 Pct Recovery = 112% Analysis Date = 05/09/16 Pct Recovery = 112% Analysis Date = 04/29/16 Pct Recovery = 112% Analysis Date = 04/29/16 Pct Recovery = 112% Analysis Date = 04/18/16 Pct Recovery = 112% Analysis Date = 04/18/16 Pct Recovery = 112% Analysis Date = 04/07/16 Pct Recovery = 111% Analysis Date = 04/07/16 Pct Recovery = 111% Analysis Date = 03/28/16 Pct Recovery = 111% Analysis Date = 03/28/16 Pct Recovery = 111% Analysis Date = 03/17/16 Pct Recovery = 111% Analysis Date = 03/17/16 Pct Recovery = 111% Analysis Date = 03/06/16 Pct Recovery = 111% Analysis Date = 03/06/16 Pct Recovery = 111% Analysis Date = 02/24/16 Pct Recovery = 111% Analysis Date = 02/24/16 Pct Recovery = 111% Analysis Date = 02/14/16 Pct Recovery = 111% Analysis Date = 02/14/16 Pct Recovery = 111% Analysis Date = 02/03/16 Pct Recovery = 110% Analysis Date = 02/03/16 Pct Recovery = 110% Analysis Date = 01/23/16 Pct Recovery = 110% Analysis Date = 01/23/16 Pct Recovery = 110% Analysis Date = 01/13/16 Pct Recovery = 110% Analysis Date = 01/13/16 Pct Recovery = 110% Analysis Date = 01/02/16 Pct Recovery = 110% Analysis Date = 01/02/16 Pct Recovery = 110% Analysis Date = 12/22/15 Pct Recovery = 109% Analysis Date = 12/22/15 Pct Recovery = 109% Analysis Date = 12/12/15 Pct Recovery = 109% Analysis Date = 12/12/15 Pct Recovery = 109% Analysis Date = 12/01/15 Pct Recovery = 109% Analysis Date = 12/01/15 Pct Recovery = 109% Analysis Date = 11/20/15 Pct Recovery = 109% Analysis Date = 11/20/15 Pct Recovery = 109% Analysis Date = 11/10/15 Pct Recovery = 108% Analysis Date = 11/10/15 Pct Recovery = 108% Analysis Date = 10/30/15 Pct Recovery = 108% Analysis Date = 10/30/15 Pct Recovery = 108% Analysis Date = 10/19/15 Pct Recovery = 108% Analysis Date = 10/19/15 Pct Recovery = 108% Analysis Date = 10/09/15 Pct Recovery = 108% Analysis Date = 10/09/15 Pct Recovery = 108% Analysis Date = 09/28/15 Pct Recovery = 108% Analysis Date = 09/28/15 Pct Recovery = 108% Analysis Date = 09/17/15 Pct Recovery = 107% Analysis Date = 09/17/15 Pct Recovery = 107% Analysis Date = 09/07/15 Pct Recovery = 107% Analysis Date = 09/07/15 Pct Recovery = 107% Analysis Date = 08/27/15 Pct Recovery = 107% Analysis Date = 08/27/15 Pct Recovery = 107% Analysis Date = 08/16/15 Pct Recovery = 107% Analysis Date = 08/16/15 Pct Recovery = 107% Analysis Date = 08/06/15 Pct Recovery = 107% Analysis Date = 08/06/15 Pct Recovery = 107% Analysis Date = 07/26/15 Pct Recovery = 107% Analysis Date = 07/26/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/15/15 Pct Recovery = 107% Analysis Date = 07/05/15 Pct Recovery = 107% Analysis Date = 07/05/15 Pct Recovery = 107% Analysis Date = 06/24/15 Pct Recovery = 107% Analysis Date = 06/24/15 Pct Recovery = 107% Analysis Date = 06/13/15 Pct Recovery = 107% Analysis Date = 06/13/15 Pct Recovery = 107% Analysis Date = 06/02/15 Pct Recovery = 106% Analysis Date = 06/02/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 106% Analysis Date = 05/23/15 Pct Recovery = 106% Analysis Date = 05/12/15 Pct Recovery = 106% Analysis Date = 05/12/15 Pct Recovery = 106% Analysis Date = 05/01/15 Pct Recovery = 106% Analysis Date = 05/01/15 Pct Recovery = 106% Analysis Date = 04/21/15 Pct Recovery = 106% Analysis Date = 04/21/15 Pct Recovery = 106% Analysis Date = 04/10/15 Pct Recovery = 106% Analysis Date = 04/10/15 Pct Recovery = 106% Analysis Date = 03/30/15 Pct Recovery = 106% Analysis Date = 03/30/15 Pct Recovery = 106% Analysis Date = 03/20/15 Pct Recovery = 106% Analysis Date = 03/20/15 Pct Recovery = 106% Analysis Date = 03/09/15 Pct Recovery = 106% Analysis Date = 03/09/15 Pct Recovery = 106% Analysis Date = 02/26/15 Pct Recovery = 106% Analysis Date = 02/26/15 Pct Recovery = 106% Analysis Date = 02/16/15 Pct Recovery = 106% Analysis Date = 02/16/15 Pct Recovery = 106% Analysis Date = 02/05/15 Pct Recovery = 106% Analysis Date = 02/05/15 Pct Recovery = 106% Analysis Date = 01/25/15 Pct Recovery = 106% Analysis Date = 01/25/15 Pct Recovery = 106% Analysis Date = 01/15/15 Pct Recovery = 106% Analysis Date = 01/15/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 01/04/15 Pct Recovery = 106% Analysis Date = 12/24/14 Pct Recovery = 106% Analysis Date = 12/24/14 Pct Recovery = 106% Analysis Date = 12/14/14 Pct Recovery = 106% Analysis Date = 12/14/14 Pct Recovery = 106% Analysis Date = 12/03/14 Pct Recovery = 106% Analysis Date = 12/03/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/22/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/12/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 11/01/14 Pct Recovery = 106% Analysis Date = 10/21/14 Pct Recovery = 106% Analysis Date = 10/21/14 Pct Recovery = 106% Analysis Date = 10/11/14 Pct Recovery = 106% Analysis Date = 10/11/14 Pct Recovery = 106% Analysis Date = 09/30/14 Pct Recovery = 106% Analysis Date = 09/30/14 Pct Recovery = 106% Analysis Date = 09/19/14 Pct Recovery = 106% Analysis Date = 09/19/14 Pct Recovery = 106% Analysis Date = 09/08/14 Pct Recovery = 106% Analysis Date = 09/08/14 Pct Recovery = 106% Analysis Date = 08/29/14 Pct Recovery = 106% Analysis Date = 08/29/14 Pct Recovery = 106% Analysis Date = 08/18/14 Pct Recovery = 106% Analysis Date = 08/18/14 Pct Recovery = 106% Analysis Date = 08/07/14 Pct Recovery = 106% Analysis Date = 08/07/14 Pct Recovery = 106% Analysis Date = 07/28/14 Pct Recovery = 106% Analysis Date = 07/28/14 Pct Recovery = 106% Analysis Date = 07/17/14 Pct Recovery = 106% Analysis Date = 07/17/14 Pct Recovery = 106% Analysis Date = 07/06/14 Pct Recovery = 106% Analysis Date = 07/06/14 Pct Recovery = 106% Analysis Date = 06/26/14 Pct Recovery = 106% Analysis Date = 06/26/14 Pct Recovery = 106% Analysis Date = 06/15/14 Pct Recovery = 106% Analysis Date = 06/15/14 Pct Recovery = 106% Analysis Date = 06/04/14 Pct Recovery = 106% Analysis Date = 06/04/14 Pct Recovery = 106% Analysis Date = 05/25/14 Pct Recovery = 105% Analysis Date = 05/25/14 Pct Recovery = 105% Analysis Date = 05/14/14 Pct Recovery = 105% Analysis Date = 05/14/14 Pct Recovery = 105% Analysis Date = 05/03/14 Pct Recovery = 105% Analysis Date = 05/03/14 Pct Recovery = 105% Analysis Date = 04/23/14 Pct Recovery = 105% Analysis Date = 04/23/14 Pct Recovery = 105% Analysis Date = 04/12/14 Pct Recovery = 105% Analysis Date = 04/12/14 Pct Recovery = 105% Analysis Date = 04/01/14 Pct Recovery = 105% Analysis Date = 04/01/14 Pct Recovery = 105% Analysis Date = 03/22/14 Pct Recovery = 105% Analysis Date = 03/22/14 Pct Recovery = 105% Analysis Date = 03/11/14 Pct Recovery = 105% Analysis Date = 03/11/14 Pct Recovery = 105% Analysis Date = 02/28/14 Pct Recovery = 104% Analysis Date = 02/28/14 Pct Recovery = 104% Analysis Date = 02/18/14 Pct Recovery = 104% Analysis Date = 02/18/14 Pct Recovery = 104% Analysis Date = 02/07/14 Pct Recovery = 104% Analysis Date = 02/07/14 Pct Recovery = 104% Analysis Date = 01/27/14 Pct Recovery = 104% Analysis Date = 01/27/14 Pct Recovery = 104% Analysis Date = 01/17/14 Pct Recovery = 104% Analysis Date = 01/17/14 Pct Recovery = 104% Analysis Date = 01/06/14 Pct Recovery = 104% Analysis Date = 01/06/14 Pct Recovery = 104% Analysis Date = 12/26/13 Pct Recovery = 104% Analysis Date = 12/26/13 Pct Recovery = 104% Analysis Date = 12/15/13 Pct Recovery = 104% Analysis Date = 12/15/13 Pct Recovery = 104% Analysis Date = 12/05/13 Pct Recovery = 104% Analysis Date = 12/05/13 Pct Recovery = 104% Analysis Date = 11/24/13 Pct Recovery = 103% Analysis Date = 11/24/13 Pct Recovery = 103% Analysis Date = 11/13/13 Pct Recovery = 103% Analysis Date = 11/13/13 Pct Recovery = 103% Analysis Date = 11/03/13 Pct Recovery = 103% Analysis Date = 11/03/13 Pct Recovery = 103% Analysis Date = 10/23/13 Pct Recovery = 103% Analysis Date = 10/23/13 Pct Recovery = 103% Analysis Date = 10/12/13 Pct Recovery = 103% Analysis Date = 10/12/13 Pct Recovery = 103% Analysis Date = 10/02/13 Pct Recovery = 103% Analysis Date = 10/02/13 Pct Recovery = 103% Analysis Date = 09/21/13 Pct Recovery = 102% Analysis Date = 09/21/13 Pct Recovery = 102% Analysis Date = 09/10/13 Pct Recovery = 102% Analysis Date = 09/10/13 Pct Recovery = 102% Analysis Date = 08/31/13 Pct Recovery = 102% Analysis Date = 08/31/13 Pct Recovery = 102% Analysis Date = 08/20/13 Pct Recovery = 102% Analysis Date = 08/20/13 Pct Recovery = 102% Analysis Date = 08/09/13 Pct Recovery = 102% Analysis Date = 08/09/13 Pct Recovery = 102% Analysis Date = 07/30/13 Pct Recovery = 102% Analysis Date = 07/30/13 Pct Recovery = 102% Analysis Date = 07/19/13 Pct Recovery = 101% Analysis Date = 07/19/13 Pct Recovery = 101% Analysis Date = 07/08/13 Pct Recovery = 101% Analysis Date = 07/08/13 Pct Recovery = 101% Analysis Date = 06/28/13 Pct Recovery = 101% Analysis Date = 06/28/13 Pct Recovery = 101% Analysis Date = 06/17/13 Pct Recovery = 101% Analysis Date = 06/17/13 Pct Recovery = 101% Analysis Date = 06/06/13 Pct Recovery = 101% Analysis Date = 06/06/13 Pct Recovery = 101% Analysis Date = 05/27/13 Pct Recovery = 101% Analysis Date = 05/27/13 Pct Recovery = 101% Analysis Date = 05/16/13 Pct Recovery = 100% Analysis Date = 05/16/13 Pct Recovery = 100% Analysis Date = 05/05/13 Pct Recovery = 100% Analysis Date = 05/05/13 Pct Recovery = 100% Analysis Date = 04/25/13 Pct Recovery = 100% Analysis Date = 04/25/13 Pct Recovery = 100% Analysis Date = 04/14/13 Pct Recovery = 99% Analysis Date = 04/14/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 04/03/13 Pct Recovery = 99% Analysis Date = 03/23/13 Pct Recovery = 99% Analysis Date = 03/23/13 Pct Recovery = 99% Analysis Date = 03/13/13 Pct Recovery = 98% Analysis Date = 03/13/13 Pct Recovery = 98% Analysis Date = 03/02/13 Pct Recovery = 98% Analysis Date = 03/02/13 Pct Recovery = 98% Analysis Date = 02/19/13 Pct Recovery = 98% Analysis Date = 02/19/13 Pct Recovery = 98% Analysis Date = 02/09/13 Pct Recovery = 98% Analysis Date = 02/09/13 Pct Recovery = 98% Analysis Date = 01/29/13 Pct Recovery = 97% Analysis Date = 01/29/13 Pct Recovery = 97% Analysis Date = 01/18/13 Pct Recovery = 97% Analysis Date = 01/18/13 Pct Recovery = 97% Analysis Date = 01/08/13 Pct Recovery = 97% Analysis Date = 01/08/13 Pct Recovery = 97% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 95% Analysis Date = 11/26/12 Pct Recovery = 95% Analysis Date = 11/15/12 Pct Recovery = 95% Analysis Date = 11/15/12 Pct Recovery = 95% Analysis Date = 11/05/12 Pct Recovery = 95% Analysis Date = 11/05/12 Pct Recovery = 95% Analysis Date = 10/25/12 Pct Recovery = 95% Analysis Date = 10/25/12 Pct Recovery = 95% Analysis Date = 10/14/12 Pct Recovery = 94% Analysis Date = 10/14/12 Pct Recovery = 94% Analysis Date = 10/04/12 Pct Recovery = 94% Analysis Date = 10/04/12 Pct Recovery = 94% Analysis Date = 09/23/12 Pct Recovery = 94% Analysis Date = 09/23/12 Pct Recovery = 94% Analysis Date = 09/12/12 Pct Recovery = 93% Analysis Date = 09/12/12 Pct Recovery = 93% Analysis Date = 09/02/12 Pct Recovery = 93% Analysis Date = 09/02/12 Pct Recovery = 93% Analysis Date = 08/22/12 Pct Recovery = 93% Analysis Date = 08/22/12 Pct Recovery = 93% Analysis Date = 08/11/12 Pct Recovery = 92% Analysis Date = 08/11/12 Pct Recovery = 92% Analysis Date = 08/01/12 Pct Recovery = 92% Analysis Date = 08/01/12 Pct Recovery = 92% Analysis Date = 07/21/12 Pct Recovery = 92% Analysis Date = 07/21/12 Pct Recovery = 92% Analysis Date = 07/10/12 Pct Recovery = 91% Analysis Date = 07/10/12 Pct Recovery = 91% Analysis Date = 06/29/12 Pct Recovery = 91% Analysis Date = 06/29/12 Pct Recovery = 91% Analysis Date = 06/19/12 Pct Recovery = 91% Analysis Date = 06/19/12 Pct Recovery = 91% Analysis Date = 06/08/12 Pct Recovery = 91% Analysis Date = 06/08/12 Pct Recovery = 91% Analysis Date = 05/28/12 Pct Recovery = 90% Analysis Date = 05/28/12 Pct Recovery = 90% Analysis Date = 05/18/12 Pct Recovery = 90% Analysis Date = 05/18/12 Pct Recovery = 90% Analysis Date = 05/07/12 Pct Recovery = 90% Analysis Date = 05/07/12 Pct Recovery = 90% Analysis Date = 04/26/12 Pct Recovery = 89% Analysis Date = 04/26/12 Pct Recovery = 89% Analysis Date = 04/16/12 Pct Recovery = 89% Analysis Date = 04/16/12 Pct Recovery = 89% Analysis Date = 04/05/12 Pct Recovery = 89% Analysis Date = 04/05/12 Pct Recovery = 89% Analysis Date = 03/25/12 Pct Recovery = 88% Analysis Date = 03/25/12 Pct Recovery = 88% Analysis Date = 03/15/12 Pct Recovery = 88% Analysis Date = 03/15/12 Pct Recovery = 88% Analysis Date = 03/04/12 Pct Recovery = 88% Analysis Date = 03/04/12 Pct Recovery = 88% Analysis Date = 02/22/12 Pct Recovery = 87% Analysis Date = 02/22/12 Pct Recovery = 87% Analysis Date = 02/12/12 Pct Recovery = 87% Analysis Date = 02/12/12 Pct Recovery = 87% Analysis Date = 02/01/12 Pct Recovery = 87% Analysis Date = 02/01/12 Pct Recovery = 87% Analysis Date = 01/21/12 Pct Recovery = 87% Analysis Date = 01/21/12 Pct Recovery = 87% Analysis Date = 01/11/12 Pct Recovery = 86% Analysis Date = 01/11/12 Pct Recovery = 86% Analysis Date = 12/31/11 Pct Recovery = 86% Analysis Date = 12/31/11 Pct Recovery = 86% Analysis Date = 12/20/11 Pct Recovery = 86% Analysis Date = 12/20/11 Pct Recovery = 86% Analysis Date = 12/10/11 Pct Recovery = 85% Analysis Date = 12/10/11 Pct Recovery = 85% Analysis Date = 11/29/11 Pct Recovery = 85% Analysis Date = 11/29/11 Pct Recovery = 85% Analysis Date = 11/18/11 Pct Recovery = 85% Analysis Date = 11/18/11 Pct Recovery = 85% Analysis Date = 11/08/11 Pct Recovery = 85% Analysis Date = 11/08/11 Pct Recovery = 85% Analysis Date = 10/28/11 Pct Recovery = 84% Analysis Date = 10/28/11 Pct Recovery = 84% Analysis Date = 10/17/11 Pct Recovery = 84% Analysis Date = 10/17/11 Pct Recovery = 84% Analysis Date = 10/06/11 Pct Recovery = 84% Analysis Date = 10/06/11 Pct Recovery = 84% Analysis Date = 09/26/11 Pct Recovery = 84% Analysis Date = 09/26/11 Pct Recovery = 84% Analysis Date = 09/15/11 Pct Recovery = 83% Analysis Date = 09/15/11 Pct Recovery = 83% Analysis Date = 09/04/11 Pct Recovery = 83% Analysis Date = 09/04/11 Pct Recovery = 83% Analysis Date = 08/25/11 Pct Recovery = 83% Analysis Date = 08/25/11 Pct Recovery = 83% Analysis Date = 08/14/11 Pct Recovery = 82% Analysis Date = 08/14/11 Pct Recovery = 82% Analysis Date = 08/03/11 Pct Recovery = 82% Analysis Date = 08/03/11 Pct Recovery = 82% Analysis Date = 07/24/11 Pct Recovery = 82% Analysis Date = 07/24/11 Pct Recovery = 82% Analysis Date = 07/13/11 Pct Recovery = 82% Analysis Date = 07/13/11 Pct Recovery = 82% Analysis Date = 07/02/11 Pct Recovery = 81% Analysis Date = 07/02/11 Pct Recovery = 81% Analysis Date = 06/22/11 Pct Recovery = 81% Analysis Date = 06/22/11 Pct Recovery = 81% Analysis Date = 06/11/11 Pct Recovery = 81% Analysis Date = 06/11/11 Pct Recovery = 81% Analysis Date = 05/31/11 Pct Recovery = 81% Analysis Date = 05/31/11 Pct Recovery = 81% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/10/11 Pct Recovery = 80% Analysis Date = 05/10/11 Pct Recovery = 80% Analysis Date = 04/29/11 Pct Recovery = 80% Analysis Date = 04/29/11 Pct Recovery = 80% Analysis Date = 04/19/11 Pct Recovery = 80% Analysis Date = 04/19/11 Pct Recovery = 80% Analysis Date = 04/08/11 Pct Recovery = 79% Analysis Date = 04/08/11 Pct Recovery = 79% Analysis Date = 03/28/11 Pct Recovery = 79% Analysis Date = 03/28/11 Pct Recovery = 79% Analysis Date = 03/18/11 Pct Recovery = 79% Analysis Date = 03/18/11 Pct Recovery = 79% Analysis Date = 03/07/11 Pct Recovery = 79% Analysis Date = 03/07/11 Pct Recovery = 79% Analysis Date = 02/24/11 Pct Recovery = 78% Analysis Date = 02/24/11 Pct Recovery = 78% Analysis Date = 02/14/11 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON, OXYGEN ANALOG

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 84 99% 27% 92% 24%
Total 84 99% 27% 92% 24%

Sample Statistics
DIAZINON, OXYGEN ANALOG

Characteristic N % % Basis
Plotted 84 97% Spiked
Estimated Values 9 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 87 .  
False Negatives 2 2% 2 out of 87
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
DICHLOROVOS (DICHLORVOS)
METHOD: 2033 , TESTIDCODE: 38775GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 61% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 47% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 48% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 47% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 48% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 45% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 53% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 26% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 52% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 62% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 41% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 64% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 49% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 39% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 65% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 65% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 60% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 48% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 66% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 73% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 54% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 75% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 26% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 37% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 40% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 45% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 43% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 23% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 18% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 65% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 51% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 96% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 69% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 39% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 80% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 47% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 62% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 33% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 46% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 93% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 75% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 68% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 38% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 54% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 44% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 71% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 88% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 88% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 50% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 50% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 75% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 19% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 49% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 33% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 30% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 18% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 33% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 60% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 60% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 56% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 71% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 76% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 84% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 51% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 25% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 40% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 42% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 102% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 79% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 69% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 72% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 96% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 106% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 69% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 75% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 44% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 69% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 69% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 76% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 60% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 41% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 60% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 111% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 77% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 81% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 69% Analysis Date = 12/19/16 Pct Recovery = 32% Analysis Date = 12/09/16 Pct Recovery = 32% Analysis Date = 12/09/16 Pct Recovery = 32% Analysis Date = 11/28/16 Pct Recovery = 32% Analysis Date = 11/28/16 Pct Recovery = 32% Analysis Date = 11/17/16 Pct Recovery = 33% Analysis Date = 11/17/16 Pct Recovery = 33% Analysis Date = 11/07/16 Pct Recovery = 33% Analysis Date = 11/07/16 Pct Recovery = 33% Analysis Date = 10/27/16 Pct Recovery = 33% Analysis Date = 10/27/16 Pct Recovery = 33% Analysis Date = 10/16/16 Pct Recovery = 33% Analysis Date = 10/16/16 Pct Recovery = 33% Analysis Date = 10/06/16 Pct Recovery = 34% Analysis Date = 10/06/16 Pct Recovery = 34% Analysis Date = 09/25/16 Pct Recovery = 34% Analysis Date = 09/25/16 Pct Recovery = 34% Analysis Date = 09/14/16 Pct Recovery = 34% Analysis Date = 09/14/16 Pct Recovery = 34% Analysis Date = 09/03/16 Pct Recovery = 35% Analysis Date = 09/03/16 Pct Recovery = 35% Analysis Date = 08/24/16 Pct Recovery = 35% Analysis Date = 08/24/16 Pct Recovery = 35% Analysis Date = 08/13/16 Pct Recovery = 35% Analysis Date = 08/13/16 Pct Recovery = 35% Analysis Date = 08/02/16 Pct Recovery = 35% Analysis Date = 08/02/16 Pct Recovery = 35% Analysis Date = 07/23/16 Pct Recovery = 36% Analysis Date = 07/23/16 Pct Recovery = 36% Analysis Date = 07/12/16 Pct Recovery = 36% Analysis Date = 07/12/16 Pct Recovery = 36% Analysis Date = 07/01/16 Pct Recovery = 36% Analysis Date = 07/01/16 Pct Recovery = 36% Analysis Date = 06/20/16 Pct Recovery = 36% Analysis Date = 06/20/16 Pct Recovery = 36% Analysis Date = 06/10/16 Pct Recovery = 37% Analysis Date = 06/10/16 Pct Recovery = 37% Analysis Date = 05/30/16 Pct Recovery = 37% Analysis Date = 05/30/16 Pct Recovery = 37% Analysis Date = 05/19/16 Pct Recovery = 37% Analysis Date = 05/19/16 Pct Recovery = 37% Analysis Date = 05/09/16 Pct Recovery = 38% Analysis Date = 05/09/16 Pct Recovery = 38% Analysis Date = 04/28/16 Pct Recovery = 38% Analysis Date = 04/28/16 Pct Recovery = 38% Analysis Date = 04/17/16 Pct Recovery = 38% Analysis Date = 04/17/16 Pct Recovery = 38% Analysis Date = 04/06/16 Pct Recovery = 38% Analysis Date = 04/06/16 Pct Recovery = 38% Analysis Date = 03/27/16 Pct Recovery = 39% Analysis Date = 03/27/16 Pct Recovery = 39% Analysis Date = 03/16/16 Pct Recovery = 39% Analysis Date = 03/16/16 Pct Recovery = 39% Analysis Date = 03/05/16 Pct Recovery = 39% Analysis Date = 03/05/16 Pct Recovery = 39% Analysis Date = 02/24/16 Pct Recovery = 40% Analysis Date = 02/24/16 Pct Recovery = 40% Analysis Date = 02/13/16 Pct Recovery = 40% Analysis Date = 02/13/16 Pct Recovery = 40% Analysis Date = 02/02/16 Pct Recovery = 40% Analysis Date = 02/02/16 Pct Recovery = 40% Analysis Date = 01/22/16 Pct Recovery = 40% Analysis Date = 01/22/16 Pct Recovery = 40% Analysis Date = 01/12/16 Pct Recovery = 41% Analysis Date = 01/12/16 Pct Recovery = 41% Analysis Date = 01/01/16 Pct Recovery = 41% Analysis Date = 01/01/16 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/11/15 Pct Recovery = 41% Analysis Date = 12/11/15 Pct Recovery = 41% Analysis Date = 11/30/15 Pct Recovery = 42% Analysis Date = 11/30/15 Pct Recovery = 42% Analysis Date = 11/19/15 Pct Recovery = 42% Analysis Date = 11/19/15 Pct Recovery = 42% Analysis Date = 11/09/15 Pct Recovery = 42% Analysis Date = 11/09/15 Pct Recovery = 42% Analysis Date = 10/29/15 Pct Recovery = 42% Analysis Date = 10/29/15 Pct Recovery = 42% Analysis Date = 10/18/15 Pct Recovery = 43% Analysis Date = 10/18/15 Pct Recovery = 43% Analysis Date = 10/07/15 Pct Recovery = 43% Analysis Date = 10/07/15 Pct Recovery = 43% Analysis Date = 09/27/15 Pct Recovery = 43% Analysis Date = 09/27/15 Pct Recovery = 43% Analysis Date = 09/16/15 Pct Recovery = 43% Analysis Date = 09/16/15 Pct Recovery = 43% Analysis Date = 09/05/15 Pct Recovery = 44% Analysis Date = 09/05/15 Pct Recovery = 44% Analysis Date = 08/26/15 Pct Recovery = 44% Analysis Date = 08/26/15 Pct Recovery = 44% Analysis Date = 08/15/15 Pct Recovery = 44% Analysis Date = 08/15/15 Pct Recovery = 44% Analysis Date = 08/04/15 Pct Recovery = 44% Analysis Date = 08/04/15 Pct Recovery = 44% Analysis Date = 07/24/15 Pct Recovery = 45% Analysis Date = 07/24/15 Pct Recovery = 45% Analysis Date = 07/14/15 Pct Recovery = 45% Analysis Date = 07/14/15 Pct Recovery = 45% Analysis Date = 07/03/15 Pct Recovery = 45% Analysis Date = 07/03/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 46% Analysis Date = 06/22/15 Pct Recovery = 46% Analysis Date = 06/12/15 Pct Recovery = 46% Analysis Date = 06/12/15 Pct Recovery = 46% Analysis Date = 06/01/15 Pct Recovery = 46% Analysis Date = 06/01/15 Pct Recovery = 46% Analysis Date = 05/21/15 Pct Recovery = 47% Analysis Date = 05/21/15 Pct Recovery = 47% Analysis Date = 05/10/15 Pct Recovery = 47% Analysis Date = 05/10/15 Pct Recovery = 47% Analysis Date = 04/30/15 Pct Recovery = 47% Analysis Date = 04/30/15 Pct Recovery = 47% Analysis Date = 04/19/15 Pct Recovery = 48% Analysis Date = 04/19/15 Pct Recovery = 48% Analysis Date = 04/08/15 Pct Recovery = 48% Analysis Date = 04/08/15 Pct Recovery = 48% Analysis Date = 03/29/15 Pct Recovery = 48% Analysis Date = 03/29/15 Pct Recovery = 48% Analysis Date = 03/18/15 Pct Recovery = 49% Analysis Date = 03/18/15 Pct Recovery = 49% Analysis Date = 03/07/15 Pct Recovery = 49% Analysis Date = 03/07/15 Pct Recovery = 49% Analysis Date = 02/24/15 Pct Recovery = 49% Analysis Date = 02/24/15 Pct Recovery = 49% Analysis Date = 02/14/15 Pct Recovery = 50% Analysis Date = 02/14/15 Pct Recovery = 50% Analysis Date = 02/03/15 Pct Recovery = 50% Analysis Date = 02/03/15 Pct Recovery = 50% Analysis Date = 01/23/15 Pct Recovery = 50% Analysis Date = 01/23/15 Pct Recovery = 50% Analysis Date = 01/13/15 Pct Recovery = 51% Analysis Date = 01/13/15 Pct Recovery = 51% Analysis Date = 01/02/15 Pct Recovery = 51% Analysis Date = 01/02/15 Pct Recovery = 51% Analysis Date = 12/22/14 Pct Recovery = 51% Analysis Date = 12/22/14 Pct Recovery = 51% Analysis Date = 12/12/14 Pct Recovery = 51% Analysis Date = 12/12/14 Pct Recovery = 51% Analysis Date = 12/01/14 Pct Recovery = 52% Analysis Date = 12/01/14 Pct Recovery = 52% Analysis Date = 11/20/14 Pct Recovery = 52% Analysis Date = 11/20/14 Pct Recovery = 52% Analysis Date = 11/09/14 Pct Recovery = 52% Analysis Date = 11/09/14 Pct Recovery = 52% Analysis Date = 10/30/14 Pct Recovery = 53% Analysis Date = 10/30/14 Pct Recovery = 53% Analysis Date = 10/19/14 Pct Recovery = 53% Analysis Date = 10/19/14 Pct Recovery = 53% Analysis Date = 10/08/14 Pct Recovery = 53% Analysis Date = 10/08/14 Pct Recovery = 53% Analysis Date = 09/28/14 Pct Recovery = 54% Analysis Date = 09/28/14 Pct Recovery = 54% Analysis Date = 09/17/14 Pct Recovery = 54% Analysis Date = 09/17/14 Pct Recovery = 54% Analysis Date = 09/06/14 Pct Recovery = 54% Analysis Date = 09/06/14 Pct Recovery = 54% Analysis Date = 08/26/14 Pct Recovery = 55% Analysis Date = 08/26/14 Pct Recovery = 55% Analysis Date = 08/16/14 Pct Recovery = 55% Analysis Date = 08/16/14 Pct Recovery = 55% Analysis Date = 08/05/14 Pct Recovery = 55% Analysis Date = 08/05/14 Pct Recovery = 55% Analysis Date = 07/25/14 Pct Recovery = 56% Analysis Date = 07/25/14 Pct Recovery = 56% Analysis Date = 07/15/14 Pct Recovery = 56% Analysis Date = 07/15/14 Pct Recovery = 56% Analysis Date = 07/04/14 Pct Recovery = 56% Analysis Date = 07/04/14 Pct Recovery = 56% Analysis Date = 06/23/14 Pct Recovery = 57% Analysis Date = 06/23/14 Pct Recovery = 57% Analysis Date = 06/12/14 Pct Recovery = 57% Analysis Date = 06/12/14 Pct Recovery = 57% Analysis Date = 06/02/14 Pct Recovery = 57% Analysis Date = 06/02/14 Pct Recovery = 57% Analysis Date = 05/22/14 Pct Recovery = 57% Analysis Date = 05/22/14 Pct Recovery = 57% Analysis Date = 05/11/14 Pct Recovery = 58% Analysis Date = 05/11/14 Pct Recovery = 58% Analysis Date = 05/01/14 Pct Recovery = 58% Analysis Date = 05/01/14 Pct Recovery = 58% Analysis Date = 04/20/14 Pct Recovery = 58% Analysis Date = 04/20/14 Pct Recovery = 58% Analysis Date = 04/09/14 Pct Recovery = 58% Analysis Date = 04/09/14 Pct Recovery = 58% Analysis Date = 03/29/14 Pct Recovery = 59% Analysis Date = 03/29/14 Pct Recovery = 59% Analysis Date = 03/19/14 Pct Recovery = 59% Analysis Date = 03/19/14 Pct Recovery = 59% Analysis Date = 03/08/14 Pct Recovery = 59% Analysis Date = 03/08/14 Pct Recovery = 59% Analysis Date = 02/25/14 Pct Recovery = 59% Analysis Date = 02/25/14 Pct Recovery = 59% Analysis Date = 02/15/14 Pct Recovery = 59% Analysis Date = 02/15/14 Pct Recovery = 59% Analysis Date = 02/04/14 Pct Recovery = 60% Analysis Date = 02/04/14 Pct Recovery = 60% Analysis Date = 01/24/14 Pct Recovery = 60% Analysis Date = 01/24/14 Pct Recovery = 60% Analysis Date = 01/13/14 Pct Recovery = 60% Analysis Date = 01/13/14 Pct Recovery = 60% Analysis Date = 01/03/14 Pct Recovery = 60% Analysis Date = 01/03/14 Pct Recovery = 60% Analysis Date = 12/23/13 Pct Recovery = 61% Analysis Date = 12/23/13 Pct Recovery = 61% Analysis Date = 12/12/13 Pct Recovery = 61% Analysis Date = 12/12/13 Pct Recovery = 61% Analysis Date = 12/02/13 Pct Recovery = 61% Analysis Date = 12/02/13 Pct Recovery = 61% Analysis Date = 11/21/13 Pct Recovery = 61% Analysis Date = 11/21/13 Pct Recovery = 61% Analysis Date = 11/10/13 Pct Recovery = 62% Analysis Date = 11/10/13 Pct Recovery = 62% Analysis Date = 10/31/13 Pct Recovery = 62% Analysis Date = 10/31/13 Pct Recovery = 62% Analysis Date = 10/20/13 Pct Recovery = 62% Analysis Date = 10/20/13 Pct Recovery = 62% Analysis Date = 10/09/13 Pct Recovery = 62% Analysis Date = 10/09/13 Pct Recovery = 62% Analysis Date = 09/28/13 Pct Recovery = 62% Analysis Date = 09/28/13 Pct Recovery = 62% Analysis Date = 09/18/13 Pct Recovery = 62% Analysis Date = 09/18/13 Pct Recovery = 62% Analysis Date = 09/07/13 Pct Recovery = 63% Analysis Date = 09/07/13 Pct Recovery = 63% Analysis Date = 08/27/13 Pct Recovery = 63% Analysis Date = 08/27/13 Pct Recovery = 63% Analysis Date = 08/17/13 Pct Recovery = 63% Analysis Date = 08/17/13 Pct Recovery = 63% Analysis Date = 08/06/13 Pct Recovery = 63% Analysis Date = 08/06/13 Pct Recovery = 63% Analysis Date = 07/26/13 Pct Recovery = 63% Analysis Date = 07/26/13 Pct Recovery = 63% Analysis Date = 07/15/13 Pct Recovery = 63% Analysis Date = 07/15/13 Pct Recovery = 63% Analysis Date = 07/05/13 Pct Recovery = 64% Analysis Date = 07/05/13 Pct Recovery = 64% Analysis Date = 06/24/13 Pct Recovery = 64% Analysis Date = 06/24/13 Pct Recovery = 64% Analysis Date = 06/13/13 Pct Recovery = 64% Analysis Date = 06/13/13 Pct Recovery = 64% Analysis Date = 06/03/13 Pct Recovery = 64% Analysis Date = 06/03/13 Pct Recovery = 64% Analysis Date = 05/23/13 Pct Recovery = 64% Analysis Date = 05/23/13 Pct Recovery = 64% Analysis Date = 05/12/13 Pct Recovery = 65% Analysis Date = 05/12/13 Pct Recovery = 65% Analysis Date = 05/01/13 Pct Recovery = 65% Analysis Date = 05/01/13 Pct Recovery = 65% Analysis Date = 04/21/13 Pct Recovery = 65% Analysis Date = 04/21/13 Pct Recovery = 65% Analysis Date = 04/10/13 Pct Recovery = 65% Analysis Date = 04/10/13 Pct Recovery = 65% Analysis Date = 03/30/13 Pct Recovery = 65% Analysis Date = 03/30/13 Pct Recovery = 65% Analysis Date = 03/20/13 Pct Recovery = 65% Analysis Date = 03/20/13 Pct Recovery = 65% Analysis Date = 03/09/13 Pct Recovery = 65% Analysis Date = 03/09/13 Pct Recovery = 65% Analysis Date = 02/26/13 Pct Recovery = 65% Analysis Date = 02/26/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 65% Analysis Date = 02/15/13 Pct Recovery = 65% Analysis Date = 02/05/13 Pct Recovery = 65% Analysis Date = 02/05/13 Pct Recovery = 65% Analysis Date = 01/25/13 Pct Recovery = 65% Analysis Date = 01/25/13 Pct Recovery = 65% Analysis Date = 01/14/13 Pct Recovery = 65% Analysis Date = 01/14/13 Pct Recovery = 65% Analysis Date = 01/04/13 Pct Recovery = 65% Analysis Date = 01/04/13 Pct Recovery = 65% Analysis Date = 12/24/12 Pct Recovery = 65% Analysis Date = 12/24/12 Pct Recovery = 65% Analysis Date = 12/13/12 Pct Recovery = 65% Analysis Date = 12/13/12 Pct Recovery = 65% Analysis Date = 12/03/12 Pct Recovery = 65% Analysis Date = 12/03/12 Pct Recovery = 65% Analysis Date = 11/22/12 Pct Recovery = 65% Analysis Date = 11/22/12 Pct Recovery = 65% Analysis Date = 11/11/12 Pct Recovery = 65% Analysis Date = 11/11/12 Pct Recovery = 65% Analysis Date = 10/31/12 Pct Recovery = 65% Analysis Date = 10/31/12 Pct Recovery = 65% Analysis Date = 10/21/12 Pct Recovery = 65% Analysis Date = 10/21/12 Pct Recovery = 65% Analysis Date = 10/10/12 Pct Recovery = 65% Analysis Date = 10/10/12 Pct Recovery = 65% Analysis Date = 09/29/12 Pct Recovery = 65% Analysis Date = 09/29/12 Pct Recovery = 65% Analysis Date = 09/19/12 Pct Recovery = 65% Analysis Date = 09/19/12 Pct Recovery = 65% Analysis Date = 09/08/12 Pct Recovery = 66% Analysis Date = 09/08/12 Pct Recovery = 66% Analysis Date = 08/28/12 Pct Recovery = 66% Analysis Date = 08/28/12 Pct Recovery = 66% Analysis Date = 08/17/12 Pct Recovery = 66% Analysis Date = 08/17/12 Pct Recovery = 66% Analysis Date = 08/07/12 Pct Recovery = 66% Analysis Date = 08/07/12 Pct Recovery = 66% Analysis Date = 07/27/12 Pct Recovery = 66% Analysis Date = 07/27/12 Pct Recovery = 66% Analysis Date = 07/16/12 Pct Recovery = 66% Analysis Date = 07/16/12 Pct Recovery = 66% Analysis Date = 07/06/12 Pct Recovery = 66% Analysis Date = 07/06/12 Pct Recovery = 66% Analysis Date = 06/25/12 Pct Recovery = 66% Analysis Date = 06/25/12 Pct Recovery = 66% Analysis Date = 06/14/12 Pct Recovery = 66% Analysis Date = 06/14/12 Pct Recovery = 66% Analysis Date = 06/03/12 Pct Recovery = 66% Analysis Date = 06/03/12 Pct Recovery = 66% Analysis Date = 05/24/12 Pct Recovery = 67% Analysis Date = 05/24/12 Pct Recovery = 67% Analysis Date = 05/13/12 Pct Recovery = 67% Analysis Date = 05/13/12 Pct Recovery = 67% Analysis Date = 05/02/12 Pct Recovery = 67% Analysis Date = 05/02/12 Pct Recovery = 67% Analysis Date = 04/22/12 Pct Recovery = 67% Analysis Date = 04/22/12 Pct Recovery = 67% Analysis Date = 04/11/12 Pct Recovery = 67% Analysis Date = 04/11/12 Pct Recovery = 67% Analysis Date = 03/31/12 Pct Recovery = 68% Analysis Date = 03/31/12 Pct Recovery = 68% Analysis Date = 03/20/12 Pct Recovery = 68% Analysis Date = 03/20/12 Pct Recovery = 68% Analysis Date = 03/10/12 Pct Recovery = 68% Analysis Date = 03/10/12 Pct Recovery = 68% Analysis Date = 02/28/12 Pct Recovery = 68% Analysis Date = 02/28/12 Pct Recovery = 68% Analysis Date = 02/17/12 Pct Recovery = 68% Analysis Date = 02/17/12 Pct Recovery = 68% Analysis Date = 02/07/12 Pct Recovery = 68% Analysis Date = 02/07/12 Pct Recovery = 68% Analysis Date = 01/27/12 Pct Recovery = 69% Analysis Date = 01/27/12 Pct Recovery = 69% Analysis Date = 01/16/12 Pct Recovery = 69% Analysis Date = 01/16/12 Pct Recovery = 69% Analysis Date = 01/06/12 Pct Recovery = 69% Analysis Date = 01/06/12 Pct Recovery = 69% Analysis Date = 12/26/11 Pct Recovery = 69% Analysis Date = 12/26/11 Pct Recovery = 69% Analysis Date = 12/15/11 Pct Recovery = 69% Analysis Date = 12/15/11 Pct Recovery = 69% Analysis Date = 12/04/11 Pct Recovery = 69% Analysis Date = 12/04/11 Pct Recovery = 69% Analysis Date = 11/24/11 Pct Recovery = 70% Analysis Date = 11/24/11 Pct Recovery = 70% Analysis Date = 11/13/11 Pct Recovery = 70% Analysis Date = 11/13/11 Pct Recovery = 70% Analysis Date = 11/02/11 Pct Recovery = 70% Analysis Date = 11/02/11 Pct Recovery = 70% Analysis Date = 10/23/11 Pct Recovery = 70% Analysis Date = 10/23/11 Pct Recovery = 70% Analysis Date = 10/12/11 Pct Recovery = 70% Analysis Date = 10/12/11 Pct Recovery = 70% Analysis Date = 10/01/11 Pct Recovery = 70% Analysis Date = 10/01/11 Pct Recovery = 70% Analysis Date = 09/20/11 Pct Recovery = 71% Analysis Date = 09/20/11 Pct Recovery = 71% Analysis Date = 09/10/11 Pct Recovery = 71% Analysis Date = 09/10/11 Pct Recovery = 71% Analysis Date = 08/30/11 Pct Recovery = 71% Analysis Date = 08/30/11 Pct Recovery = 71% Analysis Date = 08/19/11 Pct Recovery = 71% Analysis Date = 08/19/11 Pct Recovery = 71% Analysis Date = 08/09/11 Pct Recovery = 71% Analysis Date = 08/09/11 Pct Recovery = 71% Analysis Date = 07/29/11 Pct Recovery = 71% Analysis Date = 07/29/11 Pct Recovery = 71% Analysis Date = 07/18/11 Pct Recovery = 71% Analysis Date = 07/18/11 Pct Recovery = 71% Analysis Date = 07/07/11 Pct Recovery = 72% Analysis Date = 07/07/11 Pct Recovery = 72% Analysis Date = 06/27/11 Pct Recovery = 72% Analysis Date = 06/27/11 Pct Recovery = 72% Analysis Date = 06/16/11 Pct Recovery = 72% Analysis Date = 06/16/11 Pct Recovery = 72% Analysis Date = 06/05/11 Pct Recovery = 72% Analysis Date = 06/05/11 Pct Recovery = 72% Analysis Date = 05/26/11 Pct Recovery = 72% Analysis Date = 05/26/11 Pct Recovery = 72% Analysis Date = 05/15/11 Pct Recovery = 73% Analysis Date = 05/15/11 Pct Recovery = 73% Analysis Date = 05/04/11 Pct Recovery = 73% Analysis Date = 05/04/11 Pct Recovery = 73% Analysis Date = 04/23/11 Pct Recovery = 73% Analysis Date = 04/23/11 Pct Recovery = 73% Analysis Date = 04/13/11 Pct Recovery = 73% Analysis Date = 04/13/11 Pct Recovery = 73% Analysis Date = 04/02/11 Pct Recovery = 73% Analysis Date = 04/02/11 Pct Recovery = 73% Analysis Date = 03/22/11 Pct Recovery = 73% Analysis Date = 03/22/11 Pct Recovery = 73% Analysis Date = 03/12/11 Pct Recovery = 74% Analysis Date = 03/12/11 Pct Recovery = 74% Analysis Date = 03/01/11 Pct Recovery = 74% Analysis Date = 03/01/11 Pct Recovery = 74% Analysis Date = 02/18/11 Pct Recovery = 74% Analysis Date = 02/18/11 Pct Recovery = 74% Analysis Date = 02/08/11 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLOROVOS (DICHLORVOS)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 15 73% 20% 69% 15%
>= Reporting Level 78 55% 19% 54% 18%
Total 93 58% 20% 60% 18%

Sample Statistics
DICHLOROVOS (DICHLORVOS)

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 93 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 1 1% 1 out of 76

BQS OBSP Determination:
DICROTOPHOS
METHOD: 2033 , TESTIDCODE: 38454GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 22% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 26% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 31% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 24% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 19% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 15% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 17% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 18% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 25% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 21% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 2% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 20% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 29% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 31% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 23% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 21% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 36% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 34% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 19% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 39% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 35% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 18% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 29% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 52% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 18% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 26% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 29% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 24% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 24% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 24% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 24% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 14% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 13% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 10% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 9% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 19% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 35% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 40% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 17% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 24% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 14% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 12% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 11% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 10% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 49% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 30% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 23% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 21% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 21% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 32% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 26% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 21% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 26% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 30% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 30% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 28% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 43% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 41% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 45% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 22% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 34% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 52% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 28% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 19% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 26% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 43% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 40% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 33% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 44% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 30% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 26% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 25% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 23% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 42% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 46% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 27% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 23% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 20% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 19% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 24% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 17% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 37% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 40% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 44% Analysis Date = 01/17/17 Pct Recovery = 14% Analysis Date = 01/07/17 Pct Recovery = 14% Analysis Date = 01/07/17 Pct Recovery = 14% Analysis Date = 12/27/16 Pct Recovery = 15% Analysis Date = 12/27/16 Pct Recovery = 15% Analysis Date = 12/16/16 Pct Recovery = 15% Analysis Date = 12/16/16 Pct Recovery = 15% Analysis Date = 12/05/16 Pct Recovery = 15% Analysis Date = 12/05/16 Pct Recovery = 15% Analysis Date = 11/24/16 Pct Recovery = 15% Analysis Date = 11/24/16 Pct Recovery = 15% Analysis Date = 11/13/16 Pct Recovery = 15% Analysis Date = 11/13/16 Pct Recovery = 15% Analysis Date = 11/03/16 Pct Recovery = 15% Analysis Date = 11/03/16 Pct Recovery = 15% Analysis Date = 10/23/16 Pct Recovery = 15% Analysis Date = 10/23/16 Pct Recovery = 15% Analysis Date = 10/12/16 Pct Recovery = 16% Analysis Date = 10/12/16 Pct Recovery = 16% Analysis Date = 10/01/16 Pct Recovery = 16% Analysis Date = 10/01/16 Pct Recovery = 16% Analysis Date = 09/20/16 Pct Recovery = 16% Analysis Date = 09/20/16 Pct Recovery = 16% Analysis Date = 09/09/16 Pct Recovery = 16% Analysis Date = 09/09/16 Pct Recovery = 16% Analysis Date = 08/29/16 Pct Recovery = 16% Analysis Date = 08/29/16 Pct Recovery = 16% Analysis Date = 08/19/16 Pct Recovery = 16% Analysis Date = 08/19/16 Pct Recovery = 16% Analysis Date = 08/08/16 Pct Recovery = 16% Analysis Date = 08/08/16 Pct Recovery = 16% Analysis Date = 07/28/16 Pct Recovery = 17% Analysis Date = 07/28/16 Pct Recovery = 17% Analysis Date = 07/17/16 Pct Recovery = 17% Analysis Date = 07/17/16 Pct Recovery = 17% Analysis Date = 07/06/16 Pct Recovery = 17% Analysis Date = 07/06/16 Pct Recovery = 17% Analysis Date = 06/25/16 Pct Recovery = 17% Analysis Date = 06/25/16 Pct Recovery = 17% Analysis Date = 06/14/16 Pct Recovery = 17% Analysis Date = 06/14/16 Pct Recovery = 17% Analysis Date = 06/04/16 Pct Recovery = 17% Analysis Date = 06/04/16 Pct Recovery = 17% Analysis Date = 05/24/16 Pct Recovery = 17% Analysis Date = 05/24/16 Pct Recovery = 17% Analysis Date = 05/13/16 Pct Recovery = 18% Analysis Date = 05/13/16 Pct Recovery = 18% Analysis Date = 05/02/16 Pct Recovery = 18% Analysis Date = 05/02/16 Pct Recovery = 18% Analysis Date = 04/21/16 Pct Recovery = 18% Analysis Date = 04/21/16 Pct Recovery = 18% Analysis Date = 04/10/16 Pct Recovery = 18% Analysis Date = 04/10/16 Pct Recovery = 18% Analysis Date = 03/31/16 Pct Recovery = 18% Analysis Date = 03/31/16 Pct Recovery = 18% Analysis Date = 03/20/16 Pct Recovery = 18% Analysis Date = 03/20/16 Pct Recovery = 18% Analysis Date = 03/09/16 Pct Recovery = 18% Analysis Date = 03/09/16 Pct Recovery = 18% Analysis Date = 02/27/16 Pct Recovery = 19% Analysis Date = 02/27/16 Pct Recovery = 19% Analysis Date = 02/16/16 Pct Recovery = 19% Analysis Date = 02/16/16 Pct Recovery = 19% Analysis Date = 02/05/16 Pct Recovery = 19% Analysis Date = 02/05/16 Pct Recovery = 19% Analysis Date = 01/25/16 Pct Recovery = 19% Analysis Date = 01/25/16 Pct Recovery = 19% Analysis Date = 01/15/16 Pct Recovery = 19% Analysis Date = 01/15/16 Pct Recovery = 19% Analysis Date = 01/04/16 Pct Recovery = 19% Analysis Date = 01/04/16 Pct Recovery = 19% Analysis Date = 12/24/15 Pct Recovery = 19% Analysis Date = 12/24/15 Pct Recovery = 19% Analysis Date = 12/13/15 Pct Recovery = 19% Analysis Date = 12/13/15 Pct Recovery = 19% Analysis Date = 12/02/15 Pct Recovery = 20% Analysis Date = 12/02/15 Pct Recovery = 20% Analysis Date = 11/21/15 Pct Recovery = 20% Analysis Date = 11/21/15 Pct Recovery = 20% Analysis Date = 11/10/15 Pct Recovery = 20% Analysis Date = 11/10/15 Pct Recovery = 20% Analysis Date = 10/31/15 Pct Recovery = 20% Analysis Date = 10/31/15 Pct Recovery = 20% Analysis Date = 10/20/15 Pct Recovery = 20% Analysis Date = 10/20/15 Pct Recovery = 20% Analysis Date = 10/09/15 Pct Recovery = 20% Analysis Date = 10/09/15 Pct Recovery = 20% Analysis Date = 09/28/15 Pct Recovery = 20% Analysis Date = 09/28/15 Pct Recovery = 20% Analysis Date = 09/17/15 Pct Recovery = 21% Analysis Date = 09/17/15 Pct Recovery = 21% Analysis Date = 09/06/15 Pct Recovery = 21% Analysis Date = 09/06/15 Pct Recovery = 21% Analysis Date = 08/27/15 Pct Recovery = 21% Analysis Date = 08/27/15 Pct Recovery = 21% Analysis Date = 08/16/15 Pct Recovery = 21% Analysis Date = 08/16/15 Pct Recovery = 21% Analysis Date = 08/05/15 Pct Recovery = 21% Analysis Date = 08/05/15 Pct Recovery = 21% Analysis Date = 07/25/15 Pct Recovery = 21% Analysis Date = 07/25/15 Pct Recovery = 21% Analysis Date = 07/14/15 Pct Recovery = 21% Analysis Date = 07/14/15 Pct Recovery = 21% Analysis Date = 07/03/15 Pct Recovery = 21% Analysis Date = 07/03/15 Pct Recovery = 21% Analysis Date = 06/22/15 Pct Recovery = 22% Analysis Date = 06/22/15 Pct Recovery = 22% Analysis Date = 06/12/15 Pct Recovery = 22% Analysis Date = 06/12/15 Pct Recovery = 22% Analysis Date = 06/01/15 Pct Recovery = 22% Analysis Date = 06/01/15 Pct Recovery = 22% Analysis Date = 05/21/15 Pct Recovery = 22% Analysis Date = 05/21/15 Pct Recovery = 22% Analysis Date = 05/10/15 Pct Recovery = 22% Analysis Date = 05/10/15 Pct Recovery = 22% Analysis Date = 04/29/15 Pct Recovery = 22% Analysis Date = 04/29/15 Pct Recovery = 22% Analysis Date = 04/18/15 Pct Recovery = 22% Analysis Date = 04/18/15 Pct Recovery = 22% Analysis Date = 04/07/15 Pct Recovery = 23% Analysis Date = 04/07/15 Pct Recovery = 23% Analysis Date = 03/28/15 Pct Recovery = 23% Analysis Date = 03/28/15 Pct Recovery = 23% Analysis Date = 03/17/15 Pct Recovery = 23% Analysis Date = 03/17/15 Pct Recovery = 23% Analysis Date = 03/06/15 Pct Recovery = 23% Analysis Date = 03/06/15 Pct Recovery = 23% Analysis Date = 02/23/15 Pct Recovery = 23% Analysis Date = 02/23/15 Pct Recovery = 23% Analysis Date = 02/12/15 Pct Recovery = 23% Analysis Date = 02/12/15 Pct Recovery = 23% Analysis Date = 02/01/15 Pct Recovery = 24% Analysis Date = 02/01/15 Pct Recovery = 24% Analysis Date = 01/22/15 Pct Recovery = 24% Analysis Date = 01/22/15 Pct Recovery = 24% Analysis Date = 01/11/15 Pct Recovery = 24% Analysis Date = 01/11/15 Pct Recovery = 24% Analysis Date = 12/31/14 Pct Recovery = 24% Analysis Date = 12/31/14 Pct Recovery = 24% Analysis Date = 12/20/14 Pct Recovery = 24% Analysis Date = 12/20/14 Pct Recovery = 24% Analysis Date = 12/09/14 Pct Recovery = 24% Analysis Date = 12/09/14 Pct Recovery = 24% Analysis Date = 11/28/14 Pct Recovery = 25% Analysis Date = 11/28/14 Pct Recovery = 25% Analysis Date = 11/17/14 Pct Recovery = 25% Analysis Date = 11/17/14 Pct Recovery = 25% Analysis Date = 11/07/14 Pct Recovery = 25% Analysis Date = 11/07/14 Pct Recovery = 25% Analysis Date = 10/27/14 Pct Recovery = 25% Analysis Date = 10/27/14 Pct Recovery = 25% Analysis Date = 10/16/14 Pct Recovery = 25% Analysis Date = 10/16/14 Pct Recovery = 25% Analysis Date = 10/05/14 Pct Recovery = 25% Analysis Date = 10/05/14 Pct Recovery = 25% Analysis Date = 09/24/14 Pct Recovery = 26% Analysis Date = 09/24/14 Pct Recovery = 26% Analysis Date = 09/13/14 Pct Recovery = 26% Analysis Date = 09/13/14 Pct Recovery = 26% Analysis Date = 09/02/14 Pct Recovery = 26% Analysis Date = 09/02/14 Pct Recovery = 26% Analysis Date = 08/23/14 Pct Recovery = 26% Analysis Date = 08/23/14 Pct Recovery = 26% Analysis Date = 08/12/14 Pct Recovery = 26% Analysis Date = 08/12/14 Pct Recovery = 26% Analysis Date = 08/01/14 Pct Recovery = 26% Analysis Date = 08/01/14 Pct Recovery = 26% Analysis Date = 07/21/14 Pct Recovery = 26% Analysis Date = 07/21/14 Pct Recovery = 26% Analysis Date = 07/10/14 Pct Recovery = 26% Analysis Date = 07/10/14 Pct Recovery = 26% Analysis Date = 06/29/14 Pct Recovery = 26% Analysis Date = 06/29/14 Pct Recovery = 26% Analysis Date = 06/19/14 Pct Recovery = 26% Analysis Date = 06/19/14 Pct Recovery = 26% Analysis Date = 06/08/14 Pct Recovery = 26% Analysis Date = 06/08/14 Pct Recovery = 26% Analysis Date = 05/28/14 Pct Recovery = 26% Analysis Date = 05/28/14 Pct Recovery = 26% Analysis Date = 05/17/14 Pct Recovery = 26% Analysis Date = 05/17/14 Pct Recovery = 26% Analysis Date = 05/06/14 Pct Recovery = 26% Analysis Date = 05/06/14 Pct Recovery = 26% Analysis Date = 04/25/14 Pct Recovery = 26% Analysis Date = 04/25/14 Pct Recovery = 26% Analysis Date = 04/14/14 Pct Recovery = 26% Analysis Date = 04/14/14 Pct Recovery = 26% Analysis Date = 04/04/14 Pct Recovery = 26% Analysis Date = 04/04/14 Pct Recovery = 26% Analysis Date = 03/24/14 Pct Recovery = 26% Analysis Date = 03/24/14 Pct Recovery = 26% Analysis Date = 03/13/14 Pct Recovery = 26% Analysis Date = 03/13/14 Pct Recovery = 26% Analysis Date = 03/02/14 Pct Recovery = 26% Analysis Date = 03/02/14 Pct Recovery = 26% Analysis Date = 02/19/14 Pct Recovery = 26% Analysis Date = 02/19/14 Pct Recovery = 26% Analysis Date = 02/08/14 Pct Recovery = 26% Analysis Date = 02/08/14 Pct Recovery = 26% Analysis Date = 01/28/14 Pct Recovery = 26% Analysis Date = 01/28/14 Pct Recovery = 26% Analysis Date = 01/18/14 Pct Recovery = 26% Analysis Date = 01/18/14 Pct Recovery = 26% Analysis Date = 01/07/14 Pct Recovery = 26% Analysis Date = 01/07/14 Pct Recovery = 26% Analysis Date = 12/27/13 Pct Recovery = 26% Analysis Date = 12/27/13 Pct Recovery = 26% Analysis Date = 12/16/13 Pct Recovery = 26% Analysis Date = 12/16/13 Pct Recovery = 26% Analysis Date = 12/05/13 Pct Recovery = 26% Analysis Date = 12/05/13 Pct Recovery = 26% Analysis Date = 11/24/13 Pct Recovery = 26% Analysis Date = 11/24/13 Pct Recovery = 26% Analysis Date = 11/14/13 Pct Recovery = 26% Analysis Date = 11/14/13 Pct Recovery = 26% Analysis Date = 11/03/13 Pct Recovery = 26% Analysis Date = 11/03/13 Pct Recovery = 26% Analysis Date = 10/23/13 Pct Recovery = 26% Analysis Date = 10/23/13 Pct Recovery = 26% Analysis Date = 10/12/13 Pct Recovery = 26% Analysis Date = 10/12/13 Pct Recovery = 26% Analysis Date = 10/01/13 Pct Recovery = 26% Analysis Date = 10/01/13 Pct Recovery = 26% Analysis Date = 09/20/13 Pct Recovery = 26% Analysis Date = 09/20/13 Pct Recovery = 26% Analysis Date = 09/09/13 Pct Recovery = 26% Analysis Date = 09/09/13 Pct Recovery = 26% Analysis Date = 08/30/13 Pct Recovery = 26% Analysis Date = 08/30/13 Pct Recovery = 26% Analysis Date = 08/19/13 Pct Recovery = 26% Analysis Date = 08/19/13 Pct Recovery = 26% Analysis Date = 08/08/13 Pct Recovery = 26% Analysis Date = 08/08/13 Pct Recovery = 26% Analysis Date = 07/28/13 Pct Recovery = 26% Analysis Date = 07/28/13 Pct Recovery = 26% Analysis Date = 07/17/13 Pct Recovery = 26% Analysis Date = 07/17/13 Pct Recovery = 26% Analysis Date = 07/06/13 Pct Recovery = 26% Analysis Date = 07/06/13 Pct Recovery = 26% Analysis Date = 06/25/13 Pct Recovery = 26% Analysis Date = 06/25/13 Pct Recovery = 26% Analysis Date = 06/15/13 Pct Recovery = 26% Analysis Date = 06/15/13 Pct Recovery = 26% Analysis Date = 06/04/13 Pct Recovery = 26% Analysis Date = 06/04/13 Pct Recovery = 26% Analysis Date = 05/24/13 Pct Recovery = 26% Analysis Date = 05/24/13 Pct Recovery = 26% Analysis Date = 05/13/13 Pct Recovery = 26% Analysis Date = 05/13/13 Pct Recovery = 26% Analysis Date = 05/02/13 Pct Recovery = 26% Analysis Date = 05/02/13 Pct Recovery = 26% Analysis Date = 04/21/13 Pct Recovery = 26% Analysis Date = 04/21/13 Pct Recovery = 26% Analysis Date = 04/11/13 Pct Recovery = 26% Analysis Date = 04/11/13 Pct Recovery = 26% Analysis Date = 03/31/13 Pct Recovery = 26% Analysis Date = 03/31/13 Pct Recovery = 26% Analysis Date = 03/20/13 Pct Recovery = 26% Analysis Date = 03/20/13 Pct Recovery = 26% Analysis Date = 03/09/13 Pct Recovery = 26% Analysis Date = 03/09/13 Pct Recovery = 26% Analysis Date = 02/26/13 Pct Recovery = 26% Analysis Date = 02/26/13 Pct Recovery = 26% Analysis Date = 02/15/13 Pct Recovery = 26% Analysis Date = 02/15/13 Pct Recovery = 26% Analysis Date = 02/04/13 Pct Recovery = 26% Analysis Date = 02/04/13 Pct Recovery = 26% Analysis Date = 01/25/13 Pct Recovery = 26% Analysis Date = 01/25/13 Pct Recovery = 26% Analysis Date = 01/14/13 Pct Recovery = 26% Analysis Date = 01/14/13 Pct Recovery = 26% Analysis Date = 01/03/13 Pct Recovery = 26% Analysis Date = 01/03/13 Pct Recovery = 26% Analysis Date = 12/23/12 Pct Recovery = 26% Analysis Date = 12/23/12 Pct Recovery = 26% Analysis Date = 12/12/12 Pct Recovery = 26% Analysis Date = 12/12/12 Pct Recovery = 26% Analysis Date = 12/01/12 Pct Recovery = 26% Analysis Date = 12/01/12 Pct Recovery = 26% Analysis Date = 11/20/12 Pct Recovery = 26% Analysis Date = 11/20/12 Pct Recovery = 26% Analysis Date = 11/10/12 Pct Recovery = 26% Analysis Date = 11/10/12 Pct Recovery = 26% Analysis Date = 10/30/12 Pct Recovery = 26% Analysis Date = 10/30/12 Pct Recovery = 26% Analysis Date = 10/19/12 Pct Recovery = 27% Analysis Date = 10/19/12 Pct Recovery = 27% Analysis Date = 10/08/12 Pct Recovery = 27% Analysis Date = 10/08/12 Pct Recovery = 27% Analysis Date = 09/27/12 Pct Recovery = 27% Analysis Date = 09/27/12 Pct Recovery = 27% Analysis Date = 09/16/12 Pct Recovery = 27% Analysis Date = 09/16/12 Pct Recovery = 27% Analysis Date = 09/06/12 Pct Recovery = 27% Analysis Date = 09/06/12 Pct Recovery = 27% Analysis Date = 08/26/12 Pct Recovery = 27% Analysis Date = 08/26/12 Pct Recovery = 27% Analysis Date = 08/15/12 Pct Recovery = 27% Analysis Date = 08/15/12 Pct Recovery = 27% Analysis Date = 08/04/12 Pct Recovery = 28% Analysis Date = 08/04/12 Pct Recovery = 28% Analysis Date = 07/24/12 Pct Recovery = 28% Analysis Date = 07/24/12 Pct Recovery = 28% Analysis Date = 07/13/12 Pct Recovery = 28% Analysis Date = 07/13/12 Pct Recovery = 28% Analysis Date = 07/02/12 Pct Recovery = 28% Analysis Date = 07/02/12 Pct Recovery = 28% Analysis Date = 06/22/12 Pct Recovery = 29% Analysis Date = 06/22/12 Pct Recovery = 29% Analysis Date = 06/11/12 Pct Recovery = 29% Analysis Date = 06/11/12 Pct Recovery = 29% Analysis Date = 05/31/12 Pct Recovery = 29% Analysis Date = 05/31/12 Pct Recovery = 29% Analysis Date = 05/20/12 Pct Recovery = 29% Analysis Date = 05/20/12 Pct Recovery = 29% Analysis Date = 05/09/12 Pct Recovery = 29% Analysis Date = 05/09/12 Pct Recovery = 29% Analysis Date = 04/28/12 Pct Recovery = 30% Analysis Date = 04/28/12 Pct Recovery = 30% Analysis Date = 04/17/12 Pct Recovery = 30% Analysis Date = 04/17/12 Pct Recovery = 30% Analysis Date = 04/07/12 Pct Recovery = 30% Analysis Date = 04/07/12 Pct Recovery = 30% Analysis Date = 03/27/12 Pct Recovery = 30% Analysis Date = 03/27/12 Pct Recovery = 30% Analysis Date = 03/16/12 Pct Recovery = 31% Analysis Date = 03/16/12 Pct Recovery = 31% Analysis Date = 03/05/12 Pct Recovery = 31% Analysis Date = 03/05/12 Pct Recovery = 31% Analysis Date = 02/23/12 Pct Recovery = 31% Analysis Date = 02/23/12 Pct Recovery = 31% Analysis Date = 02/12/12 Pct Recovery = 31% Analysis Date = 02/12/12 Pct Recovery = 31% Analysis Date = 02/02/12 Pct Recovery = 32% Analysis Date = 02/02/12 Pct Recovery = 32% Analysis Date = 01/22/12 Pct Recovery = 32% Analysis Date = 01/22/12 Pct Recovery = 32% Analysis Date = 01/11/12 Pct Recovery = 32% Analysis Date = 01/11/12 Pct Recovery = 32% Analysis Date = 12/31/11 Pct Recovery = 32% Analysis Date = 12/31/11 Pct Recovery = 32% Analysis Date = 12/20/11 Pct Recovery = 32% Analysis Date = 12/20/11 Pct Recovery = 32% Analysis Date = 12/09/11 Pct Recovery = 33% Analysis Date = 12/09/11 Pct Recovery = 33% Analysis Date = 11/28/11 Pct Recovery = 33% Analysis Date = 11/28/11 Pct Recovery = 33% Analysis Date = 11/18/11 Pct Recovery = 33% Analysis Date = 11/18/11 Pct Recovery = 33% Analysis Date = 11/07/11 Pct Recovery = 33% Analysis Date = 11/07/11 Pct Recovery = 33% Analysis Date = 10/27/11 Pct Recovery = 34% Analysis Date = 10/27/11 Pct Recovery = 34% Analysis Date = 10/16/11 Pct Recovery = 34% Analysis Date = 10/16/11 Pct Recovery = 34% Analysis Date = 10/05/11 Pct Recovery = 34% Analysis Date = 10/05/11 Pct Recovery = 34% Analysis Date = 09/24/11 Pct Recovery = 34% Analysis Date = 09/24/11 Pct Recovery = 34% Analysis Date = 09/13/11 Pct Recovery = 35% Analysis Date = 09/13/11 Pct Recovery = 35% Analysis Date = 09/03/11 Pct Recovery = 35% Analysis Date = 09/03/11 Pct Recovery = 35% Analysis Date = 08/23/11 Pct Recovery = 35% Analysis Date = 08/23/11 Pct Recovery = 35% Analysis Date = 08/12/11 Pct Recovery = 35% Analysis Date = 08/12/11 Pct Recovery = 35% Analysis Date = 08/01/11 Pct Recovery = 35% Analysis Date = 08/01/11 Pct Recovery = 35% Analysis Date = 07/21/11 Pct Recovery = 36% Analysis Date = 07/21/11 Pct Recovery = 36% Analysis Date = 07/10/11 Pct Recovery = 36% Analysis Date = 07/10/11 Pct Recovery = 36% Analysis Date = 06/30/11 Pct Recovery = 36% Analysis Date = 06/30/11 Pct Recovery = 36% Analysis Date = 06/19/11 Pct Recovery = 36% Analysis Date = 06/19/11 Pct Recovery = 36% Analysis Date = 06/08/11 Pct Recovery = 37% Analysis Date = 06/08/11 Pct Recovery = 37% Analysis Date = 05/28/11 Pct Recovery = 37% Analysis Date = 05/28/11 Pct Recovery = 37% Analysis Date = 05/17/11 Pct Recovery = 37% Analysis Date = 05/17/11 Pct Recovery = 37% Analysis Date = 05/06/11 Pct Recovery = 37% Analysis Date = 05/06/11 Pct Recovery = 37% Analysis Date = 04/25/11 Pct Recovery = 38% Analysis Date = 04/25/11 Pct Recovery = 38% Analysis Date = 04/15/11 Pct Recovery = 38% Analysis Date = 04/15/11 Pct Recovery = 38% Analysis Date = 04/04/11 Pct Recovery = 38% Analysis Date = 04/04/11 Pct Recovery = 38% Analysis Date = 03/24/11 Pct Recovery = 38% Analysis Date = 03/24/11 Pct Recovery = 38% Analysis Date = 03/13/11 Pct Recovery = 39% Analysis Date = 03/13/11 Pct Recovery = 39% Analysis Date = 03/02/11 Pct Recovery = 39% Analysis Date = 03/02/11 Pct Recovery = 39% Analysis Date = 02/19/11 Pct Recovery = 39% Analysis Date = 02/19/11 Pct Recovery = 39% Analysis Date = 02/09/11 Pct Recovery = 39% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICROTOPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 42% 3% 42% 3%
>= Reporting Level 82 26% 10% 25% 9%
Total 84 27% 10% 25% 10%

Sample Statistics
DICROTOPHOS

Characteristic N % % Basis
Plotted 84 97% Spiked
Estimated Values 84 97% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 3 3% 3 out of 87
Not Spiked 74 .  
False Positives 1 1% 1 out of 72

BQS OBSP Determination:
DIELDRIN
METHOD: 2033 , TESTIDCODE: 39381GCM35
Open Data Set

Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 90% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 82% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 95% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 78% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 78% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 94% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 97% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 88% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 94% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 64% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 103% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 78% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 100% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 85% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 101% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 89% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 69% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 78% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 81% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 102% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 82% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 92% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 85% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 79% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 114% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 94% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 83% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 80% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 92% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 106% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 72% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 55% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 100% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 84% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 93% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 88% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 92% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 101% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 111% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 151% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 102% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 85% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 95% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 105% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 94% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 83% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 84% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 85% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 74% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 49% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 81% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 106% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 77% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 87% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 88% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 116% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 95% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 67% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 80% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 108% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 85% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 93% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 121% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 104% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 82% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 78% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 90% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 83% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 91% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 79% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 103% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 60% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 98% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 76% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 87% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 01/18/17 Pct Recovery = 86% Analysis Date = 01/07/17 Pct Recovery = 86% Analysis Date = 01/07/17 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 85% Analysis Date = 12/27/16 Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/16/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/03/16 Pct Recovery = 85% Analysis Date = 11/03/16 Pct Recovery = 85% Analysis Date = 10/23/16 Pct Recovery = 85% Analysis Date = 10/23/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 08/30/16 Pct Recovery = 85% Analysis Date = 08/30/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 07/28/16 Pct Recovery = 85% Analysis Date = 07/28/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 84% Analysis Date = 06/26/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 84% Analysis Date = 05/03/16 Pct Recovery = 84% Analysis Date = 05/03/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 84% Analysis Date = 01/15/16 Pct Recovery = 84% Analysis Date = 01/15/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 01/05/16 Pct Recovery = 84% Analysis Date = 12/25/15 Pct Recovery = 84% Analysis Date = 12/25/15 Pct Recovery = 84% Analysis Date = 12/14/15 Pct Recovery = 84% Analysis Date = 12/14/15 Pct Recovery = 84% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/18/15 Pct Recovery = 83% Analysis Date = 09/18/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 06/24/15 Pct Recovery = 83% Analysis Date = 06/24/15 Pct Recovery = 83% Analysis Date = 06/13/15 Pct Recovery = 83% Analysis Date = 06/13/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 83% Analysis Date = 05/22/15 Pct Recovery = 83% Analysis Date = 05/22/15 Pct Recovery = 83% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 04/20/15 Pct Recovery = 82% Analysis Date = 04/20/15 Pct Recovery = 82% Analysis Date = 04/09/15 Pct Recovery = 82% Analysis Date = 04/09/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/18/15 Pct Recovery = 82% Analysis Date = 03/18/15 Pct Recovery = 82% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 03/08/15 Pct Recovery = 83% Analysis Date = 02/25/15 Pct Recovery = 83% Analysis Date = 02/25/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/14/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 02/03/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/23/15 Pct Recovery = 83% Analysis Date = 01/12/15 Pct Recovery = 83% Analysis Date = 01/12/15 Pct Recovery = 83% Analysis Date = 01/02/15 Pct Recovery = 83% Analysis Date = 01/02/15 Pct Recovery = 83% Analysis Date = 12/22/14 Pct Recovery = 84% Analysis Date = 12/22/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 11/30/14 Pct Recovery = 84% Analysis Date = 11/30/14 Pct Recovery = 84% Analysis Date = 11/19/14 Pct Recovery = 84% Analysis Date = 11/19/14 Pct Recovery = 84% Analysis Date = 11/08/14 Pct Recovery = 84% Analysis Date = 11/08/14 Pct Recovery = 84% Analysis Date = 10/29/14 Pct Recovery = 84% Analysis Date = 10/29/14 Pct Recovery = 84% Analysis Date = 10/18/14 Pct Recovery = 84% Analysis Date = 10/18/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 85% Analysis Date = 10/07/14 Pct Recovery = 85% Analysis Date = 09/26/14 Pct Recovery = 85% Analysis Date = 09/26/14 Pct Recovery = 85% Analysis Date = 09/15/14 Pct Recovery = 85% Analysis Date = 09/15/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 08/25/14 Pct Recovery = 85% Analysis Date = 08/25/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/03/14 Pct Recovery = 85% Analysis Date = 08/03/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/19/14 Pct Recovery = 86% Analysis Date = 05/19/14 Pct Recovery = 86% Analysis Date = 05/08/14 Pct Recovery = 86% Analysis Date = 05/08/14 Pct Recovery = 86% Analysis Date = 04/28/14 Pct Recovery = 86% Analysis Date = 04/28/14 Pct Recovery = 86% Analysis Date = 04/17/14 Pct Recovery = 86% Analysis Date = 04/17/14 Pct Recovery = 86% Analysis Date = 04/06/14 Pct Recovery = 86% Analysis Date = 04/06/14 Pct Recovery = 86% Analysis Date = 03/26/14 Pct Recovery = 86% Analysis Date = 03/26/14 Pct Recovery = 86% Analysis Date = 03/15/14 Pct Recovery = 86% Analysis Date = 03/15/14 Pct Recovery = 86% Analysis Date = 03/04/14 Pct Recovery = 86% Analysis Date = 03/04/14 Pct Recovery = 86% Analysis Date = 02/22/14 Pct Recovery = 86% Analysis Date = 02/22/14 Pct Recovery = 86% Analysis Date = 02/11/14 Pct Recovery = 86% Analysis Date = 02/11/14 Pct Recovery = 86% Analysis Date = 01/31/14 Pct Recovery = 86% Analysis Date = 01/31/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/20/14 Pct Recovery = 86% Analysis Date = 01/09/14 Pct Recovery = 86% Analysis Date = 01/09/14 Pct Recovery = 86% Analysis Date = 12/30/13 Pct Recovery = 86% Analysis Date = 12/30/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/19/13 Pct Recovery = 86% Analysis Date = 12/08/13 Pct Recovery = 86% Analysis Date = 12/08/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/16/13 Pct Recovery = 86% Analysis Date = 11/16/13 Pct Recovery = 86% Analysis Date = 11/05/13 Pct Recovery = 86% Analysis Date = 11/05/13 Pct Recovery = 86% Analysis Date = 10/26/13 Pct Recovery = 86% Analysis Date = 10/26/13 Pct Recovery = 86% Analysis Date = 10/15/13 Pct Recovery = 86% Analysis Date = 10/15/13 Pct Recovery = 86% Analysis Date = 10/04/13 Pct Recovery = 86% Analysis Date = 10/04/13 Pct Recovery = 86% Analysis Date = 09/23/13 Pct Recovery = 86% Analysis Date = 09/23/13 Pct Recovery = 86% Analysis Date = 09/12/13 Pct Recovery = 86% Analysis Date = 09/12/13 Pct Recovery = 86% Analysis Date = 09/01/13 Pct Recovery = 86% Analysis Date = 09/01/13 Pct Recovery = 86% Analysis Date = 08/22/13 Pct Recovery = 87% Analysis Date = 08/22/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 87% Analysis Date = 08/11/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/31/13 Pct Recovery = 87% Analysis Date = 07/20/13 Pct Recovery = 87% Analysis Date = 07/20/13 Pct Recovery = 87% Analysis Date = 07/09/13 Pct Recovery = 87% Analysis Date = 07/09/13 Pct Recovery = 87% Analysis Date = 06/29/13 Pct Recovery = 87% Analysis Date = 06/29/13 Pct Recovery = 87% Analysis Date = 06/18/13 Pct Recovery = 87% Analysis Date = 06/18/13 Pct Recovery = 87% Analysis Date = 06/07/13 Pct Recovery = 87% Analysis Date = 06/07/13 Pct Recovery = 87% Analysis Date = 05/27/13 Pct Recovery = 87% Analysis Date = 05/27/13 Pct Recovery = 87% Analysis Date = 05/16/13 Pct Recovery = 87% Analysis Date = 05/16/13 Pct Recovery = 87% Analysis Date = 05/05/13 Pct Recovery = 87% Analysis Date = 05/05/13 Pct Recovery = 87% Analysis Date = 04/25/13 Pct Recovery = 87% Analysis Date = 04/25/13 Pct Recovery = 87% Analysis Date = 04/14/13 Pct Recovery = 87% Analysis Date = 04/14/13 Pct Recovery = 87% Analysis Date = 04/03/13 Pct Recovery = 87% Analysis Date = 04/03/13 Pct Recovery = 87% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/01/13 Pct Recovery = 88% Analysis Date = 03/01/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 89% Analysis Date = 10/23/12 Pct Recovery = 89% Analysis Date = 10/12/12 Pct Recovery = 89% Analysis Date = 10/12/12 Pct Recovery = 89% Analysis Date = 10/01/12 Pct Recovery = 89% Analysis Date = 10/01/12 Pct Recovery = 89% Analysis Date = 09/20/12 Pct Recovery = 89% Analysis Date = 09/20/12 Pct Recovery = 89% Analysis Date = 09/09/12 Pct Recovery = 89% Analysis Date = 09/09/12 Pct Recovery = 89% Analysis Date = 08/29/12 Pct Recovery = 89% Analysis Date = 08/29/12 Pct Recovery = 89% Analysis Date = 08/19/12 Pct Recovery = 89% Analysis Date = 08/19/12 Pct Recovery = 89% Analysis Date = 08/08/12 Pct Recovery = 90% Analysis Date = 08/08/12 Pct Recovery = 90% Analysis Date = 07/28/12 Pct Recovery = 90% Analysis Date = 07/28/12 Pct Recovery = 90% Analysis Date = 07/17/12 Pct Recovery = 90% Analysis Date = 07/17/12 Pct Recovery = 90% Analysis Date = 07/06/12 Pct Recovery = 90% Analysis Date = 07/06/12 Pct Recovery = 90% Analysis Date = 06/25/12 Pct Recovery = 90% Analysis Date = 06/25/12 Pct Recovery = 90% Analysis Date = 06/15/12 Pct Recovery = 90% Analysis Date = 06/15/12 Pct Recovery = 90% Analysis Date = 06/04/12 Pct Recovery = 90% Analysis Date = 06/04/12 Pct Recovery = 90% Analysis Date = 05/24/12 Pct Recovery = 91% Analysis Date = 05/24/12 Pct Recovery = 91% Analysis Date = 05/13/12 Pct Recovery = 91% Analysis Date = 05/13/12 Pct Recovery = 91% Analysis Date = 05/02/12 Pct Recovery = 91% Analysis Date = 05/02/12 Pct Recovery = 91% Analysis Date = 04/22/12 Pct Recovery = 91% Analysis Date = 04/22/12 Pct Recovery = 91% Analysis Date = 04/11/12 Pct Recovery = 91% Analysis Date = 04/11/12 Pct Recovery = 91% Analysis Date = 03/31/12 Pct Recovery = 91% Analysis Date = 03/31/12 Pct Recovery = 91% Analysis Date = 03/20/12 Pct Recovery = 92% Analysis Date = 03/20/12 Pct Recovery = 92% Analysis Date = 03/09/12 Pct Recovery = 92% Analysis Date = 03/09/12 Pct Recovery = 92% Analysis Date = 02/27/12 Pct Recovery = 92% Analysis Date = 02/27/12 Pct Recovery = 92% Analysis Date = 02/17/12 Pct Recovery = 92% Analysis Date = 02/17/12 Pct Recovery = 92% Analysis Date = 02/06/12 Pct Recovery = 92% Analysis Date = 02/06/12 Pct Recovery = 92% Analysis Date = 01/26/12 Pct Recovery = 92% Analysis Date = 01/26/12 Pct Recovery = 92% Analysis Date = 01/15/12 Pct Recovery = 93% Analysis Date = 01/15/12 Pct Recovery = 93% Analysis Date = 01/04/12 Pct Recovery = 93% Analysis Date = 01/04/12 Pct Recovery = 93% Analysis Date = 12/24/11 Pct Recovery = 93% Analysis Date = 12/24/11 Pct Recovery = 93% Analysis Date = 12/14/11 Pct Recovery = 93% Analysis Date = 12/14/11 Pct Recovery = 93% Analysis Date = 12/03/11 Pct Recovery = 93% Analysis Date = 12/03/11 Pct Recovery = 93% Analysis Date = 11/22/11 Pct Recovery = 93% Analysis Date = 11/22/11 Pct Recovery = 93% Analysis Date = 11/11/11 Pct Recovery = 94% Analysis Date = 11/11/11 Pct Recovery = 94% Analysis Date = 10/31/11 Pct Recovery = 94% Analysis Date = 10/31/11 Pct Recovery = 94% Analysis Date = 10/20/11 Pct Recovery = 94% Analysis Date = 10/20/11 Pct Recovery = 94% Analysis Date = 10/10/11 Pct Recovery = 94% Analysis Date = 10/10/11 Pct Recovery = 94% Analysis Date = 09/29/11 Pct Recovery = 94% Analysis Date = 09/29/11 Pct Recovery = 94% Analysis Date = 09/18/11 Pct Recovery = 95% Analysis Date = 09/18/11 Pct Recovery = 95% Analysis Date = 09/07/11 Pct Recovery = 95% Analysis Date = 09/07/11 Pct Recovery = 95% Analysis Date = 08/27/11 Pct Recovery = 95% Analysis Date = 08/27/11 Pct Recovery = 95% Analysis Date = 08/17/11 Pct Recovery = 95% Analysis Date = 08/17/11 Pct Recovery = 95% Analysis Date = 08/06/11 Pct Recovery = 95% Analysis Date = 08/06/11 Pct Recovery = 95% Analysis Date = 07/26/11 Pct Recovery = 96% Analysis Date = 07/26/11 Pct Recovery = 96% Analysis Date = 07/15/11 Pct Recovery = 96% Analysis Date = 07/15/11 Pct Recovery = 96% Analysis Date = 07/04/11 Pct Recovery = 96% Analysis Date = 07/04/11 Pct Recovery = 96% Analysis Date = 06/23/11 Pct Recovery = 96% Analysis Date = 06/23/11 Pct Recovery = 96% Analysis Date = 06/13/11 Pct Recovery = 96% Analysis Date = 06/13/11 Pct Recovery = 96% Analysis Date = 06/02/11 Pct Recovery = 97% Analysis Date = 06/02/11 Pct Recovery = 97% Analysis Date = 05/22/11 Pct Recovery = 97% Analysis Date = 05/22/11 Pct Recovery = 97% Analysis Date = 05/11/11 Pct Recovery = 97% Analysis Date = 05/11/11 Pct Recovery = 97% Analysis Date = 04/30/11 Pct Recovery = 97% Analysis Date = 04/30/11 Pct Recovery = 97% Analysis Date = 04/19/11 Pct Recovery = 97% Analysis Date = 04/19/11 Pct Recovery = 97% Analysis Date = 04/09/11 Pct Recovery = 98% Analysis Date = 04/09/11 Pct Recovery = 98% Analysis Date = 03/29/11 Pct Recovery = 98% Analysis Date = 03/29/11 Pct Recovery = 98% Analysis Date = 03/18/11 Pct Recovery = 98% Analysis Date = 03/18/11 Pct Recovery = 98% Analysis Date = 03/07/11 Pct Recovery = 98% Analysis Date = 03/07/11 Pct Recovery = 98% Analysis Date = 02/24/11 Pct Recovery = 98% Analysis Date = 02/24/11 Pct Recovery = 98% Analysis Date = 02/14/11 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIELDRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 96 88% 15% 87% 12%
Total 96 88% 15% 87% 12%

Sample Statistics
DIELDRIN

Characteristic N % % Basis
Plotted 96 100% Spiked
Estimated Values 5 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 96 .  
False Negatives 0 0% 0 out of 96
Not Spiked 73 .  
False Positives 1 1% 1 out of 73

BQS OBSP Determination:
DIMETHOATE
METHOD: 2033 , TESTIDCODE: 82662GCM40
Open Data Set

Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 25% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 33% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 27% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 29% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 35% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 38% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 37% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 32% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 36% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 40% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 56% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 28% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 47% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 50% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 56% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 27% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 46% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 34% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 48% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 53% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 47% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 49% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 54% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 55% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 24% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 33% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 49% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 53% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 47% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 66% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 71% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 10% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 33% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 29% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 31% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 42% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 33% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 42% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 35% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 44% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 48% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 39% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 52% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 52% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 69% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 68% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 69% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 42% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 36% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 32% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 32% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 47% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 50% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 57% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 66% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 75% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 61% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 53% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 44% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 54% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 55% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 48% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 72% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 59% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 51% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 42% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 38% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 35% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 38% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 82% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 48% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 37% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 44% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 44% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 49% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 46% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 54% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 43% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 57% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 46% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 36% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 46% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 48% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 38% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 38% Analysis Date = 12/20/16 Pct Recovery = 39% Analysis Date = 12/09/16 Pct Recovery = 39% Analysis Date = 12/09/16 Pct Recovery = 39% Analysis Date = 11/28/16 Pct Recovery = 39% Analysis Date = 11/28/16 Pct Recovery = 39% Analysis Date = 11/17/16 Pct Recovery = 39% Analysis Date = 11/17/16 Pct Recovery = 39% Analysis Date = 11/07/16 Pct Recovery = 39% Analysis Date = 11/07/16 Pct Recovery = 39% Analysis Date = 10/27/16 Pct Recovery = 39% Analysis Date = 10/27/16 Pct Recovery = 39% Analysis Date = 10/16/16 Pct Recovery = 39% Analysis Date = 10/16/16 Pct Recovery = 39% Analysis Date = 10/06/16 Pct Recovery = 39% Analysis Date = 10/06/16 Pct Recovery = 39% Analysis Date = 09/25/16 Pct Recovery = 39% Analysis Date = 09/25/16 Pct Recovery = 39% Analysis Date = 09/14/16 Pct Recovery = 39% Analysis Date = 09/14/16 Pct Recovery = 39% Analysis Date = 09/04/16 Pct Recovery = 39% Analysis Date = 09/04/16 Pct Recovery = 39% Analysis Date = 08/24/16 Pct Recovery = 39% Analysis Date = 08/24/16 Pct Recovery = 39% Analysis Date = 08/13/16 Pct Recovery = 39% Analysis Date = 08/13/16 Pct Recovery = 39% Analysis Date = 08/03/16 Pct Recovery = 39% Analysis Date = 08/03/16 Pct Recovery = 39% Analysis Date = 07/23/16 Pct Recovery = 39% Analysis Date = 07/23/16 Pct Recovery = 39% Analysis Date = 07/12/16 Pct Recovery = 39% Analysis Date = 07/12/16 Pct Recovery = 39% Analysis Date = 07/02/16 Pct Recovery = 39% Analysis Date = 07/02/16 Pct Recovery = 39% Analysis Date = 06/21/16 Pct Recovery = 39% Analysis Date = 06/21/16 Pct Recovery = 39% Analysis Date = 06/10/16 Pct Recovery = 39% Analysis Date = 06/10/16 Pct Recovery = 39% Analysis Date = 05/31/16 Pct Recovery = 39% Analysis Date = 05/31/16 Pct Recovery = 39% Analysis Date = 05/20/16 Pct Recovery = 39% Analysis Date = 05/20/16 Pct Recovery = 39% Analysis Date = 05/09/16 Pct Recovery = 39% Analysis Date = 05/09/16 Pct Recovery = 39% Analysis Date = 04/29/16 Pct Recovery = 39% Analysis Date = 04/29/16 Pct Recovery = 39% Analysis Date = 04/18/16 Pct Recovery = 39% Analysis Date = 04/18/16 Pct Recovery = 39% Analysis Date = 04/07/16 Pct Recovery = 39% Analysis Date = 04/07/16 Pct Recovery = 39% Analysis Date = 03/28/16 Pct Recovery = 39% Analysis Date = 03/28/16 Pct Recovery = 39% Analysis Date = 03/17/16 Pct Recovery = 39% Analysis Date = 03/17/16 Pct Recovery = 39% Analysis Date = 03/06/16 Pct Recovery = 39% Analysis Date = 03/06/16 Pct Recovery = 39% Analysis Date = 02/24/16 Pct Recovery = 39% Analysis Date = 02/24/16 Pct Recovery = 39% Analysis Date = 02/14/16 Pct Recovery = 39% Analysis Date = 02/14/16 Pct Recovery = 39% Analysis Date = 02/03/16 Pct Recovery = 39% Analysis Date = 02/03/16 Pct Recovery = 39% Analysis Date = 01/23/16 Pct Recovery = 39% Analysis Date = 01/23/16 Pct Recovery = 39% Analysis Date = 01/13/16 Pct Recovery = 39% Analysis Date = 01/13/16 Pct Recovery = 39% Analysis Date = 01/02/16 Pct Recovery = 39% Analysis Date = 01/02/16 Pct Recovery = 39% Analysis Date = 12/22/15 Pct Recovery = 39% Analysis Date = 12/22/15 Pct Recovery = 39% Analysis Date = 12/12/15 Pct Recovery = 39% Analysis Date = 12/12/15 Pct Recovery = 39% Analysis Date = 12/01/15 Pct Recovery = 39% Analysis Date = 12/01/15 Pct Recovery = 39% Analysis Date = 11/20/15 Pct Recovery = 39% Analysis Date = 11/20/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 10/30/15 Pct Recovery = 39% Analysis Date = 10/30/15 Pct Recovery = 39% Analysis Date = 10/19/15 Pct Recovery = 39% Analysis Date = 10/19/15 Pct Recovery = 39% Analysis Date = 10/09/15 Pct Recovery = 39% Analysis Date = 10/09/15 Pct Recovery = 39% Analysis Date = 09/28/15 Pct Recovery = 39% Analysis Date = 09/28/15 Pct Recovery = 39% Analysis Date = 09/17/15 Pct Recovery = 39% Analysis Date = 09/17/15 Pct Recovery = 39% Analysis Date = 09/07/15 Pct Recovery = 39% Analysis Date = 09/07/15 Pct Recovery = 39% Analysis Date = 08/27/15 Pct Recovery = 39% Analysis Date = 08/27/15 Pct Recovery = 39% Analysis Date = 08/16/15 Pct Recovery = 39% Analysis Date = 08/16/15 Pct Recovery = 39% Analysis Date = 08/06/15 Pct Recovery = 39% Analysis Date = 08/06/15 Pct Recovery = 39% Analysis Date = 07/26/15 Pct Recovery = 39% Analysis Date = 07/26/15 Pct Recovery = 39% Analysis Date = 07/15/15 Pct Recovery = 39% Analysis Date = 07/15/15 Pct Recovery = 39% Analysis Date = 07/05/15 Pct Recovery = 39% Analysis Date = 07/05/15 Pct Recovery = 39% Analysis Date = 06/24/15 Pct Recovery = 39% Analysis Date = 06/24/15 Pct Recovery = 39% Analysis Date = 06/13/15 Pct Recovery = 39% Analysis Date = 06/13/15 Pct Recovery = 39% Analysis Date = 06/02/15 Pct Recovery = 39% Analysis Date = 06/02/15 Pct Recovery = 39% Analysis Date = 05/23/15 Pct Recovery = 39% Analysis Date = 05/23/15 Pct Recovery = 39% Analysis Date = 05/12/15 Pct Recovery = 39% Analysis Date = 05/12/15 Pct Recovery = 39% Analysis Date = 05/01/15 Pct Recovery = 39% Analysis Date = 05/01/15 Pct Recovery = 39% Analysis Date = 04/21/15 Pct Recovery = 39% Analysis Date = 04/21/15 Pct Recovery = 39% Analysis Date = 04/10/15 Pct Recovery = 39% Analysis Date = 04/10/15 Pct Recovery = 39% Analysis Date = 03/30/15 Pct Recovery = 39% Analysis Date = 03/30/15 Pct Recovery = 39% Analysis Date = 03/20/15 Pct Recovery = 39% Analysis Date = 03/20/15 Pct Recovery = 39% Analysis Date = 03/09/15 Pct Recovery = 39% Analysis Date = 03/09/15 Pct Recovery = 39% Analysis Date = 02/26/15 Pct Recovery = 39% Analysis Date = 02/26/15 Pct Recovery = 39% Analysis Date = 02/16/15 Pct Recovery = 39% Analysis Date = 02/16/15 Pct Recovery = 39% Analysis Date = 02/05/15 Pct Recovery = 40% Analysis Date = 02/05/15 Pct Recovery = 40% Analysis Date = 01/25/15 Pct Recovery = 40% Analysis Date = 01/25/15 Pct Recovery = 40% Analysis Date = 01/15/15 Pct Recovery = 40% Analysis Date = 01/15/15 Pct Recovery = 40% Analysis Date = 01/04/15 Pct Recovery = 40% Analysis Date = 01/04/15 Pct Recovery = 40% Analysis Date = 12/24/14 Pct Recovery = 40% Analysis Date = 12/24/14 Pct Recovery = 40% Analysis Date = 12/14/14 Pct Recovery = 40% Analysis Date = 12/14/14 Pct Recovery = 40% Analysis Date = 12/03/14 Pct Recovery = 40% Analysis Date = 12/03/14 Pct Recovery = 40% Analysis Date = 11/22/14 Pct Recovery = 40% Analysis Date = 11/22/14 Pct Recovery = 40% Analysis Date = 11/12/14 Pct Recovery = 40% Analysis Date = 11/12/14 Pct Recovery = 40% Analysis Date = 11/01/14 Pct Recovery = 40% Analysis Date = 11/01/14 Pct Recovery = 40% Analysis Date = 10/21/14 Pct Recovery = 40% Analysis Date = 10/21/14 Pct Recovery = 40% Analysis Date = 10/11/14 Pct Recovery = 40% Analysis Date = 10/11/14 Pct Recovery = 40% Analysis Date = 09/30/14 Pct Recovery = 40% Analysis Date = 09/30/14 Pct Recovery = 40% Analysis Date = 09/19/14 Pct Recovery = 41% Analysis Date = 09/19/14 Pct Recovery = 41% Analysis Date = 09/08/14 Pct Recovery = 41% Analysis Date = 09/08/14 Pct Recovery = 41% Analysis Date = 08/29/14 Pct Recovery = 41% Analysis Date = 08/29/14 Pct Recovery = 41% Analysis Date = 08/18/14 Pct Recovery = 41% Analysis Date = 08/18/14 Pct Recovery = 41% Analysis Date = 08/07/14 Pct Recovery = 41% Analysis Date = 08/07/14 Pct Recovery = 41% Analysis Date = 07/28/14 Pct Recovery = 41% Analysis Date = 07/28/14 Pct Recovery = 41% Analysis Date = 07/17/14 Pct Recovery = 41% Analysis Date = 07/17/14 Pct Recovery = 41% Analysis Date = 07/06/14 Pct Recovery = 41% Analysis Date = 07/06/14 Pct Recovery = 41% Analysis Date = 06/26/14 Pct Recovery = 41% Analysis Date = 06/26/14 Pct Recovery = 41% Analysis Date = 06/15/14 Pct Recovery = 41% Analysis Date = 06/15/14 Pct Recovery = 41% Analysis Date = 06/04/14 Pct Recovery = 41% Analysis Date = 06/04/14 Pct Recovery = 41% Analysis Date = 05/25/14 Pct Recovery = 41% Analysis Date = 05/25/14 Pct Recovery = 41% Analysis Date = 05/14/14 Pct Recovery = 41% Analysis Date = 05/14/14 Pct Recovery = 41% Analysis Date = 05/03/14 Pct Recovery = 42% Analysis Date = 05/03/14 Pct Recovery = 42% Analysis Date = 04/23/14 Pct Recovery = 42% Analysis Date = 04/23/14 Pct Recovery = 42% Analysis Date = 04/12/14 Pct Recovery = 42% Analysis Date = 04/12/14 Pct Recovery = 42% Analysis Date = 04/01/14 Pct Recovery = 42% Analysis Date = 04/01/14 Pct Recovery = 42% Analysis Date = 03/22/14 Pct Recovery = 42% Analysis Date = 03/22/14 Pct Recovery = 42% Analysis Date = 03/11/14 Pct Recovery = 42% Analysis Date = 03/11/14 Pct Recovery = 42% Analysis Date = 02/28/14 Pct Recovery = 42% Analysis Date = 02/28/14 Pct Recovery = 42% Analysis Date = 02/18/14 Pct Recovery = 42% Analysis Date = 02/18/14 Pct Recovery = 42% Analysis Date = 02/07/14 Pct Recovery = 42% Analysis Date = 02/07/14 Pct Recovery = 42% Analysis Date = 01/27/14 Pct Recovery = 42% Analysis Date = 01/27/14 Pct Recovery = 42% Analysis Date = 01/17/14 Pct Recovery = 42% Analysis Date = 01/17/14 Pct Recovery = 42% Analysis Date = 01/06/14 Pct Recovery = 42% Analysis Date = 01/06/14 Pct Recovery = 42% Analysis Date = 12/26/13 Pct Recovery = 43% Analysis Date = 12/26/13 Pct Recovery = 43% Analysis Date = 12/15/13 Pct Recovery = 43% Analysis Date = 12/15/13 Pct Recovery = 43% Analysis Date = 12/05/13 Pct Recovery = 43% Analysis Date = 12/05/13 Pct Recovery = 43% Analysis Date = 11/24/13 Pct Recovery = 43% Analysis Date = 11/24/13 Pct Recovery = 43% Analysis Date = 11/13/13 Pct Recovery = 43% Analysis Date = 11/13/13 Pct Recovery = 43% Analysis Date = 11/03/13 Pct Recovery = 43% Analysis Date = 11/03/13 Pct Recovery = 43% Analysis Date = 10/23/13 Pct Recovery = 43% Analysis Date = 10/23/13 Pct Recovery = 43% Analysis Date = 10/12/13 Pct Recovery = 43% Analysis Date = 10/12/13 Pct Recovery = 43% Analysis Date = 10/02/13 Pct Recovery = 43% Analysis Date = 10/02/13 Pct Recovery = 43% Analysis Date = 09/21/13 Pct Recovery = 43% Analysis Date = 09/21/13 Pct Recovery = 43% Analysis Date = 09/10/13 Pct Recovery = 44% Analysis Date = 09/10/13 Pct Recovery = 44% Analysis Date = 08/31/13 Pct Recovery = 44% Analysis Date = 08/31/13 Pct Recovery = 44% Analysis Date = 08/20/13 Pct Recovery = 44% Analysis Date = 08/20/13 Pct Recovery = 44% Analysis Date = 08/09/13 Pct Recovery = 44% Analysis Date = 08/09/13 Pct Recovery = 44% Analysis Date = 07/30/13 Pct Recovery = 44% Analysis Date = 07/30/13 Pct Recovery = 44% Analysis Date = 07/19/13 Pct Recovery = 44% Analysis Date = 07/19/13 Pct Recovery = 44% Analysis Date = 07/08/13 Pct Recovery = 44% Analysis Date = 07/08/13 Pct Recovery = 44% Analysis Date = 06/28/13 Pct Recovery = 44% Analysis Date = 06/28/13 Pct Recovery = 44% Analysis Date = 06/17/13 Pct Recovery = 45% Analysis Date = 06/17/13 Pct Recovery = 45% Analysis Date = 06/06/13 Pct Recovery = 45% Analysis Date = 06/06/13 Pct Recovery = 45% Analysis Date = 05/27/13 Pct Recovery = 45% Analysis Date = 05/27/13 Pct Recovery = 45% Analysis Date = 05/16/13 Pct Recovery = 45% Analysis Date = 05/16/13 Pct Recovery = 45% Analysis Date = 05/05/13 Pct Recovery = 45% Analysis Date = 05/05/13 Pct Recovery = 45% Analysis Date = 04/25/13 Pct Recovery = 45% Analysis Date = 04/25/13 Pct Recovery = 45% Analysis Date = 04/14/13 Pct Recovery = 45% Analysis Date = 04/14/13 Pct Recovery = 45% Analysis Date = 04/03/13 Pct Recovery = 46% Analysis Date = 04/03/13 Pct Recovery = 46% Analysis Date = 03/23/13 Pct Recovery = 46% Analysis Date = 03/23/13 Pct Recovery = 46% Analysis Date = 03/13/13 Pct Recovery = 46% Analysis Date = 03/13/13 Pct Recovery = 46% Analysis Date = 03/02/13 Pct Recovery = 46% Analysis Date = 03/02/13 Pct Recovery = 46% Analysis Date = 02/19/13 Pct Recovery = 46% Analysis Date = 02/19/13 Pct Recovery = 46% Analysis Date = 02/09/13 Pct Recovery = 46% Analysis Date = 02/09/13 Pct Recovery = 46% Analysis Date = 01/29/13 Pct Recovery = 46% Analysis Date = 01/29/13 Pct Recovery = 46% Analysis Date = 01/18/13 Pct Recovery = 46% Analysis Date = 01/18/13 Pct Recovery = 46% Analysis Date = 01/08/13 Pct Recovery = 47% Analysis Date = 01/08/13 Pct Recovery = 47% Analysis Date = 12/28/12 Pct Recovery = 47% Analysis Date = 12/28/12 Pct Recovery = 47% Analysis Date = 12/17/12 Pct Recovery = 47% Analysis Date = 12/17/12 Pct Recovery = 47% Analysis Date = 12/07/12 Pct Recovery = 47% Analysis Date = 12/07/12 Pct Recovery = 47% Analysis Date = 11/26/12 Pct Recovery = 47% Analysis Date = 11/26/12 Pct Recovery = 47% Analysis Date = 11/15/12 Pct Recovery = 47% Analysis Date = 11/15/12 Pct Recovery = 47% Analysis Date = 11/05/12 Pct Recovery = 47% Analysis Date = 11/05/12 Pct Recovery = 47% Analysis Date = 10/25/12 Pct Recovery = 47% Analysis Date = 10/25/12 Pct Recovery = 47% Analysis Date = 10/14/12 Pct Recovery = 47% Analysis Date = 10/14/12 Pct Recovery = 47% Analysis Date = 10/04/12 Pct Recovery = 48% Analysis Date = 10/04/12 Pct Recovery = 48% Analysis Date = 09/23/12 Pct Recovery = 48% Analysis Date = 09/23/12 Pct Recovery = 48% Analysis Date = 09/12/12 Pct Recovery = 48% Analysis Date = 09/12/12 Pct Recovery = 48% Analysis Date = 09/02/12 Pct Recovery = 48% Analysis Date = 09/02/12 Pct Recovery = 48% Analysis Date = 08/22/12 Pct Recovery = 48% Analysis Date = 08/22/12 Pct Recovery = 48% Analysis Date = 08/11/12 Pct Recovery = 48% Analysis Date = 08/11/12 Pct Recovery = 48% Analysis Date = 08/01/12 Pct Recovery = 49% Analysis Date = 08/01/12 Pct Recovery = 49% Analysis Date = 07/21/12 Pct Recovery = 49% Analysis Date = 07/21/12 Pct Recovery = 49% Analysis Date = 07/10/12 Pct Recovery = 49% Analysis Date = 07/10/12 Pct Recovery = 49% Analysis Date = 06/29/12 Pct Recovery = 49% Analysis Date = 06/29/12 Pct Recovery = 49% Analysis Date = 06/19/12 Pct Recovery = 49% Analysis Date = 06/19/12 Pct Recovery = 49% Analysis Date = 06/08/12 Pct Recovery = 50% Analysis Date = 06/08/12 Pct Recovery = 50% Analysis Date = 05/28/12 Pct Recovery = 50% Analysis Date = 05/28/12 Pct Recovery = 50% Analysis Date = 05/18/12 Pct Recovery = 50% Analysis Date = 05/18/12 Pct Recovery = 50% Analysis Date = 05/07/12 Pct Recovery = 50% Analysis Date = 05/07/12 Pct Recovery = 50% Analysis Date = 04/26/12 Pct Recovery = 50% Analysis Date = 04/26/12 Pct Recovery = 50% Analysis Date = 04/16/12 Pct Recovery = 51% Analysis Date = 04/16/12 Pct Recovery = 51% Analysis Date = 04/05/12 Pct Recovery = 51% Analysis Date = 04/05/12 Pct Recovery = 51% Analysis Date = 03/25/12 Pct Recovery = 51% Analysis Date = 03/25/12 Pct Recovery = 51% Analysis Date = 03/15/12 Pct Recovery = 51% Analysis Date = 03/15/12 Pct Recovery = 51% Analysis Date = 03/04/12 Pct Recovery = 51% Analysis Date = 03/04/12 Pct Recovery = 51% Analysis Date = 02/22/12 Pct Recovery = 52% Analysis Date = 02/22/12 Pct Recovery = 52% Analysis Date = 02/12/12 Pct Recovery = 52% Analysis Date = 02/12/12 Pct Recovery = 52% Analysis Date = 02/01/12 Pct Recovery = 52% Analysis Date = 02/01/12 Pct Recovery = 52% Analysis Date = 01/21/12 Pct Recovery = 52% Analysis Date = 01/21/12 Pct Recovery = 52% Analysis Date = 01/11/12 Pct Recovery = 53% Analysis Date = 01/11/12 Pct Recovery = 53% Analysis Date = 12/31/11 Pct Recovery = 53% Analysis Date = 12/31/11 Pct Recovery = 53% Analysis Date = 12/20/11 Pct Recovery = 53% Analysis Date = 12/20/11 Pct Recovery = 53% Analysis Date = 12/10/11 Pct Recovery = 53% Analysis Date = 12/10/11 Pct Recovery = 53% Analysis Date = 11/29/11 Pct Recovery = 53% Analysis Date = 11/29/11 Pct Recovery = 53% Analysis Date = 11/18/11 Pct Recovery = 54% Analysis Date = 11/18/11 Pct Recovery = 54% Analysis Date = 11/08/11 Pct Recovery = 54% Analysis Date = 11/08/11 Pct Recovery = 54% Analysis Date = 10/28/11 Pct Recovery = 54% Analysis Date = 10/28/11 Pct Recovery = 54% Analysis Date = 10/17/11 Pct Recovery = 54% Analysis Date = 10/17/11 Pct Recovery = 54% Analysis Date = 10/06/11 Pct Recovery = 55% Analysis Date = 10/06/11 Pct Recovery = 55% Analysis Date = 09/26/11 Pct Recovery = 55% Analysis Date = 09/26/11 Pct Recovery = 55% Analysis Date = 09/15/11 Pct Recovery = 55% Analysis Date = 09/15/11 Pct Recovery = 55% Analysis Date = 09/04/11 Pct Recovery = 55% Analysis Date = 09/04/11 Pct Recovery = 55% Analysis Date = 08/25/11 Pct Recovery = 55% Analysis Date = 08/25/11 Pct Recovery = 55% Analysis Date = 08/14/11 Pct Recovery = 56% Analysis Date = 08/14/11 Pct Recovery = 56% Analysis Date = 08/03/11 Pct Recovery = 56% Analysis Date = 08/03/11 Pct Recovery = 56% Analysis Date = 07/24/11 Pct Recovery = 56% Analysis Date = 07/24/11 Pct Recovery = 56% Analysis Date = 07/13/11 Pct Recovery = 56% Analysis Date = 07/13/11 Pct Recovery = 56% Analysis Date = 07/02/11 Pct Recovery = 56% Analysis Date = 07/02/11 Pct Recovery = 56% Analysis Date = 06/22/11 Pct Recovery = 57% Analysis Date = 06/22/11 Pct Recovery = 57% Analysis Date = 06/11/11 Pct Recovery = 57% Analysis Date = 06/11/11 Pct Recovery = 57% Analysis Date = 05/31/11 Pct Recovery = 57% Analysis Date = 05/31/11 Pct Recovery = 57% Analysis Date = 05/21/11 Pct Recovery = 57% Analysis Date = 05/21/11 Pct Recovery = 57% Analysis Date = 05/10/11 Pct Recovery = 58% Analysis Date = 05/10/11 Pct Recovery = 58% Analysis Date = 04/29/11 Pct Recovery = 58% Analysis Date = 04/29/11 Pct Recovery = 58% Analysis Date = 04/19/11 Pct Recovery = 58% Analysis Date = 04/19/11 Pct Recovery = 58% Analysis Date = 04/08/11 Pct Recovery = 58% Analysis Date = 04/08/11 Pct Recovery = 58% Analysis Date = 03/28/11 Pct Recovery = 59% Analysis Date = 03/28/11 Pct Recovery = 59% Analysis Date = 03/18/11 Pct Recovery = 59% Analysis Date = 03/18/11 Pct Recovery = 59% Analysis Date = 03/07/11 Pct Recovery = 59% Analysis Date = 03/07/11 Pct Recovery = 59% Analysis Date = 02/24/11 Pct Recovery = 59% Analysis Date = 02/24/11 Pct Recovery = 59% Analysis Date = 02/14/11 Pct Recovery = 59% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHOATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 85 45% 13% 46% 12%
Total 85 45% 13% 46% 12%

Sample Statistics
DIMETHOATE

Characteristic N % % Basis
Plotted 85 98% Spiked
Estimated Values 85 98% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 2 2% 2 out of 87
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

BQS OBSP Determination:
DISULFOTON
METHOD: 2033 , TESTIDCODE: 82677GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 90% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 43% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 40% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 91% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 37% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 62% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 77% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 67% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 38% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 41% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 44% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 42% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 30% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 39% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 30% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 18% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 66% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 11% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 42% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 54% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 66% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 40% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 48% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 12% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 56% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 70% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 61% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 55% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 60% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 44% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 58% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 60% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 48% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 71% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 51% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 54% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 7% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 63% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 50% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 7% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 22% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 26% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 30% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 24% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 6% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 61% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 37% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 70% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 51% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 40% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 15% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 32% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 20% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 52% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 55% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 73% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 30% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 12% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 48% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 58% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 8% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 62% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 14% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 32% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 68% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 18% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 58% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 18% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 56% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 67% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 67% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 75% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 45% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 30% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 77% Analysis Date = 01/17/17 Pct Recovery = 59% Analysis Date = 01/07/17 Pct Recovery = 59% Analysis Date = 01/07/17 Pct Recovery = 59% Analysis Date = 12/27/16 Pct Recovery = 59% Analysis Date = 12/27/16 Pct Recovery = 59% Analysis Date = 12/16/16 Pct Recovery = 58% Analysis Date = 12/16/16 Pct Recovery = 58% Analysis Date = 12/05/16 Pct Recovery = 58% Analysis Date = 12/05/16 Pct Recovery = 58% Analysis Date = 11/24/16 Pct Recovery = 58% Analysis Date = 11/24/16 Pct Recovery = 58% Analysis Date = 11/13/16 Pct Recovery = 58% Analysis Date = 11/13/16 Pct Recovery = 58% Analysis Date = 11/03/16 Pct Recovery = 57% Analysis Date = 11/03/16 Pct Recovery = 57% Analysis Date = 10/23/16 Pct Recovery = 57% Analysis Date = 10/23/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 57% Analysis Date = 10/01/16 Pct Recovery = 56% Analysis Date = 10/01/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/20/16 Pct Recovery = 56% Analysis Date = 09/09/16 Pct Recovery = 56% Analysis Date = 09/09/16 Pct Recovery = 56% Analysis Date = 08/29/16 Pct Recovery = 56% Analysis Date = 08/29/16 Pct Recovery = 56% Analysis Date = 08/19/16 Pct Recovery = 55% Analysis Date = 08/19/16 Pct Recovery = 55% Analysis Date = 08/08/16 Pct Recovery = 55% Analysis Date = 08/08/16 Pct Recovery = 55% Analysis Date = 07/28/16 Pct Recovery = 55% Analysis Date = 07/28/16 Pct Recovery = 55% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 06/25/16 Pct Recovery = 54% Analysis Date = 06/25/16 Pct Recovery = 54% Analysis Date = 06/14/16 Pct Recovery = 54% Analysis Date = 06/14/16 Pct Recovery = 54% Analysis Date = 06/04/16 Pct Recovery = 53% Analysis Date = 06/04/16 Pct Recovery = 53% Analysis Date = 05/24/16 Pct Recovery = 53% Analysis Date = 05/24/16 Pct Recovery = 53% Analysis Date = 05/13/16 Pct Recovery = 53% Analysis Date = 05/13/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 05/02/16 Pct Recovery = 53% Analysis Date = 04/21/16 Pct Recovery = 52% Analysis Date = 04/21/16 Pct Recovery = 52% Analysis Date = 04/10/16 Pct Recovery = 52% Analysis Date = 04/10/16 Pct Recovery = 52% Analysis Date = 03/31/16 Pct Recovery = 52% Analysis Date = 03/31/16 Pct Recovery = 52% Analysis Date = 03/20/16 Pct Recovery = 52% Analysis Date = 03/20/16 Pct Recovery = 52% Analysis Date = 03/09/16 Pct Recovery = 51% Analysis Date = 03/09/16 Pct Recovery = 51% Analysis Date = 02/27/16 Pct Recovery = 51% Analysis Date = 02/27/16 Pct Recovery = 51% Analysis Date = 02/16/16 Pct Recovery = 51% Analysis Date = 02/16/16 Pct Recovery = 51% Analysis Date = 02/05/16 Pct Recovery = 51% Analysis Date = 02/05/16 Pct Recovery = 51% Analysis Date = 01/25/16 Pct Recovery = 50% Analysis Date = 01/25/16 Pct Recovery = 50% Analysis Date = 01/15/16 Pct Recovery = 50% Analysis Date = 01/15/16 Pct Recovery = 50% Analysis Date = 01/04/16 Pct Recovery = 50% Analysis Date = 01/04/16 Pct Recovery = 50% Analysis Date = 12/24/15 Pct Recovery = 49% Analysis Date = 12/24/15 Pct Recovery = 49% Analysis Date = 12/13/15 Pct Recovery = 49% Analysis Date = 12/13/15 Pct Recovery = 49% Analysis Date = 12/02/15 Pct Recovery = 49% Analysis Date = 12/02/15 Pct Recovery = 49% Analysis Date = 11/21/15 Pct Recovery = 49% Analysis Date = 11/21/15 Pct Recovery = 49% Analysis Date = 11/10/15 Pct Recovery = 48% Analysis Date = 11/10/15 Pct Recovery = 48% Analysis Date = 10/31/15 Pct Recovery = 48% Analysis Date = 10/31/15 Pct Recovery = 48% Analysis Date = 10/20/15 Pct Recovery = 48% Analysis Date = 10/20/15 Pct Recovery = 48% Analysis Date = 10/09/15 Pct Recovery = 48% Analysis Date = 10/09/15 Pct Recovery = 48% Analysis Date = 09/28/15 Pct Recovery = 47% Analysis Date = 09/28/15 Pct Recovery = 47% Analysis Date = 09/17/15 Pct Recovery = 47% Analysis Date = 09/17/15 Pct Recovery = 47% Analysis Date = 09/06/15 Pct Recovery = 47% Analysis Date = 09/06/15 Pct Recovery = 47% Analysis Date = 08/27/15 Pct Recovery = 47% Analysis Date = 08/27/15 Pct Recovery = 47% Analysis Date = 08/16/15 Pct Recovery = 46% Analysis Date = 08/16/15 Pct Recovery = 46% Analysis Date = 08/05/15 Pct Recovery = 46% Analysis Date = 08/05/15 Pct Recovery = 46% Analysis Date = 07/25/15 Pct Recovery = 46% Analysis Date = 07/25/15 Pct Recovery = 46% Analysis Date = 07/14/15 Pct Recovery = 46% Analysis Date = 07/14/15 Pct Recovery = 46% Analysis Date = 07/03/15 Pct Recovery = 45% Analysis Date = 07/03/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 45% Analysis Date = 06/12/15 Pct Recovery = 45% Analysis Date = 06/12/15 Pct Recovery = 45% Analysis Date = 06/01/15 Pct Recovery = 45% Analysis Date = 06/01/15 Pct Recovery = 45% Analysis Date = 05/21/15 Pct Recovery = 44% Analysis Date = 05/21/15 Pct Recovery = 44% Analysis Date = 05/10/15 Pct Recovery = 44% Analysis Date = 05/10/15 Pct Recovery = 44% Analysis Date = 04/29/15 Pct Recovery = 44% Analysis Date = 04/29/15 Pct Recovery = 44% Analysis Date = 04/18/15 Pct Recovery = 43% Analysis Date = 04/18/15 Pct Recovery = 43% Analysis Date = 04/07/15 Pct Recovery = 43% Analysis Date = 04/07/15 Pct Recovery = 43% Analysis Date = 03/28/15 Pct Recovery = 43% Analysis Date = 03/28/15 Pct Recovery = 43% Analysis Date = 03/17/15 Pct Recovery = 43% Analysis Date = 03/17/15 Pct Recovery = 43% Analysis Date = 03/06/15 Pct Recovery = 42% Analysis Date = 03/06/15 Pct Recovery = 42% Analysis Date = 02/23/15 Pct Recovery = 42% Analysis Date = 02/23/15 Pct Recovery = 42% Analysis Date = 02/12/15 Pct Recovery = 42% Analysis Date = 02/12/15 Pct Recovery = 42% Analysis Date = 02/01/15 Pct Recovery = 42% Analysis Date = 02/01/15 Pct Recovery = 42% Analysis Date = 01/22/15 Pct Recovery = 41% Analysis Date = 01/22/15 Pct Recovery = 41% Analysis Date = 01/11/15 Pct Recovery = 41% Analysis Date = 01/11/15 Pct Recovery = 41% Analysis Date = 12/31/14 Pct Recovery = 41% Analysis Date = 12/31/14 Pct Recovery = 41% Analysis Date = 12/20/14 Pct Recovery = 41% Analysis Date = 12/20/14 Pct Recovery = 41% Analysis Date = 12/09/14 Pct Recovery = 40% Analysis Date = 12/09/14 Pct Recovery = 40% Analysis Date = 11/28/14 Pct Recovery = 40% Analysis Date = 11/28/14 Pct Recovery = 40% Analysis Date = 11/17/14 Pct Recovery = 40% Analysis Date = 11/17/14 Pct Recovery = 40% Analysis Date = 11/07/14 Pct Recovery = 40% Analysis Date = 11/07/14 Pct Recovery = 40% Analysis Date = 10/27/14 Pct Recovery = 40% Analysis Date = 10/27/14 Pct Recovery = 40% Analysis Date = 10/16/14 Pct Recovery = 40% Analysis Date = 10/16/14 Pct Recovery = 40% Analysis Date = 10/05/14 Pct Recovery = 40% Analysis Date = 10/05/14 Pct Recovery = 40% Analysis Date = 09/24/14 Pct Recovery = 39% Analysis Date = 09/24/14 Pct Recovery = 39% Analysis Date = 09/13/14 Pct Recovery = 39% Analysis Date = 09/13/14 Pct Recovery = 39% Analysis Date = 09/02/14 Pct Recovery = 39% Analysis Date = 09/02/14 Pct Recovery = 39% Analysis Date = 08/23/14 Pct Recovery = 39% Analysis Date = 08/23/14 Pct Recovery = 39% Analysis Date = 08/12/14 Pct Recovery = 39% Analysis Date = 08/12/14 Pct Recovery = 39% Analysis Date = 08/01/14 Pct Recovery = 39% Analysis Date = 08/01/14 Pct Recovery = 39% Analysis Date = 07/21/14 Pct Recovery = 39% Analysis Date = 07/21/14 Pct Recovery = 39% Analysis Date = 07/10/14 Pct Recovery = 39% Analysis Date = 07/10/14 Pct Recovery = 39% Analysis Date = 06/29/14 Pct Recovery = 40% Analysis Date = 06/29/14 Pct Recovery = 40% Analysis Date = 06/19/14 Pct Recovery = 40% Analysis Date = 06/19/14 Pct Recovery = 40% Analysis Date = 06/08/14 Pct Recovery = 40% Analysis Date = 06/08/14 Pct Recovery = 40% Analysis Date = 05/28/14 Pct Recovery = 40% Analysis Date = 05/28/14 Pct Recovery = 40% Analysis Date = 05/17/14 Pct Recovery = 40% Analysis Date = 05/17/14 Pct Recovery = 40% Analysis Date = 05/06/14 Pct Recovery = 40% Analysis Date = 05/06/14 Pct Recovery = 40% Analysis Date = 04/25/14 Pct Recovery = 40% Analysis Date = 04/25/14 Pct Recovery = 40% Analysis Date = 04/14/14 Pct Recovery = 40% Analysis Date = 04/14/14 Pct Recovery = 40% Analysis Date = 04/04/14 Pct Recovery = 40% Analysis Date = 04/04/14 Pct Recovery = 40% Analysis Date = 03/24/14 Pct Recovery = 40% Analysis Date = 03/24/14 Pct Recovery = 40% Analysis Date = 03/13/14 Pct Recovery = 40% Analysis Date = 03/13/14 Pct Recovery = 40% Analysis Date = 03/02/14 Pct Recovery = 40% Analysis Date = 03/02/14 Pct Recovery = 40% Analysis Date = 02/19/14 Pct Recovery = 40% Analysis Date = 02/19/14 Pct Recovery = 40% Analysis Date = 02/08/14 Pct Recovery = 40% Analysis Date = 02/08/14 Pct Recovery = 40% Analysis Date = 01/28/14 Pct Recovery = 40% Analysis Date = 01/28/14 Pct Recovery = 40% Analysis Date = 01/18/14 Pct Recovery = 40% Analysis Date = 01/18/14 Pct Recovery = 40% Analysis Date = 01/07/14 Pct Recovery = 40% Analysis Date = 01/07/14 Pct Recovery = 40% Analysis Date = 12/27/13 Pct Recovery = 40% Analysis Date = 12/27/13 Pct Recovery = 40% Analysis Date = 12/16/13 Pct Recovery = 40% Analysis Date = 12/16/13 Pct Recovery = 40% Analysis Date = 12/05/13 Pct Recovery = 40% Analysis Date = 12/05/13 Pct Recovery = 40% Analysis Date = 11/24/13 Pct Recovery = 40% Analysis Date = 11/24/13 Pct Recovery = 40% Analysis Date = 11/14/13 Pct Recovery = 40% Analysis Date = 11/14/13 Pct Recovery = 40% Analysis Date = 11/03/13 Pct Recovery = 40% Analysis Date = 11/03/13 Pct Recovery = 40% Analysis Date = 10/23/13 Pct Recovery = 41% Analysis Date = 10/23/13 Pct Recovery = 41% Analysis Date = 10/12/13 Pct Recovery = 41% Analysis Date = 10/12/13 Pct Recovery = 41% Analysis Date = 10/01/13 Pct Recovery = 41% Analysis Date = 10/01/13 Pct Recovery = 41% Analysis Date = 09/20/13 Pct Recovery = 41% Analysis Date = 09/20/13 Pct Recovery = 41% Analysis Date = 09/09/13 Pct Recovery = 41% Analysis Date = 09/09/13 Pct Recovery = 41% Analysis Date = 08/30/13 Pct Recovery = 41% Analysis Date = 08/30/13 Pct Recovery = 41% Analysis Date = 08/19/13 Pct Recovery = 41% Analysis Date = 08/19/13 Pct Recovery = 41% Analysis Date = 08/08/13 Pct Recovery = 41% Analysis Date = 08/08/13 Pct Recovery = 41% Analysis Date = 07/28/13 Pct Recovery = 41% Analysis Date = 07/28/13 Pct Recovery = 41% Analysis Date = 07/17/13 Pct Recovery = 41% Analysis Date = 07/17/13 Pct Recovery = 41% Analysis Date = 07/06/13 Pct Recovery = 41% Analysis Date = 07/06/13 Pct Recovery = 41% Analysis Date = 06/25/13 Pct Recovery = 41% Analysis Date = 06/25/13 Pct Recovery = 41% Analysis Date = 06/15/13 Pct Recovery = 41% Analysis Date = 06/15/13 Pct Recovery = 41% Analysis Date = 06/04/13 Pct Recovery = 41% Analysis Date = 06/04/13 Pct Recovery = 41% Analysis Date = 05/24/13 Pct Recovery = 41% Analysis Date = 05/24/13 Pct Recovery = 41% Analysis Date = 05/13/13 Pct Recovery = 41% Analysis Date = 05/13/13 Pct Recovery = 41% Analysis Date = 05/02/13 Pct Recovery = 41% Analysis Date = 05/02/13 Pct Recovery = 41% Analysis Date = 04/21/13 Pct Recovery = 41% Analysis Date = 04/21/13 Pct Recovery = 41% Analysis Date = 04/11/13 Pct Recovery = 40% Analysis Date = 04/11/13 Pct Recovery = 40% Analysis Date = 03/31/13 Pct Recovery = 40% Analysis Date = 03/31/13 Pct Recovery = 40% Analysis Date = 03/20/13 Pct Recovery = 40% Analysis Date = 03/20/13 Pct Recovery = 40% Analysis Date = 03/09/13 Pct Recovery = 40% Analysis Date = 03/09/13 Pct Recovery = 40% Analysis Date = 02/26/13 Pct Recovery = 40% Analysis Date = 02/26/13 Pct Recovery = 40% Analysis Date = 02/15/13 Pct Recovery = 40% Analysis Date = 02/15/13 Pct Recovery = 40% Analysis Date = 02/04/13 Pct Recovery = 40% Analysis Date = 02/04/13 Pct Recovery = 40% Analysis Date = 01/25/13 Pct Recovery = 40% Analysis Date = 01/25/13 Pct Recovery = 40% Analysis Date = 01/14/13 Pct Recovery = 40% Analysis Date = 01/14/13 Pct Recovery = 40% Analysis Date = 01/03/13 Pct Recovery = 40% Analysis Date = 01/03/13 Pct Recovery = 40% Analysis Date = 12/23/12 Pct Recovery = 40% Analysis Date = 12/23/12 Pct Recovery = 40% Analysis Date = 12/12/12 Pct Recovery = 40% Analysis Date = 12/12/12 Pct Recovery = 40% Analysis Date = 12/01/12 Pct Recovery = 40% Analysis Date = 12/01/12 Pct Recovery = 40% Analysis Date = 11/20/12 Pct Recovery = 40% Analysis Date = 11/20/12 Pct Recovery = 40% Analysis Date = 11/10/12 Pct Recovery = 40% Analysis Date = 11/10/12 Pct Recovery = 40% Analysis Date = 10/30/12 Pct Recovery = 40% Analysis Date = 10/30/12 Pct Recovery = 40% Analysis Date = 10/19/12 Pct Recovery = 40% Analysis Date = 10/19/12 Pct Recovery = 40% Analysis Date = 10/08/12 Pct Recovery = 40% Analysis Date = 10/08/12 Pct Recovery = 40% Analysis Date = 09/27/12 Pct Recovery = 40% Analysis Date = 09/27/12 Pct Recovery = 40% Analysis Date = 09/16/12 Pct Recovery = 40% Analysis Date = 09/16/12 Pct Recovery = 40% Analysis Date = 09/06/12 Pct Recovery = 40% Analysis Date = 09/06/12 Pct Recovery = 40% Analysis Date = 08/26/12 Pct Recovery = 41% Analysis Date = 08/26/12 Pct Recovery = 41% Analysis Date = 08/15/12 Pct Recovery = 41% Analysis Date = 08/15/12 Pct Recovery = 41% Analysis Date = 08/04/12 Pct Recovery = 42% Analysis Date = 08/04/12 Pct Recovery = 42% Analysis Date = 07/24/12 Pct Recovery = 42% Analysis Date = 07/24/12 Pct Recovery = 42% Analysis Date = 07/13/12 Pct Recovery = 43% Analysis Date = 07/13/12 Pct Recovery = 43% Analysis Date = 07/02/12 Pct Recovery = 43% Analysis Date = 07/02/12 Pct Recovery = 43% Analysis Date = 06/22/12 Pct Recovery = 43% Analysis Date = 06/22/12 Pct Recovery = 43% Analysis Date = 06/11/12 Pct Recovery = 44% Analysis Date = 06/11/12 Pct Recovery = 44% Analysis Date = 05/31/12 Pct Recovery = 44% Analysis Date = 05/31/12 Pct Recovery = 44% Analysis Date = 05/20/12 Pct Recovery = 45% Analysis Date = 05/20/12 Pct Recovery = 45% Analysis Date = 05/09/12 Pct Recovery = 45% Analysis Date = 05/09/12 Pct Recovery = 45% Analysis Date = 04/28/12 Pct Recovery = 46% Analysis Date = 04/28/12 Pct Recovery = 46% Analysis Date = 04/17/12 Pct Recovery = 46% Analysis Date = 04/17/12 Pct Recovery = 46% Analysis Date = 04/07/12 Pct Recovery = 47% Analysis Date = 04/07/12 Pct Recovery = 47% Analysis Date = 03/27/12 Pct Recovery = 47% Analysis Date = 03/27/12 Pct Recovery = 47% Analysis Date = 03/16/12 Pct Recovery = 48% Analysis Date = 03/16/12 Pct Recovery = 48% Analysis Date = 03/05/12 Pct Recovery = 48% Analysis Date = 03/05/12 Pct Recovery = 48% Analysis Date = 02/23/12 Pct Recovery = 49% Analysis Date = 02/23/12 Pct Recovery = 49% Analysis Date = 02/12/12 Pct Recovery = 49% Analysis Date = 02/12/12 Pct Recovery = 49% Analysis Date = 02/02/12 Pct Recovery = 50% Analysis Date = 02/02/12 Pct Recovery = 50% Analysis Date = 01/22/12 Pct Recovery = 50% Analysis Date = 01/22/12 Pct Recovery = 50% Analysis Date = 01/11/12 Pct Recovery = 51% Analysis Date = 01/11/12 Pct Recovery = 51% Analysis Date = 12/31/11 Pct Recovery = 51% Analysis Date = 12/31/11 Pct Recovery = 51% Analysis Date = 12/20/11 Pct Recovery = 52% Analysis Date = 12/20/11 Pct Recovery = 52% Analysis Date = 12/09/11 Pct Recovery = 52% Analysis Date = 12/09/11 Pct Recovery = 52% Analysis Date = 11/28/11 Pct Recovery = 53% Analysis Date = 11/28/11 Pct Recovery = 53% Analysis Date = 11/18/11 Pct Recovery = 53% Analysis Date = 11/18/11 Pct Recovery = 53% Analysis Date = 11/07/11 Pct Recovery = 54% Analysis Date = 11/07/11 Pct Recovery = 54% Analysis Date = 10/27/11 Pct Recovery = 54% Analysis Date = 10/27/11 Pct Recovery = 54% Analysis Date = 10/16/11 Pct Recovery = 55% Analysis Date = 10/16/11 Pct Recovery = 55% Analysis Date = 10/05/11 Pct Recovery = 55% Analysis Date = 10/05/11 Pct Recovery = 55% Analysis Date = 09/24/11 Pct Recovery = 56% Analysis Date = 09/24/11 Pct Recovery = 56% Analysis Date = 09/13/11 Pct Recovery = 56% Analysis Date = 09/13/11 Pct Recovery = 56% Analysis Date = 09/03/11 Pct Recovery = 57% Analysis Date = 09/03/11 Pct Recovery = 57% Analysis Date = 08/23/11 Pct Recovery = 57% Analysis Date = 08/23/11 Pct Recovery = 57% Analysis Date = 08/12/11 Pct Recovery = 58% Analysis Date = 08/12/11 Pct Recovery = 58% Analysis Date = 08/01/11 Pct Recovery = 58% Analysis Date = 08/01/11 Pct Recovery = 58% Analysis Date = 07/21/11 Pct Recovery = 59% Analysis Date = 07/21/11 Pct Recovery = 59% Analysis Date = 07/10/11 Pct Recovery = 59% Analysis Date = 07/10/11 Pct Recovery = 59% Analysis Date = 06/30/11 Pct Recovery = 60% Analysis Date = 06/30/11 Pct Recovery = 60% Analysis Date = 06/19/11 Pct Recovery = 61% Analysis Date = 06/19/11 Pct Recovery = 61% Analysis Date = 06/08/11 Pct Recovery = 61% Analysis Date = 06/08/11 Pct Recovery = 61% Analysis Date = 05/28/11 Pct Recovery = 62% Analysis Date = 05/28/11 Pct Recovery = 62% Analysis Date = 05/17/11 Pct Recovery = 62% Analysis Date = 05/17/11 Pct Recovery = 62% Analysis Date = 05/06/11 Pct Recovery = 63% Analysis Date = 05/06/11 Pct Recovery = 63% Analysis Date = 04/25/11 Pct Recovery = 63% Analysis Date = 04/25/11 Pct Recovery = 63% Analysis Date = 04/15/11 Pct Recovery = 64% Analysis Date = 04/15/11 Pct Recovery = 64% Analysis Date = 04/04/11 Pct Recovery = 64% Analysis Date = 04/04/11 Pct Recovery = 64% Analysis Date = 03/24/11 Pct Recovery = 65% Analysis Date = 03/24/11 Pct Recovery = 65% Analysis Date = 03/13/11 Pct Recovery = 66% Analysis Date = 03/13/11 Pct Recovery = 66% Analysis Date = 03/02/11 Pct Recovery = 66% Analysis Date = 03/02/11 Pct Recovery = 66% Analysis Date = 02/19/11 Pct Recovery = 67% Analysis Date = 02/19/11 Pct Recovery = 67% Analysis Date = 02/09/11 Pct Recovery = 67% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 77% . 77% 0%
>= Reporting Level 81 47% 21% 50% 24%
Total 82 47% 21% 51% 24%

Sample Statistics
DISULFOTON

Characteristic N % % Basis
Plotted 82 90% Spiked
Estimated Values 82 90% Spiked
Deleted Values 5 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 95 .  
False Negatives 9 10% 9 out of 91
Not Spiked 74 .  
False Positives 0 0% 0 out of 73

BQS OBSP Determination:
DISULFOTON SULFONE
METHOD: 2033 , TESTIDCODE: 61640GCM39
Open Data Set

Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 314% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 76% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 66% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 69% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 85% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 73% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 70% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 81% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 75% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 86% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 95% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 79% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 73% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 103% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 104% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 91% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 103% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 73% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 77% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 165% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 78% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 106% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 111% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 108% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 94% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 105% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 85% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 89% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 97% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 108% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 97% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 91% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 81% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 83% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 89% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 96% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 78% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 82% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 131% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 88% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 98% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 199% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 112% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 97% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 96% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 97% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 98% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 100% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 95% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 157% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 110% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 94% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 106% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 108% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 83% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 84% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 81% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 94% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 103% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 178% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 161% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/09/16 Pct Recovery = 99% Analysis Date = 12/09/16 Pct Recovery = 99% Analysis Date = 11/28/16 Pct Recovery = 99% Analysis Date = 11/28/16 Pct Recovery = 99% Analysis Date = 11/17/16 Pct Recovery = 100% Analysis Date = 11/17/16 Pct Recovery = 100% Analysis Date = 11/07/16 Pct Recovery = 100% Analysis Date = 11/07/16 Pct Recovery = 100% Analysis Date = 10/27/16 Pct Recovery = 100% Analysis Date = 10/27/16 Pct Recovery = 100% Analysis Date = 10/16/16 Pct Recovery = 101% Analysis Date = 10/16/16 Pct Recovery = 101% Analysis Date = 10/06/16 Pct Recovery = 101% Analysis Date = 10/06/16 Pct Recovery = 101% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/14/16 Pct Recovery = 102% Analysis Date = 09/14/16 Pct Recovery = 102% Analysis Date = 09/03/16 Pct Recovery = 102% Analysis Date = 09/03/16 Pct Recovery = 102% Analysis Date = 08/24/16 Pct Recovery = 103% Analysis Date = 08/24/16 Pct Recovery = 103% Analysis Date = 08/13/16 Pct Recovery = 103% Analysis Date = 08/13/16 Pct Recovery = 103% Analysis Date = 08/02/16 Pct Recovery = 103% Analysis Date = 08/02/16 Pct Recovery = 103% Analysis Date = 07/23/16 Pct Recovery = 104% Analysis Date = 07/23/16 Pct Recovery = 104% Analysis Date = 07/12/16 Pct Recovery = 104% Analysis Date = 07/12/16 Pct Recovery = 104% Analysis Date = 07/01/16 Pct Recovery = 105% Analysis Date = 07/01/16 Pct Recovery = 105% Analysis Date = 06/20/16 Pct Recovery = 105% Analysis Date = 06/20/16 Pct Recovery = 105% Analysis Date = 06/10/16 Pct Recovery = 105% Analysis Date = 06/10/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 106% Analysis Date = 05/30/16 Pct Recovery = 106% Analysis Date = 05/19/16 Pct Recovery = 106% Analysis Date = 05/19/16 Pct Recovery = 106% Analysis Date = 05/09/16 Pct Recovery = 106% Analysis Date = 05/09/16 Pct Recovery = 106% Analysis Date = 04/28/16 Pct Recovery = 107% Analysis Date = 04/28/16 Pct Recovery = 107% Analysis Date = 04/17/16 Pct Recovery = 107% Analysis Date = 04/17/16 Pct Recovery = 107% Analysis Date = 04/06/16 Pct Recovery = 107% Analysis Date = 04/06/16 Pct Recovery = 107% Analysis Date = 03/27/16 Pct Recovery = 108% Analysis Date = 03/27/16 Pct Recovery = 108% Analysis Date = 03/16/16 Pct Recovery = 108% Analysis Date = 03/16/16 Pct Recovery = 108% Analysis Date = 03/05/16 Pct Recovery = 108% Analysis Date = 03/05/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/13/16 Pct Recovery = 109% Analysis Date = 02/13/16 Pct Recovery = 109% Analysis Date = 02/02/16 Pct Recovery = 109% Analysis Date = 02/02/16 Pct Recovery = 109% Analysis Date = 01/22/16 Pct Recovery = 109% Analysis Date = 01/22/16 Pct Recovery = 109% Analysis Date = 01/12/16 Pct Recovery = 109% Analysis Date = 01/12/16 Pct Recovery = 109% Analysis Date = 01/01/16 Pct Recovery = 109% Analysis Date = 01/01/16 Pct Recovery = 109% Analysis Date = 12/21/15 Pct Recovery = 110% Analysis Date = 12/21/15 Pct Recovery = 110% Analysis Date = 12/11/15 Pct Recovery = 110% Analysis Date = 12/11/15 Pct Recovery = 110% Analysis Date = 11/30/15 Pct Recovery = 110% Analysis Date = 11/30/15 Pct Recovery = 110% Analysis Date = 11/19/15 Pct Recovery = 110% Analysis Date = 11/19/15 Pct Recovery = 110% Analysis Date = 11/09/15 Pct Recovery = 110% Analysis Date = 11/09/15 Pct Recovery = 110% Analysis Date = 10/29/15 Pct Recovery = 111% Analysis Date = 10/29/15 Pct Recovery = 111% Analysis Date = 10/18/15 Pct Recovery = 111% Analysis Date = 10/18/15 Pct Recovery = 111% Analysis Date = 10/07/15 Pct Recovery = 111% Analysis Date = 10/07/15 Pct Recovery = 111% Analysis Date = 09/27/15 Pct Recovery = 111% Analysis Date = 09/27/15 Pct Recovery = 111% Analysis Date = 09/16/15 Pct Recovery = 111% Analysis Date = 09/16/15 Pct Recovery = 111% Analysis Date = 09/05/15 Pct Recovery = 112% Analysis Date = 09/05/15 Pct Recovery = 112% Analysis Date = 08/26/15 Pct Recovery = 112% Analysis Date = 08/26/15 Pct Recovery = 112% Analysis Date = 08/15/15 Pct Recovery = 112% Analysis Date = 08/15/15 Pct Recovery = 112% Analysis Date = 08/04/15 Pct Recovery = 112% Analysis Date = 08/04/15 Pct Recovery = 112% Analysis Date = 07/24/15 Pct Recovery = 112% Analysis Date = 07/24/15 Pct Recovery = 112% Analysis Date = 07/14/15 Pct Recovery = 112% Analysis Date = 07/14/15 Pct Recovery = 112% Analysis Date = 07/03/15 Pct Recovery = 113% Analysis Date = 07/03/15 Pct Recovery = 113% Analysis Date = 06/22/15 Pct Recovery = 113% Analysis Date = 06/22/15 Pct Recovery = 113% Analysis Date = 06/12/15 Pct Recovery = 113% Analysis Date = 06/12/15 Pct Recovery = 113% Analysis Date = 06/01/15 Pct Recovery = 113% Analysis Date = 06/01/15 Pct Recovery = 113% Analysis Date = 05/21/15 Pct Recovery = 113% Analysis Date = 05/21/15 Pct Recovery = 113% Analysis Date = 05/10/15 Pct Recovery = 113% Analysis Date = 05/10/15 Pct Recovery = 113% Analysis Date = 04/30/15 Pct Recovery = 113% Analysis Date = 04/30/15 Pct Recovery = 113% Analysis Date = 04/19/15 Pct Recovery = 113% Analysis Date = 04/19/15 Pct Recovery = 113% Analysis Date = 04/08/15 Pct Recovery = 114% Analysis Date = 04/08/15 Pct Recovery = 114% Analysis Date = 03/29/15 Pct Recovery = 114% Analysis Date = 03/29/15 Pct Recovery = 114% Analysis Date = 03/18/15 Pct Recovery = 114% Analysis Date = 03/18/15 Pct Recovery = 114% Analysis Date = 03/07/15 Pct Recovery = 114% Analysis Date = 03/07/15 Pct Recovery = 114% Analysis Date = 02/24/15 Pct Recovery = 114% Analysis Date = 02/24/15 Pct Recovery = 114% Analysis Date = 02/14/15 Pct Recovery = 114% Analysis Date = 02/14/15 Pct Recovery = 114% Analysis Date = 02/03/15 Pct Recovery = 114% Analysis Date = 02/03/15 Pct Recovery = 114% Analysis Date = 01/23/15 Pct Recovery = 113% Analysis Date = 01/23/15 Pct Recovery = 113% Analysis Date = 01/13/15 Pct Recovery = 113% Analysis Date = 01/13/15 Pct Recovery = 113% Analysis Date = 01/02/15 Pct Recovery = 113% Analysis Date = 01/02/15 Pct Recovery = 113% Analysis Date = 12/22/14 Pct Recovery = 113% Analysis Date = 12/22/14 Pct Recovery = 113% Analysis Date = 12/12/14 Pct Recovery = 112% Analysis Date = 12/12/14 Pct Recovery = 112% Analysis Date = 12/01/14 Pct Recovery = 112% Analysis Date = 12/01/14 Pct Recovery = 112% Analysis Date = 11/20/14 Pct Recovery = 112% Analysis Date = 11/20/14 Pct Recovery = 112% Analysis Date = 11/09/14 Pct Recovery = 111% Analysis Date = 11/09/14 Pct Recovery = 111% Analysis Date = 10/30/14 Pct Recovery = 111% Analysis Date = 10/30/14 Pct Recovery = 111% Analysis Date = 10/19/14 Pct Recovery = 111% Analysis Date = 10/19/14 Pct Recovery = 111% Analysis Date = 10/08/14 Pct Recovery = 111% Analysis Date = 10/08/14 Pct Recovery = 111% Analysis Date = 09/28/14 Pct Recovery = 110% Analysis Date = 09/28/14 Pct Recovery = 110% Analysis Date = 09/17/14 Pct Recovery = 109% Analysis Date = 09/17/14 Pct Recovery = 109% Analysis Date = 09/06/14 Pct Recovery = 108% Analysis Date = 09/06/14 Pct Recovery = 108% Analysis Date = 08/26/14 Pct Recovery = 108% Analysis Date = 08/26/14 Pct Recovery = 108% Analysis Date = 08/16/14 Pct Recovery = 107% Analysis Date = 08/16/14 Pct Recovery = 107% Analysis Date = 08/05/14 Pct Recovery = 106% Analysis Date = 08/05/14 Pct Recovery = 106% Analysis Date = 07/25/14 Pct Recovery = 105% Analysis Date = 07/25/14 Pct Recovery = 105% Analysis Date = 07/15/14 Pct Recovery = 105% Analysis Date = 07/15/14 Pct Recovery = 105% Analysis Date = 07/04/14 Pct Recovery = 104% Analysis Date = 07/04/14 Pct Recovery = 104% Analysis Date = 06/23/14 Pct Recovery = 103% Analysis Date = 06/23/14 Pct Recovery = 103% Analysis Date = 06/12/14 Pct Recovery = 103% Analysis Date = 06/12/14 Pct Recovery = 103% Analysis Date = 06/02/14 Pct Recovery = 102% Analysis Date = 06/02/14 Pct Recovery = 102% Analysis Date = 05/22/14 Pct Recovery = 102% Analysis Date = 05/22/14 Pct Recovery = 102% Analysis Date = 05/11/14 Pct Recovery = 101% Analysis Date = 05/11/14 Pct Recovery = 101% Analysis Date = 05/01/14 Pct Recovery = 101% Analysis Date = 05/01/14 Pct Recovery = 101% Analysis Date = 04/20/14 Pct Recovery = 101% Analysis Date = 04/20/14 Pct Recovery = 101% Analysis Date = 04/09/14 Pct Recovery = 100% Analysis Date = 04/09/14 Pct Recovery = 100% Analysis Date = 03/29/14 Pct Recovery = 100% Analysis Date = 03/29/14 Pct Recovery = 100% Analysis Date = 03/19/14 Pct Recovery = 99% Analysis Date = 03/19/14 Pct Recovery = 99% Analysis Date = 03/08/14 Pct Recovery = 99% Analysis Date = 03/08/14 Pct Recovery = 99% Analysis Date = 02/25/14 Pct Recovery = 98% Analysis Date = 02/25/14 Pct Recovery = 98% Analysis Date = 02/15/14 Pct Recovery = 98% Analysis Date = 02/15/14 Pct Recovery = 98% Analysis Date = 02/04/14 Pct Recovery = 97% Analysis Date = 02/04/14 Pct Recovery = 97% Analysis Date = 01/24/14 Pct Recovery = 97% Analysis Date = 01/24/14 Pct Recovery = 97% Analysis Date = 01/13/14 Pct Recovery = 97% Analysis Date = 01/13/14 Pct Recovery = 97% Analysis Date = 01/03/14 Pct Recovery = 96% Analysis Date = 01/03/14 Pct Recovery = 96% Analysis Date = 12/23/13 Pct Recovery = 96% Analysis Date = 12/23/13 Pct Recovery = 96% Analysis Date = 12/12/13 Pct Recovery = 95% Analysis Date = 12/12/13 Pct Recovery = 95% Analysis Date = 12/02/13 Pct Recovery = 95% Analysis Date = 12/02/13 Pct Recovery = 95% Analysis Date = 11/21/13 Pct Recovery = 94% Analysis Date = 11/21/13 Pct Recovery = 94% Analysis Date = 11/10/13 Pct Recovery = 94% Analysis Date = 11/10/13 Pct Recovery = 94% Analysis Date = 10/31/13 Pct Recovery = 93% Analysis Date = 10/31/13 Pct Recovery = 93% Analysis Date = 10/20/13 Pct Recovery = 93% Analysis Date = 10/20/13 Pct Recovery = 93% Analysis Date = 10/09/13 Pct Recovery = 93% Analysis Date = 10/09/13 Pct Recovery = 93% Analysis Date = 09/28/13 Pct Recovery = 92% Analysis Date = 09/28/13 Pct Recovery = 92% Analysis Date = 09/18/13 Pct Recovery = 92% Analysis Date = 09/18/13 Pct Recovery = 92% Analysis Date = 09/07/13 Pct Recovery = 91% Analysis Date = 09/07/13 Pct Recovery = 91% Analysis Date = 08/27/13 Pct Recovery = 91% Analysis Date = 08/27/13 Pct Recovery = 91% Analysis Date = 08/17/13 Pct Recovery = 90% Analysis Date = 08/17/13 Pct Recovery = 90% Analysis Date = 08/06/13 Pct Recovery = 90% Analysis Date = 08/06/13 Pct Recovery = 90% Analysis Date = 07/26/13 Pct Recovery = 89% Analysis Date = 07/26/13 Pct Recovery = 89% Analysis Date = 07/15/13 Pct Recovery = 89% Analysis Date = 07/15/13 Pct Recovery = 89% Analysis Date = 07/05/13 Pct Recovery = 89% Analysis Date = 07/05/13 Pct Recovery = 89% Analysis Date = 06/24/13 Pct Recovery = 88% Analysis Date = 06/24/13 Pct Recovery = 88% Analysis Date = 06/13/13 Pct Recovery = 88% Analysis Date = 06/13/13 Pct Recovery = 88% Analysis Date = 06/03/13 Pct Recovery = 87% Analysis Date = 06/03/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/12/13 Pct Recovery = 86% Analysis Date = 05/12/13 Pct Recovery = 86% Analysis Date = 05/01/13 Pct Recovery = 86% Analysis Date = 05/01/13 Pct Recovery = 86% Analysis Date = 04/21/13 Pct Recovery = 85% Analysis Date = 04/21/13 Pct Recovery = 85% Analysis Date = 04/10/13 Pct Recovery = 85% Analysis Date = 04/10/13 Pct Recovery = 85% Analysis Date = 03/30/13 Pct Recovery = 85% Analysis Date = 03/30/13 Pct Recovery = 85% Analysis Date = 03/20/13 Pct Recovery = 85% Analysis Date = 03/20/13 Pct Recovery = 85% Analysis Date = 03/09/13 Pct Recovery = 84% Analysis Date = 03/09/13 Pct Recovery = 84% Analysis Date = 02/26/13 Pct Recovery = 84% Analysis Date = 02/26/13 Pct Recovery = 84% Analysis Date = 02/15/13 Pct Recovery = 84% Analysis Date = 02/15/13 Pct Recovery = 84% Analysis Date = 02/05/13 Pct Recovery = 84% Analysis Date = 02/05/13 Pct Recovery = 84% Analysis Date = 01/25/13 Pct Recovery = 83% Analysis Date = 01/25/13 Pct Recovery = 83% Analysis Date = 01/14/13 Pct Recovery = 83% Analysis Date = 01/14/13 Pct Recovery = 83% Analysis Date = 01/04/13 Pct Recovery = 83% Analysis Date = 01/04/13 Pct Recovery = 83% Analysis Date = 12/24/12 Pct Recovery = 83% Analysis Date = 12/24/12 Pct Recovery = 83% Analysis Date = 12/13/12 Pct Recovery = 83% Analysis Date = 12/13/12 Pct Recovery = 83% Analysis Date = 12/03/12 Pct Recovery = 83% Analysis Date = 12/03/12 Pct Recovery = 83% Analysis Date = 11/22/12 Pct Recovery = 83% Analysis Date = 11/22/12 Pct Recovery = 83% Analysis Date = 11/11/12 Pct Recovery = 83% Analysis Date = 11/11/12 Pct Recovery = 83% Analysis Date = 10/31/12 Pct Recovery = 83% Analysis Date = 10/31/12 Pct Recovery = 83% Analysis Date = 10/21/12 Pct Recovery = 83% Analysis Date = 10/21/12 Pct Recovery = 83% Analysis Date = 10/10/12 Pct Recovery = 83% Analysis Date = 10/10/12 Pct Recovery = 83% Analysis Date = 09/29/12 Pct Recovery = 83% Analysis Date = 09/29/12 Pct Recovery = 83% Analysis Date = 09/19/12 Pct Recovery = 83% Analysis Date = 09/19/12 Pct Recovery = 83% Analysis Date = 09/08/12 Pct Recovery = 83% Analysis Date = 09/08/12 Pct Recovery = 83% Analysis Date = 08/28/12 Pct Recovery = 84% Analysis Date = 08/28/12 Pct Recovery = 84% Analysis Date = 08/17/12 Pct Recovery = 84% Analysis Date = 08/17/12 Pct Recovery = 84% Analysis Date = 08/07/12 Pct Recovery = 84% Analysis Date = 08/07/12 Pct Recovery = 84% Analysis Date = 07/27/12 Pct Recovery = 84% Analysis Date = 07/27/12 Pct Recovery = 84% Analysis Date = 07/16/12 Pct Recovery = 85% Analysis Date = 07/16/12 Pct Recovery = 85% Analysis Date = 07/06/12 Pct Recovery = 85% Analysis Date = 07/06/12 Pct Recovery = 85% Analysis Date = 06/25/12 Pct Recovery = 85% Analysis Date = 06/25/12 Pct Recovery = 85% Analysis Date = 06/14/12 Pct Recovery = 85% Analysis Date = 06/14/12 Pct Recovery = 85% Analysis Date = 06/03/12 Pct Recovery = 85% Analysis Date = 06/03/12 Pct Recovery = 85% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/13/12 Pct Recovery = 86% Analysis Date = 05/13/12 Pct Recovery = 86% Analysis Date = 05/02/12 Pct Recovery = 86% Analysis Date = 05/02/12 Pct Recovery = 86% Analysis Date = 04/22/12 Pct Recovery = 86% Analysis Date = 04/22/12 Pct Recovery = 86% Analysis Date = 04/11/12 Pct Recovery = 86% Analysis Date = 04/11/12 Pct Recovery = 86% Analysis Date = 03/31/12 Pct Recovery = 87% Analysis Date = 03/31/12 Pct Recovery = 87% Analysis Date = 03/20/12 Pct Recovery = 87% Analysis Date = 03/20/12 Pct Recovery = 87% Analysis Date = 03/10/12 Pct Recovery = 87% Analysis Date = 03/10/12 Pct Recovery = 87% Analysis Date = 02/28/12 Pct Recovery = 87% Analysis Date = 02/28/12 Pct Recovery = 87% Analysis Date = 02/17/12 Pct Recovery = 87% Analysis Date = 02/17/12 Pct Recovery = 87% Analysis Date = 02/07/12 Pct Recovery = 87% Analysis Date = 02/07/12 Pct Recovery = 87% Analysis Date = 01/27/12 Pct Recovery = 88% Analysis Date = 01/27/12 Pct Recovery = 88% Analysis Date = 01/16/12 Pct Recovery = 88% Analysis Date = 01/16/12 Pct Recovery = 88% Analysis Date = 01/06/12 Pct Recovery = 88% Analysis Date = 01/06/12 Pct Recovery = 88% Analysis Date = 12/26/11 Pct Recovery = 88% Analysis Date = 12/26/11 Pct Recovery = 88% Analysis Date = 12/15/11 Pct Recovery = 88% Analysis Date = 12/15/11 Pct Recovery = 88% Analysis Date = 12/04/11 Pct Recovery = 88% Analysis Date = 12/04/11 Pct Recovery = 88% Analysis Date = 11/24/11 Pct Recovery = 89% Analysis Date = 11/24/11 Pct Recovery = 89% Analysis Date = 11/13/11 Pct Recovery = 89% Analysis Date = 11/13/11 Pct Recovery = 89% Analysis Date = 11/02/11 Pct Recovery = 89% Analysis Date = 11/02/11 Pct Recovery = 89% Analysis Date = 10/23/11 Pct Recovery = 89% Analysis Date = 10/23/11 Pct Recovery = 89% Analysis Date = 10/12/11 Pct Recovery = 89% Analysis Date = 10/12/11 Pct Recovery = 89% Analysis Date = 10/01/11 Pct Recovery = 89% Analysis Date = 10/01/11 Pct Recovery = 89% Analysis Date = 09/20/11 Pct Recovery = 90% Analysis Date = 09/20/11 Pct Recovery = 90% Analysis Date = 09/10/11 Pct Recovery = 90% Analysis Date = 09/10/11 Pct Recovery = 90% Analysis Date = 08/30/11 Pct Recovery = 90% Analysis Date = 08/30/11 Pct Recovery = 90% Analysis Date = 08/19/11 Pct Recovery = 90% Analysis Date = 08/19/11 Pct Recovery = 90% Analysis Date = 08/09/11 Pct Recovery = 90% Analysis Date = 08/09/11 Pct Recovery = 90% Analysis Date = 07/29/11 Pct Recovery = 90% Analysis Date = 07/29/11 Pct Recovery = 90% Analysis Date = 07/18/11 Pct Recovery = 91% Analysis Date = 07/18/11 Pct Recovery = 91% Analysis Date = 07/07/11 Pct Recovery = 91% Analysis Date = 07/07/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/16/11 Pct Recovery = 91% Analysis Date = 06/16/11 Pct Recovery = 91% Analysis Date = 06/05/11 Pct Recovery = 91% Analysis Date = 06/05/11 Pct Recovery = 91% Analysis Date = 05/26/11 Pct Recovery = 91% Analysis Date = 05/26/11 Pct Recovery = 91% Analysis Date = 05/15/11 Pct Recovery = 91% Analysis Date = 05/15/11 Pct Recovery = 91% Analysis Date = 05/04/11 Pct Recovery = 92% Analysis Date = 05/04/11 Pct Recovery = 92% Analysis Date = 04/23/11 Pct Recovery = 92% Analysis Date = 04/23/11 Pct Recovery = 92% Analysis Date = 04/13/11 Pct Recovery = 92% Analysis Date = 04/13/11 Pct Recovery = 92% Analysis Date = 04/02/11 Pct Recovery = 92% Analysis Date = 04/02/11 Pct Recovery = 92% Analysis Date = 03/22/11 Pct Recovery = 92% Analysis Date = 03/22/11 Pct Recovery = 92% Analysis Date = 03/12/11 Pct Recovery = 92% Analysis Date = 03/12/11 Pct Recovery = 92% Analysis Date = 03/01/11 Pct Recovery = 92% Analysis Date = 03/01/11 Pct Recovery = 92% Analysis Date = 02/18/11 Pct Recovery = 93% Analysis Date = 02/18/11 Pct Recovery = 93% Analysis Date = 02/08/11 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 74 99% 35% 91% 16%
Total 74 99% 35% 91% 16%

Sample Statistics
DISULFOTON SULFONE

Characteristic N % % Basis
Plotted 74 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 74 .  
False Negatives 0 0% 0 out of 74
Not Spiked 89 .  
False Positives 4 4% 4 out of 89

BQS OBSP Determination:
ENDOSULFAN SULFATE
METHOD: 2033 , TESTIDCODE: 61590GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 84% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 92% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 86% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 94% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 83% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 84% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 82% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 75% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 85% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 87% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 82% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 86% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 42% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 76% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 93% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 76% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 71% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 89% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 77% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 96% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 77% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 80% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 125% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 75% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 95% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 90% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 97% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 62% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 100% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 67% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 94% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 76% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 72% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 80% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 110% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 90% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 93% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 86% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 90% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 89% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 79% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 79% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 64% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 75% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 72% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 70% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 72% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 78% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 65% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 83% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 81% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 117% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 85% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 90% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 86% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 62% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 98% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 68% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 67% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 51% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 71% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 73% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 64% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 60% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 71% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 76% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 66% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 69% Analysis Date = 01/17/17 Pct Recovery = 84% Analysis Date = 01/07/17 Pct Recovery = 84% Analysis Date = 01/07/17 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/05/16 Pct Recovery = 84% Analysis Date = 12/05/16 Pct Recovery = 84% Analysis Date = 11/24/16 Pct Recovery = 83% Analysis Date = 11/24/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/13/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 11/03/16 Pct Recovery = 83% Analysis Date = 10/23/16 Pct Recovery = 83% Analysis Date = 10/23/16 Pct Recovery = 83% Analysis Date = 10/12/16 Pct Recovery = 83% Analysis Date = 10/12/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 82% Analysis Date = 10/01/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/20/16 Pct Recovery = 82% Analysis Date = 09/09/16 Pct Recovery = 82% Analysis Date = 09/09/16 Pct Recovery = 82% Analysis Date = 08/29/16 Pct Recovery = 82% Analysis Date = 08/29/16 Pct Recovery = 82% Analysis Date = 08/19/16 Pct Recovery = 82% Analysis Date = 08/19/16 Pct Recovery = 82% Analysis Date = 08/08/16 Pct Recovery = 82% Analysis Date = 08/08/16 Pct Recovery = 82% Analysis Date = 07/28/16 Pct Recovery = 81% Analysis Date = 07/28/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 81% Analysis Date = 06/14/16 Pct Recovery = 81% Analysis Date = 06/14/16 Pct Recovery = 81% Analysis Date = 06/04/16 Pct Recovery = 81% Analysis Date = 06/04/16 Pct Recovery = 81% Analysis Date = 05/24/16 Pct Recovery = 80% Analysis Date = 05/24/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 04/21/16 Pct Recovery = 80% Analysis Date = 04/21/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/20/16 Pct Recovery = 79% Analysis Date = 03/20/16 Pct Recovery = 79% Analysis Date = 03/09/16 Pct Recovery = 79% Analysis Date = 03/09/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/16/16 Pct Recovery = 79% Analysis Date = 02/16/16 Pct Recovery = 79% Analysis Date = 02/05/16 Pct Recovery = 79% Analysis Date = 02/05/16 Pct Recovery = 79% Analysis Date = 01/25/16 Pct Recovery = 78% Analysis Date = 01/25/16 Pct Recovery = 78% Analysis Date = 01/15/16 Pct Recovery = 78% Analysis Date = 01/15/16 Pct Recovery = 78% Analysis Date = 01/04/16 Pct Recovery = 78% Analysis Date = 01/04/16 Pct Recovery = 78% Analysis Date = 12/24/15 Pct Recovery = 78% Analysis Date = 12/24/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/13/15 Pct Recovery = 78% Analysis Date = 12/02/15 Pct Recovery = 78% Analysis Date = 12/02/15 Pct Recovery = 78% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/10/15 Pct Recovery = 77% Analysis Date = 11/10/15 Pct Recovery = 77% Analysis Date = 10/31/15 Pct Recovery = 77% Analysis Date = 10/31/15 Pct Recovery = 77% Analysis Date = 10/20/15 Pct Recovery = 77% Analysis Date = 10/20/15 Pct Recovery = 77% Analysis Date = 10/09/15 Pct Recovery = 77% Analysis Date = 10/09/15 Pct Recovery = 77% Analysis Date = 09/28/15 Pct Recovery = 77% Analysis Date = 09/28/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/06/15 Pct Recovery = 76% Analysis Date = 09/06/15 Pct Recovery = 76% Analysis Date = 08/27/15 Pct Recovery = 76% Analysis Date = 08/27/15 Pct Recovery = 76% Analysis Date = 08/16/15 Pct Recovery = 76% Analysis Date = 08/16/15 Pct Recovery = 76% Analysis Date = 08/05/15 Pct Recovery = 76% Analysis Date = 08/05/15 Pct Recovery = 76% Analysis Date = 07/25/15 Pct Recovery = 76% Analysis Date = 07/25/15 Pct Recovery = 76% Analysis Date = 07/14/15 Pct Recovery = 75% Analysis Date = 07/14/15 Pct Recovery = 75% Analysis Date = 07/03/15 Pct Recovery = 75% Analysis Date = 07/03/15 Pct Recovery = 75% Analysis Date = 06/22/15 Pct Recovery = 75% Analysis Date = 06/22/15 Pct Recovery = 75% Analysis Date = 06/12/15 Pct Recovery = 75% Analysis Date = 06/12/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 06/01/15 Pct Recovery = 75% Analysis Date = 05/21/15 Pct Recovery = 75% Analysis Date = 05/21/15 Pct Recovery = 75% Analysis Date = 05/10/15 Pct Recovery = 75% Analysis Date = 05/10/15 Pct Recovery = 75% Analysis Date = 04/29/15 Pct Recovery = 75% Analysis Date = 04/29/15 Pct Recovery = 75% Analysis Date = 04/18/15 Pct Recovery = 75% Analysis Date = 04/18/15 Pct Recovery = 75% Analysis Date = 04/07/15 Pct Recovery = 75% Analysis Date = 04/07/15 Pct Recovery = 75% Analysis Date = 03/28/15 Pct Recovery = 75% Analysis Date = 03/28/15 Pct Recovery = 75% Analysis Date = 03/17/15 Pct Recovery = 75% Analysis Date = 03/17/15 Pct Recovery = 75% Analysis Date = 03/06/15 Pct Recovery = 75% Analysis Date = 03/06/15 Pct Recovery = 75% Analysis Date = 02/23/15 Pct Recovery = 74% Analysis Date = 02/23/15 Pct Recovery = 74% Analysis Date = 02/12/15 Pct Recovery = 74% Analysis Date = 02/12/15 Pct Recovery = 74% Analysis Date = 02/01/15 Pct Recovery = 74% Analysis Date = 02/01/15 Pct Recovery = 74% Analysis Date = 01/22/15 Pct Recovery = 74% Analysis Date = 01/22/15 Pct Recovery = 74% Analysis Date = 01/11/15 Pct Recovery = 74% Analysis Date = 01/11/15 Pct Recovery = 74% Analysis Date = 12/31/14 Pct Recovery = 74% Analysis Date = 12/31/14 Pct Recovery = 74% Analysis Date = 12/20/14 Pct Recovery = 74% Analysis Date = 12/20/14 Pct Recovery = 74% Analysis Date = 12/09/14 Pct Recovery = 74% Analysis Date = 12/09/14 Pct Recovery = 74% Analysis Date = 11/28/14 Pct Recovery = 74% Analysis Date = 11/28/14 Pct Recovery = 74% Analysis Date = 11/17/14 Pct Recovery = 74% Analysis Date = 11/17/14 Pct Recovery = 74% Analysis Date = 11/07/14 Pct Recovery = 74% Analysis Date = 11/07/14 Pct Recovery = 74% Analysis Date = 10/27/14 Pct Recovery = 74% Analysis Date = 10/27/14 Pct Recovery = 74% Analysis Date = 10/16/14 Pct Recovery = 74% Analysis Date = 10/16/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 10/05/14 Pct Recovery = 74% Analysis Date = 09/24/14 Pct Recovery = 74% Analysis Date = 09/24/14 Pct Recovery = 74% Analysis Date = 09/13/14 Pct Recovery = 74% Analysis Date = 09/13/14 Pct Recovery = 74% Analysis Date = 09/02/14 Pct Recovery = 75% Analysis Date = 09/02/14 Pct Recovery = 75% Analysis Date = 08/23/14 Pct Recovery = 75% Analysis Date = 08/23/14 Pct Recovery = 75% Analysis Date = 08/12/14 Pct Recovery = 75% Analysis Date = 08/12/14 Pct Recovery = 75% Analysis Date = 08/01/14 Pct Recovery = 75% Analysis Date = 08/01/14 Pct Recovery = 75% Analysis Date = 07/21/14 Pct Recovery = 75% Analysis Date = 07/21/14 Pct Recovery = 75% Analysis Date = 07/10/14 Pct Recovery = 75% Analysis Date = 07/10/14 Pct Recovery = 75% Analysis Date = 06/29/14 Pct Recovery = 75% Analysis Date = 06/29/14 Pct Recovery = 75% Analysis Date = 06/19/14 Pct Recovery = 75% Analysis Date = 06/19/14 Pct Recovery = 75% Analysis Date = 06/08/14 Pct Recovery = 75% Analysis Date = 06/08/14 Pct Recovery = 75% Analysis Date = 05/28/14 Pct Recovery = 75% Analysis Date = 05/28/14 Pct Recovery = 75% Analysis Date = 05/17/14 Pct Recovery = 76% Analysis Date = 05/17/14 Pct Recovery = 76% Analysis Date = 05/06/14 Pct Recovery = 76% Analysis Date = 05/06/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/04/14 Pct Recovery = 76% Analysis Date = 04/04/14 Pct Recovery = 76% Analysis Date = 03/24/14 Pct Recovery = 77% Analysis Date = 03/24/14 Pct Recovery = 77% Analysis Date = 03/13/14 Pct Recovery = 77% Analysis Date = 03/13/14 Pct Recovery = 77% Analysis Date = 03/02/14 Pct Recovery = 77% Analysis Date = 03/02/14 Pct Recovery = 77% Analysis Date = 02/19/14 Pct Recovery = 77% Analysis Date = 02/19/14 Pct Recovery = 77% Analysis Date = 02/08/14 Pct Recovery = 77% Analysis Date = 02/08/14 Pct Recovery = 77% Analysis Date = 01/28/14 Pct Recovery = 78% Analysis Date = 01/28/14 Pct Recovery = 78% Analysis Date = 01/18/14 Pct Recovery = 78% Analysis Date = 01/18/14 Pct Recovery = 78% Analysis Date = 01/07/14 Pct Recovery = 78% Analysis Date = 01/07/14 Pct Recovery = 78% Analysis Date = 12/27/13 Pct Recovery = 78% Analysis Date = 12/27/13 Pct Recovery = 78% Analysis Date = 12/16/13 Pct Recovery = 78% Analysis Date = 12/16/13 Pct Recovery = 78% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 11/24/13 Pct Recovery = 79% Analysis Date = 11/24/13 Pct Recovery = 79% Analysis Date = 11/14/13 Pct Recovery = 79% Analysis Date = 11/14/13 Pct Recovery = 79% Analysis Date = 11/03/13 Pct Recovery = 79% Analysis Date = 11/03/13 Pct Recovery = 79% Analysis Date = 10/23/13 Pct Recovery = 80% Analysis Date = 10/23/13 Pct Recovery = 80% Analysis Date = 10/12/13 Pct Recovery = 80% Analysis Date = 10/12/13 Pct Recovery = 80% Analysis Date = 10/01/13 Pct Recovery = 80% Analysis Date = 10/01/13 Pct Recovery = 80% Analysis Date = 09/20/13 Pct Recovery = 80% Analysis Date = 09/20/13 Pct Recovery = 80% Analysis Date = 09/09/13 Pct Recovery = 81% Analysis Date = 09/09/13 Pct Recovery = 81% Analysis Date = 08/30/13 Pct Recovery = 81% Analysis Date = 08/30/13 Pct Recovery = 81% Analysis Date = 08/19/13 Pct Recovery = 81% Analysis Date = 08/19/13 Pct Recovery = 81% Analysis Date = 08/08/13 Pct Recovery = 82% Analysis Date = 08/08/13 Pct Recovery = 82% Analysis Date = 07/28/13 Pct Recovery = 82% Analysis Date = 07/28/13 Pct Recovery = 82% Analysis Date = 07/17/13 Pct Recovery = 82% Analysis Date = 07/17/13 Pct Recovery = 82% Analysis Date = 07/06/13 Pct Recovery = 82% Analysis Date = 07/06/13 Pct Recovery = 82% Analysis Date = 06/25/13 Pct Recovery = 83% Analysis Date = 06/25/13 Pct Recovery = 83% Analysis Date = 06/15/13 Pct Recovery = 83% Analysis Date = 06/15/13 Pct Recovery = 83% Analysis Date = 06/04/13 Pct Recovery = 83% Analysis Date = 06/04/13 Pct Recovery = 83% Analysis Date = 05/24/13 Pct Recovery = 83% Analysis Date = 05/24/13 Pct Recovery = 83% Analysis Date = 05/13/13 Pct Recovery = 84% Analysis Date = 05/13/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 04/21/13 Pct Recovery = 84% Analysis Date = 04/21/13 Pct Recovery = 84% Analysis Date = 04/11/13 Pct Recovery = 84% Analysis Date = 04/11/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/31/13 Pct Recovery = 84% Analysis Date = 03/20/13 Pct Recovery = 85% Analysis Date = 03/20/13 Pct Recovery = 85% Analysis Date = 03/09/13 Pct Recovery = 85% Analysis Date = 03/09/13 Pct Recovery = 85% Analysis Date = 02/26/13 Pct Recovery = 85% Analysis Date = 02/26/13 Pct Recovery = 85% Analysis Date = 02/15/13 Pct Recovery = 85% Analysis Date = 02/15/13 Pct Recovery = 85% Analysis Date = 02/04/13 Pct Recovery = 86% Analysis Date = 02/04/13 Pct Recovery = 86% Analysis Date = 01/25/13 Pct Recovery = 86% Analysis Date = 01/25/13 Pct Recovery = 86% Analysis Date = 01/14/13 Pct Recovery = 86% Analysis Date = 01/14/13 Pct Recovery = 86% Analysis Date = 01/03/13 Pct Recovery = 86% Analysis Date = 01/03/13 Pct Recovery = 86% Analysis Date = 12/23/12 Pct Recovery = 86% Analysis Date = 12/23/12 Pct Recovery = 86% Analysis Date = 12/12/12 Pct Recovery = 86% Analysis Date = 12/12/12 Pct Recovery = 86% Analysis Date = 12/01/12 Pct Recovery = 86% Analysis Date = 12/01/12 Pct Recovery = 86% Analysis Date = 11/20/12 Pct Recovery = 86% Analysis Date = 11/20/12 Pct Recovery = 86% Analysis Date = 11/10/12 Pct Recovery = 86% Analysis Date = 11/10/12 Pct Recovery = 86% Analysis Date = 10/30/12 Pct Recovery = 86% Analysis Date = 10/30/12 Pct Recovery = 86% Analysis Date = 10/19/12 Pct Recovery = 86% Analysis Date = 10/19/12 Pct Recovery = 86% Analysis Date = 10/08/12 Pct Recovery = 86% Analysis Date = 10/08/12 Pct Recovery = 86% Analysis Date = 09/27/12 Pct Recovery = 86% Analysis Date = 09/27/12 Pct Recovery = 86% Analysis Date = 09/16/12 Pct Recovery = 86% Analysis Date = 09/16/12 Pct Recovery = 86% Analysis Date = 09/06/12 Pct Recovery = 86% Analysis Date = 09/06/12 Pct Recovery = 86% Analysis Date = 08/26/12 Pct Recovery = 86% Analysis Date = 08/26/12 Pct Recovery = 86% Analysis Date = 08/15/12 Pct Recovery = 86% Analysis Date = 08/15/12 Pct Recovery = 86% Analysis Date = 08/04/12 Pct Recovery = 86% Analysis Date = 08/04/12 Pct Recovery = 86% Analysis Date = 07/24/12 Pct Recovery = 86% Analysis Date = 07/24/12 Pct Recovery = 86% Analysis Date = 07/13/12 Pct Recovery = 86% Analysis Date = 07/13/12 Pct Recovery = 86% Analysis Date = 07/02/12 Pct Recovery = 86% Analysis Date = 07/02/12 Pct Recovery = 86% Analysis Date = 06/22/12 Pct Recovery = 86% Analysis Date = 06/22/12 Pct Recovery = 86% Analysis Date = 06/11/12 Pct Recovery = 85% Analysis Date = 06/11/12 Pct Recovery = 85% Analysis Date = 05/31/12 Pct Recovery = 85% Analysis Date = 05/31/12 Pct Recovery = 85% Analysis Date = 05/20/12 Pct Recovery = 85% Analysis Date = 05/20/12 Pct Recovery = 85% Analysis Date = 05/09/12 Pct Recovery = 85% Analysis Date = 05/09/12 Pct Recovery = 85% Analysis Date = 04/28/12 Pct Recovery = 85% Analysis Date = 04/28/12 Pct Recovery = 85% Analysis Date = 04/17/12 Pct Recovery = 85% Analysis Date = 04/17/12 Pct Recovery = 85% Analysis Date = 04/07/12 Pct Recovery = 85% Analysis Date = 04/07/12 Pct Recovery = 85% Analysis Date = 03/27/12 Pct Recovery = 85% Analysis Date = 03/27/12 Pct Recovery = 85% Analysis Date = 03/16/12 Pct Recovery = 85% Analysis Date = 03/16/12 Pct Recovery = 85% Analysis Date = 03/05/12 Pct Recovery = 85% Analysis Date = 03/05/12 Pct Recovery = 85% Analysis Date = 02/23/12 Pct Recovery = 85% Analysis Date = 02/23/12 Pct Recovery = 85% Analysis Date = 02/12/12 Pct Recovery = 85% Analysis Date = 02/12/12 Pct Recovery = 85% Analysis Date = 02/02/12 Pct Recovery = 85% Analysis Date = 02/02/12 Pct Recovery = 85% Analysis Date = 01/22/12 Pct Recovery = 85% Analysis Date = 01/22/12 Pct Recovery = 85% Analysis Date = 01/11/12 Pct Recovery = 85% Analysis Date = 01/11/12 Pct Recovery = 85% Analysis Date = 12/31/11 Pct Recovery = 85% Analysis Date = 12/31/11 Pct Recovery = 85% Analysis Date = 12/20/11 Pct Recovery = 85% Analysis Date = 12/20/11 Pct Recovery = 85% Analysis Date = 12/09/11 Pct Recovery = 85% Analysis Date = 12/09/11 Pct Recovery = 85% Analysis Date = 11/28/11 Pct Recovery = 84% Analysis Date = 11/28/11 Pct Recovery = 84% Analysis Date = 11/18/11 Pct Recovery = 84% Analysis Date = 11/18/11 Pct Recovery = 84% Analysis Date = 11/07/11 Pct Recovery = 84% Analysis Date = 11/07/11 Pct Recovery = 84% Analysis Date = 10/27/11 Pct Recovery = 84% Analysis Date = 10/27/11 Pct Recovery = 84% Analysis Date = 10/16/11 Pct Recovery = 84% Analysis Date = 10/16/11 Pct Recovery = 84% Analysis Date = 10/05/11 Pct Recovery = 84% Analysis Date = 10/05/11 Pct Recovery = 84% Analysis Date = 09/24/11 Pct Recovery = 84% Analysis Date = 09/24/11 Pct Recovery = 84% Analysis Date = 09/13/11 Pct Recovery = 84% Analysis Date = 09/13/11 Pct Recovery = 84% Analysis Date = 09/03/11 Pct Recovery = 84% Analysis Date = 09/03/11 Pct Recovery = 84% Analysis Date = 08/23/11 Pct Recovery = 84% Analysis Date = 08/23/11 Pct Recovery = 84% Analysis Date = 08/12/11 Pct Recovery = 84% Analysis Date = 08/12/11 Pct Recovery = 84% Analysis Date = 08/01/11 Pct Recovery = 84% Analysis Date = 08/01/11 Pct Recovery = 84% Analysis Date = 07/21/11 Pct Recovery = 84% Analysis Date = 07/21/11 Pct Recovery = 84% Analysis Date = 07/10/11 Pct Recovery = 84% Analysis Date = 07/10/11 Pct Recovery = 84% Analysis Date = 06/30/11 Pct Recovery = 84% Analysis Date = 06/30/11 Pct Recovery = 84% Analysis Date = 06/19/11 Pct Recovery = 84% Analysis Date = 06/19/11 Pct Recovery = 84% Analysis Date = 06/08/11 Pct Recovery = 84% Analysis Date = 06/08/11 Pct Recovery = 84% Analysis Date = 05/28/11 Pct Recovery = 83% Analysis Date = 05/28/11 Pct Recovery = 83% Analysis Date = 05/17/11 Pct Recovery = 83% Analysis Date = 05/17/11 Pct Recovery = 83% Analysis Date = 05/06/11 Pct Recovery = 83% Analysis Date = 05/06/11 Pct Recovery = 83% Analysis Date = 04/25/11 Pct Recovery = 83% Analysis Date = 04/25/11 Pct Recovery = 83% Analysis Date = 04/15/11 Pct Recovery = 83% Analysis Date = 04/15/11 Pct Recovery = 83% Analysis Date = 04/04/11 Pct Recovery = 83% Analysis Date = 04/04/11 Pct Recovery = 83% Analysis Date = 03/24/11 Pct Recovery = 83% Analysis Date = 03/24/11 Pct Recovery = 83% Analysis Date = 03/13/11 Pct Recovery = 83% Analysis Date = 03/13/11 Pct Recovery = 83% Analysis Date = 03/02/11 Pct Recovery = 83% Analysis Date = 03/02/11 Pct Recovery = 83% Analysis Date = 02/19/11 Pct Recovery = 83% Analysis Date = 02/19/11 Pct Recovery = 83% Analysis Date = 02/09/11 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ENDOSULFAN SULFATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 88 81% 13% 80% 13%
Total 88 81% 13% 80% 13%

Sample Statistics
ENDOSULFAN SULFATE

Characteristic N % % Basis
Plotted 88 99% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 89 .  
False Negatives 1 1% 1 out of 89
Not Spiked 80 .  
False Positives 0 0% 0 out of 80

BQS OBSP Determination:
EPTC
METHOD: 2033 , TESTIDCODE: 82668GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 91% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 74% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 93% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 101% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 90% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 108% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 95% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 104% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 95% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 90% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 105% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 114% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 93% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 96% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 89% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 97% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 103% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 92% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 107% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 100% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 102% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 96% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 94% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 105% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 95% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 117% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 103% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 97% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 99% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 53% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 99% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 85% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 102% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 95% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 97% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 102% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 82% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 87% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 91% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 104% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 98% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 100% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 80% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 83% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 105% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 113% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 109% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 93% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 89% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 102% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 93% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 106% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 89% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 91% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 93% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 98% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 79% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 102% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 112% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 94% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 88% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 94% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 101% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 103% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 102% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 105% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 114% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 104% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 104% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 110% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 108% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 112% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 99% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 98% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 101% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 105% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 110% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 55% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 12/20/16 Pct Recovery = 95% Analysis Date = 12/09/16 Pct Recovery = 95% Analysis Date = 12/09/16 Pct Recovery = 95% Analysis Date = 11/28/16 Pct Recovery = 95% Analysis Date = 11/28/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/07/16 Pct Recovery = 95% Analysis Date = 11/07/16 Pct Recovery = 95% Analysis Date = 10/27/16 Pct Recovery = 95% Analysis Date = 10/27/16 Pct Recovery = 95% Analysis Date = 10/16/16 Pct Recovery = 94% Analysis Date = 10/16/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/25/16 Pct Recovery = 94% Analysis Date = 09/14/16 Pct Recovery = 94% Analysis Date = 09/14/16 Pct Recovery = 94% Analysis Date = 09/04/16 Pct Recovery = 94% Analysis Date = 09/04/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 07/23/16 Pct Recovery = 94% Analysis Date = 07/23/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/02/16 Pct Recovery = 94% Analysis Date = 07/02/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/10/16 Pct Recovery = 94% Analysis Date = 06/10/16 Pct Recovery = 94% Analysis Date = 05/31/16 Pct Recovery = 94% Analysis Date = 05/31/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/20/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 05/09/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/29/16 Pct Recovery = 94% Analysis Date = 04/18/16 Pct Recovery = 94% Analysis Date = 04/18/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/28/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 94% Analysis Date = 03/17/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 03/06/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/14/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 02/03/16 Pct Recovery = 94% Analysis Date = 01/23/16 Pct Recovery = 94% Analysis Date = 01/23/16 Pct Recovery = 94% Analysis Date = 01/13/16 Pct Recovery = 94% Analysis Date = 01/13/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 01/02/16 Pct Recovery = 94% Analysis Date = 12/22/15 Pct Recovery = 94% Analysis Date = 12/22/15 Pct Recovery = 94% Analysis Date = 12/12/15 Pct Recovery = 94% Analysis Date = 12/12/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/20/15 Pct Recovery = 94% Analysis Date = 11/10/15 Pct Recovery = 94% Analysis Date = 11/10/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/19/15 Pct Recovery = 94% Analysis Date = 10/19/15 Pct Recovery = 94% Analysis Date = 10/09/15 Pct Recovery = 94% Analysis Date = 10/09/15 Pct Recovery = 94% Analysis Date = 09/28/15 Pct Recovery = 94% Analysis Date = 09/28/15 Pct Recovery = 94% Analysis Date = 09/17/15 Pct Recovery = 94% Analysis Date = 09/17/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 09/07/15 Pct Recovery = 94% Analysis Date = 08/27/15 Pct Recovery = 94% Analysis Date = 08/27/15 Pct Recovery = 94% Analysis Date = 08/16/15 Pct Recovery = 94% Analysis Date = 08/16/15 Pct Recovery = 94% Analysis Date = 08/06/15 Pct Recovery = 94% Analysis Date = 08/06/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/26/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/15/15 Pct Recovery = 94% Analysis Date = 07/05/15 Pct Recovery = 94% Analysis Date = 07/05/15 Pct Recovery = 94% Analysis Date = 06/24/15 Pct Recovery = 94% Analysis Date = 06/24/15 Pct Recovery = 94% Analysis Date = 06/13/15 Pct Recovery = 94% Analysis Date = 06/13/15 Pct Recovery = 94% Analysis Date = 06/02/15 Pct Recovery = 94% Analysis Date = 06/02/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/23/15 Pct Recovery = 94% Analysis Date = 05/12/15 Pct Recovery = 94% Analysis Date = 05/12/15 Pct Recovery = 94% Analysis Date = 05/01/15 Pct Recovery = 94% Analysis Date = 05/01/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/21/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 04/10/15 Pct Recovery = 94% Analysis Date = 03/30/15 Pct Recovery = 94% Analysis Date = 03/30/15 Pct Recovery = 94% Analysis Date = 03/20/15 Pct Recovery = 94% Analysis Date = 03/20/15 Pct Recovery = 94% Analysis Date = 03/09/15 Pct Recovery = 94% Analysis Date = 03/09/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/26/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/16/15 Pct Recovery = 94% Analysis Date = 02/05/15 Pct Recovery = 94% Analysis Date = 02/05/15 Pct Recovery = 94% Analysis Date = 01/25/15 Pct Recovery = 94% Analysis Date = 01/25/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/15/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 94% Analysis Date = 01/04/15 Pct Recovery = 94% Analysis Date = 12/24/14 Pct Recovery = 94% Analysis Date = 12/24/14 Pct Recovery = 94% Analysis Date = 12/14/14 Pct Recovery = 94% Analysis Date = 12/14/14 Pct Recovery = 94% Analysis Date = 12/03/14 Pct Recovery = 95% Analysis Date = 12/03/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/22/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 95% Analysis Date = 11/01/14 Pct Recovery = 95% Analysis Date = 11/01/14 Pct Recovery = 95% Analysis Date = 10/21/14 Pct Recovery = 95% Analysis Date = 10/21/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 10/11/14 Pct Recovery = 95% Analysis Date = 09/30/14 Pct Recovery = 95% Analysis Date = 09/30/14 Pct Recovery = 95% Analysis Date = 09/19/14 Pct Recovery = 95% Analysis Date = 09/19/14 Pct Recovery = 95% Analysis Date = 09/08/14 Pct Recovery = 95% Analysis Date = 09/08/14 Pct Recovery = 95% Analysis Date = 08/29/14 Pct Recovery = 96% Analysis Date = 08/29/14 Pct Recovery = 96% Analysis Date = 08/18/14 Pct Recovery = 96% Analysis Date = 08/18/14 Pct Recovery = 96% Analysis Date = 08/07/14 Pct Recovery = 96% Analysis Date = 08/07/14 Pct Recovery = 96% Analysis Date = 07/28/14 Pct Recovery = 96% Analysis Date = 07/28/14 Pct Recovery = 96% Analysis Date = 07/17/14 Pct Recovery = 96% Analysis Date = 07/17/14 Pct Recovery = 96% Analysis Date = 07/06/14 Pct Recovery = 96% Analysis Date = 07/06/14 Pct Recovery = 96% Analysis Date = 06/26/14 Pct Recovery = 96% Analysis Date = 06/26/14 Pct Recovery = 96% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/04/14 Pct Recovery = 97% Analysis Date = 06/04/14 Pct Recovery = 97% Analysis Date = 05/25/14 Pct Recovery = 97% Analysis Date = 05/25/14 Pct Recovery = 97% Analysis Date = 05/14/14 Pct Recovery = 97% Analysis Date = 05/14/14 Pct Recovery = 97% Analysis Date = 05/03/14 Pct Recovery = 97% Analysis Date = 05/03/14 Pct Recovery = 97% Analysis Date = 04/23/14 Pct Recovery = 97% Analysis Date = 04/23/14 Pct Recovery = 97% Analysis Date = 04/12/14 Pct Recovery = 97% Analysis Date = 04/12/14 Pct Recovery = 97% Analysis Date = 04/01/14 Pct Recovery = 97% Analysis Date = 04/01/14 Pct Recovery = 97% Analysis Date = 03/22/14 Pct Recovery = 97% Analysis Date = 03/22/14 Pct Recovery = 97% Analysis Date = 03/11/14 Pct Recovery = 97% Analysis Date = 03/11/14 Pct Recovery = 97% Analysis Date = 02/28/14 Pct Recovery = 97% Analysis Date = 02/28/14 Pct Recovery = 97% Analysis Date = 02/18/14 Pct Recovery = 97% Analysis Date = 02/18/14 Pct Recovery = 97% Analysis Date = 02/07/14 Pct Recovery = 97% Analysis Date = 02/07/14 Pct Recovery = 97% Analysis Date = 01/27/14 Pct Recovery = 97% Analysis Date = 01/27/14 Pct Recovery = 97% Analysis Date = 01/17/14 Pct Recovery = 97% Analysis Date = 01/17/14 Pct Recovery = 97% Analysis Date = 01/06/14 Pct Recovery = 97% Analysis Date = 01/06/14 Pct Recovery = 97% Analysis Date = 12/26/13 Pct Recovery = 97% Analysis Date = 12/26/13 Pct Recovery = 97% Analysis Date = 12/15/13 Pct Recovery = 97% Analysis Date = 12/15/13 Pct Recovery = 97% Analysis Date = 12/05/13 Pct Recovery = 97% Analysis Date = 12/05/13 Pct Recovery = 97% Analysis Date = 11/24/13 Pct Recovery = 97% Analysis Date = 11/24/13 Pct Recovery = 97% Analysis Date = 11/13/13 Pct Recovery = 97% Analysis Date = 11/13/13 Pct Recovery = 97% Analysis Date = 11/03/13 Pct Recovery = 97% Analysis Date = 11/03/13 Pct Recovery = 97% Analysis Date = 10/23/13 Pct Recovery = 97% Analysis Date = 10/23/13 Pct Recovery = 97% Analysis Date = 10/12/13 Pct Recovery = 97% Analysis Date = 10/12/13 Pct Recovery = 97% Analysis Date = 10/02/13 Pct Recovery = 97% Analysis Date = 10/02/13 Pct Recovery = 97% Analysis Date = 09/21/13 Pct Recovery = 97% Analysis Date = 09/21/13 Pct Recovery = 97% Analysis Date = 09/10/13 Pct Recovery = 97% Analysis Date = 09/10/13 Pct Recovery = 97% Analysis Date = 08/31/13 Pct Recovery = 97% Analysis Date = 08/31/13 Pct Recovery = 97% Analysis Date = 08/20/13 Pct Recovery = 97% Analysis Date = 08/20/13 Pct Recovery = 97% Analysis Date = 08/09/13 Pct Recovery = 97% Analysis Date = 08/09/13 Pct Recovery = 97% Analysis Date = 07/30/13 Pct Recovery = 97% Analysis Date = 07/30/13 Pct Recovery = 97% Analysis Date = 07/19/13 Pct Recovery = 97% Analysis Date = 07/19/13 Pct Recovery = 97% Analysis Date = 07/08/13 Pct Recovery = 97% Analysis Date = 07/08/13 Pct Recovery = 97% Analysis Date = 06/28/13 Pct Recovery = 97% Analysis Date = 06/28/13 Pct Recovery = 97% Analysis Date = 06/17/13 Pct Recovery = 97% Analysis Date = 06/17/13 Pct Recovery = 97% Analysis Date = 06/06/13 Pct Recovery = 97% Analysis Date = 06/06/13 Pct Recovery = 97% Analysis Date = 05/27/13 Pct Recovery = 97% Analysis Date = 05/27/13 Pct Recovery = 97% Analysis Date = 05/16/13 Pct Recovery = 97% Analysis Date = 05/16/13 Pct Recovery = 97% Analysis Date = 05/05/13 Pct Recovery = 97% Analysis Date = 05/05/13 Pct Recovery = 97% Analysis Date = 04/25/13 Pct Recovery = 97% Analysis Date = 04/25/13 Pct Recovery = 97% Analysis Date = 04/14/13 Pct Recovery = 97% Analysis Date = 04/14/13 Pct Recovery = 97% Analysis Date = 04/03/13 Pct Recovery = 97% Analysis Date = 04/03/13 Pct Recovery = 97% Analysis Date = 03/23/13 Pct Recovery = 97% Analysis Date = 03/23/13 Pct Recovery = 97% Analysis Date = 03/13/13 Pct Recovery = 97% Analysis Date = 03/13/13 Pct Recovery = 97% Analysis Date = 03/02/13 Pct Recovery = 97% Analysis Date = 03/02/13 Pct Recovery = 97% Analysis Date = 02/19/13 Pct Recovery = 96% Analysis Date = 02/19/13 Pct Recovery = 96% Analysis Date = 02/09/13 Pct Recovery = 96% Analysis Date = 02/09/13 Pct Recovery = 96% Analysis Date = 01/29/13 Pct Recovery = 96% Analysis Date = 01/29/13 Pct Recovery = 96% Analysis Date = 01/18/13 Pct Recovery = 96% Analysis Date = 01/18/13 Pct Recovery = 96% Analysis Date = 01/08/13 Pct Recovery = 96% Analysis Date = 01/08/13 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 96% Analysis Date = 11/15/12 Pct Recovery = 96% Analysis Date = 11/15/12 Pct Recovery = 96% Analysis Date = 11/05/12 Pct Recovery = 96% Analysis Date = 11/05/12 Pct Recovery = 96% Analysis Date = 10/25/12 Pct Recovery = 96% Analysis Date = 10/25/12 Pct Recovery = 96% Analysis Date = 10/14/12 Pct Recovery = 96% Analysis Date = 10/14/12 Pct Recovery = 96% Analysis Date = 10/04/12 Pct Recovery = 96% Analysis Date = 10/04/12 Pct Recovery = 96% Analysis Date = 09/23/12 Pct Recovery = 96% Analysis Date = 09/23/12 Pct Recovery = 96% Analysis Date = 09/12/12 Pct Recovery = 96% Analysis Date = 09/12/12 Pct Recovery = 96% Analysis Date = 09/02/12 Pct Recovery = 97% Analysis Date = 09/02/12 Pct Recovery = 97% Analysis Date = 08/22/12 Pct Recovery = 97% Analysis Date = 08/22/12 Pct Recovery = 97% Analysis Date = 08/11/12 Pct Recovery = 97% Analysis Date = 08/11/12 Pct Recovery = 97% Analysis Date = 08/01/12 Pct Recovery = 97% Analysis Date = 08/01/12 Pct Recovery = 97% Analysis Date = 07/21/12 Pct Recovery = 97% Analysis Date = 07/21/12 Pct Recovery = 97% Analysis Date = 07/10/12 Pct Recovery = 97% Analysis Date = 07/10/12 Pct Recovery = 97% Analysis Date = 06/29/12 Pct Recovery = 97% Analysis Date = 06/29/12 Pct Recovery = 97% Analysis Date = 06/19/12 Pct Recovery = 97% Analysis Date = 06/19/12 Pct Recovery = 97% Analysis Date = 06/08/12 Pct Recovery = 97% Analysis Date = 06/08/12 Pct Recovery = 97% Analysis Date = 05/28/12 Pct Recovery = 97% Analysis Date = 05/28/12 Pct Recovery = 97% Analysis Date = 05/18/12 Pct Recovery = 97% Analysis Date = 05/18/12 Pct Recovery = 97% Analysis Date = 05/07/12 Pct Recovery = 97% Analysis Date = 05/07/12 Pct Recovery = 97% Analysis Date = 04/26/12 Pct Recovery = 97% Analysis Date = 04/26/12 Pct Recovery = 97% Analysis Date = 04/16/12 Pct Recovery = 97% Analysis Date = 04/16/12 Pct Recovery = 97% Analysis Date = 04/05/12 Pct Recovery = 98% Analysis Date = 04/05/12 Pct Recovery = 98% Analysis Date = 03/25/12 Pct Recovery = 98% Analysis Date = 03/25/12 Pct Recovery = 98% Analysis Date = 03/15/12 Pct Recovery = 98% Analysis Date = 03/15/12 Pct Recovery = 98% Analysis Date = 03/04/12 Pct Recovery = 98% Analysis Date = 03/04/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/12/12 Pct Recovery = 98% Analysis Date = 02/12/12 Pct Recovery = 98% Analysis Date = 02/01/12 Pct Recovery = 98% Analysis Date = 02/01/12 Pct Recovery = 98% Analysis Date = 01/21/12 Pct Recovery = 98% Analysis Date = 01/21/12 Pct Recovery = 98% Analysis Date = 01/11/12 Pct Recovery = 99% Analysis Date = 01/11/12 Pct Recovery = 99% Analysis Date = 12/31/11 Pct Recovery = 99% Analysis Date = 12/31/11 Pct Recovery = 99% Analysis Date = 12/20/11 Pct Recovery = 99% Analysis Date = 12/20/11 Pct Recovery = 99% Analysis Date = 12/10/11 Pct Recovery = 99% Analysis Date = 12/10/11 Pct Recovery = 99% Analysis Date = 11/29/11 Pct Recovery = 99% Analysis Date = 11/29/11 Pct Recovery = 99% Analysis Date = 11/18/11 Pct Recovery = 99% Analysis Date = 11/18/11 Pct Recovery = 99% Analysis Date = 11/08/11 Pct Recovery = 99% Analysis Date = 11/08/11 Pct Recovery = 99% Analysis Date = 10/28/11 Pct Recovery = 99% Analysis Date = 10/28/11 Pct Recovery = 99% Analysis Date = 10/17/11 Pct Recovery = 100% Analysis Date = 10/17/11 Pct Recovery = 100% Analysis Date = 10/06/11 Pct Recovery = 100% Analysis Date = 10/06/11 Pct Recovery = 100% Analysis Date = 09/26/11 Pct Recovery = 100% Analysis Date = 09/26/11 Pct Recovery = 100% Analysis Date = 09/15/11 Pct Recovery = 100% Analysis Date = 09/15/11 Pct Recovery = 100% Analysis Date = 09/04/11 Pct Recovery = 100% Analysis Date = 09/04/11 Pct Recovery = 100% Analysis Date = 08/25/11 Pct Recovery = 100% Analysis Date = 08/25/11 Pct Recovery = 100% Analysis Date = 08/14/11 Pct Recovery = 100% Analysis Date = 08/14/11 Pct Recovery = 100% Analysis Date = 08/03/11 Pct Recovery = 100% Analysis Date = 08/03/11 Pct Recovery = 100% Analysis Date = 07/24/11 Pct Recovery = 101% Analysis Date = 07/24/11 Pct Recovery = 101% Analysis Date = 07/13/11 Pct Recovery = 101% Analysis Date = 07/13/11 Pct Recovery = 101% Analysis Date = 07/02/11 Pct Recovery = 101% Analysis Date = 07/02/11 Pct Recovery = 101% Analysis Date = 06/22/11 Pct Recovery = 101% Analysis Date = 06/22/11 Pct Recovery = 101% Analysis Date = 06/11/11 Pct Recovery = 101% Analysis Date = 06/11/11 Pct Recovery = 101% Analysis Date = 05/31/11 Pct Recovery = 101% Analysis Date = 05/31/11 Pct Recovery = 101% Analysis Date = 05/21/11 Pct Recovery = 101% Analysis Date = 05/21/11 Pct Recovery = 101% Analysis Date = 05/10/11 Pct Recovery = 102% Analysis Date = 05/10/11 Pct Recovery = 102% Analysis Date = 04/29/11 Pct Recovery = 102% Analysis Date = 04/29/11 Pct Recovery = 102% Analysis Date = 04/19/11 Pct Recovery = 102% Analysis Date = 04/19/11 Pct Recovery = 102% Analysis Date = 04/08/11 Pct Recovery = 102% Analysis Date = 04/08/11 Pct Recovery = 102% Analysis Date = 03/28/11 Pct Recovery = 102% Analysis Date = 03/28/11 Pct Recovery = 102% Analysis Date = 03/18/11 Pct Recovery = 102% Analysis Date = 03/18/11 Pct Recovery = 102% Analysis Date = 03/07/11 Pct Recovery = 102% Analysis Date = 03/07/11 Pct Recovery = 102% Analysis Date = 02/24/11 Pct Recovery = 103% Analysis Date = 02/24/11 Pct Recovery = 103% Analysis Date = 02/14/11 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EPTC

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 97% 11% 97% 9%
Total 94 97% 11% 97% 9%

Sample Statistics
EPTC

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 3 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
ETHION
METHOD: 2033 , TESTIDCODE: 82346GCM40
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 75% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 75% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 59% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 59% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 90% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 81% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 66% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 66% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 68% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 83% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 88% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 70% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 74% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 84% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 70% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 77% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 66% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 94% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 84% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 80% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 78% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 89% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 113% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 92% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 92% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 66% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 80% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 104% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 97% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 94% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 86% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 121% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 81% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 87% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 129% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 110% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 94% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 56% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 87% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 91% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 113% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 108% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 115% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 105% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 103% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 96% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 128% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 91% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 99% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 113% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 94% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 128% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 193% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 102% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 110% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 111% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 74% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 93% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 91% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 133% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 112% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 110% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 110% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 111% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 121% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 141% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 103% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 120% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 107% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 134% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 106% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 106% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 89% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 127% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 104% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 117% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 103% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 117% Analysis Date = 01/17/17 Pct Recovery = 117% Analysis Date = 01/07/17 Pct Recovery = 117% Analysis Date = 01/07/17 Pct Recovery = 117% Analysis Date = 12/27/16 Pct Recovery = 116% Analysis Date = 12/27/16 Pct Recovery = 116% Analysis Date = 12/16/16 Pct Recovery = 116% Analysis Date = 12/16/16 Pct Recovery = 116% Analysis Date = 12/05/16 Pct Recovery = 116% Analysis Date = 12/05/16 Pct Recovery = 116% Analysis Date = 11/24/16 Pct Recovery = 116% Analysis Date = 11/24/16 Pct Recovery = 116% Analysis Date = 11/13/16 Pct Recovery = 116% Analysis Date = 11/13/16 Pct Recovery = 116% Analysis Date = 11/03/16 Pct Recovery = 116% Analysis Date = 11/03/16 Pct Recovery = 116% Analysis Date = 10/23/16 Pct Recovery = 115% Analysis Date = 10/23/16 Pct Recovery = 115% Analysis Date = 10/12/16 Pct Recovery = 115% Analysis Date = 10/12/16 Pct Recovery = 115% Analysis Date = 10/01/16 Pct Recovery = 115% Analysis Date = 10/01/16 Pct Recovery = 115% Analysis Date = 09/20/16 Pct Recovery = 115% Analysis Date = 09/20/16 Pct Recovery = 115% Analysis Date = 09/09/16 Pct Recovery = 115% Analysis Date = 09/09/16 Pct Recovery = 115% Analysis Date = 08/29/16 Pct Recovery = 114% Analysis Date = 08/29/16 Pct Recovery = 114% Analysis Date = 08/19/16 Pct Recovery = 114% Analysis Date = 08/19/16 Pct Recovery = 114% Analysis Date = 08/08/16 Pct Recovery = 114% Analysis Date = 08/08/16 Pct Recovery = 114% Analysis Date = 07/28/16 Pct Recovery = 114% Analysis Date = 07/28/16 Pct Recovery = 114% Analysis Date = 07/17/16 Pct Recovery = 114% Analysis Date = 07/17/16 Pct Recovery = 114% Analysis Date = 07/06/16 Pct Recovery = 113% Analysis Date = 07/06/16 Pct Recovery = 113% Analysis Date = 06/25/16 Pct Recovery = 113% Analysis Date = 06/25/16 Pct Recovery = 113% Analysis Date = 06/14/16 Pct Recovery = 113% Analysis Date = 06/14/16 Pct Recovery = 113% Analysis Date = 06/04/16 Pct Recovery = 113% Analysis Date = 06/04/16 Pct Recovery = 113% Analysis Date = 05/24/16 Pct Recovery = 113% Analysis Date = 05/24/16 Pct Recovery = 113% Analysis Date = 05/13/16 Pct Recovery = 113% Analysis Date = 05/13/16 Pct Recovery = 113% Analysis Date = 05/02/16 Pct Recovery = 112% Analysis Date = 05/02/16 Pct Recovery = 112% Analysis Date = 04/21/16 Pct Recovery = 112% Analysis Date = 04/21/16 Pct Recovery = 112% Analysis Date = 04/10/16 Pct Recovery = 112% Analysis Date = 04/10/16 Pct Recovery = 112% Analysis Date = 03/30/16 Pct Recovery = 112% Analysis Date = 03/30/16 Pct Recovery = 112% Analysis Date = 03/20/16 Pct Recovery = 112% Analysis Date = 03/20/16 Pct Recovery = 112% Analysis Date = 03/09/16 Pct Recovery = 111% Analysis Date = 03/09/16 Pct Recovery = 111% Analysis Date = 02/27/16 Pct Recovery = 111% Analysis Date = 02/27/16 Pct Recovery = 111% Analysis Date = 02/16/16 Pct Recovery = 111% Analysis Date = 02/16/16 Pct Recovery = 111% Analysis Date = 02/05/16 Pct Recovery = 111% Analysis Date = 02/05/16 Pct Recovery = 111% Analysis Date = 01/25/16 Pct Recovery = 111% Analysis Date = 01/25/16 Pct Recovery = 111% Analysis Date = 01/14/16 Pct Recovery = 111% Analysis Date = 01/14/16 Pct Recovery = 111% Analysis Date = 01/04/16 Pct Recovery = 110% Analysis Date = 01/04/16 Pct Recovery = 110% Analysis Date = 12/24/15 Pct Recovery = 110% Analysis Date = 12/24/15 Pct Recovery = 110% Analysis Date = 12/13/15 Pct Recovery = 110% Analysis Date = 12/13/15 Pct Recovery = 110% Analysis Date = 12/02/15 Pct Recovery = 110% Analysis Date = 12/02/15 Pct Recovery = 110% Analysis Date = 11/21/15 Pct Recovery = 110% Analysis Date = 11/21/15 Pct Recovery = 110% Analysis Date = 11/10/15 Pct Recovery = 109% Analysis Date = 11/10/15 Pct Recovery = 109% Analysis Date = 10/30/15 Pct Recovery = 109% Analysis Date = 10/30/15 Pct Recovery = 109% Analysis Date = 10/20/15 Pct Recovery = 109% Analysis Date = 10/20/15 Pct Recovery = 109% Analysis Date = 10/09/15 Pct Recovery = 109% Analysis Date = 10/09/15 Pct Recovery = 109% Analysis Date = 09/28/15 Pct Recovery = 109% Analysis Date = 09/28/15 Pct Recovery = 109% Analysis Date = 09/17/15 Pct Recovery = 108% Analysis Date = 09/17/15 Pct Recovery = 108% Analysis Date = 09/06/15 Pct Recovery = 108% Analysis Date = 09/06/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/26/15 Pct Recovery = 108% Analysis Date = 08/15/15 Pct Recovery = 108% Analysis Date = 08/15/15 Pct Recovery = 108% Analysis Date = 08/05/15 Pct Recovery = 108% Analysis Date = 08/05/15 Pct Recovery = 108% Analysis Date = 07/25/15 Pct Recovery = 107% Analysis Date = 07/25/15 Pct Recovery = 107% Analysis Date = 07/14/15 Pct Recovery = 107% Analysis Date = 07/14/15 Pct Recovery = 107% Analysis Date = 07/03/15 Pct Recovery = 107% Analysis Date = 07/03/15 Pct Recovery = 107% Analysis Date = 06/22/15 Pct Recovery = 107% Analysis Date = 06/22/15 Pct Recovery = 107% Analysis Date = 06/11/15 Pct Recovery = 107% Analysis Date = 06/11/15 Pct Recovery = 107% Analysis Date = 05/31/15 Pct Recovery = 106% Analysis Date = 05/31/15 Pct Recovery = 106% Analysis Date = 05/21/15 Pct Recovery = 106% Analysis Date = 05/21/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 106% Analysis Date = 05/10/15 Pct Recovery = 106% Analysis Date = 04/29/15 Pct Recovery = 106% Analysis Date = 04/29/15 Pct Recovery = 106% Analysis Date = 04/18/15 Pct Recovery = 106% Analysis Date = 04/18/15 Pct Recovery = 106% Analysis Date = 04/07/15 Pct Recovery = 106% Analysis Date = 04/07/15 Pct Recovery = 106% Analysis Date = 03/27/15 Pct Recovery = 105% Analysis Date = 03/27/15 Pct Recovery = 105% Analysis Date = 03/16/15 Pct Recovery = 105% Analysis Date = 03/16/15 Pct Recovery = 105% Analysis Date = 03/06/15 Pct Recovery = 105% Analysis Date = 03/06/15 Pct Recovery = 105% Analysis Date = 02/23/15 Pct Recovery = 105% Analysis Date = 02/23/15 Pct Recovery = 105% Analysis Date = 02/12/15 Pct Recovery = 105% Analysis Date = 02/12/15 Pct Recovery = 105% Analysis Date = 02/01/15 Pct Recovery = 105% Analysis Date = 02/01/15 Pct Recovery = 105% Analysis Date = 01/21/15 Pct Recovery = 105% Analysis Date = 01/21/15 Pct Recovery = 105% Analysis Date = 01/10/15 Pct Recovery = 104% Analysis Date = 01/10/15 Pct Recovery = 104% Analysis Date = 12/31/14 Pct Recovery = 104% Analysis Date = 12/31/14 Pct Recovery = 104% Analysis Date = 12/20/14 Pct Recovery = 104% Analysis Date = 12/20/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 11/28/14 Pct Recovery = 104% Analysis Date = 11/28/14 Pct Recovery = 104% Analysis Date = 11/17/14 Pct Recovery = 104% Analysis Date = 11/17/14 Pct Recovery = 104% Analysis Date = 11/06/14 Pct Recovery = 104% Analysis Date = 11/06/14 Pct Recovery = 104% Analysis Date = 10/26/14 Pct Recovery = 103% Analysis Date = 10/26/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/05/14 Pct Recovery = 103% Analysis Date = 10/05/14 Pct Recovery = 103% Analysis Date = 09/24/14 Pct Recovery = 103% Analysis Date = 09/24/14 Pct Recovery = 103% Analysis Date = 09/13/14 Pct Recovery = 103% Analysis Date = 09/13/14 Pct Recovery = 103% Analysis Date = 09/02/14 Pct Recovery = 103% Analysis Date = 09/02/14 Pct Recovery = 103% Analysis Date = 08/22/14 Pct Recovery = 103% Analysis Date = 08/22/14 Pct Recovery = 103% Analysis Date = 08/11/14 Pct Recovery = 103% Analysis Date = 08/11/14 Pct Recovery = 103% Analysis Date = 08/01/14 Pct Recovery = 103% Analysis Date = 08/01/14 Pct Recovery = 103% Analysis Date = 07/21/14 Pct Recovery = 103% Analysis Date = 07/21/14 Pct Recovery = 103% Analysis Date = 07/10/14 Pct Recovery = 103% Analysis Date = 07/10/14 Pct Recovery = 103% Analysis Date = 06/29/14 Pct Recovery = 102% Analysis Date = 06/29/14 Pct Recovery = 102% Analysis Date = 06/18/14 Pct Recovery = 102% Analysis Date = 06/18/14 Pct Recovery = 102% Analysis Date = 06/07/14 Pct Recovery = 102% Analysis Date = 06/07/14 Pct Recovery = 102% Analysis Date = 05/27/14 Pct Recovery = 101% Analysis Date = 05/27/14 Pct Recovery = 101% Analysis Date = 05/17/14 Pct Recovery = 101% Analysis Date = 05/17/14 Pct Recovery = 101% Analysis Date = 05/06/14 Pct Recovery = 101% Analysis Date = 05/06/14 Pct Recovery = 101% Analysis Date = 04/25/14 Pct Recovery = 100% Analysis Date = 04/25/14 Pct Recovery = 100% Analysis Date = 04/14/14 Pct Recovery = 100% Analysis Date = 04/14/14 Pct Recovery = 100% Analysis Date = 04/03/14 Pct Recovery = 100% Analysis Date = 04/03/14 Pct Recovery = 100% Analysis Date = 03/23/14 Pct Recovery = 99% Analysis Date = 03/23/14 Pct Recovery = 99% Analysis Date = 03/12/14 Pct Recovery = 99% Analysis Date = 03/12/14 Pct Recovery = 99% Analysis Date = 03/02/14 Pct Recovery = 98% Analysis Date = 03/02/14 Pct Recovery = 98% Analysis Date = 02/19/14 Pct Recovery = 98% Analysis Date = 02/19/14 Pct Recovery = 98% Analysis Date = 02/08/14 Pct Recovery = 98% Analysis Date = 02/08/14 Pct Recovery = 98% Analysis Date = 01/28/14 Pct Recovery = 97% Analysis Date = 01/28/14 Pct Recovery = 97% Analysis Date = 01/17/14 Pct Recovery = 97% Analysis Date = 01/17/14 Pct Recovery = 97% Analysis Date = 01/06/14 Pct Recovery = 96% Analysis Date = 01/06/14 Pct Recovery = 96% Analysis Date = 12/26/13 Pct Recovery = 96% Analysis Date = 12/26/13 Pct Recovery = 96% Analysis Date = 12/16/13 Pct Recovery = 96% Analysis Date = 12/16/13 Pct Recovery = 96% Analysis Date = 12/05/13 Pct Recovery = 95% Analysis Date = 12/05/13 Pct Recovery = 95% Analysis Date = 11/24/13 Pct Recovery = 95% Analysis Date = 11/24/13 Pct Recovery = 95% Analysis Date = 11/13/13 Pct Recovery = 94% Analysis Date = 11/13/13 Pct Recovery = 94% Analysis Date = 11/02/13 Pct Recovery = 94% Analysis Date = 11/02/13 Pct Recovery = 94% Analysis Date = 10/22/13 Pct Recovery = 94% Analysis Date = 10/22/13 Pct Recovery = 94% Analysis Date = 10/11/13 Pct Recovery = 93% Analysis Date = 10/11/13 Pct Recovery = 93% Analysis Date = 10/01/13 Pct Recovery = 93% Analysis Date = 10/01/13 Pct Recovery = 93% Analysis Date = 09/20/13 Pct Recovery = 93% Analysis Date = 09/20/13 Pct Recovery = 93% Analysis Date = 09/09/13 Pct Recovery = 92% Analysis Date = 09/09/13 Pct Recovery = 92% Analysis Date = 08/29/13 Pct Recovery = 92% Analysis Date = 08/29/13 Pct Recovery = 92% Analysis Date = 08/18/13 Pct Recovery = 92% Analysis Date = 08/18/13 Pct Recovery = 92% Analysis Date = 08/07/13 Pct Recovery = 91% Analysis Date = 08/07/13 Pct Recovery = 91% Analysis Date = 07/27/13 Pct Recovery = 91% Analysis Date = 07/27/13 Pct Recovery = 91% Analysis Date = 07/17/13 Pct Recovery = 91% Analysis Date = 07/17/13 Pct Recovery = 91% Analysis Date = 07/06/13 Pct Recovery = 90% Analysis Date = 07/06/13 Pct Recovery = 90% Analysis Date = 06/25/13 Pct Recovery = 90% Analysis Date = 06/25/13 Pct Recovery = 90% Analysis Date = 06/14/13 Pct Recovery = 90% Analysis Date = 06/14/13 Pct Recovery = 90% Analysis Date = 06/03/13 Pct Recovery = 89% Analysis Date = 06/03/13 Pct Recovery = 89% Analysis Date = 05/23/13 Pct Recovery = 89% Analysis Date = 05/23/13 Pct Recovery = 89% Analysis Date = 05/12/13 Pct Recovery = 89% Analysis Date = 05/12/13 Pct Recovery = 89% Analysis Date = 05/02/13 Pct Recovery = 88% Analysis Date = 05/02/13 Pct Recovery = 88% Analysis Date = 04/21/13 Pct Recovery = 88% Analysis Date = 04/21/13 Pct Recovery = 88% Analysis Date = 04/10/13 Pct Recovery = 88% Analysis Date = 04/10/13 Pct Recovery = 88% Analysis Date = 03/30/13 Pct Recovery = 87% Analysis Date = 03/30/13 Pct Recovery = 87% Analysis Date = 03/19/13 Pct Recovery = 87% Analysis Date = 03/19/13 Pct Recovery = 87% Analysis Date = 03/08/13 Pct Recovery = 87% Analysis Date = 03/08/13 Pct Recovery = 87% Analysis Date = 02/25/13 Pct Recovery = 86% Analysis Date = 02/25/13 Pct Recovery = 86% Analysis Date = 02/15/13 Pct Recovery = 86% Analysis Date = 02/15/13 Pct Recovery = 86% Analysis Date = 02/04/13 Pct Recovery = 86% Analysis Date = 02/04/13 Pct Recovery = 86% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/13/13 Pct Recovery = 85% Analysis Date = 01/13/13 Pct Recovery = 85% Analysis Date = 01/02/13 Pct Recovery = 85% Analysis Date = 01/02/13 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/12/12 Pct Recovery = 85% Analysis Date = 12/12/12 Pct Recovery = 85% Analysis Date = 12/01/12 Pct Recovery = 84% Analysis Date = 12/01/12 Pct Recovery = 84% Analysis Date = 11/20/12 Pct Recovery = 84% Analysis Date = 11/20/12 Pct Recovery = 84% Analysis Date = 11/09/12 Pct Recovery = 84% Analysis Date = 11/09/12 Pct Recovery = 84% Analysis Date = 10/29/12 Pct Recovery = 84% Analysis Date = 10/29/12 Pct Recovery = 84% Analysis Date = 10/18/12 Pct Recovery = 83% Analysis Date = 10/18/12 Pct Recovery = 83% Analysis Date = 10/07/12 Pct Recovery = 83% Analysis Date = 10/07/12 Pct Recovery = 83% Analysis Date = 09/27/12 Pct Recovery = 83% Analysis Date = 09/27/12 Pct Recovery = 83% Analysis Date = 09/16/12 Pct Recovery = 84% Analysis Date = 09/16/12 Pct Recovery = 84% Analysis Date = 09/05/12 Pct Recovery = 84% Analysis Date = 09/05/12 Pct Recovery = 84% Analysis Date = 08/25/12 Pct Recovery = 84% Analysis Date = 08/25/12 Pct Recovery = 84% Analysis Date = 08/14/12 Pct Recovery = 84% Analysis Date = 08/14/12 Pct Recovery = 84% Analysis Date = 08/03/12 Pct Recovery = 84% Analysis Date = 08/03/12 Pct Recovery = 84% Analysis Date = 07/23/12 Pct Recovery = 84% Analysis Date = 07/23/12 Pct Recovery = 84% Analysis Date = 07/13/12 Pct Recovery = 84% Analysis Date = 07/13/12 Pct Recovery = 84% Analysis Date = 07/02/12 Pct Recovery = 84% Analysis Date = 07/02/12 Pct Recovery = 84% Analysis Date = 06/21/12 Pct Recovery = 84% Analysis Date = 06/21/12 Pct Recovery = 84% Analysis Date = 06/10/12 Pct Recovery = 85% Analysis Date = 06/10/12 Pct Recovery = 85% Analysis Date = 05/30/12 Pct Recovery = 85% Analysis Date = 05/30/12 Pct Recovery = 85% Analysis Date = 05/19/12 Pct Recovery = 85% Analysis Date = 05/19/12 Pct Recovery = 85% Analysis Date = 05/08/12 Pct Recovery = 85% Analysis Date = 05/08/12 Pct Recovery = 85% Analysis Date = 04/28/12 Pct Recovery = 85% Analysis Date = 04/28/12 Pct Recovery = 85% Analysis Date = 04/17/12 Pct Recovery = 85% Analysis Date = 04/17/12 Pct Recovery = 85% Analysis Date = 04/06/12 Pct Recovery = 85% Analysis Date = 04/06/12 Pct Recovery = 85% Analysis Date = 03/26/12 Pct Recovery = 86% Analysis Date = 03/26/12 Pct Recovery = 86% Analysis Date = 03/15/12 Pct Recovery = 86% Analysis Date = 03/15/12 Pct Recovery = 86% Analysis Date = 03/04/12 Pct Recovery = 86% Analysis Date = 03/04/12 Pct Recovery = 86% Analysis Date = 02/22/12 Pct Recovery = 86% Analysis Date = 02/22/12 Pct Recovery = 86% Analysis Date = 02/12/12 Pct Recovery = 86% Analysis Date = 02/12/12 Pct Recovery = 86% Analysis Date = 02/01/12 Pct Recovery = 86% Analysis Date = 02/01/12 Pct Recovery = 86% Analysis Date = 01/21/12 Pct Recovery = 86% Analysis Date = 01/21/12 Pct Recovery = 86% Analysis Date = 01/10/12 Pct Recovery = 87% Analysis Date = 01/10/12 Pct Recovery = 87% Analysis Date = 12/30/11 Pct Recovery = 87% Analysis Date = 12/30/11 Pct Recovery = 87% Analysis Date = 12/19/11 Pct Recovery = 87% Analysis Date = 12/19/11 Pct Recovery = 87% Analysis Date = 12/08/11 Pct Recovery = 87% Analysis Date = 12/08/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 87% Analysis Date = 11/17/11 Pct Recovery = 87% Analysis Date = 11/17/11 Pct Recovery = 87% Analysis Date = 11/06/11 Pct Recovery = 88% Analysis Date = 11/06/11 Pct Recovery = 88% Analysis Date = 10/26/11 Pct Recovery = 88% Analysis Date = 10/26/11 Pct Recovery = 88% Analysis Date = 10/15/11 Pct Recovery = 88% Analysis Date = 10/15/11 Pct Recovery = 88% Analysis Date = 10/04/11 Pct Recovery = 88% Analysis Date = 10/04/11 Pct Recovery = 88% Analysis Date = 09/23/11 Pct Recovery = 88% Analysis Date = 09/23/11 Pct Recovery = 88% Analysis Date = 09/13/11 Pct Recovery = 88% Analysis Date = 09/13/11 Pct Recovery = 88% Analysis Date = 09/02/11 Pct Recovery = 89% Analysis Date = 09/02/11 Pct Recovery = 89% Analysis Date = 08/22/11 Pct Recovery = 89% Analysis Date = 08/22/11 Pct Recovery = 89% Analysis Date = 08/11/11 Pct Recovery = 89% Analysis Date = 08/11/11 Pct Recovery = 89% Analysis Date = 07/31/11 Pct Recovery = 89% Analysis Date = 07/31/11 Pct Recovery = 89% Analysis Date = 07/20/11 Pct Recovery = 89% Analysis Date = 07/20/11 Pct Recovery = 89% Analysis Date = 07/09/11 Pct Recovery = 90% Analysis Date = 07/09/11 Pct Recovery = 90% Analysis Date = 06/29/11 Pct Recovery = 90% Analysis Date = 06/29/11 Pct Recovery = 90% Analysis Date = 06/18/11 Pct Recovery = 90% Analysis Date = 06/18/11 Pct Recovery = 90% Analysis Date = 06/07/11 Pct Recovery = 90% Analysis Date = 06/07/11 Pct Recovery = 90% Analysis Date = 05/27/11 Pct Recovery = 90% Analysis Date = 05/27/11 Pct Recovery = 90% Analysis Date = 05/16/11 Pct Recovery = 91% Analysis Date = 05/16/11 Pct Recovery = 91% Analysis Date = 05/05/11 Pct Recovery = 91% Analysis Date = 05/05/11 Pct Recovery = 91% Analysis Date = 04/24/11 Pct Recovery = 91% Analysis Date = 04/24/11 Pct Recovery = 91% Analysis Date = 04/14/11 Pct Recovery = 91% Analysis Date = 04/14/11 Pct Recovery = 91% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 03/23/11 Pct Recovery = 92% Analysis Date = 03/23/11 Pct Recovery = 92% Analysis Date = 03/12/11 Pct Recovery = 92% Analysis Date = 03/12/11 Pct Recovery = 92% Analysis Date = 03/01/11 Pct Recovery = 92% Analysis Date = 03/01/11 Pct Recovery = 92% Analysis Date = 02/18/11 Pct Recovery = 93% Analysis Date = 02/18/11 Pct Recovery = 93% Analysis Date = 02/08/11 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 86 97% 22% 94% 20%
Total 86 97% 22% 94% 20%

Sample Statistics
ETHION

Characteristic N % % Basis
Plotted 86 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 86 .  
False Negatives 0 0% 0 out of 86
Not Spiked 83 .  
False Positives 2 2% 2 out of 83

BQS OBSP Determination:
ETHION MONOXON
METHOD: 2033 , TESTIDCODE: 61644GCM39
Open Data Set

Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 76% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 82% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 117% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHION MONOXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 3 91% 22% 82% 31%
Total 3 91% 22% 82% 31%

Sample Statistics
ETHION MONOXON

Characteristic N % % Basis
Plotted 3 100% Spiked
Estimated Values 3 100% Spiked
Deleted Values 7 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 3 .  
False Negatives 0 0% 0 out of 3
Not Spiked 166 .  
False Positives 2 1% 2 out of 159

BQS OBSP Determination:
ETHOPROPHOS
METHOD: 2033 , TESTIDCODE: 82672GCM35
Open Data Set

Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 84% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 80% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 94% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 82% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 92% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 82% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 69% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 84% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 113% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 72% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 101% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 93% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 86% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 91% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 71% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 107% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 108% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 96% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 114% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 103% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 107% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 84% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 82% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 76% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 80% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 103% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 70% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 100% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 110% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 91% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 111% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 99% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 116% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 106% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 100% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 93% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 86% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 79% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 104% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 124% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 112% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 95% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 126% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 73% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 106% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 107% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 61% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 84% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 107% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 115% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 72% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 94% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 75% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 101% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 117% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 103% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 78% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 93% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 81% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 100% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 120% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 92% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 128% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 86% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 93% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 77% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 12/19/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/07/16 Pct Recovery = 81% Analysis Date = 11/07/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/16/16 Pct Recovery = 81% Analysis Date = 10/16/16 Pct Recovery = 81% Analysis Date = 10/06/16 Pct Recovery = 81% Analysis Date = 10/06/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/13/16 Pct Recovery = 82% Analysis Date = 08/13/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 07/23/16 Pct Recovery = 82% Analysis Date = 07/23/16 Pct Recovery = 82% Analysis Date = 07/12/16 Pct Recovery = 82% Analysis Date = 07/12/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 06/20/16 Pct Recovery = 82% Analysis Date = 06/20/16 Pct Recovery = 82% Analysis Date = 06/10/16 Pct Recovery = 82% Analysis Date = 06/10/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/09/16 Pct Recovery = 83% Analysis Date = 05/09/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/17/16 Pct Recovery = 83% Analysis Date = 04/17/16 Pct Recovery = 83% Analysis Date = 04/06/16 Pct Recovery = 83% Analysis Date = 04/06/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/16/16 Pct Recovery = 83% Analysis Date = 03/16/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 02/24/16 Pct Recovery = 83% Analysis Date = 02/24/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/02/16 Pct Recovery = 84% Analysis Date = 02/02/16 Pct Recovery = 84% Analysis Date = 01/22/16 Pct Recovery = 84% Analysis Date = 01/22/16 Pct Recovery = 84% Analysis Date = 01/12/16 Pct Recovery = 84% Analysis Date = 01/12/16 Pct Recovery = 84% Analysis Date = 01/01/16 Pct Recovery = 84% Analysis Date = 01/01/16 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/21/15 Pct Recovery = 84% Analysis Date = 12/11/15 Pct Recovery = 84% Analysis Date = 12/11/15 Pct Recovery = 84% Analysis Date = 11/30/15 Pct Recovery = 84% Analysis Date = 11/30/15 Pct Recovery = 84% Analysis Date = 11/19/15 Pct Recovery = 84% Analysis Date = 11/19/15 Pct Recovery = 84% Analysis Date = 11/09/15 Pct Recovery = 84% Analysis Date = 11/09/15 Pct Recovery = 84% Analysis Date = 10/29/15 Pct Recovery = 84% Analysis Date = 10/29/15 Pct Recovery = 84% Analysis Date = 10/18/15 Pct Recovery = 85% Analysis Date = 10/18/15 Pct Recovery = 85% Analysis Date = 10/07/15 Pct Recovery = 85% Analysis Date = 10/07/15 Pct Recovery = 85% Analysis Date = 09/27/15 Pct Recovery = 85% Analysis Date = 09/27/15 Pct Recovery = 85% Analysis Date = 09/16/15 Pct Recovery = 85% Analysis Date = 09/16/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 09/05/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/26/15 Pct Recovery = 85% Analysis Date = 08/15/15 Pct Recovery = 85% Analysis Date = 08/15/15 Pct Recovery = 85% Analysis Date = 08/04/15 Pct Recovery = 85% Analysis Date = 08/04/15 Pct Recovery = 85% Analysis Date = 07/24/15 Pct Recovery = 85% Analysis Date = 07/24/15 Pct Recovery = 85% Analysis Date = 07/14/15 Pct Recovery = 85% Analysis Date = 07/14/15 Pct Recovery = 85% Analysis Date = 07/03/15 Pct Recovery = 85% Analysis Date = 07/03/15 Pct Recovery = 85% Analysis Date = 06/22/15 Pct Recovery = 86% Analysis Date = 06/22/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/01/15 Pct Recovery = 86% Analysis Date = 06/01/15 Pct Recovery = 86% Analysis Date = 05/21/15 Pct Recovery = 86% Analysis Date = 05/21/15 Pct Recovery = 86% Analysis Date = 05/10/15 Pct Recovery = 86% Analysis Date = 05/10/15 Pct Recovery = 86% Analysis Date = 04/30/15 Pct Recovery = 86% Analysis Date = 04/30/15 Pct Recovery = 86% Analysis Date = 04/19/15 Pct Recovery = 86% Analysis Date = 04/19/15 Pct Recovery = 86% Analysis Date = 04/08/15 Pct Recovery = 86% Analysis Date = 04/08/15 Pct Recovery = 86% Analysis Date = 03/29/15 Pct Recovery = 87% Analysis Date = 03/29/15 Pct Recovery = 87% Analysis Date = 03/18/15 Pct Recovery = 87% Analysis Date = 03/18/15 Pct Recovery = 87% Analysis Date = 03/07/15 Pct Recovery = 87% Analysis Date = 03/07/15 Pct Recovery = 87% Analysis Date = 02/24/15 Pct Recovery = 87% Analysis Date = 02/24/15 Pct Recovery = 87% Analysis Date = 02/14/15 Pct Recovery = 87% Analysis Date = 02/14/15 Pct Recovery = 87% Analysis Date = 02/03/15 Pct Recovery = 87% Analysis Date = 02/03/15 Pct Recovery = 87% Analysis Date = 01/23/15 Pct Recovery = 87% Analysis Date = 01/23/15 Pct Recovery = 87% Analysis Date = 01/13/15 Pct Recovery = 88% Analysis Date = 01/13/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 88% Analysis Date = 12/12/14 Pct Recovery = 88% Analysis Date = 12/12/14 Pct Recovery = 88% Analysis Date = 12/01/14 Pct Recovery = 88% Analysis Date = 12/01/14 Pct Recovery = 88% Analysis Date = 11/20/14 Pct Recovery = 88% Analysis Date = 11/20/14 Pct Recovery = 88% Analysis Date = 11/09/14 Pct Recovery = 88% Analysis Date = 11/09/14 Pct Recovery = 88% Analysis Date = 10/30/14 Pct Recovery = 89% Analysis Date = 10/30/14 Pct Recovery = 89% Analysis Date = 10/19/14 Pct Recovery = 89% Analysis Date = 10/19/14 Pct Recovery = 89% Analysis Date = 10/08/14 Pct Recovery = 89% Analysis Date = 10/08/14 Pct Recovery = 89% Analysis Date = 09/28/14 Pct Recovery = 89% Analysis Date = 09/28/14 Pct Recovery = 89% Analysis Date = 09/17/14 Pct Recovery = 89% Analysis Date = 09/17/14 Pct Recovery = 89% Analysis Date = 09/06/14 Pct Recovery = 89% Analysis Date = 09/06/14 Pct Recovery = 89% Analysis Date = 08/26/14 Pct Recovery = 89% Analysis Date = 08/26/14 Pct Recovery = 89% Analysis Date = 08/16/14 Pct Recovery = 89% Analysis Date = 08/16/14 Pct Recovery = 89% Analysis Date = 08/05/14 Pct Recovery = 89% Analysis Date = 08/05/14 Pct Recovery = 89% Analysis Date = 07/25/14 Pct Recovery = 89% Analysis Date = 07/25/14 Pct Recovery = 89% Analysis Date = 07/15/14 Pct Recovery = 89% Analysis Date = 07/15/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 06/23/14 Pct Recovery = 89% Analysis Date = 06/23/14 Pct Recovery = 89% Analysis Date = 06/12/14 Pct Recovery = 89% Analysis Date = 06/12/14 Pct Recovery = 89% Analysis Date = 06/02/14 Pct Recovery = 89% Analysis Date = 06/02/14 Pct Recovery = 89% Analysis Date = 05/22/14 Pct Recovery = 89% Analysis Date = 05/22/14 Pct Recovery = 89% Analysis Date = 05/11/14 Pct Recovery = 89% Analysis Date = 05/11/14 Pct Recovery = 89% Analysis Date = 05/01/14 Pct Recovery = 89% Analysis Date = 05/01/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/20/14 Pct Recovery = 89% Analysis Date = 04/09/14 Pct Recovery = 89% Analysis Date = 04/09/14 Pct Recovery = 89% Analysis Date = 03/29/14 Pct Recovery = 89% Analysis Date = 03/29/14 Pct Recovery = 89% Analysis Date = 03/19/14 Pct Recovery = 89% Analysis Date = 03/19/14 Pct Recovery = 89% Analysis Date = 03/08/14 Pct Recovery = 89% Analysis Date = 03/08/14 Pct Recovery = 89% Analysis Date = 02/25/14 Pct Recovery = 89% Analysis Date = 02/25/14 Pct Recovery = 89% Analysis Date = 02/15/14 Pct Recovery = 89% Analysis Date = 02/15/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 89% Analysis Date = 02/04/14 Pct Recovery = 89% Analysis Date = 01/24/14 Pct Recovery = 89% Analysis Date = 01/24/14 Pct Recovery = 89% Analysis Date = 01/13/14 Pct Recovery = 89% Analysis Date = 01/13/14 Pct Recovery = 89% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 12/23/13 Pct Recovery = 89% Analysis Date = 12/23/13 Pct Recovery = 89% Analysis Date = 12/12/13 Pct Recovery = 89% Analysis Date = 12/12/13 Pct Recovery = 89% Analysis Date = 12/02/13 Pct Recovery = 89% Analysis Date = 12/02/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/10/13 Pct Recovery = 89% Analysis Date = 11/10/13 Pct Recovery = 89% Analysis Date = 10/31/13 Pct Recovery = 89% Analysis Date = 10/31/13 Pct Recovery = 89% Analysis Date = 10/20/13 Pct Recovery = 89% Analysis Date = 10/20/13 Pct Recovery = 89% Analysis Date = 10/09/13 Pct Recovery = 89% Analysis Date = 10/09/13 Pct Recovery = 89% Analysis Date = 09/28/13 Pct Recovery = 89% Analysis Date = 09/28/13 Pct Recovery = 89% Analysis Date = 09/18/13 Pct Recovery = 89% Analysis Date = 09/18/13 Pct Recovery = 89% Analysis Date = 09/07/13 Pct Recovery = 89% Analysis Date = 09/07/13 Pct Recovery = 89% Analysis Date = 08/27/13 Pct Recovery = 89% Analysis Date = 08/27/13 Pct Recovery = 89% Analysis Date = 08/17/13 Pct Recovery = 89% Analysis Date = 08/17/13 Pct Recovery = 89% Analysis Date = 08/06/13 Pct Recovery = 89% Analysis Date = 08/06/13 Pct Recovery = 89% Analysis Date = 07/26/13 Pct Recovery = 90% Analysis Date = 07/26/13 Pct Recovery = 90% Analysis Date = 07/15/13 Pct Recovery = 90% Analysis Date = 07/15/13 Pct Recovery = 90% Analysis Date = 07/05/13 Pct Recovery = 90% Analysis Date = 07/05/13 Pct Recovery = 90% Analysis Date = 06/24/13 Pct Recovery = 90% Analysis Date = 06/24/13 Pct Recovery = 90% Analysis Date = 06/13/13 Pct Recovery = 90% Analysis Date = 06/13/13 Pct Recovery = 90% Analysis Date = 06/03/13 Pct Recovery = 90% Analysis Date = 06/03/13 Pct Recovery = 90% Analysis Date = 05/23/13 Pct Recovery = 91% Analysis Date = 05/23/13 Pct Recovery = 91% Analysis Date = 05/12/13 Pct Recovery = 91% Analysis Date = 05/12/13 Pct Recovery = 91% Analysis Date = 05/01/13 Pct Recovery = 91% Analysis Date = 05/01/13 Pct Recovery = 91% Analysis Date = 04/21/13 Pct Recovery = 91% Analysis Date = 04/21/13 Pct Recovery = 91% Analysis Date = 04/10/13 Pct Recovery = 91% Analysis Date = 04/10/13 Pct Recovery = 91% Analysis Date = 03/30/13 Pct Recovery = 91% Analysis Date = 03/30/13 Pct Recovery = 91% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/09/13 Pct Recovery = 92% Analysis Date = 03/09/13 Pct Recovery = 92% Analysis Date = 02/26/13 Pct Recovery = 92% Analysis Date = 02/26/13 Pct Recovery = 92% Analysis Date = 02/15/13 Pct Recovery = 92% Analysis Date = 02/15/13 Pct Recovery = 92% Analysis Date = 02/05/13 Pct Recovery = 92% Analysis Date = 02/05/13 Pct Recovery = 92% Analysis Date = 01/25/13 Pct Recovery = 92% Analysis Date = 01/25/13 Pct Recovery = 92% Analysis Date = 01/14/13 Pct Recovery = 93% Analysis Date = 01/14/13 Pct Recovery = 93% Analysis Date = 01/04/13 Pct Recovery = 93% Analysis Date = 01/04/13 Pct Recovery = 93% Analysis Date = 12/24/12 Pct Recovery = 93% Analysis Date = 12/24/12 Pct Recovery = 93% Analysis Date = 12/13/12 Pct Recovery = 93% Analysis Date = 12/13/12 Pct Recovery = 93% Analysis Date = 12/03/12 Pct Recovery = 94% Analysis Date = 12/03/12 Pct Recovery = 94% Analysis Date = 11/22/12 Pct Recovery = 94% Analysis Date = 11/22/12 Pct Recovery = 94% Analysis Date = 11/11/12 Pct Recovery = 94% Analysis Date = 11/11/12 Pct Recovery = 94% Analysis Date = 10/31/12 Pct Recovery = 94% Analysis Date = 10/31/12 Pct Recovery = 94% Analysis Date = 10/21/12 Pct Recovery = 95% Analysis Date = 10/21/12 Pct Recovery = 95% Analysis Date = 10/10/12 Pct Recovery = 95% Analysis Date = 10/10/12 Pct Recovery = 95% Analysis Date = 09/29/12 Pct Recovery = 95% Analysis Date = 09/29/12 Pct Recovery = 95% Analysis Date = 09/19/12 Pct Recovery = 95% Analysis Date = 09/19/12 Pct Recovery = 95% Analysis Date = 09/08/12 Pct Recovery = 96% Analysis Date = 09/08/12 Pct Recovery = 96% Analysis Date = 08/28/12 Pct Recovery = 96% Analysis Date = 08/28/12 Pct Recovery = 96% Analysis Date = 08/17/12 Pct Recovery = 96% Analysis Date = 08/17/12 Pct Recovery = 96% Analysis Date = 08/07/12 Pct Recovery = 96% Analysis Date = 08/07/12 Pct Recovery = 96% Analysis Date = 07/27/12 Pct Recovery = 97% Analysis Date = 07/27/12 Pct Recovery = 97% Analysis Date = 07/16/12 Pct Recovery = 97% Analysis Date = 07/16/12 Pct Recovery = 97% Analysis Date = 07/06/12 Pct Recovery = 97% Analysis Date = 07/06/12 Pct Recovery = 97% Analysis Date = 06/25/12 Pct Recovery = 97% Analysis Date = 06/25/12 Pct Recovery = 97% Analysis Date = 06/14/12 Pct Recovery = 97% Analysis Date = 06/14/12 Pct Recovery = 97% Analysis Date = 06/03/12 Pct Recovery = 98% Analysis Date = 06/03/12 Pct Recovery = 98% Analysis Date = 05/24/12 Pct Recovery = 98% Analysis Date = 05/24/12 Pct Recovery = 98% Analysis Date = 05/13/12 Pct Recovery = 98% Analysis Date = 05/13/12 Pct Recovery = 98% Analysis Date = 05/02/12 Pct Recovery = 98% Analysis Date = 05/02/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 99% Analysis Date = 04/11/12 Pct Recovery = 99% Analysis Date = 04/11/12 Pct Recovery = 99% Analysis Date = 03/31/12 Pct Recovery = 99% Analysis Date = 03/31/12 Pct Recovery = 99% Analysis Date = 03/20/12 Pct Recovery = 99% Analysis Date = 03/20/12 Pct Recovery = 99% Analysis Date = 03/10/12 Pct Recovery = 100% Analysis Date = 03/10/12 Pct Recovery = 100% Analysis Date = 02/28/12 Pct Recovery = 100% Analysis Date = 02/28/12 Pct Recovery = 100% Analysis Date = 02/17/12 Pct Recovery = 100% Analysis Date = 02/17/12 Pct Recovery = 100% Analysis Date = 02/07/12 Pct Recovery = 100% Analysis Date = 02/07/12 Pct Recovery = 100% Analysis Date = 01/27/12 Pct Recovery = 101% Analysis Date = 01/27/12 Pct Recovery = 101% Analysis Date = 01/16/12 Pct Recovery = 101% Analysis Date = 01/16/12 Pct Recovery = 101% Analysis Date = 01/06/12 Pct Recovery = 101% Analysis Date = 01/06/12 Pct Recovery = 101% Analysis Date = 12/26/11 Pct Recovery = 101% Analysis Date = 12/26/11 Pct Recovery = 101% Analysis Date = 12/15/11 Pct Recovery = 102% Analysis Date = 12/15/11 Pct Recovery = 102% Analysis Date = 12/04/11 Pct Recovery = 102% Analysis Date = 12/04/11 Pct Recovery = 102% Analysis Date = 11/24/11 Pct Recovery = 102% Analysis Date = 11/24/11 Pct Recovery = 102% Analysis Date = 11/13/11 Pct Recovery = 102% Analysis Date = 11/13/11 Pct Recovery = 102% Analysis Date = 11/02/11 Pct Recovery = 103% Analysis Date = 11/02/11 Pct Recovery = 103% Analysis Date = 10/23/11 Pct Recovery = 103% Analysis Date = 10/23/11 Pct Recovery = 103% Analysis Date = 10/12/11 Pct Recovery = 103% Analysis Date = 10/12/11 Pct Recovery = 103% Analysis Date = 10/01/11 Pct Recovery = 103% Analysis Date = 10/01/11 Pct Recovery = 103% Analysis Date = 09/20/11 Pct Recovery = 104% Analysis Date = 09/20/11 Pct Recovery = 104% Analysis Date = 09/10/11 Pct Recovery = 104% Analysis Date = 09/10/11 Pct Recovery = 104% Analysis Date = 08/30/11 Pct Recovery = 104% Analysis Date = 08/30/11 Pct Recovery = 104% Analysis Date = 08/19/11 Pct Recovery = 104% Analysis Date = 08/19/11 Pct Recovery = 104% Analysis Date = 08/09/11 Pct Recovery = 105% Analysis Date = 08/09/11 Pct Recovery = 105% Analysis Date = 07/29/11 Pct Recovery = 105% Analysis Date = 07/29/11 Pct Recovery = 105% Analysis Date = 07/18/11 Pct Recovery = 105% Analysis Date = 07/18/11 Pct Recovery = 105% Analysis Date = 07/07/11 Pct Recovery = 105% Analysis Date = 07/07/11 Pct Recovery = 105% Analysis Date = 06/27/11 Pct Recovery = 105% Analysis Date = 06/27/11 Pct Recovery = 105% Analysis Date = 06/16/11 Pct Recovery = 106% Analysis Date = 06/16/11 Pct Recovery = 106% Analysis Date = 06/05/11 Pct Recovery = 106% Analysis Date = 06/05/11 Pct Recovery = 106% Analysis Date = 05/26/11 Pct Recovery = 106% Analysis Date = 05/26/11 Pct Recovery = 106% Analysis Date = 05/15/11 Pct Recovery = 106% Analysis Date = 05/15/11 Pct Recovery = 106% Analysis Date = 05/04/11 Pct Recovery = 107% Analysis Date = 05/04/11 Pct Recovery = 107% Analysis Date = 04/23/11 Pct Recovery = 107% Analysis Date = 04/23/11 Pct Recovery = 107% Analysis Date = 04/13/11 Pct Recovery = 107% Analysis Date = 04/13/11 Pct Recovery = 107% Analysis Date = 04/02/11 Pct Recovery = 107% Analysis Date = 04/02/11 Pct Recovery = 107% Analysis Date = 03/22/11 Pct Recovery = 107% Analysis Date = 03/22/11 Pct Recovery = 107% Analysis Date = 03/12/11 Pct Recovery = 108% Analysis Date = 03/12/11 Pct Recovery = 108% Analysis Date = 03/01/11 Pct Recovery = 108% Analysis Date = 03/01/11 Pct Recovery = 108% Analysis Date = 02/18/11 Pct Recovery = 108% Analysis Date = 02/18/11 Pct Recovery = 108% Analysis Date = 02/08/11 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHOPROPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 77 93% 16% 93% 19%
Total 77 93% 16% 93% 19%

Sample Statistics
ETHOPROPHOS

Characteristic N % % Basis
Plotted 77 89% Spiked
Estimated Values 11 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 3% Spiked
Spiked 87 .  
False Negatives 7 8% 7 out of 87
Not Spiked 82 .  
False Positives 2 2% 2 out of 82

BQS OBSP Determination:
FENAMIPHOS
METHOD: 2033 , TESTIDCODE: 61591GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 58% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 42% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 68% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 69% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 61% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 27% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 49% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 76% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 49% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 95% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 83% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 34% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 80% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 84% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 86% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 73% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 103% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 76% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 85% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 72% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 76% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 64% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 89% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 57% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 76% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 68% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 78% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 68% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 3% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 57% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 72% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 115% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 86% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 71% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 108% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 77% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 97% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 46% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 82% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 98% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 84% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 94% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 143% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 87% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 87% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 25% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 83% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 100% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 118% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 53% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 11% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 76% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 79% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 61% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 75% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 91% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 63% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 62% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 64% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 79% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 80% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 103% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 109% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 104% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 88% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 73% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 117% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 104% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 78% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 96% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 139% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 104% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 87% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 114% Analysis Date = 01/17/17 Pct Recovery = 97% Analysis Date = 01/07/17 Pct Recovery = 97% Analysis Date = 01/07/17 Pct Recovery = 97% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/05/16 Pct Recovery = 96% Analysis Date = 12/05/16 Pct Recovery = 96% Analysis Date = 11/24/16 Pct Recovery = 96% Analysis Date = 11/24/16 Pct Recovery = 96% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/03/16 Pct Recovery = 95% Analysis Date = 11/03/16 Pct Recovery = 95% Analysis Date = 10/23/16 Pct Recovery = 95% Analysis Date = 10/23/16 Pct Recovery = 95% Analysis Date = 10/12/16 Pct Recovery = 94% Analysis Date = 10/12/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/20/16 Pct Recovery = 94% Analysis Date = 09/09/16 Pct Recovery = 94% Analysis Date = 09/09/16 Pct Recovery = 94% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 92% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/02/16 Pct Recovery = 91% Analysis Date = 05/02/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 90% Analysis Date = 04/21/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/16/16 Pct Recovery = 89% Analysis Date = 02/16/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 02/05/16 Pct Recovery = 88% Analysis Date = 01/25/16 Pct Recovery = 88% Analysis Date = 01/25/16 Pct Recovery = 88% Analysis Date = 01/15/16 Pct Recovery = 88% Analysis Date = 01/15/16 Pct Recovery = 88% Analysis Date = 01/04/16 Pct Recovery = 88% Analysis Date = 01/04/16 Pct Recovery = 88% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/24/15 Pct Recovery = 87% Analysis Date = 12/13/15 Pct Recovery = 87% Analysis Date = 12/13/15 Pct Recovery = 87% Analysis Date = 12/02/15 Pct Recovery = 87% Analysis Date = 12/02/15 Pct Recovery = 87% Analysis Date = 11/21/15 Pct Recovery = 87% Analysis Date = 11/21/15 Pct Recovery = 87% Analysis Date = 11/10/15 Pct Recovery = 86% Analysis Date = 11/10/15 Pct Recovery = 86% Analysis Date = 10/31/15 Pct Recovery = 86% Analysis Date = 10/31/15 Pct Recovery = 86% Analysis Date = 10/20/15 Pct Recovery = 86% Analysis Date = 10/20/15 Pct Recovery = 86% Analysis Date = 10/09/15 Pct Recovery = 86% Analysis Date = 10/09/15 Pct Recovery = 86% Analysis Date = 09/28/15 Pct Recovery = 85% Analysis Date = 09/28/15 Pct Recovery = 85% Analysis Date = 09/17/15 Pct Recovery = 85% Analysis Date = 09/17/15 Pct Recovery = 85% Analysis Date = 09/06/15 Pct Recovery = 85% Analysis Date = 09/06/15 Pct Recovery = 85% Analysis Date = 08/27/15 Pct Recovery = 85% Analysis Date = 08/27/15 Pct Recovery = 85% Analysis Date = 08/16/15 Pct Recovery = 84% Analysis Date = 08/16/15 Pct Recovery = 84% Analysis Date = 08/05/15 Pct Recovery = 84% Analysis Date = 08/05/15 Pct Recovery = 84% Analysis Date = 07/25/15 Pct Recovery = 84% Analysis Date = 07/25/15 Pct Recovery = 84% Analysis Date = 07/14/15 Pct Recovery = 84% Analysis Date = 07/14/15 Pct Recovery = 84% Analysis Date = 07/03/15 Pct Recovery = 83% Analysis Date = 07/03/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/12/15 Pct Recovery = 83% Analysis Date = 06/01/15 Pct Recovery = 83% Analysis Date = 06/01/15 Pct Recovery = 83% Analysis Date = 05/21/15 Pct Recovery = 82% Analysis Date = 05/21/15 Pct Recovery = 82% Analysis Date = 05/10/15 Pct Recovery = 82% Analysis Date = 05/10/15 Pct Recovery = 82% Analysis Date = 04/29/15 Pct Recovery = 82% Analysis Date = 04/29/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/18/15 Pct Recovery = 82% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/28/15 Pct Recovery = 81% Analysis Date = 03/17/15 Pct Recovery = 81% Analysis Date = 03/17/15 Pct Recovery = 81% Analysis Date = 03/06/15 Pct Recovery = 81% Analysis Date = 03/06/15 Pct Recovery = 81% Analysis Date = 02/23/15 Pct Recovery = 80% Analysis Date = 02/23/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/01/15 Pct Recovery = 80% Analysis Date = 02/01/15 Pct Recovery = 80% Analysis Date = 01/22/15 Pct Recovery = 80% Analysis Date = 01/22/15 Pct Recovery = 80% Analysis Date = 01/11/15 Pct Recovery = 79% Analysis Date = 01/11/15 Pct Recovery = 79% Analysis Date = 12/31/14 Pct Recovery = 79% Analysis Date = 12/31/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 79% Analysis Date = 12/09/14 Pct Recovery = 79% Analysis Date = 12/09/14 Pct Recovery = 79% Analysis Date = 11/28/14 Pct Recovery = 78% Analysis Date = 11/28/14 Pct Recovery = 78% Analysis Date = 11/17/14 Pct Recovery = 78% Analysis Date = 11/17/14 Pct Recovery = 78% Analysis Date = 11/07/14 Pct Recovery = 78% Analysis Date = 11/07/14 Pct Recovery = 78% Analysis Date = 10/27/14 Pct Recovery = 78% Analysis Date = 10/27/14 Pct Recovery = 78% Analysis Date = 10/16/14 Pct Recovery = 77% Analysis Date = 10/16/14 Pct Recovery = 77% Analysis Date = 10/05/14 Pct Recovery = 77% Analysis Date = 10/05/14 Pct Recovery = 77% Analysis Date = 09/24/14 Pct Recovery = 77% Analysis Date = 09/24/14 Pct Recovery = 77% Analysis Date = 09/13/14 Pct Recovery = 77% Analysis Date = 09/13/14 Pct Recovery = 77% Analysis Date = 09/02/14 Pct Recovery = 77% Analysis Date = 09/02/14 Pct Recovery = 77% Analysis Date = 08/23/14 Pct Recovery = 76% Analysis Date = 08/23/14 Pct Recovery = 76% Analysis Date = 08/12/14 Pct Recovery = 76% Analysis Date = 08/12/14 Pct Recovery = 76% Analysis Date = 08/01/14 Pct Recovery = 76% Analysis Date = 08/01/14 Pct Recovery = 76% Analysis Date = 07/21/14 Pct Recovery = 76% Analysis Date = 07/21/14 Pct Recovery = 76% Analysis Date = 07/10/14 Pct Recovery = 76% Analysis Date = 07/10/14 Pct Recovery = 76% Analysis Date = 06/29/14 Pct Recovery = 75% Analysis Date = 06/29/14 Pct Recovery = 75% Analysis Date = 06/19/14 Pct Recovery = 75% Analysis Date = 06/19/14 Pct Recovery = 75% Analysis Date = 06/08/14 Pct Recovery = 74% Analysis Date = 06/08/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 74% Analysis Date = 05/17/14 Pct Recovery = 73% Analysis Date = 05/17/14 Pct Recovery = 73% Analysis Date = 05/06/14 Pct Recovery = 73% Analysis Date = 05/06/14 Pct Recovery = 73% Analysis Date = 04/25/14 Pct Recovery = 72% Analysis Date = 04/25/14 Pct Recovery = 72% Analysis Date = 04/14/14 Pct Recovery = 72% Analysis Date = 04/14/14 Pct Recovery = 72% Analysis Date = 04/04/14 Pct Recovery = 71% Analysis Date = 04/04/14 Pct Recovery = 71% Analysis Date = 03/24/14 Pct Recovery = 71% Analysis Date = 03/24/14 Pct Recovery = 71% Analysis Date = 03/13/14 Pct Recovery = 70% Analysis Date = 03/13/14 Pct Recovery = 70% Analysis Date = 03/02/14 Pct Recovery = 70% Analysis Date = 03/02/14 Pct Recovery = 70% Analysis Date = 02/19/14 Pct Recovery = 69% Analysis Date = 02/19/14 Pct Recovery = 69% Analysis Date = 02/08/14 Pct Recovery = 69% Analysis Date = 02/08/14 Pct Recovery = 69% Analysis Date = 01/28/14 Pct Recovery = 68% Analysis Date = 01/28/14 Pct Recovery = 68% Analysis Date = 01/18/14 Pct Recovery = 68% Analysis Date = 01/18/14 Pct Recovery = 68% Analysis Date = 01/07/14 Pct Recovery = 68% Analysis Date = 01/07/14 Pct Recovery = 68% Analysis Date = 12/27/13 Pct Recovery = 67% Analysis Date = 12/27/13 Pct Recovery = 67% Analysis Date = 12/16/13 Pct Recovery = 67% Analysis Date = 12/16/13 Pct Recovery = 67% Analysis Date = 12/05/13 Pct Recovery = 66% Analysis Date = 12/05/13 Pct Recovery = 66% Analysis Date = 11/24/13 Pct Recovery = 66% Analysis Date = 11/24/13 Pct Recovery = 66% Analysis Date = 11/14/13 Pct Recovery = 66% Analysis Date = 11/14/13 Pct Recovery = 66% Analysis Date = 11/03/13 Pct Recovery = 65% Analysis Date = 11/03/13 Pct Recovery = 65% Analysis Date = 10/23/13 Pct Recovery = 65% Analysis Date = 10/23/13 Pct Recovery = 65% Analysis Date = 10/12/13 Pct Recovery = 65% Analysis Date = 10/12/13 Pct Recovery = 65% Analysis Date = 10/01/13 Pct Recovery = 64% Analysis Date = 10/01/13 Pct Recovery = 64% Analysis Date = 09/20/13 Pct Recovery = 64% Analysis Date = 09/20/13 Pct Recovery = 64% Analysis Date = 09/09/13 Pct Recovery = 63% Analysis Date = 09/09/13 Pct Recovery = 63% Analysis Date = 08/30/13 Pct Recovery = 63% Analysis Date = 08/30/13 Pct Recovery = 63% Analysis Date = 08/19/13 Pct Recovery = 63% Analysis Date = 08/19/13 Pct Recovery = 63% Analysis Date = 08/08/13 Pct Recovery = 63% Analysis Date = 08/08/13 Pct Recovery = 63% Analysis Date = 07/28/13 Pct Recovery = 63% Analysis Date = 07/28/13 Pct Recovery = 63% Analysis Date = 07/17/13 Pct Recovery = 62% Analysis Date = 07/17/13 Pct Recovery = 62% Analysis Date = 07/06/13 Pct Recovery = 62% Analysis Date = 07/06/13 Pct Recovery = 62% Analysis Date = 06/25/13 Pct Recovery = 62% Analysis Date = 06/25/13 Pct Recovery = 62% Analysis Date = 06/15/13 Pct Recovery = 62% Analysis Date = 06/15/13 Pct Recovery = 62% Analysis Date = 06/04/13 Pct Recovery = 62% Analysis Date = 06/04/13 Pct Recovery = 62% Analysis Date = 05/24/13 Pct Recovery = 62% Analysis Date = 05/24/13 Pct Recovery = 62% Analysis Date = 05/13/13 Pct Recovery = 62% Analysis Date = 05/13/13 Pct Recovery = 62% Analysis Date = 05/02/13 Pct Recovery = 62% Analysis Date = 05/02/13 Pct Recovery = 62% Analysis Date = 04/21/13 Pct Recovery = 62% Analysis Date = 04/21/13 Pct Recovery = 62% Analysis Date = 04/11/13 Pct Recovery = 62% Analysis Date = 04/11/13 Pct Recovery = 62% Analysis Date = 03/31/13 Pct Recovery = 62% Analysis Date = 03/31/13 Pct Recovery = 62% Analysis Date = 03/20/13 Pct Recovery = 62% Analysis Date = 03/20/13 Pct Recovery = 62% Analysis Date = 03/09/13 Pct Recovery = 62% Analysis Date = 03/09/13 Pct Recovery = 62% Analysis Date = 02/26/13 Pct Recovery = 62% Analysis Date = 02/26/13 Pct Recovery = 62% Analysis Date = 02/15/13 Pct Recovery = 62% Analysis Date = 02/15/13 Pct Recovery = 62% Analysis Date = 02/04/13 Pct Recovery = 62% Analysis Date = 02/04/13 Pct Recovery = 62% Analysis Date = 01/25/13 Pct Recovery = 62% Analysis Date = 01/25/13 Pct Recovery = 62% Analysis Date = 01/14/13 Pct Recovery = 62% Analysis Date = 01/14/13 Pct Recovery = 62% Analysis Date = 01/03/13 Pct Recovery = 63% Analysis Date = 01/03/13 Pct Recovery = 63% Analysis Date = 12/23/12 Pct Recovery = 63% Analysis Date = 12/23/12 Pct Recovery = 63% Analysis Date = 12/12/12 Pct Recovery = 63% Analysis Date = 12/12/12 Pct Recovery = 63% Analysis Date = 12/01/12 Pct Recovery = 64% Analysis Date = 12/01/12 Pct Recovery = 64% Analysis Date = 11/20/12 Pct Recovery = 64% Analysis Date = 11/20/12 Pct Recovery = 64% Analysis Date = 11/10/12 Pct Recovery = 65% Analysis Date = 11/10/12 Pct Recovery = 65% Analysis Date = 10/30/12 Pct Recovery = 65% Analysis Date = 10/30/12 Pct Recovery = 65% Analysis Date = 10/19/12 Pct Recovery = 66% Analysis Date = 10/19/12 Pct Recovery = 66% Analysis Date = 10/08/12 Pct Recovery = 66% Analysis Date = 10/08/12 Pct Recovery = 66% Analysis Date = 09/27/12 Pct Recovery = 67% Analysis Date = 09/27/12 Pct Recovery = 67% Analysis Date = 09/16/12 Pct Recovery = 67% Analysis Date = 09/16/12 Pct Recovery = 67% Analysis Date = 09/06/12 Pct Recovery = 68% Analysis Date = 09/06/12 Pct Recovery = 68% Analysis Date = 08/26/12 Pct Recovery = 69% Analysis Date = 08/26/12 Pct Recovery = 69% Analysis Date = 08/15/12 Pct Recovery = 69% Analysis Date = 08/15/12 Pct Recovery = 69% Analysis Date = 08/04/12 Pct Recovery = 70% Analysis Date = 08/04/12 Pct Recovery = 70% Analysis Date = 07/24/12 Pct Recovery = 71% Analysis Date = 07/24/12 Pct Recovery = 71% Analysis Date = 07/13/12 Pct Recovery = 71% Analysis Date = 07/13/12 Pct Recovery = 71% Analysis Date = 07/02/12 Pct Recovery = 72% Analysis Date = 07/02/12 Pct Recovery = 72% Analysis Date = 06/22/12 Pct Recovery = 72% Analysis Date = 06/22/12 Pct Recovery = 72% Analysis Date = 06/11/12 Pct Recovery = 73% Analysis Date = 06/11/12 Pct Recovery = 73% Analysis Date = 05/31/12 Pct Recovery = 74% Analysis Date = 05/31/12 Pct Recovery = 74% Analysis Date = 05/20/12 Pct Recovery = 74% Analysis Date = 05/20/12 Pct Recovery = 74% Analysis Date = 05/09/12 Pct Recovery = 75% Analysis Date = 05/09/12 Pct Recovery = 75% Analysis Date = 04/28/12 Pct Recovery = 76% Analysis Date = 04/28/12 Pct Recovery = 76% Analysis Date = 04/17/12 Pct Recovery = 76% Analysis Date = 04/17/12 Pct Recovery = 76% Analysis Date = 04/07/12 Pct Recovery = 77% Analysis Date = 04/07/12 Pct Recovery = 77% Analysis Date = 03/27/12 Pct Recovery = 78% Analysis Date = 03/27/12 Pct Recovery = 78% Analysis Date = 03/16/12 Pct Recovery = 78% Analysis Date = 03/16/12 Pct Recovery = 78% Analysis Date = 03/05/12 Pct Recovery = 79% Analysis Date = 03/05/12 Pct Recovery = 79% Analysis Date = 02/23/12 Pct Recovery = 80% Analysis Date = 02/23/12 Pct Recovery = 80% Analysis Date = 02/12/12 Pct Recovery = 80% Analysis Date = 02/12/12 Pct Recovery = 80% Analysis Date = 02/02/12 Pct Recovery = 81% Analysis Date = 02/02/12 Pct Recovery = 81% Analysis Date = 01/22/12 Pct Recovery = 82% Analysis Date = 01/22/12 Pct Recovery = 82% Analysis Date = 01/11/12 Pct Recovery = 82% Analysis Date = 01/11/12 Pct Recovery = 82% Analysis Date = 12/31/11 Pct Recovery = 83% Analysis Date = 12/31/11 Pct Recovery = 83% Analysis Date = 12/20/11 Pct Recovery = 84% Analysis Date = 12/20/11 Pct Recovery = 84% Analysis Date = 12/09/11 Pct Recovery = 85% Analysis Date = 12/09/11 Pct Recovery = 85% Analysis Date = 11/28/11 Pct Recovery = 85% Analysis Date = 11/28/11 Pct Recovery = 85% Analysis Date = 11/18/11 Pct Recovery = 86% Analysis Date = 11/18/11 Pct Recovery = 86% Analysis Date = 11/07/11 Pct Recovery = 87% Analysis Date = 11/07/11 Pct Recovery = 87% Analysis Date = 10/27/11 Pct Recovery = 87% Analysis Date = 10/27/11 Pct Recovery = 87% Analysis Date = 10/16/11 Pct Recovery = 88% Analysis Date = 10/16/11 Pct Recovery = 88% Analysis Date = 10/05/11 Pct Recovery = 89% Analysis Date = 10/05/11 Pct Recovery = 89% Analysis Date = 09/24/11 Pct Recovery = 89% Analysis Date = 09/24/11 Pct Recovery = 89% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/03/11 Pct Recovery = 91% Analysis Date = 09/03/11 Pct Recovery = 91% Analysis Date = 08/23/11 Pct Recovery = 91% Analysis Date = 08/23/11 Pct Recovery = 91% Analysis Date = 08/12/11 Pct Recovery = 92% Analysis Date = 08/12/11 Pct Recovery = 92% Analysis Date = 08/01/11 Pct Recovery = 93% Analysis Date = 08/01/11 Pct Recovery = 93% Analysis Date = 07/21/11 Pct Recovery = 94% Analysis Date = 07/21/11 Pct Recovery = 94% Analysis Date = 07/10/11 Pct Recovery = 94% Analysis Date = 07/10/11 Pct Recovery = 94% Analysis Date = 06/30/11 Pct Recovery = 95% Analysis Date = 06/30/11 Pct Recovery = 95% Analysis Date = 06/19/11 Pct Recovery = 96% Analysis Date = 06/19/11 Pct Recovery = 96% Analysis Date = 06/08/11 Pct Recovery = 96% Analysis Date = 06/08/11 Pct Recovery = 96% Analysis Date = 05/28/11 Pct Recovery = 97% Analysis Date = 05/28/11 Pct Recovery = 97% Analysis Date = 05/17/11 Pct Recovery = 98% Analysis Date = 05/17/11 Pct Recovery = 98% Analysis Date = 05/06/11 Pct Recovery = 98% Analysis Date = 05/06/11 Pct Recovery = 98% Analysis Date = 04/25/11 Pct Recovery = 99% Analysis Date = 04/25/11 Pct Recovery = 99% Analysis Date = 04/15/11 Pct Recovery = 99% Analysis Date = 04/15/11 Pct Recovery = 99% Analysis Date = 04/04/11 Pct Recovery = 100% Analysis Date = 04/04/11 Pct Recovery = 100% Analysis Date = 03/24/11 Pct Recovery = 101% Analysis Date = 03/24/11 Pct Recovery = 101% Analysis Date = 03/13/11 Pct Recovery = 101% Analysis Date = 03/13/11 Pct Recovery = 101% Analysis Date = 03/02/11 Pct Recovery = 102% Analysis Date = 03/02/11 Pct Recovery = 102% Analysis Date = 02/19/11 Pct Recovery = 103% Analysis Date = 02/19/11 Pct Recovery = 103% Analysis Date = 02/09/11 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 114% . 114% 0%
>= Reporting Level 86 78% 24% 77% 17%
Total 87 78% 24% 78% 17%

Sample Statistics
FENAMIPHOS

Characteristic N % % Basis
Plotted 87 97% Spiked
Estimated Values 1 1% Spiked
Deleted Values 4 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 3 3% 3 out of 90
Not Spiked 76 .  
False Positives 1 1% 1 out of 75

BQS OBSP Determination:
FENAMIPHOS SULFONE
METHOD: 2033 , TESTIDCODE: 61645GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 79% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 81% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 84% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 66% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 70% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 68% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 71% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 43% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 59% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 59% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 40% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 37% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 68% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 73% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 70% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 54% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 59% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 64% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 58% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 76% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 80% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 75% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 92% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 85% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 78% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 75% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 75% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 77% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 77% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 75% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 57% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 67% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 85% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 90% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 95% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 70% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 95% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 69% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 69% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 54% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 75% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 89% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 44% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 74% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 52% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 76% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 132% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 101% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 96% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 85% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 48% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 160% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 108% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 121% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 69% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 128% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 110% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 97% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 112% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 75% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 118% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 93% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 148% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 78% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 119% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 88% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 82% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 97% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 88% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 79% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 79% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 65% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 151% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 147% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 120% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 108% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 95% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 81% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 196% Analysis Date = 01/17/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/16/16 Pct Recovery = 82% Analysis Date = 12/16/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/13/16 Pct Recovery = 81% Analysis Date = 11/13/16 Pct Recovery = 81% Analysis Date = 11/03/16 Pct Recovery = 81% Analysis Date = 11/03/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/12/16 Pct Recovery = 81% Analysis Date = 10/12/16 Pct Recovery = 81% Analysis Date = 10/01/16 Pct Recovery = 80% Analysis Date = 10/01/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/20/16 Pct Recovery = 80% Analysis Date = 09/09/16 Pct Recovery = 80% Analysis Date = 09/09/16 Pct Recovery = 80% Analysis Date = 08/29/16 Pct Recovery = 80% Analysis Date = 08/29/16 Pct Recovery = 80% Analysis Date = 08/19/16 Pct Recovery = 79% Analysis Date = 08/19/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 07/28/16 Pct Recovery = 79% Analysis Date = 07/28/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/06/16 Pct Recovery = 78% Analysis Date = 07/06/16 Pct Recovery = 78% Analysis Date = 06/25/16 Pct Recovery = 78% Analysis Date = 06/25/16 Pct Recovery = 78% Analysis Date = 06/14/16 Pct Recovery = 78% Analysis Date = 06/14/16 Pct Recovery = 78% Analysis Date = 06/04/16 Pct Recovery = 78% Analysis Date = 06/04/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/13/16 Pct Recovery = 77% Analysis Date = 05/13/16 Pct Recovery = 77% Analysis Date = 05/02/16 Pct Recovery = 77% Analysis Date = 05/02/16 Pct Recovery = 77% Analysis Date = 04/21/16 Pct Recovery = 77% Analysis Date = 04/21/16 Pct Recovery = 77% Analysis Date = 04/10/16 Pct Recovery = 77% Analysis Date = 04/10/16 Pct Recovery = 77% Analysis Date = 03/31/16 Pct Recovery = 76% Analysis Date = 03/31/16 Pct Recovery = 76% Analysis Date = 03/20/16 Pct Recovery = 76% Analysis Date = 03/20/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 76% Analysis Date = 02/16/16 Pct Recovery = 76% Analysis Date = 02/16/16 Pct Recovery = 76% Analysis Date = 02/05/16 Pct Recovery = 75% Analysis Date = 02/05/16 Pct Recovery = 75% Analysis Date = 01/25/16 Pct Recovery = 75% Analysis Date = 01/25/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/04/16 Pct Recovery = 75% Analysis Date = 01/04/16 Pct Recovery = 75% Analysis Date = 12/24/15 Pct Recovery = 75% Analysis Date = 12/24/15 Pct Recovery = 75% Analysis Date = 12/13/15 Pct Recovery = 74% Analysis Date = 12/13/15 Pct Recovery = 74% Analysis Date = 12/02/15 Pct Recovery = 74% Analysis Date = 12/02/15 Pct Recovery = 74% Analysis Date = 11/21/15 Pct Recovery = 74% Analysis Date = 11/21/15 Pct Recovery = 74% Analysis Date = 11/10/15 Pct Recovery = 74% Analysis Date = 11/10/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 74% Analysis Date = 10/31/15 Pct Recovery = 74% Analysis Date = 10/20/15 Pct Recovery = 74% Analysis Date = 10/20/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 73% Analysis Date = 10/09/15 Pct Recovery = 73% Analysis Date = 09/28/15 Pct Recovery = 73% Analysis Date = 09/28/15 Pct Recovery = 73% Analysis Date = 09/17/15 Pct Recovery = 73% Analysis Date = 09/17/15 Pct Recovery = 73% Analysis Date = 09/06/15 Pct Recovery = 73% Analysis Date = 09/06/15 Pct Recovery = 73% Analysis Date = 08/27/15 Pct Recovery = 73% Analysis Date = 08/27/15 Pct Recovery = 73% Analysis Date = 08/16/15 Pct Recovery = 72% Analysis Date = 08/16/15 Pct Recovery = 72% Analysis Date = 08/05/15 Pct Recovery = 72% Analysis Date = 08/05/15 Pct Recovery = 72% Analysis Date = 07/25/15 Pct Recovery = 72% Analysis Date = 07/25/15 Pct Recovery = 72% Analysis Date = 07/14/15 Pct Recovery = 72% Analysis Date = 07/14/15 Pct Recovery = 72% Analysis Date = 07/03/15 Pct Recovery = 72% Analysis Date = 07/03/15 Pct Recovery = 72% Analysis Date = 06/22/15 Pct Recovery = 72% Analysis Date = 06/22/15 Pct Recovery = 72% Analysis Date = 06/12/15 Pct Recovery = 72% Analysis Date = 06/12/15 Pct Recovery = 72% Analysis Date = 06/01/15 Pct Recovery = 71% Analysis Date = 06/01/15 Pct Recovery = 71% Analysis Date = 05/21/15 Pct Recovery = 71% Analysis Date = 05/21/15 Pct Recovery = 71% Analysis Date = 05/10/15 Pct Recovery = 71% Analysis Date = 05/10/15 Pct Recovery = 71% Analysis Date = 04/29/15 Pct Recovery = 71% Analysis Date = 04/29/15 Pct Recovery = 71% Analysis Date = 04/18/15 Pct Recovery = 71% Analysis Date = 04/18/15 Pct Recovery = 71% Analysis Date = 04/07/15 Pct Recovery = 71% Analysis Date = 04/07/15 Pct Recovery = 71% Analysis Date = 03/28/15 Pct Recovery = 70% Analysis Date = 03/28/15 Pct Recovery = 70% Analysis Date = 03/17/15 Pct Recovery = 70% Analysis Date = 03/17/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 03/06/15 Pct Recovery = 70% Analysis Date = 02/23/15 Pct Recovery = 70% Analysis Date = 02/23/15 Pct Recovery = 70% Analysis Date = 02/12/15 Pct Recovery = 70% Analysis Date = 02/12/15 Pct Recovery = 70% Analysis Date = 02/01/15 Pct Recovery = 70% Analysis Date = 02/01/15 Pct Recovery = 70% Analysis Date = 01/22/15 Pct Recovery = 70% Analysis Date = 01/22/15 Pct Recovery = 70% Analysis Date = 01/11/15 Pct Recovery = 71% Analysis Date = 01/11/15 Pct Recovery = 71% Analysis Date = 12/31/14 Pct Recovery = 71% Analysis Date = 12/31/14 Pct Recovery = 71% Analysis Date = 12/20/14 Pct Recovery = 71% Analysis Date = 12/20/14 Pct Recovery = 71% Analysis Date = 12/09/14 Pct Recovery = 71% Analysis Date = 12/09/14 Pct Recovery = 71% Analysis Date = 11/28/14 Pct Recovery = 71% Analysis Date = 11/28/14 Pct Recovery = 71% Analysis Date = 11/17/14 Pct Recovery = 71% Analysis Date = 11/17/14 Pct Recovery = 71% Analysis Date = 11/07/14 Pct Recovery = 72% Analysis Date = 11/07/14 Pct Recovery = 72% Analysis Date = 10/27/14 Pct Recovery = 72% Analysis Date = 10/27/14 Pct Recovery = 72% Analysis Date = 10/16/14 Pct Recovery = 72% Analysis Date = 10/16/14 Pct Recovery = 72% Analysis Date = 10/05/14 Pct Recovery = 72% Analysis Date = 10/05/14 Pct Recovery = 72% Analysis Date = 09/24/14 Pct Recovery = 72% Analysis Date = 09/24/14 Pct Recovery = 72% Analysis Date = 09/13/14 Pct Recovery = 72% Analysis Date = 09/13/14 Pct Recovery = 72% Analysis Date = 09/02/14 Pct Recovery = 72% Analysis Date = 09/02/14 Pct Recovery = 72% Analysis Date = 08/23/14 Pct Recovery = 73% Analysis Date = 08/23/14 Pct Recovery = 73% Analysis Date = 08/12/14 Pct Recovery = 73% Analysis Date = 08/12/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 08/01/14 Pct Recovery = 73% Analysis Date = 07/21/14 Pct Recovery = 73% Analysis Date = 07/21/14 Pct Recovery = 73% Analysis Date = 07/10/14 Pct Recovery = 73% Analysis Date = 07/10/14 Pct Recovery = 73% Analysis Date = 06/29/14 Pct Recovery = 73% Analysis Date = 06/29/14 Pct Recovery = 73% Analysis Date = 06/19/14 Pct Recovery = 74% Analysis Date = 06/19/14 Pct Recovery = 74% Analysis Date = 06/08/14 Pct Recovery = 74% Analysis Date = 06/08/14 Pct Recovery = 74% Analysis Date = 05/28/14 Pct Recovery = 75% Analysis Date = 05/28/14 Pct Recovery = 75% Analysis Date = 05/17/14 Pct Recovery = 75% Analysis Date = 05/17/14 Pct Recovery = 75% Analysis Date = 05/06/14 Pct Recovery = 75% Analysis Date = 05/06/14 Pct Recovery = 75% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/25/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/14/14 Pct Recovery = 76% Analysis Date = 04/04/14 Pct Recovery = 77% Analysis Date = 04/04/14 Pct Recovery = 77% Analysis Date = 03/24/14 Pct Recovery = 77% Analysis Date = 03/24/14 Pct Recovery = 77% Analysis Date = 03/13/14 Pct Recovery = 78% Analysis Date = 03/13/14 Pct Recovery = 78% Analysis Date = 03/02/14 Pct Recovery = 78% Analysis Date = 03/02/14 Pct Recovery = 78% Analysis Date = 02/19/14 Pct Recovery = 79% Analysis Date = 02/19/14 Pct Recovery = 79% Analysis Date = 02/08/14 Pct Recovery = 79% Analysis Date = 02/08/14 Pct Recovery = 79% Analysis Date = 01/28/14 Pct Recovery = 79% Analysis Date = 01/28/14 Pct Recovery = 79% Analysis Date = 01/18/14 Pct Recovery = 80% Analysis Date = 01/18/14 Pct Recovery = 80% Analysis Date = 01/07/14 Pct Recovery = 80% Analysis Date = 01/07/14 Pct Recovery = 80% Analysis Date = 12/27/13 Pct Recovery = 81% Analysis Date = 12/27/13 Pct Recovery = 81% Analysis Date = 12/16/13 Pct Recovery = 81% Analysis Date = 12/16/13 Pct Recovery = 81% Analysis Date = 12/05/13 Pct Recovery = 81% Analysis Date = 12/05/13 Pct Recovery = 81% Analysis Date = 11/24/13 Pct Recovery = 82% Analysis Date = 11/24/13 Pct Recovery = 82% Analysis Date = 11/14/13 Pct Recovery = 82% Analysis Date = 11/14/13 Pct Recovery = 82% Analysis Date = 11/03/13 Pct Recovery = 83% Analysis Date = 11/03/13 Pct Recovery = 83% Analysis Date = 10/23/13 Pct Recovery = 83% Analysis Date = 10/23/13 Pct Recovery = 83% Analysis Date = 10/12/13 Pct Recovery = 83% Analysis Date = 10/12/13 Pct Recovery = 83% Analysis Date = 10/01/13 Pct Recovery = 84% Analysis Date = 10/01/13 Pct Recovery = 84% Analysis Date = 09/20/13 Pct Recovery = 84% Analysis Date = 09/20/13 Pct Recovery = 84% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 08/30/13 Pct Recovery = 85% Analysis Date = 08/30/13 Pct Recovery = 85% Analysis Date = 08/19/13 Pct Recovery = 86% Analysis Date = 08/19/13 Pct Recovery = 86% Analysis Date = 08/08/13 Pct Recovery = 86% Analysis Date = 08/08/13 Pct Recovery = 86% Analysis Date = 07/28/13 Pct Recovery = 86% Analysis Date = 07/28/13 Pct Recovery = 86% Analysis Date = 07/17/13 Pct Recovery = 87% Analysis Date = 07/17/13 Pct Recovery = 87% Analysis Date = 07/06/13 Pct Recovery = 87% Analysis Date = 07/06/13 Pct Recovery = 87% Analysis Date = 06/25/13 Pct Recovery = 88% Analysis Date = 06/25/13 Pct Recovery = 88% Analysis Date = 06/15/13 Pct Recovery = 88% Analysis Date = 06/15/13 Pct Recovery = 88% Analysis Date = 06/04/13 Pct Recovery = 89% Analysis Date = 06/04/13 Pct Recovery = 89% Analysis Date = 05/24/13 Pct Recovery = 89% Analysis Date = 05/24/13 Pct Recovery = 89% Analysis Date = 05/13/13 Pct Recovery = 89% Analysis Date = 05/13/13 Pct Recovery = 89% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 04/21/13 Pct Recovery = 90% Analysis Date = 04/21/13 Pct Recovery = 90% Analysis Date = 04/11/13 Pct Recovery = 91% Analysis Date = 04/11/13 Pct Recovery = 91% Analysis Date = 03/31/13 Pct Recovery = 91% Analysis Date = 03/31/13 Pct Recovery = 91% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/20/13 Pct Recovery = 92% Analysis Date = 03/09/13 Pct Recovery = 92% Analysis Date = 03/09/13 Pct Recovery = 92% Analysis Date = 02/26/13 Pct Recovery = 92% Analysis Date = 02/26/13 Pct Recovery = 92% Analysis Date = 02/15/13 Pct Recovery = 92% Analysis Date = 02/15/13 Pct Recovery = 92% Analysis Date = 02/04/13 Pct Recovery = 92% Analysis Date = 02/04/13 Pct Recovery = 92% Analysis Date = 01/25/13 Pct Recovery = 92% Analysis Date = 01/25/13 Pct Recovery = 92% Analysis Date = 01/14/13 Pct Recovery = 92% Analysis Date = 01/14/13 Pct Recovery = 92% Analysis Date = 01/03/13 Pct Recovery = 92% Analysis Date = 01/03/13 Pct Recovery = 92% Analysis Date = 12/23/12 Pct Recovery = 92% Analysis Date = 12/23/12 Pct Recovery = 92% Analysis Date = 12/12/12 Pct Recovery = 92% Analysis Date = 12/12/12 Pct Recovery = 92% Analysis Date = 12/01/12 Pct Recovery = 93% Analysis Date = 12/01/12 Pct Recovery = 93% Analysis Date = 11/20/12 Pct Recovery = 93% Analysis Date = 11/20/12 Pct Recovery = 93% Analysis Date = 11/10/12 Pct Recovery = 93% Analysis Date = 11/10/12 Pct Recovery = 93% Analysis Date = 10/30/12 Pct Recovery = 93% Analysis Date = 10/30/12 Pct Recovery = 93% Analysis Date = 10/19/12 Pct Recovery = 93% Analysis Date = 10/19/12 Pct Recovery = 93% Analysis Date = 10/08/12 Pct Recovery = 93% Analysis Date = 10/08/12 Pct Recovery = 93% Analysis Date = 09/27/12 Pct Recovery = 93% Analysis Date = 09/27/12 Pct Recovery = 93% Analysis Date = 09/16/12 Pct Recovery = 93% Analysis Date = 09/16/12 Pct Recovery = 93% Analysis Date = 09/06/12 Pct Recovery = 93% Analysis Date = 09/06/12 Pct Recovery = 93% Analysis Date = 08/26/12 Pct Recovery = 93% Analysis Date = 08/26/12 Pct Recovery = 93% Analysis Date = 08/15/12 Pct Recovery = 93% Analysis Date = 08/15/12 Pct Recovery = 93% Analysis Date = 08/04/12 Pct Recovery = 92% Analysis Date = 08/04/12 Pct Recovery = 92% Analysis Date = 07/24/12 Pct Recovery = 92% Analysis Date = 07/24/12 Pct Recovery = 92% Analysis Date = 07/13/12 Pct Recovery = 92% Analysis Date = 07/13/12 Pct Recovery = 92% Analysis Date = 07/02/12 Pct Recovery = 92% Analysis Date = 07/02/12 Pct Recovery = 92% Analysis Date = 06/22/12 Pct Recovery = 92% Analysis Date = 06/22/12 Pct Recovery = 92% Analysis Date = 06/11/12 Pct Recovery = 92% Analysis Date = 06/11/12 Pct Recovery = 92% Analysis Date = 05/31/12 Pct Recovery = 93% Analysis Date = 05/31/12 Pct Recovery = 93% Analysis Date = 05/20/12 Pct Recovery = 93% Analysis Date = 05/20/12 Pct Recovery = 93% Analysis Date = 05/09/12 Pct Recovery = 93% Analysis Date = 05/09/12 Pct Recovery = 93% Analysis Date = 04/28/12 Pct Recovery = 93% Analysis Date = 04/28/12 Pct Recovery = 93% Analysis Date = 04/17/12 Pct Recovery = 93% Analysis Date = 04/17/12 Pct Recovery = 93% Analysis Date = 04/07/12 Pct Recovery = 93% Analysis Date = 04/07/12 Pct Recovery = 93% Analysis Date = 03/27/12 Pct Recovery = 94% Analysis Date = 03/27/12 Pct Recovery = 94% Analysis Date = 03/16/12 Pct Recovery = 94% Analysis Date = 03/16/12 Pct Recovery = 94% Analysis Date = 03/05/12 Pct Recovery = 94% Analysis Date = 03/05/12 Pct Recovery = 94% Analysis Date = 02/23/12 Pct Recovery = 94% Analysis Date = 02/23/12 Pct Recovery = 94% Analysis Date = 02/12/12 Pct Recovery = 94% Analysis Date = 02/12/12 Pct Recovery = 94% Analysis Date = 02/02/12 Pct Recovery = 94% Analysis Date = 02/02/12 Pct Recovery = 94% Analysis Date = 01/22/12 Pct Recovery = 94% Analysis Date = 01/22/12 Pct Recovery = 94% Analysis Date = 01/11/12 Pct Recovery = 95% Analysis Date = 01/11/12 Pct Recovery = 95% Analysis Date = 12/31/11 Pct Recovery = 95% Analysis Date = 12/31/11 Pct Recovery = 95% Analysis Date = 12/20/11 Pct Recovery = 95% Analysis Date = 12/20/11 Pct Recovery = 95% Analysis Date = 12/09/11 Pct Recovery = 95% Analysis Date = 12/09/11 Pct Recovery = 95% Analysis Date = 11/28/11 Pct Recovery = 95% Analysis Date = 11/28/11 Pct Recovery = 95% Analysis Date = 11/18/11 Pct Recovery = 95% Analysis Date = 11/18/11 Pct Recovery = 95% Analysis Date = 11/07/11 Pct Recovery = 96% Analysis Date = 11/07/11 Pct Recovery = 96% Analysis Date = 10/27/11 Pct Recovery = 96% Analysis Date = 10/27/11 Pct Recovery = 96% Analysis Date = 10/16/11 Pct Recovery = 96% Analysis Date = 10/16/11 Pct Recovery = 96% Analysis Date = 10/05/11 Pct Recovery = 96% Analysis Date = 10/05/11 Pct Recovery = 96% Analysis Date = 09/24/11 Pct Recovery = 96% Analysis Date = 09/24/11 Pct Recovery = 96% Analysis Date = 09/13/11 Pct Recovery = 96% Analysis Date = 09/13/11 Pct Recovery = 96% Analysis Date = 09/03/11 Pct Recovery = 96% Analysis Date = 09/03/11 Pct Recovery = 96% Analysis Date = 08/23/11 Pct Recovery = 97% Analysis Date = 08/23/11 Pct Recovery = 97% Analysis Date = 08/12/11 Pct Recovery = 97% Analysis Date = 08/12/11 Pct Recovery = 97% Analysis Date = 08/01/11 Pct Recovery = 97% Analysis Date = 08/01/11 Pct Recovery = 97% Analysis Date = 07/21/11 Pct Recovery = 97% Analysis Date = 07/21/11 Pct Recovery = 97% Analysis Date = 07/10/11 Pct Recovery = 97% Analysis Date = 07/10/11 Pct Recovery = 97% Analysis Date = 06/30/11 Pct Recovery = 97% Analysis Date = 06/30/11 Pct Recovery = 97% Analysis Date = 06/19/11 Pct Recovery = 97% Analysis Date = 06/19/11 Pct Recovery = 97% Analysis Date = 06/08/11 Pct Recovery = 98% Analysis Date = 06/08/11 Pct Recovery = 98% Analysis Date = 05/28/11 Pct Recovery = 98% Analysis Date = 05/28/11 Pct Recovery = 98% Analysis Date = 05/17/11 Pct Recovery = 98% Analysis Date = 05/17/11 Pct Recovery = 98% Analysis Date = 05/06/11 Pct Recovery = 98% Analysis Date = 05/06/11 Pct Recovery = 98% Analysis Date = 04/25/11 Pct Recovery = 98% Analysis Date = 04/25/11 Pct Recovery = 98% Analysis Date = 04/15/11 Pct Recovery = 98% Analysis Date = 04/15/11 Pct Recovery = 98% Analysis Date = 04/04/11 Pct Recovery = 98% Analysis Date = 04/04/11 Pct Recovery = 98% Analysis Date = 03/24/11 Pct Recovery = 99% Analysis Date = 03/24/11 Pct Recovery = 99% Analysis Date = 03/13/11 Pct Recovery = 99% Analysis Date = 03/13/11 Pct Recovery = 99% Analysis Date = 03/02/11 Pct Recovery = 99% Analysis Date = 03/02/11 Pct Recovery = 99% Analysis Date = 02/19/11 Pct Recovery = 99% Analysis Date = 02/19/11 Pct Recovery = 99% Analysis Date = 02/09/11 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 196% . 196% 0%
>= Reporting Level 92 83% 24% 78% 17%
Total 93 84% 27% 79% 17%

Sample Statistics
FENAMIPHOS SULFONE

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 14 15% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 2 3% 2 out of 75

BQS OBSP Determination:
FENAMIPHOS SULFOXIDE
METHOD: 2033 , TESTIDCODE: 61646GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 17% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 31% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 35% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 20% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 12% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 25% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 23% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 23% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 14% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 17% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 13% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 12% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 12% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 23% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 30% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 14% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 6% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 25% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 24% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 13% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 17% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 14% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 16% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 9% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 27% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 44% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 79% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 47% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 18% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 54% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 16% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 15% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 7% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 25% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 21% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 13% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 17% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 8% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 24% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 8% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 20% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 17% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 35% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 26% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 26% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 22% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 26% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 59% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 15% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 25% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 13% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 44% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 25% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 21% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 32% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 23% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 60% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 78% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 12% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 25% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 15% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 10% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 24% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 35% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 64% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 48% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 97% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 73% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 56% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 124% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 73% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 35% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 31% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 11% Analysis Date = 12/20/16 Pct Recovery = 6% Analysis Date = 12/09/16 Pct Recovery = 7% Analysis Date = 12/09/16 Pct Recovery = 7% Analysis Date = 11/28/16 Pct Recovery = 7% Analysis Date = 11/28/16 Pct Recovery = 7% Analysis Date = 11/17/16 Pct Recovery = 7% Analysis Date = 11/17/16 Pct Recovery = 7% Analysis Date = 11/07/16 Pct Recovery = 7% Analysis Date = 11/07/16 Pct Recovery = 7% Analysis Date = 10/27/16 Pct Recovery = 7% Analysis Date = 10/27/16 Pct Recovery = 7% Analysis Date = 10/16/16 Pct Recovery = 8% Analysis Date = 10/16/16 Pct Recovery = 8% Analysis Date = 10/06/16 Pct Recovery = 8% Analysis Date = 10/06/16 Pct Recovery = 8% Analysis Date = 09/25/16 Pct Recovery = 8% Analysis Date = 09/25/16 Pct Recovery = 8% Analysis Date = 09/14/16 Pct Recovery = 8% Analysis Date = 09/14/16 Pct Recovery = 8% Analysis Date = 09/03/16 Pct Recovery = 9% Analysis Date = 09/03/16 Pct Recovery = 9% Analysis Date = 08/24/16 Pct Recovery = 9% Analysis Date = 08/24/16 Pct Recovery = 9% Analysis Date = 08/13/16 Pct Recovery = 9% Analysis Date = 08/13/16 Pct Recovery = 9% Analysis Date = 08/02/16 Pct Recovery = 9% Analysis Date = 08/02/16 Pct Recovery = 9% Analysis Date = 07/23/16 Pct Recovery = 9% Analysis Date = 07/23/16 Pct Recovery = 9% Analysis Date = 07/12/16 Pct Recovery = 10% Analysis Date = 07/12/16 Pct Recovery = 10% Analysis Date = 07/01/16 Pct Recovery = 10% Analysis Date = 07/01/16 Pct Recovery = 10% Analysis Date = 06/21/16 Pct Recovery = 10% Analysis Date = 06/21/16 Pct Recovery = 10% Analysis Date = 06/10/16 Pct Recovery = 10% Analysis Date = 06/10/16 Pct Recovery = 10% Analysis Date = 05/30/16 Pct Recovery = 10% Analysis Date = 05/30/16 Pct Recovery = 10% Analysis Date = 05/19/16 Pct Recovery = 11% Analysis Date = 05/19/16 Pct Recovery = 11% Analysis Date = 05/09/16 Pct Recovery = 11% Analysis Date = 05/09/16 Pct Recovery = 11% Analysis Date = 04/28/16 Pct Recovery = 11% Analysis Date = 04/28/16 Pct Recovery = 11% Analysis Date = 04/17/16 Pct Recovery = 11% Analysis Date = 04/17/16 Pct Recovery = 11% Analysis Date = 04/07/16 Pct Recovery = 12% Analysis Date = 04/07/16 Pct Recovery = 12% Analysis Date = 03/27/16 Pct Recovery = 12% Analysis Date = 03/27/16 Pct Recovery = 12% Analysis Date = 03/16/16 Pct Recovery = 12% Analysis Date = 03/16/16 Pct Recovery = 12% Analysis Date = 03/05/16 Pct Recovery = 12% Analysis Date = 03/05/16 Pct Recovery = 12% Analysis Date = 02/24/16 Pct Recovery = 12% Analysis Date = 02/24/16 Pct Recovery = 12% Analysis Date = 02/13/16 Pct Recovery = 13% Analysis Date = 02/13/16 Pct Recovery = 13% Analysis Date = 02/02/16 Pct Recovery = 13% Analysis Date = 02/02/16 Pct Recovery = 13% Analysis Date = 01/23/16 Pct Recovery = 13% Analysis Date = 01/23/16 Pct Recovery = 13% Analysis Date = 01/12/16 Pct Recovery = 13% Analysis Date = 01/12/16 Pct Recovery = 13% Analysis Date = 01/01/16 Pct Recovery = 14% Analysis Date = 01/01/16 Pct Recovery = 14% Analysis Date = 12/22/15 Pct Recovery = 14% Analysis Date = 12/22/15 Pct Recovery = 14% Analysis Date = 12/11/15 Pct Recovery = 14% Analysis Date = 12/11/15 Pct Recovery = 14% Analysis Date = 11/30/15 Pct Recovery = 14% Analysis Date = 11/30/15 Pct Recovery = 14% Analysis Date = 11/19/15 Pct Recovery = 14% Analysis Date = 11/19/15 Pct Recovery = 14% Analysis Date = 11/09/15 Pct Recovery = 15% Analysis Date = 11/09/15 Pct Recovery = 15% Analysis Date = 10/29/15 Pct Recovery = 15% Analysis Date = 10/29/15 Pct Recovery = 15% Analysis Date = 10/18/15 Pct Recovery = 15% Analysis Date = 10/18/15 Pct Recovery = 15% Analysis Date = 10/08/15 Pct Recovery = 15% Analysis Date = 10/08/15 Pct Recovery = 15% Analysis Date = 09/27/15 Pct Recovery = 15% Analysis Date = 09/27/15 Pct Recovery = 15% Analysis Date = 09/16/15 Pct Recovery = 16% Analysis Date = 09/16/15 Pct Recovery = 16% Analysis Date = 09/05/15 Pct Recovery = 16% Analysis Date = 09/05/15 Pct Recovery = 16% Analysis Date = 08/26/15 Pct Recovery = 16% Analysis Date = 08/26/15 Pct Recovery = 16% Analysis Date = 08/15/15 Pct Recovery = 16% Analysis Date = 08/15/15 Pct Recovery = 16% Analysis Date = 08/04/15 Pct Recovery = 17% Analysis Date = 08/04/15 Pct Recovery = 17% Analysis Date = 07/25/15 Pct Recovery = 17% Analysis Date = 07/25/15 Pct Recovery = 17% Analysis Date = 07/14/15 Pct Recovery = 17% Analysis Date = 07/14/15 Pct Recovery = 17% Analysis Date = 07/03/15 Pct Recovery = 17% Analysis Date = 07/03/15 Pct Recovery = 17% Analysis Date = 06/23/15 Pct Recovery = 17% Analysis Date = 06/23/15 Pct Recovery = 17% Analysis Date = 06/12/15 Pct Recovery = 18% Analysis Date = 06/12/15 Pct Recovery = 18% Analysis Date = 06/01/15 Pct Recovery = 18% Analysis Date = 06/01/15 Pct Recovery = 18% Analysis Date = 05/21/15 Pct Recovery = 18% Analysis Date = 05/21/15 Pct Recovery = 18% Analysis Date = 05/11/15 Pct Recovery = 18% Analysis Date = 05/11/15 Pct Recovery = 18% Analysis Date = 04/30/15 Pct Recovery = 19% Analysis Date = 04/30/15 Pct Recovery = 19% Analysis Date = 04/19/15 Pct Recovery = 19% Analysis Date = 04/19/15 Pct Recovery = 19% Analysis Date = 04/09/15 Pct Recovery = 19% Analysis Date = 04/09/15 Pct Recovery = 19% Analysis Date = 03/29/15 Pct Recovery = 19% Analysis Date = 03/29/15 Pct Recovery = 19% Analysis Date = 03/18/15 Pct Recovery = 20% Analysis Date = 03/18/15 Pct Recovery = 20% Analysis Date = 03/07/15 Pct Recovery = 20% Analysis Date = 03/07/15 Pct Recovery = 20% Analysis Date = 02/25/15 Pct Recovery = 20% Analysis Date = 02/25/15 Pct Recovery = 20% Analysis Date = 02/14/15 Pct Recovery = 21% Analysis Date = 02/14/15 Pct Recovery = 21% Analysis Date = 02/03/15 Pct Recovery = 21% Analysis Date = 02/03/15 Pct Recovery = 21% Analysis Date = 01/24/15 Pct Recovery = 21% Analysis Date = 01/24/15 Pct Recovery = 21% Analysis Date = 01/13/15 Pct Recovery = 21% Analysis Date = 01/13/15 Pct Recovery = 21% Analysis Date = 01/02/15 Pct Recovery = 22% Analysis Date = 01/02/15 Pct Recovery = 22% Analysis Date = 12/23/14 Pct Recovery = 22% Analysis Date = 12/23/14 Pct Recovery = 22% Analysis Date = 12/12/14 Pct Recovery = 22% Analysis Date = 12/12/14 Pct Recovery = 22% Analysis Date = 12/01/14 Pct Recovery = 22% Analysis Date = 12/01/14 Pct Recovery = 22% Analysis Date = 11/20/14 Pct Recovery = 23% Analysis Date = 11/20/14 Pct Recovery = 23% Analysis Date = 11/10/14 Pct Recovery = 23% Analysis Date = 11/10/14 Pct Recovery = 23% Analysis Date = 10/30/14 Pct Recovery = 23% Analysis Date = 10/30/14 Pct Recovery = 23% Analysis Date = 10/19/14 Pct Recovery = 24% Analysis Date = 10/19/14 Pct Recovery = 24% Analysis Date = 10/09/14 Pct Recovery = 24% Analysis Date = 10/09/14 Pct Recovery = 24% Analysis Date = 09/28/14 Pct Recovery = 24% Analysis Date = 09/28/14 Pct Recovery = 24% Analysis Date = 09/17/14 Pct Recovery = 24% Analysis Date = 09/17/14 Pct Recovery = 24% Analysis Date = 09/07/14 Pct Recovery = 25% Analysis Date = 09/07/14 Pct Recovery = 25% Analysis Date = 08/27/14 Pct Recovery = 25% Analysis Date = 08/27/14 Pct Recovery = 25% Analysis Date = 08/16/14 Pct Recovery = 25% Analysis Date = 08/16/14 Pct Recovery = 25% Analysis Date = 08/05/14 Pct Recovery = 26% Analysis Date = 08/05/14 Pct Recovery = 26% Analysis Date = 07/26/14 Pct Recovery = 26% Analysis Date = 07/26/14 Pct Recovery = 26% Analysis Date = 07/15/14 Pct Recovery = 27% Analysis Date = 07/15/14 Pct Recovery = 27% Analysis Date = 07/04/14 Pct Recovery = 28% Analysis Date = 07/04/14 Pct Recovery = 28% Analysis Date = 06/24/14 Pct Recovery = 28% Analysis Date = 06/24/14 Pct Recovery = 28% Analysis Date = 06/13/14 Pct Recovery = 29% Analysis Date = 06/13/14 Pct Recovery = 29% Analysis Date = 06/02/14 Pct Recovery = 29% Analysis Date = 06/02/14 Pct Recovery = 29% Analysis Date = 05/22/14 Pct Recovery = 30% Analysis Date = 05/22/14 Pct Recovery = 30% Analysis Date = 05/12/14 Pct Recovery = 30% Analysis Date = 05/12/14 Pct Recovery = 30% Analysis Date = 05/01/14 Pct Recovery = 31% Analysis Date = 05/01/14 Pct Recovery = 31% Analysis Date = 04/20/14 Pct Recovery = 32% Analysis Date = 04/20/14 Pct Recovery = 32% Analysis Date = 04/10/14 Pct Recovery = 32% Analysis Date = 04/10/14 Pct Recovery = 32% Analysis Date = 03/30/14 Pct Recovery = 33% Analysis Date = 03/30/14 Pct Recovery = 33% Analysis Date = 03/19/14 Pct Recovery = 33% Analysis Date = 03/19/14 Pct Recovery = 33% Analysis Date = 03/09/14 Pct Recovery = 34% Analysis Date = 03/09/14 Pct Recovery = 34% Analysis Date = 02/26/14 Pct Recovery = 35% Analysis Date = 02/26/14 Pct Recovery = 35% Analysis Date = 02/15/14 Pct Recovery = 35% Analysis Date = 02/15/14 Pct Recovery = 35% Analysis Date = 02/04/14 Pct Recovery = 36% Analysis Date = 02/04/14 Pct Recovery = 36% Analysis Date = 01/25/14 Pct Recovery = 36% Analysis Date = 01/25/14 Pct Recovery = 36% Analysis Date = 01/14/14 Pct Recovery = 37% Analysis Date = 01/14/14 Pct Recovery = 37% Analysis Date = 01/03/14 Pct Recovery = 37% Analysis Date = 01/03/14 Pct Recovery = 37% Analysis Date = 12/24/13 Pct Recovery = 38% Analysis Date = 12/24/13 Pct Recovery = 38% Analysis Date = 12/13/13 Pct Recovery = 39% Analysis Date = 12/13/13 Pct Recovery = 39% Analysis Date = 12/02/13 Pct Recovery = 39% Analysis Date = 12/02/13 Pct Recovery = 39% Analysis Date = 11/21/13 Pct Recovery = 40% Analysis Date = 11/21/13 Pct Recovery = 40% Analysis Date = 11/11/13 Pct Recovery = 40% Analysis Date = 11/11/13 Pct Recovery = 40% Analysis Date = 10/31/13 Pct Recovery = 41% Analysis Date = 10/31/13 Pct Recovery = 41% Analysis Date = 10/20/13 Pct Recovery = 41% Analysis Date = 10/20/13 Pct Recovery = 41% Analysis Date = 10/10/13 Pct Recovery = 42% Analysis Date = 10/10/13 Pct Recovery = 42% Analysis Date = 09/29/13 Pct Recovery = 42% Analysis Date = 09/29/13 Pct Recovery = 42% Analysis Date = 09/18/13 Pct Recovery = 42% Analysis Date = 09/18/13 Pct Recovery = 42% Analysis Date = 09/08/13 Pct Recovery = 43% Analysis Date = 09/08/13 Pct Recovery = 43% Analysis Date = 08/28/13 Pct Recovery = 43% Analysis Date = 08/28/13 Pct Recovery = 43% Analysis Date = 08/17/13 Pct Recovery = 43% Analysis Date = 08/17/13 Pct Recovery = 43% Analysis Date = 08/06/13 Pct Recovery = 44% Analysis Date = 08/06/13 Pct Recovery = 44% Analysis Date = 07/27/13 Pct Recovery = 44% Analysis Date = 07/27/13 Pct Recovery = 44% Analysis Date = 07/16/13 Pct Recovery = 44% Analysis Date = 07/16/13 Pct Recovery = 44% Analysis Date = 07/05/13 Pct Recovery = 44% Analysis Date = 07/05/13 Pct Recovery = 44% Analysis Date = 06/25/13 Pct Recovery = 44% Analysis Date = 06/25/13 Pct Recovery = 44% Analysis Date = 06/14/13 Pct Recovery = 44% Analysis Date = 06/14/13 Pct Recovery = 44% Analysis Date = 06/03/13 Pct Recovery = 45% Analysis Date = 06/03/13 Pct Recovery = 45% Analysis Date = 05/23/13 Pct Recovery = 45% Analysis Date = 05/23/13 Pct Recovery = 45% Analysis Date = 05/13/13 Pct Recovery = 45% Analysis Date = 05/13/13 Pct Recovery = 45% Analysis Date = 05/02/13 Pct Recovery = 45% Analysis Date = 05/02/13 Pct Recovery = 45% Analysis Date = 04/21/13 Pct Recovery = 45% Analysis Date = 04/21/13 Pct Recovery = 45% Analysis Date = 04/11/13 Pct Recovery = 45% Analysis Date = 04/11/13 Pct Recovery = 45% Analysis Date = 03/31/13 Pct Recovery = 45% Analysis Date = 03/31/13 Pct Recovery = 45% Analysis Date = 03/20/13 Pct Recovery = 45% Analysis Date = 03/20/13 Pct Recovery = 45% Analysis Date = 03/10/13 Pct Recovery = 45% Analysis Date = 03/10/13 Pct Recovery = 45% Analysis Date = 02/27/13 Pct Recovery = 45% Analysis Date = 02/27/13 Pct Recovery = 45% Analysis Date = 02/16/13 Pct Recovery = 45% Analysis Date = 02/16/13 Pct Recovery = 45% Analysis Date = 02/05/13 Pct Recovery = 45% Analysis Date = 02/05/13 Pct Recovery = 45% Analysis Date = 01/26/13 Pct Recovery = 45% Analysis Date = 01/26/13 Pct Recovery = 45% Analysis Date = 01/15/13 Pct Recovery = 45% Analysis Date = 01/15/13 Pct Recovery = 45% Analysis Date = 01/04/13 Pct Recovery = 46% Analysis Date = 01/04/13 Pct Recovery = 46% Analysis Date = 12/25/12 Pct Recovery = 46% Analysis Date = 12/25/12 Pct Recovery = 46% Analysis Date = 12/14/12 Pct Recovery = 45% Analysis Date = 12/14/12 Pct Recovery = 45% Analysis Date = 12/03/12 Pct Recovery = 45% Analysis Date = 12/03/12 Pct Recovery = 45% Analysis Date = 11/23/12 Pct Recovery = 45% Analysis Date = 11/23/12 Pct Recovery = 45% Analysis Date = 11/12/12 Pct Recovery = 44% Analysis Date = 11/12/12 Pct Recovery = 44% Analysis Date = 11/01/12 Pct Recovery = 44% Analysis Date = 11/01/12 Pct Recovery = 44% Analysis Date = 10/21/12 Pct Recovery = 43% Analysis Date = 10/21/12 Pct Recovery = 43% Analysis Date = 10/11/12 Pct Recovery = 43% Analysis Date = 10/11/12 Pct Recovery = 43% Analysis Date = 09/30/12 Pct Recovery = 43% Analysis Date = 09/30/12 Pct Recovery = 43% Analysis Date = 09/19/12 Pct Recovery = 42% Analysis Date = 09/19/12 Pct Recovery = 42% Analysis Date = 09/09/12 Pct Recovery = 42% Analysis Date = 09/09/12 Pct Recovery = 42% Analysis Date = 08/29/12 Pct Recovery = 41% Analysis Date = 08/29/12 Pct Recovery = 41% Analysis Date = 08/18/12 Pct Recovery = 41% Analysis Date = 08/18/12 Pct Recovery = 41% Analysis Date = 08/07/12 Pct Recovery = 40% Analysis Date = 08/07/12 Pct Recovery = 40% Analysis Date = 07/28/12 Pct Recovery = 40% Analysis Date = 07/28/12 Pct Recovery = 40% Analysis Date = 07/17/12 Pct Recovery = 39% Analysis Date = 07/17/12 Pct Recovery = 39% Analysis Date = 07/06/12 Pct Recovery = 39% Analysis Date = 07/06/12 Pct Recovery = 39% Analysis Date = 06/26/12 Pct Recovery = 38% Analysis Date = 06/26/12 Pct Recovery = 38% Analysis Date = 06/15/12 Pct Recovery = 38% Analysis Date = 06/15/12 Pct Recovery = 38% Analysis Date = 06/04/12 Pct Recovery = 37% Analysis Date = 06/04/12 Pct Recovery = 37% Analysis Date = 05/25/12 Pct Recovery = 37% Analysis Date = 05/25/12 Pct Recovery = 37% Analysis Date = 05/14/12 Pct Recovery = 36% Analysis Date = 05/14/12 Pct Recovery = 36% Analysis Date = 05/03/12 Pct Recovery = 35% Analysis Date = 05/03/12 Pct Recovery = 35% Analysis Date = 04/22/12 Pct Recovery = 35% Analysis Date = 04/22/12 Pct Recovery = 35% Analysis Date = 04/12/12 Pct Recovery = 34% Analysis Date = 04/12/12 Pct Recovery = 34% Analysis Date = 04/01/12 Pct Recovery = 34% Analysis Date = 04/01/12 Pct Recovery = 34% Analysis Date = 03/21/12 Pct Recovery = 33% Analysis Date = 03/21/12 Pct Recovery = 33% Analysis Date = 03/11/12 Pct Recovery = 33% Analysis Date = 03/11/12 Pct Recovery = 33% Analysis Date = 02/29/12 Pct Recovery = 32% Analysis Date = 02/29/12 Pct Recovery = 32% Analysis Date = 02/18/12 Pct Recovery = 32% Analysis Date = 02/18/12 Pct Recovery = 32% Analysis Date = 02/07/12 Pct Recovery = 31% Analysis Date = 02/07/12 Pct Recovery = 31% Analysis Date = 01/28/12 Pct Recovery = 31% Analysis Date = 01/28/12 Pct Recovery = 31% Analysis Date = 01/17/12 Pct Recovery = 30% Analysis Date = 01/17/12 Pct Recovery = 30% Analysis Date = 01/06/12 Pct Recovery = 29% Analysis Date = 01/06/12 Pct Recovery = 29% Analysis Date = 12/27/11 Pct Recovery = 29% Analysis Date = 12/27/11 Pct Recovery = 29% Analysis Date = 12/16/11 Pct Recovery = 28% Analysis Date = 12/16/11 Pct Recovery = 28% Analysis Date = 12/05/11 Pct Recovery = 28% Analysis Date = 12/05/11 Pct Recovery = 28% Analysis Date = 11/25/11 Pct Recovery = 27% Analysis Date = 11/25/11 Pct Recovery = 27% Analysis Date = 11/14/11 Pct Recovery = 27% Analysis Date = 11/14/11 Pct Recovery = 27% Analysis Date = 11/03/11 Pct Recovery = 26% Analysis Date = 11/03/11 Pct Recovery = 26% Analysis Date = 10/23/11 Pct Recovery = 26% Analysis Date = 10/23/11 Pct Recovery = 26% Analysis Date = 10/13/11 Pct Recovery = 25% Analysis Date = 10/13/11 Pct Recovery = 25% Analysis Date = 10/02/11 Pct Recovery = 25% Analysis Date = 10/02/11 Pct Recovery = 25% Analysis Date = 09/21/11 Pct Recovery = 24% Analysis Date = 09/21/11 Pct Recovery = 24% Analysis Date = 09/11/11 Pct Recovery = 24% Analysis Date = 09/11/11 Pct Recovery = 24% Analysis Date = 08/31/11 Pct Recovery = 23% Analysis Date = 08/31/11 Pct Recovery = 23% Analysis Date = 08/20/11 Pct Recovery = 23% Analysis Date = 08/20/11 Pct Recovery = 23% Analysis Date = 08/09/11 Pct Recovery = 22% Analysis Date = 08/09/11 Pct Recovery = 22% Analysis Date = 07/30/11 Pct Recovery = 22% Analysis Date = 07/30/11 Pct Recovery = 22% Analysis Date = 07/19/11 Pct Recovery = 21% Analysis Date = 07/19/11 Pct Recovery = 21% Analysis Date = 07/08/11 Pct Recovery = 21% Analysis Date = 07/08/11 Pct Recovery = 21% Analysis Date = 06/28/11 Pct Recovery = 20% Analysis Date = 06/28/11 Pct Recovery = 20% Analysis Date = 06/17/11 Pct Recovery = 20% Analysis Date = 06/17/11 Pct Recovery = 20% Analysis Date = 06/06/11 Pct Recovery = 19% Analysis Date = 06/06/11 Pct Recovery = 19% Analysis Date = 05/27/11 Pct Recovery = 19% Analysis Date = 05/27/11 Pct Recovery = 19% Analysis Date = 05/16/11 Pct Recovery = 18% Analysis Date = 05/16/11 Pct Recovery = 18% Analysis Date = 05/05/11 Pct Recovery = 18% Analysis Date = 05/05/11 Pct Recovery = 18% Analysis Date = 04/24/11 Pct Recovery = 17% Analysis Date = 04/24/11 Pct Recovery = 17% Analysis Date = 04/14/11 Pct Recovery = 17% Analysis Date = 04/14/11 Pct Recovery = 17% Analysis Date = 04/03/11 Pct Recovery = 16% Analysis Date = 04/03/11 Pct Recovery = 16% Analysis Date = 03/23/11 Pct Recovery = 16% Analysis Date = 03/23/11 Pct Recovery = 16% Analysis Date = 03/13/11 Pct Recovery = 15% Analysis Date = 03/13/11 Pct Recovery = 15% Analysis Date = 03/02/11 Pct Recovery = 15% Analysis Date = 03/02/11 Pct Recovery = 15% Analysis Date = 02/19/11 Pct Recovery = 15% Analysis Date = 02/19/11 Pct Recovery = 15% Analysis Date = 02/09/11 Pct Recovery = 14% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 11% . 11% 0%
>= Reporting Level 74 30% 24% 24% 15%
Total 75 30% 24% 23% 15%

Sample Statistics
FENAMIPHOS SULFOXIDE

Characteristic N % % Basis
Plotted 75 90% Spiked
Estimated Values 75 90% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 84 .  
False Negatives 7 8% 7 out of 83
Not Spiked 65 .  
False Positives 0 0% 0 out of 65

BQS OBSP Determination:
FIPRONIL
METHOD: 2033 , TESTIDCODE: 62166GCM29
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 88% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 82% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 72% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 76% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 104% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 83% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 59% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 76% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 110% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 86% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 90% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 85% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 101% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 114% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 76% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 94% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 88% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 83% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 95% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 104% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 113% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 101% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 109% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 111% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 116% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 107% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 85% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 121% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 93% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 129% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 107% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 83% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 108% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 104% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 103% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 99% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 98% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 100% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 88% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 94% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 106% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 93% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 101% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 100% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 111% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 105% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 86% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 111% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 91% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 91% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 153% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 108% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 49% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 101% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 101% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 126% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 136% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 123% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 138% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 115% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 119% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 108% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 121% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 95% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 91% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 88% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 125% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 116% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 121% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 110% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 151% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 138% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 121% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 118% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 122% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 107% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 123% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 133% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 155% Analysis Date = 12/20/16 Pct Recovery = 111% Analysis Date = 12/09/16 Pct Recovery = 111% Analysis Date = 12/09/16 Pct Recovery = 111% Analysis Date = 11/28/16 Pct Recovery = 111% Analysis Date = 11/28/16 Pct Recovery = 111% Analysis Date = 11/17/16 Pct Recovery = 111% Analysis Date = 11/17/16 Pct Recovery = 111% Analysis Date = 11/07/16 Pct Recovery = 111% Analysis Date = 11/07/16 Pct Recovery = 111% Analysis Date = 10/27/16 Pct Recovery = 110% Analysis Date = 10/27/16 Pct Recovery = 110% Analysis Date = 10/16/16 Pct Recovery = 110% Analysis Date = 10/16/16 Pct Recovery = 110% Analysis Date = 10/06/16 Pct Recovery = 110% Analysis Date = 10/06/16 Pct Recovery = 110% Analysis Date = 09/25/16 Pct Recovery = 110% Analysis Date = 09/25/16 Pct Recovery = 110% Analysis Date = 09/14/16 Pct Recovery = 110% Analysis Date = 09/14/16 Pct Recovery = 110% Analysis Date = 09/03/16 Pct Recovery = 110% Analysis Date = 09/03/16 Pct Recovery = 110% Analysis Date = 08/24/16 Pct Recovery = 110% Analysis Date = 08/24/16 Pct Recovery = 110% Analysis Date = 08/13/16 Pct Recovery = 110% Analysis Date = 08/13/16 Pct Recovery = 110% Analysis Date = 08/02/16 Pct Recovery = 110% Analysis Date = 08/02/16 Pct Recovery = 110% Analysis Date = 07/23/16 Pct Recovery = 110% Analysis Date = 07/23/16 Pct Recovery = 110% Analysis Date = 07/12/16 Pct Recovery = 110% Analysis Date = 07/12/16 Pct Recovery = 110% Analysis Date = 07/01/16 Pct Recovery = 109% Analysis Date = 07/01/16 Pct Recovery = 109% Analysis Date = 06/21/16 Pct Recovery = 109% Analysis Date = 06/21/16 Pct Recovery = 109% Analysis Date = 06/10/16 Pct Recovery = 109% Analysis Date = 06/10/16 Pct Recovery = 109% Analysis Date = 05/30/16 Pct Recovery = 109% Analysis Date = 05/30/16 Pct Recovery = 109% Analysis Date = 05/19/16 Pct Recovery = 109% Analysis Date = 05/19/16 Pct Recovery = 109% Analysis Date = 05/09/16 Pct Recovery = 109% Analysis Date = 05/09/16 Pct Recovery = 109% Analysis Date = 04/28/16 Pct Recovery = 109% Analysis Date = 04/28/16 Pct Recovery = 109% Analysis Date = 04/17/16 Pct Recovery = 109% Analysis Date = 04/17/16 Pct Recovery = 109% Analysis Date = 04/07/16 Pct Recovery = 109% Analysis Date = 04/07/16 Pct Recovery = 109% Analysis Date = 03/27/16 Pct Recovery = 109% Analysis Date = 03/27/16 Pct Recovery = 109% Analysis Date = 03/16/16 Pct Recovery = 108% Analysis Date = 03/16/16 Pct Recovery = 108% Analysis Date = 03/05/16 Pct Recovery = 108% Analysis Date = 03/05/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/13/16 Pct Recovery = 108% Analysis Date = 02/13/16 Pct Recovery = 108% Analysis Date = 02/02/16 Pct Recovery = 108% Analysis Date = 02/02/16 Pct Recovery = 108% Analysis Date = 01/23/16 Pct Recovery = 108% Analysis Date = 01/23/16 Pct Recovery = 108% Analysis Date = 01/12/16 Pct Recovery = 108% Analysis Date = 01/12/16 Pct Recovery = 108% Analysis Date = 01/01/16 Pct Recovery = 108% Analysis Date = 01/01/16 Pct Recovery = 108% Analysis Date = 12/22/15 Pct Recovery = 108% Analysis Date = 12/22/15 Pct Recovery = 108% Analysis Date = 12/11/15 Pct Recovery = 108% Analysis Date = 12/11/15 Pct Recovery = 108% Analysis Date = 11/30/15 Pct Recovery = 107% Analysis Date = 11/30/15 Pct Recovery = 107% Analysis Date = 11/19/15 Pct Recovery = 107% Analysis Date = 11/19/15 Pct Recovery = 107% Analysis Date = 11/09/15 Pct Recovery = 107% Analysis Date = 11/09/15 Pct Recovery = 107% Analysis Date = 10/29/15 Pct Recovery = 107% Analysis Date = 10/29/15 Pct Recovery = 107% Analysis Date = 10/18/15 Pct Recovery = 107% Analysis Date = 10/18/15 Pct Recovery = 107% Analysis Date = 10/08/15 Pct Recovery = 107% Analysis Date = 10/08/15 Pct Recovery = 107% Analysis Date = 09/27/15 Pct Recovery = 107% Analysis Date = 09/27/15 Pct Recovery = 107% Analysis Date = 09/16/15 Pct Recovery = 107% Analysis Date = 09/16/15 Pct Recovery = 107% Analysis Date = 09/05/15 Pct Recovery = 107% Analysis Date = 09/05/15 Pct Recovery = 107% Analysis Date = 08/26/15 Pct Recovery = 106% Analysis Date = 08/26/15 Pct Recovery = 106% Analysis Date = 08/15/15 Pct Recovery = 106% Analysis Date = 08/15/15 Pct Recovery = 106% Analysis Date = 08/04/15 Pct Recovery = 106% Analysis Date = 08/04/15 Pct Recovery = 106% Analysis Date = 07/25/15 Pct Recovery = 106% Analysis Date = 07/25/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/14/15 Pct Recovery = 106% Analysis Date = 07/03/15 Pct Recovery = 106% Analysis Date = 07/03/15 Pct Recovery = 106% Analysis Date = 06/23/15 Pct Recovery = 106% Analysis Date = 06/23/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/12/15 Pct Recovery = 106% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 06/01/15 Pct Recovery = 105% Analysis Date = 05/21/15 Pct Recovery = 105% Analysis Date = 05/21/15 Pct Recovery = 105% Analysis Date = 05/11/15 Pct Recovery = 105% Analysis Date = 05/11/15 Pct Recovery = 105% Analysis Date = 04/30/15 Pct Recovery = 105% Analysis Date = 04/30/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/09/15 Pct Recovery = 105% Analysis Date = 04/09/15 Pct Recovery = 105% Analysis Date = 03/29/15 Pct Recovery = 105% Analysis Date = 03/29/15 Pct Recovery = 105% Analysis Date = 03/18/15 Pct Recovery = 105% Analysis Date = 03/18/15 Pct Recovery = 105% Analysis Date = 03/07/15 Pct Recovery = 104% Analysis Date = 03/07/15 Pct Recovery = 104% Analysis Date = 02/25/15 Pct Recovery = 104% Analysis Date = 02/25/15 Pct Recovery = 104% Analysis Date = 02/14/15 Pct Recovery = 104% Analysis Date = 02/14/15 Pct Recovery = 104% Analysis Date = 02/03/15 Pct Recovery = 104% Analysis Date = 02/03/15 Pct Recovery = 104% Analysis Date = 01/24/15 Pct Recovery = 104% Analysis Date = 01/24/15 Pct Recovery = 104% Analysis Date = 01/13/15 Pct Recovery = 104% Analysis Date = 01/13/15 Pct Recovery = 104% Analysis Date = 01/02/15 Pct Recovery = 104% Analysis Date = 01/02/15 Pct Recovery = 104% Analysis Date = 12/23/14 Pct Recovery = 104% Analysis Date = 12/23/14 Pct Recovery = 104% Analysis Date = 12/12/14 Pct Recovery = 104% Analysis Date = 12/12/14 Pct Recovery = 104% Analysis Date = 12/01/14 Pct Recovery = 103% Analysis Date = 12/01/14 Pct Recovery = 103% Analysis Date = 11/20/14 Pct Recovery = 103% Analysis Date = 11/20/14 Pct Recovery = 103% Analysis Date = 11/10/14 Pct Recovery = 103% Analysis Date = 11/10/14 Pct Recovery = 103% Analysis Date = 10/30/14 Pct Recovery = 103% Analysis Date = 10/30/14 Pct Recovery = 103% Analysis Date = 10/19/14 Pct Recovery = 103% Analysis Date = 10/19/14 Pct Recovery = 103% Analysis Date = 10/09/14 Pct Recovery = 103% Analysis Date = 10/09/14 Pct Recovery = 103% Analysis Date = 09/28/14 Pct Recovery = 103% Analysis Date = 09/28/14 Pct Recovery = 103% Analysis Date = 09/17/14 Pct Recovery = 103% Analysis Date = 09/17/14 Pct Recovery = 103% Analysis Date = 09/07/14 Pct Recovery = 103% Analysis Date = 09/07/14 Pct Recovery = 103% Analysis Date = 08/27/14 Pct Recovery = 102% Analysis Date = 08/27/14 Pct Recovery = 102% Analysis Date = 08/16/14 Pct Recovery = 102% Analysis Date = 08/16/14 Pct Recovery = 102% Analysis Date = 08/05/14 Pct Recovery = 102% Analysis Date = 08/05/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/26/14 Pct Recovery = 102% Analysis Date = 07/15/14 Pct Recovery = 102% Analysis Date = 07/15/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 07/04/14 Pct Recovery = 102% Analysis Date = 06/24/14 Pct Recovery = 102% Analysis Date = 06/24/14 Pct Recovery = 102% Analysis Date = 06/13/14 Pct Recovery = 102% Analysis Date = 06/13/14 Pct Recovery = 102% Analysis Date = 06/02/14 Pct Recovery = 102% Analysis Date = 06/02/14 Pct Recovery = 102% Analysis Date = 05/22/14 Pct Recovery = 102% Analysis Date = 05/22/14 Pct Recovery = 102% Analysis Date = 05/12/14 Pct Recovery = 102% Analysis Date = 05/12/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Analysis Date = 05/01/14 Pct Recovery = 102% Analysis Date = 04/20/14 Pct Recovery = 102% Analysis Date = 04/20/14 Pct Recovery = 102% Analysis Date = 04/10/14 Pct Recovery = 101% Analysis Date = 04/10/14 Pct Recovery = 101% Analysis Date = 03/30/14 Pct Recovery = 101% Analysis Date = 03/30/14 Pct Recovery = 101% Analysis Date = 03/19/14 Pct Recovery = 101% Analysis Date = 03/19/14 Pct Recovery = 101% Analysis Date = 03/09/14 Pct Recovery = 101% Analysis Date = 03/09/14 Pct Recovery = 101% Analysis Date = 02/26/14 Pct Recovery = 101% Analysis Date = 02/26/14 Pct Recovery = 101% Analysis Date = 02/15/14 Pct Recovery = 101% Analysis Date = 02/15/14 Pct Recovery = 101% Analysis Date = 02/04/14 Pct Recovery = 101% Analysis Date = 02/04/14 Pct Recovery = 101% Analysis Date = 01/25/14 Pct Recovery = 101% Analysis Date = 01/25/14 Pct Recovery = 101% Analysis Date = 01/14/14 Pct Recovery = 101% Analysis Date = 01/14/14 Pct Recovery = 101% Analysis Date = 01/03/14 Pct Recovery = 101% Analysis Date = 01/03/14 Pct Recovery = 101% Analysis Date = 12/24/13 Pct Recovery = 101% Analysis Date = 12/24/13 Pct Recovery = 101% Analysis Date = 12/13/13 Pct Recovery = 101% Analysis Date = 12/13/13 Pct Recovery = 101% Analysis Date = 12/02/13 Pct Recovery = 101% Analysis Date = 12/02/13 Pct Recovery = 101% Analysis Date = 11/21/13 Pct Recovery = 101% Analysis Date = 11/21/13 Pct Recovery = 101% Analysis Date = 11/11/13 Pct Recovery = 101% Analysis Date = 11/11/13 Pct Recovery = 101% Analysis Date = 10/31/13 Pct Recovery = 101% Analysis Date = 10/31/13 Pct Recovery = 101% Analysis Date = 10/20/13 Pct Recovery = 102% Analysis Date = 10/20/13 Pct Recovery = 102% Analysis Date = 10/10/13 Pct Recovery = 102% Analysis Date = 10/10/13 Pct Recovery = 102% Analysis Date = 09/29/13 Pct Recovery = 102% Analysis Date = 09/29/13 Pct Recovery = 102% Analysis Date = 09/18/13 Pct Recovery = 102% Analysis Date = 09/18/13 Pct Recovery = 102% Analysis Date = 09/08/13 Pct Recovery = 102% Analysis Date = 09/08/13 Pct Recovery = 102% Analysis Date = 08/28/13 Pct Recovery = 102% Analysis Date = 08/28/13 Pct Recovery = 102% Analysis Date = 08/17/13 Pct Recovery = 102% Analysis Date = 08/17/13 Pct Recovery = 102% Analysis Date = 08/06/13 Pct Recovery = 102% Analysis Date = 08/06/13 Pct Recovery = 102% Analysis Date = 07/27/13 Pct Recovery = 102% Analysis Date = 07/27/13 Pct Recovery = 102% Analysis Date = 07/16/13 Pct Recovery = 102% Analysis Date = 07/16/13 Pct Recovery = 102% Analysis Date = 07/05/13 Pct Recovery = 102% Analysis Date = 07/05/13 Pct Recovery = 102% Analysis Date = 06/25/13 Pct Recovery = 103% Analysis Date = 06/25/13 Pct Recovery = 103% Analysis Date = 06/14/13 Pct Recovery = 103% Analysis Date = 06/14/13 Pct Recovery = 103% Analysis Date = 06/03/13 Pct Recovery = 103% Analysis Date = 06/03/13 Pct Recovery = 103% Analysis Date = 05/23/13 Pct Recovery = 103% Analysis Date = 05/23/13 Pct Recovery = 103% Analysis Date = 05/13/13 Pct Recovery = 103% Analysis Date = 05/13/13 Pct Recovery = 103% Analysis Date = 05/02/13 Pct Recovery = 103% Analysis Date = 05/02/13 Pct Recovery = 103% Analysis Date = 04/21/13 Pct Recovery = 103% Analysis Date = 04/21/13 Pct Recovery = 103% Analysis Date = 04/11/13 Pct Recovery = 104% Analysis Date = 04/11/13 Pct Recovery = 104% Analysis Date = 03/31/13 Pct Recovery = 104% Analysis Date = 03/31/13 Pct Recovery = 104% Analysis Date = 03/20/13 Pct Recovery = 104% Analysis Date = 03/20/13 Pct Recovery = 104% Analysis Date = 03/10/13 Pct Recovery = 104% Analysis Date = 03/10/13 Pct Recovery = 104% Analysis Date = 02/27/13 Pct Recovery = 104% Analysis Date = 02/27/13 Pct Recovery = 104% Analysis Date = 02/16/13 Pct Recovery = 104% Analysis Date = 02/16/13 Pct Recovery = 104% Analysis Date = 02/05/13 Pct Recovery = 104% Analysis Date = 02/05/13 Pct Recovery = 104% Analysis Date = 01/26/13 Pct Recovery = 104% Analysis Date = 01/26/13 Pct Recovery = 104% Analysis Date = 01/15/13 Pct Recovery = 104% Analysis Date = 01/15/13 Pct Recovery = 104% Analysis Date = 01/04/13 Pct Recovery = 104% Analysis Date = 01/04/13 Pct Recovery = 104% Analysis Date = 12/25/12 Pct Recovery = 104% Analysis Date = 12/25/12 Pct Recovery = 104% Analysis Date = 12/14/12 Pct Recovery = 104% Analysis Date = 12/14/12 Pct Recovery = 104% Analysis Date = 12/03/12 Pct Recovery = 104% Analysis Date = 12/03/12 Pct Recovery = 104% Analysis Date = 11/23/12 Pct Recovery = 104% Analysis Date = 11/23/12 Pct Recovery = 104% Analysis Date = 11/12/12 Pct Recovery = 104% Analysis Date = 11/12/12 Pct Recovery = 104% Analysis Date = 11/01/12 Pct Recovery = 104% Analysis Date = 11/01/12 Pct Recovery = 104% Analysis Date = 10/21/12 Pct Recovery = 104% Analysis Date = 10/21/12 Pct Recovery = 104% Analysis Date = 10/11/12 Pct Recovery = 104% Analysis Date = 10/11/12 Pct Recovery = 104% Analysis Date = 09/30/12 Pct Recovery = 104% Analysis Date = 09/30/12 Pct Recovery = 104% Analysis Date = 09/19/12 Pct Recovery = 104% Analysis Date = 09/19/12 Pct Recovery = 104% Analysis Date = 09/09/12 Pct Recovery = 104% Analysis Date = 09/09/12 Pct Recovery = 104% Analysis Date = 08/29/12 Pct Recovery = 104% Analysis Date = 08/29/12 Pct Recovery = 104% Analysis Date = 08/18/12 Pct Recovery = 104% Analysis Date = 08/18/12 Pct Recovery = 104% Analysis Date = 08/07/12 Pct Recovery = 104% Analysis Date = 08/07/12 Pct Recovery = 104% Analysis Date = 07/28/12 Pct Recovery = 104% Analysis Date = 07/28/12 Pct Recovery = 104% Analysis Date = 07/17/12 Pct Recovery = 103% Analysis Date = 07/17/12 Pct Recovery = 103% Analysis Date = 07/06/12 Pct Recovery = 103% Analysis Date = 07/06/12 Pct Recovery = 103% Analysis Date = 06/26/12 Pct Recovery = 103% Analysis Date = 06/26/12 Pct Recovery = 103% Analysis Date = 06/15/12 Pct Recovery = 103% Analysis Date = 06/15/12 Pct Recovery = 103% Analysis Date = 06/04/12 Pct Recovery = 103% Analysis Date = 06/04/12 Pct Recovery = 103% Analysis Date = 05/25/12 Pct Recovery = 103% Analysis Date = 05/25/12 Pct Recovery = 103% Analysis Date = 05/14/12 Pct Recovery = 103% Analysis Date = 05/14/12 Pct Recovery = 103% Analysis Date = 05/03/12 Pct Recovery = 103% Analysis Date = 05/03/12 Pct Recovery = 103% Analysis Date = 04/22/12 Pct Recovery = 103% Analysis Date = 04/22/12 Pct Recovery = 103% Analysis Date = 04/12/12 Pct Recovery = 103% Analysis Date = 04/12/12 Pct Recovery = 103% Analysis Date = 04/01/12 Pct Recovery = 102% Analysis Date = 04/01/12 Pct Recovery = 102% Analysis Date = 03/21/12 Pct Recovery = 102% Analysis Date = 03/21/12 Pct Recovery = 102% Analysis Date = 03/11/12 Pct Recovery = 102% Analysis Date = 03/11/12 Pct Recovery = 102% Analysis Date = 02/29/12 Pct Recovery = 102% Analysis Date = 02/29/12 Pct Recovery = 102% Analysis Date = 02/18/12 Pct Recovery = 102% Analysis Date = 02/18/12 Pct Recovery = 102% Analysis Date = 02/07/12 Pct Recovery = 102% Analysis Date = 02/07/12 Pct Recovery = 102% Analysis Date = 01/28/12 Pct Recovery = 102% Analysis Date = 01/28/12 Pct Recovery = 102% Analysis Date = 01/17/12 Pct Recovery = 102% Analysis Date = 01/17/12 Pct Recovery = 102% Analysis Date = 01/06/12 Pct Recovery = 102% Analysis Date = 01/06/12 Pct Recovery = 102% Analysis Date = 12/27/11 Pct Recovery = 102% Analysis Date = 12/27/11 Pct Recovery = 102% Analysis Date = 12/16/11 Pct Recovery = 102% Analysis Date = 12/16/11 Pct Recovery = 102% Analysis Date = 12/05/11 Pct Recovery = 102% Analysis Date = 12/05/11 Pct Recovery = 102% Analysis Date = 11/25/11 Pct Recovery = 102% Analysis Date = 11/25/11 Pct Recovery = 102% Analysis Date = 11/14/11 Pct Recovery = 102% Analysis Date = 11/14/11 Pct Recovery = 102% Analysis Date = 11/03/11 Pct Recovery = 101% Analysis Date = 11/03/11 Pct Recovery = 101% Analysis Date = 10/23/11 Pct Recovery = 101% Analysis Date = 10/23/11 Pct Recovery = 101% Analysis Date = 10/13/11 Pct Recovery = 101% Analysis Date = 10/13/11 Pct Recovery = 101% Analysis Date = 10/02/11 Pct Recovery = 101% Analysis Date = 10/02/11 Pct Recovery = 101% Analysis Date = 09/21/11 Pct Recovery = 101% Analysis Date = 09/21/11 Pct Recovery = 101% Analysis Date = 09/11/11 Pct Recovery = 101% Analysis Date = 09/11/11 Pct Recovery = 101% Analysis Date = 08/31/11 Pct Recovery = 101% Analysis Date = 08/31/11 Pct Recovery = 101% Analysis Date = 08/20/11 Pct Recovery = 101% Analysis Date = 08/20/11 Pct Recovery = 101% Analysis Date = 08/09/11 Pct Recovery = 101% Analysis Date = 08/09/11 Pct Recovery = 101% Analysis Date = 07/30/11 Pct Recovery = 101% Analysis Date = 07/30/11 Pct Recovery = 101% Analysis Date = 07/19/11 Pct Recovery = 101% Analysis Date = 07/19/11 Pct Recovery = 101% Analysis Date = 07/08/11 Pct Recovery = 100% Analysis Date = 07/08/11 Pct Recovery = 100% Analysis Date = 06/28/11 Pct Recovery = 100% Analysis Date = 06/28/11 Pct Recovery = 100% Analysis Date = 06/17/11 Pct Recovery = 100% Analysis Date = 06/17/11 Pct Recovery = 100% Analysis Date = 06/06/11 Pct Recovery = 100% Analysis Date = 06/06/11 Pct Recovery = 100% Analysis Date = 05/27/11 Pct Recovery = 100% Analysis Date = 05/27/11 Pct Recovery = 100% Analysis Date = 05/16/11 Pct Recovery = 100% Analysis Date = 05/16/11 Pct Recovery = 100% Analysis Date = 05/05/11 Pct Recovery = 100% Analysis Date = 05/05/11 Pct Recovery = 100% Analysis Date = 04/24/11 Pct Recovery = 100% Analysis Date = 04/24/11 Pct Recovery = 100% Analysis Date = 04/14/11 Pct Recovery = 99% Analysis Date = 04/14/11 Pct Recovery = 99% Analysis Date = 04/03/11 Pct Recovery = 99% Analysis Date = 04/03/11 Pct Recovery = 99% Analysis Date = 03/23/11 Pct Recovery = 99% Analysis Date = 03/23/11 Pct Recovery = 99% Analysis Date = 03/13/11 Pct Recovery = 99% Analysis Date = 03/13/11 Pct Recovery = 99% Analysis Date = 03/02/11 Pct Recovery = 99% Analysis Date = 03/02/11 Pct Recovery = 99% Analysis Date = 02/19/11 Pct Recovery = 99% Analysis Date = 02/19/11 Pct Recovery = 99% Analysis Date = 02/09/11 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 85 103% 20% 103% 19%
Total 85 103% 20% 103% 19%

Sample Statistics
FIPRONIL

Characteristic N % % Basis
Plotted 85 98% Spiked
Estimated Values 85 98% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 2 2% 2 out of 87
Not Spiked 82 .  
False Positives 3 4% 3 out of 82

BQS OBSP Determination:
FIPRONIL SULFIDE
METHOD: 2033 , TESTIDCODE: 62167GCM29
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 95% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 115% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 89% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 95% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 114% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 79% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 90% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 92% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 93% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 78% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 79% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 91% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 86% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 110% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 93% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 97% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 103% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 96% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 120% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 91% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 101% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 93% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 96% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 90% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 79% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 87% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 86% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 99% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 79% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 105% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 92% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 112% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 85% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 67% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 106% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 68% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 144% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 92% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 99% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 115% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 88% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 81% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 101% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 92% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 99% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 134% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 110% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 102% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 69% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 141% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 94% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 107% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 82% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 78% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 98% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 104% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 114% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 98% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 97% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 112% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 114% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 90% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 153% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 110% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 114% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 110% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 88% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Analysis Date = 01/17/17 Pct Recovery = 94% Analysis Date = 01/07/17 Pct Recovery = 94% Analysis Date = 01/07/17 Pct Recovery = 94% Analysis Date = 12/27/16 Pct Recovery = 94% Analysis Date = 12/27/16 Pct Recovery = 94% Analysis Date = 12/16/16 Pct Recovery = 94% Analysis Date = 12/16/16 Pct Recovery = 94% Analysis Date = 12/05/16 Pct Recovery = 93% Analysis Date = 12/05/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/09/16 Pct Recovery = 93% Analysis Date = 09/09/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/13/16 Pct Recovery = 93% Analysis Date = 05/13/16 Pct Recovery = 93% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 04/21/16 Pct Recovery = 92% Analysis Date = 04/21/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 03/30/16 Pct Recovery = 92% Analysis Date = 03/30/16 Pct Recovery = 92% Analysis Date = 03/20/16 Pct Recovery = 92% Analysis Date = 03/20/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/16/16 Pct Recovery = 92% Analysis Date = 02/16/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/04/16 Pct Recovery = 92% Analysis Date = 01/04/16 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/10/15 Pct Recovery = 92% Analysis Date = 11/10/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/09/15 Pct Recovery = 92% Analysis Date = 10/09/15 Pct Recovery = 92% Analysis Date = 09/28/15 Pct Recovery = 92% Analysis Date = 09/28/15 Pct Recovery = 92% Analysis Date = 09/17/15 Pct Recovery = 91% Analysis Date = 09/17/15 Pct Recovery = 91% Analysis Date = 09/06/15 Pct Recovery = 91% Analysis Date = 09/06/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 05/31/15 Pct Recovery = 91% Analysis Date = 05/31/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/16/15 Pct Recovery = 91% Analysis Date = 03/16/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/01/15 Pct Recovery = 90% Analysis Date = 02/01/15 Pct Recovery = 90% Analysis Date = 01/21/15 Pct Recovery = 90% Analysis Date = 01/21/15 Pct Recovery = 90% Analysis Date = 01/10/15 Pct Recovery = 90% Analysis Date = 01/10/15 Pct Recovery = 90% Analysis Date = 12/31/14 Pct Recovery = 90% Analysis Date = 12/31/14 Pct Recovery = 90% Analysis Date = 12/20/14 Pct Recovery = 90% Analysis Date = 12/20/14 Pct Recovery = 90% Analysis Date = 12/09/14 Pct Recovery = 90% Analysis Date = 12/09/14 Pct Recovery = 90% Analysis Date = 11/28/14 Pct Recovery = 90% Analysis Date = 11/28/14 Pct Recovery = 90% Analysis Date = 11/17/14 Pct Recovery = 90% Analysis Date = 11/17/14 Pct Recovery = 90% Analysis Date = 11/06/14 Pct Recovery = 90% Analysis Date = 11/06/14 Pct Recovery = 90% Analysis Date = 10/26/14 Pct Recovery = 90% Analysis Date = 10/26/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/05/14 Pct Recovery = 90% Analysis Date = 10/05/14 Pct Recovery = 90% Analysis Date = 09/24/14 Pct Recovery = 90% Analysis Date = 09/24/14 Pct Recovery = 90% Analysis Date = 09/13/14 Pct Recovery = 90% Analysis Date = 09/13/14 Pct Recovery = 90% Analysis Date = 09/02/14 Pct Recovery = 90% Analysis Date = 09/02/14 Pct Recovery = 90% Analysis Date = 08/22/14 Pct Recovery = 90% Analysis Date = 08/22/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/01/14 Pct Recovery = 90% Analysis Date = 08/01/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/10/14 Pct Recovery = 90% Analysis Date = 07/10/14 Pct Recovery = 90% Analysis Date = 06/29/14 Pct Recovery = 90% Analysis Date = 06/29/14 Pct Recovery = 90% Analysis Date = 06/18/14 Pct Recovery = 91% Analysis Date = 06/18/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 05/27/14 Pct Recovery = 91% Analysis Date = 05/27/14 Pct Recovery = 91% Analysis Date = 05/17/14 Pct Recovery = 91% Analysis Date = 05/17/14 Pct Recovery = 91% Analysis Date = 05/06/14 Pct Recovery = 91% Analysis Date = 05/06/14 Pct Recovery = 91% Analysis Date = 04/25/14 Pct Recovery = 91% Analysis Date = 04/25/14 Pct Recovery = 91% Analysis Date = 04/14/14 Pct Recovery = 91% Analysis Date = 04/14/14 Pct Recovery = 91% Analysis Date = 04/03/14 Pct Recovery = 91% Analysis Date = 04/03/14 Pct Recovery = 91% Analysis Date = 03/23/14 Pct Recovery = 91% Analysis Date = 03/23/14 Pct Recovery = 91% Analysis Date = 03/12/14 Pct Recovery = 92% Analysis Date = 03/12/14 Pct Recovery = 92% Analysis Date = 03/02/14 Pct Recovery = 92% Analysis Date = 03/02/14 Pct Recovery = 92% Analysis Date = 02/19/14 Pct Recovery = 92% Analysis Date = 02/19/14 Pct Recovery = 92% Analysis Date = 02/08/14 Pct Recovery = 92% Analysis Date = 02/08/14 Pct Recovery = 92% Analysis Date = 01/28/14 Pct Recovery = 92% Analysis Date = 01/28/14 Pct Recovery = 92% Analysis Date = 01/17/14 Pct Recovery = 93% Analysis Date = 01/17/14 Pct Recovery = 93% Analysis Date = 01/06/14 Pct Recovery = 93% Analysis Date = 01/06/14 Pct Recovery = 93% Analysis Date = 12/26/13 Pct Recovery = 93% Analysis Date = 12/26/13 Pct Recovery = 93% Analysis Date = 12/16/13 Pct Recovery = 93% Analysis Date = 12/16/13 Pct Recovery = 93% Analysis Date = 12/05/13 Pct Recovery = 93% Analysis Date = 12/05/13 Pct Recovery = 93% Analysis Date = 11/24/13 Pct Recovery = 94% Analysis Date = 11/24/13 Pct Recovery = 94% Analysis Date = 11/13/13 Pct Recovery = 94% Analysis Date = 11/13/13 Pct Recovery = 94% Analysis Date = 11/02/13 Pct Recovery = 94% Analysis Date = 11/02/13 Pct Recovery = 94% Analysis Date = 10/22/13 Pct Recovery = 94% Analysis Date = 10/22/13 Pct Recovery = 94% Analysis Date = 10/11/13 Pct Recovery = 94% Analysis Date = 10/11/13 Pct Recovery = 94% Analysis Date = 10/01/13 Pct Recovery = 94% Analysis Date = 10/01/13 Pct Recovery = 94% Analysis Date = 09/20/13 Pct Recovery = 95% Analysis Date = 09/20/13 Pct Recovery = 95% Analysis Date = 09/09/13 Pct Recovery = 95% Analysis Date = 09/09/13 Pct Recovery = 95% Analysis Date = 08/29/13 Pct Recovery = 95% Analysis Date = 08/29/13 Pct Recovery = 95% Analysis Date = 08/18/13 Pct Recovery = 96% Analysis Date = 08/18/13 Pct Recovery = 96% Analysis Date = 08/07/13 Pct Recovery = 96% Analysis Date = 08/07/13 Pct Recovery = 96% Analysis Date = 07/27/13 Pct Recovery = 96% Analysis Date = 07/27/13 Pct Recovery = 96% Analysis Date = 07/17/13 Pct Recovery = 96% Analysis Date = 07/17/13 Pct Recovery = 96% Analysis Date = 07/06/13 Pct Recovery = 97% Analysis Date = 07/06/13 Pct Recovery = 97% Analysis Date = 06/25/13 Pct Recovery = 97% Analysis Date = 06/25/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 97% Analysis Date = 06/14/13 Pct Recovery = 97% Analysis Date = 06/03/13 Pct Recovery = 98% Analysis Date = 06/03/13 Pct Recovery = 98% Analysis Date = 05/23/13 Pct Recovery = 98% Analysis Date = 05/23/13 Pct Recovery = 98% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 04/21/13 Pct Recovery = 99% Analysis Date = 04/21/13 Pct Recovery = 99% Analysis Date = 04/10/13 Pct Recovery = 99% Analysis Date = 04/10/13 Pct Recovery = 99% Analysis Date = 03/30/13 Pct Recovery = 99% Analysis Date = 03/30/13 Pct Recovery = 99% Analysis Date = 03/19/13 Pct Recovery = 100% Analysis Date = 03/19/13 Pct Recovery = 100% Analysis Date = 03/08/13 Pct Recovery = 100% Analysis Date = 03/08/13 Pct Recovery = 100% Analysis Date = 02/25/13 Pct Recovery = 100% Analysis Date = 02/25/13 Pct Recovery = 100% Analysis Date = 02/15/13 Pct Recovery = 100% Analysis Date = 02/15/13 Pct Recovery = 100% Analysis Date = 02/04/13 Pct Recovery = 101% Analysis Date = 02/04/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/13/13 Pct Recovery = 101% Analysis Date = 01/13/13 Pct Recovery = 101% Analysis Date = 01/02/13 Pct Recovery = 101% Analysis Date = 01/02/13 Pct Recovery = 101% Analysis Date = 12/22/12 Pct Recovery = 102% Analysis Date = 12/22/12 Pct Recovery = 102% Analysis Date = 12/12/12 Pct Recovery = 102% Analysis Date = 12/12/12 Pct Recovery = 102% Analysis Date = 12/01/12 Pct Recovery = 102% Analysis Date = 12/01/12 Pct Recovery = 102% Analysis Date = 11/20/12 Pct Recovery = 102% Analysis Date = 11/20/12 Pct Recovery = 102% Analysis Date = 11/09/12 Pct Recovery = 102% Analysis Date = 11/09/12 Pct Recovery = 102% Analysis Date = 10/29/12 Pct Recovery = 103% Analysis Date = 10/29/12 Pct Recovery = 103% Analysis Date = 10/18/12 Pct Recovery = 103% Analysis Date = 10/18/12 Pct Recovery = 103% Analysis Date = 10/07/12 Pct Recovery = 103% Analysis Date = 10/07/12 Pct Recovery = 103% Analysis Date = 09/27/12 Pct Recovery = 103% Analysis Date = 09/27/12 Pct Recovery = 103% Analysis Date = 09/16/12 Pct Recovery = 103% Analysis Date = 09/16/12 Pct Recovery = 103% Analysis Date = 09/05/12 Pct Recovery = 103% Analysis Date = 09/05/12 Pct Recovery = 103% Analysis Date = 08/25/12 Pct Recovery = 103% Analysis Date = 08/25/12 Pct Recovery = 103% Analysis Date = 08/14/12 Pct Recovery = 102% Analysis Date = 08/14/12 Pct Recovery = 102% Analysis Date = 08/03/12 Pct Recovery = 102% Analysis Date = 08/03/12 Pct Recovery = 102% Analysis Date = 07/23/12 Pct Recovery = 102% Analysis Date = 07/23/12 Pct Recovery = 102% Analysis Date = 07/13/12 Pct Recovery = 102% Analysis Date = 07/13/12 Pct Recovery = 102% Analysis Date = 07/02/12 Pct Recovery = 102% Analysis Date = 07/02/12 Pct Recovery = 102% Analysis Date = 06/21/12 Pct Recovery = 102% Analysis Date = 06/21/12 Pct Recovery = 102% Analysis Date = 06/10/12 Pct Recovery = 102% Analysis Date = 06/10/12 Pct Recovery = 102% Analysis Date = 05/30/12 Pct Recovery = 102% Analysis Date = 05/30/12 Pct Recovery = 102% Analysis Date = 05/19/12 Pct Recovery = 102% Analysis Date = 05/19/12 Pct Recovery = 102% Analysis Date = 05/08/12 Pct Recovery = 102% Analysis Date = 05/08/12 Pct Recovery = 102% Analysis Date = 04/28/12 Pct Recovery = 102% Analysis Date = 04/28/12 Pct Recovery = 102% Analysis Date = 04/17/12 Pct Recovery = 101% Analysis Date = 04/17/12 Pct Recovery = 101% Analysis Date = 04/06/12 Pct Recovery = 101% Analysis Date = 04/06/12 Pct Recovery = 101% Analysis Date = 03/26/12 Pct Recovery = 101% Analysis Date = 03/26/12 Pct Recovery = 101% Analysis Date = 03/15/12 Pct Recovery = 101% Analysis Date = 03/15/12 Pct Recovery = 101% Analysis Date = 03/04/12 Pct Recovery = 101% Analysis Date = 03/04/12 Pct Recovery = 101% Analysis Date = 02/22/12 Pct Recovery = 101% Analysis Date = 02/22/12 Pct Recovery = 101% Analysis Date = 02/12/12 Pct Recovery = 101% Analysis Date = 02/12/12 Pct Recovery = 101% Analysis Date = 02/01/12 Pct Recovery = 101% Analysis Date = 02/01/12 Pct Recovery = 101% Analysis Date = 01/21/12 Pct Recovery = 100% Analysis Date = 01/21/12 Pct Recovery = 100% Analysis Date = 01/10/12 Pct Recovery = 100% Analysis Date = 01/10/12 Pct Recovery = 100% Analysis Date = 12/30/11 Pct Recovery = 100% Analysis Date = 12/30/11 Pct Recovery = 100% Analysis Date = 12/19/11 Pct Recovery = 100% Analysis Date = 12/19/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 100% Analysis Date = 11/28/11 Pct Recovery = 100% Analysis Date = 11/28/11 Pct Recovery = 100% Analysis Date = 11/17/11 Pct Recovery = 100% Analysis Date = 11/17/11 Pct Recovery = 100% Analysis Date = 11/06/11 Pct Recovery = 99% Analysis Date = 11/06/11 Pct Recovery = 99% Analysis Date = 10/26/11 Pct Recovery = 99% Analysis Date = 10/26/11 Pct Recovery = 99% Analysis Date = 10/15/11 Pct Recovery = 99% Analysis Date = 10/15/11 Pct Recovery = 99% Analysis Date = 10/04/11 Pct Recovery = 99% Analysis Date = 10/04/11 Pct Recovery = 99% Analysis Date = 09/23/11 Pct Recovery = 99% Analysis Date = 09/23/11 Pct Recovery = 99% Analysis Date = 09/13/11 Pct Recovery = 99% Analysis Date = 09/13/11 Pct Recovery = 99% Analysis Date = 09/02/11 Pct Recovery = 98% Analysis Date = 09/02/11 Pct Recovery = 98% Analysis Date = 08/22/11 Pct Recovery = 98% Analysis Date = 08/22/11 Pct Recovery = 98% Analysis Date = 08/11/11 Pct Recovery = 98% Analysis Date = 08/11/11 Pct Recovery = 98% Analysis Date = 07/31/11 Pct Recovery = 98% Analysis Date = 07/31/11 Pct Recovery = 98% Analysis Date = 07/20/11 Pct Recovery = 98% Analysis Date = 07/20/11 Pct Recovery = 98% Analysis Date = 07/09/11 Pct Recovery = 98% Analysis Date = 07/09/11 Pct Recovery = 98% Analysis Date = 06/29/11 Pct Recovery = 97% Analysis Date = 06/29/11 Pct Recovery = 97% Analysis Date = 06/18/11 Pct Recovery = 97% Analysis Date = 06/18/11 Pct Recovery = 97% Analysis Date = 06/07/11 Pct Recovery = 97% Analysis Date = 06/07/11 Pct Recovery = 97% Analysis Date = 05/27/11 Pct Recovery = 97% Analysis Date = 05/27/11 Pct Recovery = 97% Analysis Date = 05/16/11 Pct Recovery = 97% Analysis Date = 05/16/11 Pct Recovery = 97% Analysis Date = 05/05/11 Pct Recovery = 96% Analysis Date = 05/05/11 Pct Recovery = 96% Analysis Date = 04/24/11 Pct Recovery = 96% Analysis Date = 04/24/11 Pct Recovery = 96% Analysis Date = 04/14/11 Pct Recovery = 96% Analysis Date = 04/14/11 Pct Recovery = 96% Analysis Date = 04/03/11 Pct Recovery = 96% Analysis Date = 04/03/11 Pct Recovery = 96% Analysis Date = 03/23/11 Pct Recovery = 96% Analysis Date = 03/23/11 Pct Recovery = 96% Analysis Date = 03/12/11 Pct Recovery = 95% Analysis Date = 03/12/11 Pct Recovery = 95% Analysis Date = 03/01/11 Pct Recovery = 95% Analysis Date = 03/01/11 Pct Recovery = 95% Analysis Date = 02/18/11 Pct Recovery = 95% Analysis Date = 02/18/11 Pct Recovery = 95% Analysis Date = 02/08/11 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 86 95% 17% 93% 13%
Total 86 95% 17% 93% 13%

Sample Statistics
FIPRONIL SULFIDE

Characteristic N % % Basis
Plotted 86 99% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 1 1% 1 out of 87
Not Spiked 62 .  
False Positives 3 5% 3 out of 62

BQS OBSP Determination:
FIPRONIL SULFONE
METHOD: 2033 , TESTIDCODE: 62168GCM29
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 73% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 76% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 79% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 73% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 169% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 63% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 74% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 72% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 44% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 62% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 83% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 90% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 84% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 69% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 71% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 78% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 95% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 87% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 73% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 80% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 88% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 75% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 82% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 62% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 93% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 74% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 64% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 79% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 71% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 114% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 80% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 75% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 92% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 87% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 131% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 86% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 59% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 92% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 116% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 81% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 90% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 86% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 113% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 70% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 78% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 103% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 122% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 102% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 84% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 108% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 97% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 72% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 62% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 106% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 102% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 59% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 86% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 74% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 81% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 101% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 141% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 112% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 64% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 92% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 147% Analysis Date = 01/17/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/16/16 Pct Recovery = 92% Analysis Date = 12/16/16 Pct Recovery = 92% Analysis Date = 12/05/16 Pct Recovery = 92% Analysis Date = 12/05/16 Pct Recovery = 92% Analysis Date = 11/24/16 Pct Recovery = 92% Analysis Date = 11/24/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 10/23/16 Pct Recovery = 92% Analysis Date = 10/23/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/09/16 Pct Recovery = 91% Analysis Date = 09/09/16 Pct Recovery = 91% Analysis Date = 08/29/16 Pct Recovery = 91% Analysis Date = 08/29/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 07/28/16 Pct Recovery = 91% Analysis Date = 07/28/16 Pct Recovery = 91% Analysis Date = 07/17/16 Pct Recovery = 90% Analysis Date = 07/17/16 Pct Recovery = 90% Analysis Date = 07/06/16 Pct Recovery = 90% Analysis Date = 07/06/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 90% Analysis Date = 06/14/16 Pct Recovery = 90% Analysis Date = 06/14/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/02/16 Pct Recovery = 90% Analysis Date = 05/02/16 Pct Recovery = 90% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/21/16 Pct Recovery = 89% Analysis Date = 04/10/16 Pct Recovery = 89% Analysis Date = 04/10/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 89% Analysis Date = 03/20/16 Pct Recovery = 89% Analysis Date = 03/20/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/27/16 Pct Recovery = 89% Analysis Date = 02/16/16 Pct Recovery = 89% Analysis Date = 02/16/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 89% Analysis Date = 02/05/16 Pct Recovery = 89% Analysis Date = 01/25/16 Pct Recovery = 88% Analysis Date = 01/25/16 Pct Recovery = 88% Analysis Date = 01/15/16 Pct Recovery = 88% Analysis Date = 01/15/16 Pct Recovery = 88% Analysis Date = 01/04/16 Pct Recovery = 88% Analysis Date = 01/04/16 Pct Recovery = 88% Analysis Date = 12/24/15 Pct Recovery = 88% Analysis Date = 12/24/15 Pct Recovery = 88% Analysis Date = 12/13/15 Pct Recovery = 88% Analysis Date = 12/13/15 Pct Recovery = 88% Analysis Date = 12/02/15 Pct Recovery = 88% Analysis Date = 12/02/15 Pct Recovery = 88% Analysis Date = 11/21/15 Pct Recovery = 88% Analysis Date = 11/21/15 Pct Recovery = 88% Analysis Date = 11/10/15 Pct Recovery = 88% Analysis Date = 11/10/15 Pct Recovery = 88% Analysis Date = 10/31/15 Pct Recovery = 88% Analysis Date = 10/31/15 Pct Recovery = 88% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/20/15 Pct Recovery = 87% Analysis Date = 10/09/15 Pct Recovery = 87% Analysis Date = 10/09/15 Pct Recovery = 87% Analysis Date = 09/28/15 Pct Recovery = 87% Analysis Date = 09/28/15 Pct Recovery = 87% Analysis Date = 09/17/15 Pct Recovery = 87% Analysis Date = 09/17/15 Pct Recovery = 87% Analysis Date = 09/06/15 Pct Recovery = 87% Analysis Date = 09/06/15 Pct Recovery = 87% Analysis Date = 08/27/15 Pct Recovery = 87% Analysis Date = 08/27/15 Pct Recovery = 87% Analysis Date = 08/16/15 Pct Recovery = 87% Analysis Date = 08/16/15 Pct Recovery = 87% Analysis Date = 08/05/15 Pct Recovery = 87% Analysis Date = 08/05/15 Pct Recovery = 87% Analysis Date = 07/25/15 Pct Recovery = 87% Analysis Date = 07/25/15 Pct Recovery = 87% Analysis Date = 07/14/15 Pct Recovery = 86% Analysis Date = 07/14/15 Pct Recovery = 86% Analysis Date = 07/03/15 Pct Recovery = 86% Analysis Date = 07/03/15 Pct Recovery = 86% Analysis Date = 06/22/15 Pct Recovery = 86% Analysis Date = 06/22/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/12/15 Pct Recovery = 86% Analysis Date = 06/01/15 Pct Recovery = 86% Analysis Date = 06/01/15 Pct Recovery = 86% Analysis Date = 05/21/15 Pct Recovery = 86% Analysis Date = 05/21/15 Pct Recovery = 86% Analysis Date = 05/10/15 Pct Recovery = 86% Analysis Date = 05/10/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 86% Analysis Date = 04/29/15 Pct Recovery = 86% Analysis Date = 04/18/15 Pct Recovery = 85% Analysis Date = 04/18/15 Pct Recovery = 85% Analysis Date = 04/07/15 Pct Recovery = 85% Analysis Date = 04/07/15 Pct Recovery = 85% Analysis Date = 03/28/15 Pct Recovery = 85% Analysis Date = 03/28/15 Pct Recovery = 85% Analysis Date = 03/17/15 Pct Recovery = 85% Analysis Date = 03/17/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 85% Analysis Date = 03/06/15 Pct Recovery = 85% Analysis Date = 02/23/15 Pct Recovery = 84% Analysis Date = 02/23/15 Pct Recovery = 84% Analysis Date = 02/12/15 Pct Recovery = 84% Analysis Date = 02/12/15 Pct Recovery = 84% Analysis Date = 02/01/15 Pct Recovery = 84% Analysis Date = 02/01/15 Pct Recovery = 84% Analysis Date = 01/22/15 Pct Recovery = 84% Analysis Date = 01/22/15 Pct Recovery = 84% Analysis Date = 01/11/15 Pct Recovery = 84% Analysis Date = 01/11/15 Pct Recovery = 84% Analysis Date = 12/31/14 Pct Recovery = 84% Analysis Date = 12/31/14 Pct Recovery = 84% Analysis Date = 12/20/14 Pct Recovery = 83% Analysis Date = 12/20/14 Pct Recovery = 83% Analysis Date = 12/09/14 Pct Recovery = 83% Analysis Date = 12/09/14 Pct Recovery = 83% Analysis Date = 11/28/14 Pct Recovery = 83% Analysis Date = 11/28/14 Pct Recovery = 83% Analysis Date = 11/17/14 Pct Recovery = 83% Analysis Date = 11/17/14 Pct Recovery = 83% Analysis Date = 11/07/14 Pct Recovery = 83% Analysis Date = 11/07/14 Pct Recovery = 83% Analysis Date = 10/27/14 Pct Recovery = 82% Analysis Date = 10/27/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 82% Analysis Date = 09/24/14 Pct Recovery = 83% Analysis Date = 09/24/14 Pct Recovery = 83% Analysis Date = 09/13/14 Pct Recovery = 83% Analysis Date = 09/13/14 Pct Recovery = 83% Analysis Date = 09/02/14 Pct Recovery = 83% Analysis Date = 09/02/14 Pct Recovery = 83% Analysis Date = 08/23/14 Pct Recovery = 83% Analysis Date = 08/23/14 Pct Recovery = 83% Analysis Date = 08/12/14 Pct Recovery = 83% Analysis Date = 08/12/14 Pct Recovery = 83% Analysis Date = 08/01/14 Pct Recovery = 83% Analysis Date = 08/01/14 Pct Recovery = 83% Analysis Date = 07/21/14 Pct Recovery = 83% Analysis Date = 07/21/14 Pct Recovery = 83% Analysis Date = 07/10/14 Pct Recovery = 83% Analysis Date = 07/10/14 Pct Recovery = 83% Analysis Date = 06/29/14 Pct Recovery = 83% Analysis Date = 06/29/14 Pct Recovery = 83% Analysis Date = 06/19/14 Pct Recovery = 84% Analysis Date = 06/19/14 Pct Recovery = 84% Analysis Date = 06/08/14 Pct Recovery = 84% Analysis Date = 06/08/14 Pct Recovery = 84% Analysis Date = 05/28/14 Pct Recovery = 84% Analysis Date = 05/28/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 84% Analysis Date = 05/06/14 Pct Recovery = 84% Analysis Date = 05/06/14 Pct Recovery = 84% Analysis Date = 04/25/14 Pct Recovery = 84% Analysis Date = 04/25/14 Pct Recovery = 84% Analysis Date = 04/14/14 Pct Recovery = 85% Analysis Date = 04/14/14 Pct Recovery = 85% Analysis Date = 04/04/14 Pct Recovery = 85% Analysis Date = 04/04/14 Pct Recovery = 85% Analysis Date = 03/24/14 Pct Recovery = 85% Analysis Date = 03/24/14 Pct Recovery = 85% Analysis Date = 03/13/14 Pct Recovery = 85% Analysis Date = 03/13/14 Pct Recovery = 85% Analysis Date = 03/02/14 Pct Recovery = 85% Analysis Date = 03/02/14 Pct Recovery = 85% Analysis Date = 02/19/14 Pct Recovery = 85% Analysis Date = 02/19/14 Pct Recovery = 85% Analysis Date = 02/08/14 Pct Recovery = 85% Analysis Date = 02/08/14 Pct Recovery = 85% Analysis Date = 01/28/14 Pct Recovery = 85% Analysis Date = 01/28/14 Pct Recovery = 85% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 12/27/13 Pct Recovery = 86% Analysis Date = 12/27/13 Pct Recovery = 86% Analysis Date = 12/16/13 Pct Recovery = 86% Analysis Date = 12/16/13 Pct Recovery = 86% Analysis Date = 12/05/13 Pct Recovery = 86% Analysis Date = 12/05/13 Pct Recovery = 86% Analysis Date = 11/24/13 Pct Recovery = 86% Analysis Date = 11/24/13 Pct Recovery = 86% Analysis Date = 11/14/13 Pct Recovery = 86% Analysis Date = 11/14/13 Pct Recovery = 86% Analysis Date = 11/03/13 Pct Recovery = 87% Analysis Date = 11/03/13 Pct Recovery = 87% Analysis Date = 10/23/13 Pct Recovery = 87% Analysis Date = 10/23/13 Pct Recovery = 87% Analysis Date = 10/12/13 Pct Recovery = 87% Analysis Date = 10/12/13 Pct Recovery = 87% Analysis Date = 10/01/13 Pct Recovery = 87% Analysis Date = 10/01/13 Pct Recovery = 87% Analysis Date = 09/20/13 Pct Recovery = 87% Analysis Date = 09/20/13 Pct Recovery = 87% Analysis Date = 09/09/13 Pct Recovery = 87% Analysis Date = 09/09/13 Pct Recovery = 87% Analysis Date = 08/30/13 Pct Recovery = 87% Analysis Date = 08/30/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 87% Analysis Date = 08/08/13 Pct Recovery = 88% Analysis Date = 08/08/13 Pct Recovery = 88% Analysis Date = 07/28/13 Pct Recovery = 88% Analysis Date = 07/28/13 Pct Recovery = 88% Analysis Date = 07/17/13 Pct Recovery = 88% Analysis Date = 07/17/13 Pct Recovery = 88% Analysis Date = 07/06/13 Pct Recovery = 88% Analysis Date = 07/06/13 Pct Recovery = 88% Analysis Date = 06/25/13 Pct Recovery = 88% Analysis Date = 06/25/13 Pct Recovery = 88% Analysis Date = 06/15/13 Pct Recovery = 88% Analysis Date = 06/15/13 Pct Recovery = 88% Analysis Date = 06/04/13 Pct Recovery = 88% Analysis Date = 06/04/13 Pct Recovery = 88% Analysis Date = 05/24/13 Pct Recovery = 88% Analysis Date = 05/24/13 Pct Recovery = 88% Analysis Date = 05/13/13 Pct Recovery = 89% Analysis Date = 05/13/13 Pct Recovery = 89% Analysis Date = 05/02/13 Pct Recovery = 89% Analysis Date = 05/02/13 Pct Recovery = 89% Analysis Date = 04/21/13 Pct Recovery = 89% Analysis Date = 04/21/13 Pct Recovery = 89% Analysis Date = 04/11/13 Pct Recovery = 89% Analysis Date = 04/11/13 Pct Recovery = 89% Analysis Date = 03/31/13 Pct Recovery = 89% Analysis Date = 03/31/13 Pct Recovery = 89% Analysis Date = 03/20/13 Pct Recovery = 89% Analysis Date = 03/20/13 Pct Recovery = 89% Analysis Date = 03/09/13 Pct Recovery = 89% Analysis Date = 03/09/13 Pct Recovery = 89% Analysis Date = 02/26/13 Pct Recovery = 89% Analysis Date = 02/26/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 01/25/13 Pct Recovery = 89% Analysis Date = 01/25/13 Pct Recovery = 89% Analysis Date = 01/14/13 Pct Recovery = 89% Analysis Date = 01/14/13 Pct Recovery = 89% Analysis Date = 01/03/13 Pct Recovery = 89% Analysis Date = 01/03/13 Pct Recovery = 89% Analysis Date = 12/23/12 Pct Recovery = 89% Analysis Date = 12/23/12 Pct Recovery = 89% Analysis Date = 12/12/12 Pct Recovery = 89% Analysis Date = 12/12/12 Pct Recovery = 89% Analysis Date = 12/01/12 Pct Recovery = 89% Analysis Date = 12/01/12 Pct Recovery = 89% Analysis Date = 11/20/12 Pct Recovery = 89% Analysis Date = 11/20/12 Pct Recovery = 89% Analysis Date = 11/10/12 Pct Recovery = 89% Analysis Date = 11/10/12 Pct Recovery = 89% Analysis Date = 10/30/12 Pct Recovery = 88% Analysis Date = 10/30/12 Pct Recovery = 88% Analysis Date = 10/19/12 Pct Recovery = 88% Analysis Date = 10/19/12 Pct Recovery = 88% Analysis Date = 10/08/12 Pct Recovery = 88% Analysis Date = 10/08/12 Pct Recovery = 88% Analysis Date = 09/27/12 Pct Recovery = 88% Analysis Date = 09/27/12 Pct Recovery = 88% Analysis Date = 09/16/12 Pct Recovery = 88% Analysis Date = 09/16/12 Pct Recovery = 88% Analysis Date = 09/06/12 Pct Recovery = 88% Analysis Date = 09/06/12 Pct Recovery = 88% Analysis Date = 08/26/12 Pct Recovery = 88% Analysis Date = 08/26/12 Pct Recovery = 88% Analysis Date = 08/15/12 Pct Recovery = 87% Analysis Date = 08/15/12 Pct Recovery = 87% Analysis Date = 08/04/12 Pct Recovery = 87% Analysis Date = 08/04/12 Pct Recovery = 87% Analysis Date = 07/24/12 Pct Recovery = 87% Analysis Date = 07/24/12 Pct Recovery = 87% Analysis Date = 07/13/12 Pct Recovery = 87% Analysis Date = 07/13/12 Pct Recovery = 87% Analysis Date = 07/02/12 Pct Recovery = 87% Analysis Date = 07/02/12 Pct Recovery = 87% Analysis Date = 06/22/12 Pct Recovery = 87% Analysis Date = 06/22/12 Pct Recovery = 87% Analysis Date = 06/11/12 Pct Recovery = 87% Analysis Date = 06/11/12 Pct Recovery = 87% Analysis Date = 05/31/12 Pct Recovery = 87% Analysis Date = 05/31/12 Pct Recovery = 87% Analysis Date = 05/20/12 Pct Recovery = 87% Analysis Date = 05/20/12 Pct Recovery = 87% Analysis Date = 05/09/12 Pct Recovery = 87% Analysis Date = 05/09/12 Pct Recovery = 87% Analysis Date = 04/28/12 Pct Recovery = 87% Analysis Date = 04/28/12 Pct Recovery = 87% Analysis Date = 04/17/12 Pct Recovery = 86% Analysis Date = 04/17/12 Pct Recovery = 86% Analysis Date = 04/07/12 Pct Recovery = 86% Analysis Date = 04/07/12 Pct Recovery = 86% Analysis Date = 03/27/12 Pct Recovery = 86% Analysis Date = 03/27/12 Pct Recovery = 86% Analysis Date = 03/16/12 Pct Recovery = 86% Analysis Date = 03/16/12 Pct Recovery = 86% Analysis Date = 03/05/12 Pct Recovery = 86% Analysis Date = 03/05/12 Pct Recovery = 86% Analysis Date = 02/23/12 Pct Recovery = 86% Analysis Date = 02/23/12 Pct Recovery = 86% Analysis Date = 02/12/12 Pct Recovery = 86% Analysis Date = 02/12/12 Pct Recovery = 86% Analysis Date = 02/02/12 Pct Recovery = 86% Analysis Date = 02/02/12 Pct Recovery = 86% Analysis Date = 01/22/12 Pct Recovery = 86% Analysis Date = 01/22/12 Pct Recovery = 86% Analysis Date = 01/11/12 Pct Recovery = 86% Analysis Date = 01/11/12 Pct Recovery = 86% Analysis Date = 12/31/11 Pct Recovery = 86% Analysis Date = 12/31/11 Pct Recovery = 86% Analysis Date = 12/20/11 Pct Recovery = 86% Analysis Date = 12/20/11 Pct Recovery = 86% Analysis Date = 12/09/11 Pct Recovery = 86% Analysis Date = 12/09/11 Pct Recovery = 86% Analysis Date = 11/28/11 Pct Recovery = 85% Analysis Date = 11/28/11 Pct Recovery = 85% Analysis Date = 11/18/11 Pct Recovery = 85% Analysis Date = 11/18/11 Pct Recovery = 85% Analysis Date = 11/07/11 Pct Recovery = 85% Analysis Date = 11/07/11 Pct Recovery = 85% Analysis Date = 10/27/11 Pct Recovery = 85% Analysis Date = 10/27/11 Pct Recovery = 85% Analysis Date = 10/16/11 Pct Recovery = 85% Analysis Date = 10/16/11 Pct Recovery = 85% Analysis Date = 10/05/11 Pct Recovery = 85% Analysis Date = 10/05/11 Pct Recovery = 85% Analysis Date = 09/24/11 Pct Recovery = 85% Analysis Date = 09/24/11 Pct Recovery = 85% Analysis Date = 09/13/11 Pct Recovery = 85% Analysis Date = 09/13/11 Pct Recovery = 85% Analysis Date = 09/03/11 Pct Recovery = 85% Analysis Date = 09/03/11 Pct Recovery = 85% Analysis Date = 08/23/11 Pct Recovery = 85% Analysis Date = 08/23/11 Pct Recovery = 85% Analysis Date = 08/12/11 Pct Recovery = 85% Analysis Date = 08/12/11 Pct Recovery = 85% Analysis Date = 08/01/11 Pct Recovery = 85% Analysis Date = 08/01/11 Pct Recovery = 85% Analysis Date = 07/21/11 Pct Recovery = 85% Analysis Date = 07/21/11 Pct Recovery = 85% Analysis Date = 07/10/11 Pct Recovery = 85% Analysis Date = 07/10/11 Pct Recovery = 85% Analysis Date = 06/30/11 Pct Recovery = 85% Analysis Date = 06/30/11 Pct Recovery = 85% Analysis Date = 06/19/11 Pct Recovery = 85% Analysis Date = 06/19/11 Pct Recovery = 85% Analysis Date = 06/08/11 Pct Recovery = 85% Analysis Date = 06/08/11 Pct Recovery = 85% Analysis Date = 05/28/11 Pct Recovery = 85% Analysis Date = 05/28/11 Pct Recovery = 85% Analysis Date = 05/17/11 Pct Recovery = 85% Analysis Date = 05/17/11 Pct Recovery = 85% Analysis Date = 05/06/11 Pct Recovery = 85% Analysis Date = 05/06/11 Pct Recovery = 85% Analysis Date = 04/25/11 Pct Recovery = 85% Analysis Date = 04/25/11 Pct Recovery = 85% Analysis Date = 04/15/11 Pct Recovery = 85% Analysis Date = 04/15/11 Pct Recovery = 85% Analysis Date = 04/04/11 Pct Recovery = 85% Analysis Date = 04/04/11 Pct Recovery = 85% Analysis Date = 03/24/11 Pct Recovery = 85% Analysis Date = 03/24/11 Pct Recovery = 85% Analysis Date = 03/13/11 Pct Recovery = 85% Analysis Date = 03/13/11 Pct Recovery = 85% Analysis Date = 03/02/11 Pct Recovery = 85% Analysis Date = 03/02/11 Pct Recovery = 85% Analysis Date = 02/19/11 Pct Recovery = 85% Analysis Date = 02/19/11 Pct Recovery = 85% Analysis Date = 02/09/11 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 86% 21% 81% 16%
Total 79 86% 21% 81% 16%

Sample Statistics
FIPRONIL SULFONE

Characteristic N % % Basis
Plotted 79 99% Spiked
Estimated Values 6 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 1 1% 1 out of 80
Not Spiked 75 .  
False Positives 2 3% 2 out of 75

BQS OBSP Determination:
FONOFOS
METHOD: 2033 , TESTIDCODE: 04095GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 93% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 146% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 132% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 90% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 88% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 87% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 76% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 111% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 125% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 93% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 85% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 90% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 80% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 63% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 76% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 70% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 89% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 131% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 126% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 91% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 77% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 86% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 84% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 90% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 87% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 79% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 70% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 84% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 87% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 55% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 51% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 86% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 85% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 70% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 77% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 99% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 98% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 85% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 92% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 106% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 75% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 63% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 74% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 70% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 74% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 60% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 94% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 91% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 59% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 78% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 82% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 77% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 84% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 71% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 78% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 74% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 86% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 76% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 86% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 84% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 71% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 32% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 110% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 114% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 103% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 114% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 72% Analysis Date = 12/20/16 Pct Recovery = 76% Analysis Date = 12/09/16 Pct Recovery = 76% Analysis Date = 12/09/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/16/16 Pct Recovery = 76% Analysis Date = 10/16/16 Pct Recovery = 76% Analysis Date = 10/06/16 Pct Recovery = 76% Analysis Date = 10/06/16 Pct Recovery = 76% Analysis Date = 09/25/16 Pct Recovery = 76% Analysis Date = 09/25/16 Pct Recovery = 76% Analysis Date = 09/14/16 Pct Recovery = 76% Analysis Date = 09/14/16 Pct Recovery = 76% Analysis Date = 09/04/16 Pct Recovery = 76% Analysis Date = 09/04/16 Pct Recovery = 76% Analysis Date = 08/24/16 Pct Recovery = 76% Analysis Date = 08/24/16 Pct Recovery = 76% Analysis Date = 08/13/16 Pct Recovery = 76% Analysis Date = 08/13/16 Pct Recovery = 76% Analysis Date = 08/03/16 Pct Recovery = 76% Analysis Date = 08/03/16 Pct Recovery = 76% Analysis Date = 07/23/16 Pct Recovery = 76% Analysis Date = 07/23/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/02/16 Pct Recovery = 76% Analysis Date = 07/02/16 Pct Recovery = 76% Analysis Date = 06/21/16 Pct Recovery = 76% Analysis Date = 06/21/16 Pct Recovery = 76% Analysis Date = 06/10/16 Pct Recovery = 75% Analysis Date = 06/10/16 Pct Recovery = 75% Analysis Date = 05/31/16 Pct Recovery = 75% Analysis Date = 05/31/16 Pct Recovery = 75% Analysis Date = 05/20/16 Pct Recovery = 75% Analysis Date = 05/20/16 Pct Recovery = 75% Analysis Date = 05/09/16 Pct Recovery = 75% Analysis Date = 05/09/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/07/16 Pct Recovery = 75% Analysis Date = 04/07/16 Pct Recovery = 75% Analysis Date = 03/28/16 Pct Recovery = 75% Analysis Date = 03/28/16 Pct Recovery = 75% Analysis Date = 03/17/16 Pct Recovery = 75% Analysis Date = 03/17/16 Pct Recovery = 75% Analysis Date = 03/06/16 Pct Recovery = 75% Analysis Date = 03/06/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/14/16 Pct Recovery = 75% Analysis Date = 02/14/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 02/03/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/23/16 Pct Recovery = 75% Analysis Date = 01/13/16 Pct Recovery = 75% Analysis Date = 01/13/16 Pct Recovery = 75% Analysis Date = 01/02/16 Pct Recovery = 75% Analysis Date = 01/02/16 Pct Recovery = 75% Analysis Date = 12/22/15 Pct Recovery = 75% Analysis Date = 12/22/15 Pct Recovery = 75% Analysis Date = 12/12/15 Pct Recovery = 75% Analysis Date = 12/12/15 Pct Recovery = 75% Analysis Date = 12/01/15 Pct Recovery = 75% Analysis Date = 12/01/15 Pct Recovery = 75% Analysis Date = 11/20/15 Pct Recovery = 75% Analysis Date = 11/20/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 10/30/15 Pct Recovery = 75% Analysis Date = 10/30/15 Pct Recovery = 75% Analysis Date = 10/19/15 Pct Recovery = 75% Analysis Date = 10/19/15 Pct Recovery = 75% Analysis Date = 10/09/15 Pct Recovery = 75% Analysis Date = 10/09/15 Pct Recovery = 75% Analysis Date = 09/28/15 Pct Recovery = 75% Analysis Date = 09/28/15 Pct Recovery = 75% Analysis Date = 09/17/15 Pct Recovery = 75% Analysis Date = 09/17/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 09/07/15 Pct Recovery = 75% Analysis Date = 08/27/15 Pct Recovery = 75% Analysis Date = 08/27/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 76% Analysis Date = 08/16/15 Pct Recovery = 76% Analysis Date = 08/06/15 Pct Recovery = 76% Analysis Date = 08/06/15 Pct Recovery = 76% Analysis Date = 07/26/15 Pct Recovery = 76% Analysis Date = 07/26/15 Pct Recovery = 76% Analysis Date = 07/15/15 Pct Recovery = 76% Analysis Date = 07/15/15 Pct Recovery = 76% Analysis Date = 07/05/15 Pct Recovery = 76% Analysis Date = 07/05/15 Pct Recovery = 76% Analysis Date = 06/24/15 Pct Recovery = 76% Analysis Date = 06/24/15 Pct Recovery = 76% Analysis Date = 06/13/15 Pct Recovery = 76% Analysis Date = 06/13/15 Pct Recovery = 76% Analysis Date = 06/02/15 Pct Recovery = 76% Analysis Date = 06/02/15 Pct Recovery = 76% Analysis Date = 05/23/15 Pct Recovery = 76% Analysis Date = 05/23/15 Pct Recovery = 76% Analysis Date = 05/12/15 Pct Recovery = 76% Analysis Date = 05/12/15 Pct Recovery = 76% Analysis Date = 05/01/15 Pct Recovery = 76% Analysis Date = 05/01/15 Pct Recovery = 76% Analysis Date = 04/21/15 Pct Recovery = 76% Analysis Date = 04/21/15 Pct Recovery = 76% Analysis Date = 04/10/15 Pct Recovery = 76% Analysis Date = 04/10/15 Pct Recovery = 76% Analysis Date = 03/30/15 Pct Recovery = 76% Analysis Date = 03/30/15 Pct Recovery = 76% Analysis Date = 03/20/15 Pct Recovery = 76% Analysis Date = 03/20/15 Pct Recovery = 76% Analysis Date = 03/09/15 Pct Recovery = 76% Analysis Date = 03/09/15 Pct Recovery = 76% Analysis Date = 02/26/15 Pct Recovery = 76% Analysis Date = 02/26/15 Pct Recovery = 76% Analysis Date = 02/16/15 Pct Recovery = 76% Analysis Date = 02/16/15 Pct Recovery = 76% Analysis Date = 02/05/15 Pct Recovery = 77% Analysis Date = 02/05/15 Pct Recovery = 77% Analysis Date = 01/25/15 Pct Recovery = 77% Analysis Date = 01/25/15 Pct Recovery = 77% Analysis Date = 01/15/15 Pct Recovery = 77% Analysis Date = 01/15/15 Pct Recovery = 77% Analysis Date = 01/04/15 Pct Recovery = 77% Analysis Date = 01/04/15 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/24/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 77% Analysis Date = 12/14/14 Pct Recovery = 77% Analysis Date = 12/03/14 Pct Recovery = 77% Analysis Date = 12/03/14 Pct Recovery = 77% Analysis Date = 11/22/14 Pct Recovery = 77% Analysis Date = 11/22/14 Pct Recovery = 77% Analysis Date = 11/12/14 Pct Recovery = 77% Analysis Date = 11/12/14 Pct Recovery = 77% Analysis Date = 11/01/14 Pct Recovery = 77% Analysis Date = 11/01/14 Pct Recovery = 77% Analysis Date = 10/21/14 Pct Recovery = 78% Analysis Date = 10/21/14 Pct Recovery = 78% Analysis Date = 10/11/14 Pct Recovery = 78% Analysis Date = 10/11/14 Pct Recovery = 78% Analysis Date = 09/30/14 Pct Recovery = 78% Analysis Date = 09/30/14 Pct Recovery = 78% Analysis Date = 09/19/14 Pct Recovery = 78% Analysis Date = 09/19/14 Pct Recovery = 78% Analysis Date = 09/08/14 Pct Recovery = 79% Analysis Date = 09/08/14 Pct Recovery = 79% Analysis Date = 08/29/14 Pct Recovery = 79% Analysis Date = 08/29/14 Pct Recovery = 79% Analysis Date = 08/18/14 Pct Recovery = 79% Analysis Date = 08/18/14 Pct Recovery = 79% Analysis Date = 08/07/14 Pct Recovery = 80% Analysis Date = 08/07/14 Pct Recovery = 80% Analysis Date = 07/28/14 Pct Recovery = 80% Analysis Date = 07/28/14 Pct Recovery = 80% Analysis Date = 07/17/14 Pct Recovery = 81% Analysis Date = 07/17/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 07/06/14 Pct Recovery = 81% Analysis Date = 06/26/14 Pct Recovery = 81% Analysis Date = 06/26/14 Pct Recovery = 81% Analysis Date = 06/15/14 Pct Recovery = 82% Analysis Date = 06/15/14 Pct Recovery = 82% Analysis Date = 06/04/14 Pct Recovery = 82% Analysis Date = 06/04/14 Pct Recovery = 82% Analysis Date = 05/25/14 Pct Recovery = 83% Analysis Date = 05/25/14 Pct Recovery = 83% Analysis Date = 05/14/14 Pct Recovery = 83% Analysis Date = 05/14/14 Pct Recovery = 83% Analysis Date = 05/03/14 Pct Recovery = 84% Analysis Date = 05/03/14 Pct Recovery = 84% Analysis Date = 04/23/14 Pct Recovery = 84% Analysis Date = 04/23/14 Pct Recovery = 84% Analysis Date = 04/12/14 Pct Recovery = 85% Analysis Date = 04/12/14 Pct Recovery = 85% Analysis Date = 04/01/14 Pct Recovery = 85% Analysis Date = 04/01/14 Pct Recovery = 85% Analysis Date = 03/22/14 Pct Recovery = 86% Analysis Date = 03/22/14 Pct Recovery = 86% Analysis Date = 03/11/14 Pct Recovery = 86% Analysis Date = 03/11/14 Pct Recovery = 86% Analysis Date = 02/28/14 Pct Recovery = 87% Analysis Date = 02/28/14 Pct Recovery = 87% Analysis Date = 02/18/14 Pct Recovery = 87% Analysis Date = 02/18/14 Pct Recovery = 87% Analysis Date = 02/07/14 Pct Recovery = 87% Analysis Date = 02/07/14 Pct Recovery = 87% Analysis Date = 01/27/14 Pct Recovery = 88% Analysis Date = 01/27/14 Pct Recovery = 88% Analysis Date = 01/17/14 Pct Recovery = 88% Analysis Date = 01/17/14 Pct Recovery = 88% Analysis Date = 01/06/14 Pct Recovery = 89% Analysis Date = 01/06/14 Pct Recovery = 89% Analysis Date = 12/26/13 Pct Recovery = 89% Analysis Date = 12/26/13 Pct Recovery = 89% Analysis Date = 12/15/13 Pct Recovery = 90% Analysis Date = 12/15/13 Pct Recovery = 90% Analysis Date = 12/05/13 Pct Recovery = 90% Analysis Date = 12/05/13 Pct Recovery = 90% Analysis Date = 11/24/13 Pct Recovery = 91% Analysis Date = 11/24/13 Pct Recovery = 91% Analysis Date = 11/13/13 Pct Recovery = 91% Analysis Date = 11/13/13 Pct Recovery = 91% Analysis Date = 11/03/13 Pct Recovery = 92% Analysis Date = 11/03/13 Pct Recovery = 92% Analysis Date = 10/23/13 Pct Recovery = 92% Analysis Date = 10/23/13 Pct Recovery = 92% Analysis Date = 10/12/13 Pct Recovery = 92% Analysis Date = 10/12/13 Pct Recovery = 92% Analysis Date = 10/02/13 Pct Recovery = 92% Analysis Date = 10/02/13 Pct Recovery = 92% Analysis Date = 09/21/13 Pct Recovery = 93% Analysis Date = 09/21/13 Pct Recovery = 93% Analysis Date = 09/10/13 Pct Recovery = 93% Analysis Date = 09/10/13 Pct Recovery = 93% Analysis Date = 08/31/13 Pct Recovery = 93% Analysis Date = 08/31/13 Pct Recovery = 93% Analysis Date = 08/20/13 Pct Recovery = 93% Analysis Date = 08/20/13 Pct Recovery = 93% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 08/09/13 Pct Recovery = 94% Analysis Date = 07/30/13 Pct Recovery = 94% Analysis Date = 07/30/13 Pct Recovery = 94% Analysis Date = 07/19/13 Pct Recovery = 94% Analysis Date = 07/19/13 Pct Recovery = 94% Analysis Date = 07/08/13 Pct Recovery = 94% Analysis Date = 07/08/13 Pct Recovery = 94% Analysis Date = 06/28/13 Pct Recovery = 95% Analysis Date = 06/28/13 Pct Recovery = 95% Analysis Date = 06/17/13 Pct Recovery = 95% Analysis Date = 06/17/13 Pct Recovery = 95% Analysis Date = 06/06/13 Pct Recovery = 95% Analysis Date = 06/06/13 Pct Recovery = 95% Analysis Date = 05/27/13 Pct Recovery = 95% Analysis Date = 05/27/13 Pct Recovery = 95% Analysis Date = 05/16/13 Pct Recovery = 95% Analysis Date = 05/16/13 Pct Recovery = 95% Analysis Date = 05/05/13 Pct Recovery = 95% Analysis Date = 05/05/13 Pct Recovery = 95% Analysis Date = 04/25/13 Pct Recovery = 95% Analysis Date = 04/25/13 Pct Recovery = 95% Analysis Date = 04/14/13 Pct Recovery = 96% Analysis Date = 04/14/13 Pct Recovery = 96% Analysis Date = 04/03/13 Pct Recovery = 96% Analysis Date = 04/03/13 Pct Recovery = 96% Analysis Date = 03/23/13 Pct Recovery = 96% Analysis Date = 03/23/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/13/13 Pct Recovery = 96% Analysis Date = 03/02/13 Pct Recovery = 96% Analysis Date = 03/02/13 Pct Recovery = 96% Analysis Date = 02/19/13 Pct Recovery = 96% Analysis Date = 02/19/13 Pct Recovery = 96% Analysis Date = 02/09/13 Pct Recovery = 96% Analysis Date = 02/09/13 Pct Recovery = 96% Analysis Date = 01/29/13 Pct Recovery = 96% Analysis Date = 01/29/13 Pct Recovery = 96% Analysis Date = 01/18/13 Pct Recovery = 96% Analysis Date = 01/18/13 Pct Recovery = 96% Analysis Date = 01/08/13 Pct Recovery = 96% Analysis Date = 01/08/13 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/28/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/17/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 12/07/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 96% Analysis Date = 11/26/12 Pct Recovery = 96% Analysis Date = 11/15/12 Pct Recovery = 96% Analysis Date = 11/15/12 Pct Recovery = 96% Analysis Date = 11/05/12 Pct Recovery = 95% Analysis Date = 11/05/12 Pct Recovery = 95% Analysis Date = 10/25/12 Pct Recovery = 95% Analysis Date = 10/25/12 Pct Recovery = 95% Analysis Date = 10/14/12 Pct Recovery = 95% Analysis Date = 10/14/12 Pct Recovery = 95% Analysis Date = 10/04/12 Pct Recovery = 95% Analysis Date = 10/04/12 Pct Recovery = 95% Analysis Date = 09/23/12 Pct Recovery = 95% Analysis Date = 09/23/12 Pct Recovery = 95% Analysis Date = 09/12/12 Pct Recovery = 95% Analysis Date = 09/12/12 Pct Recovery = 95% Analysis Date = 09/02/12 Pct Recovery = 95% Analysis Date = 09/02/12 Pct Recovery = 95% Analysis Date = 08/22/12 Pct Recovery = 94% Analysis Date = 08/22/12 Pct Recovery = 94% Analysis Date = 08/11/12 Pct Recovery = 94% Analysis Date = 08/11/12 Pct Recovery = 94% Analysis Date = 08/01/12 Pct Recovery = 94% Analysis Date = 08/01/12 Pct Recovery = 94% Analysis Date = 07/21/12 Pct Recovery = 94% Analysis Date = 07/21/12 Pct Recovery = 94% Analysis Date = 07/10/12 Pct Recovery = 94% Analysis Date = 07/10/12 Pct Recovery = 94% Analysis Date = 06/29/12 Pct Recovery = 93% Analysis Date = 06/29/12 Pct Recovery = 93% Analysis Date = 06/19/12 Pct Recovery = 93% Analysis Date = 06/19/12 Pct Recovery = 93% Analysis Date = 06/08/12 Pct Recovery = 93% Analysis Date = 06/08/12 Pct Recovery = 93% Analysis Date = 05/28/12 Pct Recovery = 93% Analysis Date = 05/28/12 Pct Recovery = 93% Analysis Date = 05/18/12 Pct Recovery = 93% Analysis Date = 05/18/12 Pct Recovery = 93% Analysis Date = 05/07/12 Pct Recovery = 92% Analysis Date = 05/07/12 Pct Recovery = 92% Analysis Date = 04/26/12 Pct Recovery = 92% Analysis Date = 04/26/12 Pct Recovery = 92% Analysis Date = 04/16/12 Pct Recovery = 92% Analysis Date = 04/16/12 Pct Recovery = 92% Analysis Date = 04/05/12 Pct Recovery = 92% Analysis Date = 04/05/12 Pct Recovery = 92% Analysis Date = 03/25/12 Pct Recovery = 92% Analysis Date = 03/25/12 Pct Recovery = 92% Analysis Date = 03/15/12 Pct Recovery = 91% Analysis Date = 03/15/12 Pct Recovery = 91% Analysis Date = 03/04/12 Pct Recovery = 91% Analysis Date = 03/04/12 Pct Recovery = 91% Analysis Date = 02/22/12 Pct Recovery = 91% Analysis Date = 02/22/12 Pct Recovery = 91% Analysis Date = 02/12/12 Pct Recovery = 91% Analysis Date = 02/12/12 Pct Recovery = 91% Analysis Date = 02/01/12 Pct Recovery = 90% Analysis Date = 02/01/12 Pct Recovery = 90% Analysis Date = 01/21/12 Pct Recovery = 90% Analysis Date = 01/21/12 Pct Recovery = 90% Analysis Date = 01/11/12 Pct Recovery = 90% Analysis Date = 01/11/12 Pct Recovery = 90% Analysis Date = 12/31/11 Pct Recovery = 90% Analysis Date = 12/31/11 Pct Recovery = 90% Analysis Date = 12/20/11 Pct Recovery = 90% Analysis Date = 12/20/11 Pct Recovery = 90% Analysis Date = 12/10/11 Pct Recovery = 89% Analysis Date = 12/10/11 Pct Recovery = 89% Analysis Date = 11/29/11 Pct Recovery = 89% Analysis Date = 11/29/11 Pct Recovery = 89% Analysis Date = 11/18/11 Pct Recovery = 89% Analysis Date = 11/18/11 Pct Recovery = 89% Analysis Date = 11/08/11 Pct Recovery = 89% Analysis Date = 11/08/11 Pct Recovery = 89% Analysis Date = 10/28/11 Pct Recovery = 88% Analysis Date = 10/28/11 Pct Recovery = 88% Analysis Date = 10/17/11 Pct Recovery = 88% Analysis Date = 10/17/11 Pct Recovery = 88% Analysis Date = 10/06/11 Pct Recovery = 88% Analysis Date = 10/06/11 Pct Recovery = 88% Analysis Date = 09/26/11 Pct Recovery = 88% Analysis Date = 09/26/11 Pct Recovery = 88% Analysis Date = 09/15/11 Pct Recovery = 87% Analysis Date = 09/15/11 Pct Recovery = 87% Analysis Date = 09/04/11 Pct Recovery = 87% Analysis Date = 09/04/11 Pct Recovery = 87% Analysis Date = 08/25/11 Pct Recovery = 87% Analysis Date = 08/25/11 Pct Recovery = 87% Analysis Date = 08/14/11 Pct Recovery = 87% Analysis Date = 08/14/11 Pct Recovery = 87% Analysis Date = 08/03/11 Pct Recovery = 86% Analysis Date = 08/03/11 Pct Recovery = 86% Analysis Date = 07/24/11 Pct Recovery = 86% Analysis Date = 07/24/11 Pct Recovery = 86% Analysis Date = 07/13/11 Pct Recovery = 86% Analysis Date = 07/13/11 Pct Recovery = 86% Analysis Date = 07/02/11 Pct Recovery = 86% Analysis Date = 07/02/11 Pct Recovery = 86% Analysis Date = 06/22/11 Pct Recovery = 86% Analysis Date = 06/22/11 Pct Recovery = 86% Analysis Date = 06/11/11 Pct Recovery = 85% Analysis Date = 06/11/11 Pct Recovery = 85% Analysis Date = 05/31/11 Pct Recovery = 85% Analysis Date = 05/31/11 Pct Recovery = 85% Analysis Date = 05/21/11 Pct Recovery = 85% Analysis Date = 05/21/11 Pct Recovery = 85% Analysis Date = 05/10/11 Pct Recovery = 85% Analysis Date = 05/10/11 Pct Recovery = 85% Analysis Date = 04/29/11 Pct Recovery = 84% Analysis Date = 04/29/11 Pct Recovery = 84% Analysis Date = 04/19/11 Pct Recovery = 84% Analysis Date = 04/19/11 Pct Recovery = 84% Analysis Date = 04/08/11 Pct Recovery = 84% Analysis Date = 04/08/11 Pct Recovery = 84% Analysis Date = 03/28/11 Pct Recovery = 84% Analysis Date = 03/28/11 Pct Recovery = 84% Analysis Date = 03/18/11 Pct Recovery = 83% Analysis Date = 03/18/11 Pct Recovery = 83% Analysis Date = 03/07/11 Pct Recovery = 83% Analysis Date = 03/07/11 Pct Recovery = 83% Analysis Date = 02/24/11 Pct Recovery = 83% Analysis Date = 02/24/11 Pct Recovery = 83% Analysis Date = 02/14/11 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FONOFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 85% 18% 84% 12%
Total 87 85% 18% 84% 12%

Sample Statistics
FONOFOS

Characteristic N % % Basis
Plotted 87 99% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 88 .  
False Negatives 1 1% 1 out of 88
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
HEXAZINONE
METHOD: 2033 , TESTIDCODE: 04025GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 51% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 59% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 36% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 45% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 47% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 39% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 42% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 47% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 42% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 51% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 41% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 51% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 50% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 57% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 56% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 46% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 78% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 35% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 51% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 63% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 77% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 60% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 29% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 64% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 19% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 56% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 34% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 57% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 46% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 56% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 45% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 75% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 58% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 87% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 43% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 77% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 31% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 32% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 76% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 67% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 43% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 58% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 78% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 56% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 48% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 60% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 89% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 68% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 61% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 63% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 90% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 70% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 50% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 45% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 40% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 57% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 47% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 54% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 75% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 115% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 84% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 105% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 68% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 87% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 78% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 79% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 82% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 99% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 69% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 63% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 147% Analysis Date = 01/18/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 12/27/16 Pct Recovery = 71% Analysis Date = 12/27/16 Pct Recovery = 71% Analysis Date = 12/16/16 Pct Recovery = 71% Analysis Date = 12/16/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 11/24/16 Pct Recovery = 71% Analysis Date = 11/24/16 Pct Recovery = 71% Analysis Date = 11/14/16 Pct Recovery = 71% Analysis Date = 11/14/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 71% Analysis Date = 11/03/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/12/16 Pct Recovery = 70% Analysis Date = 10/12/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/10/16 Pct Recovery = 70% Analysis Date = 09/10/16 Pct Recovery = 70% Analysis Date = 08/30/16 Pct Recovery = 70% Analysis Date = 08/30/16 Pct Recovery = 70% Analysis Date = 08/19/16 Pct Recovery = 70% Analysis Date = 08/19/16 Pct Recovery = 70% Analysis Date = 08/08/16 Pct Recovery = 70% Analysis Date = 08/08/16 Pct Recovery = 70% Analysis Date = 07/28/16 Pct Recovery = 69% Analysis Date = 07/28/16 Pct Recovery = 69% Analysis Date = 07/17/16 Pct Recovery = 69% Analysis Date = 07/17/16 Pct Recovery = 69% Analysis Date = 07/07/16 Pct Recovery = 69% Analysis Date = 07/07/16 Pct Recovery = 69% Analysis Date = 06/26/16 Pct Recovery = 69% Analysis Date = 06/26/16 Pct Recovery = 69% Analysis Date = 06/15/16 Pct Recovery = 69% Analysis Date = 06/15/16 Pct Recovery = 69% Analysis Date = 06/04/16 Pct Recovery = 69% Analysis Date = 06/04/16 Pct Recovery = 69% Analysis Date = 05/24/16 Pct Recovery = 68% Analysis Date = 05/24/16 Pct Recovery = 68% Analysis Date = 05/14/16 Pct Recovery = 68% Analysis Date = 05/14/16 Pct Recovery = 68% Analysis Date = 05/03/16 Pct Recovery = 68% Analysis Date = 05/03/16 Pct Recovery = 68% Analysis Date = 04/22/16 Pct Recovery = 68% Analysis Date = 04/22/16 Pct Recovery = 68% Analysis Date = 04/11/16 Pct Recovery = 68% Analysis Date = 04/11/16 Pct Recovery = 68% Analysis Date = 03/31/16 Pct Recovery = 68% Analysis Date = 03/31/16 Pct Recovery = 68% Analysis Date = 03/20/16 Pct Recovery = 67% Analysis Date = 03/20/16 Pct Recovery = 67% Analysis Date = 03/10/16 Pct Recovery = 67% Analysis Date = 03/10/16 Pct Recovery = 67% Analysis Date = 02/28/16 Pct Recovery = 67% Analysis Date = 02/28/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/06/16 Pct Recovery = 67% Analysis Date = 02/06/16 Pct Recovery = 67% Analysis Date = 01/26/16 Pct Recovery = 66% Analysis Date = 01/26/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/05/16 Pct Recovery = 66% Analysis Date = 01/05/16 Pct Recovery = 66% Analysis Date = 12/25/15 Pct Recovery = 66% Analysis Date = 12/25/15 Pct Recovery = 66% Analysis Date = 12/14/15 Pct Recovery = 66% Analysis Date = 12/14/15 Pct Recovery = 66% Analysis Date = 12/03/15 Pct Recovery = 65% Analysis Date = 12/03/15 Pct Recovery = 65% Analysis Date = 11/22/15 Pct Recovery = 65% Analysis Date = 11/22/15 Pct Recovery = 65% Analysis Date = 11/12/15 Pct Recovery = 65% Analysis Date = 11/12/15 Pct Recovery = 65% Analysis Date = 11/01/15 Pct Recovery = 65% Analysis Date = 11/01/15 Pct Recovery = 65% Analysis Date = 10/21/15 Pct Recovery = 65% Analysis Date = 10/21/15 Pct Recovery = 65% Analysis Date = 10/10/15 Pct Recovery = 64% Analysis Date = 10/10/15 Pct Recovery = 64% Analysis Date = 09/29/15 Pct Recovery = 64% Analysis Date = 09/29/15 Pct Recovery = 64% Analysis Date = 09/18/15 Pct Recovery = 64% Analysis Date = 09/18/15 Pct Recovery = 64% Analysis Date = 09/08/15 Pct Recovery = 64% Analysis Date = 09/08/15 Pct Recovery = 64% Analysis Date = 08/28/15 Pct Recovery = 64% Analysis Date = 08/28/15 Pct Recovery = 64% Analysis Date = 08/17/15 Pct Recovery = 64% Analysis Date = 08/17/15 Pct Recovery = 64% Analysis Date = 08/06/15 Pct Recovery = 63% Analysis Date = 08/06/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 63% Analysis Date = 07/26/15 Pct Recovery = 63% Analysis Date = 07/15/15 Pct Recovery = 63% Analysis Date = 07/15/15 Pct Recovery = 63% Analysis Date = 07/05/15 Pct Recovery = 63% Analysis Date = 07/05/15 Pct Recovery = 63% Analysis Date = 06/24/15 Pct Recovery = 63% Analysis Date = 06/24/15 Pct Recovery = 63% Analysis Date = 06/13/15 Pct Recovery = 62% Analysis Date = 06/13/15 Pct Recovery = 62% Analysis Date = 06/02/15 Pct Recovery = 62% Analysis Date = 06/02/15 Pct Recovery = 62% Analysis Date = 05/22/15 Pct Recovery = 62% Analysis Date = 05/22/15 Pct Recovery = 62% Analysis Date = 05/11/15 Pct Recovery = 62% Analysis Date = 05/11/15 Pct Recovery = 62% Analysis Date = 05/01/15 Pct Recovery = 62% Analysis Date = 05/01/15 Pct Recovery = 62% Analysis Date = 04/20/15 Pct Recovery = 62% Analysis Date = 04/20/15 Pct Recovery = 62% Analysis Date = 04/09/15 Pct Recovery = 62% Analysis Date = 04/09/15 Pct Recovery = 62% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/18/15 Pct Recovery = 61% Analysis Date = 03/18/15 Pct Recovery = 61% Analysis Date = 03/08/15 Pct Recovery = 61% Analysis Date = 03/08/15 Pct Recovery = 61% Analysis Date = 02/25/15 Pct Recovery = 61% Analysis Date = 02/25/15 Pct Recovery = 61% Analysis Date = 02/14/15 Pct Recovery = 61% Analysis Date = 02/14/15 Pct Recovery = 61% Analysis Date = 02/03/15 Pct Recovery = 61% Analysis Date = 02/03/15 Pct Recovery = 61% Analysis Date = 01/23/15 Pct Recovery = 61% Analysis Date = 01/23/15 Pct Recovery = 61% Analysis Date = 01/12/15 Pct Recovery = 60% Analysis Date = 01/12/15 Pct Recovery = 60% Analysis Date = 01/02/15 Pct Recovery = 60% Analysis Date = 01/02/15 Pct Recovery = 60% Analysis Date = 12/22/14 Pct Recovery = 60% Analysis Date = 12/22/14 Pct Recovery = 60% Analysis Date = 12/11/14 Pct Recovery = 60% Analysis Date = 12/11/14 Pct Recovery = 60% Analysis Date = 11/30/14 Pct Recovery = 60% Analysis Date = 11/30/14 Pct Recovery = 60% Analysis Date = 11/19/14 Pct Recovery = 60% Analysis Date = 11/19/14 Pct Recovery = 60% Analysis Date = 11/08/14 Pct Recovery = 60% Analysis Date = 11/08/14 Pct Recovery = 60% Analysis Date = 10/29/14 Pct Recovery = 59% Analysis Date = 10/29/14 Pct Recovery = 59% Analysis Date = 10/18/14 Pct Recovery = 59% Analysis Date = 10/18/14 Pct Recovery = 59% Analysis Date = 10/07/14 Pct Recovery = 59% Analysis Date = 10/07/14 Pct Recovery = 59% Analysis Date = 09/26/14 Pct Recovery = 59% Analysis Date = 09/26/14 Pct Recovery = 59% Analysis Date = 09/15/14 Pct Recovery = 58% Analysis Date = 09/15/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 09/05/14 Pct Recovery = 58% Analysis Date = 08/25/14 Pct Recovery = 58% Analysis Date = 08/25/14 Pct Recovery = 58% Analysis Date = 08/14/14 Pct Recovery = 58% Analysis Date = 08/14/14 Pct Recovery = 58% Analysis Date = 08/03/14 Pct Recovery = 57% Analysis Date = 08/03/14 Pct Recovery = 57% Analysis Date = 07/23/14 Pct Recovery = 57% Analysis Date = 07/23/14 Pct Recovery = 57% Analysis Date = 07/12/14 Pct Recovery = 57% Analysis Date = 07/12/14 Pct Recovery = 57% Analysis Date = 07/02/14 Pct Recovery = 57% Analysis Date = 07/02/14 Pct Recovery = 57% Analysis Date = 06/21/14 Pct Recovery = 56% Analysis Date = 06/21/14 Pct Recovery = 56% Analysis Date = 06/10/14 Pct Recovery = 56% Analysis Date = 06/10/14 Pct Recovery = 56% Analysis Date = 05/30/14 Pct Recovery = 56% Analysis Date = 05/30/14 Pct Recovery = 56% Analysis Date = 05/19/14 Pct Recovery = 55% Analysis Date = 05/19/14 Pct Recovery = 55% Analysis Date = 05/08/14 Pct Recovery = 55% Analysis Date = 05/08/14 Pct Recovery = 55% Analysis Date = 04/28/14 Pct Recovery = 55% Analysis Date = 04/28/14 Pct Recovery = 55% Analysis Date = 04/17/14 Pct Recovery = 55% Analysis Date = 04/17/14 Pct Recovery = 55% Analysis Date = 04/06/14 Pct Recovery = 54% Analysis Date = 04/06/14 Pct Recovery = 54% Analysis Date = 03/26/14 Pct Recovery = 54% Analysis Date = 03/26/14 Pct Recovery = 54% Analysis Date = 03/15/14 Pct Recovery = 54% Analysis Date = 03/15/14 Pct Recovery = 54% Analysis Date = 03/04/14 Pct Recovery = 54% Analysis Date = 03/04/14 Pct Recovery = 54% Analysis Date = 02/22/14 Pct Recovery = 54% Analysis Date = 02/22/14 Pct Recovery = 54% Analysis Date = 02/11/14 Pct Recovery = 53% Analysis Date = 02/11/14 Pct Recovery = 53% Analysis Date = 01/31/14 Pct Recovery = 53% Analysis Date = 01/31/14 Pct Recovery = 53% Analysis Date = 01/20/14 Pct Recovery = 53% Analysis Date = 01/20/14 Pct Recovery = 53% Analysis Date = 01/09/14 Pct Recovery = 53% Analysis Date = 01/09/14 Pct Recovery = 53% Analysis Date = 12/30/13 Pct Recovery = 52% Analysis Date = 12/30/13 Pct Recovery = 52% Analysis Date = 12/19/13 Pct Recovery = 52% Analysis Date = 12/19/13 Pct Recovery = 52% Analysis Date = 12/08/13 Pct Recovery = 52% Analysis Date = 12/08/13 Pct Recovery = 52% Analysis Date = 11/27/13 Pct Recovery = 52% Analysis Date = 11/27/13 Pct Recovery = 52% Analysis Date = 11/16/13 Pct Recovery = 52% Analysis Date = 11/16/13 Pct Recovery = 52% Analysis Date = 11/05/13 Pct Recovery = 51% Analysis Date = 11/05/13 Pct Recovery = 51% Analysis Date = 10/26/13 Pct Recovery = 51% Analysis Date = 10/26/13 Pct Recovery = 51% Analysis Date = 10/15/13 Pct Recovery = 52% Analysis Date = 10/15/13 Pct Recovery = 52% Analysis Date = 10/04/13 Pct Recovery = 52% Analysis Date = 10/04/13 Pct Recovery = 52% Analysis Date = 09/23/13 Pct Recovery = 52% Analysis Date = 09/23/13 Pct Recovery = 52% Analysis Date = 09/12/13 Pct Recovery = 52% Analysis Date = 09/12/13 Pct Recovery = 52% Analysis Date = 09/01/13 Pct Recovery = 52% Analysis Date = 09/01/13 Pct Recovery = 52% Analysis Date = 08/22/13 Pct Recovery = 52% Analysis Date = 08/22/13 Pct Recovery = 52% Analysis Date = 08/11/13 Pct Recovery = 52% Analysis Date = 08/11/13 Pct Recovery = 52% Analysis Date = 07/31/13 Pct Recovery = 52% Analysis Date = 07/31/13 Pct Recovery = 52% Analysis Date = 07/20/13 Pct Recovery = 52% Analysis Date = 07/20/13 Pct Recovery = 52% Analysis Date = 07/09/13 Pct Recovery = 52% Analysis Date = 07/09/13 Pct Recovery = 52% Analysis Date = 06/29/13 Pct Recovery = 52% Analysis Date = 06/29/13 Pct Recovery = 52% Analysis Date = 06/18/13 Pct Recovery = 53% Analysis Date = 06/18/13 Pct Recovery = 53% Analysis Date = 06/07/13 Pct Recovery = 53% Analysis Date = 06/07/13 Pct Recovery = 53% Analysis Date = 05/27/13 Pct Recovery = 53% Analysis Date = 05/27/13 Pct Recovery = 53% Analysis Date = 05/16/13 Pct Recovery = 53% Analysis Date = 05/16/13 Pct Recovery = 53% Analysis Date = 05/05/13 Pct Recovery = 53% Analysis Date = 05/05/13 Pct Recovery = 53% Analysis Date = 04/25/13 Pct Recovery = 54% Analysis Date = 04/25/13 Pct Recovery = 54% Analysis Date = 04/14/13 Pct Recovery = 54% Analysis Date = 04/14/13 Pct Recovery = 54% Analysis Date = 04/03/13 Pct Recovery = 54% Analysis Date = 04/03/13 Pct Recovery = 54% Analysis Date = 03/23/13 Pct Recovery = 54% Analysis Date = 03/23/13 Pct Recovery = 54% Analysis Date = 03/12/13 Pct Recovery = 54% Analysis Date = 03/12/13 Pct Recovery = 54% Analysis Date = 03/01/13 Pct Recovery = 55% Analysis Date = 03/01/13 Pct Recovery = 55% Analysis Date = 02/19/13 Pct Recovery = 55% Analysis Date = 02/19/13 Pct Recovery = 55% Analysis Date = 02/08/13 Pct Recovery = 55% Analysis Date = 02/08/13 Pct Recovery = 55% Analysis Date = 01/28/13 Pct Recovery = 55% Analysis Date = 01/28/13 Pct Recovery = 55% Analysis Date = 01/17/13 Pct Recovery = 56% Analysis Date = 01/17/13 Pct Recovery = 56% Analysis Date = 01/06/13 Pct Recovery = 56% Analysis Date = 01/06/13 Pct Recovery = 56% Analysis Date = 12/26/12 Pct Recovery = 56% Analysis Date = 12/26/12 Pct Recovery = 56% Analysis Date = 12/16/12 Pct Recovery = 56% Analysis Date = 12/16/12 Pct Recovery = 56% Analysis Date = 12/05/12 Pct Recovery = 57% Analysis Date = 12/05/12 Pct Recovery = 57% Analysis Date = 11/24/12 Pct Recovery = 57% Analysis Date = 11/24/12 Pct Recovery = 57% Analysis Date = 11/13/12 Pct Recovery = 57% Analysis Date = 11/13/12 Pct Recovery = 57% Analysis Date = 11/02/12 Pct Recovery = 58% Analysis Date = 11/02/12 Pct Recovery = 58% Analysis Date = 10/23/12 Pct Recovery = 58% Analysis Date = 10/23/12 Pct Recovery = 58% Analysis Date = 10/12/12 Pct Recovery = 58% Analysis Date = 10/12/12 Pct Recovery = 58% Analysis Date = 10/01/12 Pct Recovery = 59% Analysis Date = 10/01/12 Pct Recovery = 59% Analysis Date = 09/20/12 Pct Recovery = 59% Analysis Date = 09/20/12 Pct Recovery = 59% Analysis Date = 09/09/12 Pct Recovery = 60% Analysis Date = 09/09/12 Pct Recovery = 60% Analysis Date = 08/29/12 Pct Recovery = 60% Analysis Date = 08/29/12 Pct Recovery = 60% Analysis Date = 08/19/12 Pct Recovery = 61% Analysis Date = 08/19/12 Pct Recovery = 61% Analysis Date = 08/08/12 Pct Recovery = 61% Analysis Date = 08/08/12 Pct Recovery = 61% Analysis Date = 07/28/12 Pct Recovery = 61% Analysis Date = 07/28/12 Pct Recovery = 61% Analysis Date = 07/17/12 Pct Recovery = 62% Analysis Date = 07/17/12 Pct Recovery = 62% Analysis Date = 07/06/12 Pct Recovery = 62% Analysis Date = 07/06/12 Pct Recovery = 62% Analysis Date = 06/25/12 Pct Recovery = 63% Analysis Date = 06/25/12 Pct Recovery = 63% Analysis Date = 06/15/12 Pct Recovery = 63% Analysis Date = 06/15/12 Pct Recovery = 63% Analysis Date = 06/04/12 Pct Recovery = 64% Analysis Date = 06/04/12 Pct Recovery = 64% Analysis Date = 05/24/12 Pct Recovery = 64% Analysis Date = 05/24/12 Pct Recovery = 64% Analysis Date = 05/13/12 Pct Recovery = 64% Analysis Date = 05/13/12 Pct Recovery = 64% Analysis Date = 05/02/12 Pct Recovery = 65% Analysis Date = 05/02/12 Pct Recovery = 65% Analysis Date = 04/22/12 Pct Recovery = 65% Analysis Date = 04/22/12 Pct Recovery = 65% Analysis Date = 04/11/12 Pct Recovery = 66% Analysis Date = 04/11/12 Pct Recovery = 66% Analysis Date = 03/31/12 Pct Recovery = 66% Analysis Date = 03/31/12 Pct Recovery = 66% Analysis Date = 03/20/12 Pct Recovery = 67% Analysis Date = 03/20/12 Pct Recovery = 67% Analysis Date = 03/09/12 Pct Recovery = 67% Analysis Date = 03/09/12 Pct Recovery = 67% Analysis Date = 02/27/12 Pct Recovery = 67% Analysis Date = 02/27/12 Pct Recovery = 67% Analysis Date = 02/17/12 Pct Recovery = 68% Analysis Date = 02/17/12 Pct Recovery = 68% Analysis Date = 02/06/12 Pct Recovery = 68% Analysis Date = 02/06/12 Pct Recovery = 68% Analysis Date = 01/26/12 Pct Recovery = 69% Analysis Date = 01/26/12 Pct Recovery = 69% Analysis Date = 01/15/12 Pct Recovery = 69% Analysis Date = 01/15/12 Pct Recovery = 69% Analysis Date = 01/04/12 Pct Recovery = 70% Analysis Date = 01/04/12 Pct Recovery = 70% Analysis Date = 12/24/11 Pct Recovery = 70% Analysis Date = 12/24/11 Pct Recovery = 70% Analysis Date = 12/14/11 Pct Recovery = 70% Analysis Date = 12/14/11 Pct Recovery = 70% Analysis Date = 12/03/11 Pct Recovery = 71% Analysis Date = 12/03/11 Pct Recovery = 71% Analysis Date = 11/22/11 Pct Recovery = 71% Analysis Date = 11/22/11 Pct Recovery = 71% Analysis Date = 11/11/11 Pct Recovery = 72% Analysis Date = 11/11/11 Pct Recovery = 72% Analysis Date = 10/31/11 Pct Recovery = 72% Analysis Date = 10/31/11 Pct Recovery = 72% Analysis Date = 10/20/11 Pct Recovery = 73% Analysis Date = 10/20/11 Pct Recovery = 73% Analysis Date = 10/10/11 Pct Recovery = 73% Analysis Date = 10/10/11 Pct Recovery = 73% Analysis Date = 09/29/11 Pct Recovery = 73% Analysis Date = 09/29/11 Pct Recovery = 73% Analysis Date = 09/18/11 Pct Recovery = 74% Analysis Date = 09/18/11 Pct Recovery = 74% Analysis Date = 09/07/11 Pct Recovery = 74% Analysis Date = 09/07/11 Pct Recovery = 74% Analysis Date = 08/27/11 Pct Recovery = 75% Analysis Date = 08/27/11 Pct Recovery = 75% Analysis Date = 08/17/11 Pct Recovery = 75% Analysis Date = 08/17/11 Pct Recovery = 75% Analysis Date = 08/06/11 Pct Recovery = 76% Analysis Date = 08/06/11 Pct Recovery = 76% Analysis Date = 07/26/11 Pct Recovery = 76% Analysis Date = 07/26/11 Pct Recovery = 76% Analysis Date = 07/15/11 Pct Recovery = 77% Analysis Date = 07/15/11 Pct Recovery = 77% Analysis Date = 07/04/11 Pct Recovery = 77% Analysis Date = 07/04/11 Pct Recovery = 77% Analysis Date = 06/23/11 Pct Recovery = 77% Analysis Date = 06/23/11 Pct Recovery = 77% Analysis Date = 06/13/11 Pct Recovery = 78% Analysis Date = 06/13/11 Pct Recovery = 78% Analysis Date = 06/02/11 Pct Recovery = 78% Analysis Date = 06/02/11 Pct Recovery = 78% Analysis Date = 05/22/11 Pct Recovery = 79% Analysis Date = 05/22/11 Pct Recovery = 79% Analysis Date = 05/11/11 Pct Recovery = 79% Analysis Date = 05/11/11 Pct Recovery = 79% Analysis Date = 04/30/11 Pct Recovery = 80% Analysis Date = 04/30/11 Pct Recovery = 80% Analysis Date = 04/19/11 Pct Recovery = 80% Analysis Date = 04/19/11 Pct Recovery = 80% Analysis Date = 04/09/11 Pct Recovery = 81% Analysis Date = 04/09/11 Pct Recovery = 81% Analysis Date = 03/29/11 Pct Recovery = 81% Analysis Date = 03/29/11 Pct Recovery = 81% Analysis Date = 03/18/11 Pct Recovery = 81% Analysis Date = 03/18/11 Pct Recovery = 81% Analysis Date = 03/07/11 Pct Recovery = 82% Analysis Date = 03/07/11 Pct Recovery = 82% Analysis Date = 02/24/11 Pct Recovery = 82% Analysis Date = 02/24/11 Pct Recovery = 82% Analysis Date = 02/14/11 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXAZINONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 63% 20% 61% 21%
Total 89 63% 20% 61% 21%

Sample Statistics
HEXAZINONE

Characteristic N % % Basis
Plotted 89 99% Spiked
Estimated Values 8 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 90 .  
False Negatives 1 1% 1 out of 90
Not Spiked 79 .  
False Positives 0 0% 0 out of 79

BQS OBSP Determination:
IPRODIONE
METHOD: 2033 , TESTIDCODE: 61593GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 93% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 71% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 60% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 67% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 84% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 65% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 98% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 85% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 83% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 91% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 49% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 9% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 37% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 112% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 97% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 86% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 100% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 56% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 63% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 64% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 74% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 65% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 85% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 117% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 61% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 81% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 94% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 95% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 86% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 56% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 121% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 96% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 84% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 122% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 111% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 82% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 68% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 97% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 76% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 94% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 114% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 92% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 86% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 105% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 93% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 74% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 76% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 113% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 73% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 73% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 93% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 79% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 81% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 76% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 85% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 71% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 88% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 113% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 96% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 68% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 88% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 40% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 71% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 59% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 126% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 123% Analysis Date = 01/17/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/16/16 Pct Recovery = 93% Analysis Date = 12/16/16 Pct Recovery = 93% Analysis Date = 12/05/16 Pct Recovery = 93% Analysis Date = 12/05/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 11/03/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/09/16 Pct Recovery = 93% Analysis Date = 09/09/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/29/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/19/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 08/08/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 06/04/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/13/16 Pct Recovery = 93% Analysis Date = 05/13/16 Pct Recovery = 93% Analysis Date = 05/02/16 Pct Recovery = 93% Analysis Date = 05/02/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/21/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 93% Analysis Date = 03/30/16 Pct Recovery = 93% Analysis Date = 03/30/16 Pct Recovery = 93% Analysis Date = 03/20/16 Pct Recovery = 93% Analysis Date = 03/20/16 Pct Recovery = 93% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/16/16 Pct Recovery = 92% Analysis Date = 02/16/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/04/16 Pct Recovery = 92% Analysis Date = 01/04/16 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 92% Analysis Date = 11/10/15 Pct Recovery = 92% Analysis Date = 11/10/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/30/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/20/15 Pct Recovery = 92% Analysis Date = 10/09/15 Pct Recovery = 92% Analysis Date = 10/09/15 Pct Recovery = 92% Analysis Date = 09/28/15 Pct Recovery = 92% Analysis Date = 09/28/15 Pct Recovery = 92% Analysis Date = 09/17/15 Pct Recovery = 92% Analysis Date = 09/17/15 Pct Recovery = 92% Analysis Date = 09/06/15 Pct Recovery = 92% Analysis Date = 09/06/15 Pct Recovery = 92% Analysis Date = 08/26/15 Pct Recovery = 92% Analysis Date = 08/26/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 05/31/15 Pct Recovery = 91% Analysis Date = 05/31/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/16/15 Pct Recovery = 91% Analysis Date = 03/16/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/01/15 Pct Recovery = 91% Analysis Date = 02/01/15 Pct Recovery = 91% Analysis Date = 01/21/15 Pct Recovery = 91% Analysis Date = 01/21/15 Pct Recovery = 91% Analysis Date = 01/10/15 Pct Recovery = 91% Analysis Date = 01/10/15 Pct Recovery = 91% Analysis Date = 12/31/14 Pct Recovery = 91% Analysis Date = 12/31/14 Pct Recovery = 91% Analysis Date = 12/20/14 Pct Recovery = 91% Analysis Date = 12/20/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 11/28/14 Pct Recovery = 90% Analysis Date = 11/28/14 Pct Recovery = 90% Analysis Date = 11/17/14 Pct Recovery = 90% Analysis Date = 11/17/14 Pct Recovery = 90% Analysis Date = 11/06/14 Pct Recovery = 90% Analysis Date = 11/06/14 Pct Recovery = 90% Analysis Date = 10/26/14 Pct Recovery = 90% Analysis Date = 10/26/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/16/14 Pct Recovery = 90% Analysis Date = 10/05/14 Pct Recovery = 90% Analysis Date = 10/05/14 Pct Recovery = 90% Analysis Date = 09/24/14 Pct Recovery = 90% Analysis Date = 09/24/14 Pct Recovery = 90% Analysis Date = 09/13/14 Pct Recovery = 90% Analysis Date = 09/13/14 Pct Recovery = 90% Analysis Date = 09/02/14 Pct Recovery = 90% Analysis Date = 09/02/14 Pct Recovery = 90% Analysis Date = 08/22/14 Pct Recovery = 90% Analysis Date = 08/22/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/11/14 Pct Recovery = 90% Analysis Date = 08/01/14 Pct Recovery = 90% Analysis Date = 08/01/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/21/14 Pct Recovery = 90% Analysis Date = 07/10/14 Pct Recovery = 90% Analysis Date = 07/10/14 Pct Recovery = 90% Analysis Date = 06/29/14 Pct Recovery = 89% Analysis Date = 06/29/14 Pct Recovery = 89% Analysis Date = 06/18/14 Pct Recovery = 89% Analysis Date = 06/18/14 Pct Recovery = 89% Analysis Date = 06/07/14 Pct Recovery = 89% Analysis Date = 06/07/14 Pct Recovery = 89% Analysis Date = 05/27/14 Pct Recovery = 89% Analysis Date = 05/27/14 Pct Recovery = 89% Analysis Date = 05/17/14 Pct Recovery = 89% Analysis Date = 05/17/14 Pct Recovery = 89% Analysis Date = 05/06/14 Pct Recovery = 89% Analysis Date = 05/06/14 Pct Recovery = 89% Analysis Date = 04/25/14 Pct Recovery = 89% Analysis Date = 04/25/14 Pct Recovery = 89% Analysis Date = 04/14/14 Pct Recovery = 89% Analysis Date = 04/14/14 Pct Recovery = 89% Analysis Date = 04/03/14 Pct Recovery = 88% Analysis Date = 04/03/14 Pct Recovery = 88% Analysis Date = 03/23/14 Pct Recovery = 88% Analysis Date = 03/23/14 Pct Recovery = 88% Analysis Date = 03/12/14 Pct Recovery = 88% Analysis Date = 03/12/14 Pct Recovery = 88% Analysis Date = 03/02/14 Pct Recovery = 88% Analysis Date = 03/02/14 Pct Recovery = 88% Analysis Date = 02/19/14 Pct Recovery = 88% Analysis Date = 02/19/14 Pct Recovery = 88% Analysis Date = 02/08/14 Pct Recovery = 87% Analysis Date = 02/08/14 Pct Recovery = 87% Analysis Date = 01/28/14 Pct Recovery = 87% Analysis Date = 01/28/14 Pct Recovery = 87% Analysis Date = 01/17/14 Pct Recovery = 87% Analysis Date = 01/17/14 Pct Recovery = 87% Analysis Date = 01/06/14 Pct Recovery = 87% Analysis Date = 01/06/14 Pct Recovery = 87% Analysis Date = 12/26/13 Pct Recovery = 86% Analysis Date = 12/26/13 Pct Recovery = 86% Analysis Date = 12/16/13 Pct Recovery = 86% Analysis Date = 12/16/13 Pct Recovery = 86% Analysis Date = 12/05/13 Pct Recovery = 86% Analysis Date = 12/05/13 Pct Recovery = 86% Analysis Date = 11/24/13 Pct Recovery = 86% Analysis Date = 11/24/13 Pct Recovery = 86% Analysis Date = 11/13/13 Pct Recovery = 86% Analysis Date = 11/13/13 Pct Recovery = 86% Analysis Date = 11/02/13 Pct Recovery = 85% Analysis Date = 11/02/13 Pct Recovery = 85% Analysis Date = 10/22/13 Pct Recovery = 85% Analysis Date = 10/22/13 Pct Recovery = 85% Analysis Date = 10/11/13 Pct Recovery = 85% Analysis Date = 10/11/13 Pct Recovery = 85% Analysis Date = 10/01/13 Pct Recovery = 85% Analysis Date = 10/01/13 Pct Recovery = 85% Analysis Date = 09/20/13 Pct Recovery = 85% Analysis Date = 09/20/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 08/29/13 Pct Recovery = 85% Analysis Date = 08/29/13 Pct Recovery = 85% Analysis Date = 08/18/13 Pct Recovery = 85% Analysis Date = 08/18/13 Pct Recovery = 85% Analysis Date = 08/07/13 Pct Recovery = 84% Analysis Date = 08/07/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/17/13 Pct Recovery = 84% Analysis Date = 07/17/13 Pct Recovery = 84% Analysis Date = 07/06/13 Pct Recovery = 84% Analysis Date = 07/06/13 Pct Recovery = 84% Analysis Date = 06/25/13 Pct Recovery = 84% Analysis Date = 06/25/13 Pct Recovery = 84% Analysis Date = 06/14/13 Pct Recovery = 84% Analysis Date = 06/14/13 Pct Recovery = 84% Analysis Date = 06/03/13 Pct Recovery = 84% Analysis Date = 06/03/13 Pct Recovery = 84% Analysis Date = 05/23/13 Pct Recovery = 84% Analysis Date = 05/23/13 Pct Recovery = 84% Analysis Date = 05/12/13 Pct Recovery = 84% Analysis Date = 05/12/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 04/21/13 Pct Recovery = 84% Analysis Date = 04/21/13 Pct Recovery = 84% Analysis Date = 04/10/13 Pct Recovery = 84% Analysis Date = 04/10/13 Pct Recovery = 84% Analysis Date = 03/30/13 Pct Recovery = 84% Analysis Date = 03/30/13 Pct Recovery = 84% Analysis Date = 03/19/13 Pct Recovery = 84% Analysis Date = 03/19/13 Pct Recovery = 84% Analysis Date = 03/08/13 Pct Recovery = 84% Analysis Date = 03/08/13 Pct Recovery = 84% Analysis Date = 02/25/13 Pct Recovery = 84% Analysis Date = 02/25/13 Pct Recovery = 84% Analysis Date = 02/15/13 Pct Recovery = 84% Analysis Date = 02/15/13 Pct Recovery = 84% Analysis Date = 02/04/13 Pct Recovery = 84% Analysis Date = 02/04/13 Pct Recovery = 84% Analysis Date = 01/24/13 Pct Recovery = 84% Analysis Date = 01/24/13 Pct Recovery = 84% Analysis Date = 01/13/13 Pct Recovery = 84% Analysis Date = 01/13/13 Pct Recovery = 84% Analysis Date = 01/02/13 Pct Recovery = 84% Analysis Date = 01/02/13 Pct Recovery = 84% Analysis Date = 12/22/12 Pct Recovery = 84% Analysis Date = 12/22/12 Pct Recovery = 84% Analysis Date = 12/12/12 Pct Recovery = 83% Analysis Date = 12/12/12 Pct Recovery = 83% Analysis Date = 12/01/12 Pct Recovery = 83% Analysis Date = 12/01/12 Pct Recovery = 83% Analysis Date = 11/20/12 Pct Recovery = 83% Analysis Date = 11/20/12 Pct Recovery = 83% Analysis Date = 11/09/12 Pct Recovery = 83% Analysis Date = 11/09/12 Pct Recovery = 83% Analysis Date = 10/29/12 Pct Recovery = 83% Analysis Date = 10/29/12 Pct Recovery = 83% Analysis Date = 10/18/12 Pct Recovery = 83% Analysis Date = 10/18/12 Pct Recovery = 83% Analysis Date = 10/07/12 Pct Recovery = 83% Analysis Date = 10/07/12 Pct Recovery = 83% Analysis Date = 09/27/12 Pct Recovery = 83% Analysis Date = 09/27/12 Pct Recovery = 83% Analysis Date = 09/16/12 Pct Recovery = 82% Analysis Date = 09/16/12 Pct Recovery = 82% Analysis Date = 09/05/12 Pct Recovery = 82% Analysis Date = 09/05/12 Pct Recovery = 82% Analysis Date = 08/25/12 Pct Recovery = 82% Analysis Date = 08/25/12 Pct Recovery = 82% Analysis Date = 08/14/12 Pct Recovery = 82% Analysis Date = 08/14/12 Pct Recovery = 82% Analysis Date = 08/03/12 Pct Recovery = 82% Analysis Date = 08/03/12 Pct Recovery = 82% Analysis Date = 07/23/12 Pct Recovery = 81% Analysis Date = 07/23/12 Pct Recovery = 81% Analysis Date = 07/13/12 Pct Recovery = 81% Analysis Date = 07/13/12 Pct Recovery = 81% Analysis Date = 07/02/12 Pct Recovery = 81% Analysis Date = 07/02/12 Pct Recovery = 81% Analysis Date = 06/21/12 Pct Recovery = 80% Analysis Date = 06/21/12 Pct Recovery = 80% Analysis Date = 06/10/12 Pct Recovery = 80% Analysis Date = 06/10/12 Pct Recovery = 80% Analysis Date = 05/30/12 Pct Recovery = 80% Analysis Date = 05/30/12 Pct Recovery = 80% Analysis Date = 05/19/12 Pct Recovery = 79% Analysis Date = 05/19/12 Pct Recovery = 79% Analysis Date = 05/08/12 Pct Recovery = 79% Analysis Date = 05/08/12 Pct Recovery = 79% Analysis Date = 04/28/12 Pct Recovery = 79% Analysis Date = 04/28/12 Pct Recovery = 79% Analysis Date = 04/17/12 Pct Recovery = 78% Analysis Date = 04/17/12 Pct Recovery = 78% Analysis Date = 04/06/12 Pct Recovery = 78% Analysis Date = 04/06/12 Pct Recovery = 78% Analysis Date = 03/26/12 Pct Recovery = 78% Analysis Date = 03/26/12 Pct Recovery = 78% Analysis Date = 03/15/12 Pct Recovery = 78% Analysis Date = 03/15/12 Pct Recovery = 78% Analysis Date = 03/04/12 Pct Recovery = 77% Analysis Date = 03/04/12 Pct Recovery = 77% Analysis Date = 02/22/12 Pct Recovery = 77% Analysis Date = 02/22/12 Pct Recovery = 77% Analysis Date = 02/12/12 Pct Recovery = 77% Analysis Date = 02/12/12 Pct Recovery = 77% Analysis Date = 02/01/12 Pct Recovery = 76% Analysis Date = 02/01/12 Pct Recovery = 76% Analysis Date = 01/21/12 Pct Recovery = 76% Analysis Date = 01/21/12 Pct Recovery = 76% Analysis Date = 01/10/12 Pct Recovery = 76% Analysis Date = 01/10/12 Pct Recovery = 76% Analysis Date = 12/30/11 Pct Recovery = 75% Analysis Date = 12/30/11 Pct Recovery = 75% Analysis Date = 12/19/11 Pct Recovery = 75% Analysis Date = 12/19/11 Pct Recovery = 75% Analysis Date = 12/08/11 Pct Recovery = 75% Analysis Date = 12/08/11 Pct Recovery = 75% Analysis Date = 11/28/11 Pct Recovery = 74% Analysis Date = 11/28/11 Pct Recovery = 74% Analysis Date = 11/17/11 Pct Recovery = 74% Analysis Date = 11/17/11 Pct Recovery = 74% Analysis Date = 11/06/11 Pct Recovery = 74% Analysis Date = 11/06/11 Pct Recovery = 74% Analysis Date = 10/26/11 Pct Recovery = 73% Analysis Date = 10/26/11 Pct Recovery = 73% Analysis Date = 10/15/11 Pct Recovery = 73% Analysis Date = 10/15/11 Pct Recovery = 73% Analysis Date = 10/04/11 Pct Recovery = 73% Analysis Date = 10/04/11 Pct Recovery = 73% Analysis Date = 09/23/11 Pct Recovery = 72% Analysis Date = 09/23/11 Pct Recovery = 72% Analysis Date = 09/13/11 Pct Recovery = 72% Analysis Date = 09/13/11 Pct Recovery = 72% Analysis Date = 09/02/11 Pct Recovery = 72% Analysis Date = 09/02/11 Pct Recovery = 72% Analysis Date = 08/22/11 Pct Recovery = 71% Analysis Date = 08/22/11 Pct Recovery = 71% Analysis Date = 08/11/11 Pct Recovery = 71% Analysis Date = 08/11/11 Pct Recovery = 71% Analysis Date = 07/31/11 Pct Recovery = 70% Analysis Date = 07/31/11 Pct Recovery = 70% Analysis Date = 07/20/11 Pct Recovery = 70% Analysis Date = 07/20/11 Pct Recovery = 70% Analysis Date = 07/09/11 Pct Recovery = 70% Analysis Date = 07/09/11 Pct Recovery = 70% Analysis Date = 06/29/11 Pct Recovery = 69% Analysis Date = 06/29/11 Pct Recovery = 69% Analysis Date = 06/18/11 Pct Recovery = 69% Analysis Date = 06/18/11 Pct Recovery = 69% Analysis Date = 06/07/11 Pct Recovery = 69% Analysis Date = 06/07/11 Pct Recovery = 69% Analysis Date = 05/27/11 Pct Recovery = 68% Analysis Date = 05/27/11 Pct Recovery = 68% Analysis Date = 05/16/11 Pct Recovery = 68% Analysis Date = 05/16/11 Pct Recovery = 68% Analysis Date = 05/05/11 Pct Recovery = 67% Analysis Date = 05/05/11 Pct Recovery = 67% Analysis Date = 04/24/11 Pct Recovery = 67% Analysis Date = 04/24/11 Pct Recovery = 67% Analysis Date = 04/14/11 Pct Recovery = 67% Analysis Date = 04/14/11 Pct Recovery = 67% Analysis Date = 04/03/11 Pct Recovery = 66% Analysis Date = 04/03/11 Pct Recovery = 66% Analysis Date = 03/23/11 Pct Recovery = 66% Analysis Date = 03/23/11 Pct Recovery = 66% Analysis Date = 03/12/11 Pct Recovery = 66% Analysis Date = 03/12/11 Pct Recovery = 66% Analysis Date = 03/01/11 Pct Recovery = 65% Analysis Date = 03/01/11 Pct Recovery = 65% Analysis Date = 02/18/11 Pct Recovery = 65% Analysis Date = 02/18/11 Pct Recovery = 65% Analysis Date = 02/08/11 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
IPRODIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 80 84% 20% 85% 16%
Total 80 84% 20% 85% 16%

Sample Statistics
IPRODIONE

Characteristic N % % Basis
Plotted 80 99% Spiked
Estimated Values 80 99% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 1 1% 1 out of 81
Not Spiked 80 .  
False Positives 0 0% 0 out of 80

BQS OBSP Determination:
ISOFENPHOS
METHOD: 2033 , TESTIDCODE: 61594GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 78% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 109% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 100% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 77% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 80% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 82% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 101% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 93% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 90% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 100% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 87% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 81% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 86% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 88% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 63% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 70% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 93% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 69% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 112% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 96% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 95% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 35% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 82% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 74% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 107% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 85% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 80% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 80% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 103% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 77% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 113% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 9% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 100% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 90% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 100% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 119% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 100% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 103% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 94% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 101% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 75% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 119% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 71% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 106% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 105% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 125% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 93% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 104% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 97% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 74% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 98% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 121% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 104% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 83% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 102% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 100% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 93% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 87% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 53% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 18% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 127% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 133% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 129% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 138% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 178% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 116% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 113% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 123% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 119% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 121% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 135% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 145% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 107% Analysis Date = 01/18/17 Pct Recovery = 86% Analysis Date = 01/07/17 Pct Recovery = 86% Analysis Date = 01/07/17 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/05/16 Pct Recovery = 86% Analysis Date = 12/05/16 Pct Recovery = 86% Analysis Date = 11/24/16 Pct Recovery = 86% Analysis Date = 11/24/16 Pct Recovery = 86% Analysis Date = 11/14/16 Pct Recovery = 86% Analysis Date = 11/14/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 10/23/16 Pct Recovery = 85% Analysis Date = 10/23/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 08/30/16 Pct Recovery = 85% Analysis Date = 08/30/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 07/28/16 Pct Recovery = 85% Analysis Date = 07/28/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/26/16 Pct Recovery = 85% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 84% Analysis Date = 05/03/16 Pct Recovery = 84% Analysis Date = 05/03/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/22/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 03/10/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/28/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/17/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 02/06/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 84% Analysis Date = 01/26/16 Pct Recovery = 84% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/15/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 01/05/16 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/25/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/14/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 12/03/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/22/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/12/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 11/01/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/21/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 10/10/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/29/15 Pct Recovery = 83% Analysis Date = 09/18/15 Pct Recovery = 83% Analysis Date = 09/18/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 09/08/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/28/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/17/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 08/06/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/26/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/15/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 07/05/15 Pct Recovery = 83% Analysis Date = 06/24/15 Pct Recovery = 83% Analysis Date = 06/24/15 Pct Recovery = 83% Analysis Date = 06/13/15 Pct Recovery = 83% Analysis Date = 06/13/15 Pct Recovery = 83% Analysis Date = 06/02/15 Pct Recovery = 82% Analysis Date = 06/02/15 Pct Recovery = 82% Analysis Date = 05/22/15 Pct Recovery = 82% Analysis Date = 05/22/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 05/01/15 Pct Recovery = 82% Analysis Date = 04/20/15 Pct Recovery = 82% Analysis Date = 04/20/15 Pct Recovery = 82% Analysis Date = 04/09/15 Pct Recovery = 82% Analysis Date = 04/09/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/29/15 Pct Recovery = 82% Analysis Date = 03/18/15 Pct Recovery = 82% Analysis Date = 03/18/15 Pct Recovery = 82% Analysis Date = 03/08/15 Pct Recovery = 82% Analysis Date = 03/08/15 Pct Recovery = 82% Analysis Date = 02/25/15 Pct Recovery = 82% Analysis Date = 02/25/15 Pct Recovery = 82% Analysis Date = 02/14/15 Pct Recovery = 82% Analysis Date = 02/14/15 Pct Recovery = 82% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 01/23/15 Pct Recovery = 82% Analysis Date = 01/23/15 Pct Recovery = 82% Analysis Date = 01/12/15 Pct Recovery = 82% Analysis Date = 01/12/15 Pct Recovery = 82% Analysis Date = 01/02/15 Pct Recovery = 82% Analysis Date = 01/02/15 Pct Recovery = 82% Analysis Date = 12/22/14 Pct Recovery = 82% Analysis Date = 12/22/14 Pct Recovery = 82% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 83% Analysis Date = 11/30/14 Pct Recovery = 83% Analysis Date = 11/30/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/19/14 Pct Recovery = 83% Analysis Date = 11/08/14 Pct Recovery = 83% Analysis Date = 11/08/14 Pct Recovery = 83% Analysis Date = 10/29/14 Pct Recovery = 84% Analysis Date = 10/29/14 Pct Recovery = 84% Analysis Date = 10/18/14 Pct Recovery = 84% Analysis Date = 10/18/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 84% Analysis Date = 10/07/14 Pct Recovery = 84% Analysis Date = 09/26/14 Pct Recovery = 84% Analysis Date = 09/26/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 85% Analysis Date = 09/15/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 09/05/14 Pct Recovery = 85% Analysis Date = 08/25/14 Pct Recovery = 85% Analysis Date = 08/25/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/14/14 Pct Recovery = 85% Analysis Date = 08/03/14 Pct Recovery = 86% Analysis Date = 08/03/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/23/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/12/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 87% Analysis Date = 06/10/14 Pct Recovery = 87% Analysis Date = 05/30/14 Pct Recovery = 87% Analysis Date = 05/30/14 Pct Recovery = 87% Analysis Date = 05/19/14 Pct Recovery = 87% Analysis Date = 05/19/14 Pct Recovery = 87% Analysis Date = 05/08/14 Pct Recovery = 87% Analysis Date = 05/08/14 Pct Recovery = 87% Analysis Date = 04/28/14 Pct Recovery = 87% Analysis Date = 04/28/14 Pct Recovery = 87% Analysis Date = 04/17/14 Pct Recovery = 88% Analysis Date = 04/17/14 Pct Recovery = 88% Analysis Date = 04/06/14 Pct Recovery = 88% Analysis Date = 04/06/14 Pct Recovery = 88% Analysis Date = 03/26/14 Pct Recovery = 88% Analysis Date = 03/26/14 Pct Recovery = 88% Analysis Date = 03/15/14 Pct Recovery = 88% Analysis Date = 03/15/14 Pct Recovery = 88% Analysis Date = 03/04/14 Pct Recovery = 88% Analysis Date = 03/04/14 Pct Recovery = 88% Analysis Date = 02/22/14 Pct Recovery = 88% Analysis Date = 02/22/14 Pct Recovery = 88% Analysis Date = 02/11/14 Pct Recovery = 88% Analysis Date = 02/11/14 Pct Recovery = 88% Analysis Date = 01/31/14 Pct Recovery = 88% Analysis Date = 01/31/14 Pct Recovery = 88% Analysis Date = 01/20/14 Pct Recovery = 89% Analysis Date = 01/20/14 Pct Recovery = 89% Analysis Date = 01/09/14 Pct Recovery = 89% Analysis Date = 01/09/14 Pct Recovery = 89% Analysis Date = 12/30/13 Pct Recovery = 89% Analysis Date = 12/30/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/19/13 Pct Recovery = 89% Analysis Date = 12/08/13 Pct Recovery = 89% Analysis Date = 12/08/13 Pct Recovery = 89% Analysis Date = 11/27/13 Pct Recovery = 89% Analysis Date = 11/27/13 Pct Recovery = 89% Analysis Date = 11/16/13 Pct Recovery = 89% Analysis Date = 11/16/13 Pct Recovery = 89% Analysis Date = 11/05/13 Pct Recovery = 89% Analysis Date = 11/05/13 Pct Recovery = 89% Analysis Date = 10/26/13 Pct Recovery = 89% Analysis Date = 10/26/13 Pct Recovery = 89% Analysis Date = 10/15/13 Pct Recovery = 89% Analysis Date = 10/15/13 Pct Recovery = 89% Analysis Date = 10/04/13 Pct Recovery = 89% Analysis Date = 10/04/13 Pct Recovery = 89% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 08/22/13 Pct Recovery = 90% Analysis Date = 08/22/13 Pct Recovery = 90% Analysis Date = 08/11/13 Pct Recovery = 90% Analysis Date = 08/11/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 90% Analysis Date = 07/20/13 Pct Recovery = 90% Analysis Date = 07/20/13 Pct Recovery = 90% Analysis Date = 07/09/13 Pct Recovery = 90% Analysis Date = 07/09/13 Pct Recovery = 90% Analysis Date = 06/29/13 Pct Recovery = 91% Analysis Date = 06/29/13 Pct Recovery = 91% Analysis Date = 06/18/13 Pct Recovery = 91% Analysis Date = 06/18/13 Pct Recovery = 91% Analysis Date = 06/07/13 Pct Recovery = 91% Analysis Date = 06/07/13 Pct Recovery = 91% Analysis Date = 05/27/13 Pct Recovery = 91% Analysis Date = 05/27/13 Pct Recovery = 91% Analysis Date = 05/16/13 Pct Recovery = 91% Analysis Date = 05/16/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 04/25/13 Pct Recovery = 91% Analysis Date = 04/25/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/03/13 Pct Recovery = 92% Analysis Date = 04/03/13 Pct Recovery = 92% Analysis Date = 03/23/13 Pct Recovery = 92% Analysis Date = 03/23/13 Pct Recovery = 92% Analysis Date = 03/12/13 Pct Recovery = 92% Analysis Date = 03/12/13 Pct Recovery = 92% Analysis Date = 03/01/13 Pct Recovery = 92% Analysis Date = 03/01/13 Pct Recovery = 92% Analysis Date = 02/19/13 Pct Recovery = 92% Analysis Date = 02/19/13 Pct Recovery = 92% Analysis Date = 02/08/13 Pct Recovery = 92% Analysis Date = 02/08/13 Pct Recovery = 92% Analysis Date = 01/28/13 Pct Recovery = 92% Analysis Date = 01/28/13 Pct Recovery = 92% Analysis Date = 01/17/13 Pct Recovery = 92% Analysis Date = 01/17/13 Pct Recovery = 92% Analysis Date = 01/06/13 Pct Recovery = 93% Analysis Date = 01/06/13 Pct Recovery = 93% Analysis Date = 12/26/12 Pct Recovery = 93% Analysis Date = 12/26/12 Pct Recovery = 93% Analysis Date = 12/16/12 Pct Recovery = 94% Analysis Date = 12/16/12 Pct Recovery = 94% Analysis Date = 12/05/12 Pct Recovery = 94% Analysis Date = 12/05/12 Pct Recovery = 94% Analysis Date = 11/24/12 Pct Recovery = 94% Analysis Date = 11/24/12 Pct Recovery = 94% Analysis Date = 11/13/12 Pct Recovery = 95% Analysis Date = 11/13/12 Pct Recovery = 95% Analysis Date = 11/02/12 Pct Recovery = 95% Analysis Date = 11/02/12 Pct Recovery = 95% Analysis Date = 10/23/12 Pct Recovery = 95% Analysis Date = 10/23/12 Pct Recovery = 95% Analysis Date = 10/12/12 Pct Recovery = 96% Analysis Date = 10/12/12 Pct Recovery = 96% Analysis Date = 10/01/12 Pct Recovery = 96% Analysis Date = 10/01/12 Pct Recovery = 96% Analysis Date = 09/20/12 Pct Recovery = 97% Analysis Date = 09/20/12 Pct Recovery = 97% Analysis Date = 09/09/12 Pct Recovery = 97% Analysis Date = 09/09/12 Pct Recovery = 97% Analysis Date = 08/29/12 Pct Recovery = 97% Analysis Date = 08/29/12 Pct Recovery = 97% Analysis Date = 08/19/12 Pct Recovery = 98% Analysis Date = 08/19/12 Pct Recovery = 98% Analysis Date = 08/08/12 Pct Recovery = 98% Analysis Date = 08/08/12 Pct Recovery = 98% Analysis Date = 07/28/12 Pct Recovery = 99% Analysis Date = 07/28/12 Pct Recovery = 99% Analysis Date = 07/17/12 Pct Recovery = 99% Analysis Date = 07/17/12 Pct Recovery = 99% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 06/25/12 Pct Recovery = 100% Analysis Date = 06/25/12 Pct Recovery = 100% Analysis Date = 06/15/12 Pct Recovery = 101% Analysis Date = 06/15/12 Pct Recovery = 101% Analysis Date = 06/04/12 Pct Recovery = 101% Analysis Date = 06/04/12 Pct Recovery = 101% Analysis Date = 05/24/12 Pct Recovery = 102% Analysis Date = 05/24/12 Pct Recovery = 102% Analysis Date = 05/13/12 Pct Recovery = 102% Analysis Date = 05/13/12 Pct Recovery = 102% Analysis Date = 05/02/12 Pct Recovery = 103% Analysis Date = 05/02/12 Pct Recovery = 103% Analysis Date = 04/22/12 Pct Recovery = 103% Analysis Date = 04/22/12 Pct Recovery = 103% Analysis Date = 04/11/12 Pct Recovery = 103% Analysis Date = 04/11/12 Pct Recovery = 103% Analysis Date = 03/31/12 Pct Recovery = 104% Analysis Date = 03/31/12 Pct Recovery = 104% Analysis Date = 03/20/12 Pct Recovery = 104% Analysis Date = 03/20/12 Pct Recovery = 104% Analysis Date = 03/09/12 Pct Recovery = 105% Analysis Date = 03/09/12 Pct Recovery = 105% Analysis Date = 02/27/12 Pct Recovery = 105% Analysis Date = 02/27/12 Pct Recovery = 105% Analysis Date = 02/17/12 Pct Recovery = 106% Analysis Date = 02/17/12 Pct Recovery = 106% Analysis Date = 02/06/12 Pct Recovery = 106% Analysis Date = 02/06/12 Pct Recovery = 106% Analysis Date = 01/26/12 Pct Recovery = 107% Analysis Date = 01/26/12 Pct Recovery = 107% Analysis Date = 01/15/12 Pct Recovery = 107% Analysis Date = 01/15/12 Pct Recovery = 107% Analysis Date = 01/04/12 Pct Recovery = 107% Analysis Date = 01/04/12 Pct Recovery = 107% Analysis Date = 12/24/11 Pct Recovery = 108% Analysis Date = 12/24/11 Pct Recovery = 108% Analysis Date = 12/14/11 Pct Recovery = 108% Analysis Date = 12/14/11 Pct Recovery = 108% Analysis Date = 12/03/11 Pct Recovery = 109% Analysis Date = 12/03/11 Pct Recovery = 109% Analysis Date = 11/22/11 Pct Recovery = 109% Analysis Date = 11/22/11 Pct Recovery = 109% Analysis Date = 11/11/11 Pct Recovery = 110% Analysis Date = 11/11/11 Pct Recovery = 110% Analysis Date = 10/31/11 Pct Recovery = 110% Analysis Date = 10/31/11 Pct Recovery = 110% Analysis Date = 10/20/11 Pct Recovery = 111% Analysis Date = 10/20/11 Pct Recovery = 111% Analysis Date = 10/10/11 Pct Recovery = 111% Analysis Date = 10/10/11 Pct Recovery = 111% Analysis Date = 09/29/11 Pct Recovery = 112% Analysis Date = 09/29/11 Pct Recovery = 112% Analysis Date = 09/18/11 Pct Recovery = 112% Analysis Date = 09/18/11 Pct Recovery = 112% Analysis Date = 09/07/11 Pct Recovery = 112% Analysis Date = 09/07/11 Pct Recovery = 112% Analysis Date = 08/27/11 Pct Recovery = 113% Analysis Date = 08/27/11 Pct Recovery = 113% Analysis Date = 08/17/11 Pct Recovery = 113% Analysis Date = 08/17/11 Pct Recovery = 113% Analysis Date = 08/06/11 Pct Recovery = 114% Analysis Date = 08/06/11 Pct Recovery = 114% Analysis Date = 07/26/11 Pct Recovery = 114% Analysis Date = 07/26/11 Pct Recovery = 114% Analysis Date = 07/15/11 Pct Recovery = 115% Analysis Date = 07/15/11 Pct Recovery = 115% Analysis Date = 07/04/11 Pct Recovery = 115% Analysis Date = 07/04/11 Pct Recovery = 115% Analysis Date = 06/23/11 Pct Recovery = 116% Analysis Date = 06/23/11 Pct Recovery = 116% Analysis Date = 06/13/11 Pct Recovery = 116% Analysis Date = 06/13/11 Pct Recovery = 116% Analysis Date = 06/02/11 Pct Recovery = 117% Analysis Date = 06/02/11 Pct Recovery = 117% Analysis Date = 05/22/11 Pct Recovery = 117% Analysis Date = 05/22/11 Pct Recovery = 117% Analysis Date = 05/11/11 Pct Recovery = 118% Analysis Date = 05/11/11 Pct Recovery = 118% Analysis Date = 04/30/11 Pct Recovery = 118% Analysis Date = 04/30/11 Pct Recovery = 118% Analysis Date = 04/19/11 Pct Recovery = 118% Analysis Date = 04/19/11 Pct Recovery = 118% Analysis Date = 04/09/11 Pct Recovery = 119% Analysis Date = 04/09/11 Pct Recovery = 119% Analysis Date = 03/29/11 Pct Recovery = 119% Analysis Date = 03/29/11 Pct Recovery = 119% Analysis Date = 03/18/11 Pct Recovery = 120% Analysis Date = 03/18/11 Pct Recovery = 120% Analysis Date = 03/07/11 Pct Recovery = 120% Analysis Date = 03/07/11 Pct Recovery = 120% Analysis Date = 02/24/11 Pct Recovery = 121% Analysis Date = 02/24/11 Pct Recovery = 121% Analysis Date = 02/14/11 Pct Recovery = 121% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOFENPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 85 94% 26% 95% 21%
Total 85 94% 26% 95% 21%

Sample Statistics
ISOFENPHOS

Characteristic N % % Basis
Plotted 85 99% Spiked
Estimated Values 1 1% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 1 1% 1 out of 86
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

BQS OBSP Determination:
MALAOXON
METHOD: 2033 , TESTIDCODE: 61652GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 121% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 85% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 67% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 61% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 98% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 111% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 41% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 84% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 116% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 78% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 95% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 73% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 69% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 70% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 107% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 118% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 66% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 52% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 83% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 102% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 102% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 112% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 93% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 92% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 108% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 88% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 80% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 90% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 100% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 92% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 79% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 79% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 80% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 86% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 124% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 113% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 109% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 101% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 117% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 104% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 98% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 101% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 83% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 94% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 90% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 125% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 122% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 160% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 141% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 75% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 117% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 110% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 100% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 129% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 78% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 93% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 87% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 118% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 136% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 74% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 138% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 112% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 124% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 125% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 95% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 109% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 115% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 155% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 141% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 109% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 116% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 120% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 90% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 93% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 117% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 101% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 81% Analysis Date = 11/28/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/07/16 Pct Recovery = 81% Analysis Date = 11/07/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/16/16 Pct Recovery = 82% Analysis Date = 10/16/16 Pct Recovery = 82% Analysis Date = 10/06/16 Pct Recovery = 82% Analysis Date = 10/06/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/25/16 Pct Recovery = 82% Analysis Date = 09/14/16 Pct Recovery = 83% Analysis Date = 09/14/16 Pct Recovery = 83% Analysis Date = 09/03/16 Pct Recovery = 83% Analysis Date = 09/03/16 Pct Recovery = 83% Analysis Date = 08/24/16 Pct Recovery = 83% Analysis Date = 08/24/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/02/16 Pct Recovery = 84% Analysis Date = 08/02/16 Pct Recovery = 84% Analysis Date = 07/23/16 Pct Recovery = 84% Analysis Date = 07/23/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/12/16 Pct Recovery = 84% Analysis Date = 07/01/16 Pct Recovery = 85% Analysis Date = 07/01/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/21/16 Pct Recovery = 85% Analysis Date = 06/10/16 Pct Recovery = 85% Analysis Date = 06/10/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 86% Analysis Date = 05/19/16 Pct Recovery = 86% Analysis Date = 05/09/16 Pct Recovery = 86% Analysis Date = 05/09/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 87% Analysis Date = 04/17/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/13/16 Pct Recovery = 88% Analysis Date = 02/13/16 Pct Recovery = 88% Analysis Date = 02/02/16 Pct Recovery = 89% Analysis Date = 02/02/16 Pct Recovery = 89% Analysis Date = 01/23/16 Pct Recovery = 89% Analysis Date = 01/23/16 Pct Recovery = 89% Analysis Date = 01/12/16 Pct Recovery = 89% Analysis Date = 01/12/16 Pct Recovery = 89% Analysis Date = 01/01/16 Pct Recovery = 89% Analysis Date = 01/01/16 Pct Recovery = 89% Analysis Date = 12/22/15 Pct Recovery = 90% Analysis Date = 12/22/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 11/30/15 Pct Recovery = 90% Analysis Date = 11/30/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 91% Analysis Date = 11/09/15 Pct Recovery = 91% Analysis Date = 10/29/15 Pct Recovery = 91% Analysis Date = 10/29/15 Pct Recovery = 91% Analysis Date = 10/18/15 Pct Recovery = 91% Analysis Date = 10/18/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 91% Analysis Date = 10/08/15 Pct Recovery = 91% Analysis Date = 09/27/15 Pct Recovery = 92% Analysis Date = 09/27/15 Pct Recovery = 92% Analysis Date = 09/16/15 Pct Recovery = 92% Analysis Date = 09/16/15 Pct Recovery = 92% Analysis Date = 09/05/15 Pct Recovery = 92% Analysis Date = 09/05/15 Pct Recovery = 92% Analysis Date = 08/26/15 Pct Recovery = 92% Analysis Date = 08/26/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 93% Analysis Date = 08/15/15 Pct Recovery = 93% Analysis Date = 08/04/15 Pct Recovery = 93% Analysis Date = 08/04/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/25/15 Pct Recovery = 93% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/14/15 Pct Recovery = 94% Analysis Date = 07/03/15 Pct Recovery = 94% Analysis Date = 07/03/15 Pct Recovery = 94% Analysis Date = 06/23/15 Pct Recovery = 94% Analysis Date = 06/23/15 Pct Recovery = 94% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/12/15 Pct Recovery = 95% Analysis Date = 06/01/15 Pct Recovery = 95% Analysis Date = 06/01/15 Pct Recovery = 95% Analysis Date = 05/21/15 Pct Recovery = 95% Analysis Date = 05/21/15 Pct Recovery = 95% Analysis Date = 05/11/15 Pct Recovery = 96% Analysis Date = 05/11/15 Pct Recovery = 96% Analysis Date = 04/30/15 Pct Recovery = 96% Analysis Date = 04/30/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/19/15 Pct Recovery = 96% Analysis Date = 04/09/15 Pct Recovery = 97% Analysis Date = 04/09/15 Pct Recovery = 97% Analysis Date = 03/29/15 Pct Recovery = 97% Analysis Date = 03/29/15 Pct Recovery = 97% Analysis Date = 03/18/15 Pct Recovery = 97% Analysis Date = 03/18/15 Pct Recovery = 97% Analysis Date = 03/07/15 Pct Recovery = 98% Analysis Date = 03/07/15 Pct Recovery = 98% Analysis Date = 02/25/15 Pct Recovery = 98% Analysis Date = 02/25/15 Pct Recovery = 98% Analysis Date = 02/14/15 Pct Recovery = 98% Analysis Date = 02/14/15 Pct Recovery = 98% Analysis Date = 02/03/15 Pct Recovery = 99% Analysis Date = 02/03/15 Pct Recovery = 99% Analysis Date = 01/24/15 Pct Recovery = 99% Analysis Date = 01/24/15 Pct Recovery = 99% Analysis Date = 01/13/15 Pct Recovery = 99% Analysis Date = 01/13/15 Pct Recovery = 99% Analysis Date = 01/02/15 Pct Recovery = 99% Analysis Date = 01/02/15 Pct Recovery = 99% Analysis Date = 12/23/14 Pct Recovery = 100% Analysis Date = 12/23/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/12/14 Pct Recovery = 100% Analysis Date = 12/01/14 Pct Recovery = 100% Analysis Date = 12/01/14 Pct Recovery = 100% Analysis Date = 11/20/14 Pct Recovery = 100% Analysis Date = 11/20/14 Pct Recovery = 100% Analysis Date = 11/10/14 Pct Recovery = 101% Analysis Date = 11/10/14 Pct Recovery = 101% Analysis Date = 10/30/14 Pct Recovery = 101% Analysis Date = 10/30/14 Pct Recovery = 101% Analysis Date = 10/19/14 Pct Recovery = 101% Analysis Date = 10/19/14 Pct Recovery = 101% Analysis Date = 10/09/14 Pct Recovery = 101% Analysis Date = 10/09/14 Pct Recovery = 101% Analysis Date = 09/28/14 Pct Recovery = 101% Analysis Date = 09/28/14 Pct Recovery = 101% Analysis Date = 09/17/14 Pct Recovery = 102% Analysis Date = 09/17/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 09/07/14 Pct Recovery = 102% Analysis Date = 08/27/14 Pct Recovery = 102% Analysis Date = 08/27/14 Pct Recovery = 102% Analysis Date = 08/16/14 Pct Recovery = 102% Analysis Date = 08/16/14 Pct Recovery = 102% Analysis Date = 08/05/14 Pct Recovery = 103% Analysis Date = 08/05/14 Pct Recovery = 103% Analysis Date = 07/26/14 Pct Recovery = 103% Analysis Date = 07/26/14 Pct Recovery = 103% Analysis Date = 07/15/14 Pct Recovery = 103% Analysis Date = 07/15/14 Pct Recovery = 103% Analysis Date = 07/04/14 Pct Recovery = 103% Analysis Date = 07/04/14 Pct Recovery = 103% Analysis Date = 06/24/14 Pct Recovery = 103% Analysis Date = 06/24/14 Pct Recovery = 103% Analysis Date = 06/13/14 Pct Recovery = 104% Analysis Date = 06/13/14 Pct Recovery = 104% Analysis Date = 06/02/14 Pct Recovery = 104% Analysis Date = 06/02/14 Pct Recovery = 104% Analysis Date = 05/22/14 Pct Recovery = 104% Analysis Date = 05/22/14 Pct Recovery = 104% Analysis Date = 05/12/14 Pct Recovery = 104% Analysis Date = 05/12/14 Pct Recovery = 104% Analysis Date = 05/01/14 Pct Recovery = 104% Analysis Date = 05/01/14 Pct Recovery = 104% Analysis Date = 04/20/14 Pct Recovery = 104% Analysis Date = 04/20/14 Pct Recovery = 104% Analysis Date = 04/10/14 Pct Recovery = 104% Analysis Date = 04/10/14 Pct Recovery = 104% Analysis Date = 03/30/14 Pct Recovery = 104% Analysis Date = 03/30/14 Pct Recovery = 104% Analysis Date = 03/19/14 Pct Recovery = 104% Analysis Date = 03/19/14 Pct Recovery = 104% Analysis Date = 03/09/14 Pct Recovery = 104% Analysis Date = 03/09/14 Pct Recovery = 104% Analysis Date = 02/26/14 Pct Recovery = 104% Analysis Date = 02/26/14 Pct Recovery = 104% Analysis Date = 02/15/14 Pct Recovery = 104% Analysis Date = 02/15/14 Pct Recovery = 104% Analysis Date = 02/04/14 Pct Recovery = 104% Analysis Date = 02/04/14 Pct Recovery = 104% Analysis Date = 01/25/14 Pct Recovery = 104% Analysis Date = 01/25/14 Pct Recovery = 104% Analysis Date = 01/14/14 Pct Recovery = 104% Analysis Date = 01/14/14 Pct Recovery = 104% Analysis Date = 01/03/14 Pct Recovery = 104% Analysis Date = 01/03/14 Pct Recovery = 104% Analysis Date = 12/24/13 Pct Recovery = 104% Analysis Date = 12/24/13 Pct Recovery = 104% Analysis Date = 12/13/13 Pct Recovery = 104% Analysis Date = 12/13/13 Pct Recovery = 104% Analysis Date = 12/02/13 Pct Recovery = 104% Analysis Date = 12/02/13 Pct Recovery = 104% Analysis Date = 11/21/13 Pct Recovery = 104% Analysis Date = 11/21/13 Pct Recovery = 104% Analysis Date = 11/11/13 Pct Recovery = 104% Analysis Date = 11/11/13 Pct Recovery = 104% Analysis Date = 10/31/13 Pct Recovery = 104% Analysis Date = 10/31/13 Pct Recovery = 104% Analysis Date = 10/20/13 Pct Recovery = 104% Analysis Date = 10/20/13 Pct Recovery = 104% Analysis Date = 10/10/13 Pct Recovery = 104% Analysis Date = 10/10/13 Pct Recovery = 104% Analysis Date = 09/29/13 Pct Recovery = 104% Analysis Date = 09/29/13 Pct Recovery = 104% Analysis Date = 09/18/13 Pct Recovery = 104% Analysis Date = 09/18/13 Pct Recovery = 104% Analysis Date = 09/08/13 Pct Recovery = 105% Analysis Date = 09/08/13 Pct Recovery = 105% Analysis Date = 08/28/13 Pct Recovery = 105% Analysis Date = 08/28/13 Pct Recovery = 105% Analysis Date = 08/17/13 Pct Recovery = 105% Analysis Date = 08/17/13 Pct Recovery = 105% Analysis Date = 08/06/13 Pct Recovery = 105% Analysis Date = 08/06/13 Pct Recovery = 105% Analysis Date = 07/27/13 Pct Recovery = 105% Analysis Date = 07/27/13 Pct Recovery = 105% Analysis Date = 07/16/13 Pct Recovery = 105% Analysis Date = 07/16/13 Pct Recovery = 105% Analysis Date = 07/05/13 Pct Recovery = 105% Analysis Date = 07/05/13 Pct Recovery = 105% Analysis Date = 06/25/13 Pct Recovery = 105% Analysis Date = 06/25/13 Pct Recovery = 105% Analysis Date = 06/14/13 Pct Recovery = 105% Analysis Date = 06/14/13 Pct Recovery = 105% Analysis Date = 06/03/13 Pct Recovery = 105% Analysis Date = 06/03/13 Pct Recovery = 105% Analysis Date = 05/23/13 Pct Recovery = 105% Analysis Date = 05/23/13 Pct Recovery = 105% Analysis Date = 05/13/13 Pct Recovery = 105% Analysis Date = 05/13/13 Pct Recovery = 105% Analysis Date = 05/02/13 Pct Recovery = 105% Analysis Date = 05/02/13 Pct Recovery = 105% Analysis Date = 04/21/13 Pct Recovery = 105% Analysis Date = 04/21/13 Pct Recovery = 105% Analysis Date = 04/11/13 Pct Recovery = 105% Analysis Date = 04/11/13 Pct Recovery = 105% Analysis Date = 03/31/13 Pct Recovery = 105% Analysis Date = 03/31/13 Pct Recovery = 105% Analysis Date = 03/20/13 Pct Recovery = 105% Analysis Date = 03/20/13 Pct Recovery = 105% Analysis Date = 03/10/13 Pct Recovery = 105% Analysis Date = 03/10/13 Pct Recovery = 105% Analysis Date = 02/27/13 Pct Recovery = 105% Analysis Date = 02/27/13 Pct Recovery = 105% Analysis Date = 02/16/13 Pct Recovery = 105% Analysis Date = 02/16/13 Pct Recovery = 105% Analysis Date = 02/05/13 Pct Recovery = 104% Analysis Date = 02/05/13 Pct Recovery = 104% Analysis Date = 01/26/13 Pct Recovery = 104% Analysis Date = 01/26/13 Pct Recovery = 104% Analysis Date = 01/15/13 Pct Recovery = 104% Analysis Date = 01/15/13 Pct Recovery = 104% Analysis Date = 01/04/13 Pct Recovery = 104% Analysis Date = 01/04/13 Pct Recovery = 104% Analysis Date = 12/25/12 Pct Recovery = 103% Analysis Date = 12/25/12 Pct Recovery = 103% Analysis Date = 12/14/12 Pct Recovery = 103% Analysis Date = 12/14/12 Pct Recovery = 103% Analysis Date = 12/03/12 Pct Recovery = 103% Analysis Date = 12/03/12 Pct Recovery = 103% Analysis Date = 11/23/12 Pct Recovery = 103% Analysis Date = 11/23/12 Pct Recovery = 103% Analysis Date = 11/12/12 Pct Recovery = 103% Analysis Date = 11/12/12 Pct Recovery = 103% Analysis Date = 11/01/12 Pct Recovery = 102% Analysis Date = 11/01/12 Pct Recovery = 102% Analysis Date = 10/21/12 Pct Recovery = 102% Analysis Date = 10/21/12 Pct Recovery = 102% Analysis Date = 10/11/12 Pct Recovery = 102% Analysis Date = 10/11/12 Pct Recovery = 102% Analysis Date = 09/30/12 Pct Recovery = 101% Analysis Date = 09/30/12 Pct Recovery = 101% Analysis Date = 09/19/12 Pct Recovery = 101% Analysis Date = 09/19/12 Pct Recovery = 101% Analysis Date = 09/09/12 Pct Recovery = 101% Analysis Date = 09/09/12 Pct Recovery = 101% Analysis Date = 08/29/12 Pct Recovery = 100% Analysis Date = 08/29/12 Pct Recovery = 100% Analysis Date = 08/18/12 Pct Recovery = 100% Analysis Date = 08/18/12 Pct Recovery = 100% Analysis Date = 08/07/12 Pct Recovery = 100% Analysis Date = 08/07/12 Pct Recovery = 100% Analysis Date = 07/28/12 Pct Recovery = 99% Analysis Date = 07/28/12 Pct Recovery = 99% Analysis Date = 07/17/12 Pct Recovery = 99% Analysis Date = 07/17/12 Pct Recovery = 99% Analysis Date = 07/06/12 Pct Recovery = 99% Analysis Date = 07/06/12 Pct Recovery = 99% Analysis Date = 06/26/12 Pct Recovery = 99% Analysis Date = 06/26/12 Pct Recovery = 99% Analysis Date = 06/15/12 Pct Recovery = 98% Analysis Date = 06/15/12 Pct Recovery = 98% Analysis Date = 06/04/12 Pct Recovery = 98% Analysis Date = 06/04/12 Pct Recovery = 98% Analysis Date = 05/25/12 Pct Recovery = 98% Analysis Date = 05/25/12 Pct Recovery = 98% Analysis Date = 05/14/12 Pct Recovery = 98% Analysis Date = 05/14/12 Pct Recovery = 98% Analysis Date = 05/03/12 Pct Recovery = 97% Analysis Date = 05/03/12 Pct Recovery = 97% Analysis Date = 04/22/12 Pct Recovery = 97% Analysis Date = 04/22/12 Pct Recovery = 97% Analysis Date = 04/12/12 Pct Recovery = 97% Analysis Date = 04/12/12 Pct Recovery = 97% Analysis Date = 04/01/12 Pct Recovery = 97% Analysis Date = 04/01/12 Pct Recovery = 97% Analysis Date = 03/21/12 Pct Recovery = 97% Analysis Date = 03/21/12 Pct Recovery = 97% Analysis Date = 03/11/12 Pct Recovery = 96% Analysis Date = 03/11/12 Pct Recovery = 96% Analysis Date = 02/29/12 Pct Recovery = 96% Analysis Date = 02/29/12 Pct Recovery = 96% Analysis Date = 02/18/12 Pct Recovery = 96% Analysis Date = 02/18/12 Pct Recovery = 96% Analysis Date = 02/07/12 Pct Recovery = 96% Analysis Date = 02/07/12 Pct Recovery = 96% Analysis Date = 01/28/12 Pct Recovery = 95% Analysis Date = 01/28/12 Pct Recovery = 95% Analysis Date = 01/17/12 Pct Recovery = 95% Analysis Date = 01/17/12 Pct Recovery = 95% Analysis Date = 01/06/12 Pct Recovery = 95% Analysis Date = 01/06/12 Pct Recovery = 95% Analysis Date = 12/27/11 Pct Recovery = 95% Analysis Date = 12/27/11 Pct Recovery = 95% Analysis Date = 12/16/11 Pct Recovery = 95% Analysis Date = 12/16/11 Pct Recovery = 95% Analysis Date = 12/05/11 Pct Recovery = 94% Analysis Date = 12/05/11 Pct Recovery = 94% Analysis Date = 11/25/11 Pct Recovery = 94% Analysis Date = 11/25/11 Pct Recovery = 94% Analysis Date = 11/14/11 Pct Recovery = 94% Analysis Date = 11/14/11 Pct Recovery = 94% Analysis Date = 11/03/11 Pct Recovery = 94% Analysis Date = 11/03/11 Pct Recovery = 94% Analysis Date = 10/23/11 Pct Recovery = 94% Analysis Date = 10/23/11 Pct Recovery = 94% Analysis Date = 10/13/11 Pct Recovery = 93% Analysis Date = 10/13/11 Pct Recovery = 93% Analysis Date = 10/02/11 Pct Recovery = 93% Analysis Date = 10/02/11 Pct Recovery = 93% Analysis Date = 09/21/11 Pct Recovery = 93% Analysis Date = 09/21/11 Pct Recovery = 93% Analysis Date = 09/11/11 Pct Recovery = 93% Analysis Date = 09/11/11 Pct Recovery = 93% Analysis Date = 08/31/11 Pct Recovery = 92% Analysis Date = 08/31/11 Pct Recovery = 92% Analysis Date = 08/20/11 Pct Recovery = 92% Analysis Date = 08/20/11 Pct Recovery = 92% Analysis Date = 08/09/11 Pct Recovery = 92% Analysis Date = 08/09/11 Pct Recovery = 92% Analysis Date = 07/30/11 Pct Recovery = 92% Analysis Date = 07/30/11 Pct Recovery = 92% Analysis Date = 07/19/11 Pct Recovery = 91% Analysis Date = 07/19/11 Pct Recovery = 91% Analysis Date = 07/08/11 Pct Recovery = 91% Analysis Date = 07/08/11 Pct Recovery = 91% Analysis Date = 06/28/11 Pct Recovery = 91% Analysis Date = 06/28/11 Pct Recovery = 91% Analysis Date = 06/17/11 Pct Recovery = 91% Analysis Date = 06/17/11 Pct Recovery = 91% Analysis Date = 06/06/11 Pct Recovery = 90% Analysis Date = 06/06/11 Pct Recovery = 90% Analysis Date = 05/27/11 Pct Recovery = 90% Analysis Date = 05/27/11 Pct Recovery = 90% Analysis Date = 05/16/11 Pct Recovery = 90% Analysis Date = 05/16/11 Pct Recovery = 90% Analysis Date = 05/05/11 Pct Recovery = 90% Analysis Date = 05/05/11 Pct Recovery = 90% Analysis Date = 04/24/11 Pct Recovery = 89% Analysis Date = 04/24/11 Pct Recovery = 89% Analysis Date = 04/14/11 Pct Recovery = 89% Analysis Date = 04/14/11 Pct Recovery = 89% Analysis Date = 04/03/11 Pct Recovery = 89% Analysis Date = 04/03/11 Pct Recovery = 89% Analysis Date = 03/23/11 Pct Recovery = 89% Analysis Date = 03/23/11 Pct Recovery = 89% Analysis Date = 03/13/11 Pct Recovery = 88% Analysis Date = 03/13/11 Pct Recovery = 88% Analysis Date = 03/02/11 Pct Recovery = 88% Analysis Date = 03/02/11 Pct Recovery = 88% Analysis Date = 02/19/11 Pct Recovery = 88% Analysis Date = 02/19/11 Pct Recovery = 88% Analysis Date = 02/09/11 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALAOXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 93 97% 22% 95% 23%
Total 93 97% 22% 95% 23%

Sample Statistics
MALAOXON

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 8 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 3 4% 3 out of 76

BQS OBSP Determination:
MALATHION
METHOD: 2033 , TESTIDCODE: 39532GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 91% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 84% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 73% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 87% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 77% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 71% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 98% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 104% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 92% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 96% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 105% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 72% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 69% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 93% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 97% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 120% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 73% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 73% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 87% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 82% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 73% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 76% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 81% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 73% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 88% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 76% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 75% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 98% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 74% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 118% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 89% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 77% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 99% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 91% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 80% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 85% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 96% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 127% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 76% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 107% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 91% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 78% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 90% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 72% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 125% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 81% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 106% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 86% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 93% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 67% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 100% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 78% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 107% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 81% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 104% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 83% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 95% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 136% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 133% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 66% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 78% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 76% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 63% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 102% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 96% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 97% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 59% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 119% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 114% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 100% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 156% Analysis Date = 01/17/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/16/16 Pct Recovery = 92% Analysis Date = 12/16/16 Pct Recovery = 92% Analysis Date = 12/05/16 Pct Recovery = 92% Analysis Date = 12/05/16 Pct Recovery = 92% Analysis Date = 11/24/16 Pct Recovery = 92% Analysis Date = 11/24/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 10/23/16 Pct Recovery = 92% Analysis Date = 10/23/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/20/16 Pct Recovery = 92% Analysis Date = 09/09/16 Pct Recovery = 92% Analysis Date = 09/09/16 Pct Recovery = 92% Analysis Date = 08/29/16 Pct Recovery = 92% Analysis Date = 08/29/16 Pct Recovery = 92% Analysis Date = 08/19/16 Pct Recovery = 92% Analysis Date = 08/19/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 08/08/16 Pct Recovery = 92% Analysis Date = 07/28/16 Pct Recovery = 92% Analysis Date = 07/28/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 92% Analysis Date = 06/04/16 Pct Recovery = 92% Analysis Date = 06/04/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/13/16 Pct Recovery = 92% Analysis Date = 05/13/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 04/21/16 Pct Recovery = 92% Analysis Date = 04/21/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 03/30/16 Pct Recovery = 92% Analysis Date = 03/30/16 Pct Recovery = 92% Analysis Date = 03/20/16 Pct Recovery = 92% Analysis Date = 03/20/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 03/09/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/16/16 Pct Recovery = 92% Analysis Date = 02/16/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 02/05/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/25/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/14/16 Pct Recovery = 92% Analysis Date = 01/04/16 Pct Recovery = 92% Analysis Date = 01/04/16 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/24/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/13/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 12/02/15 Pct Recovery = 92% Analysis Date = 11/21/15 Pct Recovery = 91% Analysis Date = 11/21/15 Pct Recovery = 91% Analysis Date = 11/10/15 Pct Recovery = 91% Analysis Date = 11/10/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/30/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/20/15 Pct Recovery = 91% Analysis Date = 10/09/15 Pct Recovery = 91% Analysis Date = 10/09/15 Pct Recovery = 91% Analysis Date = 09/28/15 Pct Recovery = 91% Analysis Date = 09/28/15 Pct Recovery = 91% Analysis Date = 09/17/15 Pct Recovery = 91% Analysis Date = 09/17/15 Pct Recovery = 91% Analysis Date = 09/06/15 Pct Recovery = 91% Analysis Date = 09/06/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/26/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/15/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 08/05/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/25/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/14/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 07/03/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/22/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 06/11/15 Pct Recovery = 91% Analysis Date = 05/31/15 Pct Recovery = 91% Analysis Date = 05/31/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/21/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 05/10/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/18/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 04/07/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/16/15 Pct Recovery = 91% Analysis Date = 03/16/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 03/06/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/23/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/12/15 Pct Recovery = 91% Analysis Date = 02/01/15 Pct Recovery = 91% Analysis Date = 02/01/15 Pct Recovery = 91% Analysis Date = 01/21/15 Pct Recovery = 91% Analysis Date = 01/21/15 Pct Recovery = 91% Analysis Date = 01/10/15 Pct Recovery = 91% Analysis Date = 01/10/15 Pct Recovery = 91% Analysis Date = 12/31/14 Pct Recovery = 91% Analysis Date = 12/31/14 Pct Recovery = 91% Analysis Date = 12/20/14 Pct Recovery = 91% Analysis Date = 12/20/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 11/28/14 Pct Recovery = 91% Analysis Date = 11/28/14 Pct Recovery = 91% Analysis Date = 11/17/14 Pct Recovery = 91% Analysis Date = 11/17/14 Pct Recovery = 91% Analysis Date = 11/06/14 Pct Recovery = 92% Analysis Date = 11/06/14 Pct Recovery = 92% Analysis Date = 10/26/14 Pct Recovery = 92% Analysis Date = 10/26/14 Pct Recovery = 92% Analysis Date = 10/16/14 Pct Recovery = 92% Analysis Date = 10/16/14 Pct Recovery = 92% Analysis Date = 10/05/14 Pct Recovery = 92% Analysis Date = 10/05/14 Pct Recovery = 92% Analysis Date = 09/24/14 Pct Recovery = 92% Analysis Date = 09/24/14 Pct Recovery = 92% Analysis Date = 09/13/14 Pct Recovery = 92% Analysis Date = 09/13/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 09/02/14 Pct Recovery = 92% Analysis Date = 08/22/14 Pct Recovery = 92% Analysis Date = 08/22/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/11/14 Pct Recovery = 92% Analysis Date = 08/01/14 Pct Recovery = 91% Analysis Date = 08/01/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/10/14 Pct Recovery = 91% Analysis Date = 07/10/14 Pct Recovery = 91% Analysis Date = 06/29/14 Pct Recovery = 91% Analysis Date = 06/29/14 Pct Recovery = 91% Analysis Date = 06/18/14 Pct Recovery = 91% Analysis Date = 06/18/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 06/07/14 Pct Recovery = 91% Analysis Date = 05/27/14 Pct Recovery = 91% Analysis Date = 05/27/14 Pct Recovery = 91% Analysis Date = 05/17/14 Pct Recovery = 91% Analysis Date = 05/17/14 Pct Recovery = 91% Analysis Date = 05/06/14 Pct Recovery = 91% Analysis Date = 05/06/14 Pct Recovery = 91% Analysis Date = 04/25/14 Pct Recovery = 90% Analysis Date = 04/25/14 Pct Recovery = 90% Analysis Date = 04/14/14 Pct Recovery = 90% Analysis Date = 04/14/14 Pct Recovery = 90% Analysis Date = 04/03/14 Pct Recovery = 90% Analysis Date = 04/03/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 90% Analysis Date = 03/23/14 Pct Recovery = 90% Analysis Date = 03/12/14 Pct Recovery = 90% Analysis Date = 03/12/14 Pct Recovery = 90% Analysis Date = 03/02/14 Pct Recovery = 89% Analysis Date = 03/02/14 Pct Recovery = 89% Analysis Date = 02/19/14 Pct Recovery = 89% Analysis Date = 02/19/14 Pct Recovery = 89% Analysis Date = 02/08/14 Pct Recovery = 89% Analysis Date = 02/08/14 Pct Recovery = 89% Analysis Date = 01/28/14 Pct Recovery = 89% Analysis Date = 01/28/14 Pct Recovery = 89% Analysis Date = 01/17/14 Pct Recovery = 89% Analysis Date = 01/17/14 Pct Recovery = 89% Analysis Date = 01/06/14 Pct Recovery = 89% Analysis Date = 01/06/14 Pct Recovery = 89% Analysis Date = 12/26/13 Pct Recovery = 89% Analysis Date = 12/26/13 Pct Recovery = 89% Analysis Date = 12/16/13 Pct Recovery = 89% Analysis Date = 12/16/13 Pct Recovery = 89% Analysis Date = 12/05/13 Pct Recovery = 89% Analysis Date = 12/05/13 Pct Recovery = 89% Analysis Date = 11/24/13 Pct Recovery = 89% Analysis Date = 11/24/13 Pct Recovery = 89% Analysis Date = 11/13/13 Pct Recovery = 89% Analysis Date = 11/13/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 11/02/13 Pct Recovery = 89% Analysis Date = 10/22/13 Pct Recovery = 89% Analysis Date = 10/22/13 Pct Recovery = 89% Analysis Date = 10/11/13 Pct Recovery = 89% Analysis Date = 10/11/13 Pct Recovery = 89% Analysis Date = 10/01/13 Pct Recovery = 88% Analysis Date = 10/01/13 Pct Recovery = 88% Analysis Date = 09/20/13 Pct Recovery = 88% Analysis Date = 09/20/13 Pct Recovery = 88% Analysis Date = 09/09/13 Pct Recovery = 89% Analysis Date = 09/09/13 Pct Recovery = 89% Analysis Date = 08/29/13 Pct Recovery = 89% Analysis Date = 08/29/13 Pct Recovery = 89% Analysis Date = 08/18/13 Pct Recovery = 89% Analysis Date = 08/18/13 Pct Recovery = 89% Analysis Date = 08/07/13 Pct Recovery = 89% Analysis Date = 08/07/13 Pct Recovery = 89% Analysis Date = 07/27/13 Pct Recovery = 89% Analysis Date = 07/27/13 Pct Recovery = 89% Analysis Date = 07/17/13 Pct Recovery = 89% Analysis Date = 07/17/13 Pct Recovery = 89% Analysis Date = 07/06/13 Pct Recovery = 89% Analysis Date = 07/06/13 Pct Recovery = 89% Analysis Date = 06/25/13 Pct Recovery = 89% Analysis Date = 06/25/13 Pct Recovery = 89% Analysis Date = 06/14/13 Pct Recovery = 89% Analysis Date = 06/14/13 Pct Recovery = 89% Analysis Date = 06/03/13 Pct Recovery = 89% Analysis Date = 06/03/13 Pct Recovery = 89% Analysis Date = 05/23/13 Pct Recovery = 89% Analysis Date = 05/23/13 Pct Recovery = 89% Analysis Date = 05/12/13 Pct Recovery = 90% Analysis Date = 05/12/13 Pct Recovery = 90% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 05/02/13 Pct Recovery = 90% Analysis Date = 04/21/13 Pct Recovery = 90% Analysis Date = 04/21/13 Pct Recovery = 90% Analysis Date = 04/10/13 Pct Recovery = 90% Analysis Date = 04/10/13 Pct Recovery = 90% Analysis Date = 03/30/13 Pct Recovery = 90% Analysis Date = 03/30/13 Pct Recovery = 90% Analysis Date = 03/19/13 Pct Recovery = 90% Analysis Date = 03/19/13 Pct Recovery = 90% Analysis Date = 03/08/13 Pct Recovery = 90% Analysis Date = 03/08/13 Pct Recovery = 90% Analysis Date = 02/25/13 Pct Recovery = 90% Analysis Date = 02/25/13 Pct Recovery = 90% Analysis Date = 02/15/13 Pct Recovery = 90% Analysis Date = 02/15/13 Pct Recovery = 90% Analysis Date = 02/04/13 Pct Recovery = 90% Analysis Date = 02/04/13 Pct Recovery = 90% Analysis Date = 01/24/13 Pct Recovery = 90% Analysis Date = 01/24/13 Pct Recovery = 90% Analysis Date = 01/13/13 Pct Recovery = 90% Analysis Date = 01/13/13 Pct Recovery = 90% Analysis Date = 01/02/13 Pct Recovery = 90% Analysis Date = 01/02/13 Pct Recovery = 90% Analysis Date = 12/22/12 Pct Recovery = 90% Analysis Date = 12/22/12 Pct Recovery = 90% Analysis Date = 12/12/12 Pct Recovery = 90% Analysis Date = 12/12/12 Pct Recovery = 90% Analysis Date = 12/01/12 Pct Recovery = 90% Analysis Date = 12/01/12 Pct Recovery = 90% Analysis Date = 11/20/12 Pct Recovery = 90% Analysis Date = 11/20/12 Pct Recovery = 90% Analysis Date = 11/09/12 Pct Recovery = 90% Analysis Date = 11/09/12 Pct Recovery = 90% Analysis Date = 10/29/12 Pct Recovery = 90% Analysis Date = 10/29/12 Pct Recovery = 90% Analysis Date = 10/18/12 Pct Recovery = 90% Analysis Date = 10/18/12 Pct Recovery = 90% Analysis Date = 10/07/12 Pct Recovery = 90% Analysis Date = 10/07/12 Pct Recovery = 90% Analysis Date = 09/27/12 Pct Recovery = 90% Analysis Date = 09/27/12 Pct Recovery = 90% Analysis Date = 09/16/12 Pct Recovery = 90% Analysis Date = 09/16/12 Pct Recovery = 90% Analysis Date = 09/05/12 Pct Recovery = 90% Analysis Date = 09/05/12 Pct Recovery = 90% Analysis Date = 08/25/12 Pct Recovery = 90% Analysis Date = 08/25/12 Pct Recovery = 90% Analysis Date = 08/14/12 Pct Recovery = 90% Analysis Date = 08/14/12 Pct Recovery = 90% Analysis Date = 08/03/12 Pct Recovery = 90% Analysis Date = 08/03/12 Pct Recovery = 90% Analysis Date = 07/23/12 Pct Recovery = 90% Analysis Date = 07/23/12 Pct Recovery = 90% Analysis Date = 07/13/12 Pct Recovery = 90% Analysis Date = 07/13/12 Pct Recovery = 90% Analysis Date = 07/02/12 Pct Recovery = 90% Analysis Date = 07/02/12 Pct Recovery = 90% Analysis Date = 06/21/12 Pct Recovery = 90% Analysis Date = 06/21/12 Pct Recovery = 90% Analysis Date = 06/10/12 Pct Recovery = 90% Analysis Date = 06/10/12 Pct Recovery = 90% Analysis Date = 05/30/12 Pct Recovery = 90% Analysis Date = 05/30/12 Pct Recovery = 90% Analysis Date = 05/19/12 Pct Recovery = 90% Analysis Date = 05/19/12 Pct Recovery = 90% Analysis Date = 05/08/12 Pct Recovery = 90% Analysis Date = 05/08/12 Pct Recovery = 90% Analysis Date = 04/28/12 Pct Recovery = 90% Analysis Date = 04/28/12 Pct Recovery = 90% Analysis Date = 04/17/12 Pct Recovery = 90% Analysis Date = 04/17/12 Pct Recovery = 90% Analysis Date = 04/06/12 Pct Recovery = 90% Analysis Date = 04/06/12 Pct Recovery = 90% Analysis Date = 03/26/12 Pct Recovery = 90% Analysis Date = 03/26/12 Pct Recovery = 90% Analysis Date = 03/15/12 Pct Recovery = 90% Analysis Date = 03/15/12 Pct Recovery = 90% Analysis Date = 03/04/12 Pct Recovery = 90% Analysis Date = 03/04/12 Pct Recovery = 90% Analysis Date = 02/22/12 Pct Recovery = 90% Analysis Date = 02/22/12 Pct Recovery = 90% Analysis Date = 02/12/12 Pct Recovery = 90% Analysis Date = 02/12/12 Pct Recovery = 90% Analysis Date = 02/01/12 Pct Recovery = 90% Analysis Date = 02/01/12 Pct Recovery = 90% Analysis Date = 01/21/12 Pct Recovery = 90% Analysis Date = 01/21/12 Pct Recovery = 90% Analysis Date = 01/10/12 Pct Recovery = 90% Analysis Date = 01/10/12 Pct Recovery = 90% Analysis Date = 12/30/11 Pct Recovery = 90% Analysis Date = 12/30/11 Pct Recovery = 90% Analysis Date = 12/19/11 Pct Recovery = 90% Analysis Date = 12/19/11 Pct Recovery = 90% Analysis Date = 12/08/11 Pct Recovery = 90% Analysis Date = 12/08/11 Pct Recovery = 90% Analysis Date = 11/28/11 Pct Recovery = 90% Analysis Date = 11/28/11 Pct Recovery = 90% Analysis Date = 11/17/11 Pct Recovery = 90% Analysis Date = 11/17/11 Pct Recovery = 90% Analysis Date = 11/06/11 Pct Recovery = 90% Analysis Date = 11/06/11 Pct Recovery = 90% Analysis Date = 10/26/11 Pct Recovery = 90% Analysis Date = 10/26/11 Pct Recovery = 90% Analysis Date = 10/15/11 Pct Recovery = 90% Analysis Date = 10/15/11 Pct Recovery = 90% Analysis Date = 10/04/11 Pct Recovery = 90% Analysis Date = 10/04/11 Pct Recovery = 90% Analysis Date = 09/23/11 Pct Recovery = 90% Analysis Date = 09/23/11 Pct Recovery = 90% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/02/11 Pct Recovery = 89% Analysis Date = 09/02/11 Pct Recovery = 89% Analysis Date = 08/22/11 Pct Recovery = 89% Analysis Date = 08/22/11 Pct Recovery = 89% Analysis Date = 08/11/11 Pct Recovery = 89% Analysis Date = 08/11/11 Pct Recovery = 89% Analysis Date = 07/31/11 Pct Recovery = 89% Analysis Date = 07/31/11 Pct Recovery = 89% Analysis Date = 07/20/11 Pct Recovery = 89% Analysis Date = 07/20/11 Pct Recovery = 89% Analysis Date = 07/09/11 Pct Recovery = 89% Analysis Date = 07/09/11 Pct Recovery = 89% Analysis Date = 06/29/11 Pct Recovery = 89% Analysis Date = 06/29/11 Pct Recovery = 89% Analysis Date = 06/18/11 Pct Recovery = 89% Analysis Date = 06/18/11 Pct Recovery = 89% Analysis Date = 06/07/11 Pct Recovery = 89% Analysis Date = 06/07/11 Pct Recovery = 89% Analysis Date = 05/27/11 Pct Recovery = 89% Analysis Date = 05/27/11 Pct Recovery = 89% Analysis Date = 05/16/11 Pct Recovery = 89% Analysis Date = 05/16/11 Pct Recovery = 89% Analysis Date = 05/05/11 Pct Recovery = 89% Analysis Date = 05/05/11 Pct Recovery = 89% Analysis Date = 04/24/11 Pct Recovery = 89% Analysis Date = 04/24/11 Pct Recovery = 89% Analysis Date = 04/14/11 Pct Recovery = 89% Analysis Date = 04/14/11 Pct Recovery = 89% Analysis Date = 04/03/11 Pct Recovery = 89% Analysis Date = 04/03/11 Pct Recovery = 89% Analysis Date = 03/23/11 Pct Recovery = 89% Analysis Date = 03/23/11 Pct Recovery = 89% Analysis Date = 03/12/11 Pct Recovery = 89% Analysis Date = 03/12/11 Pct Recovery = 89% Analysis Date = 03/01/11 Pct Recovery = 89% Analysis Date = 03/01/11 Pct Recovery = 89% Analysis Date = 02/18/11 Pct Recovery = 89% Analysis Date = 02/18/11 Pct Recovery = 89% Analysis Date = 02/08/11 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALATHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 86 90% 18% 89% 16%
Total 86 90% 18% 89% 16%

Sample Statistics
MALATHION

Characteristic N % % Basis
Plotted 86 97% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 89 .  
False Negatives 3 3% 3 out of 89
Not Spiked 80 .  
False Positives 0 0% 0 out of 80

BQS OBSP Determination:
METALAXYL
METHOD: 2033 , TESTIDCODE: 61596GCM39
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 97% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 97% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 89% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 79% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 101% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 104% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 102% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 97% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 126% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 102% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 85% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 82% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 82% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 103% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 90% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 95% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 86% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 100% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 72% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 106% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 93% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 104% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 93% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 104% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 71% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 118% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 98% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 75% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 100% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 125% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 74% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 79% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 83% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 77% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 69% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 83% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 77% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 101% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 102% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 94% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 73% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 73% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 71% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 115% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 94% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 83% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 94% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 102% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 72% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 104% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 113% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 87% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 93% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 110% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 108% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 134% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 110% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 78% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 90% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 98% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 77% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 126% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 130% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 104% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 119% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 69% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 81% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 81% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 93% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 114% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 96% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 76% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 92% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 88% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 78% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 131% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 149% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 01/18/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 12/27/16 Pct Recovery = 91% Analysis Date = 12/27/16 Pct Recovery = 91% Analysis Date = 12/16/16 Pct Recovery = 91% Analysis Date = 12/16/16 Pct Recovery = 91% Analysis Date = 12/05/16 Pct Recovery = 91% Analysis Date = 12/05/16 Pct Recovery = 91% Analysis Date = 11/24/16 Pct Recovery = 91% Analysis Date = 11/24/16 Pct Recovery = 91% Analysis Date = 11/14/16 Pct Recovery = 91% Analysis Date = 11/14/16 Pct Recovery = 91% Analysis Date = 11/03/16 Pct Recovery = 91% Analysis Date = 11/03/16 Pct Recovery = 91% Analysis Date = 10/23/16 Pct Recovery = 91% Analysis Date = 10/23/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/20/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/19/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 08/08/16 Pct Recovery = 91% Analysis Date = 07/28/16 Pct Recovery = 91% Analysis Date = 07/28/16 Pct Recovery = 91% Analysis Date = 07/17/16 Pct Recovery = 91% Analysis Date = 07/17/16 Pct Recovery = 91% Analysis Date = 07/07/16 Pct Recovery = 91% Analysis Date = 07/07/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/15/16 Pct Recovery = 91% Analysis Date = 06/15/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/03/16 Pct Recovery = 91% Analysis Date = 05/03/16 Pct Recovery = 91% Analysis Date = 04/22/16 Pct Recovery = 91% Analysis Date = 04/22/16 Pct Recovery = 91% Analysis Date = 04/11/16 Pct Recovery = 91% Analysis Date = 04/11/16 Pct Recovery = 91% Analysis Date = 03/31/16 Pct Recovery = 91% Analysis Date = 03/31/16 Pct Recovery = 91% Analysis Date = 03/20/16 Pct Recovery = 91% Analysis Date = 03/20/16 Pct Recovery = 91% Analysis Date = 03/10/16 Pct Recovery = 91% Analysis Date = 03/10/16 Pct Recovery = 91% Analysis Date = 02/28/16 Pct Recovery = 91% Analysis Date = 02/28/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/06/16 Pct Recovery = 91% Analysis Date = 02/06/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 11/22/15 Pct Recovery = 91% Analysis Date = 11/22/15 Pct Recovery = 91% Analysis Date = 11/12/15 Pct Recovery = 91% Analysis Date = 11/12/15 Pct Recovery = 91% Analysis Date = 11/01/15 Pct Recovery = 91% Analysis Date = 11/01/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 91% Analysis Date = 10/21/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 10/10/15 Pct Recovery = 91% Analysis Date = 09/29/15 Pct Recovery = 91% Analysis Date = 09/29/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/18/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 09/08/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/28/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 91% Analysis Date = 08/17/15 Pct Recovery = 91% Analysis Date = 08/06/15 Pct Recovery = 91% Analysis Date = 08/06/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/26/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 05/22/15 Pct Recovery = 91% Analysis Date = 05/22/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/09/15 Pct Recovery = 91% Analysis Date = 04/09/15 Pct Recovery = 91% Analysis Date = 03/29/15 Pct Recovery = 91% Analysis Date = 03/29/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 02/25/15 Pct Recovery = 91% Analysis Date = 02/25/15 Pct Recovery = 91% Analysis Date = 02/14/15 Pct Recovery = 91% Analysis Date = 02/14/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 01/23/15 Pct Recovery = 91% Analysis Date = 01/23/15 Pct Recovery = 91% Analysis Date = 01/12/15 Pct Recovery = 91% Analysis Date = 01/12/15 Pct Recovery = 91% Analysis Date = 01/02/15 Pct Recovery = 91% Analysis Date = 01/02/15 Pct Recovery = 91% Analysis Date = 12/22/14 Pct Recovery = 91% Analysis Date = 12/22/14 Pct Recovery = 91% Analysis Date = 12/11/14 Pct Recovery = 91% Analysis Date = 12/11/14 Pct Recovery = 91% Analysis Date = 11/30/14 Pct Recovery = 91% Analysis Date = 11/30/14 Pct Recovery = 91% Analysis Date = 11/19/14 Pct Recovery = 91% Analysis Date = 11/19/14 Pct Recovery = 91% Analysis Date = 11/08/14 Pct Recovery = 91% Analysis Date = 11/08/14 Pct Recovery = 91% Analysis Date = 10/29/14 Pct Recovery = 91% Analysis Date = 10/29/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/07/14 Pct Recovery = 91% Analysis Date = 10/07/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 91% Analysis Date = 08/25/14 Pct Recovery = 91% Analysis Date = 08/25/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/14/14 Pct Recovery = 91% Analysis Date = 08/03/14 Pct Recovery = 91% Analysis Date = 08/03/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/23/14 Pct Recovery = 91% Analysis Date = 07/12/14 Pct Recovery = 91% Analysis Date = 07/12/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/21/14 Pct Recovery = 91% Analysis Date = 06/21/14 Pct Recovery = 91% Analysis Date = 06/10/14 Pct Recovery = 91% Analysis Date = 06/10/14 Pct Recovery = 91% Analysis Date = 05/30/14 Pct Recovery = 91% Analysis Date = 05/30/14 Pct Recovery = 91% Analysis Date = 05/19/14 Pct Recovery = 91% Analysis Date = 05/19/14 Pct Recovery = 91% Analysis Date = 05/08/14 Pct Recovery = 91% Analysis Date = 05/08/14 Pct Recovery = 91% Analysis Date = 04/28/14 Pct Recovery = 90% Analysis Date = 04/28/14 Pct Recovery = 90% Analysis Date = 04/17/14 Pct Recovery = 90% Analysis Date = 04/17/14 Pct Recovery = 90% Analysis Date = 04/06/14 Pct Recovery = 90% Analysis Date = 04/06/14 Pct Recovery = 90% Analysis Date = 03/26/14 Pct Recovery = 90% Analysis Date = 03/26/14 Pct Recovery = 90% Analysis Date = 03/15/14 Pct Recovery = 90% Analysis Date = 03/15/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 90% Analysis Date = 03/04/14 Pct Recovery = 90% Analysis Date = 02/22/14 Pct Recovery = 90% Analysis Date = 02/22/14 Pct Recovery = 90% Analysis Date = 02/11/14 Pct Recovery = 90% Analysis Date = 02/11/14 Pct Recovery = 90% Analysis Date = 01/31/14 Pct Recovery = 90% Analysis Date = 01/31/14 Pct Recovery = 90% Analysis Date = 01/20/14 Pct Recovery = 90% Analysis Date = 01/20/14 Pct Recovery = 90% Analysis Date = 01/09/14 Pct Recovery = 90% Analysis Date = 01/09/14 Pct Recovery = 90% Analysis Date = 12/30/13 Pct Recovery = 90% Analysis Date = 12/30/13 Pct Recovery = 90% Analysis Date = 12/19/13 Pct Recovery = 90% Analysis Date = 12/19/13 Pct Recovery = 90% Analysis Date = 12/08/13 Pct Recovery = 90% Analysis Date = 12/08/13 Pct Recovery = 90% Analysis Date = 11/27/13 Pct Recovery = 90% Analysis Date = 11/27/13 Pct Recovery = 90% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 90% Analysis Date = 10/26/13 Pct Recovery = 90% Analysis Date = 10/26/13 Pct Recovery = 90% Analysis Date = 10/15/13 Pct Recovery = 90% Analysis Date = 10/15/13 Pct Recovery = 90% Analysis Date = 10/04/13 Pct Recovery = 90% Analysis Date = 10/04/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 08/22/13 Pct Recovery = 90% Analysis Date = 08/22/13 Pct Recovery = 90% Analysis Date = 08/11/13 Pct Recovery = 90% Analysis Date = 08/11/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 90% Analysis Date = 07/31/13 Pct Recovery = 90% Analysis Date = 07/20/13 Pct Recovery = 90% Analysis Date = 07/20/13 Pct Recovery = 90% Analysis Date = 07/09/13 Pct Recovery = 91% Analysis Date = 07/09/13 Pct Recovery = 91% Analysis Date = 06/29/13 Pct Recovery = 91% Analysis Date = 06/29/13 Pct Recovery = 91% Analysis Date = 06/18/13 Pct Recovery = 91% Analysis Date = 06/18/13 Pct Recovery = 91% Analysis Date = 06/07/13 Pct Recovery = 91% Analysis Date = 06/07/13 Pct Recovery = 91% Analysis Date = 05/27/13 Pct Recovery = 91% Analysis Date = 05/27/13 Pct Recovery = 91% Analysis Date = 05/16/13 Pct Recovery = 91% Analysis Date = 05/16/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 04/25/13 Pct Recovery = 91% Analysis Date = 04/25/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/03/13 Pct Recovery = 92% Analysis Date = 04/03/13 Pct Recovery = 92% Analysis Date = 03/23/13 Pct Recovery = 92% Analysis Date = 03/23/13 Pct Recovery = 92% Analysis Date = 03/12/13 Pct Recovery = 92% Analysis Date = 03/12/13 Pct Recovery = 92% Analysis Date = 03/01/13 Pct Recovery = 92% Analysis Date = 03/01/13 Pct Recovery = 92% Analysis Date = 02/19/13 Pct Recovery = 92% Analysis Date = 02/19/13 Pct Recovery = 92% Analysis Date = 02/08/13 Pct Recovery = 92% Analysis Date = 02/08/13 Pct Recovery = 92% Analysis Date = 01/28/13 Pct Recovery = 92% Analysis Date = 01/28/13 Pct Recovery = 92% Analysis Date = 01/17/13 Pct Recovery = 92% Analysis Date = 01/17/13 Pct Recovery = 92% Analysis Date = 01/06/13 Pct Recovery = 93% Analysis Date = 01/06/13 Pct Recovery = 93% Analysis Date = 12/26/12 Pct Recovery = 93% Analysis Date = 12/26/12 Pct Recovery = 93% Analysis Date = 12/16/12 Pct Recovery = 93% Analysis Date = 12/16/12 Pct Recovery = 93% Analysis Date = 12/05/12 Pct Recovery = 93% Analysis Date = 12/05/12 Pct Recovery = 93% Analysis Date = 11/24/12 Pct Recovery = 93% Analysis Date = 11/24/12 Pct Recovery = 93% Analysis Date = 11/13/12 Pct Recovery = 93% Analysis Date = 11/13/12 Pct Recovery = 93% Analysis Date = 11/02/12 Pct Recovery = 94% Analysis Date = 11/02/12 Pct Recovery = 94% Analysis Date = 10/23/12 Pct Recovery = 94% Analysis Date = 10/23/12 Pct Recovery = 94% Analysis Date = 10/12/12 Pct Recovery = 94% Analysis Date = 10/12/12 Pct Recovery = 94% Analysis Date = 10/01/12 Pct Recovery = 94% Analysis Date = 10/01/12 Pct Recovery = 94% Analysis Date = 09/20/12 Pct Recovery = 94% Analysis Date = 09/20/12 Pct Recovery = 94% Analysis Date = 09/09/12 Pct Recovery = 94% Analysis Date = 09/09/12 Pct Recovery = 94% Analysis Date = 08/29/12 Pct Recovery = 95% Analysis Date = 08/29/12 Pct Recovery = 95% Analysis Date = 08/19/12 Pct Recovery = 95% Analysis Date = 08/19/12 Pct Recovery = 95% Analysis Date = 08/08/12 Pct Recovery = 95% Analysis Date = 08/08/12 Pct Recovery = 95% Analysis Date = 07/28/12 Pct Recovery = 95% Analysis Date = 07/28/12 Pct Recovery = 95% Analysis Date = 07/17/12 Pct Recovery = 96% Analysis Date = 07/17/12 Pct Recovery = 96% Analysis Date = 07/06/12 Pct Recovery = 96% Analysis Date = 07/06/12 Pct Recovery = 96% Analysis Date = 06/25/12 Pct Recovery = 96% Analysis Date = 06/25/12 Pct Recovery = 96% Analysis Date = 06/15/12 Pct Recovery = 96% Analysis Date = 06/15/12 Pct Recovery = 96% Analysis Date = 06/04/12 Pct Recovery = 97% Analysis Date = 06/04/12 Pct Recovery = 97% Analysis Date = 05/24/12 Pct Recovery = 97% Analysis Date = 05/24/12 Pct Recovery = 97% Analysis Date = 05/13/12 Pct Recovery = 97% Analysis Date = 05/13/12 Pct Recovery = 97% Analysis Date = 05/02/12 Pct Recovery = 97% Analysis Date = 05/02/12 Pct Recovery = 97% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 98% Analysis Date = 03/20/12 Pct Recovery = 98% Analysis Date = 03/20/12 Pct Recovery = 98% Analysis Date = 03/09/12 Pct Recovery = 99% Analysis Date = 03/09/12 Pct Recovery = 99% Analysis Date = 02/27/12 Pct Recovery = 99% Analysis Date = 02/27/12 Pct Recovery = 99% Analysis Date = 02/17/12 Pct Recovery = 99% Analysis Date = 02/17/12 Pct Recovery = 99% Analysis Date = 02/06/12 Pct Recovery = 99% Analysis Date = 02/06/12 Pct Recovery = 99% Analysis Date = 01/26/12 Pct Recovery = 100% Analysis Date = 01/26/12 Pct Recovery = 100% Analysis Date = 01/15/12 Pct Recovery = 100% Analysis Date = 01/15/12 Pct Recovery = 100% Analysis Date = 01/04/12 Pct Recovery = 100% Analysis Date = 01/04/12 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/14/11 Pct Recovery = 101% Analysis Date = 12/14/11 Pct Recovery = 101% Analysis Date = 12/03/11 Pct Recovery = 101% Analysis Date = 12/03/11 Pct Recovery = 101% Analysis Date = 11/22/11 Pct Recovery = 101% Analysis Date = 11/22/11 Pct Recovery = 101% Analysis Date = 11/11/11 Pct Recovery = 101% Analysis Date = 11/11/11 Pct Recovery = 101% Analysis Date = 10/31/11 Pct Recovery = 102% Analysis Date = 10/31/11 Pct Recovery = 102% Analysis Date = 10/20/11 Pct Recovery = 102% Analysis Date = 10/20/11 Pct Recovery = 102% Analysis Date = 10/10/11 Pct Recovery = 102% Analysis Date = 10/10/11 Pct Recovery = 102% Analysis Date = 09/29/11 Pct Recovery = 102% Analysis Date = 09/29/11 Pct Recovery = 102% Analysis Date = 09/18/11 Pct Recovery = 103% Analysis Date = 09/18/11 Pct Recovery = 103% Analysis Date = 09/07/11 Pct Recovery = 103% Analysis Date = 09/07/11 Pct Recovery = 103% Analysis Date = 08/27/11 Pct Recovery = 103% Analysis Date = 08/27/11 Pct Recovery = 103% Analysis Date = 08/17/11 Pct Recovery = 103% Analysis Date = 08/17/11 Pct Recovery = 103% Analysis Date = 08/06/11 Pct Recovery = 104% Analysis Date = 08/06/11 Pct Recovery = 104% Analysis Date = 07/26/11 Pct Recovery = 104% Analysis Date = 07/26/11 Pct Recovery = 104% Analysis Date = 07/15/11 Pct Recovery = 104% Analysis Date = 07/15/11 Pct Recovery = 104% Analysis Date = 07/04/11 Pct Recovery = 104% Analysis Date = 07/04/11 Pct Recovery = 104% Analysis Date = 06/23/11 Pct Recovery = 105% Analysis Date = 06/23/11 Pct Recovery = 105% Analysis Date = 06/13/11 Pct Recovery = 105% Analysis Date = 06/13/11 Pct Recovery = 105% Analysis Date = 06/02/11 Pct Recovery = 105% Analysis Date = 06/02/11 Pct Recovery = 105% Analysis Date = 05/22/11 Pct Recovery = 105% Analysis Date = 05/22/11 Pct Recovery = 105% Analysis Date = 05/11/11 Pct Recovery = 106% Analysis Date = 05/11/11 Pct Recovery = 106% Analysis Date = 04/30/11 Pct Recovery = 106% Analysis Date = 04/30/11 Pct Recovery = 106% Analysis Date = 04/19/11 Pct Recovery = 106% Analysis Date = 04/19/11 Pct Recovery = 106% Analysis Date = 04/09/11 Pct Recovery = 106% Analysis Date = 04/09/11 Pct Recovery = 106% Analysis Date = 03/29/11 Pct Recovery = 107% Analysis Date = 03/29/11 Pct Recovery = 107% Analysis Date = 03/18/11 Pct Recovery = 107% Analysis Date = 03/18/11 Pct Recovery = 107% Analysis Date = 03/07/11 Pct Recovery = 107% Analysis Date = 03/07/11 Pct Recovery = 107% Analysis Date = 02/24/11 Pct Recovery = 107% Analysis Date = 02/24/11 Pct Recovery = 107% Analysis Date = 02/14/11 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METALAXYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 94% 17% 93% 16%
Total 87 94% 17% 93% 16%

Sample Statistics
METALAXYL

Characteristic N % % Basis
Plotted 87 99% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 88 .  
False Negatives 1 1% 1 out of 88
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

BQS OBSP Determination:
METHIDATHION (SUPRACIDE)
METHOD: 2033 , TESTIDCODE: 61598GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 73% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 79% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 83% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 83% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 74% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 102% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 79% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 68% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 76% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 86% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 71% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 97% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 85% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 79% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 76% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 85% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 116% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 77% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 76% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 94% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 93% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 85% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 105% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 90% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 104% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 78% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 90% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 119% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 105% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 84% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 79% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 85% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 99% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 127% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 72% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 59% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 95% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 102% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 84% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 99% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 107% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 105% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 95% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 81% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 103% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 104% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 125% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 99% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 94% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 85% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 87% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 136% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 98% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 90% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 97% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 128% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 89% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 103% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 102% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 73% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 114% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 127% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 72% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 190% Analysis Date = 01/18/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 11/24/16 Pct Recovery = 87% Analysis Date = 11/24/16 Pct Recovery = 87% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 10/23/16 Pct Recovery = 88% Analysis Date = 10/23/16 Pct Recovery = 88% Analysis Date = 10/12/16 Pct Recovery = 88% Analysis Date = 10/12/16 Pct Recovery = 88% Analysis Date = 10/01/16 Pct Recovery = 88% Analysis Date = 10/01/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/14/16 Pct Recovery = 90% Analysis Date = 05/14/16 Pct Recovery = 90% Analysis Date = 05/03/16 Pct Recovery = 90% Analysis Date = 05/03/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/11/16 Pct Recovery = 90% Analysis Date = 04/11/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 91% Analysis Date = 03/10/16 Pct Recovery = 91% Analysis Date = 02/28/16 Pct Recovery = 91% Analysis Date = 02/28/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/06/16 Pct Recovery = 91% Analysis Date = 02/06/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 11/22/15 Pct Recovery = 92% Analysis Date = 11/22/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 06/24/15 Pct Recovery = 93% Analysis Date = 06/24/15 Pct Recovery = 93% Analysis Date = 06/13/15 Pct Recovery = 93% Analysis Date = 06/13/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 05/22/15 Pct Recovery = 93% Analysis Date = 05/22/15 Pct Recovery = 93% Analysis Date = 05/11/15 Pct Recovery = 93% Analysis Date = 05/11/15 Pct Recovery = 93% Analysis Date = 05/01/15 Pct Recovery = 93% Analysis Date = 05/01/15 Pct Recovery = 93% Analysis Date = 04/20/15 Pct Recovery = 94% Analysis Date = 04/20/15 Pct Recovery = 94% Analysis Date = 04/09/15 Pct Recovery = 94% Analysis Date = 04/09/15 Pct Recovery = 94% Analysis Date = 03/29/15 Pct Recovery = 94% Analysis Date = 03/29/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/08/15 Pct Recovery = 94% Analysis Date = 03/08/15 Pct Recovery = 94% Analysis Date = 02/25/15 Pct Recovery = 94% Analysis Date = 02/25/15 Pct Recovery = 94% Analysis Date = 02/14/15 Pct Recovery = 94% Analysis Date = 02/14/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/23/15 Pct Recovery = 95% Analysis Date = 01/23/15 Pct Recovery = 95% Analysis Date = 01/12/15 Pct Recovery = 95% Analysis Date = 01/12/15 Pct Recovery = 95% Analysis Date = 01/02/15 Pct Recovery = 95% Analysis Date = 01/02/15 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 11/30/14 Pct Recovery = 96% Analysis Date = 11/30/14 Pct Recovery = 96% Analysis Date = 11/19/14 Pct Recovery = 96% Analysis Date = 11/19/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 10/29/14 Pct Recovery = 96% Analysis Date = 10/29/14 Pct Recovery = 96% Analysis Date = 10/18/14 Pct Recovery = 96% Analysis Date = 10/18/14 Pct Recovery = 96% Analysis Date = 10/07/14 Pct Recovery = 96% Analysis Date = 10/07/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 08/25/14 Pct Recovery = 96% Analysis Date = 08/25/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/03/14 Pct Recovery = 96% Analysis Date = 08/03/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/12/14 Pct Recovery = 96% Analysis Date = 07/12/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 06/21/14 Pct Recovery = 96% Analysis Date = 06/21/14 Pct Recovery = 96% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 95% Analysis Date = 05/08/14 Pct Recovery = 94% Analysis Date = 05/08/14 Pct Recovery = 94% Analysis Date = 04/28/14 Pct Recovery = 94% Analysis Date = 04/28/14 Pct Recovery = 94% Analysis Date = 04/17/14 Pct Recovery = 94% Analysis Date = 04/17/14 Pct Recovery = 94% Analysis Date = 04/06/14 Pct Recovery = 94% Analysis Date = 04/06/14 Pct Recovery = 94% Analysis Date = 03/26/14 Pct Recovery = 93% Analysis Date = 03/26/14 Pct Recovery = 93% Analysis Date = 03/15/14 Pct Recovery = 93% Analysis Date = 03/15/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 02/22/14 Pct Recovery = 93% Analysis Date = 02/22/14 Pct Recovery = 93% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 01/31/14 Pct Recovery = 92% Analysis Date = 01/31/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/09/14 Pct Recovery = 92% Analysis Date = 01/09/14 Pct Recovery = 92% Analysis Date = 12/30/13 Pct Recovery = 91% Analysis Date = 12/30/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 90% Analysis Date = 10/26/13 Pct Recovery = 90% Analysis Date = 10/26/13 Pct Recovery = 90% Analysis Date = 10/15/13 Pct Recovery = 90% Analysis Date = 10/15/13 Pct Recovery = 90% Analysis Date = 10/04/13 Pct Recovery = 90% Analysis Date = 10/04/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/11/13 Pct Recovery = 89% Analysis Date = 08/11/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/09/13 Pct Recovery = 89% Analysis Date = 07/09/13 Pct Recovery = 89% Analysis Date = 06/29/13 Pct Recovery = 89% Analysis Date = 06/29/13 Pct Recovery = 89% Analysis Date = 06/18/13 Pct Recovery = 89% Analysis Date = 06/18/13 Pct Recovery = 89% Analysis Date = 06/07/13 Pct Recovery = 89% Analysis Date = 06/07/13 Pct Recovery = 89% Analysis Date = 05/27/13 Pct Recovery = 89% Analysis Date = 05/27/13 Pct Recovery = 89% Analysis Date = 05/16/13 Pct Recovery = 89% Analysis Date = 05/16/13 Pct Recovery = 89% Analysis Date = 05/05/13 Pct Recovery = 89% Analysis Date = 05/05/13 Pct Recovery = 89% Analysis Date = 04/25/13 Pct Recovery = 88% Analysis Date = 04/25/13 Pct Recovery = 88% Analysis Date = 04/14/13 Pct Recovery = 88% Analysis Date = 04/14/13 Pct Recovery = 88% Analysis Date = 04/03/13 Pct Recovery = 88% Analysis Date = 04/03/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/01/13 Pct Recovery = 88% Analysis Date = 03/01/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 88% Analysis Date = 10/12/12 Pct Recovery = 87% Analysis Date = 10/12/12 Pct Recovery = 87% Analysis Date = 10/01/12 Pct Recovery = 88% Analysis Date = 10/01/12 Pct Recovery = 88% Analysis Date = 09/20/12 Pct Recovery = 88% Analysis Date = 09/20/12 Pct Recovery = 88% Analysis Date = 09/09/12 Pct Recovery = 88% Analysis Date = 09/09/12 Pct Recovery = 88% Analysis Date = 08/29/12 Pct Recovery = 88% Analysis Date = 08/29/12 Pct Recovery = 88% Analysis Date = 08/19/12 Pct Recovery = 88% Analysis Date = 08/19/12 Pct Recovery = 88% Analysis Date = 08/08/12 Pct Recovery = 88% Analysis Date = 08/08/12 Pct Recovery = 88% Analysis Date = 07/28/12 Pct Recovery = 88% Analysis Date = 07/28/12 Pct Recovery = 88% Analysis Date = 07/17/12 Pct Recovery = 88% Analysis Date = 07/17/12 Pct Recovery = 88% Analysis Date = 07/06/12 Pct Recovery = 88% Analysis Date = 07/06/12 Pct Recovery = 88% Analysis Date = 06/25/12 Pct Recovery = 88% Analysis Date = 06/25/12 Pct Recovery = 88% Analysis Date = 06/15/12 Pct Recovery = 88% Analysis Date = 06/15/12 Pct Recovery = 88% Analysis Date = 06/04/12 Pct Recovery = 88% Analysis Date = 06/04/12 Pct Recovery = 88% Analysis Date = 05/24/12 Pct Recovery = 88% Analysis Date = 05/24/12 Pct Recovery = 88% Analysis Date = 05/13/12 Pct Recovery = 88% Analysis Date = 05/13/12 Pct Recovery = 88% Analysis Date = 05/02/12 Pct Recovery = 88% Analysis Date = 05/02/12 Pct Recovery = 88% Analysis Date = 04/22/12 Pct Recovery = 88% Analysis Date = 04/22/12 Pct Recovery = 88% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/09/12 Pct Recovery = 89% Analysis Date = 03/09/12 Pct Recovery = 89% Analysis Date = 02/27/12 Pct Recovery = 89% Analysis Date = 02/27/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/06/12 Pct Recovery = 89% Analysis Date = 02/06/12 Pct Recovery = 89% Analysis Date = 01/26/12 Pct Recovery = 89% Analysis Date = 01/26/12 Pct Recovery = 89% Analysis Date = 01/15/12 Pct Recovery = 89% Analysis Date = 01/15/12 Pct Recovery = 89% Analysis Date = 01/04/12 Pct Recovery = 89% Analysis Date = 01/04/12 Pct Recovery = 89% Analysis Date = 12/24/11 Pct Recovery = 89% Analysis Date = 12/24/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 89% Analysis Date = 12/03/11 Pct Recovery = 89% Analysis Date = 12/03/11 Pct Recovery = 89% Analysis Date = 11/22/11 Pct Recovery = 89% Analysis Date = 11/22/11 Pct Recovery = 89% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 10/31/11 Pct Recovery = 89% Analysis Date = 10/31/11 Pct Recovery = 89% Analysis Date = 10/20/11 Pct Recovery = 89% Analysis Date = 10/20/11 Pct Recovery = 89% Analysis Date = 10/10/11 Pct Recovery = 89% Analysis Date = 10/10/11 Pct Recovery = 89% Analysis Date = 09/29/11 Pct Recovery = 89% Analysis Date = 09/29/11 Pct Recovery = 89% Analysis Date = 09/18/11 Pct Recovery = 90% Analysis Date = 09/18/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 08/27/11 Pct Recovery = 90% Analysis Date = 08/27/11 Pct Recovery = 90% Analysis Date = 08/17/11 Pct Recovery = 90% Analysis Date = 08/17/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/15/11 Pct Recovery = 90% Analysis Date = 07/15/11 Pct Recovery = 90% Analysis Date = 07/04/11 Pct Recovery = 90% Analysis Date = 07/04/11 Pct Recovery = 90% Analysis Date = 06/23/11 Pct Recovery = 90% Analysis Date = 06/23/11 Pct Recovery = 90% Analysis Date = 06/13/11 Pct Recovery = 90% Analysis Date = 06/13/11 Pct Recovery = 90% Analysis Date = 06/02/11 Pct Recovery = 90% Analysis Date = 06/02/11 Pct Recovery = 90% Analysis Date = 05/22/11 Pct Recovery = 90% Analysis Date = 05/22/11 Pct Recovery = 90% Analysis Date = 05/11/11 Pct Recovery = 90% Analysis Date = 05/11/11 Pct Recovery = 90% Analysis Date = 04/30/11 Pct Recovery = 90% Analysis Date = 04/30/11 Pct Recovery = 90% Analysis Date = 04/19/11 Pct Recovery = 90% Analysis Date = 04/19/11 Pct Recovery = 90% Analysis Date = 04/09/11 Pct Recovery = 90% Analysis Date = 04/09/11 Pct Recovery = 90% Analysis Date = 03/29/11 Pct Recovery = 90% Analysis Date = 03/29/11 Pct Recovery = 90% Analysis Date = 03/18/11 Pct Recovery = 90% Analysis Date = 03/18/11 Pct Recovery = 90% Analysis Date = 03/07/11 Pct Recovery = 91% Analysis Date = 03/07/11 Pct Recovery = 91% Analysis Date = 02/24/11 Pct Recovery = 91% Analysis Date = 02/24/11 Pct Recovery = 91% Analysis Date = 02/14/11 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHIDATHION (SUPRACIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 91% 19% 87% 14%
Total 89 91% 19% 87% 14%

Sample Statistics
METHIDATHION (SUPRACIDE)

Characteristic N % % Basis
Plotted 89 99% Spiked
Estimated Values 6 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 90 .  
False Negatives 1 1% 1 out of 90
Not Spiked 79 .  
False Positives 0 0% 0 out of 79

BQS OBSP Determination:
METOLACHLOR
METHOD: 2033 , TESTIDCODE: 39415GCM35
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 100% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 99% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 87% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 104% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 93% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 92% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 92% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 116% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 79% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 90% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 75% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 73% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 86% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 95% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 84% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 97% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 69% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 92% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 72% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 90% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 86% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 116% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 78% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 89% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 66% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 70% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 93% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 98% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 86% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 83% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 66% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 112% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 86% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 85% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 109% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 75% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 83% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 69% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 69% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 76% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 71% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 72% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 72% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 67% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 121% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 83% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 125% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 87% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 82% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 95% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 82% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 76% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 70% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 85% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 88% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 89% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 73% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 67% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 83% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 107% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 108% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 84% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 112% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 74% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 90% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 90% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 103% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 81% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 88% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 73% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 86% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 94% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 72% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 88% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 92% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 81% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 84% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 86% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 73% Analysis Date = 01/17/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 12/27/16 Pct Recovery = 88% Analysis Date = 12/27/16 Pct Recovery = 88% Analysis Date = 12/16/16 Pct Recovery = 88% Analysis Date = 12/16/16 Pct Recovery = 88% Analysis Date = 12/05/16 Pct Recovery = 88% Analysis Date = 12/05/16 Pct Recovery = 88% Analysis Date = 11/24/16 Pct Recovery = 88% Analysis Date = 11/24/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/09/16 Pct Recovery = 87% Analysis Date = 09/09/16 Pct Recovery = 87% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/14/16 Pct Recovery = 85% Analysis Date = 06/14/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/02/16 Pct Recovery = 85% Analysis Date = 05/02/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 84% Analysis Date = 03/30/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 84% Analysis Date = 03/09/16 Pct Recovery = 84% Analysis Date = 03/09/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/16/16 Pct Recovery = 84% Analysis Date = 02/16/16 Pct Recovery = 84% Analysis Date = 02/05/16 Pct Recovery = 84% Analysis Date = 02/05/16 Pct Recovery = 84% Analysis Date = 01/25/16 Pct Recovery = 84% Analysis Date = 01/25/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/04/16 Pct Recovery = 83% Analysis Date = 01/04/16 Pct Recovery = 83% Analysis Date = 12/24/15 Pct Recovery = 83% Analysis Date = 12/24/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/13/15 Pct Recovery = 83% Analysis Date = 12/02/15 Pct Recovery = 83% Analysis Date = 12/02/15 Pct Recovery = 83% Analysis Date = 11/21/15 Pct Recovery = 83% Analysis Date = 11/21/15 Pct Recovery = 83% Analysis Date = 11/10/15 Pct Recovery = 83% Analysis Date = 11/10/15 Pct Recovery = 83% Analysis Date = 10/30/15 Pct Recovery = 83% Analysis Date = 10/30/15 Pct Recovery = 83% Analysis Date = 10/20/15 Pct Recovery = 83% Analysis Date = 10/20/15 Pct Recovery = 83% Analysis Date = 10/09/15 Pct Recovery = 82% Analysis Date = 10/09/15 Pct Recovery = 82% Analysis Date = 09/28/15 Pct Recovery = 82% Analysis Date = 09/28/15 Pct Recovery = 82% Analysis Date = 09/17/15 Pct Recovery = 82% Analysis Date = 09/17/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 09/06/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/26/15 Pct Recovery = 82% Analysis Date = 08/15/15 Pct Recovery = 82% Analysis Date = 08/15/15 Pct Recovery = 82% Analysis Date = 08/05/15 Pct Recovery = 82% Analysis Date = 08/05/15 Pct Recovery = 82% Analysis Date = 07/25/15 Pct Recovery = 82% Analysis Date = 07/25/15 Pct Recovery = 82% Analysis Date = 07/14/15 Pct Recovery = 82% Analysis Date = 07/14/15 Pct Recovery = 82% Analysis Date = 07/03/15 Pct Recovery = 82% Analysis Date = 07/03/15 Pct Recovery = 82% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/22/15 Pct Recovery = 81% Analysis Date = 06/11/15 Pct Recovery = 81% Analysis Date = 06/11/15 Pct Recovery = 81% Analysis Date = 05/31/15 Pct Recovery = 81% Analysis Date = 05/31/15 Pct Recovery = 81% Analysis Date = 05/21/15 Pct Recovery = 81% Analysis Date = 05/21/15 Pct Recovery = 81% Analysis Date = 05/10/15 Pct Recovery = 81% Analysis Date = 05/10/15 Pct Recovery = 81% Analysis Date = 04/29/15 Pct Recovery = 81% Analysis Date = 04/29/15 Pct Recovery = 81% Analysis Date = 04/18/15 Pct Recovery = 81% Analysis Date = 04/18/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 04/07/15 Pct Recovery = 81% Analysis Date = 03/27/15 Pct Recovery = 81% Analysis Date = 03/27/15 Pct Recovery = 81% Analysis Date = 03/16/15 Pct Recovery = 81% Analysis Date = 03/16/15 Pct Recovery = 81% Analysis Date = 03/06/15 Pct Recovery = 80% Analysis Date = 03/06/15 Pct Recovery = 80% Analysis Date = 02/23/15 Pct Recovery = 80% Analysis Date = 02/23/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/12/15 Pct Recovery = 80% Analysis Date = 02/01/15 Pct Recovery = 80% Analysis Date = 02/01/15 Pct Recovery = 80% Analysis Date = 01/21/15 Pct Recovery = 80% Analysis Date = 01/21/15 Pct Recovery = 80% Analysis Date = 01/10/15 Pct Recovery = 80% Analysis Date = 01/10/15 Pct Recovery = 80% Analysis Date = 12/31/14 Pct Recovery = 80% Analysis Date = 12/31/14 Pct Recovery = 80% Analysis Date = 12/20/14 Pct Recovery = 80% Analysis Date = 12/20/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 11/28/14 Pct Recovery = 80% Analysis Date = 11/28/14 Pct Recovery = 80% Analysis Date = 11/17/14 Pct Recovery = 80% Analysis Date = 11/17/14 Pct Recovery = 80% Analysis Date = 11/06/14 Pct Recovery = 80% Analysis Date = 11/06/14 Pct Recovery = 80% Analysis Date = 10/26/14 Pct Recovery = 80% Analysis Date = 10/26/14 Pct Recovery = 80% Analysis Date = 10/16/14 Pct Recovery = 80% Analysis Date = 10/16/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 09/24/14 Pct Recovery = 80% Analysis Date = 09/24/14 Pct Recovery = 80% Analysis Date = 09/13/14 Pct Recovery = 80% Analysis Date = 09/13/14 Pct Recovery = 80% Analysis Date = 09/02/14 Pct Recovery = 80% Analysis Date = 09/02/14 Pct Recovery = 80% Analysis Date = 08/22/14 Pct Recovery = 80% Analysis Date = 08/22/14 Pct Recovery = 80% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/01/14 Pct Recovery = 81% Analysis Date = 08/01/14 Pct Recovery = 81% Analysis Date = 07/21/14 Pct Recovery = 81% Analysis Date = 07/21/14 Pct Recovery = 81% Analysis Date = 07/10/14 Pct Recovery = 81% Analysis Date = 07/10/14 Pct Recovery = 81% Analysis Date = 06/29/14 Pct Recovery = 81% Analysis Date = 06/29/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/18/14 Pct Recovery = 81% Analysis Date = 06/07/14 Pct Recovery = 81% Analysis Date = 06/07/14 Pct Recovery = 81% Analysis Date = 05/27/14 Pct Recovery = 81% Analysis Date = 05/27/14 Pct Recovery = 81% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/06/14 Pct Recovery = 82% Analysis Date = 05/06/14 Pct Recovery = 82% Analysis Date = 04/25/14 Pct Recovery = 82% Analysis Date = 04/25/14 Pct Recovery = 82% Analysis Date = 04/14/14 Pct Recovery = 82% Analysis Date = 04/14/14 Pct Recovery = 82% Analysis Date = 04/03/14 Pct Recovery = 82% Analysis Date = 04/03/14 Pct Recovery = 82% Analysis Date = 03/23/14 Pct Recovery = 82% Analysis Date = 03/23/14 Pct Recovery = 82% Analysis Date = 03/12/14 Pct Recovery = 82% Analysis Date = 03/12/14 Pct Recovery = 82% Analysis Date = 03/02/14 Pct Recovery = 83% Analysis Date = 03/02/14 Pct Recovery = 83% Analysis Date = 02/19/14 Pct Recovery = 83% Analysis Date = 02/19/14 Pct Recovery = 83% Analysis Date = 02/08/14 Pct Recovery = 83% Analysis Date = 02/08/14 Pct Recovery = 83% Analysis Date = 01/28/14 Pct Recovery = 83% Analysis Date = 01/28/14 Pct Recovery = 83% Analysis Date = 01/17/14 Pct Recovery = 83% Analysis Date = 01/17/14 Pct Recovery = 83% Analysis Date = 01/06/14 Pct Recovery = 83% Analysis Date = 01/06/14 Pct Recovery = 83% Analysis Date = 12/26/13 Pct Recovery = 83% Analysis Date = 12/26/13 Pct Recovery = 83% Analysis Date = 12/16/13 Pct Recovery = 84% Analysis Date = 12/16/13 Pct Recovery = 84% Analysis Date = 12/05/13 Pct Recovery = 84% Analysis Date = 12/05/13 Pct Recovery = 84% Analysis Date = 11/24/13 Pct Recovery = 84% Analysis Date = 11/24/13 Pct Recovery = 84% Analysis Date = 11/13/13 Pct Recovery = 84% Analysis Date = 11/13/13 Pct Recovery = 84% Analysis Date = 11/02/13 Pct Recovery = 84% Analysis Date = 11/02/13 Pct Recovery = 84% Analysis Date = 10/22/13 Pct Recovery = 85% Analysis Date = 10/22/13 Pct Recovery = 85% Analysis Date = 10/11/13 Pct Recovery = 85% Analysis Date = 10/11/13 Pct Recovery = 85% Analysis Date = 10/01/13 Pct Recovery = 85% Analysis Date = 10/01/13 Pct Recovery = 85% Analysis Date = 09/20/13 Pct Recovery = 85% Analysis Date = 09/20/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 85% Analysis Date = 08/29/13 Pct Recovery = 86% Analysis Date = 08/29/13 Pct Recovery = 86% Analysis Date = 08/18/13 Pct Recovery = 86% Analysis Date = 08/18/13 Pct Recovery = 86% Analysis Date = 08/07/13 Pct Recovery = 86% Analysis Date = 08/07/13 Pct Recovery = 86% Analysis Date = 07/27/13 Pct Recovery = 86% Analysis Date = 07/27/13 Pct Recovery = 86% Analysis Date = 07/17/13 Pct Recovery = 86% Analysis Date = 07/17/13 Pct Recovery = 86% Analysis Date = 07/06/13 Pct Recovery = 87% Analysis Date = 07/06/13 Pct Recovery = 87% Analysis Date = 06/25/13 Pct Recovery = 87% Analysis Date = 06/25/13 Pct Recovery = 87% Analysis Date = 06/14/13 Pct Recovery = 87% Analysis Date = 06/14/13 Pct Recovery = 87% Analysis Date = 06/03/13 Pct Recovery = 87% Analysis Date = 06/03/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/12/13 Pct Recovery = 88% Analysis Date = 05/12/13 Pct Recovery = 88% Analysis Date = 05/02/13 Pct Recovery = 88% Analysis Date = 05/02/13 Pct Recovery = 88% Analysis Date = 04/21/13 Pct Recovery = 88% Analysis Date = 04/21/13 Pct Recovery = 88% Analysis Date = 04/10/13 Pct Recovery = 88% Analysis Date = 04/10/13 Pct Recovery = 88% Analysis Date = 03/30/13 Pct Recovery = 88% Analysis Date = 03/30/13 Pct Recovery = 88% Analysis Date = 03/19/13 Pct Recovery = 89% Analysis Date = 03/19/13 Pct Recovery = 89% Analysis Date = 03/08/13 Pct Recovery = 89% Analysis Date = 03/08/13 Pct Recovery = 89% Analysis Date = 02/25/13 Pct Recovery = 89% Analysis Date = 02/25/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 01/24/13 Pct Recovery = 89% Analysis Date = 01/24/13 Pct Recovery = 89% Analysis Date = 01/13/13 Pct Recovery = 89% Analysis Date = 01/13/13 Pct Recovery = 89% Analysis Date = 01/02/13 Pct Recovery = 89% Analysis Date = 01/02/13 Pct Recovery = 89% Analysis Date = 12/22/12 Pct Recovery = 89% Analysis Date = 12/22/12 Pct Recovery = 89% Analysis Date = 12/12/12 Pct Recovery = 90% Analysis Date = 12/12/12 Pct Recovery = 90% Analysis Date = 12/01/12 Pct Recovery = 90% Analysis Date = 12/01/12 Pct Recovery = 90% Analysis Date = 11/20/12 Pct Recovery = 90% Analysis Date = 11/20/12 Pct Recovery = 90% Analysis Date = 11/09/12 Pct Recovery = 90% Analysis Date = 11/09/12 Pct Recovery = 90% Analysis Date = 10/29/12 Pct Recovery = 90% Analysis Date = 10/29/12 Pct Recovery = 90% Analysis Date = 10/18/12 Pct Recovery = 90% Analysis Date = 10/18/12 Pct Recovery = 90% Analysis Date = 10/07/12 Pct Recovery = 90% Analysis Date = 10/07/12 Pct Recovery = 90% Analysis Date = 09/27/12 Pct Recovery = 90% Analysis Date = 09/27/12 Pct Recovery = 90% Analysis Date = 09/16/12 Pct Recovery = 90% Analysis Date = 09/16/12 Pct Recovery = 90% Analysis Date = 09/05/12 Pct Recovery = 90% Analysis Date = 09/05/12 Pct Recovery = 90% Analysis Date = 08/25/12 Pct Recovery = 90% Analysis Date = 08/25/12 Pct Recovery = 90% Analysis Date = 08/14/12 Pct Recovery = 90% Analysis Date = 08/14/12 Pct Recovery = 90% Analysis Date = 08/03/12 Pct Recovery = 90% Analysis Date = 08/03/12 Pct Recovery = 90% Analysis Date = 07/23/12 Pct Recovery = 90% Analysis Date = 07/23/12 Pct Recovery = 90% Analysis Date = 07/13/12 Pct Recovery = 90% Analysis Date = 07/13/12 Pct Recovery = 90% Analysis Date = 07/02/12 Pct Recovery = 90% Analysis Date = 07/02/12 Pct Recovery = 90% Analysis Date = 06/21/12 Pct Recovery = 89% Analysis Date = 06/21/12 Pct Recovery = 89% Analysis Date = 06/10/12 Pct Recovery = 89% Analysis Date = 06/10/12 Pct Recovery = 89% Analysis Date = 05/30/12 Pct Recovery = 89% Analysis Date = 05/30/12 Pct Recovery = 89% Analysis Date = 05/19/12 Pct Recovery = 89% Analysis Date = 05/19/12 Pct Recovery = 89% Analysis Date = 05/08/12 Pct Recovery = 89% Analysis Date = 05/08/12 Pct Recovery = 89% Analysis Date = 04/28/12 Pct Recovery = 89% Analysis Date = 04/28/12 Pct Recovery = 89% Analysis Date = 04/17/12 Pct Recovery = 89% Analysis Date = 04/17/12 Pct Recovery = 89% Analysis Date = 04/06/12 Pct Recovery = 89% Analysis Date = 04/06/12 Pct Recovery = 89% Analysis Date = 03/26/12 Pct Recovery = 89% Analysis Date = 03/26/12 Pct Recovery = 89% Analysis Date = 03/15/12 Pct Recovery = 89% Analysis Date = 03/15/12 Pct Recovery = 89% Analysis Date = 03/04/12 Pct Recovery = 89% Analysis Date = 03/04/12 Pct Recovery = 89% Analysis Date = 02/22/12 Pct Recovery = 89% Analysis Date = 02/22/12 Pct Recovery = 89% Analysis Date = 02/12/12 Pct Recovery = 89% Analysis Date = 02/12/12 Pct Recovery = 89% Analysis Date = 02/01/12 Pct Recovery = 89% Analysis Date = 02/01/12 Pct Recovery = 89% Analysis Date = 01/21/12 Pct Recovery = 88% Analysis Date = 01/21/12 Pct Recovery = 88% Analysis Date = 01/10/12 Pct Recovery = 88% Analysis Date = 01/10/12 Pct Recovery = 88% Analysis Date = 12/30/11 Pct Recovery = 88% Analysis Date = 12/30/11 Pct Recovery = 88% Analysis Date = 12/19/11 Pct Recovery = 88% Analysis Date = 12/19/11 Pct Recovery = 88% Analysis Date = 12/08/11 Pct Recovery = 88% Analysis Date = 12/08/11 Pct Recovery = 88% Analysis Date = 11/28/11 Pct Recovery = 88% Analysis Date = 11/28/11 Pct Recovery = 88% Analysis Date = 11/17/11 Pct Recovery = 88% Analysis Date = 11/17/11 Pct Recovery = 88% Analysis Date = 11/06/11 Pct Recovery = 88% Analysis Date = 11/06/11 Pct Recovery = 88% Analysis Date = 10/26/11 Pct Recovery = 88% Analysis Date = 10/26/11 Pct Recovery = 88% Analysis Date = 10/15/11 Pct Recovery = 88% Analysis Date = 10/15/11 Pct Recovery = 88% Analysis Date = 10/04/11 Pct Recovery = 88% Analysis Date = 10/04/11 Pct Recovery = 88% Analysis Date = 09/23/11 Pct Recovery = 88% Analysis Date = 09/23/11 Pct Recovery = 88% Analysis Date = 09/13/11 Pct Recovery = 87% Analysis Date = 09/13/11 Pct Recovery = 87% Analysis Date = 09/02/11 Pct Recovery = 87% Analysis Date = 09/02/11 Pct Recovery = 87% Analysis Date = 08/22/11 Pct Recovery = 87% Analysis Date = 08/22/11 Pct Recovery = 87% Analysis Date = 08/11/11 Pct Recovery = 87% Analysis Date = 08/11/11 Pct Recovery = 87% Analysis Date = 07/31/11 Pct Recovery = 87% Analysis Date = 07/31/11 Pct Recovery = 87% Analysis Date = 07/20/11 Pct Recovery = 87% Analysis Date = 07/20/11 Pct Recovery = 87% Analysis Date = 07/09/11 Pct Recovery = 87% Analysis Date = 07/09/11 Pct Recovery = 87% Analysis Date = 06/29/11 Pct Recovery = 87% Analysis Date = 06/29/11 Pct Recovery = 87% Analysis Date = 06/18/11 Pct Recovery = 87% Analysis Date = 06/18/11 Pct Recovery = 87% Analysis Date = 06/07/11 Pct Recovery = 87% Analysis Date = 06/07/11 Pct Recovery = 87% Analysis Date = 05/27/11 Pct Recovery = 86% Analysis Date = 05/27/11 Pct Recovery = 86% Analysis Date = 05/16/11 Pct Recovery = 86% Analysis Date = 05/16/11 Pct Recovery = 86% Analysis Date = 05/05/11 Pct Recovery = 86% Analysis Date = 05/05/11 Pct Recovery = 86% Analysis Date = 04/24/11 Pct Recovery = 86% Analysis Date = 04/24/11 Pct Recovery = 86% Analysis Date = 04/14/11 Pct Recovery = 86% Analysis Date = 04/14/11 Pct Recovery = 86% Analysis Date = 04/03/11 Pct Recovery = 86% Analysis Date = 04/03/11 Pct Recovery = 86% Analysis Date = 03/23/11 Pct Recovery = 86% Analysis Date = 03/23/11 Pct Recovery = 86% Analysis Date = 03/12/11 Pct Recovery = 86% Analysis Date = 03/12/11 Pct Recovery = 86% Analysis Date = 03/01/11 Pct Recovery = 85% Analysis Date = 03/01/11 Pct Recovery = 85% Analysis Date = 02/18/11 Pct Recovery = 85% Analysis Date = 02/18/11 Pct Recovery = 85% Analysis Date = 02/08/11 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOLACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 96 85% 13% 85% 13%
Total 96 85% 13% 85% 13%

Sample Statistics
METOLACHLOR

Characteristic N % % Basis
Plotted 96 100% Spiked
Estimated Values 5 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 96 .  
False Negatives 0 0% 0 out of 96
Not Spiked 73 .  
False Positives 0 0% 0 out of 73

BQS OBSP Determination:
METRIBUZIN
METHOD: 2033 , TESTIDCODE: 82630GCM35
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 62% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 74% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 80% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 58% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 75% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 96% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 84% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 35% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 64% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 79% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 76% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 88% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 81% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 69% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 80% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 28% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 63% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 77% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 27% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 86% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 70% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 64% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 66% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 101% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 67% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 81% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 59% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 53% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 94% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 116% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 100% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 59% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 68% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 97% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 106% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 100% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 107% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 93% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 83% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 73% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 100% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 108% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 64% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 77% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 69% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 70% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 90% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 105% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 97% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 78% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 92% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 71% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 81% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 93% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 79% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 93% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 86% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 79% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 111% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 82% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 109% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 87% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 90% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 93% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 107% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 124% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 100% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 94% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 111% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 73% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 116% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 119% Analysis Date = 01/17/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/05/16 Pct Recovery = 75% Analysis Date = 12/05/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/03/16 Pct Recovery = 75% Analysis Date = 11/03/16 Pct Recovery = 75% Analysis Date = 10/23/16 Pct Recovery = 75% Analysis Date = 10/23/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 75% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/09/16 Pct Recovery = 75% Analysis Date = 09/09/16 Pct Recovery = 75% Analysis Date = 08/29/16 Pct Recovery = 76% Analysis Date = 08/29/16 Pct Recovery = 76% Analysis Date = 08/19/16 Pct Recovery = 76% Analysis Date = 08/19/16 Pct Recovery = 76% Analysis Date = 08/08/16 Pct Recovery = 76% Analysis Date = 08/08/16 Pct Recovery = 76% Analysis Date = 07/28/16 Pct Recovery = 76% Analysis Date = 07/28/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 76% Analysis Date = 06/14/16 Pct Recovery = 76% Analysis Date = 06/14/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 76% Analysis Date = 05/24/16 Pct Recovery = 76% Analysis Date = 05/24/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/02/16 Pct Recovery = 76% Analysis Date = 05/02/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/10/16 Pct Recovery = 76% Analysis Date = 04/10/16 Pct Recovery = 76% Analysis Date = 03/30/16 Pct Recovery = 76% Analysis Date = 03/30/16 Pct Recovery = 76% Analysis Date = 03/20/16 Pct Recovery = 76% Analysis Date = 03/20/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 03/09/16 Pct Recovery = 76% Analysis Date = 02/27/16 Pct Recovery = 77% Analysis Date = 02/27/16 Pct Recovery = 77% Analysis Date = 02/16/16 Pct Recovery = 77% Analysis Date = 02/16/16 Pct Recovery = 77% Analysis Date = 02/05/16 Pct Recovery = 77% Analysis Date = 02/05/16 Pct Recovery = 77% Analysis Date = 01/25/16 Pct Recovery = 77% Analysis Date = 01/25/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/14/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 01/04/16 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/24/15 Pct Recovery = 77% Analysis Date = 12/13/15 Pct Recovery = 77% Analysis Date = 12/13/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 12/02/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/21/15 Pct Recovery = 77% Analysis Date = 11/10/15 Pct Recovery = 77% Analysis Date = 11/10/15 Pct Recovery = 77% Analysis Date = 10/30/15 Pct Recovery = 77% Analysis Date = 10/30/15 Pct Recovery = 77% Analysis Date = 10/20/15 Pct Recovery = 77% Analysis Date = 10/20/15 Pct Recovery = 77% Analysis Date = 10/09/15 Pct Recovery = 77% Analysis Date = 10/09/15 Pct Recovery = 77% Analysis Date = 09/28/15 Pct Recovery = 77% Analysis Date = 09/28/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 77% Analysis Date = 09/06/15 Pct Recovery = 77% Analysis Date = 09/06/15 Pct Recovery = 77% Analysis Date = 08/26/15 Pct Recovery = 77% Analysis Date = 08/26/15 Pct Recovery = 77% Analysis Date = 08/15/15 Pct Recovery = 77% Analysis Date = 08/15/15 Pct Recovery = 77% Analysis Date = 08/05/15 Pct Recovery = 78% Analysis Date = 08/05/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/14/15 Pct Recovery = 78% Analysis Date = 07/14/15 Pct Recovery = 78% Analysis Date = 07/03/15 Pct Recovery = 78% Analysis Date = 07/03/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/11/15 Pct Recovery = 78% Analysis Date = 06/11/15 Pct Recovery = 78% Analysis Date = 05/31/15 Pct Recovery = 78% Analysis Date = 05/31/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/10/15 Pct Recovery = 78% Analysis Date = 05/10/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/07/15 Pct Recovery = 78% Analysis Date = 04/07/15 Pct Recovery = 78% Analysis Date = 03/27/15 Pct Recovery = 78% Analysis Date = 03/27/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/01/15 Pct Recovery = 78% Analysis Date = 02/01/15 Pct Recovery = 78% Analysis Date = 01/21/15 Pct Recovery = 78% Analysis Date = 01/21/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/20/14 Pct Recovery = 78% Analysis Date = 12/20/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 11/28/14 Pct Recovery = 79% Analysis Date = 11/28/14 Pct Recovery = 79% Analysis Date = 11/17/14 Pct Recovery = 79% Analysis Date = 11/17/14 Pct Recovery = 79% Analysis Date = 11/06/14 Pct Recovery = 79% Analysis Date = 11/06/14 Pct Recovery = 79% Analysis Date = 10/26/14 Pct Recovery = 79% Analysis Date = 10/26/14 Pct Recovery = 79% Analysis Date = 10/16/14 Pct Recovery = 79% Analysis Date = 10/16/14 Pct Recovery = 79% Analysis Date = 10/05/14 Pct Recovery = 79% Analysis Date = 10/05/14 Pct Recovery = 79% Analysis Date = 09/24/14 Pct Recovery = 79% Analysis Date = 09/24/14 Pct Recovery = 79% Analysis Date = 09/13/14 Pct Recovery = 79% Analysis Date = 09/13/14 Pct Recovery = 79% Analysis Date = 09/02/14 Pct Recovery = 79% Analysis Date = 09/02/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/10/14 Pct Recovery = 79% Analysis Date = 07/10/14 Pct Recovery = 79% Analysis Date = 06/29/14 Pct Recovery = 79% Analysis Date = 06/29/14 Pct Recovery = 79% Analysis Date = 06/18/14 Pct Recovery = 79% Analysis Date = 06/18/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 78% Analysis Date = 06/07/14 Pct Recovery = 78% Analysis Date = 05/27/14 Pct Recovery = 78% Analysis Date = 05/27/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/17/14 Pct Recovery = 78% Analysis Date = 05/06/14 Pct Recovery = 78% Analysis Date = 05/06/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/25/14 Pct Recovery = 78% Analysis Date = 04/14/14 Pct Recovery = 78% Analysis Date = 04/14/14 Pct Recovery = 78% Analysis Date = 04/03/14 Pct Recovery = 78% Analysis Date = 04/03/14 Pct Recovery = 78% Analysis Date = 03/23/14 Pct Recovery = 78% Analysis Date = 03/23/14 Pct Recovery = 78% Analysis Date = 03/12/14 Pct Recovery = 78% Analysis Date = 03/12/14 Pct Recovery = 78% Analysis Date = 03/02/14 Pct Recovery = 79% Analysis Date = 03/02/14 Pct Recovery = 79% Analysis Date = 02/19/14 Pct Recovery = 79% Analysis Date = 02/19/14 Pct Recovery = 79% Analysis Date = 02/08/14 Pct Recovery = 79% Analysis Date = 02/08/14 Pct Recovery = 79% Analysis Date = 01/28/14 Pct Recovery = 79% Analysis Date = 01/28/14 Pct Recovery = 79% Analysis Date = 01/17/14 Pct Recovery = 79% Analysis Date = 01/17/14 Pct Recovery = 79% Analysis Date = 01/06/14 Pct Recovery = 79% Analysis Date = 01/06/14 Pct Recovery = 79% Analysis Date = 12/26/13 Pct Recovery = 79% Analysis Date = 12/26/13 Pct Recovery = 79% Analysis Date = 12/16/13 Pct Recovery = 79% Analysis Date = 12/16/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 11/24/13 Pct Recovery = 79% Analysis Date = 11/24/13 Pct Recovery = 79% Analysis Date = 11/13/13 Pct Recovery = 79% Analysis Date = 11/13/13 Pct Recovery = 79% Analysis Date = 11/02/13 Pct Recovery = 79% Analysis Date = 11/02/13 Pct Recovery = 79% Analysis Date = 10/22/13 Pct Recovery = 79% Analysis Date = 10/22/13 Pct Recovery = 79% Analysis Date = 10/11/13 Pct Recovery = 79% Analysis Date = 10/11/13 Pct Recovery = 79% Analysis Date = 10/01/13 Pct Recovery = 79% Analysis Date = 10/01/13 Pct Recovery = 79% Analysis Date = 09/20/13 Pct Recovery = 80% Analysis Date = 09/20/13 Pct Recovery = 80% Analysis Date = 09/09/13 Pct Recovery = 80% Analysis Date = 09/09/13 Pct Recovery = 80% Analysis Date = 08/29/13 Pct Recovery = 80% Analysis Date = 08/29/13 Pct Recovery = 80% Analysis Date = 08/18/13 Pct Recovery = 80% Analysis Date = 08/18/13 Pct Recovery = 80% Analysis Date = 08/07/13 Pct Recovery = 80% Analysis Date = 08/07/13 Pct Recovery = 80% Analysis Date = 07/27/13 Pct Recovery = 80% Analysis Date = 07/27/13 Pct Recovery = 80% Analysis Date = 07/17/13 Pct Recovery = 81% Analysis Date = 07/17/13 Pct Recovery = 81% Analysis Date = 07/06/13 Pct Recovery = 81% Analysis Date = 07/06/13 Pct Recovery = 81% Analysis Date = 06/25/13 Pct Recovery = 81% Analysis Date = 06/25/13 Pct Recovery = 81% Analysis Date = 06/14/13 Pct Recovery = 81% Analysis Date = 06/14/13 Pct Recovery = 81% Analysis Date = 06/03/13 Pct Recovery = 81% Analysis Date = 06/03/13 Pct Recovery = 81% Analysis Date = 05/23/13 Pct Recovery = 82% Analysis Date = 05/23/13 Pct Recovery = 82% Analysis Date = 05/12/13 Pct Recovery = 82% Analysis Date = 05/12/13 Pct Recovery = 82% Analysis Date = 05/02/13 Pct Recovery = 82% Analysis Date = 05/02/13 Pct Recovery = 82% Analysis Date = 04/21/13 Pct Recovery = 82% Analysis Date = 04/21/13 Pct Recovery = 82% Analysis Date = 04/10/13 Pct Recovery = 82% Analysis Date = 04/10/13 Pct Recovery = 82% Analysis Date = 03/30/13 Pct Recovery = 83% Analysis Date = 03/30/13 Pct Recovery = 83% Analysis Date = 03/19/13 Pct Recovery = 83% Analysis Date = 03/19/13 Pct Recovery = 83% Analysis Date = 03/08/13 Pct Recovery = 83% Analysis Date = 03/08/13 Pct Recovery = 83% Analysis Date = 02/25/13 Pct Recovery = 83% Analysis Date = 02/25/13 Pct Recovery = 83% Analysis Date = 02/15/13 Pct Recovery = 84% Analysis Date = 02/15/13 Pct Recovery = 84% Analysis Date = 02/04/13 Pct Recovery = 84% Analysis Date = 02/04/13 Pct Recovery = 84% Analysis Date = 01/24/13 Pct Recovery = 84% Analysis Date = 01/24/13 Pct Recovery = 84% Analysis Date = 01/13/13 Pct Recovery = 84% Analysis Date = 01/13/13 Pct Recovery = 84% Analysis Date = 01/02/13 Pct Recovery = 84% Analysis Date = 01/02/13 Pct Recovery = 84% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/12/12 Pct Recovery = 85% Analysis Date = 12/12/12 Pct Recovery = 85% Analysis Date = 12/01/12 Pct Recovery = 85% Analysis Date = 12/01/12 Pct Recovery = 85% Analysis Date = 11/20/12 Pct Recovery = 85% Analysis Date = 11/20/12 Pct Recovery = 85% Analysis Date = 11/09/12 Pct Recovery = 85% Analysis Date = 11/09/12 Pct Recovery = 85% Analysis Date = 10/29/12 Pct Recovery = 86% Analysis Date = 10/29/12 Pct Recovery = 86% Analysis Date = 10/18/12 Pct Recovery = 86% Analysis Date = 10/18/12 Pct Recovery = 86% Analysis Date = 10/07/12 Pct Recovery = 86% Analysis Date = 10/07/12 Pct Recovery = 86% Analysis Date = 09/27/12 Pct Recovery = 86% Analysis Date = 09/27/12 Pct Recovery = 86% Analysis Date = 09/16/12 Pct Recovery = 86% Analysis Date = 09/16/12 Pct Recovery = 86% Analysis Date = 09/05/12 Pct Recovery = 86% Analysis Date = 09/05/12 Pct Recovery = 86% Analysis Date = 08/25/12 Pct Recovery = 86% Analysis Date = 08/25/12 Pct Recovery = 86% Analysis Date = 08/14/12 Pct Recovery = 87% Analysis Date = 08/14/12 Pct Recovery = 87% Analysis Date = 08/03/12 Pct Recovery = 87% Analysis Date = 08/03/12 Pct Recovery = 87% Analysis Date = 07/23/12 Pct Recovery = 87% Analysis Date = 07/23/12 Pct Recovery = 87% Analysis Date = 07/13/12 Pct Recovery = 87% Analysis Date = 07/13/12 Pct Recovery = 87% Analysis Date = 07/02/12 Pct Recovery = 87% Analysis Date = 07/02/12 Pct Recovery = 87% Analysis Date = 06/21/12 Pct Recovery = 87% Analysis Date = 06/21/12 Pct Recovery = 87% Analysis Date = 06/10/12 Pct Recovery = 87% Analysis Date = 06/10/12 Pct Recovery = 87% Analysis Date = 05/30/12 Pct Recovery = 87% Analysis Date = 05/30/12 Pct Recovery = 87% Analysis Date = 05/19/12 Pct Recovery = 88% Analysis Date = 05/19/12 Pct Recovery = 88% Analysis Date = 05/08/12 Pct Recovery = 88% Analysis Date = 05/08/12 Pct Recovery = 88% Analysis Date = 04/28/12 Pct Recovery = 88% Analysis Date = 04/28/12 Pct Recovery = 88% Analysis Date = 04/17/12 Pct Recovery = 88% Analysis Date = 04/17/12 Pct Recovery = 88% Analysis Date = 04/06/12 Pct Recovery = 88% Analysis Date = 04/06/12 Pct Recovery = 88% Analysis Date = 03/26/12 Pct Recovery = 88% Analysis Date = 03/26/12 Pct Recovery = 88% Analysis Date = 03/15/12 Pct Recovery = 88% Analysis Date = 03/15/12 Pct Recovery = 88% Analysis Date = 03/04/12 Pct Recovery = 89% Analysis Date = 03/04/12 Pct Recovery = 89% Analysis Date = 02/22/12 Pct Recovery = 89% Analysis Date = 02/22/12 Pct Recovery = 89% Analysis Date = 02/12/12 Pct Recovery = 89% Analysis Date = 02/12/12 Pct Recovery = 89% Analysis Date = 02/01/12 Pct Recovery = 89% Analysis Date = 02/01/12 Pct Recovery = 89% Analysis Date = 01/21/12 Pct Recovery = 89% Analysis Date = 01/21/12 Pct Recovery = 89% Analysis Date = 01/10/12 Pct Recovery = 89% Analysis Date = 01/10/12 Pct Recovery = 89% Analysis Date = 12/30/11 Pct Recovery = 89% Analysis Date = 12/30/11 Pct Recovery = 89% Analysis Date = 12/19/11 Pct Recovery = 90% Analysis Date = 12/19/11 Pct Recovery = 90% Analysis Date = 12/08/11 Pct Recovery = 90% Analysis Date = 12/08/11 Pct Recovery = 90% Analysis Date = 11/28/11 Pct Recovery = 90% Analysis Date = 11/28/11 Pct Recovery = 90% Analysis Date = 11/17/11 Pct Recovery = 90% Analysis Date = 11/17/11 Pct Recovery = 90% Analysis Date = 11/06/11 Pct Recovery = 90% Analysis Date = 11/06/11 Pct Recovery = 90% Analysis Date = 10/26/11 Pct Recovery = 90% Analysis Date = 10/26/11 Pct Recovery = 90% Analysis Date = 10/15/11 Pct Recovery = 90% Analysis Date = 10/15/11 Pct Recovery = 90% Analysis Date = 10/04/11 Pct Recovery = 91% Analysis Date = 10/04/11 Pct Recovery = 91% Analysis Date = 09/23/11 Pct Recovery = 91% Analysis Date = 09/23/11 Pct Recovery = 91% Analysis Date = 09/13/11 Pct Recovery = 91% Analysis Date = 09/13/11 Pct Recovery = 91% Analysis Date = 09/02/11 Pct Recovery = 91% Analysis Date = 09/02/11 Pct Recovery = 91% Analysis Date = 08/22/11 Pct Recovery = 91% Analysis Date = 08/22/11 Pct Recovery = 91% Analysis Date = 08/11/11 Pct Recovery = 91% Analysis Date = 08/11/11 Pct Recovery = 91% Analysis Date = 07/31/11 Pct Recovery = 91% Analysis Date = 07/31/11 Pct Recovery = 91% Analysis Date = 07/20/11 Pct Recovery = 91% Analysis Date = 07/20/11 Pct Recovery = 91% Analysis Date = 07/09/11 Pct Recovery = 91% Analysis Date = 07/09/11 Pct Recovery = 91% Analysis Date = 06/29/11 Pct Recovery = 92% Analysis Date = 06/29/11 Pct Recovery = 92% Analysis Date = 06/18/11 Pct Recovery = 92% Analysis Date = 06/18/11 Pct Recovery = 92% Analysis Date = 06/07/11 Pct Recovery = 92% Analysis Date = 06/07/11 Pct Recovery = 92% Analysis Date = 05/27/11 Pct Recovery = 92% Analysis Date = 05/27/11 Pct Recovery = 92% Analysis Date = 05/16/11 Pct Recovery = 92% Analysis Date = 05/16/11 Pct Recovery = 92% Analysis Date = 05/05/11 Pct Recovery = 92% Analysis Date = 05/05/11 Pct Recovery = 92% Analysis Date = 04/24/11 Pct Recovery = 92% Analysis Date = 04/24/11 Pct Recovery = 92% Analysis Date = 04/14/11 Pct Recovery = 92% Analysis Date = 04/14/11 Pct Recovery = 92% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 04/03/11 Pct Recovery = 92% Analysis Date = 03/23/11 Pct Recovery = 92% Analysis Date = 03/23/11 Pct Recovery = 92% Analysis Date = 03/12/11 Pct Recovery = 93% Analysis Date = 03/12/11 Pct Recovery = 93% Analysis Date = 03/01/11 Pct Recovery = 93% Analysis Date = 03/01/11 Pct Recovery = 93% Analysis Date = 02/18/11 Pct Recovery = 93% Analysis Date = 02/18/11 Pct Recovery = 93% Analysis Date = 02/08/11 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METRIBUZIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 82% 19% 81% 17%
Total 89 82% 19% 81% 17%

Sample Statistics
METRIBUZIN

Characteristic N % % Basis
Plotted 89 100% Spiked
Estimated Values 3 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 89 .  
False Negatives 0 0% 0 out of 89
Not Spiked 80 .  
False Positives 0 0% 0 out of 80

BQS OBSP Determination:
MOLINATE
METHOD: 2033 , TESTIDCODE: 82671GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 89% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 89% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 93% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 89% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 84% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 99% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 96% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 102% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 96% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 114% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 96% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 100% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 86% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 108% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 107% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 107% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 96% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 89% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 105% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 86% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 100% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 99% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 100% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 106% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 91% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 82% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 92% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 100% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 88% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 105% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 123% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 87% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 122% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 41% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 96% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 103% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 103% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 94% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 100% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 109% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 100% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 89% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 99% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 102% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 98% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 104% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 117% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 102% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 98% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 77% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 86% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 87% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 87% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 79% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 108% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 118% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 109% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 73% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 109% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 117% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 105% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 98% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 110% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 103% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 105% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 113% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 118% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 108% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 118% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 82% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 92% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 85% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 90% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 89% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 93% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 92% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 108% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 107% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 94% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 113% Analysis Date = 01/18/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 12/27/16 Pct Recovery = 99% Analysis Date = 12/27/16 Pct Recovery = 99% Analysis Date = 12/16/16 Pct Recovery = 98% Analysis Date = 12/16/16 Pct Recovery = 98% Analysis Date = 12/05/16 Pct Recovery = 98% Analysis Date = 12/05/16 Pct Recovery = 98% Analysis Date = 11/24/16 Pct Recovery = 98% Analysis Date = 11/24/16 Pct Recovery = 98% Analysis Date = 11/14/16 Pct Recovery = 98% Analysis Date = 11/14/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 11/03/16 Pct Recovery = 98% Analysis Date = 10/23/16 Pct Recovery = 98% Analysis Date = 10/23/16 Pct Recovery = 98% Analysis Date = 10/12/16 Pct Recovery = 97% Analysis Date = 10/12/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 97% Analysis Date = 08/30/16 Pct Recovery = 97% Analysis Date = 08/30/16 Pct Recovery = 97% Analysis Date = 08/19/16 Pct Recovery = 97% Analysis Date = 08/19/16 Pct Recovery = 97% Analysis Date = 08/08/16 Pct Recovery = 96% Analysis Date = 08/08/16 Pct Recovery = 96% Analysis Date = 07/28/16 Pct Recovery = 96% Analysis Date = 07/28/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/26/16 Pct Recovery = 96% Analysis Date = 06/15/16 Pct Recovery = 96% Analysis Date = 06/15/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 95% Analysis Date = 05/24/16 Pct Recovery = 95% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/03/16 Pct Recovery = 95% Analysis Date = 05/03/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/11/16 Pct Recovery = 95% Analysis Date = 04/11/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/31/16 Pct Recovery = 95% Analysis Date = 03/20/16 Pct Recovery = 95% Analysis Date = 03/20/16 Pct Recovery = 95% Analysis Date = 03/10/16 Pct Recovery = 95% Analysis Date = 03/10/16 Pct Recovery = 95% Analysis Date = 02/28/16 Pct Recovery = 94% Analysis Date = 02/28/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/06/16 Pct Recovery = 94% Analysis Date = 02/06/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 94% Analysis Date = 01/15/16 Pct Recovery = 94% Analysis Date = 01/15/16 Pct Recovery = 94% Analysis Date = 01/05/16 Pct Recovery = 94% Analysis Date = 01/05/16 Pct Recovery = 94% Analysis Date = 12/25/15 Pct Recovery = 94% Analysis Date = 12/25/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/22/15 Pct Recovery = 93% Analysis Date = 11/22/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 92% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 92% Analysis Date = 06/13/15 Pct Recovery = 92% Analysis Date = 06/02/15 Pct Recovery = 92% Analysis Date = 06/02/15 Pct Recovery = 92% Analysis Date = 05/22/15 Pct Recovery = 92% Analysis Date = 05/22/15 Pct Recovery = 92% Analysis Date = 05/11/15 Pct Recovery = 92% Analysis Date = 05/11/15 Pct Recovery = 92% Analysis Date = 05/01/15 Pct Recovery = 92% Analysis Date = 05/01/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/20/15 Pct Recovery = 92% Analysis Date = 04/09/15 Pct Recovery = 92% Analysis Date = 04/09/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/29/15 Pct Recovery = 92% Analysis Date = 03/18/15 Pct Recovery = 92% Analysis Date = 03/18/15 Pct Recovery = 92% Analysis Date = 03/08/15 Pct Recovery = 92% Analysis Date = 03/08/15 Pct Recovery = 92% Analysis Date = 02/25/15 Pct Recovery = 92% Analysis Date = 02/25/15 Pct Recovery = 92% Analysis Date = 02/14/15 Pct Recovery = 92% Analysis Date = 02/14/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 02/03/15 Pct Recovery = 92% Analysis Date = 01/23/15 Pct Recovery = 92% Analysis Date = 01/23/15 Pct Recovery = 92% Analysis Date = 01/12/15 Pct Recovery = 92% Analysis Date = 01/12/15 Pct Recovery = 92% Analysis Date = 01/02/15 Pct Recovery = 92% Analysis Date = 01/02/15 Pct Recovery = 92% Analysis Date = 12/22/14 Pct Recovery = 92% Analysis Date = 12/22/14 Pct Recovery = 92% Analysis Date = 12/11/14 Pct Recovery = 92% Analysis Date = 12/11/14 Pct Recovery = 92% Analysis Date = 11/30/14 Pct Recovery = 92% Analysis Date = 11/30/14 Pct Recovery = 92% Analysis Date = 11/19/14 Pct Recovery = 92% Analysis Date = 11/19/14 Pct Recovery = 92% Analysis Date = 11/08/14 Pct Recovery = 92% Analysis Date = 11/08/14 Pct Recovery = 92% Analysis Date = 10/29/14 Pct Recovery = 92% Analysis Date = 10/29/14 Pct Recovery = 92% Analysis Date = 10/18/14 Pct Recovery = 92% Analysis Date = 10/18/14 Pct Recovery = 92% Analysis Date = 10/07/14 Pct Recovery = 93% Analysis Date = 10/07/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/26/14 Pct Recovery = 93% Analysis Date = 09/15/14 Pct Recovery = 93% Analysis Date = 09/15/14 Pct Recovery = 93% Analysis Date = 09/05/14 Pct Recovery = 93% Analysis Date = 09/05/14 Pct Recovery = 93% Analysis Date = 08/25/14 Pct Recovery = 94% Analysis Date = 08/25/14 Pct Recovery = 94% Analysis Date = 08/14/14 Pct Recovery = 94% Analysis Date = 08/14/14 Pct Recovery = 94% Analysis Date = 08/03/14 Pct Recovery = 94% Analysis Date = 08/03/14 Pct Recovery = 94% Analysis Date = 07/23/14 Pct Recovery = 94% Analysis Date = 07/23/14 Pct Recovery = 94% Analysis Date = 07/12/14 Pct Recovery = 95% Analysis Date = 07/12/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 07/02/14 Pct Recovery = 95% Analysis Date = 06/21/14 Pct Recovery = 95% Analysis Date = 06/21/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 96% Analysis Date = 05/19/14 Pct Recovery = 96% Analysis Date = 05/08/14 Pct Recovery = 96% Analysis Date = 05/08/14 Pct Recovery = 96% Analysis Date = 04/28/14 Pct Recovery = 96% Analysis Date = 04/28/14 Pct Recovery = 96% Analysis Date = 04/17/14 Pct Recovery = 96% Analysis Date = 04/17/14 Pct Recovery = 96% Analysis Date = 04/06/14 Pct Recovery = 96% Analysis Date = 04/06/14 Pct Recovery = 96% Analysis Date = 03/26/14 Pct Recovery = 96% Analysis Date = 03/26/14 Pct Recovery = 96% Analysis Date = 03/15/14 Pct Recovery = 97% Analysis Date = 03/15/14 Pct Recovery = 97% Analysis Date = 03/04/14 Pct Recovery = 97% Analysis Date = 03/04/14 Pct Recovery = 97% Analysis Date = 02/22/14 Pct Recovery = 97% Analysis Date = 02/22/14 Pct Recovery = 97% Analysis Date = 02/11/14 Pct Recovery = 97% Analysis Date = 02/11/14 Pct Recovery = 97% Analysis Date = 01/31/14 Pct Recovery = 97% Analysis Date = 01/31/14 Pct Recovery = 97% Analysis Date = 01/20/14 Pct Recovery = 97% Analysis Date = 01/20/14 Pct Recovery = 97% Analysis Date = 01/09/14 Pct Recovery = 97% Analysis Date = 01/09/14 Pct Recovery = 97% Analysis Date = 12/30/13 Pct Recovery = 98% Analysis Date = 12/30/13 Pct Recovery = 98% Analysis Date = 12/19/13 Pct Recovery = 98% Analysis Date = 12/19/13 Pct Recovery = 98% Analysis Date = 12/08/13 Pct Recovery = 98% Analysis Date = 12/08/13 Pct Recovery = 98% Analysis Date = 11/27/13 Pct Recovery = 98% Analysis Date = 11/27/13 Pct Recovery = 98% Analysis Date = 11/16/13 Pct Recovery = 98% Analysis Date = 11/16/13 Pct Recovery = 98% Analysis Date = 11/05/13 Pct Recovery = 98% Analysis Date = 11/05/13 Pct Recovery = 98% Analysis Date = 10/26/13 Pct Recovery = 98% Analysis Date = 10/26/13 Pct Recovery = 98% Analysis Date = 10/15/13 Pct Recovery = 98% Analysis Date = 10/15/13 Pct Recovery = 98% Analysis Date = 10/04/13 Pct Recovery = 98% Analysis Date = 10/04/13 Pct Recovery = 98% Analysis Date = 09/23/13 Pct Recovery = 98% Analysis Date = 09/23/13 Pct Recovery = 98% Analysis Date = 09/12/13 Pct Recovery = 98% Analysis Date = 09/12/13 Pct Recovery = 98% Analysis Date = 09/01/13 Pct Recovery = 98% Analysis Date = 09/01/13 Pct Recovery = 98% Analysis Date = 08/22/13 Pct Recovery = 98% Analysis Date = 08/22/13 Pct Recovery = 98% Analysis Date = 08/11/13 Pct Recovery = 98% Analysis Date = 08/11/13 Pct Recovery = 98% Analysis Date = 07/31/13 Pct Recovery = 98% Analysis Date = 07/31/13 Pct Recovery = 98% Analysis Date = 07/20/13 Pct Recovery = 98% Analysis Date = 07/20/13 Pct Recovery = 98% Analysis Date = 07/09/13 Pct Recovery = 98% Analysis Date = 07/09/13 Pct Recovery = 98% Analysis Date = 06/29/13 Pct Recovery = 98% Analysis Date = 06/29/13 Pct Recovery = 98% Analysis Date = 06/18/13 Pct Recovery = 98% Analysis Date = 06/18/13 Pct Recovery = 98% Analysis Date = 06/07/13 Pct Recovery = 98% Analysis Date = 06/07/13 Pct Recovery = 98% Analysis Date = 05/27/13 Pct Recovery = 98% Analysis Date = 05/27/13 Pct Recovery = 98% Analysis Date = 05/16/13 Pct Recovery = 98% Analysis Date = 05/16/13 Pct Recovery = 98% Analysis Date = 05/05/13 Pct Recovery = 98% Analysis Date = 05/05/13 Pct Recovery = 98% Analysis Date = 04/25/13 Pct Recovery = 98% Analysis Date = 04/25/13 Pct Recovery = 98% Analysis Date = 04/14/13 Pct Recovery = 98% Analysis Date = 04/14/13 Pct Recovery = 98% Analysis Date = 04/03/13 Pct Recovery = 98% Analysis Date = 04/03/13 Pct Recovery = 98% Analysis Date = 03/23/13 Pct Recovery = 98% Analysis Date = 03/23/13 Pct Recovery = 98% Analysis Date = 03/12/13 Pct Recovery = 98% Analysis Date = 03/12/13 Pct Recovery = 98% Analysis Date = 03/01/13 Pct Recovery = 98% Analysis Date = 03/01/13 Pct Recovery = 98% Analysis Date = 02/19/13 Pct Recovery = 98% Analysis Date = 02/19/13 Pct Recovery = 98% Analysis Date = 02/08/13 Pct Recovery = 98% Analysis Date = 02/08/13 Pct Recovery = 98% Analysis Date = 01/28/13 Pct Recovery = 98% Analysis Date = 01/28/13 Pct Recovery = 98% Analysis Date = 01/17/13 Pct Recovery = 98% Analysis Date = 01/17/13 Pct Recovery = 98% Analysis Date = 01/06/13 Pct Recovery = 98% Analysis Date = 01/06/13 Pct Recovery = 98% Analysis Date = 12/26/12 Pct Recovery = 98% Analysis Date = 12/26/12 Pct Recovery = 98% Analysis Date = 12/16/12 Pct Recovery = 98% Analysis Date = 12/16/12 Pct Recovery = 98% Analysis Date = 12/05/12 Pct Recovery = 98% Analysis Date = 12/05/12 Pct Recovery = 98% Analysis Date = 11/24/12 Pct Recovery = 97% Analysis Date = 11/24/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 97% Analysis Date = 11/02/12 Pct Recovery = 97% Analysis Date = 11/02/12 Pct Recovery = 97% Analysis Date = 10/23/12 Pct Recovery = 97% Analysis Date = 10/23/12 Pct Recovery = 97% Analysis Date = 10/12/12 Pct Recovery = 97% Analysis Date = 10/12/12 Pct Recovery = 97% Analysis Date = 10/01/12 Pct Recovery = 97% Analysis Date = 10/01/12 Pct Recovery = 97% Analysis Date = 09/20/12 Pct Recovery = 97% Analysis Date = 09/20/12 Pct Recovery = 97% Analysis Date = 09/09/12 Pct Recovery = 97% Analysis Date = 09/09/12 Pct Recovery = 97% Analysis Date = 08/29/12 Pct Recovery = 97% Analysis Date = 08/29/12 Pct Recovery = 97% Analysis Date = 08/19/12 Pct Recovery = 97% Analysis Date = 08/19/12 Pct Recovery = 97% Analysis Date = 08/08/12 Pct Recovery = 97% Analysis Date = 08/08/12 Pct Recovery = 97% Analysis Date = 07/28/12 Pct Recovery = 98% Analysis Date = 07/28/12 Pct Recovery = 98% Analysis Date = 07/17/12 Pct Recovery = 98% Analysis Date = 07/17/12 Pct Recovery = 98% Analysis Date = 07/06/12 Pct Recovery = 98% Analysis Date = 07/06/12 Pct Recovery = 98% Analysis Date = 06/25/12 Pct Recovery = 98% Analysis Date = 06/25/12 Pct Recovery = 98% Analysis Date = 06/15/12 Pct Recovery = 98% Analysis Date = 06/15/12 Pct Recovery = 98% Analysis Date = 06/04/12 Pct Recovery = 98% Analysis Date = 06/04/12 Pct Recovery = 98% Analysis Date = 05/24/12 Pct Recovery = 98% Analysis Date = 05/24/12 Pct Recovery = 98% Analysis Date = 05/13/12 Pct Recovery = 98% Analysis Date = 05/13/12 Pct Recovery = 98% Analysis Date = 05/02/12 Pct Recovery = 98% Analysis Date = 05/02/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 99% Analysis Date = 03/31/12 Pct Recovery = 99% Analysis Date = 03/20/12 Pct Recovery = 99% Analysis Date = 03/20/12 Pct Recovery = 99% Analysis Date = 03/09/12 Pct Recovery = 99% Analysis Date = 03/09/12 Pct Recovery = 99% Analysis Date = 02/27/12 Pct Recovery = 99% Analysis Date = 02/27/12 Pct Recovery = 99% Analysis Date = 02/17/12 Pct Recovery = 99% Analysis Date = 02/17/12 Pct Recovery = 99% Analysis Date = 02/06/12 Pct Recovery = 99% Analysis Date = 02/06/12 Pct Recovery = 99% Analysis Date = 01/26/12 Pct Recovery = 99% Analysis Date = 01/26/12 Pct Recovery = 99% Analysis Date = 01/15/12 Pct Recovery = 99% Analysis Date = 01/15/12 Pct Recovery = 99% Analysis Date = 01/04/12 Pct Recovery = 100% Analysis Date = 01/04/12 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/24/11 Pct Recovery = 100% Analysis Date = 12/14/11 Pct Recovery = 100% Analysis Date = 12/14/11 Pct Recovery = 100% Analysis Date = 12/03/11 Pct Recovery = 100% Analysis Date = 12/03/11 Pct Recovery = 100% Analysis Date = 11/22/11 Pct Recovery = 100% Analysis Date = 11/22/11 Pct Recovery = 100% Analysis Date = 11/11/11 Pct Recovery = 100% Analysis Date = 11/11/11 Pct Recovery = 100% Analysis Date = 10/31/11 Pct Recovery = 101% Analysis Date = 10/31/11 Pct Recovery = 101% Analysis Date = 10/20/11 Pct Recovery = 101% Analysis Date = 10/20/11 Pct Recovery = 101% Analysis Date = 10/10/11 Pct Recovery = 101% Analysis Date = 10/10/11 Pct Recovery = 101% Analysis Date = 09/29/11 Pct Recovery = 101% Analysis Date = 09/29/11 Pct Recovery = 101% Analysis Date = 09/18/11 Pct Recovery = 101% Analysis Date = 09/18/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 09/07/11 Pct Recovery = 101% Analysis Date = 08/27/11 Pct Recovery = 101% Analysis Date = 08/27/11 Pct Recovery = 101% Analysis Date = 08/17/11 Pct Recovery = 102% Analysis Date = 08/17/11 Pct Recovery = 102% Analysis Date = 08/06/11 Pct Recovery = 102% Analysis Date = 08/06/11 Pct Recovery = 102% Analysis Date = 07/26/11 Pct Recovery = 102% Analysis Date = 07/26/11 Pct Recovery = 102% Analysis Date = 07/15/11 Pct Recovery = 102% Analysis Date = 07/15/11 Pct Recovery = 102% Analysis Date = 07/04/11 Pct Recovery = 102% Analysis Date = 07/04/11 Pct Recovery = 102% Analysis Date = 06/23/11 Pct Recovery = 102% Analysis Date = 06/23/11 Pct Recovery = 102% Analysis Date = 06/13/11 Pct Recovery = 103% Analysis Date = 06/13/11 Pct Recovery = 103% Analysis Date = 06/02/11 Pct Recovery = 103% Analysis Date = 06/02/11 Pct Recovery = 103% Analysis Date = 05/22/11 Pct Recovery = 103% Analysis Date = 05/22/11 Pct Recovery = 103% Analysis Date = 05/11/11 Pct Recovery = 103% Analysis Date = 05/11/11 Pct Recovery = 103% Analysis Date = 04/30/11 Pct Recovery = 103% Analysis Date = 04/30/11 Pct Recovery = 103% Analysis Date = 04/19/11 Pct Recovery = 104% Analysis Date = 04/19/11 Pct Recovery = 104% Analysis Date = 04/09/11 Pct Recovery = 104% Analysis Date = 04/09/11 Pct Recovery = 104% Analysis Date = 03/29/11 Pct Recovery = 104% Analysis Date = 03/29/11 Pct Recovery = 104% Analysis Date = 03/18/11 Pct Recovery = 104% Analysis Date = 03/18/11 Pct Recovery = 104% Analysis Date = 03/07/11 Pct Recovery = 104% Analysis Date = 03/07/11 Pct Recovery = 104% Analysis Date = 02/24/11 Pct Recovery = 104% Analysis Date = 02/24/11 Pct Recovery = 104% Analysis Date = 02/14/11 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MOLINATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 97% 13% 98% 13%
Total 89 97% 13% 98% 13%

Sample Statistics
MOLINATE

Characteristic N % % Basis
Plotted 89 95% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 2% Spiked
Spiked 94 .  
False Negatives 3 3% 3 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
MYCLOBUTANIL
METHOD: 2033 , TESTIDCODE: 61599GCM39
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 81% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 67% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 81% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 87% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 60% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 71% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 108% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 88% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 53% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 79% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 71% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 68% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 96% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 55% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 55% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 72% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 78% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 79% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 64% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 72% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 67% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 67% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 58% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 69% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 79% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 67% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 85% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 72% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 78% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 71% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 77% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 74% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 105% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 70% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 82% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 76% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 71% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 67% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 82% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 71% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 69% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 73% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 82% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 81% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 82% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 61% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 67% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 85% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 112% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 101% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 66% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 72% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 88% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 81% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 92% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 53% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 61% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 62% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 96% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 82% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 75% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 76% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 71% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 79% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 94% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 147% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 87% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 66% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 70% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 82% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 60% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 115% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 71% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 94% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Analysis Date = 12/19/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 12/09/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/28/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/16/16 Pct Recovery = 81% Analysis Date = 10/16/16 Pct Recovery = 81% Analysis Date = 10/06/16 Pct Recovery = 81% Analysis Date = 10/06/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/25/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/14/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/13/16 Pct Recovery = 81% Analysis Date = 08/13/16 Pct Recovery = 81% Analysis Date = 08/02/16 Pct Recovery = 81% Analysis Date = 08/02/16 Pct Recovery = 81% Analysis Date = 07/23/16 Pct Recovery = 81% Analysis Date = 07/23/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 06/20/16 Pct Recovery = 82% Analysis Date = 06/20/16 Pct Recovery = 82% Analysis Date = 06/10/16 Pct Recovery = 82% Analysis Date = 06/10/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/09/16 Pct Recovery = 82% Analysis Date = 05/09/16 Pct Recovery = 82% Analysis Date = 04/28/16 Pct Recovery = 82% Analysis Date = 04/28/16 Pct Recovery = 82% Analysis Date = 04/17/16 Pct Recovery = 82% Analysis Date = 04/17/16 Pct Recovery = 82% Analysis Date = 04/06/16 Pct Recovery = 82% Analysis Date = 04/06/16 Pct Recovery = 82% Analysis Date = 03/27/16 Pct Recovery = 82% Analysis Date = 03/27/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 02/24/16 Pct Recovery = 83% Analysis Date = 02/24/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/02/16 Pct Recovery = 83% Analysis Date = 02/02/16 Pct Recovery = 83% Analysis Date = 01/22/16 Pct Recovery = 83% Analysis Date = 01/22/16 Pct Recovery = 83% Analysis Date = 01/12/16 Pct Recovery = 83% Analysis Date = 01/12/16 Pct Recovery = 83% Analysis Date = 01/01/16 Pct Recovery = 83% Analysis Date = 01/01/16 Pct Recovery = 83% Analysis Date = 12/21/15 Pct Recovery = 83% Analysis Date = 12/21/15 Pct Recovery = 83% Analysis Date = 12/11/15 Pct Recovery = 83% Analysis Date = 12/11/15 Pct Recovery = 83% Analysis Date = 11/30/15 Pct Recovery = 83% Analysis Date = 11/30/15 Pct Recovery = 83% Analysis Date = 11/19/15 Pct Recovery = 83% Analysis Date = 11/19/15 Pct Recovery = 83% Analysis Date = 11/09/15 Pct Recovery = 83% Analysis Date = 11/09/15 Pct Recovery = 83% Analysis Date = 10/29/15 Pct Recovery = 83% Analysis Date = 10/29/15 Pct Recovery = 83% Analysis Date = 10/18/15 Pct Recovery = 83% Analysis Date = 10/18/15 Pct Recovery = 83% Analysis Date = 10/07/15 Pct Recovery = 83% Analysis Date = 10/07/15 Pct Recovery = 83% Analysis Date = 09/27/15 Pct Recovery = 83% Analysis Date = 09/27/15 Pct Recovery = 83% Analysis Date = 09/16/15 Pct Recovery = 83% Analysis Date = 09/16/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 09/05/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 83% Analysis Date = 08/15/15 Pct Recovery = 83% Analysis Date = 08/15/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 08/04/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/24/15 Pct Recovery = 83% Analysis Date = 07/14/15 Pct Recovery = 83% Analysis Date = 07/14/15 Pct Recovery = 83% Analysis Date = 07/03/15 Pct Recovery = 84% Analysis Date = 07/03/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/22/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/12/15 Pct Recovery = 84% Analysis Date = 06/01/15 Pct Recovery = 84% Analysis Date = 06/01/15 Pct Recovery = 84% Analysis Date = 05/21/15 Pct Recovery = 84% Analysis Date = 05/21/15 Pct Recovery = 84% Analysis Date = 05/10/15 Pct Recovery = 84% Analysis Date = 05/10/15 Pct Recovery = 84% Analysis Date = 04/30/15 Pct Recovery = 84% Analysis Date = 04/30/15 Pct Recovery = 84% Analysis Date = 04/19/15 Pct Recovery = 84% Analysis Date = 04/19/15 Pct Recovery = 84% Analysis Date = 04/08/15 Pct Recovery = 84% Analysis Date = 04/08/15 Pct Recovery = 84% Analysis Date = 03/29/15 Pct Recovery = 84% Analysis Date = 03/29/15 Pct Recovery = 84% Analysis Date = 03/18/15 Pct Recovery = 84% Analysis Date = 03/18/15 Pct Recovery = 84% Analysis Date = 03/07/15 Pct Recovery = 84% Analysis Date = 03/07/15 Pct Recovery = 84% Analysis Date = 02/24/15 Pct Recovery = 84% Analysis Date = 02/24/15 Pct Recovery = 84% Analysis Date = 02/14/15 Pct Recovery = 84% Analysis Date = 02/14/15 Pct Recovery = 84% Analysis Date = 02/03/15 Pct Recovery = 84% Analysis Date = 02/03/15 Pct Recovery = 84% Analysis Date = 01/23/15 Pct Recovery = 84% Analysis Date = 01/23/15 Pct Recovery = 84% Analysis Date = 01/13/15 Pct Recovery = 84% Analysis Date = 01/13/15 Pct Recovery = 84% Analysis Date = 01/02/15 Pct Recovery = 84% Analysis Date = 01/02/15 Pct Recovery = 84% Analysis Date = 12/22/14 Pct Recovery = 84% Analysis Date = 12/22/14 Pct Recovery = 84% Analysis Date = 12/12/14 Pct Recovery = 84% Analysis Date = 12/12/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 83% Analysis Date = 12/01/14 Pct Recovery = 83% Analysis Date = 11/20/14 Pct Recovery = 83% Analysis Date = 11/20/14 Pct Recovery = 83% Analysis Date = 11/09/14 Pct Recovery = 83% Analysis Date = 11/09/14 Pct Recovery = 83% Analysis Date = 10/30/14 Pct Recovery = 83% Analysis Date = 10/30/14 Pct Recovery = 83% Analysis Date = 10/19/14 Pct Recovery = 83% Analysis Date = 10/19/14 Pct Recovery = 83% Analysis Date = 10/08/14 Pct Recovery = 83% Analysis Date = 10/08/14 Pct Recovery = 83% Analysis Date = 09/28/14 Pct Recovery = 83% Analysis Date = 09/28/14 Pct Recovery = 83% Analysis Date = 09/17/14 Pct Recovery = 83% Analysis Date = 09/17/14 Pct Recovery = 83% Analysis Date = 09/06/14 Pct Recovery = 83% Analysis Date = 09/06/14 Pct Recovery = 83% Analysis Date = 08/26/14 Pct Recovery = 83% Analysis Date = 08/26/14 Pct Recovery = 83% Analysis Date = 08/16/14 Pct Recovery = 82% Analysis Date = 08/16/14 Pct Recovery = 82% Analysis Date = 08/05/14 Pct Recovery = 82% Analysis Date = 08/05/14 Pct Recovery = 82% Analysis Date = 07/25/14 Pct Recovery = 82% Analysis Date = 07/25/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/15/14 Pct Recovery = 82% Analysis Date = 07/04/14 Pct Recovery = 81% Analysis Date = 07/04/14 Pct Recovery = 81% Analysis Date = 06/23/14 Pct Recovery = 81% Analysis Date = 06/23/14 Pct Recovery = 81% Analysis Date = 06/12/14 Pct Recovery = 81% Analysis Date = 06/12/14 Pct Recovery = 81% Analysis Date = 06/02/14 Pct Recovery = 81% Analysis Date = 06/02/14 Pct Recovery = 81% Analysis Date = 05/22/14 Pct Recovery = 81% Analysis Date = 05/22/14 Pct Recovery = 81% Analysis Date = 05/11/14 Pct Recovery = 80% Analysis Date = 05/11/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 04/20/14 Pct Recovery = 80% Analysis Date = 04/20/14 Pct Recovery = 80% Analysis Date = 04/09/14 Pct Recovery = 80% Analysis Date = 04/09/14 Pct Recovery = 80% Analysis Date = 03/29/14 Pct Recovery = 79% Analysis Date = 03/29/14 Pct Recovery = 79% Analysis Date = 03/19/14 Pct Recovery = 79% Analysis Date = 03/19/14 Pct Recovery = 79% Analysis Date = 03/08/14 Pct Recovery = 79% Analysis Date = 03/08/14 Pct Recovery = 79% Analysis Date = 02/25/14 Pct Recovery = 79% Analysis Date = 02/25/14 Pct Recovery = 79% Analysis Date = 02/15/14 Pct Recovery = 78% Analysis Date = 02/15/14 Pct Recovery = 78% Analysis Date = 02/04/14 Pct Recovery = 78% Analysis Date = 02/04/14 Pct Recovery = 78% Analysis Date = 01/24/14 Pct Recovery = 78% Analysis Date = 01/24/14 Pct Recovery = 78% Analysis Date = 01/13/14 Pct Recovery = 78% Analysis Date = 01/13/14 Pct Recovery = 78% Analysis Date = 01/03/14 Pct Recovery = 78% Analysis Date = 01/03/14 Pct Recovery = 78% Analysis Date = 12/23/13 Pct Recovery = 78% Analysis Date = 12/23/13 Pct Recovery = 78% Analysis Date = 12/12/13 Pct Recovery = 77% Analysis Date = 12/12/13 Pct Recovery = 77% Analysis Date = 12/02/13 Pct Recovery = 77% Analysis Date = 12/02/13 Pct Recovery = 77% Analysis Date = 11/21/13 Pct Recovery = 77% Analysis Date = 11/21/13 Pct Recovery = 77% Analysis Date = 11/10/13 Pct Recovery = 77% Analysis Date = 11/10/13 Pct Recovery = 77% Analysis Date = 10/31/13 Pct Recovery = 77% Analysis Date = 10/31/13 Pct Recovery = 77% Analysis Date = 10/20/13 Pct Recovery = 77% Analysis Date = 10/20/13 Pct Recovery = 77% Analysis Date = 10/09/13 Pct Recovery = 77% Analysis Date = 10/09/13 Pct Recovery = 77% Analysis Date = 09/28/13 Pct Recovery = 77% Analysis Date = 09/28/13 Pct Recovery = 77% Analysis Date = 09/18/13 Pct Recovery = 77% Analysis Date = 09/18/13 Pct Recovery = 77% Analysis Date = 09/07/13 Pct Recovery = 77% Analysis Date = 09/07/13 Pct Recovery = 77% Analysis Date = 08/27/13 Pct Recovery = 77% Analysis Date = 08/27/13 Pct Recovery = 77% Analysis Date = 08/17/13 Pct Recovery = 77% Analysis Date = 08/17/13 Pct Recovery = 77% Analysis Date = 08/06/13 Pct Recovery = 77% Analysis Date = 08/06/13 Pct Recovery = 77% Analysis Date = 07/26/13 Pct Recovery = 77% Analysis Date = 07/26/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/05/13 Pct Recovery = 77% Analysis Date = 07/05/13 Pct Recovery = 77% Analysis Date = 06/24/13 Pct Recovery = 76% Analysis Date = 06/24/13 Pct Recovery = 76% Analysis Date = 06/13/13 Pct Recovery = 76% Analysis Date = 06/13/13 Pct Recovery = 76% Analysis Date = 06/03/13 Pct Recovery = 76% Analysis Date = 06/03/13 Pct Recovery = 76% Analysis Date = 05/23/13 Pct Recovery = 76% Analysis Date = 05/23/13 Pct Recovery = 76% Analysis Date = 05/12/13 Pct Recovery = 76% Analysis Date = 05/12/13 Pct Recovery = 76% Analysis Date = 05/01/13 Pct Recovery = 76% Analysis Date = 05/01/13 Pct Recovery = 76% Analysis Date = 04/21/13 Pct Recovery = 76% Analysis Date = 04/21/13 Pct Recovery = 76% Analysis Date = 04/10/13 Pct Recovery = 76% Analysis Date = 04/10/13 Pct Recovery = 76% Analysis Date = 03/30/13 Pct Recovery = 76% Analysis Date = 03/30/13 Pct Recovery = 76% Analysis Date = 03/20/13 Pct Recovery = 76% Analysis Date = 03/20/13 Pct Recovery = 76% Analysis Date = 03/09/13 Pct Recovery = 76% Analysis Date = 03/09/13 Pct Recovery = 76% Analysis Date = 02/26/13 Pct Recovery = 76% Analysis Date = 02/26/13 Pct Recovery = 76% Analysis Date = 02/15/13 Pct Recovery = 76% Analysis Date = 02/15/13 Pct Recovery = 76% Analysis Date = 02/05/13 Pct Recovery = 76% Analysis Date = 02/05/13 Pct Recovery = 76% Analysis Date = 01/25/13 Pct Recovery = 76% Analysis Date = 01/25/13 Pct Recovery = 76% Analysis Date = 01/14/13 Pct Recovery = 76% Analysis Date = 01/14/13 Pct Recovery = 76% Analysis Date = 01/04/13 Pct Recovery = 76% Analysis Date = 01/04/13 Pct Recovery = 76% Analysis Date = 12/24/12 Pct Recovery = 76% Analysis Date = 12/24/12 Pct Recovery = 76% Analysis Date = 12/13/12 Pct Recovery = 75% Analysis Date = 12/13/12 Pct Recovery = 75% Analysis Date = 12/03/12 Pct Recovery = 75% Analysis Date = 12/03/12 Pct Recovery = 75% Analysis Date = 11/22/12 Pct Recovery = 75% Analysis Date = 11/22/12 Pct Recovery = 75% Analysis Date = 11/11/12 Pct Recovery = 75% Analysis Date = 11/11/12 Pct Recovery = 75% Analysis Date = 10/31/12 Pct Recovery = 75% Analysis Date = 10/31/12 Pct Recovery = 75% Analysis Date = 10/21/12 Pct Recovery = 75% Analysis Date = 10/21/12 Pct Recovery = 75% Analysis Date = 10/10/12 Pct Recovery = 75% Analysis Date = 10/10/12 Pct Recovery = 75% Analysis Date = 09/29/12 Pct Recovery = 75% Analysis Date = 09/29/12 Pct Recovery = 75% Analysis Date = 09/19/12 Pct Recovery = 75% Analysis Date = 09/19/12 Pct Recovery = 75% Analysis Date = 09/08/12 Pct Recovery = 75% Analysis Date = 09/08/12 Pct Recovery = 75% Analysis Date = 08/28/12 Pct Recovery = 75% Analysis Date = 08/28/12 Pct Recovery = 75% Analysis Date = 08/17/12 Pct Recovery = 75% Analysis Date = 08/17/12 Pct Recovery = 75% Analysis Date = 08/07/12 Pct Recovery = 75% Analysis Date = 08/07/12 Pct Recovery = 75% Analysis Date = 07/27/12 Pct Recovery = 75% Analysis Date = 07/27/12 Pct Recovery = 75% Analysis Date = 07/16/12 Pct Recovery = 75% Analysis Date = 07/16/12 Pct Recovery = 75% Analysis Date = 07/06/12 Pct Recovery = 75% Analysis Date = 07/06/12 Pct Recovery = 75% Analysis Date = 06/25/12 Pct Recovery = 75% Analysis Date = 06/25/12 Pct Recovery = 75% Analysis Date = 06/14/12 Pct Recovery = 75% Analysis Date = 06/14/12 Pct Recovery = 75% Analysis Date = 06/03/12 Pct Recovery = 75% Analysis Date = 06/03/12 Pct Recovery = 75% Analysis Date = 05/24/12 Pct Recovery = 75% Analysis Date = 05/24/12 Pct Recovery = 75% Analysis Date = 05/13/12 Pct Recovery = 75% Analysis Date = 05/13/12 Pct Recovery = 75% Analysis Date = 05/02/12 Pct Recovery = 75% Analysis Date = 05/02/12 Pct Recovery = 75% Analysis Date = 04/22/12 Pct Recovery = 75% Analysis Date = 04/22/12 Pct Recovery = 75% Analysis Date = 04/11/12 Pct Recovery = 74% Analysis Date = 04/11/12 Pct Recovery = 74% Analysis Date = 03/31/12 Pct Recovery = 74% Analysis Date = 03/31/12 Pct Recovery = 74% Analysis Date = 03/20/12 Pct Recovery = 74% Analysis Date = 03/20/12 Pct Recovery = 74% Analysis Date = 03/10/12 Pct Recovery = 74% Analysis Date = 03/10/12 Pct Recovery = 74% Analysis Date = 02/28/12 Pct Recovery = 74% Analysis Date = 02/28/12 Pct Recovery = 74% Analysis Date = 02/17/12 Pct Recovery = 74% Analysis Date = 02/17/12 Pct Recovery = 74% Analysis Date = 02/07/12 Pct Recovery = 74% Analysis Date = 02/07/12 Pct Recovery = 74% Analysis Date = 01/27/12 Pct Recovery = 74% Analysis Date = 01/27/12 Pct Recovery = 74% Analysis Date = 01/16/12 Pct Recovery = 74% Analysis Date = 01/16/12 Pct Recovery = 74% Analysis Date = 01/06/12 Pct Recovery = 74% Analysis Date = 01/06/12 Pct Recovery = 74% Analysis Date = 12/26/11 Pct Recovery = 74% Analysis Date = 12/26/11 Pct Recovery = 74% Analysis Date = 12/15/11 Pct Recovery = 74% Analysis Date = 12/15/11 Pct Recovery = 74% Analysis Date = 12/04/11 Pct Recovery = 74% Analysis Date = 12/04/11 Pct Recovery = 74% Analysis Date = 11/24/11 Pct Recovery = 74% Analysis Date = 11/24/11 Pct Recovery = 74% Analysis Date = 11/13/11 Pct Recovery = 74% Analysis Date = 11/13/11 Pct Recovery = 74% Analysis Date = 11/02/11 Pct Recovery = 74% Analysis Date = 11/02/11 Pct Recovery = 74% Analysis Date = 10/23/11 Pct Recovery = 74% Analysis Date = 10/23/11 Pct Recovery = 74% Analysis Date = 10/12/11 Pct Recovery = 74% Analysis Date = 10/12/11 Pct Recovery = 74% Analysis Date = 10/01/11 Pct Recovery = 74% Analysis Date = 10/01/11 Pct Recovery = 74% Analysis Date = 09/20/11 Pct Recovery = 74% Analysis Date = 09/20/11 Pct Recovery = 74% Analysis Date = 09/10/11 Pct Recovery = 74% Analysis Date = 09/10/11 Pct Recovery = 74% Analysis Date = 08/30/11 Pct Recovery = 74% Analysis Date = 08/30/11 Pct Recovery = 74% Analysis Date = 08/19/11 Pct Recovery = 74% Analysis Date = 08/19/11 Pct Recovery = 74% Analysis Date = 08/09/11 Pct Recovery = 74% Analysis Date = 08/09/11 Pct Recovery = 74% Analysis Date = 07/29/11 Pct Recovery = 74% Analysis Date = 07/29/11 Pct Recovery = 74% Analysis Date = 07/18/11 Pct Recovery = 74% Analysis Date = 07/18/11 Pct Recovery = 74% Analysis Date = 07/07/11 Pct Recovery = 74% Analysis Date = 07/07/11 Pct Recovery = 74% Analysis Date = 06/27/11 Pct Recovery = 74% Analysis Date = 06/27/11 Pct Recovery = 74% Analysis Date = 06/16/11 Pct Recovery = 74% Analysis Date = 06/16/11 Pct Recovery = 74% Analysis Date = 06/05/11 Pct Recovery = 74% Analysis Date = 06/05/11 Pct Recovery = 74% Analysis Date = 05/26/11 Pct Recovery = 74% Analysis Date = 05/26/11 Pct Recovery = 74% Analysis Date = 05/15/11 Pct Recovery = 74% Analysis Date = 05/15/11 Pct Recovery = 74% Analysis Date = 05/04/11 Pct Recovery = 73% Analysis Date = 05/04/11 Pct Recovery = 73% Analysis Date = 04/23/11 Pct Recovery = 73% Analysis Date = 04/23/11 Pct Recovery = 73% Analysis Date = 04/13/11 Pct Recovery = 73% Analysis Date = 04/13/11 Pct Recovery = 73% Analysis Date = 04/02/11 Pct Recovery = 73% Analysis Date = 04/02/11 Pct Recovery = 73% Analysis Date = 03/22/11 Pct Recovery = 73% Analysis Date = 03/22/11 Pct Recovery = 73% Analysis Date = 03/12/11 Pct Recovery = 73% Analysis Date = 03/12/11 Pct Recovery = 73% Analysis Date = 03/01/11 Pct Recovery = 73% Analysis Date = 03/01/11 Pct Recovery = 73% Analysis Date = 02/18/11 Pct Recovery = 73% Analysis Date = 02/18/11 Pct Recovery = 73% Analysis Date = 02/08/11 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MYCLOBUTANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 78% 14% 77% 11%
Total 94 78% 14% 77% 11%

Sample Statistics
MYCLOBUTANIL

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
OXYFLUORFEN
METHOD: 2033 , TESTIDCODE: 61600GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 46% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 58% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 56% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 56% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 59% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 66% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 67% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 60% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 66% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 73% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 78% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 67% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 103% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 84% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 89% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 71% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 74% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 88% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 85% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 85% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 89% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 76% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 61% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 67% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 67% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 79% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 70% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 77% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 78% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 67% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 62% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 65% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 66% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 92% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 117% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 102% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 95% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 98% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 87% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 98% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 85% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 88% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 65% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 85% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 103% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 81% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 82% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 93% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 89% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 74% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 83% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 80% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 111% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 85% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 73% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 143% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 78% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 104% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 94% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 93% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 178% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 83% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 92% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 122% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 84% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 96% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 110% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 84% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 111% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 121% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 102% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 82% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 89% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 72% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 80% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 88% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 93% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 71% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 105% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 106% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 01/18/17 Pct Recovery = 101% Analysis Date = 01/07/17 Pct Recovery = 101% Analysis Date = 01/07/17 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/16/16 Pct Recovery = 100% Analysis Date = 12/16/16 Pct Recovery = 100% Analysis Date = 12/05/16 Pct Recovery = 100% Analysis Date = 12/05/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 100% Analysis Date = 11/14/16 Pct Recovery = 100% Analysis Date = 11/14/16 Pct Recovery = 100% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 11/03/16 Pct Recovery = 99% Analysis Date = 10/23/16 Pct Recovery = 99% Analysis Date = 10/23/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 99% Analysis Date = 08/30/16 Pct Recovery = 98% Analysis Date = 08/30/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 08/08/16 Pct Recovery = 98% Analysis Date = 07/28/16 Pct Recovery = 98% Analysis Date = 07/28/16 Pct Recovery = 98% Analysis Date = 07/17/16 Pct Recovery = 98% Analysis Date = 07/17/16 Pct Recovery = 98% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 07/07/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/26/16 Pct Recovery = 97% Analysis Date = 06/15/16 Pct Recovery = 97% Analysis Date = 06/15/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/14/16 Pct Recovery = 97% Analysis Date = 05/14/16 Pct Recovery = 97% Analysis Date = 05/03/16 Pct Recovery = 96% Analysis Date = 05/03/16 Pct Recovery = 96% Analysis Date = 04/22/16 Pct Recovery = 96% Analysis Date = 04/22/16 Pct Recovery = 96% Analysis Date = 04/11/16 Pct Recovery = 96% Analysis Date = 04/11/16 Pct Recovery = 96% Analysis Date = 03/31/16 Pct Recovery = 96% Analysis Date = 03/31/16 Pct Recovery = 96% Analysis Date = 03/20/16 Pct Recovery = 96% Analysis Date = 03/20/16 Pct Recovery = 96% Analysis Date = 03/10/16 Pct Recovery = 95% Analysis Date = 03/10/16 Pct Recovery = 95% Analysis Date = 02/28/16 Pct Recovery = 95% Analysis Date = 02/28/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 95% Analysis Date = 02/06/16 Pct Recovery = 95% Analysis Date = 02/06/16 Pct Recovery = 95% Analysis Date = 01/26/16 Pct Recovery = 95% Analysis Date = 01/26/16 Pct Recovery = 95% Analysis Date = 01/15/16 Pct Recovery = 95% Analysis Date = 01/15/16 Pct Recovery = 95% Analysis Date = 01/05/16 Pct Recovery = 94% Analysis Date = 01/05/16 Pct Recovery = 94% Analysis Date = 12/25/15 Pct Recovery = 94% Analysis Date = 12/25/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/14/15 Pct Recovery = 94% Analysis Date = 12/03/15 Pct Recovery = 94% Analysis Date = 12/03/15 Pct Recovery = 94% Analysis Date = 11/22/15 Pct Recovery = 94% Analysis Date = 11/22/15 Pct Recovery = 94% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 10/10/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/29/15 Pct Recovery = 93% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 05/22/15 Pct Recovery = 90% Analysis Date = 05/22/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/11/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 05/01/15 Pct Recovery = 90% Analysis Date = 04/20/15 Pct Recovery = 90% Analysis Date = 04/20/15 Pct Recovery = 90% Analysis Date = 04/09/15 Pct Recovery = 90% Analysis Date = 04/09/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 89% Analysis Date = 03/29/15 Pct Recovery = 89% Analysis Date = 03/18/15 Pct Recovery = 89% Analysis Date = 03/18/15 Pct Recovery = 89% Analysis Date = 03/08/15 Pct Recovery = 89% Analysis Date = 03/08/15 Pct Recovery = 89% Analysis Date = 02/25/15 Pct Recovery = 89% Analysis Date = 02/25/15 Pct Recovery = 89% Analysis Date = 02/14/15 Pct Recovery = 89% Analysis Date = 02/14/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 88% Analysis Date = 02/03/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/23/15 Pct Recovery = 88% Analysis Date = 01/12/15 Pct Recovery = 88% Analysis Date = 01/12/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 01/02/15 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 88% Analysis Date = 12/22/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 12/11/14 Pct Recovery = 88% Analysis Date = 11/30/14 Pct Recovery = 88% Analysis Date = 11/30/14 Pct Recovery = 88% Analysis Date = 11/19/14 Pct Recovery = 88% Analysis Date = 11/19/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 11/08/14 Pct Recovery = 88% Analysis Date = 10/29/14 Pct Recovery = 88% Analysis Date = 10/29/14 Pct Recovery = 88% Analysis Date = 10/18/14 Pct Recovery = 88% Analysis Date = 10/18/14 Pct Recovery = 88% Analysis Date = 10/07/14 Pct Recovery = 88% Analysis Date = 10/07/14 Pct Recovery = 88% Analysis Date = 09/26/14 Pct Recovery = 87% Analysis Date = 09/26/14 Pct Recovery = 87% Analysis Date = 09/15/14 Pct Recovery = 87% Analysis Date = 09/15/14 Pct Recovery = 87% Analysis Date = 09/05/14 Pct Recovery = 87% Analysis Date = 09/05/14 Pct Recovery = 87% Analysis Date = 08/25/14 Pct Recovery = 87% Analysis Date = 08/25/14 Pct Recovery = 87% Analysis Date = 08/14/14 Pct Recovery = 87% Analysis Date = 08/14/14 Pct Recovery = 87% Analysis Date = 08/03/14 Pct Recovery = 87% Analysis Date = 08/03/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/23/14 Pct Recovery = 87% Analysis Date = 07/12/14 Pct Recovery = 87% Analysis Date = 07/12/14 Pct Recovery = 87% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/19/14 Pct Recovery = 85% Analysis Date = 05/19/14 Pct Recovery = 85% Analysis Date = 05/08/14 Pct Recovery = 85% Analysis Date = 05/08/14 Pct Recovery = 85% Analysis Date = 04/28/14 Pct Recovery = 85% Analysis Date = 04/28/14 Pct Recovery = 85% Analysis Date = 04/17/14 Pct Recovery = 84% Analysis Date = 04/17/14 Pct Recovery = 84% Analysis Date = 04/06/14 Pct Recovery = 84% Analysis Date = 04/06/14 Pct Recovery = 84% Analysis Date = 03/26/14 Pct Recovery = 84% Analysis Date = 03/26/14 Pct Recovery = 84% Analysis Date = 03/15/14 Pct Recovery = 84% Analysis Date = 03/15/14 Pct Recovery = 84% Analysis Date = 03/04/14 Pct Recovery = 83% Analysis Date = 03/04/14 Pct Recovery = 83% Analysis Date = 02/22/14 Pct Recovery = 83% Analysis Date = 02/22/14 Pct Recovery = 83% Analysis Date = 02/11/14 Pct Recovery = 83% Analysis Date = 02/11/14 Pct Recovery = 83% Analysis Date = 01/31/14 Pct Recovery = 82% Analysis Date = 01/31/14 Pct Recovery = 82% Analysis Date = 01/20/14 Pct Recovery = 82% Analysis Date = 01/20/14 Pct Recovery = 82% Analysis Date = 01/09/14 Pct Recovery = 82% Analysis Date = 01/09/14 Pct Recovery = 82% Analysis Date = 12/30/13 Pct Recovery = 81% Analysis Date = 12/30/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/19/13 Pct Recovery = 81% Analysis Date = 12/08/13 Pct Recovery = 81% Analysis Date = 12/08/13 Pct Recovery = 81% Analysis Date = 11/27/13 Pct Recovery = 80% Analysis Date = 11/27/13 Pct Recovery = 80% Analysis Date = 11/16/13 Pct Recovery = 80% Analysis Date = 11/16/13 Pct Recovery = 80% Analysis Date = 11/05/13 Pct Recovery = 79% Analysis Date = 11/05/13 Pct Recovery = 79% Analysis Date = 10/26/13 Pct Recovery = 79% Analysis Date = 10/26/13 Pct Recovery = 79% Analysis Date = 10/15/13 Pct Recovery = 79% Analysis Date = 10/15/13 Pct Recovery = 79% Analysis Date = 10/04/13 Pct Recovery = 79% Analysis Date = 10/04/13 Pct Recovery = 79% Analysis Date = 09/23/13 Pct Recovery = 79% Analysis Date = 09/23/13 Pct Recovery = 79% Analysis Date = 09/12/13 Pct Recovery = 78% Analysis Date = 09/12/13 Pct Recovery = 78% Analysis Date = 09/01/13 Pct Recovery = 78% Analysis Date = 09/01/13 Pct Recovery = 78% Analysis Date = 08/22/13 Pct Recovery = 78% Analysis Date = 08/22/13 Pct Recovery = 78% Analysis Date = 08/11/13 Pct Recovery = 78% Analysis Date = 08/11/13 Pct Recovery = 78% Analysis Date = 07/31/13 Pct Recovery = 78% Analysis Date = 07/31/13 Pct Recovery = 78% Analysis Date = 07/20/13 Pct Recovery = 78% Analysis Date = 07/20/13 Pct Recovery = 78% Analysis Date = 07/09/13 Pct Recovery = 77% Analysis Date = 07/09/13 Pct Recovery = 77% Analysis Date = 06/29/13 Pct Recovery = 77% Analysis Date = 06/29/13 Pct Recovery = 77% Analysis Date = 06/18/13 Pct Recovery = 77% Analysis Date = 06/18/13 Pct Recovery = 77% Analysis Date = 06/07/13 Pct Recovery = 77% Analysis Date = 06/07/13 Pct Recovery = 77% Analysis Date = 05/27/13 Pct Recovery = 77% Analysis Date = 05/27/13 Pct Recovery = 77% Analysis Date = 05/16/13 Pct Recovery = 77% Analysis Date = 05/16/13 Pct Recovery = 77% Analysis Date = 05/05/13 Pct Recovery = 76% Analysis Date = 05/05/13 Pct Recovery = 76% Analysis Date = 04/25/13 Pct Recovery = 76% Analysis Date = 04/25/13 Pct Recovery = 76% Analysis Date = 04/14/13 Pct Recovery = 76% Analysis Date = 04/14/13 Pct Recovery = 76% Analysis Date = 04/03/13 Pct Recovery = 76% Analysis Date = 04/03/13 Pct Recovery = 76% Analysis Date = 03/23/13 Pct Recovery = 76% Analysis Date = 03/23/13 Pct Recovery = 76% Analysis Date = 03/12/13 Pct Recovery = 76% Analysis Date = 03/12/13 Pct Recovery = 76% Analysis Date = 03/01/13 Pct Recovery = 76% Analysis Date = 03/01/13 Pct Recovery = 76% Analysis Date = 02/19/13 Pct Recovery = 76% Analysis Date = 02/19/13 Pct Recovery = 76% Analysis Date = 02/08/13 Pct Recovery = 76% Analysis Date = 02/08/13 Pct Recovery = 76% Analysis Date = 01/28/13 Pct Recovery = 76% Analysis Date = 01/28/13 Pct Recovery = 76% Analysis Date = 01/17/13 Pct Recovery = 76% Analysis Date = 01/17/13 Pct Recovery = 76% Analysis Date = 01/06/13 Pct Recovery = 76% Analysis Date = 01/06/13 Pct Recovery = 76% Analysis Date = 12/26/12 Pct Recovery = 76% Analysis Date = 12/26/12 Pct Recovery = 76% Analysis Date = 12/16/12 Pct Recovery = 76% Analysis Date = 12/16/12 Pct Recovery = 76% Analysis Date = 12/05/12 Pct Recovery = 76% Analysis Date = 12/05/12 Pct Recovery = 76% Analysis Date = 11/24/12 Pct Recovery = 76% Analysis Date = 11/24/12 Pct Recovery = 76% Analysis Date = 11/13/12 Pct Recovery = 76% Analysis Date = 11/13/12 Pct Recovery = 76% Analysis Date = 11/02/12 Pct Recovery = 76% Analysis Date = 11/02/12 Pct Recovery = 76% Analysis Date = 10/23/12 Pct Recovery = 76% Analysis Date = 10/23/12 Pct Recovery = 76% Analysis Date = 10/12/12 Pct Recovery = 76% Analysis Date = 10/12/12 Pct Recovery = 76% Analysis Date = 10/01/12 Pct Recovery = 77% Analysis Date = 10/01/12 Pct Recovery = 77% Analysis Date = 09/20/12 Pct Recovery = 77% Analysis Date = 09/20/12 Pct Recovery = 77% Analysis Date = 09/09/12 Pct Recovery = 77% Analysis Date = 09/09/12 Pct Recovery = 77% Analysis Date = 08/29/12 Pct Recovery = 77% Analysis Date = 08/29/12 Pct Recovery = 77% Analysis Date = 08/19/12 Pct Recovery = 77% Analysis Date = 08/19/12 Pct Recovery = 77% Analysis Date = 08/08/12 Pct Recovery = 77% Analysis Date = 08/08/12 Pct Recovery = 77% Analysis Date = 07/28/12 Pct Recovery = 78% Analysis Date = 07/28/12 Pct Recovery = 78% Analysis Date = 07/17/12 Pct Recovery = 78% Analysis Date = 07/17/12 Pct Recovery = 78% Analysis Date = 07/06/12 Pct Recovery = 78% Analysis Date = 07/06/12 Pct Recovery = 78% Analysis Date = 06/25/12 Pct Recovery = 78% Analysis Date = 06/25/12 Pct Recovery = 78% Analysis Date = 06/15/12 Pct Recovery = 78% Analysis Date = 06/15/12 Pct Recovery = 78% Analysis Date = 06/04/12 Pct Recovery = 78% Analysis Date = 06/04/12 Pct Recovery = 78% Analysis Date = 05/24/12 Pct Recovery = 79% Analysis Date = 05/24/12 Pct Recovery = 79% Analysis Date = 05/13/12 Pct Recovery = 79% Analysis Date = 05/13/12 Pct Recovery = 79% Analysis Date = 05/02/12 Pct Recovery = 79% Analysis Date = 05/02/12 Pct Recovery = 79% Analysis Date = 04/22/12 Pct Recovery = 79% Analysis Date = 04/22/12 Pct Recovery = 79% Analysis Date = 04/11/12 Pct Recovery = 79% Analysis Date = 04/11/12 Pct Recovery = 79% Analysis Date = 03/31/12 Pct Recovery = 80% Analysis Date = 03/31/12 Pct Recovery = 80% Analysis Date = 03/20/12 Pct Recovery = 80% Analysis Date = 03/20/12 Pct Recovery = 80% Analysis Date = 03/09/12 Pct Recovery = 80% Analysis Date = 03/09/12 Pct Recovery = 80% Analysis Date = 02/27/12 Pct Recovery = 80% Analysis Date = 02/27/12 Pct Recovery = 80% Analysis Date = 02/17/12 Pct Recovery = 81% Analysis Date = 02/17/12 Pct Recovery = 81% Analysis Date = 02/06/12 Pct Recovery = 81% Analysis Date = 02/06/12 Pct Recovery = 81% Analysis Date = 01/26/12 Pct Recovery = 81% Analysis Date = 01/26/12 Pct Recovery = 81% Analysis Date = 01/15/12 Pct Recovery = 81% Analysis Date = 01/15/12 Pct Recovery = 81% Analysis Date = 01/04/12 Pct Recovery = 82% Analysis Date = 01/04/12 Pct Recovery = 82% Analysis Date = 12/24/11 Pct Recovery = 82% Analysis Date = 12/24/11 Pct Recovery = 82% Analysis Date = 12/14/11 Pct Recovery = 82% Analysis Date = 12/14/11 Pct Recovery = 82% Analysis Date = 12/03/11 Pct Recovery = 82% Analysis Date = 12/03/11 Pct Recovery = 82% Analysis Date = 11/22/11 Pct Recovery = 83% Analysis Date = 11/22/11 Pct Recovery = 83% Analysis Date = 11/11/11 Pct Recovery = 83% Analysis Date = 11/11/11 Pct Recovery = 83% Analysis Date = 10/31/11 Pct Recovery = 83% Analysis Date = 10/31/11 Pct Recovery = 83% Analysis Date = 10/20/11 Pct Recovery = 84% Analysis Date = 10/20/11 Pct Recovery = 84% Analysis Date = 10/10/11 Pct Recovery = 84% Analysis Date = 10/10/11 Pct Recovery = 84% Analysis Date = 09/29/11 Pct Recovery = 84% Analysis Date = 09/29/11 Pct Recovery = 84% Analysis Date = 09/18/11 Pct Recovery = 84% Analysis Date = 09/18/11 Pct Recovery = 84% Analysis Date = 09/07/11 Pct Recovery = 85% Analysis Date = 09/07/11 Pct Recovery = 85% Analysis Date = 08/27/11 Pct Recovery = 85% Analysis Date = 08/27/11 Pct Recovery = 85% Analysis Date = 08/17/11 Pct Recovery = 85% Analysis Date = 08/17/11 Pct Recovery = 85% Analysis Date = 08/06/11 Pct Recovery = 86% Analysis Date = 08/06/11 Pct Recovery = 86% Analysis Date = 07/26/11 Pct Recovery = 86% Analysis Date = 07/26/11 Pct Recovery = 86% Analysis Date = 07/15/11 Pct Recovery = 86% Analysis Date = 07/15/11 Pct Recovery = 86% Analysis Date = 07/04/11 Pct Recovery = 86% Analysis Date = 07/04/11 Pct Recovery = 86% Analysis Date = 06/23/11 Pct Recovery = 87% Analysis Date = 06/23/11 Pct Recovery = 87% Analysis Date = 06/13/11 Pct Recovery = 87% Analysis Date = 06/13/11 Pct Recovery = 87% Analysis Date = 06/02/11 Pct Recovery = 87% Analysis Date = 06/02/11 Pct Recovery = 87% Analysis Date = 05/22/11 Pct Recovery = 88% Analysis Date = 05/22/11 Pct Recovery = 88% Analysis Date = 05/11/11 Pct Recovery = 88% Analysis Date = 05/11/11 Pct Recovery = 88% Analysis Date = 04/30/11 Pct Recovery = 88% Analysis Date = 04/30/11 Pct Recovery = 88% Analysis Date = 04/19/11 Pct Recovery = 89% Analysis Date = 04/19/11 Pct Recovery = 89% Analysis Date = 04/09/11 Pct Recovery = 89% Analysis Date = 04/09/11 Pct Recovery = 89% Analysis Date = 03/29/11 Pct Recovery = 89% Analysis Date = 03/29/11 Pct Recovery = 89% Analysis Date = 03/18/11 Pct Recovery = 89% Analysis Date = 03/18/11 Pct Recovery = 89% Analysis Date = 03/07/11 Pct Recovery = 90% Analysis Date = 03/07/11 Pct Recovery = 90% Analysis Date = 02/24/11 Pct Recovery = 90% Analysis Date = 02/24/11 Pct Recovery = 90% Analysis Date = 02/14/11 Pct Recovery = 90% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXYFLUORFEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 85% 19% 84% 16%
Total 94 85% 19% 84% 16%

Sample Statistics
OXYFLUORFEN

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 4 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
PARAOXON-METHYL
METHOD: 2033 , TESTIDCODE: 61664GCM39
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 70% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 93% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 78% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 75% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 75% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 92% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 77% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 76% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 93% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 44% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 82% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 93% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 76% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 96% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 140% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 89% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 103% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 79% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 82% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 34% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 86% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 66% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 85% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 71% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 68% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 98% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 112% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 94% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 100% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 92% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 92% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 101% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 85% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 86% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 117% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 97% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 104% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 134% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 109% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 83% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 97% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 106% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 74% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 77% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 107% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 126% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 105% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 140% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 105% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 72% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 126% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 96% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 98% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 147% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 127% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 117% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 86% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 68% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 67% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 70% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 72% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 59% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 82% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 112% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 114% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 85% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 147% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 133% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 106% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 92% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 129% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 129% Analysis Date = 01/17/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 11/24/16 Pct Recovery = 87% Analysis Date = 11/24/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 11/03/16 Pct Recovery = 87% Analysis Date = 10/23/16 Pct Recovery = 86% Analysis Date = 10/23/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/09/16 Pct Recovery = 86% Analysis Date = 09/09/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/29/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/14/16 Pct Recovery = 85% Analysis Date = 06/14/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/13/16 Pct Recovery = 85% Analysis Date = 05/02/16 Pct Recovery = 85% Analysis Date = 05/02/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/21/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/20/16 Pct Recovery = 85% Analysis Date = 03/20/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/16/16 Pct Recovery = 84% Analysis Date = 02/16/16 Pct Recovery = 84% Analysis Date = 02/05/16 Pct Recovery = 84% Analysis Date = 02/05/16 Pct Recovery = 84% Analysis Date = 01/25/16 Pct Recovery = 84% Analysis Date = 01/25/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/14/16 Pct Recovery = 84% Analysis Date = 01/04/16 Pct Recovery = 84% Analysis Date = 01/04/16 Pct Recovery = 84% Analysis Date = 12/24/15 Pct Recovery = 84% Analysis Date = 12/24/15 Pct Recovery = 84% Analysis Date = 12/13/15 Pct Recovery = 84% Analysis Date = 12/13/15 Pct Recovery = 84% Analysis Date = 12/02/15 Pct Recovery = 84% Analysis Date = 12/02/15 Pct Recovery = 84% Analysis Date = 11/21/15 Pct Recovery = 84% Analysis Date = 11/21/15 Pct Recovery = 84% Analysis Date = 11/10/15 Pct Recovery = 84% Analysis Date = 11/10/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/30/15 Pct Recovery = 84% Analysis Date = 10/20/15 Pct Recovery = 84% Analysis Date = 10/20/15 Pct Recovery = 84% Analysis Date = 10/09/15 Pct Recovery = 84% Analysis Date = 10/09/15 Pct Recovery = 84% Analysis Date = 09/28/15 Pct Recovery = 84% Analysis Date = 09/28/15 Pct Recovery = 84% Analysis Date = 09/17/15 Pct Recovery = 83% Analysis Date = 09/17/15 Pct Recovery = 83% Analysis Date = 09/06/15 Pct Recovery = 83% Analysis Date = 09/06/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 83% Analysis Date = 08/26/15 Pct Recovery = 83% Analysis Date = 08/15/15 Pct Recovery = 83% Analysis Date = 08/15/15 Pct Recovery = 83% Analysis Date = 08/05/15 Pct Recovery = 83% Analysis Date = 08/05/15 Pct Recovery = 83% Analysis Date = 07/25/15 Pct Recovery = 83% Analysis Date = 07/25/15 Pct Recovery = 83% Analysis Date = 07/14/15 Pct Recovery = 83% Analysis Date = 07/14/15 Pct Recovery = 83% Analysis Date = 07/03/15 Pct Recovery = 83% Analysis Date = 07/03/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/22/15 Pct Recovery = 83% Analysis Date = 06/11/15 Pct Recovery = 83% Analysis Date = 06/11/15 Pct Recovery = 83% Analysis Date = 05/31/15 Pct Recovery = 83% Analysis Date = 05/31/15 Pct Recovery = 83% Analysis Date = 05/21/15 Pct Recovery = 83% Analysis Date = 05/21/15 Pct Recovery = 83% Analysis Date = 05/10/15 Pct Recovery = 83% Analysis Date = 05/10/15 Pct Recovery = 83% Analysis Date = 04/29/15 Pct Recovery = 83% Analysis Date = 04/29/15 Pct Recovery = 83% Analysis Date = 04/18/15 Pct Recovery = 83% Analysis Date = 04/18/15 Pct Recovery = 83% Analysis Date = 04/07/15 Pct Recovery = 83% Analysis Date = 04/07/15 Pct Recovery = 83% Analysis Date = 03/27/15 Pct Recovery = 83% Analysis Date = 03/27/15 Pct Recovery = 83% Analysis Date = 03/16/15 Pct Recovery = 82% Analysis Date = 03/16/15 Pct Recovery = 82% Analysis Date = 03/06/15 Pct Recovery = 82% Analysis Date = 03/06/15 Pct Recovery = 82% Analysis Date = 02/23/15 Pct Recovery = 82% Analysis Date = 02/23/15 Pct Recovery = 82% Analysis Date = 02/12/15 Pct Recovery = 82% Analysis Date = 02/12/15 Pct Recovery = 82% Analysis Date = 02/01/15 Pct Recovery = 82% Analysis Date = 02/01/15 Pct Recovery = 82% Analysis Date = 01/21/15 Pct Recovery = 82% Analysis Date = 01/21/15 Pct Recovery = 82% Analysis Date = 01/10/15 Pct Recovery = 82% Analysis Date = 01/10/15 Pct Recovery = 82% Analysis Date = 12/31/14 Pct Recovery = 82% Analysis Date = 12/31/14 Pct Recovery = 82% Analysis Date = 12/20/14 Pct Recovery = 82% Analysis Date = 12/20/14 Pct Recovery = 82% Analysis Date = 12/09/14 Pct Recovery = 82% Analysis Date = 12/09/14 Pct Recovery = 82% Analysis Date = 11/28/14 Pct Recovery = 82% Analysis Date = 11/28/14 Pct Recovery = 82% Analysis Date = 11/17/14 Pct Recovery = 82% Analysis Date = 11/17/14 Pct Recovery = 82% Analysis Date = 11/06/14 Pct Recovery = 82% Analysis Date = 11/06/14 Pct Recovery = 82% Analysis Date = 10/26/14 Pct Recovery = 82% Analysis Date = 10/26/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/16/14 Pct Recovery = 82% Analysis Date = 10/05/14 Pct Recovery = 83% Analysis Date = 10/05/14 Pct Recovery = 83% Analysis Date = 09/24/14 Pct Recovery = 83% Analysis Date = 09/24/14 Pct Recovery = 83% Analysis Date = 09/13/14 Pct Recovery = 83% Analysis Date = 09/13/14 Pct Recovery = 83% Analysis Date = 09/02/14 Pct Recovery = 83% Analysis Date = 09/02/14 Pct Recovery = 83% Analysis Date = 08/22/14 Pct Recovery = 83% Analysis Date = 08/22/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/11/14 Pct Recovery = 83% Analysis Date = 08/01/14 Pct Recovery = 83% Analysis Date = 08/01/14 Pct Recovery = 83% Analysis Date = 07/21/14 Pct Recovery = 84% Analysis Date = 07/21/14 Pct Recovery = 84% Analysis Date = 07/10/14 Pct Recovery = 84% Analysis Date = 07/10/14 Pct Recovery = 84% Analysis Date = 06/29/14 Pct Recovery = 84% Analysis Date = 06/29/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/18/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 06/07/14 Pct Recovery = 84% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/17/14 Pct Recovery = 85% Analysis Date = 05/17/14 Pct Recovery = 85% Analysis Date = 05/06/14 Pct Recovery = 85% Analysis Date = 05/06/14 Pct Recovery = 85% Analysis Date = 04/25/14 Pct Recovery = 85% Analysis Date = 04/25/14 Pct Recovery = 85% Analysis Date = 04/14/14 Pct Recovery = 86% Analysis Date = 04/14/14 Pct Recovery = 86% Analysis Date = 04/03/14 Pct Recovery = 86% Analysis Date = 04/03/14 Pct Recovery = 86% Analysis Date = 03/23/14 Pct Recovery = 86% Analysis Date = 03/23/14 Pct Recovery = 86% Analysis Date = 03/12/14 Pct Recovery = 87% Analysis Date = 03/12/14 Pct Recovery = 87% Analysis Date = 03/02/14 Pct Recovery = 87% Analysis Date = 03/02/14 Pct Recovery = 87% Analysis Date = 02/19/14 Pct Recovery = 87% Analysis Date = 02/19/14 Pct Recovery = 87% Analysis Date = 02/08/14 Pct Recovery = 88% Analysis Date = 02/08/14 Pct Recovery = 88% Analysis Date = 01/28/14 Pct Recovery = 88% Analysis Date = 01/28/14 Pct Recovery = 88% Analysis Date = 01/17/14 Pct Recovery = 88% Analysis Date = 01/17/14 Pct Recovery = 88% Analysis Date = 01/06/14 Pct Recovery = 88% Analysis Date = 01/06/14 Pct Recovery = 88% Analysis Date = 12/26/13 Pct Recovery = 89% Analysis Date = 12/26/13 Pct Recovery = 89% Analysis Date = 12/16/13 Pct Recovery = 89% Analysis Date = 12/16/13 Pct Recovery = 89% Analysis Date = 12/05/13 Pct Recovery = 89% Analysis Date = 12/05/13 Pct Recovery = 89% Analysis Date = 11/24/13 Pct Recovery = 90% Analysis Date = 11/24/13 Pct Recovery = 90% Analysis Date = 11/13/13 Pct Recovery = 90% Analysis Date = 11/13/13 Pct Recovery = 90% Analysis Date = 11/02/13 Pct Recovery = 90% Analysis Date = 11/02/13 Pct Recovery = 90% Analysis Date = 10/22/13 Pct Recovery = 91% Analysis Date = 10/22/13 Pct Recovery = 91% Analysis Date = 10/11/13 Pct Recovery = 91% Analysis Date = 10/11/13 Pct Recovery = 91% Analysis Date = 10/01/13 Pct Recovery = 92% Analysis Date = 10/01/13 Pct Recovery = 92% Analysis Date = 09/20/13 Pct Recovery = 92% Analysis Date = 09/20/13 Pct Recovery = 92% Analysis Date = 09/09/13 Pct Recovery = 93% Analysis Date = 09/09/13 Pct Recovery = 93% Analysis Date = 08/29/13 Pct Recovery = 93% Analysis Date = 08/29/13 Pct Recovery = 93% Analysis Date = 08/18/13 Pct Recovery = 94% Analysis Date = 08/18/13 Pct Recovery = 94% Analysis Date = 08/07/13 Pct Recovery = 94% Analysis Date = 08/07/13 Pct Recovery = 94% Analysis Date = 07/27/13 Pct Recovery = 95% Analysis Date = 07/27/13 Pct Recovery = 95% Analysis Date = 07/17/13 Pct Recovery = 95% Analysis Date = 07/17/13 Pct Recovery = 95% Analysis Date = 07/06/13 Pct Recovery = 95% Analysis Date = 07/06/13 Pct Recovery = 95% Analysis Date = 06/25/13 Pct Recovery = 96% Analysis Date = 06/25/13 Pct Recovery = 96% Analysis Date = 06/14/13 Pct Recovery = 96% Analysis Date = 06/14/13 Pct Recovery = 96% Analysis Date = 06/03/13 Pct Recovery = 97% Analysis Date = 06/03/13 Pct Recovery = 97% Analysis Date = 05/23/13 Pct Recovery = 97% Analysis Date = 05/23/13 Pct Recovery = 97% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/12/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 04/21/13 Pct Recovery = 98% Analysis Date = 04/21/13 Pct Recovery = 98% Analysis Date = 04/10/13 Pct Recovery = 99% Analysis Date = 04/10/13 Pct Recovery = 99% Analysis Date = 03/30/13 Pct Recovery = 99% Analysis Date = 03/30/13 Pct Recovery = 99% Analysis Date = 03/19/13 Pct Recovery = 99% Analysis Date = 03/19/13 Pct Recovery = 99% Analysis Date = 03/08/13 Pct Recovery = 100% Analysis Date = 03/08/13 Pct Recovery = 100% Analysis Date = 02/25/13 Pct Recovery = 100% Analysis Date = 02/25/13 Pct Recovery = 100% Analysis Date = 02/15/13 Pct Recovery = 101% Analysis Date = 02/15/13 Pct Recovery = 101% Analysis Date = 02/04/13 Pct Recovery = 101% Analysis Date = 02/04/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/24/13 Pct Recovery = 101% Analysis Date = 01/13/13 Pct Recovery = 102% Analysis Date = 01/13/13 Pct Recovery = 102% Analysis Date = 01/02/13 Pct Recovery = 102% Analysis Date = 01/02/13 Pct Recovery = 102% Analysis Date = 12/22/12 Pct Recovery = 102% Analysis Date = 12/22/12 Pct Recovery = 102% Analysis Date = 12/12/12 Pct Recovery = 102% Analysis Date = 12/12/12 Pct Recovery = 102% Analysis Date = 12/01/12 Pct Recovery = 102% Analysis Date = 12/01/12 Pct Recovery = 102% Analysis Date = 11/20/12 Pct Recovery = 103% Analysis Date = 11/20/12 Pct Recovery = 103% Analysis Date = 11/09/12 Pct Recovery = 103% Analysis Date = 11/09/12 Pct Recovery = 103% Analysis Date = 10/29/12 Pct Recovery = 103% Analysis Date = 10/29/12 Pct Recovery = 103% Analysis Date = 10/18/12 Pct Recovery = 103% Analysis Date = 10/18/12 Pct Recovery = 103% Analysis Date = 10/07/12 Pct Recovery = 103% Analysis Date = 10/07/12 Pct Recovery = 103% Analysis Date = 09/27/12 Pct Recovery = 103% Analysis Date = 09/27/12 Pct Recovery = 103% Analysis Date = 09/16/12 Pct Recovery = 103% Analysis Date = 09/16/12 Pct Recovery = 103% Analysis Date = 09/05/12 Pct Recovery = 103% Analysis Date = 09/05/12 Pct Recovery = 103% Analysis Date = 08/25/12 Pct Recovery = 103% Analysis Date = 08/25/12 Pct Recovery = 103% Analysis Date = 08/14/12 Pct Recovery = 103% Analysis Date = 08/14/12 Pct Recovery = 103% Analysis Date = 08/03/12 Pct Recovery = 103% Analysis Date = 08/03/12 Pct Recovery = 103% Analysis Date = 07/23/12 Pct Recovery = 103% Analysis Date = 07/23/12 Pct Recovery = 103% Analysis Date = 07/13/12 Pct Recovery = 103% Analysis Date = 07/13/12 Pct Recovery = 103% Analysis Date = 07/02/12 Pct Recovery = 103% Analysis Date = 07/02/12 Pct Recovery = 103% Analysis Date = 06/21/12 Pct Recovery = 103% Analysis Date = 06/21/12 Pct Recovery = 103% Analysis Date = 06/10/12 Pct Recovery = 103% Analysis Date = 06/10/12 Pct Recovery = 103% Analysis Date = 05/30/12 Pct Recovery = 103% Analysis Date = 05/30/12 Pct Recovery = 103% Analysis Date = 05/19/12 Pct Recovery = 103% Analysis Date = 05/19/12 Pct Recovery = 103% Analysis Date = 05/08/12 Pct Recovery = 103% Analysis Date = 05/08/12 Pct Recovery = 103% Analysis Date = 04/28/12 Pct Recovery = 103% Analysis Date = 04/28/12 Pct Recovery = 103% Analysis Date = 04/17/12 Pct Recovery = 103% Analysis Date = 04/17/12 Pct Recovery = 103% Analysis Date = 04/06/12 Pct Recovery = 103% Analysis Date = 04/06/12 Pct Recovery = 103% Analysis Date = 03/26/12 Pct Recovery = 103% Analysis Date = 03/26/12 Pct Recovery = 103% Analysis Date = 03/15/12 Pct Recovery = 103% Analysis Date = 03/15/12 Pct Recovery = 103% Analysis Date = 03/04/12 Pct Recovery = 103% Analysis Date = 03/04/12 Pct Recovery = 103% Analysis Date = 02/22/12 Pct Recovery = 103% Analysis Date = 02/22/12 Pct Recovery = 103% Analysis Date = 02/12/12 Pct Recovery = 103% Analysis Date = 02/12/12 Pct Recovery = 103% Analysis Date = 02/01/12 Pct Recovery = 103% Analysis Date = 02/01/12 Pct Recovery = 103% Analysis Date = 01/21/12 Pct Recovery = 103% Analysis Date = 01/21/12 Pct Recovery = 103% Analysis Date = 01/10/12 Pct Recovery = 103% Analysis Date = 01/10/12 Pct Recovery = 103% Analysis Date = 12/30/11 Pct Recovery = 103% Analysis Date = 12/30/11 Pct Recovery = 103% Analysis Date = 12/19/11 Pct Recovery = 103% Analysis Date = 12/19/11 Pct Recovery = 103% Analysis Date = 12/08/11 Pct Recovery = 103% Analysis Date = 12/08/11 Pct Recovery = 103% Analysis Date = 11/28/11 Pct Recovery = 103% Analysis Date = 11/28/11 Pct Recovery = 103% Analysis Date = 11/17/11 Pct Recovery = 103% Analysis Date = 11/17/11 Pct Recovery = 103% Analysis Date = 11/06/11 Pct Recovery = 103% Analysis Date = 11/06/11 Pct Recovery = 103% Analysis Date = 10/26/11 Pct Recovery = 103% Analysis Date = 10/26/11 Pct Recovery = 103% Analysis Date = 10/15/11 Pct Recovery = 103% Analysis Date = 10/15/11 Pct Recovery = 103% Analysis Date = 10/04/11 Pct Recovery = 103% Analysis Date = 10/04/11 Pct Recovery = 103% Analysis Date = 09/23/11 Pct Recovery = 103% Analysis Date = 09/23/11 Pct Recovery = 103% Analysis Date = 09/13/11 Pct Recovery = 103% Analysis Date = 09/13/11 Pct Recovery = 103% Analysis Date = 09/02/11 Pct Recovery = 103% Analysis Date = 09/02/11 Pct Recovery = 103% Analysis Date = 08/22/11 Pct Recovery = 103% Analysis Date = 08/22/11 Pct Recovery = 103% Analysis Date = 08/11/11 Pct Recovery = 103% Analysis Date = 08/11/11 Pct Recovery = 103% Analysis Date = 07/31/11 Pct Recovery = 103% Analysis Date = 07/31/11 Pct Recovery = 103% Analysis Date = 07/20/11 Pct Recovery = 103% Analysis Date = 07/20/11 Pct Recovery = 103% Analysis Date = 07/09/11 Pct Recovery = 103% Analysis Date = 07/09/11 Pct Recovery = 103% Analysis Date = 06/29/11 Pct Recovery = 103% Analysis Date = 06/29/11 Pct Recovery = 103% Analysis Date = 06/18/11 Pct Recovery = 103% Analysis Date = 06/18/11 Pct Recovery = 103% Analysis Date = 06/07/11 Pct Recovery = 103% Analysis Date = 06/07/11 Pct Recovery = 103% Analysis Date = 05/27/11 Pct Recovery = 103% Analysis Date = 05/27/11 Pct Recovery = 103% Analysis Date = 05/16/11 Pct Recovery = 103% Analysis Date = 05/16/11 Pct Recovery = 103% Analysis Date = 05/05/11 Pct Recovery = 103% Analysis Date = 05/05/11 Pct Recovery = 103% Analysis Date = 04/24/11 Pct Recovery = 103% Analysis Date = 04/24/11 Pct Recovery = 103% Analysis Date = 04/14/11 Pct Recovery = 103% Analysis Date = 04/14/11 Pct Recovery = 103% Analysis Date = 04/03/11 Pct Recovery = 103% Analysis Date = 04/03/11 Pct Recovery = 103% Analysis Date = 03/23/11 Pct Recovery = 103% Analysis Date = 03/23/11 Pct Recovery = 103% Analysis Date = 03/12/11 Pct Recovery = 103% Analysis Date = 03/12/11 Pct Recovery = 103% Analysis Date = 03/01/11 Pct Recovery = 102% Analysis Date = 03/01/11 Pct Recovery = 102% Analysis Date = 02/18/11 Pct Recovery = 102% Analysis Date = 02/18/11 Pct Recovery = 102% Analysis Date = 02/08/11 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PARAOXON-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 93% 22% 92% 22%
Total 87 93% 22% 92% 22%

Sample Statistics
PARAOXON-METHYL

Characteristic N % % Basis
Plotted 87 97% Spiked
Estimated Values 87 97% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 90 .  
False Negatives 3 3% 3 out of 90
Not Spiked 79 .  
False Positives 0 0% 0 out of 79

BQS OBSP Determination:
PARATHION-METHYL
METHOD: 2033 , TESTIDCODE: 82667GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 82% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 75% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 79% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 95% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 92% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 89% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 90% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 96% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 129% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 118% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 142% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 100% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 88% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 99% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 93% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 117% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 75% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 97% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 133% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 91% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 90% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 95% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 102% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 111% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 98% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 104% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 79% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 123% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 90% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 96% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 102% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 86% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 103% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 141% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 104% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 141% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 92% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 83% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 100% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 116% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 136% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 93% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 108% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 117% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 107% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 108% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 86% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 101% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 120% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 96% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 80% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 84% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 148% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 107% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 116% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 151% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 144% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 127% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 107% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 109% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 103% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 108% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 135% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 98% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 100% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 107% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 103% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 135% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 92% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 92% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 95% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 118% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 106% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 117% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 130% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 91% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 103% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 116% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 102% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 114% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 116% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 112% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 106% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 176% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 158% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 01/18/17 Pct Recovery = 110% Analysis Date = 01/07/17 Pct Recovery = 110% Analysis Date = 01/07/17 Pct Recovery = 110% Analysis Date = 12/27/16 Pct Recovery = 110% Analysis Date = 12/27/16 Pct Recovery = 110% Analysis Date = 12/16/16 Pct Recovery = 110% Analysis Date = 12/16/16 Pct Recovery = 110% Analysis Date = 12/05/16 Pct Recovery = 110% Analysis Date = 12/05/16 Pct Recovery = 110% Analysis Date = 11/24/16 Pct Recovery = 110% Analysis Date = 11/24/16 Pct Recovery = 110% Analysis Date = 11/14/16 Pct Recovery = 110% Analysis Date = 11/14/16 Pct Recovery = 110% Analysis Date = 11/03/16 Pct Recovery = 110% Analysis Date = 11/03/16 Pct Recovery = 110% Analysis Date = 10/23/16 Pct Recovery = 110% Analysis Date = 10/23/16 Pct Recovery = 110% Analysis Date = 10/12/16 Pct Recovery = 110% Analysis Date = 10/12/16 Pct Recovery = 110% Analysis Date = 10/01/16 Pct Recovery = 110% Analysis Date = 10/01/16 Pct Recovery = 110% Analysis Date = 09/20/16 Pct Recovery = 110% Analysis Date = 09/20/16 Pct Recovery = 110% Analysis Date = 09/10/16 Pct Recovery = 110% Analysis Date = 09/10/16 Pct Recovery = 110% Analysis Date = 08/30/16 Pct Recovery = 110% Analysis Date = 08/30/16 Pct Recovery = 110% Analysis Date = 08/19/16 Pct Recovery = 110% Analysis Date = 08/19/16 Pct Recovery = 110% Analysis Date = 08/08/16 Pct Recovery = 110% Analysis Date = 08/08/16 Pct Recovery = 110% Analysis Date = 07/28/16 Pct Recovery = 110% Analysis Date = 07/28/16 Pct Recovery = 110% Analysis Date = 07/17/16 Pct Recovery = 110% Analysis Date = 07/17/16 Pct Recovery = 110% Analysis Date = 07/07/16 Pct Recovery = 110% Analysis Date = 07/07/16 Pct Recovery = 110% Analysis Date = 06/26/16 Pct Recovery = 110% Analysis Date = 06/26/16 Pct Recovery = 110% Analysis Date = 06/15/16 Pct Recovery = 110% Analysis Date = 06/15/16 Pct Recovery = 110% Analysis Date = 06/04/16 Pct Recovery = 110% Analysis Date = 06/04/16 Pct Recovery = 110% Analysis Date = 05/24/16 Pct Recovery = 110% Analysis Date = 05/24/16 Pct Recovery = 110% Analysis Date = 05/14/16 Pct Recovery = 110% Analysis Date = 05/14/16 Pct Recovery = 110% Analysis Date = 05/03/16 Pct Recovery = 110% Analysis Date = 05/03/16 Pct Recovery = 110% Analysis Date = 04/22/16 Pct Recovery = 109% Analysis Date = 04/22/16 Pct Recovery = 109% Analysis Date = 04/11/16 Pct Recovery = 109% Analysis Date = 04/11/16 Pct Recovery = 109% Analysis Date = 03/31/16 Pct Recovery = 109% Analysis Date = 03/31/16 Pct Recovery = 109% Analysis Date = 03/20/16 Pct Recovery = 109% Analysis Date = 03/20/16 Pct Recovery = 109% Analysis Date = 03/10/16 Pct Recovery = 109% Analysis Date = 03/10/16 Pct Recovery = 109% Analysis Date = 02/28/16 Pct Recovery = 109% Analysis Date = 02/28/16 Pct Recovery = 109% Analysis Date = 02/17/16 Pct Recovery = 109% Analysis Date = 02/17/16 Pct Recovery = 109% Analysis Date = 02/06/16 Pct Recovery = 109% Analysis Date = 02/06/16 Pct Recovery = 109% Analysis Date = 01/26/16 Pct Recovery = 109% Analysis Date = 01/26/16 Pct Recovery = 109% Analysis Date = 01/15/16 Pct Recovery = 109% Analysis Date = 01/15/16 Pct Recovery = 109% Analysis Date = 01/05/16 Pct Recovery = 109% Analysis Date = 01/05/16 Pct Recovery = 109% Analysis Date = 12/25/15 Pct Recovery = 109% Analysis Date = 12/25/15 Pct Recovery = 109% Analysis Date = 12/14/15 Pct Recovery = 109% Analysis Date = 12/14/15 Pct Recovery = 109% Analysis Date = 12/03/15 Pct Recovery = 109% Analysis Date = 12/03/15 Pct Recovery = 109% Analysis Date = 11/22/15 Pct Recovery = 109% Analysis Date = 11/22/15 Pct Recovery = 109% Analysis Date = 11/12/15 Pct Recovery = 109% Analysis Date = 11/12/15 Pct Recovery = 109% Analysis Date = 11/01/15 Pct Recovery = 109% Analysis Date = 11/01/15 Pct Recovery = 109% Analysis Date = 10/21/15 Pct Recovery = 109% Analysis Date = 10/21/15 Pct Recovery = 109% Analysis Date = 10/10/15 Pct Recovery = 109% Analysis Date = 10/10/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/29/15 Pct Recovery = 109% Analysis Date = 09/18/15 Pct Recovery = 109% Analysis Date = 09/18/15 Pct Recovery = 109% Analysis Date = 09/08/15 Pct Recovery = 109% Analysis Date = 09/08/15 Pct Recovery = 109% Analysis Date = 08/28/15 Pct Recovery = 108% Analysis Date = 08/28/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 108% Analysis Date = 08/17/15 Pct Recovery = 108% Analysis Date = 08/06/15 Pct Recovery = 108% Analysis Date = 08/06/15 Pct Recovery = 108% Analysis Date = 07/26/15 Pct Recovery = 108% Analysis Date = 07/26/15 Pct Recovery = 108% Analysis Date = 07/15/15 Pct Recovery = 108% Analysis Date = 07/15/15 Pct Recovery = 108% Analysis Date = 07/05/15 Pct Recovery = 108% Analysis Date = 07/05/15 Pct Recovery = 108% Analysis Date = 06/24/15 Pct Recovery = 108% Analysis Date = 06/24/15 Pct Recovery = 108% Analysis Date = 06/13/15 Pct Recovery = 108% Analysis Date = 06/13/15 Pct Recovery = 108% Analysis Date = 06/02/15 Pct Recovery = 108% Analysis Date = 06/02/15 Pct Recovery = 108% Analysis Date = 05/22/15 Pct Recovery = 108% Analysis Date = 05/22/15 Pct Recovery = 108% Analysis Date = 05/11/15 Pct Recovery = 108% Analysis Date = 05/11/15 Pct Recovery = 108% Analysis Date = 05/01/15 Pct Recovery = 108% Analysis Date = 05/01/15 Pct Recovery = 108% Analysis Date = 04/20/15 Pct Recovery = 108% Analysis Date = 04/20/15 Pct Recovery = 108% Analysis Date = 04/09/15 Pct Recovery = 108% Analysis Date = 04/09/15 Pct Recovery = 108% Analysis Date = 03/29/15 Pct Recovery = 108% Analysis Date = 03/29/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/08/15 Pct Recovery = 108% Analysis Date = 03/08/15 Pct Recovery = 108% Analysis Date = 02/25/15 Pct Recovery = 108% Analysis Date = 02/25/15 Pct Recovery = 108% Analysis Date = 02/14/15 Pct Recovery = 108% Analysis Date = 02/14/15 Pct Recovery = 108% Analysis Date = 02/03/15 Pct Recovery = 108% Analysis Date = 02/03/15 Pct Recovery = 108% Analysis Date = 01/23/15 Pct Recovery = 108% Analysis Date = 01/23/15 Pct Recovery = 108% Analysis Date = 01/12/15 Pct Recovery = 108% Analysis Date = 01/12/15 Pct Recovery = 108% Analysis Date = 01/02/15 Pct Recovery = 108% Analysis Date = 01/02/15 Pct Recovery = 108% Analysis Date = 12/22/14 Pct Recovery = 108% Analysis Date = 12/22/14 Pct Recovery = 108% Analysis Date = 12/11/14 Pct Recovery = 108% Analysis Date = 12/11/14 Pct Recovery = 108% Analysis Date = 11/30/14 Pct Recovery = 108% Analysis Date = 11/30/14 Pct Recovery = 108% Analysis Date = 11/19/14 Pct Recovery = 108% Analysis Date = 11/19/14 Pct Recovery = 108% Analysis Date = 11/08/14 Pct Recovery = 108% Analysis Date = 11/08/14 Pct Recovery = 108% Analysis Date = 10/29/14 Pct Recovery = 108% Analysis Date = 10/29/14 Pct Recovery = 108% Analysis Date = 10/18/14 Pct Recovery = 108% Analysis Date = 10/18/14 Pct Recovery = 108% Analysis Date = 10/07/14 Pct Recovery = 108% Analysis Date = 10/07/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/26/14 Pct Recovery = 108% Analysis Date = 09/15/14 Pct Recovery = 108% Analysis Date = 09/15/14 Pct Recovery = 108% Analysis Date = 09/05/14 Pct Recovery = 108% Analysis Date = 09/05/14 Pct Recovery = 108% Analysis Date = 08/25/14 Pct Recovery = 108% Analysis Date = 08/25/14 Pct Recovery = 108% Analysis Date = 08/14/14 Pct Recovery = 108% Analysis Date = 08/14/14 Pct Recovery = 108% Analysis Date = 08/03/14 Pct Recovery = 108% Analysis Date = 08/03/14 Pct Recovery = 108% Analysis Date = 07/23/14 Pct Recovery = 108% Analysis Date = 07/23/14 Pct Recovery = 108% Analysis Date = 07/12/14 Pct Recovery = 108% Analysis Date = 07/12/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 07/02/14 Pct Recovery = 108% Analysis Date = 06/21/14 Pct Recovery = 108% Analysis Date = 06/21/14 Pct Recovery = 108% Analysis Date = 06/10/14 Pct Recovery = 108% Analysis Date = 06/10/14 Pct Recovery = 108% Analysis Date = 05/30/14 Pct Recovery = 108% Analysis Date = 05/30/14 Pct Recovery = 108% Analysis Date = 05/19/14 Pct Recovery = 107% Analysis Date = 05/19/14 Pct Recovery = 107% Analysis Date = 05/08/14 Pct Recovery = 107% Analysis Date = 05/08/14 Pct Recovery = 107% Analysis Date = 04/28/14 Pct Recovery = 107% Analysis Date = 04/28/14 Pct Recovery = 107% Analysis Date = 04/17/14 Pct Recovery = 107% Analysis Date = 04/17/14 Pct Recovery = 107% Analysis Date = 04/06/14 Pct Recovery = 106% Analysis Date = 04/06/14 Pct Recovery = 106% Analysis Date = 03/26/14 Pct Recovery = 106% Analysis Date = 03/26/14 Pct Recovery = 106% Analysis Date = 03/15/14 Pct Recovery = 106% Analysis Date = 03/15/14 Pct Recovery = 106% Analysis Date = 03/04/14 Pct Recovery = 106% Analysis Date = 03/04/14 Pct Recovery = 106% Analysis Date = 02/22/14 Pct Recovery = 106% Analysis Date = 02/22/14 Pct Recovery = 106% Analysis Date = 02/11/14 Pct Recovery = 105% Analysis Date = 02/11/14 Pct Recovery = 105% Analysis Date = 01/31/14 Pct Recovery = 105% Analysis Date = 01/31/14 Pct Recovery = 105% Analysis Date = 01/20/14 Pct Recovery = 105% Analysis Date = 01/20/14 Pct Recovery = 105% Analysis Date = 01/09/14 Pct Recovery = 105% Analysis Date = 01/09/14 Pct Recovery = 105% Analysis Date = 12/30/13 Pct Recovery = 105% Analysis Date = 12/30/13 Pct Recovery = 105% Analysis Date = 12/19/13 Pct Recovery = 105% Analysis Date = 12/19/13 Pct Recovery = 105% Analysis Date = 12/08/13 Pct Recovery = 105% Analysis Date = 12/08/13 Pct Recovery = 105% Analysis Date = 11/27/13 Pct Recovery = 105% Analysis Date = 11/27/13 Pct Recovery = 105% Analysis Date = 11/16/13 Pct Recovery = 104% Analysis Date = 11/16/13 Pct Recovery = 104% Analysis Date = 11/05/13 Pct Recovery = 104% Analysis Date = 11/05/13 Pct Recovery = 104% Analysis Date = 10/26/13 Pct Recovery = 104% Analysis Date = 10/26/13 Pct Recovery = 104% Analysis Date = 10/15/13 Pct Recovery = 104% Analysis Date = 10/15/13 Pct Recovery = 104% Analysis Date = 10/04/13 Pct Recovery = 104% Analysis Date = 10/04/13 Pct Recovery = 104% Analysis Date = 09/23/13 Pct Recovery = 104% Analysis Date = 09/23/13 Pct Recovery = 104% Analysis Date = 09/12/13 Pct Recovery = 104% Analysis Date = 09/12/13 Pct Recovery = 104% Analysis Date = 09/01/13 Pct Recovery = 104% Analysis Date = 09/01/13 Pct Recovery = 104% Analysis Date = 08/22/13 Pct Recovery = 104% Analysis Date = 08/22/13 Pct Recovery = 104% Analysis Date = 08/11/13 Pct Recovery = 104% Analysis Date = 08/11/13 Pct Recovery = 104% Analysis Date = 07/31/13 Pct Recovery = 104% Analysis Date = 07/31/13 Pct Recovery = 104% Analysis Date = 07/20/13 Pct Recovery = 104% Analysis Date = 07/20/13 Pct Recovery = 104% Analysis Date = 07/09/13 Pct Recovery = 104% Analysis Date = 07/09/13 Pct Recovery = 104% Analysis Date = 06/29/13 Pct Recovery = 104% Analysis Date = 06/29/13 Pct Recovery = 104% Analysis Date = 06/18/13 Pct Recovery = 104% Analysis Date = 06/18/13 Pct Recovery = 104% Analysis Date = 06/07/13 Pct Recovery = 104% Analysis Date = 06/07/13 Pct Recovery = 104% Analysis Date = 05/27/13 Pct Recovery = 104% Analysis Date = 05/27/13 Pct Recovery = 104% Analysis Date = 05/16/13 Pct Recovery = 104% Analysis Date = 05/16/13 Pct Recovery = 104% Analysis Date = 05/05/13 Pct Recovery = 104% Analysis Date = 05/05/13 Pct Recovery = 104% Analysis Date = 04/25/13 Pct Recovery = 104% Analysis Date = 04/25/13 Pct Recovery = 104% Analysis Date = 04/14/13 Pct Recovery = 104% Analysis Date = 04/14/13 Pct Recovery = 104% Analysis Date = 04/03/13 Pct Recovery = 104% Analysis Date = 04/03/13 Pct Recovery = 104% Analysis Date = 03/23/13 Pct Recovery = 104% Analysis Date = 03/23/13 Pct Recovery = 104% Analysis Date = 03/12/13 Pct Recovery = 104% Analysis Date = 03/12/13 Pct Recovery = 104% Analysis Date = 03/01/13 Pct Recovery = 104% Analysis Date = 03/01/13 Pct Recovery = 104% Analysis Date = 02/19/13 Pct Recovery = 104% Analysis Date = 02/19/13 Pct Recovery = 104% Analysis Date = 02/08/13 Pct Recovery = 104% Analysis Date = 02/08/13 Pct Recovery = 104% Analysis Date = 01/28/13 Pct Recovery = 104% Analysis Date = 01/28/13 Pct Recovery = 104% Analysis Date = 01/17/13 Pct Recovery = 104% Analysis Date = 01/17/13 Pct Recovery = 104% Analysis Date = 01/06/13 Pct Recovery = 104% Analysis Date = 01/06/13 Pct Recovery = 104% Analysis Date = 12/26/12 Pct Recovery = 104% Analysis Date = 12/26/12 Pct Recovery = 104% Analysis Date = 12/16/12 Pct Recovery = 104% Analysis Date = 12/16/12 Pct Recovery = 104% Analysis Date = 12/05/12 Pct Recovery = 104% Analysis Date = 12/05/12 Pct Recovery = 104% Analysis Date = 11/24/12 Pct Recovery = 104% Analysis Date = 11/24/12 Pct Recovery = 104% Analysis Date = 11/13/12 Pct Recovery = 104% Analysis Date = 11/13/12 Pct Recovery = 104% Analysis Date = 11/02/12 Pct Recovery = 104% Analysis Date = 11/02/12 Pct Recovery = 104% Analysis Date = 10/23/12 Pct Recovery = 104% Analysis Date = 10/23/12 Pct Recovery = 104% Analysis Date = 10/12/12 Pct Recovery = 104% Analysis Date = 10/12/12 Pct Recovery = 104% Analysis Date = 10/01/12 Pct Recovery = 104% Analysis Date = 10/01/12 Pct Recovery = 104% Analysis Date = 09/20/12 Pct Recovery = 104% Analysis Date = 09/20/12 Pct Recovery = 104% Analysis Date = 09/09/12 Pct Recovery = 104% Analysis Date = 09/09/12 Pct Recovery = 104% Analysis Date = 08/29/12 Pct Recovery = 104% Analysis Date = 08/29/12 Pct Recovery = 104% Analysis Date = 08/19/12 Pct Recovery = 104% Analysis Date = 08/19/12 Pct Recovery = 104% Analysis Date = 08/08/12 Pct Recovery = 104% Analysis Date = 08/08/12 Pct Recovery = 104% Analysis Date = 07/28/12 Pct Recovery = 104% Analysis Date = 07/28/12 Pct Recovery = 104% Analysis Date = 07/17/12 Pct Recovery = 104% Analysis Date = 07/17/12 Pct Recovery = 104% Analysis Date = 07/06/12 Pct Recovery = 104% Analysis Date = 07/06/12 Pct Recovery = 104% Analysis Date = 06/25/12 Pct Recovery = 104% Analysis Date = 06/25/12 Pct Recovery = 104% Analysis Date = 06/15/12 Pct Recovery = 104% Analysis Date = 06/15/12 Pct Recovery = 104% Analysis Date = 06/04/12 Pct Recovery = 104% Analysis Date = 06/04/12 Pct Recovery = 104% Analysis Date = 05/24/12 Pct Recovery = 104% Analysis Date = 05/24/12 Pct Recovery = 104% Analysis Date = 05/13/12 Pct Recovery = 105% Analysis Date = 05/13/12 Pct Recovery = 105% Analysis Date = 05/02/12 Pct Recovery = 105% Analysis Date = 05/02/12 Pct Recovery = 105% Analysis Date = 04/22/12 Pct Recovery = 105% Analysis Date = 04/22/12 Pct Recovery = 105% Analysis Date = 04/11/12 Pct Recovery = 105% Analysis Date = 04/11/12 Pct Recovery = 105% Analysis Date = 03/31/12 Pct Recovery = 105% Analysis Date = 03/31/12 Pct Recovery = 105% Analysis Date = 03/20/12 Pct Recovery = 105% Analysis Date = 03/20/12 Pct Recovery = 105% Analysis Date = 03/09/12 Pct Recovery = 105% Analysis Date = 03/09/12 Pct Recovery = 105% Analysis Date = 02/27/12 Pct Recovery = 105% Analysis Date = 02/27/12 Pct Recovery = 105% Analysis Date = 02/17/12 Pct Recovery = 105% Analysis Date = 02/17/12 Pct Recovery = 105% Analysis Date = 02/06/12 Pct Recovery = 106% Analysis Date = 02/06/12 Pct Recovery = 106% Analysis Date = 01/26/12 Pct Recovery = 106% Analysis Date = 01/26/12 Pct Recovery = 106% Analysis Date = 01/15/12 Pct Recovery = 106% Analysis Date = 01/15/12 Pct Recovery = 106% Analysis Date = 01/04/12 Pct Recovery = 106% Analysis Date = 01/04/12 Pct Recovery = 106% Analysis Date = 12/24/11 Pct Recovery = 106% Analysis Date = 12/24/11 Pct Recovery = 106% Analysis Date = 12/14/11 Pct Recovery = 106% Analysis Date = 12/14/11 Pct Recovery = 106% Analysis Date = 12/03/11 Pct Recovery = 106% Analysis Date = 12/03/11 Pct Recovery = 106% Analysis Date = 11/22/11 Pct Recovery = 107% Analysis Date = 11/22/11 Pct Recovery = 107% Analysis Date = 11/11/11 Pct Recovery = 107% Analysis Date = 11/11/11 Pct Recovery = 107% Analysis Date = 10/31/11 Pct Recovery = 107% Analysis Date = 10/31/11 Pct Recovery = 107% Analysis Date = 10/20/11 Pct Recovery = 107% Analysis Date = 10/20/11 Pct Recovery = 107% Analysis Date = 10/10/11 Pct Recovery = 107% Analysis Date = 10/10/11 Pct Recovery = 107% Analysis Date = 09/29/11 Pct Recovery = 107% Analysis Date = 09/29/11 Pct Recovery = 107% Analysis Date = 09/18/11 Pct Recovery = 107% Analysis Date = 09/18/11 Pct Recovery = 107% Analysis Date = 09/07/11 Pct Recovery = 108% Analysis Date = 09/07/11 Pct Recovery = 108% Analysis Date = 08/27/11 Pct Recovery = 108% Analysis Date = 08/27/11 Pct Recovery = 108% Analysis Date = 08/17/11 Pct Recovery = 108% Analysis Date = 08/17/11 Pct Recovery = 108% Analysis Date = 08/06/11 Pct Recovery = 108% Analysis Date = 08/06/11 Pct Recovery = 108% Analysis Date = 07/26/11 Pct Recovery = 108% Analysis Date = 07/26/11 Pct Recovery = 108% Analysis Date = 07/15/11 Pct Recovery = 108% Analysis Date = 07/15/11 Pct Recovery = 108% Analysis Date = 07/04/11 Pct Recovery = 108% Analysis Date = 07/04/11 Pct Recovery = 108% Analysis Date = 06/23/11 Pct Recovery = 109% Analysis Date = 06/23/11 Pct Recovery = 109% Analysis Date = 06/13/11 Pct Recovery = 109% Analysis Date = 06/13/11 Pct Recovery = 109% Analysis Date = 06/02/11 Pct Recovery = 109% Analysis Date = 06/02/11 Pct Recovery = 109% Analysis Date = 05/22/11 Pct Recovery = 109% Analysis Date = 05/22/11 Pct Recovery = 109% Analysis Date = 05/11/11 Pct Recovery = 109% Analysis Date = 05/11/11 Pct Recovery = 109% Analysis Date = 04/30/11 Pct Recovery = 109% Analysis Date = 04/30/11 Pct Recovery = 109% Analysis Date = 04/19/11 Pct Recovery = 110% Analysis Date = 04/19/11 Pct Recovery = 110% Analysis Date = 04/09/11 Pct Recovery = 110% Analysis Date = 04/09/11 Pct Recovery = 110% Analysis Date = 03/29/11 Pct Recovery = 110% Analysis Date = 03/29/11 Pct Recovery = 110% Analysis Date = 03/18/11 Pct Recovery = 110% Analysis Date = 03/18/11 Pct Recovery = 110% Analysis Date = 03/07/11 Pct Recovery = 110% Analysis Date = 03/07/11 Pct Recovery = 110% Analysis Date = 02/24/11 Pct Recovery = 110% Analysis Date = 02/24/11 Pct Recovery = 110% Analysis Date = 02/14/11 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PARATHION-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 107% 20% 103% 17%
Total 89 107% 20% 103% 17%

Sample Statistics
PARATHION-METHYL

Characteristic N % % Basis
Plotted 89 99% Spiked
Estimated Values 9 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 90 .  
False Negatives 1 1% 1 out of 90
Not Spiked 71 .  
False Positives 0 0% 0 out of 71

BQS OBSP Determination:
PENDIMETHALIN
METHOD: 2033 , TESTIDCODE: 82683GCM35
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 78% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 79% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 77% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 78% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 73% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 93% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 78% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 113% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 97% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 92% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 97% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 81% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 80% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 98% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 80% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 79% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 73% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 70% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 91% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 89% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 105% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 156% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 73% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 88% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 90% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 89% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 84% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 81% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 93% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 58% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 126% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 95% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 88% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 138% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 117% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 101% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 103% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 104% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 129% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 101% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 95% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 125% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 90% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 102% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 84% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 96% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 82% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 98% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 101% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 133% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 83% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 91% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 86% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 76% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 126% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 132% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 114% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 90% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 69% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 88% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 81% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 84% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 76% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 81% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 109% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 74% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 111% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 109% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 118% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 121% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 92% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 147% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 86% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 123% Analysis Date = 12/19/16 Pct Recovery = 91% Analysis Date = 12/09/16 Pct Recovery = 91% Analysis Date = 12/09/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 11/07/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 91% Analysis Date = 10/27/16 Pct Recovery = 91% Analysis Date = 10/16/16 Pct Recovery = 91% Analysis Date = 10/16/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 10/06/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/25/16 Pct Recovery = 91% Analysis Date = 09/14/16 Pct Recovery = 91% Analysis Date = 09/14/16 Pct Recovery = 91% Analysis Date = 09/03/16 Pct Recovery = 91% Analysis Date = 09/03/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/24/16 Pct Recovery = 91% Analysis Date = 08/13/16 Pct Recovery = 91% Analysis Date = 08/13/16 Pct Recovery = 91% Analysis Date = 08/02/16 Pct Recovery = 91% Analysis Date = 08/02/16 Pct Recovery = 91% Analysis Date = 07/23/16 Pct Recovery = 91% Analysis Date = 07/23/16 Pct Recovery = 91% Analysis Date = 07/12/16 Pct Recovery = 91% Analysis Date = 07/12/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/10/16 Pct Recovery = 91% Analysis Date = 06/10/16 Pct Recovery = 91% Analysis Date = 05/30/16 Pct Recovery = 91% Analysis Date = 05/30/16 Pct Recovery = 91% Analysis Date = 05/19/16 Pct Recovery = 91% Analysis Date = 05/19/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 04/28/16 Pct Recovery = 91% Analysis Date = 04/28/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 04/06/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/05/16 Pct Recovery = 91% Analysis Date = 03/05/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 91% Analysis Date = 02/13/16 Pct Recovery = 91% Analysis Date = 02/02/16 Pct Recovery = 91% Analysis Date = 02/02/16 Pct Recovery = 91% Analysis Date = 01/22/16 Pct Recovery = 90% Analysis Date = 01/22/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/12/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 01/01/16 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/21/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 12/11/15 Pct Recovery = 90% Analysis Date = 11/30/15 Pct Recovery = 90% Analysis Date = 11/30/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/19/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 90% Analysis Date = 11/09/15 Pct Recovery = 90% Analysis Date = 10/29/15 Pct Recovery = 90% Analysis Date = 10/29/15 Pct Recovery = 90% Analysis Date = 10/18/15 Pct Recovery = 90% Analysis Date = 10/18/15 Pct Recovery = 90% Analysis Date = 10/07/15 Pct Recovery = 90% Analysis Date = 10/07/15 Pct Recovery = 90% Analysis Date = 09/27/15 Pct Recovery = 90% Analysis Date = 09/27/15 Pct Recovery = 90% Analysis Date = 09/16/15 Pct Recovery = 90% Analysis Date = 09/16/15 Pct Recovery = 90% Analysis Date = 09/05/15 Pct Recovery = 90% Analysis Date = 09/05/15 Pct Recovery = 90% Analysis Date = 08/26/15 Pct Recovery = 90% Analysis Date = 08/26/15 Pct Recovery = 90% Analysis Date = 08/15/15 Pct Recovery = 90% Analysis Date = 08/15/15 Pct Recovery = 90% Analysis Date = 08/04/15 Pct Recovery = 90% Analysis Date = 08/04/15 Pct Recovery = 90% Analysis Date = 07/24/15 Pct Recovery = 90% Analysis Date = 07/24/15 Pct Recovery = 90% Analysis Date = 07/14/15 Pct Recovery = 90% Analysis Date = 07/14/15 Pct Recovery = 90% Analysis Date = 07/03/15 Pct Recovery = 90% Analysis Date = 07/03/15 Pct Recovery = 90% Analysis Date = 06/22/15 Pct Recovery = 90% Analysis Date = 06/22/15 Pct Recovery = 90% Analysis Date = 06/12/15 Pct Recovery = 90% Analysis Date = 06/12/15 Pct Recovery = 90% Analysis Date = 06/01/15 Pct Recovery = 90% Analysis Date = 06/01/15 Pct Recovery = 90% Analysis Date = 05/21/15 Pct Recovery = 90% Analysis Date = 05/21/15 Pct Recovery = 90% Analysis Date = 05/10/15 Pct Recovery = 90% Analysis Date = 05/10/15 Pct Recovery = 90% Analysis Date = 04/30/15 Pct Recovery = 90% Analysis Date = 04/30/15 Pct Recovery = 90% Analysis Date = 04/19/15 Pct Recovery = 90% Analysis Date = 04/19/15 Pct Recovery = 90% Analysis Date = 04/08/15 Pct Recovery = 90% Analysis Date = 04/08/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/07/15 Pct Recovery = 90% Analysis Date = 03/07/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 89% Analysis Date = 02/14/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 89% Analysis Date = 01/23/15 Pct Recovery = 89% Analysis Date = 01/23/15 Pct Recovery = 89% Analysis Date = 01/13/15 Pct Recovery = 89% Analysis Date = 01/13/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 89% Analysis Date = 12/12/14 Pct Recovery = 89% Analysis Date = 12/12/14 Pct Recovery = 89% Analysis Date = 12/01/14 Pct Recovery = 89% Analysis Date = 12/01/14 Pct Recovery = 89% Analysis Date = 11/20/14 Pct Recovery = 89% Analysis Date = 11/20/14 Pct Recovery = 89% Analysis Date = 11/09/14 Pct Recovery = 89% Analysis Date = 11/09/14 Pct Recovery = 89% Analysis Date = 10/30/14 Pct Recovery = 89% Analysis Date = 10/30/14 Pct Recovery = 89% Analysis Date = 10/19/14 Pct Recovery = 89% Analysis Date = 10/19/14 Pct Recovery = 89% Analysis Date = 10/08/14 Pct Recovery = 89% Analysis Date = 10/08/14 Pct Recovery = 89% Analysis Date = 09/28/14 Pct Recovery = 89% Analysis Date = 09/28/14 Pct Recovery = 89% Analysis Date = 09/17/14 Pct Recovery = 89% Analysis Date = 09/17/14 Pct Recovery = 89% Analysis Date = 09/06/14 Pct Recovery = 89% Analysis Date = 09/06/14 Pct Recovery = 89% Analysis Date = 08/26/14 Pct Recovery = 89% Analysis Date = 08/26/14 Pct Recovery = 89% Analysis Date = 08/16/14 Pct Recovery = 89% Analysis Date = 08/16/14 Pct Recovery = 89% Analysis Date = 08/05/14 Pct Recovery = 89% Analysis Date = 08/05/14 Pct Recovery = 89% Analysis Date = 07/25/14 Pct Recovery = 89% Analysis Date = 07/25/14 Pct Recovery = 89% Analysis Date = 07/15/14 Pct Recovery = 89% Analysis Date = 07/15/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 06/23/14 Pct Recovery = 89% Analysis Date = 06/23/14 Pct Recovery = 89% Analysis Date = 06/12/14 Pct Recovery = 89% Analysis Date = 06/12/14 Pct Recovery = 89% Analysis Date = 06/02/14 Pct Recovery = 88% Analysis Date = 06/02/14 Pct Recovery = 88% Analysis Date = 05/22/14 Pct Recovery = 88% Analysis Date = 05/22/14 Pct Recovery = 88% Analysis Date = 05/11/14 Pct Recovery = 88% Analysis Date = 05/11/14 Pct Recovery = 88% Analysis Date = 05/01/14 Pct Recovery = 88% Analysis Date = 05/01/14 Pct Recovery = 88% Analysis Date = 04/20/14 Pct Recovery = 88% Analysis Date = 04/20/14 Pct Recovery = 88% Analysis Date = 04/09/14 Pct Recovery = 88% Analysis Date = 04/09/14 Pct Recovery = 88% Analysis Date = 03/29/14 Pct Recovery = 88% Analysis Date = 03/29/14 Pct Recovery = 88% Analysis Date = 03/19/14 Pct Recovery = 88% Analysis Date = 03/19/14 Pct Recovery = 88% Analysis Date = 03/08/14 Pct Recovery = 88% Analysis Date = 03/08/14 Pct Recovery = 88% Analysis Date = 02/25/14 Pct Recovery = 88% Analysis Date = 02/25/14 Pct Recovery = 88% Analysis Date = 02/15/14 Pct Recovery = 88% Analysis Date = 02/15/14 Pct Recovery = 88% Analysis Date = 02/04/14 Pct Recovery = 88% Analysis Date = 02/04/14 Pct Recovery = 88% Analysis Date = 01/24/14 Pct Recovery = 88% Analysis Date = 01/24/14 Pct Recovery = 88% Analysis Date = 01/13/14 Pct Recovery = 88% Analysis Date = 01/13/14 Pct Recovery = 88% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 01/03/14 Pct Recovery = 89% Analysis Date = 12/23/13 Pct Recovery = 89% Analysis Date = 12/23/13 Pct Recovery = 89% Analysis Date = 12/12/13 Pct Recovery = 89% Analysis Date = 12/12/13 Pct Recovery = 89% Analysis Date = 12/02/13 Pct Recovery = 89% Analysis Date = 12/02/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/21/13 Pct Recovery = 89% Analysis Date = 11/10/13 Pct Recovery = 89% Analysis Date = 11/10/13 Pct Recovery = 89% Analysis Date = 10/31/13 Pct Recovery = 89% Analysis Date = 10/31/13 Pct Recovery = 89% Analysis Date = 10/20/13 Pct Recovery = 89% Analysis Date = 10/20/13 Pct Recovery = 89% Analysis Date = 10/09/13 Pct Recovery = 89% Analysis Date = 10/09/13 Pct Recovery = 89% Analysis Date = 09/28/13 Pct Recovery = 89% Analysis Date = 09/28/13 Pct Recovery = 89% Analysis Date = 09/18/13 Pct Recovery = 90% Analysis Date = 09/18/13 Pct Recovery = 90% Analysis Date = 09/07/13 Pct Recovery = 90% Analysis Date = 09/07/13 Pct Recovery = 90% Analysis Date = 08/27/13 Pct Recovery = 90% Analysis Date = 08/27/13 Pct Recovery = 90% Analysis Date = 08/17/13 Pct Recovery = 90% Analysis Date = 08/17/13 Pct Recovery = 90% Analysis Date = 08/06/13 Pct Recovery = 90% Analysis Date = 08/06/13 Pct Recovery = 90% Analysis Date = 07/26/13 Pct Recovery = 91% Analysis Date = 07/26/13 Pct Recovery = 91% Analysis Date = 07/15/13 Pct Recovery = 91% Analysis Date = 07/15/13 Pct Recovery = 91% Analysis Date = 07/05/13 Pct Recovery = 91% Analysis Date = 07/05/13 Pct Recovery = 91% Analysis Date = 06/24/13 Pct Recovery = 91% Analysis Date = 06/24/13 Pct Recovery = 91% Analysis Date = 06/13/13 Pct Recovery = 92% Analysis Date = 06/13/13 Pct Recovery = 92% Analysis Date = 06/03/13 Pct Recovery = 92% Analysis Date = 06/03/13 Pct Recovery = 92% Analysis Date = 05/23/13 Pct Recovery = 92% Analysis Date = 05/23/13 Pct Recovery = 92% Analysis Date = 05/12/13 Pct Recovery = 92% Analysis Date = 05/12/13 Pct Recovery = 92% Analysis Date = 05/01/13 Pct Recovery = 93% Analysis Date = 05/01/13 Pct Recovery = 93% Analysis Date = 04/21/13 Pct Recovery = 93% Analysis Date = 04/21/13 Pct Recovery = 93% Analysis Date = 04/10/13 Pct Recovery = 93% Analysis Date = 04/10/13 Pct Recovery = 93% Analysis Date = 03/30/13 Pct Recovery = 93% Analysis Date = 03/30/13 Pct Recovery = 93% Analysis Date = 03/20/13 Pct Recovery = 94% Analysis Date = 03/20/13 Pct Recovery = 94% Analysis Date = 03/09/13 Pct Recovery = 94% Analysis Date = 03/09/13 Pct Recovery = 94% Analysis Date = 02/26/13 Pct Recovery = 94% Analysis Date = 02/26/13 Pct Recovery = 94% Analysis Date = 02/15/13 Pct Recovery = 94% Analysis Date = 02/15/13 Pct Recovery = 94% Analysis Date = 02/05/13 Pct Recovery = 95% Analysis Date = 02/05/13 Pct Recovery = 95% Analysis Date = 01/25/13 Pct Recovery = 95% Analysis Date = 01/25/13 Pct Recovery = 95% Analysis Date = 01/14/13 Pct Recovery = 95% Analysis Date = 01/14/13 Pct Recovery = 95% Analysis Date = 01/04/13 Pct Recovery = 95% Analysis Date = 01/04/13 Pct Recovery = 95% Analysis Date = 12/24/12 Pct Recovery = 96% Analysis Date = 12/24/12 Pct Recovery = 96% Analysis Date = 12/13/12 Pct Recovery = 96% Analysis Date = 12/13/12 Pct Recovery = 96% Analysis Date = 12/03/12 Pct Recovery = 96% Analysis Date = 12/03/12 Pct Recovery = 96% Analysis Date = 11/22/12 Pct Recovery = 96% Analysis Date = 11/22/12 Pct Recovery = 96% Analysis Date = 11/11/12 Pct Recovery = 96% Analysis Date = 11/11/12 Pct Recovery = 96% Analysis Date = 10/31/12 Pct Recovery = 97% Analysis Date = 10/31/12 Pct Recovery = 97% Analysis Date = 10/21/12 Pct Recovery = 97% Analysis Date = 10/21/12 Pct Recovery = 97% Analysis Date = 10/10/12 Pct Recovery = 97% Analysis Date = 10/10/12 Pct Recovery = 97% Analysis Date = 09/29/12 Pct Recovery = 97% Analysis Date = 09/29/12 Pct Recovery = 97% Analysis Date = 09/19/12 Pct Recovery = 97% Analysis Date = 09/19/12 Pct Recovery = 97% Analysis Date = 09/08/12 Pct Recovery = 98% Analysis Date = 09/08/12 Pct Recovery = 98% Analysis Date = 08/28/12 Pct Recovery = 98% Analysis Date = 08/28/12 Pct Recovery = 98% Analysis Date = 08/17/12 Pct Recovery = 98% Analysis Date = 08/17/12 Pct Recovery = 98% Analysis Date = 08/07/12 Pct Recovery = 98% Analysis Date = 08/07/12 Pct Recovery = 98% Analysis Date = 07/27/12 Pct Recovery = 98% Analysis Date = 07/27/12 Pct Recovery = 98% Analysis Date = 07/16/12 Pct Recovery = 98% Analysis Date = 07/16/12 Pct Recovery = 98% Analysis Date = 07/06/12 Pct Recovery = 99% Analysis Date = 07/06/12 Pct Recovery = 99% Analysis Date = 06/25/12 Pct Recovery = 99% Analysis Date = 06/25/12 Pct Recovery = 99% Analysis Date = 06/14/12 Pct Recovery = 99% Analysis Date = 06/14/12 Pct Recovery = 99% Analysis Date = 06/03/12 Pct Recovery = 99% Analysis Date = 06/03/12 Pct Recovery = 99% Analysis Date = 05/24/12 Pct Recovery = 99% Analysis Date = 05/24/12 Pct Recovery = 99% Analysis Date = 05/13/12 Pct Recovery = 99% Analysis Date = 05/13/12 Pct Recovery = 99% Analysis Date = 05/02/12 Pct Recovery = 99% Analysis Date = 05/02/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 100% Analysis Date = 04/22/12 Pct Recovery = 100% Analysis Date = 04/11/12 Pct Recovery = 100% Analysis Date = 04/11/12 Pct Recovery = 100% Analysis Date = 03/31/12 Pct Recovery = 100% Analysis Date = 03/31/12 Pct Recovery = 100% Analysis Date = 03/20/12 Pct Recovery = 100% Analysis Date = 03/20/12 Pct Recovery = 100% Analysis Date = 03/10/12 Pct Recovery = 100% Analysis Date = 03/10/12 Pct Recovery = 100% Analysis Date = 02/28/12 Pct Recovery = 100% Analysis Date = 02/28/12 Pct Recovery = 100% Analysis Date = 02/17/12 Pct Recovery = 101% Analysis Date = 02/17/12 Pct Recovery = 101% Analysis Date = 02/07/12 Pct Recovery = 101% Analysis Date = 02/07/12 Pct Recovery = 101% Analysis Date = 01/27/12 Pct Recovery = 101% Analysis Date = 01/27/12 Pct Recovery = 101% Analysis Date = 01/16/12 Pct Recovery = 101% Analysis Date = 01/16/12 Pct Recovery = 101% Analysis Date = 01/06/12 Pct Recovery = 101% Analysis Date = 01/06/12 Pct Recovery = 101% Analysis Date = 12/26/11 Pct Recovery = 101% Analysis Date = 12/26/11 Pct Recovery = 101% Analysis Date = 12/15/11 Pct Recovery = 102% Analysis Date = 12/15/11 Pct Recovery = 102% Analysis Date = 12/04/11 Pct Recovery = 102% Analysis Date = 12/04/11 Pct Recovery = 102% Analysis Date = 11/24/11 Pct Recovery = 102% Analysis Date = 11/24/11 Pct Recovery = 102% Analysis Date = 11/13/11 Pct Recovery = 102% Analysis Date = 11/13/11 Pct Recovery = 102% Analysis Date = 11/02/11 Pct Recovery = 102% Analysis Date = 11/02/11 Pct Recovery = 102% Analysis Date = 10/23/11 Pct Recovery = 102% Analysis Date = 10/23/11 Pct Recovery = 102% Analysis Date = 10/12/11 Pct Recovery = 103% Analysis Date = 10/12/11 Pct Recovery = 103% Analysis Date = 10/01/11 Pct Recovery = 103% Analysis Date = 10/01/11 Pct Recovery = 103% Analysis Date = 09/20/11 Pct Recovery = 103% Analysis Date = 09/20/11 Pct Recovery = 103% Analysis Date = 09/10/11 Pct Recovery = 103% Analysis Date = 09/10/11 Pct Recovery = 103% Analysis Date = 08/30/11 Pct Recovery = 103% Analysis Date = 08/30/11 Pct Recovery = 103% Analysis Date = 08/19/11 Pct Recovery = 103% Analysis Date = 08/19/11 Pct Recovery = 103% Analysis Date = 08/09/11 Pct Recovery = 104% Analysis Date = 08/09/11 Pct Recovery = 104% Analysis Date = 07/29/11 Pct Recovery = 104% Analysis Date = 07/29/11 Pct Recovery = 104% Analysis Date = 07/18/11 Pct Recovery = 104% Analysis Date = 07/18/11 Pct Recovery = 104% Analysis Date = 07/07/11 Pct Recovery = 104% Analysis Date = 07/07/11 Pct Recovery = 104% Analysis Date = 06/27/11 Pct Recovery = 104% Analysis Date = 06/27/11 Pct Recovery = 104% Analysis Date = 06/16/11 Pct Recovery = 104% Analysis Date = 06/16/11 Pct Recovery = 104% Analysis Date = 06/05/11 Pct Recovery = 104% Analysis Date = 06/05/11 Pct Recovery = 104% Analysis Date = 05/26/11 Pct Recovery = 105% Analysis Date = 05/26/11 Pct Recovery = 105% Analysis Date = 05/15/11 Pct Recovery = 105% Analysis Date = 05/15/11 Pct Recovery = 105% Analysis Date = 05/04/11 Pct Recovery = 105% Analysis Date = 05/04/11 Pct Recovery = 105% Analysis Date = 04/23/11 Pct Recovery = 105% Analysis Date = 04/23/11 Pct Recovery = 105% Analysis Date = 04/13/11 Pct Recovery = 105% Analysis Date = 04/13/11 Pct Recovery = 105% Analysis Date = 04/02/11 Pct Recovery = 105% Analysis Date = 04/02/11 Pct Recovery = 105% Analysis Date = 03/22/11 Pct Recovery = 105% Analysis Date = 03/22/11 Pct Recovery = 105% Analysis Date = 03/12/11 Pct Recovery = 105% Analysis Date = 03/12/11 Pct Recovery = 105% Analysis Date = 03/01/11 Pct Recovery = 106% Analysis Date = 03/01/11 Pct Recovery = 106% Analysis Date = 02/18/11 Pct Recovery = 106% Analysis Date = 02/18/11 Pct Recovery = 106% Analysis Date = 02/08/11 Pct Recovery = 106% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENDIMETHALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 94% 19% 90% 16%
Total 87 94% 19% 90% 16%

Sample Statistics
PENDIMETHALIN

Characteristic N % % Basis
Plotted 87 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 0 0% 0 out of 87
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

BQS OBSP Determination:
PHORATE
METHOD: 2033 , TESTIDCODE: 82664GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 63% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 60% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 68% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 92% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 27% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 53% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 69% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 75% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 69% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 46% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 113% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 83% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 26% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 60% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 82% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 18% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 76% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 78% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 70% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 72% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 88% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 91% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 85% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 64% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 33% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 67% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 56% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 81% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 74% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 71% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 45% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 63% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 51% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 68% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 38% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 48% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 55% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 43% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 52% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 80% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 22% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 75% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 58% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 72% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 86% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 84% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 89% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 61% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 83% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 61% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 89% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 85% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 81% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 80% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 78% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 39% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 42% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 38% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 81% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 57% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 30% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 84% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 32% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 52% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 63% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 50% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 40% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 63% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 81% Analysis Date = 01/17/17 Pct Recovery = 69% Analysis Date = 01/07/17 Pct Recovery = 69% Analysis Date = 01/07/17 Pct Recovery = 69% Analysis Date = 12/27/16 Pct Recovery = 69% Analysis Date = 12/27/16 Pct Recovery = 69% Analysis Date = 12/16/16 Pct Recovery = 68% Analysis Date = 12/16/16 Pct Recovery = 68% Analysis Date = 12/05/16 Pct Recovery = 68% Analysis Date = 12/05/16 Pct Recovery = 68% Analysis Date = 11/24/16 Pct Recovery = 68% Analysis Date = 11/24/16 Pct Recovery = 68% Analysis Date = 11/13/16 Pct Recovery = 68% Analysis Date = 11/13/16 Pct Recovery = 68% Analysis Date = 11/03/16 Pct Recovery = 68% Analysis Date = 11/03/16 Pct Recovery = 68% Analysis Date = 10/23/16 Pct Recovery = 68% Analysis Date = 10/23/16 Pct Recovery = 68% Analysis Date = 10/12/16 Pct Recovery = 68% Analysis Date = 10/12/16 Pct Recovery = 68% Analysis Date = 10/01/16 Pct Recovery = 67% Analysis Date = 10/01/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/09/16 Pct Recovery = 67% Analysis Date = 09/09/16 Pct Recovery = 67% Analysis Date = 08/29/16 Pct Recovery = 67% Analysis Date = 08/29/16 Pct Recovery = 67% Analysis Date = 08/19/16 Pct Recovery = 67% Analysis Date = 08/19/16 Pct Recovery = 67% Analysis Date = 08/08/16 Pct Recovery = 67% Analysis Date = 08/08/16 Pct Recovery = 67% Analysis Date = 07/28/16 Pct Recovery = 66% Analysis Date = 07/28/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 65% Analysis Date = 05/24/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/02/16 Pct Recovery = 65% Analysis Date = 05/02/16 Pct Recovery = 65% Analysis Date = 04/21/16 Pct Recovery = 65% Analysis Date = 04/21/16 Pct Recovery = 65% Analysis Date = 04/10/16 Pct Recovery = 65% Analysis Date = 04/10/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/20/16 Pct Recovery = 65% Analysis Date = 03/20/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 64% Analysis Date = 03/09/16 Pct Recovery = 64% Analysis Date = 02/27/16 Pct Recovery = 64% Analysis Date = 02/27/16 Pct Recovery = 64% Analysis Date = 02/16/16 Pct Recovery = 64% Analysis Date = 02/16/16 Pct Recovery = 64% Analysis Date = 02/05/16 Pct Recovery = 64% Analysis Date = 02/05/16 Pct Recovery = 64% Analysis Date = 01/25/16 Pct Recovery = 64% Analysis Date = 01/25/16 Pct Recovery = 64% Analysis Date = 01/15/16 Pct Recovery = 64% Analysis Date = 01/15/16 Pct Recovery = 64% Analysis Date = 01/04/16 Pct Recovery = 64% Analysis Date = 01/04/16 Pct Recovery = 64% Analysis Date = 12/24/15 Pct Recovery = 64% Analysis Date = 12/24/15 Pct Recovery = 64% Analysis Date = 12/13/15 Pct Recovery = 64% Analysis Date = 12/13/15 Pct Recovery = 64% Analysis Date = 12/02/15 Pct Recovery = 63% Analysis Date = 12/02/15 Pct Recovery = 63% Analysis Date = 11/21/15 Pct Recovery = 63% Analysis Date = 11/21/15 Pct Recovery = 63% Analysis Date = 11/10/15 Pct Recovery = 63% Analysis Date = 11/10/15 Pct Recovery = 63% Analysis Date = 10/31/15 Pct Recovery = 63% Analysis Date = 10/31/15 Pct Recovery = 63% Analysis Date = 10/20/15 Pct Recovery = 63% Analysis Date = 10/20/15 Pct Recovery = 63% Analysis Date = 10/09/15 Pct Recovery = 63% Analysis Date = 10/09/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/17/15 Pct Recovery = 63% Analysis Date = 09/17/15 Pct Recovery = 63% Analysis Date = 09/06/15 Pct Recovery = 63% Analysis Date = 09/06/15 Pct Recovery = 63% Analysis Date = 08/27/15 Pct Recovery = 63% Analysis Date = 08/27/15 Pct Recovery = 63% Analysis Date = 08/16/15 Pct Recovery = 62% Analysis Date = 08/16/15 Pct Recovery = 62% Analysis Date = 08/05/15 Pct Recovery = 62% Analysis Date = 08/05/15 Pct Recovery = 62% Analysis Date = 07/25/15 Pct Recovery = 62% Analysis Date = 07/25/15 Pct Recovery = 62% Analysis Date = 07/14/15 Pct Recovery = 62% Analysis Date = 07/14/15 Pct Recovery = 62% Analysis Date = 07/03/15 Pct Recovery = 62% Analysis Date = 07/03/15 Pct Recovery = 62% Analysis Date = 06/22/15 Pct Recovery = 62% Analysis Date = 06/22/15 Pct Recovery = 62% Analysis Date = 06/12/15 Pct Recovery = 62% Analysis Date = 06/12/15 Pct Recovery = 62% Analysis Date = 06/01/15 Pct Recovery = 62% Analysis Date = 06/01/15 Pct Recovery = 62% Analysis Date = 05/21/15 Pct Recovery = 62% Analysis Date = 05/21/15 Pct Recovery = 62% Analysis Date = 05/10/15 Pct Recovery = 61% Analysis Date = 05/10/15 Pct Recovery = 61% Analysis Date = 04/29/15 Pct Recovery = 61% Analysis Date = 04/29/15 Pct Recovery = 61% Analysis Date = 04/18/15 Pct Recovery = 61% Analysis Date = 04/18/15 Pct Recovery = 61% Analysis Date = 04/07/15 Pct Recovery = 61% Analysis Date = 04/07/15 Pct Recovery = 61% Analysis Date = 03/28/15 Pct Recovery = 61% Analysis Date = 03/28/15 Pct Recovery = 61% Analysis Date = 03/17/15 Pct Recovery = 61% Analysis Date = 03/17/15 Pct Recovery = 61% Analysis Date = 03/06/15 Pct Recovery = 61% Analysis Date = 03/06/15 Pct Recovery = 61% Analysis Date = 02/23/15 Pct Recovery = 61% Analysis Date = 02/23/15 Pct Recovery = 61% Analysis Date = 02/12/15 Pct Recovery = 61% Analysis Date = 02/12/15 Pct Recovery = 61% Analysis Date = 02/01/15 Pct Recovery = 61% Analysis Date = 02/01/15 Pct Recovery = 61% Analysis Date = 01/22/15 Pct Recovery = 60% Analysis Date = 01/22/15 Pct Recovery = 60% Analysis Date = 01/11/15 Pct Recovery = 60% Analysis Date = 01/11/15 Pct Recovery = 60% Analysis Date = 12/31/14 Pct Recovery = 60% Analysis Date = 12/31/14 Pct Recovery = 60% Analysis Date = 12/20/14 Pct Recovery = 60% Analysis Date = 12/20/14 Pct Recovery = 60% Analysis Date = 12/09/14 Pct Recovery = 60% Analysis Date = 12/09/14 Pct Recovery = 60% Analysis Date = 11/28/14 Pct Recovery = 60% Analysis Date = 11/28/14 Pct Recovery = 60% Analysis Date = 11/17/14 Pct Recovery = 60% Analysis Date = 11/17/14 Pct Recovery = 60% Analysis Date = 11/07/14 Pct Recovery = 60% Analysis Date = 11/07/14 Pct Recovery = 60% Analysis Date = 10/27/14 Pct Recovery = 60% Analysis Date = 10/27/14 Pct Recovery = 60% Analysis Date = 10/16/14 Pct Recovery = 60% Analysis Date = 10/16/14 Pct Recovery = 60% Analysis Date = 10/05/14 Pct Recovery = 59% Analysis Date = 10/05/14 Pct Recovery = 59% Analysis Date = 09/24/14 Pct Recovery = 59% Analysis Date = 09/24/14 Pct Recovery = 59% Analysis Date = 09/13/14 Pct Recovery = 59% Analysis Date = 09/13/14 Pct Recovery = 59% Analysis Date = 09/02/14 Pct Recovery = 59% Analysis Date = 09/02/14 Pct Recovery = 59% Analysis Date = 08/23/14 Pct Recovery = 59% Analysis Date = 08/23/14 Pct Recovery = 59% Analysis Date = 08/12/14 Pct Recovery = 59% Analysis Date = 08/12/14 Pct Recovery = 59% Analysis Date = 08/01/14 Pct Recovery = 59% Analysis Date = 08/01/14 Pct Recovery = 59% Analysis Date = 07/21/14 Pct Recovery = 59% Analysis Date = 07/21/14 Pct Recovery = 59% Analysis Date = 07/10/14 Pct Recovery = 59% Analysis Date = 07/10/14 Pct Recovery = 59% Analysis Date = 06/29/14 Pct Recovery = 59% Analysis Date = 06/29/14 Pct Recovery = 59% Analysis Date = 06/19/14 Pct Recovery = 59% Analysis Date = 06/19/14 Pct Recovery = 59% Analysis Date = 06/08/14 Pct Recovery = 59% Analysis Date = 06/08/14 Pct Recovery = 59% Analysis Date = 05/28/14 Pct Recovery = 59% Analysis Date = 05/28/14 Pct Recovery = 59% Analysis Date = 05/17/14 Pct Recovery = 59% Analysis Date = 05/17/14 Pct Recovery = 59% Analysis Date = 05/06/14 Pct Recovery = 59% Analysis Date = 05/06/14 Pct Recovery = 59% Analysis Date = 04/25/14 Pct Recovery = 59% Analysis Date = 04/25/14 Pct Recovery = 59% Analysis Date = 04/14/14 Pct Recovery = 59% Analysis Date = 04/14/14 Pct Recovery = 59% Analysis Date = 04/04/14 Pct Recovery = 59% Analysis Date = 04/04/14 Pct Recovery = 59% Analysis Date = 03/24/14 Pct Recovery = 59% Analysis Date = 03/24/14 Pct Recovery = 59% Analysis Date = 03/13/14 Pct Recovery = 59% Analysis Date = 03/13/14 Pct Recovery = 59% Analysis Date = 03/02/14 Pct Recovery = 59% Analysis Date = 03/02/14 Pct Recovery = 59% Analysis Date = 02/19/14 Pct Recovery = 59% Analysis Date = 02/19/14 Pct Recovery = 59% Analysis Date = 02/08/14 Pct Recovery = 59% Analysis Date = 02/08/14 Pct Recovery = 59% Analysis Date = 01/28/14 Pct Recovery = 59% Analysis Date = 01/28/14 Pct Recovery = 59% Analysis Date = 01/18/14 Pct Recovery = 59% Analysis Date = 01/18/14 Pct Recovery = 59% Analysis Date = 01/07/14 Pct Recovery = 59% Analysis Date = 01/07/14 Pct Recovery = 59% Analysis Date = 12/27/13 Pct Recovery = 59% Analysis Date = 12/27/13 Pct Recovery = 59% Analysis Date = 12/16/13 Pct Recovery = 59% Analysis Date = 12/16/13 Pct Recovery = 59% Analysis Date = 12/05/13 Pct Recovery = 59% Analysis Date = 12/05/13 Pct Recovery = 59% Analysis Date = 11/24/13 Pct Recovery = 59% Analysis Date = 11/24/13 Pct Recovery = 59% Analysis Date = 11/14/13 Pct Recovery = 59% Analysis Date = 11/14/13 Pct Recovery = 59% Analysis Date = 11/03/13 Pct Recovery = 59% Analysis Date = 11/03/13 Pct Recovery = 59% Analysis Date = 10/23/13 Pct Recovery = 59% Analysis Date = 10/23/13 Pct Recovery = 59% Analysis Date = 10/12/13 Pct Recovery = 59% Analysis Date = 10/12/13 Pct Recovery = 59% Analysis Date = 10/01/13 Pct Recovery = 59% Analysis Date = 10/01/13 Pct Recovery = 59% Analysis Date = 09/20/13 Pct Recovery = 59% Analysis Date = 09/20/13 Pct Recovery = 59% Analysis Date = 09/09/13 Pct Recovery = 59% Analysis Date = 09/09/13 Pct Recovery = 59% Analysis Date = 08/30/13 Pct Recovery = 59% Analysis Date = 08/30/13 Pct Recovery = 59% Analysis Date = 08/19/13 Pct Recovery = 59% Analysis Date = 08/19/13 Pct Recovery = 59% Analysis Date = 08/08/13 Pct Recovery = 59% Analysis Date = 08/08/13 Pct Recovery = 59% Analysis Date = 07/28/13 Pct Recovery = 59% Analysis Date = 07/28/13 Pct Recovery = 59% Analysis Date = 07/17/13 Pct Recovery = 59% Analysis Date = 07/17/13 Pct Recovery = 59% Analysis Date = 07/06/13 Pct Recovery = 59% Analysis Date = 07/06/13 Pct Recovery = 59% Analysis Date = 06/25/13 Pct Recovery = 59% Analysis Date = 06/25/13 Pct Recovery = 59% Analysis Date = 06/15/13 Pct Recovery = 59% Analysis Date = 06/15/13 Pct Recovery = 59% Analysis Date = 06/04/13 Pct Recovery = 59% Analysis Date = 06/04/13 Pct Recovery = 59% Analysis Date = 05/24/13 Pct Recovery = 59% Analysis Date = 05/24/13 Pct Recovery = 59% Analysis Date = 05/13/13 Pct Recovery = 59% Analysis Date = 05/13/13 Pct Recovery = 59% Analysis Date = 05/02/13 Pct Recovery = 59% Analysis Date = 05/02/13 Pct Recovery = 59% Analysis Date = 04/21/13 Pct Recovery = 59% Analysis Date = 04/21/13 Pct Recovery = 59% Analysis Date = 04/11/13 Pct Recovery = 59% Analysis Date = 04/11/13 Pct Recovery = 59% Analysis Date = 03/31/13 Pct Recovery = 59% Analysis Date = 03/31/13 Pct Recovery = 59% Analysis Date = 03/20/13 Pct Recovery = 59% Analysis Date = 03/20/13 Pct Recovery = 59% Analysis Date = 03/09/13 Pct Recovery = 59% Analysis Date = 03/09/13 Pct Recovery = 59% Analysis Date = 02/26/13 Pct Recovery = 59% Analysis Date = 02/26/13 Pct Recovery = 59% Analysis Date = 02/15/13 Pct Recovery = 59% Analysis Date = 02/15/13 Pct Recovery = 59% Analysis Date = 02/04/13 Pct Recovery = 59% Analysis Date = 02/04/13 Pct Recovery = 59% Analysis Date = 01/25/13 Pct Recovery = 59% Analysis Date = 01/25/13 Pct Recovery = 59% Analysis Date = 01/14/13 Pct Recovery = 59% Analysis Date = 01/14/13 Pct Recovery = 59% Analysis Date = 01/03/13 Pct Recovery = 59% Analysis Date = 01/03/13 Pct Recovery = 59% Analysis Date = 12/23/12 Pct Recovery = 59% Analysis Date = 12/23/12 Pct Recovery = 59% Analysis Date = 12/12/12 Pct Recovery = 59% Analysis Date = 12/12/12 Pct Recovery = 59% Analysis Date = 12/01/12 Pct Recovery = 60% Analysis Date = 12/01/12 Pct Recovery = 60% Analysis Date = 11/20/12 Pct Recovery = 60% Analysis Date = 11/20/12 Pct Recovery = 60% Analysis Date = 11/10/12 Pct Recovery = 60% Analysis Date = 11/10/12 Pct Recovery = 60% Analysis Date = 10/30/12 Pct Recovery = 60% Analysis Date = 10/30/12 Pct Recovery = 60% Analysis Date = 10/19/12 Pct Recovery = 60% Analysis Date = 10/19/12 Pct Recovery = 60% Analysis Date = 10/08/12 Pct Recovery = 60% Analysis Date = 10/08/12 Pct Recovery = 60% Analysis Date = 09/27/12 Pct Recovery = 60% Analysis Date = 09/27/12 Pct Recovery = 60% Analysis Date = 09/16/12 Pct Recovery = 61% Analysis Date = 09/16/12 Pct Recovery = 61% Analysis Date = 09/06/12 Pct Recovery = 61% Analysis Date = 09/06/12 Pct Recovery = 61% Analysis Date = 08/26/12 Pct Recovery = 61% Analysis Date = 08/26/12 Pct Recovery = 61% Analysis Date = 08/15/12 Pct Recovery = 61% Analysis Date = 08/15/12 Pct Recovery = 61% Analysis Date = 08/04/12 Pct Recovery = 62% Analysis Date = 08/04/12 Pct Recovery = 62% Analysis Date = 07/24/12 Pct Recovery = 62% Analysis Date = 07/24/12 Pct Recovery = 62% Analysis Date = 07/13/12 Pct Recovery = 63% Analysis Date = 07/13/12 Pct Recovery = 63% Analysis Date = 07/02/12 Pct Recovery = 63% Analysis Date = 07/02/12 Pct Recovery = 63% Analysis Date = 06/22/12 Pct Recovery = 63% Analysis Date = 06/22/12 Pct Recovery = 63% Analysis Date = 06/11/12 Pct Recovery = 64% Analysis Date = 06/11/12 Pct Recovery = 64% Analysis Date = 05/31/12 Pct Recovery = 64% Analysis Date = 05/31/12 Pct Recovery = 64% Analysis Date = 05/20/12 Pct Recovery = 65% Analysis Date = 05/20/12 Pct Recovery = 65% Analysis Date = 05/09/12 Pct Recovery = 65% Analysis Date = 05/09/12 Pct Recovery = 65% Analysis Date = 04/28/12 Pct Recovery = 66% Analysis Date = 04/28/12 Pct Recovery = 66% Analysis Date = 04/17/12 Pct Recovery = 66% Analysis Date = 04/17/12 Pct Recovery = 66% Analysis Date = 04/07/12 Pct Recovery = 66% Analysis Date = 04/07/12 Pct Recovery = 66% Analysis Date = 03/27/12 Pct Recovery = 67% Analysis Date = 03/27/12 Pct Recovery = 67% Analysis Date = 03/16/12 Pct Recovery = 67% Analysis Date = 03/16/12 Pct Recovery = 67% Analysis Date = 03/05/12 Pct Recovery = 68% Analysis Date = 03/05/12 Pct Recovery = 68% Analysis Date = 02/23/12 Pct Recovery = 68% Analysis Date = 02/23/12 Pct Recovery = 68% Analysis Date = 02/12/12 Pct Recovery = 69% Analysis Date = 02/12/12 Pct Recovery = 69% Analysis Date = 02/02/12 Pct Recovery = 69% Analysis Date = 02/02/12 Pct Recovery = 69% Analysis Date = 01/22/12 Pct Recovery = 69% Analysis Date = 01/22/12 Pct Recovery = 69% Analysis Date = 01/11/12 Pct Recovery = 70% Analysis Date = 01/11/12 Pct Recovery = 70% Analysis Date = 12/31/11 Pct Recovery = 70% Analysis Date = 12/31/11 Pct Recovery = 70% Analysis Date = 12/20/11 Pct Recovery = 71% Analysis Date = 12/20/11 Pct Recovery = 71% Analysis Date = 12/09/11 Pct Recovery = 71% Analysis Date = 12/09/11 Pct Recovery = 71% Analysis Date = 11/28/11 Pct Recovery = 72% Analysis Date = 11/28/11 Pct Recovery = 72% Analysis Date = 11/18/11 Pct Recovery = 72% Analysis Date = 11/18/11 Pct Recovery = 72% Analysis Date = 11/07/11 Pct Recovery = 72% Analysis Date = 11/07/11 Pct Recovery = 72% Analysis Date = 10/27/11 Pct Recovery = 73% Analysis Date = 10/27/11 Pct Recovery = 73% Analysis Date = 10/16/11 Pct Recovery = 73% Analysis Date = 10/16/11 Pct Recovery = 73% Analysis Date = 10/05/11 Pct Recovery = 74% Analysis Date = 10/05/11 Pct Recovery = 74% Analysis Date = 09/24/11 Pct Recovery = 74% Analysis Date = 09/24/11 Pct Recovery = 74% Analysis Date = 09/13/11 Pct Recovery = 75% Analysis Date = 09/13/11 Pct Recovery = 75% Analysis Date = 09/03/11 Pct Recovery = 75% Analysis Date = 09/03/11 Pct Recovery = 75% Analysis Date = 08/23/11 Pct Recovery = 75% Analysis Date = 08/23/11 Pct Recovery = 75% Analysis Date = 08/12/11 Pct Recovery = 76% Analysis Date = 08/12/11 Pct Recovery = 76% Analysis Date = 08/01/11 Pct Recovery = 76% Analysis Date = 08/01/11 Pct Recovery = 76% Analysis Date = 07/21/11 Pct Recovery = 77% Analysis Date = 07/21/11 Pct Recovery = 77% Analysis Date = 07/10/11 Pct Recovery = 77% Analysis Date = 07/10/11 Pct Recovery = 77% Analysis Date = 06/30/11 Pct Recovery = 77% Analysis Date = 06/30/11 Pct Recovery = 77% Analysis Date = 06/19/11 Pct Recovery = 78% Analysis Date = 06/19/11 Pct Recovery = 78% Analysis Date = 06/08/11 Pct Recovery = 78% Analysis Date = 06/08/11 Pct Recovery = 78% Analysis Date = 05/28/11 Pct Recovery = 79% Analysis Date = 05/28/11 Pct Recovery = 79% Analysis Date = 05/17/11 Pct Recovery = 79% Analysis Date = 05/17/11 Pct Recovery = 79% Analysis Date = 05/06/11 Pct Recovery = 79% Analysis Date = 05/06/11 Pct Recovery = 79% Analysis Date = 04/25/11 Pct Recovery = 80% Analysis Date = 04/25/11 Pct Recovery = 80% Analysis Date = 04/15/11 Pct Recovery = 80% Analysis Date = 04/15/11 Pct Recovery = 80% Analysis Date = 04/04/11 Pct Recovery = 81% Analysis Date = 04/04/11 Pct Recovery = 81% Analysis Date = 03/24/11 Pct Recovery = 81% Analysis Date = 03/24/11 Pct Recovery = 81% Analysis Date = 03/13/11 Pct Recovery = 81% Analysis Date = 03/13/11 Pct Recovery = 81% Analysis Date = 03/02/11 Pct Recovery = 82% Analysis Date = 03/02/11 Pct Recovery = 82% Analysis Date = 02/19/11 Pct Recovery = 82% Analysis Date = 02/19/11 Pct Recovery = 82% Analysis Date = 02/09/11 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHORATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 79 65% 20% 68% 21%
Total 79 65% 20% 68% 21%

Sample Statistics
PHORATE

Characteristic N % % Basis
Plotted 79 91% Spiked
Estimated Values 1 1% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 8 9% 8 out of 87
Not Spiked 74 .  
False Positives 0 0% 0 out of 73

BQS OBSP Determination:
PHORATE OXON
METHOD: 2033 , TESTIDCODE: 61666GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 78% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 64% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 51% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 58% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 20% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 46% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 95% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 50% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 58% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 78% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 49% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 35% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 70% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 75% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 72% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 67% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 46% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 54% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 42% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 81% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 40% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 43% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 22% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 115% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 50% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 95% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 73% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 56% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 65% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 33% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 61% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 83% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 69% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 63% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 43% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 61% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 83% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 81% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 101% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 47% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 96% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 84% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 118% Analysis Date = 01/17/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 76% Analysis Date = 01/07/17 Pct Recovery = 76% Analysis Date = 12/27/16 Pct Recovery = 76% Analysis Date = 12/27/16 Pct Recovery = 76% Analysis Date = 12/16/16 Pct Recovery = 76% Analysis Date = 12/16/16 Pct Recovery = 76% Analysis Date = 12/06/16 Pct Recovery = 75% Analysis Date = 12/06/16 Pct Recovery = 75% Analysis Date = 11/25/16 Pct Recovery = 75% Analysis Date = 11/25/16 Pct Recovery = 75% Analysis Date = 11/14/16 Pct Recovery = 75% Analysis Date = 11/14/16 Pct Recovery = 75% Analysis Date = 11/03/16 Pct Recovery = 75% Analysis Date = 11/03/16 Pct Recovery = 75% Analysis Date = 10/24/16 Pct Recovery = 74% Analysis Date = 10/24/16 Pct Recovery = 74% Analysis Date = 10/13/16 Pct Recovery = 74% Analysis Date = 10/13/16 Pct Recovery = 74% Analysis Date = 10/02/16 Pct Recovery = 74% Analysis Date = 10/02/16 Pct Recovery = 74% Analysis Date = 09/21/16 Pct Recovery = 74% Analysis Date = 09/21/16 Pct Recovery = 74% Analysis Date = 09/11/16 Pct Recovery = 73% Analysis Date = 09/11/16 Pct Recovery = 73% Analysis Date = 08/31/16 Pct Recovery = 73% Analysis Date = 08/31/16 Pct Recovery = 73% Analysis Date = 08/20/16 Pct Recovery = 73% Analysis Date = 08/20/16 Pct Recovery = 73% Analysis Date = 08/10/16 Pct Recovery = 72% Analysis Date = 08/10/16 Pct Recovery = 72% Analysis Date = 07/30/16 Pct Recovery = 72% Analysis Date = 07/30/16 Pct Recovery = 72% Analysis Date = 07/19/16 Pct Recovery = 72% Analysis Date = 07/19/16 Pct Recovery = 72% Analysis Date = 07/08/16 Pct Recovery = 72% Analysis Date = 07/08/16 Pct Recovery = 72% Analysis Date = 06/28/16 Pct Recovery = 71% Analysis Date = 06/28/16 Pct Recovery = 71% Analysis Date = 06/17/16 Pct Recovery = 71% Analysis Date = 06/17/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 70% Analysis Date = 05/26/16 Pct Recovery = 70% Analysis Date = 05/16/16 Pct Recovery = 70% Analysis Date = 05/16/16 Pct Recovery = 70% Analysis Date = 05/05/16 Pct Recovery = 70% Analysis Date = 05/05/16 Pct Recovery = 70% Analysis Date = 04/24/16 Pct Recovery = 70% Analysis Date = 04/24/16 Pct Recovery = 70% Analysis Date = 04/14/16 Pct Recovery = 70% Analysis Date = 04/14/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 69% Analysis Date = 04/03/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 69% Analysis Date = 03/12/16 Pct Recovery = 69% Analysis Date = 03/12/16 Pct Recovery = 69% Analysis Date = 03/02/16 Pct Recovery = 69% Analysis Date = 03/02/16 Pct Recovery = 69% Analysis Date = 02/20/16 Pct Recovery = 69% Analysis Date = 02/20/16 Pct Recovery = 69% Analysis Date = 02/09/16 Pct Recovery = 68% Analysis Date = 02/09/16 Pct Recovery = 68% Analysis Date = 01/29/16 Pct Recovery = 68% Analysis Date = 01/29/16 Pct Recovery = 68% Analysis Date = 01/19/16 Pct Recovery = 68% Analysis Date = 01/19/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 01/08/16 Pct Recovery = 68% Analysis Date = 12/28/15 Pct Recovery = 68% Analysis Date = 12/28/15 Pct Recovery = 68% Analysis Date = 12/17/15 Pct Recovery = 67% Analysis Date = 12/17/15 Pct Recovery = 67% Analysis Date = 12/07/15 Pct Recovery = 67% Analysis Date = 12/07/15 Pct Recovery = 67% Analysis Date = 11/26/15 Pct Recovery = 67% Analysis Date = 11/26/15 Pct Recovery = 67% Analysis Date = 11/15/15 Pct Recovery = 67% Analysis Date = 11/15/15 Pct Recovery = 67% Analysis Date = 11/05/15 Pct Recovery = 67% Analysis Date = 11/05/15 Pct Recovery = 67% Analysis Date = 10/25/15 Pct Recovery = 66% Analysis Date = 10/25/15 Pct Recovery = 66% Analysis Date = 10/14/15 Pct Recovery = 66% Analysis Date = 10/14/15 Pct Recovery = 66% Analysis Date = 10/03/15 Pct Recovery = 66% Analysis Date = 10/03/15 Pct Recovery = 66% Analysis Date = 09/23/15 Pct Recovery = 66% Analysis Date = 09/23/15 Pct Recovery = 66% Analysis Date = 09/12/15 Pct Recovery = 66% Analysis Date = 09/12/15 Pct Recovery = 66% Analysis Date = 09/01/15 Pct Recovery = 65% Analysis Date = 09/01/15 Pct Recovery = 65% Analysis Date = 08/21/15 Pct Recovery = 65% Analysis Date = 08/21/15 Pct Recovery = 65% Analysis Date = 08/11/15 Pct Recovery = 65% Analysis Date = 08/11/15 Pct Recovery = 65% Analysis Date = 07/31/15 Pct Recovery = 65% Analysis Date = 07/31/15 Pct Recovery = 65% Analysis Date = 07/20/15 Pct Recovery = 65% Analysis Date = 07/20/15 Pct Recovery = 65% Analysis Date = 07/10/15 Pct Recovery = 64% Analysis Date = 07/10/15 Pct Recovery = 64% Analysis Date = 06/29/15 Pct Recovery = 64% Analysis Date = 06/29/15 Pct Recovery = 64% Analysis Date = 06/18/15 Pct Recovery = 64% Analysis Date = 06/18/15 Pct Recovery = 64% Analysis Date = 06/07/15 Pct Recovery = 64% Analysis Date = 06/07/15 Pct Recovery = 64% Analysis Date = 05/28/15 Pct Recovery = 64% Analysis Date = 05/28/15 Pct Recovery = 64% Analysis Date = 05/17/15 Pct Recovery = 64% Analysis Date = 05/17/15 Pct Recovery = 64% Analysis Date = 05/06/15 Pct Recovery = 63% Analysis Date = 05/06/15 Pct Recovery = 63% Analysis Date = 04/25/15 Pct Recovery = 63% Analysis Date = 04/25/15 Pct Recovery = 63% Analysis Date = 04/15/15 Pct Recovery = 63% Analysis Date = 04/15/15 Pct Recovery = 63% Analysis Date = 04/04/15 Pct Recovery = 63% Analysis Date = 04/04/15 Pct Recovery = 63% Analysis Date = 03/24/15 Pct Recovery = 63% Analysis Date = 03/24/15 Pct Recovery = 63% Analysis Date = 03/14/15 Pct Recovery = 63% Analysis Date = 03/14/15 Pct Recovery = 63% Analysis Date = 03/03/15 Pct Recovery = 63% Analysis Date = 03/03/15 Pct Recovery = 63% Analysis Date = 02/20/15 Pct Recovery = 63% Analysis Date = 02/20/15 Pct Recovery = 63% Analysis Date = 02/09/15 Pct Recovery = 63% Analysis Date = 02/09/15 Pct Recovery = 63% Analysis Date = 01/30/15 Pct Recovery = 63% Analysis Date = 01/30/15 Pct Recovery = 63% Analysis Date = 01/19/15 Pct Recovery = 63% Analysis Date = 01/19/15 Pct Recovery = 63% Analysis Date = 01/08/15 Pct Recovery = 63% Analysis Date = 01/08/15 Pct Recovery = 63% Analysis Date = 12/28/14 Pct Recovery = 63% Analysis Date = 12/28/14 Pct Recovery = 63% Analysis Date = 12/18/14 Pct Recovery = 63% Analysis Date = 12/18/14 Pct Recovery = 63% Analysis Date = 12/07/14 Pct Recovery = 63% Analysis Date = 12/07/14 Pct Recovery = 63% Analysis Date = 11/26/14 Pct Recovery = 63% Analysis Date = 11/26/14 Pct Recovery = 63% Analysis Date = 11/15/14 Pct Recovery = 63% Analysis Date = 11/15/14 Pct Recovery = 63% Analysis Date = 11/05/14 Pct Recovery = 63% Analysis Date = 11/05/14 Pct Recovery = 63% Analysis Date = 10/25/14 Pct Recovery = 63% Analysis Date = 10/25/14 Pct Recovery = 63% Analysis Date = 10/14/14 Pct Recovery = 63% Analysis Date = 10/14/14 Pct Recovery = 63% Analysis Date = 10/04/14 Pct Recovery = 63% Analysis Date = 10/04/14 Pct Recovery = 63% Analysis Date = 09/23/14 Pct Recovery = 63% Analysis Date = 09/23/14 Pct Recovery = 63% Analysis Date = 09/12/14 Pct Recovery = 63% Analysis Date = 09/12/14 Pct Recovery = 63% Analysis Date = 09/01/14 Pct Recovery = 63% Analysis Date = 09/01/14 Pct Recovery = 63% Analysis Date = 08/22/14 Pct Recovery = 63% Analysis Date = 08/22/14 Pct Recovery = 63% Analysis Date = 08/11/14 Pct Recovery = 63% Analysis Date = 08/11/14 Pct Recovery = 63% Analysis Date = 07/31/14 Pct Recovery = 63% Analysis Date = 07/31/14 Pct Recovery = 63% Analysis Date = 07/20/14 Pct Recovery = 63% Analysis Date = 07/20/14 Pct Recovery = 63% Analysis Date = 07/10/14 Pct Recovery = 63% Analysis Date = 07/10/14 Pct Recovery = 63% Analysis Date = 06/29/14 Pct Recovery = 63% Analysis Date = 06/29/14 Pct Recovery = 63% Analysis Date = 06/18/14 Pct Recovery = 63% Analysis Date = 06/18/14 Pct Recovery = 63% Analysis Date = 06/08/14 Pct Recovery = 63% Analysis Date = 06/08/14 Pct Recovery = 63% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/17/14 Pct Recovery = 62% Analysis Date = 05/17/14 Pct Recovery = 62% Analysis Date = 05/06/14 Pct Recovery = 62% Analysis Date = 05/06/14 Pct Recovery = 62% Analysis Date = 04/26/14 Pct Recovery = 62% Analysis Date = 04/26/14 Pct Recovery = 62% Analysis Date = 04/15/14 Pct Recovery = 61% Analysis Date = 04/15/14 Pct Recovery = 61% Analysis Date = 04/04/14 Pct Recovery = 61% Analysis Date = 04/04/14 Pct Recovery = 61% Analysis Date = 03/24/14 Pct Recovery = 61% Analysis Date = 03/24/14 Pct Recovery = 61% Analysis Date = 03/14/14 Pct Recovery = 61% Analysis Date = 03/14/14 Pct Recovery = 61% Analysis Date = 03/03/14 Pct Recovery = 60% Analysis Date = 03/03/14 Pct Recovery = 60% Analysis Date = 02/20/14 Pct Recovery = 60% Analysis Date = 02/20/14 Pct Recovery = 60% Analysis Date = 02/09/14 Pct Recovery = 59% Analysis Date = 02/09/14 Pct Recovery = 59% Analysis Date = 01/30/14 Pct Recovery = 59% Analysis Date = 01/30/14 Pct Recovery = 59% Analysis Date = 01/19/14 Pct Recovery = 58% Analysis Date = 01/19/14 Pct Recovery = 58% Analysis Date = 01/08/14 Pct Recovery = 57% Analysis Date = 01/08/14 Pct Recovery = 57% Analysis Date = 12/29/13 Pct Recovery = 57% Analysis Date = 12/29/13 Pct Recovery = 57% Analysis Date = 12/18/13 Pct Recovery = 56% Analysis Date = 12/18/13 Pct Recovery = 56% Analysis Date = 12/07/13 Pct Recovery = 56% Analysis Date = 12/07/13 Pct Recovery = 56% Analysis Date = 11/26/13 Pct Recovery = 55% Analysis Date = 11/26/13 Pct Recovery = 55% Analysis Date = 11/16/13 Pct Recovery = 55% Analysis Date = 11/16/13 Pct Recovery = 55% Analysis Date = 11/05/13 Pct Recovery = 54% Analysis Date = 11/05/13 Pct Recovery = 54% Analysis Date = 10/25/13 Pct Recovery = 54% Analysis Date = 10/25/13 Pct Recovery = 54% Analysis Date = 10/14/13 Pct Recovery = 53% Analysis Date = 10/14/13 Pct Recovery = 53% Analysis Date = 10/04/13 Pct Recovery = 53% Analysis Date = 10/04/13 Pct Recovery = 53% Analysis Date = 09/23/13 Pct Recovery = 52% Analysis Date = 09/23/13 Pct Recovery = 52% Analysis Date = 09/12/13 Pct Recovery = 52% Analysis Date = 09/12/13 Pct Recovery = 52% Analysis Date = 09/02/13 Pct Recovery = 52% Analysis Date = 09/02/13 Pct Recovery = 52% Analysis Date = 08/22/13 Pct Recovery = 52% Analysis Date = 08/22/13 Pct Recovery = 52% Analysis Date = 08/11/13 Pct Recovery = 52% Analysis Date = 08/11/13 Pct Recovery = 52% Analysis Date = 07/31/13 Pct Recovery = 53% Analysis Date = 07/31/13 Pct Recovery = 53% Analysis Date = 07/21/13 Pct Recovery = 53% Analysis Date = 07/21/13 Pct Recovery = 53% Analysis Date = 07/10/13 Pct Recovery = 53% Analysis Date = 07/10/13 Pct Recovery = 53% Analysis Date = 06/29/13 Pct Recovery = 54% Analysis Date = 06/29/13 Pct Recovery = 54% Analysis Date = 06/18/13 Pct Recovery = 54% Analysis Date = 06/18/13 Pct Recovery = 54% Analysis Date = 06/08/13 Pct Recovery = 55% Analysis Date = 06/08/13 Pct Recovery = 55% Analysis Date = 05/28/13 Pct Recovery = 56% Analysis Date = 05/28/13 Pct Recovery = 56% Analysis Date = 05/17/13 Pct Recovery = 57% Analysis Date = 05/17/13 Pct Recovery = 57% Analysis Date = 05/07/13 Pct Recovery = 57% Analysis Date = 05/07/13 Pct Recovery = 57% Analysis Date = 04/26/13 Pct Recovery = 58% Analysis Date = 04/26/13 Pct Recovery = 58% Analysis Date = 04/15/13 Pct Recovery = 59% Analysis Date = 04/15/13 Pct Recovery = 59% Analysis Date = 04/04/13 Pct Recovery = 60% Analysis Date = 04/04/13 Pct Recovery = 60% Analysis Date = 03/25/13 Pct Recovery = 61% Analysis Date = 03/25/13 Pct Recovery = 61% Analysis Date = 03/14/13 Pct Recovery = 61% Analysis Date = 03/14/13 Pct Recovery = 61% Analysis Date = 03/03/13 Pct Recovery = 62% Analysis Date = 03/03/13 Pct Recovery = 62% Analysis Date = 02/20/13 Pct Recovery = 63% Analysis Date = 02/20/13 Pct Recovery = 63% Analysis Date = 02/10/13 Pct Recovery = 64% Analysis Date = 02/10/13 Pct Recovery = 64% Analysis Date = 01/30/13 Pct Recovery = 65% Analysis Date = 01/30/13 Pct Recovery = 65% Analysis Date = 01/19/13 Pct Recovery = 66% Analysis Date = 01/19/13 Pct Recovery = 66% Analysis Date = 01/08/13 Pct Recovery = 66% Analysis Date = 01/08/13 Pct Recovery = 66% Analysis Date = 12/29/12 Pct Recovery = 67% Analysis Date = 12/29/12 Pct Recovery = 67% Analysis Date = 12/18/12 Pct Recovery = 68% Analysis Date = 12/18/12 Pct Recovery = 68% Analysis Date = 12/07/12 Pct Recovery = 69% Analysis Date = 12/07/12 Pct Recovery = 69% Analysis Date = 11/27/12 Pct Recovery = 70% Analysis Date = 11/27/12 Pct Recovery = 70% Analysis Date = 11/16/12 Pct Recovery = 71% Analysis Date = 11/16/12 Pct Recovery = 71% Analysis Date = 11/05/12 Pct Recovery = 72% Analysis Date = 11/05/12 Pct Recovery = 72% Analysis Date = 10/25/12 Pct Recovery = 74% Analysis Date = 10/25/12 Pct Recovery = 74% Analysis Date = 10/15/12 Pct Recovery = 75% Analysis Date = 10/15/12 Pct Recovery = 75% Analysis Date = 10/04/12 Pct Recovery = 76% Analysis Date = 10/04/12 Pct Recovery = 76% Analysis Date = 09/23/12 Pct Recovery = 77% Analysis Date = 09/23/12 Pct Recovery = 77% Analysis Date = 09/12/12 Pct Recovery = 78% Analysis Date = 09/12/12 Pct Recovery = 78% Analysis Date = 09/02/12 Pct Recovery = 78% Analysis Date = 09/02/12 Pct Recovery = 78% Analysis Date = 08/22/12 Pct Recovery = 79% Analysis Date = 08/22/12 Pct Recovery = 79% Analysis Date = 08/11/12 Pct Recovery = 79% Analysis Date = 08/11/12 Pct Recovery = 79% Analysis Date = 08/01/12 Pct Recovery = 80% Analysis Date = 08/01/12 Pct Recovery = 80% Analysis Date = 07/21/12 Pct Recovery = 80% Analysis Date = 07/21/12 Pct Recovery = 80% Analysis Date = 07/10/12 Pct Recovery = 81% Analysis Date = 07/10/12 Pct Recovery = 81% Analysis Date = 06/29/12 Pct Recovery = 81% Analysis Date = 06/29/12 Pct Recovery = 81% Analysis Date = 06/19/12 Pct Recovery = 82% Analysis Date = 06/19/12 Pct Recovery = 82% Analysis Date = 06/08/12 Pct Recovery = 82% Analysis Date = 06/08/12 Pct Recovery = 82% Analysis Date = 05/28/12 Pct Recovery = 83% Analysis Date = 05/28/12 Pct Recovery = 83% Analysis Date = 05/17/12 Pct Recovery = 84% Analysis Date = 05/17/12 Pct Recovery = 84% Analysis Date = 05/07/12 Pct Recovery = 84% Analysis Date = 05/07/12 Pct Recovery = 84% Analysis Date = 04/26/12 Pct Recovery = 85% Analysis Date = 04/26/12 Pct Recovery = 85% Analysis Date = 04/15/12 Pct Recovery = 85% Analysis Date = 04/15/12 Pct Recovery = 85% Analysis Date = 04/05/12 Pct Recovery = 86% Analysis Date = 04/05/12 Pct Recovery = 86% Analysis Date = 03/25/12 Pct Recovery = 87% Analysis Date = 03/25/12 Pct Recovery = 87% Analysis Date = 03/14/12 Pct Recovery = 87% Analysis Date = 03/14/12 Pct Recovery = 87% Analysis Date = 03/03/12 Pct Recovery = 88% Analysis Date = 03/03/12 Pct Recovery = 88% Analysis Date = 02/22/12 Pct Recovery = 89% Analysis Date = 02/22/12 Pct Recovery = 89% Analysis Date = 02/11/12 Pct Recovery = 89% Analysis Date = 02/11/12 Pct Recovery = 89% Analysis Date = 01/31/12 Pct Recovery = 90% Analysis Date = 01/31/12 Pct Recovery = 90% Analysis Date = 01/20/12 Pct Recovery = 91% Analysis Date = 01/20/12 Pct Recovery = 91% Analysis Date = 01/10/12 Pct Recovery = 91% Analysis Date = 01/10/12 Pct Recovery = 91% Analysis Date = 12/30/11 Pct Recovery = 92% Analysis Date = 12/30/11 Pct Recovery = 92% Analysis Date = 12/19/11 Pct Recovery = 93% Analysis Date = 12/19/11 Pct Recovery = 93% Analysis Date = 12/08/11 Pct Recovery = 93% Analysis Date = 12/08/11 Pct Recovery = 93% Analysis Date = 11/28/11 Pct Recovery = 94% Analysis Date = 11/28/11 Pct Recovery = 94% Analysis Date = 11/17/11 Pct Recovery = 94% Analysis Date = 11/17/11 Pct Recovery = 94% Analysis Date = 11/06/11 Pct Recovery = 95% Analysis Date = 11/06/11 Pct Recovery = 95% Analysis Date = 10/27/11 Pct Recovery = 96% Analysis Date = 10/27/11 Pct Recovery = 96% Analysis Date = 10/16/11 Pct Recovery = 96% Analysis Date = 10/16/11 Pct Recovery = 96% Analysis Date = 10/05/11 Pct Recovery = 97% Analysis Date = 10/05/11 Pct Recovery = 97% Analysis Date = 09/24/11 Pct Recovery = 98% Analysis Date = 09/24/11 Pct Recovery = 98% Analysis Date = 09/14/11 Pct Recovery = 98% Analysis Date = 09/14/11 Pct Recovery = 98% Analysis Date = 09/03/11 Pct Recovery = 99% Analysis Date = 09/03/11 Pct Recovery = 99% Analysis Date = 08/23/11 Pct Recovery = 100% Analysis Date = 08/23/11 Pct Recovery = 100% Analysis Date = 08/12/11 Pct Recovery = 100% Analysis Date = 08/12/11 Pct Recovery = 100% Analysis Date = 08/02/11 Pct Recovery = 101% Analysis Date = 08/02/11 Pct Recovery = 101% Analysis Date = 07/22/11 Pct Recovery = 102% Analysis Date = 07/22/11 Pct Recovery = 102% Analysis Date = 07/11/11 Pct Recovery = 102% Analysis Date = 07/11/11 Pct Recovery = 102% Analysis Date = 07/01/11 Pct Recovery = 103% Analysis Date = 07/01/11 Pct Recovery = 103% Analysis Date = 06/20/11 Pct Recovery = 104% Analysis Date = 06/20/11 Pct Recovery = 104% Analysis Date = 06/09/11 Pct Recovery = 104% Analysis Date = 06/09/11 Pct Recovery = 104% Analysis Date = 05/29/11 Pct Recovery = 105% Analysis Date = 05/29/11 Pct Recovery = 105% Analysis Date = 05/19/11 Pct Recovery = 105% Analysis Date = 05/19/11 Pct Recovery = 105% Analysis Date = 05/08/11 Pct Recovery = 106% Analysis Date = 05/08/11 Pct Recovery = 106% Analysis Date = 04/27/11 Pct Recovery = 107% Analysis Date = 04/27/11 Pct Recovery = 107% Analysis Date = 04/16/11 Pct Recovery = 107% Analysis Date = 04/16/11 Pct Recovery = 107% Analysis Date = 04/06/11 Pct Recovery = 108% Analysis Date = 04/06/11 Pct Recovery = 108% Analysis Date = 03/26/11 Pct Recovery = 109% Analysis Date = 03/26/11 Pct Recovery = 109% Analysis Date = 03/15/11 Pct Recovery = 109% Analysis Date = 03/15/11 Pct Recovery = 109% Analysis Date = 03/05/11 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHORATE OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 118% . 118% 0%
>= Reporting Level 55 65% 20% 64% 21%
Total 56 66% 21% 64% 20%

Sample Statistics
PHORATE OXON

Characteristic N % % Basis
Plotted 56 95% Spiked
Estimated Values 56 95% Spiked
Deleted Values 7 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 3 5% 3 out of 59
Not Spiked 105 .  
False Positives 0 0% 0 out of 103

BQS OBSP Determination:
PHOSMET (IMIDAN)
METHOD: 2033 , TESTIDCODE: 61601GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 79% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 46% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 41% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 80% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 58% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 61% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 71% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 52% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 41% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 90% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 77% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 29% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 58% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 79% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 57% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 48% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 70% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 52% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 37% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 61% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 56% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 65% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 86% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 80% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 84% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 50% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 48% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 56% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 53% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 51% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 56% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 73% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 67% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 57% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 66% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 73% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 51% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 54% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 72% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 45% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 62% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 59% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 50% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 47% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 58% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 82% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 44% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 79% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 75% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 53% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 46% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 59% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 53% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 46% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 39% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 61% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 74% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 48% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 53% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 88% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 71% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 88% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 49% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 51% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 50% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 49% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 55% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 47% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 51% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 97% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 112% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 83% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 84% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 74% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 57% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 57% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 44% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 68% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 52% Analysis Date = 12/09/16 Pct Recovery = 52% Analysis Date = 12/09/16 Pct Recovery = 52% Analysis Date = 11/28/16 Pct Recovery = 52% Analysis Date = 11/28/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/07/16 Pct Recovery = 52% Analysis Date = 11/07/16 Pct Recovery = 52% Analysis Date = 10/27/16 Pct Recovery = 52% Analysis Date = 10/27/16 Pct Recovery = 52% Analysis Date = 10/16/16 Pct Recovery = 52% Analysis Date = 10/16/16 Pct Recovery = 52% Analysis Date = 10/06/16 Pct Recovery = 52% Analysis Date = 10/06/16 Pct Recovery = 52% Analysis Date = 09/25/16 Pct Recovery = 52% Analysis Date = 09/25/16 Pct Recovery = 52% Analysis Date = 09/14/16 Pct Recovery = 52% Analysis Date = 09/14/16 Pct Recovery = 52% Analysis Date = 09/03/16 Pct Recovery = 52% Analysis Date = 09/03/16 Pct Recovery = 52% Analysis Date = 08/24/16 Pct Recovery = 52% Analysis Date = 08/24/16 Pct Recovery = 52% Analysis Date = 08/13/16 Pct Recovery = 52% Analysis Date = 08/13/16 Pct Recovery = 52% Analysis Date = 08/02/16 Pct Recovery = 52% Analysis Date = 08/02/16 Pct Recovery = 52% Analysis Date = 07/23/16 Pct Recovery = 52% Analysis Date = 07/23/16 Pct Recovery = 52% Analysis Date = 07/12/16 Pct Recovery = 52% Analysis Date = 07/12/16 Pct Recovery = 52% Analysis Date = 07/01/16 Pct Recovery = 52% Analysis Date = 07/01/16 Pct Recovery = 52% Analysis Date = 06/21/16 Pct Recovery = 52% Analysis Date = 06/21/16 Pct Recovery = 52% Analysis Date = 06/10/16 Pct Recovery = 52% Analysis Date = 06/10/16 Pct Recovery = 52% Analysis Date = 05/30/16 Pct Recovery = 52% Analysis Date = 05/30/16 Pct Recovery = 52% Analysis Date = 05/19/16 Pct Recovery = 52% Analysis Date = 05/19/16 Pct Recovery = 52% Analysis Date = 05/09/16 Pct Recovery = 52% Analysis Date = 05/09/16 Pct Recovery = 52% Analysis Date = 04/28/16 Pct Recovery = 52% Analysis Date = 04/28/16 Pct Recovery = 52% Analysis Date = 04/17/16 Pct Recovery = 52% Analysis Date = 04/17/16 Pct Recovery = 52% Analysis Date = 04/07/16 Pct Recovery = 52% Analysis Date = 04/07/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/16/16 Pct Recovery = 52% Analysis Date = 03/16/16 Pct Recovery = 52% Analysis Date = 03/05/16 Pct Recovery = 52% Analysis Date = 03/05/16 Pct Recovery = 52% Analysis Date = 02/24/16 Pct Recovery = 52% Analysis Date = 02/24/16 Pct Recovery = 52% Analysis Date = 02/13/16 Pct Recovery = 52% Analysis Date = 02/13/16 Pct Recovery = 52% Analysis Date = 02/02/16 Pct Recovery = 52% Analysis Date = 02/02/16 Pct Recovery = 52% Analysis Date = 01/23/16 Pct Recovery = 52% Analysis Date = 01/23/16 Pct Recovery = 52% Analysis Date = 01/12/16 Pct Recovery = 52% Analysis Date = 01/12/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 01/01/16 Pct Recovery = 52% Analysis Date = 12/22/15 Pct Recovery = 52% Analysis Date = 12/22/15 Pct Recovery = 52% Analysis Date = 12/11/15 Pct Recovery = 52% Analysis Date = 12/11/15 Pct Recovery = 52% Analysis Date = 11/30/15 Pct Recovery = 52% Analysis Date = 11/30/15 Pct Recovery = 52% Analysis Date = 11/19/15 Pct Recovery = 52% Analysis Date = 11/19/15 Pct Recovery = 52% Analysis Date = 11/09/15 Pct Recovery = 52% Analysis Date = 11/09/15 Pct Recovery = 52% Analysis Date = 10/29/15 Pct Recovery = 52% Analysis Date = 10/29/15 Pct Recovery = 52% Analysis Date = 10/18/15 Pct Recovery = 52% Analysis Date = 10/18/15 Pct Recovery = 52% Analysis Date = 10/08/15 Pct Recovery = 52% Analysis Date = 10/08/15 Pct Recovery = 52% Analysis Date = 09/27/15 Pct Recovery = 52% Analysis Date = 09/27/15 Pct Recovery = 52% Analysis Date = 09/16/15 Pct Recovery = 52% Analysis Date = 09/16/15 Pct Recovery = 52% Analysis Date = 09/05/15 Pct Recovery = 52% Analysis Date = 09/05/15 Pct Recovery = 52% Analysis Date = 08/26/15 Pct Recovery = 52% Analysis Date = 08/26/15 Pct Recovery = 52% Analysis Date = 08/15/15 Pct Recovery = 52% Analysis Date = 08/15/15 Pct Recovery = 52% Analysis Date = 08/04/15 Pct Recovery = 52% Analysis Date = 08/04/15 Pct Recovery = 52% Analysis Date = 07/25/15 Pct Recovery = 52% Analysis Date = 07/25/15 Pct Recovery = 52% Analysis Date = 07/14/15 Pct Recovery = 52% Analysis Date = 07/14/15 Pct Recovery = 52% Analysis Date = 07/03/15 Pct Recovery = 52% Analysis Date = 07/03/15 Pct Recovery = 52% Analysis Date = 06/23/15 Pct Recovery = 53% Analysis Date = 06/23/15 Pct Recovery = 53% Analysis Date = 06/12/15 Pct Recovery = 53% Analysis Date = 06/12/15 Pct Recovery = 53% Analysis Date = 06/01/15 Pct Recovery = 53% Analysis Date = 06/01/15 Pct Recovery = 53% Analysis Date = 05/21/15 Pct Recovery = 53% Analysis Date = 05/21/15 Pct Recovery = 53% Analysis Date = 05/11/15 Pct Recovery = 53% Analysis Date = 05/11/15 Pct Recovery = 53% Analysis Date = 04/30/15 Pct Recovery = 53% Analysis Date = 04/30/15 Pct Recovery = 53% Analysis Date = 04/19/15 Pct Recovery = 53% Analysis Date = 04/19/15 Pct Recovery = 53% Analysis Date = 04/09/15 Pct Recovery = 53% Analysis Date = 04/09/15 Pct Recovery = 53% Analysis Date = 03/29/15 Pct Recovery = 53% Analysis Date = 03/29/15 Pct Recovery = 53% Analysis Date = 03/18/15 Pct Recovery = 53% Analysis Date = 03/18/15 Pct Recovery = 53% Analysis Date = 03/07/15 Pct Recovery = 53% Analysis Date = 03/07/15 Pct Recovery = 53% Analysis Date = 02/25/15 Pct Recovery = 53% Analysis Date = 02/25/15 Pct Recovery = 53% Analysis Date = 02/14/15 Pct Recovery = 53% Analysis Date = 02/14/15 Pct Recovery = 53% Analysis Date = 02/03/15 Pct Recovery = 53% Analysis Date = 02/03/15 Pct Recovery = 53% Analysis Date = 01/24/15 Pct Recovery = 53% Analysis Date = 01/24/15 Pct Recovery = 53% Analysis Date = 01/13/15 Pct Recovery = 53% Analysis Date = 01/13/15 Pct Recovery = 53% Analysis Date = 01/02/15 Pct Recovery = 54% Analysis Date = 01/02/15 Pct Recovery = 54% Analysis Date = 12/23/14 Pct Recovery = 54% Analysis Date = 12/23/14 Pct Recovery = 54% Analysis Date = 12/12/14 Pct Recovery = 54% Analysis Date = 12/12/14 Pct Recovery = 54% Analysis Date = 12/01/14 Pct Recovery = 54% Analysis Date = 12/01/14 Pct Recovery = 54% Analysis Date = 11/20/14 Pct Recovery = 54% Analysis Date = 11/20/14 Pct Recovery = 54% Analysis Date = 11/10/14 Pct Recovery = 54% Analysis Date = 11/10/14 Pct Recovery = 54% Analysis Date = 10/30/14 Pct Recovery = 55% Analysis Date = 10/30/14 Pct Recovery = 55% Analysis Date = 10/19/14 Pct Recovery = 55% Analysis Date = 10/19/14 Pct Recovery = 55% Analysis Date = 10/09/14 Pct Recovery = 55% Analysis Date = 10/09/14 Pct Recovery = 55% Analysis Date = 09/28/14 Pct Recovery = 55% Analysis Date = 09/28/14 Pct Recovery = 55% Analysis Date = 09/17/14 Pct Recovery = 55% Analysis Date = 09/17/14 Pct Recovery = 55% Analysis Date = 09/07/14 Pct Recovery = 56% Analysis Date = 09/07/14 Pct Recovery = 56% Analysis Date = 08/27/14 Pct Recovery = 56% Analysis Date = 08/27/14 Pct Recovery = 56% Analysis Date = 08/16/14 Pct Recovery = 56% Analysis Date = 08/16/14 Pct Recovery = 56% Analysis Date = 08/05/14 Pct Recovery = 56% Analysis Date = 08/05/14 Pct Recovery = 56% Analysis Date = 07/26/14 Pct Recovery = 57% Analysis Date = 07/26/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/15/14 Pct Recovery = 57% Analysis Date = 07/04/14 Pct Recovery = 57% Analysis Date = 07/04/14 Pct Recovery = 57% Analysis Date = 06/24/14 Pct Recovery = 57% Analysis Date = 06/24/14 Pct Recovery = 57% Analysis Date = 06/13/14 Pct Recovery = 58% Analysis Date = 06/13/14 Pct Recovery = 58% Analysis Date = 06/02/14 Pct Recovery = 58% Analysis Date = 06/02/14 Pct Recovery = 58% Analysis Date = 05/22/14 Pct Recovery = 58% Analysis Date = 05/22/14 Pct Recovery = 58% Analysis Date = 05/12/14 Pct Recovery = 59% Analysis Date = 05/12/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 05/01/14 Pct Recovery = 59% Analysis Date = 04/20/14 Pct Recovery = 59% Analysis Date = 04/20/14 Pct Recovery = 59% Analysis Date = 04/10/14 Pct Recovery = 60% Analysis Date = 04/10/14 Pct Recovery = 60% Analysis Date = 03/30/14 Pct Recovery = 60% Analysis Date = 03/30/14 Pct Recovery = 60% Analysis Date = 03/19/14 Pct Recovery = 60% Analysis Date = 03/19/14 Pct Recovery = 60% Analysis Date = 03/09/14 Pct Recovery = 61% Analysis Date = 03/09/14 Pct Recovery = 61% Analysis Date = 02/26/14 Pct Recovery = 61% Analysis Date = 02/26/14 Pct Recovery = 61% Analysis Date = 02/15/14 Pct Recovery = 62% Analysis Date = 02/15/14 Pct Recovery = 62% Analysis Date = 02/04/14 Pct Recovery = 62% Analysis Date = 02/04/14 Pct Recovery = 62% Analysis Date = 01/25/14 Pct Recovery = 62% Analysis Date = 01/25/14 Pct Recovery = 62% Analysis Date = 01/14/14 Pct Recovery = 63% Analysis Date = 01/14/14 Pct Recovery = 63% Analysis Date = 01/03/14 Pct Recovery = 63% Analysis Date = 01/03/14 Pct Recovery = 63% Analysis Date = 12/24/13 Pct Recovery = 64% Analysis Date = 12/24/13 Pct Recovery = 64% Analysis Date = 12/13/13 Pct Recovery = 64% Analysis Date = 12/13/13 Pct Recovery = 64% Analysis Date = 12/02/13 Pct Recovery = 64% Analysis Date = 12/02/13 Pct Recovery = 64% Analysis Date = 11/21/13 Pct Recovery = 65% Analysis Date = 11/21/13 Pct Recovery = 65% Analysis Date = 11/11/13 Pct Recovery = 65% Analysis Date = 11/11/13 Pct Recovery = 65% Analysis Date = 10/31/13 Pct Recovery = 66% Analysis Date = 10/31/13 Pct Recovery = 66% Analysis Date = 10/20/13 Pct Recovery = 66% Analysis Date = 10/20/13 Pct Recovery = 66% Analysis Date = 10/10/13 Pct Recovery = 67% Analysis Date = 10/10/13 Pct Recovery = 67% Analysis Date = 09/29/13 Pct Recovery = 67% Analysis Date = 09/29/13 Pct Recovery = 67% Analysis Date = 09/18/13 Pct Recovery = 68% Analysis Date = 09/18/13 Pct Recovery = 68% Analysis Date = 09/08/13 Pct Recovery = 68% Analysis Date = 09/08/13 Pct Recovery = 68% Analysis Date = 08/28/13 Pct Recovery = 68% Analysis Date = 08/28/13 Pct Recovery = 68% Analysis Date = 08/17/13 Pct Recovery = 69% Analysis Date = 08/17/13 Pct Recovery = 69% Analysis Date = 08/06/13 Pct Recovery = 69% Analysis Date = 08/06/13 Pct Recovery = 69% Analysis Date = 07/27/13 Pct Recovery = 70% Analysis Date = 07/27/13 Pct Recovery = 70% Analysis Date = 07/16/13 Pct Recovery = 70% Analysis Date = 07/16/13 Pct Recovery = 70% Analysis Date = 07/05/13 Pct Recovery = 70% Analysis Date = 07/05/13 Pct Recovery = 70% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/25/13 Pct Recovery = 71% Analysis Date = 06/14/13 Pct Recovery = 71% Analysis Date = 06/14/13 Pct Recovery = 71% Analysis Date = 06/03/13 Pct Recovery = 72% Analysis Date = 06/03/13 Pct Recovery = 72% Analysis Date = 05/23/13 Pct Recovery = 72% Analysis Date = 05/23/13 Pct Recovery = 72% Analysis Date = 05/13/13 Pct Recovery = 73% Analysis Date = 05/13/13 Pct Recovery = 73% Analysis Date = 05/02/13 Pct Recovery = 73% Analysis Date = 05/02/13 Pct Recovery = 73% Analysis Date = 04/21/13 Pct Recovery = 73% Analysis Date = 04/21/13 Pct Recovery = 73% Analysis Date = 04/11/13 Pct Recovery = 74% Analysis Date = 04/11/13 Pct Recovery = 74% Analysis Date = 03/31/13 Pct Recovery = 74% Analysis Date = 03/31/13 Pct Recovery = 74% Analysis Date = 03/20/13 Pct Recovery = 74% Analysis Date = 03/20/13 Pct Recovery = 74% Analysis Date = 03/10/13 Pct Recovery = 74% Analysis Date = 03/10/13 Pct Recovery = 74% Analysis Date = 02/27/13 Pct Recovery = 74% Analysis Date = 02/27/13 Pct Recovery = 74% Analysis Date = 02/16/13 Pct Recovery = 74% Analysis Date = 02/16/13 Pct Recovery = 74% Analysis Date = 02/05/13 Pct Recovery = 74% Analysis Date = 02/05/13 Pct Recovery = 74% Analysis Date = 01/26/13 Pct Recovery = 75% Analysis Date = 01/26/13 Pct Recovery = 75% Analysis Date = 01/15/13 Pct Recovery = 75% Analysis Date = 01/15/13 Pct Recovery = 75% Analysis Date = 01/04/13 Pct Recovery = 75% Analysis Date = 01/04/13 Pct Recovery = 75% Analysis Date = 12/25/12 Pct Recovery = 75% Analysis Date = 12/25/12 Pct Recovery = 75% Analysis Date = 12/14/12 Pct Recovery = 75% Analysis Date = 12/14/12 Pct Recovery = 75% Analysis Date = 12/03/12 Pct Recovery = 75% Analysis Date = 12/03/12 Pct Recovery = 75% Analysis Date = 11/23/12 Pct Recovery = 74% Analysis Date = 11/23/12 Pct Recovery = 74% Analysis Date = 11/12/12 Pct Recovery = 74% Analysis Date = 11/12/12 Pct Recovery = 74% Analysis Date = 11/01/12 Pct Recovery = 74% Analysis Date = 11/01/12 Pct Recovery = 74% Analysis Date = 10/21/12 Pct Recovery = 74% Analysis Date = 10/21/12 Pct Recovery = 74% Analysis Date = 10/11/12 Pct Recovery = 74% Analysis Date = 10/11/12 Pct Recovery = 74% Analysis Date = 09/30/12 Pct Recovery = 73% Analysis Date = 09/30/12 Pct Recovery = 73% Analysis Date = 09/19/12 Pct Recovery = 73% Analysis Date = 09/19/12 Pct Recovery = 73% Analysis Date = 09/09/12 Pct Recovery = 73% Analysis Date = 09/09/12 Pct Recovery = 73% Analysis Date = 08/29/12 Pct Recovery = 73% Analysis Date = 08/29/12 Pct Recovery = 73% Analysis Date = 08/18/12 Pct Recovery = 73% Analysis Date = 08/18/12 Pct Recovery = 73% Analysis Date = 08/07/12 Pct Recovery = 72% Analysis Date = 08/07/12 Pct Recovery = 72% Analysis Date = 07/28/12 Pct Recovery = 72% Analysis Date = 07/28/12 Pct Recovery = 72% Analysis Date = 07/17/12 Pct Recovery = 72% Analysis Date = 07/17/12 Pct Recovery = 72% Analysis Date = 07/06/12 Pct Recovery = 71% Analysis Date = 07/06/12 Pct Recovery = 71% Analysis Date = 06/26/12 Pct Recovery = 71% Analysis Date = 06/26/12 Pct Recovery = 71% Analysis Date = 06/15/12 Pct Recovery = 71% Analysis Date = 06/15/12 Pct Recovery = 71% Analysis Date = 06/04/12 Pct Recovery = 71% Analysis Date = 06/04/12 Pct Recovery = 71% Analysis Date = 05/25/12 Pct Recovery = 70% Analysis Date = 05/25/12 Pct Recovery = 70% Analysis Date = 05/14/12 Pct Recovery = 70% Analysis Date = 05/14/12 Pct Recovery = 70% Analysis Date = 05/03/12 Pct Recovery = 70% Analysis Date = 05/03/12 Pct Recovery = 70% Analysis Date = 04/22/12 Pct Recovery = 70% Analysis Date = 04/22/12 Pct Recovery = 70% Analysis Date = 04/12/12 Pct Recovery = 69% Analysis Date = 04/12/12 Pct Recovery = 69% Analysis Date = 04/01/12 Pct Recovery = 69% Analysis Date = 04/01/12 Pct Recovery = 69% Analysis Date = 03/21/12 Pct Recovery = 69% Analysis Date = 03/21/12 Pct Recovery = 69% Analysis Date = 03/11/12 Pct Recovery = 68% Analysis Date = 03/11/12 Pct Recovery = 68% Analysis Date = 02/29/12 Pct Recovery = 68% Analysis Date = 02/29/12 Pct Recovery = 68% Analysis Date = 02/18/12 Pct Recovery = 68% Analysis Date = 02/18/12 Pct Recovery = 68% Analysis Date = 02/07/12 Pct Recovery = 68% Analysis Date = 02/07/12 Pct Recovery = 68% Analysis Date = 01/28/12 Pct Recovery = 67% Analysis Date = 01/28/12 Pct Recovery = 67% Analysis Date = 01/17/12 Pct Recovery = 67% Analysis Date = 01/17/12 Pct Recovery = 67% Analysis Date = 01/06/12 Pct Recovery = 67% Analysis Date = 01/06/12 Pct Recovery = 67% Analysis Date = 12/27/11 Pct Recovery = 66% Analysis Date = 12/27/11 Pct Recovery = 66% Analysis Date = 12/16/11 Pct Recovery = 66% Analysis Date = 12/16/11 Pct Recovery = 66% Analysis Date = 12/05/11 Pct Recovery = 66% Analysis Date = 12/05/11 Pct Recovery = 66% Analysis Date = 11/25/11 Pct Recovery = 66% Analysis Date = 11/25/11 Pct Recovery = 66% Analysis Date = 11/14/11 Pct Recovery = 65% Analysis Date = 11/14/11 Pct Recovery = 65% Analysis Date = 11/03/11 Pct Recovery = 65% Analysis Date = 11/03/11 Pct Recovery = 65% Analysis Date = 10/23/11 Pct Recovery = 65% Analysis Date = 10/23/11 Pct Recovery = 65% Analysis Date = 10/13/11 Pct Recovery = 64% Analysis Date = 10/13/11 Pct Recovery = 64% Analysis Date = 10/02/11 Pct Recovery = 64% Analysis Date = 10/02/11 Pct Recovery = 64% Analysis Date = 09/21/11 Pct Recovery = 64% Analysis Date = 09/21/11 Pct Recovery = 64% Analysis Date = 09/11/11 Pct Recovery = 64% Analysis Date = 09/11/11 Pct Recovery = 64% Analysis Date = 08/31/11 Pct Recovery = 63% Analysis Date = 08/31/11 Pct Recovery = 63% Analysis Date = 08/20/11 Pct Recovery = 63% Analysis Date = 08/20/11 Pct Recovery = 63% Analysis Date = 08/09/11 Pct Recovery = 63% Analysis Date = 08/09/11 Pct Recovery = 63% Analysis Date = 07/30/11 Pct Recovery = 62% Analysis Date = 07/30/11 Pct Recovery = 62% Analysis Date = 07/19/11 Pct Recovery = 62% Analysis Date = 07/19/11 Pct Recovery = 62% Analysis Date = 07/08/11 Pct Recovery = 62% Analysis Date = 07/08/11 Pct Recovery = 62% Analysis Date = 06/28/11 Pct Recovery = 61% Analysis Date = 06/28/11 Pct Recovery = 61% Analysis Date = 06/17/11 Pct Recovery = 61% Analysis Date = 06/17/11 Pct Recovery = 61% Analysis Date = 06/06/11 Pct Recovery = 61% Analysis Date = 06/06/11 Pct Recovery = 61% Analysis Date = 05/27/11 Pct Recovery = 60% Analysis Date = 05/27/11 Pct Recovery = 60% Analysis Date = 05/16/11 Pct Recovery = 60% Analysis Date = 05/16/11 Pct Recovery = 60% Analysis Date = 05/05/11 Pct Recovery = 60% Analysis Date = 05/05/11 Pct Recovery = 60% Analysis Date = 04/24/11 Pct Recovery = 59% Analysis Date = 04/24/11 Pct Recovery = 59% Analysis Date = 04/14/11 Pct Recovery = 59% Analysis Date = 04/14/11 Pct Recovery = 59% Analysis Date = 04/03/11 Pct Recovery = 58% Analysis Date = 04/03/11 Pct Recovery = 58% Analysis Date = 03/23/11 Pct Recovery = 58% Analysis Date = 03/23/11 Pct Recovery = 58% Analysis Date = 03/13/11 Pct Recovery = 58% Analysis Date = 03/13/11 Pct Recovery = 58% Analysis Date = 03/02/11 Pct Recovery = 57% Analysis Date = 03/02/11 Pct Recovery = 57% Analysis Date = 02/19/11 Pct Recovery = 57% Analysis Date = 02/19/11 Pct Recovery = 57% Analysis Date = 02/09/11 Pct Recovery = 57% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET (IMIDAN)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 68% 17% 68% 24%
>= Reporting Level 82 61% 15% 57% 17%
Total 89 62% 16% 57% 17%

Sample Statistics
PHOSMET (IMIDAN)

Characteristic N % % Basis
Plotted 89 97% Spiked
Estimated Values 89 97% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 3 3% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 92
Not Spiked 76 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
PHOSMET OXON
METHOD: 2033 , TESTIDCODE: 61668GCM39
Open Data Set

Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 390% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 267% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 62% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 97% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 74% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 87% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 35% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 69% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 31% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 31% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 29% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 56% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 56% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 52% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 101% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 166% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 61% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 63% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 56% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 76% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 37% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 71% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 67% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 29% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 92% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 35% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 42% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 106% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 95% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 94% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 93% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 50% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 65% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 83% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 87% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 46% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 80% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 66% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 52% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 78% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 121% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 142% Analysis Date = 01/17/17 Pct Recovery = 76% Analysis Date = 01/09/17 Pct Recovery = 76% Analysis Date = 01/09/17 Pct Recovery = 76% Analysis Date = 01/01/17 Pct Recovery = 76% Analysis Date = 01/01/17 Pct Recovery = 76% Analysis Date = 12/23/16 Pct Recovery = 76% Analysis Date = 12/23/16 Pct Recovery = 76% Analysis Date = 12/15/16 Pct Recovery = 75% Analysis Date = 12/15/16 Pct Recovery = 75% Analysis Date = 12/07/16 Pct Recovery = 75% Analysis Date = 12/07/16 Pct Recovery = 75% Analysis Date = 11/28/16 Pct Recovery = 75% Analysis Date = 11/28/16 Pct Recovery = 75% Analysis Date = 11/20/16 Pct Recovery = 75% Analysis Date = 11/20/16 Pct Recovery = 75% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 10/26/16 Pct Recovery = 74% Analysis Date = 10/26/16 Pct Recovery = 74% Analysis Date = 10/17/16 Pct Recovery = 74% Analysis Date = 10/17/16 Pct Recovery = 74% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/22/16 Pct Recovery = 73% Analysis Date = 09/22/16 Pct Recovery = 73% Analysis Date = 09/14/16 Pct Recovery = 73% Analysis Date = 09/14/16 Pct Recovery = 73% Analysis Date = 09/05/16 Pct Recovery = 72% Analysis Date = 09/05/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/11/16 Pct Recovery = 72% Analysis Date = 08/11/16 Pct Recovery = 72% Analysis Date = 08/03/16 Pct Recovery = 72% Analysis Date = 08/03/16 Pct Recovery = 72% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/09/16 Pct Recovery = 71% Analysis Date = 07/09/16 Pct Recovery = 71% Analysis Date = 06/30/16 Pct Recovery = 71% Analysis Date = 06/30/16 Pct Recovery = 71% Analysis Date = 06/22/16 Pct Recovery = 70% Analysis Date = 06/22/16 Pct Recovery = 70% Analysis Date = 06/13/16 Pct Recovery = 70% Analysis Date = 06/13/16 Pct Recovery = 70% Analysis Date = 06/05/16 Pct Recovery = 70% Analysis Date = 06/05/16 Pct Recovery = 70% Analysis Date = 05/28/16 Pct Recovery = 70% Analysis Date = 05/28/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/11/16 Pct Recovery = 69% Analysis Date = 05/11/16 Pct Recovery = 69% Analysis Date = 05/03/16 Pct Recovery = 69% Analysis Date = 05/03/16 Pct Recovery = 69% Analysis Date = 04/24/16 Pct Recovery = 69% Analysis Date = 04/24/16 Pct Recovery = 69% Analysis Date = 04/16/16 Pct Recovery = 68% Analysis Date = 04/16/16 Pct Recovery = 68% Analysis Date = 04/07/16 Pct Recovery = 68% Analysis Date = 04/07/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/22/16 Pct Recovery = 68% Analysis Date = 03/22/16 Pct Recovery = 68% Analysis Date = 03/13/16 Pct Recovery = 68% Analysis Date = 03/13/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 02/25/16 Pct Recovery = 67% Analysis Date = 02/25/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/09/16 Pct Recovery = 67% Analysis Date = 02/09/16 Pct Recovery = 67% Analysis Date = 01/31/16 Pct Recovery = 66% Analysis Date = 01/31/16 Pct Recovery = 66% Analysis Date = 01/23/16 Pct Recovery = 66% Analysis Date = 01/23/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/06/16 Pct Recovery = 66% Analysis Date = 01/06/16 Pct Recovery = 66% Analysis Date = 12/29/15 Pct Recovery = 65% Analysis Date = 12/29/15 Pct Recovery = 65% Analysis Date = 12/20/15 Pct Recovery = 65% Analysis Date = 12/20/15 Pct Recovery = 65% Analysis Date = 12/12/15 Pct Recovery = 65% Analysis Date = 12/12/15 Pct Recovery = 65% Analysis Date = 12/04/15 Pct Recovery = 65% Analysis Date = 12/04/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/17/15 Pct Recovery = 64% Analysis Date = 11/17/15 Pct Recovery = 64% Analysis Date = 11/08/15 Pct Recovery = 64% Analysis Date = 11/08/15 Pct Recovery = 64% Analysis Date = 10/31/15 Pct Recovery = 64% Analysis Date = 10/31/15 Pct Recovery = 64% Analysis Date = 10/23/15 Pct Recovery = 64% Analysis Date = 10/23/15 Pct Recovery = 64% Analysis Date = 10/14/15 Pct Recovery = 63% Analysis Date = 10/14/15 Pct Recovery = 63% Analysis Date = 10/06/15 Pct Recovery = 63% Analysis Date = 10/06/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/19/15 Pct Recovery = 63% Analysis Date = 09/19/15 Pct Recovery = 63% Analysis Date = 09/11/15 Pct Recovery = 62% Analysis Date = 09/11/15 Pct Recovery = 62% Analysis Date = 09/02/15 Pct Recovery = 62% Analysis Date = 09/02/15 Pct Recovery = 62% Analysis Date = 08/25/15 Pct Recovery = 62% Analysis Date = 08/25/15 Pct Recovery = 62% Analysis Date = 08/17/15 Pct Recovery = 62% Analysis Date = 08/17/15 Pct Recovery = 62% Analysis Date = 08/08/15 Pct Recovery = 62% Analysis Date = 08/08/15 Pct Recovery = 62% Analysis Date = 07/31/15 Pct Recovery = 61% Analysis Date = 07/31/15 Pct Recovery = 61% Analysis Date = 07/22/15 Pct Recovery = 61% Analysis Date = 07/22/15 Pct Recovery = 61% Analysis Date = 07/14/15 Pct Recovery = 61% Analysis Date = 07/14/15 Pct Recovery = 61% Analysis Date = 07/06/15 Pct Recovery = 61% Analysis Date = 07/06/15 Pct Recovery = 61% Analysis Date = 06/27/15 Pct Recovery = 61% Analysis Date = 06/27/15 Pct Recovery = 61% Analysis Date = 06/19/15 Pct Recovery = 60% Analysis Date = 06/19/15 Pct Recovery = 60% Analysis Date = 06/11/15 Pct Recovery = 60% Analysis Date = 06/11/15 Pct Recovery = 60% Analysis Date = 06/02/15 Pct Recovery = 60% Analysis Date = 06/02/15 Pct Recovery = 60% Analysis Date = 05/25/15 Pct Recovery = 60% Analysis Date = 05/25/15 Pct Recovery = 60% Analysis Date = 05/16/15 Pct Recovery = 60% Analysis Date = 05/16/15 Pct Recovery = 60% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 04/30/15 Pct Recovery = 59% Analysis Date = 04/30/15 Pct Recovery = 59% Analysis Date = 04/21/15 Pct Recovery = 59% Analysis Date = 04/21/15 Pct Recovery = 59% Analysis Date = 04/13/15 Pct Recovery = 59% Analysis Date = 04/13/15 Pct Recovery = 59% Analysis Date = 04/04/15 Pct Recovery = 59% Analysis Date = 04/04/15 Pct Recovery = 59% Analysis Date = 03/27/15 Pct Recovery = 59% Analysis Date = 03/27/15 Pct Recovery = 59% Analysis Date = 03/19/15 Pct Recovery = 58% Analysis Date = 03/19/15 Pct Recovery = 58% Analysis Date = 03/10/15 Pct Recovery = 58% Analysis Date = 03/10/15 Pct Recovery = 58% Analysis Date = 03/02/15 Pct Recovery = 58% Analysis Date = 03/02/15 Pct Recovery = 58% Analysis Date = 02/22/15 Pct Recovery = 58% Analysis Date = 02/22/15 Pct Recovery = 58% Analysis Date = 02/13/15 Pct Recovery = 58% Analysis Date = 02/13/15 Pct Recovery = 58% Analysis Date = 02/05/15 Pct Recovery = 58% Analysis Date = 02/05/15 Pct Recovery = 58% Analysis Date = 01/27/15 Pct Recovery = 58% Analysis Date = 01/27/15 Pct Recovery = 58% Analysis Date = 01/19/15 Pct Recovery = 58% Analysis Date = 01/19/15 Pct Recovery = 58% Analysis Date = 01/11/15 Pct Recovery = 58% Analysis Date = 01/11/15 Pct Recovery = 58% Analysis Date = 01/02/15 Pct Recovery = 58% Analysis Date = 01/02/15 Pct Recovery = 58% Analysis Date = 12/25/14 Pct Recovery = 58% Analysis Date = 12/25/14 Pct Recovery = 58% Analysis Date = 12/16/14 Pct Recovery = 57% Analysis Date = 12/16/14 Pct Recovery = 57% Analysis Date = 12/08/14 Pct Recovery = 57% Analysis Date = 12/08/14 Pct Recovery = 57% Analysis Date = 11/30/14 Pct Recovery = 57% Analysis Date = 11/30/14 Pct Recovery = 57% Analysis Date = 11/21/14 Pct Recovery = 57% Analysis Date = 11/21/14 Pct Recovery = 57% Analysis Date = 11/13/14 Pct Recovery = 57% Analysis Date = 11/13/14 Pct Recovery = 57% Analysis Date = 11/05/14 Pct Recovery = 57% Analysis Date = 11/05/14 Pct Recovery = 57% Analysis Date = 10/27/14 Pct Recovery = 57% Analysis Date = 10/27/14 Pct Recovery = 57% Analysis Date = 10/19/14 Pct Recovery = 57% Analysis Date = 10/19/14 Pct Recovery = 57% Analysis Date = 10/10/14 Pct Recovery = 57% Analysis Date = 10/10/14 Pct Recovery = 57% Analysis Date = 10/02/14 Pct Recovery = 57% Analysis Date = 10/02/14 Pct Recovery = 57% Analysis Date = 09/24/14 Pct Recovery = 57% Analysis Date = 09/24/14 Pct Recovery = 57% Analysis Date = 09/15/14 Pct Recovery = 57% Analysis Date = 09/15/14 Pct Recovery = 57% Analysis Date = 09/07/14 Pct Recovery = 56% Analysis Date = 09/07/14 Pct Recovery = 56% Analysis Date = 08/29/14 Pct Recovery = 56% Analysis Date = 08/29/14 Pct Recovery = 56% Analysis Date = 08/21/14 Pct Recovery = 56% Analysis Date = 08/21/14 Pct Recovery = 56% Analysis Date = 08/13/14 Pct Recovery = 56% Analysis Date = 08/13/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 07/27/14 Pct Recovery = 56% Analysis Date = 07/27/14 Pct Recovery = 56% Analysis Date = 07/19/14 Pct Recovery = 56% Analysis Date = 07/19/14 Pct Recovery = 56% Analysis Date = 07/10/14 Pct Recovery = 56% Analysis Date = 07/10/14 Pct Recovery = 56% Analysis Date = 07/02/14 Pct Recovery = 56% Analysis Date = 07/02/14 Pct Recovery = 56% Analysis Date = 06/23/14 Pct Recovery = 56% Analysis Date = 06/23/14 Pct Recovery = 56% Analysis Date = 06/15/14 Pct Recovery = 56% Analysis Date = 06/15/14 Pct Recovery = 56% Analysis Date = 06/07/14 Pct Recovery = 56% Analysis Date = 06/07/14 Pct Recovery = 56% Analysis Date = 05/29/14 Pct Recovery = 57% Analysis Date = 05/29/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/12/14 Pct Recovery = 57% Analysis Date = 05/12/14 Pct Recovery = 57% Analysis Date = 05/04/14 Pct Recovery = 58% Analysis Date = 05/04/14 Pct Recovery = 58% Analysis Date = 04/26/14 Pct Recovery = 58% Analysis Date = 04/26/14 Pct Recovery = 58% Analysis Date = 04/17/14 Pct Recovery = 58% Analysis Date = 04/17/14 Pct Recovery = 58% Analysis Date = 04/09/14 Pct Recovery = 59% Analysis Date = 04/09/14 Pct Recovery = 59% Analysis Date = 04/01/14 Pct Recovery = 59% Analysis Date = 04/01/14 Pct Recovery = 59% Analysis Date = 03/23/14 Pct Recovery = 60% Analysis Date = 03/23/14 Pct Recovery = 60% Analysis Date = 03/15/14 Pct Recovery = 60% Analysis Date = 03/15/14 Pct Recovery = 60% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 02/26/14 Pct Recovery = 61% Analysis Date = 02/26/14 Pct Recovery = 61% Analysis Date = 02/18/14 Pct Recovery = 62% Analysis Date = 02/18/14 Pct Recovery = 62% Analysis Date = 02/09/14 Pct Recovery = 62% Analysis Date = 02/09/14 Pct Recovery = 62% Analysis Date = 02/01/14 Pct Recovery = 63% Analysis Date = 02/01/14 Pct Recovery = 63% Analysis Date = 01/23/14 Pct Recovery = 63% Analysis Date = 01/23/14 Pct Recovery = 63% Analysis Date = 01/15/14 Pct Recovery = 64% Analysis Date = 01/15/14 Pct Recovery = 64% Analysis Date = 01/07/14 Pct Recovery = 64% Analysis Date = 01/07/14 Pct Recovery = 64% Analysis Date = 12/29/13 Pct Recovery = 65% Analysis Date = 12/29/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/13/13 Pct Recovery = 66% Analysis Date = 12/13/13 Pct Recovery = 66% Analysis Date = 12/04/13 Pct Recovery = 66% Analysis Date = 12/04/13 Pct Recovery = 66% Analysis Date = 11/26/13 Pct Recovery = 67% Analysis Date = 11/26/13 Pct Recovery = 67% Analysis Date = 11/17/13 Pct Recovery = 67% Analysis Date = 11/17/13 Pct Recovery = 67% Analysis Date = 11/09/13 Pct Recovery = 68% Analysis Date = 11/09/13 Pct Recovery = 68% Analysis Date = 11/01/13 Pct Recovery = 68% Analysis Date = 11/01/13 Pct Recovery = 68% Analysis Date = 10/23/13 Pct Recovery = 69% Analysis Date = 10/23/13 Pct Recovery = 69% Analysis Date = 10/15/13 Pct Recovery = 69% Analysis Date = 10/15/13 Pct Recovery = 69% Analysis Date = 10/06/13 Pct Recovery = 70% Analysis Date = 10/06/13 Pct Recovery = 70% Analysis Date = 09/28/13 Pct Recovery = 70% Analysis Date = 09/28/13 Pct Recovery = 70% Analysis Date = 09/20/13 Pct Recovery = 71% Analysis Date = 09/20/13 Pct Recovery = 71% Analysis Date = 09/11/13 Pct Recovery = 71% Analysis Date = 09/11/13 Pct Recovery = 71% Analysis Date = 09/03/13 Pct Recovery = 72% Analysis Date = 09/03/13 Pct Recovery = 72% Analysis Date = 08/26/13 Pct Recovery = 72% Analysis Date = 08/26/13 Pct Recovery = 72% Analysis Date = 08/17/13 Pct Recovery = 73% Analysis Date = 08/17/13 Pct Recovery = 73% Analysis Date = 08/09/13 Pct Recovery = 74% Analysis Date = 08/09/13 Pct Recovery = 74% Analysis Date = 07/31/13 Pct Recovery = 75% Analysis Date = 07/31/13 Pct Recovery = 75% Analysis Date = 07/23/13 Pct Recovery = 76% Analysis Date = 07/23/13 Pct Recovery = 76% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/06/13 Pct Recovery = 78% Analysis Date = 07/06/13 Pct Recovery = 78% Analysis Date = 06/28/13 Pct Recovery = 79% Analysis Date = 06/28/13 Pct Recovery = 79% Analysis Date = 06/19/13 Pct Recovery = 80% Analysis Date = 06/19/13 Pct Recovery = 80% Analysis Date = 06/11/13 Pct Recovery = 82% Analysis Date = 06/11/13 Pct Recovery = 82% Analysis Date = 06/03/13 Pct Recovery = 83% Analysis Date = 06/03/13 Pct Recovery = 83% Analysis Date = 05/25/13 Pct Recovery = 84% Analysis Date = 05/25/13 Pct Recovery = 84% Analysis Date = 05/17/13 Pct Recovery = 86% Analysis Date = 05/17/13 Pct Recovery = 86% Analysis Date = 05/09/13 Pct Recovery = 88% Analysis Date = 05/09/13 Pct Recovery = 88% Analysis Date = 04/30/13 Pct Recovery = 91% Analysis Date = 04/30/13 Pct Recovery = 91% Analysis Date = 04/22/13 Pct Recovery = 93% Analysis Date = 04/22/13 Pct Recovery = 93% Analysis Date = 04/13/13 Pct Recovery = 96% Analysis Date = 04/13/13 Pct Recovery = 96% Analysis Date = 04/05/13 Pct Recovery = 99% Analysis Date = 04/05/13 Pct Recovery = 99% Analysis Date = 03/28/13 Pct Recovery = 101% Analysis Date = 03/28/13 Pct Recovery = 101% Analysis Date = 03/19/13 Pct Recovery = 104% Analysis Date = 03/19/13 Pct Recovery = 104% Analysis Date = 03/11/13 Pct Recovery = 106% Analysis Date = 03/11/13 Pct Recovery = 106% Analysis Date = 03/02/13 Pct Recovery = 109% Analysis Date = 03/02/13 Pct Recovery = 109% Analysis Date = 02/22/13 Pct Recovery = 112% Analysis Date = 02/22/13 Pct Recovery = 112% Analysis Date = 02/14/13 Pct Recovery = 114% Analysis Date = 02/14/13 Pct Recovery = 114% Analysis Date = 02/05/13 Pct Recovery = 117% Analysis Date = 02/05/13 Pct Recovery = 117% Analysis Date = 01/28/13 Pct Recovery = 120% Analysis Date = 01/28/13 Pct Recovery = 120% Analysis Date = 01/20/13 Pct Recovery = 122% Analysis Date = 01/20/13 Pct Recovery = 122% Analysis Date = 01/11/13 Pct Recovery = 125% Analysis Date = 01/11/13 Pct Recovery = 125% Analysis Date = 01/03/13 Pct Recovery = 128% Analysis Date = 01/03/13 Pct Recovery = 128% Analysis Date = 12/25/12 Pct Recovery = 130% Analysis Date = 12/25/12 Pct Recovery = 130% Analysis Date = 12/17/12 Pct Recovery = 133% Analysis Date = 12/17/12 Pct Recovery = 133% Analysis Date = 12/09/12 Pct Recovery = 136% Analysis Date = 12/09/12 Pct Recovery = 136% Analysis Date = 11/30/12 Pct Recovery = 138% Analysis Date = 11/30/12 Pct Recovery = 138% Analysis Date = 11/22/12 Pct Recovery = 141% Analysis Date = 11/22/12 Pct Recovery = 141% Analysis Date = 11/13/12 Pct Recovery = 144% Analysis Date = 11/13/12 Pct Recovery = 144% Analysis Date = 11/05/12 Pct Recovery = 147% Analysis Date = 11/05/12 Pct Recovery = 147% Analysis Date = 10/28/12 Pct Recovery = 149% Analysis Date = 10/28/12 Pct Recovery = 149% Analysis Date = 10/19/12 Pct Recovery = 152% Analysis Date = 10/19/12 Pct Recovery = 152% Analysis Date = 10/11/12 Pct Recovery = 155% Analysis Date = 10/11/12 Pct Recovery = 155% Analysis Date = 10/03/12 Pct Recovery = 157% Analysis Date = 10/03/12 Pct Recovery = 157% Analysis Date = 09/24/12 Pct Recovery = 160% Analysis Date = 09/24/12 Pct Recovery = 160% Analysis Date = 09/16/12 Pct Recovery = 163% Analysis Date = 09/16/12 Pct Recovery = 163% Analysis Date = 09/07/12 Pct Recovery = 166% Analysis Date = 09/07/12 Pct Recovery = 166% Analysis Date = 08/30/12 Pct Recovery = 169% Analysis Date = 08/30/12 Pct Recovery = 169% Analysis Date = 08/22/12 Pct Recovery = 172% Analysis Date = 08/22/12 Pct Recovery = 172% Analysis Date = 08/13/12 Pct Recovery = 175% Analysis Date = 08/13/12 Pct Recovery = 175% Analysis Date = 08/05/12 Pct Recovery = 178% Analysis Date = 08/05/12 Pct Recovery = 178% Analysis Date = 07/27/12 Pct Recovery = 181% Analysis Date = 07/27/12 Pct Recovery = 181% Analysis Date = 07/19/12 Pct Recovery = 184% Analysis Date = 07/19/12 Pct Recovery = 184% Analysis Date = 07/11/12 Pct Recovery = 187% Analysis Date = 07/11/12 Pct Recovery = 187% Analysis Date = 07/02/12 Pct Recovery = 190% Analysis Date = 07/02/12 Pct Recovery = 190% Analysis Date = 06/24/12 Pct Recovery = 193% Analysis Date = 06/24/12 Pct Recovery = 193% Analysis Date = 06/16/12 Pct Recovery = 196% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 80% 56% 70% 23%
Total 56 80% 56% 70% 23%

Sample Statistics
PHOSMET OXON

Characteristic N % % Basis
Plotted 56 93% Spiked
Estimated Values 56 93% Spiked
Deleted Values 9 5% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 64 .  
False Negatives 3 5% 3 out of 60
Not Spiked 105 .  
False Positives 3 3% 3 out of 100

BQS OBSP Determination:
PROMETON
METHOD: 2033 , TESTIDCODE: 04037GCM35
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 88% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 93% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 79% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 93% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 73% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 74% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 84% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 93% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 89% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 99% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 93% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 110% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 59% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 98% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 95% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 72% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 75% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 50% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 99% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 78% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 71% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 81% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 94% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 81% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 77% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 101% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 47% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 66% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 67% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 73% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 100% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 87% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 73% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 83% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 113% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 77% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 79% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 92% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 77% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 95% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 101% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 87% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 82% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 72% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 95% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 49% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 106% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 75% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 86% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 90% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 117% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 66% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 60% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 80% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 107% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 74% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 88% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 76% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 58% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 80% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 100% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 75% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 85% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 78% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 98% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 101% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 67% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 117% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 102% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 54% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 55% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 110% Analysis Date = 12/19/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/17/16 Pct Recovery = 71% Analysis Date = 11/07/16 Pct Recovery = 71% Analysis Date = 11/07/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/27/16 Pct Recovery = 71% Analysis Date = 10/16/16 Pct Recovery = 71% Analysis Date = 10/16/16 Pct Recovery = 71% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 10/06/16 Pct Recovery = 72% Analysis Date = 09/25/16 Pct Recovery = 72% Analysis Date = 09/25/16 Pct Recovery = 72% Analysis Date = 09/14/16 Pct Recovery = 72% Analysis Date = 09/14/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/13/16 Pct Recovery = 72% Analysis Date = 08/13/16 Pct Recovery = 72% Analysis Date = 08/02/16 Pct Recovery = 72% Analysis Date = 08/02/16 Pct Recovery = 72% Analysis Date = 07/23/16 Pct Recovery = 72% Analysis Date = 07/23/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/10/16 Pct Recovery = 73% Analysis Date = 06/10/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/17/16 Pct Recovery = 73% Analysis Date = 04/17/16 Pct Recovery = 73% Analysis Date = 04/06/16 Pct Recovery = 73% Analysis Date = 04/06/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/16/16 Pct Recovery = 74% Analysis Date = 03/05/16 Pct Recovery = 74% Analysis Date = 03/05/16 Pct Recovery = 74% Analysis Date = 02/24/16 Pct Recovery = 74% Analysis Date = 02/24/16 Pct Recovery = 74% Analysis Date = 02/13/16 Pct Recovery = 74% Analysis Date = 02/13/16 Pct Recovery = 74% Analysis Date = 02/02/16 Pct Recovery = 74% Analysis Date = 02/02/16 Pct Recovery = 74% Analysis Date = 01/22/16 Pct Recovery = 74% Analysis Date = 01/22/16 Pct Recovery = 74% Analysis Date = 01/12/16 Pct Recovery = 74% Analysis Date = 01/12/16 Pct Recovery = 74% Analysis Date = 01/01/16 Pct Recovery = 74% Analysis Date = 01/01/16 Pct Recovery = 74% Analysis Date = 12/21/15 Pct Recovery = 74% Analysis Date = 12/21/15 Pct Recovery = 74% Analysis Date = 12/11/15 Pct Recovery = 74% Analysis Date = 12/11/15 Pct Recovery = 74% Analysis Date = 11/30/15 Pct Recovery = 74% Analysis Date = 11/30/15 Pct Recovery = 74% Analysis Date = 11/19/15 Pct Recovery = 75% Analysis Date = 11/19/15 Pct Recovery = 75% Analysis Date = 11/09/15 Pct Recovery = 75% Analysis Date = 11/09/15 Pct Recovery = 75% Analysis Date = 10/29/15 Pct Recovery = 75% Analysis Date = 10/29/15 Pct Recovery = 75% Analysis Date = 10/18/15 Pct Recovery = 75% Analysis Date = 10/18/15 Pct Recovery = 75% Analysis Date = 10/07/15 Pct Recovery = 75% Analysis Date = 10/07/15 Pct Recovery = 75% Analysis Date = 09/27/15 Pct Recovery = 75% Analysis Date = 09/27/15 Pct Recovery = 75% Analysis Date = 09/16/15 Pct Recovery = 75% Analysis Date = 09/16/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/15/15 Pct Recovery = 75% Analysis Date = 08/15/15 Pct Recovery = 75% Analysis Date = 08/04/15 Pct Recovery = 76% Analysis Date = 08/04/15 Pct Recovery = 76% Analysis Date = 07/24/15 Pct Recovery = 76% Analysis Date = 07/24/15 Pct Recovery = 76% Analysis Date = 07/14/15 Pct Recovery = 76% Analysis Date = 07/14/15 Pct Recovery = 76% Analysis Date = 07/03/15 Pct Recovery = 76% Analysis Date = 07/03/15 Pct Recovery = 76% Analysis Date = 06/22/15 Pct Recovery = 76% Analysis Date = 06/22/15 Pct Recovery = 76% Analysis Date = 06/12/15 Pct Recovery = 76% Analysis Date = 06/12/15 Pct Recovery = 76% Analysis Date = 06/01/15 Pct Recovery = 76% Analysis Date = 06/01/15 Pct Recovery = 76% Analysis Date = 05/21/15 Pct Recovery = 76% Analysis Date = 05/21/15 Pct Recovery = 76% Analysis Date = 05/10/15 Pct Recovery = 76% Analysis Date = 05/10/15 Pct Recovery = 76% Analysis Date = 04/30/15 Pct Recovery = 77% Analysis Date = 04/30/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/19/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/18/15 Pct Recovery = 77% Analysis Date = 03/18/15 Pct Recovery = 77% Analysis Date = 03/07/15 Pct Recovery = 78% Analysis Date = 03/07/15 Pct Recovery = 78% Analysis Date = 02/24/15 Pct Recovery = 78% Analysis Date = 02/24/15 Pct Recovery = 78% Analysis Date = 02/14/15 Pct Recovery = 78% Analysis Date = 02/14/15 Pct Recovery = 78% Analysis Date = 02/03/15 Pct Recovery = 78% Analysis Date = 02/03/15 Pct Recovery = 78% Analysis Date = 01/23/15 Pct Recovery = 78% Analysis Date = 01/23/15 Pct Recovery = 78% Analysis Date = 01/13/15 Pct Recovery = 78% Analysis Date = 01/13/15 Pct Recovery = 78% Analysis Date = 01/02/15 Pct Recovery = 79% Analysis Date = 01/02/15 Pct Recovery = 79% Analysis Date = 12/22/14 Pct Recovery = 79% Analysis Date = 12/22/14 Pct Recovery = 79% Analysis Date = 12/12/14 Pct Recovery = 79% Analysis Date = 12/12/14 Pct Recovery = 79% Analysis Date = 12/01/14 Pct Recovery = 79% Analysis Date = 12/01/14 Pct Recovery = 79% Analysis Date = 11/20/14 Pct Recovery = 79% Analysis Date = 11/20/14 Pct Recovery = 79% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 11/09/14 Pct Recovery = 80% Analysis Date = 10/30/14 Pct Recovery = 80% Analysis Date = 10/30/14 Pct Recovery = 80% Analysis Date = 10/19/14 Pct Recovery = 80% Analysis Date = 10/19/14 Pct Recovery = 80% Analysis Date = 10/08/14 Pct Recovery = 80% Analysis Date = 10/08/14 Pct Recovery = 80% Analysis Date = 09/28/14 Pct Recovery = 80% Analysis Date = 09/28/14 Pct Recovery = 80% Analysis Date = 09/17/14 Pct Recovery = 80% Analysis Date = 09/17/14 Pct Recovery = 80% Analysis Date = 09/06/14 Pct Recovery = 81% Analysis Date = 09/06/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/26/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/16/14 Pct Recovery = 81% Analysis Date = 08/05/14 Pct Recovery = 81% Analysis Date = 08/05/14 Pct Recovery = 81% Analysis Date = 07/25/14 Pct Recovery = 81% Analysis Date = 07/25/14 Pct Recovery = 81% Analysis Date = 07/15/14 Pct Recovery = 81% Analysis Date = 07/15/14 Pct Recovery = 81% Analysis Date = 07/04/14 Pct Recovery = 81% Analysis Date = 07/04/14 Pct Recovery = 81% Analysis Date = 06/23/14 Pct Recovery = 81% Analysis Date = 06/23/14 Pct Recovery = 81% Analysis Date = 06/12/14 Pct Recovery = 82% Analysis Date = 06/12/14 Pct Recovery = 82% Analysis Date = 06/02/14 Pct Recovery = 82% Analysis Date = 06/02/14 Pct Recovery = 82% Analysis Date = 05/22/14 Pct Recovery = 82% Analysis Date = 05/22/14 Pct Recovery = 82% Analysis Date = 05/11/14 Pct Recovery = 82% Analysis Date = 05/11/14 Pct Recovery = 82% Analysis Date = 05/01/14 Pct Recovery = 82% Analysis Date = 05/01/14 Pct Recovery = 82% Analysis Date = 04/20/14 Pct Recovery = 82% Analysis Date = 04/20/14 Pct Recovery = 82% Analysis Date = 04/09/14 Pct Recovery = 82% Analysis Date = 04/09/14 Pct Recovery = 82% Analysis Date = 03/29/14 Pct Recovery = 82% Analysis Date = 03/29/14 Pct Recovery = 82% Analysis Date = 03/19/14 Pct Recovery = 82% Analysis Date = 03/19/14 Pct Recovery = 82% Analysis Date = 03/08/14 Pct Recovery = 82% Analysis Date = 03/08/14 Pct Recovery = 82% Analysis Date = 02/25/14 Pct Recovery = 82% Analysis Date = 02/25/14 Pct Recovery = 82% Analysis Date = 02/15/14 Pct Recovery = 82% Analysis Date = 02/15/14 Pct Recovery = 82% Analysis Date = 02/04/14 Pct Recovery = 82% Analysis Date = 02/04/14 Pct Recovery = 82% Analysis Date = 01/24/14 Pct Recovery = 83% Analysis Date = 01/24/14 Pct Recovery = 83% Analysis Date = 01/13/14 Pct Recovery = 83% Analysis Date = 01/13/14 Pct Recovery = 83% Analysis Date = 01/03/14 Pct Recovery = 83% Analysis Date = 01/03/14 Pct Recovery = 83% Analysis Date = 12/23/13 Pct Recovery = 83% Analysis Date = 12/23/13 Pct Recovery = 83% Analysis Date = 12/12/13 Pct Recovery = 83% Analysis Date = 12/12/13 Pct Recovery = 83% Analysis Date = 12/02/13 Pct Recovery = 83% Analysis Date = 12/02/13 Pct Recovery = 83% Analysis Date = 11/21/13 Pct Recovery = 83% Analysis Date = 11/21/13 Pct Recovery = 83% Analysis Date = 11/10/13 Pct Recovery = 84% Analysis Date = 11/10/13 Pct Recovery = 84% Analysis Date = 10/31/13 Pct Recovery = 84% Analysis Date = 10/31/13 Pct Recovery = 84% Analysis Date = 10/20/13 Pct Recovery = 84% Analysis Date = 10/20/13 Pct Recovery = 84% Analysis Date = 10/09/13 Pct Recovery = 84% Analysis Date = 10/09/13 Pct Recovery = 84% Analysis Date = 09/28/13 Pct Recovery = 84% Analysis Date = 09/28/13 Pct Recovery = 84% Analysis Date = 09/18/13 Pct Recovery = 84% Analysis Date = 09/18/13 Pct Recovery = 84% Analysis Date = 09/07/13 Pct Recovery = 85% Analysis Date = 09/07/13 Pct Recovery = 85% Analysis Date = 08/27/13 Pct Recovery = 85% Analysis Date = 08/27/13 Pct Recovery = 85% Analysis Date = 08/17/13 Pct Recovery = 85% Analysis Date = 08/17/13 Pct Recovery = 85% Analysis Date = 08/06/13 Pct Recovery = 85% Analysis Date = 08/06/13 Pct Recovery = 85% Analysis Date = 07/26/13 Pct Recovery = 86% Analysis Date = 07/26/13 Pct Recovery = 86% Analysis Date = 07/15/13 Pct Recovery = 86% Analysis Date = 07/15/13 Pct Recovery = 86% Analysis Date = 07/05/13 Pct Recovery = 86% Analysis Date = 07/05/13 Pct Recovery = 86% Analysis Date = 06/24/13 Pct Recovery = 86% Analysis Date = 06/24/13 Pct Recovery = 86% Analysis Date = 06/13/13 Pct Recovery = 86% Analysis Date = 06/13/13 Pct Recovery = 86% Analysis Date = 06/03/13 Pct Recovery = 87% Analysis Date = 06/03/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/23/13 Pct Recovery = 87% Analysis Date = 05/12/13 Pct Recovery = 87% Analysis Date = 05/12/13 Pct Recovery = 87% Analysis Date = 05/01/13 Pct Recovery = 87% Analysis Date = 05/01/13 Pct Recovery = 87% Analysis Date = 04/21/13 Pct Recovery = 87% Analysis Date = 04/21/13 Pct Recovery = 87% Analysis Date = 04/10/13 Pct Recovery = 87% Analysis Date = 04/10/13 Pct Recovery = 87% Analysis Date = 03/30/13 Pct Recovery = 88% Analysis Date = 03/30/13 Pct Recovery = 88% Analysis Date = 03/20/13 Pct Recovery = 88% Analysis Date = 03/20/13 Pct Recovery = 88% Analysis Date = 03/09/13 Pct Recovery = 88% Analysis Date = 03/09/13 Pct Recovery = 88% Analysis Date = 02/26/13 Pct Recovery = 88% Analysis Date = 02/26/13 Pct Recovery = 88% Analysis Date = 02/15/13 Pct Recovery = 88% Analysis Date = 02/15/13 Pct Recovery = 88% Analysis Date = 02/05/13 Pct Recovery = 88% Analysis Date = 02/05/13 Pct Recovery = 88% Analysis Date = 01/25/13 Pct Recovery = 88% Analysis Date = 01/25/13 Pct Recovery = 88% Analysis Date = 01/14/13 Pct Recovery = 89% Analysis Date = 01/14/13 Pct Recovery = 89% Analysis Date = 01/04/13 Pct Recovery = 89% Analysis Date = 01/04/13 Pct Recovery = 89% Analysis Date = 12/24/12 Pct Recovery = 89% Analysis Date = 12/24/12 Pct Recovery = 89% Analysis Date = 12/13/12 Pct Recovery = 89% Analysis Date = 12/13/12 Pct Recovery = 89% Analysis Date = 12/03/12 Pct Recovery = 89% Analysis Date = 12/03/12 Pct Recovery = 89% Analysis Date = 11/22/12 Pct Recovery = 89% Analysis Date = 11/22/12 Pct Recovery = 89% Analysis Date = 11/11/12 Pct Recovery = 89% Analysis Date = 11/11/12 Pct Recovery = 89% Analysis Date = 10/31/12 Pct Recovery = 89% Analysis Date = 10/31/12 Pct Recovery = 89% Analysis Date = 10/21/12 Pct Recovery = 89% Analysis Date = 10/21/12 Pct Recovery = 89% Analysis Date = 10/10/12 Pct Recovery = 89% Analysis Date = 10/10/12 Pct Recovery = 89% Analysis Date = 09/29/12 Pct Recovery = 89% Analysis Date = 09/29/12 Pct Recovery = 89% Analysis Date = 09/19/12 Pct Recovery = 89% Analysis Date = 09/19/12 Pct Recovery = 89% Analysis Date = 09/08/12 Pct Recovery = 89% Analysis Date = 09/08/12 Pct Recovery = 89% Analysis Date = 08/28/12 Pct Recovery = 89% Analysis Date = 08/28/12 Pct Recovery = 89% Analysis Date = 08/17/12 Pct Recovery = 89% Analysis Date = 08/17/12 Pct Recovery = 89% Analysis Date = 08/07/12 Pct Recovery = 89% Analysis Date = 08/07/12 Pct Recovery = 89% Analysis Date = 07/27/12 Pct Recovery = 89% Analysis Date = 07/27/12 Pct Recovery = 89% Analysis Date = 07/16/12 Pct Recovery = 89% Analysis Date = 07/16/12 Pct Recovery = 89% Analysis Date = 07/06/12 Pct Recovery = 89% Analysis Date = 07/06/12 Pct Recovery = 89% Analysis Date = 06/25/12 Pct Recovery = 89% Analysis Date = 06/25/12 Pct Recovery = 89% Analysis Date = 06/14/12 Pct Recovery = 89% Analysis Date = 06/14/12 Pct Recovery = 89% Analysis Date = 06/03/12 Pct Recovery = 89% Analysis Date = 06/03/12 Pct Recovery = 89% Analysis Date = 05/24/12 Pct Recovery = 89% Analysis Date = 05/24/12 Pct Recovery = 89% Analysis Date = 05/13/12 Pct Recovery = 89% Analysis Date = 05/13/12 Pct Recovery = 89% Analysis Date = 05/02/12 Pct Recovery = 89% Analysis Date = 05/02/12 Pct Recovery = 89% Analysis Date = 04/22/12 Pct Recovery = 89% Analysis Date = 04/22/12 Pct Recovery = 89% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/10/12 Pct Recovery = 89% Analysis Date = 03/10/12 Pct Recovery = 89% Analysis Date = 02/28/12 Pct Recovery = 89% Analysis Date = 02/28/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/07/12 Pct Recovery = 89% Analysis Date = 02/07/12 Pct Recovery = 89% Analysis Date = 01/27/12 Pct Recovery = 89% Analysis Date = 01/27/12 Pct Recovery = 89% Analysis Date = 01/16/12 Pct Recovery = 89% Analysis Date = 01/16/12 Pct Recovery = 89% Analysis Date = 01/06/12 Pct Recovery = 89% Analysis Date = 01/06/12 Pct Recovery = 89% Analysis Date = 12/26/11 Pct Recovery = 89% Analysis Date = 12/26/11 Pct Recovery = 89% Analysis Date = 12/15/11 Pct Recovery = 89% Analysis Date = 12/15/11 Pct Recovery = 89% Analysis Date = 12/04/11 Pct Recovery = 89% Analysis Date = 12/04/11 Pct Recovery = 89% Analysis Date = 11/24/11 Pct Recovery = 88% Analysis Date = 11/24/11 Pct Recovery = 88% Analysis Date = 11/13/11 Pct Recovery = 88% Analysis Date = 11/13/11 Pct Recovery = 88% Analysis Date = 11/02/11 Pct Recovery = 88% Analysis Date = 11/02/11 Pct Recovery = 88% Analysis Date = 10/23/11 Pct Recovery = 88% Analysis Date = 10/23/11 Pct Recovery = 88% Analysis Date = 10/12/11 Pct Recovery = 88% Analysis Date = 10/12/11 Pct Recovery = 88% Analysis Date = 10/01/11 Pct Recovery = 88% Analysis Date = 10/01/11 Pct Recovery = 88% Analysis Date = 09/20/11 Pct Recovery = 88% Analysis Date = 09/20/11 Pct Recovery = 88% Analysis Date = 09/10/11 Pct Recovery = 88% Analysis Date = 09/10/11 Pct Recovery = 88% Analysis Date = 08/30/11 Pct Recovery = 88% Analysis Date = 08/30/11 Pct Recovery = 88% Analysis Date = 08/19/11 Pct Recovery = 88% Analysis Date = 08/19/11 Pct Recovery = 88% Analysis Date = 08/09/11 Pct Recovery = 88% Analysis Date = 08/09/11 Pct Recovery = 88% Analysis Date = 07/29/11 Pct Recovery = 88% Analysis Date = 07/29/11 Pct Recovery = 88% Analysis Date = 07/18/11 Pct Recovery = 88% Analysis Date = 07/18/11 Pct Recovery = 88% Analysis Date = 07/07/11 Pct Recovery = 88% Analysis Date = 07/07/11 Pct Recovery = 88% Analysis Date = 06/27/11 Pct Recovery = 88% Analysis Date = 06/27/11 Pct Recovery = 88% Analysis Date = 06/16/11 Pct Recovery = 88% Analysis Date = 06/16/11 Pct Recovery = 88% Analysis Date = 06/05/11 Pct Recovery = 88% Analysis Date = 06/05/11 Pct Recovery = 88% Analysis Date = 05/26/11 Pct Recovery = 88% Analysis Date = 05/26/11 Pct Recovery = 88% Analysis Date = 05/15/11 Pct Recovery = 88% Analysis Date = 05/15/11 Pct Recovery = 88% Analysis Date = 05/04/11 Pct Recovery = 88% Analysis Date = 05/04/11 Pct Recovery = 88% Analysis Date = 04/23/11 Pct Recovery = 88% Analysis Date = 04/23/11 Pct Recovery = 88% Analysis Date = 04/13/11 Pct Recovery = 88% Analysis Date = 04/13/11 Pct Recovery = 88% Analysis Date = 04/02/11 Pct Recovery = 88% Analysis Date = 04/02/11 Pct Recovery = 88% Analysis Date = 03/22/11 Pct Recovery = 88% Analysis Date = 03/22/11 Pct Recovery = 88% Analysis Date = 03/12/11 Pct Recovery = 87% Analysis Date = 03/12/11 Pct Recovery = 87% Analysis Date = 03/01/11 Pct Recovery = 87% Analysis Date = 03/01/11 Pct Recovery = 87% Analysis Date = 02/18/11 Pct Recovery = 87% Analysis Date = 02/18/11 Pct Recovery = 87% Analysis Date = 02/08/11 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 83% 16% 83% 16%
Total 87 83% 16% 83% 16%

Sample Statistics
PROMETON

Characteristic N % % Basis
Plotted 87 100% Spiked
Estimated Values 2 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 0 0% 0 out of 87
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

BQS OBSP Determination:
PROMETRYN
METHOD: 2033 , TESTIDCODE: 04036GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 76% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 101% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 87% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 90% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 84% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 99% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 84% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 90% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 87% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 70% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 91% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 110% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 90% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 89% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 122% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 15% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 54% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 94% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 69% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 72% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 81% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 85% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 70% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 84% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 69% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 75% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 72% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 65% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 70% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 93% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 102% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 81% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 79% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 95% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 71% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 96% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 115% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 82% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 117% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 85% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 78% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 67% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 90% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 97% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 85% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 31% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 28% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 65% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 75% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 78% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 105% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 73% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 63% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 80% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 69% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 76% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 85% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 108% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 80% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 71% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 87% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 66% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 76% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 102% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 65% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 76% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 94% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 64% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 101% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 85% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 85% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 19% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 01/18/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 77% Analysis Date = 12/27/16 Pct Recovery = 77% Analysis Date = 12/27/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 76% Analysis Date = 12/16/16 Pct Recovery = 76% Analysis Date = 12/05/16 Pct Recovery = 76% Analysis Date = 12/05/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/14/16 Pct Recovery = 76% Analysis Date = 11/14/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 11/03/16 Pct Recovery = 76% Analysis Date = 10/23/16 Pct Recovery = 76% Analysis Date = 10/23/16 Pct Recovery = 76% Analysis Date = 10/12/16 Pct Recovery = 76% Analysis Date = 10/12/16 Pct Recovery = 76% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/08/16 Pct Recovery = 75% Analysis Date = 08/08/16 Pct Recovery = 75% Analysis Date = 07/28/16 Pct Recovery = 75% Analysis Date = 07/28/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 74% Analysis Date = 06/26/16 Pct Recovery = 74% Analysis Date = 06/15/16 Pct Recovery = 74% Analysis Date = 06/15/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 74% Analysis Date = 05/14/16 Pct Recovery = 74% Analysis Date = 05/14/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 04/22/16 Pct Recovery = 74% Analysis Date = 04/22/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 03/31/16 Pct Recovery = 74% Analysis Date = 03/31/16 Pct Recovery = 74% Analysis Date = 03/20/16 Pct Recovery = 74% Analysis Date = 03/20/16 Pct Recovery = 74% Analysis Date = 03/10/16 Pct Recovery = 74% Analysis Date = 03/10/16 Pct Recovery = 74% Analysis Date = 02/28/16 Pct Recovery = 74% Analysis Date = 02/28/16 Pct Recovery = 74% Analysis Date = 02/17/16 Pct Recovery = 74% Analysis Date = 02/17/16 Pct Recovery = 74% Analysis Date = 02/06/16 Pct Recovery = 73% Analysis Date = 02/06/16 Pct Recovery = 73% Analysis Date = 01/26/16 Pct Recovery = 73% Analysis Date = 01/26/16 Pct Recovery = 73% Analysis Date = 01/15/16 Pct Recovery = 73% Analysis Date = 01/15/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 12/25/15 Pct Recovery = 73% Analysis Date = 12/25/15 Pct Recovery = 73% Analysis Date = 12/14/15 Pct Recovery = 73% Analysis Date = 12/14/15 Pct Recovery = 73% Analysis Date = 12/03/15 Pct Recovery = 73% Analysis Date = 12/03/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/22/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/01/15 Pct Recovery = 73% Analysis Date = 11/01/15 Pct Recovery = 73% Analysis Date = 10/21/15 Pct Recovery = 73% Analysis Date = 10/21/15 Pct Recovery = 73% Analysis Date = 10/10/15 Pct Recovery = 73% Analysis Date = 10/10/15 Pct Recovery = 73% Analysis Date = 09/29/15 Pct Recovery = 73% Analysis Date = 09/29/15 Pct Recovery = 73% Analysis Date = 09/18/15 Pct Recovery = 73% Analysis Date = 09/18/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 73% Analysis Date = 09/08/15 Pct Recovery = 73% Analysis Date = 08/28/15 Pct Recovery = 73% Analysis Date = 08/28/15 Pct Recovery = 73% Analysis Date = 08/17/15 Pct Recovery = 73% Analysis Date = 08/17/15 Pct Recovery = 73% Analysis Date = 08/06/15 Pct Recovery = 73% Analysis Date = 08/06/15 Pct Recovery = 73% Analysis Date = 07/26/15 Pct Recovery = 72% Analysis Date = 07/26/15 Pct Recovery = 72% Analysis Date = 07/15/15 Pct Recovery = 72% Analysis Date = 07/15/15 Pct Recovery = 72% Analysis Date = 07/05/15 Pct Recovery = 72% Analysis Date = 07/05/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/24/15 Pct Recovery = 72% Analysis Date = 06/13/15 Pct Recovery = 72% Analysis Date = 06/13/15 Pct Recovery = 72% Analysis Date = 06/02/15 Pct Recovery = 72% Analysis Date = 06/02/15 Pct Recovery = 72% Analysis Date = 05/22/15 Pct Recovery = 72% Analysis Date = 05/22/15 Pct Recovery = 72% Analysis Date = 05/11/15 Pct Recovery = 72% Analysis Date = 05/11/15 Pct Recovery = 72% Analysis Date = 05/01/15 Pct Recovery = 72% Analysis Date = 05/01/15 Pct Recovery = 72% Analysis Date = 04/20/15 Pct Recovery = 72% Analysis Date = 04/20/15 Pct Recovery = 72% Analysis Date = 04/09/15 Pct Recovery = 72% Analysis Date = 04/09/15 Pct Recovery = 72% Analysis Date = 03/29/15 Pct Recovery = 72% Analysis Date = 03/29/15 Pct Recovery = 72% Analysis Date = 03/18/15 Pct Recovery = 72% Analysis Date = 03/18/15 Pct Recovery = 72% Analysis Date = 03/08/15 Pct Recovery = 72% Analysis Date = 03/08/15 Pct Recovery = 72% Analysis Date = 02/25/15 Pct Recovery = 72% Analysis Date = 02/25/15 Pct Recovery = 72% Analysis Date = 02/14/15 Pct Recovery = 72% Analysis Date = 02/14/15 Pct Recovery = 72% Analysis Date = 02/03/15 Pct Recovery = 72% Analysis Date = 02/03/15 Pct Recovery = 72% Analysis Date = 01/23/15 Pct Recovery = 72% Analysis Date = 01/23/15 Pct Recovery = 72% Analysis Date = 01/12/15 Pct Recovery = 72% Analysis Date = 01/12/15 Pct Recovery = 72% Analysis Date = 01/02/15 Pct Recovery = 72% Analysis Date = 01/02/15 Pct Recovery = 72% Analysis Date = 12/22/14 Pct Recovery = 72% Analysis Date = 12/22/14 Pct Recovery = 72% Analysis Date = 12/11/14 Pct Recovery = 73% Analysis Date = 12/11/14 Pct Recovery = 73% Analysis Date = 11/30/14 Pct Recovery = 73% Analysis Date = 11/30/14 Pct Recovery = 73% Analysis Date = 11/19/14 Pct Recovery = 73% Analysis Date = 11/19/14 Pct Recovery = 73% Analysis Date = 11/08/14 Pct Recovery = 73% Analysis Date = 11/08/14 Pct Recovery = 73% Analysis Date = 10/29/14 Pct Recovery = 73% Analysis Date = 10/29/14 Pct Recovery = 73% Analysis Date = 10/18/14 Pct Recovery = 73% Analysis Date = 10/18/14 Pct Recovery = 73% Analysis Date = 10/07/14 Pct Recovery = 73% Analysis Date = 10/07/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 73% Analysis Date = 09/26/14 Pct Recovery = 73% Analysis Date = 09/15/14 Pct Recovery = 74% Analysis Date = 09/15/14 Pct Recovery = 74% Analysis Date = 09/05/14 Pct Recovery = 74% Analysis Date = 09/05/14 Pct Recovery = 74% Analysis Date = 08/25/14 Pct Recovery = 74% Analysis Date = 08/25/14 Pct Recovery = 74% Analysis Date = 08/14/14 Pct Recovery = 75% Analysis Date = 08/14/14 Pct Recovery = 75% Analysis Date = 08/03/14 Pct Recovery = 75% Analysis Date = 08/03/14 Pct Recovery = 75% Analysis Date = 07/23/14 Pct Recovery = 75% Analysis Date = 07/23/14 Pct Recovery = 75% Analysis Date = 07/12/14 Pct Recovery = 76% Analysis Date = 07/12/14 Pct Recovery = 76% Analysis Date = 07/02/14 Pct Recovery = 76% Analysis Date = 07/02/14 Pct Recovery = 76% Analysis Date = 06/21/14 Pct Recovery = 76% Analysis Date = 06/21/14 Pct Recovery = 76% Analysis Date = 06/10/14 Pct Recovery = 77% Analysis Date = 06/10/14 Pct Recovery = 77% Analysis Date = 05/30/14 Pct Recovery = 77% Analysis Date = 05/30/14 Pct Recovery = 77% Analysis Date = 05/19/14 Pct Recovery = 77% Analysis Date = 05/19/14 Pct Recovery = 77% Analysis Date = 05/08/14 Pct Recovery = 78% Analysis Date = 05/08/14 Pct Recovery = 78% Analysis Date = 04/28/14 Pct Recovery = 78% Analysis Date = 04/28/14 Pct Recovery = 78% Analysis Date = 04/17/14 Pct Recovery = 78% Analysis Date = 04/17/14 Pct Recovery = 78% Analysis Date = 04/06/14 Pct Recovery = 78% Analysis Date = 04/06/14 Pct Recovery = 78% Analysis Date = 03/26/14 Pct Recovery = 79% Analysis Date = 03/26/14 Pct Recovery = 79% Analysis Date = 03/15/14 Pct Recovery = 79% Analysis Date = 03/15/14 Pct Recovery = 79% Analysis Date = 03/04/14 Pct Recovery = 79% Analysis Date = 03/04/14 Pct Recovery = 79% Analysis Date = 02/22/14 Pct Recovery = 79% Analysis Date = 02/22/14 Pct Recovery = 79% Analysis Date = 02/11/14 Pct Recovery = 79% Analysis Date = 02/11/14 Pct Recovery = 79% Analysis Date = 01/31/14 Pct Recovery = 80% Analysis Date = 01/31/14 Pct Recovery = 80% Analysis Date = 01/20/14 Pct Recovery = 80% Analysis Date = 01/20/14 Pct Recovery = 80% Analysis Date = 01/09/14 Pct Recovery = 80% Analysis Date = 01/09/14 Pct Recovery = 80% Analysis Date = 12/30/13 Pct Recovery = 80% Analysis Date = 12/30/13 Pct Recovery = 80% Analysis Date = 12/19/13 Pct Recovery = 80% Analysis Date = 12/19/13 Pct Recovery = 80% Analysis Date = 12/08/13 Pct Recovery = 80% Analysis Date = 12/08/13 Pct Recovery = 80% Analysis Date = 11/27/13 Pct Recovery = 81% Analysis Date = 11/27/13 Pct Recovery = 81% Analysis Date = 11/16/13 Pct Recovery = 81% Analysis Date = 11/16/13 Pct Recovery = 81% Analysis Date = 11/05/13 Pct Recovery = 81% Analysis Date = 11/05/13 Pct Recovery = 81% Analysis Date = 10/26/13 Pct Recovery = 81% Analysis Date = 10/26/13 Pct Recovery = 81% Analysis Date = 10/15/13 Pct Recovery = 81% Analysis Date = 10/15/13 Pct Recovery = 81% Analysis Date = 10/04/13 Pct Recovery = 81% Analysis Date = 10/04/13 Pct Recovery = 81% Analysis Date = 09/23/13 Pct Recovery = 81% Analysis Date = 09/23/13 Pct Recovery = 81% Analysis Date = 09/12/13 Pct Recovery = 81% Analysis Date = 09/12/13 Pct Recovery = 81% Analysis Date = 09/01/13 Pct Recovery = 82% Analysis Date = 09/01/13 Pct Recovery = 82% Analysis Date = 08/22/13 Pct Recovery = 82% Analysis Date = 08/22/13 Pct Recovery = 82% Analysis Date = 08/11/13 Pct Recovery = 82% Analysis Date = 08/11/13 Pct Recovery = 82% Analysis Date = 07/31/13 Pct Recovery = 82% Analysis Date = 07/31/13 Pct Recovery = 82% Analysis Date = 07/20/13 Pct Recovery = 82% Analysis Date = 07/20/13 Pct Recovery = 82% Analysis Date = 07/09/13 Pct Recovery = 82% Analysis Date = 07/09/13 Pct Recovery = 82% Analysis Date = 06/29/13 Pct Recovery = 82% Analysis Date = 06/29/13 Pct Recovery = 82% Analysis Date = 06/18/13 Pct Recovery = 82% Analysis Date = 06/18/13 Pct Recovery = 82% Analysis Date = 06/07/13 Pct Recovery = 82% Analysis Date = 06/07/13 Pct Recovery = 82% Analysis Date = 05/27/13 Pct Recovery = 82% Analysis Date = 05/27/13 Pct Recovery = 82% Analysis Date = 05/16/13 Pct Recovery = 82% Analysis Date = 05/16/13 Pct Recovery = 82% Analysis Date = 05/05/13 Pct Recovery = 82% Analysis Date = 05/05/13 Pct Recovery = 82% Analysis Date = 04/25/13 Pct Recovery = 83% Analysis Date = 04/25/13 Pct Recovery = 83% Analysis Date = 04/14/13 Pct Recovery = 83% Analysis Date = 04/14/13 Pct Recovery = 83% Analysis Date = 04/03/13 Pct Recovery = 83% Analysis Date = 04/03/13 Pct Recovery = 83% Analysis Date = 03/23/13 Pct Recovery = 83% Analysis Date = 03/23/13 Pct Recovery = 83% Analysis Date = 03/12/13 Pct Recovery = 83% Analysis Date = 03/12/13 Pct Recovery = 83% Analysis Date = 03/01/13 Pct Recovery = 83% Analysis Date = 03/01/13 Pct Recovery = 83% Analysis Date = 02/19/13 Pct Recovery = 83% Analysis Date = 02/19/13 Pct Recovery = 83% Analysis Date = 02/08/13 Pct Recovery = 83% Analysis Date = 02/08/13 Pct Recovery = 83% Analysis Date = 01/28/13 Pct Recovery = 83% Analysis Date = 01/28/13 Pct Recovery = 83% Analysis Date = 01/17/13 Pct Recovery = 83% Analysis Date = 01/17/13 Pct Recovery = 83% Analysis Date = 01/06/13 Pct Recovery = 83% Analysis Date = 01/06/13 Pct Recovery = 83% Analysis Date = 12/26/12 Pct Recovery = 83% Analysis Date = 12/26/12 Pct Recovery = 83% Analysis Date = 12/16/12 Pct Recovery = 83% Analysis Date = 12/16/12 Pct Recovery = 83% Analysis Date = 12/05/12 Pct Recovery = 84% Analysis Date = 12/05/12 Pct Recovery = 84% Analysis Date = 11/24/12 Pct Recovery = 84% Analysis Date = 11/24/12 Pct Recovery = 84% Analysis Date = 11/13/12 Pct Recovery = 84% Analysis Date = 11/13/12 Pct Recovery = 84% Analysis Date = 11/02/12 Pct Recovery = 84% Analysis Date = 11/02/12 Pct Recovery = 84% Analysis Date = 10/23/12 Pct Recovery = 84% Analysis Date = 10/23/12 Pct Recovery = 84% Analysis Date = 10/12/12 Pct Recovery = 84% Analysis Date = 10/12/12 Pct Recovery = 84% Analysis Date = 10/01/12 Pct Recovery = 84% Analysis Date = 10/01/12 Pct Recovery = 84% Analysis Date = 09/20/12 Pct Recovery = 85% Analysis Date = 09/20/12 Pct Recovery = 85% Analysis Date = 09/09/12 Pct Recovery = 85% Analysis Date = 09/09/12 Pct Recovery = 85% Analysis Date = 08/29/12 Pct Recovery = 85% Analysis Date = 08/29/12 Pct Recovery = 85% Analysis Date = 08/19/12 Pct Recovery = 85% Analysis Date = 08/19/12 Pct Recovery = 85% Analysis Date = 08/08/12 Pct Recovery = 85% Analysis Date = 08/08/12 Pct Recovery = 85% Analysis Date = 07/28/12 Pct Recovery = 85% Analysis Date = 07/28/12 Pct Recovery = 85% Analysis Date = 07/17/12 Pct Recovery = 86% Analysis Date = 07/17/12 Pct Recovery = 86% Analysis Date = 07/06/12 Pct Recovery = 86% Analysis Date = 07/06/12 Pct Recovery = 86% Analysis Date = 06/25/12 Pct Recovery = 86% Analysis Date = 06/25/12 Pct Recovery = 86% Analysis Date = 06/15/12 Pct Recovery = 86% Analysis Date = 06/15/12 Pct Recovery = 86% Analysis Date = 06/04/12 Pct Recovery = 86% Analysis Date = 06/04/12 Pct Recovery = 86% Analysis Date = 05/24/12 Pct Recovery = 87% Analysis Date = 05/24/12 Pct Recovery = 87% Analysis Date = 05/13/12 Pct Recovery = 87% Analysis Date = 05/13/12 Pct Recovery = 87% Analysis Date = 05/02/12 Pct Recovery = 87% Analysis Date = 05/02/12 Pct Recovery = 87% Analysis Date = 04/22/12 Pct Recovery = 87% Analysis Date = 04/22/12 Pct Recovery = 87% Analysis Date = 04/11/12 Pct Recovery = 87% Analysis Date = 04/11/12 Pct Recovery = 87% Analysis Date = 03/31/12 Pct Recovery = 88% Analysis Date = 03/31/12 Pct Recovery = 88% Analysis Date = 03/20/12 Pct Recovery = 88% Analysis Date = 03/20/12 Pct Recovery = 88% Analysis Date = 03/09/12 Pct Recovery = 88% Analysis Date = 03/09/12 Pct Recovery = 88% Analysis Date = 02/27/12 Pct Recovery = 88% Analysis Date = 02/27/12 Pct Recovery = 88% Analysis Date = 02/17/12 Pct Recovery = 88% Analysis Date = 02/17/12 Pct Recovery = 88% Analysis Date = 02/06/12 Pct Recovery = 89% Analysis Date = 02/06/12 Pct Recovery = 89% Analysis Date = 01/26/12 Pct Recovery = 89% Analysis Date = 01/26/12 Pct Recovery = 89% Analysis Date = 01/15/12 Pct Recovery = 89% Analysis Date = 01/15/12 Pct Recovery = 89% Analysis Date = 01/04/12 Pct Recovery = 89% Analysis Date = 01/04/12 Pct Recovery = 89% Analysis Date = 12/24/11 Pct Recovery = 89% Analysis Date = 12/24/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 90% Analysis Date = 12/14/11 Pct Recovery = 90% Analysis Date = 12/03/11 Pct Recovery = 90% Analysis Date = 12/03/11 Pct Recovery = 90% Analysis Date = 11/22/11 Pct Recovery = 90% Analysis Date = 11/22/11 Pct Recovery = 90% Analysis Date = 11/11/11 Pct Recovery = 90% Analysis Date = 11/11/11 Pct Recovery = 90% Analysis Date = 10/31/11 Pct Recovery = 90% Analysis Date = 10/31/11 Pct Recovery = 90% Analysis Date = 10/20/11 Pct Recovery = 91% Analysis Date = 10/20/11 Pct Recovery = 91% Analysis Date = 10/10/11 Pct Recovery = 91% Analysis Date = 10/10/11 Pct Recovery = 91% Analysis Date = 09/29/11 Pct Recovery = 91% Analysis Date = 09/29/11 Pct Recovery = 91% Analysis Date = 09/18/11 Pct Recovery = 91% Analysis Date = 09/18/11 Pct Recovery = 91% Analysis Date = 09/07/11 Pct Recovery = 91% Analysis Date = 09/07/11 Pct Recovery = 91% Analysis Date = 08/27/11 Pct Recovery = 91% Analysis Date = 08/27/11 Pct Recovery = 91% Analysis Date = 08/17/11 Pct Recovery = 92% Analysis Date = 08/17/11 Pct Recovery = 92% Analysis Date = 08/06/11 Pct Recovery = 92% Analysis Date = 08/06/11 Pct Recovery = 92% Analysis Date = 07/26/11 Pct Recovery = 92% Analysis Date = 07/26/11 Pct Recovery = 92% Analysis Date = 07/15/11 Pct Recovery = 92% Analysis Date = 07/15/11 Pct Recovery = 92% Analysis Date = 07/04/11 Pct Recovery = 92% Analysis Date = 07/04/11 Pct Recovery = 92% Analysis Date = 06/23/11 Pct Recovery = 93% Analysis Date = 06/23/11 Pct Recovery = 93% Analysis Date = 06/13/11 Pct Recovery = 93% Analysis Date = 06/13/11 Pct Recovery = 93% Analysis Date = 06/02/11 Pct Recovery = 93% Analysis Date = 06/02/11 Pct Recovery = 93% Analysis Date = 05/22/11 Pct Recovery = 93% Analysis Date = 05/22/11 Pct Recovery = 93% Analysis Date = 05/11/11 Pct Recovery = 93% Analysis Date = 05/11/11 Pct Recovery = 93% Analysis Date = 04/30/11 Pct Recovery = 94% Analysis Date = 04/30/11 Pct Recovery = 94% Analysis Date = 04/19/11 Pct Recovery = 94% Analysis Date = 04/19/11 Pct Recovery = 94% Analysis Date = 04/09/11 Pct Recovery = 94% Analysis Date = 04/09/11 Pct Recovery = 94% Analysis Date = 03/29/11 Pct Recovery = 94% Analysis Date = 03/29/11 Pct Recovery = 94% Analysis Date = 03/18/11 Pct Recovery = 94% Analysis Date = 03/18/11 Pct Recovery = 94% Analysis Date = 03/07/11 Pct Recovery = 95% Analysis Date = 03/07/11 Pct Recovery = 95% Analysis Date = 02/24/11 Pct Recovery = 95% Analysis Date = 02/24/11 Pct Recovery = 95% Analysis Date = 02/14/11 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETRYN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 88 81% 18% 82% 14%
Total 88 81% 18% 82% 14%

Sample Statistics
PROMETRYN

Characteristic N % % Basis
Plotted 88 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 88 .  
False Negatives 0 0% 0 out of 88
Not Spiked 74 .  
False Positives 1 1% 1 out of 74

BQS OBSP Determination:
PROPANIL
METHOD: 2033 , TESTIDCODE: 82679GCM35
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 81% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 101% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 97% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 80% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 113% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 76% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 87% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 100% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 118% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 103% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 113% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 110% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 103% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 108% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 92% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 105% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 104% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 86% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 97% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 109% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 111% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 132% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 105% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 124% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 77% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 106% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 120% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 90% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 124% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 92% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 99% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 95% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 90% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 89% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 121% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 98% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 113% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 103% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 113% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 126% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 116% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 92% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 102% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 64% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 66% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 101% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 176% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 132% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 115% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 125% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 140% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 104% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 92% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 101% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 125% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 106% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 96% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 88% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 99% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 125% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 97% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 126% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 98% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 102% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 130% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 126% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 98% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 111% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 133% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 121% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 120% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 95% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 110% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 88% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 102% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 73% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 134% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 139% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 125% Analysis Date = 01/17/17 Pct Recovery = 103% Analysis Date = 01/07/17 Pct Recovery = 103% Analysis Date = 01/07/17 Pct Recovery = 103% Analysis Date = 12/27/16 Pct Recovery = 103% Analysis Date = 12/27/16 Pct Recovery = 103% Analysis Date = 12/16/16 Pct Recovery = 103% Analysis Date = 12/16/16 Pct Recovery = 103% Analysis Date = 12/05/16 Pct Recovery = 103% Analysis Date = 12/05/16 Pct Recovery = 103% Analysis Date = 11/24/16 Pct Recovery = 103% Analysis Date = 11/24/16 Pct Recovery = 103% Analysis Date = 11/13/16 Pct Recovery = 103% Analysis Date = 11/13/16 Pct Recovery = 103% Analysis Date = 11/03/16 Pct Recovery = 103% Analysis Date = 11/03/16 Pct Recovery = 103% Analysis Date = 10/23/16 Pct Recovery = 103% Analysis Date = 10/23/16 Pct Recovery = 103% Analysis Date = 10/12/16 Pct Recovery = 103% Analysis Date = 10/12/16 Pct Recovery = 103% Analysis Date = 10/01/16 Pct Recovery = 103% Analysis Date = 10/01/16 Pct Recovery = 103% Analysis Date = 09/20/16 Pct Recovery = 103% Analysis Date = 09/20/16 Pct Recovery = 103% Analysis Date = 09/09/16 Pct Recovery = 103% Analysis Date = 09/09/16 Pct Recovery = 103% Analysis Date = 08/29/16 Pct Recovery = 103% Analysis Date = 08/29/16 Pct Recovery = 103% Analysis Date = 08/19/16 Pct Recovery = 103% Analysis Date = 08/19/16 Pct Recovery = 103% Analysis Date = 08/08/16 Pct Recovery = 103% Analysis Date = 08/08/16 Pct Recovery = 103% Analysis Date = 07/28/16 Pct Recovery = 103% Analysis Date = 07/28/16 Pct Recovery = 103% Analysis Date = 07/17/16 Pct Recovery = 103% Analysis Date = 07/17/16 Pct Recovery = 103% Analysis Date = 07/06/16 Pct Recovery = 103% Analysis Date = 07/06/16 Pct Recovery = 103% Analysis Date = 06/25/16 Pct Recovery = 103% Analysis Date = 06/25/16 Pct Recovery = 103% Analysis Date = 06/14/16 Pct Recovery = 103% Analysis Date = 06/14/16 Pct Recovery = 103% Analysis Date = 06/04/16 Pct Recovery = 103% Analysis Date = 06/04/16 Pct Recovery = 103% Analysis Date = 05/24/16 Pct Recovery = 103% Analysis Date = 05/24/16 Pct Recovery = 103% Analysis Date = 05/13/16 Pct Recovery = 103% Analysis Date = 05/13/16 Pct Recovery = 103% Analysis Date = 05/02/16 Pct Recovery = 103% Analysis Date = 05/02/16 Pct Recovery = 103% Analysis Date = 04/21/16 Pct Recovery = 103% Analysis Date = 04/21/16 Pct Recovery = 103% Analysis Date = 04/10/16 Pct Recovery = 103% Analysis Date = 04/10/16 Pct Recovery = 103% Analysis Date = 03/30/16 Pct Recovery = 104% Analysis Date = 03/30/16 Pct Recovery = 104% Analysis Date = 03/20/16 Pct Recovery = 104% Analysis Date = 03/20/16 Pct Recovery = 104% Analysis Date = 03/09/16 Pct Recovery = 104% Analysis Date = 03/09/16 Pct Recovery = 104% Analysis Date = 02/27/16 Pct Recovery = 104% Analysis Date = 02/27/16 Pct Recovery = 104% Analysis Date = 02/16/16 Pct Recovery = 104% Analysis Date = 02/16/16 Pct Recovery = 104% Analysis Date = 02/05/16 Pct Recovery = 104% Analysis Date = 02/05/16 Pct Recovery = 104% Analysis Date = 01/25/16 Pct Recovery = 104% Analysis Date = 01/25/16 Pct Recovery = 104% Analysis Date = 01/14/16 Pct Recovery = 104% Analysis Date = 01/14/16 Pct Recovery = 104% Analysis Date = 01/04/16 Pct Recovery = 104% Analysis Date = 01/04/16 Pct Recovery = 104% Analysis Date = 12/24/15 Pct Recovery = 104% Analysis Date = 12/24/15 Pct Recovery = 104% Analysis Date = 12/13/15 Pct Recovery = 104% Analysis Date = 12/13/15 Pct Recovery = 104% Analysis Date = 12/02/15 Pct Recovery = 104% Analysis Date = 12/02/15 Pct Recovery = 104% Analysis Date = 11/21/15 Pct Recovery = 104% Analysis Date = 11/21/15 Pct Recovery = 104% Analysis Date = 11/10/15 Pct Recovery = 104% Analysis Date = 11/10/15 Pct Recovery = 104% Analysis Date = 10/30/15 Pct Recovery = 104% Analysis Date = 10/30/15 Pct Recovery = 104% Analysis Date = 10/20/15 Pct Recovery = 104% Analysis Date = 10/20/15 Pct Recovery = 104% Analysis Date = 10/09/15 Pct Recovery = 104% Analysis Date = 10/09/15 Pct Recovery = 104% Analysis Date = 09/28/15 Pct Recovery = 104% Analysis Date = 09/28/15 Pct Recovery = 104% Analysis Date = 09/17/15 Pct Recovery = 104% Analysis Date = 09/17/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 09/06/15 Pct Recovery = 104% Analysis Date = 08/26/15 Pct Recovery = 103% Analysis Date = 08/26/15 Pct Recovery = 103% Analysis Date = 08/15/15 Pct Recovery = 103% Analysis Date = 08/15/15 Pct Recovery = 103% Analysis Date = 08/05/15 Pct Recovery = 103% Analysis Date = 08/05/15 Pct Recovery = 103% Analysis Date = 07/25/15 Pct Recovery = 103% Analysis Date = 07/25/15 Pct Recovery = 103% Analysis Date = 07/14/15 Pct Recovery = 103% Analysis Date = 07/14/15 Pct Recovery = 103% Analysis Date = 07/03/15 Pct Recovery = 103% Analysis Date = 07/03/15 Pct Recovery = 103% Analysis Date = 06/22/15 Pct Recovery = 103% Analysis Date = 06/22/15 Pct Recovery = 103% Analysis Date = 06/11/15 Pct Recovery = 103% Analysis Date = 06/11/15 Pct Recovery = 103% Analysis Date = 05/31/15 Pct Recovery = 103% Analysis Date = 05/31/15 Pct Recovery = 103% Analysis Date = 05/21/15 Pct Recovery = 103% Analysis Date = 05/21/15 Pct Recovery = 103% Analysis Date = 05/10/15 Pct Recovery = 103% Analysis Date = 05/10/15 Pct Recovery = 103% Analysis Date = 04/29/15 Pct Recovery = 103% Analysis Date = 04/29/15 Pct Recovery = 103% Analysis Date = 04/18/15 Pct Recovery = 103% Analysis Date = 04/18/15 Pct Recovery = 103% Analysis Date = 04/07/15 Pct Recovery = 103% Analysis Date = 04/07/15 Pct Recovery = 103% Analysis Date = 03/27/15 Pct Recovery = 103% Analysis Date = 03/27/15 Pct Recovery = 103% Analysis Date = 03/16/15 Pct Recovery = 103% Analysis Date = 03/16/15 Pct Recovery = 103% Analysis Date = 03/06/15 Pct Recovery = 103% Analysis Date = 03/06/15 Pct Recovery = 103% Analysis Date = 02/23/15 Pct Recovery = 103% Analysis Date = 02/23/15 Pct Recovery = 103% Analysis Date = 02/12/15 Pct Recovery = 103% Analysis Date = 02/12/15 Pct Recovery = 103% Analysis Date = 02/01/15 Pct Recovery = 103% Analysis Date = 02/01/15 Pct Recovery = 103% Analysis Date = 01/21/15 Pct Recovery = 103% Analysis Date = 01/21/15 Pct Recovery = 103% Analysis Date = 01/10/15 Pct Recovery = 103% Analysis Date = 01/10/15 Pct Recovery = 103% Analysis Date = 12/31/14 Pct Recovery = 103% Analysis Date = 12/31/14 Pct Recovery = 103% Analysis Date = 12/20/14 Pct Recovery = 103% Analysis Date = 12/20/14 Pct Recovery = 103% Analysis Date = 12/09/14 Pct Recovery = 103% Analysis Date = 12/09/14 Pct Recovery = 103% Analysis Date = 11/28/14 Pct Recovery = 103% Analysis Date = 11/28/14 Pct Recovery = 103% Analysis Date = 11/17/14 Pct Recovery = 103% Analysis Date = 11/17/14 Pct Recovery = 103% Analysis Date = 11/06/14 Pct Recovery = 103% Analysis Date = 11/06/14 Pct Recovery = 103% Analysis Date = 10/26/14 Pct Recovery = 103% Analysis Date = 10/26/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/16/14 Pct Recovery = 103% Analysis Date = 10/05/14 Pct Recovery = 103% Analysis Date = 10/05/14 Pct Recovery = 103% Analysis Date = 09/24/14 Pct Recovery = 103% Analysis Date = 09/24/14 Pct Recovery = 103% Analysis Date = 09/13/14 Pct Recovery = 103% Analysis Date = 09/13/14 Pct Recovery = 103% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 09/02/14 Pct Recovery = 102% Analysis Date = 08/22/14 Pct Recovery = 102% Analysis Date = 08/22/14 Pct Recovery = 102% Analysis Date = 08/11/14 Pct Recovery = 102% Analysis Date = 08/11/14 Pct Recovery = 102% Analysis Date = 08/01/14 Pct Recovery = 102% Analysis Date = 08/01/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/21/14 Pct Recovery = 102% Analysis Date = 07/10/14 Pct Recovery = 102% Analysis Date = 07/10/14 Pct Recovery = 102% Analysis Date = 06/29/14 Pct Recovery = 102% Analysis Date = 06/29/14 Pct Recovery = 102% Analysis Date = 06/18/14 Pct Recovery = 102% Analysis Date = 06/18/14 Pct Recovery = 102% Analysis Date = 06/07/14 Pct Recovery = 101% Analysis Date = 06/07/14 Pct Recovery = 101% Analysis Date = 05/27/14 Pct Recovery = 101% Analysis Date = 05/27/14 Pct Recovery = 101% Analysis Date = 05/17/14 Pct Recovery = 101% Analysis Date = 05/17/14 Pct Recovery = 101% Analysis Date = 05/06/14 Pct Recovery = 101% Analysis Date = 05/06/14 Pct Recovery = 101% Analysis Date = 04/25/14 Pct Recovery = 100% Analysis Date = 04/25/14 Pct Recovery = 100% Analysis Date = 04/14/14 Pct Recovery = 100% Analysis Date = 04/14/14 Pct Recovery = 100% Analysis Date = 04/03/14 Pct Recovery = 100% Analysis Date = 04/03/14 Pct Recovery = 100% Analysis Date = 03/23/14 Pct Recovery = 100% Analysis Date = 03/23/14 Pct Recovery = 100% Analysis Date = 03/12/14 Pct Recovery = 100% Analysis Date = 03/12/14 Pct Recovery = 100% Analysis Date = 03/02/14 Pct Recovery = 99% Analysis Date = 03/02/14 Pct Recovery = 99% Analysis Date = 02/19/14 Pct Recovery = 99% Analysis Date = 02/19/14 Pct Recovery = 99% Analysis Date = 02/08/14 Pct Recovery = 99% Analysis Date = 02/08/14 Pct Recovery = 99% Analysis Date = 01/28/14 Pct Recovery = 99% Analysis Date = 01/28/14 Pct Recovery = 99% Analysis Date = 01/17/14 Pct Recovery = 99% Analysis Date = 01/17/14 Pct Recovery = 99% Analysis Date = 01/06/14 Pct Recovery = 99% Analysis Date = 01/06/14 Pct Recovery = 99% Analysis Date = 12/26/13 Pct Recovery = 99% Analysis Date = 12/26/13 Pct Recovery = 99% Analysis Date = 12/16/13 Pct Recovery = 99% Analysis Date = 12/16/13 Pct Recovery = 99% Analysis Date = 12/05/13 Pct Recovery = 99% Analysis Date = 12/05/13 Pct Recovery = 99% Analysis Date = 11/24/13 Pct Recovery = 99% Analysis Date = 11/24/13 Pct Recovery = 99% Analysis Date = 11/13/13 Pct Recovery = 99% Analysis Date = 11/13/13 Pct Recovery = 99% Analysis Date = 11/02/13 Pct Recovery = 99% Analysis Date = 11/02/13 Pct Recovery = 99% Analysis Date = 10/22/13 Pct Recovery = 98% Analysis Date = 10/22/13 Pct Recovery = 98% Analysis Date = 10/11/13 Pct Recovery = 98% Analysis Date = 10/11/13 Pct Recovery = 98% Analysis Date = 10/01/13 Pct Recovery = 98% Analysis Date = 10/01/13 Pct Recovery = 98% Analysis Date = 09/20/13 Pct Recovery = 98% Analysis Date = 09/20/13 Pct Recovery = 98% Analysis Date = 09/09/13 Pct Recovery = 98% Analysis Date = 09/09/13 Pct Recovery = 98% Analysis Date = 08/29/13 Pct Recovery = 98% Analysis Date = 08/29/13 Pct Recovery = 98% Analysis Date = 08/18/13 Pct Recovery = 99% Analysis Date = 08/18/13 Pct Recovery = 99% Analysis Date = 08/07/13 Pct Recovery = 99% Analysis Date = 08/07/13 Pct Recovery = 99% Analysis Date = 07/27/13 Pct Recovery = 99% Analysis Date = 07/27/13 Pct Recovery = 99% Analysis Date = 07/17/13 Pct Recovery = 99% Analysis Date = 07/17/13 Pct Recovery = 99% Analysis Date = 07/06/13 Pct Recovery = 99% Analysis Date = 07/06/13 Pct Recovery = 99% Analysis Date = 06/25/13 Pct Recovery = 99% Analysis Date = 06/25/13 Pct Recovery = 99% Analysis Date = 06/14/13 Pct Recovery = 99% Analysis Date = 06/14/13 Pct Recovery = 99% Analysis Date = 06/03/13 Pct Recovery = 99% Analysis Date = 06/03/13 Pct Recovery = 99% Analysis Date = 05/23/13 Pct Recovery = 99% Analysis Date = 05/23/13 Pct Recovery = 99% Analysis Date = 05/12/13 Pct Recovery = 100% Analysis Date = 05/12/13 Pct Recovery = 100% Analysis Date = 05/02/13 Pct Recovery = 100% Analysis Date = 05/02/13 Pct Recovery = 100% Analysis Date = 04/21/13 Pct Recovery = 100% Analysis Date = 04/21/13 Pct Recovery = 100% Analysis Date = 04/10/13 Pct Recovery = 100% Analysis Date = 04/10/13 Pct Recovery = 100% Analysis Date = 03/30/13 Pct Recovery = 101% Analysis Date = 03/30/13 Pct Recovery = 101% Analysis Date = 03/19/13 Pct Recovery = 101% Analysis Date = 03/19/13 Pct Recovery = 101% Analysis Date = 03/08/13 Pct Recovery = 101% Analysis Date = 03/08/13 Pct Recovery = 101% Analysis Date = 02/25/13 Pct Recovery = 101% Analysis Date = 02/25/13 Pct Recovery = 101% Analysis Date = 02/15/13 Pct Recovery = 102% Analysis Date = 02/15/13 Pct Recovery = 102% Analysis Date = 02/04/13 Pct Recovery = 102% Analysis Date = 02/04/13 Pct Recovery = 102% Analysis Date = 01/24/13 Pct Recovery = 102% Analysis Date = 01/24/13 Pct Recovery = 102% Analysis Date = 01/13/13 Pct Recovery = 102% Analysis Date = 01/13/13 Pct Recovery = 102% Analysis Date = 01/02/13 Pct Recovery = 103% Analysis Date = 01/02/13 Pct Recovery = 103% Analysis Date = 12/22/12 Pct Recovery = 103% Analysis Date = 12/22/12 Pct Recovery = 103% Analysis Date = 12/12/12 Pct Recovery = 103% Analysis Date = 12/12/12 Pct Recovery = 103% Analysis Date = 12/01/12 Pct Recovery = 104% Analysis Date = 12/01/12 Pct Recovery = 104% Analysis Date = 11/20/12 Pct Recovery = 104% Analysis Date = 11/20/12 Pct Recovery = 104% Analysis Date = 11/09/12 Pct Recovery = 104% Analysis Date = 11/09/12 Pct Recovery = 104% Analysis Date = 10/29/12 Pct Recovery = 105% Analysis Date = 10/29/12 Pct Recovery = 105% Analysis Date = 10/18/12 Pct Recovery = 105% Analysis Date = 10/18/12 Pct Recovery = 105% Analysis Date = 10/07/12 Pct Recovery = 105% Analysis Date = 10/07/12 Pct Recovery = 105% Analysis Date = 09/27/12 Pct Recovery = 106% Analysis Date = 09/27/12 Pct Recovery = 106% Analysis Date = 09/16/12 Pct Recovery = 106% Analysis Date = 09/16/12 Pct Recovery = 106% Analysis Date = 09/05/12 Pct Recovery = 106% Analysis Date = 09/05/12 Pct Recovery = 106% Analysis Date = 08/25/12 Pct Recovery = 106% Analysis Date = 08/25/12 Pct Recovery = 106% Analysis Date = 08/14/12 Pct Recovery = 106% Analysis Date = 08/14/12 Pct Recovery = 106% Analysis Date = 08/03/12 Pct Recovery = 107% Analysis Date = 08/03/12 Pct Recovery = 107% Analysis Date = 07/23/12 Pct Recovery = 107% Analysis Date = 07/23/12 Pct Recovery = 107% Analysis Date = 07/13/12 Pct Recovery = 107% Analysis Date = 07/13/12 Pct Recovery = 107% Analysis Date = 07/02/12 Pct Recovery = 107% Analysis Date = 07/02/12 Pct Recovery = 107% Analysis Date = 06/21/12 Pct Recovery = 107% Analysis Date = 06/21/12 Pct Recovery = 107% Analysis Date = 06/10/12 Pct Recovery = 108% Analysis Date = 06/10/12 Pct Recovery = 108% Analysis Date = 05/30/12 Pct Recovery = 108% Analysis Date = 05/30/12 Pct Recovery = 108% Analysis Date = 05/19/12 Pct Recovery = 108% Analysis Date = 05/19/12 Pct Recovery = 108% Analysis Date = 05/08/12 Pct Recovery = 108% Analysis Date = 05/08/12 Pct Recovery = 108% Analysis Date = 04/28/12 Pct Recovery = 108% Analysis Date = 04/28/12 Pct Recovery = 108% Analysis Date = 04/17/12 Pct Recovery = 108% Analysis Date = 04/17/12 Pct Recovery = 108% Analysis Date = 04/06/12 Pct Recovery = 109% Analysis Date = 04/06/12 Pct Recovery = 109% Analysis Date = 03/26/12 Pct Recovery = 109% Analysis Date = 03/26/12 Pct Recovery = 109% Analysis Date = 03/15/12 Pct Recovery = 109% Analysis Date = 03/15/12 Pct Recovery = 109% Analysis Date = 03/04/12 Pct Recovery = 109% Analysis Date = 03/04/12 Pct Recovery = 109% Analysis Date = 02/22/12 Pct Recovery = 109% Analysis Date = 02/22/12 Pct Recovery = 109% Analysis Date = 02/12/12 Pct Recovery = 110% Analysis Date = 02/12/12 Pct Recovery = 110% Analysis Date = 02/01/12 Pct Recovery = 110% Analysis Date = 02/01/12 Pct Recovery = 110% Analysis Date = 01/21/12 Pct Recovery = 110% Analysis Date = 01/21/12 Pct Recovery = 110% Analysis Date = 01/10/12 Pct Recovery = 110% Analysis Date = 01/10/12 Pct Recovery = 110% Analysis Date = 12/30/11 Pct Recovery = 110% Analysis Date = 12/30/11 Pct Recovery = 110% Analysis Date = 12/19/11 Pct Recovery = 110% Analysis Date = 12/19/11 Pct Recovery = 110% Analysis Date = 12/08/11 Pct Recovery = 111% Analysis Date = 12/08/11 Pct Recovery = 111% Analysis Date = 11/28/11 Pct Recovery = 111% Analysis Date = 11/28/11 Pct Recovery = 111% Analysis Date = 11/17/11 Pct Recovery = 111% Analysis Date = 11/17/11 Pct Recovery = 111% Analysis Date = 11/06/11 Pct Recovery = 111% Analysis Date = 11/06/11 Pct Recovery = 111% Analysis Date = 10/26/11 Pct Recovery = 111% Analysis Date = 10/26/11 Pct Recovery = 111% Analysis Date = 10/15/11 Pct Recovery = 111% Analysis Date = 10/15/11 Pct Recovery = 111% Analysis Date = 10/04/11 Pct Recovery = 112% Analysis Date = 10/04/11 Pct Recovery = 112% Analysis Date = 09/23/11 Pct Recovery = 112% Analysis Date = 09/23/11 Pct Recovery = 112% Analysis Date = 09/13/11 Pct Recovery = 112% Analysis Date = 09/13/11 Pct Recovery = 112% Analysis Date = 09/02/11 Pct Recovery = 112% Analysis Date = 09/02/11 Pct Recovery = 112% Analysis Date = 08/22/11 Pct Recovery = 112% Analysis Date = 08/22/11 Pct Recovery = 112% Analysis Date = 08/11/11 Pct Recovery = 112% Analysis Date = 08/11/11 Pct Recovery = 112% Analysis Date = 07/31/11 Pct Recovery = 113% Analysis Date = 07/31/11 Pct Recovery = 113% Analysis Date = 07/20/11 Pct Recovery = 113% Analysis Date = 07/20/11 Pct Recovery = 113% Analysis Date = 07/09/11 Pct Recovery = 113% Analysis Date = 07/09/11 Pct Recovery = 113% Analysis Date = 06/29/11 Pct Recovery = 113% Analysis Date = 06/29/11 Pct Recovery = 113% Analysis Date = 06/18/11 Pct Recovery = 113% Analysis Date = 06/18/11 Pct Recovery = 113% Analysis Date = 06/07/11 Pct Recovery = 113% Analysis Date = 06/07/11 Pct Recovery = 113% Analysis Date = 05/27/11 Pct Recovery = 113% Analysis Date = 05/27/11 Pct Recovery = 113% Analysis Date = 05/16/11 Pct Recovery = 113% Analysis Date = 05/16/11 Pct Recovery = 113% Analysis Date = 05/05/11 Pct Recovery = 114% Analysis Date = 05/05/11 Pct Recovery = 114% Analysis Date = 04/24/11 Pct Recovery = 114% Analysis Date = 04/24/11 Pct Recovery = 114% Analysis Date = 04/14/11 Pct Recovery = 114% Analysis Date = 04/14/11 Pct Recovery = 114% Analysis Date = 04/03/11 Pct Recovery = 114% Analysis Date = 04/03/11 Pct Recovery = 114% Analysis Date = 03/23/11 Pct Recovery = 114% Analysis Date = 03/23/11 Pct Recovery = 114% Analysis Date = 03/12/11 Pct Recovery = 114% Analysis Date = 03/12/11 Pct Recovery = 114% Analysis Date = 03/01/11 Pct Recovery = 114% Analysis Date = 03/01/11 Pct Recovery = 114% Analysis Date = 02/18/11 Pct Recovery = 114% Analysis Date = 02/18/11 Pct Recovery = 114% Analysis Date = 02/08/11 Pct Recovery = 114% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 105% 19% 103% 19%
Total 87 105% 19% 103% 19%

Sample Statistics
PROPANIL

Characteristic N % % Basis
Plotted 87 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 0 0% 0 out of 87
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

BQS OBSP Determination:
PROPARGITE
METHOD: 2033 , TESTIDCODE: 82685GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 141% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 101% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 146% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 87% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 59% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 185% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 127% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 56% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 52% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 126% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 94% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 108% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 89% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 67% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 59% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 56% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 123% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 157% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 148% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 61% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 66% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 87% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 55% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 150% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 163% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 44% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 42% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 44% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 75% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 69% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 33% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 63% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 152% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 38% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 57% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 88% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 69% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 81% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 36% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 34% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 32% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 33% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 80% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 131% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 90% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 57% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 98% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 62% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 82% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 104% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 76% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 85% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 100% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 89% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 35% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 52% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 50% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 52% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 35% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 80% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 86% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 108% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 83% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 77% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 95% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 55% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 37% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 37% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 43% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 35% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 75% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 77% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 82% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 100% Analysis Date = 09/20/16 Pct Recovery = 90% Analysis Date = 09/09/16 Pct Recovery = 89% Analysis Date = 09/09/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/20/16 Pct Recovery = 89% Analysis Date = 08/20/16 Pct Recovery = 89% Analysis Date = 08/10/16 Pct Recovery = 88% Analysis Date = 08/10/16 Pct Recovery = 88% Analysis Date = 07/30/16 Pct Recovery = 88% Analysis Date = 07/30/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 06/30/16 Pct Recovery = 87% Analysis Date = 06/30/16 Pct Recovery = 87% Analysis Date = 06/19/16 Pct Recovery = 86% Analysis Date = 06/19/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/20/16 Pct Recovery = 85% Analysis Date = 05/20/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 85% Analysis Date = 05/09/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 84% Analysis Date = 04/19/16 Pct Recovery = 84% Analysis Date = 04/09/16 Pct Recovery = 84% Analysis Date = 04/09/16 Pct Recovery = 84% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/28/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 02/07/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/28/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/07/16 Pct Recovery = 80% Analysis Date = 01/07/16 Pct Recovery = 80% Analysis Date = 12/28/15 Pct Recovery = 80% Analysis Date = 12/28/15 Pct Recovery = 80% Analysis Date = 12/18/15 Pct Recovery = 80% Analysis Date = 12/18/15 Pct Recovery = 80% Analysis Date = 12/08/15 Pct Recovery = 79% Analysis Date = 12/08/15 Pct Recovery = 79% Analysis Date = 11/27/15 Pct Recovery = 79% Analysis Date = 11/27/15 Pct Recovery = 79% Analysis Date = 11/17/15 Pct Recovery = 79% Analysis Date = 11/17/15 Pct Recovery = 79% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 11/07/15 Pct Recovery = 78% Analysis Date = 10/28/15 Pct Recovery = 78% Analysis Date = 10/28/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/17/15 Pct Recovery = 78% Analysis Date = 10/07/15 Pct Recovery = 77% Analysis Date = 10/07/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/06/15 Pct Recovery = 76% Analysis Date = 09/06/15 Pct Recovery = 76% Analysis Date = 08/27/15 Pct Recovery = 76% Analysis Date = 08/27/15 Pct Recovery = 76% Analysis Date = 08/17/15 Pct Recovery = 75% Analysis Date = 08/17/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 08/07/15 Pct Recovery = 75% Analysis Date = 07/27/15 Pct Recovery = 75% Analysis Date = 07/27/15 Pct Recovery = 75% Analysis Date = 07/17/15 Pct Recovery = 74% Analysis Date = 07/17/15 Pct Recovery = 74% Analysis Date = 07/07/15 Pct Recovery = 74% Analysis Date = 07/07/15 Pct Recovery = 74% Analysis Date = 06/27/15 Pct Recovery = 74% Analysis Date = 06/27/15 Pct Recovery = 74% Analysis Date = 06/16/15 Pct Recovery = 74% Analysis Date = 06/16/15 Pct Recovery = 74% Analysis Date = 06/06/15 Pct Recovery = 73% Analysis Date = 06/06/15 Pct Recovery = 73% Analysis Date = 05/27/15 Pct Recovery = 73% Analysis Date = 05/27/15 Pct Recovery = 73% Analysis Date = 05/17/15 Pct Recovery = 73% Analysis Date = 05/17/15 Pct Recovery = 73% Analysis Date = 05/06/15 Pct Recovery = 73% Analysis Date = 05/06/15 Pct Recovery = 73% Analysis Date = 04/26/15 Pct Recovery = 72% Analysis Date = 04/26/15 Pct Recovery = 72% Analysis Date = 04/16/15 Pct Recovery = 72% Analysis Date = 04/16/15 Pct Recovery = 72% Analysis Date = 04/06/15 Pct Recovery = 72% Analysis Date = 04/06/15 Pct Recovery = 72% Analysis Date = 03/26/15 Pct Recovery = 72% Analysis Date = 03/26/15 Pct Recovery = 72% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/16/15 Pct Recovery = 71% Analysis Date = 03/06/15 Pct Recovery = 71% Analysis Date = 03/06/15 Pct Recovery = 71% Analysis Date = 02/24/15 Pct Recovery = 71% Analysis Date = 02/24/15 Pct Recovery = 71% Analysis Date = 02/13/15 Pct Recovery = 71% Analysis Date = 02/13/15 Pct Recovery = 71% Analysis Date = 02/03/15 Pct Recovery = 71% Analysis Date = 02/03/15 Pct Recovery = 71% Analysis Date = 01/24/15 Pct Recovery = 70% Analysis Date = 01/24/15 Pct Recovery = 70% Analysis Date = 01/14/15 Pct Recovery = 70% Analysis Date = 01/14/15 Pct Recovery = 70% Analysis Date = 01/03/15 Pct Recovery = 70% Analysis Date = 01/03/15 Pct Recovery = 70% Analysis Date = 12/24/14 Pct Recovery = 70% Analysis Date = 12/24/14 Pct Recovery = 70% Analysis Date = 12/14/14 Pct Recovery = 69% Analysis Date = 12/14/14 Pct Recovery = 69% Analysis Date = 12/04/14 Pct Recovery = 69% Analysis Date = 12/04/14 Pct Recovery = 69% Analysis Date = 11/23/14 Pct Recovery = 69% Analysis Date = 11/23/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 69% Analysis Date = 11/13/14 Pct Recovery = 69% Analysis Date = 11/03/14 Pct Recovery = 68% Analysis Date = 11/03/14 Pct Recovery = 68% Analysis Date = 10/24/14 Pct Recovery = 68% Analysis Date = 10/24/14 Pct Recovery = 68% Analysis Date = 10/13/14 Pct Recovery = 68% Analysis Date = 10/13/14 Pct Recovery = 68% Analysis Date = 10/03/14 Pct Recovery = 68% Analysis Date = 10/03/14 Pct Recovery = 68% Analysis Date = 09/23/14 Pct Recovery = 67% Analysis Date = 09/23/14 Pct Recovery = 67% Analysis Date = 09/13/14 Pct Recovery = 67% Analysis Date = 09/13/14 Pct Recovery = 67% Analysis Date = 09/02/14 Pct Recovery = 67% Analysis Date = 09/02/14 Pct Recovery = 67% Analysis Date = 08/23/14 Pct Recovery = 67% Analysis Date = 08/23/14 Pct Recovery = 67% Analysis Date = 08/13/14 Pct Recovery = 67% Analysis Date = 08/13/14 Pct Recovery = 67% Analysis Date = 08/03/14 Pct Recovery = 67% Analysis Date = 08/03/14 Pct Recovery = 67% Analysis Date = 07/23/14 Pct Recovery = 67% Analysis Date = 07/23/14 Pct Recovery = 67% Analysis Date = 07/13/14 Pct Recovery = 67% Analysis Date = 07/13/14 Pct Recovery = 67% Analysis Date = 07/03/14 Pct Recovery = 67% Analysis Date = 07/03/14 Pct Recovery = 67% Analysis Date = 06/23/14 Pct Recovery = 67% Analysis Date = 06/23/14 Pct Recovery = 67% Analysis Date = 06/12/14 Pct Recovery = 67% Analysis Date = 06/12/14 Pct Recovery = 67% Analysis Date = 06/02/14 Pct Recovery = 67% Analysis Date = 06/02/14 Pct Recovery = 67% Analysis Date = 05/23/14 Pct Recovery = 67% Analysis Date = 05/23/14 Pct Recovery = 67% Analysis Date = 05/13/14 Pct Recovery = 67% Analysis Date = 05/13/14 Pct Recovery = 67% Analysis Date = 05/02/14 Pct Recovery = 68% Analysis Date = 05/02/14 Pct Recovery = 68% Analysis Date = 04/22/14 Pct Recovery = 68% Analysis Date = 04/22/14 Pct Recovery = 68% Analysis Date = 04/12/14 Pct Recovery = 69% Analysis Date = 04/12/14 Pct Recovery = 69% Analysis Date = 04/02/14 Pct Recovery = 69% Analysis Date = 04/02/14 Pct Recovery = 69% Analysis Date = 03/22/14 Pct Recovery = 70% Analysis Date = 03/22/14 Pct Recovery = 70% Analysis Date = 03/12/14 Pct Recovery = 70% Analysis Date = 03/12/14 Pct Recovery = 70% Analysis Date = 03/02/14 Pct Recovery = 70% Analysis Date = 03/02/14 Pct Recovery = 70% Analysis Date = 02/20/14 Pct Recovery = 71% Analysis Date = 02/20/14 Pct Recovery = 71% Analysis Date = 02/09/14 Pct Recovery = 71% Analysis Date = 02/09/14 Pct Recovery = 71% Analysis Date = 01/30/14 Pct Recovery = 72% Analysis Date = 01/30/14 Pct Recovery = 72% Analysis Date = 01/20/14 Pct Recovery = 72% Analysis Date = 01/20/14 Pct Recovery = 72% Analysis Date = 01/10/14 Pct Recovery = 73% Analysis Date = 01/10/14 Pct Recovery = 73% Analysis Date = 12/30/13 Pct Recovery = 74% Analysis Date = 12/30/13 Pct Recovery = 74% Analysis Date = 12/20/13 Pct Recovery = 75% Analysis Date = 12/20/13 Pct Recovery = 75% Analysis Date = 12/10/13 Pct Recovery = 76% Analysis Date = 12/10/13 Pct Recovery = 76% Analysis Date = 11/30/13 Pct Recovery = 78% Analysis Date = 11/30/13 Pct Recovery = 78% Analysis Date = 11/19/13 Pct Recovery = 79% Analysis Date = 11/19/13 Pct Recovery = 79% Analysis Date = 11/09/13 Pct Recovery = 80% Analysis Date = 11/09/13 Pct Recovery = 80% Analysis Date = 10/30/13 Pct Recovery = 81% Analysis Date = 10/30/13 Pct Recovery = 81% Analysis Date = 10/20/13 Pct Recovery = 82% Analysis Date = 10/20/13 Pct Recovery = 82% Analysis Date = 10/09/13 Pct Recovery = 83% Analysis Date = 10/09/13 Pct Recovery = 83% Analysis Date = 09/29/13 Pct Recovery = 84% Analysis Date = 09/29/13 Pct Recovery = 84% Analysis Date = 09/19/13 Pct Recovery = 85% Analysis Date = 09/19/13 Pct Recovery = 85% Analysis Date = 09/09/13 Pct Recovery = 86% Analysis Date = 09/09/13 Pct Recovery = 86% Analysis Date = 08/29/13 Pct Recovery = 87% Analysis Date = 08/29/13 Pct Recovery = 87% Analysis Date = 08/19/13 Pct Recovery = 88% Analysis Date = 08/19/13 Pct Recovery = 88% Analysis Date = 08/09/13 Pct Recovery = 90% Analysis Date = 08/09/13 Pct Recovery = 90% Analysis Date = 07/30/13 Pct Recovery = 91% Analysis Date = 07/30/13 Pct Recovery = 91% Analysis Date = 07/19/13 Pct Recovery = 92% Analysis Date = 07/19/13 Pct Recovery = 92% Analysis Date = 07/09/13 Pct Recovery = 92% Analysis Date = 07/09/13 Pct Recovery = 92% Analysis Date = 06/29/13 Pct Recovery = 93% Analysis Date = 06/29/13 Pct Recovery = 93% Analysis Date = 06/19/13 Pct Recovery = 94% Analysis Date = 06/19/13 Pct Recovery = 94% Analysis Date = 06/08/13 Pct Recovery = 95% Analysis Date = 06/08/13 Pct Recovery = 95% Analysis Date = 05/29/13 Pct Recovery = 96% Analysis Date = 05/29/13 Pct Recovery = 96% Analysis Date = 05/19/13 Pct Recovery = 97% Analysis Date = 05/19/13 Pct Recovery = 97% Analysis Date = 05/09/13 Pct Recovery = 97% Analysis Date = 05/09/13 Pct Recovery = 97% Analysis Date = 04/28/13 Pct Recovery = 98% Analysis Date = 04/28/13 Pct Recovery = 98% Analysis Date = 04/18/13 Pct Recovery = 99% Analysis Date = 04/18/13 Pct Recovery = 99% Analysis Date = 04/08/13 Pct Recovery = 100% Analysis Date = 04/08/13 Pct Recovery = 100% Analysis Date = 03/29/13 Pct Recovery = 101% Analysis Date = 03/29/13 Pct Recovery = 101% Analysis Date = 03/18/13 Pct Recovery = 102% Analysis Date = 03/18/13 Pct Recovery = 102% Analysis Date = 03/08/13 Pct Recovery = 102% Analysis Date = 03/08/13 Pct Recovery = 102% Analysis Date = 02/26/13 Pct Recovery = 102% Analysis Date = 02/26/13 Pct Recovery = 102% Analysis Date = 02/16/13 Pct Recovery = 102% Analysis Date = 02/16/13 Pct Recovery = 102% Analysis Date = 02/05/13 Pct Recovery = 102% Analysis Date = 02/05/13 Pct Recovery = 102% Analysis Date = 01/26/13 Pct Recovery = 101% Analysis Date = 01/26/13 Pct Recovery = 101% Analysis Date = 01/16/13 Pct Recovery = 101% Analysis Date = 01/16/13 Pct Recovery = 101% Analysis Date = 01/06/13 Pct Recovery = 101% Analysis Date = 01/06/13 Pct Recovery = 101% Analysis Date = 12/26/12 Pct Recovery = 100% Analysis Date = 12/26/12 Pct Recovery = 100% Analysis Date = 12/16/12 Pct Recovery = 100% Analysis Date = 12/16/12 Pct Recovery = 100% Analysis Date = 12/06/12 Pct Recovery = 100% Analysis Date = 12/06/12 Pct Recovery = 100% Analysis Date = 11/26/12 Pct Recovery = 99% Analysis Date = 11/26/12 Pct Recovery = 99% Analysis Date = 11/15/12 Pct Recovery = 99% Analysis Date = 11/15/12 Pct Recovery = 99% Analysis Date = 11/05/12 Pct Recovery = 99% Analysis Date = 11/05/12 Pct Recovery = 99% Analysis Date = 10/26/12 Pct Recovery = 98% Analysis Date = 10/26/12 Pct Recovery = 98% Analysis Date = 10/16/12 Pct Recovery = 98% Analysis Date = 10/16/12 Pct Recovery = 98% Analysis Date = 10/05/12 Pct Recovery = 98% Analysis Date = 10/05/12 Pct Recovery = 98% Analysis Date = 09/25/12 Pct Recovery = 97% Analysis Date = 09/25/12 Pct Recovery = 97% Analysis Date = 09/15/12 Pct Recovery = 97% Analysis Date = 09/15/12 Pct Recovery = 97% Analysis Date = 09/05/12 Pct Recovery = 96% Analysis Date = 09/05/12 Pct Recovery = 96% Analysis Date = 08/25/12 Pct Recovery = 96% Analysis Date = 08/25/12 Pct Recovery = 96% Analysis Date = 08/15/12 Pct Recovery = 96% Analysis Date = 08/15/12 Pct Recovery = 96% Analysis Date = 08/05/12 Pct Recovery = 95% Analysis Date = 08/05/12 Pct Recovery = 95% Analysis Date = 07/26/12 Pct Recovery = 95% Analysis Date = 07/26/12 Pct Recovery = 95% Analysis Date = 07/15/12 Pct Recovery = 95% Analysis Date = 07/15/12 Pct Recovery = 95% Analysis Date = 07/05/12 Pct Recovery = 94% Analysis Date = 07/05/12 Pct Recovery = 94% Analysis Date = 06/25/12 Pct Recovery = 94% Analysis Date = 06/25/12 Pct Recovery = 94% Analysis Date = 06/15/12 Pct Recovery = 94% Analysis Date = 06/15/12 Pct Recovery = 94% Analysis Date = 06/04/12 Pct Recovery = 93% Analysis Date = 06/04/12 Pct Recovery = 93% Analysis Date = 05/25/12 Pct Recovery = 92% Analysis Date = 05/25/12 Pct Recovery = 92% Analysis Date = 05/15/12 Pct Recovery = 92% Analysis Date = 05/15/12 Pct Recovery = 92% Analysis Date = 05/05/12 Pct Recovery = 91% Analysis Date = 05/05/12 Pct Recovery = 91% Analysis Date = 04/24/12 Pct Recovery = 91% Analysis Date = 04/24/12 Pct Recovery = 91% Analysis Date = 04/14/12 Pct Recovery = 90% Analysis Date = 04/14/12 Pct Recovery = 90% Analysis Date = 04/04/12 Pct Recovery = 89% Analysis Date = 04/04/12 Pct Recovery = 89% Analysis Date = 03/25/12 Pct Recovery = 89% Analysis Date = 03/25/12 Pct Recovery = 89% Analysis Date = 03/14/12 Pct Recovery = 88% Analysis Date = 03/14/12 Pct Recovery = 88% Analysis Date = 03/04/12 Pct Recovery = 88% Analysis Date = 03/04/12 Pct Recovery = 88% Analysis Date = 02/23/12 Pct Recovery = 87% Analysis Date = 02/23/12 Pct Recovery = 87% Analysis Date = 02/13/12 Pct Recovery = 86% Analysis Date = 02/13/12 Pct Recovery = 86% Analysis Date = 02/02/12 Pct Recovery = 86% Analysis Date = 02/02/12 Pct Recovery = 86% Analysis Date = 01/23/12 Pct Recovery = 85% Analysis Date = 01/23/12 Pct Recovery = 85% Analysis Date = 01/13/12 Pct Recovery = 85% Analysis Date = 01/13/12 Pct Recovery = 85% Analysis Date = 01/03/12 Pct Recovery = 84% Analysis Date = 01/03/12 Pct Recovery = 84% Analysis Date = 12/23/11 Pct Recovery = 83% Analysis Date = 12/23/11 Pct Recovery = 83% Analysis Date = 12/13/11 Pct Recovery = 83% Analysis Date = 12/13/11 Pct Recovery = 83% Analysis Date = 12/03/11 Pct Recovery = 82% Analysis Date = 12/03/11 Pct Recovery = 82% Analysis Date = 11/23/11 Pct Recovery = 82% Analysis Date = 11/23/11 Pct Recovery = 82% Analysis Date = 11/12/11 Pct Recovery = 81% Analysis Date = 11/12/11 Pct Recovery = 81% Analysis Date = 11/02/11 Pct Recovery = 80% Analysis Date = 11/02/11 Pct Recovery = 80% Analysis Date = 10/23/11 Pct Recovery = 79% Analysis Date = 10/23/11 Pct Recovery = 79% Analysis Date = 10/13/11 Pct Recovery = 79% Analysis Date = 10/13/11 Pct Recovery = 79% Analysis Date = 10/02/11 Pct Recovery = 78% Analysis Date = 10/02/11 Pct Recovery = 78% Analysis Date = 09/22/11 Pct Recovery = 77% Analysis Date = 09/22/11 Pct Recovery = 77% Analysis Date = 09/12/11 Pct Recovery = 76% Analysis Date = 09/12/11 Pct Recovery = 76% Analysis Date = 09/02/11 Pct Recovery = 76% Analysis Date = 09/02/11 Pct Recovery = 76% Analysis Date = 08/22/11 Pct Recovery = 75% Analysis Date = 08/22/11 Pct Recovery = 75% Analysis Date = 08/12/11 Pct Recovery = 74% Analysis Date = 08/12/11 Pct Recovery = 74% Analysis Date = 08/02/11 Pct Recovery = 73% Analysis Date = 08/02/11 Pct Recovery = 73% Analysis Date = 07/23/11 Pct Recovery = 73% Analysis Date = 07/23/11 Pct Recovery = 73% Analysis Date = 07/12/11 Pct Recovery = 72% Analysis Date = 07/12/11 Pct Recovery = 72% Analysis Date = 07/02/11 Pct Recovery = 71% Analysis Date = 07/02/11 Pct Recovery = 71% Analysis Date = 06/22/11 Pct Recovery = 70% Analysis Date = 06/22/11 Pct Recovery = 70% Analysis Date = 06/12/11 Pct Recovery = 69% Analysis Date = 06/12/11 Pct Recovery = 69% Analysis Date = 06/01/11 Pct Recovery = 69% Analysis Date = 06/01/11 Pct Recovery = 69% Analysis Date = 05/22/11 Pct Recovery = 68% Analysis Date = 05/22/11 Pct Recovery = 68% Analysis Date = 05/12/11 Pct Recovery = 67% Analysis Date = 05/12/11 Pct Recovery = 67% Analysis Date = 05/02/11 Pct Recovery = 66% Analysis Date = 05/02/11 Pct Recovery = 66% Analysis Date = 04/21/11 Pct Recovery = 65% Analysis Date = 04/21/11 Pct Recovery = 65% Analysis Date = 04/11/11 Pct Recovery = 65% Analysis Date = 04/11/11 Pct Recovery = 65% Analysis Date = 04/01/11 Pct Recovery = 64% Analysis Date = 04/01/11 Pct Recovery = 64% Analysis Date = 03/22/11 Pct Recovery = 63% Analysis Date = 03/22/11 Pct Recovery = 63% Analysis Date = 03/11/11 Pct Recovery = 62% Analysis Date = 03/11/11 Pct Recovery = 62% Analysis Date = 03/01/11 Pct Recovery = 61% Analysis Date = 03/01/11 Pct Recovery = 61% Analysis Date = 02/19/11 Pct Recovery = 61% Analysis Date = 02/19/11 Pct Recovery = 61% Analysis Date = 02/09/11 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPARGITE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 80% 34% 76% 28%
Total 89 80% 34% 76% 28%

Sample Statistics
PROPARGITE

Characteristic N % % Basis
Plotted 89 96% Spiked
Estimated Values 16 17% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 93 .  
False Negatives 3 3% 3 out of 93
Not Spiked 76 .  
False Positives 0 0% 0 out of 76

BQS OBSP Determination:
PROPYZAMIDE (PRONAMIDE)
METHOD: 2033 , TESTIDCODE: 82676GCM35
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 91% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 102% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 89% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 101% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 84% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 93% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 89% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 74% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 98% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 111% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 93% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 84% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 86% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 85% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 92% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 100% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 92% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 89% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 106% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 91% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 80% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 71% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 79% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 92% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 79% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 107% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 81% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 108% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 82% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 87% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 96% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 81% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 94% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 117% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 74% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 72% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 84% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 106% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 100% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 107% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 101% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 73% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 77% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 76% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 110% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 118% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 89% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 66% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 76% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 70% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 68% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 66% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 91% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 92% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 104% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 70% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 100% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 77% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 71% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 94% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 102% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 119% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 103% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 105% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 111% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 128% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 84% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 70% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 84% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 65% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 74% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 81% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 96% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 82% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 72% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 84% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 88% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 01/18/17 Pct Recovery = 74% Analysis Date = 01/07/17 Pct Recovery = 74% Analysis Date = 01/07/17 Pct Recovery = 74% Analysis Date = 12/27/16 Pct Recovery = 74% Analysis Date = 12/27/16 Pct Recovery = 74% Analysis Date = 12/16/16 Pct Recovery = 74% Analysis Date = 12/16/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 11/24/16 Pct Recovery = 74% Analysis Date = 11/24/16 Pct Recovery = 74% Analysis Date = 11/14/16 Pct Recovery = 74% Analysis Date = 11/14/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 10/23/16 Pct Recovery = 74% Analysis Date = 10/23/16 Pct Recovery = 74% Analysis Date = 10/12/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 75% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 10/01/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/08/16 Pct Recovery = 75% Analysis Date = 08/08/16 Pct Recovery = 75% Analysis Date = 07/28/16 Pct Recovery = 75% Analysis Date = 07/28/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/26/16 Pct Recovery = 75% Analysis Date = 06/15/16 Pct Recovery = 76% Analysis Date = 06/15/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 76% Analysis Date = 05/24/16 Pct Recovery = 76% Analysis Date = 05/24/16 Pct Recovery = 76% Analysis Date = 05/14/16 Pct Recovery = 76% Analysis Date = 05/14/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/11/16 Pct Recovery = 76% Analysis Date = 04/11/16 Pct Recovery = 76% Analysis Date = 03/31/16 Pct Recovery = 76% Analysis Date = 03/31/16 Pct Recovery = 76% Analysis Date = 03/20/16 Pct Recovery = 76% Analysis Date = 03/20/16 Pct Recovery = 76% Analysis Date = 03/10/16 Pct Recovery = 76% Analysis Date = 03/10/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/06/16 Pct Recovery = 77% Analysis Date = 02/06/16 Pct Recovery = 77% Analysis Date = 01/26/16 Pct Recovery = 77% Analysis Date = 01/26/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/15/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 01/05/16 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/25/15 Pct Recovery = 77% Analysis Date = 12/14/15 Pct Recovery = 77% Analysis Date = 12/14/15 Pct Recovery = 77% Analysis Date = 12/03/15 Pct Recovery = 77% Analysis Date = 12/03/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/22/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/12/15 Pct Recovery = 77% Analysis Date = 11/01/15 Pct Recovery = 77% Analysis Date = 11/01/15 Pct Recovery = 77% Analysis Date = 10/21/15 Pct Recovery = 77% Analysis Date = 10/21/15 Pct Recovery = 77% Analysis Date = 10/10/15 Pct Recovery = 78% Analysis Date = 10/10/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 78% Analysis Date = 09/18/15 Pct Recovery = 78% Analysis Date = 09/18/15 Pct Recovery = 78% Analysis Date = 09/08/15 Pct Recovery = 78% Analysis Date = 09/08/15 Pct Recovery = 78% Analysis Date = 08/28/15 Pct Recovery = 78% Analysis Date = 08/28/15 Pct Recovery = 78% Analysis Date = 08/17/15 Pct Recovery = 78% Analysis Date = 08/17/15 Pct Recovery = 78% Analysis Date = 08/06/15 Pct Recovery = 78% Analysis Date = 08/06/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/26/15 Pct Recovery = 78% Analysis Date = 07/15/15 Pct Recovery = 78% Analysis Date = 07/15/15 Pct Recovery = 78% Analysis Date = 07/05/15 Pct Recovery = 78% Analysis Date = 07/05/15 Pct Recovery = 78% Analysis Date = 06/24/15 Pct Recovery = 79% Analysis Date = 06/24/15 Pct Recovery = 79% Analysis Date = 06/13/15 Pct Recovery = 79% Analysis Date = 06/13/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 06/02/15 Pct Recovery = 79% Analysis Date = 05/22/15 Pct Recovery = 79% Analysis Date = 05/22/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/11/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 04/20/15 Pct Recovery = 79% Analysis Date = 04/20/15 Pct Recovery = 79% Analysis Date = 04/09/15 Pct Recovery = 79% Analysis Date = 04/09/15 Pct Recovery = 79% Analysis Date = 03/29/15 Pct Recovery = 80% Analysis Date = 03/29/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/08/15 Pct Recovery = 80% Analysis Date = 03/08/15 Pct Recovery = 80% Analysis Date = 02/25/15 Pct Recovery = 80% Analysis Date = 02/25/15 Pct Recovery = 80% Analysis Date = 02/14/15 Pct Recovery = 80% Analysis Date = 02/14/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 02/03/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/23/15 Pct Recovery = 80% Analysis Date = 01/12/15 Pct Recovery = 81% Analysis Date = 01/12/15 Pct Recovery = 81% Analysis Date = 01/02/15 Pct Recovery = 81% Analysis Date = 01/02/15 Pct Recovery = 81% Analysis Date = 12/22/14 Pct Recovery = 81% Analysis Date = 12/22/14 Pct Recovery = 81% Analysis Date = 12/11/14 Pct Recovery = 81% Analysis Date = 12/11/14 Pct Recovery = 81% Analysis Date = 11/30/14 Pct Recovery = 82% Analysis Date = 11/30/14 Pct Recovery = 82% Analysis Date = 11/19/14 Pct Recovery = 82% Analysis Date = 11/19/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 11/08/14 Pct Recovery = 82% Analysis Date = 10/29/14 Pct Recovery = 83% Analysis Date = 10/29/14 Pct Recovery = 83% Analysis Date = 10/18/14 Pct Recovery = 83% Analysis Date = 10/18/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 10/07/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/26/14 Pct Recovery = 83% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/15/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 84% Analysis Date = 09/05/14 Pct Recovery = 84% Analysis Date = 08/25/14 Pct Recovery = 84% Analysis Date = 08/25/14 Pct Recovery = 84% Analysis Date = 08/14/14 Pct Recovery = 84% Analysis Date = 08/14/14 Pct Recovery = 84% Analysis Date = 08/03/14 Pct Recovery = 85% Analysis Date = 08/03/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/23/14 Pct Recovery = 85% Analysis Date = 07/12/14 Pct Recovery = 85% Analysis Date = 07/12/14 Pct Recovery = 85% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 07/02/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/21/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 06/10/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/30/14 Pct Recovery = 86% Analysis Date = 05/19/14 Pct Recovery = 87% Analysis Date = 05/19/14 Pct Recovery = 87% Analysis Date = 05/08/14 Pct Recovery = 87% Analysis Date = 05/08/14 Pct Recovery = 87% Analysis Date = 04/28/14 Pct Recovery = 87% Analysis Date = 04/28/14 Pct Recovery = 87% Analysis Date = 04/17/14 Pct Recovery = 88% Analysis Date = 04/17/14 Pct Recovery = 88% Analysis Date = 04/06/14 Pct Recovery = 88% Analysis Date = 04/06/14 Pct Recovery = 88% Analysis Date = 03/26/14 Pct Recovery = 88% Analysis Date = 03/26/14 Pct Recovery = 88% Analysis Date = 03/15/14 Pct Recovery = 88% Analysis Date = 03/15/14 Pct Recovery = 88% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 03/04/14 Pct Recovery = 89% Analysis Date = 02/22/14 Pct Recovery = 89% Analysis Date = 02/22/14 Pct Recovery = 89% Analysis Date = 02/11/14 Pct Recovery = 89% Analysis Date = 02/11/14 Pct Recovery = 89% Analysis Date = 01/31/14 Pct Recovery = 89% Analysis Date = 01/31/14 Pct Recovery = 89% Analysis Date = 01/20/14 Pct Recovery = 90% Analysis Date = 01/20/14 Pct Recovery = 90% Analysis Date = 01/09/14 Pct Recovery = 90% Analysis Date = 01/09/14 Pct Recovery = 90% Analysis Date = 12/30/13 Pct Recovery = 90% Analysis Date = 12/30/13 Pct Recovery = 90% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 91% Analysis Date = 11/05/13 Pct Recovery = 92% Analysis Date = 11/05/13 Pct Recovery = 92% Analysis Date = 10/26/13 Pct Recovery = 92% Analysis Date = 10/26/13 Pct Recovery = 92% Analysis Date = 10/15/13 Pct Recovery = 92% Analysis Date = 10/15/13 Pct Recovery = 92% Analysis Date = 10/04/13 Pct Recovery = 92% Analysis Date = 10/04/13 Pct Recovery = 92% Analysis Date = 09/23/13 Pct Recovery = 92% Analysis Date = 09/23/13 Pct Recovery = 92% Analysis Date = 09/12/13 Pct Recovery = 92% Analysis Date = 09/12/13 Pct Recovery = 92% Analysis Date = 09/01/13 Pct Recovery = 93% Analysis Date = 09/01/13 Pct Recovery = 93% Analysis Date = 08/22/13 Pct Recovery = 93% Analysis Date = 08/22/13 Pct Recovery = 93% Analysis Date = 08/11/13 Pct Recovery = 93% Analysis Date = 08/11/13 Pct Recovery = 93% Analysis Date = 07/31/13 Pct Recovery = 93% Analysis Date = 07/31/13 Pct Recovery = 93% Analysis Date = 07/20/13 Pct Recovery = 93% Analysis Date = 07/20/13 Pct Recovery = 93% Analysis Date = 07/09/13 Pct Recovery = 93% Analysis Date = 07/09/13 Pct Recovery = 93% Analysis Date = 06/29/13 Pct Recovery = 93% Analysis Date = 06/29/13 Pct Recovery = 93% Analysis Date = 06/18/13 Pct Recovery = 93% Analysis Date = 06/18/13 Pct Recovery = 93% Analysis Date = 06/07/13 Pct Recovery = 94% Analysis Date = 06/07/13 Pct Recovery = 94% Analysis Date = 05/27/13 Pct Recovery = 94% Analysis Date = 05/27/13 Pct Recovery = 94% Analysis Date = 05/16/13 Pct Recovery = 94% Analysis Date = 05/16/13 Pct Recovery = 94% Analysis Date = 05/05/13 Pct Recovery = 94% Analysis Date = 05/05/13 Pct Recovery = 94% Analysis Date = 04/25/13 Pct Recovery = 94% Analysis Date = 04/25/13 Pct Recovery = 94% Analysis Date = 04/14/13 Pct Recovery = 94% Analysis Date = 04/14/13 Pct Recovery = 94% Analysis Date = 04/03/13 Pct Recovery = 94% Analysis Date = 04/03/13 Pct Recovery = 94% Analysis Date = 03/23/13 Pct Recovery = 94% Analysis Date = 03/23/13 Pct Recovery = 94% Analysis Date = 03/12/13 Pct Recovery = 94% Analysis Date = 03/12/13 Pct Recovery = 94% Analysis Date = 03/01/13 Pct Recovery = 94% Analysis Date = 03/01/13 Pct Recovery = 94% Analysis Date = 02/19/13 Pct Recovery = 94% Analysis Date = 02/19/13 Pct Recovery = 94% Analysis Date = 02/08/13 Pct Recovery = 94% Analysis Date = 02/08/13 Pct Recovery = 94% Analysis Date = 01/28/13 Pct Recovery = 94% Analysis Date = 01/28/13 Pct Recovery = 94% Analysis Date = 01/17/13 Pct Recovery = 94% Analysis Date = 01/17/13 Pct Recovery = 94% Analysis Date = 01/06/13 Pct Recovery = 94% Analysis Date = 01/06/13 Pct Recovery = 94% Analysis Date = 12/26/12 Pct Recovery = 94% Analysis Date = 12/26/12 Pct Recovery = 94% Analysis Date = 12/16/12 Pct Recovery = 93% Analysis Date = 12/16/12 Pct Recovery = 93% Analysis Date = 12/05/12 Pct Recovery = 93% Analysis Date = 12/05/12 Pct Recovery = 93% Analysis Date = 11/24/12 Pct Recovery = 93% Analysis Date = 11/24/12 Pct Recovery = 93% Analysis Date = 11/13/12 Pct Recovery = 93% Analysis Date = 11/13/12 Pct Recovery = 93% Analysis Date = 11/02/12 Pct Recovery = 93% Analysis Date = 11/02/12 Pct Recovery = 93% Analysis Date = 10/23/12 Pct Recovery = 93% Analysis Date = 10/23/12 Pct Recovery = 93% Analysis Date = 10/12/12 Pct Recovery = 93% Analysis Date = 10/12/12 Pct Recovery = 93% Analysis Date = 10/01/12 Pct Recovery = 93% Analysis Date = 10/01/12 Pct Recovery = 93% Analysis Date = 09/20/12 Pct Recovery = 93% Analysis Date = 09/20/12 Pct Recovery = 93% Analysis Date = 09/09/12 Pct Recovery = 93% Analysis Date = 09/09/12 Pct Recovery = 93% Analysis Date = 08/29/12 Pct Recovery = 93% Analysis Date = 08/29/12 Pct Recovery = 93% Analysis Date = 08/19/12 Pct Recovery = 93% Analysis Date = 08/19/12 Pct Recovery = 93% Analysis Date = 08/08/12 Pct Recovery = 93% Analysis Date = 08/08/12 Pct Recovery = 93% Analysis Date = 07/28/12 Pct Recovery = 93% Analysis Date = 07/28/12 Pct Recovery = 93% Analysis Date = 07/17/12 Pct Recovery = 92% Analysis Date = 07/17/12 Pct Recovery = 92% Analysis Date = 07/06/12 Pct Recovery = 92% Analysis Date = 07/06/12 Pct Recovery = 92% Analysis Date = 06/25/12 Pct Recovery = 92% Analysis Date = 06/25/12 Pct Recovery = 92% Analysis Date = 06/15/12 Pct Recovery = 92% Analysis Date = 06/15/12 Pct Recovery = 92% Analysis Date = 06/04/12 Pct Recovery = 92% Analysis Date = 06/04/12 Pct Recovery = 92% Analysis Date = 05/24/12 Pct Recovery = 92% Analysis Date = 05/24/12 Pct Recovery = 92% Analysis Date = 05/13/12 Pct Recovery = 92% Analysis Date = 05/13/12 Pct Recovery = 92% Analysis Date = 05/02/12 Pct Recovery = 92% Analysis Date = 05/02/12 Pct Recovery = 92% Analysis Date = 04/22/12 Pct Recovery = 92% Analysis Date = 04/22/12 Pct Recovery = 92% Analysis Date = 04/11/12 Pct Recovery = 92% Analysis Date = 04/11/12 Pct Recovery = 92% Analysis Date = 03/31/12 Pct Recovery = 92% Analysis Date = 03/31/12 Pct Recovery = 92% Analysis Date = 03/20/12 Pct Recovery = 92% Analysis Date = 03/20/12 Pct Recovery = 92% Analysis Date = 03/09/12 Pct Recovery = 92% Analysis Date = 03/09/12 Pct Recovery = 92% Analysis Date = 02/27/12 Pct Recovery = 92% Analysis Date = 02/27/12 Pct Recovery = 92% Analysis Date = 02/17/12 Pct Recovery = 92% Analysis Date = 02/17/12 Pct Recovery = 92% Analysis Date = 02/06/12 Pct Recovery = 92% Analysis Date = 02/06/12 Pct Recovery = 92% Analysis Date = 01/26/12 Pct Recovery = 92% Analysis Date = 01/26/12 Pct Recovery = 92% Analysis Date = 01/15/12 Pct Recovery = 92% Analysis Date = 01/15/12 Pct Recovery = 92% Analysis Date = 01/04/12 Pct Recovery = 92% Analysis Date = 01/04/12 Pct Recovery = 92% Analysis Date = 12/24/11 Pct Recovery = 92% Analysis Date = 12/24/11 Pct Recovery = 92% Analysis Date = 12/14/11 Pct Recovery = 92% Analysis Date = 12/14/11 Pct Recovery = 92% Analysis Date = 12/03/11 Pct Recovery = 92% Analysis Date = 12/03/11 Pct Recovery = 92% Analysis Date = 11/22/11 Pct Recovery = 92% Analysis Date = 11/22/11 Pct Recovery = 92% Analysis Date = 11/11/11 Pct Recovery = 92% Analysis Date = 11/11/11 Pct Recovery = 92% Analysis Date = 10/31/11 Pct Recovery = 92% Analysis Date = 10/31/11 Pct Recovery = 92% Analysis Date = 10/20/11 Pct Recovery = 92% Analysis Date = 10/20/11 Pct Recovery = 92% Analysis Date = 10/10/11 Pct Recovery = 92% Analysis Date = 10/10/11 Pct Recovery = 92% Analysis Date = 09/29/11 Pct Recovery = 92% Analysis Date = 09/29/11 Pct Recovery = 92% Analysis Date = 09/18/11 Pct Recovery = 92% Analysis Date = 09/18/11 Pct Recovery = 92% Analysis Date = 09/07/11 Pct Recovery = 92% Analysis Date = 09/07/11 Pct Recovery = 92% Analysis Date = 08/27/11 Pct Recovery = 92% Analysis Date = 08/27/11 Pct Recovery = 92% Analysis Date = 08/17/11 Pct Recovery = 92% Analysis Date = 08/17/11 Pct Recovery = 92% Analysis Date = 08/06/11 Pct Recovery = 92% Analysis Date = 08/06/11 Pct Recovery = 92% Analysis Date = 07/26/11 Pct Recovery = 92% Analysis Date = 07/26/11 Pct Recovery = 92% Analysis Date = 07/15/11 Pct Recovery = 92% Analysis Date = 07/15/11 Pct Recovery = 92% Analysis Date = 07/04/11 Pct Recovery = 92% Analysis Date = 07/04/11 Pct Recovery = 92% Analysis Date = 06/23/11 Pct Recovery = 92% Analysis Date = 06/23/11 Pct Recovery = 92% Analysis Date = 06/13/11 Pct Recovery = 92% Analysis Date = 06/13/11 Pct Recovery = 92% Analysis Date = 06/02/11 Pct Recovery = 92% Analysis Date = 06/02/11 Pct Recovery = 92% Analysis Date = 05/22/11 Pct Recovery = 92% Analysis Date = 05/22/11 Pct Recovery = 92% Analysis Date = 05/11/11 Pct Recovery = 92% Analysis Date = 05/11/11 Pct Recovery = 92% Analysis Date = 04/30/11 Pct Recovery = 92% Analysis Date = 04/30/11 Pct Recovery = 92% Analysis Date = 04/19/11 Pct Recovery = 92% Analysis Date = 04/19/11 Pct Recovery = 92% Analysis Date = 04/09/11 Pct Recovery = 92% Analysis Date = 04/09/11 Pct Recovery = 92% Analysis Date = 03/29/11 Pct Recovery = 92% Analysis Date = 03/29/11 Pct Recovery = 92% Analysis Date = 03/18/11 Pct Recovery = 92% Analysis Date = 03/18/11 Pct Recovery = 92% Analysis Date = 03/07/11 Pct Recovery = 92% Analysis Date = 03/07/11 Pct Recovery = 92% Analysis Date = 02/24/11 Pct Recovery = 92% Analysis Date = 02/24/11 Pct Recovery = 92% Analysis Date = 02/14/11 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPYZAMIDE (PRONAMIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 87% 15% 87% 15%
Total 94 87% 15% 87% 15%

Sample Statistics
PROPYZAMIDE (PRONAMIDE)

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
SIMAZINE
METHOD: 2033 , TESTIDCODE: 04035GCM35
Open Data Set

Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 96% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 93% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 94% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 103% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 84% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 103% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 108% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 105% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 93% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 90% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 100% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 74% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 104% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 82% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 84% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 86% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 78% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 71% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 106% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 94% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 76% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 81% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 93% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 98% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 91% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 82% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 87% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 64% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 113% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 92% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 95% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 89% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 87% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 71% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 67% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 111% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 96% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 84% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 79% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 70% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 85% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 117% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 90% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 68% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 98% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 72% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 94% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 100% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 95% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 86% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 103% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 97% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 106% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 121% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 119% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 76% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 89% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 101% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 65% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 89% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 82% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 104% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 87% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 86% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 118% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 85% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 85% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 81% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 91% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 108% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 95% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 96% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 93% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 118% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 100% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 101% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 93% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 92% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 113% Analysis Date = 01/18/17 Pct Recovery = 97% Analysis Date = 01/07/17 Pct Recovery = 97% Analysis Date = 01/07/17 Pct Recovery = 97% Analysis Date = 12/27/16 Pct Recovery = 97% Analysis Date = 12/27/16 Pct Recovery = 97% Analysis Date = 12/16/16 Pct Recovery = 97% Analysis Date = 12/16/16 Pct Recovery = 97% Analysis Date = 12/05/16 Pct Recovery = 97% Analysis Date = 12/05/16 Pct Recovery = 97% Analysis Date = 11/24/16 Pct Recovery = 97% Analysis Date = 11/24/16 Pct Recovery = 97% Analysis Date = 11/14/16 Pct Recovery = 97% Analysis Date = 11/14/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 11/03/16 Pct Recovery = 97% Analysis Date = 10/23/16 Pct Recovery = 96% Analysis Date = 10/23/16 Pct Recovery = 96% Analysis Date = 10/12/16 Pct Recovery = 96% Analysis Date = 10/12/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 08/30/16 Pct Recovery = 96% Analysis Date = 08/30/16 Pct Recovery = 96% Analysis Date = 08/19/16 Pct Recovery = 96% Analysis Date = 08/19/16 Pct Recovery = 96% Analysis Date = 08/08/16 Pct Recovery = 96% Analysis Date = 08/08/16 Pct Recovery = 96% Analysis Date = 07/28/16 Pct Recovery = 95% Analysis Date = 07/28/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/07/16 Pct Recovery = 95% Analysis Date = 07/07/16 Pct Recovery = 95% Analysis Date = 06/26/16 Pct Recovery = 95% Analysis Date = 06/26/16 Pct Recovery = 95% Analysis Date = 06/15/16 Pct Recovery = 95% Analysis Date = 06/15/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 05/24/16 Pct Recovery = 95% Analysis Date = 05/24/16 Pct Recovery = 95% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/03/16 Pct Recovery = 95% Analysis Date = 05/03/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 94% Analysis Date = 04/22/16 Pct Recovery = 94% Analysis Date = 04/11/16 Pct Recovery = 94% Analysis Date = 04/11/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/20/16 Pct Recovery = 94% Analysis Date = 03/20/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 03/10/16 Pct Recovery = 94% Analysis Date = 02/28/16 Pct Recovery = 94% Analysis Date = 02/28/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/06/16 Pct Recovery = 94% Analysis Date = 02/06/16 Pct Recovery = 94% Analysis Date = 01/26/16 Pct Recovery = 93% Analysis Date = 01/26/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/05/16 Pct Recovery = 93% Analysis Date = 01/05/16 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/25/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/14/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 12/03/15 Pct Recovery = 93% Analysis Date = 11/22/15 Pct Recovery = 93% Analysis Date = 11/22/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/12/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 11/01/15 Pct Recovery = 93% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/15/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 07/05/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 91% Analysis Date = 06/13/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 06/02/15 Pct Recovery = 91% Analysis Date = 05/22/15 Pct Recovery = 91% Analysis Date = 05/22/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/11/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 91% Analysis Date = 05/01/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/09/15 Pct Recovery = 90% Analysis Date = 04/09/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 90% Analysis Date = 03/29/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/18/15 Pct Recovery = 90% Analysis Date = 03/08/15 Pct Recovery = 90% Analysis Date = 03/08/15 Pct Recovery = 90% Analysis Date = 02/25/15 Pct Recovery = 90% Analysis Date = 02/25/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/14/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 02/03/15 Pct Recovery = 90% Analysis Date = 01/23/15 Pct Recovery = 90% Analysis Date = 01/23/15 Pct Recovery = 90% Analysis Date = 01/12/15 Pct Recovery = 90% Analysis Date = 01/12/15 Pct Recovery = 90% Analysis Date = 01/02/15 Pct Recovery = 90% Analysis Date = 01/02/15 Pct Recovery = 90% Analysis Date = 12/22/14 Pct Recovery = 90% Analysis Date = 12/22/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 11/30/14 Pct Recovery = 90% Analysis Date = 11/30/14 Pct Recovery = 90% Analysis Date = 11/19/14 Pct Recovery = 90% Analysis Date = 11/19/14 Pct Recovery = 90% Analysis Date = 11/08/14 Pct Recovery = 90% Analysis Date = 11/08/14 Pct Recovery = 90% Analysis Date = 10/29/14 Pct Recovery = 90% Analysis Date = 10/29/14 Pct Recovery = 90% Analysis Date = 10/18/14 Pct Recovery = 90% Analysis Date = 10/18/14 Pct Recovery = 90% Analysis Date = 10/07/14 Pct Recovery = 90% Analysis Date = 10/07/14 Pct Recovery = 90% Analysis Date = 09/26/14 Pct Recovery = 90% Analysis Date = 09/26/14 Pct Recovery = 90% Analysis Date = 09/15/14 Pct Recovery = 90% Analysis Date = 09/15/14 Pct Recovery = 90% Analysis Date = 09/05/14 Pct Recovery = 90% Analysis Date = 09/05/14 Pct Recovery = 90% Analysis Date = 08/25/14 Pct Recovery = 90% Analysis Date = 08/25/14 Pct Recovery = 90% Analysis Date = 08/14/14 Pct Recovery = 90% Analysis Date = 08/14/14 Pct Recovery = 90% Analysis Date = 08/03/14 Pct Recovery = 90% Analysis Date = 08/03/14 Pct Recovery = 90% Analysis Date = 07/23/14 Pct Recovery = 90% Analysis Date = 07/23/14 Pct Recovery = 90% Analysis Date = 07/12/14 Pct Recovery = 90% Analysis Date = 07/12/14 Pct Recovery = 90% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/21/14 Pct Recovery = 91% Analysis Date = 06/21/14 Pct Recovery = 91% Analysis Date = 06/10/14 Pct Recovery = 91% Analysis Date = 06/10/14 Pct Recovery = 91% Analysis Date = 05/30/14 Pct Recovery = 91% Analysis Date = 05/30/14 Pct Recovery = 91% Analysis Date = 05/19/14 Pct Recovery = 91% Analysis Date = 05/19/14 Pct Recovery = 91% Analysis Date = 05/08/14 Pct Recovery = 91% Analysis Date = 05/08/14 Pct Recovery = 91% Analysis Date = 04/28/14 Pct Recovery = 91% Analysis Date = 04/28/14 Pct Recovery = 91% Analysis Date = 04/17/14 Pct Recovery = 91% Analysis Date = 04/17/14 Pct Recovery = 91% Analysis Date = 04/06/14 Pct Recovery = 91% Analysis Date = 04/06/14 Pct Recovery = 91% Analysis Date = 03/26/14 Pct Recovery = 91% Analysis Date = 03/26/14 Pct Recovery = 91% Analysis Date = 03/15/14 Pct Recovery = 91% Analysis Date = 03/15/14 Pct Recovery = 91% Analysis Date = 03/04/14 Pct Recovery = 91% Analysis Date = 03/04/14 Pct Recovery = 91% Analysis Date = 02/22/14 Pct Recovery = 91% Analysis Date = 02/22/14 Pct Recovery = 91% Analysis Date = 02/11/14 Pct Recovery = 91% Analysis Date = 02/11/14 Pct Recovery = 91% Analysis Date = 01/31/14 Pct Recovery = 91% Analysis Date = 01/31/14 Pct Recovery = 91% Analysis Date = 01/20/14 Pct Recovery = 91% Analysis Date = 01/20/14 Pct Recovery = 91% Analysis Date = 01/09/14 Pct Recovery = 91% Analysis Date = 01/09/14 Pct Recovery = 91% Analysis Date = 12/30/13 Pct Recovery = 91% Analysis Date = 12/30/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 91% Analysis Date = 11/05/13 Pct Recovery = 91% Analysis Date = 11/05/13 Pct Recovery = 91% Analysis Date = 10/26/13 Pct Recovery = 91% Analysis Date = 10/26/13 Pct Recovery = 91% Analysis Date = 10/15/13 Pct Recovery = 91% Analysis Date = 10/15/13 Pct Recovery = 91% Analysis Date = 10/04/13 Pct Recovery = 91% Analysis Date = 10/04/13 Pct Recovery = 91% Analysis Date = 09/23/13 Pct Recovery = 91% Analysis Date = 09/23/13 Pct Recovery = 91% Analysis Date = 09/12/13 Pct Recovery = 91% Analysis Date = 09/12/13 Pct Recovery = 91% Analysis Date = 09/01/13 Pct Recovery = 91% Analysis Date = 09/01/13 Pct Recovery = 91% Analysis Date = 08/22/13 Pct Recovery = 91% Analysis Date = 08/22/13 Pct Recovery = 91% Analysis Date = 08/11/13 Pct Recovery = 91% Analysis Date = 08/11/13 Pct Recovery = 91% Analysis Date = 07/31/13 Pct Recovery = 91% Analysis Date = 07/31/13 Pct Recovery = 91% Analysis Date = 07/20/13 Pct Recovery = 91% Analysis Date = 07/20/13 Pct Recovery = 91% Analysis Date = 07/09/13 Pct Recovery = 91% Analysis Date = 07/09/13 Pct Recovery = 91% Analysis Date = 06/29/13 Pct Recovery = 91% Analysis Date = 06/29/13 Pct Recovery = 91% Analysis Date = 06/18/13 Pct Recovery = 91% Analysis Date = 06/18/13 Pct Recovery = 91% Analysis Date = 06/07/13 Pct Recovery = 91% Analysis Date = 06/07/13 Pct Recovery = 91% Analysis Date = 05/27/13 Pct Recovery = 91% Analysis Date = 05/27/13 Pct Recovery = 91% Analysis Date = 05/16/13 Pct Recovery = 91% Analysis Date = 05/16/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 05/05/13 Pct Recovery = 91% Analysis Date = 04/25/13 Pct Recovery = 91% Analysis Date = 04/25/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/14/13 Pct Recovery = 91% Analysis Date = 04/03/13 Pct Recovery = 91% Analysis Date = 04/03/13 Pct Recovery = 91% Analysis Date = 03/23/13 Pct Recovery = 91% Analysis Date = 03/23/13 Pct Recovery = 91% Analysis Date = 03/12/13 Pct Recovery = 91% Analysis Date = 03/12/13 Pct Recovery = 91% Analysis Date = 03/01/13 Pct Recovery = 91% Analysis Date = 03/01/13 Pct Recovery = 91% Analysis Date = 02/19/13 Pct Recovery = 91% Analysis Date = 02/19/13 Pct Recovery = 91% Analysis Date = 02/08/13 Pct Recovery = 90% Analysis Date = 02/08/13 Pct Recovery = 90% Analysis Date = 01/28/13 Pct Recovery = 90% Analysis Date = 01/28/13 Pct Recovery = 90% Analysis Date = 01/17/13 Pct Recovery = 90% Analysis Date = 01/17/13 Pct Recovery = 90% Analysis Date = 01/06/13 Pct Recovery = 90% Analysis Date = 01/06/13 Pct Recovery = 90% Analysis Date = 12/26/12 Pct Recovery = 90% Analysis Date = 12/26/12 Pct Recovery = 90% Analysis Date = 12/16/12 Pct Recovery = 90% Analysis Date = 12/16/12 Pct Recovery = 90% Analysis Date = 12/05/12 Pct Recovery = 90% Analysis Date = 12/05/12 Pct Recovery = 90% Analysis Date = 11/24/12 Pct Recovery = 90% Analysis Date = 11/24/12 Pct Recovery = 90% Analysis Date = 11/13/12 Pct Recovery = 90% Analysis Date = 11/13/12 Pct Recovery = 90% Analysis Date = 11/02/12 Pct Recovery = 90% Analysis Date = 11/02/12 Pct Recovery = 90% Analysis Date = 10/23/12 Pct Recovery = 90% Analysis Date = 10/23/12 Pct Recovery = 90% Analysis Date = 10/12/12 Pct Recovery = 90% Analysis Date = 10/12/12 Pct Recovery = 90% Analysis Date = 10/01/12 Pct Recovery = 90% Analysis Date = 10/01/12 Pct Recovery = 90% Analysis Date = 09/20/12 Pct Recovery = 90% Analysis Date = 09/20/12 Pct Recovery = 90% Analysis Date = 09/09/12 Pct Recovery = 90% Analysis Date = 09/09/12 Pct Recovery = 90% Analysis Date = 08/29/12 Pct Recovery = 90% Analysis Date = 08/29/12 Pct Recovery = 90% Analysis Date = 08/19/12 Pct Recovery = 90% Analysis Date = 08/19/12 Pct Recovery = 90% Analysis Date = 08/08/12 Pct Recovery = 90% Analysis Date = 08/08/12 Pct Recovery = 90% Analysis Date = 07/28/12 Pct Recovery = 90% Analysis Date = 07/28/12 Pct Recovery = 90% Analysis Date = 07/17/12 Pct Recovery = 90% Analysis Date = 07/17/12 Pct Recovery = 90% Analysis Date = 07/06/12 Pct Recovery = 90% Analysis Date = 07/06/12 Pct Recovery = 90% Analysis Date = 06/25/12 Pct Recovery = 90% Analysis Date = 06/25/12 Pct Recovery = 90% Analysis Date = 06/15/12 Pct Recovery = 90% Analysis Date = 06/15/12 Pct Recovery = 90% Analysis Date = 06/04/12 Pct Recovery = 90% Analysis Date = 06/04/12 Pct Recovery = 90% Analysis Date = 05/24/12 Pct Recovery = 90% Analysis Date = 05/24/12 Pct Recovery = 90% Analysis Date = 05/13/12 Pct Recovery = 90% Analysis Date = 05/13/12 Pct Recovery = 90% Analysis Date = 05/02/12 Pct Recovery = 90% Analysis Date = 05/02/12 Pct Recovery = 90% Analysis Date = 04/22/12 Pct Recovery = 90% Analysis Date = 04/22/12 Pct Recovery = 90% Analysis Date = 04/11/12 Pct Recovery = 90% Analysis Date = 04/11/12 Pct Recovery = 90% Analysis Date = 03/31/12 Pct Recovery = 90% Analysis Date = 03/31/12 Pct Recovery = 90% Analysis Date = 03/20/12 Pct Recovery = 90% Analysis Date = 03/20/12 Pct Recovery = 90% Analysis Date = 03/09/12 Pct Recovery = 90% Analysis Date = 03/09/12 Pct Recovery = 90% Analysis Date = 02/27/12 Pct Recovery = 90% Analysis Date = 02/27/12 Pct Recovery = 90% Analysis Date = 02/17/12 Pct Recovery = 90% Analysis Date = 02/17/12 Pct Recovery = 90% Analysis Date = 02/06/12 Pct Recovery = 90% Analysis Date = 02/06/12 Pct Recovery = 90% Analysis Date = 01/26/12 Pct Recovery = 90% Analysis Date = 01/26/12 Pct Recovery = 90% Analysis Date = 01/15/12 Pct Recovery = 90% Analysis Date = 01/15/12 Pct Recovery = 90% Analysis Date = 01/04/12 Pct Recovery = 90% Analysis Date = 01/04/12 Pct Recovery = 90% Analysis Date = 12/24/11 Pct Recovery = 90% Analysis Date = 12/24/11 Pct Recovery = 90% Analysis Date = 12/14/11 Pct Recovery = 90% Analysis Date = 12/14/11 Pct Recovery = 90% Analysis Date = 12/03/11 Pct Recovery = 90% Analysis Date = 12/03/11 Pct Recovery = 90% Analysis Date = 11/22/11 Pct Recovery = 90% Analysis Date = 11/22/11 Pct Recovery = 90% Analysis Date = 11/11/11 Pct Recovery = 90% Analysis Date = 11/11/11 Pct Recovery = 90% Analysis Date = 10/31/11 Pct Recovery = 90% Analysis Date = 10/31/11 Pct Recovery = 90% Analysis Date = 10/20/11 Pct Recovery = 90% Analysis Date = 10/20/11 Pct Recovery = 90% Analysis Date = 10/10/11 Pct Recovery = 90% Analysis Date = 10/10/11 Pct Recovery = 90% Analysis Date = 09/29/11 Pct Recovery = 90% Analysis Date = 09/29/11 Pct Recovery = 90% Analysis Date = 09/18/11 Pct Recovery = 90% Analysis Date = 09/18/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 08/27/11 Pct Recovery = 90% Analysis Date = 08/27/11 Pct Recovery = 90% Analysis Date = 08/17/11 Pct Recovery = 90% Analysis Date = 08/17/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 91% Analysis Date = 07/26/11 Pct Recovery = 91% Analysis Date = 07/15/11 Pct Recovery = 91% Analysis Date = 07/15/11 Pct Recovery = 91% Analysis Date = 07/04/11 Pct Recovery = 91% Analysis Date = 07/04/11 Pct Recovery = 91% Analysis Date = 06/23/11 Pct Recovery = 91% Analysis Date = 06/23/11 Pct Recovery = 91% Analysis Date = 06/13/11 Pct Recovery = 91% Analysis Date = 06/13/11 Pct Recovery = 91% Analysis Date = 06/02/11 Pct Recovery = 91% Analysis Date = 06/02/11 Pct Recovery = 91% Analysis Date = 05/22/11 Pct Recovery = 91% Analysis Date = 05/22/11 Pct Recovery = 91% Analysis Date = 05/11/11 Pct Recovery = 91% Analysis Date = 05/11/11 Pct Recovery = 91% Analysis Date = 04/30/11 Pct Recovery = 91% Analysis Date = 04/30/11 Pct Recovery = 91% Analysis Date = 04/19/11 Pct Recovery = 91% Analysis Date = 04/19/11 Pct Recovery = 91% Analysis Date = 04/09/11 Pct Recovery = 91% Analysis Date = 04/09/11 Pct Recovery = 91% Analysis Date = 03/29/11 Pct Recovery = 91% Analysis Date = 03/29/11 Pct Recovery = 91% Analysis Date = 03/18/11 Pct Recovery = 91% Analysis Date = 03/18/11 Pct Recovery = 91% Analysis Date = 03/07/11 Pct Recovery = 91% Analysis Date = 03/07/11 Pct Recovery = 91% Analysis Date = 02/24/11 Pct Recovery = 91% Analysis Date = 02/24/11 Pct Recovery = 91% Analysis Date = 02/14/11 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SIMAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 91% 13% 92% 13%
Total 94 91% 13% 92% 13%

Sample Statistics
SIMAZINE

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 1 1% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
TEBUCONAZOLE
METHOD: 2033 , TESTIDCODE: 62852GCM14
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 59% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 53% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 61% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 54% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 49% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 56% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 101% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 54% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 62% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 67% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 53% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 72% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 54% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 65% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 81% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 54% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 59% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 47% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 58% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 51% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 57% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 108% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 78% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 44% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 54% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 64% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 56% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 51% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 57% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 52% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 50% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 78% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 93% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 74% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 64% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 66% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 65% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 55% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 52% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 48% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 66% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 90% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 54% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 69% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 60% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 66% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 96% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 70% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 78% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 85% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 58% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 48% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 52% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 53% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 62% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 48% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 44% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 107% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 78% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 64% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 104% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 71% Analysis Date = 12/19/16 Pct Recovery = 59% Analysis Date = 12/09/16 Pct Recovery = 59% Analysis Date = 12/09/16 Pct Recovery = 59% Analysis Date = 11/28/16 Pct Recovery = 60% Analysis Date = 11/28/16 Pct Recovery = 60% Analysis Date = 11/18/16 Pct Recovery = 60% Analysis Date = 11/18/16 Pct Recovery = 60% Analysis Date = 11/07/16 Pct Recovery = 60% Analysis Date = 11/07/16 Pct Recovery = 60% Analysis Date = 10/28/16 Pct Recovery = 61% Analysis Date = 10/28/16 Pct Recovery = 61% Analysis Date = 10/17/16 Pct Recovery = 61% Analysis Date = 10/17/16 Pct Recovery = 61% Analysis Date = 10/06/16 Pct Recovery = 61% Analysis Date = 10/06/16 Pct Recovery = 61% Analysis Date = 09/26/16 Pct Recovery = 62% Analysis Date = 09/26/16 Pct Recovery = 62% Analysis Date = 09/15/16 Pct Recovery = 62% Analysis Date = 09/15/16 Pct Recovery = 62% Analysis Date = 09/05/16 Pct Recovery = 62% Analysis Date = 09/05/16 Pct Recovery = 62% Analysis Date = 08/25/16 Pct Recovery = 63% Analysis Date = 08/25/16 Pct Recovery = 63% Analysis Date = 08/14/16 Pct Recovery = 63% Analysis Date = 08/14/16 Pct Recovery = 63% Analysis Date = 08/04/16 Pct Recovery = 63% Analysis Date = 08/04/16 Pct Recovery = 63% Analysis Date = 07/24/16 Pct Recovery = 63% Analysis Date = 07/24/16 Pct Recovery = 63% Analysis Date = 07/14/16 Pct Recovery = 64% Analysis Date = 07/14/16 Pct Recovery = 64% Analysis Date = 07/03/16 Pct Recovery = 64% Analysis Date = 07/03/16 Pct Recovery = 64% Analysis Date = 06/23/16 Pct Recovery = 64% Analysis Date = 06/23/16 Pct Recovery = 64% Analysis Date = 06/12/16 Pct Recovery = 65% Analysis Date = 06/12/16 Pct Recovery = 65% Analysis Date = 06/01/16 Pct Recovery = 65% Analysis Date = 06/01/16 Pct Recovery = 65% Analysis Date = 05/22/16 Pct Recovery = 65% Analysis Date = 05/22/16 Pct Recovery = 65% Analysis Date = 05/11/16 Pct Recovery = 66% Analysis Date = 05/11/16 Pct Recovery = 66% Analysis Date = 05/01/16 Pct Recovery = 66% Analysis Date = 05/01/16 Pct Recovery = 66% Analysis Date = 04/20/16 Pct Recovery = 66% Analysis Date = 04/20/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 03/30/16 Pct Recovery = 67% Analysis Date = 03/30/16 Pct Recovery = 67% Analysis Date = 03/19/16 Pct Recovery = 67% Analysis Date = 03/19/16 Pct Recovery = 67% Analysis Date = 03/09/16 Pct Recovery = 67% Analysis Date = 03/09/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/06/16 Pct Recovery = 68% Analysis Date = 02/06/16 Pct Recovery = 68% Analysis Date = 01/26/16 Pct Recovery = 68% Analysis Date = 01/26/16 Pct Recovery = 68% Analysis Date = 01/16/16 Pct Recovery = 68% Analysis Date = 01/16/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 01/05/16 Pct Recovery = 68% Analysis Date = 12/26/15 Pct Recovery = 68% Analysis Date = 12/26/15 Pct Recovery = 68% Analysis Date = 12/15/15 Pct Recovery = 68% Analysis Date = 12/15/15 Pct Recovery = 68% Analysis Date = 12/04/15 Pct Recovery = 69% Analysis Date = 12/04/15 Pct Recovery = 69% Analysis Date = 11/24/15 Pct Recovery = 69% Analysis Date = 11/24/15 Pct Recovery = 69% Analysis Date = 11/13/15 Pct Recovery = 69% Analysis Date = 11/13/15 Pct Recovery = 69% Analysis Date = 11/03/15 Pct Recovery = 69% Analysis Date = 11/03/15 Pct Recovery = 69% Analysis Date = 10/23/15 Pct Recovery = 69% Analysis Date = 10/23/15 Pct Recovery = 69% Analysis Date = 10/13/15 Pct Recovery = 69% Analysis Date = 10/13/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 10/02/15 Pct Recovery = 69% Analysis Date = 09/21/15 Pct Recovery = 69% Analysis Date = 09/21/15 Pct Recovery = 69% Analysis Date = 09/11/15 Pct Recovery = 70% Analysis Date = 09/11/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/10/15 Pct Recovery = 70% Analysis Date = 08/10/15 Pct Recovery = 70% Analysis Date = 07/30/15 Pct Recovery = 70% Analysis Date = 07/30/15 Pct Recovery = 70% Analysis Date = 07/20/15 Pct Recovery = 70% Analysis Date = 07/20/15 Pct Recovery = 70% Analysis Date = 07/09/15 Pct Recovery = 70% Analysis Date = 07/09/15 Pct Recovery = 70% Analysis Date = 06/29/15 Pct Recovery = 70% Analysis Date = 06/29/15 Pct Recovery = 70% Analysis Date = 06/18/15 Pct Recovery = 70% Analysis Date = 06/18/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 06/07/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 70% Analysis Date = 05/28/15 Pct Recovery = 70% Analysis Date = 05/17/15 Pct Recovery = 70% Analysis Date = 05/17/15 Pct Recovery = 70% Analysis Date = 05/07/15 Pct Recovery = 70% Analysis Date = 05/07/15 Pct Recovery = 70% Analysis Date = 04/26/15 Pct Recovery = 70% Analysis Date = 04/26/15 Pct Recovery = 70% Analysis Date = 04/16/15 Pct Recovery = 70% Analysis Date = 04/16/15 Pct Recovery = 70% Analysis Date = 04/05/15 Pct Recovery = 70% Analysis Date = 04/05/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/25/15 Pct Recovery = 70% Analysis Date = 03/15/15 Pct Recovery = 70% Analysis Date = 03/15/15 Pct Recovery = 70% Analysis Date = 03/04/15 Pct Recovery = 70% Analysis Date = 03/04/15 Pct Recovery = 70% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/11/15 Pct Recovery = 69% Analysis Date = 02/11/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/31/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/21/15 Pct Recovery = 69% Analysis Date = 01/10/15 Pct Recovery = 68% Analysis Date = 01/10/15 Pct Recovery = 68% Analysis Date = 12/31/14 Pct Recovery = 68% Analysis Date = 12/31/14 Pct Recovery = 68% Analysis Date = 12/20/14 Pct Recovery = 68% Analysis Date = 12/20/14 Pct Recovery = 68% Analysis Date = 12/10/14 Pct Recovery = 68% Analysis Date = 12/10/14 Pct Recovery = 68% Analysis Date = 11/29/14 Pct Recovery = 68% Analysis Date = 11/29/14 Pct Recovery = 68% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/18/14 Pct Recovery = 67% Analysis Date = 11/08/14 Pct Recovery = 67% Analysis Date = 11/08/14 Pct Recovery = 67% Analysis Date = 10/28/14 Pct Recovery = 67% Analysis Date = 10/28/14 Pct Recovery = 67% Analysis Date = 10/18/14 Pct Recovery = 67% Analysis Date = 10/18/14 Pct Recovery = 67% Analysis Date = 10/07/14 Pct Recovery = 66% Analysis Date = 10/07/14 Pct Recovery = 66% Analysis Date = 09/26/14 Pct Recovery = 66% Analysis Date = 09/26/14 Pct Recovery = 66% Analysis Date = 09/16/14 Pct Recovery = 65% Analysis Date = 09/16/14 Pct Recovery = 65% Analysis Date = 09/05/14 Pct Recovery = 65% Analysis Date = 09/05/14 Pct Recovery = 65% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/15/14 Pct Recovery = 64% Analysis Date = 08/15/14 Pct Recovery = 64% Analysis Date = 08/05/14 Pct Recovery = 63% Analysis Date = 08/05/14 Pct Recovery = 63% Analysis Date = 07/25/14 Pct Recovery = 63% Analysis Date = 07/25/14 Pct Recovery = 63% Analysis Date = 07/14/14 Pct Recovery = 62% Analysis Date = 07/14/14 Pct Recovery = 62% Analysis Date = 07/04/14 Pct Recovery = 62% Analysis Date = 07/04/14 Pct Recovery = 62% Analysis Date = 06/23/14 Pct Recovery = 62% Analysis Date = 06/23/14 Pct Recovery = 62% Analysis Date = 06/13/14 Pct Recovery = 61% Analysis Date = 06/13/14 Pct Recovery = 61% Analysis Date = 06/02/14 Pct Recovery = 61% Analysis Date = 06/02/14 Pct Recovery = 61% Analysis Date = 05/22/14 Pct Recovery = 61% Analysis Date = 05/22/14 Pct Recovery = 61% Analysis Date = 05/12/14 Pct Recovery = 61% Analysis Date = 05/12/14 Pct Recovery = 61% Analysis Date = 05/01/14 Pct Recovery = 61% Analysis Date = 05/01/14 Pct Recovery = 61% Analysis Date = 04/21/14 Pct Recovery = 61% Analysis Date = 04/21/14 Pct Recovery = 61% Analysis Date = 04/10/14 Pct Recovery = 61% Analysis Date = 04/10/14 Pct Recovery = 61% Analysis Date = 03/31/14 Pct Recovery = 61% Analysis Date = 03/31/14 Pct Recovery = 61% Analysis Date = 03/20/14 Pct Recovery = 61% Analysis Date = 03/20/14 Pct Recovery = 61% Analysis Date = 03/09/14 Pct Recovery = 61% Analysis Date = 03/09/14 Pct Recovery = 61% Analysis Date = 02/27/14 Pct Recovery = 61% Analysis Date = 02/27/14 Pct Recovery = 61% Analysis Date = 02/16/14 Pct Recovery = 61% Analysis Date = 02/16/14 Pct Recovery = 61% Analysis Date = 02/06/14 Pct Recovery = 61% Analysis Date = 02/06/14 Pct Recovery = 61% Analysis Date = 01/26/14 Pct Recovery = 61% Analysis Date = 01/26/14 Pct Recovery = 61% Analysis Date = 01/15/14 Pct Recovery = 62% Analysis Date = 01/15/14 Pct Recovery = 62% Analysis Date = 01/05/14 Pct Recovery = 62% Analysis Date = 01/05/14 Pct Recovery = 62% Analysis Date = 12/25/13 Pct Recovery = 62% Analysis Date = 12/25/13 Pct Recovery = 62% Analysis Date = 12/15/13 Pct Recovery = 62% Analysis Date = 12/15/13 Pct Recovery = 62% Analysis Date = 12/04/13 Pct Recovery = 62% Analysis Date = 12/04/13 Pct Recovery = 62% Analysis Date = 11/23/13 Pct Recovery = 63% Analysis Date = 11/23/13 Pct Recovery = 63% Analysis Date = 11/13/13 Pct Recovery = 63% Analysis Date = 11/13/13 Pct Recovery = 63% Analysis Date = 11/02/13 Pct Recovery = 63% Analysis Date = 11/02/13 Pct Recovery = 63% Analysis Date = 10/23/13 Pct Recovery = 63% Analysis Date = 10/23/13 Pct Recovery = 63% Analysis Date = 10/12/13 Pct Recovery = 63% Analysis Date = 10/12/13 Pct Recovery = 63% Analysis Date = 10/02/13 Pct Recovery = 64% Analysis Date = 10/02/13 Pct Recovery = 64% Analysis Date = 09/21/13 Pct Recovery = 64% Analysis Date = 09/21/13 Pct Recovery = 64% Analysis Date = 09/10/13 Pct Recovery = 64% Analysis Date = 09/10/13 Pct Recovery = 64% Analysis Date = 08/31/13 Pct Recovery = 64% Analysis Date = 08/31/13 Pct Recovery = 64% Analysis Date = 08/20/13 Pct Recovery = 64% Analysis Date = 08/20/13 Pct Recovery = 64% Analysis Date = 08/10/13 Pct Recovery = 64% Analysis Date = 08/10/13 Pct Recovery = 64% Analysis Date = 07/30/13 Pct Recovery = 64% Analysis Date = 07/30/13 Pct Recovery = 64% Analysis Date = 07/19/13 Pct Recovery = 64% Analysis Date = 07/19/13 Pct Recovery = 64% Analysis Date = 07/09/13 Pct Recovery = 64% Analysis Date = 07/09/13 Pct Recovery = 64% Analysis Date = 06/28/13 Pct Recovery = 64% Analysis Date = 06/28/13 Pct Recovery = 64% Analysis Date = 06/18/13 Pct Recovery = 64% Analysis Date = 06/18/13 Pct Recovery = 64% Analysis Date = 06/07/13 Pct Recovery = 65% Analysis Date = 06/07/13 Pct Recovery = 65% Analysis Date = 05/28/13 Pct Recovery = 65% Analysis Date = 05/28/13 Pct Recovery = 65% Analysis Date = 05/17/13 Pct Recovery = 65% Analysis Date = 05/17/13 Pct Recovery = 65% Analysis Date = 05/06/13 Pct Recovery = 65% Analysis Date = 05/06/13 Pct Recovery = 65% Analysis Date = 04/26/13 Pct Recovery = 65% Analysis Date = 04/26/13 Pct Recovery = 65% Analysis Date = 04/15/13 Pct Recovery = 65% Analysis Date = 04/15/13 Pct Recovery = 65% Analysis Date = 04/05/13 Pct Recovery = 66% Analysis Date = 04/05/13 Pct Recovery = 66% Analysis Date = 03/25/13 Pct Recovery = 66% Analysis Date = 03/25/13 Pct Recovery = 66% Analysis Date = 03/14/13 Pct Recovery = 66% Analysis Date = 03/14/13 Pct Recovery = 66% Analysis Date = 03/04/13 Pct Recovery = 66% Analysis Date = 03/04/13 Pct Recovery = 66% Analysis Date = 02/21/13 Pct Recovery = 66% Analysis Date = 02/21/13 Pct Recovery = 66% Analysis Date = 02/11/13 Pct Recovery = 66% Analysis Date = 02/11/13 Pct Recovery = 66% Analysis Date = 01/31/13 Pct Recovery = 66% Analysis Date = 01/31/13 Pct Recovery = 66% Analysis Date = 01/21/13 Pct Recovery = 66% Analysis Date = 01/21/13 Pct Recovery = 66% Analysis Date = 01/10/13 Pct Recovery = 67% Analysis Date = 01/10/13 Pct Recovery = 67% Analysis Date = 12/30/12 Pct Recovery = 67% Analysis Date = 12/30/12 Pct Recovery = 67% Analysis Date = 12/20/12 Pct Recovery = 67% Analysis Date = 12/20/12 Pct Recovery = 67% Analysis Date = 12/09/12 Pct Recovery = 67% Analysis Date = 12/09/12 Pct Recovery = 67% Analysis Date = 11/29/12 Pct Recovery = 67% Analysis Date = 11/29/12 Pct Recovery = 67% Analysis Date = 11/18/12 Pct Recovery = 67% Analysis Date = 11/18/12 Pct Recovery = 67% Analysis Date = 11/07/12 Pct Recovery = 67% Analysis Date = 11/07/12 Pct Recovery = 67% Analysis Date = 10/28/12 Pct Recovery = 67% Analysis Date = 10/28/12 Pct Recovery = 67% Analysis Date = 10/17/12 Pct Recovery = 67% Analysis Date = 10/17/12 Pct Recovery = 67% Analysis Date = 10/07/12 Pct Recovery = 67% Analysis Date = 10/07/12 Pct Recovery = 67% Analysis Date = 09/26/12 Pct Recovery = 67% Analysis Date = 09/26/12 Pct Recovery = 67% Analysis Date = 09/16/12 Pct Recovery = 67% Analysis Date = 09/16/12 Pct Recovery = 67% Analysis Date = 09/05/12 Pct Recovery = 67% Analysis Date = 09/05/12 Pct Recovery = 67% Analysis Date = 08/25/12 Pct Recovery = 67% Analysis Date = 08/25/12 Pct Recovery = 67% Analysis Date = 08/15/12 Pct Recovery = 67% Analysis Date = 08/15/12 Pct Recovery = 67% Analysis Date = 08/04/12 Pct Recovery = 67% Analysis Date = 08/04/12 Pct Recovery = 67% Analysis Date = 07/25/12 Pct Recovery = 67% Analysis Date = 07/25/12 Pct Recovery = 67% Analysis Date = 07/14/12 Pct Recovery = 67% Analysis Date = 07/14/12 Pct Recovery = 67% Analysis Date = 07/03/12 Pct Recovery = 67% Analysis Date = 07/03/12 Pct Recovery = 67% Analysis Date = 06/23/12 Pct Recovery = 67% Analysis Date = 06/23/12 Pct Recovery = 67% Analysis Date = 06/12/12 Pct Recovery = 67% Analysis Date = 06/12/12 Pct Recovery = 67% Analysis Date = 06/02/12 Pct Recovery = 67% Analysis Date = 06/02/12 Pct Recovery = 67% Analysis Date = 05/22/12 Pct Recovery = 67% Analysis Date = 05/22/12 Pct Recovery = 67% Analysis Date = 05/11/12 Pct Recovery = 67% Analysis Date = 05/11/12 Pct Recovery = 67% Analysis Date = 05/01/12 Pct Recovery = 67% Analysis Date = 05/01/12 Pct Recovery = 67% Analysis Date = 04/20/12 Pct Recovery = 67% Analysis Date = 04/20/12 Pct Recovery = 67% Analysis Date = 04/10/12 Pct Recovery = 67% Analysis Date = 04/10/12 Pct Recovery = 67% Analysis Date = 03/30/12 Pct Recovery = 67% Analysis Date = 03/30/12 Pct Recovery = 67% Analysis Date = 03/20/12 Pct Recovery = 67% Analysis Date = 03/20/12 Pct Recovery = 67% Analysis Date = 03/09/12 Pct Recovery = 67% Analysis Date = 03/09/12 Pct Recovery = 67% Analysis Date = 02/27/12 Pct Recovery = 67% Analysis Date = 02/27/12 Pct Recovery = 67% Analysis Date = 02/17/12 Pct Recovery = 67% Analysis Date = 02/17/12 Pct Recovery = 67% Analysis Date = 02/06/12 Pct Recovery = 67% Analysis Date = 02/06/12 Pct Recovery = 67% Analysis Date = 01/27/12 Pct Recovery = 67% Analysis Date = 01/27/12 Pct Recovery = 67% Analysis Date = 01/16/12 Pct Recovery = 67% Analysis Date = 01/16/12 Pct Recovery = 67% Analysis Date = 01/05/12 Pct Recovery = 67% Analysis Date = 01/05/12 Pct Recovery = 67% Analysis Date = 12/26/11 Pct Recovery = 67% Analysis Date = 12/26/11 Pct Recovery = 67% Analysis Date = 12/15/11 Pct Recovery = 67% Analysis Date = 12/15/11 Pct Recovery = 67% Analysis Date = 12/05/11 Pct Recovery = 67% Analysis Date = 12/05/11 Pct Recovery = 67% Analysis Date = 11/24/11 Pct Recovery = 67% Analysis Date = 11/24/11 Pct Recovery = 67% Analysis Date = 11/14/11 Pct Recovery = 67% Analysis Date = 11/14/11 Pct Recovery = 67% Analysis Date = 11/03/11 Pct Recovery = 67% Analysis Date = 11/03/11 Pct Recovery = 67% Analysis Date = 10/23/11 Pct Recovery = 67% Analysis Date = 10/23/11 Pct Recovery = 67% Analysis Date = 10/13/11 Pct Recovery = 67% Analysis Date = 10/13/11 Pct Recovery = 67% Analysis Date = 10/02/11 Pct Recovery = 67% Analysis Date = 10/02/11 Pct Recovery = 67% Analysis Date = 09/22/11 Pct Recovery = 67% Analysis Date = 09/22/11 Pct Recovery = 67% Analysis Date = 09/11/11 Pct Recovery = 67% Analysis Date = 09/11/11 Pct Recovery = 67% Analysis Date = 08/31/11 Pct Recovery = 67% Analysis Date = 08/31/11 Pct Recovery = 67% Analysis Date = 08/21/11 Pct Recovery = 67% Analysis Date = 08/21/11 Pct Recovery = 67% Analysis Date = 08/10/11 Pct Recovery = 67% Analysis Date = 08/10/11 Pct Recovery = 67% Analysis Date = 07/31/11 Pct Recovery = 67% Analysis Date = 07/31/11 Pct Recovery = 67% Analysis Date = 07/20/11 Pct Recovery = 67% Analysis Date = 07/20/11 Pct Recovery = 67% Analysis Date = 07/10/11 Pct Recovery = 67% Analysis Date = 07/10/11 Pct Recovery = 67% Analysis Date = 06/29/11 Pct Recovery = 67% Analysis Date = 06/29/11 Pct Recovery = 67% Analysis Date = 06/18/11 Pct Recovery = 67% Analysis Date = 06/18/11 Pct Recovery = 67% Analysis Date = 06/08/11 Pct Recovery = 67% Analysis Date = 06/08/11 Pct Recovery = 67% Analysis Date = 05/28/11 Pct Recovery = 67% Analysis Date = 05/28/11 Pct Recovery = 67% Analysis Date = 05/18/11 Pct Recovery = 67% Analysis Date = 05/18/11 Pct Recovery = 67% Analysis Date = 05/07/11 Pct Recovery = 67% Analysis Date = 05/07/11 Pct Recovery = 67% Analysis Date = 04/26/11 Pct Recovery = 67% Analysis Date = 04/26/11 Pct Recovery = 67% Analysis Date = 04/16/11 Pct Recovery = 67% Analysis Date = 04/16/11 Pct Recovery = 67% Analysis Date = 04/05/11 Pct Recovery = 67% Analysis Date = 04/05/11 Pct Recovery = 67% Analysis Date = 03/26/11 Pct Recovery = 67% Analysis Date = 03/26/11 Pct Recovery = 67% Analysis Date = 03/15/11 Pct Recovery = 67% Analysis Date = 03/15/11 Pct Recovery = 67% Analysis Date = 03/05/11 Pct Recovery = 67% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 66% 15% 64% 13%
Total 73 66% 15% 64% 13%

Sample Statistics
TEBUCONAZOLE

Characteristic N % % Basis
Plotted 73 100% Spiked
Estimated Values 4 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 0 0% 0 out of 73
Not Spiked 96 .  
False Positives 0 0% 0 out of 96

BQS OBSP Determination:
TEBUTHIURON
METHOD: 2033 , TESTIDCODE: 82670GCM35
Open Data Set

Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 244% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 205% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 229% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 211% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 127% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 110% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 90% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 109% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 151% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 141% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 158% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 142% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 71% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 123% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 83% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 121% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 94% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 112% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 110% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 116% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 129% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 136% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 140% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 144% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 104% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 72% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 123% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 126% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 172% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 113% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 70% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 101% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 173% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 60% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 125% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 95% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 78% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 169% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 126% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 161% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 105% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 110% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 123% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 67% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 120% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 196% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 120% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 163% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 132% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 185% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 114% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 109% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 99% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 153% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 177% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 171% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 188% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 164% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 168% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 153% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 128% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 141% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 167% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 129% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 127% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 107% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 150% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 205% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 114% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 101% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 153% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 174% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 106% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 150% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 120% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 106% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 152% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 65% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 96% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 114% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 121% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 121% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 142% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 131% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 124% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 105% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 143% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 107% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 127% Analysis Date = 01/17/17 Pct Recovery = 124% Analysis Date = 01/07/17 Pct Recovery = 124% Analysis Date = 01/07/17 Pct Recovery = 124% Analysis Date = 12/27/16 Pct Recovery = 124% Analysis Date = 12/27/16 Pct Recovery = 124% Analysis Date = 12/16/16 Pct Recovery = 124% Analysis Date = 12/16/16 Pct Recovery = 124% Analysis Date = 12/05/16 Pct Recovery = 123% Analysis Date = 12/05/16 Pct Recovery = 123% Analysis Date = 11/24/16 Pct Recovery = 123% Analysis Date = 11/24/16 Pct Recovery = 123% Analysis Date = 11/13/16 Pct Recovery = 123% Analysis Date = 11/13/16 Pct Recovery = 123% Analysis Date = 11/03/16 Pct Recovery = 122% Analysis Date = 11/03/16 Pct Recovery = 122% Analysis Date = 10/23/16 Pct Recovery = 122% Analysis Date = 10/23/16 Pct Recovery = 122% Analysis Date = 10/12/16 Pct Recovery = 122% Analysis Date = 10/12/16 Pct Recovery = 122% Analysis Date = 10/01/16 Pct Recovery = 122% Analysis Date = 10/01/16 Pct Recovery = 122% Analysis Date = 09/20/16 Pct Recovery = 121% Analysis Date = 09/20/16 Pct Recovery = 121% Analysis Date = 09/09/16 Pct Recovery = 121% Analysis Date = 09/09/16 Pct Recovery = 121% Analysis Date = 08/29/16 Pct Recovery = 121% Analysis Date = 08/29/16 Pct Recovery = 121% Analysis Date = 08/19/16 Pct Recovery = 121% Analysis Date = 08/19/16 Pct Recovery = 121% Analysis Date = 08/08/16 Pct Recovery = 120% Analysis Date = 08/08/16 Pct Recovery = 120% Analysis Date = 07/28/16 Pct Recovery = 120% Analysis Date = 07/28/16 Pct Recovery = 120% Analysis Date = 07/17/16 Pct Recovery = 120% Analysis Date = 07/17/16 Pct Recovery = 120% Analysis Date = 07/06/16 Pct Recovery = 120% Analysis Date = 07/06/16 Pct Recovery = 120% Analysis Date = 06/25/16 Pct Recovery = 119% Analysis Date = 06/25/16 Pct Recovery = 119% Analysis Date = 06/14/16 Pct Recovery = 119% Analysis Date = 06/14/16 Pct Recovery = 119% Analysis Date = 06/04/16 Pct Recovery = 119% Analysis Date = 06/04/16 Pct Recovery = 119% Analysis Date = 05/24/16 Pct Recovery = 119% Analysis Date = 05/24/16 Pct Recovery = 119% Analysis Date = 05/13/16 Pct Recovery = 118% Analysis Date = 05/13/16 Pct Recovery = 118% Analysis Date = 05/02/16 Pct Recovery = 118% Analysis Date = 05/02/16 Pct Recovery = 118% Analysis Date = 04/21/16 Pct Recovery = 118% Analysis Date = 04/21/16 Pct Recovery = 118% Analysis Date = 04/10/16 Pct Recovery = 118% Analysis Date = 04/10/16 Pct Recovery = 118% Analysis Date = 03/31/16 Pct Recovery = 117% Analysis Date = 03/31/16 Pct Recovery = 117% Analysis Date = 03/20/16 Pct Recovery = 117% Analysis Date = 03/20/16 Pct Recovery = 117% Analysis Date = 03/09/16 Pct Recovery = 117% Analysis Date = 03/09/16 Pct Recovery = 117% Analysis Date = 02/27/16 Pct Recovery = 116% Analysis Date = 02/27/16 Pct Recovery = 116% Analysis Date = 02/16/16 Pct Recovery = 116% Analysis Date = 02/16/16 Pct Recovery = 116% Analysis Date = 02/05/16 Pct Recovery = 116% Analysis Date = 02/05/16 Pct Recovery = 116% Analysis Date = 01/25/16 Pct Recovery = 116% Analysis Date = 01/25/16 Pct Recovery = 116% Analysis Date = 01/15/16 Pct Recovery = 115% Analysis Date = 01/15/16 Pct Recovery = 115% Analysis Date = 01/04/16 Pct Recovery = 115% Analysis Date = 01/04/16 Pct Recovery = 115% Analysis Date = 12/24/15 Pct Recovery = 115% Analysis Date = 12/24/15 Pct Recovery = 115% Analysis Date = 12/13/15 Pct Recovery = 115% Analysis Date = 12/13/15 Pct Recovery = 115% Analysis Date = 12/02/15 Pct Recovery = 115% Analysis Date = 12/02/15 Pct Recovery = 115% Analysis Date = 11/21/15 Pct Recovery = 114% Analysis Date = 11/21/15 Pct Recovery = 114% Analysis Date = 11/10/15 Pct Recovery = 114% Analysis Date = 11/10/15 Pct Recovery = 114% Analysis Date = 10/31/15 Pct Recovery = 114% Analysis Date = 10/31/15 Pct Recovery = 114% Analysis Date = 10/20/15 Pct Recovery = 114% Analysis Date = 10/20/15 Pct Recovery = 114% Analysis Date = 10/09/15 Pct Recovery = 113% Analysis Date = 10/09/15 Pct Recovery = 113% Analysis Date = 09/28/15 Pct Recovery = 113% Analysis Date = 09/28/15 Pct Recovery = 113% Analysis Date = 09/17/15 Pct Recovery = 113% Analysis Date = 09/17/15 Pct Recovery = 113% Analysis Date = 09/06/15 Pct Recovery = 113% Analysis Date = 09/06/15 Pct Recovery = 113% Analysis Date = 08/27/15 Pct Recovery = 112% Analysis Date = 08/27/15 Pct Recovery = 112% Analysis Date = 08/16/15 Pct Recovery = 112% Analysis Date = 08/16/15 Pct Recovery = 112% Analysis Date = 08/05/15 Pct Recovery = 112% Analysis Date = 08/05/15 Pct Recovery = 112% Analysis Date = 07/25/15 Pct Recovery = 112% Analysis Date = 07/25/15 Pct Recovery = 112% Analysis Date = 07/14/15 Pct Recovery = 111% Analysis Date = 07/14/15 Pct Recovery = 111% Analysis Date = 07/03/15 Pct Recovery = 111% Analysis Date = 07/03/15 Pct Recovery = 111% Analysis Date = 06/22/15 Pct Recovery = 111% Analysis Date = 06/22/15 Pct Recovery = 111% Analysis Date = 06/12/15 Pct Recovery = 111% Analysis Date = 06/12/15 Pct Recovery = 111% Analysis Date = 06/01/15 Pct Recovery = 110% Analysis Date = 06/01/15 Pct Recovery = 110% Analysis Date = 05/21/15 Pct Recovery = 110% Analysis Date = 05/21/15 Pct Recovery = 110% Analysis Date = 05/10/15 Pct Recovery = 110% Analysis Date = 05/10/15 Pct Recovery = 110% Analysis Date = 04/29/15 Pct Recovery = 110% Analysis Date = 04/29/15 Pct Recovery = 110% Analysis Date = 04/18/15 Pct Recovery = 109% Analysis Date = 04/18/15 Pct Recovery = 109% Analysis Date = 04/07/15 Pct Recovery = 109% Analysis Date = 04/07/15 Pct Recovery = 109% Analysis Date = 03/28/15 Pct Recovery = 109% Analysis Date = 03/28/15 Pct Recovery = 109% Analysis Date = 03/17/15 Pct Recovery = 109% Analysis Date = 03/17/15 Pct Recovery = 109% Analysis Date = 03/06/15 Pct Recovery = 108% Analysis Date = 03/06/15 Pct Recovery = 108% Analysis Date = 02/23/15 Pct Recovery = 108% Analysis Date = 02/23/15 Pct Recovery = 108% Analysis Date = 02/12/15 Pct Recovery = 108% Analysis Date = 02/12/15 Pct Recovery = 108% Analysis Date = 02/01/15 Pct Recovery = 109% Analysis Date = 02/01/15 Pct Recovery = 109% Analysis Date = 01/22/15 Pct Recovery = 109% Analysis Date = 01/22/15 Pct Recovery = 109% Analysis Date = 01/11/15 Pct Recovery = 109% Analysis Date = 01/11/15 Pct Recovery = 109% Analysis Date = 12/31/14 Pct Recovery = 110% Analysis Date = 12/31/14 Pct Recovery = 110% Analysis Date = 12/20/14 Pct Recovery = 110% Analysis Date = 12/20/14 Pct Recovery = 110% Analysis Date = 12/09/14 Pct Recovery = 110% Analysis Date = 12/09/14 Pct Recovery = 110% Analysis Date = 11/28/14 Pct Recovery = 111% Analysis Date = 11/28/14 Pct Recovery = 111% Analysis Date = 11/17/14 Pct Recovery = 111% Analysis Date = 11/17/14 Pct Recovery = 111% Analysis Date = 11/07/14 Pct Recovery = 111% Analysis Date = 11/07/14 Pct Recovery = 111% Analysis Date = 10/27/14 Pct Recovery = 112% Analysis Date = 10/27/14 Pct Recovery = 112% Analysis Date = 10/16/14 Pct Recovery = 112% Analysis Date = 10/16/14 Pct Recovery = 112% Analysis Date = 10/05/14 Pct Recovery = 112% Analysis Date = 10/05/14 Pct Recovery = 112% Analysis Date = 09/24/14 Pct Recovery = 113% Analysis Date = 09/24/14 Pct Recovery = 113% Analysis Date = 09/13/14 Pct Recovery = 113% Analysis Date = 09/13/14 Pct Recovery = 113% Analysis Date = 09/02/14 Pct Recovery = 113% Analysis Date = 09/02/14 Pct Recovery = 113% Analysis Date = 08/23/14 Pct Recovery = 114% Analysis Date = 08/23/14 Pct Recovery = 114% Analysis Date = 08/12/14 Pct Recovery = 114% Analysis Date = 08/12/14 Pct Recovery = 114% Analysis Date = 08/01/14 Pct Recovery = 114% Analysis Date = 08/01/14 Pct Recovery = 114% Analysis Date = 07/21/14 Pct Recovery = 115% Analysis Date = 07/21/14 Pct Recovery = 115% Analysis Date = 07/10/14 Pct Recovery = 115% Analysis Date = 07/10/14 Pct Recovery = 115% Analysis Date = 06/29/14 Pct Recovery = 115% Analysis Date = 06/29/14 Pct Recovery = 115% Analysis Date = 06/19/14 Pct Recovery = 116% Analysis Date = 06/19/14 Pct Recovery = 116% Analysis Date = 06/08/14 Pct Recovery = 116% Analysis Date = 06/08/14 Pct Recovery = 116% Analysis Date = 05/28/14 Pct Recovery = 116% Analysis Date = 05/28/14 Pct Recovery = 116% Analysis Date = 05/17/14 Pct Recovery = 117% Analysis Date = 05/17/14 Pct Recovery = 117% Analysis Date = 05/06/14 Pct Recovery = 117% Analysis Date = 05/06/14 Pct Recovery = 117% Analysis Date = 04/25/14 Pct Recovery = 117% Analysis Date = 04/25/14 Pct Recovery = 117% Analysis Date = 04/14/14 Pct Recovery = 118% Analysis Date = 04/14/14 Pct Recovery = 118% Analysis Date = 04/04/14 Pct Recovery = 118% Analysis Date = 04/04/14 Pct Recovery = 118% Analysis Date = 03/24/14 Pct Recovery = 119% Analysis Date = 03/24/14 Pct Recovery = 119% Analysis Date = 03/13/14 Pct Recovery = 119% Analysis Date = 03/13/14 Pct Recovery = 119% Analysis Date = 03/02/14 Pct Recovery = 119% Analysis Date = 03/02/14 Pct Recovery = 119% Analysis Date = 02/19/14 Pct Recovery = 120% Analysis Date = 02/19/14 Pct Recovery = 120% Analysis Date = 02/08/14 Pct Recovery = 120% Analysis Date = 02/08/14 Pct Recovery = 120% Analysis Date = 01/28/14 Pct Recovery = 121% Analysis Date = 01/28/14 Pct Recovery = 121% Analysis Date = 01/18/14 Pct Recovery = 121% Analysis Date = 01/18/14 Pct Recovery = 121% Analysis Date = 01/07/14 Pct Recovery = 121% Analysis Date = 01/07/14 Pct Recovery = 121% Analysis Date = 12/27/13 Pct Recovery = 121% Analysis Date = 12/27/13 Pct Recovery = 121% Analysis Date = 12/16/13 Pct Recovery = 122% Analysis Date = 12/16/13 Pct Recovery = 122% Analysis Date = 12/05/13 Pct Recovery = 122% Analysis Date = 12/05/13 Pct Recovery = 122% Analysis Date = 11/24/13 Pct Recovery = 122% Analysis Date = 11/24/13 Pct Recovery = 122% Analysis Date = 11/14/13 Pct Recovery = 123% Analysis Date = 11/14/13 Pct Recovery = 123% Analysis Date = 11/03/13 Pct Recovery = 123% Analysis Date = 11/03/13 Pct Recovery = 123% Analysis Date = 10/23/13 Pct Recovery = 123% Analysis Date = 10/23/13 Pct Recovery = 123% Analysis Date = 10/12/13 Pct Recovery = 124% Analysis Date = 10/12/13 Pct Recovery = 124% Analysis Date = 10/01/13 Pct Recovery = 124% Analysis Date = 10/01/13 Pct Recovery = 124% Analysis Date = 09/20/13 Pct Recovery = 125% Analysis Date = 09/20/13 Pct Recovery = 125% Analysis Date = 09/09/13 Pct Recovery = 125% Analysis Date = 09/09/13 Pct Recovery = 125% Analysis Date = 08/30/13 Pct Recovery = 126% Analysis Date = 08/30/13 Pct Recovery = 126% Analysis Date = 08/19/13 Pct Recovery = 126% Analysis Date = 08/19/13 Pct Recovery = 126% Analysis Date = 08/08/13 Pct Recovery = 127% Analysis Date = 08/08/13 Pct Recovery = 127% Analysis Date = 07/28/13 Pct Recovery = 127% Analysis Date = 07/28/13 Pct Recovery = 127% Analysis Date = 07/17/13 Pct Recovery = 128% Analysis Date = 07/17/13 Pct Recovery = 128% Analysis Date = 07/06/13 Pct Recovery = 128% Analysis Date = 07/06/13 Pct Recovery = 128% Analysis Date = 06/25/13 Pct Recovery = 129% Analysis Date = 06/25/13 Pct Recovery = 129% Analysis Date = 06/15/13 Pct Recovery = 129% Analysis Date = 06/15/13 Pct Recovery = 129% Analysis Date = 06/04/13 Pct Recovery = 130% Analysis Date = 06/04/13 Pct Recovery = 130% Analysis Date = 05/24/13 Pct Recovery = 130% Analysis Date = 05/24/13 Pct Recovery = 130% Analysis Date = 05/13/13 Pct Recovery = 130% Analysis Date = 05/13/13 Pct Recovery = 130% Analysis Date = 05/02/13 Pct Recovery = 131% Analysis Date = 05/02/13 Pct Recovery = 131% Analysis Date = 04/21/13 Pct Recovery = 131% Analysis Date = 04/21/13 Pct Recovery = 131% Analysis Date = 04/11/13 Pct Recovery = 132% Analysis Date = 04/11/13 Pct Recovery = 132% Analysis Date = 03/31/13 Pct Recovery = 132% Analysis Date = 03/31/13 Pct Recovery = 132% Analysis Date = 03/20/13 Pct Recovery = 133% Analysis Date = 03/20/13 Pct Recovery = 133% Analysis Date = 03/09/13 Pct Recovery = 133% Analysis Date = 03/09/13 Pct Recovery = 133% Analysis Date = 02/26/13 Pct Recovery = 133% Analysis Date = 02/26/13 Pct Recovery = 133% Analysis Date = 02/15/13 Pct Recovery = 134% Analysis Date = 02/15/13 Pct Recovery = 134% Analysis Date = 02/04/13 Pct Recovery = 134% Analysis Date = 02/04/13 Pct Recovery = 134% Analysis Date = 01/25/13 Pct Recovery = 134% Analysis Date = 01/25/13 Pct Recovery = 134% Analysis Date = 01/14/13 Pct Recovery = 135% Analysis Date = 01/14/13 Pct Recovery = 135% Analysis Date = 01/03/13 Pct Recovery = 135% Analysis Date = 01/03/13 Pct Recovery = 135% Analysis Date = 12/23/12 Pct Recovery = 135% Analysis Date = 12/23/12 Pct Recovery = 135% Analysis Date = 12/12/12 Pct Recovery = 136% Analysis Date = 12/12/12 Pct Recovery = 136% Analysis Date = 12/01/12 Pct Recovery = 136% Analysis Date = 12/01/12 Pct Recovery = 136% Analysis Date = 11/20/12 Pct Recovery = 136% Analysis Date = 11/20/12 Pct Recovery = 136% Analysis Date = 11/10/12 Pct Recovery = 137% Analysis Date = 11/10/12 Pct Recovery = 137% Analysis Date = 10/30/12 Pct Recovery = 137% Analysis Date = 10/30/12 Pct Recovery = 137% Analysis Date = 10/19/12 Pct Recovery = 137% Analysis Date = 10/19/12 Pct Recovery = 137% Analysis Date = 10/08/12 Pct Recovery = 137% Analysis Date = 10/08/12 Pct Recovery = 137% Analysis Date = 09/27/12 Pct Recovery = 138% Analysis Date = 09/27/12 Pct Recovery = 138% Analysis Date = 09/16/12 Pct Recovery = 138% Analysis Date = 09/16/12 Pct Recovery = 138% Analysis Date = 09/06/12 Pct Recovery = 138% Analysis Date = 09/06/12 Pct Recovery = 138% Analysis Date = 08/26/12 Pct Recovery = 138% Analysis Date = 08/26/12 Pct Recovery = 138% Analysis Date = 08/15/12 Pct Recovery = 138% Analysis Date = 08/15/12 Pct Recovery = 138% Analysis Date = 08/04/12 Pct Recovery = 138% Analysis Date = 08/04/12 Pct Recovery = 138% Analysis Date = 07/24/12 Pct Recovery = 139% Analysis Date = 07/24/12 Pct Recovery = 139% Analysis Date = 07/13/12 Pct Recovery = 139% Analysis Date = 07/13/12 Pct Recovery = 139% Analysis Date = 07/02/12 Pct Recovery = 139% Analysis Date = 07/02/12 Pct Recovery = 139% Analysis Date = 06/22/12 Pct Recovery = 139% Analysis Date = 06/22/12 Pct Recovery = 139% Analysis Date = 06/11/12 Pct Recovery = 140% Analysis Date = 06/11/12 Pct Recovery = 140% Analysis Date = 05/31/12 Pct Recovery = 140% Analysis Date = 05/31/12 Pct Recovery = 140% Analysis Date = 05/20/12 Pct Recovery = 140% Analysis Date = 05/20/12 Pct Recovery = 140% Analysis Date = 05/09/12 Pct Recovery = 141% Analysis Date = 05/09/12 Pct Recovery = 141% Analysis Date = 04/28/12 Pct Recovery = 141% Analysis Date = 04/28/12 Pct Recovery = 141% Analysis Date = 04/17/12 Pct Recovery = 141% Analysis Date = 04/17/12 Pct Recovery = 141% Analysis Date = 04/07/12 Pct Recovery = 142% Analysis Date = 04/07/12 Pct Recovery = 142% Analysis Date = 03/27/12 Pct Recovery = 142% Analysis Date = 03/27/12 Pct Recovery = 142% Analysis Date = 03/16/12 Pct Recovery = 142% Analysis Date = 03/16/12 Pct Recovery = 142% Analysis Date = 03/05/12 Pct Recovery = 143% Analysis Date = 03/05/12 Pct Recovery = 143% Analysis Date = 02/23/12 Pct Recovery = 143% Analysis Date = 02/23/12 Pct Recovery = 143% Analysis Date = 02/12/12 Pct Recovery = 143% Analysis Date = 02/12/12 Pct Recovery = 143% Analysis Date = 02/02/12 Pct Recovery = 144% Analysis Date = 02/02/12 Pct Recovery = 144% Analysis Date = 01/22/12 Pct Recovery = 144% Analysis Date = 01/22/12 Pct Recovery = 144% Analysis Date = 01/11/12 Pct Recovery = 144% Analysis Date = 01/11/12 Pct Recovery = 144% Analysis Date = 12/31/11 Pct Recovery = 145% Analysis Date = 12/31/11 Pct Recovery = 145% Analysis Date = 12/20/11 Pct Recovery = 145% Analysis Date = 12/20/11 Pct Recovery = 145% Analysis Date = 12/09/11 Pct Recovery = 145% Analysis Date = 12/09/11 Pct Recovery = 145% Analysis Date = 11/28/11 Pct Recovery = 146% Analysis Date = 11/28/11 Pct Recovery = 146% Analysis Date = 11/18/11 Pct Recovery = 146% Analysis Date = 11/18/11 Pct Recovery = 146% Analysis Date = 11/07/11 Pct Recovery = 146% Analysis Date = 11/07/11 Pct Recovery = 146% Analysis Date = 10/27/11 Pct Recovery = 147% Analysis Date = 10/27/11 Pct Recovery = 147% Analysis Date = 10/16/11 Pct Recovery = 147% Analysis Date = 10/16/11 Pct Recovery = 147% Analysis Date = 10/05/11 Pct Recovery = 147% Analysis Date = 10/05/11 Pct Recovery = 147% Analysis Date = 09/24/11 Pct Recovery = 148% Analysis Date = 09/24/11 Pct Recovery = 148% Analysis Date = 09/13/11 Pct Recovery = 148% Analysis Date = 09/13/11 Pct Recovery = 148% Analysis Date = 09/03/11 Pct Recovery = 148% Analysis Date = 09/03/11 Pct Recovery = 148% Analysis Date = 08/23/11 Pct Recovery = 149% Analysis Date = 08/23/11 Pct Recovery = 149% Analysis Date = 08/12/11 Pct Recovery = 149% Analysis Date = 08/12/11 Pct Recovery = 149% Analysis Date = 08/01/11 Pct Recovery = 149% Analysis Date = 08/01/11 Pct Recovery = 149% Analysis Date = 07/21/11 Pct Recovery = 150% Analysis Date = 07/21/11 Pct Recovery = 150% Analysis Date = 07/10/11 Pct Recovery = 150% Analysis Date = 07/10/11 Pct Recovery = 150% Analysis Date = 06/30/11 Pct Recovery = 150% Analysis Date = 06/30/11 Pct Recovery = 150% Analysis Date = 06/19/11 Pct Recovery = 151% Analysis Date = 06/19/11 Pct Recovery = 151% Analysis Date = 06/08/11 Pct Recovery = 151% Analysis Date = 06/08/11 Pct Recovery = 151% Analysis Date = 05/28/11 Pct Recovery = 152% Analysis Date = 05/28/11 Pct Recovery = 152% Analysis Date = 05/17/11 Pct Recovery = 152% Analysis Date = 05/17/11 Pct Recovery = 152% Analysis Date = 05/06/11 Pct Recovery = 152% Analysis Date = 05/06/11 Pct Recovery = 152% Analysis Date = 04/25/11 Pct Recovery = 153% Analysis Date = 04/25/11 Pct Recovery = 153% Analysis Date = 04/15/11 Pct Recovery = 153% Analysis Date = 04/15/11 Pct Recovery = 153% Analysis Date = 04/04/11 Pct Recovery = 153% Analysis Date = 04/04/11 Pct Recovery = 153% Analysis Date = 03/24/11 Pct Recovery = 154% Analysis Date = 03/24/11 Pct Recovery = 154% Analysis Date = 03/13/11 Pct Recovery = 154% Analysis Date = 03/13/11 Pct Recovery = 154% Analysis Date = 03/02/11 Pct Recovery = 154% Analysis Date = 03/02/11 Pct Recovery = 154% Analysis Date = 02/19/11 Pct Recovery = 155% Analysis Date = 02/19/11 Pct Recovery = 155% Analysis Date = 02/09/11 Pct Recovery = 155% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUTHIURON

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 211% . 211% 0%
>= Reporting Level 92 126% 37% 123% 33%
Total 93 127% 38% 123% 33%

Sample Statistics
TEBUTHIURON

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 28 30% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 0 0% 0 out of 76

BQS OBSP Determination:
TEFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61606GCM39
Open Data Set

Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 51% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 51% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 58% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 52% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 56% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 54% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 54% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 42% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 66% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 64% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 73% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 52% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 52% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 62% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 68% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 57% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 61% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 61% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 40% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 63% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 31% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 48% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 58% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 65% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 50% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 54% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 65% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 61% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 52% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 52% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 52% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 63% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 52% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 69% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 45% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 56% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 65% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 73% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 66% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 66% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 58% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 75% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 53% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 57% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 59% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 53% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 58% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 56% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 56% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 58% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 69% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 42% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 41% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 56% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 60% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 54% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 62% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 50% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 56% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 72% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 64% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 58% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 82% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 61% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 56% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 56% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 41% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 61% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 76% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 64% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 73% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 42% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 73% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 75% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 71% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 73% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 84% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 71% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 71% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 82% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 79% Analysis Date = 01/17/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 12/27/16 Pct Recovery = 55% Analysis Date = 12/27/16 Pct Recovery = 55% Analysis Date = 12/16/16 Pct Recovery = 55% Analysis Date = 12/16/16 Pct Recovery = 55% Analysis Date = 12/05/16 Pct Recovery = 55% Analysis Date = 12/05/16 Pct Recovery = 55% Analysis Date = 11/24/16 Pct Recovery = 55% Analysis Date = 11/24/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 11/03/16 Pct Recovery = 55% Analysis Date = 10/23/16 Pct Recovery = 55% Analysis Date = 10/23/16 Pct Recovery = 55% Analysis Date = 10/12/16 Pct Recovery = 55% Analysis Date = 10/12/16 Pct Recovery = 55% Analysis Date = 10/01/16 Pct Recovery = 55% Analysis Date = 10/01/16 Pct Recovery = 55% Analysis Date = 09/20/16 Pct Recovery = 55% Analysis Date = 09/20/16 Pct Recovery = 55% Analysis Date = 09/09/16 Pct Recovery = 55% Analysis Date = 09/09/16 Pct Recovery = 55% Analysis Date = 08/29/16 Pct Recovery = 56% Analysis Date = 08/29/16 Pct Recovery = 56% Analysis Date = 08/19/16 Pct Recovery = 56% Analysis Date = 08/19/16 Pct Recovery = 56% Analysis Date = 08/08/16 Pct Recovery = 56% Analysis Date = 08/08/16 Pct Recovery = 56% Analysis Date = 07/28/16 Pct Recovery = 56% Analysis Date = 07/28/16 Pct Recovery = 56% Analysis Date = 07/17/16 Pct Recovery = 56% Analysis Date = 07/17/16 Pct Recovery = 56% Analysis Date = 07/06/16 Pct Recovery = 56% Analysis Date = 07/06/16 Pct Recovery = 56% Analysis Date = 06/25/16 Pct Recovery = 56% Analysis Date = 06/25/16 Pct Recovery = 56% Analysis Date = 06/14/16 Pct Recovery = 56% Analysis Date = 06/14/16 Pct Recovery = 56% Analysis Date = 06/04/16 Pct Recovery = 56% Analysis Date = 06/04/16 Pct Recovery = 56% Analysis Date = 05/24/16 Pct Recovery = 56% Analysis Date = 05/24/16 Pct Recovery = 56% Analysis Date = 05/13/16 Pct Recovery = 56% Analysis Date = 05/13/16 Pct Recovery = 56% Analysis Date = 05/02/16 Pct Recovery = 56% Analysis Date = 05/02/16 Pct Recovery = 56% Analysis Date = 04/21/16 Pct Recovery = 56% Analysis Date = 04/21/16 Pct Recovery = 56% Analysis Date = 04/10/16 Pct Recovery = 56% Analysis Date = 04/10/16 Pct Recovery = 56% Analysis Date = 03/30/16 Pct Recovery = 56% Analysis Date = 03/30/16 Pct Recovery = 56% Analysis Date = 03/20/16 Pct Recovery = 56% Analysis Date = 03/20/16 Pct Recovery = 56% Analysis Date = 03/09/16 Pct Recovery = 56% Analysis Date = 03/09/16 Pct Recovery = 56% Analysis Date = 02/27/16 Pct Recovery = 56% Analysis Date = 02/27/16 Pct Recovery = 56% Analysis Date = 02/16/16 Pct Recovery = 57% Analysis Date = 02/16/16 Pct Recovery = 57% Analysis Date = 02/05/16 Pct Recovery = 57% Analysis Date = 02/05/16 Pct Recovery = 57% Analysis Date = 01/25/16 Pct Recovery = 57% Analysis Date = 01/25/16 Pct Recovery = 57% Analysis Date = 01/14/16 Pct Recovery = 57% Analysis Date = 01/14/16 Pct Recovery = 57% Analysis Date = 01/04/16 Pct Recovery = 57% Analysis Date = 01/04/16 Pct Recovery = 57% Analysis Date = 12/24/15 Pct Recovery = 57% Analysis Date = 12/24/15 Pct Recovery = 57% Analysis Date = 12/13/15 Pct Recovery = 57% Analysis Date = 12/13/15 Pct Recovery = 57% Analysis Date = 12/02/15 Pct Recovery = 57% Analysis Date = 12/02/15 Pct Recovery = 57% Analysis Date = 11/21/15 Pct Recovery = 57% Analysis Date = 11/21/15 Pct Recovery = 57% Analysis Date = 11/10/15 Pct Recovery = 57% Analysis Date = 11/10/15 Pct Recovery = 57% Analysis Date = 10/30/15 Pct Recovery = 57% Analysis Date = 10/30/15 Pct Recovery = 57% Analysis Date = 10/20/15 Pct Recovery = 57% Analysis Date = 10/20/15 Pct Recovery = 57% Analysis Date = 10/09/15 Pct Recovery = 57% Analysis Date = 10/09/15 Pct Recovery = 57% Analysis Date = 09/28/15 Pct Recovery = 57% Analysis Date = 09/28/15 Pct Recovery = 57% Analysis Date = 09/17/15 Pct Recovery = 57% Analysis Date = 09/17/15 Pct Recovery = 57% Analysis Date = 09/06/15 Pct Recovery = 57% Analysis Date = 09/06/15 Pct Recovery = 57% Analysis Date = 08/26/15 Pct Recovery = 57% Analysis Date = 08/26/15 Pct Recovery = 57% Analysis Date = 08/15/15 Pct Recovery = 57% Analysis Date = 08/15/15 Pct Recovery = 57% Analysis Date = 08/05/15 Pct Recovery = 57% Analysis Date = 08/05/15 Pct Recovery = 57% Analysis Date = 07/25/15 Pct Recovery = 57% Analysis Date = 07/25/15 Pct Recovery = 57% Analysis Date = 07/14/15 Pct Recovery = 57% Analysis Date = 07/14/15 Pct Recovery = 57% Analysis Date = 07/03/15 Pct Recovery = 57% Analysis Date = 07/03/15 Pct Recovery = 57% Analysis Date = 06/22/15 Pct Recovery = 57% Analysis Date = 06/22/15 Pct Recovery = 57% Analysis Date = 06/11/15 Pct Recovery = 57% Analysis Date = 06/11/15 Pct Recovery = 57% Analysis Date = 05/31/15 Pct Recovery = 58% Analysis Date = 05/31/15 Pct Recovery = 58% Analysis Date = 05/21/15 Pct Recovery = 58% Analysis Date = 05/21/15 Pct Recovery = 58% Analysis Date = 05/10/15 Pct Recovery = 58% Analysis Date = 05/10/15 Pct Recovery = 58% Analysis Date = 04/29/15 Pct Recovery = 58% Analysis Date = 04/29/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/07/15 Pct Recovery = 58% Analysis Date = 04/07/15 Pct Recovery = 58% Analysis Date = 03/27/15 Pct Recovery = 58% Analysis Date = 03/27/15 Pct Recovery = 58% Analysis Date = 03/16/15 Pct Recovery = 58% Analysis Date = 03/16/15 Pct Recovery = 58% Analysis Date = 03/06/15 Pct Recovery = 58% Analysis Date = 03/06/15 Pct Recovery = 58% Analysis Date = 02/23/15 Pct Recovery = 58% Analysis Date = 02/23/15 Pct Recovery = 58% Analysis Date = 02/12/15 Pct Recovery = 58% Analysis Date = 02/12/15 Pct Recovery = 58% Analysis Date = 02/01/15 Pct Recovery = 58% Analysis Date = 02/01/15 Pct Recovery = 58% Analysis Date = 01/21/15 Pct Recovery = 58% Analysis Date = 01/21/15 Pct Recovery = 58% Analysis Date = 01/10/15 Pct Recovery = 58% Analysis Date = 01/10/15 Pct Recovery = 58% Analysis Date = 12/31/14 Pct Recovery = 58% Analysis Date = 12/31/14 Pct Recovery = 58% Analysis Date = 12/20/14 Pct Recovery = 58% Analysis Date = 12/20/14 Pct Recovery = 58% Analysis Date = 12/09/14 Pct Recovery = 58% Analysis Date = 12/09/14 Pct Recovery = 58% Analysis Date = 11/28/14 Pct Recovery = 58% Analysis Date = 11/28/14 Pct Recovery = 58% Analysis Date = 11/17/14 Pct Recovery = 58% Analysis Date = 11/17/14 Pct Recovery = 58% Analysis Date = 11/06/14 Pct Recovery = 58% Analysis Date = 11/06/14 Pct Recovery = 58% Analysis Date = 10/26/14 Pct Recovery = 58% Analysis Date = 10/26/14 Pct Recovery = 58% Analysis Date = 10/16/14 Pct Recovery = 59% Analysis Date = 10/16/14 Pct Recovery = 59% Analysis Date = 10/05/14 Pct Recovery = 59% Analysis Date = 10/05/14 Pct Recovery = 59% Analysis Date = 09/24/14 Pct Recovery = 59% Analysis Date = 09/24/14 Pct Recovery = 59% Analysis Date = 09/13/14 Pct Recovery = 59% Analysis Date = 09/13/14 Pct Recovery = 59% Analysis Date = 09/02/14 Pct Recovery = 59% Analysis Date = 09/02/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/22/14 Pct Recovery = 59% Analysis Date = 08/11/14 Pct Recovery = 59% Analysis Date = 08/11/14 Pct Recovery = 59% Analysis Date = 08/01/14 Pct Recovery = 59% Analysis Date = 08/01/14 Pct Recovery = 59% Analysis Date = 07/21/14 Pct Recovery = 59% Analysis Date = 07/21/14 Pct Recovery = 59% Analysis Date = 07/10/14 Pct Recovery = 59% Analysis Date = 07/10/14 Pct Recovery = 59% Analysis Date = 06/29/14 Pct Recovery = 59% Analysis Date = 06/29/14 Pct Recovery = 59% Analysis Date = 06/18/14 Pct Recovery = 58% Analysis Date = 06/18/14 Pct Recovery = 58% Analysis Date = 06/07/14 Pct Recovery = 58% Analysis Date = 06/07/14 Pct Recovery = 58% Analysis Date = 05/27/14 Pct Recovery = 58% Analysis Date = 05/27/14 Pct Recovery = 58% Analysis Date = 05/17/14 Pct Recovery = 58% Analysis Date = 05/17/14 Pct Recovery = 58% Analysis Date = 05/06/14 Pct Recovery = 58% Analysis Date = 05/06/14 Pct Recovery = 58% Analysis Date = 04/25/14 Pct Recovery = 58% Analysis Date = 04/25/14 Pct Recovery = 58% Analysis Date = 04/14/14 Pct Recovery = 58% Analysis Date = 04/14/14 Pct Recovery = 58% Analysis Date = 04/03/14 Pct Recovery = 58% Analysis Date = 04/03/14 Pct Recovery = 58% Analysis Date = 03/23/14 Pct Recovery = 58% Analysis Date = 03/23/14 Pct Recovery = 58% Analysis Date = 03/12/14 Pct Recovery = 58% Analysis Date = 03/12/14 Pct Recovery = 58% Analysis Date = 03/02/14 Pct Recovery = 57% Analysis Date = 03/02/14 Pct Recovery = 57% Analysis Date = 02/19/14 Pct Recovery = 57% Analysis Date = 02/19/14 Pct Recovery = 57% Analysis Date = 02/08/14 Pct Recovery = 57% Analysis Date = 02/08/14 Pct Recovery = 57% Analysis Date = 01/28/14 Pct Recovery = 57% Analysis Date = 01/28/14 Pct Recovery = 57% Analysis Date = 01/17/14 Pct Recovery = 57% Analysis Date = 01/17/14 Pct Recovery = 57% Analysis Date = 01/06/14 Pct Recovery = 57% Analysis Date = 01/06/14 Pct Recovery = 57% Analysis Date = 12/26/13 Pct Recovery = 57% Analysis Date = 12/26/13 Pct Recovery = 57% Analysis Date = 12/16/13 Pct Recovery = 57% Analysis Date = 12/16/13 Pct Recovery = 57% Analysis Date = 12/05/13 Pct Recovery = 57% Analysis Date = 12/05/13 Pct Recovery = 57% Analysis Date = 11/24/13 Pct Recovery = 57% Analysis Date = 11/24/13 Pct Recovery = 57% Analysis Date = 11/13/13 Pct Recovery = 57% Analysis Date = 11/13/13 Pct Recovery = 57% Analysis Date = 11/02/13 Pct Recovery = 57% Analysis Date = 11/02/13 Pct Recovery = 57% Analysis Date = 10/22/13 Pct Recovery = 57% Analysis Date = 10/22/13 Pct Recovery = 57% Analysis Date = 10/11/13 Pct Recovery = 57% Analysis Date = 10/11/13 Pct Recovery = 57% Analysis Date = 10/01/13 Pct Recovery = 57% Analysis Date = 10/01/13 Pct Recovery = 57% Analysis Date = 09/20/13 Pct Recovery = 57% Analysis Date = 09/20/13 Pct Recovery = 57% Analysis Date = 09/09/13 Pct Recovery = 57% Analysis Date = 09/09/13 Pct Recovery = 57% Analysis Date = 08/29/13 Pct Recovery = 57% Analysis Date = 08/29/13 Pct Recovery = 57% Analysis Date = 08/18/13 Pct Recovery = 57% Analysis Date = 08/18/13 Pct Recovery = 57% Analysis Date = 08/07/13 Pct Recovery = 57% Analysis Date = 08/07/13 Pct Recovery = 57% Analysis Date = 07/27/13 Pct Recovery = 57% Analysis Date = 07/27/13 Pct Recovery = 57% Analysis Date = 07/17/13 Pct Recovery = 57% Analysis Date = 07/17/13 Pct Recovery = 57% Analysis Date = 07/06/13 Pct Recovery = 57% Analysis Date = 07/06/13 Pct Recovery = 57% Analysis Date = 06/25/13 Pct Recovery = 57% Analysis Date = 06/25/13 Pct Recovery = 57% Analysis Date = 06/14/13 Pct Recovery = 57% Analysis Date = 06/14/13 Pct Recovery = 57% Analysis Date = 06/03/13 Pct Recovery = 57% Analysis Date = 06/03/13 Pct Recovery = 57% Analysis Date = 05/23/13 Pct Recovery = 57% Analysis Date = 05/23/13 Pct Recovery = 57% Analysis Date = 05/12/13 Pct Recovery = 57% Analysis Date = 05/12/13 Pct Recovery = 57% Analysis Date = 05/02/13 Pct Recovery = 57% Analysis Date = 05/02/13 Pct Recovery = 57% Analysis Date = 04/21/13 Pct Recovery = 57% Analysis Date = 04/21/13 Pct Recovery = 57% Analysis Date = 04/10/13 Pct Recovery = 57% Analysis Date = 04/10/13 Pct Recovery = 57% Analysis Date = 03/30/13 Pct Recovery = 57% Analysis Date = 03/30/13 Pct Recovery = 57% Analysis Date = 03/19/13 Pct Recovery = 57% Analysis Date = 03/19/13 Pct Recovery = 57% Analysis Date = 03/08/13 Pct Recovery = 57% Analysis Date = 03/08/13 Pct Recovery = 57% Analysis Date = 02/25/13 Pct Recovery = 57% Analysis Date = 02/25/13 Pct Recovery = 57% Analysis Date = 02/15/13 Pct Recovery = 58% Analysis Date = 02/15/13 Pct Recovery = 58% Analysis Date = 02/04/13 Pct Recovery = 58% Analysis Date = 02/04/13 Pct Recovery = 58% Analysis Date = 01/24/13 Pct Recovery = 58% Analysis Date = 01/24/13 Pct Recovery = 58% Analysis Date = 01/13/13 Pct Recovery = 58% Analysis Date = 01/13/13 Pct Recovery = 58% Analysis Date = 01/02/13 Pct Recovery = 58% Analysis Date = 01/02/13 Pct Recovery = 58% Analysis Date = 12/22/12 Pct Recovery = 58% Analysis Date = 12/22/12 Pct Recovery = 58% Analysis Date = 12/12/12 Pct Recovery = 58% Analysis Date = 12/12/12 Pct Recovery = 58% Analysis Date = 12/01/12 Pct Recovery = 58% Analysis Date = 12/01/12 Pct Recovery = 58% Analysis Date = 11/20/12 Pct Recovery = 58% Analysis Date = 11/20/12 Pct Recovery = 58% Analysis Date = 11/09/12 Pct Recovery = 59% Analysis Date = 11/09/12 Pct Recovery = 59% Analysis Date = 10/29/12 Pct Recovery = 59% Analysis Date = 10/29/12 Pct Recovery = 59% Analysis Date = 10/18/12 Pct Recovery = 59% Analysis Date = 10/18/12 Pct Recovery = 59% Analysis Date = 10/07/12 Pct Recovery = 59% Analysis Date = 10/07/12 Pct Recovery = 59% Analysis Date = 09/27/12 Pct Recovery = 59% Analysis Date = 09/27/12 Pct Recovery = 59% Analysis Date = 09/16/12 Pct Recovery = 59% Analysis Date = 09/16/12 Pct Recovery = 59% Analysis Date = 09/05/12 Pct Recovery = 59% Analysis Date = 09/05/12 Pct Recovery = 59% Analysis Date = 08/25/12 Pct Recovery = 60% Analysis Date = 08/25/12 Pct Recovery = 60% Analysis Date = 08/14/12 Pct Recovery = 60% Analysis Date = 08/14/12 Pct Recovery = 60% Analysis Date = 08/03/12 Pct Recovery = 60% Analysis Date = 08/03/12 Pct Recovery = 60% Analysis Date = 07/23/12 Pct Recovery = 60% Analysis Date = 07/23/12 Pct Recovery = 60% Analysis Date = 07/13/12 Pct Recovery = 60% Analysis Date = 07/13/12 Pct Recovery = 60% Analysis Date = 07/02/12 Pct Recovery = 61% Analysis Date = 07/02/12 Pct Recovery = 61% Analysis Date = 06/21/12 Pct Recovery = 61% Analysis Date = 06/21/12 Pct Recovery = 61% Analysis Date = 06/10/12 Pct Recovery = 61% Analysis Date = 06/10/12 Pct Recovery = 61% Analysis Date = 05/30/12 Pct Recovery = 61% Analysis Date = 05/30/12 Pct Recovery = 61% Analysis Date = 05/19/12 Pct Recovery = 62% Analysis Date = 05/19/12 Pct Recovery = 62% Analysis Date = 05/08/12 Pct Recovery = 62% Analysis Date = 05/08/12 Pct Recovery = 62% Analysis Date = 04/28/12 Pct Recovery = 62% Analysis Date = 04/28/12 Pct Recovery = 62% Analysis Date = 04/17/12 Pct Recovery = 62% Analysis Date = 04/17/12 Pct Recovery = 62% Analysis Date = 04/06/12 Pct Recovery = 63% Analysis Date = 04/06/12 Pct Recovery = 63% Analysis Date = 03/26/12 Pct Recovery = 63% Analysis Date = 03/26/12 Pct Recovery = 63% Analysis Date = 03/15/12 Pct Recovery = 63% Analysis Date = 03/15/12 Pct Recovery = 63% Analysis Date = 03/04/12 Pct Recovery = 63% Analysis Date = 03/04/12 Pct Recovery = 63% Analysis Date = 02/22/12 Pct Recovery = 64% Analysis Date = 02/22/12 Pct Recovery = 64% Analysis Date = 02/12/12 Pct Recovery = 64% Analysis Date = 02/12/12 Pct Recovery = 64% Analysis Date = 02/01/12 Pct Recovery = 64% Analysis Date = 02/01/12 Pct Recovery = 64% Analysis Date = 01/21/12 Pct Recovery = 64% Analysis Date = 01/21/12 Pct Recovery = 64% Analysis Date = 01/10/12 Pct Recovery = 64% Analysis Date = 01/10/12 Pct Recovery = 64% Analysis Date = 12/30/11 Pct Recovery = 65% Analysis Date = 12/30/11 Pct Recovery = 65% Analysis Date = 12/19/11 Pct Recovery = 65% Analysis Date = 12/19/11 Pct Recovery = 65% Analysis Date = 12/08/11 Pct Recovery = 65% Analysis Date = 12/08/11 Pct Recovery = 65% Analysis Date = 11/28/11 Pct Recovery = 65% Analysis Date = 11/28/11 Pct Recovery = 65% Analysis Date = 11/17/11 Pct Recovery = 66% Analysis Date = 11/17/11 Pct Recovery = 66% Analysis Date = 11/06/11 Pct Recovery = 66% Analysis Date = 11/06/11 Pct Recovery = 66% Analysis Date = 10/26/11 Pct Recovery = 66% Analysis Date = 10/26/11 Pct Recovery = 66% Analysis Date = 10/15/11 Pct Recovery = 66% Analysis Date = 10/15/11 Pct Recovery = 66% Analysis Date = 10/04/11 Pct Recovery = 67% Analysis Date = 10/04/11 Pct Recovery = 67% Analysis Date = 09/23/11 Pct Recovery = 67% Analysis Date = 09/23/11 Pct Recovery = 67% Analysis Date = 09/13/11 Pct Recovery = 67% Analysis Date = 09/13/11 Pct Recovery = 67% Analysis Date = 09/02/11 Pct Recovery = 67% Analysis Date = 09/02/11 Pct Recovery = 67% Analysis Date = 08/22/11 Pct Recovery = 68% Analysis Date = 08/22/11 Pct Recovery = 68% Analysis Date = 08/11/11 Pct Recovery = 68% Analysis Date = 08/11/11 Pct Recovery = 68% Analysis Date = 07/31/11 Pct Recovery = 68% Analysis Date = 07/31/11 Pct Recovery = 68% Analysis Date = 07/20/11 Pct Recovery = 68% Analysis Date = 07/20/11 Pct Recovery = 68% Analysis Date = 07/09/11 Pct Recovery = 69% Analysis Date = 07/09/11 Pct Recovery = 69% Analysis Date = 06/29/11 Pct Recovery = 69% Analysis Date = 06/29/11 Pct Recovery = 69% Analysis Date = 06/18/11 Pct Recovery = 69% Analysis Date = 06/18/11 Pct Recovery = 69% Analysis Date = 06/07/11 Pct Recovery = 69% Analysis Date = 06/07/11 Pct Recovery = 69% Analysis Date = 05/27/11 Pct Recovery = 70% Analysis Date = 05/27/11 Pct Recovery = 70% Analysis Date = 05/16/11 Pct Recovery = 70% Analysis Date = 05/16/11 Pct Recovery = 70% Analysis Date = 05/05/11 Pct Recovery = 70% Analysis Date = 05/05/11 Pct Recovery = 70% Analysis Date = 04/24/11 Pct Recovery = 70% Analysis Date = 04/24/11 Pct Recovery = 70% Analysis Date = 04/14/11 Pct Recovery = 71% Analysis Date = 04/14/11 Pct Recovery = 71% Analysis Date = 04/03/11 Pct Recovery = 71% Analysis Date = 04/03/11 Pct Recovery = 71% Analysis Date = 03/23/11 Pct Recovery = 71% Analysis Date = 03/23/11 Pct Recovery = 71% Analysis Date = 03/12/11 Pct Recovery = 71% Analysis Date = 03/12/11 Pct Recovery = 71% Analysis Date = 03/01/11 Pct Recovery = 72% Analysis Date = 03/01/11 Pct Recovery = 72% Analysis Date = 02/18/11 Pct Recovery = 72% Analysis Date = 02/18/11 Pct Recovery = 72% Analysis Date = 02/08/11 Pct Recovery = 72% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEFLUTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 87 60% 11% 58% 11%
Total 87 60% 11% 58% 11%

Sample Statistics
TEFLUTHRIN

Characteristic N % % Basis
Plotted 87 100% Spiked
Estimated Values 87 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 87 .  
False Negatives 0 0% 0 out of 87
Not Spiked 82 .  
False Positives 1 1% 1 out of 82

BQS OBSP Determination:
TERBUFOS
METHOD: 2033 , TESTIDCODE: 82675GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 70% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 57% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 83% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 89% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 25% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 57% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 65% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 64% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 53% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 98% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 65% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 25% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 76% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 90% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 82% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 57% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 64% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 65% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 63% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 49% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 50% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 81% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 67% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 42% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 67% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 57% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 66% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 55% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 55% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 25% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 73% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 59% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 49% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 45% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 69% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 69% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 53% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 65% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 29% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 37% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 44% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 27% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 79% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 72% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 54% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 70% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 58% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 51% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 79% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 60% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 53% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 33% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 43% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 35% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 36% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 58% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 56% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 46% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 86% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 61% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 50% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 46% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 59% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 55% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 75% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 44% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 42% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 60% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 45% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 51% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 61% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 58% Analysis Date = 01/17/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 66% Analysis Date = 12/27/16 Pct Recovery = 66% Analysis Date = 12/27/16 Pct Recovery = 66% Analysis Date = 12/16/16 Pct Recovery = 66% Analysis Date = 12/16/16 Pct Recovery = 66% Analysis Date = 12/05/16 Pct Recovery = 66% Analysis Date = 12/05/16 Pct Recovery = 66% Analysis Date = 11/24/16 Pct Recovery = 66% Analysis Date = 11/24/16 Pct Recovery = 66% Analysis Date = 11/13/16 Pct Recovery = 65% Analysis Date = 11/13/16 Pct Recovery = 65% Analysis Date = 11/03/16 Pct Recovery = 65% Analysis Date = 11/03/16 Pct Recovery = 65% Analysis Date = 10/23/16 Pct Recovery = 65% Analysis Date = 10/23/16 Pct Recovery = 65% Analysis Date = 10/12/16 Pct Recovery = 65% Analysis Date = 10/12/16 Pct Recovery = 65% Analysis Date = 10/01/16 Pct Recovery = 65% Analysis Date = 10/01/16 Pct Recovery = 65% Analysis Date = 09/20/16 Pct Recovery = 65% Analysis Date = 09/20/16 Pct Recovery = 65% Analysis Date = 09/09/16 Pct Recovery = 65% Analysis Date = 09/09/16 Pct Recovery = 65% Analysis Date = 08/29/16 Pct Recovery = 64% Analysis Date = 08/29/16 Pct Recovery = 64% Analysis Date = 08/19/16 Pct Recovery = 64% Analysis Date = 08/19/16 Pct Recovery = 64% Analysis Date = 08/08/16 Pct Recovery = 64% Analysis Date = 08/08/16 Pct Recovery = 64% Analysis Date = 07/28/16 Pct Recovery = 64% Analysis Date = 07/28/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/06/16 Pct Recovery = 64% Analysis Date = 07/06/16 Pct Recovery = 64% Analysis Date = 06/25/16 Pct Recovery = 63% Analysis Date = 06/25/16 Pct Recovery = 63% Analysis Date = 06/14/16 Pct Recovery = 63% Analysis Date = 06/14/16 Pct Recovery = 63% Analysis Date = 06/04/16 Pct Recovery = 63% Analysis Date = 06/04/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/24/16 Pct Recovery = 63% Analysis Date = 05/13/16 Pct Recovery = 63% Analysis Date = 05/13/16 Pct Recovery = 63% Analysis Date = 05/02/16 Pct Recovery = 63% Analysis Date = 05/02/16 Pct Recovery = 63% Analysis Date = 04/21/16 Pct Recovery = 62% Analysis Date = 04/21/16 Pct Recovery = 62% Analysis Date = 04/10/16 Pct Recovery = 62% Analysis Date = 04/10/16 Pct Recovery = 62% Analysis Date = 03/30/16 Pct Recovery = 62% Analysis Date = 03/30/16 Pct Recovery = 62% Analysis Date = 03/20/16 Pct Recovery = 62% Analysis Date = 03/20/16 Pct Recovery = 62% Analysis Date = 03/09/16 Pct Recovery = 62% Analysis Date = 03/09/16 Pct Recovery = 62% Analysis Date = 02/27/16 Pct Recovery = 62% Analysis Date = 02/27/16 Pct Recovery = 62% Analysis Date = 02/16/16 Pct Recovery = 62% Analysis Date = 02/16/16 Pct Recovery = 62% Analysis Date = 02/05/16 Pct Recovery = 61% Analysis Date = 02/05/16 Pct Recovery = 61% Analysis Date = 01/25/16 Pct Recovery = 61% Analysis Date = 01/25/16 Pct Recovery = 61% Analysis Date = 01/14/16 Pct Recovery = 61% Analysis Date = 01/14/16 Pct Recovery = 61% Analysis Date = 01/04/16 Pct Recovery = 61% Analysis Date = 01/04/16 Pct Recovery = 61% Analysis Date = 12/24/15 Pct Recovery = 61% Analysis Date = 12/24/15 Pct Recovery = 61% Analysis Date = 12/13/15 Pct Recovery = 61% Analysis Date = 12/13/15 Pct Recovery = 61% Analysis Date = 12/02/15 Pct Recovery = 61% Analysis Date = 12/02/15 Pct Recovery = 61% Analysis Date = 11/21/15 Pct Recovery = 60% Analysis Date = 11/21/15 Pct Recovery = 60% Analysis Date = 11/10/15 Pct Recovery = 60% Analysis Date = 11/10/15 Pct Recovery = 60% Analysis Date = 10/30/15 Pct Recovery = 60% Analysis Date = 10/30/15 Pct Recovery = 60% Analysis Date = 10/20/15 Pct Recovery = 60% Analysis Date = 10/20/15 Pct Recovery = 60% Analysis Date = 10/09/15 Pct Recovery = 60% Analysis Date = 10/09/15 Pct Recovery = 60% Analysis Date = 09/28/15 Pct Recovery = 60% Analysis Date = 09/28/15 Pct Recovery = 60% Analysis Date = 09/17/15 Pct Recovery = 60% Analysis Date = 09/17/15 Pct Recovery = 60% Analysis Date = 09/06/15 Pct Recovery = 60% Analysis Date = 09/06/15 Pct Recovery = 60% Analysis Date = 08/26/15 Pct Recovery = 59% Analysis Date = 08/26/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 07/25/15 Pct Recovery = 59% Analysis Date = 07/25/15 Pct Recovery = 59% Analysis Date = 07/14/15 Pct Recovery = 59% Analysis Date = 07/14/15 Pct Recovery = 59% Analysis Date = 07/03/15 Pct Recovery = 59% Analysis Date = 07/03/15 Pct Recovery = 59% Analysis Date = 06/22/15 Pct Recovery = 59% Analysis Date = 06/22/15 Pct Recovery = 59% Analysis Date = 06/11/15 Pct Recovery = 59% Analysis Date = 06/11/15 Pct Recovery = 59% Analysis Date = 05/31/15 Pct Recovery = 58% Analysis Date = 05/31/15 Pct Recovery = 58% Analysis Date = 05/21/15 Pct Recovery = 58% Analysis Date = 05/21/15 Pct Recovery = 58% Analysis Date = 05/10/15 Pct Recovery = 58% Analysis Date = 05/10/15 Pct Recovery = 58% Analysis Date = 04/29/15 Pct Recovery = 58% Analysis Date = 04/29/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/18/15 Pct Recovery = 58% Analysis Date = 04/07/15 Pct Recovery = 58% Analysis Date = 04/07/15 Pct Recovery = 58% Analysis Date = 03/27/15 Pct Recovery = 58% Analysis Date = 03/27/15 Pct Recovery = 58% Analysis Date = 03/16/15 Pct Recovery = 58% Analysis Date = 03/16/15 Pct Recovery = 58% Analysis Date = 03/06/15 Pct Recovery = 57% Analysis Date = 03/06/15 Pct Recovery = 57% Analysis Date = 02/23/15 Pct Recovery = 57% Analysis Date = 02/23/15 Pct Recovery = 57% Analysis Date = 02/12/15 Pct Recovery = 57% Analysis Date = 02/12/15 Pct Recovery = 57% Analysis Date = 02/01/15 Pct Recovery = 57% Analysis Date = 02/01/15 Pct Recovery = 57% Analysis Date = 01/21/15 Pct Recovery = 57% Analysis Date = 01/21/15 Pct Recovery = 57% Analysis Date = 01/10/15 Pct Recovery = 57% Analysis Date = 01/10/15 Pct Recovery = 57% Analysis Date = 12/31/14 Pct Recovery = 57% Analysis Date = 12/31/14 Pct Recovery = 57% Analysis Date = 12/20/14 Pct Recovery = 57% Analysis Date = 12/20/14 Pct Recovery = 57% Analysis Date = 12/09/14 Pct Recovery = 56% Analysis Date = 12/09/14 Pct Recovery = 56% Analysis Date = 11/28/14 Pct Recovery = 56% Analysis Date = 11/28/14 Pct Recovery = 56% Analysis Date = 11/17/14 Pct Recovery = 56% Analysis Date = 11/17/14 Pct Recovery = 56% Analysis Date = 11/06/14 Pct Recovery = 57% Analysis Date = 11/06/14 Pct Recovery = 57% Analysis Date = 10/26/14 Pct Recovery = 57% Analysis Date = 10/26/14 Pct Recovery = 57% Analysis Date = 10/16/14 Pct Recovery = 57% Analysis Date = 10/16/14 Pct Recovery = 57% Analysis Date = 10/05/14 Pct Recovery = 57% Analysis Date = 10/05/14 Pct Recovery = 57% Analysis Date = 09/24/14 Pct Recovery = 57% Analysis Date = 09/24/14 Pct Recovery = 57% Analysis Date = 09/13/14 Pct Recovery = 57% Analysis Date = 09/13/14 Pct Recovery = 57% Analysis Date = 09/02/14 Pct Recovery = 57% Analysis Date = 09/02/14 Pct Recovery = 57% Analysis Date = 08/22/14 Pct Recovery = 57% Analysis Date = 08/22/14 Pct Recovery = 57% Analysis Date = 08/11/14 Pct Recovery = 57% Analysis Date = 08/11/14 Pct Recovery = 57% Analysis Date = 08/01/14 Pct Recovery = 57% Analysis Date = 08/01/14 Pct Recovery = 57% Analysis Date = 07/21/14 Pct Recovery = 57% Analysis Date = 07/21/14 Pct Recovery = 57% Analysis Date = 07/10/14 Pct Recovery = 57% Analysis Date = 07/10/14 Pct Recovery = 57% Analysis Date = 06/29/14 Pct Recovery = 57% Analysis Date = 06/29/14 Pct Recovery = 57% Analysis Date = 06/18/14 Pct Recovery = 58% Analysis Date = 06/18/14 Pct Recovery = 58% Analysis Date = 06/07/14 Pct Recovery = 58% Analysis Date = 06/07/14 Pct Recovery = 58% Analysis Date = 05/27/14 Pct Recovery = 58% Analysis Date = 05/27/14 Pct Recovery = 58% Analysis Date = 05/17/14 Pct Recovery = 58% Analysis Date = 05/17/14 Pct Recovery = 58% Analysis Date = 05/06/14 Pct Recovery = 58% Analysis Date = 05/06/14 Pct Recovery = 58% Analysis Date = 04/25/14 Pct Recovery = 58% Analysis Date = 04/25/14 Pct Recovery = 58% Analysis Date = 04/14/14 Pct Recovery = 58% Analysis Date = 04/14/14 Pct Recovery = 58% Analysis Date = 04/03/14 Pct Recovery = 58% Analysis Date = 04/03/14 Pct Recovery = 58% Analysis Date = 03/23/14 Pct Recovery = 58% Analysis Date = 03/23/14 Pct Recovery = 58% Analysis Date = 03/12/14 Pct Recovery = 58% Analysis Date = 03/12/14 Pct Recovery = 58% Analysis Date = 03/02/14 Pct Recovery = 58% Analysis Date = 03/02/14 Pct Recovery = 58% Analysis Date = 02/19/14 Pct Recovery = 58% Analysis Date = 02/19/14 Pct Recovery = 58% Analysis Date = 02/08/14 Pct Recovery = 58% Analysis Date = 02/08/14 Pct Recovery = 58% Analysis Date = 01/28/14 Pct Recovery = 58% Analysis Date = 01/28/14 Pct Recovery = 58% Analysis Date = 01/17/14 Pct Recovery = 58% Analysis Date = 01/17/14 Pct Recovery = 58% Analysis Date = 01/06/14 Pct Recovery = 58% Analysis Date = 01/06/14 Pct Recovery = 58% Analysis Date = 12/26/13 Pct Recovery = 58% Analysis Date = 12/26/13 Pct Recovery = 58% Analysis Date = 12/16/13 Pct Recovery = 58% Analysis Date = 12/16/13 Pct Recovery = 58% Analysis Date = 12/05/13 Pct Recovery = 58% Analysis Date = 12/05/13 Pct Recovery = 58% Analysis Date = 11/24/13 Pct Recovery = 58% Analysis Date = 11/24/13 Pct Recovery = 58% Analysis Date = 11/13/13 Pct Recovery = 58% Analysis Date = 11/13/13 Pct Recovery = 58% Analysis Date = 11/02/13 Pct Recovery = 58% Analysis Date = 11/02/13 Pct Recovery = 58% Analysis Date = 10/22/13 Pct Recovery = 58% Analysis Date = 10/22/13 Pct Recovery = 58% Analysis Date = 10/11/13 Pct Recovery = 58% Analysis Date = 10/11/13 Pct Recovery = 58% Analysis Date = 10/01/13 Pct Recovery = 58% Analysis Date = 10/01/13 Pct Recovery = 58% Analysis Date = 09/20/13 Pct Recovery = 58% Analysis Date = 09/20/13 Pct Recovery = 58% Analysis Date = 09/09/13 Pct Recovery = 58% Analysis Date = 09/09/13 Pct Recovery = 58% Analysis Date = 08/29/13 Pct Recovery = 58% Analysis Date = 08/29/13 Pct Recovery = 58% Analysis Date = 08/18/13 Pct Recovery = 58% Analysis Date = 08/18/13 Pct Recovery = 58% Analysis Date = 08/07/13 Pct Recovery = 58% Analysis Date = 08/07/13 Pct Recovery = 58% Analysis Date = 07/27/13 Pct Recovery = 58% Analysis Date = 07/27/13 Pct Recovery = 58% Analysis Date = 07/17/13 Pct Recovery = 58% Analysis Date = 07/17/13 Pct Recovery = 58% Analysis Date = 07/06/13 Pct Recovery = 58% Analysis Date = 07/06/13 Pct Recovery = 58% Analysis Date = 06/25/13 Pct Recovery = 58% Analysis Date = 06/25/13 Pct Recovery = 58% Analysis Date = 06/14/13 Pct Recovery = 58% Analysis Date = 06/14/13 Pct Recovery = 58% Analysis Date = 06/03/13 Pct Recovery = 58% Analysis Date = 06/03/13 Pct Recovery = 58% Analysis Date = 05/23/13 Pct Recovery = 58% Analysis Date = 05/23/13 Pct Recovery = 58% Analysis Date = 05/12/13 Pct Recovery = 58% Analysis Date = 05/12/13 Pct Recovery = 58% Analysis Date = 05/02/13 Pct Recovery = 58% Analysis Date = 05/02/13 Pct Recovery = 58% Analysis Date = 04/21/13 Pct Recovery = 58% Analysis Date = 04/21/13 Pct Recovery = 58% Analysis Date = 04/10/13 Pct Recovery = 58% Analysis Date = 04/10/13 Pct Recovery = 58% Analysis Date = 03/30/13 Pct Recovery = 58% Analysis Date = 03/30/13 Pct Recovery = 58% Analysis Date = 03/19/13 Pct Recovery = 58% Analysis Date = 03/19/13 Pct Recovery = 58% Analysis Date = 03/08/13 Pct Recovery = 58% Analysis Date = 03/08/13 Pct Recovery = 58% Analysis Date = 02/25/13 Pct Recovery = 58% Analysis Date = 02/25/13 Pct Recovery = 58% Analysis Date = 02/15/13 Pct Recovery = 58% Analysis Date = 02/15/13 Pct Recovery = 58% Analysis Date = 02/04/13 Pct Recovery = 58% Analysis Date = 02/04/13 Pct Recovery = 58% Analysis Date = 01/24/13 Pct Recovery = 58% Analysis Date = 01/24/13 Pct Recovery = 58% Analysis Date = 01/13/13 Pct Recovery = 58% Analysis Date = 01/13/13 Pct Recovery = 58% Analysis Date = 01/02/13 Pct Recovery = 58% Analysis Date = 01/02/13 Pct Recovery = 58% Analysis Date = 12/22/12 Pct Recovery = 58% Analysis Date = 12/22/12 Pct Recovery = 58% Analysis Date = 12/12/12 Pct Recovery = 57% Analysis Date = 12/12/12 Pct Recovery = 57% Analysis Date = 12/01/12 Pct Recovery = 57% Analysis Date = 12/01/12 Pct Recovery = 57% Analysis Date = 11/20/12 Pct Recovery = 57% Analysis Date = 11/20/12 Pct Recovery = 57% Analysis Date = 11/09/12 Pct Recovery = 57% Analysis Date = 11/09/12 Pct Recovery = 57% Analysis Date = 10/29/12 Pct Recovery = 57% Analysis Date = 10/29/12 Pct Recovery = 57% Analysis Date = 10/18/12 Pct Recovery = 57% Analysis Date = 10/18/12 Pct Recovery = 57% Analysis Date = 10/07/12 Pct Recovery = 57% Analysis Date = 10/07/12 Pct Recovery = 57% Analysis Date = 09/27/12 Pct Recovery = 57% Analysis Date = 09/27/12 Pct Recovery = 57% Analysis Date = 09/16/12 Pct Recovery = 57% Analysis Date = 09/16/12 Pct Recovery = 57% Analysis Date = 09/05/12 Pct Recovery = 57% Analysis Date = 09/05/12 Pct Recovery = 57% Analysis Date = 08/25/12 Pct Recovery = 57% Analysis Date = 08/25/12 Pct Recovery = 57% Analysis Date = 08/14/12 Pct Recovery = 57% Analysis Date = 08/14/12 Pct Recovery = 57% Analysis Date = 08/03/12 Pct Recovery = 57% Analysis Date = 08/03/12 Pct Recovery = 57% Analysis Date = 07/23/12 Pct Recovery = 57% Analysis Date = 07/23/12 Pct Recovery = 57% Analysis Date = 07/13/12 Pct Recovery = 57% Analysis Date = 07/13/12 Pct Recovery = 57% Analysis Date = 07/02/12 Pct Recovery = 57% Analysis Date = 07/02/12 Pct Recovery = 57% Analysis Date = 06/21/12 Pct Recovery = 57% Analysis Date = 06/21/12 Pct Recovery = 57% Analysis Date = 06/10/12 Pct Recovery = 57% Analysis Date = 06/10/12 Pct Recovery = 57% Analysis Date = 05/30/12 Pct Recovery = 57% Analysis Date = 05/30/12 Pct Recovery = 57% Analysis Date = 05/19/12 Pct Recovery = 57% Analysis Date = 05/19/12 Pct Recovery = 57% Analysis Date = 05/08/12 Pct Recovery = 57% Analysis Date = 05/08/12 Pct Recovery = 57% Analysis Date = 04/28/12 Pct Recovery = 58% Analysis Date = 04/28/12 Pct Recovery = 58% Analysis Date = 04/17/12 Pct Recovery = 58% Analysis Date = 04/17/12 Pct Recovery = 58% Analysis Date = 04/06/12 Pct Recovery = 58% Analysis Date = 04/06/12 Pct Recovery = 58% Analysis Date = 03/26/12 Pct Recovery = 58% Analysis Date = 03/26/12 Pct Recovery = 58% Analysis Date = 03/15/12 Pct Recovery = 58% Analysis Date = 03/15/12 Pct Recovery = 58% Analysis Date = 03/04/12 Pct Recovery = 58% Analysis Date = 03/04/12 Pct Recovery = 58% Analysis Date = 02/22/12 Pct Recovery = 58% Analysis Date = 02/22/12 Pct Recovery = 58% Analysis Date = 02/12/12 Pct Recovery = 58% Analysis Date = 02/12/12 Pct Recovery = 58% Analysis Date = 02/01/12 Pct Recovery = 58% Analysis Date = 02/01/12 Pct Recovery = 58% Analysis Date = 01/21/12 Pct Recovery = 58% Analysis Date = 01/21/12 Pct Recovery = 58% Analysis Date = 01/10/12 Pct Recovery = 58% Analysis Date = 01/10/12 Pct Recovery = 58% Analysis Date = 12/30/11 Pct Recovery = 58% Analysis Date = 12/30/11 Pct Recovery = 58% Analysis Date = 12/19/11 Pct Recovery = 58% Analysis Date = 12/19/11 Pct Recovery = 58% Analysis Date = 12/08/11 Pct Recovery = 58% Analysis Date = 12/08/11 Pct Recovery = 58% Analysis Date = 11/28/11 Pct Recovery = 58% Analysis Date = 11/28/11 Pct Recovery = 58% Analysis Date = 11/17/11 Pct Recovery = 59% Analysis Date = 11/17/11 Pct Recovery = 59% Analysis Date = 11/06/11 Pct Recovery = 59% Analysis Date = 11/06/11 Pct Recovery = 59% Analysis Date = 10/26/11 Pct Recovery = 59% Analysis Date = 10/26/11 Pct Recovery = 59% Analysis Date = 10/15/11 Pct Recovery = 59% Analysis Date = 10/15/11 Pct Recovery = 59% Analysis Date = 10/04/11 Pct Recovery = 59% Analysis Date = 10/04/11 Pct Recovery = 59% Analysis Date = 09/23/11 Pct Recovery = 59% Analysis Date = 09/23/11 Pct Recovery = 59% Analysis Date = 09/13/11 Pct Recovery = 59% Analysis Date = 09/13/11 Pct Recovery = 59% Analysis Date = 09/02/11 Pct Recovery = 59% Analysis Date = 09/02/11 Pct Recovery = 59% Analysis Date = 08/22/11 Pct Recovery = 59% Analysis Date = 08/22/11 Pct Recovery = 59% Analysis Date = 08/11/11 Pct Recovery = 59% Analysis Date = 08/11/11 Pct Recovery = 59% Analysis Date = 07/31/11 Pct Recovery = 59% Analysis Date = 07/31/11 Pct Recovery = 59% Analysis Date = 07/20/11 Pct Recovery = 59% Analysis Date = 07/20/11 Pct Recovery = 59% Analysis Date = 07/09/11 Pct Recovery = 59% Analysis Date = 07/09/11 Pct Recovery = 59% Analysis Date = 06/29/11 Pct Recovery = 59% Analysis Date = 06/29/11 Pct Recovery = 59% Analysis Date = 06/18/11 Pct Recovery = 59% Analysis Date = 06/18/11 Pct Recovery = 59% Analysis Date = 06/07/11 Pct Recovery = 59% Analysis Date = 06/07/11 Pct Recovery = 59% Analysis Date = 05/27/11 Pct Recovery = 59% Analysis Date = 05/27/11 Pct Recovery = 59% Analysis Date = 05/16/11 Pct Recovery = 59% Analysis Date = 05/16/11 Pct Recovery = 59% Analysis Date = 05/05/11 Pct Recovery = 59% Analysis Date = 05/05/11 Pct Recovery = 59% Analysis Date = 04/24/11 Pct Recovery = 59% Analysis Date = 04/24/11 Pct Recovery = 59% Analysis Date = 04/14/11 Pct Recovery = 59% Analysis Date = 04/14/11 Pct Recovery = 59% Analysis Date = 04/03/11 Pct Recovery = 60% Analysis Date = 04/03/11 Pct Recovery = 60% Analysis Date = 03/23/11 Pct Recovery = 60% Analysis Date = 03/23/11 Pct Recovery = 60% Analysis Date = 03/12/11 Pct Recovery = 60% Analysis Date = 03/12/11 Pct Recovery = 60% Analysis Date = 03/01/11 Pct Recovery = 60% Analysis Date = 03/01/11 Pct Recovery = 60% Analysis Date = 02/18/11 Pct Recovery = 60% Analysis Date = 02/18/11 Pct Recovery = 60% Analysis Date = 02/08/11 Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 86 59% 16% 59% 14%
Total 86 59% 16% 59% 14%

Sample Statistics
TERBUFOS

Characteristic N % % Basis
Plotted 86 93% Spiked
Estimated Values 1 1% Spiked
Deleted Values 5 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 95 .  
False Negatives 6 7% 6 out of 92
Not Spiked 74 .  
False Positives 1 1% 1 out of 72

BQS OBSP Determination:
TERBUFOS-O-ANALOGUE SULFONE
METHOD: 2033 , TESTIDCODE: 61674GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 89% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 79% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 85% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 49% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 26% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 38% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 53% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 56% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 57% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 76% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 70% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 51% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 69% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 104% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 107% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 138% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 100% Analysis Date = 04/15/14 Pct Recovery = 37% Analysis Date = 04/09/14 Pct Recovery = 38% Analysis Date = 04/09/14 Pct Recovery = 38% Analysis Date = 04/03/14 Pct Recovery = 40% Analysis Date = 04/03/14 Pct Recovery = 40% Analysis Date = 03/28/14 Pct Recovery = 42% Analysis Date = 03/28/14 Pct Recovery = 42% Analysis Date = 03/23/14 Pct Recovery = 44% Analysis Date = 03/23/14 Pct Recovery = 44% Analysis Date = 03/17/14 Pct Recovery = 46% Analysis Date = 03/17/14 Pct Recovery = 46% Analysis Date = 03/11/14 Pct Recovery = 47% Analysis Date = 03/11/14 Pct Recovery = 47% Analysis Date = 03/06/14 Pct Recovery = 49% Analysis Date = 03/06/14 Pct Recovery = 49% Analysis Date = 02/28/14 Pct Recovery = 51% Analysis Date = 02/28/14 Pct Recovery = 51% Analysis Date = 02/22/14 Pct Recovery = 52% Analysis Date = 02/22/14 Pct Recovery = 52% Analysis Date = 02/17/14 Pct Recovery = 54% Analysis Date = 02/17/14 Pct Recovery = 54% Analysis Date = 02/11/14 Pct Recovery = 56% Analysis Date = 02/11/14 Pct Recovery = 56% Analysis Date = 02/05/14 Pct Recovery = 57% Analysis Date = 02/05/14 Pct Recovery = 57% Analysis Date = 01/31/14 Pct Recovery = 59% Analysis Date = 01/31/14 Pct Recovery = 59% Analysis Date = 01/25/14 Pct Recovery = 60% Analysis Date = 01/25/14 Pct Recovery = 60% Analysis Date = 01/19/14 Pct Recovery = 62% Analysis Date = 01/19/14 Pct Recovery = 62% Analysis Date = 01/14/14 Pct Recovery = 64% Analysis Date = 01/14/14 Pct Recovery = 64% Analysis Date = 01/08/14 Pct Recovery = 65% Analysis Date = 01/08/14 Pct Recovery = 65% Analysis Date = 01/02/14 Pct Recovery = 66% Analysis Date = 01/02/14 Pct Recovery = 66% Analysis Date = 12/27/13 Pct Recovery = 66% Analysis Date = 12/27/13 Pct Recovery = 66% Analysis Date = 12/22/13 Pct Recovery = 66% Analysis Date = 12/22/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/10/13 Pct Recovery = 67% Analysis Date = 12/10/13 Pct Recovery = 67% Analysis Date = 12/05/13 Pct Recovery = 67% Analysis Date = 12/05/13 Pct Recovery = 67% Analysis Date = 11/29/13 Pct Recovery = 67% Analysis Date = 11/29/13 Pct Recovery = 67% Analysis Date = 11/23/13 Pct Recovery = 67% Analysis Date = 11/23/13 Pct Recovery = 67% Analysis Date = 11/18/13 Pct Recovery = 67% Analysis Date = 11/18/13 Pct Recovery = 67% Analysis Date = 11/12/13 Pct Recovery = 67% Analysis Date = 11/12/13 Pct Recovery = 67% Analysis Date = 11/06/13 Pct Recovery = 67% Analysis Date = 11/06/13 Pct Recovery = 67% Analysis Date = 11/01/13 Pct Recovery = 66% Analysis Date = 11/01/13 Pct Recovery = 66% Analysis Date = 10/26/13 Pct Recovery = 66% Analysis Date = 10/26/13 Pct Recovery = 66% Analysis Date = 10/20/13 Pct Recovery = 66% Analysis Date = 10/20/13 Pct Recovery = 66% Analysis Date = 10/15/13 Pct Recovery = 66% Analysis Date = 10/15/13 Pct Recovery = 66% Analysis Date = 10/09/13 Pct Recovery = 65% Analysis Date = 10/09/13 Pct Recovery = 65% Analysis Date = 10/03/13 Pct Recovery = 65% Analysis Date = 10/03/13 Pct Recovery = 65% Analysis Date = 09/28/13 Pct Recovery = 65% Analysis Date = 09/28/13 Pct Recovery = 65% Analysis Date = 09/22/13 Pct Recovery = 65% Analysis Date = 09/22/13 Pct Recovery = 65% Analysis Date = 09/16/13 Pct Recovery = 65% Analysis Date = 09/16/13 Pct Recovery = 65% Analysis Date = 09/10/13 Pct Recovery = 65% Analysis Date = 09/10/13 Pct Recovery = 65% Analysis Date = 09/05/13 Pct Recovery = 66% Analysis Date = 09/05/13 Pct Recovery = 66% Analysis Date = 08/30/13 Pct Recovery = 66% Analysis Date = 08/30/13 Pct Recovery = 66% Analysis Date = 08/24/13 Pct Recovery = 67% Analysis Date = 08/24/13 Pct Recovery = 67% Analysis Date = 08/19/13 Pct Recovery = 68% Analysis Date = 08/19/13 Pct Recovery = 68% Analysis Date = 08/13/13 Pct Recovery = 68% Analysis Date = 08/13/13 Pct Recovery = 68% Analysis Date = 08/07/13 Pct Recovery = 69% Analysis Date = 08/07/13 Pct Recovery = 69% Analysis Date = 08/02/13 Pct Recovery = 69% Analysis Date = 08/02/13 Pct Recovery = 69% Analysis Date = 07/27/13 Pct Recovery = 70% Analysis Date = 07/27/13 Pct Recovery = 70% Analysis Date = 07/21/13 Pct Recovery = 70% Analysis Date = 07/21/13 Pct Recovery = 70% Analysis Date = 07/16/13 Pct Recovery = 71% Analysis Date = 07/16/13 Pct Recovery = 71% Analysis Date = 07/10/13 Pct Recovery = 71% Analysis Date = 07/10/13 Pct Recovery = 71% Analysis Date = 07/04/13 Pct Recovery = 72% Analysis Date = 07/04/13 Pct Recovery = 72% Analysis Date = 06/29/13 Pct Recovery = 73% Analysis Date = 06/29/13 Pct Recovery = 73% Analysis Date = 06/23/13 Pct Recovery = 73% Analysis Date = 06/23/13 Pct Recovery = 73% Analysis Date = 06/17/13 Pct Recovery = 74% Analysis Date = 06/17/13 Pct Recovery = 74% Analysis Date = 06/12/13 Pct Recovery = 74% Analysis Date = 06/12/13 Pct Recovery = 74% Analysis Date = 06/06/13 Pct Recovery = 75% Analysis Date = 06/06/13 Pct Recovery = 75% Analysis Date = 05/31/13 Pct Recovery = 75% Analysis Date = 05/31/13 Pct Recovery = 75% Analysis Date = 05/25/13 Pct Recovery = 76% Analysis Date = 05/25/13 Pct Recovery = 76% Analysis Date = 05/20/13 Pct Recovery = 77% Analysis Date = 05/20/13 Pct Recovery = 77% Analysis Date = 05/14/13 Pct Recovery = 77% Analysis Date = 05/14/13 Pct Recovery = 77% Analysis Date = 05/08/13 Pct Recovery = 78% Analysis Date = 05/08/13 Pct Recovery = 78% Analysis Date = 05/03/13 Pct Recovery = 78% Analysis Date = 05/03/13 Pct Recovery = 78% Analysis Date = 04/27/13 Pct Recovery = 79% Analysis Date = 04/27/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/16/13 Pct Recovery = 80% Analysis Date = 04/16/13 Pct Recovery = 80% Analysis Date = 04/10/13 Pct Recovery = 81% Analysis Date = 04/10/13 Pct Recovery = 81% Analysis Date = 04/04/13 Pct Recovery = 81% Analysis Date = 04/04/13 Pct Recovery = 81% Analysis Date = 03/30/13 Pct Recovery = 82% Analysis Date = 03/30/13 Pct Recovery = 82% Analysis Date = 03/24/13 Pct Recovery = 82% Analysis Date = 03/24/13 Pct Recovery = 82% Analysis Date = 03/18/13 Pct Recovery = 83% Analysis Date = 03/18/13 Pct Recovery = 83% Analysis Date = 03/13/13 Pct Recovery = 83% Analysis Date = 03/13/13 Pct Recovery = 83% Analysis Date = 03/07/13 Pct Recovery = 84% Analysis Date = 03/07/13 Pct Recovery = 84% Analysis Date = 03/01/13 Pct Recovery = 85% Analysis Date = 03/01/13 Pct Recovery = 85% Analysis Date = 02/23/13 Pct Recovery = 85% Analysis Date = 02/23/13 Pct Recovery = 85% Analysis Date = 02/18/13 Pct Recovery = 86% Analysis Date = 02/18/13 Pct Recovery = 86% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/06/13 Pct Recovery = 87% Analysis Date = 02/06/13 Pct Recovery = 87% Analysis Date = 02/01/13 Pct Recovery = 88% Analysis Date = 02/01/13 Pct Recovery = 88% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/20/13 Pct Recovery = 90% Analysis Date = 01/20/13 Pct Recovery = 90% Analysis Date = 01/15/13 Pct Recovery = 90% Analysis Date = 01/15/13 Pct Recovery = 90% Analysis Date = 01/09/13 Pct Recovery = 91% Analysis Date = 01/09/13 Pct Recovery = 91% Analysis Date = 01/03/13 Pct Recovery = 92% Analysis Date = 01/03/13 Pct Recovery = 92% Analysis Date = 12/29/12 Pct Recovery = 92% Analysis Date = 12/29/12 Pct Recovery = 92% Analysis Date = 12/23/12 Pct Recovery = 93% Analysis Date = 12/23/12 Pct Recovery = 93% Analysis Date = 12/17/12 Pct Recovery = 94% Analysis Date = 12/17/12 Pct Recovery = 94% Analysis Date = 12/12/12 Pct Recovery = 95% Analysis Date = 12/12/12 Pct Recovery = 95% Analysis Date = 12/06/12 Pct Recovery = 95% Analysis Date = 12/06/12 Pct Recovery = 95% Analysis Date = 11/30/12 Pct Recovery = 96% Analysis Date = 11/30/12 Pct Recovery = 96% Analysis Date = 11/25/12 Pct Recovery = 97% Analysis Date = 11/25/12 Pct Recovery = 97% Analysis Date = 11/19/12 Pct Recovery = 97% Analysis Date = 11/19/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 98% Analysis Date = 11/13/12 Pct Recovery = 98% Analysis Date = 11/07/12 Pct Recovery = 99% Analysis Date = 11/07/12 Pct Recovery = 99% Analysis Date = 11/02/12 Pct Recovery = 99% Analysis Date = 11/02/12 Pct Recovery = 99% Analysis Date = 10/27/12 Pct Recovery = 100% Analysis Date = 10/27/12 Pct Recovery = 100% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/16/12 Pct Recovery = 102% Analysis Date = 10/16/12 Pct Recovery = 102% Analysis Date = 10/10/12 Pct Recovery = 102% Analysis Date = 10/10/12 Pct Recovery = 102% Analysis Date = 10/04/12 Pct Recovery = 103% Analysis Date = 10/04/12 Pct Recovery = 103% Analysis Date = 09/29/12 Pct Recovery = 104% Analysis Date = 09/29/12 Pct Recovery = 104% Analysis Date = 09/23/12 Pct Recovery = 104% Analysis Date = 09/23/12 Pct Recovery = 104% Analysis Date = 09/17/12 Pct Recovery = 105% Analysis Date = 09/17/12 Pct Recovery = 105% Analysis Date = 09/12/12 Pct Recovery = 105% Analysis Date = 09/12/12 Pct Recovery = 105% Analysis Date = 09/06/12 Pct Recovery = 105% Analysis Date = 09/06/12 Pct Recovery = 105% Analysis Date = 08/31/12 Pct Recovery = 104% Analysis Date = 08/31/12 Pct Recovery = 104% Analysis Date = 08/26/12 Pct Recovery = 104% Analysis Date = 08/26/12 Pct Recovery = 104% Analysis Date = 08/20/12 Pct Recovery = 104% Analysis Date = 08/20/12 Pct Recovery = 104% Analysis Date = 08/14/12 Pct Recovery = 103% Analysis Date = 08/14/12 Pct Recovery = 103% Analysis Date = 08/09/12 Pct Recovery = 103% Analysis Date = 08/09/12 Pct Recovery = 103% Analysis Date = 08/03/12 Pct Recovery = 103% Analysis Date = 08/03/12 Pct Recovery = 103% Analysis Date = 07/28/12 Pct Recovery = 102% Analysis Date = 07/28/12 Pct Recovery = 102% Analysis Date = 07/22/12 Pct Recovery = 102% Analysis Date = 07/22/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/11/12 Pct Recovery = 101% Analysis Date = 07/11/12 Pct Recovery = 101% Analysis Date = 07/05/12 Pct Recovery = 101% Analysis Date = 07/05/12 Pct Recovery = 101% Analysis Date = 06/30/12 Pct Recovery = 100% Analysis Date = 06/30/12 Pct Recovery = 100% Analysis Date = 06/24/12 Pct Recovery = 100% Analysis Date = 06/24/12 Pct Recovery = 100% Analysis Date = 06/18/12 Pct Recovery = 100% Analysis Date = 06/18/12 Pct Recovery = 100% Analysis Date = 06/13/12 Pct Recovery = 99% Analysis Date = 06/13/12 Pct Recovery = 99% Analysis Date = 06/07/12 Pct Recovery = 99% Analysis Date = 06/07/12 Pct Recovery = 99% Analysis Date = 06/01/12 Pct Recovery = 99% Analysis Date = 06/01/12 Pct Recovery = 99% Analysis Date = 05/27/12 Pct Recovery = 98% Analysis Date = 05/27/12 Pct Recovery = 98% Analysis Date = 05/21/12 Pct Recovery = 98% Analysis Date = 05/21/12 Pct Recovery = 98% Analysis Date = 05/15/12 Pct Recovery = 98% Analysis Date = 05/15/12 Pct Recovery = 98% Analysis Date = 05/10/12 Pct Recovery = 97% Analysis Date = 05/10/12 Pct Recovery = 97% Analysis Date = 05/04/12 Pct Recovery = 97% Analysis Date = 05/04/12 Pct Recovery = 97% Analysis Date = 04/28/12 Pct Recovery = 97% Analysis Date = 04/28/12 Pct Recovery = 97% Analysis Date = 04/23/12 Pct Recovery = 96% Analysis Date = 04/23/12 Pct Recovery = 96% Analysis Date = 04/17/12 Pct Recovery = 96% Analysis Date = 04/17/12 Pct Recovery = 96% Analysis Date = 04/11/12 Pct Recovery = 96% Analysis Date = 04/11/12 Pct Recovery = 96% Analysis Date = 04/05/12 Pct Recovery = 95% Analysis Date = 04/05/12 Pct Recovery = 95% Analysis Date = 03/31/12 Pct Recovery = 95% Analysis Date = 03/31/12 Pct Recovery = 95% Analysis Date = 03/25/12 Pct Recovery = 95% Analysis Date = 03/25/12 Pct Recovery = 95% Analysis Date = 03/19/12 Pct Recovery = 94% Analysis Date = 03/19/12 Pct Recovery = 94% Analysis Date = 03/14/12 Pct Recovery = 94% Analysis Date = 03/14/12 Pct Recovery = 94% Analysis Date = 03/08/12 Pct Recovery = 93% Analysis Date = 03/08/12 Pct Recovery = 93% Analysis Date = 03/02/12 Pct Recovery = 93% Analysis Date = 03/02/12 Pct Recovery = 93% Analysis Date = 02/26/12 Pct Recovery = 93% Analysis Date = 02/26/12 Pct Recovery = 93% Analysis Date = 02/20/12 Pct Recovery = 92% Analysis Date = 02/20/12 Pct Recovery = 92% Analysis Date = 02/14/12 Pct Recovery = 92% Analysis Date = 02/14/12 Pct Recovery = 92% Analysis Date = 02/09/12 Pct Recovery = 92% Analysis Date = 02/09/12 Pct Recovery = 92% Analysis Date = 02/03/12 Pct Recovery = 91% Analysis Date = 02/03/12 Pct Recovery = 91% Analysis Date = 01/28/12 Pct Recovery = 91% Analysis Date = 01/28/12 Pct Recovery = 91% Analysis Date = 01/23/12 Pct Recovery = 91% Analysis Date = 01/23/12 Pct Recovery = 91% Analysis Date = 01/17/12 Pct Recovery = 90% Analysis Date = 01/17/12 Pct Recovery = 90% Analysis Date = 01/11/12 Pct Recovery = 90% Analysis Date = 01/11/12 Pct Recovery = 90% Analysis Date = 01/05/12 Pct Recovery = 90% Analysis Date = 01/05/12 Pct Recovery = 90% Analysis Date = 12/31/11 Pct Recovery = 89% Analysis Date = 12/31/11 Pct Recovery = 89% Analysis Date = 12/25/11 Pct Recovery = 89% Analysis Date = 12/25/11 Pct Recovery = 89% Analysis Date = 12/19/11 Pct Recovery = 89% Analysis Date = 12/19/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 88% Analysis Date = 12/14/11 Pct Recovery = 88% Analysis Date = 12/08/11 Pct Recovery = 88% Analysis Date = 12/08/11 Pct Recovery = 88% Analysis Date = 12/02/11 Pct Recovery = 88% Analysis Date = 12/02/11 Pct Recovery = 88% Analysis Date = 11/27/11 Pct Recovery = 87% Analysis Date = 11/27/11 Pct Recovery = 87% Analysis Date = 11/21/11 Pct Recovery = 87% Analysis Date = 11/21/11 Pct Recovery = 87% Analysis Date = 11/15/11 Pct Recovery = 87% Analysis Date = 11/15/11 Pct Recovery = 87% Analysis Date = 11/10/11 Pct Recovery = 86% Analysis Date = 11/10/11 Pct Recovery = 86% Analysis Date = 11/04/11 Pct Recovery = 86% Analysis Date = 11/04/11 Pct Recovery = 86% Analysis Date = 10/29/11 Pct Recovery = 85% Analysis Date = 10/29/11 Pct Recovery = 85% Analysis Date = 10/24/11 Pct Recovery = 85% Analysis Date = 10/24/11 Pct Recovery = 85% Analysis Date = 10/18/11 Pct Recovery = 85% Analysis Date = 10/18/11 Pct Recovery = 85% Analysis Date = 10/12/11 Pct Recovery = 84% Analysis Date = 10/12/11 Pct Recovery = 84% Analysis Date = 10/07/11 Pct Recovery = 84% Analysis Date = 10/07/11 Pct Recovery = 84% Analysis Date = 10/01/11 Pct Recovery = 84% Analysis Date = 10/01/11 Pct Recovery = 84% Analysis Date = 09/25/11 Pct Recovery = 83% Analysis Date = 09/25/11 Pct Recovery = 83% Analysis Date = 09/19/11 Pct Recovery = 83% Analysis Date = 09/19/11 Pct Recovery = 83% Analysis Date = 09/14/11 Pct Recovery = 83% Analysis Date = 09/14/11 Pct Recovery = 83% Analysis Date = 09/08/11 Pct Recovery = 82% Analysis Date = 09/08/11 Pct Recovery = 82% Analysis Date = 09/02/11 Pct Recovery = 82% Analysis Date = 09/02/11 Pct Recovery = 82% Analysis Date = 08/28/11 Pct Recovery = 82% Analysis Date = 08/28/11 Pct Recovery = 82% Analysis Date = 08/22/11 Pct Recovery = 81% Analysis Date = 08/22/11 Pct Recovery = 81% Analysis Date = 08/16/11 Pct Recovery = 81% Analysis Date = 08/16/11 Pct Recovery = 81% Analysis Date = 08/11/11 Pct Recovery = 81% Analysis Date = 08/11/11 Pct Recovery = 81% Analysis Date = 08/05/11 Pct Recovery = 80% Analysis Date = 08/05/11 Pct Recovery = 80% Analysis Date = 07/30/11 Pct Recovery = 80% Analysis Date = 07/30/11 Pct Recovery = 80% Analysis Date = 07/25/11 Pct Recovery = 80% Analysis Date = 07/25/11 Pct Recovery = 80% Analysis Date = 07/19/11 Pct Recovery = 79% Analysis Date = 07/19/11 Pct Recovery = 79% Analysis Date = 07/13/11 Pct Recovery = 79% Analysis Date = 07/13/11 Pct Recovery = 79% Analysis Date = 07/08/11 Pct Recovery = 78% Analysis Date = 07/08/11 Pct Recovery = 78% Analysis Date = 07/02/11 Pct Recovery = 78% Analysis Date = 07/02/11 Pct Recovery = 78% Analysis Date = 06/26/11 Pct Recovery = 78% Analysis Date = 06/26/11 Pct Recovery = 78% Analysis Date = 06/21/11 Pct Recovery = 77% Analysis Date = 06/21/11 Pct Recovery = 77% Analysis Date = 06/15/11 Pct Recovery = 77% Analysis Date = 06/15/11 Pct Recovery = 77% Analysis Date = 06/09/11 Pct Recovery = 77% Analysis Date = 06/09/11 Pct Recovery = 77% Analysis Date = 06/03/11 Pct Recovery = 77% Analysis Date = 06/03/11 Pct Recovery = 77% Analysis Date = 05/29/11 Pct Recovery = 77% Analysis Date = 05/29/11 Pct Recovery = 77% Analysis Date = 05/23/11 Pct Recovery = 76% Analysis Date = 05/23/11 Pct Recovery = 76% Analysis Date = 05/17/11 Pct Recovery = 76% Analysis Date = 05/17/11 Pct Recovery = 76% Analysis Date = 05/12/11 Pct Recovery = 76% Analysis Date = 05/12/11 Pct Recovery = 76% Analysis Date = 05/06/11 Pct Recovery = 76% Analysis Date = 05/06/11 Pct Recovery = 76% Analysis Date = 04/30/11 Pct Recovery = 75% Analysis Date = 04/30/11 Pct Recovery = 75% Analysis Date = 04/25/11 Pct Recovery = 75% Analysis Date = 04/25/11 Pct Recovery = 75% Analysis Date = 04/19/11 Pct Recovery = 75% Analysis Date = 04/19/11 Pct Recovery = 75% Analysis Date = 04/13/11 Pct Recovery = 75% Analysis Date = 04/13/11 Pct Recovery = 75% Analysis Date = 04/08/11 Pct Recovery = 75% Analysis Date = 04/08/11 Pct Recovery = 75% Analysis Date = 04/02/11 Pct Recovery = 74% Analysis Date = 04/02/11 Pct Recovery = 74% Analysis Date = 03/27/11 Pct Recovery = 74% Analysis Date = 03/27/11 Pct Recovery = 74% Analysis Date = 03/22/11 Pct Recovery = 74% Analysis Date = 03/22/11 Pct Recovery = 74% Analysis Date = 03/16/11 Pct Recovery = 74% Analysis Date = 03/16/11 Pct Recovery = 74% Analysis Date = 03/10/11 Pct Recovery = 73% Analysis Date = 03/10/11 Pct Recovery = 73% Analysis Date = 03/05/11 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS-O-ANALOGUE SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 112% 17% 105% 15%
>= Reporting Level 19 64% 17% 64% 19%
Total 23 73% 25% 69% 25%

Sample Statistics
TERBUFOS-O-ANALOGUE SULFONE

Characteristic N % % Basis
Plotted 23 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 23 .  
False Negatives 0 0% 0 out of 23
Not Spiked 139 .  
False Positives 0 0% 0 out of 139

BQS OBSP Determination:
TERBUTHYLAZINE
METHOD: 2033 , TESTIDCODE: 04022GCM39
Open Data Set

Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 98% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 113% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 97% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 108% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 108% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 95% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 100% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 103% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 98% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 97% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 79% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 98% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 111% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 104% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 109% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 105% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 105% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 93% Analysis Date = 06/28/12 SpikeMix = Restek A088380: 50 µl Pct Recovery = 104% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 90% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 119% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 88% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 128% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 105% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 84% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 85% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 97% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 89% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 79% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 110% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 96% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 92% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 80% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 95% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 81% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 88% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 86% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 83% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 95% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 81% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 83% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 107% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 110% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 98% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 72% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 87% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 77% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 88% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 114% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 105% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 109% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 127% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 78% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 81% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 90% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 125% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 106% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 102% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 100% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 106% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 101% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 122% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 129% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 116% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 116% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 103% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 82% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 109% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 99% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 74% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 75% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 88% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 77% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 75% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 71% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 76% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 86% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 92% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 84% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 86% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 92% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 104% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 83% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 86% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 97% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Analysis Date = 01/18/17 Pct Recovery = 86% Analysis Date = 01/07/17 Pct Recovery = 86% Analysis Date = 01/07/17 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 86% Analysis Date = 12/27/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/16/16 Pct Recovery = 86% Analysis Date = 12/05/16 Pct Recovery = 86% Analysis Date = 12/05/16 Pct Recovery = 86% Analysis Date = 11/24/16 Pct Recovery = 86% Analysis Date = 11/24/16 Pct Recovery = 86% Analysis Date = 11/14/16 Pct Recovery = 86% Analysis Date = 11/14/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 11/03/16 Pct Recovery = 86% Analysis Date = 10/23/16 Pct Recovery = 86% Analysis Date = 10/23/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 08/08/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/28/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 07/07/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/26/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 05/24/16 Pct Recovery = 86% Analysis Date = 05/24/16 Pct Recovery = 86% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/03/16 Pct Recovery = 87% Analysis Date = 05/03/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/11/16 Pct Recovery = 87% Analysis Date = 04/11/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/31/16 Pct Recovery = 87% Analysis Date = 03/20/16 Pct Recovery = 87% Analysis Date = 03/20/16 Pct Recovery = 87% Analysis Date = 03/10/16 Pct Recovery = 87% Analysis Date = 03/10/16 Pct Recovery = 87% Analysis Date = 02/28/16 Pct Recovery = 87% Analysis Date = 02/28/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/17/16 Pct Recovery = 87% Analysis Date = 02/06/16 Pct Recovery = 87% Analysis Date = 02/06/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/26/16 Pct Recovery = 87% Analysis Date = 01/15/16 Pct Recovery = 87% Analysis Date = 01/15/16 Pct Recovery = 87% Analysis Date = 01/05/16 Pct Recovery = 87% Analysis Date = 01/05/16 Pct Recovery = 87% Analysis Date = 12/25/15 Pct Recovery = 87% Analysis Date = 12/25/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/14/15 Pct Recovery = 87% Analysis Date = 12/03/15 Pct Recovery = 87% Analysis Date = 12/03/15 Pct Recovery = 87% Analysis Date = 11/22/15 Pct Recovery = 87% Analysis Date = 11/22/15 Pct Recovery = 87% Analysis Date = 11/12/15 Pct Recovery = 87% Analysis Date = 11/12/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 11/01/15 Pct Recovery = 87% Analysis Date = 10/21/15 Pct Recovery = 87% Analysis Date = 10/21/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 10/10/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/29/15 Pct Recovery = 87% Analysis Date = 09/18/15 Pct Recovery = 87% Analysis Date = 09/18/15 Pct Recovery = 87% Analysis Date = 09/08/15 Pct Recovery = 87% Analysis Date = 09/08/15 Pct Recovery = 87% Analysis Date = 08/28/15 Pct Recovery = 87% Analysis Date = 08/28/15 Pct Recovery = 87% Analysis Date = 08/17/15 Pct Recovery = 87% Analysis Date = 08/17/15 Pct Recovery = 87% Analysis Date = 08/06/15 Pct Recovery = 88% Analysis Date = 08/06/15 Pct Recovery = 88% Analysis Date = 07/26/15 Pct Recovery = 88% Analysis Date = 07/26/15 Pct Recovery = 88% Analysis Date = 07/15/15 Pct Recovery = 88% Analysis Date = 07/15/15 Pct Recovery = 88% Analysis Date = 07/05/15 Pct Recovery = 88% Analysis Date = 07/05/15 Pct Recovery = 88% Analysis Date = 06/24/15 Pct Recovery = 88% Analysis Date = 06/24/15 Pct Recovery = 88% Analysis Date = 06/13/15 Pct Recovery = 88% Analysis Date = 06/13/15 Pct Recovery = 88% Analysis Date = 06/02/15 Pct Recovery = 88% Analysis Date = 06/02/15 Pct Recovery = 88% Analysis Date = 05/22/15 Pct Recovery = 88% Analysis Date = 05/22/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/11/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 05/01/15 Pct Recovery = 88% Analysis Date = 04/20/15 Pct Recovery = 88% Analysis Date = 04/20/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 04/09/15 Pct Recovery = 88% Analysis Date = 03/29/15 Pct Recovery = 88% Analysis Date = 03/29/15 Pct Recovery = 88% Analysis Date = 03/18/15 Pct Recovery = 88% Analysis Date = 03/18/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 03/08/15 Pct Recovery = 88% Analysis Date = 02/25/15 Pct Recovery = 89% Analysis Date = 02/25/15 Pct Recovery = 89% Analysis Date = 02/14/15 Pct Recovery = 89% Analysis Date = 02/14/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 89% Analysis Date = 02/03/15 Pct Recovery = 89% Analysis Date = 01/23/15 Pct Recovery = 89% Analysis Date = 01/23/15 Pct Recovery = 89% Analysis Date = 01/12/15 Pct Recovery = 89% Analysis Date = 01/12/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 01/02/15 Pct Recovery = 89% Analysis Date = 12/22/14 Pct Recovery = 90% Analysis Date = 12/22/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 12/11/14 Pct Recovery = 90% Analysis Date = 11/30/14 Pct Recovery = 90% Analysis Date = 11/30/14 Pct Recovery = 90% Analysis Date = 11/19/14 Pct Recovery = 90% Analysis Date = 11/19/14 Pct Recovery = 90% Analysis Date = 11/08/14 Pct Recovery = 90% Analysis Date = 11/08/14 Pct Recovery = 90% Analysis Date = 10/29/14 Pct Recovery = 90% Analysis Date = 10/29/14 Pct Recovery = 90% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/07/14 Pct Recovery = 91% Analysis Date = 10/07/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/26/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/05/14 Pct Recovery = 92% Analysis Date = 09/05/14 Pct Recovery = 92% Analysis Date = 08/25/14 Pct Recovery = 92% Analysis Date = 08/25/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/14/14 Pct Recovery = 92% Analysis Date = 08/03/14 Pct Recovery = 93% Analysis Date = 08/03/14 Pct Recovery = 93% Analysis Date = 07/23/14 Pct Recovery = 93% Analysis Date = 07/23/14 Pct Recovery = 93% Analysis Date = 07/12/14 Pct Recovery = 94% Analysis Date = 07/12/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 94% Analysis Date = 07/02/14 Pct Recovery = 94% Analysis Date = 06/21/14 Pct Recovery = 94% Analysis Date = 06/21/14 Pct Recovery = 94% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 95% Analysis Date = 05/08/14 Pct Recovery = 96% Analysis Date = 05/08/14 Pct Recovery = 96% Analysis Date = 04/28/14 Pct Recovery = 96% Analysis Date = 04/28/14 Pct Recovery = 96% Analysis Date = 04/17/14 Pct Recovery = 96% Analysis Date = 04/17/14 Pct Recovery = 96% Analysis Date = 04/06/14 Pct Recovery = 97% Analysis Date = 04/06/14 Pct Recovery = 97% Analysis Date = 03/26/14 Pct Recovery = 97% Analysis Date = 03/26/14 Pct Recovery = 97% Analysis Date = 03/15/14 Pct Recovery = 97% Analysis Date = 03/15/14 Pct Recovery = 97% Analysis Date = 03/04/14 Pct Recovery = 98% Analysis Date = 03/04/14 Pct Recovery = 98% Analysis Date = 02/22/14 Pct Recovery = 98% Analysis Date = 02/22/14 Pct Recovery = 98% Analysis Date = 02/11/14 Pct Recovery = 98% Analysis Date = 02/11/14 Pct Recovery = 98% Analysis Date = 01/31/14 Pct Recovery = 99% Analysis Date = 01/31/14 Pct Recovery = 99% Analysis Date = 01/20/14 Pct Recovery = 99% Analysis Date = 01/20/14 Pct Recovery = 99% Analysis Date = 01/09/14 Pct Recovery = 99% Analysis Date = 01/09/14 Pct Recovery = 99% Analysis Date = 12/30/13 Pct Recovery = 100% Analysis Date = 12/30/13 Pct Recovery = 100% Analysis Date = 12/19/13 Pct Recovery = 100% Analysis Date = 12/19/13 Pct Recovery = 100% Analysis Date = 12/08/13 Pct Recovery = 100% Analysis Date = 12/08/13 Pct Recovery = 100% Analysis Date = 11/27/13 Pct Recovery = 101% Analysis Date = 11/27/13 Pct Recovery = 101% Analysis Date = 11/16/13 Pct Recovery = 101% Analysis Date = 11/16/13 Pct Recovery = 101% Analysis Date = 11/05/13 Pct Recovery = 101% Analysis Date = 11/05/13 Pct Recovery = 101% Analysis Date = 10/26/13 Pct Recovery = 101% Analysis Date = 10/26/13 Pct Recovery = 101% Analysis Date = 10/15/13 Pct Recovery = 102% Analysis Date = 10/15/13 Pct Recovery = 102% Analysis Date = 10/04/13 Pct Recovery = 102% Analysis Date = 10/04/13 Pct Recovery = 102% Analysis Date = 09/23/13 Pct Recovery = 102% Analysis Date = 09/23/13 Pct Recovery = 102% Analysis Date = 09/12/13 Pct Recovery = 102% Analysis Date = 09/12/13 Pct Recovery = 102% Analysis Date = 09/01/13 Pct Recovery = 103% Analysis Date = 09/01/13 Pct Recovery = 103% Analysis Date = 08/22/13 Pct Recovery = 103% Analysis Date = 08/22/13 Pct Recovery = 103% Analysis Date = 08/11/13 Pct Recovery = 103% Analysis Date = 08/11/13 Pct Recovery = 103% Analysis Date = 07/31/13 Pct Recovery = 103% Analysis Date = 07/31/13 Pct Recovery = 103% Analysis Date = 07/20/13 Pct Recovery = 103% Analysis Date = 07/20/13 Pct Recovery = 103% Analysis Date = 07/09/13 Pct Recovery = 103% Analysis Date = 07/09/13 Pct Recovery = 103% Analysis Date = 06/29/13 Pct Recovery = 103% Analysis Date = 06/29/13 Pct Recovery = 103% Analysis Date = 06/18/13 Pct Recovery = 103% Analysis Date = 06/18/13 Pct Recovery = 103% Analysis Date = 06/07/13 Pct Recovery = 103% Analysis Date = 06/07/13 Pct Recovery = 103% Analysis Date = 05/27/13 Pct Recovery = 103% Analysis Date = 05/27/13 Pct Recovery = 103% Analysis Date = 05/16/13 Pct Recovery = 104% Analysis Date = 05/16/13 Pct Recovery = 104% Analysis Date = 05/05/13 Pct Recovery = 104% Analysis Date = 05/05/13 Pct Recovery = 104% Analysis Date = 04/25/13 Pct Recovery = 104% Analysis Date = 04/25/13 Pct Recovery = 104% Analysis Date = 04/14/13 Pct Recovery = 104% Analysis Date = 04/14/13 Pct Recovery = 104% Analysis Date = 04/03/13 Pct Recovery = 104% Analysis Date = 04/03/13 Pct Recovery = 104% Analysis Date = 03/23/13 Pct Recovery = 104% Analysis Date = 03/23/13 Pct Recovery = 104% Analysis Date = 03/12/13 Pct Recovery = 104% Analysis Date = 03/12/13 Pct Recovery = 104% Analysis Date = 03/01/13 Pct Recovery = 103% Analysis Date = 03/01/13 Pct Recovery = 103% Analysis Date = 02/19/13 Pct Recovery = 103% Analysis Date = 02/19/13 Pct Recovery = 103% Analysis Date = 02/08/13 Pct Recovery = 103% Analysis Date = 02/08/13 Pct Recovery = 103% Analysis Date = 01/28/13 Pct Recovery = 103% Analysis Date = 01/28/13 Pct Recovery = 103% Analysis Date = 01/17/13 Pct Recovery = 103% Analysis Date = 01/17/13 Pct Recovery = 103% Analysis Date = 01/06/13 Pct Recovery = 102% Analysis Date = 01/06/13 Pct Recovery = 102% Analysis Date = 12/26/12 Pct Recovery = 102% Analysis Date = 12/26/12 Pct Recovery = 102% Analysis Date = 12/16/12 Pct Recovery = 102% Analysis Date = 12/16/12 Pct Recovery = 102% Analysis Date = 12/05/12 Pct Recovery = 102% Analysis Date = 12/05/12 Pct Recovery = 102% Analysis Date = 11/24/12 Pct Recovery = 102% Analysis Date = 11/24/12 Pct Recovery = 102% Analysis Date = 11/13/12 Pct Recovery = 102% Analysis Date = 11/13/12 Pct Recovery = 102% Analysis Date = 11/02/12 Pct Recovery = 101% Analysis Date = 11/02/12 Pct Recovery = 101% Analysis Date = 10/23/12 Pct Recovery = 101% Analysis Date = 10/23/12 Pct Recovery = 101% Analysis Date = 10/12/12 Pct Recovery = 101% Analysis Date = 10/12/12 Pct Recovery = 101% Analysis Date = 10/01/12 Pct Recovery = 101% Analysis Date = 10/01/12 Pct Recovery = 101% Analysis Date = 09/20/12 Pct Recovery = 101% Analysis Date = 09/20/12 Pct Recovery = 101% Analysis Date = 09/09/12 Pct Recovery = 101% Analysis Date = 09/09/12 Pct Recovery = 101% Analysis Date = 08/29/12 Pct Recovery = 100% Analysis Date = 08/29/12 Pct Recovery = 100% Analysis Date = 08/19/12 Pct Recovery = 100% Analysis Date = 08/19/12 Pct Recovery = 100% Analysis Date = 08/08/12 Pct Recovery = 100% Analysis Date = 08/08/12 Pct Recovery = 100% Analysis Date = 07/28/12 Pct Recovery = 100% Analysis Date = 07/28/12 Pct Recovery = 100% Analysis Date = 07/17/12 Pct Recovery = 100% Analysis Date = 07/17/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 06/25/12 Pct Recovery = 99% Analysis Date = 06/25/12 Pct Recovery = 99% Analysis Date = 06/15/12 Pct Recovery = 99% Analysis Date = 06/15/12 Pct Recovery = 99% Analysis Date = 06/04/12 Pct Recovery = 99% Analysis Date = 06/04/12 Pct Recovery = 99% Analysis Date = 05/24/12 Pct Recovery = 99% Analysis Date = 05/24/12 Pct Recovery = 99% Analysis Date = 05/13/12 Pct Recovery = 99% Analysis Date = 05/13/12 Pct Recovery = 99% Analysis Date = 05/02/12 Pct Recovery = 99% Analysis Date = 05/02/12 Pct Recovery = 99% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/22/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 04/11/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 98% Analysis Date = 03/31/12 Pct Recovery = 98% Analysis Date = 03/20/12 Pct Recovery = 98% Analysis Date = 03/20/12 Pct Recovery = 98% Analysis Date = 03/09/12 Pct Recovery = 98% Analysis Date = 03/09/12 Pct Recovery = 98% Analysis Date = 02/27/12 Pct Recovery = 98% Analysis Date = 02/27/12 Pct Recovery = 98% Analysis Date = 02/17/12 Pct Recovery = 98% Analysis Date = 02/17/12 Pct Recovery = 98% Analysis Date = 02/06/12 Pct Recovery = 97% Analysis Date = 02/06/12 Pct Recovery = 97% Analysis Date = 01/26/12 Pct Recovery = 97% Analysis Date = 01/26/12 Pct Recovery = 97% Analysis Date = 01/15/12 Pct Recovery = 97% Analysis Date = 01/15/12 Pct Recovery = 97% Analysis Date = 01/04/12 Pct Recovery = 97% Analysis Date = 01/04/12 Pct Recovery = 97% Analysis Date = 12/24/11 Pct Recovery = 97% Analysis Date = 12/24/11 Pct Recovery = 97% Analysis Date = 12/14/11 Pct Recovery = 97% Analysis Date = 12/14/11 Pct Recovery = 97% Analysis Date = 12/03/11 Pct Recovery = 97% Analysis Date = 12/03/11 Pct Recovery = 97% Analysis Date = 11/22/11 Pct Recovery = 96% Analysis Date = 11/22/11 Pct Recovery = 96% Analysis Date = 11/11/11 Pct Recovery = 96% Analysis Date = 11/11/11 Pct Recovery = 96% Analysis Date = 10/31/11 Pct Recovery = 96% Analysis Date = 10/31/11 Pct Recovery = 96% Analysis Date = 10/20/11 Pct Recovery = 96% Analysis Date = 10/20/11 Pct Recovery = 96% Analysis Date = 10/10/11 Pct Recovery = 96% Analysis Date = 10/10/11 Pct Recovery = 96% Analysis Date = 09/29/11 Pct Recovery = 96% Analysis Date = 09/29/11 Pct Recovery = 96% Analysis Date = 09/18/11 Pct Recovery = 96% Analysis Date = 09/18/11 Pct Recovery = 96% Analysis Date = 09/07/11 Pct Recovery = 95% Analysis Date = 09/07/11 Pct Recovery = 95% Analysis Date = 08/27/11 Pct Recovery = 95% Analysis Date = 08/27/11 Pct Recovery = 95% Analysis Date = 08/17/11 Pct Recovery = 95% Analysis Date = 08/17/11 Pct Recovery = 95% Analysis Date = 08/06/11 Pct Recovery = 95% Analysis Date = 08/06/11 Pct Recovery = 95% Analysis Date = 07/26/11 Pct Recovery = 95% Analysis Date = 07/26/11 Pct Recovery = 95% Analysis Date = 07/15/11 Pct Recovery = 95% Analysis Date = 07/15/11 Pct Recovery = 95% Analysis Date = 07/04/11 Pct Recovery = 95% Analysis Date = 07/04/11 Pct Recovery = 95% Analysis Date = 06/23/11 Pct Recovery = 95% Analysis Date = 06/23/11 Pct Recovery = 95% Analysis Date = 06/13/11 Pct Recovery = 94% Analysis Date = 06/13/11 Pct Recovery = 94% Analysis Date = 06/02/11 Pct Recovery = 94% Analysis Date = 06/02/11 Pct Recovery = 94% Analysis Date = 05/22/11 Pct Recovery = 94% Analysis Date = 05/22/11 Pct Recovery = 94% Analysis Date = 05/11/11 Pct Recovery = 94% Analysis Date = 05/11/11 Pct Recovery = 94% Analysis Date = 04/30/11 Pct Recovery = 94% Analysis Date = 04/30/11 Pct Recovery = 94% Analysis Date = 04/19/11 Pct Recovery = 94% Analysis Date = 04/19/11 Pct Recovery = 94% Analysis Date = 04/09/11 Pct Recovery = 94% Analysis Date = 04/09/11 Pct Recovery = 94% Analysis Date = 03/29/11 Pct Recovery = 94% Analysis Date = 03/29/11 Pct Recovery = 94% Analysis Date = 03/18/11 Pct Recovery = 94% Analysis Date = 03/18/11 Pct Recovery = 94% Analysis Date = 03/07/11 Pct Recovery = 93% Analysis Date = 03/07/11 Pct Recovery = 93% Analysis Date = 02/24/11 Pct Recovery = 93% Analysis Date = 02/24/11 Pct Recovery = 93% Analysis Date = 02/14/11 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUTHYLAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 95 95% 14% 95% 15%
Total 95 95% 14% 95% 15%

Sample Statistics
TERBUTHYLAZINE

Characteristic N % % Basis
Plotted 95 99% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 96 .  
False Negatives 0 0% 0 out of 96
Not Spiked 73 .  
False Positives 0 0% 0 out of 73

BQS OBSP Determination:
THIOBENCARB
METHOD: 2033 , TESTIDCODE: 82681GCM35
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 100% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 80% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 83% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 81% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 101% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 75% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 99% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 95% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 94% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 110% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 75% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 09/13/11 SpikeMix = ERA 0318-13-02.2: 40 µl Pct Recovery = 63% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 100% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 61% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 81% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 102% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 101% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 90% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 101% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 74% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 78% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 102% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 79% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 78% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 100% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 80% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 75% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 96% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 82% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 94% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 69% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 91% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 55% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 93% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 79% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 64% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 98% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 99% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 94% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 61% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 50% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 61% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 66% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 68% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 93% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 82% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 77% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 96% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 105% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 91% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 89% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 108% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 85% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 104% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 75% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 74% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 77% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 65% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 74% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 71% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 62% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 56% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 64% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 55% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 83% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 100% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 83% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 74% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 89% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 98% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 73% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 95% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 72% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 73% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 53% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 01/17/17 Pct Recovery = 71% Analysis Date = 01/07/17 Pct Recovery = 71% Analysis Date = 01/07/17 Pct Recovery = 71% Analysis Date = 12/27/16 Pct Recovery = 71% Analysis Date = 12/27/16 Pct Recovery = 71% Analysis Date = 12/16/16 Pct Recovery = 71% Analysis Date = 12/16/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 11/24/16 Pct Recovery = 72% Analysis Date = 11/24/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/03/16 Pct Recovery = 72% Analysis Date = 11/03/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 10/01/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 72% Analysis Date = 09/09/16 Pct Recovery = 72% Analysis Date = 09/09/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/29/16 Pct Recovery = 72% Analysis Date = 08/19/16 Pct Recovery = 72% Analysis Date = 08/19/16 Pct Recovery = 72% Analysis Date = 08/08/16 Pct Recovery = 73% Analysis Date = 08/08/16 Pct Recovery = 73% Analysis Date = 07/28/16 Pct Recovery = 73% Analysis Date = 07/28/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 74% Analysis Date = 05/02/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 03/30/16 Pct Recovery = 74% Analysis Date = 03/30/16 Pct Recovery = 74% Analysis Date = 03/20/16 Pct Recovery = 74% Analysis Date = 03/20/16 Pct Recovery = 74% Analysis Date = 03/09/16 Pct Recovery = 74% Analysis Date = 03/09/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/27/16 Pct Recovery = 74% Analysis Date = 02/16/16 Pct Recovery = 74% Analysis Date = 02/16/16 Pct Recovery = 74% Analysis Date = 02/05/16 Pct Recovery = 75% Analysis Date = 02/05/16 Pct Recovery = 75% Analysis Date = 01/25/16 Pct Recovery = 75% Analysis Date = 01/25/16 Pct Recovery = 75% Analysis Date = 01/14/16 Pct Recovery = 75% Analysis Date = 01/14/16 Pct Recovery = 75% Analysis Date = 01/04/16 Pct Recovery = 75% Analysis Date = 01/04/16 Pct Recovery = 75% Analysis Date = 12/24/15 Pct Recovery = 75% Analysis Date = 12/24/15 Pct Recovery = 75% Analysis Date = 12/13/15 Pct Recovery = 75% Analysis Date = 12/13/15 Pct Recovery = 75% Analysis Date = 12/02/15 Pct Recovery = 75% Analysis Date = 12/02/15 Pct Recovery = 75% Analysis Date = 11/21/15 Pct Recovery = 75% Analysis Date = 11/21/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 11/10/15 Pct Recovery = 75% Analysis Date = 10/30/15 Pct Recovery = 75% Analysis Date = 10/30/15 Pct Recovery = 75% Analysis Date = 10/20/15 Pct Recovery = 76% Analysis Date = 10/20/15 Pct Recovery = 76% Analysis Date = 10/09/15 Pct Recovery = 76% Analysis Date = 10/09/15 Pct Recovery = 76% Analysis Date = 09/28/15 Pct Recovery = 76% Analysis Date = 09/28/15 Pct Recovery = 76% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/17/15 Pct Recovery = 76% Analysis Date = 09/06/15 Pct Recovery = 76% Analysis Date = 09/06/15 Pct Recovery = 76% Analysis Date = 08/26/15 Pct Recovery = 76% Analysis Date = 08/26/15 Pct Recovery = 76% Analysis Date = 08/15/15 Pct Recovery = 76% Analysis Date = 08/15/15 Pct Recovery = 76% Analysis Date = 08/05/15 Pct Recovery = 76% Analysis Date = 08/05/15 Pct Recovery = 76% Analysis Date = 07/25/15 Pct Recovery = 76% Analysis Date = 07/25/15 Pct Recovery = 76% Analysis Date = 07/14/15 Pct Recovery = 77% Analysis Date = 07/14/15 Pct Recovery = 77% Analysis Date = 07/03/15 Pct Recovery = 77% Analysis Date = 07/03/15 Pct Recovery = 77% Analysis Date = 06/22/15 Pct Recovery = 77% Analysis Date = 06/22/15 Pct Recovery = 77% Analysis Date = 06/11/15 Pct Recovery = 77% Analysis Date = 06/11/15 Pct Recovery = 77% Analysis Date = 05/31/15 Pct Recovery = 77% Analysis Date = 05/31/15 Pct Recovery = 77% Analysis Date = 05/21/15 Pct Recovery = 77% Analysis Date = 05/21/15 Pct Recovery = 77% Analysis Date = 05/10/15 Pct Recovery = 77% Analysis Date = 05/10/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/07/15 Pct Recovery = 78% Analysis Date = 04/07/15 Pct Recovery = 78% Analysis Date = 03/27/15 Pct Recovery = 78% Analysis Date = 03/27/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 79% Analysis Date = 02/23/15 Pct Recovery = 79% Analysis Date = 02/12/15 Pct Recovery = 79% Analysis Date = 02/12/15 Pct Recovery = 79% Analysis Date = 02/01/15 Pct Recovery = 79% Analysis Date = 02/01/15 Pct Recovery = 79% Analysis Date = 01/21/15 Pct Recovery = 79% Analysis Date = 01/21/15 Pct Recovery = 79% Analysis Date = 01/10/15 Pct Recovery = 79% Analysis Date = 01/10/15 Pct Recovery = 79% Analysis Date = 12/31/14 Pct Recovery = 79% Analysis Date = 12/31/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 79% Analysis Date = 12/20/14 Pct Recovery = 79% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 12/09/14 Pct Recovery = 80% Analysis Date = 11/28/14 Pct Recovery = 80% Analysis Date = 11/28/14 Pct Recovery = 80% Analysis Date = 11/17/14 Pct Recovery = 80% Analysis Date = 11/17/14 Pct Recovery = 80% Analysis Date = 11/06/14 Pct Recovery = 80% Analysis Date = 11/06/14 Pct Recovery = 80% Analysis Date = 10/26/14 Pct Recovery = 80% Analysis Date = 10/26/14 Pct Recovery = 80% Analysis Date = 10/16/14 Pct Recovery = 80% Analysis Date = 10/16/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 10/05/14 Pct Recovery = 80% Analysis Date = 09/24/14 Pct Recovery = 81% Analysis Date = 09/24/14 Pct Recovery = 81% Analysis Date = 09/13/14 Pct Recovery = 81% Analysis Date = 09/13/14 Pct Recovery = 81% Analysis Date = 09/02/14 Pct Recovery = 81% Analysis Date = 09/02/14 Pct Recovery = 81% Analysis Date = 08/22/14 Pct Recovery = 81% Analysis Date = 08/22/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/11/14 Pct Recovery = 81% Analysis Date = 08/01/14 Pct Recovery = 81% Analysis Date = 08/01/14 Pct Recovery = 81% Analysis Date = 07/21/14 Pct Recovery = 81% Analysis Date = 07/21/14 Pct Recovery = 81% Analysis Date = 07/10/14 Pct Recovery = 81% Analysis Date = 07/10/14 Pct Recovery = 81% Analysis Date = 06/29/14 Pct Recovery = 82% Analysis Date = 06/29/14 Pct Recovery = 82% Analysis Date = 06/18/14 Pct Recovery = 82% Analysis Date = 06/18/14 Pct Recovery = 82% Analysis Date = 06/07/14 Pct Recovery = 82% Analysis Date = 06/07/14 Pct Recovery = 82% Analysis Date = 05/27/14 Pct Recovery = 82% Analysis Date = 05/27/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/17/14 Pct Recovery = 82% Analysis Date = 05/06/14 Pct Recovery = 82% Analysis Date = 05/06/14 Pct Recovery = 82% Analysis Date = 04/25/14 Pct Recovery = 82% Analysis Date = 04/25/14 Pct Recovery = 82% Analysis Date = 04/14/14 Pct Recovery = 82% Analysis Date = 04/14/14 Pct Recovery = 82% Analysis Date = 04/03/14 Pct Recovery = 82% Analysis Date = 04/03/14 Pct Recovery = 82% Analysis Date = 03/23/14 Pct Recovery = 82% Analysis Date = 03/23/14 Pct Recovery = 82% Analysis Date = 03/12/14 Pct Recovery = 82% Analysis Date = 03/12/14 Pct Recovery = 82% Analysis Date = 03/02/14 Pct Recovery = 82% Analysis Date = 03/02/14 Pct Recovery = 82% Analysis Date = 02/19/14 Pct Recovery = 82% Analysis Date = 02/19/14 Pct Recovery = 82% Analysis Date = 02/08/14 Pct Recovery = 82% Analysis Date = 02/08/14 Pct Recovery = 82% Analysis Date = 01/28/14 Pct Recovery = 82% Analysis Date = 01/28/14 Pct Recovery = 82% Analysis Date = 01/17/14 Pct Recovery = 82% Analysis Date = 01/17/14 Pct Recovery = 82% Analysis Date = 01/06/14 Pct Recovery = 82% Analysis Date = 01/06/14 Pct Recovery = 82% Analysis Date = 12/26/13 Pct Recovery = 83% Analysis Date = 12/26/13 Pct Recovery = 83% Analysis Date = 12/16/13 Pct Recovery = 83% Analysis Date = 12/16/13 Pct Recovery = 83% Analysis Date = 12/05/13 Pct Recovery = 83% Analysis Date = 12/05/13 Pct Recovery = 83% Analysis Date = 11/24/13 Pct Recovery = 83% Analysis Date = 11/24/13 Pct Recovery = 83% Analysis Date = 11/13/13 Pct Recovery = 83% Analysis Date = 11/13/13 Pct Recovery = 83% Analysis Date = 11/02/13 Pct Recovery = 83% Analysis Date = 11/02/13 Pct Recovery = 83% Analysis Date = 10/22/13 Pct Recovery = 83% Analysis Date = 10/22/13 Pct Recovery = 83% Analysis Date = 10/11/13 Pct Recovery = 83% Analysis Date = 10/11/13 Pct Recovery = 83% Analysis Date = 10/01/13 Pct Recovery = 83% Analysis Date = 10/01/13 Pct Recovery = 83% Analysis Date = 09/20/13 Pct Recovery = 83% Analysis Date = 09/20/13 Pct Recovery = 83% Analysis Date = 09/09/13 Pct Recovery = 83% Analysis Date = 09/09/13 Pct Recovery = 83% Analysis Date = 08/29/13 Pct Recovery = 83% Analysis Date = 08/29/13 Pct Recovery = 83% Analysis Date = 08/18/13 Pct Recovery = 83% Analysis Date = 08/18/13 Pct Recovery = 83% Analysis Date = 08/07/13 Pct Recovery = 84% Analysis Date = 08/07/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/17/13 Pct Recovery = 84% Analysis Date = 07/17/13 Pct Recovery = 84% Analysis Date = 07/06/13 Pct Recovery = 84% Analysis Date = 07/06/13 Pct Recovery = 84% Analysis Date = 06/25/13 Pct Recovery = 84% Analysis Date = 06/25/13 Pct Recovery = 84% Analysis Date = 06/14/13 Pct Recovery = 84% Analysis Date = 06/14/13 Pct Recovery = 84% Analysis Date = 06/03/13 Pct Recovery = 84% Analysis Date = 06/03/13 Pct Recovery = 84% Analysis Date = 05/23/13 Pct Recovery = 84% Analysis Date = 05/23/13 Pct Recovery = 84% Analysis Date = 05/12/13 Pct Recovery = 84% Analysis Date = 05/12/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 05/02/13 Pct Recovery = 84% Analysis Date = 04/21/13 Pct Recovery = 84% Analysis Date = 04/21/13 Pct Recovery = 84% Analysis Date = 04/10/13 Pct Recovery = 85% Analysis Date = 04/10/13 Pct Recovery = 85% Analysis Date = 03/30/13 Pct Recovery = 85% Analysis Date = 03/30/13 Pct Recovery = 85% Analysis Date = 03/19/13 Pct Recovery = 85% Analysis Date = 03/19/13 Pct Recovery = 85% Analysis Date = 03/08/13 Pct Recovery = 85% Analysis Date = 03/08/13 Pct Recovery = 85% Analysis Date = 02/25/13 Pct Recovery = 85% Analysis Date = 02/25/13 Pct Recovery = 85% Analysis Date = 02/15/13 Pct Recovery = 85% Analysis Date = 02/15/13 Pct Recovery = 85% Analysis Date = 02/04/13 Pct Recovery = 85% Analysis Date = 02/04/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/24/13 Pct Recovery = 85% Analysis Date = 01/13/13 Pct Recovery = 85% Analysis Date = 01/13/13 Pct Recovery = 85% Analysis Date = 01/02/13 Pct Recovery = 85% Analysis Date = 01/02/13 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/22/12 Pct Recovery = 85% Analysis Date = 12/12/12 Pct Recovery = 85% Analysis Date = 12/12/12 Pct Recovery = 85% Analysis Date = 12/01/12 Pct Recovery = 86% Analysis Date = 12/01/12 Pct Recovery = 86% Analysis Date = 11/20/12 Pct Recovery = 86% Analysis Date = 11/20/12 Pct Recovery = 86% Analysis Date = 11/09/12 Pct Recovery = 86% Analysis Date = 11/09/12 Pct Recovery = 86% Analysis Date = 10/29/12 Pct Recovery = 86% Analysis Date = 10/29/12 Pct Recovery = 86% Analysis Date = 10/18/12 Pct Recovery = 86% Analysis Date = 10/18/12 Pct Recovery = 86% Analysis Date = 10/07/12 Pct Recovery = 86% Analysis Date = 10/07/12 Pct Recovery = 86% Analysis Date = 09/27/12 Pct Recovery = 86% Analysis Date = 09/27/12 Pct Recovery = 86% Analysis Date = 09/16/12 Pct Recovery = 86% Analysis Date = 09/16/12 Pct Recovery = 86% Analysis Date = 09/05/12 Pct Recovery = 86% Analysis Date = 09/05/12 Pct Recovery = 86% Analysis Date = 08/25/12 Pct Recovery = 86% Analysis Date = 08/25/12 Pct Recovery = 86% Analysis Date = 08/14/12 Pct Recovery = 86% Analysis Date = 08/14/12 Pct Recovery = 86% Analysis Date = 08/03/12 Pct Recovery = 86% Analysis Date = 08/03/12 Pct Recovery = 86% Analysis Date = 07/23/12 Pct Recovery = 86% Analysis Date = 07/23/12 Pct Recovery = 86% Analysis Date = 07/13/12 Pct Recovery = 86% Analysis Date = 07/13/12 Pct Recovery = 86% Analysis Date = 07/02/12 Pct Recovery = 86% Analysis Date = 07/02/12 Pct Recovery = 86% Analysis Date = 06/21/12 Pct Recovery = 86% Analysis Date = 06/21/12 Pct Recovery = 86% Analysis Date = 06/10/12 Pct Recovery = 86% Analysis Date = 06/10/12 Pct Recovery = 86% Analysis Date = 05/30/12 Pct Recovery = 86% Analysis Date = 05/30/12 Pct Recovery = 86% Analysis Date = 05/19/12 Pct Recovery = 86% Analysis Date = 05/19/12 Pct Recovery = 86% Analysis Date = 05/08/12 Pct Recovery = 86% Analysis Date = 05/08/12 Pct Recovery = 86% Analysis Date = 04/28/12 Pct Recovery = 86% Analysis Date = 04/28/12 Pct Recovery = 86% Analysis Date = 04/17/12 Pct Recovery = 86% Analysis Date = 04/17/12 Pct Recovery = 86% Analysis Date = 04/06/12 Pct Recovery = 86% Analysis Date = 04/06/12 Pct Recovery = 86% Analysis Date = 03/26/12 Pct Recovery = 86% Analysis Date = 03/26/12 Pct Recovery = 86% Analysis Date = 03/15/12 Pct Recovery = 86% Analysis Date = 03/15/12 Pct Recovery = 86% Analysis Date = 03/04/12 Pct Recovery = 86% Analysis Date = 03/04/12 Pct Recovery = 86% Analysis Date = 02/22/12 Pct Recovery = 86% Analysis Date = 02/22/12 Pct Recovery = 86% Analysis Date = 02/12/12 Pct Recovery = 87% Analysis Date = 02/12/12 Pct Recovery = 87% Analysis Date = 02/01/12 Pct Recovery = 87% Analysis Date = 02/01/12 Pct Recovery = 87% Analysis Date = 01/21/12 Pct Recovery = 87% Analysis Date = 01/21/12 Pct Recovery = 87% Analysis Date = 01/10/12 Pct Recovery = 87% Analysis Date = 01/10/12 Pct Recovery = 87% Analysis Date = 12/30/11 Pct Recovery = 87% Analysis Date = 12/30/11 Pct Recovery = 87% Analysis Date = 12/19/11 Pct Recovery = 87% Analysis Date = 12/19/11 Pct Recovery = 87% Analysis Date = 12/08/11 Pct Recovery = 87% Analysis Date = 12/08/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 87% Analysis Date = 11/28/11 Pct Recovery = 87% Analysis Date = 11/17/11 Pct Recovery = 87% Analysis Date = 11/17/11 Pct Recovery = 87% Analysis Date = 11/06/11 Pct Recovery = 87% Analysis Date = 11/06/11 Pct Recovery = 87% Analysis Date = 10/26/11 Pct Recovery = 87% Analysis Date = 10/26/11 Pct Recovery = 87% Analysis Date = 10/15/11 Pct Recovery = 87% Analysis Date = 10/15/11 Pct Recovery = 87% Analysis Date = 10/04/11 Pct Recovery = 87% Analysis Date = 10/04/11 Pct Recovery = 87% Analysis Date = 09/23/11 Pct Recovery = 87% Analysis Date = 09/23/11 Pct Recovery = 87% Analysis Date = 09/13/11 Pct Recovery = 87% Analysis Date = 09/13/11 Pct Recovery = 87% Analysis Date = 09/02/11 Pct Recovery = 87% Analysis Date = 09/02/11 Pct Recovery = 87% Analysis Date = 08/22/11 Pct Recovery = 87% Analysis Date = 08/22/11 Pct Recovery = 87% Analysis Date = 08/11/11 Pct Recovery = 87% Analysis Date = 08/11/11 Pct Recovery = 87% Analysis Date = 07/31/11 Pct Recovery = 87% Analysis Date = 07/31/11 Pct Recovery = 87% Analysis Date = 07/20/11 Pct Recovery = 87% Analysis Date = 07/20/11 Pct Recovery = 87% Analysis Date = 07/09/11 Pct Recovery = 87% Analysis Date = 07/09/11 Pct Recovery = 87% Analysis Date = 06/29/11 Pct Recovery = 87% Analysis Date = 06/29/11 Pct Recovery = 87% Analysis Date = 06/18/11 Pct Recovery = 87% Analysis Date = 06/18/11 Pct Recovery = 87% Analysis Date = 06/07/11 Pct Recovery = 87% Analysis Date = 06/07/11 Pct Recovery = 87% Analysis Date = 05/27/11 Pct Recovery = 87% Analysis Date = 05/27/11 Pct Recovery = 87% Analysis Date = 05/16/11 Pct Recovery = 87% Analysis Date = 05/16/11 Pct Recovery = 87% Analysis Date = 05/05/11 Pct Recovery = 87% Analysis Date = 05/05/11 Pct Recovery = 87% Analysis Date = 04/24/11 Pct Recovery = 87% Analysis Date = 04/24/11 Pct Recovery = 87% Analysis Date = 04/14/11 Pct Recovery = 87% Analysis Date = 04/14/11 Pct Recovery = 87% Analysis Date = 04/03/11 Pct Recovery = 87% Analysis Date = 04/03/11 Pct Recovery = 87% Analysis Date = 03/23/11 Pct Recovery = 87% Analysis Date = 03/23/11 Pct Recovery = 87% Analysis Date = 03/12/11 Pct Recovery = 87% Analysis Date = 03/12/11 Pct Recovery = 87% Analysis Date = 03/01/11 Pct Recovery = 87% Analysis Date = 03/01/11 Pct Recovery = 87% Analysis Date = 02/18/11 Pct Recovery = 87% Analysis Date = 02/18/11 Pct Recovery = 87% Analysis Date = 02/08/11 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
THIOBENCARB

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 82% 15% 81% 17%
Total 89 82% 15% 81% 17%

Sample Statistics
THIOBENCARB

Characteristic N % % Basis
Plotted 89 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 89 .  
False Negatives 0 0% 0 out of 89
Not Spiked 80 .  
False Positives 3 4% 3 out of 80

BQS OBSP Determination:
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))
METHOD: 2033 , TESTIDCODE: 61610GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 53% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 50% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 47% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 75% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 60% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 53% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 50% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 58% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 53% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 53% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 30% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 41% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 60% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 52% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 39% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 59% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 58% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 50% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 51% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 45% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 50% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 60% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 64% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 50% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 57% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 78% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 61% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 62% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 59% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 68% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 62% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 63% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 71% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 57% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 50% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 58% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 66% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 69% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 49% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 77% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 59% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 81% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 47% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 61% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 60% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 56% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 92% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 85% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 88% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 60% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 61% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 65% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 70% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 58% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 57% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 64% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 61% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 66% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 81% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 75% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 70% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 67% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 77% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 62% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 85% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 61% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 74% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 80% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 92% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 99% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 64% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 86% Analysis Date = 12/20/16 Pct Recovery = 69% Analysis Date = 12/09/16 Pct Recovery = 69% Analysis Date = 12/09/16 Pct Recovery = 69% Analysis Date = 11/28/16 Pct Recovery = 69% Analysis Date = 11/28/16 Pct Recovery = 69% Analysis Date = 11/17/16 Pct Recovery = 69% Analysis Date = 11/17/16 Pct Recovery = 69% Analysis Date = 11/07/16 Pct Recovery = 69% Analysis Date = 11/07/16 Pct Recovery = 69% Analysis Date = 10/27/16 Pct Recovery = 69% Analysis Date = 10/27/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 09/25/16 Pct Recovery = 69% Analysis Date = 09/25/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/14/16 Pct Recovery = 69% Analysis Date = 09/03/16 Pct Recovery = 69% Analysis Date = 09/03/16 Pct Recovery = 69% Analysis Date = 08/24/16 Pct Recovery = 69% Analysis Date = 08/24/16 Pct Recovery = 69% Analysis Date = 08/13/16 Pct Recovery = 69% Analysis Date = 08/13/16 Pct Recovery = 69% Analysis Date = 08/02/16 Pct Recovery = 69% Analysis Date = 08/02/16 Pct Recovery = 69% Analysis Date = 07/23/16 Pct Recovery = 69% Analysis Date = 07/23/16 Pct Recovery = 69% Analysis Date = 07/12/16 Pct Recovery = 69% Analysis Date = 07/12/16 Pct Recovery = 69% Analysis Date = 07/01/16 Pct Recovery = 69% Analysis Date = 07/01/16 Pct Recovery = 69% Analysis Date = 06/21/16 Pct Recovery = 69% Analysis Date = 06/21/16 Pct Recovery = 69% Analysis Date = 06/10/16 Pct Recovery = 69% Analysis Date = 06/10/16 Pct Recovery = 69% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/17/16 Pct Recovery = 69% Analysis Date = 04/17/16 Pct Recovery = 69% Analysis Date = 04/07/16 Pct Recovery = 69% Analysis Date = 04/07/16 Pct Recovery = 69% Analysis Date = 03/27/16 Pct Recovery = 69% Analysis Date = 03/27/16 Pct Recovery = 69% Analysis Date = 03/16/16 Pct Recovery = 69% Analysis Date = 03/16/16 Pct Recovery = 69% Analysis Date = 03/05/16 Pct Recovery = 69% Analysis Date = 03/05/16 Pct Recovery = 69% Analysis Date = 02/24/16 Pct Recovery = 69% Analysis Date = 02/24/16 Pct Recovery = 69% Analysis Date = 02/13/16 Pct Recovery = 69% Analysis Date = 02/13/16 Pct Recovery = 69% Analysis Date = 02/02/16 Pct Recovery = 69% Analysis Date = 02/02/16 Pct Recovery = 69% Analysis Date = 01/23/16 Pct Recovery = 69% Analysis Date = 01/23/16 Pct Recovery = 69% Analysis Date = 01/12/16 Pct Recovery = 69% Analysis Date = 01/12/16 Pct Recovery = 69% Analysis Date = 01/01/16 Pct Recovery = 69% Analysis Date = 01/01/16 Pct Recovery = 69% Analysis Date = 12/22/15 Pct Recovery = 69% Analysis Date = 12/22/15 Pct Recovery = 69% Analysis Date = 12/11/15 Pct Recovery = 69% Analysis Date = 12/11/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/30/15 Pct Recovery = 69% Analysis Date = 11/19/15 Pct Recovery = 69% Analysis Date = 11/19/15 Pct Recovery = 69% Analysis Date = 11/09/15 Pct Recovery = 69% Analysis Date = 11/09/15 Pct Recovery = 69% Analysis Date = 10/29/15 Pct Recovery = 69% Analysis Date = 10/29/15 Pct Recovery = 69% Analysis Date = 10/18/15 Pct Recovery = 69% Analysis Date = 10/18/15 Pct Recovery = 69% Analysis Date = 10/08/15 Pct Recovery = 69% Analysis Date = 10/08/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/27/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/05/15 Pct Recovery = 69% Analysis Date = 09/05/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/26/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 69% Analysis Date = 08/15/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 69% Analysis Date = 08/04/15 Pct Recovery = 69% Analysis Date = 07/25/15 Pct Recovery = 69% Analysis Date = 07/25/15 Pct Recovery = 69% Analysis Date = 07/14/15 Pct Recovery = 69% Analysis Date = 07/14/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 69% Analysis Date = 06/23/15 Pct Recovery = 69% Analysis Date = 06/23/15 Pct Recovery = 69% Analysis Date = 06/12/15 Pct Recovery = 69% Analysis Date = 06/12/15 Pct Recovery = 69% Analysis Date = 06/01/15 Pct Recovery = 69% Analysis Date = 06/01/15 Pct Recovery = 69% Analysis Date = 05/21/15 Pct Recovery = 69% Analysis Date = 05/21/15 Pct Recovery = 69% Analysis Date = 05/11/15 Pct Recovery = 69% Analysis Date = 05/11/15 Pct Recovery = 69% Analysis Date = 04/30/15 Pct Recovery = 69% Analysis Date = 04/30/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/19/15 Pct Recovery = 69% Analysis Date = 04/09/15 Pct Recovery = 69% Analysis Date = 04/09/15 Pct Recovery = 69% Analysis Date = 03/29/15 Pct Recovery = 69% Analysis Date = 03/29/15 Pct Recovery = 69% Analysis Date = 03/18/15 Pct Recovery = 69% Analysis Date = 03/18/15 Pct Recovery = 69% Analysis Date = 03/07/15 Pct Recovery = 69% Analysis Date = 03/07/15 Pct Recovery = 69% Analysis Date = 02/25/15 Pct Recovery = 69% Analysis Date = 02/25/15 Pct Recovery = 69% Analysis Date = 02/14/15 Pct Recovery = 69% Analysis Date = 02/14/15 Pct Recovery = 69% Analysis Date = 02/03/15 Pct Recovery = 69% Analysis Date = 02/03/15 Pct Recovery = 69% Analysis Date = 01/24/15 Pct Recovery = 69% Analysis Date = 01/24/15 Pct Recovery = 69% Analysis Date = 01/13/15 Pct Recovery = 69% Analysis Date = 01/13/15 Pct Recovery = 69% Analysis Date = 01/02/15 Pct Recovery = 69% Analysis Date = 01/02/15 Pct Recovery = 69% Analysis Date = 12/23/14 Pct Recovery = 69% Analysis Date = 12/23/14 Pct Recovery = 69% Analysis Date = 12/12/14 Pct Recovery = 69% Analysis Date = 12/12/14 Pct Recovery = 69% Analysis Date = 12/01/14 Pct Recovery = 69% Analysis Date = 12/01/14 Pct Recovery = 69% Analysis Date = 11/20/14 Pct Recovery = 69% Analysis Date = 11/20/14 Pct Recovery = 69% Analysis Date = 11/10/14 Pct Recovery = 69% Analysis Date = 11/10/14 Pct Recovery = 69% Analysis Date = 10/30/14 Pct Recovery = 69% Analysis Date = 10/30/14 Pct Recovery = 69% Analysis Date = 10/19/14 Pct Recovery = 69% Analysis Date = 10/19/14 Pct Recovery = 69% Analysis Date = 10/09/14 Pct Recovery = 69% Analysis Date = 10/09/14 Pct Recovery = 69% Analysis Date = 09/28/14 Pct Recovery = 69% Analysis Date = 09/28/14 Pct Recovery = 69% Analysis Date = 09/17/14 Pct Recovery = 69% Analysis Date = 09/17/14 Pct Recovery = 69% Analysis Date = 09/07/14 Pct Recovery = 69% Analysis Date = 09/07/14 Pct Recovery = 69% Analysis Date = 08/27/14 Pct Recovery = 69% Analysis Date = 08/27/14 Pct Recovery = 69% Analysis Date = 08/16/14 Pct Recovery = 69% Analysis Date = 08/16/14 Pct Recovery = 69% Analysis Date = 08/05/14 Pct Recovery = 69% Analysis Date = 08/05/14 Pct Recovery = 69% Analysis Date = 07/26/14 Pct Recovery = 68% Analysis Date = 07/26/14 Pct Recovery = 68% Analysis Date = 07/15/14 Pct Recovery = 68% Analysis Date = 07/15/14 Pct Recovery = 68% Analysis Date = 07/04/14 Pct Recovery = 68% Analysis Date = 07/04/14 Pct Recovery = 68% Analysis Date = 06/24/14 Pct Recovery = 68% Analysis Date = 06/24/14 Pct Recovery = 68% Analysis Date = 06/13/14 Pct Recovery = 68% Analysis Date = 06/13/14 Pct Recovery = 68% Analysis Date = 06/02/14 Pct Recovery = 68% Analysis Date = 06/02/14 Pct Recovery = 68% Analysis Date = 05/22/14 Pct Recovery = 68% Analysis Date = 05/22/14 Pct Recovery = 68% Analysis Date = 05/12/14 Pct Recovery = 68% Analysis Date = 05/12/14 Pct Recovery = 68% Analysis Date = 05/01/14 Pct Recovery = 68% Analysis Date = 05/01/14 Pct Recovery = 68% Analysis Date = 04/20/14 Pct Recovery = 68% Analysis Date = 04/20/14 Pct Recovery = 68% Analysis Date = 04/10/14 Pct Recovery = 67% Analysis Date = 04/10/14 Pct Recovery = 67% Analysis Date = 03/30/14 Pct Recovery = 67% Analysis Date = 03/30/14 Pct Recovery = 67% Analysis Date = 03/19/14 Pct Recovery = 67% Analysis Date = 03/19/14 Pct Recovery = 67% Analysis Date = 03/09/14 Pct Recovery = 67% Analysis Date = 03/09/14 Pct Recovery = 67% Analysis Date = 02/26/14 Pct Recovery = 67% Analysis Date = 02/26/14 Pct Recovery = 67% Analysis Date = 02/15/14 Pct Recovery = 67% Analysis Date = 02/15/14 Pct Recovery = 67% Analysis Date = 02/04/14 Pct Recovery = 66% Analysis Date = 02/04/14 Pct Recovery = 66% Analysis Date = 01/25/14 Pct Recovery = 66% Analysis Date = 01/25/14 Pct Recovery = 66% Analysis Date = 01/14/14 Pct Recovery = 66% Analysis Date = 01/14/14 Pct Recovery = 66% Analysis Date = 01/03/14 Pct Recovery = 66% Analysis Date = 01/03/14 Pct Recovery = 66% Analysis Date = 12/24/13 Pct Recovery = 66% Analysis Date = 12/24/13 Pct Recovery = 66% Analysis Date = 12/13/13 Pct Recovery = 66% Analysis Date = 12/13/13 Pct Recovery = 66% Analysis Date = 12/02/13 Pct Recovery = 65% Analysis Date = 12/02/13 Pct Recovery = 65% Analysis Date = 11/21/13 Pct Recovery = 65% Analysis Date = 11/21/13 Pct Recovery = 65% Analysis Date = 11/11/13 Pct Recovery = 65% Analysis Date = 11/11/13 Pct Recovery = 65% Analysis Date = 10/31/13 Pct Recovery = 65% Analysis Date = 10/31/13 Pct Recovery = 65% Analysis Date = 10/20/13 Pct Recovery = 65% Analysis Date = 10/20/13 Pct Recovery = 65% Analysis Date = 10/10/13 Pct Recovery = 65% Analysis Date = 10/10/13 Pct Recovery = 65% Analysis Date = 09/29/13 Pct Recovery = 64% Analysis Date = 09/29/13 Pct Recovery = 64% Analysis Date = 09/18/13 Pct Recovery = 64% Analysis Date = 09/18/13 Pct Recovery = 64% Analysis Date = 09/08/13 Pct Recovery = 64% Analysis Date = 09/08/13 Pct Recovery = 64% Analysis Date = 08/28/13 Pct Recovery = 64% Analysis Date = 08/28/13 Pct Recovery = 64% Analysis Date = 08/17/13 Pct Recovery = 64% Analysis Date = 08/17/13 Pct Recovery = 64% Analysis Date = 08/06/13 Pct Recovery = 64% Analysis Date = 08/06/13 Pct Recovery = 64% Analysis Date = 07/27/13 Pct Recovery = 64% Analysis Date = 07/27/13 Pct Recovery = 64% Analysis Date = 07/16/13 Pct Recovery = 63% Analysis Date = 07/16/13 Pct Recovery = 63% Analysis Date = 07/05/13 Pct Recovery = 63% Analysis Date = 07/05/13 Pct Recovery = 63% Analysis Date = 06/25/13 Pct Recovery = 63% Analysis Date = 06/25/13 Pct Recovery = 63% Analysis Date = 06/14/13 Pct Recovery = 63% Analysis Date = 06/14/13 Pct Recovery = 63% Analysis Date = 06/03/13 Pct Recovery = 63% Analysis Date = 06/03/13 Pct Recovery = 63% Analysis Date = 05/23/13 Pct Recovery = 63% Analysis Date = 05/23/13 Pct Recovery = 63% Analysis Date = 05/13/13 Pct Recovery = 62% Analysis Date = 05/13/13 Pct Recovery = 62% Analysis Date = 05/02/13 Pct Recovery = 62% Analysis Date = 05/02/13 Pct Recovery = 62% Analysis Date = 04/21/13 Pct Recovery = 62% Analysis Date = 04/21/13 Pct Recovery = 62% Analysis Date = 04/11/13 Pct Recovery = 62% Analysis Date = 04/11/13 Pct Recovery = 62% Analysis Date = 03/31/13 Pct Recovery = 62% Analysis Date = 03/31/13 Pct Recovery = 62% Analysis Date = 03/20/13 Pct Recovery = 62% Analysis Date = 03/20/13 Pct Recovery = 62% Analysis Date = 03/10/13 Pct Recovery = 62% Analysis Date = 03/10/13 Pct Recovery = 62% Analysis Date = 02/27/13 Pct Recovery = 61% Analysis Date = 02/27/13 Pct Recovery = 61% Analysis Date = 02/16/13 Pct Recovery = 61% Analysis Date = 02/16/13 Pct Recovery = 61% Analysis Date = 02/05/13 Pct Recovery = 61% Analysis Date = 02/05/13 Pct Recovery = 61% Analysis Date = 01/26/13 Pct Recovery = 61% Analysis Date = 01/26/13 Pct Recovery = 61% Analysis Date = 01/15/13 Pct Recovery = 61% Analysis Date = 01/15/13 Pct Recovery = 61% Analysis Date = 01/04/13 Pct Recovery = 61% Analysis Date = 01/04/13 Pct Recovery = 61% Analysis Date = 12/25/12 Pct Recovery = 61% Analysis Date = 12/25/12 Pct Recovery = 61% Analysis Date = 12/14/12 Pct Recovery = 60% Analysis Date = 12/14/12 Pct Recovery = 60% Analysis Date = 12/03/12 Pct Recovery = 60% Analysis Date = 12/03/12 Pct Recovery = 60% Analysis Date = 11/23/12 Pct Recovery = 60% Analysis Date = 11/23/12 Pct Recovery = 60% Analysis Date = 11/12/12 Pct Recovery = 60% Analysis Date = 11/12/12 Pct Recovery = 60% Analysis Date = 11/01/12 Pct Recovery = 60% Analysis Date = 11/01/12 Pct Recovery = 60% Analysis Date = 10/21/12 Pct Recovery = 60% Analysis Date = 10/21/12 Pct Recovery = 60% Analysis Date = 10/11/12 Pct Recovery = 60% Analysis Date = 10/11/12 Pct Recovery = 60% Analysis Date = 09/30/12 Pct Recovery = 60% Analysis Date = 09/30/12 Pct Recovery = 60% Analysis Date = 09/19/12 Pct Recovery = 59% Analysis Date = 09/19/12 Pct Recovery = 59% Analysis Date = 09/09/12 Pct Recovery = 59% Analysis Date = 09/09/12 Pct Recovery = 59% Analysis Date = 08/29/12 Pct Recovery = 59% Analysis Date = 08/29/12 Pct Recovery = 59% Analysis Date = 08/18/12 Pct Recovery = 59% Analysis Date = 08/18/12 Pct Recovery = 59% Analysis Date = 08/07/12 Pct Recovery = 59% Analysis Date = 08/07/12 Pct Recovery = 59% Analysis Date = 07/28/12 Pct Recovery = 59% Analysis Date = 07/28/12 Pct Recovery = 59% Analysis Date = 07/17/12 Pct Recovery = 59% Analysis Date = 07/17/12 Pct Recovery = 59% Analysis Date = 07/06/12 Pct Recovery = 59% Analysis Date = 07/06/12 Pct Recovery = 59% Analysis Date = 06/26/12 Pct Recovery = 59% Analysis Date = 06/26/12 Pct Recovery = 59% Analysis Date = 06/15/12 Pct Recovery = 59% Analysis Date = 06/15/12 Pct Recovery = 59% Analysis Date = 06/04/12 Pct Recovery = 59% Analysis Date = 06/04/12 Pct Recovery = 59% Analysis Date = 05/25/12 Pct Recovery = 59% Analysis Date = 05/25/12 Pct Recovery = 59% Analysis Date = 05/14/12 Pct Recovery = 59% Analysis Date = 05/14/12 Pct Recovery = 59% Analysis Date = 05/03/12 Pct Recovery = 59% Analysis Date = 05/03/12 Pct Recovery = 59% Analysis Date = 04/22/12 Pct Recovery = 59% Analysis Date = 04/22/12 Pct Recovery = 59% Analysis Date = 04/12/12 Pct Recovery = 59% Analysis Date = 04/12/12 Pct Recovery = 59% Analysis Date = 04/01/12 Pct Recovery = 59% Analysis Date = 04/01/12 Pct Recovery = 59% Analysis Date = 03/21/12 Pct Recovery = 59% Analysis Date = 03/21/12 Pct Recovery = 59% Analysis Date = 03/11/12 Pct Recovery = 59% Analysis Date = 03/11/12 Pct Recovery = 59% Analysis Date = 02/29/12 Pct Recovery = 59% Analysis Date = 02/29/12 Pct Recovery = 59% Analysis Date = 02/18/12 Pct Recovery = 59% Analysis Date = 02/18/12 Pct Recovery = 59% Analysis Date = 02/07/12 Pct Recovery = 59% Analysis Date = 02/07/12 Pct Recovery = 59% Analysis Date = 01/28/12 Pct Recovery = 59% Analysis Date = 01/28/12 Pct Recovery = 59% Analysis Date = 01/17/12 Pct Recovery = 59% Analysis Date = 01/17/12 Pct Recovery = 59% Analysis Date = 01/06/12 Pct Recovery = 59% Analysis Date = 01/06/12 Pct Recovery = 59% Analysis Date = 12/27/11 Pct Recovery = 59% Analysis Date = 12/27/11 Pct Recovery = 59% Analysis Date = 12/16/11 Pct Recovery = 59% Analysis Date = 12/16/11 Pct Recovery = 59% Analysis Date = 12/05/11 Pct Recovery = 59% Analysis Date = 12/05/11 Pct Recovery = 59% Analysis Date = 11/25/11 Pct Recovery = 59% Analysis Date = 11/25/11 Pct Recovery = 59% Analysis Date = 11/14/11 Pct Recovery = 59% Analysis Date = 11/14/11 Pct Recovery = 59% Analysis Date = 11/03/11 Pct Recovery = 59% Analysis Date = 11/03/11 Pct Recovery = 59% Analysis Date = 10/23/11 Pct Recovery = 59% Analysis Date = 10/23/11 Pct Recovery = 59% Analysis Date = 10/13/11 Pct Recovery = 59% Analysis Date = 10/13/11 Pct Recovery = 59% Analysis Date = 10/02/11 Pct Recovery = 59% Analysis Date = 10/02/11 Pct Recovery = 59% Analysis Date = 09/21/11 Pct Recovery = 59% Analysis Date = 09/21/11 Pct Recovery = 59% Analysis Date = 09/11/11 Pct Recovery = 59% Analysis Date = 09/11/11 Pct Recovery = 59% Analysis Date = 08/31/11 Pct Recovery = 59% Analysis Date = 08/31/11 Pct Recovery = 59% Analysis Date = 08/20/11 Pct Recovery = 59% Analysis Date = 08/20/11 Pct Recovery = 59% Analysis Date = 08/09/11 Pct Recovery = 59% Analysis Date = 08/09/11 Pct Recovery = 59% Analysis Date = 07/30/11 Pct Recovery = 59% Analysis Date = 07/30/11 Pct Recovery = 59% Analysis Date = 07/19/11 Pct Recovery = 59% Analysis Date = 07/19/11 Pct Recovery = 59% Analysis Date = 07/08/11 Pct Recovery = 59% Analysis Date = 07/08/11 Pct Recovery = 59% Analysis Date = 06/28/11 Pct Recovery = 59% Analysis Date = 06/28/11 Pct Recovery = 59% Analysis Date = 06/17/11 Pct Recovery = 59% Analysis Date = 06/17/11 Pct Recovery = 59% Analysis Date = 06/06/11 Pct Recovery = 59% Analysis Date = 06/06/11 Pct Recovery = 59% Analysis Date = 05/27/11 Pct Recovery = 59% Analysis Date = 05/27/11 Pct Recovery = 59% Analysis Date = 05/16/11 Pct Recovery = 59% Analysis Date = 05/16/11 Pct Recovery = 59% Analysis Date = 05/05/11 Pct Recovery = 59% Analysis Date = 05/05/11 Pct Recovery = 59% Analysis Date = 04/24/11 Pct Recovery = 59% Analysis Date = 04/24/11 Pct Recovery = 59% Analysis Date = 04/14/11 Pct Recovery = 59% Analysis Date = 04/14/11 Pct Recovery = 59% Analysis Date = 04/03/11 Pct Recovery = 59% Analysis Date = 04/03/11 Pct Recovery = 59% Analysis Date = 03/23/11 Pct Recovery = 59% Analysis Date = 03/23/11 Pct Recovery = 59% Analysis Date = 03/13/11 Pct Recovery = 59% Analysis Date = 03/13/11 Pct Recovery = 59% Analysis Date = 03/02/11 Pct Recovery = 59% Analysis Date = 03/02/11 Pct Recovery = 59% Analysis Date = 02/19/11 Pct Recovery = 59% Analysis Date = 02/19/11 Pct Recovery = 59% Analysis Date = 02/09/11 Pct Recovery = 59% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 86 64% 13% 62% 12%
Total 86 64% 13% 62% 12%

Sample Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Characteristic N % % Basis
Plotted 86 100% Spiked
Estimated Values 86 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 86 .  
False Negatives 0 0% 0 out of 86
Not Spiked 83 .  
False Positives 2 2% 2 out of 83

BQS OBSP Determination:
TRIFLURALIN
METHOD: 2033 , TESTIDCODE: 82661GCM35
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 74% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 81% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 81% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 64% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 62% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 82% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 63% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 87% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 71% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 81% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 75% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 89% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 79% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 84% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 87% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 79% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 74% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 81% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 75% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 85% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 70% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 63% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 64% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 96% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 91% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 73% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 85% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 95% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 86% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 83% Analysis Date = 12/03/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 79% Analysis Date = 02/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 80 µl Pct Recovery = 93% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 91% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 113% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 90% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 98% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 63% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 93% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 80% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 103% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 80% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 88% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 71% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 80% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 81% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 83% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 83% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 83% Analysis Date = 06/20/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 102% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 77% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 86% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 92% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 92% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 67% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 92% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 107% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 136% Analysis Date = 04/13/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 110% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 100% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 92% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 85% Analysis Date = 05/08/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 131% Analysis Date = 03/05/12 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 101% Analysis Date = 10/25/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 102% Analysis Date = 07/28/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 139% Analysis Date = 02/08/11 SpikeMix = ERA 0818-10-05 LS 2033#2: 40 µl Pct Recovery = 109% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 108% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 98% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 107% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 106% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 103% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 100% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 112% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 99% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 92% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 69% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 119% Analysis Date = 01/17/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/16/16 Pct Recovery = 82% Analysis Date = 12/16/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 11/24/16 Pct Recovery = 82% Analysis Date = 11/24/16 Pct Recovery = 82% Analysis Date = 11/13/16 Pct Recovery = 82% Analysis Date = 11/13/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 11/03/16 Pct Recovery = 82% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/12/16 Pct Recovery = 81% Analysis Date = 10/12/16 Pct Recovery = 81% Analysis Date = 10/01/16 Pct Recovery = 81% Analysis Date = 10/01/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/20/16 Pct Recovery = 81% Analysis Date = 09/09/16 Pct Recovery = 81% Analysis Date = 09/09/16 Pct Recovery = 81% Analysis Date = 08/29/16 Pct Recovery = 81% Analysis Date = 08/29/16 Pct Recovery = 81% Analysis Date = 08/19/16 Pct Recovery = 81% Analysis Date = 08/19/16 Pct Recovery = 81% Analysis Date = 08/08/16 Pct Recovery = 81% Analysis Date = 08/08/16 Pct Recovery = 81% Analysis Date = 07/28/16 Pct Recovery = 81% Analysis Date = 07/28/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 81% Analysis Date = 06/14/16 Pct Recovery = 80% Analysis Date = 06/14/16 Pct Recovery = 80% Analysis Date = 06/04/16 Pct Recovery = 80% Analysis Date = 06/04/16 Pct Recovery = 80% Analysis Date = 05/24/16 Pct Recovery = 80% Analysis Date = 05/24/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 04/21/16 Pct Recovery = 80% Analysis Date = 04/21/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/20/16 Pct Recovery = 80% Analysis Date = 03/20/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/16/16 Pct Recovery = 80% Analysis Date = 02/05/16 Pct Recovery = 80% Analysis Date = 02/05/16 Pct Recovery = 80% Analysis Date = 01/25/16 Pct Recovery = 79% Analysis Date = 01/25/16 Pct Recovery = 79% Analysis Date = 01/14/16 Pct Recovery = 79% Analysis Date = 01/14/16 Pct Recovery = 79% Analysis Date = 01/04/16 Pct Recovery = 79% Analysis Date = 01/04/16 Pct Recovery = 79% Analysis Date = 12/24/15 Pct Recovery = 79% Analysis Date = 12/24/15 Pct Recovery = 79% Analysis Date = 12/13/15 Pct Recovery = 79% Analysis Date = 12/13/15 Pct Recovery = 79% Analysis Date = 12/02/15 Pct Recovery = 79% Analysis Date = 12/02/15 Pct Recovery = 79% Analysis Date = 11/21/15 Pct Recovery = 79% Analysis Date = 11/21/15 Pct Recovery = 79% Analysis Date = 11/10/15 Pct Recovery = 79% Analysis Date = 11/10/15 Pct Recovery = 79% Analysis Date = 10/30/15 Pct Recovery = 79% Analysis Date = 10/30/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/20/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 10/09/15 Pct Recovery = 79% Analysis Date = 09/28/15 Pct Recovery = 79% Analysis Date = 09/28/15 Pct Recovery = 79% Analysis Date = 09/17/15 Pct Recovery = 79% Analysis Date = 09/17/15 Pct Recovery = 79% Analysis Date = 09/06/15 Pct Recovery = 79% Analysis Date = 09/06/15 Pct Recovery = 79% Analysis Date = 08/26/15 Pct Recovery = 79% Analysis Date = 08/26/15 Pct Recovery = 79% Analysis Date = 08/15/15 Pct Recovery = 79% Analysis Date = 08/15/15 Pct Recovery = 79% Analysis Date = 08/05/15 Pct Recovery = 78% Analysis Date = 08/05/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/25/15 Pct Recovery = 78% Analysis Date = 07/14/15 Pct Recovery = 78% Analysis Date = 07/14/15 Pct Recovery = 78% Analysis Date = 07/03/15 Pct Recovery = 78% Analysis Date = 07/03/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/22/15 Pct Recovery = 78% Analysis Date = 06/11/15 Pct Recovery = 78% Analysis Date = 06/11/15 Pct Recovery = 78% Analysis Date = 05/31/15 Pct Recovery = 78% Analysis Date = 05/31/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/10/15 Pct Recovery = 78% Analysis Date = 05/10/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/29/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/18/15 Pct Recovery = 78% Analysis Date = 04/07/15 Pct Recovery = 78% Analysis Date = 04/07/15 Pct Recovery = 78% Analysis Date = 03/27/15 Pct Recovery = 78% Analysis Date = 03/27/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/16/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 03/06/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 78% Analysis Date = 02/23/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/12/15 Pct Recovery = 78% Analysis Date = 02/01/15 Pct Recovery = 78% Analysis Date = 02/01/15 Pct Recovery = 78% Analysis Date = 01/21/15 Pct Recovery = 78% Analysis Date = 01/21/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 78% Analysis Date = 01/10/15 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/31/14 Pct Recovery = 78% Analysis Date = 12/20/14 Pct Recovery = 78% Analysis Date = 12/20/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 12/09/14 Pct Recovery = 78% Analysis Date = 11/28/14 Pct Recovery = 78% Analysis Date = 11/28/14 Pct Recovery = 78% Analysis Date = 11/17/14 Pct Recovery = 78% Analysis Date = 11/17/14 Pct Recovery = 78% Analysis Date = 11/06/14 Pct Recovery = 78% Analysis Date = 11/06/14 Pct Recovery = 78% Analysis Date = 10/26/14 Pct Recovery = 78% Analysis Date = 10/26/14 Pct Recovery = 78% Analysis Date = 10/16/14 Pct Recovery = 78% Analysis Date = 10/16/14 Pct Recovery = 78% Analysis Date = 10/05/14 Pct Recovery = 78% Analysis Date = 10/05/14 Pct Recovery = 78% Analysis Date = 09/24/14 Pct Recovery = 78% Analysis Date = 09/24/14 Pct Recovery = 78% Analysis Date = 09/13/14 Pct Recovery = 79% Analysis Date = 09/13/14 Pct Recovery = 79% Analysis Date = 09/02/14 Pct Recovery = 79% Analysis Date = 09/02/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/22/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/11/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 08/01/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/21/14 Pct Recovery = 79% Analysis Date = 07/10/14 Pct Recovery = 79% Analysis Date = 07/10/14 Pct Recovery = 79% Analysis Date = 06/29/14 Pct Recovery = 79% Analysis Date = 06/29/14 Pct Recovery = 79% Analysis Date = 06/18/14 Pct Recovery = 79% Analysis Date = 06/18/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 79% Analysis Date = 06/07/14 Pct Recovery = 79% Analysis Date = 05/27/14 Pct Recovery = 79% Analysis Date = 05/27/14 Pct Recovery = 79% Analysis Date = 05/17/14 Pct Recovery = 79% Analysis Date = 05/17/14 Pct Recovery = 79% Analysis Date = 05/06/14 Pct Recovery = 79% Analysis Date = 05/06/14 Pct Recovery = 79% Analysis Date = 04/25/14 Pct Recovery = 80% Analysis Date = 04/25/14 Pct Recovery = 80% Analysis Date = 04/14/14 Pct Recovery = 80% Analysis Date = 04/14/14 Pct Recovery = 80% Analysis Date = 04/03/14 Pct Recovery = 80% Analysis Date = 04/03/14 Pct Recovery = 80% Analysis Date = 03/23/14 Pct Recovery = 80% Analysis Date = 03/23/14 Pct Recovery = 80% Analysis Date = 03/12/14 Pct Recovery = 80% Analysis Date = 03/12/14 Pct Recovery = 80% Analysis Date = 03/02/14 Pct Recovery = 80% Analysis Date = 03/02/14 Pct Recovery = 80% Analysis Date = 02/19/14 Pct Recovery = 80% Analysis Date = 02/19/14 Pct Recovery = 80% Analysis Date = 02/08/14 Pct Recovery = 80% Analysis Date = 02/08/14 Pct Recovery = 80% Analysis Date = 01/28/14 Pct Recovery = 80% Analysis Date = 01/28/14 Pct Recovery = 80% Analysis Date = 01/17/14 Pct Recovery = 80% Analysis Date = 01/17/14 Pct Recovery = 80% Analysis Date = 01/06/14 Pct Recovery = 80% Analysis Date = 01/06/14 Pct Recovery = 80% Analysis Date = 12/26/13 Pct Recovery = 81% Analysis Date = 12/26/13 Pct Recovery = 81% Analysis Date = 12/16/13 Pct Recovery = 81% Analysis Date = 12/16/13 Pct Recovery = 81% Analysis Date = 12/05/13 Pct Recovery = 81% Analysis Date = 12/05/13 Pct Recovery = 81% Analysis Date = 11/24/13 Pct Recovery = 81% Analysis Date = 11/24/13 Pct Recovery = 81% Analysis Date = 11/13/13 Pct Recovery = 81% Analysis Date = 11/13/13 Pct Recovery = 81% Analysis Date = 11/02/13 Pct Recovery = 81% Analysis Date = 11/02/13 Pct Recovery = 81% Analysis Date = 10/22/13 Pct Recovery = 82% Analysis Date = 10/22/13 Pct Recovery = 82% Analysis Date = 10/11/13 Pct Recovery = 82% Analysis Date = 10/11/13 Pct Recovery = 82% Analysis Date = 10/01/13 Pct Recovery = 82% Analysis Date = 10/01/13 Pct Recovery = 82% Analysis Date = 09/20/13 Pct Recovery = 83% Analysis Date = 09/20/13 Pct Recovery = 83% Analysis Date = 09/09/13 Pct Recovery = 83% Analysis Date = 09/09/13 Pct Recovery = 83% Analysis Date = 08/29/13 Pct Recovery = 83% Analysis Date = 08/29/13 Pct Recovery = 83% Analysis Date = 08/18/13 Pct Recovery = 83% Analysis Date = 08/18/13 Pct Recovery = 83% Analysis Date = 08/07/13 Pct Recovery = 84% Analysis Date = 08/07/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/27/13 Pct Recovery = 84% Analysis Date = 07/17/13 Pct Recovery = 84% Analysis Date = 07/17/13 Pct Recovery = 84% Analysis Date = 07/06/13 Pct Recovery = 85% Analysis Date = 07/06/13 Pct Recovery = 85% Analysis Date = 06/25/13 Pct Recovery = 85% Analysis Date = 06/25/13 Pct Recovery = 85% Analysis Date = 06/14/13 Pct Recovery = 85% Analysis Date = 06/14/13 Pct Recovery = 85% Analysis Date = 06/03/13 Pct Recovery = 85% Analysis Date = 06/03/13 Pct Recovery = 85% Analysis Date = 05/23/13 Pct Recovery = 86% Analysis Date = 05/23/13 Pct Recovery = 86% Analysis Date = 05/12/13 Pct Recovery = 86% Analysis Date = 05/12/13 Pct Recovery = 86% Analysis Date = 05/02/13 Pct Recovery = 86% Analysis Date = 05/02/13 Pct Recovery = 86% Analysis Date = 04/21/13 Pct Recovery = 87% Analysis Date = 04/21/13 Pct Recovery = 87% Analysis Date = 04/10/13 Pct Recovery = 87% Analysis Date = 04/10/13 Pct Recovery = 87% Analysis Date = 03/30/13 Pct Recovery = 87% Analysis Date = 03/30/13 Pct Recovery = 87% Analysis Date = 03/19/13 Pct Recovery = 88% Analysis Date = 03/19/13 Pct Recovery = 88% Analysis Date = 03/08/13 Pct Recovery = 88% Analysis Date = 03/08/13 Pct Recovery = 88% Analysis Date = 02/25/13 Pct Recovery = 88% Analysis Date = 02/25/13 Pct Recovery = 88% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/15/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 02/04/13 Pct Recovery = 89% Analysis Date = 01/24/13 Pct Recovery = 89% Analysis Date = 01/24/13 Pct Recovery = 89% Analysis Date = 01/13/13 Pct Recovery = 90% Analysis Date = 01/13/13 Pct Recovery = 90% Analysis Date = 01/02/13 Pct Recovery = 90% Analysis Date = 01/02/13 Pct Recovery = 90% Analysis Date = 12/22/12 Pct Recovery = 90% Analysis Date = 12/22/12 Pct Recovery = 90% Analysis Date = 12/12/12 Pct Recovery = 91% Analysis Date = 12/12/12 Pct Recovery = 91% Analysis Date = 12/01/12 Pct Recovery = 91% Analysis Date = 12/01/12 Pct Recovery = 91% Analysis Date = 11/20/12 Pct Recovery = 91% Analysis Date = 11/20/12 Pct Recovery = 91% Analysis Date = 11/09/12 Pct Recovery = 92% Analysis Date = 11/09/12 Pct Recovery = 92% Analysis Date = 10/29/12 Pct Recovery = 92% Analysis Date = 10/29/12 Pct Recovery = 92% Analysis Date = 10/18/12 Pct Recovery = 92% Analysis Date = 10/18/12 Pct Recovery = 92% Analysis Date = 10/07/12 Pct Recovery = 93% Analysis Date = 10/07/12 Pct Recovery = 93% Analysis Date = 09/27/12 Pct Recovery = 93% Analysis Date = 09/27/12 Pct Recovery = 93% Analysis Date = 09/16/12 Pct Recovery = 93% Analysis Date = 09/16/12 Pct Recovery = 93% Analysis Date = 09/05/12 Pct Recovery = 93% Analysis Date = 09/05/12 Pct Recovery = 93% Analysis Date = 08/25/12 Pct Recovery = 94% Analysis Date = 08/25/12 Pct Recovery = 94% Analysis Date = 08/14/12 Pct Recovery = 94% Analysis Date = 08/14/12 Pct Recovery = 94% Analysis Date = 08/03/12 Pct Recovery = 94% Analysis Date = 08/03/12 Pct Recovery = 94% Analysis Date = 07/23/12 Pct Recovery = 94% Analysis Date = 07/23/12 Pct Recovery = 94% Analysis Date = 07/13/12 Pct Recovery = 95% Analysis Date = 07/13/12 Pct Recovery = 95% Analysis Date = 07/02/12 Pct Recovery = 95% Analysis Date = 07/02/12 Pct Recovery = 95% Analysis Date = 06/21/12 Pct Recovery = 95% Analysis Date = 06/21/12 Pct Recovery = 95% Analysis Date = 06/10/12 Pct Recovery = 96% Analysis Date = 06/10/12 Pct Recovery = 96% Analysis Date = 05/30/12 Pct Recovery = 96% Analysis Date = 05/30/12 Pct Recovery = 96% Analysis Date = 05/19/12 Pct Recovery = 96% Analysis Date = 05/19/12 Pct Recovery = 96% Analysis Date = 05/08/12 Pct Recovery = 96% Analysis Date = 05/08/12 Pct Recovery = 96% Analysis Date = 04/28/12 Pct Recovery = 97% Analysis Date = 04/28/12 Pct Recovery = 97% Analysis Date = 04/17/12 Pct Recovery = 97% Analysis Date = 04/17/12 Pct Recovery = 97% Analysis Date = 04/06/12 Pct Recovery = 97% Analysis Date = 04/06/12 Pct Recovery = 97% Analysis Date = 03/26/12 Pct Recovery = 98% Analysis Date = 03/26/12 Pct Recovery = 98% Analysis Date = 03/15/12 Pct Recovery = 98% Analysis Date = 03/15/12 Pct Recovery = 98% Analysis Date = 03/04/12 Pct Recovery = 98% Analysis Date = 03/04/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/12/12 Pct Recovery = 99% Analysis Date = 02/12/12 Pct Recovery = 99% Analysis Date = 02/01/12 Pct Recovery = 99% Analysis Date = 02/01/12 Pct Recovery = 99% Analysis Date = 01/21/12 Pct Recovery = 99% Analysis Date = 01/21/12 Pct Recovery = 99% Analysis Date = 01/10/12 Pct Recovery = 99% Analysis Date = 01/10/12 Pct Recovery = 99% Analysis Date = 12/30/11 Pct Recovery = 100% Analysis Date = 12/30/11 Pct Recovery = 100% Analysis Date = 12/19/11 Pct Recovery = 100% Analysis Date = 12/19/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 100% Analysis Date = 11/28/11 Pct Recovery = 101% Analysis Date = 11/28/11 Pct Recovery = 101% Analysis Date = 11/17/11 Pct Recovery = 101% Analysis Date = 11/17/11 Pct Recovery = 101% Analysis Date = 11/06/11 Pct Recovery = 101% Analysis Date = 11/06/11 Pct Recovery = 101% Analysis Date = 10/26/11 Pct Recovery = 101% Analysis Date = 10/26/11 Pct Recovery = 101% Analysis Date = 10/15/11 Pct Recovery = 102% Analysis Date = 10/15/11 Pct Recovery = 102% Analysis Date = 10/04/11 Pct Recovery = 102% Analysis Date = 10/04/11 Pct Recovery = 102% Analysis Date = 09/23/11 Pct Recovery = 102% Analysis Date = 09/23/11 Pct Recovery = 102% Analysis Date = 09/13/11 Pct Recovery = 103% Analysis Date = 09/13/11 Pct Recovery = 103% Analysis Date = 09/02/11 Pct Recovery = 103% Analysis Date = 09/02/11 Pct Recovery = 103% Analysis Date = 08/22/11 Pct Recovery = 103% Analysis Date = 08/22/11 Pct Recovery = 103% Analysis Date = 08/11/11 Pct Recovery = 103% Analysis Date = 08/11/11 Pct Recovery = 103% Analysis Date = 07/31/11 Pct Recovery = 104% Analysis Date = 07/31/11 Pct Recovery = 104% Analysis Date = 07/20/11 Pct Recovery = 104% Analysis Date = 07/20/11 Pct Recovery = 104% Analysis Date = 07/09/11 Pct Recovery = 104% Analysis Date = 07/09/11 Pct Recovery = 104% Analysis Date = 06/29/11 Pct Recovery = 104% Analysis Date = 06/29/11 Pct Recovery = 104% Analysis Date = 06/18/11 Pct Recovery = 105% Analysis Date = 06/18/11 Pct Recovery = 105% Analysis Date = 06/07/11 Pct Recovery = 105% Analysis Date = 06/07/11 Pct Recovery = 105% Analysis Date = 05/27/11 Pct Recovery = 105% Analysis Date = 05/27/11 Pct Recovery = 105% Analysis Date = 05/16/11 Pct Recovery = 105% Analysis Date = 05/16/11 Pct Recovery = 105% Analysis Date = 05/05/11 Pct Recovery = 106% Analysis Date = 05/05/11 Pct Recovery = 106% Analysis Date = 04/24/11 Pct Recovery = 106% Analysis Date = 04/24/11 Pct Recovery = 106% Analysis Date = 04/14/11 Pct Recovery = 106% Analysis Date = 04/14/11 Pct Recovery = 106% Analysis Date = 04/03/11 Pct Recovery = 106% Analysis Date = 04/03/11 Pct Recovery = 106% Analysis Date = 03/23/11 Pct Recovery = 107% Analysis Date = 03/23/11 Pct Recovery = 107% Analysis Date = 03/12/11 Pct Recovery = 107% Analysis Date = 03/12/11 Pct Recovery = 107% Analysis Date = 03/01/11 Pct Recovery = 107% Analysis Date = 03/01/11 Pct Recovery = 107% Analysis Date = 02/18/11 Pct Recovery = 107% Analysis Date = 02/18/11 Pct Recovery = 107% Analysis Date = 02/08/11 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIFLURALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 93 87% 16% 85% 12%
Total 93 87% 16% 85% 12%

Sample Statistics
TRIFLURALIN

Characteristic N % % Basis
Plotted 93 100% Spiked
Estimated Values 4 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 93 .  
False Negatives 0 0% 0 out of 93
Not Spiked 76 .  
False Positives 1 1% 1 out of 76