BQS OBSP Determination:
HEXANE
METHOD: 4440 , TESTIDCODE: 81590GCM66
Open Data Set

Analysis Date = 12/12/16 SpikeMix = Accu 216041125: 40 µl & Crescent 03FF058: 40 µl Pct Recovery = 88% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 126% Analysis Date = 07/14/16 SpikeMix = Accu 216041125: 40 µl & NSI 041816AVOC: 40 µl Pct Recovery = 98% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 84% Analysis Date = 06/21/16 SpikeMix = Phenova B20160319: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 89% Analysis Date = 05/24/16 SpikeMix = Accu 216041125: 25 µl & Crescent 03FF058: 25 µl Pct Recovery = 71% Analysis Date = 03/19/15 SpikeMix = Spex Organics C1140417015: 20 µl & Crescent 03DD004: 20 µl Pct Recovery = 141% Analysis Date = 11/22/14 SpikeMix = NSI 032614: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 148% Analysis Date = 08/19/14 SpikeMix = Spex Organics C1140417015: 20 µl & Accu 214031115: 20 µl Pct Recovery = 167% Analysis Date = 08/16/14 SpikeMix = ERA 0227-14-06.1A: 20 µl & Spex Organics C1140417015: 20 µl Pct Recovery = 136% Analysis Date = 08/15/15 SpikeMix = Supelco LC13545: 25 µl & Crescent 04EE008: 25 µl Pct Recovery = 92% Analysis Date = 06/16/15 SpikeMix = ERA 0406-15-03: 25 µl & Supelco LC13545: 25 µl Pct Recovery = 79% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 66% Analysis Date = 09/08/16 SpikeMix = Phenova B20160319: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 93% Analysis Date = 07/29/16 SpikeMix = Phenova B20160319: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 113% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 86% Analysis Date = 10/13/16 SpikeMix = Accu 216041125: 15 µl & NSI 041816AVOC: 15 µl Pct Recovery = 118% Analysis Date = 08/20/16 SpikeMix = Accu 216041125: 15 µl & Crescent 03FF058: 15 µl Pct Recovery = 107% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 64% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 78% Analysis Date = 04/02/16 SpikeMix = Supelco LC13545: 15 µl & Accu 215041380: 15 µl Pct Recovery = 87% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 94% Analysis Date = 12/18/15 SpikeMix = Supelco LC13545: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 95% Analysis Date = 11/04/15 SpikeMix = NSI 050515AVOC: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 98% Analysis Date = 10/16/15 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 97% Analysis Date = 05/09/15 SpikeMix = Spex Organics EN150428007: 15 µl & Crescent 04EE008: 15 µl Pct Recovery = 113% Analysis Date = 11/06/14 SpikeMix = Spex Organics C1140417015: 10 µl & Crescent 03DD004: 10 µl Pct Recovery = 133% Analysis Date = 09/09/14 SpikeMix = NSI 032614: 10 µl & Spex Organics C1140417015: 10 µl Pct Recovery = 170% Analysis Date = 07/23/14 SpikeMix = Spex Organics C1140417015: 10 µl & Accu 214031115: 10 µl Pct Recovery = 170% Analysis Date = 07/11/14 SpikeMix = Spex Organics C1140417015: 10 µl & ERA 0227-14-06.1A: 10 µl Pct Recovery = 148% Analysis Date = 05/13/16 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 76% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 121% Analysis Date = 12/10/15 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 104% Analysis Date = 11/12/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 91% Analysis Date = 09/03/15 SpikeMix = NSI 050515AVOC: 10 µl & Spex Organics EN150428007: 10 µl Pct Recovery = 86% Analysis Date = 06/27/15 SpikeMix = ERA 0406-15-03: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 79% Analysis Date = 05/21/15 SpikeMix = Spex Organics EN150428007: 10 µl & Accu 215041380: 10 µl Pct Recovery = 101% Analysis Date = 05/09/15 SpikeMix = Supelco LC13545: 10 µl & Crescent 04EE008: 10 µl Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/07/16 Pct Recovery = 93% Analysis Date = 12/03/16 Pct Recovery = 93% Analysis Date = 12/03/16 Pct Recovery = 93% Analysis Date = 11/28/16 Pct Recovery = 93% Analysis Date = 11/28/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/24/16 Pct Recovery = 93% Analysis Date = 11/19/16 Pct Recovery = 93% Analysis Date = 11/19/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/15/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/15/16 Pct Recovery = 93% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/02/16 Pct Recovery = 92% Analysis Date = 10/02/16 Pct Recovery = 92% Analysis Date = 09/27/16 Pct Recovery = 92% Analysis Date = 09/27/16 Pct Recovery = 92% Analysis Date = 09/23/16 Pct Recovery = 92% Analysis Date = 09/23/16 Pct Recovery = 92% Analysis Date = 09/18/16 Pct Recovery = 92% Analysis Date = 09/18/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/14/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/10/16 Pct Recovery = 92% Analysis Date = 09/05/16 Pct Recovery = 92% Analysis Date = 09/05/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/27/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/23/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/10/16 Pct Recovery = 92% Analysis Date = 08/10/16 Pct Recovery = 92% Analysis Date = 08/05/16 Pct Recovery = 92% Analysis Date = 08/05/16 Pct Recovery = 92% Analysis Date = 08/01/16 Pct Recovery = 92% Analysis Date = 08/01/16 Pct Recovery = 92% Analysis Date = 07/27/16 Pct Recovery = 92% Analysis Date = 07/27/16 Pct Recovery = 92% Analysis Date = 07/23/16 Pct Recovery = 92% Analysis Date = 07/23/16 Pct Recovery = 92% Analysis Date = 07/18/16 Pct Recovery = 92% Analysis Date = 07/18/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/26/16 Pct Recovery = 91% Analysis Date = 06/22/16 Pct Recovery = 91% Analysis Date = 06/22/16 Pct Recovery = 91% Analysis Date = 06/17/16 Pct Recovery = 91% Analysis Date = 06/17/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 05/31/16 Pct Recovery = 91% Analysis Date = 05/31/16 Pct Recovery = 91% Analysis Date = 05/26/16 Pct Recovery = 91% Analysis Date = 05/26/16 Pct Recovery = 91% Analysis Date = 05/22/16 Pct Recovery = 91% Analysis Date = 05/22/16 Pct Recovery = 91% Analysis Date = 05/18/16 Pct Recovery = 91% Analysis Date = 05/18/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/13/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/09/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/30/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/17/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/12/16 Pct Recovery = 91% Analysis Date = 04/08/16 Pct Recovery = 91% Analysis Date = 04/08/16 Pct Recovery = 91% Analysis Date = 04/03/16 Pct Recovery = 91% Analysis Date = 04/03/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/25/16 Pct Recovery = 92% Analysis Date = 03/21/16 Pct Recovery = 92% Analysis Date = 03/21/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/17/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 92% Analysis Date = 03/03/16 Pct Recovery = 92% Analysis Date = 03/03/16 Pct Recovery = 92% Analysis Date = 02/28/16 Pct Recovery = 92% Analysis Date = 02/28/16 Pct Recovery = 92% Analysis Date = 02/23/16 Pct Recovery = 92% Analysis Date = 02/23/16 Pct Recovery = 92% Analysis Date = 02/19/16 Pct Recovery = 92% Analysis Date = 02/19/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/10/16 Pct Recovery = 92% Analysis Date = 02/10/16 Pct Recovery = 92% Analysis Date = 02/06/16 Pct Recovery = 92% Analysis Date = 02/06/16 Pct Recovery = 92% Analysis Date = 02/01/16 Pct Recovery = 93% Analysis Date = 02/01/16 Pct Recovery = 93% Analysis Date = 01/28/16 Pct Recovery = 93% Analysis Date = 01/28/16 Pct Recovery = 93% Analysis Date = 01/23/16 Pct Recovery = 93% Analysis Date = 01/23/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/19/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/15/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/10/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/06/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 01/01/16 Pct Recovery = 93% Analysis Date = 12/28/15 Pct Recovery = 93% Analysis Date = 12/28/15 Pct Recovery = 93% Analysis Date = 12/23/15 Pct Recovery = 93% Analysis Date = 12/23/15 Pct Recovery = 93% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/19/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/15/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/10/15 Pct Recovery = 94% Analysis Date = 12/06/15 Pct Recovery = 94% Analysis Date = 12/06/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 12/01/15 Pct Recovery = 94% Analysis Date = 11/27/15 Pct Recovery = 94% Analysis Date = 11/27/15 Pct Recovery = 94% Analysis Date = 11/23/15 Pct Recovery = 94% Analysis Date = 11/23/15 Pct Recovery = 94% Analysis Date = 11/18/15 Pct Recovery = 94% Analysis Date = 11/18/15 Pct Recovery = 94% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/14/15 Pct Recovery = 93% Analysis Date = 11/09/15 Pct Recovery = 94% Analysis Date = 11/09/15 Pct Recovery = 94% Analysis Date = 11/05/15 Pct Recovery = 94% Analysis Date = 11/05/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/31/15 Pct Recovery = 94% Analysis Date = 10/27/15 Pct Recovery = 94% Analysis Date = 10/27/15 Pct Recovery = 94% Analysis Date = 10/23/15 Pct Recovery = 94% Analysis Date = 10/23/15 Pct Recovery = 94% Analysis Date = 10/18/15 Pct Recovery = 94% Analysis Date = 10/18/15 Pct Recovery = 94% Analysis Date = 10/14/15 Pct Recovery = 95% Analysis Date = 10/14/15 Pct Recovery = 95% Analysis Date = 10/09/15 Pct Recovery = 95% Analysis Date = 10/09/15 Pct Recovery = 95% Analysis Date = 10/05/15 Pct Recovery = 95% Analysis Date = 10/05/15 Pct Recovery = 95% Analysis Date = 09/30/15 Pct Recovery = 95% Analysis Date = 09/30/15 Pct Recovery = 95% Analysis Date = 09/26/15 Pct Recovery = 95% Analysis Date = 09/26/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/22/15 Pct Recovery = 95% Analysis Date = 09/17/15 Pct Recovery = 96% Analysis Date = 09/17/15 Pct Recovery = 96% Analysis Date = 09/13/15 Pct Recovery = 96% Analysis Date = 09/13/15 Pct Recovery = 96% Analysis Date = 09/08/15 Pct Recovery = 96% Analysis Date = 09/08/15 Pct Recovery = 96% Analysis Date = 09/04/15 Pct Recovery = 96% Analysis Date = 09/04/15 Pct Recovery = 96% Analysis Date = 08/30/15 Pct Recovery = 96% Analysis Date = 08/30/15 Pct Recovery = 96% Analysis Date = 08/26/15 Pct Recovery = 97% Analysis Date = 08/26/15 Pct Recovery = 97% Analysis Date = 08/22/15 Pct Recovery = 97% Analysis Date = 08/22/15 Pct Recovery = 97% Analysis Date = 08/17/15 Pct Recovery = 98% Analysis Date = 08/17/15 Pct Recovery = 98% Analysis Date = 08/13/15 Pct Recovery = 98% Analysis Date = 08/13/15 Pct Recovery = 98% Analysis Date = 08/08/15 Pct Recovery = 98% Analysis Date = 08/08/15 Pct Recovery = 98% Analysis Date = 08/04/15 Pct Recovery = 99% Analysis Date = 08/04/15 Pct Recovery = 99% Analysis Date = 07/30/15 Pct Recovery = 99% Analysis Date = 07/30/15 Pct Recovery = 99% Analysis Date = 07/26/15 Pct Recovery = 99% Analysis Date = 07/26/15 Pct Recovery = 99% Analysis Date = 07/22/15 Pct Recovery = 100% Analysis Date = 07/22/15 Pct Recovery = 100% Analysis Date = 07/17/15 Pct Recovery = 100% Analysis Date = 07/17/15 Pct Recovery = 100% Analysis Date = 07/13/15 Pct Recovery = 101% Analysis Date = 07/13/15 Pct Recovery = 101% Analysis Date = 07/08/15 Pct Recovery = 101% Analysis Date = 07/08/15 Pct Recovery = 101% Analysis Date = 07/04/15 Pct Recovery = 101% Analysis Date = 07/04/15 Pct Recovery = 101% Analysis Date = 06/29/15 Pct Recovery = 102% Analysis Date = 06/29/15 Pct Recovery = 102% Analysis Date = 06/25/15 Pct Recovery = 102% Analysis Date = 06/25/15 Pct Recovery = 102% Analysis Date = 06/21/15 Pct Recovery = 103% Analysis Date = 06/21/15 Pct Recovery = 103% Analysis Date = 06/16/15 Pct Recovery = 104% Analysis Date = 06/16/15 Pct Recovery = 104% Analysis Date = 06/12/15 Pct Recovery = 104% Analysis Date = 06/12/15 Pct Recovery = 104% Analysis Date = 06/07/15 Pct Recovery = 105% Analysis Date = 06/07/15 Pct Recovery = 105% Analysis Date = 06/03/15 Pct Recovery = 106% Analysis Date = 06/03/15 Pct Recovery = 106% Analysis Date = 05/30/15 Pct Recovery = 106% Analysis Date = 05/30/15 Pct Recovery = 106% Analysis Date = 05/25/15 Pct Recovery = 107% Analysis Date = 05/25/15 Pct Recovery = 107% Analysis Date = 05/21/15 Pct Recovery = 108% Analysis Date = 05/21/15 Pct Recovery = 108% Analysis Date = 05/16/15 Pct Recovery = 108% Analysis Date = 05/16/15 Pct Recovery = 108% Analysis Date = 05/12/15 Pct Recovery = 109% Analysis Date = 05/12/15 Pct Recovery = 109% Analysis Date = 05/07/15 Pct Recovery = 110% Analysis Date = 05/07/15 Pct Recovery = 110% Analysis Date = 05/03/15 Pct Recovery = 110% Analysis Date = 05/03/15 Pct Recovery = 110% Analysis Date = 04/29/15 Pct Recovery = 111% Analysis Date = 04/29/15 Pct Recovery = 111% Analysis Date = 04/24/15 Pct Recovery = 112% Analysis Date = 04/24/15 Pct Recovery = 112% Analysis Date = 04/20/15 Pct Recovery = 113% Analysis Date = 04/20/15 Pct Recovery = 113% Analysis Date = 04/15/15 Pct Recovery = 114% Analysis Date = 04/15/15 Pct Recovery = 114% Analysis Date = 04/11/15 Pct Recovery = 114% Analysis Date = 04/11/15 Pct Recovery = 114% Analysis Date = 04/06/15 Pct Recovery = 115% Analysis Date = 04/06/15 Pct Recovery = 115% Analysis Date = 04/02/15 Pct Recovery = 116% Analysis Date = 04/02/15 Pct Recovery = 116% Analysis Date = 03/29/15 Pct Recovery = 117% Analysis Date = 03/29/15 Pct Recovery = 117% Analysis Date = 03/24/15 Pct Recovery = 118% Analysis Date = 03/24/15 Pct Recovery = 118% Analysis Date = 03/20/15 Pct Recovery = 118% Analysis Date = 03/20/15 Pct Recovery = 118% Analysis Date = 03/15/15 Pct Recovery = 119% Analysis Date = 03/15/15 Pct Recovery = 119% Analysis Date = 03/11/15 Pct Recovery = 120% Analysis Date = 03/11/15 Pct Recovery = 120% Analysis Date = 03/06/15 Pct Recovery = 121% Analysis Date = 03/06/15 Pct Recovery = 121% Analysis Date = 03/02/15 Pct Recovery = 121% Analysis Date = 03/02/15 Pct Recovery = 121% Analysis Date = 02/26/15 Pct Recovery = 122% Analysis Date = 02/26/15 Pct Recovery = 122% Analysis Date = 02/21/15 Pct Recovery = 123% Analysis Date = 02/21/15 Pct Recovery = 123% Analysis Date = 02/17/15 Pct Recovery = 124% Analysis Date = 02/17/15 Pct Recovery = 124% Analysis Date = 02/12/15 Pct Recovery = 124% Analysis Date = 02/12/15 Pct Recovery = 124% Analysis Date = 02/08/15 Pct Recovery = 125% Analysis Date = 02/08/15 Pct Recovery = 125% Analysis Date = 02/03/15 Pct Recovery = 126% Analysis Date = 02/03/15 Pct Recovery = 126% Analysis Date = 01/30/15 Pct Recovery = 127% Analysis Date = 01/30/15 Pct Recovery = 127% Analysis Date = 01/26/15 Pct Recovery = 127% Analysis Date = 01/26/15 Pct Recovery = 127% Analysis Date = 01/21/15 Pct Recovery = 128% Analysis Date = 01/21/15 Pct Recovery = 128% Analysis Date = 01/17/15 Pct Recovery = 129% Analysis Date = 01/17/15 Pct Recovery = 129% Analysis Date = 01/12/15 Pct Recovery = 130% Analysis Date = 01/12/15 Pct Recovery = 130% Analysis Date = 01/08/15 Pct Recovery = 131% Analysis Date = 01/08/15 Pct Recovery = 131% Analysis Date = 01/03/15 Pct Recovery = 131% Analysis Date = 01/03/15 Pct Recovery = 131% Analysis Date = 12/30/14 Pct Recovery = 132% Analysis Date = 12/30/14 Pct Recovery = 132% Analysis Date = 12/26/14 Pct Recovery = 133% Analysis Date = 12/26/14 Pct Recovery = 133% Analysis Date = 12/21/14 Pct Recovery = 134% Analysis Date = 12/21/14 Pct Recovery = 134% Analysis Date = 12/17/14 Pct Recovery = 134% Analysis Date = 12/17/14 Pct Recovery = 134% Analysis Date = 12/12/14 Pct Recovery = 135% Analysis Date = 12/12/14 Pct Recovery = 135% Analysis Date = 12/08/14 Pct Recovery = 136% Analysis Date = 12/08/14 Pct Recovery = 136% Analysis Date = 12/04/14 Pct Recovery = 137% Analysis Date = 12/04/14 Pct Recovery = 137% Analysis Date = 11/29/14 Pct Recovery = 137% Analysis Date = 11/29/14 Pct Recovery = 137% Analysis Date = 11/25/14 Pct Recovery = 138% Analysis Date = 11/25/14 Pct Recovery = 138% Analysis Date = 11/20/14 Pct Recovery = 139% Analysis Date = 11/20/14 Pct Recovery = 139% Analysis Date = 11/16/14 Pct Recovery = 140% Analysis Date = 11/16/14 Pct Recovery = 140% Analysis Date = 11/11/14 Pct Recovery = 140% Analysis Date = 11/11/14 Pct Recovery = 140% Analysis Date = 11/07/14 Pct Recovery = 141% Analysis Date = 11/07/14 Pct Recovery = 141% Analysis Date = 11/03/14 Pct Recovery = 142% Analysis Date = 11/03/14 Pct Recovery = 142% Analysis Date = 10/29/14 Pct Recovery = 143% Analysis Date = 10/29/14 Pct Recovery = 143% Analysis Date = 10/25/14 Pct Recovery = 144% Analysis Date = 10/25/14 Pct Recovery = 144% Analysis Date = 10/20/14 Pct Recovery = 144% Analysis Date = 10/20/14 Pct Recovery = 144% Analysis Date = 10/16/14 Pct Recovery = 145% Analysis Date = 10/16/14 Pct Recovery = 145% Analysis Date = 10/11/14 Pct Recovery = 146% Analysis Date = 10/11/14 Pct Recovery = 146% Analysis Date = 10/07/14 Pct Recovery = 147% Analysis Date = 10/07/14 Pct Recovery = 147% Analysis Date = 10/03/14 Pct Recovery = 147% Analysis Date = 10/03/14 Pct Recovery = 147% Analysis Date = 09/28/14 Pct Recovery = 148% Analysis Date = 09/28/14 Pct Recovery = 148% Analysis Date = 09/24/14 Pct Recovery = 149% Analysis Date = 09/24/14 Pct Recovery = 149% Analysis Date = 09/19/14 Pct Recovery = 150% Analysis Date = 09/19/14 Pct Recovery = 150% Analysis Date = 09/15/14 Pct Recovery = 150% Analysis Date = 09/15/14 Pct Recovery = 150% Analysis Date = 09/10/14 Pct Recovery = 151% Analysis Date = 09/10/14 Pct Recovery = 151% Analysis Date = 09/06/14 Pct Recovery = 152% Analysis Date = 09/06/14 Pct Recovery = 152% Analysis Date = 09/02/14 Pct Recovery = 153% Analysis Date = 09/02/14 Pct Recovery = 153% Analysis Date = 08/28/14 Pct Recovery = 154% Analysis Date = 08/28/14 Pct Recovery = 154% Analysis Date = 08/24/14 Pct Recovery = 154% Analysis Date = 08/24/14 Pct Recovery = 154% Analysis Date = 08/19/14 Pct Recovery = 155% Analysis Date = 08/19/14 Pct Recovery = 155% Analysis Date = 08/15/14 Pct Recovery = 156% Analysis Date = 08/15/14 Pct Recovery = 156% Analysis Date = 08/10/14 Pct Recovery = 157% Analysis Date = 08/10/14 Pct Recovery = 157% Analysis Date = 08/06/14 Pct Recovery = 158% Analysis Date = 08/06/14 Pct Recovery = 158% Analysis Date = 08/02/14 Pct Recovery = 158% Analysis Date = 08/02/14 Pct Recovery = 158% Analysis Date = 07/28/14 Pct Recovery = 159% Analysis Date = 07/28/14 Pct Recovery = 159% Analysis Date = 07/24/14 Pct Recovery = 160% Analysis Date = 07/24/14 Pct Recovery = 160% Analysis Date = 07/19/14 Pct Recovery = 161% Analysis Date = 07/19/14 Pct Recovery = 161% Analysis Date = 07/15/14 Pct Recovery = 162% Analysis Date = 07/15/14 Pct Recovery = 162% Analysis Date = 07/11/14 Pct Recovery = 162% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 104% 28% 94% 25%
Total 40 104% 28% 94% 25%

Sample Statistics
HEXANE

Characteristic N % % Basis
Plotted 40 100% Spiked
Estimated Values 40 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 40 .  
False Negatives 0 0% 0 out of 40
Not Spiked 25 .  
False Positives 8 32% 8 out of 25