BQS OBSP Determination:
ACETONITRILE
METHOD: 4437 , TESTIDCODE: 76997GM016
Open Data Set

Analysis Date = 06/23/16 SpikeMix = . Pct Recovery = 216% Analysis Date = 05/26/16 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl Pct Recovery = 216% Analysis Date = 07/15/16 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 141% Analysis Date = 07/29/16 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 127% Analysis Date = 08/11/16 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 102% Analysis Date = 05/26/16 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 106% Analysis Date = 07/23/14 SpikeMix = Accu 214031128: 20 µl & Abs 032014: 20 µl Pct Recovery = 110% Analysis Date = 07/11/14 SpikeMix = ChemService 2615700: 20 µl & Accu 214031128: 20 µl Pct Recovery = 101% Analysis Date = 05/07/14 SpikeMix = NSI 031814: 20 µl & Accu 214031128: 20 µl Pct Recovery = 114% Analysis Date = 03/19/15 SpikeMix = Supelco LC06437: 20 µl & NSI 031814: 20 µl Pct Recovery = 116% Analysis Date = 08/20/14 SpikeMix = Supelco LC06437: 20 µl & Abs 032014: 20 µl Pct Recovery = 101% Analysis Date = 06/07/14 SpikeMix = ChemService 2615700: 20 µl & Supelco LC06437: 20 µl Pct Recovery = 109% Analysis Date = 01/22/16 SpikeMix = NSI 050515HVOC: 25 µl & ERA 0601-15-05: 25 µl Pct Recovery = 107% Analysis Date = 10/09/15 SpikeMix = Supelco LC13544: 25 µl & NSI 050515HVOC: 25 µl Pct Recovery = 96% Analysis Date = 06/25/15 SpikeMix = ChemService 3818700: 25 µl & NSI 050515HVOC: 25 µl Pct Recovery = 97% Analysis Date = 08/12/16 SpikeMix = Accu 216041354: 15 µl & Abs 060916HVOC: 15 µl Pct Recovery = 154% Analysis Date = 07/06/16 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 172% Analysis Date = 07/27/16 SpikeMix = ChemService 5082800: 15 µl & Supelco LC20145V: 15 µl & Accu 216041225: 15 µl Pct Recovery = 182% Analysis Date = 11/25/15 SpikeMix = Accu 215041338: 15 µl & Abs 040315: 15 µl Pct Recovery = 129% Analysis Date = 09/24/15 SpikeMix = Abs 040315: 15 µl & ERA 0601-15-05: 15 µl Pct Recovery = 100% Analysis Date = 09/05/15 SpikeMix = Accu 215041338: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 88% Analysis Date = 07/30/15 SpikeMix = Supelco LC13544: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 106% Analysis Date = 06/16/15 SpikeMix = ChemService 3818700: 15 µl & NSI 050515HVOC: 15 µl Pct Recovery = 101% Analysis Date = 12/13/14 SpikeMix = Accu 214031128: 10 µl & NSI 031814: 10 µl Pct Recovery = 108% Analysis Date = 09/11/14 SpikeMix = Accu 214031128: 10 µl & Abs 032014: 10 µl Pct Recovery = 110% Analysis Date = 05/20/14 SpikeMix = ChemService 2615700: 10 µl & Accu 214031128: 10 µl Pct Recovery = 92% Analysis Date = 11/22/14 SpikeMix = ChemService 2615700: 10 µl & Supelco LC06437: 10 µl Pct Recovery = 103% Analysis Date = 06/17/14 SpikeMix = Supelco LC06437: 10 µl & Abs 032014: 10 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl Pct Recovery = 109% Analysis Date = 01/05/16 SpikeMix = Accu 215041338: 10 µl & Abs 040315: 10 µl Pct Recovery = 120% Analysis Date = 10/23/15 SpikeMix = Abs 040315: 10 µl & ChemService 3818700: 10 µl Pct Recovery = 116% Analysis Date = 08/14/15 SpikeMix = Abs 040315: 10 µl & ERA 0601-15-05: 10 µl Pct Recovery = 97% Analysis Date = 05/05/15 SpikeMix = Supelco LC13544: 10 µl & Abs 040315: 10 µl Pct Recovery = 115% Analysis Date = 03/22/16 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl Pct Recovery = 117% Analysis Date = 12/05/15 SpikeMix = NSI 050515HVOC: 10 µl & ERA 0601-15-05: 10 µl Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 158% Analysis Date = 08/07/16 Pct Recovery = 158% Analysis Date = 08/07/16 Pct Recovery = 158% Analysis Date = 08/03/16 Pct Recovery = 157% Analysis Date = 08/03/16 Pct Recovery = 157% Analysis Date = 07/30/16 Pct Recovery = 156% Analysis Date = 07/30/16 Pct Recovery = 156% Analysis Date = 07/26/16 Pct Recovery = 155% Analysis Date = 07/26/16 Pct Recovery = 155% Analysis Date = 07/22/16 Pct Recovery = 155% Analysis Date = 07/22/16 Pct Recovery = 155% Analysis Date = 07/18/16 Pct Recovery = 154% Analysis Date = 07/18/16 Pct Recovery = 154% Analysis Date = 07/14/16 Pct Recovery = 153% Analysis Date = 07/14/16 Pct Recovery = 153% Analysis Date = 07/09/16 Pct Recovery = 152% Analysis Date = 07/09/16 Pct Recovery = 152% Analysis Date = 07/05/16 Pct Recovery = 151% Analysis Date = 07/05/16 Pct Recovery = 151% Analysis Date = 07/01/16 Pct Recovery = 151% Analysis Date = 07/01/16 Pct Recovery = 151% Analysis Date = 06/27/16 Pct Recovery = 150% Analysis Date = 06/27/16 Pct Recovery = 150% Analysis Date = 06/23/16 Pct Recovery = 149% Analysis Date = 06/23/16 Pct Recovery = 149% Analysis Date = 06/19/16 Pct Recovery = 148% Analysis Date = 06/19/16 Pct Recovery = 148% Analysis Date = 06/15/16 Pct Recovery = 148% Analysis Date = 06/15/16 Pct Recovery = 148% Analysis Date = 06/10/16 Pct Recovery = 147% Analysis Date = 06/10/16 Pct Recovery = 147% Analysis Date = 06/06/16 Pct Recovery = 146% Analysis Date = 06/06/16 Pct Recovery = 146% Analysis Date = 06/02/16 Pct Recovery = 145% Analysis Date = 06/02/16 Pct Recovery = 145% Analysis Date = 05/29/16 Pct Recovery = 145% Analysis Date = 05/29/16 Pct Recovery = 145% Analysis Date = 05/25/16 Pct Recovery = 144% Analysis Date = 05/25/16 Pct Recovery = 144% Analysis Date = 05/21/16 Pct Recovery = 143% Analysis Date = 05/21/16 Pct Recovery = 143% Analysis Date = 05/17/16 Pct Recovery = 142% Analysis Date = 05/17/16 Pct Recovery = 142% Analysis Date = 05/12/16 Pct Recovery = 141% Analysis Date = 05/12/16 Pct Recovery = 141% Analysis Date = 05/08/16 Pct Recovery = 140% Analysis Date = 05/08/16 Pct Recovery = 140% Analysis Date = 05/04/16 Pct Recovery = 140% Analysis Date = 05/04/16 Pct Recovery = 140% Analysis Date = 04/30/16 Pct Recovery = 139% Analysis Date = 04/30/16 Pct Recovery = 139% Analysis Date = 04/26/16 Pct Recovery = 138% Analysis Date = 04/26/16 Pct Recovery = 138% Analysis Date = 04/22/16 Pct Recovery = 137% Analysis Date = 04/22/16 Pct Recovery = 137% Analysis Date = 04/18/16 Pct Recovery = 136% Analysis Date = 04/18/16 Pct Recovery = 136% Analysis Date = 04/13/16 Pct Recovery = 135% Analysis Date = 04/13/16 Pct Recovery = 135% Analysis Date = 04/09/16 Pct Recovery = 135% Analysis Date = 04/09/16 Pct Recovery = 135% Analysis Date = 04/05/16 Pct Recovery = 134% Analysis Date = 04/05/16 Pct Recovery = 134% Analysis Date = 04/01/16 Pct Recovery = 133% Analysis Date = 04/01/16 Pct Recovery = 133% Analysis Date = 03/28/16 Pct Recovery = 132% Analysis Date = 03/28/16 Pct Recovery = 132% Analysis Date = 03/24/16 Pct Recovery = 131% Analysis Date = 03/24/16 Pct Recovery = 131% Analysis Date = 03/20/16 Pct Recovery = 130% Analysis Date = 03/20/16 Pct Recovery = 130% Analysis Date = 03/15/16 Pct Recovery = 130% Analysis Date = 03/15/16 Pct Recovery = 130% Analysis Date = 03/11/16 Pct Recovery = 129% Analysis Date = 03/11/16 Pct Recovery = 129% Analysis Date = 03/07/16 Pct Recovery = 128% Analysis Date = 03/07/16 Pct Recovery = 128% Analysis Date = 03/03/16 Pct Recovery = 127% Analysis Date = 03/03/16 Pct Recovery = 127% Analysis Date = 02/28/16 Pct Recovery = 126% Analysis Date = 02/28/16 Pct Recovery = 126% Analysis Date = 02/24/16 Pct Recovery = 125% Analysis Date = 02/24/16 Pct Recovery = 125% Analysis Date = 02/20/16 Pct Recovery = 125% Analysis Date = 02/20/16 Pct Recovery = 125% Analysis Date = 02/15/16 Pct Recovery = 124% Analysis Date = 02/15/16 Pct Recovery = 124% Analysis Date = 02/11/16 Pct Recovery = 123% Analysis Date = 02/11/16 Pct Recovery = 123% Analysis Date = 02/07/16 Pct Recovery = 122% Analysis Date = 02/07/16 Pct Recovery = 122% Analysis Date = 02/03/16 Pct Recovery = 121% Analysis Date = 02/03/16 Pct Recovery = 121% Analysis Date = 01/30/16 Pct Recovery = 120% Analysis Date = 01/30/16 Pct Recovery = 120% Analysis Date = 01/26/16 Pct Recovery = 120% Analysis Date = 01/26/16 Pct Recovery = 120% Analysis Date = 01/22/16 Pct Recovery = 119% Analysis Date = 01/22/16 Pct Recovery = 119% Analysis Date = 01/17/16 Pct Recovery = 118% Analysis Date = 01/17/16 Pct Recovery = 118% Analysis Date = 01/13/16 Pct Recovery = 117% Analysis Date = 01/13/16 Pct Recovery = 117% Analysis Date = 01/09/16 Pct Recovery = 116% Analysis Date = 01/09/16 Pct Recovery = 116% Analysis Date = 01/05/16 Pct Recovery = 115% Analysis Date = 01/05/16 Pct Recovery = 115% Analysis Date = 01/01/16 Pct Recovery = 115% Analysis Date = 01/01/16 Pct Recovery = 115% Analysis Date = 12/28/15 Pct Recovery = 114% Analysis Date = 12/28/15 Pct Recovery = 114% Analysis Date = 12/24/15 Pct Recovery = 114% Analysis Date = 12/24/15 Pct Recovery = 114% Analysis Date = 12/20/15 Pct Recovery = 113% Analysis Date = 12/20/15 Pct Recovery = 113% Analysis Date = 12/15/15 Pct Recovery = 113% Analysis Date = 12/15/15 Pct Recovery = 113% Analysis Date = 12/11/15 Pct Recovery = 112% Analysis Date = 12/11/15 Pct Recovery = 112% Analysis Date = 12/07/15 Pct Recovery = 112% Analysis Date = 12/07/15 Pct Recovery = 112% Analysis Date = 12/03/15 Pct Recovery = 111% Analysis Date = 12/03/15 Pct Recovery = 111% Analysis Date = 11/29/15 Pct Recovery = 110% Analysis Date = 11/29/15 Pct Recovery = 110% Analysis Date = 11/25/15 Pct Recovery = 110% Analysis Date = 11/25/15 Pct Recovery = 110% Analysis Date = 11/21/15 Pct Recovery = 110% Analysis Date = 11/21/15 Pct Recovery = 110% Analysis Date = 11/16/15 Pct Recovery = 109% Analysis Date = 11/16/15 Pct Recovery = 109% Analysis Date = 11/12/15 Pct Recovery = 109% Analysis Date = 11/12/15 Pct Recovery = 109% Analysis Date = 11/08/15 Pct Recovery = 109% Analysis Date = 11/08/15 Pct Recovery = 109% Analysis Date = 11/04/15 Pct Recovery = 108% Analysis Date = 11/04/15 Pct Recovery = 108% Analysis Date = 10/31/15 Pct Recovery = 108% Analysis Date = 10/31/15 Pct Recovery = 108% Analysis Date = 10/27/15 Pct Recovery = 108% Analysis Date = 10/27/15 Pct Recovery = 108% Analysis Date = 10/23/15 Pct Recovery = 108% Analysis Date = 10/23/15 Pct Recovery = 108% Analysis Date = 10/18/15 Pct Recovery = 107% Analysis Date = 10/18/15 Pct Recovery = 107% Analysis Date = 10/14/15 Pct Recovery = 107% Analysis Date = 10/14/15 Pct Recovery = 107% Analysis Date = 10/10/15 Pct Recovery = 107% Analysis Date = 10/10/15 Pct Recovery = 107% Analysis Date = 10/06/15 Pct Recovery = 106% Analysis Date = 10/06/15 Pct Recovery = 106% Analysis Date = 10/02/15 Pct Recovery = 106% Analysis Date = 10/02/15 Pct Recovery = 106% Analysis Date = 09/28/15 Pct Recovery = 106% Analysis Date = 09/28/15 Pct Recovery = 106% Analysis Date = 09/24/15 Pct Recovery = 106% Analysis Date = 09/24/15 Pct Recovery = 106% Analysis Date = 09/19/15 Pct Recovery = 106% Analysis Date = 09/19/15 Pct Recovery = 106% Analysis Date = 09/15/15 Pct Recovery = 106% Analysis Date = 09/15/15 Pct Recovery = 106% Analysis Date = 09/11/15 Pct Recovery = 106% Analysis Date = 09/11/15 Pct Recovery = 106% Analysis Date = 09/07/15 Pct Recovery = 105% Analysis Date = 09/07/15 Pct Recovery = 105% Analysis Date = 09/03/15 Pct Recovery = 105% Analysis Date = 09/03/15 Pct Recovery = 105% Analysis Date = 08/30/15 Pct Recovery = 105% Analysis Date = 08/30/15 Pct Recovery = 105% Analysis Date = 08/26/15 Pct Recovery = 105% Analysis Date = 08/26/15 Pct Recovery = 105% Analysis Date = 08/21/15 Pct Recovery = 105% Analysis Date = 08/21/15 Pct Recovery = 105% Analysis Date = 08/17/15 Pct Recovery = 105% Analysis Date = 08/17/15 Pct Recovery = 105% Analysis Date = 08/13/15 Pct Recovery = 105% Analysis Date = 08/13/15 Pct Recovery = 105% Analysis Date = 08/09/15 Pct Recovery = 105% Analysis Date = 08/09/15 Pct Recovery = 105% Analysis Date = 08/05/15 Pct Recovery = 105% Analysis Date = 08/05/15 Pct Recovery = 105% Analysis Date = 08/01/15 Pct Recovery = 105% Analysis Date = 08/01/15 Pct Recovery = 105% Analysis Date = 07/28/15 Pct Recovery = 105% Analysis Date = 07/28/15 Pct Recovery = 105% Analysis Date = 07/23/15 Pct Recovery = 105% Analysis Date = 07/23/15 Pct Recovery = 105% Analysis Date = 07/19/15 Pct Recovery = 105% Analysis Date = 07/19/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/15/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/11/15 Pct Recovery = 105% Analysis Date = 07/07/15 Pct Recovery = 105% Analysis Date = 07/07/15 Pct Recovery = 105% Analysis Date = 07/03/15 Pct Recovery = 105% Analysis Date = 07/03/15 Pct Recovery = 105% Analysis Date = 06/29/15 Pct Recovery = 105% Analysis Date = 06/29/15 Pct Recovery = 105% Analysis Date = 06/24/15 Pct Recovery = 105% Analysis Date = 06/24/15 Pct Recovery = 105% Analysis Date = 06/20/15 Pct Recovery = 105% Analysis Date = 06/20/15 Pct Recovery = 105% Analysis Date = 06/16/15 Pct Recovery = 105% Analysis Date = 06/16/15 Pct Recovery = 105% Analysis Date = 06/12/15 Pct Recovery = 105% Analysis Date = 06/12/15 Pct Recovery = 105% Analysis Date = 06/08/15 Pct Recovery = 105% Analysis Date = 06/08/15 Pct Recovery = 105% Analysis Date = 06/04/15 Pct Recovery = 105% Analysis Date = 06/04/15 Pct Recovery = 105% Analysis Date = 05/31/15 Pct Recovery = 105% Analysis Date = 05/31/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/27/15 Pct Recovery = 105% Analysis Date = 05/22/15 Pct Recovery = 105% Analysis Date = 05/22/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/18/15 Pct Recovery = 105% Analysis Date = 05/14/15 Pct Recovery = 105% Analysis Date = 05/14/15 Pct Recovery = 105% Analysis Date = 05/10/15 Pct Recovery = 105% Analysis Date = 05/10/15 Pct Recovery = 105% Analysis Date = 05/06/15 Pct Recovery = 105% Analysis Date = 05/06/15 Pct Recovery = 105% Analysis Date = 05/02/15 Pct Recovery = 105% Analysis Date = 05/02/15 Pct Recovery = 105% Analysis Date = 04/28/15 Pct Recovery = 105% Analysis Date = 04/28/15 Pct Recovery = 105% Analysis Date = 04/23/15 Pct Recovery = 105% Analysis Date = 04/23/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/19/15 Pct Recovery = 105% Analysis Date = 04/15/15 Pct Recovery = 105% Analysis Date = 04/15/15 Pct Recovery = 105% Analysis Date = 04/11/15 Pct Recovery = 105% Analysis Date = 04/11/15 Pct Recovery = 105% Analysis Date = 04/07/15 Pct Recovery = 105% Analysis Date = 04/07/15 Pct Recovery = 105% Analysis Date = 04/03/15 Pct Recovery = 105% Analysis Date = 04/03/15 Pct Recovery = 105% Analysis Date = 03/30/15 Pct Recovery = 105% Analysis Date = 03/30/15 Pct Recovery = 105% Analysis Date = 03/25/15 Pct Recovery = 105% Analysis Date = 03/25/15 Pct Recovery = 105% Analysis Date = 03/21/15 Pct Recovery = 105% Analysis Date = 03/21/15 Pct Recovery = 105% Analysis Date = 03/17/15 Pct Recovery = 105% Analysis Date = 03/17/15 Pct Recovery = 105% Analysis Date = 03/13/15 Pct Recovery = 105% Analysis Date = 03/13/15 Pct Recovery = 105% Analysis Date = 03/09/15 Pct Recovery = 105% Analysis Date = 03/09/15 Pct Recovery = 105% Analysis Date = 03/05/15 Pct Recovery = 105% Analysis Date = 03/05/15 Pct Recovery = 105% Analysis Date = 03/01/15 Pct Recovery = 105% Analysis Date = 03/01/15 Pct Recovery = 105% Analysis Date = 02/24/15 Pct Recovery = 105% Analysis Date = 02/24/15 Pct Recovery = 105% Analysis Date = 02/20/15 Pct Recovery = 105% Analysis Date = 02/20/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/16/15 Pct Recovery = 105% Analysis Date = 02/12/15 Pct Recovery = 105% Analysis Date = 02/12/15 Pct Recovery = 105% Analysis Date = 02/08/15 Pct Recovery = 105% Analysis Date = 02/08/15 Pct Recovery = 105% Analysis Date = 02/04/15 Pct Recovery = 105% Analysis Date = 02/04/15 Pct Recovery = 105% Analysis Date = 01/31/15 Pct Recovery = 105% Analysis Date = 01/31/15 Pct Recovery = 105% Analysis Date = 01/26/15 Pct Recovery = 105% Analysis Date = 01/26/15 Pct Recovery = 105% Analysis Date = 01/22/15 Pct Recovery = 105% Analysis Date = 01/22/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/18/15 Pct Recovery = 105% Analysis Date = 01/14/15 Pct Recovery = 105% Analysis Date = 01/14/15 Pct Recovery = 105% Analysis Date = 01/10/15 Pct Recovery = 105% Analysis Date = 01/10/15 Pct Recovery = 105% Analysis Date = 01/06/15 Pct Recovery = 105% Analysis Date = 01/06/15 Pct Recovery = 105% Analysis Date = 01/02/15 Pct Recovery = 105% Analysis Date = 01/02/15 Pct Recovery = 105% Analysis Date = 12/28/14 Pct Recovery = 105% Analysis Date = 12/28/14 Pct Recovery = 105% Analysis Date = 12/24/14 Pct Recovery = 105% Analysis Date = 12/24/14 Pct Recovery = 105% Analysis Date = 12/20/14 Pct Recovery = 105% Analysis Date = 12/20/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/16/14 Pct Recovery = 105% Analysis Date = 12/12/14 Pct Recovery = 105% Analysis Date = 12/12/14 Pct Recovery = 105% Analysis Date = 12/08/14 Pct Recovery = 105% Analysis Date = 12/08/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 105% Analysis Date = 12/04/14 Pct Recovery = 105% Analysis Date = 11/29/14 Pct Recovery = 105% Analysis Date = 11/29/14 Pct Recovery = 105% Analysis Date = 11/25/14 Pct Recovery = 105% Analysis Date = 11/25/14 Pct Recovery = 105% Analysis Date = 11/21/14 Pct Recovery = 105% Analysis Date = 11/21/14 Pct Recovery = 105% Analysis Date = 11/17/14 Pct Recovery = 105% Analysis Date = 11/17/14 Pct Recovery = 105% Analysis Date = 11/13/14 Pct Recovery = 105% Analysis Date = 11/13/14 Pct Recovery = 105% Analysis Date = 11/09/14 Pct Recovery = 105% Analysis Date = 11/09/14 Pct Recovery = 105% Analysis Date = 11/05/14 Pct Recovery = 105% Analysis Date = 11/05/14 Pct Recovery = 105% Analysis Date = 11/01/14 Pct Recovery = 105% Analysis Date = 11/01/14 Pct Recovery = 105% Analysis Date = 10/27/14 Pct Recovery = 105% Analysis Date = 10/27/14 Pct Recovery = 105% Analysis Date = 10/23/14 Pct Recovery = 105% Analysis Date = 10/23/14 Pct Recovery = 105% Analysis Date = 10/19/14 Pct Recovery = 105% Analysis Date = 10/19/14 Pct Recovery = 105% Analysis Date = 10/15/14 Pct Recovery = 105% Analysis Date = 10/15/14 Pct Recovery = 105% Analysis Date = 10/11/14 Pct Recovery = 105% Analysis Date = 10/11/14 Pct Recovery = 105% Analysis Date = 10/07/14 Pct Recovery = 105% Analysis Date = 10/07/14 Pct Recovery = 105% Analysis Date = 10/03/14 Pct Recovery = 105% Analysis Date = 10/03/14 Pct Recovery = 105% Analysis Date = 09/28/14 Pct Recovery = 105% Analysis Date = 09/28/14 Pct Recovery = 105% Analysis Date = 09/24/14 Pct Recovery = 105% Analysis Date = 09/24/14 Pct Recovery = 105% Analysis Date = 09/20/14 Pct Recovery = 105% Analysis Date = 09/20/14 Pct Recovery = 105% Analysis Date = 09/16/14 Pct Recovery = 105% Analysis Date = 09/16/14 Pct Recovery = 105% Analysis Date = 09/12/14 Pct Recovery = 105% Analysis Date = 09/12/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/08/14 Pct Recovery = 105% Analysis Date = 09/04/14 Pct Recovery = 105% Analysis Date = 09/04/14 Pct Recovery = 105% Analysis Date = 08/30/14 Pct Recovery = 105% Analysis Date = 08/30/14 Pct Recovery = 105% Analysis Date = 08/26/14 Pct Recovery = 105% Analysis Date = 08/26/14 Pct Recovery = 105% Analysis Date = 08/22/14 Pct Recovery = 105% Analysis Date = 08/22/14 Pct Recovery = 105% Analysis Date = 08/18/14 Pct Recovery = 105% Analysis Date = 08/18/14 Pct Recovery = 105% Analysis Date = 08/14/14 Pct Recovery = 105% Analysis Date = 08/14/14 Pct Recovery = 105% Analysis Date = 08/10/14 Pct Recovery = 105% Analysis Date = 08/10/14 Pct Recovery = 105% Analysis Date = 08/06/14 Pct Recovery = 105% Analysis Date = 08/06/14 Pct Recovery = 105% Analysis Date = 08/01/14 Pct Recovery = 105% Analysis Date = 08/01/14 Pct Recovery = 105% Analysis Date = 07/28/14 Pct Recovery = 105% Analysis Date = 07/28/14 Pct Recovery = 105% Analysis Date = 07/24/14 Pct Recovery = 105% Analysis Date = 07/24/14 Pct Recovery = 105% Analysis Date = 07/20/14 Pct Recovery = 105% Analysis Date = 07/20/14 Pct Recovery = 105% Analysis Date = 07/16/14 Pct Recovery = 105% Analysis Date = 07/16/14 Pct Recovery = 105% Analysis Date = 07/12/14 Pct Recovery = 105% Analysis Date = 07/12/14 Pct Recovery = 105% Analysis Date = 07/08/14 Pct Recovery = 105% Analysis Date = 07/08/14 Pct Recovery = 105% Analysis Date = 07/03/14 Pct Recovery = 105% Analysis Date = 07/03/14 Pct Recovery = 105% Analysis Date = 06/29/14 Pct Recovery = 105% Analysis Date = 06/29/14 Pct Recovery = 105% Analysis Date = 06/25/14 Pct Recovery = 105% Analysis Date = 06/25/14 Pct Recovery = 105% Analysis Date = 06/21/14 Pct Recovery = 105% Analysis Date = 06/21/14 Pct Recovery = 105% Analysis Date = 06/17/14 Pct Recovery = 105% Analysis Date = 06/17/14 Pct Recovery = 105% Analysis Date = 06/13/14 Pct Recovery = 105% Analysis Date = 06/13/14 Pct Recovery = 105% Analysis Date = 06/09/14 Pct Recovery = 105% Analysis Date = 06/09/14 Pct Recovery = 105% Analysis Date = 06/04/14 Pct Recovery = 105% Analysis Date = 06/04/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 105% Analysis Date = 05/31/14 Pct Recovery = 105% Analysis Date = 05/27/14 Pct Recovery = 104% Analysis Date = 05/27/14 Pct Recovery = 104% Analysis Date = 05/23/14 Pct Recovery = 104% Analysis Date = 05/23/14 Pct Recovery = 104% Analysis Date = 05/19/14 Pct Recovery = 104% Analysis Date = 05/19/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/15/14 Pct Recovery = 104% Analysis Date = 05/11/14 Pct Recovery = 104% Analysis Date = 05/11/14 Pct Recovery = 104% Analysis Date = 05/07/14 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 119% 32% 109% 14%
Total 35 119% 32% 109% 14%

Sample Statistics
ACETONITRILE

Characteristic N % % Basis
Plotted 35 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 15 .  
False Positives 5 33% 5 out of 15