BQS OBSP Determination:
NICOTINE
METHOD: 2440 , TESTIDCODE: 67493LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 28% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 27% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 60% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 62% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 62% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 55% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 41% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 54% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 17% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 29% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 37% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 33% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 47% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 69% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 34% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 47% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 53% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 77% Analysis Date = 08/21/14 SpikeMix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Pct Recovery = 56% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 22% Analysis Date = 06/11/14 SpikeMix = Abs 041614: 60 µl & Abs 041714: 60 µl Pct Recovery = 54% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 75% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 64% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 77% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 32% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 79% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 53% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 36% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 35% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 31% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 65% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 13% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 16% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 19% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 41% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 44% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 40% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 42% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 33% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 58% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 33% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 37% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 26% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 52% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 34% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 31% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 139% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 44% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 46% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 109% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 31% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 70% Analysis Date = 07/20/14 SpikeMix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Pct Recovery = 43% Analysis Date = 06/28/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 35% Analysis Date = 05/17/14 SpikeMix = Abs 041614: 30 µl & Abs 041714: 30 µl Pct Recovery = 72% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 66% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 66% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 61% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 55% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 61% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 21% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 139% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 93% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 117% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 24% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 57% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 68% Analysis Date = 01/04/17 Pct Recovery = 40% Analysis Date = 12/31/16 Pct Recovery = 40% Analysis Date = 12/31/16 Pct Recovery = 40% Analysis Date = 12/26/16 Pct Recovery = 40% Analysis Date = 12/26/16 Pct Recovery = 40% Analysis Date = 12/21/16 Pct Recovery = 40% Analysis Date = 12/21/16 Pct Recovery = 40% Analysis Date = 12/16/16 Pct Recovery = 40% Analysis Date = 12/16/16 Pct Recovery = 40% Analysis Date = 12/11/16 Pct Recovery = 41% Analysis Date = 12/11/16 Pct Recovery = 41% Analysis Date = 12/06/16 Pct Recovery = 41% Analysis Date = 12/06/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 41% Analysis Date = 12/01/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/16/16 Pct Recovery = 41% Analysis Date = 11/16/16 Pct Recovery = 41% Analysis Date = 11/11/16 Pct Recovery = 41% Analysis Date = 11/11/16 Pct Recovery = 41% Analysis Date = 11/06/16 Pct Recovery = 41% Analysis Date = 11/06/16 Pct Recovery = 41% Analysis Date = 11/01/16 Pct Recovery = 41% Analysis Date = 11/01/16 Pct Recovery = 41% Analysis Date = 10/27/16 Pct Recovery = 41% Analysis Date = 10/27/16 Pct Recovery = 41% Analysis Date = 10/22/16 Pct Recovery = 41% Analysis Date = 10/22/16 Pct Recovery = 41% Analysis Date = 10/17/16 Pct Recovery = 41% Analysis Date = 10/17/16 Pct Recovery = 41% Analysis Date = 10/13/16 Pct Recovery = 41% Analysis Date = 10/13/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/08/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 10/03/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 41% Analysis Date = 09/28/16 Pct Recovery = 41% Analysis Date = 09/23/16 Pct Recovery = 41% Analysis Date = 09/23/16 Pct Recovery = 41% Analysis Date = 09/18/16 Pct Recovery = 42% Analysis Date = 09/18/16 Pct Recovery = 42% Analysis Date = 09/13/16 Pct Recovery = 42% Analysis Date = 09/13/16 Pct Recovery = 42% Analysis Date = 09/08/16 Pct Recovery = 42% Analysis Date = 09/08/16 Pct Recovery = 42% Analysis Date = 09/03/16 Pct Recovery = 42% Analysis Date = 09/03/16 Pct Recovery = 42% Analysis Date = 08/29/16 Pct Recovery = 42% Analysis Date = 08/29/16 Pct Recovery = 42% Analysis Date = 08/24/16 Pct Recovery = 42% Analysis Date = 08/24/16 Pct Recovery = 42% Analysis Date = 08/19/16 Pct Recovery = 42% Analysis Date = 08/19/16 Pct Recovery = 42% Analysis Date = 08/14/16 Pct Recovery = 42% Analysis Date = 08/14/16 Pct Recovery = 42% Analysis Date = 08/09/16 Pct Recovery = 42% Analysis Date = 08/09/16 Pct Recovery = 42% Analysis Date = 08/04/16 Pct Recovery = 42% Analysis Date = 08/04/16 Pct Recovery = 42% Analysis Date = 07/30/16 Pct Recovery = 42% Analysis Date = 07/30/16 Pct Recovery = 42% Analysis Date = 07/25/16 Pct Recovery = 43% Analysis Date = 07/25/16 Pct Recovery = 43% Analysis Date = 07/21/16 Pct Recovery = 43% Analysis Date = 07/21/16 Pct Recovery = 43% Analysis Date = 07/16/16 Pct Recovery = 43% Analysis Date = 07/16/16 Pct Recovery = 43% Analysis Date = 07/11/16 Pct Recovery = 43% Analysis Date = 07/11/16 Pct Recovery = 43% Analysis Date = 07/06/16 Pct Recovery = 43% Analysis Date = 07/06/16 Pct Recovery = 43% Analysis Date = 07/01/16 Pct Recovery = 44% Analysis Date = 07/01/16 Pct Recovery = 44% Analysis Date = 06/26/16 Pct Recovery = 44% Analysis Date = 06/26/16 Pct Recovery = 44% Analysis Date = 06/21/16 Pct Recovery = 44% Analysis Date = 06/21/16 Pct Recovery = 44% Analysis Date = 06/16/16 Pct Recovery = 44% Analysis Date = 06/16/16 Pct Recovery = 44% Analysis Date = 06/11/16 Pct Recovery = 44% Analysis Date = 06/11/16 Pct Recovery = 44% Analysis Date = 06/06/16 Pct Recovery = 45% Analysis Date = 06/06/16 Pct Recovery = 45% Analysis Date = 06/01/16 Pct Recovery = 45% Analysis Date = 06/01/16 Pct Recovery = 45% Analysis Date = 05/27/16 Pct Recovery = 45% Analysis Date = 05/27/16 Pct Recovery = 45% Analysis Date = 05/22/16 Pct Recovery = 45% Analysis Date = 05/22/16 Pct Recovery = 45% Analysis Date = 05/17/16 Pct Recovery = 45% Analysis Date = 05/17/16 Pct Recovery = 45% Analysis Date = 05/12/16 Pct Recovery = 46% Analysis Date = 05/12/16 Pct Recovery = 46% Analysis Date = 05/07/16 Pct Recovery = 46% Analysis Date = 05/07/16 Pct Recovery = 46% Analysis Date = 05/02/16 Pct Recovery = 46% Analysis Date = 05/02/16 Pct Recovery = 46% Analysis Date = 04/28/16 Pct Recovery = 46% Analysis Date = 04/28/16 Pct Recovery = 46% Analysis Date = 04/23/16 Pct Recovery = 47% Analysis Date = 04/23/16 Pct Recovery = 47% Analysis Date = 04/18/16 Pct Recovery = 47% Analysis Date = 04/18/16 Pct Recovery = 47% Analysis Date = 04/13/16 Pct Recovery = 47% Analysis Date = 04/13/16 Pct Recovery = 47% Analysis Date = 04/08/16 Pct Recovery = 47% Analysis Date = 04/08/16 Pct Recovery = 47% Analysis Date = 04/03/16 Pct Recovery = 47% Analysis Date = 04/03/16 Pct Recovery = 47% Analysis Date = 03/29/16 Pct Recovery = 48% Analysis Date = 03/29/16 Pct Recovery = 48% Analysis Date = 03/24/16 Pct Recovery = 48% Analysis Date = 03/24/16 Pct Recovery = 48% Analysis Date = 03/19/16 Pct Recovery = 48% Analysis Date = 03/19/16 Pct Recovery = 48% Analysis Date = 03/14/16 Pct Recovery = 48% Analysis Date = 03/14/16 Pct Recovery = 48% Analysis Date = 03/09/16 Pct Recovery = 48% Analysis Date = 03/09/16 Pct Recovery = 48% Analysis Date = 03/04/16 Pct Recovery = 49% Analysis Date = 03/04/16 Pct Recovery = 49% Analysis Date = 02/28/16 Pct Recovery = 49% Analysis Date = 02/28/16 Pct Recovery = 49% Analysis Date = 02/23/16 Pct Recovery = 49% Analysis Date = 02/23/16 Pct Recovery = 49% Analysis Date = 02/18/16 Pct Recovery = 49% Analysis Date = 02/18/16 Pct Recovery = 49% Analysis Date = 02/13/16 Pct Recovery = 50% Analysis Date = 02/13/16 Pct Recovery = 50% Analysis Date = 02/09/16 Pct Recovery = 50% Analysis Date = 02/09/16 Pct Recovery = 50% Analysis Date = 02/04/16 Pct Recovery = 50% Analysis Date = 02/04/16 Pct Recovery = 50% Analysis Date = 01/30/16 Pct Recovery = 50% Analysis Date = 01/30/16 Pct Recovery = 50% Analysis Date = 01/25/16 Pct Recovery = 51% Analysis Date = 01/25/16 Pct Recovery = 51% Analysis Date = 01/20/16 Pct Recovery = 51% Analysis Date = 01/20/16 Pct Recovery = 51% Analysis Date = 01/15/16 Pct Recovery = 51% Analysis Date = 01/15/16 Pct Recovery = 51% Analysis Date = 01/10/16 Pct Recovery = 51% Analysis Date = 01/10/16 Pct Recovery = 51% Analysis Date = 01/05/16 Pct Recovery = 52% Analysis Date = 01/05/16 Pct Recovery = 52% Analysis Date = 12/31/15 Pct Recovery = 52% Analysis Date = 12/31/15 Pct Recovery = 52% Analysis Date = 12/26/15 Pct Recovery = 52% Analysis Date = 12/26/15 Pct Recovery = 52% Analysis Date = 12/21/15 Pct Recovery = 52% Analysis Date = 12/21/15 Pct Recovery = 52% Analysis Date = 12/16/15 Pct Recovery = 53% Analysis Date = 12/16/15 Pct Recovery = 53% Analysis Date = 12/11/15 Pct Recovery = 53% Analysis Date = 12/11/15 Pct Recovery = 53% Analysis Date = 12/06/15 Pct Recovery = 53% Analysis Date = 12/06/15 Pct Recovery = 53% Analysis Date = 12/01/15 Pct Recovery = 54% Analysis Date = 12/01/15 Pct Recovery = 54% Analysis Date = 11/26/15 Pct Recovery = 54% Analysis Date = 11/26/15 Pct Recovery = 54% Analysis Date = 11/21/15 Pct Recovery = 54% Analysis Date = 11/21/15 Pct Recovery = 54% Analysis Date = 11/17/15 Pct Recovery = 54% Analysis Date = 11/17/15 Pct Recovery = 54% Analysis Date = 11/12/15 Pct Recovery = 55% Analysis Date = 11/12/15 Pct Recovery = 55% Analysis Date = 11/07/15 Pct Recovery = 55% Analysis Date = 11/07/15 Pct Recovery = 55% Analysis Date = 11/02/15 Pct Recovery = 55% Analysis Date = 11/02/15 Pct Recovery = 55% Analysis Date = 10/28/15 Pct Recovery = 55% Analysis Date = 10/28/15 Pct Recovery = 55% Analysis Date = 10/23/15 Pct Recovery = 56% Analysis Date = 10/23/15 Pct Recovery = 56% Analysis Date = 10/18/15 Pct Recovery = 56% Analysis Date = 10/18/15 Pct Recovery = 56% Analysis Date = 10/13/15 Pct Recovery = 56% Analysis Date = 10/13/15 Pct Recovery = 56% Analysis Date = 10/08/15 Pct Recovery = 57% Analysis Date = 10/08/15 Pct Recovery = 57% Analysis Date = 10/03/15 Pct Recovery = 57% Analysis Date = 10/03/15 Pct Recovery = 57% Analysis Date = 09/28/15 Pct Recovery = 57% Analysis Date = 09/28/15 Pct Recovery = 57% Analysis Date = 09/23/15 Pct Recovery = 57% Analysis Date = 09/23/15 Pct Recovery = 57% Analysis Date = 09/18/15 Pct Recovery = 58% Analysis Date = 09/18/15 Pct Recovery = 58% Analysis Date = 09/13/15 Pct Recovery = 58% Analysis Date = 09/13/15 Pct Recovery = 58% Analysis Date = 09/08/15 Pct Recovery = 58% Analysis Date = 09/08/15 Pct Recovery = 58% Analysis Date = 09/03/15 Pct Recovery = 58% Analysis Date = 09/03/15 Pct Recovery = 58% Analysis Date = 08/29/15 Pct Recovery = 59% Analysis Date = 08/29/15 Pct Recovery = 59% Analysis Date = 08/25/15 Pct Recovery = 59% Analysis Date = 08/25/15 Pct Recovery = 59% Analysis Date = 08/20/15 Pct Recovery = 59% Analysis Date = 08/20/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/15/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 59% Analysis Date = 08/10/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 08/05/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 59% Analysis Date = 07/31/15 Pct Recovery = 59% Analysis Date = 07/26/15 Pct Recovery = 60% Analysis Date = 07/26/15 Pct Recovery = 60% Analysis Date = 07/21/15 Pct Recovery = 60% Analysis Date = 07/21/15 Pct Recovery = 60% Analysis Date = 07/16/15 Pct Recovery = 60% Analysis Date = 07/16/15 Pct Recovery = 60% Analysis Date = 07/11/15 Pct Recovery = 60% Analysis Date = 07/11/15 Pct Recovery = 60% Analysis Date = 07/06/15 Pct Recovery = 60% Analysis Date = 07/06/15 Pct Recovery = 60% Analysis Date = 07/01/15 Pct Recovery = 60% Analysis Date = 07/01/15 Pct Recovery = 60% Analysis Date = 06/26/15 Pct Recovery = 60% Analysis Date = 06/26/15 Pct Recovery = 60% Analysis Date = 06/21/15 Pct Recovery = 60% Analysis Date = 06/21/15 Pct Recovery = 60% Analysis Date = 06/16/15 Pct Recovery = 61% Analysis Date = 06/16/15 Pct Recovery = 61% Analysis Date = 06/11/15 Pct Recovery = 61% Analysis Date = 06/11/15 Pct Recovery = 61% Analysis Date = 06/07/15 Pct Recovery = 61% Analysis Date = 06/07/15 Pct Recovery = 61% Analysis Date = 06/02/15 Pct Recovery = 61% Analysis Date = 06/02/15 Pct Recovery = 61% Analysis Date = 05/28/15 Pct Recovery = 61% Analysis Date = 05/28/15 Pct Recovery = 61% Analysis Date = 05/23/15 Pct Recovery = 61% Analysis Date = 05/23/15 Pct Recovery = 61% Analysis Date = 05/18/15 Pct Recovery = 61% Analysis Date = 05/18/15 Pct Recovery = 61% Analysis Date = 05/13/15 Pct Recovery = 61% Analysis Date = 05/13/15 Pct Recovery = 61% Analysis Date = 05/08/15 Pct Recovery = 62% Analysis Date = 05/08/15 Pct Recovery = 62% Analysis Date = 05/03/15 Pct Recovery = 62% Analysis Date = 05/03/15 Pct Recovery = 62% Analysis Date = 04/28/15 Pct Recovery = 62% Analysis Date = 04/28/15 Pct Recovery = 62% Analysis Date = 04/23/15 Pct Recovery = 62% Analysis Date = 04/23/15 Pct Recovery = 62% Analysis Date = 04/18/15 Pct Recovery = 61% Analysis Date = 04/18/15 Pct Recovery = 61% Analysis Date = 04/13/15 Pct Recovery = 61% Analysis Date = 04/13/15 Pct Recovery = 61% Analysis Date = 04/08/15 Pct Recovery = 61% Analysis Date = 04/08/15 Pct Recovery = 61% Analysis Date = 04/03/15 Pct Recovery = 61% Analysis Date = 04/03/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/29/15 Pct Recovery = 61% Analysis Date = 03/24/15 Pct Recovery = 61% Analysis Date = 03/24/15 Pct Recovery = 61% Analysis Date = 03/19/15 Pct Recovery = 61% Analysis Date = 03/19/15 Pct Recovery = 61% Analysis Date = 03/15/15 Pct Recovery = 61% Analysis Date = 03/15/15 Pct Recovery = 61% Analysis Date = 03/10/15 Pct Recovery = 61% Analysis Date = 03/10/15 Pct Recovery = 61% Analysis Date = 03/05/15 Pct Recovery = 61% Analysis Date = 03/05/15 Pct Recovery = 61% Analysis Date = 02/28/15 Pct Recovery = 61% Analysis Date = 02/28/15 Pct Recovery = 61% Analysis Date = 02/23/15 Pct Recovery = 61% Analysis Date = 02/23/15 Pct Recovery = 61% Analysis Date = 02/18/15 Pct Recovery = 61% Analysis Date = 02/18/15 Pct Recovery = 61% Analysis Date = 02/13/15 Pct Recovery = 61% Analysis Date = 02/13/15 Pct Recovery = 61% Analysis Date = 02/08/15 Pct Recovery = 60% Analysis Date = 02/08/15 Pct Recovery = 60% Analysis Date = 02/03/15 Pct Recovery = 60% Analysis Date = 02/03/15 Pct Recovery = 60% Analysis Date = 01/29/15 Pct Recovery = 60% Analysis Date = 01/29/15 Pct Recovery = 60% Analysis Date = 01/24/15 Pct Recovery = 60% Analysis Date = 01/24/15 Pct Recovery = 60% Analysis Date = 01/19/15 Pct Recovery = 60% Analysis Date = 01/19/15 Pct Recovery = 60% Analysis Date = 01/14/15 Pct Recovery = 60% Analysis Date = 01/14/15 Pct Recovery = 60% Analysis Date = 01/09/15 Pct Recovery = 60% Analysis Date = 01/09/15 Pct Recovery = 60% Analysis Date = 01/04/15 Pct Recovery = 60% Analysis Date = 01/04/15 Pct Recovery = 60% Analysis Date = 12/30/14 Pct Recovery = 60% Analysis Date = 12/30/14 Pct Recovery = 60% Analysis Date = 12/25/14 Pct Recovery = 59% Analysis Date = 12/25/14 Pct Recovery = 59% Analysis Date = 12/21/14 Pct Recovery = 59% Analysis Date = 12/21/14 Pct Recovery = 59% Analysis Date = 12/16/14 Pct Recovery = 59% Analysis Date = 12/16/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/11/14 Pct Recovery = 59% Analysis Date = 12/06/14 Pct Recovery = 59% Analysis Date = 12/06/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 12/01/14 Pct Recovery = 59% Analysis Date = 11/26/14 Pct Recovery = 59% Analysis Date = 11/26/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 59% Analysis Date = 11/21/14 Pct Recovery = 59% Analysis Date = 11/16/14 Pct Recovery = 59% Analysis Date = 11/16/14 Pct Recovery = 59% Analysis Date = 11/11/14 Pct Recovery = 59% Analysis Date = 11/11/14 Pct Recovery = 59% Analysis Date = 11/06/14 Pct Recovery = 58% Analysis Date = 11/06/14 Pct Recovery = 58% Analysis Date = 11/01/14 Pct Recovery = 58% Analysis Date = 11/01/14 Pct Recovery = 58% Analysis Date = 10/27/14 Pct Recovery = 58% Analysis Date = 10/27/14 Pct Recovery = 58% Analysis Date = 10/22/14 Pct Recovery = 58% Analysis Date = 10/22/14 Pct Recovery = 58% Analysis Date = 10/17/14 Pct Recovery = 58% Analysis Date = 10/17/14 Pct Recovery = 58% Analysis Date = 10/12/14 Pct Recovery = 58% Analysis Date = 10/12/14 Pct Recovery = 58% Analysis Date = 10/07/14 Pct Recovery = 58% Analysis Date = 10/07/14 Pct Recovery = 58% Analysis Date = 10/03/14 Pct Recovery = 58% Analysis Date = 10/03/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/23/14 Pct Recovery = 58% Analysis Date = 09/23/14 Pct Recovery = 58% Analysis Date = 09/18/14 Pct Recovery = 57% Analysis Date = 09/18/14 Pct Recovery = 57% Analysis Date = 09/13/14 Pct Recovery = 57% Analysis Date = 09/13/14 Pct Recovery = 57% Analysis Date = 09/08/14 Pct Recovery = 57% Analysis Date = 09/08/14 Pct Recovery = 57% Analysis Date = 09/03/14 Pct Recovery = 57% Analysis Date = 09/03/14 Pct Recovery = 57% Analysis Date = 08/29/14 Pct Recovery = 57% Analysis Date = 08/29/14 Pct Recovery = 57% Analysis Date = 08/24/14 Pct Recovery = 57% Analysis Date = 08/24/14 Pct Recovery = 57% Analysis Date = 08/19/14 Pct Recovery = 57% Analysis Date = 08/19/14 Pct Recovery = 57% Analysis Date = 08/14/14 Pct Recovery = 57% Analysis Date = 08/14/14 Pct Recovery = 57% Analysis Date = 08/09/14 Pct Recovery = 57% Analysis Date = 08/09/14 Pct Recovery = 57% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 07/30/14 Pct Recovery = 56% Analysis Date = 07/30/14 Pct Recovery = 56% Analysis Date = 07/25/14 Pct Recovery = 56% Analysis Date = 07/25/14 Pct Recovery = 56% Analysis Date = 07/20/14 Pct Recovery = 56% Analysis Date = 07/20/14 Pct Recovery = 56% Analysis Date = 07/15/14 Pct Recovery = 56% Analysis Date = 07/15/14 Pct Recovery = 56% Analysis Date = 07/11/14 Pct Recovery = 56% Analysis Date = 07/11/14 Pct Recovery = 56% Analysis Date = 07/06/14 Pct Recovery = 56% Analysis Date = 07/06/14 Pct Recovery = 56% Analysis Date = 07/01/14 Pct Recovery = 56% Analysis Date = 07/01/14 Pct Recovery = 56% Analysis Date = 06/26/14 Pct Recovery = 56% Analysis Date = 06/26/14 Pct Recovery = 56% Analysis Date = 06/21/14 Pct Recovery = 55% Analysis Date = 06/21/14 Pct Recovery = 55% Analysis Date = 06/16/14 Pct Recovery = 55% Analysis Date = 06/16/14 Pct Recovery = 55% Analysis Date = 06/11/14 Pct Recovery = 55% Analysis Date = 06/11/14 Pct Recovery = 55% Analysis Date = 06/06/14 Pct Recovery = 55% Analysis Date = 06/06/14 Pct Recovery = 55% Analysis Date = 06/01/14 Pct Recovery = 55% Analysis Date = 06/01/14 Pct Recovery = 55% Analysis Date = 05/27/14 Pct Recovery = 55% Analysis Date = 05/27/14 Pct Recovery = 55% Analysis Date = 05/22/14 Pct Recovery = 55% Analysis Date = 05/22/14 Pct Recovery = 55% Analysis Date = 05/17/14 Pct Recovery = 55% Analysis Date = 05/17/14 Pct Recovery = 55% Analysis Date = 05/12/14 Pct Recovery = 55% Analysis Date = 05/12/14 Pct Recovery = 55% Analysis Date = 05/07/14 Pct Recovery = 54% Analysis Date = 05/07/14 Pct Recovery = 54% Analysis Date = 05/02/14 Pct Recovery = 54% Analysis Date = 05/02/14 Pct Recovery = 54% Analysis Date = 04/27/14 Pct Recovery = 54% Analysis Date = 04/27/14 Pct Recovery = 54% Analysis Date = 04/23/14 Pct Recovery = 54% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NICOTINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 72 52% 26% 47% 22%
Total 72 52% 26% 47% 22%

Sample Statistics
NICOTINE

Characteristic N % % Basis
Plotted 72 94% Spiked
Estimated Values 22 29% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 77 .  
False Negatives 3 4% 3 out of 77
Not Spiked 38 .  
False Positives 3 8% 3 out of 38