BQS OBSP Determination:
TIOTROPIUM
METHOD: 2440 , TESTIDCODE: 67508LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 15% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 17% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 76% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 60% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 14% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 21% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 18% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 30% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 34% Analysis Date = 03/11/15 SpikeMix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Pct Recovery = 55% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 39% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 26% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 10% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 6% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 60% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 49% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 32% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 16% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 19% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 16% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 7% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 16% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 55% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 53% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 3% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 4% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 50% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 53% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 14% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 45% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 23% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 52% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 42% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 29% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 28% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 6% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 32% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 34% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 160% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 36% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 31% Analysis Date = 01/19/17 Pct Recovery = 19% Analysis Date = 01/14/17 Pct Recovery = 19% Analysis Date = 01/14/17 Pct Recovery = 19% Analysis Date = 01/09/17 Pct Recovery = 20% Analysis Date = 01/09/17 Pct Recovery = 20% Analysis Date = 01/05/17 Pct Recovery = 20% Analysis Date = 01/05/17 Pct Recovery = 20% Analysis Date = 12/31/16 Pct Recovery = 20% Analysis Date = 12/31/16 Pct Recovery = 20% Analysis Date = 12/27/16 Pct Recovery = 20% Analysis Date = 12/27/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/18/16 Pct Recovery = 21% Analysis Date = 12/18/16 Pct Recovery = 21% Analysis Date = 12/13/16 Pct Recovery = 21% Analysis Date = 12/13/16 Pct Recovery = 21% Analysis Date = 12/09/16 Pct Recovery = 21% Analysis Date = 12/09/16 Pct Recovery = 21% Analysis Date = 12/04/16 Pct Recovery = 21% Analysis Date = 12/04/16 Pct Recovery = 21% Analysis Date = 11/30/16 Pct Recovery = 21% Analysis Date = 11/30/16 Pct Recovery = 21% Analysis Date = 11/25/16 Pct Recovery = 21% Analysis Date = 11/25/16 Pct Recovery = 21% Analysis Date = 11/20/16 Pct Recovery = 22% Analysis Date = 11/20/16 Pct Recovery = 22% Analysis Date = 11/16/16 Pct Recovery = 22% Analysis Date = 11/16/16 Pct Recovery = 22% Analysis Date = 11/11/16 Pct Recovery = 22% Analysis Date = 11/11/16 Pct Recovery = 22% Analysis Date = 11/07/16 Pct Recovery = 22% Analysis Date = 11/07/16 Pct Recovery = 22% Analysis Date = 11/02/16 Pct Recovery = 22% Analysis Date = 11/02/16 Pct Recovery = 22% Analysis Date = 10/29/16 Pct Recovery = 23% Analysis Date = 10/29/16 Pct Recovery = 23% Analysis Date = 10/24/16 Pct Recovery = 23% Analysis Date = 10/24/16 Pct Recovery = 23% Analysis Date = 10/20/16 Pct Recovery = 23% Analysis Date = 10/20/16 Pct Recovery = 23% Analysis Date = 10/15/16 Pct Recovery = 23% Analysis Date = 10/15/16 Pct Recovery = 23% Analysis Date = 10/11/16 Pct Recovery = 23% Analysis Date = 10/11/16 Pct Recovery = 23% Analysis Date = 10/06/16 Pct Recovery = 24% Analysis Date = 10/06/16 Pct Recovery = 24% Analysis Date = 10/02/16 Pct Recovery = 24% Analysis Date = 10/02/16 Pct Recovery = 24% Analysis Date = 09/27/16 Pct Recovery = 24% Analysis Date = 09/27/16 Pct Recovery = 24% Analysis Date = 09/22/16 Pct Recovery = 24% Analysis Date = 09/22/16 Pct Recovery = 24% Analysis Date = 09/18/16 Pct Recovery = 24% Analysis Date = 09/18/16 Pct Recovery = 24% Analysis Date = 09/13/16 Pct Recovery = 24% Analysis Date = 09/13/16 Pct Recovery = 24% Analysis Date = 09/09/16 Pct Recovery = 25% Analysis Date = 09/09/16 Pct Recovery = 25% Analysis Date = 09/04/16 Pct Recovery = 25% Analysis Date = 09/04/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/31/16 Pct Recovery = 25% Analysis Date = 08/26/16 Pct Recovery = 25% Analysis Date = 08/26/16 Pct Recovery = 25% Analysis Date = 08/22/16 Pct Recovery = 25% Analysis Date = 08/22/16 Pct Recovery = 25% Analysis Date = 08/17/16 Pct Recovery = 26% Analysis Date = 08/17/16 Pct Recovery = 26% Analysis Date = 08/13/16 Pct Recovery = 26% Analysis Date = 08/13/16 Pct Recovery = 26% Analysis Date = 08/08/16 Pct Recovery = 26% Analysis Date = 08/08/16 Pct Recovery = 26% Analysis Date = 08/04/16 Pct Recovery = 26% Analysis Date = 08/04/16 Pct Recovery = 26% Analysis Date = 07/30/16 Pct Recovery = 27% Analysis Date = 07/30/16 Pct Recovery = 27% Analysis Date = 07/25/16 Pct Recovery = 27% Analysis Date = 07/25/16 Pct Recovery = 27% Analysis Date = 07/21/16 Pct Recovery = 27% Analysis Date = 07/21/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/16/16 Pct Recovery = 27% Analysis Date = 07/12/16 Pct Recovery = 28% Analysis Date = 07/12/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/07/16 Pct Recovery = 28% Analysis Date = 07/03/16 Pct Recovery = 28% Analysis Date = 07/03/16 Pct Recovery = 28% Analysis Date = 06/28/16 Pct Recovery = 28% Analysis Date = 06/28/16 Pct Recovery = 28% Analysis Date = 06/24/16 Pct Recovery = 29% Analysis Date = 06/24/16 Pct Recovery = 29% Analysis Date = 06/19/16 Pct Recovery = 29% Analysis Date = 06/19/16 Pct Recovery = 29% Analysis Date = 06/15/16 Pct Recovery = 29% Analysis Date = 06/15/16 Pct Recovery = 29% Analysis Date = 06/10/16 Pct Recovery = 29% Analysis Date = 06/10/16 Pct Recovery = 29% Analysis Date = 06/06/16 Pct Recovery = 30% Analysis Date = 06/06/16 Pct Recovery = 30% Analysis Date = 06/01/16 Pct Recovery = 30% Analysis Date = 06/01/16 Pct Recovery = 30% Analysis Date = 05/27/16 Pct Recovery = 30% Analysis Date = 05/27/16 Pct Recovery = 30% Analysis Date = 05/23/16 Pct Recovery = 30% Analysis Date = 05/23/16 Pct Recovery = 30% Analysis Date = 05/18/16 Pct Recovery = 31% Analysis Date = 05/18/16 Pct Recovery = 31% Analysis Date = 05/14/16 Pct Recovery = 31% Analysis Date = 05/14/16 Pct Recovery = 31% Analysis Date = 05/09/16 Pct Recovery = 31% Analysis Date = 05/09/16 Pct Recovery = 31% Analysis Date = 05/05/16 Pct Recovery = 31% Analysis Date = 05/05/16 Pct Recovery = 31% Analysis Date = 04/30/16 Pct Recovery = 32% Analysis Date = 04/30/16 Pct Recovery = 32% Analysis Date = 04/26/16 Pct Recovery = 32% Analysis Date = 04/26/16 Pct Recovery = 32% Analysis Date = 04/21/16 Pct Recovery = 32% Analysis Date = 04/21/16 Pct Recovery = 32% Analysis Date = 04/17/16 Pct Recovery = 32% Analysis Date = 04/17/16 Pct Recovery = 32% Analysis Date = 04/12/16 Pct Recovery = 33% Analysis Date = 04/12/16 Pct Recovery = 33% Analysis Date = 04/07/16 Pct Recovery = 33% Analysis Date = 04/07/16 Pct Recovery = 33% Analysis Date = 04/03/16 Pct Recovery = 33% Analysis Date = 04/03/16 Pct Recovery = 33% Analysis Date = 03/29/16 Pct Recovery = 33% Analysis Date = 03/29/16 Pct Recovery = 33% Analysis Date = 03/25/16 Pct Recovery = 34% Analysis Date = 03/25/16 Pct Recovery = 34% Analysis Date = 03/20/16 Pct Recovery = 34% Analysis Date = 03/20/16 Pct Recovery = 34% Analysis Date = 03/16/16 Pct Recovery = 34% Analysis Date = 03/16/16 Pct Recovery = 34% Analysis Date = 03/11/16 Pct Recovery = 34% Analysis Date = 03/11/16 Pct Recovery = 34% Analysis Date = 03/07/16 Pct Recovery = 35% Analysis Date = 03/07/16 Pct Recovery = 35% Analysis Date = 03/02/16 Pct Recovery = 35% Analysis Date = 03/02/16 Pct Recovery = 35% Analysis Date = 02/27/16 Pct Recovery = 35% Analysis Date = 02/27/16 Pct Recovery = 35% Analysis Date = 02/22/16 Pct Recovery = 35% Analysis Date = 02/22/16 Pct Recovery = 35% Analysis Date = 02/18/16 Pct Recovery = 35% Analysis Date = 02/18/16 Pct Recovery = 35% Analysis Date = 02/13/16 Pct Recovery = 35% Analysis Date = 02/13/16 Pct Recovery = 35% Analysis Date = 02/08/16 Pct Recovery = 36% Analysis Date = 02/08/16 Pct Recovery = 36% Analysis Date = 02/04/16 Pct Recovery = 36% Analysis Date = 02/04/16 Pct Recovery = 36% Analysis Date = 01/30/16 Pct Recovery = 36% Analysis Date = 01/30/16 Pct Recovery = 36% Analysis Date = 01/26/16 Pct Recovery = 36% Analysis Date = 01/26/16 Pct Recovery = 36% Analysis Date = 01/21/16 Pct Recovery = 36% Analysis Date = 01/21/16 Pct Recovery = 36% Analysis Date = 01/17/16 Pct Recovery = 36% Analysis Date = 01/17/16 Pct Recovery = 36% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/12/16 Pct Recovery = 36% Analysis Date = 01/08/16 Pct Recovery = 37% Analysis Date = 01/08/16 Pct Recovery = 37% Analysis Date = 01/03/16 Pct Recovery = 37% Analysis Date = 01/03/16 Pct Recovery = 37% Analysis Date = 12/30/15 Pct Recovery = 37% Analysis Date = 12/30/15 Pct Recovery = 37% Analysis Date = 12/25/15 Pct Recovery = 37% Analysis Date = 12/25/15 Pct Recovery = 37% Analysis Date = 12/21/15 Pct Recovery = 37% Analysis Date = 12/21/15 Pct Recovery = 37% Analysis Date = 12/16/15 Pct Recovery = 37% Analysis Date = 12/16/15 Pct Recovery = 37% Analysis Date = 12/11/15 Pct Recovery = 37% Analysis Date = 12/11/15 Pct Recovery = 37% Analysis Date = 12/07/15 Pct Recovery = 38% Analysis Date = 12/07/15 Pct Recovery = 38% Analysis Date = 12/02/15 Pct Recovery = 38% Analysis Date = 12/02/15 Pct Recovery = 38% Analysis Date = 11/28/15 Pct Recovery = 38% Analysis Date = 11/28/15 Pct Recovery = 38% Analysis Date = 11/23/15 Pct Recovery = 38% Analysis Date = 11/23/15 Pct Recovery = 38% Analysis Date = 11/19/15 Pct Recovery = 38% Analysis Date = 11/19/15 Pct Recovery = 38% Analysis Date = 11/14/15 Pct Recovery = 39% Analysis Date = 11/14/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/10/15 Pct Recovery = 39% Analysis Date = 11/05/15 Pct Recovery = 39% Analysis Date = 11/05/15 Pct Recovery = 39% Analysis Date = 11/01/15 Pct Recovery = 40% Analysis Date = 11/01/15 Pct Recovery = 40% Analysis Date = 10/27/15 Pct Recovery = 40% Analysis Date = 10/27/15 Pct Recovery = 40% Analysis Date = 10/23/15 Pct Recovery = 40% Analysis Date = 10/23/15 Pct Recovery = 40% Analysis Date = 10/18/15 Pct Recovery = 41% Analysis Date = 10/18/15 Pct Recovery = 41% Analysis Date = 10/13/15 Pct Recovery = 41% Analysis Date = 10/13/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/09/15 Pct Recovery = 41% Analysis Date = 10/04/15 Pct Recovery = 42% Analysis Date = 10/04/15 Pct Recovery = 42% Analysis Date = 09/30/15 Pct Recovery = 42% Analysis Date = 09/30/15 Pct Recovery = 42% Analysis Date = 09/25/15 Pct Recovery = 42% Analysis Date = 09/25/15 Pct Recovery = 42% Analysis Date = 09/21/15 Pct Recovery = 43% Analysis Date = 09/21/15 Pct Recovery = 43% Analysis Date = 09/16/15 Pct Recovery = 43% Analysis Date = 09/16/15 Pct Recovery = 43% Analysis Date = 09/12/15 Pct Recovery = 43% Analysis Date = 09/12/15 Pct Recovery = 43% Analysis Date = 09/07/15 Pct Recovery = 44% Analysis Date = 09/07/15 Pct Recovery = 44% Analysis Date = 09/03/15 Pct Recovery = 44% Analysis Date = 09/03/15 Pct Recovery = 44% Analysis Date = 08/29/15 Pct Recovery = 44% Analysis Date = 08/29/15 Pct Recovery = 44% Analysis Date = 08/24/15 Pct Recovery = 44% Analysis Date = 08/24/15 Pct Recovery = 44% Analysis Date = 08/20/15 Pct Recovery = 45% Analysis Date = 08/20/15 Pct Recovery = 45% Analysis Date = 08/15/15 Pct Recovery = 45% Analysis Date = 08/15/15 Pct Recovery = 45% Analysis Date = 08/11/15 Pct Recovery = 45% Analysis Date = 08/11/15 Pct Recovery = 45% Analysis Date = 08/06/15 Pct Recovery = 45% Analysis Date = 08/06/15 Pct Recovery = 45% Analysis Date = 08/02/15 Pct Recovery = 45% Analysis Date = 08/02/15 Pct Recovery = 45% Analysis Date = 07/28/15 Pct Recovery = 45% Analysis Date = 07/28/15 Pct Recovery = 45% Analysis Date = 07/24/15 Pct Recovery = 45% Analysis Date = 07/24/15 Pct Recovery = 45% Analysis Date = 07/19/15 Pct Recovery = 45% Analysis Date = 07/19/15 Pct Recovery = 45% Analysis Date = 07/15/15 Pct Recovery = 46% Analysis Date = 07/15/15 Pct Recovery = 46% Analysis Date = 07/10/15 Pct Recovery = 46% Analysis Date = 07/10/15 Pct Recovery = 46% Analysis Date = 07/06/15 Pct Recovery = 46% Analysis Date = 07/06/15 Pct Recovery = 46% Analysis Date = 07/01/15 Pct Recovery = 45% Analysis Date = 07/01/15 Pct Recovery = 45% Analysis Date = 06/26/15 Pct Recovery = 45% Analysis Date = 06/26/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 45% Analysis Date = 06/22/15 Pct Recovery = 45% Analysis Date = 06/17/15 Pct Recovery = 45% Analysis Date = 06/17/15 Pct Recovery = 45% Analysis Date = 06/13/15 Pct Recovery = 44% Analysis Date = 06/13/15 Pct Recovery = 44% Analysis Date = 06/08/15 Pct Recovery = 44% Analysis Date = 06/08/15 Pct Recovery = 44% Analysis Date = 06/04/15 Pct Recovery = 44% Analysis Date = 06/04/15 Pct Recovery = 44% Analysis Date = 05/30/15 Pct Recovery = 43% Analysis Date = 05/30/15 Pct Recovery = 43% Analysis Date = 05/26/15 Pct Recovery = 43% Analysis Date = 05/26/15 Pct Recovery = 43% Analysis Date = 05/21/15 Pct Recovery = 43% Analysis Date = 05/21/15 Pct Recovery = 43% Analysis Date = 05/17/15 Pct Recovery = 43% Analysis Date = 05/17/15 Pct Recovery = 43% Analysis Date = 05/12/15 Pct Recovery = 42% Analysis Date = 05/12/15 Pct Recovery = 42% Analysis Date = 05/08/15 Pct Recovery = 42% Analysis Date = 05/08/15 Pct Recovery = 42% Analysis Date = 05/03/15 Pct Recovery = 42% Analysis Date = 05/03/15 Pct Recovery = 42% Analysis Date = 04/28/15 Pct Recovery = 42% Analysis Date = 04/28/15 Pct Recovery = 42% Analysis Date = 04/24/15 Pct Recovery = 41% Analysis Date = 04/24/15 Pct Recovery = 41% Analysis Date = 04/19/15 Pct Recovery = 41% Analysis Date = 04/19/15 Pct Recovery = 41% Analysis Date = 04/15/15 Pct Recovery = 41% Analysis Date = 04/15/15 Pct Recovery = 41% Analysis Date = 04/10/15 Pct Recovery = 41% Analysis Date = 04/10/15 Pct Recovery = 41% Analysis Date = 04/06/15 Pct Recovery = 40% Analysis Date = 04/06/15 Pct Recovery = 40% Analysis Date = 04/01/15 Pct Recovery = 40% Analysis Date = 04/01/15 Pct Recovery = 40% Analysis Date = 03/28/15 Pct Recovery = 40% Analysis Date = 03/28/15 Pct Recovery = 40% Analysis Date = 03/23/15 Pct Recovery = 39% Analysis Date = 03/23/15 Pct Recovery = 39% Analysis Date = 03/19/15 Pct Recovery = 39% Analysis Date = 03/19/15 Pct Recovery = 39% Analysis Date = 03/14/15 Pct Recovery = 39% Analysis Date = 03/14/15 Pct Recovery = 39% Analysis Date = 03/10/15 Pct Recovery = 39% Analysis Date = 03/10/15 Pct Recovery = 39% Analysis Date = 03/05/15 Pct Recovery = 38% Analysis Date = 03/05/15 Pct Recovery = 38% Analysis Date = 02/28/15 Pct Recovery = 38% Analysis Date = 02/28/15 Pct Recovery = 38% Analysis Date = 02/24/15 Pct Recovery = 38% Analysis Date = 02/24/15 Pct Recovery = 38% Analysis Date = 02/19/15 Pct Recovery = 38% Analysis Date = 02/19/15 Pct Recovery = 38% Analysis Date = 02/15/15 Pct Recovery = 37% Analysis Date = 02/15/15 Pct Recovery = 37% Analysis Date = 02/10/15 Pct Recovery = 37% Analysis Date = 02/10/15 Pct Recovery = 37% Analysis Date = 02/06/15 Pct Recovery = 37% Analysis Date = 02/06/15 Pct Recovery = 37% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 02/01/15 Pct Recovery = 36% Analysis Date = 01/28/15 Pct Recovery = 36% Analysis Date = 01/28/15 Pct Recovery = 36% Analysis Date = 01/23/15 Pct Recovery = 36% Analysis Date = 01/23/15 Pct Recovery = 36% Analysis Date = 01/19/15 Pct Recovery = 36% Analysis Date = 01/19/15 Pct Recovery = 36% Analysis Date = 01/14/15 Pct Recovery = 35% Analysis Date = 01/14/15 Pct Recovery = 35% Analysis Date = 01/09/15 Pct Recovery = 35% Analysis Date = 01/09/15 Pct Recovery = 35% Analysis Date = 01/05/15 Pct Recovery = 35% Analysis Date = 01/05/15 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/31/14 Pct Recovery = 35% Analysis Date = 12/27/14 Pct Recovery = 34% Analysis Date = 12/27/14 Pct Recovery = 34% Analysis Date = 12/22/14 Pct Recovery = 34% Analysis Date = 12/22/14 Pct Recovery = 34% Analysis Date = 12/18/14 Pct Recovery = 34% Analysis Date = 12/18/14 Pct Recovery = 34% Analysis Date = 12/13/14 Pct Recovery = 34% Analysis Date = 12/13/14 Pct Recovery = 34% Analysis Date = 12/09/14 Pct Recovery = 33% Analysis Date = 12/09/14 Pct Recovery = 33% Analysis Date = 12/04/14 Pct Recovery = 33% Analysis Date = 12/04/14 Pct Recovery = 33% Analysis Date = 11/30/14 Pct Recovery = 33% Analysis Date = 11/30/14 Pct Recovery = 33% Analysis Date = 11/25/14 Pct Recovery = 32% Analysis Date = 11/25/14 Pct Recovery = 32% Analysis Date = 11/21/14 Pct Recovery = 32% Analysis Date = 11/21/14 Pct Recovery = 32% Analysis Date = 11/16/14 Pct Recovery = 32% Analysis Date = 11/16/14 Pct Recovery = 32% Analysis Date = 11/11/14 Pct Recovery = 31% Analysis Date = 11/11/14 Pct Recovery = 31% Analysis Date = 11/07/14 Pct Recovery = 31% Analysis Date = 11/07/14 Pct Recovery = 31% Analysis Date = 11/02/14 Pct Recovery = 31% Analysis Date = 11/02/14 Pct Recovery = 31% Analysis Date = 10/29/14 Pct Recovery = 30% Analysis Date = 10/29/14 Pct Recovery = 30% Analysis Date = 10/24/14 Pct Recovery = 30% Analysis Date = 10/24/14 Pct Recovery = 30% Analysis Date = 10/20/14 Pct Recovery = 30% Analysis Date = 10/20/14 Pct Recovery = 30% Analysis Date = 10/15/14 Pct Recovery = 29% Analysis Date = 10/15/14 Pct Recovery = 29% Analysis Date = 10/11/14 Pct Recovery = 29% Analysis Date = 10/11/14 Pct Recovery = 29% Analysis Date = 10/06/14 Pct Recovery = 28% Analysis Date = 10/06/14 Pct Recovery = 28% Analysis Date = 10/02/14 Pct Recovery = 28% Analysis Date = 10/02/14 Pct Recovery = 28% Analysis Date = 09/27/14 Pct Recovery = 28% Analysis Date = 09/27/14 Pct Recovery = 28% Analysis Date = 09/23/14 Pct Recovery = 27% Analysis Date = 09/23/14 Pct Recovery = 27% Analysis Date = 09/18/14 Pct Recovery = 27% Analysis Date = 09/18/14 Pct Recovery = 27% Analysis Date = 09/13/14 Pct Recovery = 27% Analysis Date = 09/13/14 Pct Recovery = 27% Analysis Date = 09/09/14 Pct Recovery = 26% Analysis Date = 09/09/14 Pct Recovery = 26% Analysis Date = 09/04/14 Pct Recovery = 26% Analysis Date = 09/04/14 Pct Recovery = 26% Analysis Date = 08/31/14 Pct Recovery = 25% Analysis Date = 08/31/14 Pct Recovery = 25% Analysis Date = 08/26/14 Pct Recovery = 25% Analysis Date = 08/26/14 Pct Recovery = 25% Analysis Date = 08/22/14 Pct Recovery = 25% Analysis Date = 08/22/14 Pct Recovery = 25% Analysis Date = 08/17/14 Pct Recovery = 24% Analysis Date = 08/17/14 Pct Recovery = 24% Analysis Date = 08/13/14 Pct Recovery = 24% Analysis Date = 08/13/14 Pct Recovery = 24% Analysis Date = 08/08/14 Pct Recovery = 23% Analysis Date = 08/08/14 Pct Recovery = 23% Analysis Date = 08/04/14 Pct Recovery = 23% Analysis Date = 08/04/14 Pct Recovery = 23% Analysis Date = 07/30/14 Pct Recovery = 23% Analysis Date = 07/30/14 Pct Recovery = 23% Analysis Date = 07/26/14 Pct Recovery = 22% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TIOTROPIUM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 33% 2% 32% 4%
>= Reporting Level 41 33% 27% 28% 24%
Total 44 33% 26% 30% 23%

Sample Statistics
TIOTROPIUM

Characteristic N % % Basis
Plotted 44 85% Spiked
Estimated Values 44 85% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 52 .  
False Negatives 6 12% 6 out of 52
Not Spiked 63 .  
False Positives 0 0% 0 out of 62