BQS OBSP Determination:
RALOXIFENE
METHOD: 2440 , TESTIDCODE: 67530LCM56
Open Data Set

Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 242% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 249% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 45% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 36% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 12% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 39% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 25% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 22% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 23% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 42% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 41% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 25% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 43% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 27% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 52% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 24% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 13% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 15% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 34% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 45% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 13% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 18% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 52% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 97% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 59% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 31% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 51% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 51% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 52% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 7% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 20% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 14% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 19% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 19% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 7% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 78% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 35% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 102% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 99% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 53% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 72% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 40% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 30% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 30% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 37% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 30% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 34% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 12% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 22% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 41% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 32% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 28% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 20% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 66% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 62% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 38% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 52% Analysis Date = 01/04/17 Pct Recovery = 51% Analysis Date = 12/31/16 Pct Recovery = 51% Analysis Date = 12/31/16 Pct Recovery = 51% Analysis Date = 12/26/16 Pct Recovery = 51% Analysis Date = 12/26/16 Pct Recovery = 51% Analysis Date = 12/21/16 Pct Recovery = 51% Analysis Date = 12/21/16 Pct Recovery = 51% Analysis Date = 12/16/16 Pct Recovery = 51% Analysis Date = 12/16/16 Pct Recovery = 51% Analysis Date = 12/11/16 Pct Recovery = 51% Analysis Date = 12/11/16 Pct Recovery = 51% Analysis Date = 12/07/16 Pct Recovery = 51% Analysis Date = 12/07/16 Pct Recovery = 51% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 12/02/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/27/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 52% Analysis Date = 11/22/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/17/16 Pct Recovery = 52% Analysis Date = 11/13/16 Pct Recovery = 52% Analysis Date = 11/13/16 Pct Recovery = 52% Analysis Date = 11/08/16 Pct Recovery = 52% Analysis Date = 11/08/16 Pct Recovery = 52% Analysis Date = 11/03/16 Pct Recovery = 52% Analysis Date = 11/03/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/29/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/24/16 Pct Recovery = 52% Analysis Date = 10/20/16 Pct Recovery = 52% Analysis Date = 10/20/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/10/16 Pct Recovery = 52% Analysis Date = 10/10/16 Pct Recovery = 52% Analysis Date = 10/05/16 Pct Recovery = 52% Analysis Date = 10/05/16 Pct Recovery = 52% Analysis Date = 09/30/16 Pct Recovery = 52% Analysis Date = 09/30/16 Pct Recovery = 52% Analysis Date = 09/26/16 Pct Recovery = 52% Analysis Date = 09/26/16 Pct Recovery = 52% Analysis Date = 09/21/16 Pct Recovery = 52% Analysis Date = 09/21/16 Pct Recovery = 52% Analysis Date = 09/16/16 Pct Recovery = 52% Analysis Date = 09/16/16 Pct Recovery = 52% Analysis Date = 09/11/16 Pct Recovery = 52% Analysis Date = 09/11/16 Pct Recovery = 52% Analysis Date = 09/06/16 Pct Recovery = 52% Analysis Date = 09/06/16 Pct Recovery = 52% Analysis Date = 09/02/16 Pct Recovery = 52% Analysis Date = 09/02/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 52% Analysis Date = 08/23/16 Pct Recovery = 52% Analysis Date = 08/23/16 Pct Recovery = 52% Analysis Date = 08/18/16 Pct Recovery = 52% Analysis Date = 08/18/16 Pct Recovery = 52% Analysis Date = 08/13/16 Pct Recovery = 52% Analysis Date = 08/13/16 Pct Recovery = 52% Analysis Date = 08/09/16 Pct Recovery = 52% Analysis Date = 08/09/16 Pct Recovery = 52% Analysis Date = 08/04/16 Pct Recovery = 51% Analysis Date = 08/04/16 Pct Recovery = 51% Analysis Date = 07/30/16 Pct Recovery = 51% Analysis Date = 07/30/16 Pct Recovery = 51% Analysis Date = 07/25/16 Pct Recovery = 51% Analysis Date = 07/25/16 Pct Recovery = 51% Analysis Date = 07/20/16 Pct Recovery = 51% Analysis Date = 07/20/16 Pct Recovery = 51% Analysis Date = 07/16/16 Pct Recovery = 51% Analysis Date = 07/16/16 Pct Recovery = 51% Analysis Date = 07/11/16 Pct Recovery = 51% Analysis Date = 07/11/16 Pct Recovery = 51% Analysis Date = 07/06/16 Pct Recovery = 51% Analysis Date = 07/06/16 Pct Recovery = 51% Analysis Date = 07/01/16 Pct Recovery = 51% Analysis Date = 07/01/16 Pct Recovery = 51% Analysis Date = 06/26/16 Pct Recovery = 51% Analysis Date = 06/26/16 Pct Recovery = 51% Analysis Date = 06/22/16 Pct Recovery = 51% Analysis Date = 06/22/16 Pct Recovery = 51% Analysis Date = 06/17/16 Pct Recovery = 51% Analysis Date = 06/17/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/12/16 Pct Recovery = 51% Analysis Date = 06/07/16 Pct Recovery = 50% Analysis Date = 06/07/16 Pct Recovery = 50% Analysis Date = 06/02/16 Pct Recovery = 50% Analysis Date = 06/02/16 Pct Recovery = 50% Analysis Date = 05/29/16 Pct Recovery = 50% Analysis Date = 05/29/16 Pct Recovery = 50% Analysis Date = 05/24/16 Pct Recovery = 50% Analysis Date = 05/24/16 Pct Recovery = 50% Analysis Date = 05/19/16 Pct Recovery = 50% Analysis Date = 05/19/16 Pct Recovery = 50% Analysis Date = 05/14/16 Pct Recovery = 50% Analysis Date = 05/14/16 Pct Recovery = 50% Analysis Date = 05/09/16 Pct Recovery = 50% Analysis Date = 05/09/16 Pct Recovery = 50% Analysis Date = 05/05/16 Pct Recovery = 49% Analysis Date = 05/05/16 Pct Recovery = 49% Analysis Date = 04/30/16 Pct Recovery = 49% Analysis Date = 04/30/16 Pct Recovery = 49% Analysis Date = 04/25/16 Pct Recovery = 49% Analysis Date = 04/25/16 Pct Recovery = 49% Analysis Date = 04/20/16 Pct Recovery = 48% Analysis Date = 04/20/16 Pct Recovery = 48% Analysis Date = 04/15/16 Pct Recovery = 48% Analysis Date = 04/15/16 Pct Recovery = 48% Analysis Date = 04/11/16 Pct Recovery = 47% Analysis Date = 04/11/16 Pct Recovery = 47% Analysis Date = 04/06/16 Pct Recovery = 47% Analysis Date = 04/06/16 Pct Recovery = 47% Analysis Date = 04/01/16 Pct Recovery = 46% Analysis Date = 04/01/16 Pct Recovery = 46% Analysis Date = 03/27/16 Pct Recovery = 46% Analysis Date = 03/27/16 Pct Recovery = 46% Analysis Date = 03/22/16 Pct Recovery = 45% Analysis Date = 03/22/16 Pct Recovery = 45% Analysis Date = 03/18/16 Pct Recovery = 45% Analysis Date = 03/18/16 Pct Recovery = 45% Analysis Date = 03/13/16 Pct Recovery = 44% Analysis Date = 03/13/16 Pct Recovery = 44% Analysis Date = 03/08/16 Pct Recovery = 44% Analysis Date = 03/08/16 Pct Recovery = 44% Analysis Date = 03/03/16 Pct Recovery = 44% Analysis Date = 03/03/16 Pct Recovery = 44% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/27/16 Pct Recovery = 43% Analysis Date = 02/23/16 Pct Recovery = 43% Analysis Date = 02/23/16 Pct Recovery = 43% Analysis Date = 02/18/16 Pct Recovery = 42% Analysis Date = 02/18/16 Pct Recovery = 42% Analysis Date = 02/13/16 Pct Recovery = 42% Analysis Date = 02/13/16 Pct Recovery = 42% Analysis Date = 02/08/16 Pct Recovery = 41% Analysis Date = 02/08/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 02/03/16 Pct Recovery = 41% Analysis Date = 01/30/16 Pct Recovery = 40% Analysis Date = 01/30/16 Pct Recovery = 40% Analysis Date = 01/25/16 Pct Recovery = 40% Analysis Date = 01/25/16 Pct Recovery = 40% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/20/16 Pct Recovery = 39% Analysis Date = 01/15/16 Pct Recovery = 39% Analysis Date = 01/15/16 Pct Recovery = 39% Analysis Date = 01/10/16 Pct Recovery = 39% Analysis Date = 01/10/16 Pct Recovery = 39% Analysis Date = 01/06/16 Pct Recovery = 38% Analysis Date = 01/06/16 Pct Recovery = 38% Analysis Date = 01/01/16 Pct Recovery = 38% Analysis Date = 01/01/16 Pct Recovery = 38% Analysis Date = 12/27/15 Pct Recovery = 37% Analysis Date = 12/27/15 Pct Recovery = 37% Analysis Date = 12/22/15 Pct Recovery = 37% Analysis Date = 12/22/15 Pct Recovery = 37% Analysis Date = 12/17/15 Pct Recovery = 36% Analysis Date = 12/17/15 Pct Recovery = 36% Analysis Date = 12/13/15 Pct Recovery = 36% Analysis Date = 12/13/15 Pct Recovery = 36% Analysis Date = 12/08/15 Pct Recovery = 35% Analysis Date = 12/08/15 Pct Recovery = 35% Analysis Date = 12/03/15 Pct Recovery = 35% Analysis Date = 12/03/15 Pct Recovery = 35% Analysis Date = 11/28/15 Pct Recovery = 35% Analysis Date = 11/28/15 Pct Recovery = 35% Analysis Date = 11/23/15 Pct Recovery = 34% Analysis Date = 11/23/15 Pct Recovery = 34% Analysis Date = 11/19/15 Pct Recovery = 34% Analysis Date = 11/19/15 Pct Recovery = 34% Analysis Date = 11/14/15 Pct Recovery = 34% Analysis Date = 11/14/15 Pct Recovery = 34% Analysis Date = 11/09/15 Pct Recovery = 34% Analysis Date = 11/09/15 Pct Recovery = 34% Analysis Date = 11/04/15 Pct Recovery = 33% Analysis Date = 11/04/15 Pct Recovery = 33% Analysis Date = 10/30/15 Pct Recovery = 33% Analysis Date = 10/30/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/16/15 Pct Recovery = 33% Analysis Date = 10/16/15 Pct Recovery = 33% Analysis Date = 10/11/15 Pct Recovery = 32% Analysis Date = 10/11/15 Pct Recovery = 32% Analysis Date = 10/06/15 Pct Recovery = 32% Analysis Date = 10/06/15 Pct Recovery = 32% Analysis Date = 10/02/15 Pct Recovery = 32% Analysis Date = 10/02/15 Pct Recovery = 32% Analysis Date = 09/27/15 Pct Recovery = 32% Analysis Date = 09/27/15 Pct Recovery = 32% Analysis Date = 09/22/15 Pct Recovery = 32% Analysis Date = 09/22/15 Pct Recovery = 32% Analysis Date = 09/17/15 Pct Recovery = 32% Analysis Date = 09/17/15 Pct Recovery = 32% Analysis Date = 09/12/15 Pct Recovery = 31% Analysis Date = 09/12/15 Pct Recovery = 31% Analysis Date = 09/08/15 Pct Recovery = 31% Analysis Date = 09/08/15 Pct Recovery = 31% Analysis Date = 09/03/15 Pct Recovery = 31% Analysis Date = 09/03/15 Pct Recovery = 31% Analysis Date = 08/29/15 Pct Recovery = 31% Analysis Date = 08/29/15 Pct Recovery = 31% Analysis Date = 08/24/15 Pct Recovery = 31% Analysis Date = 08/24/15 Pct Recovery = 31% Analysis Date = 08/19/15 Pct Recovery = 30% Analysis Date = 08/19/15 Pct Recovery = 30% Analysis Date = 08/15/15 Pct Recovery = 30% Analysis Date = 08/15/15 Pct Recovery = 30% Analysis Date = 08/10/15 Pct Recovery = 30% Analysis Date = 08/10/15 Pct Recovery = 30% Analysis Date = 08/05/15 Pct Recovery = 30% Analysis Date = 08/05/15 Pct Recovery = 30% Analysis Date = 07/31/15 Pct Recovery = 30% Analysis Date = 07/31/15 Pct Recovery = 30% Analysis Date = 07/26/15 Pct Recovery = 30% Analysis Date = 07/26/15 Pct Recovery = 30% Analysis Date = 07/22/15 Pct Recovery = 30% Analysis Date = 07/22/15 Pct Recovery = 30% Analysis Date = 07/17/15 Pct Recovery = 30% Analysis Date = 07/17/15 Pct Recovery = 30% Analysis Date = 07/12/15 Pct Recovery = 30% Analysis Date = 07/12/15 Pct Recovery = 30% Analysis Date = 07/07/15 Pct Recovery = 30% Analysis Date = 07/07/15 Pct Recovery = 30% Analysis Date = 07/02/15 Pct Recovery = 30% Analysis Date = 07/02/15 Pct Recovery = 30% Analysis Date = 06/28/15 Pct Recovery = 30% Analysis Date = 06/28/15 Pct Recovery = 30% Analysis Date = 06/23/15 Pct Recovery = 30% Analysis Date = 06/23/15 Pct Recovery = 30% Analysis Date = 06/18/15 Pct Recovery = 31% Analysis Date = 06/18/15 Pct Recovery = 31% Analysis Date = 06/13/15 Pct Recovery = 31% Analysis Date = 06/13/15 Pct Recovery = 31% Analysis Date = 06/08/15 Pct Recovery = 31% Analysis Date = 06/08/15 Pct Recovery = 31% Analysis Date = 06/04/15 Pct Recovery = 31% Analysis Date = 06/04/15 Pct Recovery = 31% Analysis Date = 05/30/15 Pct Recovery = 31% Analysis Date = 05/30/15 Pct Recovery = 31% Analysis Date = 05/25/15 Pct Recovery = 31% Analysis Date = 05/25/15 Pct Recovery = 31% Analysis Date = 05/20/15 Pct Recovery = 31% Analysis Date = 05/20/15 Pct Recovery = 31% Analysis Date = 05/15/15 Pct Recovery = 31% Analysis Date = 05/15/15 Pct Recovery = 31% Analysis Date = 05/11/15 Pct Recovery = 31% Analysis Date = 05/11/15 Pct Recovery = 31% Analysis Date = 05/06/15 Pct Recovery = 31% Analysis Date = 05/06/15 Pct Recovery = 31% Analysis Date = 05/01/15 Pct Recovery = 32% Analysis Date = 05/01/15 Pct Recovery = 32% Analysis Date = 04/26/15 Pct Recovery = 32% Analysis Date = 04/26/15 Pct Recovery = 32% Analysis Date = 04/21/15 Pct Recovery = 32% Analysis Date = 04/21/15 Pct Recovery = 32% Analysis Date = 04/17/15 Pct Recovery = 33% Analysis Date = 04/17/15 Pct Recovery = 33% Analysis Date = 04/12/15 Pct Recovery = 33% Analysis Date = 04/12/15 Pct Recovery = 33% Analysis Date = 04/07/15 Pct Recovery = 33% Analysis Date = 04/07/15 Pct Recovery = 33% Analysis Date = 04/02/15 Pct Recovery = 34% Analysis Date = 04/02/15 Pct Recovery = 34% Analysis Date = 03/28/15 Pct Recovery = 34% Analysis Date = 03/28/15 Pct Recovery = 34% Analysis Date = 03/24/15 Pct Recovery = 34% Analysis Date = 03/24/15 Pct Recovery = 34% Analysis Date = 03/19/15 Pct Recovery = 35% Analysis Date = 03/19/15 Pct Recovery = 35% Analysis Date = 03/14/15 Pct Recovery = 35% Analysis Date = 03/14/15 Pct Recovery = 35% Analysis Date = 03/09/15 Pct Recovery = 36% Analysis Date = 03/09/15 Pct Recovery = 36% Analysis Date = 03/04/15 Pct Recovery = 36% Analysis Date = 03/04/15 Pct Recovery = 36% Analysis Date = 02/28/15 Pct Recovery = 36% Analysis Date = 02/28/15 Pct Recovery = 36% Analysis Date = 02/23/15 Pct Recovery = 37% Analysis Date = 02/23/15 Pct Recovery = 37% Analysis Date = 02/18/15 Pct Recovery = 37% Analysis Date = 02/18/15 Pct Recovery = 37% Analysis Date = 02/13/15 Pct Recovery = 38% Analysis Date = 02/13/15 Pct Recovery = 38% Analysis Date = 02/08/15 Pct Recovery = 38% Analysis Date = 02/08/15 Pct Recovery = 38% Analysis Date = 02/04/15 Pct Recovery = 38% Analysis Date = 02/04/15 Pct Recovery = 38% Analysis Date = 01/30/15 Pct Recovery = 39% Analysis Date = 01/30/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/25/15 Pct Recovery = 39% Analysis Date = 01/20/15 Pct Recovery = 39% Analysis Date = 01/20/15 Pct Recovery = 39% Analysis Date = 01/15/15 Pct Recovery = 40% Analysis Date = 01/15/15 Pct Recovery = 40% Analysis Date = 01/11/15 Pct Recovery = 40% Analysis Date = 01/11/15 Pct Recovery = 40% Analysis Date = 01/06/15 Pct Recovery = 41% Analysis Date = 01/06/15 Pct Recovery = 41% Analysis Date = 01/01/15 Pct Recovery = 41% Analysis Date = 01/01/15 Pct Recovery = 41% Analysis Date = 12/27/14 Pct Recovery = 42% Analysis Date = 12/27/14 Pct Recovery = 42% Analysis Date = 12/22/14 Pct Recovery = 42% Analysis Date = 12/22/14 Pct Recovery = 42% Analysis Date = 12/18/14 Pct Recovery = 43% Analysis Date = 12/18/14 Pct Recovery = 43% Analysis Date = 12/13/14 Pct Recovery = 43% Analysis Date = 12/13/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/08/14 Pct Recovery = 43% Analysis Date = 12/03/14 Pct Recovery = 44% Analysis Date = 12/03/14 Pct Recovery = 44% Analysis Date = 11/28/14 Pct Recovery = 44% Analysis Date = 11/28/14 Pct Recovery = 44% Analysis Date = 11/24/14 Pct Recovery = 45% Analysis Date = 11/24/14 Pct Recovery = 45% Analysis Date = 11/19/14 Pct Recovery = 45% Analysis Date = 11/19/14 Pct Recovery = 45% Analysis Date = 11/14/14 Pct Recovery = 46% Analysis Date = 11/14/14 Pct Recovery = 46% Analysis Date = 11/09/14 Pct Recovery = 46% Analysis Date = 11/09/14 Pct Recovery = 46% Analysis Date = 11/04/14 Pct Recovery = 47% Analysis Date = 11/04/14 Pct Recovery = 47% Analysis Date = 10/31/14 Pct Recovery = 47% Analysis Date = 10/31/14 Pct Recovery = 47% Analysis Date = 10/26/14 Pct Recovery = 48% Analysis Date = 10/26/14 Pct Recovery = 48% Analysis Date = 10/21/14 Pct Recovery = 48% Analysis Date = 10/21/14 Pct Recovery = 48% Analysis Date = 10/16/14 Pct Recovery = 49% Analysis Date = 10/16/14 Pct Recovery = 49% Analysis Date = 10/11/14 Pct Recovery = 49% Analysis Date = 10/11/14 Pct Recovery = 49% Analysis Date = 10/07/14 Pct Recovery = 49% Analysis Date = 10/07/14 Pct Recovery = 49% Analysis Date = 10/02/14 Pct Recovery = 50% Analysis Date = 10/02/14 Pct Recovery = 50% Analysis Date = 09/27/14 Pct Recovery = 50% Analysis Date = 09/27/14 Pct Recovery = 50% Analysis Date = 09/22/14 Pct Recovery = 51% Analysis Date = 09/22/14 Pct Recovery = 51% Analysis Date = 09/17/14 Pct Recovery = 51% Analysis Date = 09/17/14 Pct Recovery = 51% Analysis Date = 09/13/14 Pct Recovery = 52% Analysis Date = 09/13/14 Pct Recovery = 52% Analysis Date = 09/08/14 Pct Recovery = 52% Analysis Date = 09/08/14 Pct Recovery = 52% Analysis Date = 09/03/14 Pct Recovery = 53% Analysis Date = 09/03/14 Pct Recovery = 53% Analysis Date = 08/29/14 Pct Recovery = 53% Analysis Date = 08/29/14 Pct Recovery = 53% Analysis Date = 08/24/14 Pct Recovery = 54% Analysis Date = 08/24/14 Pct Recovery = 54% Analysis Date = 08/20/14 Pct Recovery = 54% Analysis Date = 08/20/14 Pct Recovery = 54% Analysis Date = 08/15/14 Pct Recovery = 55% Analysis Date = 08/15/14 Pct Recovery = 55% Analysis Date = 08/10/14 Pct Recovery = 55% Analysis Date = 08/10/14 Pct Recovery = 55% Analysis Date = 08/05/14 Pct Recovery = 56% Analysis Date = 08/05/14 Pct Recovery = 56% Analysis Date = 07/31/14 Pct Recovery = 56% Analysis Date = 07/31/14 Pct Recovery = 56% Analysis Date = 07/27/14 Pct Recovery = 57% Analysis Date = 07/27/14 Pct Recovery = 57% Analysis Date = 07/22/14 Pct Recovery = 57% Analysis Date = 07/22/14 Pct Recovery = 57% Analysis Date = 07/17/14 Pct Recovery = 58% Analysis Date = 07/17/14 Pct Recovery = 58% Analysis Date = 07/12/14 Pct Recovery = 58% Analysis Date = 07/12/14 Pct Recovery = 58% Analysis Date = 07/07/14 Pct Recovery = 59% Analysis Date = 07/07/14 Pct Recovery = 59% Analysis Date = 07/03/14 Pct Recovery = 59% Analysis Date = 07/03/14 Pct Recovery = 59% Analysis Date = 06/28/14 Pct Recovery = 60% Analysis Date = 06/28/14 Pct Recovery = 60% Analysis Date = 06/23/14 Pct Recovery = 60% Analysis Date = 06/23/14 Pct Recovery = 60% Analysis Date = 06/18/14 Pct Recovery = 61% Analysis Date = 06/18/14 Pct Recovery = 61% Analysis Date = 06/13/14 Pct Recovery = 62% Analysis Date = 06/13/14 Pct Recovery = 62% Analysis Date = 06/09/14 Pct Recovery = 62% Analysis Date = 06/09/14 Pct Recovery = 62% Analysis Date = 06/04/14 Pct Recovery = 63% Analysis Date = 06/04/14 Pct Recovery = 63% Analysis Date = 05/30/14 Pct Recovery = 63% Analysis Date = 05/30/14 Pct Recovery = 63% Analysis Date = 05/25/14 Pct Recovery = 64% Analysis Date = 05/25/14 Pct Recovery = 64% Analysis Date = 05/21/14 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
RALOXIFENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 46% 17% 46% 22%
>= Reporting Level 50 45% 47% 34% 23%
Total 60 45% 43% 36% 22%

Sample Statistics
RALOXIFENE

Characteristic N % % Basis
Plotted 60 80% Spiked
Estimated Values 60 80% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 75 .  
False Negatives 11 15% 11 out of 75
Not Spiked 40 .  
False Positives 0 0% 0 out of 40