BQS OBSP Determination:
NIZATIDINE
METHOD: 2440 , TESTIDCODE: 67479LCM56
Open Data Set

Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 38% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 28% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 16% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 8% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 6% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 16% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 23% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 56% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 58% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 57% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 53% Analysis Date = 12/06/14 SpikeMix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 13% Analysis Date = 10/25/14 SpikeMix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Pct Recovery = 33% Analysis Date = 10/11/14 SpikeMix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Pct Recovery = 37% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 61% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 10% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 9% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 34% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 39% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 16% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 14% Analysis Date = 04/30/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 84% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 48% Analysis Date = 02/10/15 SpikeMix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 28% Analysis Date = 12/07/14 SpikeMix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Pct Recovery = 35% Analysis Date = 09/12/14 SpikeMix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Pct Recovery = 39% Analysis Date = 08/16/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 72% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 58% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 45% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 44% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 23% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 80% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 33% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 8% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 11% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 67% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 69% Analysis Date = 12/16/16 Pct Recovery = 44% Analysis Date = 12/11/16 Pct Recovery = 43% Analysis Date = 12/11/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/06/16 Pct Recovery = 43% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/26/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/21/16 Pct Recovery = 41% Analysis Date = 11/16/16 Pct Recovery = 40% Analysis Date = 11/16/16 Pct Recovery = 40% Analysis Date = 11/12/16 Pct Recovery = 39% Analysis Date = 11/12/16 Pct Recovery = 39% Analysis Date = 11/07/16 Pct Recovery = 38% Analysis Date = 11/07/16 Pct Recovery = 38% Analysis Date = 11/02/16 Pct Recovery = 38% Analysis Date = 11/02/16 Pct Recovery = 38% Analysis Date = 10/28/16 Pct Recovery = 37% Analysis Date = 10/28/16 Pct Recovery = 37% Analysis Date = 10/23/16 Pct Recovery = 37% Analysis Date = 10/23/16 Pct Recovery = 37% Analysis Date = 10/18/16 Pct Recovery = 36% Analysis Date = 10/18/16 Pct Recovery = 36% Analysis Date = 10/14/16 Pct Recovery = 36% Analysis Date = 10/14/16 Pct Recovery = 36% Analysis Date = 10/09/16 Pct Recovery = 35% Analysis Date = 10/09/16 Pct Recovery = 35% Analysis Date = 10/04/16 Pct Recovery = 35% Analysis Date = 10/04/16 Pct Recovery = 35% Analysis Date = 09/29/16 Pct Recovery = 34% Analysis Date = 09/29/16 Pct Recovery = 34% Analysis Date = 09/24/16 Pct Recovery = 34% Analysis Date = 09/24/16 Pct Recovery = 34% Analysis Date = 09/19/16 Pct Recovery = 33% Analysis Date = 09/19/16 Pct Recovery = 33% Analysis Date = 09/15/16 Pct Recovery = 33% Analysis Date = 09/15/16 Pct Recovery = 33% Analysis Date = 09/10/16 Pct Recovery = 32% Analysis Date = 09/10/16 Pct Recovery = 32% Analysis Date = 09/05/16 Pct Recovery = 32% Analysis Date = 09/05/16 Pct Recovery = 32% Analysis Date = 08/31/16 Pct Recovery = 32% Analysis Date = 08/31/16 Pct Recovery = 32% Analysis Date = 08/26/16 Pct Recovery = 32% Analysis Date = 08/26/16 Pct Recovery = 32% Analysis Date = 08/21/16 Pct Recovery = 31% Analysis Date = 08/21/16 Pct Recovery = 31% Analysis Date = 08/17/16 Pct Recovery = 31% Analysis Date = 08/17/16 Pct Recovery = 31% Analysis Date = 08/12/16 Pct Recovery = 31% Analysis Date = 08/12/16 Pct Recovery = 31% Analysis Date = 08/07/16 Pct Recovery = 31% Analysis Date = 08/07/16 Pct Recovery = 31% Analysis Date = 08/02/16 Pct Recovery = 31% Analysis Date = 08/02/16 Pct Recovery = 31% Analysis Date = 07/28/16 Pct Recovery = 31% Analysis Date = 07/28/16 Pct Recovery = 31% Analysis Date = 07/23/16 Pct Recovery = 31% Analysis Date = 07/23/16 Pct Recovery = 31% Analysis Date = 07/18/16 Pct Recovery = 31% Analysis Date = 07/18/16 Pct Recovery = 31% Analysis Date = 07/14/16 Pct Recovery = 31% Analysis Date = 07/14/16 Pct Recovery = 31% Analysis Date = 07/09/16 Pct Recovery = 31% Analysis Date = 07/09/16 Pct Recovery = 31% Analysis Date = 07/04/16 Pct Recovery = 31% Analysis Date = 07/04/16 Pct Recovery = 31% Analysis Date = 06/29/16 Pct Recovery = 31% Analysis Date = 06/29/16 Pct Recovery = 31% Analysis Date = 06/24/16 Pct Recovery = 31% Analysis Date = 06/24/16 Pct Recovery = 31% Analysis Date = 06/19/16 Pct Recovery = 31% Analysis Date = 06/19/16 Pct Recovery = 31% Analysis Date = 06/15/16 Pct Recovery = 31% Analysis Date = 06/15/16 Pct Recovery = 31% Analysis Date = 06/10/16 Pct Recovery = 31% Analysis Date = 06/10/16 Pct Recovery = 31% Analysis Date = 06/05/16 Pct Recovery = 31% Analysis Date = 06/05/16 Pct Recovery = 31% Analysis Date = 05/31/16 Pct Recovery = 31% Analysis Date = 05/31/16 Pct Recovery = 31% Analysis Date = 05/26/16 Pct Recovery = 31% Analysis Date = 05/26/16 Pct Recovery = 31% Analysis Date = 05/21/16 Pct Recovery = 31% Analysis Date = 05/21/16 Pct Recovery = 31% Analysis Date = 05/17/16 Pct Recovery = 31% Analysis Date = 05/17/16 Pct Recovery = 31% Analysis Date = 05/12/16 Pct Recovery = 31% Analysis Date = 05/12/16 Pct Recovery = 31% Analysis Date = 05/07/16 Pct Recovery = 31% Analysis Date = 05/07/16 Pct Recovery = 31% Analysis Date = 05/02/16 Pct Recovery = 31% Analysis Date = 05/02/16 Pct Recovery = 31% Analysis Date = 04/27/16 Pct Recovery = 31% Analysis Date = 04/27/16 Pct Recovery = 31% Analysis Date = 04/22/16 Pct Recovery = 31% Analysis Date = 04/22/16 Pct Recovery = 31% Analysis Date = 04/18/16 Pct Recovery = 31% Analysis Date = 04/18/16 Pct Recovery = 31% Analysis Date = 04/13/16 Pct Recovery = 31% Analysis Date = 04/13/16 Pct Recovery = 31% Analysis Date = 04/08/16 Pct Recovery = 31% Analysis Date = 04/08/16 Pct Recovery = 31% Analysis Date = 04/03/16 Pct Recovery = 31% Analysis Date = 04/03/16 Pct Recovery = 31% Analysis Date = 03/29/16 Pct Recovery = 31% Analysis Date = 03/29/16 Pct Recovery = 31% Analysis Date = 03/24/16 Pct Recovery = 31% Analysis Date = 03/24/16 Pct Recovery = 31% Analysis Date = 03/19/16 Pct Recovery = 32% Analysis Date = 03/19/16 Pct Recovery = 32% Analysis Date = 03/15/16 Pct Recovery = 32% Analysis Date = 03/15/16 Pct Recovery = 32% Analysis Date = 03/10/16 Pct Recovery = 32% Analysis Date = 03/10/16 Pct Recovery = 32% Analysis Date = 03/05/16 Pct Recovery = 32% Analysis Date = 03/05/16 Pct Recovery = 32% Analysis Date = 02/29/16 Pct Recovery = 32% Analysis Date = 02/29/16 Pct Recovery = 32% Analysis Date = 02/24/16 Pct Recovery = 32% Analysis Date = 02/24/16 Pct Recovery = 32% Analysis Date = 02/19/16 Pct Recovery = 32% Analysis Date = 02/19/16 Pct Recovery = 32% Analysis Date = 02/15/16 Pct Recovery = 32% Analysis Date = 02/15/16 Pct Recovery = 32% Analysis Date = 02/10/16 Pct Recovery = 32% Analysis Date = 02/10/16 Pct Recovery = 32% Analysis Date = 02/05/16 Pct Recovery = 32% Analysis Date = 02/05/16 Pct Recovery = 32% Analysis Date = 01/31/16 Pct Recovery = 32% Analysis Date = 01/31/16 Pct Recovery = 32% Analysis Date = 01/26/16 Pct Recovery = 32% Analysis Date = 01/26/16 Pct Recovery = 32% Analysis Date = 01/21/16 Pct Recovery = 32% Analysis Date = 01/21/16 Pct Recovery = 32% Analysis Date = 01/17/16 Pct Recovery = 32% Analysis Date = 01/17/16 Pct Recovery = 32% Analysis Date = 01/12/16 Pct Recovery = 32% Analysis Date = 01/12/16 Pct Recovery = 32% Analysis Date = 01/07/16 Pct Recovery = 32% Analysis Date = 01/07/16 Pct Recovery = 32% Analysis Date = 01/02/16 Pct Recovery = 32% Analysis Date = 01/02/16 Pct Recovery = 32% Analysis Date = 12/28/15 Pct Recovery = 32% Analysis Date = 12/28/15 Pct Recovery = 32% Analysis Date = 12/23/15 Pct Recovery = 32% Analysis Date = 12/23/15 Pct Recovery = 32% Analysis Date = 12/19/15 Pct Recovery = 33% Analysis Date = 12/19/15 Pct Recovery = 33% Analysis Date = 12/14/15 Pct Recovery = 33% Analysis Date = 12/14/15 Pct Recovery = 33% Analysis Date = 12/09/15 Pct Recovery = 33% Analysis Date = 12/09/15 Pct Recovery = 33% Analysis Date = 12/04/15 Pct Recovery = 33% Analysis Date = 12/04/15 Pct Recovery = 33% Analysis Date = 11/29/15 Pct Recovery = 33% Analysis Date = 11/29/15 Pct Recovery = 33% Analysis Date = 11/24/15 Pct Recovery = 33% Analysis Date = 11/24/15 Pct Recovery = 33% Analysis Date = 11/19/15 Pct Recovery = 33% Analysis Date = 11/19/15 Pct Recovery = 33% Analysis Date = 11/15/15 Pct Recovery = 33% Analysis Date = 11/15/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/10/15 Pct Recovery = 33% Analysis Date = 11/05/15 Pct Recovery = 33% Analysis Date = 11/05/15 Pct Recovery = 33% Analysis Date = 10/31/15 Pct Recovery = 33% Analysis Date = 10/31/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/26/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/21/15 Pct Recovery = 33% Analysis Date = 10/17/15 Pct Recovery = 33% Analysis Date = 10/17/15 Pct Recovery = 33% Analysis Date = 10/12/15 Pct Recovery = 33% Analysis Date = 10/12/15 Pct Recovery = 33% Analysis Date = 10/07/15 Pct Recovery = 33% Analysis Date = 10/07/15 Pct Recovery = 33% Analysis Date = 10/02/15 Pct Recovery = 34% Analysis Date = 10/02/15 Pct Recovery = 34% Analysis Date = 09/27/15 Pct Recovery = 34% Analysis Date = 09/27/15 Pct Recovery = 34% Analysis Date = 09/22/15 Pct Recovery = 34% Analysis Date = 09/22/15 Pct Recovery = 34% Analysis Date = 09/18/15 Pct Recovery = 34% Analysis Date = 09/18/15 Pct Recovery = 34% Analysis Date = 09/13/15 Pct Recovery = 34% Analysis Date = 09/13/15 Pct Recovery = 34% Analysis Date = 09/08/15 Pct Recovery = 34% Analysis Date = 09/08/15 Pct Recovery = 34% Analysis Date = 09/03/15 Pct Recovery = 34% Analysis Date = 09/03/15 Pct Recovery = 34% Analysis Date = 08/29/15 Pct Recovery = 34% Analysis Date = 08/29/15 Pct Recovery = 34% Analysis Date = 08/24/15 Pct Recovery = 34% Analysis Date = 08/24/15 Pct Recovery = 34% Analysis Date = 08/20/15 Pct Recovery = 34% Analysis Date = 08/20/15 Pct Recovery = 34% Analysis Date = 08/15/15 Pct Recovery = 34% Analysis Date = 08/15/15 Pct Recovery = 34% Analysis Date = 08/10/15 Pct Recovery = 34% Analysis Date = 08/10/15 Pct Recovery = 34% Analysis Date = 08/05/15 Pct Recovery = 35% Analysis Date = 08/05/15 Pct Recovery = 35% Analysis Date = 07/31/15 Pct Recovery = 35% Analysis Date = 07/31/15 Pct Recovery = 35% Analysis Date = 07/26/15 Pct Recovery = 35% Analysis Date = 07/26/15 Pct Recovery = 35% Analysis Date = 07/21/15 Pct Recovery = 35% Analysis Date = 07/21/15 Pct Recovery = 35% Analysis Date = 07/17/15 Pct Recovery = 35% Analysis Date = 07/17/15 Pct Recovery = 35% Analysis Date = 07/12/15 Pct Recovery = 35% Analysis Date = 07/12/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/07/15 Pct Recovery = 35% Analysis Date = 07/02/15 Pct Recovery = 35% Analysis Date = 07/02/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/27/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/22/15 Pct Recovery = 35% Analysis Date = 06/18/15 Pct Recovery = 35% Analysis Date = 06/18/15 Pct Recovery = 35% Analysis Date = 06/13/15 Pct Recovery = 35% Analysis Date = 06/13/15 Pct Recovery = 35% Analysis Date = 06/08/15 Pct Recovery = 35% Analysis Date = 06/08/15 Pct Recovery = 35% Analysis Date = 06/03/15 Pct Recovery = 36% Analysis Date = 06/03/15 Pct Recovery = 36% Analysis Date = 05/29/15 Pct Recovery = 36% Analysis Date = 05/29/15 Pct Recovery = 36% Analysis Date = 05/24/15 Pct Recovery = 36% Analysis Date = 05/24/15 Pct Recovery = 36% Analysis Date = 05/20/15 Pct Recovery = 36% Analysis Date = 05/20/15 Pct Recovery = 36% Analysis Date = 05/15/15 Pct Recovery = 36% Analysis Date = 05/15/15 Pct Recovery = 36% Analysis Date = 05/10/15 Pct Recovery = 36% Analysis Date = 05/10/15 Pct Recovery = 36% Analysis Date = 05/05/15 Pct Recovery = 36% Analysis Date = 05/05/15 Pct Recovery = 36% Analysis Date = 04/30/15 Pct Recovery = 36% Analysis Date = 04/30/15 Pct Recovery = 36% Analysis Date = 04/25/15 Pct Recovery = 36% Analysis Date = 04/25/15 Pct Recovery = 36% Analysis Date = 04/21/15 Pct Recovery = 37% Analysis Date = 04/21/15 Pct Recovery = 37% Analysis Date = 04/16/15 Pct Recovery = 37% Analysis Date = 04/16/15 Pct Recovery = 37% Analysis Date = 04/11/15 Pct Recovery = 37% Analysis Date = 04/11/15 Pct Recovery = 37% Analysis Date = 04/06/15 Pct Recovery = 37% Analysis Date = 04/06/15 Pct Recovery = 37% Analysis Date = 04/01/15 Pct Recovery = 37% Analysis Date = 04/01/15 Pct Recovery = 37% Analysis Date = 03/27/15 Pct Recovery = 38% Analysis Date = 03/27/15 Pct Recovery = 38% Analysis Date = 03/22/15 Pct Recovery = 38% Analysis Date = 03/22/15 Pct Recovery = 38% Analysis Date = 03/18/15 Pct Recovery = 38% Analysis Date = 03/18/15 Pct Recovery = 38% Analysis Date = 03/13/15 Pct Recovery = 38% Analysis Date = 03/13/15 Pct Recovery = 38% Analysis Date = 03/08/15 Pct Recovery = 38% Analysis Date = 03/08/15 Pct Recovery = 38% Analysis Date = 03/03/15 Pct Recovery = 39% Analysis Date = 03/03/15 Pct Recovery = 39% Analysis Date = 02/26/15 Pct Recovery = 39% Analysis Date = 02/26/15 Pct Recovery = 39% Analysis Date = 02/21/15 Pct Recovery = 39% Analysis Date = 02/21/15 Pct Recovery = 39% Analysis Date = 02/17/15 Pct Recovery = 39% Analysis Date = 02/17/15 Pct Recovery = 39% Analysis Date = 02/12/15 Pct Recovery = 40% Analysis Date = 02/12/15 Pct Recovery = 40% Analysis Date = 02/07/15 Pct Recovery = 40% Analysis Date = 02/07/15 Pct Recovery = 40% Analysis Date = 02/02/15 Pct Recovery = 40% Analysis Date = 02/02/15 Pct Recovery = 40% Analysis Date = 01/28/15 Pct Recovery = 40% Analysis Date = 01/28/15 Pct Recovery = 40% Analysis Date = 01/23/15 Pct Recovery = 40% Analysis Date = 01/23/15 Pct Recovery = 40% Analysis Date = 01/19/15 Pct Recovery = 41% Analysis Date = 01/19/15 Pct Recovery = 41% Analysis Date = 01/14/15 Pct Recovery = 41% Analysis Date = 01/14/15 Pct Recovery = 41% Analysis Date = 01/09/15 Pct Recovery = 41% Analysis Date = 01/09/15 Pct Recovery = 41% Analysis Date = 01/04/15 Pct Recovery = 41% Analysis Date = 01/04/15 Pct Recovery = 41% Analysis Date = 12/30/14 Pct Recovery = 41% Analysis Date = 12/30/14 Pct Recovery = 41% Analysis Date = 12/25/14 Pct Recovery = 42% Analysis Date = 12/25/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/21/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/16/14 Pct Recovery = 42% Analysis Date = 12/11/14 Pct Recovery = 42% Analysis Date = 12/11/14 Pct Recovery = 42% Analysis Date = 12/06/14 Pct Recovery = 42% Analysis Date = 12/06/14 Pct Recovery = 42% Analysis Date = 12/01/14 Pct Recovery = 43% Analysis Date = 12/01/14 Pct Recovery = 43% Analysis Date = 11/26/14 Pct Recovery = 43% Analysis Date = 11/26/14 Pct Recovery = 43% Analysis Date = 11/21/14 Pct Recovery = 43% Analysis Date = 11/21/14 Pct Recovery = 43% Analysis Date = 11/17/14 Pct Recovery = 43% Analysis Date = 11/17/14 Pct Recovery = 43% Analysis Date = 11/12/14 Pct Recovery = 44% Analysis Date = 11/12/14 Pct Recovery = 44% Analysis Date = 11/07/14 Pct Recovery = 44% Analysis Date = 11/07/14 Pct Recovery = 44% Analysis Date = 11/02/14 Pct Recovery = 44% Analysis Date = 11/02/14 Pct Recovery = 44% Analysis Date = 10/28/14 Pct Recovery = 44% Analysis Date = 10/28/14 Pct Recovery = 44% Analysis Date = 10/23/14 Pct Recovery = 44% Analysis Date = 10/23/14 Pct Recovery = 44% Analysis Date = 10/19/14 Pct Recovery = 45% Analysis Date = 10/19/14 Pct Recovery = 45% Analysis Date = 10/14/14 Pct Recovery = 45% Analysis Date = 10/14/14 Pct Recovery = 45% Analysis Date = 10/09/14 Pct Recovery = 45% Analysis Date = 10/09/14 Pct Recovery = 45% Analysis Date = 10/04/14 Pct Recovery = 45% Analysis Date = 10/04/14 Pct Recovery = 45% Analysis Date = 09/29/14 Pct Recovery = 45% Analysis Date = 09/29/14 Pct Recovery = 45% Analysis Date = 09/24/14 Pct Recovery = 46% Analysis Date = 09/24/14 Pct Recovery = 46% Analysis Date = 09/20/14 Pct Recovery = 46% Analysis Date = 09/20/14 Pct Recovery = 46% Analysis Date = 09/15/14 Pct Recovery = 46% Analysis Date = 09/15/14 Pct Recovery = 46% Analysis Date = 09/10/14 Pct Recovery = 46% Analysis Date = 09/10/14 Pct Recovery = 46% Analysis Date = 09/05/14 Pct Recovery = 46% Analysis Date = 09/05/14 Pct Recovery = 46% Analysis Date = 08/31/14 Pct Recovery = 47% Analysis Date = 08/31/14 Pct Recovery = 47% Analysis Date = 08/26/14 Pct Recovery = 47% Analysis Date = 08/26/14 Pct Recovery = 47% Analysis Date = 08/22/14 Pct Recovery = 47% Analysis Date = 08/22/14 Pct Recovery = 47% Analysis Date = 08/17/14 Pct Recovery = 47% Analysis Date = 08/17/14 Pct Recovery = 47% Analysis Date = 08/12/14 Pct Recovery = 47% Analysis Date = 08/12/14 Pct Recovery = 47% Analysis Date = 08/07/14 Pct Recovery = 48% Analysis Date = 08/07/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 08/02/14 Pct Recovery = 48% Analysis Date = 07/28/14 Pct Recovery = 48% Analysis Date = 07/28/14 Pct Recovery = 48% Analysis Date = 07/23/14 Pct Recovery = 48% Analysis Date = 07/23/14 Pct Recovery = 48% Analysis Date = 07/19/14 Pct Recovery = 49% Analysis Date = 07/19/14 Pct Recovery = 49% Analysis Date = 07/14/14 Pct Recovery = 49% Analysis Date = 07/14/14 Pct Recovery = 49% Analysis Date = 07/09/14 Pct Recovery = 49% Analysis Date = 07/09/14 Pct Recovery = 49% Analysis Date = 07/04/14 Pct Recovery = 49% Analysis Date = 07/04/14 Pct Recovery = 49% Analysis Date = 06/29/14 Pct Recovery = 49% Analysis Date = 06/29/14 Pct Recovery = 49% Analysis Date = 06/24/14 Pct Recovery = 50% Analysis Date = 06/24/14 Pct Recovery = 50% Analysis Date = 06/20/14 Pct Recovery = 50% Analysis Date = 06/20/14 Pct Recovery = 50% Analysis Date = 06/15/14 Pct Recovery = 50% Analysis Date = 06/15/14 Pct Recovery = 50% Analysis Date = 06/10/14 Pct Recovery = 50% Analysis Date = 06/10/14 Pct Recovery = 50% Analysis Date = 06/05/14 Pct Recovery = 50% Analysis Date = 06/05/14 Pct Recovery = 50% Analysis Date = 05/31/14 Pct Recovery = 51% Analysis Date = 05/31/14 Pct Recovery = 51% Analysis Date = 05/26/14 Pct Recovery = 51% Analysis Date = 05/26/14 Pct Recovery = 51% Analysis Date = 05/22/14 Pct Recovery = 51% Analysis Date = 05/22/14 Pct Recovery = 51% Analysis Date = 05/17/14 Pct Recovery = 51% Analysis Date = 05/17/14 Pct Recovery = 51% Analysis Date = 05/12/14 Pct Recovery = 52% Analysis Date = 05/12/14 Pct Recovery = 52% Analysis Date = 05/07/14 Pct Recovery = 52% Analysis Date = 05/07/14 Pct Recovery = 52% Analysis Date = 05/02/14 Pct Recovery = 52% Analysis Date = 05/02/14 Pct Recovery = 52% Analysis Date = 04/27/14 Pct Recovery = 52% Analysis Date = 04/27/14 Pct Recovery = 52% Analysis Date = 04/23/14 Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NIZATIDINE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 49% 33% 67% 43%
>= Reporting Level 35 35% 21% 34% 27%
Total 38 37% 22% 34% 30%

Sample Statistics
NIZATIDINE

Characteristic N % % Basis
Plotted 38 49% Spiked
Estimated Values 38 49% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 77 .  
False Negatives 36 47% 36 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38