BQS OBSP Determination:
GLYBURIDE
METHOD: 2440 , TESTIDCODE: 68002LCM56
Open Data Set

Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 69% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 81% Analysis Date = 10/01/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 21% Analysis Date = 11/05/15 SpikeMix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Pct Recovery = 73% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 67% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 64% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 85% Analysis Date = 07/22/16 SpikeMix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Pct Recovery = 84% Analysis Date = 09/24/16 SpikeMix = Crescent EN160610015: 80 µl & Abs 061416: 80 µl Pct Recovery = 83% Analysis Date = 09/24/16 SpikeMix = Abs 061416: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 79% Analysis Date = 05/07/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 83% Analysis Date = 04/29/15 SpikeMix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 81% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 77% Analysis Date = 01/16/15 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 84% Analysis Date = 12/07/14 SpikeMix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Pct Recovery = 72% Analysis Date = 12/06/14 SpikeMix = Abs 041714: 15 µl & ERA 0319-14-05: 15 µl Pct Recovery = 74% Analysis Date = 08/28/14 SpikeMix = ERA 0319-14-04: 60 µl & ERA 0319-14-05: 60 µl Pct Recovery = 65% Analysis Date = 07/26/14 SpikeMix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Pct Recovery = 67% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 79% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 95% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 61% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 99% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 65% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 81% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Pct Recovery = 75% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 90% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 90% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 63% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 67% Analysis Date = 09/10/16 SpikeMix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 64% Analysis Date = 08/16/16 SpikeMix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Pct Recovery = 57% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 31% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 32% Analysis Date = 04/23/14 SpikeMix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Pct Recovery = 72% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 86% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 82% Analysis Date = 11/04/14 SpikeMix = Abs 041714: 8 µl & ERA 0319-14-05: 8 µl Pct Recovery = 65% Analysis Date = 10/24/14 SpikeMix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Pct Recovery = 80% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 62% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 78% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 31% Analysis Date = 08/30/14 SpikeMix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 75% Analysis Date = 07/13/14 SpikeMix = ERA 0319-14-04: 30 µl & ERA 0319-14-05: 30 µl Pct Recovery = 47% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 38% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 32% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 54% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 8% Analysis Date = 03/04/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 70% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 53% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 62% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 50% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 54% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 62% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 88% Analysis Date = 09/09/15 SpikeMix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Pct Recovery = 86% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 63% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 60% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 66% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 88% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 74% Analysis Date = 11/03/16 SpikeMix = Crescent EN160610015: 100 µl & ERA 04281604: 100 µl Pct Recovery = 73% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 68% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 69% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 64% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 70% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 68% Analysis Date = 12/16/16 SpikeMix = Crescent EN160610015: 40 µl & Abs 061416: 40 µl Pct Recovery = 61% Analysis Date = 01/18/17 Pct Recovery = 73% Analysis Date = 01/13/17 Pct Recovery = 73% Analysis Date = 01/13/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/03/17 Pct Recovery = 72% Analysis Date = 01/03/17 Pct Recovery = 72% Analysis Date = 12/29/16 Pct Recovery = 72% Analysis Date = 12/29/16 Pct Recovery = 72% Analysis Date = 12/24/16 Pct Recovery = 72% Analysis Date = 12/24/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/09/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 71% Analysis Date = 11/29/16 Pct Recovery = 71% Analysis Date = 11/29/16 Pct Recovery = 71% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/19/16 Pct Recovery = 70% Analysis Date = 11/19/16 Pct Recovery = 70% Analysis Date = 11/14/16 Pct Recovery = 70% Analysis Date = 11/14/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 69% Analysis Date = 11/04/16 Pct Recovery = 69% Analysis Date = 10/30/16 Pct Recovery = 69% Analysis Date = 10/30/16 Pct Recovery = 69% Analysis Date = 10/25/16 Pct Recovery = 69% Analysis Date = 10/25/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 68% Analysis Date = 10/15/16 Pct Recovery = 68% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/30/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/15/16 Pct Recovery = 67% Analysis Date = 09/15/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 67% Analysis Date = 08/31/16 Pct Recovery = 67% Analysis Date = 08/31/16 Pct Recovery = 67% Analysis Date = 08/26/16 Pct Recovery = 67% Analysis Date = 08/26/16 Pct Recovery = 67% Analysis Date = 08/21/16 Pct Recovery = 66% Analysis Date = 08/21/16 Pct Recovery = 66% Analysis Date = 08/16/16 Pct Recovery = 66% Analysis Date = 08/16/16 Pct Recovery = 66% Analysis Date = 08/11/16 Pct Recovery = 66% Analysis Date = 08/11/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/01/16 Pct Recovery = 66% Analysis Date = 08/01/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/17/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/07/16 Pct Recovery = 66% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 07/02/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/17/16 Pct Recovery = 65% Analysis Date = 06/12/16 Pct Recovery = 65% Analysis Date = 06/12/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 65% Analysis Date = 06/07/16 Pct Recovery = 65% Analysis Date = 06/02/16 Pct Recovery = 65% Analysis Date = 06/02/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/28/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/23/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/18/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/13/16 Pct Recovery = 65% Analysis Date = 05/08/16 Pct Recovery = 65% Analysis Date = 05/08/16 Pct Recovery = 65% Analysis Date = 05/03/16 Pct Recovery = 65% Analysis Date = 05/03/16 Pct Recovery = 65% Analysis Date = 04/28/16 Pct Recovery = 65% Analysis Date = 04/28/16 Pct Recovery = 65% Analysis Date = 04/23/16 Pct Recovery = 64% Analysis Date = 04/23/16 Pct Recovery = 64% Analysis Date = 04/18/16 Pct Recovery = 64% Analysis Date = 04/18/16 Pct Recovery = 64% Analysis Date = 04/13/16 Pct Recovery = 64% Analysis Date = 04/13/16 Pct Recovery = 64% Analysis Date = 04/08/16 Pct Recovery = 64% Analysis Date = 04/08/16 Pct Recovery = 64% Analysis Date = 04/03/16 Pct Recovery = 64% Analysis Date = 04/03/16 Pct Recovery = 64% Analysis Date = 03/29/16 Pct Recovery = 64% Analysis Date = 03/29/16 Pct Recovery = 64% Analysis Date = 03/24/16 Pct Recovery = 64% Analysis Date = 03/24/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/14/16 Pct Recovery = 65% Analysis Date = 03/14/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 03/09/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 02/28/16 Pct Recovery = 65% Analysis Date = 02/28/16 Pct Recovery = 65% Analysis Date = 02/23/16 Pct Recovery = 65% Analysis Date = 02/23/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/08/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 65% Analysis Date = 01/29/16 Pct Recovery = 65% Analysis Date = 01/24/16 Pct Recovery = 66% Analysis Date = 01/24/16 Pct Recovery = 66% Analysis Date = 01/19/16 Pct Recovery = 66% Analysis Date = 01/19/16 Pct Recovery = 66% Analysis Date = 01/14/16 Pct Recovery = 66% Analysis Date = 01/14/16 Pct Recovery = 66% Analysis Date = 01/09/16 Pct Recovery = 66% Analysis Date = 01/09/16 Pct Recovery = 66% Analysis Date = 01/04/16 Pct Recovery = 66% Analysis Date = 01/04/16 Pct Recovery = 66% Analysis Date = 12/30/15 Pct Recovery = 66% Analysis Date = 12/30/15 Pct Recovery = 66% Analysis Date = 12/25/15 Pct Recovery = 66% Analysis Date = 12/25/15 Pct Recovery = 66% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 67% Analysis Date = 12/10/15 Pct Recovery = 67% Analysis Date = 12/10/15 Pct Recovery = 67% Analysis Date = 12/05/15 Pct Recovery = 67% Analysis Date = 12/05/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 67% Analysis Date = 11/30/15 Pct Recovery = 67% Analysis Date = 11/25/15 Pct Recovery = 67% Analysis Date = 11/25/15 Pct Recovery = 67% Analysis Date = 11/20/15 Pct Recovery = 67% Analysis Date = 11/20/15 Pct Recovery = 67% Analysis Date = 11/15/15 Pct Recovery = 68% Analysis Date = 11/15/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 68% Analysis Date = 11/10/15 Pct Recovery = 68% Analysis Date = 11/05/15 Pct Recovery = 68% Analysis Date = 11/05/15 Pct Recovery = 68% Analysis Date = 10/31/15 Pct Recovery = 68% Analysis Date = 10/31/15 Pct Recovery = 68% Analysis Date = 10/26/15 Pct Recovery = 68% Analysis Date = 10/26/15 Pct Recovery = 68% Analysis Date = 10/21/15 Pct Recovery = 68% Analysis Date = 10/21/15 Pct Recovery = 68% Analysis Date = 10/16/15 Pct Recovery = 69% Analysis Date = 10/16/15 Pct Recovery = 69% Analysis Date = 10/11/15 Pct Recovery = 69% Analysis Date = 10/11/15 Pct Recovery = 69% Analysis Date = 10/06/15 Pct Recovery = 69% Analysis Date = 10/06/15 Pct Recovery = 69% Analysis Date = 10/01/15 Pct Recovery = 69% Analysis Date = 10/01/15 Pct Recovery = 69% Analysis Date = 09/26/15 Pct Recovery = 69% Analysis Date = 09/26/15 Pct Recovery = 69% Analysis Date = 09/21/15 Pct Recovery = 69% Analysis Date = 09/21/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/16/15 Pct Recovery = 69% Analysis Date = 09/11/15 Pct Recovery = 70% Analysis Date = 09/11/15 Pct Recovery = 70% Analysis Date = 09/05/15 Pct Recovery = 70% Analysis Date = 09/05/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/26/15 Pct Recovery = 70% Analysis Date = 08/26/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/16/15 Pct Recovery = 70% Analysis Date = 08/16/15 Pct Recovery = 70% Analysis Date = 08/11/15 Pct Recovery = 71% Analysis Date = 08/11/15 Pct Recovery = 71% Analysis Date = 08/06/15 Pct Recovery = 71% Analysis Date = 08/06/15 Pct Recovery = 71% Analysis Date = 08/01/15 Pct Recovery = 71% Analysis Date = 08/01/15 Pct Recovery = 71% Analysis Date = 07/27/15 Pct Recovery = 71% Analysis Date = 07/27/15 Pct Recovery = 71% Analysis Date = 07/22/15 Pct Recovery = 71% Analysis Date = 07/22/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/17/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/12/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 71% Analysis Date = 07/07/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 07/02/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 71% Analysis Date = 06/27/15 Pct Recovery = 71% Analysis Date = 06/22/15 Pct Recovery = 71% Analysis Date = 06/22/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/17/15 Pct Recovery = 71% Analysis Date = 06/12/15 Pct Recovery = 71% Analysis Date = 06/12/15 Pct Recovery = 71% Analysis Date = 06/07/15 Pct Recovery = 71% Analysis Date = 06/07/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 06/02/15 Pct Recovery = 71% Analysis Date = 05/28/15 Pct Recovery = 71% Analysis Date = 05/28/15 Pct Recovery = 71% Analysis Date = 05/23/15 Pct Recovery = 71% Analysis Date = 05/23/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 71% Analysis Date = 05/18/15 Pct Recovery = 71% Analysis Date = 05/13/15 Pct Recovery = 71% Analysis Date = 05/13/15 Pct Recovery = 71% Analysis Date = 05/08/15 Pct Recovery = 71% Analysis Date = 05/08/15 Pct Recovery = 71% Analysis Date = 05/03/15 Pct Recovery = 71% Analysis Date = 05/03/15 Pct Recovery = 71% Analysis Date = 04/28/15 Pct Recovery = 71% Analysis Date = 04/28/15 Pct Recovery = 71% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/23/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/18/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/13/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/08/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 04/03/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/29/15 Pct Recovery = 70% Analysis Date = 03/24/15 Pct Recovery = 70% Analysis Date = 03/24/15 Pct Recovery = 70% Analysis Date = 03/19/15 Pct Recovery = 70% Analysis Date = 03/19/15 Pct Recovery = 70% Analysis Date = 03/14/15 Pct Recovery = 70% Analysis Date = 03/14/15 Pct Recovery = 70% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/09/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 03/04/15 Pct Recovery = 69% Analysis Date = 02/27/15 Pct Recovery = 69% Analysis Date = 02/27/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/22/15 Pct Recovery = 69% Analysis Date = 02/17/15 Pct Recovery = 69% Analysis Date = 02/17/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/12/15 Pct Recovery = 69% Analysis Date = 02/07/15 Pct Recovery = 69% Analysis Date = 02/07/15 Pct Recovery = 69% Analysis Date = 02/02/15 Pct Recovery = 69% Analysis Date = 02/02/15 Pct Recovery = 69% Analysis Date = 01/28/15 Pct Recovery = 69% Analysis Date = 01/28/15 Pct Recovery = 69% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/23/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/18/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/13/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/08/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 01/03/15 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/29/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/24/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/19/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/14/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/09/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 68% Analysis Date = 12/04/14 Pct Recovery = 68% Analysis Date = 11/29/14 Pct Recovery = 67% Analysis Date = 11/29/14 Pct Recovery = 67% Analysis Date = 11/24/14 Pct Recovery = 67% Analysis Date = 11/24/14 Pct Recovery = 67% Analysis Date = 11/19/14 Pct Recovery = 67% Analysis Date = 11/19/14 Pct Recovery = 67% Analysis Date = 11/14/14 Pct Recovery = 67% Analysis Date = 11/14/14 Pct Recovery = 67% Analysis Date = 11/09/14 Pct Recovery = 67% Analysis Date = 11/09/14 Pct Recovery = 67% Analysis Date = 11/04/14 Pct Recovery = 67% Analysis Date = 11/04/14 Pct Recovery = 67% Analysis Date = 10/30/14 Pct Recovery = 67% Analysis Date = 10/30/14 Pct Recovery = 67% Analysis Date = 10/25/14 Pct Recovery = 67% Analysis Date = 10/25/14 Pct Recovery = 67% Analysis Date = 10/20/14 Pct Recovery = 67% Analysis Date = 10/20/14 Pct Recovery = 67% Analysis Date = 10/15/14 Pct Recovery = 67% Analysis Date = 10/15/14 Pct Recovery = 67% Analysis Date = 10/10/14 Pct Recovery = 66% Analysis Date = 10/10/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 10/05/14 Pct Recovery = 66% Analysis Date = 09/30/14 Pct Recovery = 66% Analysis Date = 09/30/14 Pct Recovery = 66% Analysis Date = 09/25/14 Pct Recovery = 66% Analysis Date = 09/25/14 Pct Recovery = 66% Analysis Date = 09/20/14 Pct Recovery = 66% Analysis Date = 09/20/14 Pct Recovery = 66% Analysis Date = 09/15/14 Pct Recovery = 66% Analysis Date = 09/15/14 Pct Recovery = 66% Analysis Date = 09/10/14 Pct Recovery = 66% Analysis Date = 09/10/14 Pct Recovery = 66% Analysis Date = 09/05/14 Pct Recovery = 66% Analysis Date = 09/05/14 Pct Recovery = 66% Analysis Date = 08/31/14 Pct Recovery = 66% Analysis Date = 08/31/14 Pct Recovery = 66% Analysis Date = 08/26/14 Pct Recovery = 66% Analysis Date = 08/26/14 Pct Recovery = 66% Analysis Date = 08/21/14 Pct Recovery = 65% Analysis Date = 08/21/14 Pct Recovery = 65% Analysis Date = 08/16/14 Pct Recovery = 65% Analysis Date = 08/16/14 Pct Recovery = 65% Analysis Date = 08/11/14 Pct Recovery = 65% Analysis Date = 08/11/14 Pct Recovery = 65% Analysis Date = 08/06/14 Pct Recovery = 65% Analysis Date = 08/06/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 65% Analysis Date = 08/01/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/22/14 Pct Recovery = 65% Analysis Date = 07/22/14 Pct Recovery = 65% Analysis Date = 07/17/14 Pct Recovery = 65% Analysis Date = 07/17/14 Pct Recovery = 65% Analysis Date = 07/12/14 Pct Recovery = 64% Analysis Date = 07/12/14 Pct Recovery = 64% Analysis Date = 07/07/14 Pct Recovery = 64% Analysis Date = 07/07/14 Pct Recovery = 64% Analysis Date = 07/02/14 Pct Recovery = 64% Analysis Date = 07/02/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 64% Analysis Date = 06/22/14 Pct Recovery = 64% Analysis Date = 06/22/14 Pct Recovery = 64% Analysis Date = 06/17/14 Pct Recovery = 64% Analysis Date = 06/17/14 Pct Recovery = 64% Analysis Date = 06/12/14 Pct Recovery = 64% Analysis Date = 06/12/14 Pct Recovery = 64% Analysis Date = 06/07/14 Pct Recovery = 64% Analysis Date = 06/07/14 Pct Recovery = 64% Analysis Date = 06/02/14 Pct Recovery = 63% Analysis Date = 06/02/14 Pct Recovery = 63% Analysis Date = 05/28/14 Pct Recovery = 63% Analysis Date = 05/28/14 Pct Recovery = 63% Analysis Date = 05/23/14 Pct Recovery = 63% Analysis Date = 05/23/14 Pct Recovery = 63% Analysis Date = 05/18/14 Pct Recovery = 63% Analysis Date = 05/18/14 Pct Recovery = 63% Analysis Date = 05/13/14 Pct Recovery = 63% Analysis Date = 05/13/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/03/14 Pct Recovery = 63% Analysis Date = 05/03/14 Pct Recovery = 63% Analysis Date = 04/28/14 Pct Recovery = 63% Analysis Date = 04/28/14 Pct Recovery = 63% Analysis Date = 04/23/14 Pct Recovery = 62% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
GLYBURIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 70% 8% 69% 5%
>= Reporting Level 60 67% 19% 70% 15%
Total 70 68% 17% 69% 13%

Sample Statistics
GLYBURIDE

Characteristic N % % Basis
Plotted 70 92% Spiked
Estimated Values 15 20% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 76 .  
False Negatives 4 5% 4 out of 76
Not Spiked 39 .  
False Positives 0 0% 0 out of 39