BQS OBSP Determination:
GLIPIZIDE
METHOD: 2440 , TESTIDCODE: 68001LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 75% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 71% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 80 µl & ERA 0406-15-08: 80 µl Pct Recovery = 99% Analysis Date = 11/04/15 SpikeMix = Abs 052215: 80 µl & Abs 050115: 80 µl Pct Recovery = 105% Analysis Date = 01/17/16 SpikeMix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Pct Recovery = 90% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 119% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 79% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 72% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 81% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 82% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 99% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 98% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 121% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 103% Analysis Date = 02/23/16 SpikeMix = Abs 050115: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 94% Analysis Date = 02/23/16 SpikeMix = Abs 052215: 40 µl & Abs 050115: 40 µl Pct Recovery = 106% Analysis Date = 07/31/15 SpikeMix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Pct Recovery = 113% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 97% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 85% Analysis Date = 11/04/15 SpikeMix = ERA 0406-15-07A: 40 µl & ERA 0406-15-08: 40 µl Pct Recovery = 86% Analysis Date = 09/10/15 SpikeMix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Pct Recovery = 97% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 80% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 77% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 79% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 97% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 121% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 90% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 104% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 104% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 70% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 77% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 73% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 57% Analysis Date = 11/25/15 SpikeMix = Abs 050115: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 110% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Pct Recovery = 106% Analysis Date = 08/27/15 SpikeMix = Abs 052215: 20 µl & Abs 050115: 20 µl Pct Recovery = 92% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 74% Analysis Date = 07/09/15 SpikeMix = Abs 050115: 20 µl & Abs 052215: 20 µl Pct Recovery = 100% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 87% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 73% Analysis Date = 05/11/16 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 75% Analysis Date = 04/27/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 132% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 94% Analysis Date = 04/09/16 SpikeMix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 112% Analysis Date = 11/24/15 SpikeMix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Pct Recovery = 95% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-09: 20 µl Pct Recovery = 27% Analysis Date = 09/15/15 SpikeMix = ERA 0406-15-07A: 20 µl & ERA 0406-15-08: 20 µl Pct Recovery = 92% Analysis Date = 06/23/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 94% Analysis Date = 01/19/17 Pct Recovery = 87% Analysis Date = 01/14/17 Pct Recovery = 87% Analysis Date = 01/14/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 01/04/17 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/31/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/26/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/12/16 Pct Recovery = 86% Analysis Date = 12/12/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 86% Analysis Date = 12/07/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/23/16 Pct Recovery = 85% Analysis Date = 11/23/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/14/16 Pct Recovery = 85% Analysis Date = 11/09/16 Pct Recovery = 85% Analysis Date = 11/09/16 Pct Recovery = 85% Analysis Date = 11/04/16 Pct Recovery = 85% Analysis Date = 11/04/16 Pct Recovery = 85% Analysis Date = 10/31/16 Pct Recovery = 84% Analysis Date = 10/31/16 Pct Recovery = 84% Analysis Date = 10/26/16 Pct Recovery = 84% Analysis Date = 10/26/16 Pct Recovery = 84% Analysis Date = 10/21/16 Pct Recovery = 84% Analysis Date = 10/21/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/07/16 Pct Recovery = 84% Analysis Date = 10/07/16 Pct Recovery = 84% Analysis Date = 10/02/16 Pct Recovery = 84% Analysis Date = 10/02/16 Pct Recovery = 84% Analysis Date = 09/28/16 Pct Recovery = 83% Analysis Date = 09/28/16 Pct Recovery = 83% Analysis Date = 09/23/16 Pct Recovery = 83% Analysis Date = 09/23/16 Pct Recovery = 83% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/13/16 Pct Recovery = 84% Analysis Date = 09/13/16 Pct Recovery = 84% Analysis Date = 09/09/16 Pct Recovery = 84% Analysis Date = 09/09/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 09/04/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 07/28/16 Pct Recovery = 88% Analysis Date = 07/28/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/19/16 Pct Recovery = 89% Analysis Date = 07/19/16 Pct Recovery = 89% Analysis Date = 07/14/16 Pct Recovery = 89% Analysis Date = 07/14/16 Pct Recovery = 89% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/10/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 07/05/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/30/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 91% Analysis Date = 06/25/16 Pct Recovery = 91% Analysis Date = 06/21/16 Pct Recovery = 91% Analysis Date = 06/21/16 Pct Recovery = 91% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/07/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 06/02/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/14/16 Pct Recovery = 95% Analysis Date = 05/09/16 Pct Recovery = 95% Analysis Date = 05/09/16 Pct Recovery = 95% Analysis Date = 05/05/16 Pct Recovery = 95% Analysis Date = 05/05/16 Pct Recovery = 95% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/25/16 Pct Recovery = 96% Analysis Date = 04/21/16 Pct Recovery = 96% Analysis Date = 04/21/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/16/16 Pct Recovery = 96% Analysis Date = 04/11/16 Pct Recovery = 97% Analysis Date = 04/11/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/02/16 Pct Recovery = 97% Analysis Date = 04/02/16 Pct Recovery = 97% Analysis Date = 03/28/16 Pct Recovery = 97% Analysis Date = 03/28/16 Pct Recovery = 97% Analysis Date = 03/23/16 Pct Recovery = 97% Analysis Date = 03/23/16 Pct Recovery = 97% Analysis Date = 03/19/16 Pct Recovery = 97% Analysis Date = 03/19/16 Pct Recovery = 97% Analysis Date = 03/14/16 Pct Recovery = 98% Analysis Date = 03/14/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/05/16 Pct Recovery = 98% Analysis Date = 03/05/16 Pct Recovery = 98% Analysis Date = 02/29/16 Pct Recovery = 98% Analysis Date = 02/29/16 Pct Recovery = 98% Analysis Date = 02/24/16 Pct Recovery = 98% Analysis Date = 02/24/16 Pct Recovery = 98% Analysis Date = 02/19/16 Pct Recovery = 98% Analysis Date = 02/19/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 98% Analysis Date = 02/10/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/05/16 Pct Recovery = 98% Analysis Date = 02/01/16 Pct Recovery = 98% Analysis Date = 02/01/16 Pct Recovery = 98% Analysis Date = 01/27/16 Pct Recovery = 97% Analysis Date = 01/27/16 Pct Recovery = 97% Analysis Date = 01/22/16 Pct Recovery = 97% Analysis Date = 01/22/16 Pct Recovery = 97% Analysis Date = 01/18/16 Pct Recovery = 97% Analysis Date = 01/18/16 Pct Recovery = 97% Analysis Date = 01/13/16 Pct Recovery = 97% Analysis Date = 01/13/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/08/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 97% Analysis Date = 01/03/16 Pct Recovery = 97% Analysis Date = 12/30/15 Pct Recovery = 96% Analysis Date = 12/30/15 Pct Recovery = 96% Analysis Date = 12/25/15 Pct Recovery = 96% Analysis Date = 12/25/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/20/15 Pct Recovery = 96% Analysis Date = 12/16/15 Pct Recovery = 96% Analysis Date = 12/16/15 Pct Recovery = 96% Analysis Date = 12/11/15 Pct Recovery = 96% Analysis Date = 12/11/15 Pct Recovery = 96% Analysis Date = 12/06/15 Pct Recovery = 96% Analysis Date = 12/06/15 Pct Recovery = 96% Analysis Date = 12/01/15 Pct Recovery = 95% Analysis Date = 12/01/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/27/15 Pct Recovery = 95% Analysis Date = 11/22/15 Pct Recovery = 95% Analysis Date = 11/22/15 Pct Recovery = 95% Analysis Date = 11/17/15 Pct Recovery = 95% Analysis Date = 11/17/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/13/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/08/15 Pct Recovery = 95% Analysis Date = 11/03/15 Pct Recovery = 94% Analysis Date = 11/03/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/30/15 Pct Recovery = 94% Analysis Date = 10/25/15 Pct Recovery = 94% Analysis Date = 10/25/15 Pct Recovery = 94% Analysis Date = 10/20/15 Pct Recovery = 94% Analysis Date = 10/20/15 Pct Recovery = 94% Analysis Date = 10/15/15 Pct Recovery = 94% Analysis Date = 10/15/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/11/15 Pct Recovery = 94% Analysis Date = 10/06/15 Pct Recovery = 93% Analysis Date = 10/06/15 Pct Recovery = 93% Analysis Date = 10/01/15 Pct Recovery = 93% Analysis Date = 10/01/15 Pct Recovery = 93% Analysis Date = 09/27/15 Pct Recovery = 93% Analysis Date = 09/27/15 Pct Recovery = 93% Analysis Date = 09/22/15 Pct Recovery = 93% Analysis Date = 09/22/15 Pct Recovery = 93% Analysis Date = 09/17/15 Pct Recovery = 93% Analysis Date = 09/17/15 Pct Recovery = 93% Analysis Date = 09/12/15 Pct Recovery = 93% Analysis Date = 09/12/15 Pct Recovery = 93% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/03/15 Pct Recovery = 92% Analysis Date = 09/03/15 Pct Recovery = 92% Analysis Date = 08/29/15 Pct Recovery = 92% Analysis Date = 08/29/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/25/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/20/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/15/15 Pct Recovery = 92% Analysis Date = 08/11/15 Pct Recovery = 92% Analysis Date = 08/11/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 91% Analysis Date = 08/06/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 08/01/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/27/15 Pct Recovery = 91% Analysis Date = 07/23/15 Pct Recovery = 91% Analysis Date = 07/23/15 Pct Recovery = 91% Analysis Date = 07/18/15 Pct Recovery = 91% Analysis Date = 07/18/15 Pct Recovery = 91% Analysis Date = 07/13/15 Pct Recovery = 91% Analysis Date = 07/13/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/09/15 Pct Recovery = 91% Analysis Date = 07/04/15 Pct Recovery = 91% Analysis Date = 07/04/15 Pct Recovery = 91% Analysis Date = 06/29/15 Pct Recovery = 91% Analysis Date = 06/29/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/24/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/20/15 Pct Recovery = 91% Analysis Date = 06/15/15 Pct Recovery = 91% Analysis Date = 06/15/15 Pct Recovery = 91% Analysis Date = 06/10/15 Pct Recovery = 91% Analysis Date = 06/10/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/06/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 91% Analysis Date = 06/01/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/27/15 Pct Recovery = 91% Analysis Date = 05/23/15 Pct Recovery = 91% Analysis Date = 05/23/15 Pct Recovery = 91% Analysis Date = 05/18/15 Pct Recovery = 91% Analysis Date = 05/18/15 Pct Recovery = 91% Analysis Date = 05/13/15 Pct Recovery = 91% Analysis Date = 05/13/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/08/15 Pct Recovery = 91% Analysis Date = 05/04/15 Pct Recovery = 91% Analysis Date = 05/04/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/29/15 Pct Recovery = 91% Analysis Date = 04/24/15 Pct Recovery = 91% Analysis Date = 04/24/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/20/15 Pct Recovery = 91% Analysis Date = 04/15/15 Pct Recovery = 91% Analysis Date = 04/15/15 Pct Recovery = 91% Analysis Date = 04/10/15 Pct Recovery = 91% Analysis Date = 04/10/15 Pct Recovery = 91% Analysis Date = 04/06/15 Pct Recovery = 91% Analysis Date = 04/06/15 Pct Recovery = 91% Analysis Date = 04/01/15 Pct Recovery = 91% Analysis Date = 04/01/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/27/15 Pct Recovery = 91% Analysis Date = 03/22/15 Pct Recovery = 91% Analysis Date = 03/22/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/18/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/13/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/08/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 03/04/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/27/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/22/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/17/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 91% Analysis Date = 02/08/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 02/03/15 Pct Recovery = 91% Analysis Date = 01/30/15 Pct Recovery = 91% Analysis Date = 01/30/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/25/15 Pct Recovery = 91% Analysis Date = 01/20/15 Pct Recovery = 91% Analysis Date = 01/20/15 Pct Recovery = 91% Analysis Date = 01/16/15 Pct Recovery = 91% Analysis Date = 01/16/15 Pct Recovery = 91% Analysis Date = 01/11/15 Pct Recovery = 91% Analysis Date = 01/11/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 91% Analysis Date = 01/06/15 Pct Recovery = 91% Analysis Date = 01/01/15 Pct Recovery = 91% Analysis Date = 01/01/15 Pct Recovery = 91% Analysis Date = 12/28/14 Pct Recovery = 91% Analysis Date = 12/28/14 Pct Recovery = 91% Analysis Date = 12/23/14 Pct Recovery = 91% Analysis Date = 12/23/14 Pct Recovery = 91% Analysis Date = 12/18/14 Pct Recovery = 91% Analysis Date = 12/18/14 Pct Recovery = 91% Analysis Date = 12/14/14 Pct Recovery = 91% Analysis Date = 12/14/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/09/14 Pct Recovery = 91% Analysis Date = 12/04/14 Pct Recovery = 91% Analysis Date = 12/04/14 Pct Recovery = 91% Analysis Date = 11/29/14 Pct Recovery = 91% Analysis Date = 11/29/14 Pct Recovery = 91% Analysis Date = 11/25/14 Pct Recovery = 91% Analysis Date = 11/25/14 Pct Recovery = 91% Analysis Date = 11/20/14 Pct Recovery = 91% Analysis Date = 11/20/14 Pct Recovery = 91% Analysis Date = 11/15/14 Pct Recovery = 91% Analysis Date = 11/15/14 Pct Recovery = 91% Analysis Date = 11/11/14 Pct Recovery = 91% Analysis Date = 11/11/14 Pct Recovery = 91% Analysis Date = 11/06/14 Pct Recovery = 91% Analysis Date = 11/06/14 Pct Recovery = 91% Analysis Date = 11/01/14 Pct Recovery = 91% Analysis Date = 11/01/14 Pct Recovery = 91% Analysis Date = 10/28/14 Pct Recovery = 91% Analysis Date = 10/28/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/23/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/18/14 Pct Recovery = 91% Analysis Date = 10/13/14 Pct Recovery = 91% Analysis Date = 10/13/14 Pct Recovery = 91% Analysis Date = 10/09/14 Pct Recovery = 91% Analysis Date = 10/09/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 10/04/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/29/14 Pct Recovery = 91% Analysis Date = 09/25/14 Pct Recovery = 91% Analysis Date = 09/25/14 Pct Recovery = 91% Analysis Date = 09/20/14 Pct Recovery = 91% Analysis Date = 09/20/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/15/14 Pct Recovery = 91% Analysis Date = 09/10/14 Pct Recovery = 91% Analysis Date = 09/10/14 Pct Recovery = 91% Analysis Date = 09/06/14 Pct Recovery = 91% Analysis Date = 09/06/14 Pct Recovery = 91% Analysis Date = 09/01/14 Pct Recovery = 91% Analysis Date = 09/01/14 Pct Recovery = 91% Analysis Date = 08/27/14 Pct Recovery = 91% Analysis Date = 08/27/14 Pct Recovery = 91% Analysis Date = 08/23/14 Pct Recovery = 91% Analysis Date = 08/23/14 Pct Recovery = 91% Analysis Date = 08/18/14 Pct Recovery = 91% Analysis Date = 08/18/14 Pct Recovery = 91% Analysis Date = 08/13/14 Pct Recovery = 91% Analysis Date = 08/13/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/09/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 08/04/14 Pct Recovery = 91% Analysis Date = 07/30/14 Pct Recovery = 91% Analysis Date = 07/30/14 Pct Recovery = 91% Analysis Date = 07/25/14 Pct Recovery = 91% Analysis Date = 07/25/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/21/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/16/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/11/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/07/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 07/02/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/27/14 Pct Recovery = 91% Analysis Date = 06/23/14 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
GLIPIZIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 94% . 94% 0%
>= Reporting Level 51 90% 18% 92% 19%
Total 52 90% 18% 92% 18%

Sample Statistics
GLIPIZIDE

Characteristic N % % Basis
Plotted 52 68% Spiked
Estimated Values 27 35% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 24 31% Spiked
Spiked 77 .  
False Negatives 1 1% 1 out of 77
Not Spiked 38 .  
False Positives 0 0% 0 out of 38