BQS OBSP Determination:
ALPRAZOLAM
METHOD: 2440 , TESTIDCODE: 68250LCM56
Open Data Set

Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 96% Analysis Date = 01/19/17 SpikeMix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Pct Recovery = 90% Analysis Date = 11/24/15 SpikeMix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Pct Recovery = 82% Analysis Date = 10/01/15 SpikeMix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Pct Recovery = 51% Analysis Date = 11/18/16 SpikeMix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Pct Recovery = 72% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Pct Recovery = 78% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 71% Analysis Date = 11/18/16 SpikeMix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Pct Recovery = 70% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 78% Analysis Date = 09/09/16 SpikeMix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Pct Recovery = 80% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 85% Analysis Date = 07/23/16 SpikeMix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Pct Recovery = 79% Analysis Date = 03/10/15 SpikeMix = ERA 0319-14-04: 15 µl & Abs 041814: 15 µl Pct Recovery = 93% Analysis Date = 02/06/15 SpikeMix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Pct Recovery = 89% Analysis Date = 07/12/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 06/22/14 SpikeMix = Abs 041814: 60 µl & Abs 041614: 60 µl Pct Recovery = 107% Analysis Date = 05/21/14 SpikeMix = Abs 041714: 60 µl & Abs 041814: 60 µl Pct Recovery = 85% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 75% Analysis Date = 04/27/16 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 68% Analysis Date = 12/15/15 SpikeMix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Pct Recovery = 71% Analysis Date = 07/31/15 SpikeMix = Abs 051315: 40 µl & Abs 052215: 40 µl Pct Recovery = 59% Analysis Date = 07/30/15 SpikeMix = Abs 050115: 40 µl & Abs 051315: 40 µl Pct Recovery = 77% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 71% Analysis Date = 10/29/16 SpikeMix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 69% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 68% Analysis Date = 09/17/16 SpikeMix = Abs 061416: 40 µl & ERA 04281603: 40 µl Pct Recovery = 76% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 101% Analysis Date = 01/05/17 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 118% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 85% Analysis Date = 10/28/16 SpikeMix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 87% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 85% Analysis Date = 09/23/16 SpikeMix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Pct Recovery = 91% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 59% Analysis Date = 08/17/16 SpikeMix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Pct Recovery = 62% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 74% Analysis Date = 08/11/16 SpikeMix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Pct Recovery = 82% Analysis Date = 04/10/15 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 90% Analysis Date = 11/04/14 SpikeMix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Pct Recovery = 93% Analysis Date = 10/11/14 SpikeMix = ERA 0319-14-04: 8 µl & Abs 041814: 8 µl Pct Recovery = 73% Analysis Date = 10/10/14 SpikeMix = Abs 041714: 30 µl & Abs 041814: 30 µl Pct Recovery = 75% Analysis Date = 10/10/14 SpikeMix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Pct Recovery = 78% Analysis Date = 07/13/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 103% Analysis Date = 05/30/14 SpikeMix = Abs 041814: 30 µl & Abs 041614: 30 µl Pct Recovery = 77% Analysis Date = 02/23/16 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 73% Analysis Date = 08/11/15 SpikeMix = Abs 050115: 20 µl & Abs 051315: 20 µl Pct Recovery = 53% Analysis Date = 06/26/15 SpikeMix = Abs 051315: 20 µl & Abs 052215: 20 µl Pct Recovery = 76% Analysis Date = 06/09/15 SpikeMix = Abs 051315: 20 µl & Abs 050115: 20 µl Pct Recovery = 100% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 37% Analysis Date = 04/09/16 SpikeMix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Pct Recovery = 110% Analysis Date = 01/18/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 01/04/17 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/30/16 Pct Recovery = 89% Analysis Date = 12/25/16 Pct Recovery = 89% Analysis Date = 12/25/16 Pct Recovery = 89% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/01/16 Pct Recovery = 86% Analysis Date = 12/01/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/21/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 83% Analysis Date = 11/06/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 11/02/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/28/16 Pct Recovery = 82% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/23/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/18/16 Pct Recovery = 81% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/13/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/19/16 Pct Recovery = 78% Analysis Date = 09/19/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 77% Analysis Date = 09/14/16 Pct Recovery = 77% Analysis Date = 09/09/16 Pct Recovery = 77% Analysis Date = 09/09/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 09/04/16 Pct Recovery = 77% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/25/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/21/16 Pct Recovery = 76% Analysis Date = 08/16/16 Pct Recovery = 76% Analysis Date = 08/16/16 Pct Recovery = 76% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 75% Analysis Date = 08/01/16 Pct Recovery = 75% Analysis Date = 07/27/16 Pct Recovery = 75% Analysis Date = 07/27/16 Pct Recovery = 75% Analysis Date = 07/22/16 Pct Recovery = 75% Analysis Date = 07/22/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/17/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 06/28/16 Pct Recovery = 75% Analysis Date = 06/28/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/25/16 Pct Recovery = 74% Analysis Date = 05/25/16 Pct Recovery = 74% Analysis Date = 05/20/16 Pct Recovery = 74% Analysis Date = 05/20/16 Pct Recovery = 74% Analysis Date = 05/15/16 Pct Recovery = 74% Analysis Date = 05/15/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/21/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 74% Analysis Date = 04/06/16 Pct Recovery = 74% Analysis Date = 04/01/16 Pct Recovery = 73% Analysis Date = 04/01/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/18/16 Pct Recovery = 73% Analysis Date = 03/18/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/03/16 Pct Recovery = 73% Analysis Date = 03/03/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/27/16 Pct Recovery = 73% Analysis Date = 02/22/16 Pct Recovery = 73% Analysis Date = 02/22/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/17/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 73% Analysis Date = 02/08/16 Pct Recovery = 73% Analysis Date = 02/03/16 Pct Recovery = 73% Analysis Date = 02/03/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/29/16 Pct Recovery = 73% Analysis Date = 01/24/16 Pct Recovery = 73% Analysis Date = 01/24/16 Pct Recovery = 73% Analysis Date = 01/19/16 Pct Recovery = 73% Analysis Date = 01/19/16 Pct Recovery = 73% Analysis Date = 01/14/16 Pct Recovery = 73% Analysis Date = 01/14/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 01/05/16 Pct Recovery = 73% Analysis Date = 12/31/15 Pct Recovery = 73% Analysis Date = 12/31/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/26/15 Pct Recovery = 73% Analysis Date = 12/21/15 Pct Recovery = 72% Analysis Date = 12/21/15 Pct Recovery = 72% Analysis Date = 12/16/15 Pct Recovery = 72% Analysis Date = 12/16/15 Pct Recovery = 72% Analysis Date = 12/11/15 Pct Recovery = 72% Analysis Date = 12/11/15 Pct Recovery = 72% Analysis Date = 12/06/15 Pct Recovery = 72% Analysis Date = 12/06/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 12/02/15 Pct Recovery = 72% Analysis Date = 11/27/15 Pct Recovery = 72% Analysis Date = 11/27/15 Pct Recovery = 72% Analysis Date = 11/22/15 Pct Recovery = 72% Analysis Date = 11/22/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 72% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/12/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 11/02/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 73% Analysis Date = 10/24/15 Pct Recovery = 73% Analysis Date = 10/24/15 Pct Recovery = 73% Analysis Date = 10/19/15 Pct Recovery = 73% Analysis Date = 10/19/15 Pct Recovery = 73% Analysis Date = 10/14/15 Pct Recovery = 74% Analysis Date = 10/14/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 74% Analysis Date = 10/09/15 Pct Recovery = 74% Analysis Date = 10/04/15 Pct Recovery = 74% Analysis Date = 10/04/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 74% Analysis Date = 09/29/15 Pct Recovery = 74% Analysis Date = 09/24/15 Pct Recovery = 74% Analysis Date = 09/24/15 Pct Recovery = 74% Analysis Date = 09/19/15 Pct Recovery = 74% Analysis Date = 09/19/15 Pct Recovery = 74% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/15/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/10/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 09/05/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/31/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/26/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/21/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/16/15 Pct Recovery = 75% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/07/15 Pct Recovery = 76% Analysis Date = 08/07/15 Pct Recovery = 76% Analysis Date = 08/02/15 Pct Recovery = 76% Analysis Date = 08/02/15 Pct Recovery = 76% Analysis Date = 07/28/15 Pct Recovery = 76% Analysis Date = 07/28/15 Pct Recovery = 76% Analysis Date = 07/23/15 Pct Recovery = 76% Analysis Date = 07/23/15 Pct Recovery = 76% Analysis Date = 07/18/15 Pct Recovery = 76% Analysis Date = 07/18/15 Pct Recovery = 76% Analysis Date = 07/13/15 Pct Recovery = 76% Analysis Date = 07/13/15 Pct Recovery = 76% Analysis Date = 07/08/15 Pct Recovery = 77% Analysis Date = 07/08/15 Pct Recovery = 77% Analysis Date = 07/04/15 Pct Recovery = 77% Analysis Date = 07/04/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/24/15 Pct Recovery = 77% Analysis Date = 06/24/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/14/15 Pct Recovery = 77% Analysis Date = 06/14/15 Pct Recovery = 77% Analysis Date = 06/09/15 Pct Recovery = 77% Analysis Date = 06/09/15 Pct Recovery = 77% Analysis Date = 06/04/15 Pct Recovery = 77% Analysis Date = 06/04/15 Pct Recovery = 77% Analysis Date = 05/30/15 Pct Recovery = 78% Analysis Date = 05/30/15 Pct Recovery = 78% Analysis Date = 05/26/15 Pct Recovery = 78% Analysis Date = 05/26/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/21/15 Pct Recovery = 78% Analysis Date = 05/16/15 Pct Recovery = 78% Analysis Date = 05/16/15 Pct Recovery = 78% Analysis Date = 05/11/15 Pct Recovery = 78% Analysis Date = 05/11/15 Pct Recovery = 78% Analysis Date = 05/06/15 Pct Recovery = 78% Analysis Date = 05/06/15 Pct Recovery = 78% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 05/01/15 Pct Recovery = 79% Analysis Date = 04/26/15 Pct Recovery = 79% Analysis Date = 04/26/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/22/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/17/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/12/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/07/15 Pct Recovery = 79% Analysis Date = 04/02/15 Pct Recovery = 80% Analysis Date = 04/02/15 Pct Recovery = 80% Analysis Date = 03/28/15 Pct Recovery = 80% Analysis Date = 03/28/15 Pct Recovery = 80% Analysis Date = 03/23/15 Pct Recovery = 80% Analysis Date = 03/23/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/18/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/14/15 Pct Recovery = 80% Analysis Date = 03/09/15 Pct Recovery = 80% Analysis Date = 03/09/15 Pct Recovery = 80% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 03/04/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/27/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/22/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/17/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/12/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/07/15 Pct Recovery = 81% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 02/03/15 Pct Recovery = 82% Analysis Date = 01/29/15 Pct Recovery = 82% Analysis Date = 01/29/15 Pct Recovery = 82% Analysis Date = 01/24/15 Pct Recovery = 82% Analysis Date = 01/24/15 Pct Recovery = 82% Analysis Date = 01/19/15 Pct Recovery = 82% Analysis Date = 01/19/15 Pct Recovery = 82% Analysis Date = 01/14/15 Pct Recovery = 82% Analysis Date = 01/14/15 Pct Recovery = 82% Analysis Date = 01/09/15 Pct Recovery = 82% Analysis Date = 01/09/15 Pct Recovery = 82% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 01/04/15 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 83% Analysis Date = 12/31/14 Pct Recovery = 83% Analysis Date = 12/26/14 Pct Recovery = 83% Analysis Date = 12/26/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/21/14 Pct Recovery = 83% Analysis Date = 12/16/14 Pct Recovery = 83% Analysis Date = 12/16/14 Pct Recovery = 83% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/11/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/06/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 84% Analysis Date = 12/01/14 Pct Recovery = 84% Analysis Date = 11/26/14 Pct Recovery = 84% Analysis Date = 11/26/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/22/14 Pct Recovery = 84% Analysis Date = 11/17/14 Pct Recovery = 84% Analysis Date = 11/17/14 Pct Recovery = 84% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/12/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/07/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 11/02/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 85% Analysis Date = 10/28/14 Pct Recovery = 85% Analysis Date = 10/23/14 Pct Recovery = 85% Analysis Date = 10/23/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/18/14 Pct Recovery = 85% Analysis Date = 10/14/14 Pct Recovery = 86% Analysis Date = 10/14/14 Pct Recovery = 86% Analysis Date = 10/09/14 Pct Recovery = 86% Analysis Date = 10/09/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 10/04/14 Pct Recovery = 86% Analysis Date = 09/29/14 Pct Recovery = 86% Analysis Date = 09/29/14 Pct Recovery = 86% Analysis Date = 09/24/14 Pct Recovery = 86% Analysis Date = 09/24/14 Pct Recovery = 86% Analysis Date = 09/19/14 Pct Recovery = 87% Analysis Date = 09/19/14 Pct Recovery = 87% Analysis Date = 09/14/14 Pct Recovery = 87% Analysis Date = 09/14/14 Pct Recovery = 87% Analysis Date = 09/10/14 Pct Recovery = 87% Analysis Date = 09/10/14 Pct Recovery = 87% Analysis Date = 09/05/14 Pct Recovery = 87% Analysis Date = 09/05/14 Pct Recovery = 87% Analysis Date = 08/31/14 Pct Recovery = 87% Analysis Date = 08/31/14 Pct Recovery = 87% Analysis Date = 08/26/14 Pct Recovery = 87% Analysis Date = 08/26/14 Pct Recovery = 87% Analysis Date = 08/21/14 Pct Recovery = 88% Analysis Date = 08/21/14 Pct Recovery = 88% Analysis Date = 08/16/14 Pct Recovery = 88% Analysis Date = 08/16/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/11/14 Pct Recovery = 88% Analysis Date = 08/06/14 Pct Recovery = 88% Analysis Date = 08/06/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 07/28/14 Pct Recovery = 88% Analysis Date = 07/28/14 Pct Recovery = 88% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/23/14 Pct Recovery = 89% Analysis Date = 07/18/14 Pct Recovery = 89% Analysis Date = 07/18/14 Pct Recovery = 89% Analysis Date = 07/13/14 Pct Recovery = 89% Analysis Date = 07/13/14 Pct Recovery = 89% Analysis Date = 07/08/14 Pct Recovery = 89% Analysis Date = 07/08/14 Pct Recovery = 89% Analysis Date = 07/03/14 Pct Recovery = 89% Analysis Date = 07/03/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/24/14 Pct Recovery = 90% Analysis Date = 06/24/14 Pct Recovery = 90% Analysis Date = 06/19/14 Pct Recovery = 90% Analysis Date = 06/19/14 Pct Recovery = 90% Analysis Date = 06/14/14 Pct Recovery = 90% Analysis Date = 06/14/14 Pct Recovery = 90% Analysis Date = 06/09/14 Pct Recovery = 90% Analysis Date = 06/09/14 Pct Recovery = 90% Analysis Date = 06/04/14 Pct Recovery = 90% Analysis Date = 06/04/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/30/14 Pct Recovery = 90% Analysis Date = 05/25/14 Pct Recovery = 91% Analysis Date = 05/25/14 Pct Recovery = 91% Analysis Date = 05/21/14 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPRAZOLAM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 74% 51% 74% 54%
>= Reporting Level 47 80% 14% 78% 13%
Total 49 80% 15% 78% 13%

Sample Statistics
ALPRAZOLAM

Characteristic N % % Basis
Plotted 49 98% Spiked
Estimated Values 12 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 1 2% 1 out of 50
Not Spiked 65 .  
False Positives 12 18% 12 out of 65