BQS OBSP Determination:
TERBUFOS
METHOD: 2437 , TESTIDCODE: 68699LCM60
Open Data Set

Analysis Date = 12/19/13 SpikeMix = ChemService 1473000: 5 µl & Supelco LB99392: 5 µl & Abs 042413: 5 µl Pct Recovery = 101% Analysis Date = 02/19/14 SpikeMix = Spex Organics T1130514013: 5 µl & ERA 0318-13-02.2: 5 µl & Crescent 04CC101: 5 µ Pct Recovery = 85% Analysis Date = 09/25/13 SpikeMix = Spex Organics T1130514013: 5 µl & ERA 0318-13-02.2: 5 µl & Crescent 04CC101: 5 µ Pct Recovery = 62% Analysis Date = 01/23/14 SpikeMix = Abs 042413: 2 µl & Spex Organics T1130514013: 2 µl & Supelco LB99392: 2 µl Pct Recovery = 70% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 2 µl & Abs 042413: 2 µl & Spex Organics T1130514013: 2 µl Pct Recovery = 59% Analysis Date = 11/07/13 SpikeMix = Spex Organics T1130514013: 2 µl & Supelco LB99392: 2 µl & Crescent 04CC101: 2 µl Pct Recovery = 79% Analysis Date = 12/18/13 SpikeMix = Spex Organics T1130517007: 2 µl & ERA 0318-13-02.1: 2 µl & Abs 041613: 2 µl Pct Recovery = 83% Analysis Date = 12/10/13 SpikeMix = Abs 041613: 2 µl & ChemService 1466000: 2 µl & Accu 213041078: 2 µl Pct Recovery = 61% Analysis Date = 09/29/13 SpikeMix = Accu 213041078b: 2 µl & Abs 041613: 2 µl & Spex Organics T1130517007: 2 µl Pct Recovery = 66% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 65% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 62% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 72% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 52% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 60% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 59% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 70% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 57% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 66% Analysis Date = 06/11/14 SpikeMix = ChemService 2598800: 60 µl & ChemService 2609400: 60 µl Pct Recovery = 49% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 93% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 64% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 74% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 75% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 61% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 65% Analysis Date = 12/02/14 SpikeMix = ChemService 2609400: 30 µl & Abs 042914: 30 µl Pct Recovery = 58% Analysis Date = 11/18/14 SpikeMix = Abs 042814Pest3: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 80% Analysis Date = 09/04/14 SpikeMix = ChemService 2609400: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 48% Analysis Date = 02/11/15 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 59% Analysis Date = 12/31/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 65% Analysis Date = 12/16/14 SpikeMix = ChemService 2598800: 30 µl & Abs 042314: 30 µl Pct Recovery = 64% Analysis Date = 11/04/14 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 60% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 46% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 67% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 45% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 64% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 66% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 93% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 81% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 62% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 50% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 59% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 57% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 69% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 72% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 73% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 63% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 53% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 59% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 78% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 88% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 89% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 70% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 67% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 52% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 75% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 86% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 81% Analysis Date = 07/18/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 61% Analysis Date = 07/15/15 SpikeMix = ChemService 3880000: 20 µl & ChemService 3995200: 20 µl & ChemService 3880100: 2 Pct Recovery = 128% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 63% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 61% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 69% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 87% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 64% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 78% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 25% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 72% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 69% Analysis Date = 04/08/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 75% Analysis Date = 10/07/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 72% Analysis Date = 09/23/14 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 64% Analysis Date = 09/10/14 SpikeMix = ChemService 2609400: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 50% Analysis Date = 07/24/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 39% Analysis Date = 05/17/14 SpikeMix = ChemService 2598800: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 57% Analysis Date = 03/11/15 SpikeMix = Abs 042314: 15 µl & Abs 042914: 15 µl Pct Recovery = 81% Analysis Date = 08/20/14 SpikeMix = Abs 042814Pest3: 15 µl & Abs 042314: 15 µl Pct Recovery = 27% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 74% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 85% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 83% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 63% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 70% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 44% Analysis Date = 08/06/15 SpikeMix = ERA 0406-15-05: 10 µl & ChemService 4047100: 10 µl & ChemService 3880200: 10 µl Pct Recovery = 79% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 30% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 19% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 28% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 63% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 61% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 57% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 83% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 48% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 71% Analysis Date = 01/04/17 Pct Recovery = 69% Analysis Date = 12/29/16 Pct Recovery = 69% Analysis Date = 12/29/16 Pct Recovery = 69% Analysis Date = 12/23/16 Pct Recovery = 69% Analysis Date = 12/23/16 Pct Recovery = 69% Analysis Date = 12/17/16 Pct Recovery = 69% Analysis Date = 12/17/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/05/16 Pct Recovery = 69% Analysis Date = 12/05/16 Pct Recovery = 69% Analysis Date = 11/29/16 Pct Recovery = 69% Analysis Date = 11/29/16 Pct Recovery = 69% Analysis Date = 11/23/16 Pct Recovery = 69% Analysis Date = 11/23/16 Pct Recovery = 69% Analysis Date = 11/17/16 Pct Recovery = 69% Analysis Date = 11/17/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/05/16 Pct Recovery = 69% Analysis Date = 11/05/16 Pct Recovery = 69% Analysis Date = 10/30/16 Pct Recovery = 69% Analysis Date = 10/30/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/18/16 Pct Recovery = 69% Analysis Date = 10/18/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 09/30/16 Pct Recovery = 69% Analysis Date = 09/30/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 68% Analysis Date = 09/24/16 Pct Recovery = 68% Analysis Date = 09/18/16 Pct Recovery = 68% Analysis Date = 09/18/16 Pct Recovery = 68% Analysis Date = 09/12/16 Pct Recovery = 68% Analysis Date = 09/12/16 Pct Recovery = 68% Analysis Date = 09/06/16 Pct Recovery = 68% Analysis Date = 09/06/16 Pct Recovery = 68% Analysis Date = 08/31/16 Pct Recovery = 68% Analysis Date = 08/31/16 Pct Recovery = 68% Analysis Date = 08/25/16 Pct Recovery = 68% Analysis Date = 08/25/16 Pct Recovery = 68% Analysis Date = 08/19/16 Pct Recovery = 68% Analysis Date = 08/19/16 Pct Recovery = 68% Analysis Date = 08/13/16 Pct Recovery = 68% Analysis Date = 08/13/16 Pct Recovery = 68% Analysis Date = 08/07/16 Pct Recovery = 68% Analysis Date = 08/07/16 Pct Recovery = 68% Analysis Date = 08/01/16 Pct Recovery = 68% Analysis Date = 08/01/16 Pct Recovery = 68% Analysis Date = 07/26/16 Pct Recovery = 68% Analysis Date = 07/26/16 Pct Recovery = 68% Analysis Date = 07/20/16 Pct Recovery = 68% Analysis Date = 07/20/16 Pct Recovery = 68% Analysis Date = 07/14/16 Pct Recovery = 68% Analysis Date = 07/14/16 Pct Recovery = 68% Analysis Date = 07/08/16 Pct Recovery = 68% Analysis Date = 07/08/16 Pct Recovery = 68% Analysis Date = 07/02/16 Pct Recovery = 68% Analysis Date = 07/02/16 Pct Recovery = 68% Analysis Date = 06/26/16 Pct Recovery = 67% Analysis Date = 06/26/16 Pct Recovery = 67% Analysis Date = 06/20/16 Pct Recovery = 67% Analysis Date = 06/20/16 Pct Recovery = 67% Analysis Date = 06/14/16 Pct Recovery = 67% Analysis Date = 06/14/16 Pct Recovery = 67% Analysis Date = 06/08/16 Pct Recovery = 67% Analysis Date = 06/08/16 Pct Recovery = 67% Analysis Date = 06/02/16 Pct Recovery = 67% Analysis Date = 06/02/16 Pct Recovery = 67% Analysis Date = 05/27/16 Pct Recovery = 67% Analysis Date = 05/27/16 Pct Recovery = 67% Analysis Date = 05/21/16 Pct Recovery = 67% Analysis Date = 05/21/16 Pct Recovery = 67% Analysis Date = 05/15/16 Pct Recovery = 66% Analysis Date = 05/15/16 Pct Recovery = 66% Analysis Date = 05/09/16 Pct Recovery = 66% Analysis Date = 05/09/16 Pct Recovery = 66% Analysis Date = 05/03/16 Pct Recovery = 66% Analysis Date = 05/03/16 Pct Recovery = 66% Analysis Date = 04/27/16 Pct Recovery = 66% Analysis Date = 04/27/16 Pct Recovery = 66% Analysis Date = 04/21/16 Pct Recovery = 66% Analysis Date = 04/21/16 Pct Recovery = 66% Analysis Date = 04/15/16 Pct Recovery = 66% Analysis Date = 04/15/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/03/16 Pct Recovery = 66% Analysis Date = 04/03/16 Pct Recovery = 66% Analysis Date = 03/28/16 Pct Recovery = 65% Analysis Date = 03/28/16 Pct Recovery = 65% Analysis Date = 03/22/16 Pct Recovery = 65% Analysis Date = 03/22/16 Pct Recovery = 65% Analysis Date = 03/16/16 Pct Recovery = 65% Analysis Date = 03/16/16 Pct Recovery = 65% Analysis Date = 03/10/16 Pct Recovery = 65% Analysis Date = 03/10/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/27/16 Pct Recovery = 65% Analysis Date = 02/21/16 Pct Recovery = 65% Analysis Date = 02/21/16 Pct Recovery = 65% Analysis Date = 02/15/16 Pct Recovery = 65% Analysis Date = 02/15/16 Pct Recovery = 65% Analysis Date = 02/09/16 Pct Recovery = 65% Analysis Date = 02/09/16 Pct Recovery = 65% Analysis Date = 02/03/16 Pct Recovery = 64% Analysis Date = 02/03/16 Pct Recovery = 64% Analysis Date = 01/28/16 Pct Recovery = 64% Analysis Date = 01/28/16 Pct Recovery = 64% Analysis Date = 01/22/16 Pct Recovery = 64% Analysis Date = 01/22/16 Pct Recovery = 64% Analysis Date = 01/16/16 Pct Recovery = 64% Analysis Date = 01/16/16 Pct Recovery = 64% Analysis Date = 01/10/16 Pct Recovery = 64% Analysis Date = 01/10/16 Pct Recovery = 64% Analysis Date = 01/04/16 Pct Recovery = 64% Analysis Date = 01/04/16 Pct Recovery = 64% Analysis Date = 12/29/15 Pct Recovery = 64% Analysis Date = 12/29/15 Pct Recovery = 64% Analysis Date = 12/23/15 Pct Recovery = 64% Analysis Date = 12/23/15 Pct Recovery = 64% Analysis Date = 12/17/15 Pct Recovery = 64% Analysis Date = 12/17/15 Pct Recovery = 64% Analysis Date = 12/11/15 Pct Recovery = 64% Analysis Date = 12/11/15 Pct Recovery = 64% Analysis Date = 12/05/15 Pct Recovery = 64% Analysis Date = 12/05/15 Pct Recovery = 64% Analysis Date = 11/30/15 Pct Recovery = 64% Analysis Date = 11/30/15 Pct Recovery = 64% Analysis Date = 11/24/15 Pct Recovery = 65% Analysis Date = 11/24/15 Pct Recovery = 65% Analysis Date = 11/18/15 Pct Recovery = 65% Analysis Date = 11/18/15 Pct Recovery = 65% Analysis Date = 11/12/15 Pct Recovery = 65% Analysis Date = 11/12/15 Pct Recovery = 65% Analysis Date = 11/06/15 Pct Recovery = 65% Analysis Date = 11/06/15 Pct Recovery = 65% Analysis Date = 10/31/15 Pct Recovery = 66% Analysis Date = 10/31/15 Pct Recovery = 66% Analysis Date = 10/25/15 Pct Recovery = 66% Analysis Date = 10/25/15 Pct Recovery = 66% Analysis Date = 10/19/15 Pct Recovery = 66% Analysis Date = 10/19/15 Pct Recovery = 66% Analysis Date = 10/13/15 Pct Recovery = 67% Analysis Date = 10/13/15 Pct Recovery = 67% Analysis Date = 10/07/15 Pct Recovery = 67% Analysis Date = 10/07/15 Pct Recovery = 67% Analysis Date = 10/01/15 Pct Recovery = 67% Analysis Date = 10/01/15 Pct Recovery = 67% Analysis Date = 09/25/15 Pct Recovery = 68% Analysis Date = 09/25/15 Pct Recovery = 68% Analysis Date = 09/19/15 Pct Recovery = 68% Analysis Date = 09/19/15 Pct Recovery = 68% Analysis Date = 09/13/15 Pct Recovery = 68% Analysis Date = 09/13/15 Pct Recovery = 68% Analysis Date = 09/07/15 Pct Recovery = 69% Analysis Date = 09/07/15 Pct Recovery = 69% Analysis Date = 09/01/15 Pct Recovery = 70% Analysis Date = 09/01/15 Pct Recovery = 70% Analysis Date = 08/26/15 Pct Recovery = 70% Analysis Date = 08/26/15 Pct Recovery = 70% Analysis Date = 08/20/15 Pct Recovery = 71% Analysis Date = 08/20/15 Pct Recovery = 71% Analysis Date = 08/14/15 Pct Recovery = 72% Analysis Date = 08/14/15 Pct Recovery = 72% Analysis Date = 08/08/15 Pct Recovery = 72% Analysis Date = 08/08/15 Pct Recovery = 72% Analysis Date = 08/02/15 Pct Recovery = 71% Analysis Date = 08/02/15 Pct Recovery = 71% Analysis Date = 07/27/15 Pct Recovery = 71% Analysis Date = 07/27/15 Pct Recovery = 71% Analysis Date = 07/21/15 Pct Recovery = 71% Analysis Date = 07/21/15 Pct Recovery = 71% Analysis Date = 07/15/15 Pct Recovery = 71% Analysis Date = 07/15/15 Pct Recovery = 71% Analysis Date = 07/09/15 Pct Recovery = 70% Analysis Date = 07/09/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 07/03/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/27/15 Pct Recovery = 70% Analysis Date = 06/21/15 Pct Recovery = 70% Analysis Date = 06/21/15 Pct Recovery = 70% Analysis Date = 06/15/15 Pct Recovery = 69% Analysis Date = 06/15/15 Pct Recovery = 69% Analysis Date = 06/09/15 Pct Recovery = 69% Analysis Date = 06/09/15 Pct Recovery = 69% Analysis Date = 06/03/15 Pct Recovery = 69% Analysis Date = 06/03/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/28/15 Pct Recovery = 69% Analysis Date = 05/22/15 Pct Recovery = 68% Analysis Date = 05/22/15 Pct Recovery = 68% Analysis Date = 05/16/15 Pct Recovery = 68% Analysis Date = 05/16/15 Pct Recovery = 68% Analysis Date = 05/10/15 Pct Recovery = 68% Analysis Date = 05/10/15 Pct Recovery = 68% Analysis Date = 05/04/15 Pct Recovery = 68% Analysis Date = 05/04/15 Pct Recovery = 68% Analysis Date = 04/28/15 Pct Recovery = 67% Analysis Date = 04/28/15 Pct Recovery = 67% Analysis Date = 04/22/15 Pct Recovery = 67% Analysis Date = 04/22/15 Pct Recovery = 67% Analysis Date = 04/16/15 Pct Recovery = 67% Analysis Date = 04/16/15 Pct Recovery = 67% Analysis Date = 04/10/15 Pct Recovery = 67% Analysis Date = 04/10/15 Pct Recovery = 67% Analysis Date = 04/04/15 Pct Recovery = 66% Analysis Date = 04/04/15 Pct Recovery = 66% Analysis Date = 03/29/15 Pct Recovery = 66% Analysis Date = 03/29/15 Pct Recovery = 66% Analysis Date = 03/23/15 Pct Recovery = 66% Analysis Date = 03/23/15 Pct Recovery = 66% Analysis Date = 03/17/15 Pct Recovery = 65% Analysis Date = 03/17/15 Pct Recovery = 65% Analysis Date = 03/11/15 Pct Recovery = 65% Analysis Date = 03/11/15 Pct Recovery = 65% Analysis Date = 03/05/15 Pct Recovery = 65% Analysis Date = 03/05/15 Pct Recovery = 65% Analysis Date = 02/27/15 Pct Recovery = 65% Analysis Date = 02/27/15 Pct Recovery = 65% Analysis Date = 02/21/15 Pct Recovery = 65% Analysis Date = 02/21/15 Pct Recovery = 65% Analysis Date = 02/15/15 Pct Recovery = 65% Analysis Date = 02/15/15 Pct Recovery = 65% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/09/15 Pct Recovery = 64% Analysis Date = 02/03/15 Pct Recovery = 64% Analysis Date = 02/03/15 Pct Recovery = 64% Analysis Date = 01/28/15 Pct Recovery = 64% Analysis Date = 01/28/15 Pct Recovery = 64% Analysis Date = 01/22/15 Pct Recovery = 64% Analysis Date = 01/22/15 Pct Recovery = 64% Analysis Date = 01/16/15 Pct Recovery = 64% Analysis Date = 01/16/15 Pct Recovery = 64% Analysis Date = 01/10/15 Pct Recovery = 64% Analysis Date = 01/10/15 Pct Recovery = 64% Analysis Date = 01/04/15 Pct Recovery = 64% Analysis Date = 01/04/15 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 63% Analysis Date = 12/29/14 Pct Recovery = 63% Analysis Date = 12/23/14 Pct Recovery = 63% Analysis Date = 12/23/14 Pct Recovery = 63% Analysis Date = 12/17/14 Pct Recovery = 63% Analysis Date = 12/17/14 Pct Recovery = 63% Analysis Date = 12/11/14 Pct Recovery = 63% Analysis Date = 12/11/14 Pct Recovery = 63% Analysis Date = 12/05/14 Pct Recovery = 63% Analysis Date = 12/05/14 Pct Recovery = 63% Analysis Date = 11/29/14 Pct Recovery = 63% Analysis Date = 11/29/14 Pct Recovery = 63% Analysis Date = 11/23/14 Pct Recovery = 63% Analysis Date = 11/23/14 Pct Recovery = 63% Analysis Date = 11/17/14 Pct Recovery = 62% Analysis Date = 11/17/14 Pct Recovery = 62% Analysis Date = 11/11/14 Pct Recovery = 62% Analysis Date = 11/11/14 Pct Recovery = 62% Analysis Date = 11/05/14 Pct Recovery = 62% Analysis Date = 11/05/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/30/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/25/14 Pct Recovery = 62% Analysis Date = 10/19/14 Pct Recovery = 62% Analysis Date = 10/19/14 Pct Recovery = 62% Analysis Date = 10/13/14 Pct Recovery = 63% Analysis Date = 10/13/14 Pct Recovery = 63% Analysis Date = 10/07/14 Pct Recovery = 63% Analysis Date = 10/07/14 Pct Recovery = 63% Analysis Date = 10/01/14 Pct Recovery = 63% Analysis Date = 10/01/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/25/14 Pct Recovery = 63% Analysis Date = 09/19/14 Pct Recovery = 63% Analysis Date = 09/19/14 Pct Recovery = 63% Analysis Date = 09/13/14 Pct Recovery = 63% Analysis Date = 09/13/14 Pct Recovery = 63% Analysis Date = 09/07/14 Pct Recovery = 64% Analysis Date = 09/07/14 Pct Recovery = 64% Analysis Date = 09/01/14 Pct Recovery = 64% Analysis Date = 09/01/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/26/14 Pct Recovery = 64% Analysis Date = 08/20/14 Pct Recovery = 64% Analysis Date = 08/20/14 Pct Recovery = 64% Analysis Date = 08/14/14 Pct Recovery = 64% Analysis Date = 08/14/14 Pct Recovery = 64% Analysis Date = 08/08/14 Pct Recovery = 64% Analysis Date = 08/08/14 Pct Recovery = 64% Analysis Date = 08/02/14 Pct Recovery = 64% Analysis Date = 08/02/14 Pct Recovery = 64% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/27/14 Pct Recovery = 65% Analysis Date = 07/21/14 Pct Recovery = 65% Analysis Date = 07/21/14 Pct Recovery = 65% Analysis Date = 07/15/14 Pct Recovery = 65% Analysis Date = 07/15/14 Pct Recovery = 65% Analysis Date = 07/09/14 Pct Recovery = 65% Analysis Date = 07/09/14 Pct Recovery = 65% Analysis Date = 07/03/14 Pct Recovery = 65% Analysis Date = 07/03/14 Pct Recovery = 65% Analysis Date = 06/27/14 Pct Recovery = 65% Analysis Date = 06/27/14 Pct Recovery = 65% Analysis Date = 06/21/14 Pct Recovery = 65% Analysis Date = 06/21/14 Pct Recovery = 65% Analysis Date = 06/15/14 Pct Recovery = 65% Analysis Date = 06/15/14 Pct Recovery = 65% Analysis Date = 06/09/14 Pct Recovery = 65% Analysis Date = 06/09/14 Pct Recovery = 65% Analysis Date = 06/03/14 Pct Recovery = 65% Analysis Date = 06/03/14 Pct Recovery = 65% Analysis Date = 05/28/14 Pct Recovery = 65% Analysis Date = 05/28/14 Pct Recovery = 65% Analysis Date = 05/22/14 Pct Recovery = 65% Analysis Date = 05/22/14 Pct Recovery = 65% Analysis Date = 05/16/14 Pct Recovery = 66% Analysis Date = 05/16/14 Pct Recovery = 66% Analysis Date = 05/10/14 Pct Recovery = 66% Analysis Date = 05/10/14 Pct Recovery = 66% Analysis Date = 05/04/14 Pct Recovery = 66% Analysis Date = 05/04/14 Pct Recovery = 66% Analysis Date = 04/28/14 Pct Recovery = 66% Analysis Date = 04/28/14 Pct Recovery = 66% Analysis Date = 04/22/14 Pct Recovery = 66% Analysis Date = 04/22/14 Pct Recovery = 66% Analysis Date = 04/16/14 Pct Recovery = 66% Analysis Date = 04/16/14 Pct Recovery = 66% Analysis Date = 04/10/14 Pct Recovery = 66% Analysis Date = 04/10/14 Pct Recovery = 66% Analysis Date = 04/04/14 Pct Recovery = 66% Analysis Date = 04/04/14 Pct Recovery = 66% Analysis Date = 03/29/14 Pct Recovery = 66% Analysis Date = 03/29/14 Pct Recovery = 66% Analysis Date = 03/23/14 Pct Recovery = 66% Analysis Date = 03/23/14 Pct Recovery = 66% Analysis Date = 03/17/14 Pct Recovery = 66% Analysis Date = 03/17/14 Pct Recovery = 66% Analysis Date = 03/11/14 Pct Recovery = 66% Analysis Date = 03/11/14 Pct Recovery = 66% Analysis Date = 03/05/14 Pct Recovery = 67% Analysis Date = 03/05/14 Pct Recovery = 67% Analysis Date = 02/27/14 Pct Recovery = 67% Analysis Date = 02/27/14 Pct Recovery = 67% Analysis Date = 02/21/14 Pct Recovery = 67% Analysis Date = 02/21/14 Pct Recovery = 67% Analysis Date = 02/15/14 Pct Recovery = 67% Analysis Date = 02/15/14 Pct Recovery = 67% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 02/03/14 Pct Recovery = 67% Analysis Date = 02/03/14 Pct Recovery = 67% Analysis Date = 01/28/14 Pct Recovery = 67% Analysis Date = 01/28/14 Pct Recovery = 67% Analysis Date = 01/22/14 Pct Recovery = 67% Analysis Date = 01/22/14 Pct Recovery = 67% Analysis Date = 01/16/14 Pct Recovery = 67% Analysis Date = 01/16/14 Pct Recovery = 67% Analysis Date = 01/10/14 Pct Recovery = 67% Analysis Date = 01/10/14 Pct Recovery = 67% Analysis Date = 01/04/14 Pct Recovery = 67% Analysis Date = 01/04/14 Pct Recovery = 67% Analysis Date = 12/29/13 Pct Recovery = 67% Analysis Date = 12/29/13 Pct Recovery = 67% Analysis Date = 12/23/13 Pct Recovery = 68% Analysis Date = 12/23/13 Pct Recovery = 68% Analysis Date = 12/17/13 Pct Recovery = 68% Analysis Date = 12/17/13 Pct Recovery = 68% Analysis Date = 12/11/13 Pct Recovery = 68% Analysis Date = 12/11/13 Pct Recovery = 68% Analysis Date = 12/05/13 Pct Recovery = 68% Analysis Date = 12/05/13 Pct Recovery = 68% Analysis Date = 11/29/13 Pct Recovery = 68% Analysis Date = 11/29/13 Pct Recovery = 68% Analysis Date = 11/23/13 Pct Recovery = 68% Analysis Date = 11/23/13 Pct Recovery = 68% Analysis Date = 11/17/13 Pct Recovery = 68% Analysis Date = 11/17/13 Pct Recovery = 68% Analysis Date = 11/11/13 Pct Recovery = 68% Analysis Date = 11/11/13 Pct Recovery = 68% Analysis Date = 11/05/13 Pct Recovery = 69% Analysis Date = 11/05/13 Pct Recovery = 69% Analysis Date = 10/30/13 Pct Recovery = 69% Analysis Date = 10/30/13 Pct Recovery = 69% Analysis Date = 10/24/13 Pct Recovery = 69% Analysis Date = 10/24/13 Pct Recovery = 69% Analysis Date = 10/18/13 Pct Recovery = 69% Analysis Date = 10/18/13 Pct Recovery = 69% Analysis Date = 10/12/13 Pct Recovery = 69% Analysis Date = 10/12/13 Pct Recovery = 69% Analysis Date = 10/06/13 Pct Recovery = 69% Analysis Date = 10/06/13 Pct Recovery = 69% Analysis Date = 09/30/13 Pct Recovery = 70% Analysis Date = 09/30/13 Pct Recovery = 70% Analysis Date = 09/25/13 Pct Recovery = 70% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 64% 12% 62% 10%
>= Reporting Level 87 66% 17% 65% 12%
Total 93 66% 17% 65% 12%

Sample Statistics
TERBUFOS

Characteristic N % % Basis
Plotted 93 82% Spiked
Estimated Values 9 8% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 9 8% Spiked
Spiked 114 .  
False Negatives 12 11% 12 out of 114
Not Spiked 64 .  
False Positives 0 0% 0 out of 61