BQS OBSP Determination:
SULFOMETURON-METHYL
METHOD: 2437 , TESTIDCODE: 68688LCM60
Open Data Set

Analysis Date = 03/04/14 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & ChemService 1448600: 2 Pct Recovery = 91% Analysis Date = 11/21/13 SpikeMix = Supelco LC01386: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 102% Analysis Date = 10/31/13 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & Accu 213041030: 2 µl Pct Recovery = 100% Analysis Date = 02/06/14 SpikeMix = NSI 042213HPLC: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 19% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 63% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 58% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 62% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 77% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 78% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 83% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 71% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 71% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 66% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 76% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 77% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 75% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 87% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 93% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 52% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 50% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 41% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 55% Analysis Date = 02/11/15 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 57% Analysis Date = 11/04/14 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 88% Analysis Date = 10/07/14 SpikeMix = ERA 0321-14-07: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 83% Analysis Date = 09/04/14 SpikeMix = ChemService 2609400: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 56% Analysis Date = 12/31/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 111% Analysis Date = 12/02/14 SpikeMix = ChemService 2609400: 30 µl & Abs 042914: 30 µl Pct Recovery = 119% Analysis Date = 12/02/14 SpikeMix = Abs 042914: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 127% Analysis Date = 11/05/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 143% Analysis Date = 07/19/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 128% Analysis Date = 07/08/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 114% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 50% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 55% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 64% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 65% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 45% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 47% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 52% Analysis Date = 07/22/15 SpikeMix = ERA 0406-15-04: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 87% Analysis Date = 07/18/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 68% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 69% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 78% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 86% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 76% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 66% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 57% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 57% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 52% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 86% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 72% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 85% Analysis Date = 08/19/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 89% Analysis Date = 08/19/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 67% Analysis Date = 08/19/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 50% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 77% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 98% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 52% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 50% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 39% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 37% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 56% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 59% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 47% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 43% Analysis Date = 04/09/15 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 34% Analysis Date = 03/07/15 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 41% Analysis Date = 09/10/14 SpikeMix = ChemService 2609400: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 109% Analysis Date = 08/17/14 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 91% Analysis Date = 08/16/14 SpikeMix = Abs 042314: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 93% Analysis Date = 07/31/14 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 105% Analysis Date = 04/15/15 SpikeMix = ChemService 2598800: 15 µl & Abs 042914: 15 µl Pct Recovery = 101% Analysis Date = 03/11/15 SpikeMix = Abs 042314: 15 µl & Abs 042914: 15 µl Pct Recovery = 125% Analysis Date = 10/07/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 122% Analysis Date = 09/10/14 SpikeMix = Abs 042914: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 136% Analysis Date = 07/24/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 115% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 68% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 73% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 67% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 79% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 78% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 67% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 107% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 99% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 141% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 80% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 117% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 86% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 70% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 79% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 80% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 77% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 94% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 58% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 85% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 59% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 68% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 63% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 72% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 86% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 95% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 64% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 82% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 86% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 86% Analysis Date = 01/04/17 Pct Recovery = 60% Analysis Date = 12/29/16 Pct Recovery = 60% Analysis Date = 12/29/16 Pct Recovery = 60% Analysis Date = 12/23/16 Pct Recovery = 60% Analysis Date = 12/23/16 Pct Recovery = 60% Analysis Date = 12/17/16 Pct Recovery = 60% Analysis Date = 12/17/16 Pct Recovery = 60% Analysis Date = 12/11/16 Pct Recovery = 60% Analysis Date = 12/11/16 Pct Recovery = 60% Analysis Date = 12/05/16 Pct Recovery = 60% Analysis Date = 12/05/16 Pct Recovery = 60% Analysis Date = 11/30/16 Pct Recovery = 60% Analysis Date = 11/30/16 Pct Recovery = 60% Analysis Date = 11/24/16 Pct Recovery = 60% Analysis Date = 11/24/16 Pct Recovery = 60% Analysis Date = 11/18/16 Pct Recovery = 60% Analysis Date = 11/18/16 Pct Recovery = 60% Analysis Date = 11/12/16 Pct Recovery = 60% Analysis Date = 11/12/16 Pct Recovery = 60% Analysis Date = 11/06/16 Pct Recovery = 60% Analysis Date = 11/06/16 Pct Recovery = 60% Analysis Date = 11/01/16 Pct Recovery = 60% Analysis Date = 11/01/16 Pct Recovery = 60% Analysis Date = 10/26/16 Pct Recovery = 61% Analysis Date = 10/26/16 Pct Recovery = 61% Analysis Date = 10/20/16 Pct Recovery = 61% Analysis Date = 10/20/16 Pct Recovery = 61% Analysis Date = 10/14/16 Pct Recovery = 61% Analysis Date = 10/14/16 Pct Recovery = 61% Analysis Date = 10/08/16 Pct Recovery = 61% Analysis Date = 10/08/16 Pct Recovery = 61% Analysis Date = 10/03/16 Pct Recovery = 61% Analysis Date = 10/03/16 Pct Recovery = 61% Analysis Date = 09/27/16 Pct Recovery = 61% Analysis Date = 09/27/16 Pct Recovery = 61% Analysis Date = 09/21/16 Pct Recovery = 61% Analysis Date = 09/21/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/15/16 Pct Recovery = 61% Analysis Date = 09/09/16 Pct Recovery = 61% Analysis Date = 09/09/16 Pct Recovery = 61% Analysis Date = 09/04/16 Pct Recovery = 61% Analysis Date = 09/04/16 Pct Recovery = 61% Analysis Date = 08/29/16 Pct Recovery = 61% Analysis Date = 08/29/16 Pct Recovery = 61% Analysis Date = 08/23/16 Pct Recovery = 61% Analysis Date = 08/23/16 Pct Recovery = 61% Analysis Date = 08/17/16 Pct Recovery = 62% Analysis Date = 08/17/16 Pct Recovery = 62% Analysis Date = 08/11/16 Pct Recovery = 62% Analysis Date = 08/11/16 Pct Recovery = 62% Analysis Date = 08/06/16 Pct Recovery = 62% Analysis Date = 08/06/16 Pct Recovery = 62% Analysis Date = 07/31/16 Pct Recovery = 62% Analysis Date = 07/31/16 Pct Recovery = 62% Analysis Date = 07/25/16 Pct Recovery = 62% Analysis Date = 07/25/16 Pct Recovery = 62% Analysis Date = 07/19/16 Pct Recovery = 62% Analysis Date = 07/19/16 Pct Recovery = 62% Analysis Date = 07/13/16 Pct Recovery = 62% Analysis Date = 07/13/16 Pct Recovery = 62% Analysis Date = 07/08/16 Pct Recovery = 62% Analysis Date = 07/08/16 Pct Recovery = 62% Analysis Date = 07/02/16 Pct Recovery = 62% Analysis Date = 07/02/16 Pct Recovery = 62% Analysis Date = 06/26/16 Pct Recovery = 62% Analysis Date = 06/26/16 Pct Recovery = 62% Analysis Date = 06/20/16 Pct Recovery = 62% Analysis Date = 06/20/16 Pct Recovery = 62% Analysis Date = 06/14/16 Pct Recovery = 62% Analysis Date = 06/14/16 Pct Recovery = 62% Analysis Date = 06/09/16 Pct Recovery = 62% Analysis Date = 06/09/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/22/16 Pct Recovery = 62% Analysis Date = 05/22/16 Pct Recovery = 62% Analysis Date = 05/16/16 Pct Recovery = 62% Analysis Date = 05/16/16 Pct Recovery = 62% Analysis Date = 05/10/16 Pct Recovery = 62% Analysis Date = 05/10/16 Pct Recovery = 62% Analysis Date = 05/05/16 Pct Recovery = 63% Analysis Date = 05/05/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 63% Analysis Date = 04/23/16 Pct Recovery = 63% Analysis Date = 04/23/16 Pct Recovery = 63% Analysis Date = 04/17/16 Pct Recovery = 63% Analysis Date = 04/17/16 Pct Recovery = 63% Analysis Date = 04/11/16 Pct Recovery = 63% Analysis Date = 04/11/16 Pct Recovery = 63% Analysis Date = 04/06/16 Pct Recovery = 64% Analysis Date = 04/06/16 Pct Recovery = 64% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/25/16 Pct Recovery = 65% Analysis Date = 03/25/16 Pct Recovery = 65% Analysis Date = 03/19/16 Pct Recovery = 66% Analysis Date = 03/19/16 Pct Recovery = 66% Analysis Date = 03/13/16 Pct Recovery = 66% Analysis Date = 03/13/16 Pct Recovery = 66% Analysis Date = 03/08/16 Pct Recovery = 67% Analysis Date = 03/08/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 02/25/16 Pct Recovery = 68% Analysis Date = 02/25/16 Pct Recovery = 68% Analysis Date = 02/19/16 Pct Recovery = 69% Analysis Date = 02/19/16 Pct Recovery = 69% Analysis Date = 02/13/16 Pct Recovery = 70% Analysis Date = 02/13/16 Pct Recovery = 70% Analysis Date = 02/08/16 Pct Recovery = 70% Analysis Date = 02/08/16 Pct Recovery = 70% Analysis Date = 02/02/16 Pct Recovery = 71% Analysis Date = 02/02/16 Pct Recovery = 71% Analysis Date = 01/27/16 Pct Recovery = 71% Analysis Date = 01/27/16 Pct Recovery = 71% Analysis Date = 01/21/16 Pct Recovery = 72% Analysis Date = 01/21/16 Pct Recovery = 72% Analysis Date = 01/15/16 Pct Recovery = 73% Analysis Date = 01/15/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/10/16 Pct Recovery = 73% Analysis Date = 01/04/16 Pct Recovery = 74% Analysis Date = 01/04/16 Pct Recovery = 74% Analysis Date = 12/29/15 Pct Recovery = 74% Analysis Date = 12/29/15 Pct Recovery = 74% Analysis Date = 12/23/15 Pct Recovery = 75% Analysis Date = 12/23/15 Pct Recovery = 75% Analysis Date = 12/17/15 Pct Recovery = 75% Analysis Date = 12/17/15 Pct Recovery = 75% Analysis Date = 12/12/15 Pct Recovery = 75% Analysis Date = 12/12/15 Pct Recovery = 75% Analysis Date = 12/06/15 Pct Recovery = 76% Analysis Date = 12/06/15 Pct Recovery = 76% Analysis Date = 11/30/15 Pct Recovery = 76% Analysis Date = 11/30/15 Pct Recovery = 76% Analysis Date = 11/24/15 Pct Recovery = 76% Analysis Date = 11/24/15 Pct Recovery = 76% Analysis Date = 11/18/15 Pct Recovery = 76% Analysis Date = 11/18/15 Pct Recovery = 76% Analysis Date = 11/13/15 Pct Recovery = 76% Analysis Date = 11/13/15 Pct Recovery = 76% Analysis Date = 11/07/15 Pct Recovery = 76% Analysis Date = 11/07/15 Pct Recovery = 76% Analysis Date = 11/01/15 Pct Recovery = 77% Analysis Date = 11/01/15 Pct Recovery = 77% Analysis Date = 10/26/15 Pct Recovery = 77% Analysis Date = 10/26/15 Pct Recovery = 77% Analysis Date = 10/20/15 Pct Recovery = 77% Analysis Date = 10/20/15 Pct Recovery = 77% Analysis Date = 10/15/15 Pct Recovery = 77% Analysis Date = 10/15/15 Pct Recovery = 77% Analysis Date = 10/09/15 Pct Recovery = 77% Analysis Date = 10/09/15 Pct Recovery = 77% Analysis Date = 10/03/15 Pct Recovery = 77% Analysis Date = 10/03/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/27/15 Pct Recovery = 77% Analysis Date = 09/21/15 Pct Recovery = 77% Analysis Date = 09/21/15 Pct Recovery = 77% Analysis Date = 09/15/15 Pct Recovery = 77% Analysis Date = 09/15/15 Pct Recovery = 77% Analysis Date = 09/10/15 Pct Recovery = 77% Analysis Date = 09/10/15 Pct Recovery = 77% Analysis Date = 09/04/15 Pct Recovery = 77% Analysis Date = 09/04/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/23/15 Pct Recovery = 77% Analysis Date = 08/17/15 Pct Recovery = 76% Analysis Date = 08/17/15 Pct Recovery = 76% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/12/15 Pct Recovery = 76% Analysis Date = 08/06/15 Pct Recovery = 76% Analysis Date = 08/06/15 Pct Recovery = 76% Analysis Date = 07/31/15 Pct Recovery = 76% Analysis Date = 07/31/15 Pct Recovery = 76% Analysis Date = 07/25/15 Pct Recovery = 76% Analysis Date = 07/25/15 Pct Recovery = 76% Analysis Date = 07/19/15 Pct Recovery = 76% Analysis Date = 07/19/15 Pct Recovery = 76% Analysis Date = 07/14/15 Pct Recovery = 76% Analysis Date = 07/14/15 Pct Recovery = 76% Analysis Date = 07/08/15 Pct Recovery = 77% Analysis Date = 07/08/15 Pct Recovery = 77% Analysis Date = 07/02/15 Pct Recovery = 77% Analysis Date = 07/02/15 Pct Recovery = 77% Analysis Date = 06/26/15 Pct Recovery = 78% Analysis Date = 06/26/15 Pct Recovery = 78% Analysis Date = 06/20/15 Pct Recovery = 79% Analysis Date = 06/20/15 Pct Recovery = 79% Analysis Date = 06/15/15 Pct Recovery = 79% Analysis Date = 06/15/15 Pct Recovery = 79% Analysis Date = 06/09/15 Pct Recovery = 80% Analysis Date = 06/09/15 Pct Recovery = 80% Analysis Date = 06/03/15 Pct Recovery = 80% Analysis Date = 06/03/15 Pct Recovery = 80% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/28/15 Pct Recovery = 81% Analysis Date = 05/22/15 Pct Recovery = 82% Analysis Date = 05/22/15 Pct Recovery = 82% Analysis Date = 05/17/15 Pct Recovery = 82% Analysis Date = 05/17/15 Pct Recovery = 82% Analysis Date = 05/11/15 Pct Recovery = 83% Analysis Date = 05/11/15 Pct Recovery = 83% Analysis Date = 05/05/15 Pct Recovery = 83% Analysis Date = 05/05/15 Pct Recovery = 83% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/23/15 Pct Recovery = 85% Analysis Date = 04/23/15 Pct Recovery = 85% Analysis Date = 04/18/15 Pct Recovery = 85% Analysis Date = 04/18/15 Pct Recovery = 85% Analysis Date = 04/12/15 Pct Recovery = 86% Analysis Date = 04/12/15 Pct Recovery = 86% Analysis Date = 04/06/15 Pct Recovery = 86% Analysis Date = 04/06/15 Pct Recovery = 86% Analysis Date = 03/31/15 Pct Recovery = 87% Analysis Date = 03/31/15 Pct Recovery = 87% Analysis Date = 03/25/15 Pct Recovery = 88% Analysis Date = 03/25/15 Pct Recovery = 88% Analysis Date = 03/20/15 Pct Recovery = 88% Analysis Date = 03/20/15 Pct Recovery = 88% Analysis Date = 03/14/15 Pct Recovery = 89% Analysis Date = 03/14/15 Pct Recovery = 89% Analysis Date = 03/08/15 Pct Recovery = 90% Analysis Date = 03/08/15 Pct Recovery = 90% Analysis Date = 03/02/15 Pct Recovery = 90% Analysis Date = 03/02/15 Pct Recovery = 90% Analysis Date = 02/24/15 Pct Recovery = 91% Analysis Date = 02/24/15 Pct Recovery = 91% Analysis Date = 02/19/15 Pct Recovery = 91% Analysis Date = 02/19/15 Pct Recovery = 91% Analysis Date = 02/13/15 Pct Recovery = 92% Analysis Date = 02/13/15 Pct Recovery = 92% Analysis Date = 02/07/15 Pct Recovery = 92% Analysis Date = 02/07/15 Pct Recovery = 92% Analysis Date = 02/01/15 Pct Recovery = 93% Analysis Date = 02/01/15 Pct Recovery = 93% Analysis Date = 01/26/15 Pct Recovery = 93% Analysis Date = 01/26/15 Pct Recovery = 93% Analysis Date = 01/20/15 Pct Recovery = 93% Analysis Date = 01/20/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/15/15 Pct Recovery = 93% Analysis Date = 01/09/15 Pct Recovery = 93% Analysis Date = 01/09/15 Pct Recovery = 93% Analysis Date = 01/03/15 Pct Recovery = 94% Analysis Date = 01/03/15 Pct Recovery = 94% Analysis Date = 12/28/14 Pct Recovery = 94% Analysis Date = 12/28/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/22/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/17/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/11/14 Pct Recovery = 94% Analysis Date = 12/05/14 Pct Recovery = 95% Analysis Date = 12/05/14 Pct Recovery = 95% Analysis Date = 11/29/14 Pct Recovery = 95% Analysis Date = 11/29/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/23/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 95% Analysis Date = 11/18/14 Pct Recovery = 95% Analysis Date = 11/12/14 Pct Recovery = 96% Analysis Date = 11/12/14 Pct Recovery = 96% Analysis Date = 11/06/14 Pct Recovery = 96% Analysis Date = 11/06/14 Pct Recovery = 96% Analysis Date = 10/31/14 Pct Recovery = 96% Analysis Date = 10/31/14 Pct Recovery = 96% Analysis Date = 10/25/14 Pct Recovery = 96% Analysis Date = 10/25/14 Pct Recovery = 96% Analysis Date = 10/20/14 Pct Recovery = 96% Analysis Date = 10/20/14 Pct Recovery = 96% Analysis Date = 10/14/14 Pct Recovery = 97% Analysis Date = 10/14/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/08/14 Pct Recovery = 97% Analysis Date = 10/02/14 Pct Recovery = 97% Analysis Date = 10/02/14 Pct Recovery = 97% Analysis Date = 09/26/14 Pct Recovery = 97% Analysis Date = 09/26/14 Pct Recovery = 97% Analysis Date = 09/21/14 Pct Recovery = 97% Analysis Date = 09/21/14 Pct Recovery = 97% Analysis Date = 09/15/14 Pct Recovery = 97% Analysis Date = 09/15/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/09/14 Pct Recovery = 97% Analysis Date = 09/03/14 Pct Recovery = 97% Analysis Date = 09/03/14 Pct Recovery = 97% Analysis Date = 08/28/14 Pct Recovery = 97% Analysis Date = 08/28/14 Pct Recovery = 97% Analysis Date = 08/23/14 Pct Recovery = 97% Analysis Date = 08/23/14 Pct Recovery = 97% Analysis Date = 08/17/14 Pct Recovery = 97% Analysis Date = 08/17/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/11/14 Pct Recovery = 97% Analysis Date = 08/05/14 Pct Recovery = 98% Analysis Date = 08/05/14 Pct Recovery = 98% Analysis Date = 07/30/14 Pct Recovery = 98% Analysis Date = 07/30/14 Pct Recovery = 98% Analysis Date = 07/25/14 Pct Recovery = 98% Analysis Date = 07/25/14 Pct Recovery = 98% Analysis Date = 07/19/14 Pct Recovery = 98% Analysis Date = 07/19/14 Pct Recovery = 98% Analysis Date = 07/13/14 Pct Recovery = 98% Analysis Date = 07/13/14 Pct Recovery = 98% Analysis Date = 07/07/14 Pct Recovery = 98% Analysis Date = 07/07/14 Pct Recovery = 98% Analysis Date = 07/01/14 Pct Recovery = 98% Analysis Date = 07/01/14 Pct Recovery = 98% Analysis Date = 06/26/14 Pct Recovery = 98% Analysis Date = 06/26/14 Pct Recovery = 98% Analysis Date = 06/20/14 Pct Recovery = 98% Analysis Date = 06/20/14 Pct Recovery = 98% Analysis Date = 06/14/14 Pct Recovery = 98% Analysis Date = 06/14/14 Pct Recovery = 98% Analysis Date = 06/08/14 Pct Recovery = 98% Analysis Date = 06/08/14 Pct Recovery = 98% Analysis Date = 06/02/14 Pct Recovery = 98% Analysis Date = 06/02/14 Pct Recovery = 98% Analysis Date = 05/27/14 Pct Recovery = 98% Analysis Date = 05/27/14 Pct Recovery = 98% Analysis Date = 05/22/14 Pct Recovery = 98% Analysis Date = 05/22/14 Pct Recovery = 98% Analysis Date = 05/16/14 Pct Recovery = 98% Analysis Date = 05/16/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/10/14 Pct Recovery = 98% Analysis Date = 05/04/14 Pct Recovery = 98% Analysis Date = 05/04/14 Pct Recovery = 98% Analysis Date = 04/28/14 Pct Recovery = 98% Analysis Date = 04/28/14 Pct Recovery = 98% Analysis Date = 04/23/14 Pct Recovery = 98% Analysis Date = 04/23/14 Pct Recovery = 98% Analysis Date = 04/17/14 Pct Recovery = 98% Analysis Date = 04/17/14 Pct Recovery = 98% Analysis Date = 04/11/14 Pct Recovery = 98% Analysis Date = 04/11/14 Pct Recovery = 98% Analysis Date = 04/05/14 Pct Recovery = 98% Analysis Date = 04/05/14 Pct Recovery = 98% Analysis Date = 03/30/14 Pct Recovery = 98% Analysis Date = 03/30/14 Pct Recovery = 98% Analysis Date = 03/25/14 Pct Recovery = 98% Analysis Date = 03/25/14 Pct Recovery = 98% Analysis Date = 03/19/14 Pct Recovery = 98% Analysis Date = 03/19/14 Pct Recovery = 98% Analysis Date = 03/13/14 Pct Recovery = 98% Analysis Date = 03/13/14 Pct Recovery = 98% Analysis Date = 03/07/14 Pct Recovery = 98% Analysis Date = 03/07/14 Pct Recovery = 98% Analysis Date = 03/01/14 Pct Recovery = 98% Analysis Date = 03/01/14 Pct Recovery = 98% Analysis Date = 02/24/14 Pct Recovery = 98% Analysis Date = 02/24/14 Pct Recovery = 98% Analysis Date = 02/18/14 Pct Recovery = 98% Analysis Date = 02/18/14 Pct Recovery = 98% Analysis Date = 02/12/14 Pct Recovery = 98% Analysis Date = 02/12/14 Pct Recovery = 98% Analysis Date = 02/06/14 Pct Recovery = 98% Analysis Date = 02/06/14 Pct Recovery = 98% Analysis Date = 01/31/14 Pct Recovery = 98% Analysis Date = 01/31/14 Pct Recovery = 98% Analysis Date = 01/26/14 Pct Recovery = 98% Analysis Date = 01/26/14 Pct Recovery = 98% Analysis Date = 01/20/14 Pct Recovery = 98% Analysis Date = 01/20/14 Pct Recovery = 98% Analysis Date = 01/14/14 Pct Recovery = 98% Analysis Date = 01/14/14 Pct Recovery = 98% Analysis Date = 01/08/14 Pct Recovery = 98% Analysis Date = 01/08/14 Pct Recovery = 98% Analysis Date = 01/02/14 Pct Recovery = 98% Analysis Date = 01/02/14 Pct Recovery = 98% Analysis Date = 12/28/13 Pct Recovery = 98% Analysis Date = 12/28/13 Pct Recovery = 98% Analysis Date = 12/22/13 Pct Recovery = 98% Analysis Date = 12/22/13 Pct Recovery = 98% Analysis Date = 12/16/13 Pct Recovery = 98% Analysis Date = 12/16/13 Pct Recovery = 98% Analysis Date = 12/10/13 Pct Recovery = 98% Analysis Date = 12/10/13 Pct Recovery = 98% Analysis Date = 12/04/13 Pct Recovery = 98% Analysis Date = 12/04/13 Pct Recovery = 98% Analysis Date = 11/29/13 Pct Recovery = 98% Analysis Date = 11/29/13 Pct Recovery = 98% Analysis Date = 11/23/13 Pct Recovery = 98% Analysis Date = 11/23/13 Pct Recovery = 98% Analysis Date = 11/17/13 Pct Recovery = 98% Analysis Date = 11/17/13 Pct Recovery = 98% Analysis Date = 11/11/13 Pct Recovery = 98% Analysis Date = 11/11/13 Pct Recovery = 98% Analysis Date = 11/05/13 Pct Recovery = 98% Analysis Date = 11/05/13 Pct Recovery = 98% Analysis Date = 10/31/13 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFOMETURON-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 105 77% 25% 76% 23%
Total 105 77% 25% 76% 23%

Sample Statistics
SULFOMETURON-METHYL

Characteristic N % % Basis
Plotted 105 95% Spiked
Estimated Values 32 29% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 112 .  
False Negatives 6 5% 6 out of 111
Not Spiked 66 .  
False Positives 0 0% 0 out of 64