BQS OBSP Determination:
ORYZALIN
METHOD: 2437 , TESTIDCODE: 68663LCM60
Open Data Set

Analysis Date = 03/04/14 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & ChemService 1448600: 2 Pct Recovery = 102% Analysis Date = 02/05/14 SpikeMix = NSI 042213HPLC: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 92% Analysis Date = 11/23/13 SpikeMix = Supelco LC01386: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 89% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & Accu 213041030: 2 µl Pct Recovery = 114% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 99% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 88% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 92% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 111% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 111% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 103% Analysis Date = 10/15/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 92% Analysis Date = 10/15/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 93% Analysis Date = 10/15/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 100% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 139% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 127% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 105% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 118% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 29% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 46% Analysis Date = 07/20/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 77% Analysis Date = 07/20/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 107% Analysis Date = 02/11/15 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 116% Analysis Date = 01/28/15 SpikeMix = ERA 0321-14-07: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 105% Analysis Date = 11/04/14 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 172% Analysis Date = 10/07/14 SpikeMix = ERA 0321-14-07: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 123% Analysis Date = 09/03/14 SpikeMix = ChemService 2609400: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 49% Analysis Date = 12/30/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 71% Analysis Date = 12/03/14 SpikeMix = ChemService 2609400: 30 µl & Abs 042914: 30 µl Pct Recovery = 104% Analysis Date = 12/03/14 SpikeMix = Abs 042914: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 99% Analysis Date = 11/04/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 139% Analysis Date = 07/19/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 122% Analysis Date = 07/08/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 99% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 123% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 95% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 98% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 106% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 108% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 102% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 108% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 95% Analysis Date = 12/09/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 69% Analysis Date = 12/09/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 79% Analysis Date = 12/09/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 71% Analysis Date = 10/28/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 98% Analysis Date = 10/28/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 94% Analysis Date = 10/28/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 151% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 37% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 63% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 63% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 115% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 103% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 103% Analysis Date = 08/25/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 88% Analysis Date = 08/25/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 116% Analysis Date = 08/25/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 100% Analysis Date = 08/20/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 125% Analysis Date = 08/18/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 122% Analysis Date = 08/18/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 105% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 118% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 103% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 97% Analysis Date = 07/17/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 90% Analysis Date = 07/14/15 SpikeMix = ChemService 3880000: 20 µl & ChemService 3995200: 20 µl & ChemService 3880100: 2 Pct Recovery = 99% Analysis Date = 01/05/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 111% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 88% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 133% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 104% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 108% Analysis Date = 10/07/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 106% Analysis Date = 08/09/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 92% Analysis Date = 08/09/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 91% Analysis Date = 04/27/15 SpikeMix = Abs 042314: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 159% Analysis Date = 04/02/15 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 98% Analysis Date = 03/03/15 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 49% Analysis Date = 09/10/14 SpikeMix = ChemService 2609400: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 132% Analysis Date = 08/13/14 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 140% Analysis Date = 08/11/14 SpikeMix = Abs 042314: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 148% Analysis Date = 07/30/14 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 109% Analysis Date = 04/15/15 SpikeMix = ChemService 2598800: 15 µl & Abs 042914: 15 µl Pct Recovery = 115% Analysis Date = 03/11/15 SpikeMix = Abs 042314: 15 µl & Abs 042914: 15 µl Pct Recovery = 123% Analysis Date = 10/07/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 166% Analysis Date = 09/10/14 SpikeMix = Abs 042914: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 161% Analysis Date = 07/24/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 120% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 120% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 137% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 130% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 151% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 151% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 113% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 127% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 135% Analysis Date = 09/25/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 118% Analysis Date = 09/25/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 115% Analysis Date = 09/25/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 128% Analysis Date = 08/03/15 SpikeMix = ERA 0406-15-05: 10 µl & ChemService 4047100: 10 µl & ChemService 3880200: 10 µl Pct Recovery = 100% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 90% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 100% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 105% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 103% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 66% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 79% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 92% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 162% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 132% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 135% Analysis Date = 01/04/17 Pct Recovery = 106% Analysis Date = 12/29/16 Pct Recovery = 106% Analysis Date = 12/29/16 Pct Recovery = 106% Analysis Date = 12/23/16 Pct Recovery = 105% Analysis Date = 12/23/16 Pct Recovery = 105% Analysis Date = 12/17/16 Pct Recovery = 105% Analysis Date = 12/17/16 Pct Recovery = 105% Analysis Date = 12/11/16 Pct Recovery = 105% Analysis Date = 12/11/16 Pct Recovery = 105% Analysis Date = 12/05/16 Pct Recovery = 105% Analysis Date = 12/05/16 Pct Recovery = 105% Analysis Date = 11/29/16 Pct Recovery = 105% Analysis Date = 11/29/16 Pct Recovery = 105% Analysis Date = 11/23/16 Pct Recovery = 104% Analysis Date = 11/23/16 Pct Recovery = 104% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/11/16 Pct Recovery = 104% Analysis Date = 11/11/16 Pct Recovery = 104% Analysis Date = 11/05/16 Pct Recovery = 104% Analysis Date = 11/05/16 Pct Recovery = 104% Analysis Date = 10/30/16 Pct Recovery = 104% Analysis Date = 10/30/16 Pct Recovery = 104% Analysis Date = 10/24/16 Pct Recovery = 103% Analysis Date = 10/24/16 Pct Recovery = 103% Analysis Date = 10/18/16 Pct Recovery = 103% Analysis Date = 10/18/16 Pct Recovery = 103% Analysis Date = 10/12/16 Pct Recovery = 103% Analysis Date = 10/12/16 Pct Recovery = 103% Analysis Date = 10/06/16 Pct Recovery = 103% Analysis Date = 10/06/16 Pct Recovery = 103% Analysis Date = 09/30/16 Pct Recovery = 103% Analysis Date = 09/30/16 Pct Recovery = 103% Analysis Date = 09/24/16 Pct Recovery = 103% Analysis Date = 09/24/16 Pct Recovery = 103% Analysis Date = 09/18/16 Pct Recovery = 102% Analysis Date = 09/18/16 Pct Recovery = 102% Analysis Date = 09/12/16 Pct Recovery = 102% Analysis Date = 09/12/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 08/31/16 Pct Recovery = 102% Analysis Date = 08/31/16 Pct Recovery = 102% Analysis Date = 08/25/16 Pct Recovery = 102% Analysis Date = 08/25/16 Pct Recovery = 102% Analysis Date = 08/19/16 Pct Recovery = 102% Analysis Date = 08/19/16 Pct Recovery = 102% Analysis Date = 08/13/16 Pct Recovery = 102% Analysis Date = 08/13/16 Pct Recovery = 102% Analysis Date = 08/07/16 Pct Recovery = 101% Analysis Date = 08/07/16 Pct Recovery = 101% Analysis Date = 08/01/16 Pct Recovery = 101% Analysis Date = 08/01/16 Pct Recovery = 101% Analysis Date = 07/26/16 Pct Recovery = 101% Analysis Date = 07/26/16 Pct Recovery = 101% Analysis Date = 07/20/16 Pct Recovery = 101% Analysis Date = 07/20/16 Pct Recovery = 101% Analysis Date = 07/14/16 Pct Recovery = 101% Analysis Date = 07/14/16 Pct Recovery = 101% Analysis Date = 07/08/16 Pct Recovery = 101% Analysis Date = 07/08/16 Pct Recovery = 101% Analysis Date = 07/02/16 Pct Recovery = 101% Analysis Date = 07/02/16 Pct Recovery = 101% Analysis Date = 06/26/16 Pct Recovery = 100% Analysis Date = 06/26/16 Pct Recovery = 100% Analysis Date = 06/20/16 Pct Recovery = 100% Analysis Date = 06/20/16 Pct Recovery = 100% Analysis Date = 06/14/16 Pct Recovery = 100% Analysis Date = 06/14/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/08/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 06/02/16 Pct Recovery = 100% Analysis Date = 05/27/16 Pct Recovery = 100% Analysis Date = 05/27/16 Pct Recovery = 100% Analysis Date = 05/21/16 Pct Recovery = 100% Analysis Date = 05/21/16 Pct Recovery = 100% Analysis Date = 05/15/16 Pct Recovery = 99% Analysis Date = 05/15/16 Pct Recovery = 99% Analysis Date = 05/09/16 Pct Recovery = 99% Analysis Date = 05/09/16 Pct Recovery = 99% Analysis Date = 05/03/16 Pct Recovery = 99% Analysis Date = 05/03/16 Pct Recovery = 99% Analysis Date = 04/27/16 Pct Recovery = 99% Analysis Date = 04/27/16 Pct Recovery = 99% Analysis Date = 04/21/16 Pct Recovery = 99% Analysis Date = 04/21/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/09/16 Pct Recovery = 98% Analysis Date = 04/09/16 Pct Recovery = 98% Analysis Date = 04/03/16 Pct Recovery = 98% Analysis Date = 04/03/16 Pct Recovery = 98% Analysis Date = 03/28/16 Pct Recovery = 98% Analysis Date = 03/28/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 98% Analysis Date = 03/22/16 Pct Recovery = 98% Analysis Date = 03/16/16 Pct Recovery = 98% Analysis Date = 03/16/16 Pct Recovery = 98% Analysis Date = 03/10/16 Pct Recovery = 99% Analysis Date = 03/10/16 Pct Recovery = 99% Analysis Date = 03/04/16 Pct Recovery = 100% Analysis Date = 03/04/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/27/16 Pct Recovery = 100% Analysis Date = 02/21/16 Pct Recovery = 101% Analysis Date = 02/21/16 Pct Recovery = 101% Analysis Date = 02/15/16 Pct Recovery = 102% Analysis Date = 02/15/16 Pct Recovery = 102% Analysis Date = 02/09/16 Pct Recovery = 103% Analysis Date = 02/09/16 Pct Recovery = 103% Analysis Date = 02/03/16 Pct Recovery = 103% Analysis Date = 02/03/16 Pct Recovery = 103% Analysis Date = 01/28/16 Pct Recovery = 104% Analysis Date = 01/28/16 Pct Recovery = 104% Analysis Date = 01/22/16 Pct Recovery = 104% Analysis Date = 01/22/16 Pct Recovery = 104% Analysis Date = 01/16/16 Pct Recovery = 105% Analysis Date = 01/16/16 Pct Recovery = 105% Analysis Date = 01/10/16 Pct Recovery = 105% Analysis Date = 01/10/16 Pct Recovery = 105% Analysis Date = 01/04/16 Pct Recovery = 105% Analysis Date = 01/04/16 Pct Recovery = 105% Analysis Date = 12/29/15 Pct Recovery = 105% Analysis Date = 12/29/15 Pct Recovery = 105% Analysis Date = 12/23/15 Pct Recovery = 106% Analysis Date = 12/23/15 Pct Recovery = 106% Analysis Date = 12/17/15 Pct Recovery = 106% Analysis Date = 12/17/15 Pct Recovery = 106% Analysis Date = 12/11/15 Pct Recovery = 106% Analysis Date = 12/11/15 Pct Recovery = 106% Analysis Date = 12/05/15 Pct Recovery = 107% Analysis Date = 12/05/15 Pct Recovery = 107% Analysis Date = 11/28/15 Pct Recovery = 107% Analysis Date = 11/28/15 Pct Recovery = 107% Analysis Date = 11/22/15 Pct Recovery = 107% Analysis Date = 11/22/15 Pct Recovery = 107% Analysis Date = 11/16/15 Pct Recovery = 107% Analysis Date = 11/16/15 Pct Recovery = 107% Analysis Date = 11/10/15 Pct Recovery = 107% Analysis Date = 11/10/15 Pct Recovery = 107% Analysis Date = 11/04/15 Pct Recovery = 107% Analysis Date = 11/04/15 Pct Recovery = 107% Analysis Date = 10/29/15 Pct Recovery = 107% Analysis Date = 10/29/15 Pct Recovery = 107% Analysis Date = 10/23/15 Pct Recovery = 107% Analysis Date = 10/23/15 Pct Recovery = 107% Analysis Date = 10/17/15 Pct Recovery = 107% Analysis Date = 10/17/15 Pct Recovery = 107% Analysis Date = 10/11/15 Pct Recovery = 107% Analysis Date = 10/11/15 Pct Recovery = 107% Analysis Date = 10/05/15 Pct Recovery = 107% Analysis Date = 10/05/15 Pct Recovery = 107% Analysis Date = 09/29/15 Pct Recovery = 107% Analysis Date = 09/29/15 Pct Recovery = 107% Analysis Date = 09/23/15 Pct Recovery = 107% Analysis Date = 09/23/15 Pct Recovery = 107% Analysis Date = 09/17/15 Pct Recovery = 107% Analysis Date = 09/17/15 Pct Recovery = 107% Analysis Date = 09/11/15 Pct Recovery = 107% Analysis Date = 09/11/15 Pct Recovery = 107% Analysis Date = 09/05/15 Pct Recovery = 107% Analysis Date = 09/05/15 Pct Recovery = 107% Analysis Date = 08/30/15 Pct Recovery = 107% Analysis Date = 08/30/15 Pct Recovery = 107% Analysis Date = 08/24/15 Pct Recovery = 107% Analysis Date = 08/24/15 Pct Recovery = 107% Analysis Date = 08/18/15 Pct Recovery = 108% Analysis Date = 08/18/15 Pct Recovery = 108% Analysis Date = 08/12/15 Pct Recovery = 108% Analysis Date = 08/12/15 Pct Recovery = 108% Analysis Date = 08/06/15 Pct Recovery = 108% Analysis Date = 08/06/15 Pct Recovery = 108% Analysis Date = 07/31/15 Pct Recovery = 108% Analysis Date = 07/31/15 Pct Recovery = 108% Analysis Date = 07/25/15 Pct Recovery = 108% Analysis Date = 07/25/15 Pct Recovery = 108% Analysis Date = 07/19/15 Pct Recovery = 108% Analysis Date = 07/19/15 Pct Recovery = 108% Analysis Date = 07/13/15 Pct Recovery = 108% Analysis Date = 07/13/15 Pct Recovery = 108% Analysis Date = 07/07/15 Pct Recovery = 108% Analysis Date = 07/07/15 Pct Recovery = 108% Analysis Date = 07/01/15 Pct Recovery = 108% Analysis Date = 07/01/15 Pct Recovery = 108% Analysis Date = 06/25/15 Pct Recovery = 108% Analysis Date = 06/25/15 Pct Recovery = 108% Analysis Date = 06/19/15 Pct Recovery = 108% Analysis Date = 06/19/15 Pct Recovery = 108% Analysis Date = 06/13/15 Pct Recovery = 108% Analysis Date = 06/13/15 Pct Recovery = 108% Analysis Date = 06/07/15 Pct Recovery = 108% Analysis Date = 06/07/15 Pct Recovery = 108% Analysis Date = 06/01/15 Pct Recovery = 108% Analysis Date = 06/01/15 Pct Recovery = 108% Analysis Date = 05/26/15 Pct Recovery = 108% Analysis Date = 05/26/15 Pct Recovery = 108% Analysis Date = 05/20/15 Pct Recovery = 108% Analysis Date = 05/20/15 Pct Recovery = 108% Analysis Date = 05/14/15 Pct Recovery = 108% Analysis Date = 05/14/15 Pct Recovery = 108% Analysis Date = 05/08/15 Pct Recovery = 108% Analysis Date = 05/08/15 Pct Recovery = 108% Analysis Date = 05/02/15 Pct Recovery = 108% Analysis Date = 05/02/15 Pct Recovery = 108% Analysis Date = 04/26/15 Pct Recovery = 108% Analysis Date = 04/26/15 Pct Recovery = 108% Analysis Date = 04/20/15 Pct Recovery = 109% Analysis Date = 04/20/15 Pct Recovery = 109% Analysis Date = 04/14/15 Pct Recovery = 109% Analysis Date = 04/14/15 Pct Recovery = 109% Analysis Date = 04/08/15 Pct Recovery = 109% Analysis Date = 04/08/15 Pct Recovery = 109% Analysis Date = 04/02/15 Pct Recovery = 110% Analysis Date = 04/02/15 Pct Recovery = 110% Analysis Date = 03/27/15 Pct Recovery = 110% Analysis Date = 03/27/15 Pct Recovery = 110% Analysis Date = 03/21/15 Pct Recovery = 110% Analysis Date = 03/21/15 Pct Recovery = 110% Analysis Date = 03/15/15 Pct Recovery = 111% Analysis Date = 03/15/15 Pct Recovery = 111% Analysis Date = 03/09/15 Pct Recovery = 111% Analysis Date = 03/09/15 Pct Recovery = 111% Analysis Date = 03/03/15 Pct Recovery = 112% Analysis Date = 03/03/15 Pct Recovery = 112% Analysis Date = 02/25/15 Pct Recovery = 112% Analysis Date = 02/25/15 Pct Recovery = 112% Analysis Date = 02/19/15 Pct Recovery = 112% Analysis Date = 02/19/15 Pct Recovery = 112% Analysis Date = 02/13/15 Pct Recovery = 113% Analysis Date = 02/13/15 Pct Recovery = 113% Analysis Date = 02/07/15 Pct Recovery = 113% Analysis Date = 02/07/15 Pct Recovery = 113% Analysis Date = 02/01/15 Pct Recovery = 113% Analysis Date = 02/01/15 Pct Recovery = 113% Analysis Date = 01/26/15 Pct Recovery = 114% Analysis Date = 01/26/15 Pct Recovery = 114% Analysis Date = 01/20/15 Pct Recovery = 114% Analysis Date = 01/20/15 Pct Recovery = 114% Analysis Date = 01/14/15 Pct Recovery = 114% Analysis Date = 01/14/15 Pct Recovery = 114% Analysis Date = 01/08/15 Pct Recovery = 114% Analysis Date = 01/08/15 Pct Recovery = 114% Analysis Date = 01/02/15 Pct Recovery = 114% Analysis Date = 01/02/15 Pct Recovery = 114% Analysis Date = 12/27/14 Pct Recovery = 114% Analysis Date = 12/27/14 Pct Recovery = 114% Analysis Date = 12/21/14 Pct Recovery = 114% Analysis Date = 12/21/14 Pct Recovery = 114% Analysis Date = 12/15/14 Pct Recovery = 114% Analysis Date = 12/15/14 Pct Recovery = 114% Analysis Date = 12/09/14 Pct Recovery = 114% Analysis Date = 12/09/14 Pct Recovery = 114% Analysis Date = 12/03/14 Pct Recovery = 114% Analysis Date = 12/03/14 Pct Recovery = 114% Analysis Date = 11/27/14 Pct Recovery = 114% Analysis Date = 11/27/14 Pct Recovery = 114% Analysis Date = 11/21/14 Pct Recovery = 114% Analysis Date = 11/21/14 Pct Recovery = 114% Analysis Date = 11/15/14 Pct Recovery = 114% Analysis Date = 11/15/14 Pct Recovery = 114% Analysis Date = 11/09/14 Pct Recovery = 114% Analysis Date = 11/09/14 Pct Recovery = 114% Analysis Date = 11/03/14 Pct Recovery = 114% Analysis Date = 11/03/14 Pct Recovery = 114% Analysis Date = 10/28/14 Pct Recovery = 114% Analysis Date = 10/28/14 Pct Recovery = 114% Analysis Date = 10/21/14 Pct Recovery = 114% Analysis Date = 10/21/14 Pct Recovery = 114% Analysis Date = 10/15/14 Pct Recovery = 114% Analysis Date = 10/15/14 Pct Recovery = 114% Analysis Date = 10/09/14 Pct Recovery = 114% Analysis Date = 10/09/14 Pct Recovery = 114% Analysis Date = 10/03/14 Pct Recovery = 114% Analysis Date = 10/03/14 Pct Recovery = 114% Analysis Date = 09/27/14 Pct Recovery = 114% Analysis Date = 09/27/14 Pct Recovery = 114% Analysis Date = 09/21/14 Pct Recovery = 114% Analysis Date = 09/21/14 Pct Recovery = 114% Analysis Date = 09/15/14 Pct Recovery = 114% Analysis Date = 09/15/14 Pct Recovery = 114% Analysis Date = 09/09/14 Pct Recovery = 114% Analysis Date = 09/09/14 Pct Recovery = 114% Analysis Date = 09/03/14 Pct Recovery = 114% Analysis Date = 09/03/14 Pct Recovery = 114% Analysis Date = 08/28/14 Pct Recovery = 114% Analysis Date = 08/28/14 Pct Recovery = 114% Analysis Date = 08/22/14 Pct Recovery = 114% Analysis Date = 08/22/14 Pct Recovery = 114% Analysis Date = 08/16/14 Pct Recovery = 114% Analysis Date = 08/16/14 Pct Recovery = 114% Analysis Date = 08/10/14 Pct Recovery = 114% Analysis Date = 08/10/14 Pct Recovery = 114% Analysis Date = 08/04/14 Pct Recovery = 114% Analysis Date = 08/04/14 Pct Recovery = 114% Analysis Date = 07/29/14 Pct Recovery = 113% Analysis Date = 07/29/14 Pct Recovery = 113% Analysis Date = 07/23/14 Pct Recovery = 113% Analysis Date = 07/23/14 Pct Recovery = 113% Analysis Date = 07/17/14 Pct Recovery = 113% Analysis Date = 07/17/14 Pct Recovery = 113% Analysis Date = 07/11/14 Pct Recovery = 113% Analysis Date = 07/11/14 Pct Recovery = 113% Analysis Date = 07/05/14 Pct Recovery = 113% Analysis Date = 07/05/14 Pct Recovery = 113% Analysis Date = 06/29/14 Pct Recovery = 113% Analysis Date = 06/29/14 Pct Recovery = 113% Analysis Date = 06/23/14 Pct Recovery = 113% Analysis Date = 06/23/14 Pct Recovery = 113% Analysis Date = 06/17/14 Pct Recovery = 113% Analysis Date = 06/17/14 Pct Recovery = 113% Analysis Date = 06/11/14 Pct Recovery = 112% Analysis Date = 06/11/14 Pct Recovery = 112% Analysis Date = 06/05/14 Pct Recovery = 112% Analysis Date = 06/05/14 Pct Recovery = 112% Analysis Date = 05/30/14 Pct Recovery = 112% Analysis Date = 05/30/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/24/14 Pct Recovery = 112% Analysis Date = 05/18/14 Pct Recovery = 112% Analysis Date = 05/18/14 Pct Recovery = 112% Analysis Date = 05/12/14 Pct Recovery = 112% Analysis Date = 05/12/14 Pct Recovery = 112% Analysis Date = 05/06/14 Pct Recovery = 112% Analysis Date = 05/06/14 Pct Recovery = 112% Analysis Date = 04/30/14 Pct Recovery = 111% Analysis Date = 04/30/14 Pct Recovery = 111% Analysis Date = 04/24/14 Pct Recovery = 111% Analysis Date = 04/24/14 Pct Recovery = 111% Analysis Date = 04/18/14 Pct Recovery = 111% Analysis Date = 04/18/14 Pct Recovery = 111% Analysis Date = 04/12/14 Pct Recovery = 111% Analysis Date = 04/12/14 Pct Recovery = 111% Analysis Date = 04/06/14 Pct Recovery = 111% Analysis Date = 04/06/14 Pct Recovery = 111% Analysis Date = 03/31/14 Pct Recovery = 111% Analysis Date = 03/31/14 Pct Recovery = 111% Analysis Date = 03/25/14 Pct Recovery = 111% Analysis Date = 03/25/14 Pct Recovery = 111% Analysis Date = 03/19/14 Pct Recovery = 111% Analysis Date = 03/19/14 Pct Recovery = 111% Analysis Date = 03/13/14 Pct Recovery = 110% Analysis Date = 03/13/14 Pct Recovery = 110% Analysis Date = 03/07/14 Pct Recovery = 110% Analysis Date = 03/07/14 Pct Recovery = 110% Analysis Date = 03/01/14 Pct Recovery = 110% Analysis Date = 03/01/14 Pct Recovery = 110% Analysis Date = 02/23/14 Pct Recovery = 110% Analysis Date = 02/23/14 Pct Recovery = 110% Analysis Date = 02/17/14 Pct Recovery = 110% Analysis Date = 02/17/14 Pct Recovery = 110% Analysis Date = 02/11/14 Pct Recovery = 110% Analysis Date = 02/11/14 Pct Recovery = 110% Analysis Date = 02/05/14 Pct Recovery = 110% Analysis Date = 02/05/14 Pct Recovery = 110% Analysis Date = 01/30/14 Pct Recovery = 110% Analysis Date = 01/30/14 Pct Recovery = 110% Analysis Date = 01/24/14 Pct Recovery = 109% Analysis Date = 01/24/14 Pct Recovery = 109% Analysis Date = 01/18/14 Pct Recovery = 109% Analysis Date = 01/18/14 Pct Recovery = 109% Analysis Date = 01/12/14 Pct Recovery = 109% Analysis Date = 01/12/14 Pct Recovery = 109% Analysis Date = 01/06/14 Pct Recovery = 109% Analysis Date = 01/06/14 Pct Recovery = 109% Analysis Date = 12/31/13 Pct Recovery = 109% Analysis Date = 12/31/13 Pct Recovery = 109% Analysis Date = 12/25/13 Pct Recovery = 109% Analysis Date = 12/25/13 Pct Recovery = 109% Analysis Date = 12/19/13 Pct Recovery = 109% Analysis Date = 12/19/13 Pct Recovery = 109% Analysis Date = 12/13/13 Pct Recovery = 108% Analysis Date = 12/13/13 Pct Recovery = 108% Analysis Date = 12/07/13 Pct Recovery = 108% Analysis Date = 12/07/13 Pct Recovery = 108% Analysis Date = 12/01/13 Pct Recovery = 108% Analysis Date = 12/01/13 Pct Recovery = 108% Analysis Date = 11/25/13 Pct Recovery = 108% Analysis Date = 11/25/13 Pct Recovery = 108% Analysis Date = 11/19/13 Pct Recovery = 108% Analysis Date = 11/19/13 Pct Recovery = 108% Analysis Date = 11/13/13 Pct Recovery = 108% Analysis Date = 11/13/13 Pct Recovery = 108% Analysis Date = 11/07/13 Pct Recovery = 108% Analysis Date = 11/07/13 Pct Recovery = 108% Analysis Date = 11/01/13 Pct Recovery = 108% Analysis Date = 11/01/13 Pct Recovery = 108% Analysis Date = 10/26/13 Pct Recovery = 107% Analysis Date = 10/26/13 Pct Recovery = 107% Analysis Date = 10/20/13 Pct Recovery = 107% Analysis Date = 10/20/13 Pct Recovery = 107% Analysis Date = 10/14/13 Pct Recovery = 107% Analysis Date = 10/14/13 Pct Recovery = 107% Analysis Date = 10/08/13 Pct Recovery = 107% Analysis Date = 10/08/13 Pct Recovery = 107% Analysis Date = 10/02/13 Pct Recovery = 107% Analysis Date = 10/02/13 Pct Recovery = 107% Analysis Date = 09/26/13 Pct Recovery = 107% Analysis Date = 09/26/13 Pct Recovery = 107% Analysis Date = 09/20/13 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ORYZALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 108 106% 27% 104% 21%
Total 108 106% 27% 104% 21%

Sample Statistics
ORYZALIN

Characteristic N % % Basis
Plotted 108 97% Spiked
Estimated Values 12 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 3% Spiked
Spiked 111 .  
False Negatives 0 0% 0 out of 111
Not Spiked 67 .  
False Positives 0 0% 0 out of 67