BQS OBSP Determination:
NICOSULFURON
METHOD: 2437 , TESTIDCODE: 61685LCM60
Open Data Set

Analysis Date = 03/04/14 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & ChemService 1448600: 2 Pct Recovery = 46% Analysis Date = 02/06/14 SpikeMix = NSI 042213HPLC: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 42% Analysis Date = 11/21/13 SpikeMix = Supelco LC01386: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 66% Analysis Date = 10/31/13 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & Accu 213041030: 2 µl Pct Recovery = 111% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 27% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 23% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 21% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 21% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 23% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 20% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 56% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 61% Analysis Date = 12/09/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 54% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 51% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 46% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 49% Analysis Date = 06/11/14 SpikeMix = ChemService 2598800: 60 µl & ChemService 2609400: 60 µl Pct Recovery = 94% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 6% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 5% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 55% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 53% Analysis Date = 12/16/14 SpikeMix = ChemService 2598800: 30 µl & Abs 042314: 30 µl Pct Recovery = 48% Analysis Date = 12/02/14 SpikeMix = Abs 042914: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 46% Analysis Date = 10/07/14 SpikeMix = ERA 0321-14-07: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 54% Analysis Date = 06/26/14 SpikeMix = ChemService 2598800: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 80% Analysis Date = 02/11/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 50% Analysis Date = 11/18/14 SpikeMix = Abs 042814Pest3: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 68% Analysis Date = 11/05/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 64% Analysis Date = 10/21/14 SpikeMix = Abs 042814Pest3: 30 µl & Abs 042314: 30 µl Pct Recovery = 70% Analysis Date = 07/19/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 53% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 18% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 21% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 19% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 25% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 27% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 8% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 9% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 13% Analysis Date = 07/22/15 SpikeMix = ERA 0406-15-04: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 23% Analysis Date = 07/18/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 21% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 68% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 56% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 55% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 51% Analysis Date = 03/11/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 57% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 55% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 63% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 50% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 42% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 55% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 56% Analysis Date = 08/19/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 68% Analysis Date = 08/19/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 61% Analysis Date = 08/19/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 52% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 59% Analysis Date = 01/10/17 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 56% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 46% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 43% Analysis Date = 04/15/15 SpikeMix = ChemService 2598800: 15 µl & Abs 042914: 15 µl Pct Recovery = 25% Analysis Date = 03/07/15 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 39% Analysis Date = 08/17/14 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 49% Analysis Date = 05/17/14 SpikeMix = ChemService 2598800: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 108% Analysis Date = 04/09/15 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 53% Analysis Date = 04/08/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 59% Analysis Date = 09/23/14 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 49% Analysis Date = 09/10/14 SpikeMix = Abs 042914: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 46% Analysis Date = 08/20/14 SpikeMix = Abs 042814Pest3: 15 µl & Abs 042314: 15 µl Pct Recovery = 51% Analysis Date = 07/31/14 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 65% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 21% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 20% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 16% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 19% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 19% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 12% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 37% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 41% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 28% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 32% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 25% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 18% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 21% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 49% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 59% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 49% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 81% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 56% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 73% Analysis Date = 02/18/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 41% Analysis Date = 02/18/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 66% Analysis Date = 02/18/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 44% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 58% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 55% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 72% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 51% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 51% Analysis Date = 10/07/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 53% Analysis Date = 01/09/17 Pct Recovery = 44% Analysis Date = 01/04/17 Pct Recovery = 44% Analysis Date = 01/04/17 Pct Recovery = 44% Analysis Date = 12/29/16 Pct Recovery = 44% Analysis Date = 12/29/16 Pct Recovery = 44% Analysis Date = 12/23/16 Pct Recovery = 44% Analysis Date = 12/23/16 Pct Recovery = 44% Analysis Date = 12/17/16 Pct Recovery = 44% Analysis Date = 12/17/16 Pct Recovery = 44% Analysis Date = 12/11/16 Pct Recovery = 44% Analysis Date = 12/11/16 Pct Recovery = 44% Analysis Date = 12/05/16 Pct Recovery = 44% Analysis Date = 12/05/16 Pct Recovery = 44% Analysis Date = 11/30/16 Pct Recovery = 44% Analysis Date = 11/30/16 Pct Recovery = 44% Analysis Date = 11/24/16 Pct Recovery = 44% Analysis Date = 11/24/16 Pct Recovery = 44% Analysis Date = 11/18/16 Pct Recovery = 44% Analysis Date = 11/18/16 Pct Recovery = 44% Analysis Date = 11/12/16 Pct Recovery = 44% Analysis Date = 11/12/16 Pct Recovery = 44% Analysis Date = 11/06/16 Pct Recovery = 43% Analysis Date = 11/06/16 Pct Recovery = 43% Analysis Date = 10/31/16 Pct Recovery = 43% Analysis Date = 10/31/16 Pct Recovery = 43% Analysis Date = 10/26/16 Pct Recovery = 43% Analysis Date = 10/26/16 Pct Recovery = 43% Analysis Date = 10/20/16 Pct Recovery = 43% Analysis Date = 10/20/16 Pct Recovery = 43% Analysis Date = 10/14/16 Pct Recovery = 43% Analysis Date = 10/14/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/02/16 Pct Recovery = 43% Analysis Date = 10/02/16 Pct Recovery = 43% Analysis Date = 09/26/16 Pct Recovery = 43% Analysis Date = 09/26/16 Pct Recovery = 43% Analysis Date = 09/21/16 Pct Recovery = 43% Analysis Date = 09/21/16 Pct Recovery = 43% Analysis Date = 09/15/16 Pct Recovery = 43% Analysis Date = 09/15/16 Pct Recovery = 43% Analysis Date = 09/09/16 Pct Recovery = 43% Analysis Date = 09/09/16 Pct Recovery = 43% Analysis Date = 09/03/16 Pct Recovery = 43% Analysis Date = 09/03/16 Pct Recovery = 43% Analysis Date = 08/28/16 Pct Recovery = 43% Analysis Date = 08/28/16 Pct Recovery = 43% Analysis Date = 08/22/16 Pct Recovery = 43% Analysis Date = 08/22/16 Pct Recovery = 43% Analysis Date = 08/17/16 Pct Recovery = 43% Analysis Date = 08/17/16 Pct Recovery = 43% Analysis Date = 08/11/16 Pct Recovery = 43% Analysis Date = 08/11/16 Pct Recovery = 43% Analysis Date = 08/05/16 Pct Recovery = 43% Analysis Date = 08/05/16 Pct Recovery = 43% Analysis Date = 07/30/16 Pct Recovery = 43% Analysis Date = 07/30/16 Pct Recovery = 43% Analysis Date = 07/24/16 Pct Recovery = 43% Analysis Date = 07/24/16 Pct Recovery = 43% Analysis Date = 07/18/16 Pct Recovery = 43% Analysis Date = 07/18/16 Pct Recovery = 43% Analysis Date = 07/13/16 Pct Recovery = 43% Analysis Date = 07/13/16 Pct Recovery = 43% Analysis Date = 07/07/16 Pct Recovery = 43% Analysis Date = 07/07/16 Pct Recovery = 43% Analysis Date = 07/01/16 Pct Recovery = 43% Analysis Date = 07/01/16 Pct Recovery = 43% Analysis Date = 06/25/16 Pct Recovery = 43% Analysis Date = 06/25/16 Pct Recovery = 43% Analysis Date = 06/19/16 Pct Recovery = 43% Analysis Date = 06/19/16 Pct Recovery = 43% Analysis Date = 06/13/16 Pct Recovery = 43% Analysis Date = 06/13/16 Pct Recovery = 43% Analysis Date = 06/08/16 Pct Recovery = 43% Analysis Date = 06/08/16 Pct Recovery = 43% Analysis Date = 06/02/16 Pct Recovery = 43% Analysis Date = 06/02/16 Pct Recovery = 43% Analysis Date = 05/27/16 Pct Recovery = 43% Analysis Date = 05/27/16 Pct Recovery = 43% Analysis Date = 05/21/16 Pct Recovery = 43% Analysis Date = 05/21/16 Pct Recovery = 43% Analysis Date = 05/15/16 Pct Recovery = 43% Analysis Date = 05/15/16 Pct Recovery = 43% Analysis Date = 05/09/16 Pct Recovery = 43% Analysis Date = 05/09/16 Pct Recovery = 43% Analysis Date = 05/04/16 Pct Recovery = 43% Analysis Date = 05/04/16 Pct Recovery = 43% Analysis Date = 04/28/16 Pct Recovery = 43% Analysis Date = 04/28/16 Pct Recovery = 43% Analysis Date = 04/22/16 Pct Recovery = 42% Analysis Date = 04/22/16 Pct Recovery = 42% Analysis Date = 04/16/16 Pct Recovery = 42% Analysis Date = 04/16/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 04/10/16 Pct Recovery = 42% Analysis Date = 04/04/16 Pct Recovery = 42% Analysis Date = 04/04/16 Pct Recovery = 42% Analysis Date = 03/30/16 Pct Recovery = 42% Analysis Date = 03/30/16 Pct Recovery = 42% Analysis Date = 03/24/16 Pct Recovery = 42% Analysis Date = 03/24/16 Pct Recovery = 42% Analysis Date = 03/18/16 Pct Recovery = 42% Analysis Date = 03/18/16 Pct Recovery = 42% Analysis Date = 03/12/16 Pct Recovery = 42% Analysis Date = 03/12/16 Pct Recovery = 42% Analysis Date = 03/06/16 Pct Recovery = 42% Analysis Date = 03/06/16 Pct Recovery = 42% Analysis Date = 02/29/16 Pct Recovery = 42% Analysis Date = 02/29/16 Pct Recovery = 42% Analysis Date = 02/24/16 Pct Recovery = 42% Analysis Date = 02/24/16 Pct Recovery = 42% Analysis Date = 02/18/16 Pct Recovery = 42% Analysis Date = 02/18/16 Pct Recovery = 42% Analysis Date = 02/12/16 Pct Recovery = 42% Analysis Date = 02/12/16 Pct Recovery = 42% Analysis Date = 02/06/16 Pct Recovery = 42% Analysis Date = 02/06/16 Pct Recovery = 42% Analysis Date = 01/31/16 Pct Recovery = 42% Analysis Date = 01/31/16 Pct Recovery = 42% Analysis Date = 01/25/16 Pct Recovery = 42% Analysis Date = 01/25/16 Pct Recovery = 42% Analysis Date = 01/20/16 Pct Recovery = 42% Analysis Date = 01/20/16 Pct Recovery = 42% Analysis Date = 01/14/16 Pct Recovery = 41% Analysis Date = 01/14/16 Pct Recovery = 41% Analysis Date = 01/08/16 Pct Recovery = 41% Analysis Date = 01/08/16 Pct Recovery = 41% Analysis Date = 01/02/16 Pct Recovery = 41% Analysis Date = 01/02/16 Pct Recovery = 41% Analysis Date = 12/27/15 Pct Recovery = 41% Analysis Date = 12/27/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/21/15 Pct Recovery = 41% Analysis Date = 12/16/15 Pct Recovery = 41% Analysis Date = 12/16/15 Pct Recovery = 41% Analysis Date = 12/10/15 Pct Recovery = 41% Analysis Date = 12/10/15 Pct Recovery = 41% Analysis Date = 12/04/15 Pct Recovery = 41% Analysis Date = 12/04/15 Pct Recovery = 41% Analysis Date = 11/28/15 Pct Recovery = 41% Analysis Date = 11/28/15 Pct Recovery = 41% Analysis Date = 11/22/15 Pct Recovery = 41% Analysis Date = 11/22/15 Pct Recovery = 41% Analysis Date = 11/16/15 Pct Recovery = 41% Analysis Date = 11/16/15 Pct Recovery = 41% Analysis Date = 11/11/15 Pct Recovery = 41% Analysis Date = 11/11/15 Pct Recovery = 41% Analysis Date = 11/05/15 Pct Recovery = 41% Analysis Date = 11/05/15 Pct Recovery = 41% Analysis Date = 10/30/15 Pct Recovery = 41% Analysis Date = 10/30/15 Pct Recovery = 41% Analysis Date = 10/24/15 Pct Recovery = 40% Analysis Date = 10/24/15 Pct Recovery = 40% Analysis Date = 10/18/15 Pct Recovery = 40% Analysis Date = 10/18/15 Pct Recovery = 40% Analysis Date = 10/12/15 Pct Recovery = 40% Analysis Date = 10/12/15 Pct Recovery = 40% Analysis Date = 10/07/15 Pct Recovery = 40% Analysis Date = 10/07/15 Pct Recovery = 40% Analysis Date = 10/01/15 Pct Recovery = 39% Analysis Date = 10/01/15 Pct Recovery = 39% Analysis Date = 09/25/15 Pct Recovery = 39% Analysis Date = 09/25/15 Pct Recovery = 39% Analysis Date = 09/19/15 Pct Recovery = 38% Analysis Date = 09/19/15 Pct Recovery = 38% Analysis Date = 09/13/15 Pct Recovery = 38% Analysis Date = 09/13/15 Pct Recovery = 38% Analysis Date = 09/07/15 Pct Recovery = 38% Analysis Date = 09/07/15 Pct Recovery = 38% Analysis Date = 09/02/15 Pct Recovery = 38% Analysis Date = 09/02/15 Pct Recovery = 38% Analysis Date = 08/27/15 Pct Recovery = 38% Analysis Date = 08/27/15 Pct Recovery = 38% Analysis Date = 08/21/15 Pct Recovery = 38% Analysis Date = 08/21/15 Pct Recovery = 38% Analysis Date = 08/15/15 Pct Recovery = 38% Analysis Date = 08/15/15 Pct Recovery = 38% Analysis Date = 08/09/15 Pct Recovery = 38% Analysis Date = 08/09/15 Pct Recovery = 38% Analysis Date = 08/03/15 Pct Recovery = 39% Analysis Date = 08/03/15 Pct Recovery = 39% Analysis Date = 07/29/15 Pct Recovery = 39% Analysis Date = 07/29/15 Pct Recovery = 39% Analysis Date = 07/23/15 Pct Recovery = 39% Analysis Date = 07/23/15 Pct Recovery = 39% Analysis Date = 07/17/15 Pct Recovery = 40% Analysis Date = 07/17/15 Pct Recovery = 40% Analysis Date = 07/11/15 Pct Recovery = 40% Analysis Date = 07/11/15 Pct Recovery = 40% Analysis Date = 07/05/15 Pct Recovery = 40% Analysis Date = 07/05/15 Pct Recovery = 40% Analysis Date = 06/29/15 Pct Recovery = 41% Analysis Date = 06/29/15 Pct Recovery = 41% Analysis Date = 06/24/15 Pct Recovery = 41% Analysis Date = 06/24/15 Pct Recovery = 41% Analysis Date = 06/18/15 Pct Recovery = 41% Analysis Date = 06/18/15 Pct Recovery = 41% Analysis Date = 06/12/15 Pct Recovery = 42% Analysis Date = 06/12/15 Pct Recovery = 42% Analysis Date = 06/06/15 Pct Recovery = 42% Analysis Date = 06/06/15 Pct Recovery = 42% Analysis Date = 05/31/15 Pct Recovery = 42% Analysis Date = 05/31/15 Pct Recovery = 42% Analysis Date = 05/25/15 Pct Recovery = 43% Analysis Date = 05/25/15 Pct Recovery = 43% Analysis Date = 05/19/15 Pct Recovery = 43% Analysis Date = 05/19/15 Pct Recovery = 43% Analysis Date = 05/14/15 Pct Recovery = 44% Analysis Date = 05/14/15 Pct Recovery = 44% Analysis Date = 05/08/15 Pct Recovery = 44% Analysis Date = 05/08/15 Pct Recovery = 44% Analysis Date = 05/02/15 Pct Recovery = 44% Analysis Date = 05/02/15 Pct Recovery = 44% Analysis Date = 04/26/15 Pct Recovery = 45% Analysis Date = 04/26/15 Pct Recovery = 45% Analysis Date = 04/20/15 Pct Recovery = 45% Analysis Date = 04/20/15 Pct Recovery = 45% Analysis Date = 04/14/15 Pct Recovery = 45% Analysis Date = 04/14/15 Pct Recovery = 45% Analysis Date = 04/09/15 Pct Recovery = 46% Analysis Date = 04/09/15 Pct Recovery = 46% Analysis Date = 04/03/15 Pct Recovery = 46% Analysis Date = 04/03/15 Pct Recovery = 46% Analysis Date = 03/28/15 Pct Recovery = 46% Analysis Date = 03/28/15 Pct Recovery = 46% Analysis Date = 03/22/15 Pct Recovery = 47% Analysis Date = 03/22/15 Pct Recovery = 47% Analysis Date = 03/16/15 Pct Recovery = 47% Analysis Date = 03/16/15 Pct Recovery = 47% Analysis Date = 03/10/15 Pct Recovery = 48% Analysis Date = 03/10/15 Pct Recovery = 48% Analysis Date = 03/05/15 Pct Recovery = 48% Analysis Date = 03/05/15 Pct Recovery = 48% Analysis Date = 02/27/15 Pct Recovery = 49% Analysis Date = 02/27/15 Pct Recovery = 49% Analysis Date = 02/21/15 Pct Recovery = 49% Analysis Date = 02/21/15 Pct Recovery = 49% Analysis Date = 02/15/15 Pct Recovery = 49% Analysis Date = 02/15/15 Pct Recovery = 49% Analysis Date = 02/09/15 Pct Recovery = 50% Analysis Date = 02/09/15 Pct Recovery = 50% Analysis Date = 02/03/15 Pct Recovery = 50% Analysis Date = 02/03/15 Pct Recovery = 50% Analysis Date = 01/29/15 Pct Recovery = 51% Analysis Date = 01/29/15 Pct Recovery = 51% Analysis Date = 01/23/15 Pct Recovery = 51% Analysis Date = 01/23/15 Pct Recovery = 51% Analysis Date = 01/17/15 Pct Recovery = 51% Analysis Date = 01/17/15 Pct Recovery = 51% Analysis Date = 01/11/15 Pct Recovery = 52% Analysis Date = 01/11/15 Pct Recovery = 52% Analysis Date = 01/05/15 Pct Recovery = 52% Analysis Date = 01/05/15 Pct Recovery = 52% Analysis Date = 12/30/14 Pct Recovery = 53% Analysis Date = 12/30/14 Pct Recovery = 53% Analysis Date = 12/25/14 Pct Recovery = 53% Analysis Date = 12/25/14 Pct Recovery = 53% Analysis Date = 12/19/14 Pct Recovery = 53% Analysis Date = 12/19/14 Pct Recovery = 53% Analysis Date = 12/13/14 Pct Recovery = 54% Analysis Date = 12/13/14 Pct Recovery = 54% Analysis Date = 12/07/14 Pct Recovery = 54% Analysis Date = 12/07/14 Pct Recovery = 54% Analysis Date = 12/01/14 Pct Recovery = 55% Analysis Date = 12/01/14 Pct Recovery = 55% Analysis Date = 11/25/14 Pct Recovery = 55% Analysis Date = 11/25/14 Pct Recovery = 55% Analysis Date = 11/20/14 Pct Recovery = 55% Analysis Date = 11/20/14 Pct Recovery = 55% Analysis Date = 11/14/14 Pct Recovery = 56% Analysis Date = 11/14/14 Pct Recovery = 56% Analysis Date = 11/08/14 Pct Recovery = 56% Analysis Date = 11/08/14 Pct Recovery = 56% Analysis Date = 11/02/14 Pct Recovery = 56% Analysis Date = 11/02/14 Pct Recovery = 56% Analysis Date = 10/27/14 Pct Recovery = 57% Analysis Date = 10/27/14 Pct Recovery = 57% Analysis Date = 10/21/14 Pct Recovery = 57% Analysis Date = 10/21/14 Pct Recovery = 57% Analysis Date = 10/16/14 Pct Recovery = 57% Analysis Date = 10/16/14 Pct Recovery = 57% Analysis Date = 10/10/14 Pct Recovery = 58% Analysis Date = 10/10/14 Pct Recovery = 58% Analysis Date = 10/04/14 Pct Recovery = 58% Analysis Date = 10/04/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/28/14 Pct Recovery = 58% Analysis Date = 09/22/14 Pct Recovery = 59% Analysis Date = 09/22/14 Pct Recovery = 59% Analysis Date = 09/16/14 Pct Recovery = 59% Analysis Date = 09/16/14 Pct Recovery = 59% Analysis Date = 09/11/14 Pct Recovery = 59% Analysis Date = 09/11/14 Pct Recovery = 59% Analysis Date = 09/05/14 Pct Recovery = 60% Analysis Date = 09/05/14 Pct Recovery = 60% Analysis Date = 08/30/14 Pct Recovery = 60% Analysis Date = 08/30/14 Pct Recovery = 60% Analysis Date = 08/24/14 Pct Recovery = 61% Analysis Date = 08/24/14 Pct Recovery = 61% Analysis Date = 08/18/14 Pct Recovery = 61% Analysis Date = 08/18/14 Pct Recovery = 61% Analysis Date = 08/12/14 Pct Recovery = 61% Analysis Date = 08/12/14 Pct Recovery = 61% Analysis Date = 08/07/14 Pct Recovery = 62% Analysis Date = 08/07/14 Pct Recovery = 62% Analysis Date = 08/01/14 Pct Recovery = 62% Analysis Date = 08/01/14 Pct Recovery = 62% Analysis Date = 07/26/14 Pct Recovery = 63% Analysis Date = 07/26/14 Pct Recovery = 63% Analysis Date = 07/20/14 Pct Recovery = 63% Analysis Date = 07/20/14 Pct Recovery = 63% Analysis Date = 07/14/14 Pct Recovery = 63% Analysis Date = 07/14/14 Pct Recovery = 63% Analysis Date = 07/08/14 Pct Recovery = 64% Analysis Date = 07/08/14 Pct Recovery = 64% Analysis Date = 07/03/14 Pct Recovery = 64% Analysis Date = 07/03/14 Pct Recovery = 64% Analysis Date = 06/27/14 Pct Recovery = 65% Analysis Date = 06/27/14 Pct Recovery = 65% Analysis Date = 06/21/14 Pct Recovery = 65% Analysis Date = 06/21/14 Pct Recovery = 65% Analysis Date = 06/15/14 Pct Recovery = 65% Analysis Date = 06/15/14 Pct Recovery = 65% Analysis Date = 06/09/14 Pct Recovery = 66% Analysis Date = 06/09/14 Pct Recovery = 66% Analysis Date = 06/03/14 Pct Recovery = 66% Analysis Date = 06/03/14 Pct Recovery = 66% Analysis Date = 05/29/14 Pct Recovery = 67% Analysis Date = 05/29/14 Pct Recovery = 67% Analysis Date = 05/23/14 Pct Recovery = 67% Analysis Date = 05/23/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Analysis Date = 05/17/14 Pct Recovery = 67% Analysis Date = 05/11/14 Pct Recovery = 68% Analysis Date = 05/11/14 Pct Recovery = 68% Analysis Date = 05/05/14 Pct Recovery = 68% Analysis Date = 05/05/14 Pct Recovery = 68% Analysis Date = 04/29/14 Pct Recovery = 69% Analysis Date = 04/29/14 Pct Recovery = 69% Analysis Date = 04/24/14 Pct Recovery = 69% Analysis Date = 04/24/14 Pct Recovery = 69% Analysis Date = 04/18/14 Pct Recovery = 70% Analysis Date = 04/18/14 Pct Recovery = 70% Analysis Date = 04/12/14 Pct Recovery = 70% Analysis Date = 04/12/14 Pct Recovery = 70% Analysis Date = 04/06/14 Pct Recovery = 70% Analysis Date = 04/06/14 Pct Recovery = 70% Analysis Date = 03/31/14 Pct Recovery = 71% Analysis Date = 03/31/14 Pct Recovery = 71% Analysis Date = 03/25/14 Pct Recovery = 71% Analysis Date = 03/25/14 Pct Recovery = 71% Analysis Date = 03/20/14 Pct Recovery = 72% Analysis Date = 03/20/14 Pct Recovery = 72% Analysis Date = 03/14/14 Pct Recovery = 72% Analysis Date = 03/14/14 Pct Recovery = 72% Analysis Date = 03/08/14 Pct Recovery = 72% Analysis Date = 03/08/14 Pct Recovery = 72% Analysis Date = 03/02/14 Pct Recovery = 73% Analysis Date = 03/02/14 Pct Recovery = 73% Analysis Date = 02/24/14 Pct Recovery = 73% Analysis Date = 02/24/14 Pct Recovery = 73% Analysis Date = 02/18/14 Pct Recovery = 74% Analysis Date = 02/18/14 Pct Recovery = 74% Analysis Date = 02/13/14 Pct Recovery = 74% Analysis Date = 02/13/14 Pct Recovery = 74% Analysis Date = 02/07/14 Pct Recovery = 74% Analysis Date = 02/07/14 Pct Recovery = 74% Analysis Date = 02/01/14 Pct Recovery = 75% Analysis Date = 02/01/14 Pct Recovery = 75% Analysis Date = 01/26/14 Pct Recovery = 75% Analysis Date = 01/26/14 Pct Recovery = 75% Analysis Date = 01/20/14 Pct Recovery = 76% Analysis Date = 01/20/14 Pct Recovery = 76% Analysis Date = 01/14/14 Pct Recovery = 76% Analysis Date = 01/14/14 Pct Recovery = 76% Analysis Date = 01/09/14 Pct Recovery = 77% Analysis Date = 01/09/14 Pct Recovery = 77% Analysis Date = 01/03/14 Pct Recovery = 77% Analysis Date = 01/03/14 Pct Recovery = 77% Analysis Date = 12/28/13 Pct Recovery = 77% Analysis Date = 12/28/13 Pct Recovery = 77% Analysis Date = 12/22/13 Pct Recovery = 78% Analysis Date = 12/22/13 Pct Recovery = 78% Analysis Date = 12/16/13 Pct Recovery = 78% Analysis Date = 12/16/13 Pct Recovery = 78% Analysis Date = 12/10/13 Pct Recovery = 79% Analysis Date = 12/10/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 12/05/13 Pct Recovery = 79% Analysis Date = 11/29/13 Pct Recovery = 79% Analysis Date = 11/29/13 Pct Recovery = 79% Analysis Date = 11/23/13 Pct Recovery = 80% Analysis Date = 11/23/13 Pct Recovery = 80% Analysis Date = 11/17/13 Pct Recovery = 80% Analysis Date = 11/17/13 Pct Recovery = 80% Analysis Date = 11/11/13 Pct Recovery = 81% Analysis Date = 11/11/13 Pct Recovery = 81% Analysis Date = 11/05/13 Pct Recovery = 81% Analysis Date = 11/05/13 Pct Recovery = 81% Analysis Date = 10/31/13 Pct Recovery = 81% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
NICOSULFURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 96 45% 21% 49% 23%
Total 96 45% 21% 49% 23%

Sample Statistics
NICOSULFURON

Characteristic N % % Basis
Plotted 96 93% Spiked
Estimated Values 21 20% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 106 .  
False Negatives 7 7% 7 out of 103
Not Spiked 72 .  
False Positives 0 0% 0 out of 72