BQS OBSP Determination:
FIPRONIL SULFONE
METHOD: 2437 , TESTIDCODE: 66613LCM60
Open Data Set

Analysis Date = 12/18/13 SpikeMix = ChemService 1473000: 5 µl & Supelco LB99392: 5 µl & Abs 042413: 5 µl Pct Recovery = 64% Analysis Date = 02/19/14 SpikeMix = Spex Organics T1130514013: 5 µl & ERA 0318-13-02.2: 5 µl & Crescent 04CC101: 5 µ Pct Recovery = 81% Analysis Date = 09/24/13 SpikeMix = Spex Organics T1130514013: 5 µl & ERA 0318-13-02.2: 5 µl & Crescent 04CC101: 5 µ Pct Recovery = 71% Analysis Date = 01/28/14 SpikeMix = Abs 042413: 2 µl & Spex Organics T1130514013: 2 µl & Supelco LB99392: 2 µl Pct Recovery = 85% Analysis Date = 11/19/13 SpikeMix = Spex Organics T1130514013: 2 µl & Supelco LB99392: 2 µl & Crescent 04CC101: 2 µl Pct Recovery = 86% Analysis Date = 01/07/14 SpikeMix = ERA 0318-13-02.2: 2 µl & Abs 042413: 2 µl & Spex Organics T1130514013: 2 µl Pct Recovery = 65% Analysis Date = 12/17/13 SpikeMix = Spex Organics T1130517007: 2 µl & ERA 0318-13-02.1: 2 µl & Abs 041613: 2 µl Pct Recovery = 81% Analysis Date = 12/10/13 SpikeMix = Abs 041613: 2 µl & ChemService 1466000: 2 µl & Accu 213041078: 2 µl Pct Recovery = 95% Analysis Date = 09/28/13 SpikeMix = Accu 213041078b: 2 µl & Abs 041613: 2 µl & Spex Organics T1130517007: 2 µl Pct Recovery = 94% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 117% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 114% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 113% Analysis Date = 09/25/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 120% Analysis Date = 09/25/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 124% Analysis Date = 09/25/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 123% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 79% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 66% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 75% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 99% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 93% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 94% Analysis Date = 06/10/14 SpikeMix = ChemService 2598800: 60 µl & ChemService 2609400: 60 µl Pct Recovery = 96% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 115% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 121% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 70% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 56% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 13% Analysis Date = 07/22/16 SpikeMix = ChemService 5154100: 80 µl & ChemService 5154200: 80 µl & Spex Organics TS160603 Pct Recovery = 24% Analysis Date = 12/16/14 SpikeMix = ChemService 2598800: 30 µl & Abs 042314: 30 µl Pct Recovery = 104% Analysis Date = 12/03/14 SpikeMix = Abs 042914: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 92% Analysis Date = 10/07/14 SpikeMix = ERA 0321-14-07: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 120% Analysis Date = 06/25/14 SpikeMix = ChemService 2598800: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 94% Analysis Date = 02/10/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 89% Analysis Date = 01/28/15 SpikeMix = ERA 0321-14-07: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 85% Analysis Date = 11/18/14 SpikeMix = Abs 042814Pest3: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 124% Analysis Date = 11/04/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 114% Analysis Date = 10/20/14 SpikeMix = Abs 042814Pest3: 30 µl & Abs 042314: 30 µl Pct Recovery = 114% Analysis Date = 07/19/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 99% Analysis Date = 05/10/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 110% Analysis Date = 05/10/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 112% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 116% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 128% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 115% Analysis Date = 01/20/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 83% Analysis Date = 01/20/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 97% Analysis Date = 01/20/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 93% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 88% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 133% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 122% Analysis Date = 08/20/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 134% Analysis Date = 08/18/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 115% Analysis Date = 08/18/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 103% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 97% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 101% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 80% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 81% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 75% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 81% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 61% Analysis Date = 07/21/15 SpikeMix = ERA 0406-15-04: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 78% Analysis Date = 07/17/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 91% Analysis Date = 12/13/16 SpikeMix = Abs 071816: 40 µl & Spex Organics TS160603008: 40 µl Pct Recovery = 76% Analysis Date = 11/09/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 95% Analysis Date = 11/09/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 102% Analysis Date = 07/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 30% Analysis Date = 04/15/15 SpikeMix = ChemService 2598800: 15 µl & Abs 042914: 15 µl Pct Recovery = 47% Analysis Date = 03/03/15 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 38% Analysis Date = 08/13/14 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 139% Analysis Date = 05/21/14 SpikeMix = ChemService 2598800: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 88% Analysis Date = 04/07/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 156% Analysis Date = 04/02/15 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 87% Analysis Date = 09/23/14 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 115% Analysis Date = 09/10/14 SpikeMix = Abs 042914: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 190% Analysis Date = 08/19/14 SpikeMix = Abs 042814Pest3: 15 µl & Abs 042314: 15 µl Pct Recovery = 89% Analysis Date = 07/30/14 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 111% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 100% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 105% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 120% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 127% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 140% Analysis Date = 03/01/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 127% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 88% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 88% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 161% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 150% Analysis Date = 11/24/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 156% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 89% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 95% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 92% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 92% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 97% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 104% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 119% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 114% Analysis Date = 02/09/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 121% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 127% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 125% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 124% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 117% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 121% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 136% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 97% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 102% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 92% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 93% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 103% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 74% Analysis Date = 12/07/16 Pct Recovery = 74% Analysis Date = 12/07/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 75% Analysis Date = 12/01/16 Pct Recovery = 75% Analysis Date = 11/25/16 Pct Recovery = 75% Analysis Date = 11/25/16 Pct Recovery = 75% Analysis Date = 11/19/16 Pct Recovery = 76% Analysis Date = 11/19/16 Pct Recovery = 76% Analysis Date = 11/13/16 Pct Recovery = 76% Analysis Date = 11/13/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 77% Analysis Date = 11/07/16 Pct Recovery = 77% Analysis Date = 11/01/16 Pct Recovery = 77% Analysis Date = 11/01/16 Pct Recovery = 77% Analysis Date = 10/26/16 Pct Recovery = 78% Analysis Date = 10/26/16 Pct Recovery = 78% Analysis Date = 10/21/16 Pct Recovery = 78% Analysis Date = 10/21/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 79% Analysis Date = 10/15/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 09/27/16 Pct Recovery = 80% Analysis Date = 09/27/16 Pct Recovery = 80% Analysis Date = 09/21/16 Pct Recovery = 81% Analysis Date = 09/21/16 Pct Recovery = 81% Analysis Date = 09/15/16 Pct Recovery = 81% Analysis Date = 09/15/16 Pct Recovery = 81% Analysis Date = 09/09/16 Pct Recovery = 81% Analysis Date = 09/09/16 Pct Recovery = 81% Analysis Date = 09/04/16 Pct Recovery = 82% Analysis Date = 09/04/16 Pct Recovery = 82% Analysis Date = 08/29/16 Pct Recovery = 82% Analysis Date = 08/29/16 Pct Recovery = 82% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/11/16 Pct Recovery = 83% Analysis Date = 08/11/16 Pct Recovery = 83% Analysis Date = 08/05/16 Pct Recovery = 83% Analysis Date = 08/05/16 Pct Recovery = 83% Analysis Date = 07/30/16 Pct Recovery = 84% Analysis Date = 07/30/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/19/16 Pct Recovery = 84% Analysis Date = 07/19/16 Pct Recovery = 84% Analysis Date = 07/13/16 Pct Recovery = 85% Analysis Date = 07/13/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/07/16 Pct Recovery = 85% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/19/16 Pct Recovery = 86% Analysis Date = 06/19/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/07/16 Pct Recovery = 87% Analysis Date = 06/07/16 Pct Recovery = 87% Analysis Date = 06/01/16 Pct Recovery = 87% Analysis Date = 06/01/16 Pct Recovery = 87% Analysis Date = 05/27/16 Pct Recovery = 88% Analysis Date = 05/27/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/15/16 Pct Recovery = 88% Analysis Date = 05/15/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 89% Analysis Date = 05/09/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 04/27/16 Pct Recovery = 90% Analysis Date = 04/27/16 Pct Recovery = 90% Analysis Date = 04/21/16 Pct Recovery = 92% Analysis Date = 04/21/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 94% Analysis Date = 04/10/16 Pct Recovery = 94% Analysis Date = 04/04/16 Pct Recovery = 95% Analysis Date = 04/04/16 Pct Recovery = 95% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/29/16 Pct Recovery = 96% Analysis Date = 03/23/16 Pct Recovery = 98% Analysis Date = 03/23/16 Pct Recovery = 98% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/17/16 Pct Recovery = 99% Analysis Date = 03/11/16 Pct Recovery = 100% Analysis Date = 03/11/16 Pct Recovery = 100% Analysis Date = 03/05/16 Pct Recovery = 101% Analysis Date = 03/05/16 Pct Recovery = 101% Analysis Date = 02/28/16 Pct Recovery = 102% Analysis Date = 02/28/16 Pct Recovery = 102% Analysis Date = 02/23/16 Pct Recovery = 104% Analysis Date = 02/23/16 Pct Recovery = 104% Analysis Date = 02/17/16 Pct Recovery = 105% Analysis Date = 02/17/16 Pct Recovery = 105% Analysis Date = 02/11/16 Pct Recovery = 106% Analysis Date = 02/11/16 Pct Recovery = 106% Analysis Date = 02/05/16 Pct Recovery = 107% Analysis Date = 02/05/16 Pct Recovery = 107% Analysis Date = 01/30/16 Pct Recovery = 107% Analysis Date = 01/30/16 Pct Recovery = 107% Analysis Date = 01/24/16 Pct Recovery = 107% Analysis Date = 01/24/16 Pct Recovery = 107% Analysis Date = 01/18/16 Pct Recovery = 107% Analysis Date = 01/18/16 Pct Recovery = 107% Analysis Date = 01/12/16 Pct Recovery = 107% Analysis Date = 01/12/16 Pct Recovery = 107% Analysis Date = 01/06/16 Pct Recovery = 107% Analysis Date = 01/06/16 Pct Recovery = 107% Analysis Date = 01/01/16 Pct Recovery = 107% Analysis Date = 01/01/16 Pct Recovery = 107% Analysis Date = 12/26/15 Pct Recovery = 107% Analysis Date = 12/26/15 Pct Recovery = 107% Analysis Date = 12/20/15 Pct Recovery = 107% Analysis Date = 12/20/15 Pct Recovery = 107% Analysis Date = 12/14/15 Pct Recovery = 107% Analysis Date = 12/14/15 Pct Recovery = 107% Analysis Date = 12/08/15 Pct Recovery = 107% Analysis Date = 12/08/15 Pct Recovery = 107% Analysis Date = 12/02/15 Pct Recovery = 107% Analysis Date = 12/02/15 Pct Recovery = 107% Analysis Date = 11/26/15 Pct Recovery = 107% Analysis Date = 11/26/15 Pct Recovery = 107% Analysis Date = 11/20/15 Pct Recovery = 107% Analysis Date = 11/20/15 Pct Recovery = 107% Analysis Date = 11/15/15 Pct Recovery = 107% Analysis Date = 11/15/15 Pct Recovery = 107% Analysis Date = 11/09/15 Pct Recovery = 107% Analysis Date = 11/09/15 Pct Recovery = 107% Analysis Date = 11/03/15 Pct Recovery = 107% Analysis Date = 11/03/15 Pct Recovery = 107% Analysis Date = 10/28/15 Pct Recovery = 107% Analysis Date = 10/28/15 Pct Recovery = 107% Analysis Date = 10/22/15 Pct Recovery = 107% Analysis Date = 10/22/15 Pct Recovery = 107% Analysis Date = 10/16/15 Pct Recovery = 107% Analysis Date = 10/16/15 Pct Recovery = 107% Analysis Date = 10/10/15 Pct Recovery = 106% Analysis Date = 10/10/15 Pct Recovery = 106% Analysis Date = 10/04/15 Pct Recovery = 106% Analysis Date = 10/04/15 Pct Recovery = 106% Analysis Date = 09/29/15 Pct Recovery = 105% Analysis Date = 09/29/15 Pct Recovery = 105% Analysis Date = 09/23/15 Pct Recovery = 105% Analysis Date = 09/23/15 Pct Recovery = 105% Analysis Date = 09/17/15 Pct Recovery = 104% Analysis Date = 09/17/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/11/15 Pct Recovery = 104% Analysis Date = 09/05/15 Pct Recovery = 103% Analysis Date = 09/05/15 Pct Recovery = 103% Analysis Date = 08/30/15 Pct Recovery = 103% Analysis Date = 08/30/15 Pct Recovery = 103% Analysis Date = 08/24/15 Pct Recovery = 102% Analysis Date = 08/24/15 Pct Recovery = 102% Analysis Date = 08/18/15 Pct Recovery = 101% Analysis Date = 08/18/15 Pct Recovery = 101% Analysis Date = 08/12/15 Pct Recovery = 101% Analysis Date = 08/12/15 Pct Recovery = 101% Analysis Date = 08/07/15 Pct Recovery = 100% Analysis Date = 08/07/15 Pct Recovery = 100% Analysis Date = 08/01/15 Pct Recovery = 101% Analysis Date = 08/01/15 Pct Recovery = 101% Analysis Date = 07/26/15 Pct Recovery = 101% Analysis Date = 07/26/15 Pct Recovery = 101% Analysis Date = 07/20/15 Pct Recovery = 101% Analysis Date = 07/20/15 Pct Recovery = 101% Analysis Date = 07/14/15 Pct Recovery = 101% Analysis Date = 07/14/15 Pct Recovery = 101% Analysis Date = 07/08/15 Pct Recovery = 101% Analysis Date = 07/08/15 Pct Recovery = 101% Analysis Date = 07/02/15 Pct Recovery = 101% Analysis Date = 07/02/15 Pct Recovery = 101% Analysis Date = 06/26/15 Pct Recovery = 101% Analysis Date = 06/26/15 Pct Recovery = 101% Analysis Date = 06/21/15 Pct Recovery = 101% Analysis Date = 06/21/15 Pct Recovery = 101% Analysis Date = 06/15/15 Pct Recovery = 102% Analysis Date = 06/15/15 Pct Recovery = 102% Analysis Date = 06/09/15 Pct Recovery = 102% Analysis Date = 06/09/15 Pct Recovery = 102% Analysis Date = 06/03/15 Pct Recovery = 102% Analysis Date = 06/03/15 Pct Recovery = 102% Analysis Date = 05/28/15 Pct Recovery = 102% Analysis Date = 05/28/15 Pct Recovery = 102% Analysis Date = 05/22/15 Pct Recovery = 102% Analysis Date = 05/22/15 Pct Recovery = 102% Analysis Date = 05/16/15 Pct Recovery = 102% Analysis Date = 05/16/15 Pct Recovery = 102% Analysis Date = 05/10/15 Pct Recovery = 102% Analysis Date = 05/10/15 Pct Recovery = 102% Analysis Date = 05/05/15 Pct Recovery = 103% Analysis Date = 05/05/15 Pct Recovery = 103% Analysis Date = 04/29/15 Pct Recovery = 103% Analysis Date = 04/29/15 Pct Recovery = 103% Analysis Date = 04/23/15 Pct Recovery = 103% Analysis Date = 04/23/15 Pct Recovery = 103% Analysis Date = 04/17/15 Pct Recovery = 103% Analysis Date = 04/17/15 Pct Recovery = 103% Analysis Date = 04/11/15 Pct Recovery = 103% Analysis Date = 04/11/15 Pct Recovery = 103% Analysis Date = 04/05/15 Pct Recovery = 103% Analysis Date = 04/05/15 Pct Recovery = 103% Analysis Date = 03/30/15 Pct Recovery = 103% Analysis Date = 03/30/15 Pct Recovery = 103% Analysis Date = 03/24/15 Pct Recovery = 103% Analysis Date = 03/24/15 Pct Recovery = 103% Analysis Date = 03/18/15 Pct Recovery = 104% Analysis Date = 03/18/15 Pct Recovery = 104% Analysis Date = 03/13/15 Pct Recovery = 104% Analysis Date = 03/13/15 Pct Recovery = 104% Analysis Date = 03/07/15 Pct Recovery = 104% Analysis Date = 03/07/15 Pct Recovery = 104% Analysis Date = 03/01/15 Pct Recovery = 104% Analysis Date = 03/01/15 Pct Recovery = 104% Analysis Date = 02/23/15 Pct Recovery = 104% Analysis Date = 02/23/15 Pct Recovery = 104% Analysis Date = 02/17/15 Pct Recovery = 104% Analysis Date = 02/17/15 Pct Recovery = 104% Analysis Date = 02/11/15 Pct Recovery = 104% Analysis Date = 02/11/15 Pct Recovery = 104% Analysis Date = 02/05/15 Pct Recovery = 104% Analysis Date = 02/05/15 Pct Recovery = 104% Analysis Date = 01/30/15 Pct Recovery = 104% Analysis Date = 01/30/15 Pct Recovery = 104% Analysis Date = 01/25/15 Pct Recovery = 104% Analysis Date = 01/25/15 Pct Recovery = 104% Analysis Date = 01/19/15 Pct Recovery = 104% Analysis Date = 01/19/15 Pct Recovery = 104% Analysis Date = 01/13/15 Pct Recovery = 104% Analysis Date = 01/13/15 Pct Recovery = 104% Analysis Date = 01/07/15 Pct Recovery = 104% Analysis Date = 01/07/15 Pct Recovery = 104% Analysis Date = 01/01/15 Pct Recovery = 104% Analysis Date = 01/01/15 Pct Recovery = 104% Analysis Date = 12/26/14 Pct Recovery = 104% Analysis Date = 12/26/14 Pct Recovery = 104% Analysis Date = 12/20/14 Pct Recovery = 104% Analysis Date = 12/20/14 Pct Recovery = 104% Analysis Date = 12/14/14 Pct Recovery = 104% Analysis Date = 12/14/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/09/14 Pct Recovery = 104% Analysis Date = 12/03/14 Pct Recovery = 104% Analysis Date = 12/03/14 Pct Recovery = 104% Analysis Date = 11/27/14 Pct Recovery = 104% Analysis Date = 11/27/14 Pct Recovery = 104% Analysis Date = 11/21/14 Pct Recovery = 104% Analysis Date = 11/21/14 Pct Recovery = 104% Analysis Date = 11/15/14 Pct Recovery = 104% Analysis Date = 11/15/14 Pct Recovery = 104% Analysis Date = 11/09/14 Pct Recovery = 104% Analysis Date = 11/09/14 Pct Recovery = 104% Analysis Date = 11/03/14 Pct Recovery = 104% Analysis Date = 11/03/14 Pct Recovery = 104% Analysis Date = 10/28/14 Pct Recovery = 103% Analysis Date = 10/28/14 Pct Recovery = 103% Analysis Date = 10/22/14 Pct Recovery = 103% Analysis Date = 10/22/14 Pct Recovery = 103% Analysis Date = 10/17/14 Pct Recovery = 103% Analysis Date = 10/17/14 Pct Recovery = 103% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/11/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 10/05/14 Pct Recovery = 102% Analysis Date = 09/29/14 Pct Recovery = 102% Analysis Date = 09/29/14 Pct Recovery = 102% Analysis Date = 09/23/14 Pct Recovery = 102% Analysis Date = 09/23/14 Pct Recovery = 102% Analysis Date = 09/17/14 Pct Recovery = 101% Analysis Date = 09/17/14 Pct Recovery = 101% Analysis Date = 09/11/14 Pct Recovery = 101% Analysis Date = 09/11/14 Pct Recovery = 101% Analysis Date = 09/05/14 Pct Recovery = 101% Analysis Date = 09/05/14 Pct Recovery = 101% Analysis Date = 08/31/14 Pct Recovery = 100% Analysis Date = 08/31/14 Pct Recovery = 100% Analysis Date = 08/25/14 Pct Recovery = 100% Analysis Date = 08/25/14 Pct Recovery = 100% Analysis Date = 08/19/14 Pct Recovery = 100% Analysis Date = 08/19/14 Pct Recovery = 100% Analysis Date = 08/13/14 Pct Recovery = 99% Analysis Date = 08/13/14 Pct Recovery = 99% Analysis Date = 08/07/14 Pct Recovery = 99% Analysis Date = 08/07/14 Pct Recovery = 99% Analysis Date = 08/01/14 Pct Recovery = 99% Analysis Date = 08/01/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 99% Analysis Date = 07/26/14 Pct Recovery = 99% Analysis Date = 07/20/14 Pct Recovery = 98% Analysis Date = 07/20/14 Pct Recovery = 98% Analysis Date = 07/15/14 Pct Recovery = 98% Analysis Date = 07/15/14 Pct Recovery = 98% Analysis Date = 07/09/14 Pct Recovery = 98% Analysis Date = 07/09/14 Pct Recovery = 98% Analysis Date = 07/03/14 Pct Recovery = 97% Analysis Date = 07/03/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/27/14 Pct Recovery = 97% Analysis Date = 06/21/14 Pct Recovery = 97% Analysis Date = 06/21/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/15/14 Pct Recovery = 97% Analysis Date = 06/09/14 Pct Recovery = 96% Analysis Date = 06/09/14 Pct Recovery = 96% Analysis Date = 06/03/14 Pct Recovery = 96% Analysis Date = 06/03/14 Pct Recovery = 96% Analysis Date = 05/28/14 Pct Recovery = 96% Analysis Date = 05/28/14 Pct Recovery = 96% Analysis Date = 05/23/14 Pct Recovery = 95% Analysis Date = 05/23/14 Pct Recovery = 95% Analysis Date = 05/17/14 Pct Recovery = 95% Analysis Date = 05/17/14 Pct Recovery = 95% Analysis Date = 05/11/14 Pct Recovery = 95% Analysis Date = 05/11/14 Pct Recovery = 95% Analysis Date = 05/05/14 Pct Recovery = 95% Analysis Date = 05/05/14 Pct Recovery = 95% Analysis Date = 04/29/14 Pct Recovery = 94% Analysis Date = 04/29/14 Pct Recovery = 94% Analysis Date = 04/23/14 Pct Recovery = 94% Analysis Date = 04/23/14 Pct Recovery = 94% Analysis Date = 04/17/14 Pct Recovery = 94% Analysis Date = 04/17/14 Pct Recovery = 94% Analysis Date = 04/11/14 Pct Recovery = 93% Analysis Date = 04/11/14 Pct Recovery = 93% Analysis Date = 04/06/14 Pct Recovery = 93% Analysis Date = 04/06/14 Pct Recovery = 93% Analysis Date = 03/31/14 Pct Recovery = 93% Analysis Date = 03/31/14 Pct Recovery = 93% Analysis Date = 03/25/14 Pct Recovery = 93% Analysis Date = 03/25/14 Pct Recovery = 93% Analysis Date = 03/19/14 Pct Recovery = 92% Analysis Date = 03/19/14 Pct Recovery = 92% Analysis Date = 03/13/14 Pct Recovery = 92% Analysis Date = 03/13/14 Pct Recovery = 92% Analysis Date = 03/07/14 Pct Recovery = 92% Analysis Date = 03/07/14 Pct Recovery = 92% Analysis Date = 03/01/14 Pct Recovery = 91% Analysis Date = 03/01/14 Pct Recovery = 91% Analysis Date = 02/23/14 Pct Recovery = 91% Analysis Date = 02/23/14 Pct Recovery = 91% Analysis Date = 02/18/14 Pct Recovery = 91% Analysis Date = 02/18/14 Pct Recovery = 91% Analysis Date = 02/12/14 Pct Recovery = 91% Analysis Date = 02/12/14 Pct Recovery = 91% Analysis Date = 02/06/14 Pct Recovery = 90% Analysis Date = 02/06/14 Pct Recovery = 90% Analysis Date = 01/31/14 Pct Recovery = 90% Analysis Date = 01/31/14 Pct Recovery = 90% Analysis Date = 01/25/14 Pct Recovery = 90% Analysis Date = 01/25/14 Pct Recovery = 90% Analysis Date = 01/19/14 Pct Recovery = 89% Analysis Date = 01/19/14 Pct Recovery = 89% Analysis Date = 01/13/14 Pct Recovery = 89% Analysis Date = 01/13/14 Pct Recovery = 89% Analysis Date = 01/07/14 Pct Recovery = 89% Analysis Date = 01/07/14 Pct Recovery = 89% Analysis Date = 01/01/14 Pct Recovery = 88% Analysis Date = 01/01/14 Pct Recovery = 88% Analysis Date = 12/27/13 Pct Recovery = 88% Analysis Date = 12/27/13 Pct Recovery = 88% Analysis Date = 12/21/13 Pct Recovery = 88% Analysis Date = 12/21/13 Pct Recovery = 88% Analysis Date = 12/15/13 Pct Recovery = 87% Analysis Date = 12/15/13 Pct Recovery = 87% Analysis Date = 12/09/13 Pct Recovery = 87% Analysis Date = 12/09/13 Pct Recovery = 87% Analysis Date = 12/03/13 Pct Recovery = 87% Analysis Date = 12/03/13 Pct Recovery = 87% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/27/13 Pct Recovery = 86% Analysis Date = 11/21/13 Pct Recovery = 86% Analysis Date = 11/21/13 Pct Recovery = 86% Analysis Date = 11/15/13 Pct Recovery = 85% Analysis Date = 11/15/13 Pct Recovery = 85% Analysis Date = 11/10/13 Pct Recovery = 85% Analysis Date = 11/10/13 Pct Recovery = 85% Analysis Date = 11/04/13 Pct Recovery = 85% Analysis Date = 11/04/13 Pct Recovery = 85% Analysis Date = 10/29/13 Pct Recovery = 84% Analysis Date = 10/29/13 Pct Recovery = 84% Analysis Date = 10/23/13 Pct Recovery = 84% Analysis Date = 10/23/13 Pct Recovery = 84% Analysis Date = 10/17/13 Pct Recovery = 84% Analysis Date = 10/17/13 Pct Recovery = 84% Analysis Date = 10/11/13 Pct Recovery = 83% Analysis Date = 10/11/13 Pct Recovery = 83% Analysis Date = 10/05/13 Pct Recovery = 83% Analysis Date = 10/05/13 Pct Recovery = 83% Analysis Date = 09/29/13 Pct Recovery = 82% Analysis Date = 09/29/13 Pct Recovery = 82% Analysis Date = 09/24/13 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 108 100% 27% 98% 23%
Total 108 100% 27% 98% 23%

Sample Statistics
FIPRONIL SULFONE

Characteristic N % % Basis
Plotted 108 97% Spiked
Estimated Values 24 22% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 111 .  
False Negatives 3 3% 3 out of 111
Not Spiked 67 .  
False Positives 3 4% 3 out of 67