BQS OBSP Determination:
DISULFOTON OXON SULFOXIDE
METHOD: 2437 , TESTIDCODE: 68587LCM60
Open Data Set

Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 318% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 276% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 283% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 224% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 67% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 69% Analysis Date = 01/06/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 71% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 57% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 67% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 71% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 69% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 73% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 67% Analysis Date = 04/20/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 83% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 54% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 65% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 58% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 43% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 42% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 41% Analysis Date = 07/22/15 SpikeMix = ERA 0406-15-04: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 58% Analysis Date = 07/18/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 61% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 104% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 103% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 81% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 67% Analysis Date = 02/24/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 90% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 77% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 67% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 96% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 55% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 48% Analysis Date = 11/12/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 65% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 72% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 66% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 61% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 61% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 77% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 73% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 89% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 80% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 83% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 145% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 147% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 123% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 137% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 155% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 163% Analysis Date = 12/02/16 Pct Recovery = 205% Analysis Date = 11/30/16 Pct Recovery = 203% Analysis Date = 11/30/16 Pct Recovery = 203% Analysis Date = 11/27/16 Pct Recovery = 202% Analysis Date = 11/27/16 Pct Recovery = 202% Analysis Date = 11/24/16 Pct Recovery = 201% Analysis Date = 11/24/16 Pct Recovery = 201% Analysis Date = 11/22/16 Pct Recovery = 199% Analysis Date = 11/22/16 Pct Recovery = 199% Analysis Date = 11/19/16 Pct Recovery = 198% Analysis Date = 11/19/16 Pct Recovery = 198% Analysis Date = 11/16/16 Pct Recovery = 197% Analysis Date = 11/16/16 Pct Recovery = 197% Analysis Date = 11/14/16 Pct Recovery = 195% Analysis Date = 11/14/16 Pct Recovery = 195% Analysis Date = 11/11/16 Pct Recovery = 194% Analysis Date = 11/11/16 Pct Recovery = 194% Analysis Date = 11/08/16 Pct Recovery = 192% Analysis Date = 11/08/16 Pct Recovery = 192% Analysis Date = 11/06/16 Pct Recovery = 191% Analysis Date = 11/06/16 Pct Recovery = 191% Analysis Date = 11/03/16 Pct Recovery = 190% Analysis Date = 11/03/16 Pct Recovery = 190% Analysis Date = 10/31/16 Pct Recovery = 188% Analysis Date = 10/31/16 Pct Recovery = 188% Analysis Date = 10/29/16 Pct Recovery = 187% Analysis Date = 10/29/16 Pct Recovery = 187% Analysis Date = 10/26/16 Pct Recovery = 186% Analysis Date = 10/26/16 Pct Recovery = 186% Analysis Date = 10/23/16 Pct Recovery = 184% Analysis Date = 10/23/16 Pct Recovery = 184% Analysis Date = 10/20/16 Pct Recovery = 183% Analysis Date = 10/20/16 Pct Recovery = 183% Analysis Date = 10/18/16 Pct Recovery = 181% Analysis Date = 10/18/16 Pct Recovery = 181% Analysis Date = 10/15/16 Pct Recovery = 180% Analysis Date = 10/15/16 Pct Recovery = 180% Analysis Date = 10/12/16 Pct Recovery = 179% Analysis Date = 10/12/16 Pct Recovery = 179% Analysis Date = 10/10/16 Pct Recovery = 177% Analysis Date = 10/10/16 Pct Recovery = 177% Analysis Date = 10/07/16 Pct Recovery = 176% Analysis Date = 10/07/16 Pct Recovery = 176% Analysis Date = 10/04/16 Pct Recovery = 174% Analysis Date = 10/04/16 Pct Recovery = 174% Analysis Date = 10/02/16 Pct Recovery = 173% Analysis Date = 10/02/16 Pct Recovery = 173% Analysis Date = 09/29/16 Pct Recovery = 172% Analysis Date = 09/29/16 Pct Recovery = 172% Analysis Date = 09/26/16 Pct Recovery = 170% Analysis Date = 09/26/16 Pct Recovery = 170% Analysis Date = 09/24/16 Pct Recovery = 169% Analysis Date = 09/24/16 Pct Recovery = 169% Analysis Date = 09/21/16 Pct Recovery = 168% Analysis Date = 09/21/16 Pct Recovery = 168% Analysis Date = 09/18/16 Pct Recovery = 166% Analysis Date = 09/18/16 Pct Recovery = 166% Analysis Date = 09/16/16 Pct Recovery = 165% Analysis Date = 09/16/16 Pct Recovery = 165% Analysis Date = 09/13/16 Pct Recovery = 163% Analysis Date = 09/13/16 Pct Recovery = 163% Analysis Date = 09/10/16 Pct Recovery = 162% Analysis Date = 09/10/16 Pct Recovery = 162% Analysis Date = 09/08/16 Pct Recovery = 161% Analysis Date = 09/08/16 Pct Recovery = 161% Analysis Date = 09/05/16 Pct Recovery = 159% Analysis Date = 09/05/16 Pct Recovery = 159% Analysis Date = 09/02/16 Pct Recovery = 158% Analysis Date = 09/02/16 Pct Recovery = 158% Analysis Date = 08/31/16 Pct Recovery = 157% Analysis Date = 08/31/16 Pct Recovery = 157% Analysis Date = 08/28/16 Pct Recovery = 155% Analysis Date = 08/28/16 Pct Recovery = 155% Analysis Date = 08/25/16 Pct Recovery = 154% Analysis Date = 08/25/16 Pct Recovery = 154% Analysis Date = 08/23/16 Pct Recovery = 153% Analysis Date = 08/23/16 Pct Recovery = 153% Analysis Date = 08/20/16 Pct Recovery = 151% Analysis Date = 08/20/16 Pct Recovery = 151% Analysis Date = 08/17/16 Pct Recovery = 150% Analysis Date = 08/17/16 Pct Recovery = 150% Analysis Date = 08/14/16 Pct Recovery = 149% Analysis Date = 08/14/16 Pct Recovery = 149% Analysis Date = 08/12/16 Pct Recovery = 147% Analysis Date = 08/12/16 Pct Recovery = 147% Analysis Date = 08/09/16 Pct Recovery = 146% Analysis Date = 08/09/16 Pct Recovery = 146% Analysis Date = 08/06/16 Pct Recovery = 145% Analysis Date = 08/06/16 Pct Recovery = 145% Analysis Date = 08/04/16 Pct Recovery = 143% Analysis Date = 08/04/16 Pct Recovery = 143% Analysis Date = 08/01/16 Pct Recovery = 142% Analysis Date = 08/01/16 Pct Recovery = 142% Analysis Date = 07/29/16 Pct Recovery = 141% Analysis Date = 07/29/16 Pct Recovery = 141% Analysis Date = 07/27/16 Pct Recovery = 140% Analysis Date = 07/27/16 Pct Recovery = 140% Analysis Date = 07/24/16 Pct Recovery = 139% Analysis Date = 07/24/16 Pct Recovery = 139% Analysis Date = 07/21/16 Pct Recovery = 138% Analysis Date = 07/21/16 Pct Recovery = 138% Analysis Date = 07/19/16 Pct Recovery = 137% Analysis Date = 07/19/16 Pct Recovery = 137% Analysis Date = 07/16/16 Pct Recovery = 136% Analysis Date = 07/16/16 Pct Recovery = 136% Analysis Date = 07/13/16 Pct Recovery = 135% Analysis Date = 07/13/16 Pct Recovery = 135% Analysis Date = 07/11/16 Pct Recovery = 133% Analysis Date = 07/11/16 Pct Recovery = 133% Analysis Date = 07/08/16 Pct Recovery = 132% Analysis Date = 07/08/16 Pct Recovery = 132% Analysis Date = 07/05/16 Pct Recovery = 131% Analysis Date = 07/05/16 Pct Recovery = 131% Analysis Date = 07/03/16 Pct Recovery = 130% Analysis Date = 07/03/16 Pct Recovery = 130% Analysis Date = 06/30/16 Pct Recovery = 129% Analysis Date = 06/30/16 Pct Recovery = 129% Analysis Date = 06/27/16 Pct Recovery = 128% Analysis Date = 06/27/16 Pct Recovery = 128% Analysis Date = 06/25/16 Pct Recovery = 127% Analysis Date = 06/25/16 Pct Recovery = 127% Analysis Date = 06/22/16 Pct Recovery = 125% Analysis Date = 06/22/16 Pct Recovery = 125% Analysis Date = 06/19/16 Pct Recovery = 124% Analysis Date = 06/19/16 Pct Recovery = 124% Analysis Date = 06/17/16 Pct Recovery = 123% Analysis Date = 06/17/16 Pct Recovery = 123% Analysis Date = 06/14/16 Pct Recovery = 122% Analysis Date = 06/14/16 Pct Recovery = 122% Analysis Date = 06/11/16 Pct Recovery = 120% Analysis Date = 06/11/16 Pct Recovery = 120% Analysis Date = 06/08/16 Pct Recovery = 119% Analysis Date = 06/08/16 Pct Recovery = 119% Analysis Date = 06/06/16 Pct Recovery = 118% Analysis Date = 06/06/16 Pct Recovery = 118% Analysis Date = 06/03/16 Pct Recovery = 117% Analysis Date = 06/03/16 Pct Recovery = 117% Analysis Date = 05/31/16 Pct Recovery = 115% Analysis Date = 05/31/16 Pct Recovery = 115% Analysis Date = 05/29/16 Pct Recovery = 114% Analysis Date = 05/29/16 Pct Recovery = 114% Analysis Date = 05/26/16 Pct Recovery = 113% Analysis Date = 05/26/16 Pct Recovery = 113% Analysis Date = 05/23/16 Pct Recovery = 112% Analysis Date = 05/23/16 Pct Recovery = 112% Analysis Date = 05/21/16 Pct Recovery = 110% Analysis Date = 05/21/16 Pct Recovery = 110% Analysis Date = 05/18/16 Pct Recovery = 109% Analysis Date = 05/18/16 Pct Recovery = 109% Analysis Date = 05/15/16 Pct Recovery = 108% Analysis Date = 05/15/16 Pct Recovery = 108% Analysis Date = 05/13/16 Pct Recovery = 107% Analysis Date = 05/13/16 Pct Recovery = 107% Analysis Date = 05/10/16 Pct Recovery = 105% Analysis Date = 05/10/16 Pct Recovery = 105% Analysis Date = 05/07/16 Pct Recovery = 104% Analysis Date = 05/07/16 Pct Recovery = 104% Analysis Date = 05/05/16 Pct Recovery = 103% Analysis Date = 05/05/16 Pct Recovery = 103% Analysis Date = 05/02/16 Pct Recovery = 102% Analysis Date = 05/02/16 Pct Recovery = 102% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/29/16 Pct Recovery = 100% Analysis Date = 04/27/16 Pct Recovery = 99% Analysis Date = 04/27/16 Pct Recovery = 99% Analysis Date = 04/24/16 Pct Recovery = 98% Analysis Date = 04/24/16 Pct Recovery = 98% Analysis Date = 04/21/16 Pct Recovery = 97% Analysis Date = 04/21/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 95% Analysis Date = 04/19/16 Pct Recovery = 95% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/16/16 Pct Recovery = 94% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/11/16 Pct Recovery = 92% Analysis Date = 04/11/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 91% Analysis Date = 04/08/16 Pct Recovery = 91% Analysis Date = 04/05/16 Pct Recovery = 90% Analysis Date = 04/05/16 Pct Recovery = 90% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 88% Analysis Date = 03/31/16 Pct Recovery = 88% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/20/16 Pct Recovery = 83% Analysis Date = 03/20/16 Pct Recovery = 83% Analysis Date = 03/17/16 Pct Recovery = 82% Analysis Date = 03/17/16 Pct Recovery = 82% Analysis Date = 03/15/16 Pct Recovery = 81% Analysis Date = 03/15/16 Pct Recovery = 81% Analysis Date = 03/12/16 Pct Recovery = 80% Analysis Date = 03/12/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 79% Analysis Date = 03/09/16 Pct Recovery = 79% Analysis Date = 03/07/16 Pct Recovery = 78% Analysis Date = 03/07/16 Pct Recovery = 78% Analysis Date = 03/04/16 Pct Recovery = 77% Analysis Date = 03/04/16 Pct Recovery = 77% Analysis Date = 03/01/16 Pct Recovery = 76% Analysis Date = 03/01/16 Pct Recovery = 76% Analysis Date = 02/28/16 Pct Recovery = 74% Analysis Date = 02/28/16 Pct Recovery = 74% Analysis Date = 02/25/16 Pct Recovery = 73% Analysis Date = 02/25/16 Pct Recovery = 73% Analysis Date = 02/22/16 Pct Recovery = 73% Analysis Date = 02/22/16 Pct Recovery = 73% Analysis Date = 02/20/16 Pct Recovery = 72% Analysis Date = 02/20/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/17/16 Pct Recovery = 72% Analysis Date = 02/14/16 Pct Recovery = 72% Analysis Date = 02/14/16 Pct Recovery = 72% Analysis Date = 02/12/16 Pct Recovery = 72% Analysis Date = 02/12/16 Pct Recovery = 72% Analysis Date = 02/09/16 Pct Recovery = 72% Analysis Date = 02/09/16 Pct Recovery = 72% Analysis Date = 02/06/16 Pct Recovery = 71% Analysis Date = 02/06/16 Pct Recovery = 71% Analysis Date = 02/04/16 Pct Recovery = 71% Analysis Date = 02/04/16 Pct Recovery = 71% Analysis Date = 02/01/16 Pct Recovery = 71% Analysis Date = 02/01/16 Pct Recovery = 71% Analysis Date = 01/29/16 Pct Recovery = 71% Analysis Date = 01/29/16 Pct Recovery = 71% Analysis Date = 01/26/16 Pct Recovery = 70% Analysis Date = 01/26/16 Pct Recovery = 70% Analysis Date = 01/24/16 Pct Recovery = 70% Analysis Date = 01/24/16 Pct Recovery = 70% Analysis Date = 01/21/16 Pct Recovery = 70% Analysis Date = 01/21/16 Pct Recovery = 70% Analysis Date = 01/18/16 Pct Recovery = 70% Analysis Date = 01/18/16 Pct Recovery = 70% Analysis Date = 01/16/16 Pct Recovery = 70% Analysis Date = 01/16/16 Pct Recovery = 70% Analysis Date = 01/13/16 Pct Recovery = 69% Analysis Date = 01/13/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 01/10/16 Pct Recovery = 69% Analysis Date = 01/08/16 Pct Recovery = 69% Analysis Date = 01/08/16 Pct Recovery = 69% Analysis Date = 01/05/16 Pct Recovery = 69% Analysis Date = 01/05/16 Pct Recovery = 69% Analysis Date = 01/02/16 Pct Recovery = 69% Analysis Date = 01/02/16 Pct Recovery = 69% Analysis Date = 12/31/15 Pct Recovery = 68% Analysis Date = 12/31/15 Pct Recovery = 68% Analysis Date = 12/28/15 Pct Recovery = 68% Analysis Date = 12/28/15 Pct Recovery = 68% Analysis Date = 12/25/15 Pct Recovery = 68% Analysis Date = 12/25/15 Pct Recovery = 68% Analysis Date = 12/23/15 Pct Recovery = 68% Analysis Date = 12/23/15 Pct Recovery = 68% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/20/15 Pct Recovery = 67% Analysis Date = 12/17/15 Pct Recovery = 67% Analysis Date = 12/17/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 67% Analysis Date = 12/15/15 Pct Recovery = 67% Analysis Date = 12/12/15 Pct Recovery = 67% Analysis Date = 12/12/15 Pct Recovery = 67% Analysis Date = 12/09/15 Pct Recovery = 66% Analysis Date = 12/09/15 Pct Recovery = 66% Analysis Date = 12/07/15 Pct Recovery = 66% Analysis Date = 12/07/15 Pct Recovery = 66% Analysis Date = 12/04/15 Pct Recovery = 66% Analysis Date = 12/04/15 Pct Recovery = 66% Analysis Date = 12/01/15 Pct Recovery = 66% Analysis Date = 12/01/15 Pct Recovery = 66% Analysis Date = 11/29/15 Pct Recovery = 66% Analysis Date = 11/29/15 Pct Recovery = 66% Analysis Date = 11/26/15 Pct Recovery = 65% Analysis Date = 11/26/15 Pct Recovery = 65% Analysis Date = 11/23/15 Pct Recovery = 65% Analysis Date = 11/23/15 Pct Recovery = 65% Analysis Date = 11/20/15 Pct Recovery = 65% Analysis Date = 11/20/15 Pct Recovery = 65% Analysis Date = 11/18/15 Pct Recovery = 65% Analysis Date = 11/18/15 Pct Recovery = 65% Analysis Date = 11/15/15 Pct Recovery = 64% Analysis Date = 11/15/15 Pct Recovery = 64% Analysis Date = 11/12/15 Pct Recovery = 64% Analysis Date = 11/12/15 Pct Recovery = 64% Analysis Date = 11/10/15 Pct Recovery = 64% Analysis Date = 11/10/15 Pct Recovery = 64% Analysis Date = 11/07/15 Pct Recovery = 64% Analysis Date = 11/07/15 Pct Recovery = 64% Analysis Date = 11/04/15 Pct Recovery = 64% Analysis Date = 11/04/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 11/02/15 Pct Recovery = 64% Analysis Date = 10/30/15 Pct Recovery = 63% Analysis Date = 10/30/15 Pct Recovery = 63% Analysis Date = 10/27/15 Pct Recovery = 63% Analysis Date = 10/27/15 Pct Recovery = 63% Analysis Date = 10/25/15 Pct Recovery = 63% Analysis Date = 10/25/15 Pct Recovery = 63% Analysis Date = 10/22/15 Pct Recovery = 63% Analysis Date = 10/22/15 Pct Recovery = 63% Analysis Date = 10/19/15 Pct Recovery = 63% Analysis Date = 10/19/15 Pct Recovery = 63% Analysis Date = 10/17/15 Pct Recovery = 63% Analysis Date = 10/17/15 Pct Recovery = 63% Analysis Date = 10/14/15 Pct Recovery = 63% Analysis Date = 10/14/15 Pct Recovery = 63% Analysis Date = 10/11/15 Pct Recovery = 63% Analysis Date = 10/11/15 Pct Recovery = 63% Analysis Date = 10/09/15 Pct Recovery = 63% Analysis Date = 10/09/15 Pct Recovery = 63% Analysis Date = 10/06/15 Pct Recovery = 64% Analysis Date = 10/06/15 Pct Recovery = 64% Analysis Date = 10/03/15 Pct Recovery = 64% Analysis Date = 10/03/15 Pct Recovery = 64% Analysis Date = 10/01/15 Pct Recovery = 64% Analysis Date = 10/01/15 Pct Recovery = 64% Analysis Date = 09/28/15 Pct Recovery = 64% Analysis Date = 09/28/15 Pct Recovery = 64% Analysis Date = 09/25/15 Pct Recovery = 64% Analysis Date = 09/25/15 Pct Recovery = 64% Analysis Date = 09/23/15 Pct Recovery = 64% Analysis Date = 09/23/15 Pct Recovery = 64% Analysis Date = 09/20/15 Pct Recovery = 64% Analysis Date = 09/20/15 Pct Recovery = 64% Analysis Date = 09/17/15 Pct Recovery = 64% Analysis Date = 09/17/15 Pct Recovery = 64% Analysis Date = 09/14/15 Pct Recovery = 64% Analysis Date = 09/14/15 Pct Recovery = 64% Analysis Date = 09/12/15 Pct Recovery = 64% Analysis Date = 09/12/15 Pct Recovery = 64% Analysis Date = 09/09/15 Pct Recovery = 64% Analysis Date = 09/09/15 Pct Recovery = 64% Analysis Date = 09/06/15 Pct Recovery = 65% Analysis Date = 09/06/15 Pct Recovery = 65% Analysis Date = 09/04/15 Pct Recovery = 65% Analysis Date = 09/04/15 Pct Recovery = 65% Analysis Date = 09/01/15 Pct Recovery = 65% Analysis Date = 09/01/15 Pct Recovery = 65% Analysis Date = 08/29/15 Pct Recovery = 65% Analysis Date = 08/29/15 Pct Recovery = 65% Analysis Date = 08/27/15 Pct Recovery = 65% Analysis Date = 08/27/15 Pct Recovery = 65% Analysis Date = 08/24/15 Pct Recovery = 65% Analysis Date = 08/24/15 Pct Recovery = 65% Analysis Date = 08/21/15 Pct Recovery = 65% Analysis Date = 08/21/15 Pct Recovery = 65% Analysis Date = 08/19/15 Pct Recovery = 65% Analysis Date = 08/19/15 Pct Recovery = 65% Analysis Date = 08/16/15 Pct Recovery = 65% Analysis Date = 08/16/15 Pct Recovery = 65% Analysis Date = 08/13/15 Pct Recovery = 65% Analysis Date = 08/13/15 Pct Recovery = 65% Analysis Date = 08/11/15 Pct Recovery = 65% Analysis Date = 08/11/15 Pct Recovery = 65% Analysis Date = 08/08/15 Pct Recovery = 65% Analysis Date = 08/08/15 Pct Recovery = 65% Analysis Date = 08/05/15 Pct Recovery = 65% Analysis Date = 08/05/15 Pct Recovery = 65% Analysis Date = 08/03/15 Pct Recovery = 66% Analysis Date = 08/03/15 Pct Recovery = 66% Analysis Date = 07/31/15 Pct Recovery = 66% Analysis Date = 07/31/15 Pct Recovery = 66% Analysis Date = 07/28/15 Pct Recovery = 66% Analysis Date = 07/28/15 Pct Recovery = 66% Analysis Date = 07/26/15 Pct Recovery = 66% Analysis Date = 07/26/15 Pct Recovery = 66% Analysis Date = 07/23/15 Pct Recovery = 66% Analysis Date = 07/23/15 Pct Recovery = 66% Analysis Date = 07/20/15 Pct Recovery = 66% Analysis Date = 07/20/15 Pct Recovery = 66% Analysis Date = 07/18/15 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON OXON SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 48 96% 63% 72% 27%
Total 48 96% 63% 72% 27%

Sample Statistics
DISULFOTON OXON SULFOXIDE

Characteristic N % % Basis
Plotted 48 100% Spiked
Estimated Values 1 2% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 48 .  
False Negatives 0 0% 0 out of 48
Not Spiked 130 .  
False Positives 24 19% 24 out of 127