BQS OBSP Determination:
DACTHAL MONOACID
METHOD: 2437 , TESTIDCODE: 68560LCM60
Open Data Set

Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 203% Analysis Date = 04/07/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 258% Analysis Date = 10/15/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 117% Analysis Date = 10/15/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 128% Analysis Date = 10/15/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 121% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 92% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 93% Analysis Date = 01/19/16 SpikeMix = ERA 0406-15-04: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 90% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 108% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 106% Analysis Date = 12/08/15 SpikeMix = ChemService 4047000: 80 µl & ChemService 3880000: 80 µl & ERA 0406-15-05: 80 µl Pct Recovery = 102% Analysis Date = 06/10/14 SpikeMix = ChemService 2598800: 60 µl & ChemService 2609400: 60 µl Pct Recovery = 97% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 184% Analysis Date = 09/29/16 SpikeMix = ChemService 5154100: 100 µl & Abs 072516: 100 µl Pct Recovery = 190% Analysis Date = 12/03/14 SpikeMix = ChemService 2609400: 30 µl & Abs 042914: 30 µl Pct Recovery = 99% Analysis Date = 11/18/14 SpikeMix = Abs 042814Pest3: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 107% Analysis Date = 09/03/14 SpikeMix = ChemService 2609400: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 92% Analysis Date = 06/25/14 SpikeMix = ChemService 2598800: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 49% Analysis Date = 02/11/15 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 184% Analysis Date = 12/30/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 169% Analysis Date = 12/16/14 SpikeMix = ChemService 2598800: 30 µl & Abs 042314: 30 µl Pct Recovery = 149% Analysis Date = 07/08/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 28% Analysis Date = 08/25/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 173% Analysis Date = 08/25/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 130% Analysis Date = 08/25/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 177% Analysis Date = 08/20/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 79% Analysis Date = 08/18/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 95% Analysis Date = 08/18/15 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ChemService 3995200: 2 Pct Recovery = 115% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 203% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 103% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 139% Analysis Date = 07/17/15 SpikeMix = ChemService 3880100: 20 µl & ChemService 3995200: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 111% Analysis Date = 07/14/15 SpikeMix = ChemService 3880000: 20 µl & ChemService 3995200: 20 µl & ChemService 3880100: 2 Pct Recovery = 139% Analysis Date = 12/09/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 100% Analysis Date = 12/09/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 106% Analysis Date = 12/09/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 106% Analysis Date = 10/28/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 141% Analysis Date = 10/28/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 126% Analysis Date = 10/28/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 126% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 108% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 98% Analysis Date = 09/10/15 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 89% Analysis Date = 10/07/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 92% Analysis Date = 09/23/14 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 82% Analysis Date = 07/24/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 107% Analysis Date = 05/21/14 SpikeMix = ChemService 2598800: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 82% Analysis Date = 03/11/15 SpikeMix = Abs 042314: 15 µl & Abs 042914: 15 µl Pct Recovery = 148% Analysis Date = 08/19/14 SpikeMix = Abs 042814Pest3: 15 µl & Abs 042314: 15 µl Pct Recovery = 50% Analysis Date = 08/11/14 SpikeMix = Abs 042314: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 193% Analysis Date = 11/23/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 123% Analysis Date = 11/23/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 114% Analysis Date = 11/23/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 122% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 105% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 128% Analysis Date = 10/21/15 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 108% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 121% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 115% Analysis Date = 11/11/15 SpikeMix = ERA 0406-15-04: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 114% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 123% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 112% Analysis Date = 10/15/15 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ERA 0406-15-05: 10 µl Pct Recovery = 152% Analysis Date = 08/03/15 SpikeMix = ERA 0406-15-05: 10 µl & ChemService 4047100: 10 µl & ChemService 3880200: 10 µl Pct Recovery = 91% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 135% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 144% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 122% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 107% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 100% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-04: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 104% Analysis Date = 05/05/16 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 115% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 87% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 94% Analysis Date = 03/16/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 96% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 75% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 93% Analysis Date = 03/09/16 SpikeMix = ChemService 4047000: 20 µl & ChemService 3880000: 20 µl & ERA 0406-15-05: 20 µl Pct Recovery = 96% Analysis Date = 01/05/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 122% Analysis Date = 01/04/17 SpikeMix = Abs 072516: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 130% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 87% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 103% Analysis Date = 02/20/16 SpikeMix = ERA 0406-15-04: 10 µl & ChemService 3995200: 10 µl & ChemService 3880100: 10 µl Pct Recovery = 105% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 86% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 89% Analysis Date = 02/02/16 SpikeMix = ChemService 4047000: 10 µl & ChemService 3880000: 10 µl & ChemService 3995200: 1 Pct Recovery = 88% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 84% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 94% Analysis Date = 01/27/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 102% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 107% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 98% Analysis Date = 03/04/14 SpikeMix = Spex Organics T1130601011: 2 µl & Supelco LC01386: 2 µl & ChemService 1448600: 2 Pct Recovery = 96% Analysis Date = 02/05/14 SpikeMix = NSI 042213HPLC: 2 µl & ChemService 1448600: 2 µl & Spex Organics T1130601011: 2 Pct Recovery = 59% Analysis Date = 01/05/17 Pct Recovery = 157% Analysis Date = 12/30/16 Pct Recovery = 156% Analysis Date = 12/30/16 Pct Recovery = 156% Analysis Date = 12/25/16 Pct Recovery = 155% Analysis Date = 12/25/16 Pct Recovery = 155% Analysis Date = 12/20/16 Pct Recovery = 154% Analysis Date = 12/20/16 Pct Recovery = 154% Analysis Date = 12/14/16 Pct Recovery = 154% Analysis Date = 12/14/16 Pct Recovery = 154% Analysis Date = 12/09/16 Pct Recovery = 153% Analysis Date = 12/09/16 Pct Recovery = 153% Analysis Date = 12/04/16 Pct Recovery = 152% Analysis Date = 12/04/16 Pct Recovery = 152% Analysis Date = 11/28/16 Pct Recovery = 151% Analysis Date = 11/28/16 Pct Recovery = 151% Analysis Date = 11/23/16 Pct Recovery = 150% Analysis Date = 11/23/16 Pct Recovery = 150% Analysis Date = 11/18/16 Pct Recovery = 149% Analysis Date = 11/18/16 Pct Recovery = 149% Analysis Date = 11/12/16 Pct Recovery = 148% Analysis Date = 11/12/16 Pct Recovery = 148% Analysis Date = 11/07/16 Pct Recovery = 147% Analysis Date = 11/07/16 Pct Recovery = 147% Analysis Date = 11/02/16 Pct Recovery = 146% Analysis Date = 11/02/16 Pct Recovery = 146% Analysis Date = 10/27/16 Pct Recovery = 145% Analysis Date = 10/27/16 Pct Recovery = 145% Analysis Date = 10/22/16 Pct Recovery = 145% Analysis Date = 10/22/16 Pct Recovery = 145% Analysis Date = 10/17/16 Pct Recovery = 144% Analysis Date = 10/17/16 Pct Recovery = 144% Analysis Date = 10/11/16 Pct Recovery = 143% Analysis Date = 10/11/16 Pct Recovery = 143% Analysis Date = 10/06/16 Pct Recovery = 142% Analysis Date = 10/06/16 Pct Recovery = 142% Analysis Date = 10/01/16 Pct Recovery = 141% Analysis Date = 10/01/16 Pct Recovery = 141% Analysis Date = 09/25/16 Pct Recovery = 140% Analysis Date = 09/25/16 Pct Recovery = 140% Analysis Date = 09/20/16 Pct Recovery = 139% Analysis Date = 09/20/16 Pct Recovery = 139% Analysis Date = 09/15/16 Pct Recovery = 138% Analysis Date = 09/15/16 Pct Recovery = 138% Analysis Date = 09/09/16 Pct Recovery = 137% Analysis Date = 09/09/16 Pct Recovery = 137% Analysis Date = 09/04/16 Pct Recovery = 136% Analysis Date = 09/04/16 Pct Recovery = 136% Analysis Date = 08/30/16 Pct Recovery = 135% Analysis Date = 08/30/16 Pct Recovery = 135% Analysis Date = 08/24/16 Pct Recovery = 134% Analysis Date = 08/24/16 Pct Recovery = 134% Analysis Date = 08/19/16 Pct Recovery = 132% Analysis Date = 08/19/16 Pct Recovery = 132% Analysis Date = 08/14/16 Pct Recovery = 131% Analysis Date = 08/14/16 Pct Recovery = 131% Analysis Date = 08/08/16 Pct Recovery = 130% Analysis Date = 08/08/16 Pct Recovery = 130% Analysis Date = 08/03/16 Pct Recovery = 129% Analysis Date = 08/03/16 Pct Recovery = 129% Analysis Date = 07/29/16 Pct Recovery = 128% Analysis Date = 07/29/16 Pct Recovery = 128% Analysis Date = 07/23/16 Pct Recovery = 127% Analysis Date = 07/23/16 Pct Recovery = 127% Analysis Date = 07/18/16 Pct Recovery = 125% Analysis Date = 07/18/16 Pct Recovery = 125% Analysis Date = 07/13/16 Pct Recovery = 124% Analysis Date = 07/13/16 Pct Recovery = 124% Analysis Date = 07/07/16 Pct Recovery = 123% Analysis Date = 07/07/16 Pct Recovery = 123% Analysis Date = 07/02/16 Pct Recovery = 122% Analysis Date = 07/02/16 Pct Recovery = 122% Analysis Date = 06/27/16 Pct Recovery = 121% Analysis Date = 06/27/16 Pct Recovery = 121% Analysis Date = 06/21/16 Pct Recovery = 119% Analysis Date = 06/21/16 Pct Recovery = 119% Analysis Date = 06/16/16 Pct Recovery = 118% Analysis Date = 06/16/16 Pct Recovery = 118% Analysis Date = 06/11/16 Pct Recovery = 117% Analysis Date = 06/11/16 Pct Recovery = 117% Analysis Date = 06/06/16 Pct Recovery = 116% Analysis Date = 06/06/16 Pct Recovery = 116% Analysis Date = 05/31/16 Pct Recovery = 115% Analysis Date = 05/31/16 Pct Recovery = 115% Analysis Date = 05/26/16 Pct Recovery = 113% Analysis Date = 05/26/16 Pct Recovery = 113% Analysis Date = 05/21/16 Pct Recovery = 112% Analysis Date = 05/21/16 Pct Recovery = 112% Analysis Date = 05/15/16 Pct Recovery = 111% Analysis Date = 05/15/16 Pct Recovery = 111% Analysis Date = 05/10/16 Pct Recovery = 110% Analysis Date = 05/10/16 Pct Recovery = 110% Analysis Date = 05/05/16 Pct Recovery = 109% Analysis Date = 05/05/16 Pct Recovery = 109% Analysis Date = 04/29/16 Pct Recovery = 107% Analysis Date = 04/29/16 Pct Recovery = 107% Analysis Date = 04/24/16 Pct Recovery = 106% Analysis Date = 04/24/16 Pct Recovery = 106% Analysis Date = 04/19/16 Pct Recovery = 105% Analysis Date = 04/19/16 Pct Recovery = 105% Analysis Date = 04/13/16 Pct Recovery = 104% Analysis Date = 04/13/16 Pct Recovery = 104% Analysis Date = 04/08/16 Pct Recovery = 103% Analysis Date = 04/08/16 Pct Recovery = 103% Analysis Date = 04/03/16 Pct Recovery = 101% Analysis Date = 04/03/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 100% Analysis Date = 03/28/16 Pct Recovery = 100% Analysis Date = 03/23/16 Pct Recovery = 99% Analysis Date = 03/23/16 Pct Recovery = 99% Analysis Date = 03/18/16 Pct Recovery = 98% Analysis Date = 03/18/16 Pct Recovery = 98% Analysis Date = 03/12/16 Pct Recovery = 97% Analysis Date = 03/12/16 Pct Recovery = 97% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 03/07/16 Pct Recovery = 96% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/25/16 Pct Recovery = 97% Analysis Date = 02/25/16 Pct Recovery = 97% Analysis Date = 02/20/16 Pct Recovery = 98% Analysis Date = 02/20/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/09/16 Pct Recovery = 99% Analysis Date = 02/09/16 Pct Recovery = 99% Analysis Date = 02/04/16 Pct Recovery = 100% Analysis Date = 02/04/16 Pct Recovery = 100% Analysis Date = 01/30/16 Pct Recovery = 100% Analysis Date = 01/30/16 Pct Recovery = 100% Analysis Date = 01/24/16 Pct Recovery = 101% Analysis Date = 01/24/16 Pct Recovery = 101% Analysis Date = 01/19/16 Pct Recovery = 102% Analysis Date = 01/19/16 Pct Recovery = 102% Analysis Date = 01/14/16 Pct Recovery = 103% Analysis Date = 01/14/16 Pct Recovery = 103% Analysis Date = 01/08/16 Pct Recovery = 104% Analysis Date = 01/08/16 Pct Recovery = 104% Analysis Date = 01/03/16 Pct Recovery = 105% Analysis Date = 01/03/16 Pct Recovery = 105% Analysis Date = 12/29/15 Pct Recovery = 105% Analysis Date = 12/29/15 Pct Recovery = 105% Analysis Date = 12/23/15 Pct Recovery = 106% Analysis Date = 12/23/15 Pct Recovery = 106% Analysis Date = 12/18/15 Pct Recovery = 107% Analysis Date = 12/18/15 Pct Recovery = 107% Analysis Date = 12/13/15 Pct Recovery = 108% Analysis Date = 12/13/15 Pct Recovery = 108% Analysis Date = 12/07/15 Pct Recovery = 109% Analysis Date = 12/07/15 Pct Recovery = 109% Analysis Date = 12/02/15 Pct Recovery = 110% Analysis Date = 12/02/15 Pct Recovery = 110% Analysis Date = 11/27/15 Pct Recovery = 111% Analysis Date = 11/27/15 Pct Recovery = 111% Analysis Date = 11/21/15 Pct Recovery = 112% Analysis Date = 11/21/15 Pct Recovery = 112% Analysis Date = 11/16/15 Pct Recovery = 113% Analysis Date = 11/16/15 Pct Recovery = 113% Analysis Date = 11/11/15 Pct Recovery = 114% Analysis Date = 11/11/15 Pct Recovery = 114% Analysis Date = 11/06/15 Pct Recovery = 116% Analysis Date = 11/06/15 Pct Recovery = 116% Analysis Date = 10/31/15 Pct Recovery = 117% Analysis Date = 10/31/15 Pct Recovery = 117% Analysis Date = 10/26/15 Pct Recovery = 117% Analysis Date = 10/26/15 Pct Recovery = 117% Analysis Date = 10/21/15 Pct Recovery = 118% Analysis Date = 10/21/15 Pct Recovery = 118% Analysis Date = 10/15/15 Pct Recovery = 119% Analysis Date = 10/15/15 Pct Recovery = 119% Analysis Date = 10/10/15 Pct Recovery = 120% Analysis Date = 10/10/15 Pct Recovery = 120% Analysis Date = 10/05/15 Pct Recovery = 120% Analysis Date = 10/05/15 Pct Recovery = 120% Analysis Date = 09/29/15 Pct Recovery = 121% Analysis Date = 09/29/15 Pct Recovery = 121% Analysis Date = 09/24/15 Pct Recovery = 121% Analysis Date = 09/24/15 Pct Recovery = 121% Analysis Date = 09/19/15 Pct Recovery = 122% Analysis Date = 09/19/15 Pct Recovery = 122% Analysis Date = 09/13/15 Pct Recovery = 123% Analysis Date = 09/13/15 Pct Recovery = 123% Analysis Date = 09/08/15 Pct Recovery = 124% Analysis Date = 09/08/15 Pct Recovery = 124% Analysis Date = 09/03/15 Pct Recovery = 125% Analysis Date = 09/03/15 Pct Recovery = 125% Analysis Date = 08/28/15 Pct Recovery = 126% Analysis Date = 08/28/15 Pct Recovery = 126% Analysis Date = 08/23/15 Pct Recovery = 127% Analysis Date = 08/23/15 Pct Recovery = 127% Analysis Date = 08/18/15 Pct Recovery = 129% Analysis Date = 08/18/15 Pct Recovery = 129% Analysis Date = 08/12/15 Pct Recovery = 130% Analysis Date = 08/12/15 Pct Recovery = 130% Analysis Date = 08/07/15 Pct Recovery = 131% Analysis Date = 08/07/15 Pct Recovery = 131% Analysis Date = 08/02/15 Pct Recovery = 131% Analysis Date = 08/02/15 Pct Recovery = 131% Analysis Date = 07/27/15 Pct Recovery = 131% Analysis Date = 07/27/15 Pct Recovery = 131% Analysis Date = 07/22/15 Pct Recovery = 131% Analysis Date = 07/22/15 Pct Recovery = 131% Analysis Date = 07/17/15 Pct Recovery = 131% Analysis Date = 07/17/15 Pct Recovery = 131% Analysis Date = 07/11/15 Pct Recovery = 132% Analysis Date = 07/11/15 Pct Recovery = 132% Analysis Date = 07/06/15 Pct Recovery = 132% Analysis Date = 07/06/15 Pct Recovery = 132% Analysis Date = 07/01/15 Pct Recovery = 132% Analysis Date = 07/01/15 Pct Recovery = 132% Analysis Date = 06/25/15 Pct Recovery = 132% Analysis Date = 06/25/15 Pct Recovery = 132% Analysis Date = 06/20/15 Pct Recovery = 132% Analysis Date = 06/20/15 Pct Recovery = 132% Analysis Date = 06/15/15 Pct Recovery = 132% Analysis Date = 06/15/15 Pct Recovery = 132% Analysis Date = 06/09/15 Pct Recovery = 133% Analysis Date = 06/09/15 Pct Recovery = 133% Analysis Date = 06/04/15 Pct Recovery = 133% Analysis Date = 06/04/15 Pct Recovery = 133% Analysis Date = 05/30/15 Pct Recovery = 133% Analysis Date = 05/30/15 Pct Recovery = 133% Analysis Date = 05/24/15 Pct Recovery = 133% Analysis Date = 05/24/15 Pct Recovery = 133% Analysis Date = 05/19/15 Pct Recovery = 133% Analysis Date = 05/19/15 Pct Recovery = 133% Analysis Date = 05/14/15 Pct Recovery = 133% Analysis Date = 05/14/15 Pct Recovery = 133% Analysis Date = 05/08/15 Pct Recovery = 134% Analysis Date = 05/08/15 Pct Recovery = 134% Analysis Date = 05/03/15 Pct Recovery = 134% Analysis Date = 05/03/15 Pct Recovery = 134% Analysis Date = 04/28/15 Pct Recovery = 134% Analysis Date = 04/28/15 Pct Recovery = 134% Analysis Date = 04/22/15 Pct Recovery = 134% Analysis Date = 04/22/15 Pct Recovery = 134% Analysis Date = 04/17/15 Pct Recovery = 134% Analysis Date = 04/17/15 Pct Recovery = 134% Analysis Date = 04/12/15 Pct Recovery = 134% Analysis Date = 04/12/15 Pct Recovery = 134% Analysis Date = 04/07/15 Pct Recovery = 135% Analysis Date = 04/07/15 Pct Recovery = 135% Analysis Date = 04/01/15 Pct Recovery = 135% Analysis Date = 04/01/15 Pct Recovery = 135% Analysis Date = 03/27/15 Pct Recovery = 135% Analysis Date = 03/27/15 Pct Recovery = 135% Analysis Date = 03/22/15 Pct Recovery = 135% Analysis Date = 03/22/15 Pct Recovery = 135% Analysis Date = 03/16/15 Pct Recovery = 135% Analysis Date = 03/16/15 Pct Recovery = 135% Analysis Date = 03/11/15 Pct Recovery = 135% Analysis Date = 03/11/15 Pct Recovery = 135% Analysis Date = 03/06/15 Pct Recovery = 135% Analysis Date = 03/06/15 Pct Recovery = 135% Analysis Date = 02/28/15 Pct Recovery = 134% Analysis Date = 02/28/15 Pct Recovery = 134% Analysis Date = 02/23/15 Pct Recovery = 133% Analysis Date = 02/23/15 Pct Recovery = 133% Analysis Date = 02/18/15 Pct Recovery = 132% Analysis Date = 02/18/15 Pct Recovery = 132% Analysis Date = 02/12/15 Pct Recovery = 131% Analysis Date = 02/12/15 Pct Recovery = 131% Analysis Date = 02/07/15 Pct Recovery = 130% Analysis Date = 02/07/15 Pct Recovery = 130% Analysis Date = 02/02/15 Pct Recovery = 129% Analysis Date = 02/02/15 Pct Recovery = 129% Analysis Date = 01/27/15 Pct Recovery = 128% Analysis Date = 01/27/15 Pct Recovery = 128% Analysis Date = 01/22/15 Pct Recovery = 127% Analysis Date = 01/22/15 Pct Recovery = 127% Analysis Date = 01/17/15 Pct Recovery = 126% Analysis Date = 01/17/15 Pct Recovery = 126% Analysis Date = 01/11/15 Pct Recovery = 125% Analysis Date = 01/11/15 Pct Recovery = 125% Analysis Date = 01/06/15 Pct Recovery = 124% Analysis Date = 01/06/15 Pct Recovery = 124% Analysis Date = 01/01/15 Pct Recovery = 123% Analysis Date = 01/01/15 Pct Recovery = 123% Analysis Date = 12/26/14 Pct Recovery = 122% Analysis Date = 12/26/14 Pct Recovery = 122% Analysis Date = 12/21/14 Pct Recovery = 122% Analysis Date = 12/21/14 Pct Recovery = 122% Analysis Date = 12/16/14 Pct Recovery = 121% Analysis Date = 12/16/14 Pct Recovery = 121% Analysis Date = 12/10/14 Pct Recovery = 120% Analysis Date = 12/10/14 Pct Recovery = 120% Analysis Date = 12/05/14 Pct Recovery = 119% Analysis Date = 12/05/14 Pct Recovery = 119% Analysis Date = 11/30/14 Pct Recovery = 118% Analysis Date = 11/30/14 Pct Recovery = 118% Analysis Date = 11/24/14 Pct Recovery = 117% Analysis Date = 11/24/14 Pct Recovery = 117% Analysis Date = 11/19/14 Pct Recovery = 116% Analysis Date = 11/19/14 Pct Recovery = 116% Analysis Date = 11/14/14 Pct Recovery = 115% Analysis Date = 11/14/14 Pct Recovery = 115% Analysis Date = 11/08/14 Pct Recovery = 114% Analysis Date = 11/08/14 Pct Recovery = 114% Analysis Date = 11/03/14 Pct Recovery = 113% Analysis Date = 11/03/14 Pct Recovery = 113% Analysis Date = 10/29/14 Pct Recovery = 112% Analysis Date = 10/29/14 Pct Recovery = 112% Analysis Date = 10/23/14 Pct Recovery = 111% Analysis Date = 10/23/14 Pct Recovery = 111% Analysis Date = 10/18/14 Pct Recovery = 110% Analysis Date = 10/18/14 Pct Recovery = 110% Analysis Date = 10/13/14 Pct Recovery = 109% Analysis Date = 10/13/14 Pct Recovery = 109% Analysis Date = 10/07/14 Pct Recovery = 108% Analysis Date = 10/07/14 Pct Recovery = 108% Analysis Date = 10/02/14 Pct Recovery = 108% Analysis Date = 10/02/14 Pct Recovery = 108% Analysis Date = 09/27/14 Pct Recovery = 107% Analysis Date = 09/27/14 Pct Recovery = 107% Analysis Date = 09/21/14 Pct Recovery = 106% Analysis Date = 09/21/14 Pct Recovery = 106% Analysis Date = 09/16/14 Pct Recovery = 105% Analysis Date = 09/16/14 Pct Recovery = 105% Analysis Date = 09/11/14 Pct Recovery = 104% Analysis Date = 09/11/14 Pct Recovery = 104% Analysis Date = 09/06/14 Pct Recovery = 103% Analysis Date = 09/06/14 Pct Recovery = 103% Analysis Date = 08/31/14 Pct Recovery = 102% Analysis Date = 08/31/14 Pct Recovery = 102% Analysis Date = 08/26/14 Pct Recovery = 101% Analysis Date = 08/26/14 Pct Recovery = 101% Analysis Date = 08/21/14 Pct Recovery = 101% Analysis Date = 08/21/14 Pct Recovery = 101% Analysis Date = 08/15/14 Pct Recovery = 100% Analysis Date = 08/15/14 Pct Recovery = 100% Analysis Date = 08/10/14 Pct Recovery = 99% Analysis Date = 08/10/14 Pct Recovery = 99% Analysis Date = 08/05/14 Pct Recovery = 98% Analysis Date = 08/05/14 Pct Recovery = 98% Analysis Date = 07/30/14 Pct Recovery = 97% Analysis Date = 07/30/14 Pct Recovery = 97% Analysis Date = 07/25/14 Pct Recovery = 96% Analysis Date = 07/25/14 Pct Recovery = 96% Analysis Date = 07/20/14 Pct Recovery = 95% Analysis Date = 07/20/14 Pct Recovery = 95% Analysis Date = 07/14/14 Pct Recovery = 94% Analysis Date = 07/14/14 Pct Recovery = 94% Analysis Date = 07/09/14 Pct Recovery = 93% Analysis Date = 07/09/14 Pct Recovery = 93% Analysis Date = 07/04/14 Pct Recovery = 92% Analysis Date = 07/04/14 Pct Recovery = 92% Analysis Date = 06/28/14 Pct Recovery = 91% Analysis Date = 06/28/14 Pct Recovery = 91% Analysis Date = 06/23/14 Pct Recovery = 90% Analysis Date = 06/23/14 Pct Recovery = 90% Analysis Date = 06/18/14 Pct Recovery = 89% Analysis Date = 06/18/14 Pct Recovery = 89% Analysis Date = 06/12/14 Pct Recovery = 88% Analysis Date = 06/12/14 Pct Recovery = 88% Analysis Date = 06/07/14 Pct Recovery = 87% Analysis Date = 06/07/14 Pct Recovery = 87% Analysis Date = 06/02/14 Pct Recovery = 86% Analysis Date = 06/02/14 Pct Recovery = 86% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/22/14 Pct Recovery = 84% Analysis Date = 05/17/14 Pct Recovery = 83% Analysis Date = 05/17/14 Pct Recovery = 83% Analysis Date = 05/11/14 Pct Recovery = 82% Analysis Date = 05/11/14 Pct Recovery = 82% Analysis Date = 05/06/14 Pct Recovery = 81% Analysis Date = 05/06/14 Pct Recovery = 81% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 05/01/14 Pct Recovery = 80% Analysis Date = 04/25/14 Pct Recovery = 79% Analysis Date = 04/25/14 Pct Recovery = 79% Analysis Date = 04/20/14 Pct Recovery = 78% Analysis Date = 04/20/14 Pct Recovery = 78% Analysis Date = 04/15/14 Pct Recovery = 77% Analysis Date = 04/15/14 Pct Recovery = 77% Analysis Date = 04/09/14 Pct Recovery = 76% Analysis Date = 04/09/14 Pct Recovery = 76% Analysis Date = 04/04/14 Pct Recovery = 75% Analysis Date = 04/04/14 Pct Recovery = 75% Analysis Date = 03/30/14 Pct Recovery = 74% Analysis Date = 03/30/14 Pct Recovery = 74% Analysis Date = 03/24/14 Pct Recovery = 73% Analysis Date = 03/24/14 Pct Recovery = 73% Analysis Date = 03/19/14 Pct Recovery = 72% Analysis Date = 03/19/14 Pct Recovery = 72% Analysis Date = 03/14/14 Pct Recovery = 71% Analysis Date = 03/14/14 Pct Recovery = 71% Analysis Date = 03/08/14 Pct Recovery = 70% Analysis Date = 03/08/14 Pct Recovery = 70% Analysis Date = 03/03/14 Pct Recovery = 69% Analysis Date = 03/03/14 Pct Recovery = 69% Analysis Date = 02/26/14 Pct Recovery = 68% Analysis Date = 02/26/14 Pct Recovery = 68% Analysis Date = 02/20/14 Pct Recovery = 67% Analysis Date = 02/20/14 Pct Recovery = 67% Analysis Date = 02/15/14 Pct Recovery = 66% Analysis Date = 02/15/14 Pct Recovery = 66% Analysis Date = 02/10/14 Pct Recovery = 65% Analysis Date = 02/10/14 Pct Recovery = 65% Analysis Date = 02/05/14 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DACTHAL MONOACID

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 29 100% 18% 96% 13%
>= Reporting Level 61 120% 39% 112% 24%
Total 90 114% 35% 106% 24%

Sample Statistics
DACTHAL MONOACID

Characteristic N % % Basis
Plotted 90 94% Spiked
Estimated Values 90 94% Spiked
Deleted Values 6 3% Spiked + Not Spiked
Spiked, Censored 4 4% Spiked
Spiked 99 .  
False Negatives 2 2% 2 out of 96
Not Spiked 79 .  
False Positives 0 0% 0 out of 76