BQS OBSP Determination:
ASULAM
METHOD: 2437 , TESTIDCODE: 68536LCM60
Open Data Set

Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 96% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 82% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 107% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 76% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 77% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 72% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 90% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 100% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 95% Analysis Date = 06/11/14 SpikeMix = ChemService 2598800: 60 µl & ChemService 2609400: 60 µl Pct Recovery = 107% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 124% Analysis Date = 09/13/16 SpikeMix = Abs 072516: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 110% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 125% Analysis Date = 07/12/16 SpikeMix = Spex Organics TS160603008: 80 µl & Spex Organics TS160511023: 80 µl Pct Recovery = 134% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 81% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 75% Analysis Date = 02/11/15 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 101% Analysis Date = 12/31/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 87% Analysis Date = 12/16/14 SpikeMix = ChemService 2598800: 30 µl & Abs 042314: 30 µl Pct Recovery = 146% Analysis Date = 11/04/14 SpikeMix = Abs 042314: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 110% Analysis Date = 10/21/14 SpikeMix = Abs 042814Pest3: 30 µl & Abs 042314: 30 µl Pct Recovery = 135% Analysis Date = 07/08/14 SpikeMix = Abs 042314: 30 µl & Abs 042914: 30 µl Pct Recovery = 88% Analysis Date = 12/02/14 SpikeMix = ChemService 2609400: 30 µl & Abs 042914: 30 µl Pct Recovery = 99% Analysis Date = 11/18/14 SpikeMix = Abs 042814Pest3: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 99% Analysis Date = 09/04/14 SpikeMix = ChemService 2609400: 30 µl & ERA 0321-14-07: 30 µl Pct Recovery = 73% Analysis Date = 06/26/14 SpikeMix = ChemService 2598800: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 160% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 134% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 100% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 116% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 124% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 109% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 111% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 116% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 119% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 101% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 96% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 81% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 199% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 166% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 109% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 105% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 109% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 153% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 98% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 89% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 86% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 81% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 68% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 113% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 110% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 106% Analysis Date = 07/22/15 SpikeMix = ERA 0406-15-04: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 93% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 85% Analysis Date = 11/08/16 SpikeMix = Spex Organics TS160511023: 40 µl & Abs 071816: 40 µl Pct Recovery = 98% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 92% Analysis Date = 08/03/16 SpikeMix = Spex Organics TS160603008: 40 µl & Spex Organics TS160511023: 40 µl Pct Recovery = 116% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 176% Analysis Date = 06/29/16 SpikeMix = Spex Organics TS160511023: 40 µl & ChemService 5154100: 40 µl & ChemService 5154 Pct Recovery = 130% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 104% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 100% Analysis Date = 03/11/15 SpikeMix = Abs 042314: 15 µl & Abs 042914: 15 µl Pct Recovery = 97% Analysis Date = 08/20/14 SpikeMix = Abs 042814Pest3: 15 µl & Abs 042314: 15 µl Pct Recovery = 101% Analysis Date = 08/16/14 SpikeMix = Abs 042314: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 110% Analysis Date = 09/23/14 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 85% Analysis Date = 09/10/14 SpikeMix = ChemService 2609400: 15 µl & ERA 0321-14-07: 15 µl Pct Recovery = 59% Analysis Date = 07/24/14 SpikeMix = ChemService 2609400: 15 µl & Abs 042914: 15 µl Pct Recovery = 138% Analysis Date = 05/17/14 SpikeMix = ChemService 2598800: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 142% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 70% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 73% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 73% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 93% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 103% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 128% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 140% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 123% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 123% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 85% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 97% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 112% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 94% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 116% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 105% Analysis Date = 08/04/15 SpikeMix = ERA 0406-15-05: 10 µl & ChemService 4047100: 10 µl & ChemService 3880200: 10 µl Pct Recovery = 122% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 163% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 165% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 198% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 136% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 121% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 122% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 128% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 61% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 120% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 106% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 140% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 91% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 156% Analysis Date = 12/13/16 Pct Recovery = 96% Analysis Date = 12/08/16 Pct Recovery = 96% Analysis Date = 12/08/16 Pct Recovery = 96% Analysis Date = 12/03/16 Pct Recovery = 97% Analysis Date = 12/03/16 Pct Recovery = 97% Analysis Date = 11/28/16 Pct Recovery = 98% Analysis Date = 11/28/16 Pct Recovery = 98% Analysis Date = 11/24/16 Pct Recovery = 98% Analysis Date = 11/24/16 Pct Recovery = 98% Analysis Date = 11/19/16 Pct Recovery = 99% Analysis Date = 11/19/16 Pct Recovery = 99% Analysis Date = 11/14/16 Pct Recovery = 99% Analysis Date = 11/14/16 Pct Recovery = 99% Analysis Date = 11/10/16 Pct Recovery = 100% Analysis Date = 11/10/16 Pct Recovery = 100% Analysis Date = 11/05/16 Pct Recovery = 100% Analysis Date = 11/05/16 Pct Recovery = 100% Analysis Date = 10/31/16 Pct Recovery = 101% Analysis Date = 10/31/16 Pct Recovery = 101% Analysis Date = 10/26/16 Pct Recovery = 101% Analysis Date = 10/26/16 Pct Recovery = 101% Analysis Date = 10/22/16 Pct Recovery = 102% Analysis Date = 10/22/16 Pct Recovery = 102% Analysis Date = 10/17/16 Pct Recovery = 102% Analysis Date = 10/17/16 Pct Recovery = 102% Analysis Date = 10/12/16 Pct Recovery = 103% Analysis Date = 10/12/16 Pct Recovery = 103% Analysis Date = 10/08/16 Pct Recovery = 103% Analysis Date = 10/08/16 Pct Recovery = 103% Analysis Date = 10/03/16 Pct Recovery = 104% Analysis Date = 10/03/16 Pct Recovery = 104% Analysis Date = 09/28/16 Pct Recovery = 105% Analysis Date = 09/28/16 Pct Recovery = 105% Analysis Date = 09/24/16 Pct Recovery = 105% Analysis Date = 09/24/16 Pct Recovery = 105% Analysis Date = 09/19/16 Pct Recovery = 106% Analysis Date = 09/19/16 Pct Recovery = 106% Analysis Date = 09/14/16 Pct Recovery = 106% Analysis Date = 09/14/16 Pct Recovery = 106% Analysis Date = 09/09/16 Pct Recovery = 107% Analysis Date = 09/09/16 Pct Recovery = 107% Analysis Date = 09/05/16 Pct Recovery = 107% Analysis Date = 09/05/16 Pct Recovery = 107% Analysis Date = 08/31/16 Pct Recovery = 108% Analysis Date = 08/31/16 Pct Recovery = 108% Analysis Date = 08/26/16 Pct Recovery = 108% Analysis Date = 08/26/16 Pct Recovery = 108% Analysis Date = 08/22/16 Pct Recovery = 109% Analysis Date = 08/22/16 Pct Recovery = 109% Analysis Date = 08/17/16 Pct Recovery = 109% Analysis Date = 08/17/16 Pct Recovery = 109% Analysis Date = 08/12/16 Pct Recovery = 110% Analysis Date = 08/12/16 Pct Recovery = 110% Analysis Date = 08/07/16 Pct Recovery = 111% Analysis Date = 08/07/16 Pct Recovery = 111% Analysis Date = 08/03/16 Pct Recovery = 111% Analysis Date = 08/03/16 Pct Recovery = 111% Analysis Date = 07/29/16 Pct Recovery = 112% Analysis Date = 07/29/16 Pct Recovery = 112% Analysis Date = 07/24/16 Pct Recovery = 112% Analysis Date = 07/24/16 Pct Recovery = 112% Analysis Date = 07/20/16 Pct Recovery = 113% Analysis Date = 07/20/16 Pct Recovery = 113% Analysis Date = 07/15/16 Pct Recovery = 113% Analysis Date = 07/15/16 Pct Recovery = 113% Analysis Date = 07/10/16 Pct Recovery = 114% Analysis Date = 07/10/16 Pct Recovery = 114% Analysis Date = 07/06/16 Pct Recovery = 114% Analysis Date = 07/06/16 Pct Recovery = 114% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 06/26/16 Pct Recovery = 115% Analysis Date = 06/26/16 Pct Recovery = 115% Analysis Date = 06/21/16 Pct Recovery = 116% Analysis Date = 06/21/16 Pct Recovery = 116% Analysis Date = 06/17/16 Pct Recovery = 116% Analysis Date = 06/17/16 Pct Recovery = 116% Analysis Date = 06/12/16 Pct Recovery = 116% Analysis Date = 06/12/16 Pct Recovery = 116% Analysis Date = 06/07/16 Pct Recovery = 117% Analysis Date = 06/07/16 Pct Recovery = 117% Analysis Date = 06/03/16 Pct Recovery = 117% Analysis Date = 06/03/16 Pct Recovery = 117% Analysis Date = 05/29/16 Pct Recovery = 117% Analysis Date = 05/29/16 Pct Recovery = 117% Analysis Date = 05/24/16 Pct Recovery = 117% Analysis Date = 05/24/16 Pct Recovery = 117% Analysis Date = 05/19/16 Pct Recovery = 118% Analysis Date = 05/19/16 Pct Recovery = 118% Analysis Date = 05/15/16 Pct Recovery = 118% Analysis Date = 05/15/16 Pct Recovery = 118% Analysis Date = 05/10/16 Pct Recovery = 118% Analysis Date = 05/10/16 Pct Recovery = 118% Analysis Date = 05/05/16 Pct Recovery = 119% Analysis Date = 05/05/16 Pct Recovery = 119% Analysis Date = 05/01/16 Pct Recovery = 119% Analysis Date = 05/01/16 Pct Recovery = 119% Analysis Date = 04/26/16 Pct Recovery = 119% Analysis Date = 04/26/16 Pct Recovery = 119% Analysis Date = 04/21/16 Pct Recovery = 120% Analysis Date = 04/21/16 Pct Recovery = 120% Analysis Date = 04/17/16 Pct Recovery = 120% Analysis Date = 04/17/16 Pct Recovery = 120% Analysis Date = 04/12/16 Pct Recovery = 120% Analysis Date = 04/12/16 Pct Recovery = 120% Analysis Date = 04/07/16 Pct Recovery = 121% Analysis Date = 04/07/16 Pct Recovery = 121% Analysis Date = 04/02/16 Pct Recovery = 121% Analysis Date = 04/02/16 Pct Recovery = 121% Analysis Date = 03/29/16 Pct Recovery = 121% Analysis Date = 03/29/16 Pct Recovery = 121% Analysis Date = 03/24/16 Pct Recovery = 122% Analysis Date = 03/24/16 Pct Recovery = 122% Analysis Date = 03/19/16 Pct Recovery = 121% Analysis Date = 03/19/16 Pct Recovery = 121% Analysis Date = 03/15/16 Pct Recovery = 121% Analysis Date = 03/15/16 Pct Recovery = 121% Analysis Date = 03/10/16 Pct Recovery = 120% Analysis Date = 03/10/16 Pct Recovery = 120% Analysis Date = 03/05/16 Pct Recovery = 120% Analysis Date = 03/05/16 Pct Recovery = 120% Analysis Date = 02/29/16 Pct Recovery = 119% Analysis Date = 02/29/16 Pct Recovery = 119% Analysis Date = 02/25/16 Pct Recovery = 118% Analysis Date = 02/25/16 Pct Recovery = 118% Analysis Date = 02/20/16 Pct Recovery = 117% Analysis Date = 02/20/16 Pct Recovery = 117% Analysis Date = 02/15/16 Pct Recovery = 116% Analysis Date = 02/15/16 Pct Recovery = 116% Analysis Date = 02/11/16 Pct Recovery = 115% Analysis Date = 02/11/16 Pct Recovery = 115% Analysis Date = 02/06/16 Pct Recovery = 114% Analysis Date = 02/06/16 Pct Recovery = 114% Analysis Date = 02/01/16 Pct Recovery = 113% Analysis Date = 02/01/16 Pct Recovery = 113% Analysis Date = 01/28/16 Pct Recovery = 113% Analysis Date = 01/28/16 Pct Recovery = 113% Analysis Date = 01/23/16 Pct Recovery = 112% Analysis Date = 01/23/16 Pct Recovery = 112% Analysis Date = 01/18/16 Pct Recovery = 111% Analysis Date = 01/18/16 Pct Recovery = 111% Analysis Date = 01/13/16 Pct Recovery = 110% Analysis Date = 01/13/16 Pct Recovery = 110% Analysis Date = 01/09/16 Pct Recovery = 109% Analysis Date = 01/09/16 Pct Recovery = 109% Analysis Date = 01/04/16 Pct Recovery = 108% Analysis Date = 01/04/16 Pct Recovery = 108% Analysis Date = 12/30/15 Pct Recovery = 107% Analysis Date = 12/30/15 Pct Recovery = 107% Analysis Date = 12/26/15 Pct Recovery = 106% Analysis Date = 12/26/15 Pct Recovery = 106% Analysis Date = 12/21/15 Pct Recovery = 106% Analysis Date = 12/21/15 Pct Recovery = 106% Analysis Date = 12/16/15 Pct Recovery = 105% Analysis Date = 12/16/15 Pct Recovery = 105% Analysis Date = 12/12/15 Pct Recovery = 104% Analysis Date = 12/12/15 Pct Recovery = 104% Analysis Date = 12/07/15 Pct Recovery = 103% Analysis Date = 12/07/15 Pct Recovery = 103% Analysis Date = 12/02/15 Pct Recovery = 101% Analysis Date = 12/02/15 Pct Recovery = 101% Analysis Date = 11/27/15 Pct Recovery = 100% Analysis Date = 11/27/15 Pct Recovery = 100% Analysis Date = 11/23/15 Pct Recovery = 99% Analysis Date = 11/23/15 Pct Recovery = 99% Analysis Date = 11/18/15 Pct Recovery = 99% Analysis Date = 11/18/15 Pct Recovery = 99% Analysis Date = 11/13/15 Pct Recovery = 100% Analysis Date = 11/13/15 Pct Recovery = 100% Analysis Date = 11/09/15 Pct Recovery = 100% Analysis Date = 11/09/15 Pct Recovery = 100% Analysis Date = 11/04/15 Pct Recovery = 101% Analysis Date = 11/04/15 Pct Recovery = 101% Analysis Date = 10/30/15 Pct Recovery = 101% Analysis Date = 10/30/15 Pct Recovery = 101% Analysis Date = 10/25/15 Pct Recovery = 102% Analysis Date = 10/25/15 Pct Recovery = 102% Analysis Date = 10/21/15 Pct Recovery = 103% Analysis Date = 10/21/15 Pct Recovery = 103% Analysis Date = 10/16/15 Pct Recovery = 104% Analysis Date = 10/16/15 Pct Recovery = 104% Analysis Date = 10/11/15 Pct Recovery = 104% Analysis Date = 10/11/15 Pct Recovery = 104% Analysis Date = 10/07/15 Pct Recovery = 105% Analysis Date = 10/07/15 Pct Recovery = 105% Analysis Date = 10/02/15 Pct Recovery = 106% Analysis Date = 10/02/15 Pct Recovery = 106% Analysis Date = 09/27/15 Pct Recovery = 107% Analysis Date = 09/27/15 Pct Recovery = 107% Analysis Date = 09/23/15 Pct Recovery = 108% Analysis Date = 09/23/15 Pct Recovery = 108% Analysis Date = 09/18/15 Pct Recovery = 109% Analysis Date = 09/18/15 Pct Recovery = 109% Analysis Date = 09/13/15 Pct Recovery = 110% Analysis Date = 09/13/15 Pct Recovery = 110% Analysis Date = 09/08/15 Pct Recovery = 111% Analysis Date = 09/08/15 Pct Recovery = 111% Analysis Date = 09/04/15 Pct Recovery = 112% Analysis Date = 09/04/15 Pct Recovery = 112% Analysis Date = 08/30/15 Pct Recovery = 113% Analysis Date = 08/30/15 Pct Recovery = 113% Analysis Date = 08/25/15 Pct Recovery = 114% Analysis Date = 08/25/15 Pct Recovery = 114% Analysis Date = 08/21/15 Pct Recovery = 115% Analysis Date = 08/21/15 Pct Recovery = 115% Analysis Date = 08/16/15 Pct Recovery = 116% Analysis Date = 08/16/15 Pct Recovery = 116% Analysis Date = 08/11/15 Pct Recovery = 117% Analysis Date = 08/11/15 Pct Recovery = 117% Analysis Date = 08/06/15 Pct Recovery = 117% Analysis Date = 08/06/15 Pct Recovery = 117% Analysis Date = 08/02/15 Pct Recovery = 117% Analysis Date = 08/02/15 Pct Recovery = 117% Analysis Date = 07/28/15 Pct Recovery = 116% Analysis Date = 07/28/15 Pct Recovery = 116% Analysis Date = 07/23/15 Pct Recovery = 116% Analysis Date = 07/23/15 Pct Recovery = 116% Analysis Date = 07/19/15 Pct Recovery = 116% Analysis Date = 07/19/15 Pct Recovery = 116% Analysis Date = 07/14/15 Pct Recovery = 116% Analysis Date = 07/14/15 Pct Recovery = 116% Analysis Date = 07/09/15 Pct Recovery = 115% Analysis Date = 07/09/15 Pct Recovery = 115% Analysis Date = 07/05/15 Pct Recovery = 115% Analysis Date = 07/05/15 Pct Recovery = 115% Analysis Date = 06/30/15 Pct Recovery = 115% Analysis Date = 06/30/15 Pct Recovery = 115% Analysis Date = 06/25/15 Pct Recovery = 114% Analysis Date = 06/25/15 Pct Recovery = 114% Analysis Date = 06/20/15 Pct Recovery = 114% Analysis Date = 06/20/15 Pct Recovery = 114% Analysis Date = 06/16/15 Pct Recovery = 114% Analysis Date = 06/16/15 Pct Recovery = 114% Analysis Date = 06/11/15 Pct Recovery = 113% Analysis Date = 06/11/15 Pct Recovery = 113% Analysis Date = 06/06/15 Pct Recovery = 113% Analysis Date = 06/06/15 Pct Recovery = 113% Analysis Date = 06/02/15 Pct Recovery = 113% Analysis Date = 06/02/15 Pct Recovery = 113% Analysis Date = 05/28/15 Pct Recovery = 113% Analysis Date = 05/28/15 Pct Recovery = 113% Analysis Date = 05/23/15 Pct Recovery = 112% Analysis Date = 05/23/15 Pct Recovery = 112% Analysis Date = 05/18/15 Pct Recovery = 112% Analysis Date = 05/18/15 Pct Recovery = 112% Analysis Date = 05/14/15 Pct Recovery = 112% Analysis Date = 05/14/15 Pct Recovery = 112% Analysis Date = 05/09/15 Pct Recovery = 111% Analysis Date = 05/09/15 Pct Recovery = 111% Analysis Date = 05/04/15 Pct Recovery = 111% Analysis Date = 05/04/15 Pct Recovery = 111% Analysis Date = 04/30/15 Pct Recovery = 111% Analysis Date = 04/30/15 Pct Recovery = 111% Analysis Date = 04/25/15 Pct Recovery = 110% Analysis Date = 04/25/15 Pct Recovery = 110% Analysis Date = 04/20/15 Pct Recovery = 110% Analysis Date = 04/20/15 Pct Recovery = 110% Analysis Date = 04/16/15 Pct Recovery = 110% Analysis Date = 04/16/15 Pct Recovery = 110% Analysis Date = 04/11/15 Pct Recovery = 110% Analysis Date = 04/11/15 Pct Recovery = 110% Analysis Date = 04/06/15 Pct Recovery = 109% Analysis Date = 04/06/15 Pct Recovery = 109% Analysis Date = 04/01/15 Pct Recovery = 109% Analysis Date = 04/01/15 Pct Recovery = 109% Analysis Date = 03/28/15 Pct Recovery = 109% Analysis Date = 03/28/15 Pct Recovery = 109% Analysis Date = 03/23/15 Pct Recovery = 108% Analysis Date = 03/23/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/18/15 Pct Recovery = 108% Analysis Date = 03/14/15 Pct Recovery = 108% Analysis Date = 03/14/15 Pct Recovery = 108% Analysis Date = 03/09/15 Pct Recovery = 108% Analysis Date = 03/09/15 Pct Recovery = 108% Analysis Date = 03/04/15 Pct Recovery = 108% Analysis Date = 03/04/15 Pct Recovery = 108% Analysis Date = 02/28/15 Pct Recovery = 108% Analysis Date = 02/28/15 Pct Recovery = 108% Analysis Date = 02/23/15 Pct Recovery = 108% Analysis Date = 02/23/15 Pct Recovery = 108% Analysis Date = 02/18/15 Pct Recovery = 108% Analysis Date = 02/18/15 Pct Recovery = 108% Analysis Date = 02/13/15 Pct Recovery = 108% Analysis Date = 02/13/15 Pct Recovery = 108% Analysis Date = 02/09/15 Pct Recovery = 108% Analysis Date = 02/09/15 Pct Recovery = 108% Analysis Date = 02/04/15 Pct Recovery = 108% Analysis Date = 02/04/15 Pct Recovery = 108% Analysis Date = 01/30/15 Pct Recovery = 108% Analysis Date = 01/30/15 Pct Recovery = 108% Analysis Date = 01/26/15 Pct Recovery = 108% Analysis Date = 01/26/15 Pct Recovery = 108% Analysis Date = 01/21/15 Pct Recovery = 108% Analysis Date = 01/21/15 Pct Recovery = 108% Analysis Date = 01/16/15 Pct Recovery = 108% Analysis Date = 01/16/15 Pct Recovery = 108% Analysis Date = 01/11/15 Pct Recovery = 108% Analysis Date = 01/11/15 Pct Recovery = 108% Analysis Date = 01/07/15 Pct Recovery = 108% Analysis Date = 01/07/15 Pct Recovery = 108% Analysis Date = 01/02/15 Pct Recovery = 108% Analysis Date = 01/02/15 Pct Recovery = 108% Analysis Date = 12/28/14 Pct Recovery = 108% Analysis Date = 12/28/14 Pct Recovery = 108% Analysis Date = 12/24/14 Pct Recovery = 108% Analysis Date = 12/24/14 Pct Recovery = 108% Analysis Date = 12/19/14 Pct Recovery = 108% Analysis Date = 12/19/14 Pct Recovery = 108% Analysis Date = 12/14/14 Pct Recovery = 109% Analysis Date = 12/14/14 Pct Recovery = 109% Analysis Date = 12/10/14 Pct Recovery = 109% Analysis Date = 12/10/14 Pct Recovery = 109% Analysis Date = 12/05/14 Pct Recovery = 109% Analysis Date = 12/05/14 Pct Recovery = 109% Analysis Date = 11/30/14 Pct Recovery = 109% Analysis Date = 11/30/14 Pct Recovery = 109% Analysis Date = 11/25/14 Pct Recovery = 109% Analysis Date = 11/25/14 Pct Recovery = 109% Analysis Date = 11/21/14 Pct Recovery = 109% Analysis Date = 11/21/14 Pct Recovery = 109% Analysis Date = 11/16/14 Pct Recovery = 109% Analysis Date = 11/16/14 Pct Recovery = 109% Analysis Date = 11/11/14 Pct Recovery = 109% Analysis Date = 11/11/14 Pct Recovery = 109% Analysis Date = 11/07/14 Pct Recovery = 109% Analysis Date = 11/07/14 Pct Recovery = 109% Analysis Date = 11/02/14 Pct Recovery = 109% Analysis Date = 11/02/14 Pct Recovery = 109% Analysis Date = 10/28/14 Pct Recovery = 109% Analysis Date = 10/28/14 Pct Recovery = 109% Analysis Date = 10/23/14 Pct Recovery = 109% Analysis Date = 10/23/14 Pct Recovery = 109% Analysis Date = 10/19/14 Pct Recovery = 109% Analysis Date = 10/19/14 Pct Recovery = 109% Analysis Date = 10/14/14 Pct Recovery = 109% Analysis Date = 10/14/14 Pct Recovery = 109% Analysis Date = 10/09/14 Pct Recovery = 109% Analysis Date = 10/09/14 Pct Recovery = 109% Analysis Date = 10/05/14 Pct Recovery = 109% Analysis Date = 10/05/14 Pct Recovery = 109% Analysis Date = 09/30/14 Pct Recovery = 109% Analysis Date = 09/30/14 Pct Recovery = 109% Analysis Date = 09/25/14 Pct Recovery = 109% Analysis Date = 09/25/14 Pct Recovery = 109% Analysis Date = 09/21/14 Pct Recovery = 109% Analysis Date = 09/21/14 Pct Recovery = 109% Analysis Date = 09/16/14 Pct Recovery = 109% Analysis Date = 09/16/14 Pct Recovery = 109% Analysis Date = 09/11/14 Pct Recovery = 109% Analysis Date = 09/11/14 Pct Recovery = 109% Analysis Date = 09/06/14 Pct Recovery = 109% Analysis Date = 09/06/14 Pct Recovery = 109% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 09/02/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/28/14 Pct Recovery = 109% Analysis Date = 08/23/14 Pct Recovery = 110% Analysis Date = 08/23/14 Pct Recovery = 110% Analysis Date = 08/19/14 Pct Recovery = 110% Analysis Date = 08/19/14 Pct Recovery = 110% Analysis Date = 08/14/14 Pct Recovery = 110% Analysis Date = 08/14/14 Pct Recovery = 110% Analysis Date = 08/09/14 Pct Recovery = 110% Analysis Date = 08/09/14 Pct Recovery = 110% Analysis Date = 08/04/14 Pct Recovery = 110% Analysis Date = 08/04/14 Pct Recovery = 110% Analysis Date = 07/31/14 Pct Recovery = 110% Analysis Date = 07/31/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/26/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/21/14 Pct Recovery = 110% Analysis Date = 07/17/14 Pct Recovery = 110% Analysis Date = 07/17/14 Pct Recovery = 110% Analysis Date = 07/12/14 Pct Recovery = 110% Analysis Date = 07/12/14 Pct Recovery = 110% Analysis Date = 07/07/14 Pct Recovery = 110% Analysis Date = 07/07/14 Pct Recovery = 110% Analysis Date = 07/03/14 Pct Recovery = 110% Analysis Date = 07/03/14 Pct Recovery = 110% Analysis Date = 06/28/14 Pct Recovery = 110% Analysis Date = 06/28/14 Pct Recovery = 110% Analysis Date = 06/23/14 Pct Recovery = 110% Analysis Date = 06/23/14 Pct Recovery = 110% Analysis Date = 06/18/14 Pct Recovery = 110% Analysis Date = 06/18/14 Pct Recovery = 110% Analysis Date = 06/14/14 Pct Recovery = 110% Analysis Date = 06/14/14 Pct Recovery = 110% Analysis Date = 06/09/14 Pct Recovery = 110% Analysis Date = 06/09/14 Pct Recovery = 110% Analysis Date = 06/04/14 Pct Recovery = 110% Analysis Date = 06/04/14 Pct Recovery = 110% Analysis Date = 05/31/14 Pct Recovery = 110% Analysis Date = 05/31/14 Pct Recovery = 110% Analysis Date = 05/26/14 Pct Recovery = 111% Analysis Date = 05/26/14 Pct Recovery = 111% Analysis Date = 05/21/14 Pct Recovery = 111% Analysis Date = 05/21/14 Pct Recovery = 111% Analysis Date = 05/17/14 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ASULAM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 13 131% 35% 128% 26%
>= Reporting Level 83 106% 25% 103% 22%
Total 96 110% 28% 106% 24%

Sample Statistics
ASULAM

Characteristic N % % Basis
Plotted 96 90% Spiked
Estimated Values 96 90% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 7 7% Spiked
Spiked 107 .  
False Negatives 4 4% 4 out of 107
Not Spiked 71 .  
False Positives 0 0% 0 out of 68