BQS OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2437 , TESTIDCODE: 68211LCM60
Open Data Set

Analysis Date = 12/19/13 SpikeMix = ChemService 1473000: 5 µl & Supelco LB99392: 5 µl & Abs 042413: 5 µl Pct Recovery = 99% Analysis Date = 02/19/14 SpikeMix = Spex Organics T1130514013: 5 µl & ERA 0318-13-02.2: 5 µl & Crescent 04CC101: 5 µ Pct Recovery = 98% Analysis Date = 09/25/13 SpikeMix = Spex Organics T1130514013: 5 µl & ERA 0318-13-02.2: 5 µl & Crescent 04CC101: 5 µ Pct Recovery = 84% Analysis Date = 01/23/14 SpikeMix = Abs 042413: 2 µl & Spex Organics T1130514013: 2 µl & Supelco LB99392: 2 µl Pct Recovery = 92% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 2 µl & Abs 042413: 2 µl & Spex Organics T1130514013: 2 µl Pct Recovery = 103% Analysis Date = 11/07/13 SpikeMix = Spex Organics T1130514013: 2 µl & Supelco LB99392: 2 µl & Crescent 04CC101: 2 µl Pct Recovery = 94% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 78% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 86% Analysis Date = 10/20/15 SpikeMix = ERA 0406-15-06: 80 µl & ERA 0406-15-04: 80 µl Pct Recovery = 94% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 80% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 66% Analysis Date = 10/07/15 SpikeMix = ChemService 3995200: 80 µl & ChemService 3880100: 80 µl & ChemService 4047100: 8 Pct Recovery = 70% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 84% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 82% Analysis Date = 10/03/15 SpikeMix = ChemService 4047100: 80 µl & ChemService 3880200: 80 µl & ChemService 4047000: 8 Pct Recovery = 73% Analysis Date = 06/11/14 SpikeMix = ChemService 2598800: 60 µl & ChemService 2609400: 60 µl Pct Recovery = 133% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 84% Analysis Date = 12/13/16 SpikeMix = Abs 071216: 80 µl & Abs 071816: 80 µl Pct Recovery = 84% Analysis Date = 12/16/14 SpikeMix = ChemService 2598800: 30 µl & Abs 042314: 30 µl Pct Recovery = 76% Analysis Date = 12/02/14 SpikeMix = Abs 042914: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 72% Analysis Date = 10/07/14 SpikeMix = ERA 0321-14-07: 30 µl & ChemService 2598800: 30 µl Pct Recovery = 75% Analysis Date = 06/26/14 SpikeMix = ChemService 2598800: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 53% Analysis Date = 02/11/15 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 86% Analysis Date = 11/18/14 SpikeMix = Abs 042814Pest3: 30 µl & ChemService 2609400: 30 µl Pct Recovery = 99% Analysis Date = 11/05/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 99% Analysis Date = 10/21/14 SpikeMix = Abs 042814Pest3: 30 µl & Abs 042314: 30 µl Pct Recovery = 107% Analysis Date = 07/19/14 SpikeMix = Abs 042914: 30 µl & Abs 042814Pest3: 30 µl Pct Recovery = 113% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 85% Analysis Date = 05/06/16 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 75% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 62% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 51% Analysis Date = 02/17/16 SpikeMix = ERA 0406-15-06: 20 µl & ERA 0406-15-04: 20 µl Pct Recovery = 63% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 77% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 70% Analysis Date = 10/29/15 SpikeMix = ERA 0406-15-05: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 86% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 102% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 78% Analysis Date = 09/02/15 SpikeMix = ERA 0406-15-06: 20 µl & ChemService 4047000: 20 µl & ChemService 3880000: 20 µl Pct Recovery = 99% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 86% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 73% Analysis Date = 08/26/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 67% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 78% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 96% Analysis Date = 08/12/15 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ERA 0406-15-06: 20 µl Pct Recovery = 93% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 69% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 80% Analysis Date = 03/17/16 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 81% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 85% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 67% Analysis Date = 03/01/16 SpikeMix = ChemService 3995200: 20 µl & ChemService 3880100: 20 µl & ChemService 4047100: 2 Pct Recovery = 85% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 82% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 71% Analysis Date = 01/08/16 SpikeMix = ChemService 4047100: 20 µl & ChemService 3880200: 20 µl & ChemService 4047000: 2 Pct Recovery = 83% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 83% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 82% Analysis Date = 12/10/15 SpikeMix = ERA 0406-15-05: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 96% Analysis Date = 07/22/15 SpikeMix = ERA 0406-15-04: 20 µl & ChemService 4047100: 20 µl & ChemService 3880200: 20 µl Pct Recovery = 65% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 51% Analysis Date = 10/06/16 SpikeMix = Spex Organics TS160603008: 40 µl & Abs 071216: 40 µl Pct Recovery = 63% Analysis Date = 04/15/15 SpikeMix = ChemService 2598800: 15 µl & Abs 042914: 15 µl Pct Recovery = 94% Analysis Date = 03/07/15 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 96% Analysis Date = 08/17/14 SpikeMix = ERA 0321-14-07: 15 µl & ChemService 2598800: 15 µl Pct Recovery = 82% Analysis Date = 05/17/14 SpikeMix = ChemService 2598800: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 71% Analysis Date = 04/09/15 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 70% Analysis Date = 09/23/14 SpikeMix = Abs 042814Pest3: 15 µl & ChemService 2609400: 15 µl Pct Recovery = 81% Analysis Date = 09/10/14 SpikeMix = Abs 042914: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 94% Analysis Date = 08/20/14 SpikeMix = Abs 042814Pest3: 15 µl & Abs 042314: 15 µl Pct Recovery = 69% Analysis Date = 07/31/14 SpikeMix = ERA 0321-14-07: 15 µl & Abs 042814Pest3: 15 µl Pct Recovery = 71% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 86% Analysis Date = 03/02/16 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 91% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 83% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 74% Analysis Date = 02/18/16 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 77% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 53% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 46% Analysis Date = 02/12/16 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 63% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 95% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 106% Analysis Date = 11/25/15 SpikeMix = ERA 0406-15-06: 10 µl & ChemService 4047000: 10 µl & ChemService 3880000: 10 µl Pct Recovery = 79% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 94% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 80% Analysis Date = 10/02/15 SpikeMix = ERA 0406-15-05: 10 µl & ERA 0406-15-06: 10 µl Pct Recovery = 70% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 78% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 73% Analysis Date = 08/11/15 SpikeMix = ERA 0406-15-06: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 72% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 76% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 79% Analysis Date = 03/23/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ChemService 4047000: 1 Pct Recovery = 89% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 85% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 86% Analysis Date = 02/19/16 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 81% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 92% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 80% Analysis Date = 11/24/15 SpikeMix = ChemService 3995200: 10 µl & ChemService 3880100: 10 µl & ChemService 4047100: 1 Pct Recovery = 88% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 76% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 68% Analysis Date = 11/11/15 SpikeMix = ChemService 4047100: 10 µl & ChemService 3880200: 10 µl & ERA 0406-15-04: 10 µl Pct Recovery = 68% Analysis Date = 08/06/15 SpikeMix = ERA 0406-15-05: 10 µl & ChemService 4047100: 10 µl & ChemService 3880200: 10 µl Pct Recovery = 85% Analysis Date = 12/13/16 Pct Recovery = 72% Analysis Date = 12/07/16 Pct Recovery = 72% Analysis Date = 12/07/16 Pct Recovery = 72% Analysis Date = 12/01/16 Pct Recovery = 72% Analysis Date = 12/01/16 Pct Recovery = 72% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/19/16 Pct Recovery = 73% Analysis Date = 11/13/16 Pct Recovery = 73% Analysis Date = 11/13/16 Pct Recovery = 73% Analysis Date = 11/07/16 Pct Recovery = 73% Analysis Date = 11/07/16 Pct Recovery = 73% Analysis Date = 11/01/16 Pct Recovery = 73% Analysis Date = 11/01/16 Pct Recovery = 73% Analysis Date = 10/27/16 Pct Recovery = 73% Analysis Date = 10/27/16 Pct Recovery = 73% Analysis Date = 10/21/16 Pct Recovery = 73% Analysis Date = 10/21/16 Pct Recovery = 73% Analysis Date = 10/15/16 Pct Recovery = 73% Analysis Date = 10/15/16 Pct Recovery = 73% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 09/27/16 Pct Recovery = 73% Analysis Date = 09/27/16 Pct Recovery = 73% Analysis Date = 09/21/16 Pct Recovery = 74% Analysis Date = 09/21/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 74% Analysis Date = 09/10/16 Pct Recovery = 74% Analysis Date = 09/10/16 Pct Recovery = 74% Analysis Date = 09/04/16 Pct Recovery = 74% Analysis Date = 09/04/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/17/16 Pct Recovery = 74% Analysis Date = 08/17/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/05/16 Pct Recovery = 74% Analysis Date = 08/05/16 Pct Recovery = 74% Analysis Date = 07/30/16 Pct Recovery = 74% Analysis Date = 07/30/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/19/16 Pct Recovery = 74% Analysis Date = 07/19/16 Pct Recovery = 74% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/07/16 Pct Recovery = 75% Analysis Date = 07/01/16 Pct Recovery = 75% Analysis Date = 07/01/16 Pct Recovery = 75% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/19/16 Pct Recovery = 75% Analysis Date = 06/19/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/08/16 Pct Recovery = 75% Analysis Date = 06/02/16 Pct Recovery = 75% Analysis Date = 06/02/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/15/16 Pct Recovery = 75% Analysis Date = 05/15/16 Pct Recovery = 75% Analysis Date = 05/09/16 Pct Recovery = 75% Analysis Date = 05/09/16 Pct Recovery = 75% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 04/27/16 Pct Recovery = 76% Analysis Date = 04/27/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/16/16 Pct Recovery = 76% Analysis Date = 04/10/16 Pct Recovery = 76% Analysis Date = 04/10/16 Pct Recovery = 76% Analysis Date = 04/04/16 Pct Recovery = 76% Analysis Date = 04/04/16 Pct Recovery = 76% Analysis Date = 03/29/16 Pct Recovery = 76% Analysis Date = 03/29/16 Pct Recovery = 76% Analysis Date = 03/23/16 Pct Recovery = 76% Analysis Date = 03/23/16 Pct Recovery = 76% Analysis Date = 03/17/16 Pct Recovery = 76% Analysis Date = 03/17/16 Pct Recovery = 76% Analysis Date = 03/11/16 Pct Recovery = 76% Analysis Date = 03/11/16 Pct Recovery = 76% Analysis Date = 03/06/16 Pct Recovery = 77% Analysis Date = 03/06/16 Pct Recovery = 77% Analysis Date = 02/29/16 Pct Recovery = 77% Analysis Date = 02/29/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/17/16 Pct Recovery = 77% Analysis Date = 02/11/16 Pct Recovery = 77% Analysis Date = 02/11/16 Pct Recovery = 77% Analysis Date = 02/05/16 Pct Recovery = 78% Analysis Date = 02/05/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/30/16 Pct Recovery = 78% Analysis Date = 01/24/16 Pct Recovery = 78% Analysis Date = 01/24/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/19/16 Pct Recovery = 78% Analysis Date = 01/13/16 Pct Recovery = 78% Analysis Date = 01/13/16 Pct Recovery = 78% Analysis Date = 01/07/16 Pct Recovery = 78% Analysis Date = 01/07/16 Pct Recovery = 78% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 01/01/16 Pct Recovery = 79% Analysis Date = 12/26/15 Pct Recovery = 79% Analysis Date = 12/26/15 Pct Recovery = 79% Analysis Date = 12/20/15 Pct Recovery = 79% Analysis Date = 12/20/15 Pct Recovery = 79% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/14/15 Pct Recovery = 80% Analysis Date = 12/08/15 Pct Recovery = 80% Analysis Date = 12/08/15 Pct Recovery = 80% Analysis Date = 12/03/15 Pct Recovery = 80% Analysis Date = 12/03/15 Pct Recovery = 80% Analysis Date = 11/27/15 Pct Recovery = 80% Analysis Date = 11/27/15 Pct Recovery = 80% Analysis Date = 11/21/15 Pct Recovery = 81% Analysis Date = 11/21/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 81% Analysis Date = 11/09/15 Pct Recovery = 82% Analysis Date = 11/09/15 Pct Recovery = 82% Analysis Date = 11/03/15 Pct Recovery = 82% Analysis Date = 11/03/15 Pct Recovery = 82% Analysis Date = 10/28/15 Pct Recovery = 82% Analysis Date = 10/28/15 Pct Recovery = 82% Analysis Date = 10/22/15 Pct Recovery = 82% Analysis Date = 10/22/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/17/15 Pct Recovery = 82% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/11/15 Pct Recovery = 81% Analysis Date = 10/05/15 Pct Recovery = 81% Analysis Date = 10/05/15 Pct Recovery = 81% Analysis Date = 09/29/15 Pct Recovery = 81% Analysis Date = 09/29/15 Pct Recovery = 81% Analysis Date = 09/23/15 Pct Recovery = 81% Analysis Date = 09/23/15 Pct Recovery = 81% Analysis Date = 09/17/15 Pct Recovery = 81% Analysis Date = 09/17/15 Pct Recovery = 81% Analysis Date = 09/11/15 Pct Recovery = 81% Analysis Date = 09/11/15 Pct Recovery = 81% Analysis Date = 09/05/15 Pct Recovery = 81% Analysis Date = 09/05/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/31/15 Pct Recovery = 81% Analysis Date = 08/25/15 Pct Recovery = 81% Analysis Date = 08/25/15 Pct Recovery = 81% Analysis Date = 08/19/15 Pct Recovery = 81% Analysis Date = 08/19/15 Pct Recovery = 81% Analysis Date = 08/13/15 Pct Recovery = 81% Analysis Date = 08/13/15 Pct Recovery = 81% Analysis Date = 08/07/15 Pct Recovery = 81% Analysis Date = 08/07/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 08/01/15 Pct Recovery = 81% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/26/15 Pct Recovery = 81% Analysis Date = 07/20/15 Pct Recovery = 81% Analysis Date = 07/20/15 Pct Recovery = 81% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/15/15 Pct Recovery = 82% Analysis Date = 07/09/15 Pct Recovery = 82% Analysis Date = 07/09/15 Pct Recovery = 82% Analysis Date = 07/03/15 Pct Recovery = 82% Analysis Date = 07/03/15 Pct Recovery = 82% Analysis Date = 06/27/15 Pct Recovery = 82% Analysis Date = 06/27/15 Pct Recovery = 82% Analysis Date = 06/21/15 Pct Recovery = 82% Analysis Date = 06/21/15 Pct Recovery = 82% Analysis Date = 06/15/15 Pct Recovery = 82% Analysis Date = 06/15/15 Pct Recovery = 82% Analysis Date = 06/09/15 Pct Recovery = 83% Analysis Date = 06/09/15 Pct Recovery = 83% Analysis Date = 06/03/15 Pct Recovery = 83% Analysis Date = 06/03/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/29/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 83% Analysis Date = 05/23/15 Pct Recovery = 83% Analysis Date = 05/17/15 Pct Recovery = 83% Analysis Date = 05/17/15 Pct Recovery = 83% Analysis Date = 05/11/15 Pct Recovery = 83% Analysis Date = 05/11/15 Pct Recovery = 83% Analysis Date = 05/05/15 Pct Recovery = 84% Analysis Date = 05/05/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/29/15 Pct Recovery = 84% Analysis Date = 04/23/15 Pct Recovery = 84% Analysis Date = 04/23/15 Pct Recovery = 84% Analysis Date = 04/17/15 Pct Recovery = 84% Analysis Date = 04/17/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 84% Analysis Date = 04/12/15 Pct Recovery = 84% Analysis Date = 04/06/15 Pct Recovery = 84% Analysis Date = 04/06/15 Pct Recovery = 84% Analysis Date = 03/31/15 Pct Recovery = 84% Analysis Date = 03/31/15 Pct Recovery = 84% Analysis Date = 03/25/15 Pct Recovery = 84% Analysis Date = 03/25/15 Pct Recovery = 84% Analysis Date = 03/19/15 Pct Recovery = 84% Analysis Date = 03/19/15 Pct Recovery = 84% Analysis Date = 03/13/15 Pct Recovery = 84% Analysis Date = 03/13/15 Pct Recovery = 84% Analysis Date = 03/07/15 Pct Recovery = 85% Analysis Date = 03/07/15 Pct Recovery = 85% Analysis Date = 03/01/15 Pct Recovery = 85% Analysis Date = 03/01/15 Pct Recovery = 85% Analysis Date = 02/24/15 Pct Recovery = 85% Analysis Date = 02/24/15 Pct Recovery = 85% Analysis Date = 02/18/15 Pct Recovery = 85% Analysis Date = 02/18/15 Pct Recovery = 85% Analysis Date = 02/12/15 Pct Recovery = 85% Analysis Date = 02/12/15 Pct Recovery = 85% Analysis Date = 02/06/15 Pct Recovery = 85% Analysis Date = 02/06/15 Pct Recovery = 85% Analysis Date = 01/31/15 Pct Recovery = 85% Analysis Date = 01/31/15 Pct Recovery = 85% Analysis Date = 01/25/15 Pct Recovery = 85% Analysis Date = 01/25/15 Pct Recovery = 85% Analysis Date = 01/19/15 Pct Recovery = 85% Analysis Date = 01/19/15 Pct Recovery = 85% Analysis Date = 01/13/15 Pct Recovery = 85% Analysis Date = 01/13/15 Pct Recovery = 85% Analysis Date = 01/08/15 Pct Recovery = 85% Analysis Date = 01/08/15 Pct Recovery = 85% Analysis Date = 01/02/15 Pct Recovery = 85% Analysis Date = 01/02/15 Pct Recovery = 85% Analysis Date = 12/27/14 Pct Recovery = 85% Analysis Date = 12/27/14 Pct Recovery = 85% Analysis Date = 12/21/14 Pct Recovery = 85% Analysis Date = 12/21/14 Pct Recovery = 85% Analysis Date = 12/15/14 Pct Recovery = 86% Analysis Date = 12/15/14 Pct Recovery = 86% Analysis Date = 12/09/14 Pct Recovery = 86% Analysis Date = 12/09/14 Pct Recovery = 86% Analysis Date = 12/03/14 Pct Recovery = 86% Analysis Date = 12/03/14 Pct Recovery = 86% Analysis Date = 11/27/14 Pct Recovery = 86% Analysis Date = 11/27/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/22/14 Pct Recovery = 86% Analysis Date = 11/16/14 Pct Recovery = 86% Analysis Date = 11/16/14 Pct Recovery = 86% Analysis Date = 11/10/14 Pct Recovery = 86% Analysis Date = 11/10/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 11/04/14 Pct Recovery = 86% Analysis Date = 10/29/14 Pct Recovery = 86% Analysis Date = 10/29/14 Pct Recovery = 86% Analysis Date = 10/23/14 Pct Recovery = 86% Analysis Date = 10/23/14 Pct Recovery = 86% Analysis Date = 10/17/14 Pct Recovery = 87% Analysis Date = 10/17/14 Pct Recovery = 87% Analysis Date = 10/11/14 Pct Recovery = 87% Analysis Date = 10/11/14 Pct Recovery = 87% Analysis Date = 10/06/14 Pct Recovery = 87% Analysis Date = 10/06/14 Pct Recovery = 87% Analysis Date = 09/30/14 Pct Recovery = 87% Analysis Date = 09/30/14 Pct Recovery = 87% Analysis Date = 09/24/14 Pct Recovery = 87% Analysis Date = 09/24/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/18/14 Pct Recovery = 87% Analysis Date = 09/12/14 Pct Recovery = 88% Analysis Date = 09/12/14 Pct Recovery = 88% Analysis Date = 09/06/14 Pct Recovery = 88% Analysis Date = 09/06/14 Pct Recovery = 88% Analysis Date = 08/31/14 Pct Recovery = 88% Analysis Date = 08/31/14 Pct Recovery = 88% Analysis Date = 08/25/14 Pct Recovery = 88% Analysis Date = 08/25/14 Pct Recovery = 88% Analysis Date = 08/20/14 Pct Recovery = 88% Analysis Date = 08/20/14 Pct Recovery = 88% Analysis Date = 08/14/14 Pct Recovery = 88% Analysis Date = 08/14/14 Pct Recovery = 88% Analysis Date = 08/08/14 Pct Recovery = 88% Analysis Date = 08/08/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 08/02/14 Pct Recovery = 88% Analysis Date = 07/27/14 Pct Recovery = 89% Analysis Date = 07/27/14 Pct Recovery = 89% Analysis Date = 07/21/14 Pct Recovery = 89% Analysis Date = 07/21/14 Pct Recovery = 89% Analysis Date = 07/15/14 Pct Recovery = 89% Analysis Date = 07/15/14 Pct Recovery = 89% Analysis Date = 07/09/14 Pct Recovery = 89% Analysis Date = 07/09/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 07/04/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/28/14 Pct Recovery = 89% Analysis Date = 06/22/14 Pct Recovery = 89% Analysis Date = 06/22/14 Pct Recovery = 89% Analysis Date = 06/16/14 Pct Recovery = 89% Analysis Date = 06/16/14 Pct Recovery = 89% Analysis Date = 06/10/14 Pct Recovery = 90% Analysis Date = 06/10/14 Pct Recovery = 90% Analysis Date = 06/04/14 Pct Recovery = 90% Analysis Date = 06/04/14 Pct Recovery = 90% Analysis Date = 05/29/14 Pct Recovery = 90% Analysis Date = 05/29/14 Pct Recovery = 90% Analysis Date = 05/23/14 Pct Recovery = 90% Analysis Date = 05/23/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/18/14 Pct Recovery = 90% Analysis Date = 05/12/14 Pct Recovery = 90% Analysis Date = 05/12/14 Pct Recovery = 90% Analysis Date = 05/06/14 Pct Recovery = 90% Analysis Date = 05/06/14 Pct Recovery = 90% Analysis Date = 04/30/14 Pct Recovery = 90% Analysis Date = 04/30/14 Pct Recovery = 90% Analysis Date = 04/24/14 Pct Recovery = 90% Analysis Date = 04/24/14 Pct Recovery = 90% Analysis Date = 04/18/14 Pct Recovery = 91% Analysis Date = 04/18/14 Pct Recovery = 91% Analysis Date = 04/12/14 Pct Recovery = 91% Analysis Date = 04/12/14 Pct Recovery = 91% Analysis Date = 04/06/14 Pct Recovery = 91% Analysis Date = 04/06/14 Pct Recovery = 91% Analysis Date = 04/01/14 Pct Recovery = 91% Analysis Date = 04/01/14 Pct Recovery = 91% Analysis Date = 03/26/14 Pct Recovery = 91% Analysis Date = 03/26/14 Pct Recovery = 91% Analysis Date = 03/20/14 Pct Recovery = 91% Analysis Date = 03/20/14 Pct Recovery = 91% Analysis Date = 03/14/14 Pct Recovery = 91% Analysis Date = 03/14/14 Pct Recovery = 91% Analysis Date = 03/08/14 Pct Recovery = 91% Analysis Date = 03/08/14 Pct Recovery = 91% Analysis Date = 03/02/14 Pct Recovery = 92% Analysis Date = 03/02/14 Pct Recovery = 92% Analysis Date = 02/24/14 Pct Recovery = 92% Analysis Date = 02/24/14 Pct Recovery = 92% Analysis Date = 02/18/14 Pct Recovery = 92% Analysis Date = 02/18/14 Pct Recovery = 92% Analysis Date = 02/13/14 Pct Recovery = 92% Analysis Date = 02/13/14 Pct Recovery = 92% Analysis Date = 02/07/14 Pct Recovery = 92% Analysis Date = 02/07/14 Pct Recovery = 92% Analysis Date = 02/01/14 Pct Recovery = 92% Analysis Date = 02/01/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 92% Analysis Date = 01/26/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/14/14 Pct Recovery = 92% Analysis Date = 01/14/14 Pct Recovery = 92% Analysis Date = 01/08/14 Pct Recovery = 93% Analysis Date = 01/08/14 Pct Recovery = 93% Analysis Date = 01/02/14 Pct Recovery = 93% Analysis Date = 01/02/14 Pct Recovery = 93% Analysis Date = 12/28/13 Pct Recovery = 93% Analysis Date = 12/28/13 Pct Recovery = 93% Analysis Date = 12/22/13 Pct Recovery = 93% Analysis Date = 12/22/13 Pct Recovery = 93% Analysis Date = 12/16/13 Pct Recovery = 93% Analysis Date = 12/16/13 Pct Recovery = 93% Analysis Date = 12/10/13 Pct Recovery = 93% Analysis Date = 12/10/13 Pct Recovery = 93% Analysis Date = 12/04/13 Pct Recovery = 93% Analysis Date = 12/04/13 Pct Recovery = 93% Analysis Date = 11/28/13 Pct Recovery = 93% Analysis Date = 11/28/13 Pct Recovery = 93% Analysis Date = 11/22/13 Pct Recovery = 94% Analysis Date = 11/22/13 Pct Recovery = 94% Analysis Date = 11/16/13 Pct Recovery = 94% Analysis Date = 11/16/13 Pct Recovery = 94% Analysis Date = 11/11/13 Pct Recovery = 94% Analysis Date = 11/11/13 Pct Recovery = 94% Analysis Date = 11/05/13 Pct Recovery = 94% Analysis Date = 11/05/13 Pct Recovery = 94% Analysis Date = 10/30/13 Pct Recovery = 94% Analysis Date = 10/30/13 Pct Recovery = 94% Analysis Date = 10/24/13 Pct Recovery = 94% Analysis Date = 10/24/13 Pct Recovery = 94% Analysis Date = 10/18/13 Pct Recovery = 94% Analysis Date = 10/18/13 Pct Recovery = 94% Analysis Date = 10/12/13 Pct Recovery = 94% Analysis Date = 10/12/13 Pct Recovery = 94% Analysis Date = 10/06/13 Pct Recovery = 94% Analysis Date = 10/06/13 Pct Recovery = 94% Analysis Date = 09/30/13 Pct Recovery = 95% Analysis Date = 09/30/13 Pct Recovery = 95% Analysis Date = 09/25/13 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL-OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 99 81% 14% 81% 13%
Total 99 81% 14% 81% 13%

Sample Statistics
AZINPHOS-METHYL-OXON

Characteristic N % % Basis
Plotted 99 99% Spiked
Estimated Values 10 10% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 101 .  
False Negatives 1 1% 1 out of 100
Not Spiked 77 .  
False Positives 0 0% 0 out of 75