BQS OBSP Determination:
TERBUFOS-O-ANALOGUE SULFONE
METHOD: 2033 , TESTIDCODE: 61674GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 89% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 79% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 85% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 49% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 26% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 38% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 53% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 56% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 57% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 76% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 70% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 51% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 69% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 104% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 107% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 138% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 100% Analysis Date = 04/15/14 Pct Recovery = 37% Analysis Date = 04/09/14 Pct Recovery = 38% Analysis Date = 04/09/14 Pct Recovery = 38% Analysis Date = 04/03/14 Pct Recovery = 40% Analysis Date = 04/03/14 Pct Recovery = 40% Analysis Date = 03/28/14 Pct Recovery = 42% Analysis Date = 03/28/14 Pct Recovery = 42% Analysis Date = 03/23/14 Pct Recovery = 44% Analysis Date = 03/23/14 Pct Recovery = 44% Analysis Date = 03/17/14 Pct Recovery = 46% Analysis Date = 03/17/14 Pct Recovery = 46% Analysis Date = 03/11/14 Pct Recovery = 47% Analysis Date = 03/11/14 Pct Recovery = 47% Analysis Date = 03/06/14 Pct Recovery = 49% Analysis Date = 03/06/14 Pct Recovery = 49% Analysis Date = 02/28/14 Pct Recovery = 51% Analysis Date = 02/28/14 Pct Recovery = 51% Analysis Date = 02/22/14 Pct Recovery = 52% Analysis Date = 02/22/14 Pct Recovery = 52% Analysis Date = 02/17/14 Pct Recovery = 54% Analysis Date = 02/17/14 Pct Recovery = 54% Analysis Date = 02/11/14 Pct Recovery = 56% Analysis Date = 02/11/14 Pct Recovery = 56% Analysis Date = 02/05/14 Pct Recovery = 57% Analysis Date = 02/05/14 Pct Recovery = 57% Analysis Date = 01/31/14 Pct Recovery = 59% Analysis Date = 01/31/14 Pct Recovery = 59% Analysis Date = 01/25/14 Pct Recovery = 60% Analysis Date = 01/25/14 Pct Recovery = 60% Analysis Date = 01/19/14 Pct Recovery = 62% Analysis Date = 01/19/14 Pct Recovery = 62% Analysis Date = 01/14/14 Pct Recovery = 64% Analysis Date = 01/14/14 Pct Recovery = 64% Analysis Date = 01/08/14 Pct Recovery = 65% Analysis Date = 01/08/14 Pct Recovery = 65% Analysis Date = 01/02/14 Pct Recovery = 66% Analysis Date = 01/02/14 Pct Recovery = 66% Analysis Date = 12/27/13 Pct Recovery = 66% Analysis Date = 12/27/13 Pct Recovery = 66% Analysis Date = 12/22/13 Pct Recovery = 66% Analysis Date = 12/22/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/10/13 Pct Recovery = 67% Analysis Date = 12/10/13 Pct Recovery = 67% Analysis Date = 12/05/13 Pct Recovery = 67% Analysis Date = 12/05/13 Pct Recovery = 67% Analysis Date = 11/29/13 Pct Recovery = 67% Analysis Date = 11/29/13 Pct Recovery = 67% Analysis Date = 11/23/13 Pct Recovery = 67% Analysis Date = 11/23/13 Pct Recovery = 67% Analysis Date = 11/18/13 Pct Recovery = 67% Analysis Date = 11/18/13 Pct Recovery = 67% Analysis Date = 11/12/13 Pct Recovery = 67% Analysis Date = 11/12/13 Pct Recovery = 67% Analysis Date = 11/06/13 Pct Recovery = 67% Analysis Date = 11/06/13 Pct Recovery = 67% Analysis Date = 11/01/13 Pct Recovery = 66% Analysis Date = 11/01/13 Pct Recovery = 66% Analysis Date = 10/26/13 Pct Recovery = 66% Analysis Date = 10/26/13 Pct Recovery = 66% Analysis Date = 10/20/13 Pct Recovery = 66% Analysis Date = 10/20/13 Pct Recovery = 66% Analysis Date = 10/15/13 Pct Recovery = 66% Analysis Date = 10/15/13 Pct Recovery = 66% Analysis Date = 10/09/13 Pct Recovery = 65% Analysis Date = 10/09/13 Pct Recovery = 65% Analysis Date = 10/03/13 Pct Recovery = 65% Analysis Date = 10/03/13 Pct Recovery = 65% Analysis Date = 09/28/13 Pct Recovery = 65% Analysis Date = 09/28/13 Pct Recovery = 65% Analysis Date = 09/22/13 Pct Recovery = 65% Analysis Date = 09/22/13 Pct Recovery = 65% Analysis Date = 09/16/13 Pct Recovery = 65% Analysis Date = 09/16/13 Pct Recovery = 65% Analysis Date = 09/10/13 Pct Recovery = 65% Analysis Date = 09/10/13 Pct Recovery = 65% Analysis Date = 09/05/13 Pct Recovery = 66% Analysis Date = 09/05/13 Pct Recovery = 66% Analysis Date = 08/30/13 Pct Recovery = 66% Analysis Date = 08/30/13 Pct Recovery = 66% Analysis Date = 08/24/13 Pct Recovery = 67% Analysis Date = 08/24/13 Pct Recovery = 67% Analysis Date = 08/19/13 Pct Recovery = 68% Analysis Date = 08/19/13 Pct Recovery = 68% Analysis Date = 08/13/13 Pct Recovery = 68% Analysis Date = 08/13/13 Pct Recovery = 68% Analysis Date = 08/07/13 Pct Recovery = 69% Analysis Date = 08/07/13 Pct Recovery = 69% Analysis Date = 08/02/13 Pct Recovery = 69% Analysis Date = 08/02/13 Pct Recovery = 69% Analysis Date = 07/27/13 Pct Recovery = 70% Analysis Date = 07/27/13 Pct Recovery = 70% Analysis Date = 07/21/13 Pct Recovery = 70% Analysis Date = 07/21/13 Pct Recovery = 70% Analysis Date = 07/16/13 Pct Recovery = 71% Analysis Date = 07/16/13 Pct Recovery = 71% Analysis Date = 07/10/13 Pct Recovery = 71% Analysis Date = 07/10/13 Pct Recovery = 71% Analysis Date = 07/04/13 Pct Recovery = 72% Analysis Date = 07/04/13 Pct Recovery = 72% Analysis Date = 06/29/13 Pct Recovery = 73% Analysis Date = 06/29/13 Pct Recovery = 73% Analysis Date = 06/23/13 Pct Recovery = 73% Analysis Date = 06/23/13 Pct Recovery = 73% Analysis Date = 06/17/13 Pct Recovery = 74% Analysis Date = 06/17/13 Pct Recovery = 74% Analysis Date = 06/12/13 Pct Recovery = 74% Analysis Date = 06/12/13 Pct Recovery = 74% Analysis Date = 06/06/13 Pct Recovery = 75% Analysis Date = 06/06/13 Pct Recovery = 75% Analysis Date = 05/31/13 Pct Recovery = 75% Analysis Date = 05/31/13 Pct Recovery = 75% Analysis Date = 05/25/13 Pct Recovery = 76% Analysis Date = 05/25/13 Pct Recovery = 76% Analysis Date = 05/20/13 Pct Recovery = 77% Analysis Date = 05/20/13 Pct Recovery = 77% Analysis Date = 05/14/13 Pct Recovery = 77% Analysis Date = 05/14/13 Pct Recovery = 77% Analysis Date = 05/08/13 Pct Recovery = 78% Analysis Date = 05/08/13 Pct Recovery = 78% Analysis Date = 05/03/13 Pct Recovery = 78% Analysis Date = 05/03/13 Pct Recovery = 78% Analysis Date = 04/27/13 Pct Recovery = 79% Analysis Date = 04/27/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/21/13 Pct Recovery = 79% Analysis Date = 04/16/13 Pct Recovery = 80% Analysis Date = 04/16/13 Pct Recovery = 80% Analysis Date = 04/10/13 Pct Recovery = 81% Analysis Date = 04/10/13 Pct Recovery = 81% Analysis Date = 04/04/13 Pct Recovery = 81% Analysis Date = 04/04/13 Pct Recovery = 81% Analysis Date = 03/30/13 Pct Recovery = 82% Analysis Date = 03/30/13 Pct Recovery = 82% Analysis Date = 03/24/13 Pct Recovery = 82% Analysis Date = 03/24/13 Pct Recovery = 82% Analysis Date = 03/18/13 Pct Recovery = 83% Analysis Date = 03/18/13 Pct Recovery = 83% Analysis Date = 03/13/13 Pct Recovery = 83% Analysis Date = 03/13/13 Pct Recovery = 83% Analysis Date = 03/07/13 Pct Recovery = 84% Analysis Date = 03/07/13 Pct Recovery = 84% Analysis Date = 03/01/13 Pct Recovery = 85% Analysis Date = 03/01/13 Pct Recovery = 85% Analysis Date = 02/23/13 Pct Recovery = 85% Analysis Date = 02/23/13 Pct Recovery = 85% Analysis Date = 02/18/13 Pct Recovery = 86% Analysis Date = 02/18/13 Pct Recovery = 86% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/12/13 Pct Recovery = 87% Analysis Date = 02/06/13 Pct Recovery = 87% Analysis Date = 02/06/13 Pct Recovery = 87% Analysis Date = 02/01/13 Pct Recovery = 88% Analysis Date = 02/01/13 Pct Recovery = 88% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/20/13 Pct Recovery = 90% Analysis Date = 01/20/13 Pct Recovery = 90% Analysis Date = 01/15/13 Pct Recovery = 90% Analysis Date = 01/15/13 Pct Recovery = 90% Analysis Date = 01/09/13 Pct Recovery = 91% Analysis Date = 01/09/13 Pct Recovery = 91% Analysis Date = 01/03/13 Pct Recovery = 92% Analysis Date = 01/03/13 Pct Recovery = 92% Analysis Date = 12/29/12 Pct Recovery = 92% Analysis Date = 12/29/12 Pct Recovery = 92% Analysis Date = 12/23/12 Pct Recovery = 93% Analysis Date = 12/23/12 Pct Recovery = 93% Analysis Date = 12/17/12 Pct Recovery = 94% Analysis Date = 12/17/12 Pct Recovery = 94% Analysis Date = 12/12/12 Pct Recovery = 95% Analysis Date = 12/12/12 Pct Recovery = 95% Analysis Date = 12/06/12 Pct Recovery = 95% Analysis Date = 12/06/12 Pct Recovery = 95% Analysis Date = 11/30/12 Pct Recovery = 96% Analysis Date = 11/30/12 Pct Recovery = 96% Analysis Date = 11/25/12 Pct Recovery = 97% Analysis Date = 11/25/12 Pct Recovery = 97% Analysis Date = 11/19/12 Pct Recovery = 97% Analysis Date = 11/19/12 Pct Recovery = 97% Analysis Date = 11/13/12 Pct Recovery = 98% Analysis Date = 11/13/12 Pct Recovery = 98% Analysis Date = 11/07/12 Pct Recovery = 99% Analysis Date = 11/07/12 Pct Recovery = 99% Analysis Date = 11/02/12 Pct Recovery = 99% Analysis Date = 11/02/12 Pct Recovery = 99% Analysis Date = 10/27/12 Pct Recovery = 100% Analysis Date = 10/27/12 Pct Recovery = 100% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/16/12 Pct Recovery = 102% Analysis Date = 10/16/12 Pct Recovery = 102% Analysis Date = 10/10/12 Pct Recovery = 102% Analysis Date = 10/10/12 Pct Recovery = 102% Analysis Date = 10/04/12 Pct Recovery = 103% Analysis Date = 10/04/12 Pct Recovery = 103% Analysis Date = 09/29/12 Pct Recovery = 104% Analysis Date = 09/29/12 Pct Recovery = 104% Analysis Date = 09/23/12 Pct Recovery = 104% Analysis Date = 09/23/12 Pct Recovery = 104% Analysis Date = 09/17/12 Pct Recovery = 105% Analysis Date = 09/17/12 Pct Recovery = 105% Analysis Date = 09/12/12 Pct Recovery = 105% Analysis Date = 09/12/12 Pct Recovery = 105% Analysis Date = 09/06/12 Pct Recovery = 105% Analysis Date = 09/06/12 Pct Recovery = 105% Analysis Date = 08/31/12 Pct Recovery = 104% Analysis Date = 08/31/12 Pct Recovery = 104% Analysis Date = 08/26/12 Pct Recovery = 104% Analysis Date = 08/26/12 Pct Recovery = 104% Analysis Date = 08/20/12 Pct Recovery = 104% Analysis Date = 08/20/12 Pct Recovery = 104% Analysis Date = 08/14/12 Pct Recovery = 103% Analysis Date = 08/14/12 Pct Recovery = 103% Analysis Date = 08/09/12 Pct Recovery = 103% Analysis Date = 08/09/12 Pct Recovery = 103% Analysis Date = 08/03/12 Pct Recovery = 103% Analysis Date = 08/03/12 Pct Recovery = 103% Analysis Date = 07/28/12 Pct Recovery = 102% Analysis Date = 07/28/12 Pct Recovery = 102% Analysis Date = 07/22/12 Pct Recovery = 102% Analysis Date = 07/22/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/17/12 Pct Recovery = 102% Analysis Date = 07/11/12 Pct Recovery = 101% Analysis Date = 07/11/12 Pct Recovery = 101% Analysis Date = 07/05/12 Pct Recovery = 101% Analysis Date = 07/05/12 Pct Recovery = 101% Analysis Date = 06/30/12 Pct Recovery = 100% Analysis Date = 06/30/12 Pct Recovery = 100% Analysis Date = 06/24/12 Pct Recovery = 100% Analysis Date = 06/24/12 Pct Recovery = 100% Analysis Date = 06/18/12 Pct Recovery = 100% Analysis Date = 06/18/12 Pct Recovery = 100% Analysis Date = 06/13/12 Pct Recovery = 99% Analysis Date = 06/13/12 Pct Recovery = 99% Analysis Date = 06/07/12 Pct Recovery = 99% Analysis Date = 06/07/12 Pct Recovery = 99% Analysis Date = 06/01/12 Pct Recovery = 99% Analysis Date = 06/01/12 Pct Recovery = 99% Analysis Date = 05/27/12 Pct Recovery = 98% Analysis Date = 05/27/12 Pct Recovery = 98% Analysis Date = 05/21/12 Pct Recovery = 98% Analysis Date = 05/21/12 Pct Recovery = 98% Analysis Date = 05/15/12 Pct Recovery = 98% Analysis Date = 05/15/12 Pct Recovery = 98% Analysis Date = 05/10/12 Pct Recovery = 97% Analysis Date = 05/10/12 Pct Recovery = 97% Analysis Date = 05/04/12 Pct Recovery = 97% Analysis Date = 05/04/12 Pct Recovery = 97% Analysis Date = 04/28/12 Pct Recovery = 97% Analysis Date = 04/28/12 Pct Recovery = 97% Analysis Date = 04/23/12 Pct Recovery = 96% Analysis Date = 04/23/12 Pct Recovery = 96% Analysis Date = 04/17/12 Pct Recovery = 96% Analysis Date = 04/17/12 Pct Recovery = 96% Analysis Date = 04/11/12 Pct Recovery = 96% Analysis Date = 04/11/12 Pct Recovery = 96% Analysis Date = 04/05/12 Pct Recovery = 95% Analysis Date = 04/05/12 Pct Recovery = 95% Analysis Date = 03/31/12 Pct Recovery = 95% Analysis Date = 03/31/12 Pct Recovery = 95% Analysis Date = 03/25/12 Pct Recovery = 95% Analysis Date = 03/25/12 Pct Recovery = 95% Analysis Date = 03/19/12 Pct Recovery = 94% Analysis Date = 03/19/12 Pct Recovery = 94% Analysis Date = 03/14/12 Pct Recovery = 94% Analysis Date = 03/14/12 Pct Recovery = 94% Analysis Date = 03/08/12 Pct Recovery = 93% Analysis Date = 03/08/12 Pct Recovery = 93% Analysis Date = 03/02/12 Pct Recovery = 93% Analysis Date = 03/02/12 Pct Recovery = 93% Analysis Date = 02/26/12 Pct Recovery = 93% Analysis Date = 02/26/12 Pct Recovery = 93% Analysis Date = 02/20/12 Pct Recovery = 92% Analysis Date = 02/20/12 Pct Recovery = 92% Analysis Date = 02/14/12 Pct Recovery = 92% Analysis Date = 02/14/12 Pct Recovery = 92% Analysis Date = 02/09/12 Pct Recovery = 92% Analysis Date = 02/09/12 Pct Recovery = 92% Analysis Date = 02/03/12 Pct Recovery = 91% Analysis Date = 02/03/12 Pct Recovery = 91% Analysis Date = 01/28/12 Pct Recovery = 91% Analysis Date = 01/28/12 Pct Recovery = 91% Analysis Date = 01/23/12 Pct Recovery = 91% Analysis Date = 01/23/12 Pct Recovery = 91% Analysis Date = 01/17/12 Pct Recovery = 90% Analysis Date = 01/17/12 Pct Recovery = 90% Analysis Date = 01/11/12 Pct Recovery = 90% Analysis Date = 01/11/12 Pct Recovery = 90% Analysis Date = 01/05/12 Pct Recovery = 90% Analysis Date = 01/05/12 Pct Recovery = 90% Analysis Date = 12/31/11 Pct Recovery = 89% Analysis Date = 12/31/11 Pct Recovery = 89% Analysis Date = 12/25/11 Pct Recovery = 89% Analysis Date = 12/25/11 Pct Recovery = 89% Analysis Date = 12/19/11 Pct Recovery = 89% Analysis Date = 12/19/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 88% Analysis Date = 12/14/11 Pct Recovery = 88% Analysis Date = 12/08/11 Pct Recovery = 88% Analysis Date = 12/08/11 Pct Recovery = 88% Analysis Date = 12/02/11 Pct Recovery = 88% Analysis Date = 12/02/11 Pct Recovery = 88% Analysis Date = 11/27/11 Pct Recovery = 87% Analysis Date = 11/27/11 Pct Recovery = 87% Analysis Date = 11/21/11 Pct Recovery = 87% Analysis Date = 11/21/11 Pct Recovery = 87% Analysis Date = 11/15/11 Pct Recovery = 87% Analysis Date = 11/15/11 Pct Recovery = 87% Analysis Date = 11/10/11 Pct Recovery = 86% Analysis Date = 11/10/11 Pct Recovery = 86% Analysis Date = 11/04/11 Pct Recovery = 86% Analysis Date = 11/04/11 Pct Recovery = 86% Analysis Date = 10/29/11 Pct Recovery = 85% Analysis Date = 10/29/11 Pct Recovery = 85% Analysis Date = 10/24/11 Pct Recovery = 85% Analysis Date = 10/24/11 Pct Recovery = 85% Analysis Date = 10/18/11 Pct Recovery = 85% Analysis Date = 10/18/11 Pct Recovery = 85% Analysis Date = 10/12/11 Pct Recovery = 84% Analysis Date = 10/12/11 Pct Recovery = 84% Analysis Date = 10/07/11 Pct Recovery = 84% Analysis Date = 10/07/11 Pct Recovery = 84% Analysis Date = 10/01/11 Pct Recovery = 84% Analysis Date = 10/01/11 Pct Recovery = 84% Analysis Date = 09/25/11 Pct Recovery = 83% Analysis Date = 09/25/11 Pct Recovery = 83% Analysis Date = 09/19/11 Pct Recovery = 83% Analysis Date = 09/19/11 Pct Recovery = 83% Analysis Date = 09/14/11 Pct Recovery = 83% Analysis Date = 09/14/11 Pct Recovery = 83% Analysis Date = 09/08/11 Pct Recovery = 82% Analysis Date = 09/08/11 Pct Recovery = 82% Analysis Date = 09/02/11 Pct Recovery = 82% Analysis Date = 09/02/11 Pct Recovery = 82% Analysis Date = 08/28/11 Pct Recovery = 82% Analysis Date = 08/28/11 Pct Recovery = 82% Analysis Date = 08/22/11 Pct Recovery = 81% Analysis Date = 08/22/11 Pct Recovery = 81% Analysis Date = 08/16/11 Pct Recovery = 81% Analysis Date = 08/16/11 Pct Recovery = 81% Analysis Date = 08/11/11 Pct Recovery = 81% Analysis Date = 08/11/11 Pct Recovery = 81% Analysis Date = 08/05/11 Pct Recovery = 80% Analysis Date = 08/05/11 Pct Recovery = 80% Analysis Date = 07/30/11 Pct Recovery = 80% Analysis Date = 07/30/11 Pct Recovery = 80% Analysis Date = 07/25/11 Pct Recovery = 80% Analysis Date = 07/25/11 Pct Recovery = 80% Analysis Date = 07/19/11 Pct Recovery = 79% Analysis Date = 07/19/11 Pct Recovery = 79% Analysis Date = 07/13/11 Pct Recovery = 79% Analysis Date = 07/13/11 Pct Recovery = 79% Analysis Date = 07/08/11 Pct Recovery = 78% Analysis Date = 07/08/11 Pct Recovery = 78% Analysis Date = 07/02/11 Pct Recovery = 78% Analysis Date = 07/02/11 Pct Recovery = 78% Analysis Date = 06/26/11 Pct Recovery = 78% Analysis Date = 06/26/11 Pct Recovery = 78% Analysis Date = 06/21/11 Pct Recovery = 77% Analysis Date = 06/21/11 Pct Recovery = 77% Analysis Date = 06/15/11 Pct Recovery = 77% Analysis Date = 06/15/11 Pct Recovery = 77% Analysis Date = 06/09/11 Pct Recovery = 77% Analysis Date = 06/09/11 Pct Recovery = 77% Analysis Date = 06/03/11 Pct Recovery = 77% Analysis Date = 06/03/11 Pct Recovery = 77% Analysis Date = 05/29/11 Pct Recovery = 77% Analysis Date = 05/29/11 Pct Recovery = 77% Analysis Date = 05/23/11 Pct Recovery = 76% Analysis Date = 05/23/11 Pct Recovery = 76% Analysis Date = 05/17/11 Pct Recovery = 76% Analysis Date = 05/17/11 Pct Recovery = 76% Analysis Date = 05/12/11 Pct Recovery = 76% Analysis Date = 05/12/11 Pct Recovery = 76% Analysis Date = 05/06/11 Pct Recovery = 76% Analysis Date = 05/06/11 Pct Recovery = 76% Analysis Date = 04/30/11 Pct Recovery = 75% Analysis Date = 04/30/11 Pct Recovery = 75% Analysis Date = 04/25/11 Pct Recovery = 75% Analysis Date = 04/25/11 Pct Recovery = 75% Analysis Date = 04/19/11 Pct Recovery = 75% Analysis Date = 04/19/11 Pct Recovery = 75% Analysis Date = 04/13/11 Pct Recovery = 75% Analysis Date = 04/13/11 Pct Recovery = 75% Analysis Date = 04/08/11 Pct Recovery = 75% Analysis Date = 04/08/11 Pct Recovery = 75% Analysis Date = 04/02/11 Pct Recovery = 74% Analysis Date = 04/02/11 Pct Recovery = 74% Analysis Date = 03/27/11 Pct Recovery = 74% Analysis Date = 03/27/11 Pct Recovery = 74% Analysis Date = 03/22/11 Pct Recovery = 74% Analysis Date = 03/22/11 Pct Recovery = 74% Analysis Date = 03/16/11 Pct Recovery = 74% Analysis Date = 03/16/11 Pct Recovery = 74% Analysis Date = 03/10/11 Pct Recovery = 73% Analysis Date = 03/10/11 Pct Recovery = 73% Analysis Date = 03/05/11 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS-O-ANALOGUE SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 112% 17% 105% 15%
>= Reporting Level 19 64% 17% 64% 19%
Total 23 73% 25% 69% 25%

Sample Statistics
TERBUFOS-O-ANALOGUE SULFONE

Characteristic N % % Basis
Plotted 23 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 23 .  
False Negatives 0 0% 0 out of 23
Not Spiked 139 .  
False Positives 0 0% 0 out of 139