BQS OBSP Determination:
PHOSMET OXON
METHOD: 2033 , TESTIDCODE: 61668GCM39
Open Data Set

Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 390% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 267% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 62% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 97% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 74% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 87% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 35% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 69% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 31% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 31% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 29% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 56% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 56% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 52% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 101% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 166% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 61% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 63% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 56% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 76% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 37% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 71% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 67% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 29% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 87% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 92% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 35% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 42% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 106% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 95% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 94% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 93% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 50% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 65% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 83% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 70% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 87% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 46% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 80% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 66% Analysis Date = 09/26/12 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 52% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 90% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 78% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 121% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 142% Analysis Date = 01/17/17 Pct Recovery = 76% Analysis Date = 01/09/17 Pct Recovery = 76% Analysis Date = 01/09/17 Pct Recovery = 76% Analysis Date = 01/01/17 Pct Recovery = 76% Analysis Date = 01/01/17 Pct Recovery = 76% Analysis Date = 12/23/16 Pct Recovery = 76% Analysis Date = 12/23/16 Pct Recovery = 76% Analysis Date = 12/15/16 Pct Recovery = 75% Analysis Date = 12/15/16 Pct Recovery = 75% Analysis Date = 12/07/16 Pct Recovery = 75% Analysis Date = 12/07/16 Pct Recovery = 75% Analysis Date = 11/28/16 Pct Recovery = 75% Analysis Date = 11/28/16 Pct Recovery = 75% Analysis Date = 11/20/16 Pct Recovery = 75% Analysis Date = 11/20/16 Pct Recovery = 75% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 11/03/16 Pct Recovery = 74% Analysis Date = 10/26/16 Pct Recovery = 74% Analysis Date = 10/26/16 Pct Recovery = 74% Analysis Date = 10/17/16 Pct Recovery = 74% Analysis Date = 10/17/16 Pct Recovery = 74% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 10/09/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/30/16 Pct Recovery = 73% Analysis Date = 09/22/16 Pct Recovery = 73% Analysis Date = 09/22/16 Pct Recovery = 73% Analysis Date = 09/14/16 Pct Recovery = 73% Analysis Date = 09/14/16 Pct Recovery = 73% Analysis Date = 09/05/16 Pct Recovery = 72% Analysis Date = 09/05/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/11/16 Pct Recovery = 72% Analysis Date = 08/11/16 Pct Recovery = 72% Analysis Date = 08/03/16 Pct Recovery = 72% Analysis Date = 08/03/16 Pct Recovery = 72% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/25/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/09/16 Pct Recovery = 71% Analysis Date = 07/09/16 Pct Recovery = 71% Analysis Date = 06/30/16 Pct Recovery = 71% Analysis Date = 06/30/16 Pct Recovery = 71% Analysis Date = 06/22/16 Pct Recovery = 70% Analysis Date = 06/22/16 Pct Recovery = 70% Analysis Date = 06/13/16 Pct Recovery = 70% Analysis Date = 06/13/16 Pct Recovery = 70% Analysis Date = 06/05/16 Pct Recovery = 70% Analysis Date = 06/05/16 Pct Recovery = 70% Analysis Date = 05/28/16 Pct Recovery = 70% Analysis Date = 05/28/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/19/16 Pct Recovery = 69% Analysis Date = 05/11/16 Pct Recovery = 69% Analysis Date = 05/11/16 Pct Recovery = 69% Analysis Date = 05/03/16 Pct Recovery = 69% Analysis Date = 05/03/16 Pct Recovery = 69% Analysis Date = 04/24/16 Pct Recovery = 69% Analysis Date = 04/24/16 Pct Recovery = 69% Analysis Date = 04/16/16 Pct Recovery = 68% Analysis Date = 04/16/16 Pct Recovery = 68% Analysis Date = 04/07/16 Pct Recovery = 68% Analysis Date = 04/07/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/22/16 Pct Recovery = 68% Analysis Date = 03/22/16 Pct Recovery = 68% Analysis Date = 03/13/16 Pct Recovery = 68% Analysis Date = 03/13/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 02/25/16 Pct Recovery = 67% Analysis Date = 02/25/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/09/16 Pct Recovery = 67% Analysis Date = 02/09/16 Pct Recovery = 67% Analysis Date = 01/31/16 Pct Recovery = 66% Analysis Date = 01/31/16 Pct Recovery = 66% Analysis Date = 01/23/16 Pct Recovery = 66% Analysis Date = 01/23/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/15/16 Pct Recovery = 66% Analysis Date = 01/06/16 Pct Recovery = 66% Analysis Date = 01/06/16 Pct Recovery = 66% Analysis Date = 12/29/15 Pct Recovery = 65% Analysis Date = 12/29/15 Pct Recovery = 65% Analysis Date = 12/20/15 Pct Recovery = 65% Analysis Date = 12/20/15 Pct Recovery = 65% Analysis Date = 12/12/15 Pct Recovery = 65% Analysis Date = 12/12/15 Pct Recovery = 65% Analysis Date = 12/04/15 Pct Recovery = 65% Analysis Date = 12/04/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/25/15 Pct Recovery = 65% Analysis Date = 11/17/15 Pct Recovery = 64% Analysis Date = 11/17/15 Pct Recovery = 64% Analysis Date = 11/08/15 Pct Recovery = 64% Analysis Date = 11/08/15 Pct Recovery = 64% Analysis Date = 10/31/15 Pct Recovery = 64% Analysis Date = 10/31/15 Pct Recovery = 64% Analysis Date = 10/23/15 Pct Recovery = 64% Analysis Date = 10/23/15 Pct Recovery = 64% Analysis Date = 10/14/15 Pct Recovery = 63% Analysis Date = 10/14/15 Pct Recovery = 63% Analysis Date = 10/06/15 Pct Recovery = 63% Analysis Date = 10/06/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/28/15 Pct Recovery = 63% Analysis Date = 09/19/15 Pct Recovery = 63% Analysis Date = 09/19/15 Pct Recovery = 63% Analysis Date = 09/11/15 Pct Recovery = 62% Analysis Date = 09/11/15 Pct Recovery = 62% Analysis Date = 09/02/15 Pct Recovery = 62% Analysis Date = 09/02/15 Pct Recovery = 62% Analysis Date = 08/25/15 Pct Recovery = 62% Analysis Date = 08/25/15 Pct Recovery = 62% Analysis Date = 08/17/15 Pct Recovery = 62% Analysis Date = 08/17/15 Pct Recovery = 62% Analysis Date = 08/08/15 Pct Recovery = 62% Analysis Date = 08/08/15 Pct Recovery = 62% Analysis Date = 07/31/15 Pct Recovery = 61% Analysis Date = 07/31/15 Pct Recovery = 61% Analysis Date = 07/22/15 Pct Recovery = 61% Analysis Date = 07/22/15 Pct Recovery = 61% Analysis Date = 07/14/15 Pct Recovery = 61% Analysis Date = 07/14/15 Pct Recovery = 61% Analysis Date = 07/06/15 Pct Recovery = 61% Analysis Date = 07/06/15 Pct Recovery = 61% Analysis Date = 06/27/15 Pct Recovery = 61% Analysis Date = 06/27/15 Pct Recovery = 61% Analysis Date = 06/19/15 Pct Recovery = 60% Analysis Date = 06/19/15 Pct Recovery = 60% Analysis Date = 06/11/15 Pct Recovery = 60% Analysis Date = 06/11/15 Pct Recovery = 60% Analysis Date = 06/02/15 Pct Recovery = 60% Analysis Date = 06/02/15 Pct Recovery = 60% Analysis Date = 05/25/15 Pct Recovery = 60% Analysis Date = 05/25/15 Pct Recovery = 60% Analysis Date = 05/16/15 Pct Recovery = 60% Analysis Date = 05/16/15 Pct Recovery = 60% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 05/08/15 Pct Recovery = 59% Analysis Date = 04/30/15 Pct Recovery = 59% Analysis Date = 04/30/15 Pct Recovery = 59% Analysis Date = 04/21/15 Pct Recovery = 59% Analysis Date = 04/21/15 Pct Recovery = 59% Analysis Date = 04/13/15 Pct Recovery = 59% Analysis Date = 04/13/15 Pct Recovery = 59% Analysis Date = 04/04/15 Pct Recovery = 59% Analysis Date = 04/04/15 Pct Recovery = 59% Analysis Date = 03/27/15 Pct Recovery = 59% Analysis Date = 03/27/15 Pct Recovery = 59% Analysis Date = 03/19/15 Pct Recovery = 58% Analysis Date = 03/19/15 Pct Recovery = 58% Analysis Date = 03/10/15 Pct Recovery = 58% Analysis Date = 03/10/15 Pct Recovery = 58% Analysis Date = 03/02/15 Pct Recovery = 58% Analysis Date = 03/02/15 Pct Recovery = 58% Analysis Date = 02/22/15 Pct Recovery = 58% Analysis Date = 02/22/15 Pct Recovery = 58% Analysis Date = 02/13/15 Pct Recovery = 58% Analysis Date = 02/13/15 Pct Recovery = 58% Analysis Date = 02/05/15 Pct Recovery = 58% Analysis Date = 02/05/15 Pct Recovery = 58% Analysis Date = 01/27/15 Pct Recovery = 58% Analysis Date = 01/27/15 Pct Recovery = 58% Analysis Date = 01/19/15 Pct Recovery = 58% Analysis Date = 01/19/15 Pct Recovery = 58% Analysis Date = 01/11/15 Pct Recovery = 58% Analysis Date = 01/11/15 Pct Recovery = 58% Analysis Date = 01/02/15 Pct Recovery = 58% Analysis Date = 01/02/15 Pct Recovery = 58% Analysis Date = 12/25/14 Pct Recovery = 58% Analysis Date = 12/25/14 Pct Recovery = 58% Analysis Date = 12/16/14 Pct Recovery = 57% Analysis Date = 12/16/14 Pct Recovery = 57% Analysis Date = 12/08/14 Pct Recovery = 57% Analysis Date = 12/08/14 Pct Recovery = 57% Analysis Date = 11/30/14 Pct Recovery = 57% Analysis Date = 11/30/14 Pct Recovery = 57% Analysis Date = 11/21/14 Pct Recovery = 57% Analysis Date = 11/21/14 Pct Recovery = 57% Analysis Date = 11/13/14 Pct Recovery = 57% Analysis Date = 11/13/14 Pct Recovery = 57% Analysis Date = 11/05/14 Pct Recovery = 57% Analysis Date = 11/05/14 Pct Recovery = 57% Analysis Date = 10/27/14 Pct Recovery = 57% Analysis Date = 10/27/14 Pct Recovery = 57% Analysis Date = 10/19/14 Pct Recovery = 57% Analysis Date = 10/19/14 Pct Recovery = 57% Analysis Date = 10/10/14 Pct Recovery = 57% Analysis Date = 10/10/14 Pct Recovery = 57% Analysis Date = 10/02/14 Pct Recovery = 57% Analysis Date = 10/02/14 Pct Recovery = 57% Analysis Date = 09/24/14 Pct Recovery = 57% Analysis Date = 09/24/14 Pct Recovery = 57% Analysis Date = 09/15/14 Pct Recovery = 57% Analysis Date = 09/15/14 Pct Recovery = 57% Analysis Date = 09/07/14 Pct Recovery = 56% Analysis Date = 09/07/14 Pct Recovery = 56% Analysis Date = 08/29/14 Pct Recovery = 56% Analysis Date = 08/29/14 Pct Recovery = 56% Analysis Date = 08/21/14 Pct Recovery = 56% Analysis Date = 08/21/14 Pct Recovery = 56% Analysis Date = 08/13/14 Pct Recovery = 56% Analysis Date = 08/13/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 08/04/14 Pct Recovery = 56% Analysis Date = 07/27/14 Pct Recovery = 56% Analysis Date = 07/27/14 Pct Recovery = 56% Analysis Date = 07/19/14 Pct Recovery = 56% Analysis Date = 07/19/14 Pct Recovery = 56% Analysis Date = 07/10/14 Pct Recovery = 56% Analysis Date = 07/10/14 Pct Recovery = 56% Analysis Date = 07/02/14 Pct Recovery = 56% Analysis Date = 07/02/14 Pct Recovery = 56% Analysis Date = 06/23/14 Pct Recovery = 56% Analysis Date = 06/23/14 Pct Recovery = 56% Analysis Date = 06/15/14 Pct Recovery = 56% Analysis Date = 06/15/14 Pct Recovery = 56% Analysis Date = 06/07/14 Pct Recovery = 56% Analysis Date = 06/07/14 Pct Recovery = 56% Analysis Date = 05/29/14 Pct Recovery = 57% Analysis Date = 05/29/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/21/14 Pct Recovery = 57% Analysis Date = 05/12/14 Pct Recovery = 57% Analysis Date = 05/12/14 Pct Recovery = 57% Analysis Date = 05/04/14 Pct Recovery = 58% Analysis Date = 05/04/14 Pct Recovery = 58% Analysis Date = 04/26/14 Pct Recovery = 58% Analysis Date = 04/26/14 Pct Recovery = 58% Analysis Date = 04/17/14 Pct Recovery = 58% Analysis Date = 04/17/14 Pct Recovery = 58% Analysis Date = 04/09/14 Pct Recovery = 59% Analysis Date = 04/09/14 Pct Recovery = 59% Analysis Date = 04/01/14 Pct Recovery = 59% Analysis Date = 04/01/14 Pct Recovery = 59% Analysis Date = 03/23/14 Pct Recovery = 60% Analysis Date = 03/23/14 Pct Recovery = 60% Analysis Date = 03/15/14 Pct Recovery = 60% Analysis Date = 03/15/14 Pct Recovery = 60% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 03/06/14 Pct Recovery = 61% Analysis Date = 02/26/14 Pct Recovery = 61% Analysis Date = 02/26/14 Pct Recovery = 61% Analysis Date = 02/18/14 Pct Recovery = 62% Analysis Date = 02/18/14 Pct Recovery = 62% Analysis Date = 02/09/14 Pct Recovery = 62% Analysis Date = 02/09/14 Pct Recovery = 62% Analysis Date = 02/01/14 Pct Recovery = 63% Analysis Date = 02/01/14 Pct Recovery = 63% Analysis Date = 01/23/14 Pct Recovery = 63% Analysis Date = 01/23/14 Pct Recovery = 63% Analysis Date = 01/15/14 Pct Recovery = 64% Analysis Date = 01/15/14 Pct Recovery = 64% Analysis Date = 01/07/14 Pct Recovery = 64% Analysis Date = 01/07/14 Pct Recovery = 64% Analysis Date = 12/29/13 Pct Recovery = 65% Analysis Date = 12/29/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/21/13 Pct Recovery = 65% Analysis Date = 12/13/13 Pct Recovery = 66% Analysis Date = 12/13/13 Pct Recovery = 66% Analysis Date = 12/04/13 Pct Recovery = 66% Analysis Date = 12/04/13 Pct Recovery = 66% Analysis Date = 11/26/13 Pct Recovery = 67% Analysis Date = 11/26/13 Pct Recovery = 67% Analysis Date = 11/17/13 Pct Recovery = 67% Analysis Date = 11/17/13 Pct Recovery = 67% Analysis Date = 11/09/13 Pct Recovery = 68% Analysis Date = 11/09/13 Pct Recovery = 68% Analysis Date = 11/01/13 Pct Recovery = 68% Analysis Date = 11/01/13 Pct Recovery = 68% Analysis Date = 10/23/13 Pct Recovery = 69% Analysis Date = 10/23/13 Pct Recovery = 69% Analysis Date = 10/15/13 Pct Recovery = 69% Analysis Date = 10/15/13 Pct Recovery = 69% Analysis Date = 10/06/13 Pct Recovery = 70% Analysis Date = 10/06/13 Pct Recovery = 70% Analysis Date = 09/28/13 Pct Recovery = 70% Analysis Date = 09/28/13 Pct Recovery = 70% Analysis Date = 09/20/13 Pct Recovery = 71% Analysis Date = 09/20/13 Pct Recovery = 71% Analysis Date = 09/11/13 Pct Recovery = 71% Analysis Date = 09/11/13 Pct Recovery = 71% Analysis Date = 09/03/13 Pct Recovery = 72% Analysis Date = 09/03/13 Pct Recovery = 72% Analysis Date = 08/26/13 Pct Recovery = 72% Analysis Date = 08/26/13 Pct Recovery = 72% Analysis Date = 08/17/13 Pct Recovery = 73% Analysis Date = 08/17/13 Pct Recovery = 73% Analysis Date = 08/09/13 Pct Recovery = 74% Analysis Date = 08/09/13 Pct Recovery = 74% Analysis Date = 07/31/13 Pct Recovery = 75% Analysis Date = 07/31/13 Pct Recovery = 75% Analysis Date = 07/23/13 Pct Recovery = 76% Analysis Date = 07/23/13 Pct Recovery = 76% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/15/13 Pct Recovery = 77% Analysis Date = 07/06/13 Pct Recovery = 78% Analysis Date = 07/06/13 Pct Recovery = 78% Analysis Date = 06/28/13 Pct Recovery = 79% Analysis Date = 06/28/13 Pct Recovery = 79% Analysis Date = 06/19/13 Pct Recovery = 80% Analysis Date = 06/19/13 Pct Recovery = 80% Analysis Date = 06/11/13 Pct Recovery = 82% Analysis Date = 06/11/13 Pct Recovery = 82% Analysis Date = 06/03/13 Pct Recovery = 83% Analysis Date = 06/03/13 Pct Recovery = 83% Analysis Date = 05/25/13 Pct Recovery = 84% Analysis Date = 05/25/13 Pct Recovery = 84% Analysis Date = 05/17/13 Pct Recovery = 86% Analysis Date = 05/17/13 Pct Recovery = 86% Analysis Date = 05/09/13 Pct Recovery = 88% Analysis Date = 05/09/13 Pct Recovery = 88% Analysis Date = 04/30/13 Pct Recovery = 91% Analysis Date = 04/30/13 Pct Recovery = 91% Analysis Date = 04/22/13 Pct Recovery = 93% Analysis Date = 04/22/13 Pct Recovery = 93% Analysis Date = 04/13/13 Pct Recovery = 96% Analysis Date = 04/13/13 Pct Recovery = 96% Analysis Date = 04/05/13 Pct Recovery = 99% Analysis Date = 04/05/13 Pct Recovery = 99% Analysis Date = 03/28/13 Pct Recovery = 101% Analysis Date = 03/28/13 Pct Recovery = 101% Analysis Date = 03/19/13 Pct Recovery = 104% Analysis Date = 03/19/13 Pct Recovery = 104% Analysis Date = 03/11/13 Pct Recovery = 106% Analysis Date = 03/11/13 Pct Recovery = 106% Analysis Date = 03/02/13 Pct Recovery = 109% Analysis Date = 03/02/13 Pct Recovery = 109% Analysis Date = 02/22/13 Pct Recovery = 112% Analysis Date = 02/22/13 Pct Recovery = 112% Analysis Date = 02/14/13 Pct Recovery = 114% Analysis Date = 02/14/13 Pct Recovery = 114% Analysis Date = 02/05/13 Pct Recovery = 117% Analysis Date = 02/05/13 Pct Recovery = 117% Analysis Date = 01/28/13 Pct Recovery = 120% Analysis Date = 01/28/13 Pct Recovery = 120% Analysis Date = 01/20/13 Pct Recovery = 122% Analysis Date = 01/20/13 Pct Recovery = 122% Analysis Date = 01/11/13 Pct Recovery = 125% Analysis Date = 01/11/13 Pct Recovery = 125% Analysis Date = 01/03/13 Pct Recovery = 128% Analysis Date = 01/03/13 Pct Recovery = 128% Analysis Date = 12/25/12 Pct Recovery = 130% Analysis Date = 12/25/12 Pct Recovery = 130% Analysis Date = 12/17/12 Pct Recovery = 133% Analysis Date = 12/17/12 Pct Recovery = 133% Analysis Date = 12/09/12 Pct Recovery = 136% Analysis Date = 12/09/12 Pct Recovery = 136% Analysis Date = 11/30/12 Pct Recovery = 138% Analysis Date = 11/30/12 Pct Recovery = 138% Analysis Date = 11/22/12 Pct Recovery = 141% Analysis Date = 11/22/12 Pct Recovery = 141% Analysis Date = 11/13/12 Pct Recovery = 144% Analysis Date = 11/13/12 Pct Recovery = 144% Analysis Date = 11/05/12 Pct Recovery = 147% Analysis Date = 11/05/12 Pct Recovery = 147% Analysis Date = 10/28/12 Pct Recovery = 149% Analysis Date = 10/28/12 Pct Recovery = 149% Analysis Date = 10/19/12 Pct Recovery = 152% Analysis Date = 10/19/12 Pct Recovery = 152% Analysis Date = 10/11/12 Pct Recovery = 155% Analysis Date = 10/11/12 Pct Recovery = 155% Analysis Date = 10/03/12 Pct Recovery = 157% Analysis Date = 10/03/12 Pct Recovery = 157% Analysis Date = 09/24/12 Pct Recovery = 160% Analysis Date = 09/24/12 Pct Recovery = 160% Analysis Date = 09/16/12 Pct Recovery = 163% Analysis Date = 09/16/12 Pct Recovery = 163% Analysis Date = 09/07/12 Pct Recovery = 166% Analysis Date = 09/07/12 Pct Recovery = 166% Analysis Date = 08/30/12 Pct Recovery = 169% Analysis Date = 08/30/12 Pct Recovery = 169% Analysis Date = 08/22/12 Pct Recovery = 172% Analysis Date = 08/22/12 Pct Recovery = 172% Analysis Date = 08/13/12 Pct Recovery = 175% Analysis Date = 08/13/12 Pct Recovery = 175% Analysis Date = 08/05/12 Pct Recovery = 178% Analysis Date = 08/05/12 Pct Recovery = 178% Analysis Date = 07/27/12 Pct Recovery = 181% Analysis Date = 07/27/12 Pct Recovery = 181% Analysis Date = 07/19/12 Pct Recovery = 184% Analysis Date = 07/19/12 Pct Recovery = 184% Analysis Date = 07/11/12 Pct Recovery = 187% Analysis Date = 07/11/12 Pct Recovery = 187% Analysis Date = 07/02/12 Pct Recovery = 190% Analysis Date = 07/02/12 Pct Recovery = 190% Analysis Date = 06/24/12 Pct Recovery = 193% Analysis Date = 06/24/12 Pct Recovery = 193% Analysis Date = 06/16/12 Pct Recovery = 196% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 80% 56% 70% 23%
Total 56 80% 56% 70% 23%

Sample Statistics
PHOSMET OXON

Characteristic N % % Basis
Plotted 56 93% Spiked
Estimated Values 56 93% Spiked
Deleted Values 9 5% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 64 .  
False Negatives 3 5% 3 out of 60
Not Spiked 105 .  
False Positives 3 3% 3 out of 100