BQS OBSP Determination:
METHIDATHION (SUPRACIDE)
METHOD: 2033 , TESTIDCODE: 61598GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 73% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 79% Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 83% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 83% Analysis Date = 05/29/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 74% Analysis Date = 04/24/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 02/09/12 SpikeMix = Abs 080610: 80 µl Pct Recovery = 91% Analysis Date = 03/16/11 SpikeMix = Abs 080610: 80 µl Pct Recovery = 102% Analysis Date = 03/02/12 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 79% Analysis Date = 12/08/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 68% Analysis Date = 08/30/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 76% Analysis Date = 05/21/11 SpikeMix = Accu 210061341: 80 µl Pct Recovery = 86% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 71% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 97% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 85% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 79% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 76% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 85% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 116% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 77% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 76% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 94% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 93% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 85% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 105% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 90% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 104% Analysis Date = 04/12/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 91% Analysis Date = 03/08/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 78% Analysis Date = 01/20/12 SpikeMix = Abs 080610: 40 µl Pct Recovery = 81% Analysis Date = 10/20/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 90% Analysis Date = 08/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 119% Analysis Date = 05/03/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 105% Analysis Date = 02/22/11 SpikeMix = Abs 080610: 40 µl Pct Recovery = 84% Analysis Date = 04/07/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 88% Analysis Date = 03/27/12 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 79% Analysis Date = 11/05/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 85% Analysis Date = 07/20/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 99% Analysis Date = 07/02/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 127% Analysis Date = 02/14/11 SpikeMix = Accu 210061341: 40 µl Pct Recovery = 72% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 59% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 95% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 102% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 84% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 99% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 107% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 105% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 95% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 81% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 103% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 104% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 125% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 99% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 94% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 85% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 87% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 136% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 98% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 90% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 97% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 128% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 89% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 103% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 102% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 68% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 73% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 114% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 127% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 72% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 190% Analysis Date = 01/18/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 87% Analysis Date = 12/16/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 12/05/16 Pct Recovery = 87% Analysis Date = 11/24/16 Pct Recovery = 87% Analysis Date = 11/24/16 Pct Recovery = 87% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/14/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 11/03/16 Pct Recovery = 88% Analysis Date = 10/23/16 Pct Recovery = 88% Analysis Date = 10/23/16 Pct Recovery = 88% Analysis Date = 10/12/16 Pct Recovery = 88% Analysis Date = 10/12/16 Pct Recovery = 88% Analysis Date = 10/01/16 Pct Recovery = 88% Analysis Date = 10/01/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/19/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 08/08/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/28/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 07/07/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/26/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/14/16 Pct Recovery = 90% Analysis Date = 05/14/16 Pct Recovery = 90% Analysis Date = 05/03/16 Pct Recovery = 90% Analysis Date = 05/03/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/22/16 Pct Recovery = 90% Analysis Date = 04/11/16 Pct Recovery = 90% Analysis Date = 04/11/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/31/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 91% Analysis Date = 03/10/16 Pct Recovery = 91% Analysis Date = 02/28/16 Pct Recovery = 91% Analysis Date = 02/28/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 91% Analysis Date = 02/06/16 Pct Recovery = 91% Analysis Date = 02/06/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/26/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/15/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 01/05/16 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 91% Analysis Date = 12/25/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/14/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 12/03/15 Pct Recovery = 91% Analysis Date = 11/22/15 Pct Recovery = 92% Analysis Date = 11/22/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/12/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 11/01/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/21/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 10/10/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/29/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/18/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 09/08/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/28/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/17/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 08/06/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/26/15 Pct Recovery = 92% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/15/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 07/05/15 Pct Recovery = 93% Analysis Date = 06/24/15 Pct Recovery = 93% Analysis Date = 06/24/15 Pct Recovery = 93% Analysis Date = 06/13/15 Pct Recovery = 93% Analysis Date = 06/13/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 06/02/15 Pct Recovery = 93% Analysis Date = 05/22/15 Pct Recovery = 93% Analysis Date = 05/22/15 Pct Recovery = 93% Analysis Date = 05/11/15 Pct Recovery = 93% Analysis Date = 05/11/15 Pct Recovery = 93% Analysis Date = 05/01/15 Pct Recovery = 93% Analysis Date = 05/01/15 Pct Recovery = 93% Analysis Date = 04/20/15 Pct Recovery = 94% Analysis Date = 04/20/15 Pct Recovery = 94% Analysis Date = 04/09/15 Pct Recovery = 94% Analysis Date = 04/09/15 Pct Recovery = 94% Analysis Date = 03/29/15 Pct Recovery = 94% Analysis Date = 03/29/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/18/15 Pct Recovery = 94% Analysis Date = 03/08/15 Pct Recovery = 94% Analysis Date = 03/08/15 Pct Recovery = 94% Analysis Date = 02/25/15 Pct Recovery = 94% Analysis Date = 02/25/15 Pct Recovery = 94% Analysis Date = 02/14/15 Pct Recovery = 94% Analysis Date = 02/14/15 Pct Recovery = 94% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 02/03/15 Pct Recovery = 95% Analysis Date = 01/23/15 Pct Recovery = 95% Analysis Date = 01/23/15 Pct Recovery = 95% Analysis Date = 01/12/15 Pct Recovery = 95% Analysis Date = 01/12/15 Pct Recovery = 95% Analysis Date = 01/02/15 Pct Recovery = 95% Analysis Date = 01/02/15 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/22/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 12/11/14 Pct Recovery = 95% Analysis Date = 11/30/14 Pct Recovery = 96% Analysis Date = 11/30/14 Pct Recovery = 96% Analysis Date = 11/19/14 Pct Recovery = 96% Analysis Date = 11/19/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 11/08/14 Pct Recovery = 96% Analysis Date = 10/29/14 Pct Recovery = 96% Analysis Date = 10/29/14 Pct Recovery = 96% Analysis Date = 10/18/14 Pct Recovery = 96% Analysis Date = 10/18/14 Pct Recovery = 96% Analysis Date = 10/07/14 Pct Recovery = 96% Analysis Date = 10/07/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/26/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/15/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 09/05/14 Pct Recovery = 96% Analysis Date = 08/25/14 Pct Recovery = 96% Analysis Date = 08/25/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/14/14 Pct Recovery = 96% Analysis Date = 08/03/14 Pct Recovery = 96% Analysis Date = 08/03/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/23/14 Pct Recovery = 96% Analysis Date = 07/12/14 Pct Recovery = 96% Analysis Date = 07/12/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 07/02/14 Pct Recovery = 96% Analysis Date = 06/21/14 Pct Recovery = 96% Analysis Date = 06/21/14 Pct Recovery = 96% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 06/10/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/30/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 95% Analysis Date = 05/19/14 Pct Recovery = 95% Analysis Date = 05/08/14 Pct Recovery = 94% Analysis Date = 05/08/14 Pct Recovery = 94% Analysis Date = 04/28/14 Pct Recovery = 94% Analysis Date = 04/28/14 Pct Recovery = 94% Analysis Date = 04/17/14 Pct Recovery = 94% Analysis Date = 04/17/14 Pct Recovery = 94% Analysis Date = 04/06/14 Pct Recovery = 94% Analysis Date = 04/06/14 Pct Recovery = 94% Analysis Date = 03/26/14 Pct Recovery = 93% Analysis Date = 03/26/14 Pct Recovery = 93% Analysis Date = 03/15/14 Pct Recovery = 93% Analysis Date = 03/15/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 03/04/14 Pct Recovery = 93% Analysis Date = 02/22/14 Pct Recovery = 93% Analysis Date = 02/22/14 Pct Recovery = 93% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 02/11/14 Pct Recovery = 92% Analysis Date = 01/31/14 Pct Recovery = 92% Analysis Date = 01/31/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/20/14 Pct Recovery = 92% Analysis Date = 01/09/14 Pct Recovery = 92% Analysis Date = 01/09/14 Pct Recovery = 92% Analysis Date = 12/30/13 Pct Recovery = 91% Analysis Date = 12/30/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/19/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 12/08/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/27/13 Pct Recovery = 91% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/16/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 90% Analysis Date = 11/05/13 Pct Recovery = 90% Analysis Date = 10/26/13 Pct Recovery = 90% Analysis Date = 10/26/13 Pct Recovery = 90% Analysis Date = 10/15/13 Pct Recovery = 90% Analysis Date = 10/15/13 Pct Recovery = 90% Analysis Date = 10/04/13 Pct Recovery = 90% Analysis Date = 10/04/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/23/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/12/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 09/01/13 Pct Recovery = 90% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/22/13 Pct Recovery = 89% Analysis Date = 08/11/13 Pct Recovery = 89% Analysis Date = 08/11/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/31/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/20/13 Pct Recovery = 89% Analysis Date = 07/09/13 Pct Recovery = 89% Analysis Date = 07/09/13 Pct Recovery = 89% Analysis Date = 06/29/13 Pct Recovery = 89% Analysis Date = 06/29/13 Pct Recovery = 89% Analysis Date = 06/18/13 Pct Recovery = 89% Analysis Date = 06/18/13 Pct Recovery = 89% Analysis Date = 06/07/13 Pct Recovery = 89% Analysis Date = 06/07/13 Pct Recovery = 89% Analysis Date = 05/27/13 Pct Recovery = 89% Analysis Date = 05/27/13 Pct Recovery = 89% Analysis Date = 05/16/13 Pct Recovery = 89% Analysis Date = 05/16/13 Pct Recovery = 89% Analysis Date = 05/05/13 Pct Recovery = 89% Analysis Date = 05/05/13 Pct Recovery = 89% Analysis Date = 04/25/13 Pct Recovery = 88% Analysis Date = 04/25/13 Pct Recovery = 88% Analysis Date = 04/14/13 Pct Recovery = 88% Analysis Date = 04/14/13 Pct Recovery = 88% Analysis Date = 04/03/13 Pct Recovery = 88% Analysis Date = 04/03/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/01/13 Pct Recovery = 88% Analysis Date = 03/01/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/17/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 01/06/13 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/26/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 12/05/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/24/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/13/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 11/02/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 88% Analysis Date = 10/23/12 Pct Recovery = 88% Analysis Date = 10/12/12 Pct Recovery = 87% Analysis Date = 10/12/12 Pct Recovery = 87% Analysis Date = 10/01/12 Pct Recovery = 88% Analysis Date = 10/01/12 Pct Recovery = 88% Analysis Date = 09/20/12 Pct Recovery = 88% Analysis Date = 09/20/12 Pct Recovery = 88% Analysis Date = 09/09/12 Pct Recovery = 88% Analysis Date = 09/09/12 Pct Recovery = 88% Analysis Date = 08/29/12 Pct Recovery = 88% Analysis Date = 08/29/12 Pct Recovery = 88% Analysis Date = 08/19/12 Pct Recovery = 88% Analysis Date = 08/19/12 Pct Recovery = 88% Analysis Date = 08/08/12 Pct Recovery = 88% Analysis Date = 08/08/12 Pct Recovery = 88% Analysis Date = 07/28/12 Pct Recovery = 88% Analysis Date = 07/28/12 Pct Recovery = 88% Analysis Date = 07/17/12 Pct Recovery = 88% Analysis Date = 07/17/12 Pct Recovery = 88% Analysis Date = 07/06/12 Pct Recovery = 88% Analysis Date = 07/06/12 Pct Recovery = 88% Analysis Date = 06/25/12 Pct Recovery = 88% Analysis Date = 06/25/12 Pct Recovery = 88% Analysis Date = 06/15/12 Pct Recovery = 88% Analysis Date = 06/15/12 Pct Recovery = 88% Analysis Date = 06/04/12 Pct Recovery = 88% Analysis Date = 06/04/12 Pct Recovery = 88% Analysis Date = 05/24/12 Pct Recovery = 88% Analysis Date = 05/24/12 Pct Recovery = 88% Analysis Date = 05/13/12 Pct Recovery = 88% Analysis Date = 05/13/12 Pct Recovery = 88% Analysis Date = 05/02/12 Pct Recovery = 88% Analysis Date = 05/02/12 Pct Recovery = 88% Analysis Date = 04/22/12 Pct Recovery = 88% Analysis Date = 04/22/12 Pct Recovery = 88% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 04/11/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/31/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/20/12 Pct Recovery = 89% Analysis Date = 03/09/12 Pct Recovery = 89% Analysis Date = 03/09/12 Pct Recovery = 89% Analysis Date = 02/27/12 Pct Recovery = 89% Analysis Date = 02/27/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/17/12 Pct Recovery = 89% Analysis Date = 02/06/12 Pct Recovery = 89% Analysis Date = 02/06/12 Pct Recovery = 89% Analysis Date = 01/26/12 Pct Recovery = 89% Analysis Date = 01/26/12 Pct Recovery = 89% Analysis Date = 01/15/12 Pct Recovery = 89% Analysis Date = 01/15/12 Pct Recovery = 89% Analysis Date = 01/04/12 Pct Recovery = 89% Analysis Date = 01/04/12 Pct Recovery = 89% Analysis Date = 12/24/11 Pct Recovery = 89% Analysis Date = 12/24/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 89% Analysis Date = 12/14/11 Pct Recovery = 89% Analysis Date = 12/03/11 Pct Recovery = 89% Analysis Date = 12/03/11 Pct Recovery = 89% Analysis Date = 11/22/11 Pct Recovery = 89% Analysis Date = 11/22/11 Pct Recovery = 89% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 10/31/11 Pct Recovery = 89% Analysis Date = 10/31/11 Pct Recovery = 89% Analysis Date = 10/20/11 Pct Recovery = 89% Analysis Date = 10/20/11 Pct Recovery = 89% Analysis Date = 10/10/11 Pct Recovery = 89% Analysis Date = 10/10/11 Pct Recovery = 89% Analysis Date = 09/29/11 Pct Recovery = 89% Analysis Date = 09/29/11 Pct Recovery = 89% Analysis Date = 09/18/11 Pct Recovery = 90% Analysis Date = 09/18/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 09/07/11 Pct Recovery = 90% Analysis Date = 08/27/11 Pct Recovery = 90% Analysis Date = 08/27/11 Pct Recovery = 90% Analysis Date = 08/17/11 Pct Recovery = 90% Analysis Date = 08/17/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 08/06/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/15/11 Pct Recovery = 90% Analysis Date = 07/15/11 Pct Recovery = 90% Analysis Date = 07/04/11 Pct Recovery = 90% Analysis Date = 07/04/11 Pct Recovery = 90% Analysis Date = 06/23/11 Pct Recovery = 90% Analysis Date = 06/23/11 Pct Recovery = 90% Analysis Date = 06/13/11 Pct Recovery = 90% Analysis Date = 06/13/11 Pct Recovery = 90% Analysis Date = 06/02/11 Pct Recovery = 90% Analysis Date = 06/02/11 Pct Recovery = 90% Analysis Date = 05/22/11 Pct Recovery = 90% Analysis Date = 05/22/11 Pct Recovery = 90% Analysis Date = 05/11/11 Pct Recovery = 90% Analysis Date = 05/11/11 Pct Recovery = 90% Analysis Date = 04/30/11 Pct Recovery = 90% Analysis Date = 04/30/11 Pct Recovery = 90% Analysis Date = 04/19/11 Pct Recovery = 90% Analysis Date = 04/19/11 Pct Recovery = 90% Analysis Date = 04/09/11 Pct Recovery = 90% Analysis Date = 04/09/11 Pct Recovery = 90% Analysis Date = 03/29/11 Pct Recovery = 90% Analysis Date = 03/29/11 Pct Recovery = 90% Analysis Date = 03/18/11 Pct Recovery = 90% Analysis Date = 03/18/11 Pct Recovery = 90% Analysis Date = 03/07/11 Pct Recovery = 91% Analysis Date = 03/07/11 Pct Recovery = 91% Analysis Date = 02/24/11 Pct Recovery = 91% Analysis Date = 02/24/11 Pct Recovery = 91% Analysis Date = 02/14/11 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHIDATHION (SUPRACIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 91% 19% 87% 14%
Total 89 91% 19% 87% 14%

Sample Statistics
METHIDATHION (SUPRACIDE)

Characteristic N % % Basis
Plotted 89 99% Spiked
Estimated Values 6 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 90 .  
False Negatives 1 1% 1 out of 90
Not Spiked 79 .  
False Positives 0 0% 0 out of 79