BQS OBSP Determination:
DESULFINYLFIPRONIL AMIDE
METHOD: 2033 , TESTIDCODE: 62169GCM29
Open Data Set

 Analysis Date = 01/21/16 
 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl 
 Pct Recovery = 2%  Analysis Date = 04/20/11 
 SpikeMix = NWQL PSP2SP117A: 100 µl 
 Pct Recovery = 73%  Analysis Date = 06/22/11 
 SpikeMix = NWQL PSP2SP117A: 75 µl 
 Pct Recovery = 72%  Analysis Date = 02/09/16 
 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl 
 Pct Recovery = 11%  Analysis Date = 03/05/11 
 SpikeMix = NWQL PSP2SP117A: 25 µl 
 Pct Recovery = 144%  Analysis Date = 02/08/16 
 Pct Recovery = 11%  Analysis Date = 01/30/16 
 Pct Recovery = 6%  Analysis Date = 01/30/16 
 Pct Recovery = 6%  Analysis Date = 01/21/16 
 Pct Recovery = 2%  Analysis Date = 01/21/16 
 Pct Recovery = 2%  Analysis Date = 01/12/16 
 Pct Recovery = 2%  Analysis Date = 01/12/16 
 Pct Recovery = 2%  Analysis Date = 01/03/16 
 Pct Recovery = 2%  Analysis Date = 01/03/16 
 Pct Recovery = 2%  Analysis Date = 12/25/15 
 Pct Recovery = 3%  Analysis Date = 12/25/15 
 Pct Recovery = 3%  Analysis Date = 12/16/15 
 Pct Recovery = 3%  Analysis Date = 12/16/15 
 Pct Recovery = 3%  Analysis Date = 12/07/15 
 Pct Recovery = 3%  Analysis Date = 12/07/15 
 Pct Recovery = 3%  Analysis Date = 11/28/15 
 Pct Recovery = 4%  Analysis Date = 11/28/15 
 Pct Recovery = 4%  Analysis Date = 11/19/15 
 Pct Recovery = 4%  Analysis Date = 11/19/15 
 Pct Recovery = 4%  Analysis Date = 11/10/15 
 Pct Recovery = 5%  Analysis Date = 11/10/15 
 Pct Recovery = 5%  Analysis Date = 11/01/15 
 Pct Recovery = 5%  Analysis Date = 11/01/15 
 Pct Recovery = 5%  Analysis Date = 10/23/15 
 Pct Recovery = 5%  Analysis Date = 10/23/15 
 Pct Recovery = 5%  Analysis Date = 10/14/15 
 Pct Recovery = 6%  Analysis Date = 10/14/15 
 Pct Recovery = 6%  Analysis Date = 10/05/15 
 Pct Recovery = 6%  Analysis Date = 10/05/15 
 Pct Recovery = 6%  Analysis Date = 09/26/15 
 Pct Recovery = 6%  Analysis Date = 09/26/15 
 Pct Recovery = 6%  Analysis Date = 09/17/15 
 Pct Recovery = 7%  Analysis Date = 09/17/15 
 Pct Recovery = 7%  Analysis Date = 09/08/15 
 Pct Recovery = 7%  Analysis Date = 09/08/15 
 Pct Recovery = 7%  Analysis Date = 08/30/15 
 Pct Recovery = 8%  Analysis Date = 08/30/15 
 Pct Recovery = 8%  Analysis Date = 08/21/15 
 Pct Recovery = 8%  Analysis Date = 08/21/15 
 Pct Recovery = 8%  Analysis Date = 08/12/15 
 Pct Recovery = 8%  Analysis Date = 08/12/15 
 Pct Recovery = 8%  Analysis Date = 08/03/15 
 Pct Recovery = 9%  Analysis Date = 08/03/15 
 Pct Recovery = 9%  Analysis Date = 07/25/15 
 Pct Recovery = 9%  Analysis Date = 07/25/15 
 Pct Recovery = 9%  Analysis Date = 07/16/15 
 Pct Recovery = 9%  Analysis Date = 07/16/15 
 Pct Recovery = 9%  Analysis Date = 07/07/15 
 Pct Recovery = 10%  Analysis Date = 07/07/15 
 Pct Recovery = 10%  Analysis Date = 06/28/15 
 Pct Recovery = 10%  Analysis Date = 06/28/15 
 Pct Recovery = 10%  Analysis Date = 06/19/15 
 Pct Recovery = 11%  Analysis Date = 06/19/15 
 Pct Recovery = 11%  Analysis Date = 06/10/15 
 Pct Recovery = 11%  Analysis Date = 06/10/15 
 Pct Recovery = 11%  Analysis Date = 06/01/15 
 Pct Recovery = 11%  Analysis Date = 06/01/15 
 Pct Recovery = 11%  Analysis Date = 05/23/15 
 Pct Recovery = 12%  Analysis Date = 05/23/15 
 Pct Recovery = 12%  Analysis Date = 05/14/15 
 Pct Recovery = 12%  Analysis Date = 05/14/15 
 Pct Recovery = 12%  Analysis Date = 05/05/15 
 Pct Recovery = 12%  Analysis Date = 05/05/15 
 Pct Recovery = 12%  Analysis Date = 04/26/15 
 Pct Recovery = 13%  Analysis Date = 04/26/15 
 Pct Recovery = 13%  Analysis Date = 04/17/15 
 Pct Recovery = 13%  Analysis Date = 04/17/15 
 Pct Recovery = 13%  Analysis Date = 04/08/15 
 Pct Recovery = 14%  Analysis Date = 04/08/15 
 Pct Recovery = 14%  Analysis Date = 03/30/15 
 Pct Recovery = 14%  Analysis Date = 03/30/15 
 Pct Recovery = 14%  Analysis Date = 03/21/15 
 Pct Recovery = 14%  Analysis Date = 03/21/15 
 Pct Recovery = 14%  Analysis Date = 03/12/15 
 Pct Recovery = 15%  Analysis Date = 03/12/15 
 Pct Recovery = 15%  Analysis Date = 03/03/15 
 Pct Recovery = 15%  Analysis Date = 03/03/15 
 Pct Recovery = 15%  Analysis Date = 02/22/15 
 Pct Recovery = 16%  Analysis Date = 02/22/15 
 Pct Recovery = 16%  Analysis Date = 02/13/15 
 Pct Recovery = 16%  Analysis Date = 02/13/15 
 Pct Recovery = 16%  Analysis Date = 02/04/15 
 Pct Recovery = 16%  Analysis Date = 02/04/15 
 Pct Recovery = 16%  Analysis Date = 01/26/15 
 Pct Recovery = 17%  Analysis Date = 01/26/15 
 Pct Recovery = 17%  Analysis Date = 01/17/15 
 Pct Recovery = 17%  Analysis Date = 01/17/15 
 Pct Recovery = 17%  Analysis Date = 01/08/15 
 Pct Recovery = 17%  Analysis Date = 01/08/15 
 Pct Recovery = 17%  Analysis Date = 12/30/14 
 Pct Recovery = 18%  Analysis Date = 12/30/14 
 Pct Recovery = 18%  Analysis Date = 12/21/14 
 Pct Recovery = 18%  Analysis Date = 12/21/14 
 Pct Recovery = 18%  Analysis Date = 12/12/14 
 Pct Recovery = 19%  Analysis Date = 12/12/14 
 Pct Recovery = 19%  Analysis Date = 12/03/14 
 Pct Recovery = 19%  Analysis Date = 12/03/14 
 Pct Recovery = 19%  Analysis Date = 11/24/14 
 Pct Recovery = 19%  Analysis Date = 11/24/14 
 Pct Recovery = 19%  Analysis Date = 11/15/14 
 Pct Recovery = 20%  Analysis Date = 11/15/14 
 Pct Recovery = 20%  Analysis Date = 11/06/14 
 Pct Recovery = 20%  Analysis Date = 11/06/14 
 Pct Recovery = 20%  Analysis Date = 10/28/14 
 Pct Recovery = 20%  Analysis Date = 10/28/14 
 Pct Recovery = 20%  Analysis Date = 10/19/14 
 Pct Recovery = 21%  Analysis Date = 10/19/14 
 Pct Recovery = 21%  Analysis Date = 10/10/14 
 Pct Recovery = 21%  Analysis Date = 10/10/14 
 Pct Recovery = 21%  Analysis Date = 10/01/14 
 Pct Recovery = 22%  Analysis Date = 10/01/14 
 Pct Recovery = 22%  Analysis Date = 09/22/14 
 Pct Recovery = 22%  Analysis Date = 09/22/14 
 Pct Recovery = 22%  Analysis Date = 09/13/14 
 Pct Recovery = 22%  Analysis Date = 09/13/14 
 Pct Recovery = 22%  Analysis Date = 09/04/14 
 Pct Recovery = 23%  Analysis Date = 09/04/14 
 Pct Recovery = 23%  Analysis Date = 08/26/14 
 Pct Recovery = 23%  Analysis Date = 08/26/14 
 Pct Recovery = 23%  Analysis Date = 08/17/14 
 Pct Recovery = 23%  Analysis Date = 08/17/14 
 Pct Recovery = 23%  Analysis Date = 08/08/14 
 Pct Recovery = 24%  Analysis Date = 08/08/14 
 Pct Recovery = 24%  Analysis Date = 07/30/14 
 Pct Recovery = 24%  Analysis Date = 07/30/14 
 Pct Recovery = 24%  Analysis Date = 07/21/14 
 Pct Recovery = 25%  Analysis Date = 07/21/14 
 Pct Recovery = 25%  Analysis Date = 07/12/14 
 Pct Recovery = 25%  Analysis Date = 07/12/14 
 Pct Recovery = 25%  Analysis Date = 07/03/14 
 Pct Recovery = 25%  Analysis Date = 07/03/14 
 Pct Recovery = 25%  Analysis Date = 06/24/14 
 Pct Recovery = 26%  Analysis Date = 06/24/14 
 Pct Recovery = 26%  Analysis Date = 06/15/14 
 Pct Recovery = 26%  Analysis Date = 06/15/14 
 Pct Recovery = 26%  Analysis Date = 06/06/14 
 Pct Recovery = 27%  Analysis Date = 06/06/14 
 Pct Recovery = 27%  Analysis Date = 05/28/14 
 Pct Recovery = 27%  Analysis Date = 05/28/14 
 Pct Recovery = 27%  Analysis Date = 05/19/14 
 Pct Recovery = 27%  Analysis Date = 05/19/14 
 Pct Recovery = 27%  Analysis Date = 05/10/14 
 Pct Recovery = 28%  Analysis Date = 05/10/14 
 Pct Recovery = 28%  Analysis Date = 05/01/14 
 Pct Recovery = 28%  Analysis Date = 05/01/14 
 Pct Recovery = 28%  Analysis Date = 04/22/14 
 Pct Recovery = 28%  Analysis Date = 04/22/14 
 Pct Recovery = 28%  Analysis Date = 04/13/14 
 Pct Recovery = 29%  Analysis Date = 04/13/14 
 Pct Recovery = 29%  Analysis Date = 04/04/14 
 Pct Recovery = 29%  Analysis Date = 04/04/14 
 Pct Recovery = 29%  Analysis Date = 03/26/14 
 Pct Recovery = 30%  Analysis Date = 03/26/14 
 Pct Recovery = 30%  Analysis Date = 03/17/14 
 Pct Recovery = 30%  Analysis Date = 03/17/14 
 Pct Recovery = 30%  Analysis Date = 03/08/14 
 Pct Recovery = 30%  Analysis Date = 03/08/14 
 Pct Recovery = 30%  Analysis Date = 02/27/14 
 Pct Recovery = 31%  Analysis Date = 02/27/14 
 Pct Recovery = 31%  Analysis Date = 02/18/14 
 Pct Recovery = 31%  Analysis Date = 02/18/14 
 Pct Recovery = 31%  Analysis Date = 02/09/14 
 Pct Recovery = 31%  Analysis Date = 02/09/14 
 Pct Recovery = 31%  Analysis Date = 01/31/14 
 Pct Recovery = 32%  Analysis Date = 01/31/14 
 Pct Recovery = 32%  Analysis Date = 01/22/14 
 Pct Recovery = 32%  Analysis Date = 01/22/14 
 Pct Recovery = 32%  Analysis Date = 01/13/14 
 Pct Recovery = 33%  Analysis Date = 01/13/14 
 Pct Recovery = 33%  Analysis Date = 01/04/14 
 Pct Recovery = 33%  Analysis Date = 01/04/14 
 Pct Recovery = 33%  Analysis Date = 12/26/13 
 Pct Recovery = 33%  Analysis Date = 12/26/13 
 Pct Recovery = 33%  Analysis Date = 12/17/13 
 Pct Recovery = 34%  Analysis Date = 12/17/13 
 Pct Recovery = 34%  Analysis Date = 12/08/13 
 Pct Recovery = 34%  Analysis Date = 12/08/13 
 Pct Recovery = 34%  Analysis Date = 11/29/13 
 Pct Recovery = 34%  Analysis Date = 11/29/13 
 Pct Recovery = 34%  Analysis Date = 11/20/13 
 Pct Recovery = 35%  Analysis Date = 11/20/13 
 Pct Recovery = 35%  Analysis Date = 11/11/13 
 Pct Recovery = 35%  Analysis Date = 11/11/13 
 Pct Recovery = 35%  Analysis Date = 11/02/13 
 Pct Recovery = 36%  Analysis Date = 11/02/13 
 Pct Recovery = 36%  Analysis Date = 10/24/13 
 Pct Recovery = 36%  Analysis Date = 10/24/13 
 Pct Recovery = 36%  Analysis Date = 10/15/13 
 Pct Recovery = 36%  Analysis Date = 10/15/13 
 Pct Recovery = 36%  Analysis Date = 10/06/13 
 Pct Recovery = 37%  Analysis Date = 10/06/13 
 Pct Recovery = 37%  Analysis Date = 09/27/13 
 Pct Recovery = 37%  Analysis Date = 09/27/13 
 Pct Recovery = 37%  Analysis Date = 09/18/13 
 Pct Recovery = 37%  Analysis Date = 09/18/13 
 Pct Recovery = 37%  Analysis Date = 09/09/13 
 Pct Recovery = 38%  Analysis Date = 09/09/13 
 Pct Recovery = 38%  Analysis Date = 08/31/13 
 Pct Recovery = 38%  Analysis Date = 08/31/13 
 Pct Recovery = 38%  Analysis Date = 08/21/13 
 Pct Recovery = 39%  Analysis Date = 08/21/13 
 Pct Recovery = 39%  Analysis Date = 08/12/13 
 Pct Recovery = 39%  Analysis Date = 08/12/13 
 Pct Recovery = 39%  Analysis Date = 08/03/13 
 Pct Recovery = 39%  Analysis Date = 08/03/13 
 Pct Recovery = 39%  Analysis Date = 07/25/13 
 Pct Recovery = 40%  Analysis Date = 07/25/13 
 Pct Recovery = 40%  Analysis Date = 07/16/13 
 Pct Recovery = 40%  Analysis Date = 07/16/13 
 Pct Recovery = 40%  Analysis Date = 07/07/13 
 Pct Recovery = 41%  Analysis Date = 07/07/13 
 Pct Recovery = 41%  Analysis Date = 06/28/13 
 Pct Recovery = 41%  Analysis Date = 06/28/13 
 Pct Recovery = 41%  Analysis Date = 06/19/13 
 Pct Recovery = 41%  Analysis Date = 06/19/13 
 Pct Recovery = 41%  Analysis Date = 06/10/13 
 Pct Recovery = 42%  Analysis Date = 06/10/13 
 Pct Recovery = 42%  Analysis Date = 06/01/13 
 Pct Recovery = 42%  Analysis Date = 06/01/13 
 Pct Recovery = 42%  Analysis Date = 05/23/13 
 Pct Recovery = 42%  Analysis Date = 05/23/13 
 Pct Recovery = 42%  Analysis Date = 05/14/13 
 Pct Recovery = 43%  Analysis Date = 05/14/13 
 Pct Recovery = 43%  Analysis Date = 05/05/13 
 Pct Recovery = 43%  Analysis Date = 05/05/13 
 Pct Recovery = 43%  Analysis Date = 04/26/13 
 Pct Recovery = 44%  Analysis Date = 04/26/13 
 Pct Recovery = 44%  Analysis Date = 04/17/13 
 Pct Recovery = 44%  Analysis Date = 04/17/13 
 Pct Recovery = 44%  Analysis Date = 04/08/13 
 Pct Recovery = 44%  Analysis Date = 04/08/13 
 Pct Recovery = 44%  Analysis Date = 03/30/13 
 Pct Recovery = 45%  Analysis Date = 03/30/13 
 Pct Recovery = 45%  Analysis Date = 03/21/13 
 Pct Recovery = 45%  Analysis Date = 03/21/13 
 Pct Recovery = 45%  Analysis Date = 03/12/13 
 Pct Recovery = 45%  Analysis Date = 03/12/13 
 Pct Recovery = 45%  Analysis Date = 03/03/13 
 Pct Recovery = 46%  Analysis Date = 03/03/13 
 Pct Recovery = 46%  Analysis Date = 02/22/13 
 Pct Recovery = 46%  Analysis Date = 02/22/13 
 Pct Recovery = 46%  Analysis Date = 02/13/13 
 Pct Recovery = 47%  Analysis Date = 02/13/13 
 Pct Recovery = 47%  Analysis Date = 02/04/13 
 Pct Recovery = 47%  Analysis Date = 02/04/13 
 Pct Recovery = 47%  Analysis Date = 01/26/13 
 Pct Recovery = 47%  Analysis Date = 01/26/13 
 Pct Recovery = 47%  Analysis Date = 01/17/13 
 Pct Recovery = 48%  Analysis Date = 01/17/13 
 Pct Recovery = 48%  Analysis Date = 01/08/13 
 Pct Recovery = 48%  Analysis Date = 01/08/13 
 Pct Recovery = 48%  Analysis Date = 12/30/12 
 Pct Recovery = 48%  Analysis Date = 12/30/12 
 Pct Recovery = 48%  Analysis Date = 12/21/12 
 Pct Recovery = 49%  Analysis Date = 12/21/12 
 Pct Recovery = 49%  Analysis Date = 12/12/12 
 Pct Recovery = 49%  Analysis Date = 12/12/12 
 Pct Recovery = 49%  Analysis Date = 12/03/12 
 Pct Recovery = 50%  Analysis Date = 12/03/12 
 Pct Recovery = 50%  Analysis Date = 11/24/12 
 Pct Recovery = 50%  Analysis Date = 11/24/12 
 Pct Recovery = 50%  Analysis Date = 11/15/12 
 Pct Recovery = 50%  Analysis Date = 11/15/12 
 Pct Recovery = 50%  Analysis Date = 11/06/12 
 Pct Recovery = 51%  Analysis Date = 11/06/12 
 Pct Recovery = 51%  Analysis Date = 10/28/12 
 Pct Recovery = 51%  Analysis Date = 10/28/12 
 Pct Recovery = 51%  Analysis Date = 10/19/12 
 Pct Recovery = 52%  Analysis Date = 10/19/12 
 Pct Recovery = 52%  Analysis Date = 10/10/12 
 Pct Recovery = 52%  Analysis Date = 10/10/12 
 Pct Recovery = 52%  Analysis Date = 10/01/12 
 Pct Recovery = 52%  Analysis Date = 10/01/12 
 Pct Recovery = 52%  Analysis Date = 09/22/12 
 Pct Recovery = 53%  Analysis Date = 09/22/12 
 Pct Recovery = 53%  Analysis Date = 09/13/12 
 Pct Recovery = 53%  Analysis Date = 09/13/12 
 Pct Recovery = 53%  Analysis Date = 09/04/12 
 Pct Recovery = 53%  Analysis Date = 09/04/12 
 Pct Recovery = 53%  Analysis Date = 08/26/12 
 Pct Recovery = 54%  Analysis Date = 08/26/12 
 Pct Recovery = 54%  Analysis Date = 08/17/12 
 Pct Recovery = 54%  Analysis Date = 08/17/12 
 Pct Recovery = 54%  Analysis Date = 08/08/12 
 Pct Recovery = 55%  Analysis Date = 08/08/12 
 Pct Recovery = 55%  Analysis Date = 07/30/12 
 Pct Recovery = 55%  Analysis Date = 07/30/12 
 Pct Recovery = 55%  Analysis Date = 07/21/12 
 Pct Recovery = 55%  Analysis Date = 07/21/12 
 Pct Recovery = 55%  Analysis Date = 07/12/12 
 Pct Recovery = 56%  Analysis Date = 07/12/12 
 Pct Recovery = 56%  Analysis Date = 07/03/12 
 Pct Recovery = 56%  Analysis Date = 07/03/12 
 Pct Recovery = 56%  Analysis Date = 06/24/12 
 Pct Recovery = 56%  Analysis Date = 06/24/12 
 Pct Recovery = 56%  Analysis Date = 06/15/12 
 Pct Recovery = 57%  Analysis Date = 06/15/12 
 Pct Recovery = 57%  Analysis Date = 06/06/12 
 Pct Recovery = 57%  Analysis Date = 06/06/12 
 Pct Recovery = 57%  Analysis Date = 05/28/12 
 Pct Recovery = 58%  Analysis Date = 05/28/12 
 Pct Recovery = 58%  Analysis Date = 05/19/12 
 Pct Recovery = 58%  Analysis Date = 05/19/12 
 Pct Recovery = 58%  Analysis Date = 05/10/12 
 Pct Recovery = 58%  Analysis Date = 05/10/12 
 Pct Recovery = 58%  Analysis Date = 05/01/12 
 Pct Recovery = 59%  Analysis Date = 05/01/12 
 Pct Recovery = 59%  Analysis Date = 04/22/12 
 Pct Recovery = 59%  Analysis Date = 04/22/12 
 Pct Recovery = 59%  Analysis Date = 04/13/12 
 Pct Recovery = 59%  Analysis Date = 04/13/12 
 Pct Recovery = 59%  Analysis Date = 04/04/12 
 Pct Recovery = 60%  Analysis Date = 04/04/12 
 Pct Recovery = 60%  Analysis Date = 03/26/12 
 Pct Recovery = 60%  Analysis Date = 03/26/12 
 Pct Recovery = 60%  Analysis Date = 03/17/12 
 Pct Recovery = 61%  Analysis Date = 03/17/12 
 Pct Recovery = 61%  Analysis Date = 03/08/12 
 Pct Recovery = 61%  Analysis Date = 03/08/12 
 Pct Recovery = 61%  Analysis Date = 02/28/12 
 Pct Recovery = 61%  Analysis Date = 02/28/12 
 Pct Recovery = 61%  Analysis Date = 02/19/12 
 Pct Recovery = 62%  Analysis Date = 02/19/12 
 Pct Recovery = 62%  Analysis Date = 02/10/12 
 Pct Recovery = 62%  Analysis Date = 02/10/12 
 Pct Recovery = 62%  Analysis Date = 02/01/12 
 Pct Recovery = 62%  Analysis Date = 02/01/12 
 Pct Recovery = 62%  Analysis Date = 01/23/12 
 Pct Recovery = 63%  Analysis Date = 01/23/12 
 Pct Recovery = 63%  Analysis Date = 01/14/12 
 Pct Recovery = 63%  Analysis Date = 01/14/12 
 Pct Recovery = 63%  Analysis Date = 01/05/12 
 Pct Recovery = 64%  Analysis Date = 01/05/12 
 Pct Recovery = 64%  Analysis Date = 12/27/11 
 Pct Recovery = 64%  Analysis Date = 12/27/11 
 Pct Recovery = 64%  Analysis Date = 12/18/11 
 Pct Recovery = 64%  Analysis Date = 12/18/11 
 Pct Recovery = 64%  Analysis Date = 12/09/11 
 Pct Recovery = 65%  Analysis Date = 12/09/11 
 Pct Recovery = 65%  Analysis Date = 11/30/11 
 Pct Recovery = 65%  Analysis Date = 11/30/11 
 Pct Recovery = 65%  Analysis Date = 11/21/11 
 Pct Recovery = 66%  Analysis Date = 11/21/11 
 Pct Recovery = 66%  Analysis Date = 11/12/11 
 Pct Recovery = 66%  Analysis Date = 11/12/11 
 Pct Recovery = 66%  Analysis Date = 11/03/11 
 Pct Recovery = 66%  Analysis Date = 11/03/11 
 Pct Recovery = 66%  Analysis Date = 10/25/11 
 Pct Recovery = 67%  Analysis Date = 10/25/11 
 Pct Recovery = 67%  Analysis Date = 10/16/11 
 Pct Recovery = 67%  Analysis Date = 10/16/11 
 Pct Recovery = 67%  Analysis Date = 10/07/11 
 Pct Recovery = 67%  Analysis Date = 10/07/11 
 Pct Recovery = 67%  Analysis Date = 09/28/11 
 Pct Recovery = 68%  Analysis Date = 09/28/11 
 Pct Recovery = 68%  Analysis Date = 09/19/11 
 Pct Recovery = 68%  Analysis Date = 09/19/11 
 Pct Recovery = 68%  Analysis Date = 09/10/11 
 Pct Recovery = 69%  Analysis Date = 09/10/11 
 Pct Recovery = 69%  Analysis Date = 09/01/11 
 Pct Recovery = 69%  Analysis Date = 09/01/11 
 Pct Recovery = 69%  Analysis Date = 08/23/11 
 Pct Recovery = 69%  Analysis Date = 08/23/11 
 Pct Recovery = 69%  Analysis Date = 08/14/11 
 Pct Recovery = 70%  Analysis Date = 08/14/11 
 Pct Recovery = 70%  Analysis Date = 08/05/11 
 Pct Recovery = 70%  Analysis Date = 08/05/11 
 Pct Recovery = 70%  Analysis Date = 07/27/11 
 Pct Recovery = 70%  Analysis Date = 07/27/11 
 Pct Recovery = 70%  Analysis Date = 07/18/11 
 Pct Recovery = 71%  Analysis Date = 07/18/11 
 Pct Recovery = 71%  Analysis Date = 07/09/11 
 Pct Recovery = 71%  Analysis Date = 07/09/11 
 Pct Recovery = 71%  Analysis Date = 06/30/11 
 Pct Recovery = 72%  Analysis Date = 06/30/11 
 Pct Recovery = 72%  Analysis Date = 06/21/11 
 Pct Recovery = 72%  Analysis Date = 06/21/11 
 Pct Recovery = 72%  Analysis Date = 06/12/11 
 Pct Recovery = 72%  Analysis Date = 06/12/11 
 Pct Recovery = 72%  Analysis Date = 06/03/11 
 Pct Recovery = 72%  Analysis Date = 06/03/11 
 Pct Recovery = 72%  Analysis Date = 05/25/11 
 Pct Recovery = 72%  Analysis Date = 05/25/11 
 Pct Recovery = 72%  Analysis Date = 05/16/11 
 Pct Recovery = 73%  Analysis Date = 05/16/11 
 Pct Recovery = 73%  Analysis Date = 05/07/11 
 Pct Recovery = 73%  Analysis Date = 05/07/11 
 Pct Recovery = 73%  Analysis Date = 04/28/11 
 Pct Recovery = 73%  Analysis Date = 04/28/11 
 Pct Recovery = 73%  Analysis Date = 04/19/11 
 Pct Recovery = 75%  Analysis Date = 04/19/11 
 Pct Recovery = 75%  Analysis Date = 04/10/11 
 Pct Recovery = 88%  Analysis Date = 04/10/11 
 Pct Recovery = 88%  Analysis Date = 04/01/11 
 Pct Recovery = 102%  Analysis Date = 04/01/11 
 Pct Recovery = 102%  Analysis Date = 03/23/11 
 Pct Recovery = 116%  Analysis Date = 03/23/11 
 Pct Recovery = 116%  Analysis Date = 03/14/11 
 Pct Recovery = 130%  Analysis Date = 03/14/11 
 Pct Recovery = 130%  Analysis Date = 03/05/11 
 Pct Recovery = 144%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL AMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 144% . 144% 0%
>= Reporting Level 4 39% 39% 41% 49%
Total 5 60% 57% 72% 46%

Sample Statistics
DESULFINYLFIPRONIL AMIDE

Characteristic N % % Basis
Plotted 5 50% Spiked
Estimated Values 5 50% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 10 .  
False Negatives 5 50% 5 out of 10
Not Spiked 159 .  
False Positives 0 0% 0 out of 159