BQS OBSP Determination:
DESULFINYLFIPRONIL
METHOD: 2033 , TESTIDCODE: 62170GCM29
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 81% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 99% Analysis Date = 01/27/12 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 66% Analysis Date = 12/21/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 82% Analysis Date = 09/29/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 72% Analysis Date = 07/07/11 SpikeMix = Spex Organics T1100628017: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 135% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 74% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 83% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 94% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 91% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 91% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 70% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 65% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 100% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 64% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 66% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 70% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 63% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 110% Analysis Date = 05/14/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 64% Analysis Date = 02/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 61% Analysis Date = 06/02/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 70% Analysis Date = 04/05/12 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 86% Analysis Date = 11/17/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 73% Analysis Date = 09/19/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 67% Analysis Date = 03/23/11 SpikeMix = Spex Organics T1100628017: 40 µl Pct Recovery = 81% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 58% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 99% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 83% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 80% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 98% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 107% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 72% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 84% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 79% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 57% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 67% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 92% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 61% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 73% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 78% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 57% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 83% Analysis Date = 09/09/16 Pct Recovery = 83% Analysis Date = 09/09/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/20/16 Pct Recovery = 83% Analysis Date = 08/20/16 Pct Recovery = 83% Analysis Date = 08/10/16 Pct Recovery = 82% Analysis Date = 08/10/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/10/16 Pct Recovery = 82% Analysis Date = 07/10/16 Pct Recovery = 82% Analysis Date = 06/30/16 Pct Recovery = 82% Analysis Date = 06/30/16 Pct Recovery = 82% Analysis Date = 06/20/16 Pct Recovery = 81% Analysis Date = 06/20/16 Pct Recovery = 81% Analysis Date = 06/10/16 Pct Recovery = 81% Analysis Date = 06/10/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/20/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/20/16 Pct Recovery = 80% Analysis Date = 03/20/16 Pct Recovery = 80% Analysis Date = 03/10/16 Pct Recovery = 80% Analysis Date = 03/10/16 Pct Recovery = 80% Analysis Date = 02/29/16 Pct Recovery = 80% Analysis Date = 02/29/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 02/08/16 Pct Recovery = 79% Analysis Date = 01/29/16 Pct Recovery = 79% Analysis Date = 01/29/16 Pct Recovery = 79% Analysis Date = 01/19/16 Pct Recovery = 79% Analysis Date = 01/19/16 Pct Recovery = 79% Analysis Date = 01/09/16 Pct Recovery = 79% Analysis Date = 01/09/16 Pct Recovery = 79% Analysis Date = 12/29/15 Pct Recovery = 79% Analysis Date = 12/29/15 Pct Recovery = 79% Analysis Date = 12/19/15 Pct Recovery = 79% Analysis Date = 12/19/15 Pct Recovery = 79% Analysis Date = 12/09/15 Pct Recovery = 78% Analysis Date = 12/09/15 Pct Recovery = 78% Analysis Date = 11/29/15 Pct Recovery = 78% Analysis Date = 11/29/15 Pct Recovery = 78% Analysis Date = 11/19/15 Pct Recovery = 78% Analysis Date = 11/19/15 Pct Recovery = 78% Analysis Date = 11/08/15 Pct Recovery = 78% Analysis Date = 11/08/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/29/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 78% Analysis Date = 10/19/15 Pct Recovery = 78% Analysis Date = 10/09/15 Pct Recovery = 78% Analysis Date = 10/09/15 Pct Recovery = 78% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/29/15 Pct Recovery = 77% Analysis Date = 09/18/15 Pct Recovery = 77% Analysis Date = 09/18/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 09/08/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/29/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 77% Analysis Date = 08/19/15 Pct Recovery = 77% Analysis Date = 08/09/15 Pct Recovery = 77% Analysis Date = 08/09/15 Pct Recovery = 77% Analysis Date = 07/29/15 Pct Recovery = 77% Analysis Date = 07/29/15 Pct Recovery = 77% Analysis Date = 07/19/15 Pct Recovery = 77% Analysis Date = 07/19/15 Pct Recovery = 77% Analysis Date = 07/09/15 Pct Recovery = 77% Analysis Date = 07/09/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/29/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/19/15 Pct Recovery = 77% Analysis Date = 06/08/15 Pct Recovery = 77% Analysis Date = 06/08/15 Pct Recovery = 77% Analysis Date = 05/29/15 Pct Recovery = 77% Analysis Date = 05/29/15 Pct Recovery = 77% Analysis Date = 05/19/15 Pct Recovery = 77% Analysis Date = 05/19/15 Pct Recovery = 77% Analysis Date = 05/09/15 Pct Recovery = 77% Analysis Date = 05/09/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 77% Analysis Date = 04/29/15 Pct Recovery = 77% Analysis Date = 04/18/15 Pct Recovery = 77% Analysis Date = 04/18/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 04/08/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/29/15 Pct Recovery = 77% Analysis Date = 03/19/15 Pct Recovery = 77% Analysis Date = 03/19/15 Pct Recovery = 77% Analysis Date = 03/09/15 Pct Recovery = 77% Analysis Date = 03/09/15 Pct Recovery = 77% Analysis Date = 02/26/15 Pct Recovery = 77% Analysis Date = 02/26/15 Pct Recovery = 77% Analysis Date = 02/16/15 Pct Recovery = 77% Analysis Date = 02/16/15 Pct Recovery = 77% Analysis Date = 02/06/15 Pct Recovery = 77% Analysis Date = 02/06/15 Pct Recovery = 77% Analysis Date = 01/27/15 Pct Recovery = 77% Analysis Date = 01/27/15 Pct Recovery = 77% Analysis Date = 01/17/15 Pct Recovery = 77% Analysis Date = 01/17/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 01/06/15 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/27/14 Pct Recovery = 77% Analysis Date = 12/17/14 Pct Recovery = 77% Analysis Date = 12/17/14 Pct Recovery = 77% Analysis Date = 12/07/14 Pct Recovery = 77% Analysis Date = 12/07/14 Pct Recovery = 77% Analysis Date = 11/27/14 Pct Recovery = 77% Analysis Date = 11/27/14 Pct Recovery = 77% Analysis Date = 11/16/14 Pct Recovery = 77% Analysis Date = 11/16/14 Pct Recovery = 77% Analysis Date = 11/06/14 Pct Recovery = 77% Analysis Date = 11/06/14 Pct Recovery = 77% Analysis Date = 10/27/14 Pct Recovery = 77% Analysis Date = 10/27/14 Pct Recovery = 77% Analysis Date = 10/17/14 Pct Recovery = 77% Analysis Date = 10/17/14 Pct Recovery = 77% Analysis Date = 10/07/14 Pct Recovery = 77% Analysis Date = 10/07/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/26/14 Pct Recovery = 77% Analysis Date = 09/16/14 Pct Recovery = 77% Analysis Date = 09/16/14 Pct Recovery = 77% Analysis Date = 09/06/14 Pct Recovery = 77% Analysis Date = 09/06/14 Pct Recovery = 77% Analysis Date = 08/27/14 Pct Recovery = 77% Analysis Date = 08/27/14 Pct Recovery = 77% Analysis Date = 08/17/14 Pct Recovery = 77% Analysis Date = 08/17/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 08/06/14 Pct Recovery = 77% Analysis Date = 07/27/14 Pct Recovery = 77% Analysis Date = 07/27/14 Pct Recovery = 77% Analysis Date = 07/17/14 Pct Recovery = 77% Analysis Date = 07/17/14 Pct Recovery = 77% Analysis Date = 07/07/14 Pct Recovery = 77% Analysis Date = 07/07/14 Pct Recovery = 77% Analysis Date = 06/27/14 Pct Recovery = 77% Analysis Date = 06/27/14 Pct Recovery = 77% Analysis Date = 06/16/14 Pct Recovery = 77% Analysis Date = 06/16/14 Pct Recovery = 77% Analysis Date = 06/06/14 Pct Recovery = 77% Analysis Date = 06/06/14 Pct Recovery = 77% Analysis Date = 05/27/14 Pct Recovery = 77% Analysis Date = 05/27/14 Pct Recovery = 77% Analysis Date = 05/17/14 Pct Recovery = 77% Analysis Date = 05/17/14 Pct Recovery = 77% Analysis Date = 05/07/14 Pct Recovery = 77% Analysis Date = 05/07/14 Pct Recovery = 77% Analysis Date = 04/26/14 Pct Recovery = 77% Analysis Date = 04/26/14 Pct Recovery = 77% Analysis Date = 04/16/14 Pct Recovery = 77% Analysis Date = 04/16/14 Pct Recovery = 77% Analysis Date = 04/06/14 Pct Recovery = 78% Analysis Date = 04/06/14 Pct Recovery = 78% Analysis Date = 03/27/14 Pct Recovery = 78% Analysis Date = 03/27/14 Pct Recovery = 78% Analysis Date = 03/17/14 Pct Recovery = 78% Analysis Date = 03/17/14 Pct Recovery = 78% Analysis Date = 03/06/14 Pct Recovery = 78% Analysis Date = 03/06/14 Pct Recovery = 78% Analysis Date = 02/24/14 Pct Recovery = 78% Analysis Date = 02/24/14 Pct Recovery = 78% Analysis Date = 02/14/14 Pct Recovery = 78% Analysis Date = 02/14/14 Pct Recovery = 78% Analysis Date = 02/04/14 Pct Recovery = 78% Analysis Date = 02/04/14 Pct Recovery = 78% Analysis Date = 01/25/14 Pct Recovery = 78% Analysis Date = 01/25/14 Pct Recovery = 78% Analysis Date = 01/14/14 Pct Recovery = 78% Analysis Date = 01/14/14 Pct Recovery = 78% Analysis Date = 01/04/14 Pct Recovery = 78% Analysis Date = 01/04/14 Pct Recovery = 78% Analysis Date = 12/25/13 Pct Recovery = 78% Analysis Date = 12/25/13 Pct Recovery = 78% Analysis Date = 12/15/13 Pct Recovery = 78% Analysis Date = 12/15/13 Pct Recovery = 78% Analysis Date = 12/05/13 Pct Recovery = 78% Analysis Date = 12/05/13 Pct Recovery = 78% Analysis Date = 11/24/13 Pct Recovery = 78% Analysis Date = 11/24/13 Pct Recovery = 78% Analysis Date = 11/14/13 Pct Recovery = 79% Analysis Date = 11/14/13 Pct Recovery = 79% Analysis Date = 11/04/13 Pct Recovery = 79% Analysis Date = 11/04/13 Pct Recovery = 79% Analysis Date = 10/25/13 Pct Recovery = 79% Analysis Date = 10/25/13 Pct Recovery = 79% Analysis Date = 10/15/13 Pct Recovery = 79% Analysis Date = 10/15/13 Pct Recovery = 79% Analysis Date = 10/04/13 Pct Recovery = 79% Analysis Date = 10/04/13 Pct Recovery = 79% Analysis Date = 09/24/13 Pct Recovery = 79% Analysis Date = 09/24/13 Pct Recovery = 79% Analysis Date = 09/14/13 Pct Recovery = 79% Analysis Date = 09/14/13 Pct Recovery = 79% Analysis Date = 09/04/13 Pct Recovery = 79% Analysis Date = 09/04/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/25/13 Pct Recovery = 79% Analysis Date = 08/14/13 Pct Recovery = 79% Analysis Date = 08/14/13 Pct Recovery = 79% Analysis Date = 08/04/13 Pct Recovery = 79% Analysis Date = 08/04/13 Pct Recovery = 79% Analysis Date = 07/25/13 Pct Recovery = 79% Analysis Date = 07/25/13 Pct Recovery = 79% Analysis Date = 07/15/13 Pct Recovery = 79% Analysis Date = 07/15/13 Pct Recovery = 79% Analysis Date = 07/05/13 Pct Recovery = 80% Analysis Date = 07/05/13 Pct Recovery = 80% Analysis Date = 06/24/13 Pct Recovery = 80% Analysis Date = 06/24/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/14/13 Pct Recovery = 80% Analysis Date = 06/04/13 Pct Recovery = 80% Analysis Date = 06/04/13 Pct Recovery = 80% Analysis Date = 05/25/13 Pct Recovery = 80% Analysis Date = 05/25/13 Pct Recovery = 80% Analysis Date = 05/15/13 Pct Recovery = 80% Analysis Date = 05/15/13 Pct Recovery = 80% Analysis Date = 05/04/13 Pct Recovery = 80% Analysis Date = 05/04/13 Pct Recovery = 80% Analysis Date = 04/24/13 Pct Recovery = 80% Analysis Date = 04/24/13 Pct Recovery = 80% Analysis Date = 04/14/13 Pct Recovery = 80% Analysis Date = 04/14/13 Pct Recovery = 80% Analysis Date = 04/04/13 Pct Recovery = 80% Analysis Date = 04/04/13 Pct Recovery = 80% Analysis Date = 03/25/13 Pct Recovery = 80% Analysis Date = 03/25/13 Pct Recovery = 80% Analysis Date = 03/14/13 Pct Recovery = 80% Analysis Date = 03/14/13 Pct Recovery = 80% Analysis Date = 03/04/13 Pct Recovery = 80% Analysis Date = 03/04/13 Pct Recovery = 80% Analysis Date = 02/22/13 Pct Recovery = 80% Analysis Date = 02/22/13 Pct Recovery = 80% Analysis Date = 02/12/13 Pct Recovery = 81% Analysis Date = 02/12/13 Pct Recovery = 81% Analysis Date = 02/02/13 Pct Recovery = 81% Analysis Date = 02/02/13 Pct Recovery = 81% Analysis Date = 01/22/13 Pct Recovery = 81% Analysis Date = 01/22/13 Pct Recovery = 81% Analysis Date = 01/12/13 Pct Recovery = 81% Analysis Date = 01/12/13 Pct Recovery = 81% Analysis Date = 01/02/13 Pct Recovery = 81% Analysis Date = 01/02/13 Pct Recovery = 81% Analysis Date = 12/23/12 Pct Recovery = 81% Analysis Date = 12/23/12 Pct Recovery = 81% Analysis Date = 12/13/12 Pct Recovery = 81% Analysis Date = 12/13/12 Pct Recovery = 81% Analysis Date = 12/02/12 Pct Recovery = 81% Analysis Date = 12/02/12 Pct Recovery = 81% Analysis Date = 11/22/12 Pct Recovery = 81% Analysis Date = 11/22/12 Pct Recovery = 81% Analysis Date = 11/12/12 Pct Recovery = 81% Analysis Date = 11/12/12 Pct Recovery = 81% Analysis Date = 11/02/12 Pct Recovery = 81% Analysis Date = 11/02/12 Pct Recovery = 81% Analysis Date = 10/23/12 Pct Recovery = 81% Analysis Date = 10/23/12 Pct Recovery = 81% Analysis Date = 10/12/12 Pct Recovery = 81% Analysis Date = 10/12/12 Pct Recovery = 81% Analysis Date = 10/02/12 Pct Recovery = 81% Analysis Date = 10/02/12 Pct Recovery = 81% Analysis Date = 09/22/12 Pct Recovery = 81% Analysis Date = 09/22/12 Pct Recovery = 81% Analysis Date = 09/12/12 Pct Recovery = 81% Analysis Date = 09/12/12 Pct Recovery = 81% Analysis Date = 09/02/12 Pct Recovery = 81% Analysis Date = 09/02/12 Pct Recovery = 81% Analysis Date = 08/22/12 Pct Recovery = 81% Analysis Date = 08/22/12 Pct Recovery = 81% Analysis Date = 08/12/12 Pct Recovery = 81% Analysis Date = 08/12/12 Pct Recovery = 81% Analysis Date = 08/02/12 Pct Recovery = 81% Analysis Date = 08/02/12 Pct Recovery = 81% Analysis Date = 07/23/12 Pct Recovery = 80% Analysis Date = 07/23/12 Pct Recovery = 80% Analysis Date = 07/13/12 Pct Recovery = 80% Analysis Date = 07/13/12 Pct Recovery = 80% Analysis Date = 07/02/12 Pct Recovery = 80% Analysis Date = 07/02/12 Pct Recovery = 80% Analysis Date = 06/22/12 Pct Recovery = 80% Analysis Date = 06/22/12 Pct Recovery = 80% Analysis Date = 06/12/12 Pct Recovery = 80% Analysis Date = 06/12/12 Pct Recovery = 80% Analysis Date = 06/02/12 Pct Recovery = 80% Analysis Date = 06/02/12 Pct Recovery = 80% Analysis Date = 05/23/12 Pct Recovery = 80% Analysis Date = 05/23/12 Pct Recovery = 80% Analysis Date = 05/12/12 Pct Recovery = 80% Analysis Date = 05/12/12 Pct Recovery = 80% Analysis Date = 05/02/12 Pct Recovery = 80% Analysis Date = 05/02/12 Pct Recovery = 80% Analysis Date = 04/22/12 Pct Recovery = 80% Analysis Date = 04/22/12 Pct Recovery = 80% Analysis Date = 04/12/12 Pct Recovery = 80% Analysis Date = 04/12/12 Pct Recovery = 80% Analysis Date = 04/02/12 Pct Recovery = 80% Analysis Date = 04/02/12 Pct Recovery = 80% Analysis Date = 03/22/12 Pct Recovery = 80% Analysis Date = 03/22/12 Pct Recovery = 80% Analysis Date = 03/12/12 Pct Recovery = 80% Analysis Date = 03/12/12 Pct Recovery = 80% Analysis Date = 03/02/12 Pct Recovery = 80% Analysis Date = 03/02/12 Pct Recovery = 80% Analysis Date = 02/21/12 Pct Recovery = 80% Analysis Date = 02/21/12 Pct Recovery = 80% Analysis Date = 02/11/12 Pct Recovery = 80% Analysis Date = 02/11/12 Pct Recovery = 80% Analysis Date = 01/31/12 Pct Recovery = 80% Analysis Date = 01/31/12 Pct Recovery = 80% Analysis Date = 01/21/12 Pct Recovery = 80% Analysis Date = 01/21/12 Pct Recovery = 80% Analysis Date = 01/11/12 Pct Recovery = 80% Analysis Date = 01/11/12 Pct Recovery = 80% Analysis Date = 01/01/12 Pct Recovery = 80% Analysis Date = 01/01/12 Pct Recovery = 80% Analysis Date = 12/22/11 Pct Recovery = 80% Analysis Date = 12/22/11 Pct Recovery = 80% Analysis Date = 12/11/11 Pct Recovery = 80% Analysis Date = 12/11/11 Pct Recovery = 80% Analysis Date = 12/01/11 Pct Recovery = 80% Analysis Date = 12/01/11 Pct Recovery = 80% Analysis Date = 11/21/11 Pct Recovery = 80% Analysis Date = 11/21/11 Pct Recovery = 80% Analysis Date = 11/11/11 Pct Recovery = 80% Analysis Date = 11/11/11 Pct Recovery = 80% Analysis Date = 11/01/11 Pct Recovery = 80% Analysis Date = 11/01/11 Pct Recovery = 80% Analysis Date = 10/21/11 Pct Recovery = 80% Analysis Date = 10/21/11 Pct Recovery = 80% Analysis Date = 10/11/11 Pct Recovery = 80% Analysis Date = 10/11/11 Pct Recovery = 80% Analysis Date = 10/01/11 Pct Recovery = 80% Analysis Date = 10/01/11 Pct Recovery = 80% Analysis Date = 09/21/11 Pct Recovery = 80% Analysis Date = 09/21/11 Pct Recovery = 80% Analysis Date = 09/11/11 Pct Recovery = 80% Analysis Date = 09/11/11 Pct Recovery = 80% Analysis Date = 08/31/11 Pct Recovery = 80% Analysis Date = 08/31/11 Pct Recovery = 80% Analysis Date = 08/21/11 Pct Recovery = 80% Analysis Date = 08/21/11 Pct Recovery = 80% Analysis Date = 08/11/11 Pct Recovery = 80% Analysis Date = 08/11/11 Pct Recovery = 80% Analysis Date = 08/01/11 Pct Recovery = 80% Analysis Date = 08/01/11 Pct Recovery = 80% Analysis Date = 07/22/11 Pct Recovery = 80% Analysis Date = 07/22/11 Pct Recovery = 80% Analysis Date = 07/11/11 Pct Recovery = 80% Analysis Date = 07/11/11 Pct Recovery = 80% Analysis Date = 07/01/11 Pct Recovery = 80% Analysis Date = 07/01/11 Pct Recovery = 80% Analysis Date = 06/21/11 Pct Recovery = 80% Analysis Date = 06/21/11 Pct Recovery = 80% Analysis Date = 06/11/11 Pct Recovery = 80% Analysis Date = 06/11/11 Pct Recovery = 80% Analysis Date = 06/01/11 Pct Recovery = 80% Analysis Date = 06/01/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/21/11 Pct Recovery = 80% Analysis Date = 05/11/11 Pct Recovery = 79% Analysis Date = 05/11/11 Pct Recovery = 79% Analysis Date = 05/01/11 Pct Recovery = 79% Analysis Date = 05/01/11 Pct Recovery = 79% Analysis Date = 04/21/11 Pct Recovery = 79% Analysis Date = 04/21/11 Pct Recovery = 79% Analysis Date = 04/11/11 Pct Recovery = 79% Analysis Date = 04/11/11 Pct Recovery = 79% Analysis Date = 03/31/11 Pct Recovery = 79% Analysis Date = 03/31/11 Pct Recovery = 79% Analysis Date = 03/21/11 Pct Recovery = 79% Analysis Date = 03/21/11 Pct Recovery = 79% Analysis Date = 03/11/11 Pct Recovery = 79% Analysis Date = 03/11/11 Pct Recovery = 79% Analysis Date = 03/01/11 Pct Recovery = 79% Analysis Date = 03/01/11 Pct Recovery = 79% Analysis Date = 02/19/11 Pct Recovery = 79% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 55 79% 15% 76% 15%
Total 55 79% 15% 76% 15%

Sample Statistics
DESULFINYLFIPRONIL

Characteristic N % % Basis
Plotted 55 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 55 .  
False Negatives 0 0% 0 out of 55
Not Spiked 114 .  
False Positives 1 1% 1 out of 114