BQS OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2033 , TESTIDCODE: 61635GCM39
Open Data Set

Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 72% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 29% Analysis Date = 02/06/13 SpikeMix = Restek A088380: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 64% Analysis Date = 12/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Crescent 05BB029: 100 µl Pct Recovery = 58% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 67% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 64% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 56% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 88% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 63% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 64% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 52% Analysis Date = 11/14/12 SpikeMix = Restek A088380: 50 µl & Crescent 05BB029: 50 µl Pct Recovery = 87% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 64% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 66% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 65% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 27% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 54% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 50% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 80% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 74% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 40% Analysis Date = 07/23/13 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl Pct Recovery = 65% Analysis Date = 03/18/13 SpikeMix = Restek A088380: 20 µl & Abs 052412: 20 µl Pct Recovery = 54% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 28% Analysis Date = 06/16/12 SpikeMix = Abs 052412: 20 µl Pct Recovery = 172% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 74% Analysis Date = 05/22/13 SpikeMix = Restek A088380: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 79% Analysis Date = 08/29/12 SpikeMix = Spex Organics T1120530013: 20 µl & Crescent 05BB029: 20 µl Pct Recovery = 106% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 70% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 39% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 80% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 78% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 91% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 113% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 92% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 99% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 113% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 54% Analysis Date = 08/26/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 82% Analysis Date = 08/17/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 07/28/16 Pct Recovery = 82% Analysis Date = 07/28/16 Pct Recovery = 82% Analysis Date = 07/18/16 Pct Recovery = 81% Analysis Date = 07/18/16 Pct Recovery = 81% Analysis Date = 07/09/16 Pct Recovery = 81% Analysis Date = 07/09/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/19/16 Pct Recovery = 80% Analysis Date = 06/19/16 Pct Recovery = 80% Analysis Date = 06/09/16 Pct Recovery = 80% Analysis Date = 06/09/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/30/16 Pct Recovery = 80% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/21/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/21/16 Pct Recovery = 78% Analysis Date = 04/21/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/02/16 Pct Recovery = 78% Analysis Date = 04/02/16 Pct Recovery = 78% Analysis Date = 03/23/16 Pct Recovery = 77% Analysis Date = 03/23/16 Pct Recovery = 77% Analysis Date = 03/13/16 Pct Recovery = 77% Analysis Date = 03/13/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 03/03/16 Pct Recovery = 77% Analysis Date = 02/23/16 Pct Recovery = 76% Analysis Date = 02/23/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 02/03/16 Pct Recovery = 76% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/24/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/15/16 Pct Recovery = 75% Analysis Date = 01/05/16 Pct Recovery = 75% Analysis Date = 01/05/16 Pct Recovery = 75% Analysis Date = 12/26/15 Pct Recovery = 74% Analysis Date = 12/26/15 Pct Recovery = 74% Analysis Date = 12/16/15 Pct Recovery = 74% Analysis Date = 12/16/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 12/06/15 Pct Recovery = 74% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/27/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/17/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 11/07/15 Pct Recovery = 73% Analysis Date = 10/28/15 Pct Recovery = 72% Analysis Date = 10/28/15 Pct Recovery = 72% Analysis Date = 10/19/15 Pct Recovery = 72% Analysis Date = 10/19/15 Pct Recovery = 72% Analysis Date = 10/09/15 Pct Recovery = 72% Analysis Date = 10/09/15 Pct Recovery = 72% Analysis Date = 09/29/15 Pct Recovery = 71% Analysis Date = 09/29/15 Pct Recovery = 71% Analysis Date = 09/19/15 Pct Recovery = 71% Analysis Date = 09/19/15 Pct Recovery = 71% Analysis Date = 09/09/15 Pct Recovery = 71% Analysis Date = 09/09/15 Pct Recovery = 71% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/31/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/21/15 Pct Recovery = 70% Analysis Date = 08/11/15 Pct Recovery = 70% Analysis Date = 08/11/15 Pct Recovery = 70% Analysis Date = 08/01/15 Pct Recovery = 69% Analysis Date = 08/01/15 Pct Recovery = 69% Analysis Date = 07/23/15 Pct Recovery = 69% Analysis Date = 07/23/15 Pct Recovery = 69% Analysis Date = 07/13/15 Pct Recovery = 69% Analysis Date = 07/13/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 69% Analysis Date = 07/03/15 Pct Recovery = 69% Analysis Date = 06/23/15 Pct Recovery = 68% Analysis Date = 06/23/15 Pct Recovery = 68% Analysis Date = 06/13/15 Pct Recovery = 68% Analysis Date = 06/13/15 Pct Recovery = 68% Analysis Date = 06/04/15 Pct Recovery = 68% Analysis Date = 06/04/15 Pct Recovery = 68% Analysis Date = 05/25/15 Pct Recovery = 67% Analysis Date = 05/25/15 Pct Recovery = 67% Analysis Date = 05/15/15 Pct Recovery = 67% Analysis Date = 05/15/15 Pct Recovery = 67% Analysis Date = 05/05/15 Pct Recovery = 67% Analysis Date = 05/05/15 Pct Recovery = 67% Analysis Date = 04/25/15 Pct Recovery = 67% Analysis Date = 04/25/15 Pct Recovery = 67% Analysis Date = 04/16/15 Pct Recovery = 67% Analysis Date = 04/16/15 Pct Recovery = 67% Analysis Date = 04/06/15 Pct Recovery = 66% Analysis Date = 04/06/15 Pct Recovery = 66% Analysis Date = 03/27/15 Pct Recovery = 66% Analysis Date = 03/27/15 Pct Recovery = 66% Analysis Date = 03/17/15 Pct Recovery = 66% Analysis Date = 03/17/15 Pct Recovery = 66% Analysis Date = 03/08/15 Pct Recovery = 66% Analysis Date = 03/08/15 Pct Recovery = 66% Analysis Date = 02/26/15 Pct Recovery = 65% Analysis Date = 02/26/15 Pct Recovery = 65% Analysis Date = 02/16/15 Pct Recovery = 65% Analysis Date = 02/16/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 02/06/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/27/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 65% Analysis Date = 01/18/15 Pct Recovery = 65% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 01/08/15 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 64% Analysis Date = 12/29/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/19/14 Pct Recovery = 64% Analysis Date = 12/10/14 Pct Recovery = 64% Analysis Date = 12/10/14 Pct Recovery = 64% Analysis Date = 11/30/14 Pct Recovery = 64% Analysis Date = 11/30/14 Pct Recovery = 64% Analysis Date = 11/20/14 Pct Recovery = 63% Analysis Date = 11/20/14 Pct Recovery = 63% Analysis Date = 11/10/14 Pct Recovery = 63% Analysis Date = 11/10/14 Pct Recovery = 63% Analysis Date = 10/31/14 Pct Recovery = 63% Analysis Date = 10/31/14 Pct Recovery = 63% Analysis Date = 10/22/14 Pct Recovery = 63% Analysis Date = 10/22/14 Pct Recovery = 63% Analysis Date = 10/12/14 Pct Recovery = 63% Analysis Date = 10/12/14 Pct Recovery = 63% Analysis Date = 10/02/14 Pct Recovery = 62% Analysis Date = 10/02/14 Pct Recovery = 62% Analysis Date = 09/22/14 Pct Recovery = 62% Analysis Date = 09/22/14 Pct Recovery = 62% Analysis Date = 09/13/14 Pct Recovery = 62% Analysis Date = 09/13/14 Pct Recovery = 62% Analysis Date = 09/03/14 Pct Recovery = 62% Analysis Date = 09/03/14 Pct Recovery = 62% Analysis Date = 08/24/14 Pct Recovery = 61% Analysis Date = 08/24/14 Pct Recovery = 61% Analysis Date = 08/14/14 Pct Recovery = 61% Analysis Date = 08/14/14 Pct Recovery = 61% Analysis Date = 08/04/14 Pct Recovery = 61% Analysis Date = 08/04/14 Pct Recovery = 61% Analysis Date = 07/26/14 Pct Recovery = 61% Analysis Date = 07/26/14 Pct Recovery = 61% Analysis Date = 07/16/14 Pct Recovery = 61% Analysis Date = 07/16/14 Pct Recovery = 61% Analysis Date = 07/06/14 Pct Recovery = 60% Analysis Date = 07/06/14 Pct Recovery = 60% Analysis Date = 06/26/14 Pct Recovery = 60% Analysis Date = 06/26/14 Pct Recovery = 60% Analysis Date = 06/17/14 Pct Recovery = 61% Analysis Date = 06/17/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 06/07/14 Pct Recovery = 61% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/28/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/18/14 Pct Recovery = 62% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 05/08/14 Pct Recovery = 63% Analysis Date = 04/29/14 Pct Recovery = 63% Analysis Date = 04/29/14 Pct Recovery = 63% Analysis Date = 04/19/14 Pct Recovery = 64% Analysis Date = 04/19/14 Pct Recovery = 64% Analysis Date = 04/09/14 Pct Recovery = 64% Analysis Date = 04/09/14 Pct Recovery = 64% Analysis Date = 03/30/14 Pct Recovery = 64% Analysis Date = 03/30/14 Pct Recovery = 64% Analysis Date = 03/21/14 Pct Recovery = 65% Analysis Date = 03/21/14 Pct Recovery = 65% Analysis Date = 03/11/14 Pct Recovery = 65% Analysis Date = 03/11/14 Pct Recovery = 65% Analysis Date = 03/01/14 Pct Recovery = 66% Analysis Date = 03/01/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 66% Analysis Date = 02/19/14 Pct Recovery = 66% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 02/09/14 Pct Recovery = 67% Analysis Date = 01/31/14 Pct Recovery = 67% Analysis Date = 01/31/14 Pct Recovery = 67% Analysis Date = 01/21/14 Pct Recovery = 68% Analysis Date = 01/21/14 Pct Recovery = 68% Analysis Date = 01/11/14 Pct Recovery = 68% Analysis Date = 01/11/14 Pct Recovery = 68% Analysis Date = 01/01/14 Pct Recovery = 69% Analysis Date = 01/01/14 Pct Recovery = 69% Analysis Date = 12/22/13 Pct Recovery = 69% Analysis Date = 12/22/13 Pct Recovery = 69% Analysis Date = 12/13/13 Pct Recovery = 70% Analysis Date = 12/13/13 Pct Recovery = 70% Analysis Date = 12/03/13 Pct Recovery = 70% Analysis Date = 12/03/13 Pct Recovery = 70% Analysis Date = 11/23/13 Pct Recovery = 71% Analysis Date = 11/23/13 Pct Recovery = 71% Analysis Date = 11/13/13 Pct Recovery = 71% Analysis Date = 11/13/13 Pct Recovery = 71% Analysis Date = 11/04/13 Pct Recovery = 71% Analysis Date = 11/04/13 Pct Recovery = 71% Analysis Date = 10/25/13 Pct Recovery = 72% Analysis Date = 10/25/13 Pct Recovery = 72% Analysis Date = 10/15/13 Pct Recovery = 72% Analysis Date = 10/15/13 Pct Recovery = 72% Analysis Date = 10/05/13 Pct Recovery = 72% Analysis Date = 10/05/13 Pct Recovery = 72% Analysis Date = 09/25/13 Pct Recovery = 72% Analysis Date = 09/25/13 Pct Recovery = 72% Analysis Date = 09/16/13 Pct Recovery = 72% Analysis Date = 09/16/13 Pct Recovery = 72% Analysis Date = 09/06/13 Pct Recovery = 72% Analysis Date = 09/06/13 Pct Recovery = 72% Analysis Date = 08/27/13 Pct Recovery = 71% Analysis Date = 08/27/13 Pct Recovery = 71% Analysis Date = 08/17/13 Pct Recovery = 71% Analysis Date = 08/17/13 Pct Recovery = 71% Analysis Date = 08/08/13 Pct Recovery = 71% Analysis Date = 08/08/13 Pct Recovery = 71% Analysis Date = 07/29/13 Pct Recovery = 71% Analysis Date = 07/29/13 Pct Recovery = 71% Analysis Date = 07/19/13 Pct Recovery = 71% Analysis Date = 07/19/13 Pct Recovery = 71% Analysis Date = 07/09/13 Pct Recovery = 71% Analysis Date = 07/09/13 Pct Recovery = 71% Analysis Date = 06/29/13 Pct Recovery = 71% Analysis Date = 06/29/13 Pct Recovery = 71% Analysis Date = 06/20/13 Pct Recovery = 70% Analysis Date = 06/20/13 Pct Recovery = 70% Analysis Date = 06/10/13 Pct Recovery = 70% Analysis Date = 06/10/13 Pct Recovery = 70% Analysis Date = 05/31/13 Pct Recovery = 70% Analysis Date = 05/31/13 Pct Recovery = 70% Analysis Date = 05/21/13 Pct Recovery = 70% Analysis Date = 05/21/13 Pct Recovery = 70% Analysis Date = 05/12/13 Pct Recovery = 70% Analysis Date = 05/12/13 Pct Recovery = 70% Analysis Date = 05/02/13 Pct Recovery = 70% Analysis Date = 05/02/13 Pct Recovery = 70% Analysis Date = 04/22/13 Pct Recovery = 70% Analysis Date = 04/22/13 Pct Recovery = 70% Analysis Date = 04/12/13 Pct Recovery = 69% Analysis Date = 04/12/13 Pct Recovery = 69% Analysis Date = 04/02/13 Pct Recovery = 69% Analysis Date = 04/02/13 Pct Recovery = 69% Analysis Date = 03/24/13 Pct Recovery = 69% Analysis Date = 03/24/13 Pct Recovery = 69% Analysis Date = 03/14/13 Pct Recovery = 69% Analysis Date = 03/14/13 Pct Recovery = 69% Analysis Date = 03/04/13 Pct Recovery = 69% Analysis Date = 03/04/13 Pct Recovery = 69% Analysis Date = 02/22/13 Pct Recovery = 70% Analysis Date = 02/22/13 Pct Recovery = 70% Analysis Date = 02/13/13 Pct Recovery = 70% Analysis Date = 02/13/13 Pct Recovery = 70% Analysis Date = 02/03/13 Pct Recovery = 71% Analysis Date = 02/03/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 71% Analysis Date = 01/24/13 Pct Recovery = 71% Analysis Date = 01/14/13 Pct Recovery = 71% Analysis Date = 01/14/13 Pct Recovery = 71% Analysis Date = 01/04/13 Pct Recovery = 72% Analysis Date = 01/04/13 Pct Recovery = 72% Analysis Date = 12/26/12 Pct Recovery = 73% Analysis Date = 12/26/12 Pct Recovery = 73% Analysis Date = 12/16/12 Pct Recovery = 74% Analysis Date = 12/16/12 Pct Recovery = 74% Analysis Date = 12/06/12 Pct Recovery = 74% Analysis Date = 12/06/12 Pct Recovery = 74% Analysis Date = 11/26/12 Pct Recovery = 75% Analysis Date = 11/26/12 Pct Recovery = 75% Analysis Date = 11/17/12 Pct Recovery = 76% Analysis Date = 11/17/12 Pct Recovery = 76% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 11/07/12 Pct Recovery = 77% Analysis Date = 10/28/12 Pct Recovery = 78% Analysis Date = 10/28/12 Pct Recovery = 78% Analysis Date = 10/18/12 Pct Recovery = 79% Analysis Date = 10/18/12 Pct Recovery = 79% Analysis Date = 10/08/12 Pct Recovery = 80% Analysis Date = 10/08/12 Pct Recovery = 80% Analysis Date = 09/29/12 Pct Recovery = 81% Analysis Date = 09/29/12 Pct Recovery = 81% Analysis Date = 09/19/12 Pct Recovery = 82% Analysis Date = 09/19/12 Pct Recovery = 82% Analysis Date = 09/09/12 Pct Recovery = 83% Analysis Date = 09/09/12 Pct Recovery = 83% Analysis Date = 08/30/12 Pct Recovery = 84% Analysis Date = 08/30/12 Pct Recovery = 84% Analysis Date = 08/20/12 Pct Recovery = 84% Analysis Date = 08/20/12 Pct Recovery = 84% Analysis Date = 08/11/12 Pct Recovery = 84% Analysis Date = 08/11/12 Pct Recovery = 84% Analysis Date = 08/01/12 Pct Recovery = 85% Analysis Date = 08/01/12 Pct Recovery = 85% Analysis Date = 07/22/12 Pct Recovery = 85% Analysis Date = 07/22/12 Pct Recovery = 85% Analysis Date = 07/12/12 Pct Recovery = 85% Analysis Date = 07/12/12 Pct Recovery = 85% Analysis Date = 07/03/12 Pct Recovery = 85% Analysis Date = 07/03/12 Pct Recovery = 85% Analysis Date = 06/23/12 Pct Recovery = 85% Analysis Date = 06/23/12 Pct Recovery = 85% Analysis Date = 06/13/12 Pct Recovery = 85% Analysis Date = 06/13/12 Pct Recovery = 85% Analysis Date = 06/03/12 Pct Recovery = 85% Analysis Date = 06/03/12 Pct Recovery = 85% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/24/12 Pct Recovery = 86% Analysis Date = 05/15/12 Pct Recovery = 86% Analysis Date = 05/15/12 Pct Recovery = 86% Analysis Date = 05/05/12 Pct Recovery = 86% Analysis Date = 05/05/12 Pct Recovery = 86% Analysis Date = 04/25/12 Pct Recovery = 86% Analysis Date = 04/25/12 Pct Recovery = 86% Analysis Date = 04/15/12 Pct Recovery = 86% Analysis Date = 04/15/12 Pct Recovery = 86% Analysis Date = 04/06/12 Pct Recovery = 86% Analysis Date = 04/06/12 Pct Recovery = 86% Analysis Date = 03/27/12 Pct Recovery = 87% Analysis Date = 03/27/12 Pct Recovery = 87% Analysis Date = 03/17/12 Pct Recovery = 87% Analysis Date = 03/17/12 Pct Recovery = 87% Analysis Date = 03/07/12 Pct Recovery = 87% Analysis Date = 03/07/12 Pct Recovery = 87% Analysis Date = 02/26/12 Pct Recovery = 87% Analysis Date = 02/26/12 Pct Recovery = 87% Analysis Date = 02/17/12 Pct Recovery = 87% Analysis Date = 02/17/12 Pct Recovery = 87% Analysis Date = 02/07/12 Pct Recovery = 87% Analysis Date = 02/07/12 Pct Recovery = 87% Analysis Date = 01/28/12 Pct Recovery = 87% Analysis Date = 01/28/12 Pct Recovery = 87% Analysis Date = 01/18/12 Pct Recovery = 88% Analysis Date = 01/18/12 Pct Recovery = 88% Analysis Date = 01/09/12 Pct Recovery = 88% Analysis Date = 01/09/12 Pct Recovery = 88% Analysis Date = 12/30/11 Pct Recovery = 88% Analysis Date = 12/30/11 Pct Recovery = 88% Analysis Date = 12/20/11 Pct Recovery = 88% Analysis Date = 12/20/11 Pct Recovery = 88% Analysis Date = 12/10/11 Pct Recovery = 88% Analysis Date = 12/10/11 Pct Recovery = 88% Analysis Date = 11/30/11 Pct Recovery = 88% Analysis Date = 11/30/11 Pct Recovery = 88% Analysis Date = 11/21/11 Pct Recovery = 88% Analysis Date = 11/21/11 Pct Recovery = 88% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 11/11/11 Pct Recovery = 89% Analysis Date = 11/01/11 Pct Recovery = 89% Analysis Date = 11/01/11 Pct Recovery = 89% Analysis Date = 10/22/11 Pct Recovery = 89% Analysis Date = 10/22/11 Pct Recovery = 89% Analysis Date = 10/13/11 Pct Recovery = 89% Analysis Date = 10/13/11 Pct Recovery = 89% Analysis Date = 10/03/11 Pct Recovery = 89% Analysis Date = 10/03/11 Pct Recovery = 89% Analysis Date = 09/23/11 Pct Recovery = 89% Analysis Date = 09/23/11 Pct Recovery = 89% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/13/11 Pct Recovery = 90% Analysis Date = 09/03/11 Pct Recovery = 90% Analysis Date = 09/03/11 Pct Recovery = 90% Analysis Date = 08/25/11 Pct Recovery = 90% Analysis Date = 08/25/11 Pct Recovery = 90% Analysis Date = 08/15/11 Pct Recovery = 90% Analysis Date = 08/15/11 Pct Recovery = 90% Analysis Date = 08/05/11 Pct Recovery = 90% Analysis Date = 08/05/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/26/11 Pct Recovery = 90% Analysis Date = 07/17/11 Pct Recovery = 90% Analysis Date = 07/17/11 Pct Recovery = 90% Analysis Date = 07/07/11 Pct Recovery = 91% Analysis Date = 07/07/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/27/11 Pct Recovery = 91% Analysis Date = 06/17/11 Pct Recovery = 91% Analysis Date = 06/17/11 Pct Recovery = 91% Analysis Date = 06/07/11 Pct Recovery = 91% Analysis Date = 06/07/11 Pct Recovery = 91% Analysis Date = 05/29/11 Pct Recovery = 91% Analysis Date = 05/29/11 Pct Recovery = 91% Analysis Date = 05/19/11 Pct Recovery = 91% Analysis Date = 05/19/11 Pct Recovery = 91% Analysis Date = 05/09/11 Pct Recovery = 91% Analysis Date = 05/09/11 Pct Recovery = 91% Analysis Date = 04/29/11 Pct Recovery = 92% Analysis Date = 04/29/11 Pct Recovery = 92% Analysis Date = 04/20/11 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL-OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 45 71% 25% 65% 16%
Total 45 71% 25% 65% 16%

Sample Statistics
AZINPHOS-METHYL-OXON

Characteristic N % % Basis
Plotted 45 78% Spiked
Estimated Values 45 78% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 58 .  
False Negatives 12 21% 12 out of 58
Not Spiked 111 .  
False Positives 1 1% 1 out of 110