BQS Organic Blind Sample Program
False Positives & False Negatives
FIPRONIL SULFONE
Method: 2033 Testid: 62168GCM29
Open Data Set

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newdate = 09/13/11 falseneg = -0.01 newdate = 01/21/16 falsepos = 0.0139 newdate = 09/05/15 falsepos = 0.0114 newdate = 07/21/15 falsepos = 0.0052 newdate = 02/09/16 CENC_VAL = 0.057 newdate = 02/08/16 CENC_VAL = 0.063 newdate = 01/28/16 CENC_VAL = 0.023 newdate = 01/26/16 CENC_VAL = 0.036 newdate = 09/24/15 CENC_VAL = 0.100 newdate = 09/17/15 CENC_VAL = 0.111 newdate = 08/19/15 CENC_VAL = 0.029 newdate = 07/31/15 CENC_VAL = 0.033 newdate = 07/10/15 CENC_VAL = 0.039 newdate = 06/17/15 CENC_VAL = 0.057 newdate = 05/12/15 CENC_VAL = 0.051 newdate = 02/21/15 CENC_VAL = 0.085 newdate = 01/31/15 CENC_VAL = 0.043 newdate = 12/04/14 CENC_VAL = 0.072 newdate = 11/19/14 CENC_VAL = 0.064 newdate = 10/21/14 CENC_VAL = 0.052 newdate = 10/04/14 CENC_VAL = 0.079 newdate = 09/22/14 CENC_VAL = 0.047 newdate = 08/27/14 CENC_VAL = 0.060 newdate = 07/17/14 CENC_VAL = 0.035 newdate = 07/09/14 CENC_VAL = 0.089 newdate = 06/30/14 CENC_VAL = 0.030 newdate = 06/26/14 CENC_VAL = 0.051 newdate = 05/28/14 CENC_VAL = 0.049 newdate = 05/20/14 CENC_VAL = 0.071 newdate = 04/29/14 CENC_VAL = 0.028 newdate = 03/05/14 CENC_VAL = 0.047 newdate = 02/12/14 CENC_VAL = 0.094 newdate = 01/10/14 CENC_VAL = 0.043 newdate = 01/08/14 CENC_VAL = 0.052 newdate = 11/23/13 CENC_VAL = 0.078 newdate = 11/09/13 CENC_VAL = 0.052 newdate = 09/24/13 CENC_VAL = 0.111 newdate = 09/20/13 CENC_VAL = 0.219 newdate = 08/19/13 CENC_VAL = 0.110 newdate = 07/11/13 CENC_VAL = 0.050 newdate = 06/11/13 CENC_VAL = 0.062 newdate = 06/05/13 CENC_VAL = 0.254 newdate = 04/22/13 CENC_VAL = 0.081 newdate = 04/02/13 CENC_VAL = 0.088 newdate = 03/07/13 CENC_VAL = 0.035 newdate = 02/22/13 CENC_VAL = 0.041 newdate = 01/17/13 CENC_VAL = 0.080 newdate = 01/15/13 CENC_VAL = 0.079 newdate = 12/06/12 CENC_VAL = 0.155 newdate = 11/20/12 CENC_VAL = 0.158 newdate = 10/18/12 CENC_VAL = 0.073 newdate = 10/12/12 CENC_VAL = 0.096 newdate = 09/17/12 CENC_VAL = 0.030 newdate = 09/05/12 CENC_VAL = 0.033 newdate = 08/14/12 CENC_VAL = 0.057 newdate = 07/14/12 CENC_VAL = 0.045 newdate = 05/15/12 CENC_VAL = 0.088 newdate = 03/09/12 CENC_VAL = 0.049 newdate = 02/14/12 CENC_VAL = 0.036 newdate = 12/22/11 CENC_VAL = 0.054 newdate = 12/04/11 CENC_VAL = 0.055 newdate = 11/17/11 CENC_VAL = 0.099 newdate = 11/01/11 CENC_VAL = 0.086 newdate = 10/02/11 CENC_VAL = 0.107 newdate = 09/24/11 CENC_VAL = 0.051 newdate = 09/13/11 CENC_VAL = 0.052 newdate = 09/01/11 CENC_VAL = 0.074 newdate = 08/17/11 CENC_VAL = 0.069 newdate = 07/20/11 CENC_VAL = 0.067 newdate = 07/14/11 CENC_VAL = 0.100 newdate = 06/22/11 CENC_VAL = 0.047 newdate = 06/20/11 CENC_VAL = 0.081 newdate = 05/25/11 CENC_VAL = 0.048 newdate = 04/23/11 CENC_VAL = 0.044 newdate = 04/20/11 CENC_VAL = 0.079 newdate = 03/30/11 CENC_VAL = 0.042 newdate = 03/08/11 CENC_VAL = 0.070 newdate = 03/05/11 CENC_VAL = 0.036 newdate = 02/09/11 CENC_VAL = 0.081 newdate = 01/28/11 CENC_VAL = 0.105 newdate = 01/20/11 CENC_VAL = 0.090 newdate = 01/18/11 CENC_VAL = 0.034 newdate = 01/09/11 CENC_VAL = 0.056 newdate = 12/16/10 CENC_VAL = 0.039 newdate = 12/14/10 CENC_VAL = 0.078 newdate = 10/19/10 CENC_VAL = 0.047 newdate = 09/09/10 CENC_VAL = 0.087 newdate = 08/25/10 CENC_VAL = 0.049 newdate = 07/21/10 CENC_VAL = 0.047 newdate = 06/30/10 CENC_VAL = 0.023 newdate = 06/03/10 CENC_VAL = 0.024 newdate = 05/07/10 CENC_VAL = 0.051 newdate = 03/24/10 CENC_VAL = 0.048 newdate = 02/09/16 REPORTING LEVEL = 0.024 newdate = 02/08/16 REPORTING LEVEL = 0.024 newdate = 02/08/16 REPORTING LEVEL = 0.024 newdate = 01/28/16 REPORTING LEVEL = 0.024 newdate = 01/28/16 REPORTING LEVEL = 0.024 newdate = 01/26/16 REPORTING LEVEL = 0.024 newdate = 01/26/16 REPORTING LEVEL = 0.024 newdate = 01/21/16 REPORTING LEVEL = 0.024 newdate = 01/21/16 REPORTING LEVEL = 0.024 newdate = 09/24/15 REPORTING LEVEL = 0.024 newdate = 09/24/15 REPORTING LEVEL = 0.024 newdate = 09/17/15 REPORTING LEVEL = 0.024 newdate = 09/17/15 REPORTING LEVEL = 0.024 newdate = 09/05/15 REPORTING LEVEL = 0.024 newdate = 09/05/15 REPORTING LEVEL = 0.024 newdate = 08/19/15 REPORTING LEVEL = 0.024 newdate = 08/19/15 REPORTING LEVEL = 0.024 newdate = 07/31/15 REPORTING LEVEL = 0.024 newdate = 07/31/15 REPORTING LEVEL = 0.024 newdate = 07/21/15 REPORTING LEVEL = 0.024 newdate = 07/21/15 REPORTING LEVEL = 0.024 newdate = 07/10/15 REPORTING LEVEL = 0.024 newdate = 07/10/15 REPORTING LEVEL = 0.024 newdate = 06/17/15 REPORTING LEVEL = 0.024 newdate = 06/17/15 REPORTING LEVEL = 0.024 newdate = 05/12/15 REPORTING LEVEL = 0.024 newdate = 05/12/15 REPORTING LEVEL = 0.024 newdate = 02/21/15 REPORTING LEVEL = 0.024 newdate = 02/21/15 REPORTING LEVEL = 0.024 newdate = 01/31/15 REPORTING LEVEL = 0.024 newdate = 01/31/15 REPORTING LEVEL = 0.024 newdate = 12/04/14 REPORTING LEVEL = 0.024 newdate = 12/04/14 REPORTING LEVEL = 0.024 newdate = 11/19/14 REPORTING LEVEL = 0.024 newdate = 11/19/14 REPORTING LEVEL = 0.024 newdate = 10/21/14 REPORTING LEVEL = 0.024 newdate = 10/21/14 REPORTING LEVEL = 0.024 newdate = 10/04/14 REPORTING LEVEL = 0.024 newdate = 10/04/14 REPORTING LEVEL = 0.024 newdate = 09/22/14 REPORTING LEVEL = 0.024 newdate = 09/22/14 REPORTING LEVEL = 0.024 newdate = 08/27/14 REPORTING LEVEL = 0.024 newdate = 08/27/14 REPORTING LEVEL = 0.024 newdate = 07/17/14 REPORTING LEVEL = 0.024 newdate = 07/17/14 REPORTING LEVEL = 0.024 newdate = 07/09/14 REPORTING LEVEL = 0.024 newdate = 07/09/14 REPORTING LEVEL = 0.024 newdate = 06/30/14 REPORTING LEVEL = 0.024 newdate = 06/30/14 REPORTING LEVEL = 0.024 newdate = 06/26/14 REPORTING LEVEL = 0.024 newdate = 06/26/14 REPORTING LEVEL = 0.024 newdate = 05/28/14 REPORTING LEVEL = 0.024 newdate = 05/28/14 REPORTING LEVEL = 0.024 newdate = 05/20/14 REPORTING LEVEL = 0.024 newdate = 05/20/14 REPORTING LEVEL = 0.024 newdate = 04/29/14 REPORTING LEVEL = 0.024 newdate = 04/29/14 REPORTING LEVEL = 0.024 newdate = 03/05/14 REPORTING LEVEL = 0.024 newdate = 03/05/14 REPORTING LEVEL = 0.024 newdate = 02/12/14 REPORTING LEVEL = 0.024 newdate = 02/12/14 REPORTING LEVEL = 0.024 newdate = 01/10/14 REPORTING LEVEL = 0.024 newdate = 01/10/14 REPORTING LEVEL = 0.024 newdate = 01/08/14 REPORTING LEVEL = 0.024 newdate = 01/08/14 REPORTING LEVEL = 0.024 newdate = 11/23/13 REPORTING LEVEL = 0.024 newdate = 11/23/13 REPORTING LEVEL = 0.024 newdate = 11/09/13 REPORTING LEVEL = 0.024 newdate = 11/09/13 REPORTING LEVEL = 0.024 newdate = 09/24/13 REPORTING LEVEL = 0.024 newdate = 09/24/13 REPORTING LEVEL = 0.024 newdate = 09/20/13 REPORTING LEVEL = 0.024 newdate = 09/20/13 REPORTING LEVEL = 0.024 newdate = 08/19/13 REPORTING LEVEL = 0.024 newdate = 08/19/13 REPORTING LEVEL = 0.024 newdate = 07/11/13 REPORTING LEVEL = 0.024 newdate = 07/11/13 REPORTING LEVEL = 0.024 newdate = 06/11/13 REPORTING LEVEL = 0.024 newdate = 06/11/13 REPORTING LEVEL = 0.024 newdate = 06/05/13 REPORTING LEVEL = 0.024 newdate = 06/05/13 REPORTING LEVEL = 0.024 newdate = 04/22/13 REPORTING LEVEL = 0.024 newdate = 04/22/13 REPORTING LEVEL = 0.024 newdate = 04/02/13 REPORTING LEVEL = 0.024 newdate = 04/02/13 REPORTING LEVEL = 0.024 newdate = 03/07/13 REPORTING LEVEL = 0.024 newdate = 03/07/13 REPORTING LEVEL = 0.024 newdate = 02/22/13 REPORTING LEVEL = 0.024 newdate = 02/22/13 REPORTING LEVEL = 0.024 newdate = 01/17/13 REPORTING LEVEL = 0.024 newdate = 01/17/13 REPORTING LEVEL = 0.024 newdate = 01/15/13 REPORTING LEVEL = 0.024 newdate = 01/15/13 REPORTING LEVEL = 0.024 newdate = 12/06/12 REPORTING LEVEL = 0.024 newdate = 12/06/12 REPORTING LEVEL = 0.024 newdate = 11/20/12 REPORTING LEVEL = 0.024 newdate = 11/20/12 REPORTING LEVEL = 0.024 newdate = 10/18/12 REPORTING LEVEL = 0.024 newdate = 10/18/12 REPORTING LEVEL = 0.024 newdate = 10/12/12 REPORTING LEVEL = 0.024 newdate = 10/12/12 REPORTING LEVEL = 0.024 newdate = 09/17/12 REPORTING LEVEL = 0.024 newdate = 09/17/12 REPORTING LEVEL = 0.024 newdate = 09/05/12 REPORTING LEVEL = 0.024 newdate = 09/05/12 REPORTING LEVEL = 0.024 newdate = 08/14/12 REPORTING LEVEL = 0.024 newdate = 08/14/12 REPORTING LEVEL = 0.024 newdate = 07/14/12 REPORTING LEVEL = 0.024 newdate = 07/14/12 REPORTING LEVEL = 0.024 newdate = 05/15/12 REPORTING LEVEL = 0.024 newdate = 05/15/12 REPORTING LEVEL = 0.024 newdate = 03/09/12 REPORTING LEVEL = 0.024 newdate = 03/09/12 REPORTING LEVEL = 0.024 newdate = 02/14/12 REPORTING LEVEL = 0.024 newdate = 02/14/12 REPORTING LEVEL = 0.024 newdate = 12/22/11 REPORTING LEVEL = 0.024 newdate = 12/22/11 REPORTING LEVEL = 0.024 newdate = 12/04/11 REPORTING LEVEL = 0.024 newdate = 12/04/11 REPORTING LEVEL = 0.024 newdate = 11/17/11 REPORTING LEVEL = 0.024 newdate = 11/17/11 REPORTING LEVEL = 0.024 newdate = 11/01/11 REPORTING LEVEL = 0.024 newdate = 11/01/11 REPORTING LEVEL = 0.024 newdate = 10/02/11 REPORTING LEVEL = 0.024 newdate = 10/02/11 REPORTING LEVEL = 0.024 newdate = 09/24/11 REPORTING LEVEL = 0.024 newdate = 09/24/11 REPORTING LEVEL = 0.024 newdate = 09/13/11 REPORTING LEVEL = 0.024 newdate = 09/13/11 REPORTING LEVEL = 0.024 newdate = 09/13/11 REPORTING LEVEL = 0.024 newdate = 09/13/11 REPORTING LEVEL = 0.024 newdate = 09/01/11 REPORTING LEVEL = 0.024 newdate = 09/01/11 REPORTING LEVEL = 0.024 newdate = 08/17/11 REPORTING LEVEL = 0.024 newdate = 08/17/11 REPORTING LEVEL = 0.024 newdate = 07/20/11 REPORTING LEVEL = 0.024 newdate = 07/20/11 REPORTING LEVEL = 0.024 newdate = 07/14/11 REPORTING LEVEL = 0.024 newdate = 07/14/11 REPORTING LEVEL = 0.024 newdate = 06/22/11 REPORTING LEVEL = 0.024 newdate = 06/22/11 REPORTING LEVEL = 0.024 newdate = 06/20/11 REPORTING LEVEL = 0.024 newdate = 06/20/11 REPORTING LEVEL = 0.024 newdate = 05/25/11 REPORTING LEVEL = 0.024 newdate = 05/25/11 REPORTING LEVEL = 0.024 newdate = 04/23/11 REPORTING LEVEL = 0.024 newdate = 04/23/11 REPORTING LEVEL = 0.024 newdate = 04/20/11 REPORTING LEVEL = 0.024 newdate = 04/20/11 REPORTING LEVEL = 0.024 newdate = 03/30/11 REPORTING LEVEL = 0.024 newdate = 03/30/11 REPORTING LEVEL = 0.024 newdate = 03/08/11 REPORTING LEVEL = 0.024 newdate = 03/08/11 REPORTING LEVEL = 0.024 newdate = 03/05/11 REPORTING LEVEL = 0.024 newdate = 03/05/11 REPORTING LEVEL = 0.024 newdate = 02/09/11 REPORTING LEVEL = 0.024 newdate = 02/09/11 REPORTING LEVEL = 0.024 newdate = 01/28/11 REPORTING LEVEL = 0.024 newdate = 01/28/11 REPORTING LEVEL = 0.024 newdate = 01/20/11 REPORTING LEVEL = 0.024 newdate = 01/20/11 REPORTING LEVEL = 0.024 newdate = 01/18/11 REPORTING LEVEL = 0.024 newdate = 01/18/11 REPORTING LEVEL = 0.024 newdate = 01/09/11 REPORTING LEVEL = 0.024 newdate = 01/09/11 REPORTING LEVEL = 0.024 newdate = 12/16/10 REPORTING LEVEL = 0.024 newdate = 12/16/10 REPORTING LEVEL = 0.024 newdate = 12/14/10 REPORTING LEVEL = 0.024 newdate = 12/14/10 REPORTING LEVEL = 0.024 newdate = 10/19/10 REPORTING LEVEL = 0.024 newdate = 10/19/10 REPORTING LEVEL = 0.024 newdate = 09/09/10 REPORTING LEVEL = 0.024 newdate = 09/09/10 REPORTING LEVEL = 0.024 newdate = 08/25/10 REPORTING LEVEL = 0.024 newdate = 08/25/10 REPORTING LEVEL = 0.024 newdate = 07/21/10 REPORTING LEVEL = 0.024 newdate = 07/21/10 REPORTING LEVEL = 0.024 newdate = 06/30/10 REPORTING LEVEL = 0.024 newdate = 06/30/10 REPORTING LEVEL = 0.024 newdate = 06/03/10 REPORTING LEVEL = 0.024 newdate = 06/03/10 REPORTING LEVEL = 0.024 newdate = 05/07/10 REPORTING LEVEL = 0.024 newdate = 05/07/10 REPORTING LEVEL = 0.024 newdate = 03/24/10 REPORTING LEVEL = 0.024 Y = 0
The SGPlot Procedure

Updated 06/06/2016

False Positive & Negative Listing for FIPRONIL SULFONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20112310030 ERA 0318-13-02.2: 40 µl 0.024 09/13/11 < 0.024 0.1192
False Positive 20151900132 Abs 040615: 40 µl & Abs 041415: 40 µl 0.024 07/21/15 . 0.0052 0
  20152330039 Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl 0.024 09/05/15 . 0.0114 0
  20152750006 Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl 0.024 01/21/16 . 0.0139 0

Updated 06/06/2016