BQS Organic Blind Sample Program
False Positives & False Negatives
FIPRONIL SULFIDE
Method: 2033 Testid: 62167GCM29
Open Data Set

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newdate = 06/20/11 falseneg = -0.01 newdate = 09/17/15 falsepos = 0.0048 newdate = 05/15/12 falsepos = 0.0037 newdate = 02/14/12 falsepos = 0.0036 newdate = 12/04/11 falsepos = 0.0054 newdate = 11/17/11 falsepos = 0.0043 newdate = 11/01/11 falsepos = 0.0052 newdate = 10/02/11 falsepos = 0.0081 newdate = 09/24/11 falsepos = 0.0027 newdate = 09/13/11 falsepos = 0.0021 newdate = 09/01/11 falsepos = 0.0083 newdate = 07/19/11 falsepos = 0.0058 newdate = 07/13/11 falsepos = 0.0051 newdate = 06/20/11 falsepos = 0.0053 newdate = 04/23/11 falsepos = 0.0041 newdate = 03/30/11 falsepos = 0.0027 newdate = 03/08/11 falsepos = 0.0095 newdate = 02/09/11 falsepos = 0.0061 newdate = 01/28/11 falsepos = 0.0098 newdate = 01/09/11 falsepos = 0.0032 newdate = 02/09/16 CENC_VAL = 0.039 newdate = 02/02/16 CENC_VAL = 0.021 newdate = 01/26/16 CENC_VAL = 0.021 newdate = 01/21/16 CENC_VAL = 0.085 newdate = 09/24/15 CENC_VAL = 0.087 newdate = 09/05/15 CENC_VAL = 0.033 newdate = 08/19/15 CENC_VAL = 0.018 newdate = 07/21/15 CENC_VAL = 0.049 newdate = 06/17/15 CENC_VAL = 0.044 newdate = 05/12/15 CENC_VAL = 0.023 newdate = 02/21/15 CENC_VAL = 0.060 newdate = 01/31/15 CENC_VAL = 0.032 newdate = 12/04/14 CENC_VAL = 0.064 newdate = 11/19/14 CENC_VAL = 0.052 newdate = 10/21/14 CENC_VAL = 0.034 newdate = 10/04/14 CENC_VAL = 0.057 newdate = 09/22/14 CENC_VAL = 0.035 newdate = 08/27/14 CENC_VAL = 0.051 newdate = 07/17/14 CENC_VAL = 0.027 newdate = 07/09/14 CENC_VAL = 0.057 newdate = 06/30/14 CENC_VAL = 0.026 newdate = 06/26/14 CENC_VAL = 0.037 newdate = 05/28/14 CENC_VAL = 0.023 newdate = 05/20/14 CENC_VAL = 0.067 newdate = 04/29/14 CENC_VAL = 0.032 newdate = 03/05/14 CENC_VAL = 0.037 newdate = 02/12/14 CENC_VAL = 0.097 newdate = 01/10/14 CENC_VAL = 0.036 newdate = 01/08/14 CENC_VAL = 0.046 newdate = 11/23/13 CENC_VAL = 0.056 newdate = 11/09/13 CENC_VAL = 0.042 newdate = 09/24/13 CENC_VAL = 0.111 newdate = 09/20/13 CENC_VAL = 0.234 newdate = 08/19/13 CENC_VAL = 0.119 newdate = 07/11/13 CENC_VAL = 0.033 newdate = 06/11/13 CENC_VAL = 0.052 newdate = 06/05/13 CENC_VAL = 0.142 newdate = 04/22/13 CENC_VAL = 0.073 newdate = 04/02/13 CENC_VAL = 0.068 newdate = 03/07/13 CENC_VAL = 0.030 newdate = 02/22/13 CENC_VAL = 0.027 newdate = 01/17/13 CENC_VAL = 0.076 newdate = 01/15/13 CENC_VAL = 0.061 newdate = 12/06/12 CENC_VAL = 0.176 newdate = 11/20/12 CENC_VAL = 0.133 newdate = 10/18/12 CENC_VAL = 0.070 newdate = 10/12/12 CENC_VAL = 0.092 newdate = 09/17/12 CENC_VAL = 0.034 newdate = 09/05/12 CENC_VAL = 0.035 newdate = 08/14/12 CENC_VAL = 0.046 newdate = 07/14/12 CENC_VAL = 0.033 newdate = 06/02/12 CENC_VAL = 0.048 newdate = 05/08/12 CENC_VAL = 0.071 newdate = 04/05/12 CENC_VAL = 0.064 newdate = 03/05/12 CENC_VAL = 0.045 newdate = 01/27/12 CENC_VAL = 0.083 newdate = 12/21/11 CENC_VAL = 0.106 newdate = 12/03/11 CENC_VAL = 0.076 newdate = 11/17/11 CENC_VAL = 0.053 newdate = 10/25/11 CENC_VAL = 0.049 newdate = 09/29/11 CENC_VAL = 0.089 newdate = 09/19/11 CENC_VAL = 0.049 newdate = 09/13/11 CENC_VAL = 0.092 newdate = 07/28/11 CENC_VAL = 0.056 newdate = 07/07/11 CENC_VAL = 0.093 newdate = 06/22/11 CENC_VAL = 0.071 newdate = 05/14/11 CENC_VAL = 0.043 newdate = 04/20/11 CENC_VAL = 0.092 newdate = 04/13/11 CENC_VAL = 0.034 newdate = 03/23/11 CENC_VAL = 0.066 newdate = 03/05/11 CENC_VAL = 0.028 newdate = 02/28/11 CENC_VAL = 0.076 newdate = 02/19/11 CENC_VAL = 0.035 newdate = 02/08/11 CENC_VAL = 0.033 newdate = 01/21/11 CENC_VAL = 0.051 newdate = 01/20/11 CENC_VAL = 0.111 newdate = 01/13/11 CENC_VAL = 0.095 newdate = 01/11/11 CENC_VAL = 0.099 newdate = 12/16/10 CENC_VAL = 0.050 newdate = 12/14/10 CENC_VAL = 0.086 newdate = 10/19/10 CENC_VAL = 0.047 newdate = 09/09/10 CENC_VAL = 0.080 newdate = 08/25/10 CENC_VAL = 0.054 newdate = 07/21/10 CENC_VAL = 0.060 newdate = 06/30/10 CENC_VAL = 0.028 newdate = 06/03/10 CENC_VAL = 0.021 newdate = 05/07/10 CENC_VAL = 0.045 newdate = 03/24/10 CENC_VAL = 0.040 newdate = 02/09/16 REPORTING LEVEL = 0.016 newdate = 02/02/16 REPORTING LEVEL = 0.016 newdate = 02/02/16 REPORTING LEVEL = 0.016 newdate = 01/26/16 REPORTING LEVEL = 0.016 newdate = 01/26/16 REPORTING LEVEL = 0.016 newdate = 01/21/16 REPORTING LEVEL = 0.016 newdate = 01/21/16 REPORTING LEVEL = 0.016 newdate = 09/24/15 REPORTING LEVEL = 0.016 newdate = 09/24/15 REPORTING LEVEL = 0.016 newdate = 09/17/15 REPORTING LEVEL = 0.016 newdate = 09/17/15 REPORTING LEVEL = 0.016 newdate = 09/05/15 REPORTING LEVEL = 0.016 newdate = 09/05/15 REPORTING LEVEL = 0.016 newdate = 08/19/15 REPORTING LEVEL = 0.016 newdate = 08/19/15 REPORTING LEVEL = 0.016 newdate = 07/21/15 REPORTING LEVEL = 0.016 newdate = 07/21/15 REPORTING LEVEL = 0.016 newdate = 06/17/15 REPORTING LEVEL = 0.016 newdate = 06/17/15 REPORTING LEVEL = 0.016 newdate = 05/12/15 REPORTING LEVEL = 0.016 newdate = 05/12/15 REPORTING LEVEL = 0.016 newdate = 02/21/15 REPORTING LEVEL = 0.016 newdate = 02/21/15 REPORTING LEVEL = 0.016 newdate = 01/31/15 REPORTING LEVEL = 0.016 newdate = 01/31/15 REPORTING LEVEL = 0.016 newdate = 12/04/14 REPORTING LEVEL = 0.016 newdate = 12/04/14 REPORTING LEVEL = 0.016 newdate = 11/19/14 REPORTING LEVEL = 0.016 newdate = 11/19/14 REPORTING LEVEL = 0.016 newdate = 10/21/14 REPORTING LEVEL = 0.016 newdate = 10/21/14 REPORTING LEVEL = 0.016 newdate = 10/04/14 REPORTING LEVEL = 0.016 newdate = 10/04/14 REPORTING LEVEL = 0.016 newdate = 09/22/14 REPORTING LEVEL = 0.016 newdate = 09/22/14 REPORTING LEVEL = 0.016 newdate = 08/27/14 REPORTING LEVEL = 0.016 newdate = 08/27/14 REPORTING LEVEL = 0.016 newdate = 07/17/14 REPORTING LEVEL = 0.016 newdate = 07/17/14 REPORTING LEVEL = 0.016 newdate = 07/09/14 REPORTING LEVEL = 0.016 newdate = 07/09/14 REPORTING LEVEL = 0.016 newdate = 06/30/14 REPORTING LEVEL = 0.016 newdate = 06/30/14 REPORTING LEVEL = 0.016 newdate = 06/26/14 REPORTING LEVEL = 0.016 newdate = 06/26/14 REPORTING LEVEL = 0.016 newdate = 05/28/14 REPORTING LEVEL = 0.016 newdate = 05/28/14 REPORTING LEVEL = 0.016 newdate = 05/20/14 REPORTING LEVEL = 0.016 newdate = 05/20/14 REPORTING LEVEL = 0.016 newdate = 04/29/14 REPORTING LEVEL = 0.016 newdate = 04/29/14 REPORTING LEVEL = 0.016 newdate = 03/05/14 REPORTING LEVEL = 0.016 newdate = 03/05/14 REPORTING LEVEL = 0.016 newdate = 02/12/14 REPORTING LEVEL = 0.016 newdate = 02/12/14 REPORTING LEVEL = 0.016 newdate = 01/10/14 REPORTING LEVEL = 0.016 newdate = 01/10/14 REPORTING LEVEL = 0.016 newdate = 01/08/14 REPORTING LEVEL = 0.016 newdate = 01/08/14 REPORTING LEVEL = 0.016 newdate = 11/23/13 REPORTING LEVEL = 0.016 newdate = 11/23/13 REPORTING LEVEL = 0.016 newdate = 11/09/13 REPORTING LEVEL = 0.016 newdate = 11/09/13 REPORTING LEVEL = 0.016 newdate = 09/24/13 REPORTING LEVEL = 0.016 newdate = 09/24/13 REPORTING LEVEL = 0.016 newdate = 09/20/13 REPORTING LEVEL = 0.016 newdate = 09/20/13 REPORTING LEVEL = 0.016 newdate = 08/19/13 REPORTING LEVEL = 0.016 newdate = 08/19/13 REPORTING LEVEL = 0.016 newdate = 07/11/13 REPORTING LEVEL = 0.016 newdate = 07/11/13 REPORTING LEVEL = 0.016 newdate = 06/11/13 REPORTING LEVEL = 0.016 newdate = 06/11/13 REPORTING LEVEL = 0.016 newdate = 06/05/13 REPORTING LEVEL = 0.016 newdate = 06/05/13 REPORTING LEVEL = 0.016 newdate = 04/22/13 REPORTING LEVEL = 0.016 newdate = 04/22/13 REPORTING LEVEL = 0.016 newdate = 04/02/13 REPORTING LEVEL = 0.016 newdate = 04/02/13 REPORTING LEVEL = 0.016 newdate = 03/07/13 REPORTING LEVEL = 0.016 newdate = 03/07/13 REPORTING LEVEL = 0.016 newdate = 02/22/13 REPORTING LEVEL = 0.016 newdate = 02/22/13 REPORTING LEVEL = 0.016 newdate = 01/17/13 REPORTING LEVEL = 0.016 newdate = 01/17/13 REPORTING LEVEL = 0.016 newdate = 01/15/13 REPORTING LEVEL = 0.016 newdate = 01/15/13 REPORTING LEVEL = 0.016 newdate = 12/06/12 REPORTING LEVEL = 0.016 newdate = 12/06/12 REPORTING LEVEL = 0.016 newdate = 11/20/12 REPORTING LEVEL = 0.016 newdate = 11/20/12 REPORTING LEVEL = 0.016 newdate = 10/18/12 REPORTING LEVEL = 0.016 newdate = 10/18/12 REPORTING LEVEL = 0.016 newdate = 10/12/12 REPORTING LEVEL = 0.016 newdate = 10/12/12 REPORTING LEVEL = 0.016 newdate = 09/17/12 REPORTING LEVEL = 0.012 newdate = 09/17/12 REPORTING LEVEL = 0.012 newdate = 09/05/12 REPORTING LEVEL = 0.012 newdate = 09/05/12 REPORTING LEVEL = 0.012 newdate = 08/14/12 REPORTING LEVEL = 0.012 newdate = 08/14/12 REPORTING LEVEL = 0.012 newdate = 07/14/12 REPORTING LEVEL = 0.012 newdate = 07/14/12 REPORTING LEVEL = 0.012 newdate = 06/02/12 REPORTING LEVEL = 0.012 newdate = 06/02/12 REPORTING LEVEL = 0.012 newdate = 05/15/12 REPORTING LEVEL = 0.012 newdate = 05/15/12 REPORTING LEVEL = 0.012 newdate = 05/08/12 REPORTING LEVEL = 0.012 newdate = 05/08/12 REPORTING LEVEL = 0.012 newdate = 04/05/12 REPORTING LEVEL = 0.012 newdate = 04/05/12 REPORTING LEVEL = 0.012 newdate = 03/05/12 REPORTING LEVEL = 0.012 newdate = 03/05/12 REPORTING LEVEL = 0.012 newdate = 02/14/12 REPORTING LEVEL = 0.012 newdate = 02/14/12 REPORTING LEVEL = 0.012 newdate = 01/27/12 REPORTING LEVEL = 0.012 newdate = 01/27/12 REPORTING LEVEL = 0.012 newdate = 12/21/11 REPORTING LEVEL = 0.012 newdate = 12/21/11 REPORTING LEVEL = 0.012 newdate = 12/04/11 REPORTING LEVEL = 0.012 newdate = 12/04/11 REPORTING LEVEL = 0.012 newdate = 12/03/11 REPORTING LEVEL = 0.012 newdate = 12/03/11 REPORTING LEVEL = 0.012 newdate = 11/17/11 REPORTING LEVEL = 0.012 newdate = 11/17/11 REPORTING LEVEL = 0.012 newdate = 11/17/11 REPORTING LEVEL = 0.012 newdate = 11/17/11 REPORTING LEVEL = 0.012 newdate = 11/01/11 REPORTING LEVEL = 0.012 newdate = 11/01/11 REPORTING LEVEL = 0.012 newdate = 10/25/11 REPORTING LEVEL = 0.012 newdate = 10/25/11 REPORTING LEVEL = 0.012 newdate = 10/02/11 REPORTING LEVEL = 0.012 newdate = 10/02/11 REPORTING LEVEL = 0.012 newdate = 09/29/11 REPORTING LEVEL = 0.012 newdate = 09/29/11 REPORTING LEVEL = 0.012 newdate = 09/24/11 REPORTING LEVEL = 0.012 newdate = 09/24/11 REPORTING LEVEL = 0.012 newdate = 09/19/11 REPORTING LEVEL = 0.012 newdate = 09/19/11 REPORTING LEVEL = 0.012 newdate = 09/13/11 REPORTING LEVEL = 0.012 newdate = 09/13/11 REPORTING LEVEL = 0.012 newdate = 09/13/11 REPORTING LEVEL = 0.012 newdate = 09/13/11 REPORTING LEVEL = 0.012 newdate = 09/01/11 REPORTING LEVEL = 0.012 newdate = 09/01/11 REPORTING LEVEL = 0.012 newdate = 07/28/11 REPORTING LEVEL = 0.012 newdate = 07/28/11 REPORTING LEVEL = 0.012 newdate = 07/19/11 REPORTING LEVEL = 0.012 newdate = 07/19/11 REPORTING LEVEL = 0.012 newdate = 07/13/11 REPORTING LEVEL = 0.012 newdate = 07/13/11 REPORTING LEVEL = 0.012 newdate = 07/07/11 REPORTING LEVEL = 0.012 newdate = 07/07/11 REPORTING LEVEL = 0.012 newdate = 06/22/11 REPORTING LEVEL = 0.012 newdate = 06/22/11 REPORTING LEVEL = 0.012 newdate = 06/20/11 REPORTING LEVEL = 0.012 newdate = 06/20/11 REPORTING LEVEL = 0.012 newdate = 06/20/11 REPORTING LEVEL = 0.012 newdate = 06/20/11 REPORTING LEVEL = 0.012 newdate = 05/14/11 REPORTING LEVEL = 0.012 newdate = 05/14/11 REPORTING LEVEL = 0.012 newdate = 04/23/11 REPORTING LEVEL = 0.012 newdate = 04/23/11 REPORTING LEVEL = 0.012 newdate = 04/20/11 REPORTING LEVEL = 0.012 newdate = 04/20/11 REPORTING LEVEL = 0.012 newdate = 04/13/11 REPORTING LEVEL = 0.012 newdate = 04/13/11 REPORTING LEVEL = 0.012 newdate = 03/30/11 REPORTING LEVEL = 0.012 newdate = 03/30/11 REPORTING LEVEL = 0.012 newdate = 03/23/11 REPORTING LEVEL = 0.012 newdate = 03/23/11 REPORTING LEVEL = 0.012 newdate = 03/08/11 REPORTING LEVEL = 0.012 newdate = 03/08/11 REPORTING LEVEL = 0.012 newdate = 03/05/11 REPORTING LEVEL = 0.012 newdate = 03/05/11 REPORTING LEVEL = 0.012 newdate = 02/28/11 REPORTING LEVEL = 0.012 newdate = 02/28/11 REPORTING LEVEL = 0.012 newdate = 02/19/11 REPORTING LEVEL = 0.012 newdate = 02/19/11 REPORTING LEVEL = 0.012 newdate = 02/09/11 REPORTING LEVEL = 0.012 newdate = 02/09/11 REPORTING LEVEL = 0.012 newdate = 02/08/11 REPORTING LEVEL = 0.012 newdate = 02/08/11 REPORTING LEVEL = 0.012 newdate = 01/28/11 REPORTING LEVEL = 0.012 newdate = 01/28/11 REPORTING LEVEL = 0.012 newdate = 01/21/11 REPORTING LEVEL = 0.012 newdate = 01/21/11 REPORTING LEVEL = 0.012 newdate = 01/20/11 REPORTING LEVEL = 0.012 newdate = 01/20/11 REPORTING LEVEL = 0.012 newdate = 01/13/11 REPORTING LEVEL = 0.012 newdate = 01/13/11 REPORTING LEVEL = 0.012 newdate = 01/11/11 REPORTING LEVEL = 0.012 newdate = 01/11/11 REPORTING LEVEL = 0.012 newdate = 01/09/11 REPORTING LEVEL = 0.012 newdate = 01/09/11 REPORTING LEVEL = 0.012 newdate = 12/16/10 REPORTING LEVEL = 0.012 newdate = 12/16/10 REPORTING LEVEL = 0.012 newdate = 12/14/10 REPORTING LEVEL = 0.012 newdate = 12/14/10 REPORTING LEVEL = 0.012 newdate = 10/19/10 REPORTING LEVEL = 0.012 newdate = 10/19/10 REPORTING LEVEL = 0.012 newdate = 09/09/10 REPORTING LEVEL = 0.013 newdate = 09/09/10 REPORTING LEVEL = 0.013 newdate = 08/25/10 REPORTING LEVEL = 0.013 newdate = 08/25/10 REPORTING LEVEL = 0.013 newdate = 07/21/10 REPORTING LEVEL = 0.013 newdate = 07/21/10 REPORTING LEVEL = 0.013 newdate = 06/30/10 REPORTING LEVEL = 0.013 newdate = 06/30/10 REPORTING LEVEL = 0.013 newdate = 06/03/10 REPORTING LEVEL = 0.013 newdate = 06/03/10 REPORTING LEVEL = 0.013 newdate = 05/07/10 REPORTING LEVEL = 0.013 newdate = 05/07/10 REPORTING LEVEL = 0.013 newdate = 03/24/10 REPORTING LEVEL = 0.013 Y = 0
The SGPlot Procedure

Updated 06/06/2016

False Positive & Negative Listing for FIPRONIL SULFIDE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20111470065 ERA 0818-10-05 LS 2033#2: 40 µl 0.012 06/20/11 < 0.012 0.0493228
False Positive 20102950072 Restek A075606: 40 µl 0.012 01/09/11 . 0.0032 0
  20103430087 Restek A075606: 80 µl 0.012 01/28/11 . 0.0098 0
  20110130056 Supelco LB77168: 80 µl 0.012 02/09/11 . 0.0061 0
  20110560005 Restek A075606: 40 µl 0.012 03/08/11 . 0.0095 0
  20110770001 Supelco LB77168: 40 µl 0.012 03/30/11 . 0.0027 0
  20111050150 Restek A075606: 40 µl 0.012 04/23/11 . 0.0041 0
  20111540007 Restek A075606: 80 µl 0.012 06/20/11 . 0.0053 0
  20111810004 Supelco LB77168: 80 µl 0.012 07/13/11 . 0.0051 0
  20111890005 Supelco LB77168: 40 µl 0.012 07/19/11 . 0.0058 0
  20112220126 Restek A075606: 80 µl 0.012 09/01/11 . 0.0083 0
  20112310032 Restek A075606: 80 µl 0.012 09/13/11 . 0.0021 0
  20112450022 Supelco LB77168: 40 µl 0.012 09/24/11 . 0.0027 0
  20112590005 Supelco LB77168: 80 µl 0.012 10/02/11 . 0.0081 0
  20112930085 Restek A075606: 80 µl 0.012 11/01/11 . 0.0052 0
  20113130085 Supelco LB77168: 80 µl 0.012 11/17/11 . 0.0043 0
  20113260111 Restek A075606: 40 µl 0.012 12/04/11 . 0.0054 0
  20120370001 Restek A075606: 40 µl 0.012 02/14/12 . 0.0036 0
  20121310027 Restek A075606: 80 µl 0.012 05/15/12 . 0.0037 0
  20152460215 Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl 0.016 09/17/15 . 0.0048 0

Updated 06/06/2016