BQS Organic Blind Sample Program
False Positives & False Negatives
TERBUFOS-O-ANALOGUE SULFONE
Method: 2033 Testid: 61674GCM39
Open Data Set

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newdate = 04/02/13 falseneg = -0.01 newdate = 02/22/13 falseneg = -0.01 newdate = 01/17/13 falseneg = -0.01 newdate = 11/20/12 falseneg = -0.01 newdate = 10/18/12 falseneg = -0.01 newdate = 08/14/12 falseneg = -0.01 newdate = 07/14/12 falseneg = -0.01 newdate = 04/15/14 CENC_VAL = 0.049 newdate = 04/03/14 CENC_VAL = 0.027 newdate = 03/05/14 CENC_VAL = 0.039 newdate = 01/31/14 CENC_VAL = 0.060 newdate = 01/18/14 CENC_VAL = 0.178 newdate = 01/10/14 CENC_VAL = 0.057 newdate = 01/08/14 CENC_VAL = 0.034 newdate = 12/05/13 CENC_VAL = 0.159 newdate = 11/23/13 CENC_VAL = 0.089 newdate = 11/04/13 CENC_VAL = 0.026 newdate = 10/19/13 CENC_VAL = 0.128 newdate = 09/24/13 CENC_VAL = 0.053 newdate = 09/14/13 CENC_VAL = 0.035 newdate = 04/22/13 CENC_VAL = 0.041 newdate = 03/07/13 CENC_VAL = 0.023 newdate = 01/15/13 CENC_VAL = 0.037 newdate = 12/06/12 CENC_VAL = 0.091 newdate = 10/12/12 CENC_VAL = 0.047 newdate = 09/17/12 CENC_VAL = 0.030 newdate = 09/05/12 CENC_VAL = 0.021 newdate = 06/22/11 CENC_VAL = 0.043 newdate = 04/20/11 CENC_VAL = 0.055 newdate = 03/05/11 CENC_VAL = 0.026 newdate = 01/20/11 CENC_VAL = 0.092 newdate = 12/16/10 CENC_VAL = 0.043 newdate = 08/25/10 CENC_VAL = 0.046 newdate = 06/30/10 CENC_VAL = 0.028 newdate = 04/15/14 REPORTING LEVEL = 0.045 newdate = 04/03/14 REPORTING LEVEL = 0.045 newdate = 04/03/14 REPORTING LEVEL = 0.045 newdate = 03/05/14 REPORTING LEVEL = 0.045 newdate = 03/05/14 REPORTING LEVEL = 0.045 newdate = 01/31/14 REPORTING LEVEL = 0.045 newdate = 01/31/14 REPORTING LEVEL = 0.045 newdate = 01/18/14 REPORTING LEVEL = 0.045 newdate = 01/18/14 REPORTING LEVEL = 0.045 newdate = 01/10/14 REPORTING LEVEL = 0.045 newdate = 01/10/14 REPORTING LEVEL = 0.045 newdate = 01/08/14 REPORTING LEVEL = 0.045 newdate = 01/08/14 REPORTING LEVEL = 0.045 newdate = 12/05/13 REPORTING LEVEL = 0.045 newdate = 12/05/13 REPORTING LEVEL = 0.045 newdate = 11/23/13 REPORTING LEVEL = 0.045 newdate = 11/23/13 REPORTING LEVEL = 0.045 newdate = 11/04/13 REPORTING LEVEL = 0.045 newdate = 11/04/13 REPORTING LEVEL = 0.045 newdate = 10/19/13 REPORTING LEVEL = 0.045 newdate = 10/19/13 REPORTING LEVEL = 0.045 newdate = 09/24/13 REPORTING LEVEL = 0.045 newdate = 09/24/13 REPORTING LEVEL = 0.045 newdate = 09/14/13 REPORTING LEVEL = 0.045 newdate = 09/14/13 REPORTING LEVEL = 0.045 newdate = 04/22/13 REPORTING LEVEL = 0.045 newdate = 04/22/13 REPORTING LEVEL = 0.045 newdate = 04/02/13 REPORTING LEVEL = 0.045 newdate = 04/02/13 REPORTING LEVEL = 0.045 newdate = 03/07/13 REPORTING LEVEL = 0.045 newdate = 03/07/13 REPORTING LEVEL = 0.045 newdate = 02/22/13 REPORTING LEVEL = 0.045 newdate = 02/22/13 REPORTING LEVEL = 0.045 newdate = 01/17/13 REPORTING LEVEL = 0.045 newdate = 01/17/13 REPORTING LEVEL = 0.045 newdate = 01/15/13 REPORTING LEVEL = 0.045 newdate = 01/15/13 REPORTING LEVEL = 0.045 newdate = 12/06/12 REPORTING LEVEL = 0.045 newdate = 12/06/12 REPORTING LEVEL = 0.045 newdate = 11/20/12 REPORTING LEVEL = 0.045 newdate = 11/20/12 REPORTING LEVEL = 0.045 newdate = 10/18/12 REPORTING LEVEL = 0.045 newdate = 10/18/12 REPORTING LEVEL = 0.045 newdate = 10/12/12 REPORTING LEVEL = 0.045 newdate = 10/12/12 REPORTING LEVEL = 0.045 newdate = 09/17/12 REPORTING LEVEL = 0.045 newdate = 09/17/12 REPORTING LEVEL = 0.045 newdate = 09/05/12 REPORTING LEVEL = 0.045 newdate = 09/05/12 REPORTING LEVEL = 0.045 newdate = 08/14/12 REPORTING LEVEL = 0.045 newdate = 08/14/12 REPORTING LEVEL = 0.045 newdate = 07/14/12 REPORTING LEVEL = 0.045 newdate = 07/14/12 REPORTING LEVEL = 0.045 newdate = 06/22/11 REPORTING LEVEL = 0.045 newdate = 06/22/11 REPORTING LEVEL = 0.045 newdate = 04/20/11 REPORTING LEVEL = 0.045 newdate = 04/20/11 REPORTING LEVEL = 0.045 newdate = 03/05/11 REPORTING LEVEL = 0.045 newdate = 03/05/11 REPORTING LEVEL = 0.045 newdate = 01/20/11 REPORTING LEVEL = 0.045 newdate = 01/20/11 REPORTING LEVEL = 0.045 newdate = 12/16/10 REPORTING LEVEL = 0.045 newdate = 12/16/10 REPORTING LEVEL = 0.045 newdate = 08/25/10 REPORTING LEVEL = 0.045 newdate = 08/25/10 REPORTING LEVEL = 0.045 newdate = 06/30/10 REPORTING LEVEL = 0.045 Y = 0
The SGPlot Procedure

Updated 06/06/2016

False Positive & Negative Listing for TERBUFOS-O-ANALOGUE SULFONE

Status Lab ID Spike Mix Reporting Level Analysis Date Result Conc. Expected Conc.
False Negative 20121870008 Restek A088380: 20 µl & Supelco LB92783: 20 µl 0.045 07/14/12 < 0.045 0.06416
  20122020004 Abs 052412: 20 µl & Supelco LB92783: 20 µl 0.045 08/14/12 < 0.045 0.06416
  20122850005 Supelco LB92783: 50 µl & Abs 052412: 50 µl 0.045 10/18/12 < 0.045 0.1604
  20123140095 Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl 0.045 11/20/12 < 0.045 0.3208
  20130100066 Supelco LB92783: 50 µl & Abs 052412: 50 µl 0.045 01/17/13 < 0.045 0.1604
  20130390105 Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl 0.045 02/22/13 < 0.045 0.06416
  20130810108 Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl 0.045 04/02/13 < 0.045 0.1604

Updated 06/06/2016