BQS OBSP Determination:
11-KETOTESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64527GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
11-KETOTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 91% 17% 90% 18%
Total 32 91% 17% 90% 18%

Sample Statistics
11-KETOTESTOSTERONE

Characteristic N % % Basis
Plotted 32 86% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 5 14% 5 out of 37
Not Spiked 97 .  
False Positives 0 0% 0 out of 96

BQS OBSP Determination:
17-ALPHA-ESTRADIOL
METHOD: 4434 , TESTIDCODE: 64528GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 73 86% 13% 86% 13%
Total 73 86% 13% 86% 13%

Sample Statistics
17-ALPHA-ESTRADIOL

Characteristic N % % Basis
Plotted 73 94% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 79 .  
False Negatives 2 3% 2 out of 78
Not Spiked 56 .  
False Positives 0 0% 0 out of 56

BQS OBSP Determination:
17-ALPHA-ETHYNYLESTRADIOL
METHOD: 4434 , TESTIDCODE: 64529GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ETHYNYLESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 68 80% 13% 79% 13%
Total 68 80% 13% 79% 13%

Sample Statistics
17-ALPHA-ETHYNYLESTRADIOL

Characteristic N % % Basis
Plotted 68 85% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 81 .  
False Negatives 12 15% 12 out of 80
Not Spiked 54 .  
False Positives 0 0% 0 out of 54

BQS OBSP Determination:
17-BETA-ESTRADIOL
METHOD: 4434 , TESTIDCODE: 64530GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
17-BETA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 88% 18% 85% 15%
Total 71 88% 18% 85% 15%

Sample Statistics
17-BETA-ESTRADIOL

Characteristic N % % Basis
Plotted 71 91% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 79 .  
False Negatives 6 8% 6 out of 78
Not Spiked 56 .  
False Positives 0 0% 0 out of 56

BQS OBSP Determination:
3-BETA-COPROSTANOL
METHOD: 4434 , TESTIDCODE: 64532GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
3-BETA-COPROSTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 59 87% 25% 89% 26%
Total 59 87% 25% 89% 26%

Sample Statistics
3-BETA-COPROSTANOL

Characteristic N % % Basis
Plotted 59 83% Spiked
Estimated Values 2 3% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 73 .  
False Negatives 12 17% 12 out of 71
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

BQS OBSP Determination:
4,4BISPHENOL F
METHOD: 4434 , TESTIDCODE: 51294GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
4,4BISPHENOL F

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 100% 29% 88% 32%
Total 11 100% 29% 88% 32%

Sample Statistics
4,4BISPHENOL F

Characteristic N % % Basis
Plotted 11 100% Spiked
Estimated Values 11 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 11 .  
False Negatives 0 0% 0 out of 11
Not Spiked 15 .  
False Positives 0 0% 0 out of 15

BQS OBSP Determination:
4,4BISPHENOL S
METHOD: 4434 , TESTIDCODE: 51295GM005
Open Data Set

The SGPlot Procedure

Sample Statistics
4,4BISPHENOL S

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 2 100% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 2 .  
False Positives 0 . 0 out of 0

BQS OBSP Determination:
4-ANDROSTENE-3,17-DIONE
METHOD: 4434 , TESTIDCODE: 64533GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
4-ANDROSTENE-3,17-DIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 70% 21% 70% 20%
Total 36 70% 21% 70% 20%

Sample Statistics
4-ANDROSTENE-3,17-DIONE

Characteristic N % % Basis
Plotted 36 88% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 42 .  
False Negatives 4 10% 4 out of 41
Not Spiked 93 .  
False Positives 0 0% 0 out of 92

BQS OBSP Determination:
BISPHENOL A
METHOD: 4434 , TESTIDCODE: 67305GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BISPHENOL A

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 111% 8% 108% 8%
>= Reporting Level 64 78% 21% 77% 24%
Total 68 80% 22% 80% 23%

Sample Statistics
BISPHENOL A

Characteristic N % % Basis
Plotted 68 94% Spiked
Estimated Values 24 33% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 3 4% Spiked
Spiked 74 .  
False Negatives 1 1% 1 out of 72
Not Spiked 61 .  
False Positives 0 0% 0 out of 60

BQS OBSP Determination:
CHOLESTEROL
METHOD: 4434 , TESTIDCODE: 64534GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CHOLESTEROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 89% 20% 88% 20%
Total 71 89% 20% 88% 20%

Sample Statistics
CHOLESTEROL

Characteristic N % % Basis
Plotted 71 99% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 74 .  
False Negatives 1 1% 1 out of 72
Not Spiked 50 .  
False Positives 2 4% 2 out of 50

BQS OBSP Determination:
CIS-ANDROSTERONE
METHOD: 4434 , TESTIDCODE: 64535GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CIS-ANDROSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 57 80% 26% 80% 16%
Total 57 80% 26% 80% 16%

Sample Statistics
CIS-ANDROSTERONE

Characteristic N % % Basis
Plotted 57 89% Spiked
Estimated Values 2 3% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 64 .  
False Negatives 6 9% 6 out of 64
Not Spiked 71 .  
False Positives 1 1% 1 out of 69

BQS OBSP Determination:
DIHYDROTESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64544GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DIHYDROTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 39 67% 24% 66% 12%
Total 39 67% 24% 66% 12%

Sample Statistics
DIHYDROTESTOSTERONE

Characteristic N % % Basis
Plotted 39 87% Spiked
Estimated Values 4 9% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 6 13% 6 out of 45
Not Spiked 90 .  
False Positives 1 1% 1 out of 89

BQS OBSP Determination:
EPITESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64537GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
EPITESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 61 75% 20% 73% 13%
Total 61 75% 20% 73% 13%

Sample Statistics
EPITESTOSTERONE

Characteristic N % % Basis
Plotted 61 95% Spiked
Estimated Values 3 5% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 66 .  
False Negatives 3 5% 3 out of 64
Not Spiked 69 .  
False Positives 0 0% 0 out of 69

BQS OBSP Determination:
EQUILENIN
METHOD: 4434 , TESTIDCODE: 64538GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
EQUILENIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 89% 37% 85% 44%
Total 32 89% 37% 85% 44%

Sample Statistics
EQUILENIN

Characteristic N % % Basis
Plotted 32 86% Spiked
Estimated Values 2 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 37 .  
False Negatives 5 14% 5 out of 37
Not Spiked 45 .  
False Positives 3 7% 3 out of 45

BQS OBSP Determination:
EQUILIN
METHOD: 4434 , TESTIDCODE: 64539GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
EQUILIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 71% 18% 64% 1%
>= Reporting Level 62 68% 17% 66% 18%
Total 67 68% 17% 66% 17%

Sample Statistics
EQUILIN

Characteristic N % % Basis
Plotted 67 88% Spiked
Estimated Values 67 88% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 78 .  
False Negatives 8 11% 8 out of 76
Not Spiked 57 .  
False Positives 0 0% 0 out of 57

BQS OBSP Determination:
ESTRIOL
METHOD: 4434 , TESTIDCODE: 64540GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ESTRIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 76% 11% 81% 15%
>= Reporting Level 72 78% 16% 78% 17%
Total 75 78% 15% 78% 17%

Sample Statistics
ESTRIOL

Characteristic N % % Basis
Plotted 75 90% Spiked
Estimated Values 5 6% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 84 .  
False Negatives 7 8% 7 out of 83
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

BQS OBSP Determination:
ESTRONE
METHOD: 4434 , TESTIDCODE: 64541GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ESTRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 69 82% 19% 77% 19%
Total 69 82% 19% 77% 19%

Sample Statistics
ESTRONE

Characteristic N % % Basis
Plotted 69 85% Spiked
Estimated Values 3 4% Spiked
Deleted Values 3 2% Spiked + Not Spiked
Spiked, Censored 4 5% Spiked
Spiked 81 .  
False Negatives 8 10% 8 out of 81
Not Spiked 54 .  
False Positives 0 0% 0 out of 51

BQS OBSP Determination:
MESTRANOL
METHOD: 4434 , TESTIDCODE: 64542GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
MESTRANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 143% . 143% 0%
>= Reporting Level 58 59% 30% 52% 16%
Total 59 60% 31% 52% 17%

Sample Statistics
MESTRANOL

Characteristic N % % Basis
Plotted 59 75% Spiked
Estimated Values 2 3% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 20 25% 20 out of 79
Not Spiked 56 .  
False Positives 1 2% 1 out of 55

BQS OBSP Determination:
NORETHINDRONE
METHOD: 4434 , TESTIDCODE: 64531GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 105% . 105% 0%
>= Reporting Level 63 80% 16% 77% 17%
Total 64 80% 16% 77% 18%

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 64 82% Spiked
Estimated Values 2 3% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 79 .  
False Negatives 12 15% 12 out of 78
Not Spiked 56 .  
False Positives 0 0% 0 out of 55

BQS OBSP Determination:
PROGESTERONE
METHOD: 4434 , TESTIDCODE: 64543GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
PROGESTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 71 48% 22% 44% 14%
Total 71 48% 22% 44% 14%

Sample Statistics
PROGESTERONE

Characteristic N % % Basis
Plotted 71 90% Spiked
Estimated Values 71 90% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 80 .  
False Negatives 8 10% 8 out of 79
Not Spiked 55 .  
False Positives 0 0% 0 out of 55

BQS OBSP Determination:
TESTOSTERONE
METHOD: 4434 , TESTIDCODE: 64545GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 77% 13% 77% 11%
Total 50 77% 13% 77% 11%

Sample Statistics
TESTOSTERONE

Characteristic N % % Basis
Plotted 50 89% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 56 .  
False Negatives 6 11% 6 out of 56
Not Spiked 79 .  
False Positives 0 0% 0 out of 77

BQS OBSP Determination:
TRANS-DIETHYLSTILBESTROL
METHOD: 4434 , TESTIDCODE: 64536GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRANS-DIETHYLSTILBESTROL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 80% . 80% 0%
>= Reporting Level 72 68% 14% 66% 16%
Total 73 68% 14% 67% 16%

Sample Statistics
TRANS-DIETHYLSTILBESTROL

Characteristic N % % Basis
Plotted 73 92% Spiked
Estimated Values 1 1% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 79 .  
False Negatives 6 8% 6 out of 79
Not Spiked 56 .  
False Positives 0 0% 0 out of 55