BQS OBSP Determination:
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))
METHOD: 2033 , TESTIDCODE: 61610GCM39
Open Data Set

Analysis Date = 07/15/10 SpikeMix = Spex Organics T1090901009: 100 µl Pct Recovery = 74% Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 53% Analysis Date = 12/22/10 SpikeMix = Spex Organics T1090901009: 40 µl Pct Recovery = 45% Analysis Date = 08/10/10 SpikeMix = Ultra CF-3558: 40 µl Pct Recovery = 51% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 50% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 47% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 75% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 63% Analysis Date = 09/30/10 SpikeMix = Spex Organics T1090901009: 20 µl Pct Recovery = 97% Analysis Date = 05/19/10 SpikeMix = Ultra CF-3558: 20 µl Pct Recovery = 88% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 60% Analysis Date = 12/01/10 SpikeMix = Ultra CF-3558: 20 µl Pct Recovery = 43% Analysis Date = 06/16/10 SpikeMix = Spex Organics T1090901009: 20 µl Pct Recovery = 58% Analysis Date = 01/28/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 68% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 53% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 50% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 58% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 53% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 53% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 30% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 41% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 60% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 39% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 52% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 59% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 58% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 50% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 51% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 45% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 50% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 60% Analysis Date = 01/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 80% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 64% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 57% Analysis Date = 09/23/14 SpikeMix = NSI 042814: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 59% Analysis Date = 06/28/14 SpikeMix = ERA 0227-14-08: 60 µl & Supelco LC06435: 60 µl Pct Recovery = 62% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 78% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 61% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 68% Analysis Date = 10/30/14 SpikeMix = NSI 042814: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 62% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 63% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 71% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 57% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 50% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 58% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 66% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 69% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 49% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 77% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 59% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 81% Analysis Date = 01/18/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 43% Analysis Date = 01/09/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 78% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 47% Analysis Date = 06/26/13 SpikeMix = Abs 042413: 20 µl & ChemService 1473000: 20 µl Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 61% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 60% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 81% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 56% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 92% Analysis Date = 09/05/13 SpikeMix = Crescent 04CC101: 20 µl & Spex Organics T1130514013: 20 µl Pct Recovery = 85% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 88% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 60% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 70% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 61% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 65% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 58% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 64% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 57% Analysis Date = 08/25/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 77% Analysis Date = 12/16/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 75% Analysis Date = 06/30/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 58% Analysis Date = 12/15/14 SpikeMix = NSI 042814: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 81% Analysis Date = 07/16/14 SpikeMix = ERA 0227-14-08: 30 µl & Supelco LC06435: 30 µl Pct Recovery = 77% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 70% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 75% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 61% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 62% Analysis Date = 08/16/14 SpikeMix = NSI 042814: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 67% Analysis Date = 06/24/14 SpikeMix = ERA 0227-14-08: 30 µl & Crescent 03DD006: 30 µl Pct Recovery = 85% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 80% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 92% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 64% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 99% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 86% Analysis Date = 02/08/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/29/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/19/16 Pct Recovery = 72% Analysis Date = 01/08/16 Pct Recovery = 72% Analysis Date = 01/08/16 Pct Recovery = 72% Analysis Date = 12/29/15 Pct Recovery = 72% Analysis Date = 12/29/15 Pct Recovery = 72% Analysis Date = 12/18/15 Pct Recovery = 72% Analysis Date = 12/18/15 Pct Recovery = 72% Analysis Date = 12/08/15 Pct Recovery = 72% Analysis Date = 12/08/15 Pct Recovery = 72% Analysis Date = 11/27/15 Pct Recovery = 72% Analysis Date = 11/27/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 72% Analysis Date = 11/17/15 Pct Recovery = 72% Analysis Date = 11/06/15 Pct Recovery = 72% Analysis Date = 11/06/15 Pct Recovery = 72% Analysis Date = 10/27/15 Pct Recovery = 71% Analysis Date = 10/27/15 Pct Recovery = 71% Analysis Date = 10/16/15 Pct Recovery = 71% Analysis Date = 10/16/15 Pct Recovery = 71% Analysis Date = 10/06/15 Pct Recovery = 71% Analysis Date = 10/06/15 Pct Recovery = 71% Analysis Date = 09/26/15 Pct Recovery = 71% Analysis Date = 09/26/15 Pct Recovery = 71% Analysis Date = 09/15/15 Pct Recovery = 71% Analysis Date = 09/15/15 Pct Recovery = 71% Analysis Date = 09/05/15 Pct Recovery = 71% Analysis Date = 09/05/15 Pct Recovery = 71% Analysis Date = 08/25/15 Pct Recovery = 71% Analysis Date = 08/25/15 Pct Recovery = 71% Analysis Date = 08/15/15 Pct Recovery = 71% Analysis Date = 08/15/15 Pct Recovery = 71% Analysis Date = 08/04/15 Pct Recovery = 71% Analysis Date = 08/04/15 Pct Recovery = 71% Analysis Date = 07/25/15 Pct Recovery = 71% Analysis Date = 07/25/15 Pct Recovery = 71% Analysis Date = 07/14/15 Pct Recovery = 71% Analysis Date = 07/14/15 Pct Recovery = 71% Analysis Date = 07/04/15 Pct Recovery = 71% Analysis Date = 07/04/15 Pct Recovery = 71% Analysis Date = 06/23/15 Pct Recovery = 71% Analysis Date = 06/23/15 Pct Recovery = 71% Analysis Date = 06/13/15 Pct Recovery = 70% Analysis Date = 06/13/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 70% Analysis Date = 06/02/15 Pct Recovery = 70% Analysis Date = 05/23/15 Pct Recovery = 70% Analysis Date = 05/23/15 Pct Recovery = 70% Analysis Date = 05/13/15 Pct Recovery = 70% Analysis Date = 05/13/15 Pct Recovery = 70% Analysis Date = 05/02/15 Pct Recovery = 70% Analysis Date = 05/02/15 Pct Recovery = 70% Analysis Date = 04/22/15 Pct Recovery = 70% Analysis Date = 04/22/15 Pct Recovery = 70% Analysis Date = 04/11/15 Pct Recovery = 70% Analysis Date = 04/11/15 Pct Recovery = 70% Analysis Date = 04/01/15 Pct Recovery = 70% Analysis Date = 04/01/15 Pct Recovery = 70% Analysis Date = 03/21/15 Pct Recovery = 70% Analysis Date = 03/21/15 Pct Recovery = 70% Analysis Date = 03/11/15 Pct Recovery = 70% Analysis Date = 03/11/15 Pct Recovery = 70% Analysis Date = 02/28/15 Pct Recovery = 70% Analysis Date = 02/28/15 Pct Recovery = 70% Analysis Date = 02/18/15 Pct Recovery = 70% Analysis Date = 02/18/15 Pct Recovery = 70% Analysis Date = 02/07/15 Pct Recovery = 70% Analysis Date = 02/07/15 Pct Recovery = 70% Analysis Date = 01/28/15 Pct Recovery = 69% Analysis Date = 01/28/15 Pct Recovery = 69% Analysis Date = 01/17/15 Pct Recovery = 69% Analysis Date = 01/17/15 Pct Recovery = 69% Analysis Date = 01/07/15 Pct Recovery = 69% Analysis Date = 01/07/15 Pct Recovery = 69% Analysis Date = 12/28/14 Pct Recovery = 69% Analysis Date = 12/28/14 Pct Recovery = 69% Analysis Date = 12/17/14 Pct Recovery = 69% Analysis Date = 12/17/14 Pct Recovery = 69% Analysis Date = 12/07/14 Pct Recovery = 69% Analysis Date = 12/07/14 Pct Recovery = 69% Analysis Date = 11/26/14 Pct Recovery = 69% Analysis Date = 11/26/14 Pct Recovery = 69% Analysis Date = 11/16/14 Pct Recovery = 69% Analysis Date = 11/16/14 Pct Recovery = 69% Analysis Date = 11/05/14 Pct Recovery = 69% Analysis Date = 11/05/14 Pct Recovery = 69% Analysis Date = 10/26/14 Pct Recovery = 69% Analysis Date = 10/26/14 Pct Recovery = 69% Analysis Date = 10/15/14 Pct Recovery = 69% Analysis Date = 10/15/14 Pct Recovery = 69% Analysis Date = 10/05/14 Pct Recovery = 69% Analysis Date = 10/05/14 Pct Recovery = 69% Analysis Date = 09/24/14 Pct Recovery = 68% Analysis Date = 09/24/14 Pct Recovery = 68% Analysis Date = 09/14/14 Pct Recovery = 68% Analysis Date = 09/14/14 Pct Recovery = 68% Analysis Date = 09/03/14 Pct Recovery = 68% Analysis Date = 09/03/14 Pct Recovery = 68% Analysis Date = 08/24/14 Pct Recovery = 68% Analysis Date = 08/24/14 Pct Recovery = 68% Analysis Date = 08/14/14 Pct Recovery = 68% Analysis Date = 08/14/14 Pct Recovery = 68% Analysis Date = 08/03/14 Pct Recovery = 68% Analysis Date = 08/03/14 Pct Recovery = 68% Analysis Date = 07/24/14 Pct Recovery = 68% Analysis Date = 07/24/14 Pct Recovery = 68% Analysis Date = 07/13/14 Pct Recovery = 68% Analysis Date = 07/13/14 Pct Recovery = 68% Analysis Date = 07/03/14 Pct Recovery = 68% Analysis Date = 07/03/14 Pct Recovery = 68% Analysis Date = 06/22/14 Pct Recovery = 68% Analysis Date = 06/22/14 Pct Recovery = 68% Analysis Date = 06/12/14 Pct Recovery = 68% Analysis Date = 06/12/14 Pct Recovery = 68% Analysis Date = 06/01/14 Pct Recovery = 68% Analysis Date = 06/01/14 Pct Recovery = 68% Analysis Date = 05/22/14 Pct Recovery = 67% Analysis Date = 05/22/14 Pct Recovery = 67% Analysis Date = 05/11/14 Pct Recovery = 67% Analysis Date = 05/11/14 Pct Recovery = 67% Analysis Date = 05/01/14 Pct Recovery = 67% Analysis Date = 05/01/14 Pct Recovery = 67% Analysis Date = 04/21/14 Pct Recovery = 67% Analysis Date = 04/21/14 Pct Recovery = 67% Analysis Date = 04/10/14 Pct Recovery = 67% Analysis Date = 04/10/14 Pct Recovery = 67% Analysis Date = 03/31/14 Pct Recovery = 67% Analysis Date = 03/31/14 Pct Recovery = 67% Analysis Date = 03/20/14 Pct Recovery = 67% Analysis Date = 03/20/14 Pct Recovery = 67% Analysis Date = 03/10/14 Pct Recovery = 67% Analysis Date = 03/10/14 Pct Recovery = 67% Analysis Date = 02/27/14 Pct Recovery = 67% Analysis Date = 02/27/14 Pct Recovery = 67% Analysis Date = 02/17/14 Pct Recovery = 66% Analysis Date = 02/17/14 Pct Recovery = 66% Analysis Date = 02/06/14 Pct Recovery = 66% Analysis Date = 02/06/14 Pct Recovery = 66% Analysis Date = 01/27/14 Pct Recovery = 66% Analysis Date = 01/27/14 Pct Recovery = 66% Analysis Date = 01/16/14 Pct Recovery = 66% Analysis Date = 01/16/14 Pct Recovery = 66% Analysis Date = 01/06/14 Pct Recovery = 66% Analysis Date = 01/06/14 Pct Recovery = 66% Analysis Date = 12/26/13 Pct Recovery = 66% Analysis Date = 12/26/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/16/13 Pct Recovery = 66% Analysis Date = 12/06/13 Pct Recovery = 65% Analysis Date = 12/06/13 Pct Recovery = 65% Analysis Date = 11/25/13 Pct Recovery = 65% Analysis Date = 11/25/13 Pct Recovery = 65% Analysis Date = 11/15/13 Pct Recovery = 65% Analysis Date = 11/15/13 Pct Recovery = 65% Analysis Date = 11/04/13 Pct Recovery = 65% Analysis Date = 11/04/13 Pct Recovery = 65% Analysis Date = 10/25/13 Pct Recovery = 65% Analysis Date = 10/25/13 Pct Recovery = 65% Analysis Date = 10/14/13 Pct Recovery = 65% Analysis Date = 10/14/13 Pct Recovery = 65% Analysis Date = 10/04/13 Pct Recovery = 64% Analysis Date = 10/04/13 Pct Recovery = 64% Analysis Date = 09/23/13 Pct Recovery = 64% Analysis Date = 09/23/13 Pct Recovery = 64% Analysis Date = 09/13/13 Pct Recovery = 64% Analysis Date = 09/13/13 Pct Recovery = 64% Analysis Date = 09/02/13 Pct Recovery = 64% Analysis Date = 09/02/13 Pct Recovery = 64% Analysis Date = 08/23/13 Pct Recovery = 64% Analysis Date = 08/23/13 Pct Recovery = 64% Analysis Date = 08/12/13 Pct Recovery = 64% Analysis Date = 08/12/13 Pct Recovery = 64% Analysis Date = 08/02/13 Pct Recovery = 64% Analysis Date = 08/02/13 Pct Recovery = 64% Analysis Date = 07/23/13 Pct Recovery = 63% Analysis Date = 07/23/13 Pct Recovery = 63% Analysis Date = 07/12/13 Pct Recovery = 63% Analysis Date = 07/12/13 Pct Recovery = 63% Analysis Date = 07/02/13 Pct Recovery = 63% Analysis Date = 07/02/13 Pct Recovery = 63% Analysis Date = 06/21/13 Pct Recovery = 63% Analysis Date = 06/21/13 Pct Recovery = 63% Analysis Date = 06/11/13 Pct Recovery = 63% Analysis Date = 06/11/13 Pct Recovery = 63% Analysis Date = 05/31/13 Pct Recovery = 63% Analysis Date = 05/31/13 Pct Recovery = 63% Analysis Date = 05/21/13 Pct Recovery = 63% Analysis Date = 05/21/13 Pct Recovery = 63% Analysis Date = 05/10/13 Pct Recovery = 62% Analysis Date = 05/10/13 Pct Recovery = 62% Analysis Date = 04/30/13 Pct Recovery = 62% Analysis Date = 04/30/13 Pct Recovery = 62% Analysis Date = 04/19/13 Pct Recovery = 62% Analysis Date = 04/19/13 Pct Recovery = 62% Analysis Date = 04/09/13 Pct Recovery = 62% Analysis Date = 04/09/13 Pct Recovery = 62% Analysis Date = 03/29/13 Pct Recovery = 62% Analysis Date = 03/29/13 Pct Recovery = 62% Analysis Date = 03/19/13 Pct Recovery = 62% Analysis Date = 03/19/13 Pct Recovery = 62% Analysis Date = 03/09/13 Pct Recovery = 62% Analysis Date = 03/09/13 Pct Recovery = 62% Analysis Date = 02/26/13 Pct Recovery = 61% Analysis Date = 02/26/13 Pct Recovery = 61% Analysis Date = 02/16/13 Pct Recovery = 61% Analysis Date = 02/16/13 Pct Recovery = 61% Analysis Date = 02/05/13 Pct Recovery = 61% Analysis Date = 02/05/13 Pct Recovery = 61% Analysis Date = 01/26/13 Pct Recovery = 61% Analysis Date = 01/26/13 Pct Recovery = 61% Analysis Date = 01/15/13 Pct Recovery = 61% Analysis Date = 01/15/13 Pct Recovery = 61% Analysis Date = 01/05/13 Pct Recovery = 61% Analysis Date = 01/05/13 Pct Recovery = 61% Analysis Date = 12/25/12 Pct Recovery = 60% Analysis Date = 12/25/12 Pct Recovery = 60% Analysis Date = 12/15/12 Pct Recovery = 60% Analysis Date = 12/15/12 Pct Recovery = 60% Analysis Date = 12/04/12 Pct Recovery = 60% Analysis Date = 12/04/12 Pct Recovery = 60% Analysis Date = 11/24/12 Pct Recovery = 60% Analysis Date = 11/24/12 Pct Recovery = 60% Analysis Date = 11/14/12 Pct Recovery = 60% Analysis Date = 11/14/12 Pct Recovery = 60% Analysis Date = 11/03/12 Pct Recovery = 60% Analysis Date = 11/03/12 Pct Recovery = 60% Analysis Date = 10/24/12 Pct Recovery = 60% Analysis Date = 10/24/12 Pct Recovery = 60% Analysis Date = 10/13/12 Pct Recovery = 59% Analysis Date = 10/13/12 Pct Recovery = 59% Analysis Date = 10/03/12 Pct Recovery = 59% Analysis Date = 10/03/12 Pct Recovery = 59% Analysis Date = 09/22/12 Pct Recovery = 59% Analysis Date = 09/22/12 Pct Recovery = 59% Analysis Date = 09/12/12 Pct Recovery = 59% Analysis Date = 09/12/12 Pct Recovery = 59% Analysis Date = 09/01/12 Pct Recovery = 59% Analysis Date = 09/01/12 Pct Recovery = 59% Analysis Date = 08/22/12 Pct Recovery = 59% Analysis Date = 08/22/12 Pct Recovery = 59% Analysis Date = 08/11/12 Pct Recovery = 58% Analysis Date = 08/11/12 Pct Recovery = 58% Analysis Date = 08/01/12 Pct Recovery = 58% Analysis Date = 08/01/12 Pct Recovery = 58% Analysis Date = 07/21/12 Pct Recovery = 58% Analysis Date = 07/21/12 Pct Recovery = 58% Analysis Date = 07/11/12 Pct Recovery = 58% Analysis Date = 07/11/12 Pct Recovery = 58% Analysis Date = 07/01/12 Pct Recovery = 58% Analysis Date = 07/01/12 Pct Recovery = 58% Analysis Date = 06/20/12 Pct Recovery = 58% Analysis Date = 06/20/12 Pct Recovery = 58% Analysis Date = 06/10/12 Pct Recovery = 58% Analysis Date = 06/10/12 Pct Recovery = 58% Analysis Date = 05/30/12 Pct Recovery = 58% Analysis Date = 05/30/12 Pct Recovery = 58% Analysis Date = 05/20/12 Pct Recovery = 58% Analysis Date = 05/20/12 Pct Recovery = 58% Analysis Date = 05/09/12 Pct Recovery = 58% Analysis Date = 05/09/12 Pct Recovery = 58% Analysis Date = 04/29/12 Pct Recovery = 58% Analysis Date = 04/29/12 Pct Recovery = 58% Analysis Date = 04/18/12 Pct Recovery = 59% Analysis Date = 04/18/12 Pct Recovery = 59% Analysis Date = 04/08/12 Pct Recovery = 59% Analysis Date = 04/08/12 Pct Recovery = 59% Analysis Date = 03/28/12 Pct Recovery = 59% Analysis Date = 03/28/12 Pct Recovery = 59% Analysis Date = 03/18/12 Pct Recovery = 59% Analysis Date = 03/18/12 Pct Recovery = 59% Analysis Date = 03/07/12 Pct Recovery = 59% Analysis Date = 03/07/12 Pct Recovery = 59% Analysis Date = 02/26/12 Pct Recovery = 59% Analysis Date = 02/26/12 Pct Recovery = 59% Analysis Date = 02/16/12 Pct Recovery = 59% Analysis Date = 02/16/12 Pct Recovery = 59% Analysis Date = 02/05/12 Pct Recovery = 59% Analysis Date = 02/05/12 Pct Recovery = 59% Analysis Date = 01/26/12 Pct Recovery = 59% Analysis Date = 01/26/12 Pct Recovery = 59% Analysis Date = 01/15/12 Pct Recovery = 59% Analysis Date = 01/15/12 Pct Recovery = 59% Analysis Date = 01/05/12 Pct Recovery = 59% Analysis Date = 01/05/12 Pct Recovery = 59% Analysis Date = 12/25/11 Pct Recovery = 59% Analysis Date = 12/25/11 Pct Recovery = 59% Analysis Date = 12/15/11 Pct Recovery = 59% Analysis Date = 12/15/11 Pct Recovery = 59% Analysis Date = 12/04/11 Pct Recovery = 59% Analysis Date = 12/04/11 Pct Recovery = 59% Analysis Date = 11/24/11 Pct Recovery = 59% Analysis Date = 11/24/11 Pct Recovery = 59% Analysis Date = 11/13/11 Pct Recovery = 59% Analysis Date = 11/13/11 Pct Recovery = 59% Analysis Date = 11/03/11 Pct Recovery = 59% Analysis Date = 11/03/11 Pct Recovery = 59% Analysis Date = 10/23/11 Pct Recovery = 59% Analysis Date = 10/23/11 Pct Recovery = 59% Analysis Date = 10/13/11 Pct Recovery = 59% Analysis Date = 10/13/11 Pct Recovery = 59% Analysis Date = 10/03/11 Pct Recovery = 59% Analysis Date = 10/03/11 Pct Recovery = 59% Analysis Date = 09/22/11 Pct Recovery = 60% Analysis Date = 09/22/11 Pct Recovery = 60% Analysis Date = 09/12/11 Pct Recovery = 60% Analysis Date = 09/12/11 Pct Recovery = 60% Analysis Date = 09/01/11 Pct Recovery = 60% Analysis Date = 09/01/11 Pct Recovery = 60% Analysis Date = 08/22/11 Pct Recovery = 60% Analysis Date = 08/22/11 Pct Recovery = 60% Analysis Date = 08/11/11 Pct Recovery = 60% Analysis Date = 08/11/11 Pct Recovery = 60% Analysis Date = 08/01/11 Pct Recovery = 60% Analysis Date = 08/01/11 Pct Recovery = 60% Analysis Date = 07/21/11 Pct Recovery = 61% Analysis Date = 07/21/11 Pct Recovery = 61% Analysis Date = 07/11/11 Pct Recovery = 61% Analysis Date = 07/11/11 Pct Recovery = 61% Analysis Date = 06/30/11 Pct Recovery = 61% Analysis Date = 06/30/11 Pct Recovery = 61% Analysis Date = 06/20/11 Pct Recovery = 61% Analysis Date = 06/20/11 Pct Recovery = 61% Analysis Date = 06/10/11 Pct Recovery = 61% Analysis Date = 06/10/11 Pct Recovery = 61% Analysis Date = 05/30/11 Pct Recovery = 62% Analysis Date = 05/30/11 Pct Recovery = 62% Analysis Date = 05/20/11 Pct Recovery = 62% Analysis Date = 05/20/11 Pct Recovery = 62% Analysis Date = 05/09/11 Pct Recovery = 62% Analysis Date = 05/09/11 Pct Recovery = 62% Analysis Date = 04/29/11 Pct Recovery = 62% Analysis Date = 04/29/11 Pct Recovery = 62% Analysis Date = 04/18/11 Pct Recovery = 62% Analysis Date = 04/18/11 Pct Recovery = 62% Analysis Date = 04/08/11 Pct Recovery = 62% Analysis Date = 04/08/11 Pct Recovery = 62% Analysis Date = 03/28/11 Pct Recovery = 63% Analysis Date = 03/28/11 Pct Recovery = 63% Analysis Date = 03/18/11 Pct Recovery = 63% Analysis Date = 03/18/11 Pct Recovery = 63% Analysis Date = 03/07/11 Pct Recovery = 63% Analysis Date = 03/07/11 Pct Recovery = 63% Analysis Date = 02/25/11 Pct Recovery = 63% Analysis Date = 02/25/11 Pct Recovery = 63% Analysis Date = 02/14/11 Pct Recovery = 63% Analysis Date = 02/14/11 Pct Recovery = 63% Analysis Date = 02/04/11 Pct Recovery = 64% Analysis Date = 02/04/11 Pct Recovery = 64% Analysis Date = 01/25/11 Pct Recovery = 64% Analysis Date = 01/25/11 Pct Recovery = 64% Analysis Date = 01/14/11 Pct Recovery = 64% Analysis Date = 01/14/11 Pct Recovery = 64% Analysis Date = 01/04/11 Pct Recovery = 64% Analysis Date = 01/04/11 Pct Recovery = 64% Analysis Date = 12/24/10 Pct Recovery = 64% Analysis Date = 12/24/10 Pct Recovery = 64% Analysis Date = 12/14/10 Pct Recovery = 65% Analysis Date = 12/14/10 Pct Recovery = 65% Analysis Date = 12/03/10 Pct Recovery = 65% Analysis Date = 12/03/10 Pct Recovery = 65% Analysis Date = 11/23/10 Pct Recovery = 65% Analysis Date = 11/23/10 Pct Recovery = 65% Analysis Date = 11/12/10 Pct Recovery = 65% Analysis Date = 11/12/10 Pct Recovery = 65% Analysis Date = 11/02/10 Pct Recovery = 66% Analysis Date = 11/02/10 Pct Recovery = 66% Analysis Date = 10/22/10 Pct Recovery = 66% Analysis Date = 10/22/10 Pct Recovery = 66% Analysis Date = 10/12/10 Pct Recovery = 66% Analysis Date = 10/12/10 Pct Recovery = 66% Analysis Date = 10/01/10 Pct Recovery = 66% Analysis Date = 10/01/10 Pct Recovery = 66% Analysis Date = 09/21/10 Pct Recovery = 66% Analysis Date = 09/21/10 Pct Recovery = 66% Analysis Date = 09/11/10 Pct Recovery = 67% Analysis Date = 09/11/10 Pct Recovery = 67% Analysis Date = 08/31/10 Pct Recovery = 67% Analysis Date = 08/31/10 Pct Recovery = 67% Analysis Date = 08/21/10 Pct Recovery = 67% Analysis Date = 08/21/10 Pct Recovery = 67% Analysis Date = 08/10/10 Pct Recovery = 67% Analysis Date = 08/10/10 Pct Recovery = 67% Analysis Date = 07/31/10 Pct Recovery = 67% Analysis Date = 07/31/10 Pct Recovery = 67% Analysis Date = 07/20/10 Pct Recovery = 68% Analysis Date = 07/20/10 Pct Recovery = 68% Analysis Date = 07/10/10 Pct Recovery = 68% Analysis Date = 07/10/10 Pct Recovery = 68% Analysis Date = 06/29/10 Pct Recovery = 68% Analysis Date = 06/29/10 Pct Recovery = 68% Analysis Date = 06/19/10 Pct Recovery = 68% Analysis Date = 06/19/10 Pct Recovery = 68% Analysis Date = 06/08/10 Pct Recovery = 69% Analysis Date = 06/08/10 Pct Recovery = 69% Analysis Date = 05/29/10 Pct Recovery = 69% Analysis Date = 05/29/10 Pct Recovery = 69% Analysis Date = 05/19/10 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 88 64% 14% 62% 15%
Total 88 64% 14% 62% 15%

Sample Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Characteristic N % % Basis
Plotted 88 100% Spiked
Estimated Values 88 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 88 .  
False Negatives 0 0% 0 out of 88
Not Spiked 102 .  
False Positives 2 2% 2 out of 102