BQS OBSP Determination:
TERBUFOS-O-ANALOGUE SULFONE
METHOD: 2033 , TESTIDCODE: 61674GCM39
Open Data Set

Analysis Date = 01/18/14 SpikeMix = Abs 042413: 100 µl & Spex Organics T1130514013: 100 µl & Crescent 10802AL: 20 µl Pct Recovery = 89% Analysis Date = 10/19/13 SpikeMix = Abs 042413: 50 µl & Spex Organics T1130514013: 50 µl & Crescent 10802AL: 20 µl Pct Recovery = 64% Analysis Date = 12/05/13 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 20 µl Pct Recovery = 79% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 85% Analysis Date = 01/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 92% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 38% Analysis Date = 04/03/14 SpikeMix = Crescent 04CC101: 20 µl & ChemService 1473000: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 26% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 89% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 57% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 53% Analysis Date = 04/15/14 SpikeMix = Restek A093651: 20 µl & Abs 012513: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 49% Analysis Date = 01/31/14 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 60% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 56% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 57% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 70% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 76% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 87% Analysis Date = 01/08/14 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 68% Analysis Date = 11/04/13 SpikeMix = Restek A093651: 20 µl & Abs 052412: 20 µl & Crescent 10802AL: 5 µl Pct Recovery = 51% Analysis Date = 09/14/13 SpikeMix = Restek A093651: 50 µl & Abs 012513: 50 µl & Crescent 10802AL: 5 µl Pct Recovery = 69% Analysis Date = 08/25/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 114% Analysis Date = 12/16/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 106% Analysis Date = 06/30/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 72% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 104% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 100% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 107% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 138% Analysis Date = 04/14/14 Pct Recovery = 48% Analysis Date = 04/08/14 Pct Recovery = 48% Analysis Date = 04/08/14 Pct Recovery = 48% Analysis Date = 04/01/14 Pct Recovery = 49% Analysis Date = 04/01/14 Pct Recovery = 49% Analysis Date = 03/25/14 Pct Recovery = 50% Analysis Date = 03/25/14 Pct Recovery = 50% Analysis Date = 03/18/14 Pct Recovery = 51% Analysis Date = 03/18/14 Pct Recovery = 51% Analysis Date = 03/11/14 Pct Recovery = 52% Analysis Date = 03/11/14 Pct Recovery = 52% Analysis Date = 03/04/14 Pct Recovery = 53% Analysis Date = 03/04/14 Pct Recovery = 53% Analysis Date = 02/25/14 Pct Recovery = 54% Analysis Date = 02/25/14 Pct Recovery = 54% Analysis Date = 02/18/14 Pct Recovery = 55% Analysis Date = 02/18/14 Pct Recovery = 55% Analysis Date = 02/11/14 Pct Recovery = 55% Analysis Date = 02/11/14 Pct Recovery = 55% Analysis Date = 02/04/14 Pct Recovery = 56% Analysis Date = 02/04/14 Pct Recovery = 56% Analysis Date = 01/28/14 Pct Recovery = 57% Analysis Date = 01/28/14 Pct Recovery = 57% Analysis Date = 01/21/14 Pct Recovery = 58% Analysis Date = 01/21/14 Pct Recovery = 58% Analysis Date = 01/14/14 Pct Recovery = 59% Analysis Date = 01/14/14 Pct Recovery = 59% Analysis Date = 01/08/14 Pct Recovery = 60% Analysis Date = 01/08/14 Pct Recovery = 60% Analysis Date = 01/01/14 Pct Recovery = 60% Analysis Date = 01/01/14 Pct Recovery = 60% Analysis Date = 12/25/13 Pct Recovery = 61% Analysis Date = 12/25/13 Pct Recovery = 61% Analysis Date = 12/18/13 Pct Recovery = 62% Analysis Date = 12/18/13 Pct Recovery = 62% Analysis Date = 12/11/13 Pct Recovery = 63% Analysis Date = 12/11/13 Pct Recovery = 63% Analysis Date = 12/04/13 Pct Recovery = 63% Analysis Date = 12/04/13 Pct Recovery = 63% Analysis Date = 11/27/13 Pct Recovery = 64% Analysis Date = 11/27/13 Pct Recovery = 64% Analysis Date = 11/20/13 Pct Recovery = 65% Analysis Date = 11/20/13 Pct Recovery = 65% Analysis Date = 11/13/13 Pct Recovery = 66% Analysis Date = 11/13/13 Pct Recovery = 66% Analysis Date = 11/06/13 Pct Recovery = 66% Analysis Date = 11/06/13 Pct Recovery = 66% Analysis Date = 10/30/13 Pct Recovery = 67% Analysis Date = 10/30/13 Pct Recovery = 67% Analysis Date = 10/23/13 Pct Recovery = 67% Analysis Date = 10/23/13 Pct Recovery = 67% Analysis Date = 10/16/13 Pct Recovery = 68% Analysis Date = 10/16/13 Pct Recovery = 68% Analysis Date = 10/10/13 Pct Recovery = 68% Analysis Date = 10/10/13 Pct Recovery = 68% Analysis Date = 10/03/13 Pct Recovery = 69% Analysis Date = 10/03/13 Pct Recovery = 69% Analysis Date = 09/26/13 Pct Recovery = 69% Analysis Date = 09/26/13 Pct Recovery = 69% Analysis Date = 09/19/13 Pct Recovery = 70% Analysis Date = 09/19/13 Pct Recovery = 70% Analysis Date = 09/12/13 Pct Recovery = 70% Analysis Date = 09/12/13 Pct Recovery = 70% Analysis Date = 09/05/13 Pct Recovery = 71% Analysis Date = 09/05/13 Pct Recovery = 71% Analysis Date = 08/29/13 Pct Recovery = 71% Analysis Date = 08/29/13 Pct Recovery = 71% Analysis Date = 08/22/13 Pct Recovery = 72% Analysis Date = 08/22/13 Pct Recovery = 72% Analysis Date = 08/15/13 Pct Recovery = 72% Analysis Date = 08/15/13 Pct Recovery = 72% Analysis Date = 08/08/13 Pct Recovery = 72% Analysis Date = 08/08/13 Pct Recovery = 72% Analysis Date = 08/01/13 Pct Recovery = 73% Analysis Date = 08/01/13 Pct Recovery = 73% Analysis Date = 07/25/13 Pct Recovery = 73% Analysis Date = 07/25/13 Pct Recovery = 73% Analysis Date = 07/18/13 Pct Recovery = 74% Analysis Date = 07/18/13 Pct Recovery = 74% Analysis Date = 07/11/13 Pct Recovery = 74% Analysis Date = 07/11/13 Pct Recovery = 74% Analysis Date = 07/05/13 Pct Recovery = 75% Analysis Date = 07/05/13 Pct Recovery = 75% Analysis Date = 06/28/13 Pct Recovery = 75% Analysis Date = 06/28/13 Pct Recovery = 75% Analysis Date = 06/21/13 Pct Recovery = 75% Analysis Date = 06/21/13 Pct Recovery = 75% Analysis Date = 06/14/13 Pct Recovery = 76% Analysis Date = 06/14/13 Pct Recovery = 76% Analysis Date = 06/07/13 Pct Recovery = 76% Analysis Date = 06/07/13 Pct Recovery = 76% Analysis Date = 05/31/13 Pct Recovery = 77% Analysis Date = 05/31/13 Pct Recovery = 77% Analysis Date = 05/24/13 Pct Recovery = 77% Analysis Date = 05/24/13 Pct Recovery = 77% Analysis Date = 05/17/13 Pct Recovery = 78% Analysis Date = 05/17/13 Pct Recovery = 78% Analysis Date = 05/10/13 Pct Recovery = 78% Analysis Date = 05/10/13 Pct Recovery = 78% Analysis Date = 05/03/13 Pct Recovery = 79% Analysis Date = 05/03/13 Pct Recovery = 79% Analysis Date = 04/26/13 Pct Recovery = 79% Analysis Date = 04/26/13 Pct Recovery = 79% Analysis Date = 04/19/13 Pct Recovery = 80% Analysis Date = 04/19/13 Pct Recovery = 80% Analysis Date = 04/12/13 Pct Recovery = 80% Analysis Date = 04/12/13 Pct Recovery = 80% Analysis Date = 04/06/13 Pct Recovery = 81% Analysis Date = 04/06/13 Pct Recovery = 81% Analysis Date = 03/30/13 Pct Recovery = 82% Analysis Date = 03/30/13 Pct Recovery = 82% Analysis Date = 03/23/13 Pct Recovery = 83% Analysis Date = 03/23/13 Pct Recovery = 83% Analysis Date = 03/16/13 Pct Recovery = 84% Analysis Date = 03/16/13 Pct Recovery = 84% Analysis Date = 03/09/13 Pct Recovery = 84% Analysis Date = 03/09/13 Pct Recovery = 84% Analysis Date = 03/02/13 Pct Recovery = 85% Analysis Date = 03/02/13 Pct Recovery = 85% Analysis Date = 02/23/13 Pct Recovery = 86% Analysis Date = 02/23/13 Pct Recovery = 86% Analysis Date = 02/16/13 Pct Recovery = 87% Analysis Date = 02/16/13 Pct Recovery = 87% Analysis Date = 02/09/13 Pct Recovery = 88% Analysis Date = 02/09/13 Pct Recovery = 88% Analysis Date = 02/02/13 Pct Recovery = 88% Analysis Date = 02/02/13 Pct Recovery = 88% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/26/13 Pct Recovery = 89% Analysis Date = 01/19/13 Pct Recovery = 90% Analysis Date = 01/19/13 Pct Recovery = 90% Analysis Date = 01/12/13 Pct Recovery = 91% Analysis Date = 01/12/13 Pct Recovery = 91% Analysis Date = 01/06/13 Pct Recovery = 92% Analysis Date = 01/06/13 Pct Recovery = 92% Analysis Date = 12/30/12 Pct Recovery = 93% Analysis Date = 12/30/12 Pct Recovery = 93% Analysis Date = 12/23/12 Pct Recovery = 93% Analysis Date = 12/23/12 Pct Recovery = 93% Analysis Date = 12/16/12 Pct Recovery = 94% Analysis Date = 12/16/12 Pct Recovery = 94% Analysis Date = 12/09/12 Pct Recovery = 95% Analysis Date = 12/09/12 Pct Recovery = 95% Analysis Date = 12/02/12 Pct Recovery = 96% Analysis Date = 12/02/12 Pct Recovery = 96% Analysis Date = 11/25/12 Pct Recovery = 97% Analysis Date = 11/25/12 Pct Recovery = 97% Analysis Date = 11/18/12 Pct Recovery = 97% Analysis Date = 11/18/12 Pct Recovery = 97% Analysis Date = 11/11/12 Pct Recovery = 98% Analysis Date = 11/11/12 Pct Recovery = 98% Analysis Date = 11/04/12 Pct Recovery = 99% Analysis Date = 11/04/12 Pct Recovery = 99% Analysis Date = 10/28/12 Pct Recovery = 100% Analysis Date = 10/28/12 Pct Recovery = 100% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/21/12 Pct Recovery = 101% Analysis Date = 10/14/12 Pct Recovery = 101% Analysis Date = 10/14/12 Pct Recovery = 101% Analysis Date = 10/07/12 Pct Recovery = 102% Analysis Date = 10/07/12 Pct Recovery = 102% Analysis Date = 10/01/12 Pct Recovery = 103% Analysis Date = 10/01/12 Pct Recovery = 103% Analysis Date = 09/24/12 Pct Recovery = 104% Analysis Date = 09/24/12 Pct Recovery = 104% Analysis Date = 09/17/12 Pct Recovery = 105% Analysis Date = 09/17/12 Pct Recovery = 105% Analysis Date = 09/10/12 Pct Recovery = 104% Analysis Date = 09/10/12 Pct Recovery = 104% Analysis Date = 09/03/12 Pct Recovery = 104% Analysis Date = 09/03/12 Pct Recovery = 104% Analysis Date = 08/27/12 Pct Recovery = 104% Analysis Date = 08/27/12 Pct Recovery = 104% Analysis Date = 08/20/12 Pct Recovery = 104% Analysis Date = 08/20/12 Pct Recovery = 104% Analysis Date = 08/13/12 Pct Recovery = 103% Analysis Date = 08/13/12 Pct Recovery = 103% Analysis Date = 08/06/12 Pct Recovery = 103% Analysis Date = 08/06/12 Pct Recovery = 103% Analysis Date = 07/30/12 Pct Recovery = 103% Analysis Date = 07/30/12 Pct Recovery = 103% Analysis Date = 07/23/12 Pct Recovery = 103% Analysis Date = 07/23/12 Pct Recovery = 103% Analysis Date = 07/16/12 Pct Recovery = 102% Analysis Date = 07/16/12 Pct Recovery = 102% Analysis Date = 07/09/12 Pct Recovery = 102% Analysis Date = 07/09/12 Pct Recovery = 102% Analysis Date = 07/03/12 Pct Recovery = 102% Analysis Date = 07/03/12 Pct Recovery = 102% Analysis Date = 06/26/12 Pct Recovery = 102% Analysis Date = 06/26/12 Pct Recovery = 102% Analysis Date = 06/19/12 Pct Recovery = 102% Analysis Date = 06/19/12 Pct Recovery = 102% Analysis Date = 06/12/12 Pct Recovery = 101% Analysis Date = 06/12/12 Pct Recovery = 101% Analysis Date = 06/05/12 Pct Recovery = 101% Analysis Date = 06/05/12 Pct Recovery = 101% Analysis Date = 05/29/12 Pct Recovery = 101% Analysis Date = 05/29/12 Pct Recovery = 101% Analysis Date = 05/22/12 Pct Recovery = 101% Analysis Date = 05/22/12 Pct Recovery = 101% Analysis Date = 05/15/12 Pct Recovery = 100% Analysis Date = 05/15/12 Pct Recovery = 100% Analysis Date = 05/08/12 Pct Recovery = 100% Analysis Date = 05/08/12 Pct Recovery = 100% Analysis Date = 05/01/12 Pct Recovery = 100% Analysis Date = 05/01/12 Pct Recovery = 100% Analysis Date = 04/24/12 Pct Recovery = 100% Analysis Date = 04/24/12 Pct Recovery = 100% Analysis Date = 04/17/12 Pct Recovery = 99% Analysis Date = 04/17/12 Pct Recovery = 99% Analysis Date = 04/10/12 Pct Recovery = 99% Analysis Date = 04/10/12 Pct Recovery = 99% Analysis Date = 04/04/12 Pct Recovery = 99% Analysis Date = 04/04/12 Pct Recovery = 99% Analysis Date = 03/28/12 Pct Recovery = 99% Analysis Date = 03/28/12 Pct Recovery = 99% Analysis Date = 03/21/12 Pct Recovery = 99% Analysis Date = 03/21/12 Pct Recovery = 99% Analysis Date = 03/14/12 Pct Recovery = 98% Analysis Date = 03/14/12 Pct Recovery = 98% Analysis Date = 03/07/12 Pct Recovery = 98% Analysis Date = 03/07/12 Pct Recovery = 98% Analysis Date = 02/29/12 Pct Recovery = 98% Analysis Date = 02/29/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/22/12 Pct Recovery = 98% Analysis Date = 02/15/12 Pct Recovery = 97% Analysis Date = 02/15/12 Pct Recovery = 97% Analysis Date = 02/08/12 Pct Recovery = 97% Analysis Date = 02/08/12 Pct Recovery = 97% Analysis Date = 02/01/12 Pct Recovery = 97% Analysis Date = 02/01/12 Pct Recovery = 97% Analysis Date = 01/25/12 Pct Recovery = 97% Analysis Date = 01/25/12 Pct Recovery = 97% Analysis Date = 01/18/12 Pct Recovery = 96% Analysis Date = 01/18/12 Pct Recovery = 96% Analysis Date = 01/11/12 Pct Recovery = 96% Analysis Date = 01/11/12 Pct Recovery = 96% Analysis Date = 01/04/12 Pct Recovery = 96% Analysis Date = 01/04/12 Pct Recovery = 96% Analysis Date = 12/29/11 Pct Recovery = 96% Analysis Date = 12/29/11 Pct Recovery = 96% Analysis Date = 12/22/11 Pct Recovery = 96% Analysis Date = 12/22/11 Pct Recovery = 96% Analysis Date = 12/15/11 Pct Recovery = 95% Analysis Date = 12/15/11 Pct Recovery = 95% Analysis Date = 12/08/11 Pct Recovery = 95% Analysis Date = 12/08/11 Pct Recovery = 95% Analysis Date = 12/01/11 Pct Recovery = 95% Analysis Date = 12/01/11 Pct Recovery = 95% Analysis Date = 11/24/11 Pct Recovery = 95% Analysis Date = 11/24/11 Pct Recovery = 95% Analysis Date = 11/17/11 Pct Recovery = 94% Analysis Date = 11/17/11 Pct Recovery = 94% Analysis Date = 11/10/11 Pct Recovery = 94% Analysis Date = 11/10/11 Pct Recovery = 94% Analysis Date = 11/03/11 Pct Recovery = 94% Analysis Date = 11/03/11 Pct Recovery = 94% Analysis Date = 10/27/11 Pct Recovery = 94% Analysis Date = 10/27/11 Pct Recovery = 94% Analysis Date = 10/20/11 Pct Recovery = 93% Analysis Date = 10/20/11 Pct Recovery = 93% Analysis Date = 10/13/11 Pct Recovery = 93% Analysis Date = 10/13/11 Pct Recovery = 93% Analysis Date = 10/06/11 Pct Recovery = 93% Analysis Date = 10/06/11 Pct Recovery = 93% Analysis Date = 09/30/11 Pct Recovery = 93% Analysis Date = 09/30/11 Pct Recovery = 93% Analysis Date = 09/23/11 Pct Recovery = 93% Analysis Date = 09/23/11 Pct Recovery = 93% Analysis Date = 09/16/11 Pct Recovery = 92% Analysis Date = 09/16/11 Pct Recovery = 92% Analysis Date = 09/09/11 Pct Recovery = 92% Analysis Date = 09/09/11 Pct Recovery = 92% Analysis Date = 09/02/11 Pct Recovery = 92% Analysis Date = 09/02/11 Pct Recovery = 92% Analysis Date = 08/26/11 Pct Recovery = 92% Analysis Date = 08/26/11 Pct Recovery = 92% Analysis Date = 08/19/11 Pct Recovery = 91% Analysis Date = 08/19/11 Pct Recovery = 91% Analysis Date = 08/12/11 Pct Recovery = 91% Analysis Date = 08/12/11 Pct Recovery = 91% Analysis Date = 08/05/11 Pct Recovery = 91% Analysis Date = 08/05/11 Pct Recovery = 91% Analysis Date = 07/29/11 Pct Recovery = 91% Analysis Date = 07/29/11 Pct Recovery = 91% Analysis Date = 07/22/11 Pct Recovery = 90% Analysis Date = 07/22/11 Pct Recovery = 90% Analysis Date = 07/15/11 Pct Recovery = 90% Analysis Date = 07/15/11 Pct Recovery = 90% Analysis Date = 07/08/11 Pct Recovery = 90% Analysis Date = 07/08/11 Pct Recovery = 90% Analysis Date = 07/02/11 Pct Recovery = 90% Analysis Date = 07/02/11 Pct Recovery = 90% Analysis Date = 06/25/11 Pct Recovery = 89% Analysis Date = 06/25/11 Pct Recovery = 89% Analysis Date = 06/18/11 Pct Recovery = 89% Analysis Date = 06/18/11 Pct Recovery = 89% Analysis Date = 06/11/11 Pct Recovery = 89% Analysis Date = 06/11/11 Pct Recovery = 89% Analysis Date = 06/04/11 Pct Recovery = 89% Analysis Date = 06/04/11 Pct Recovery = 89% Analysis Date = 05/28/11 Pct Recovery = 89% Analysis Date = 05/28/11 Pct Recovery = 89% Analysis Date = 05/21/11 Pct Recovery = 89% Analysis Date = 05/21/11 Pct Recovery = 89% Analysis Date = 05/14/11 Pct Recovery = 89% Analysis Date = 05/14/11 Pct Recovery = 89% Analysis Date = 05/07/11 Pct Recovery = 89% Analysis Date = 05/07/11 Pct Recovery = 89% Analysis Date = 04/30/11 Pct Recovery = 89% Analysis Date = 04/30/11 Pct Recovery = 89% Analysis Date = 04/23/11 Pct Recovery = 89% Analysis Date = 04/23/11 Pct Recovery = 89% Analysis Date = 04/16/11 Pct Recovery = 89% Analysis Date = 04/16/11 Pct Recovery = 89% Analysis Date = 04/09/11 Pct Recovery = 89% Analysis Date = 04/09/11 Pct Recovery = 89% Analysis Date = 04/02/11 Pct Recovery = 89% Analysis Date = 04/02/11 Pct Recovery = 89% Analysis Date = 03/27/11 Pct Recovery = 89% Analysis Date = 03/27/11 Pct Recovery = 89% Analysis Date = 03/20/11 Pct Recovery = 89% Analysis Date = 03/20/11 Pct Recovery = 89% Analysis Date = 03/13/11 Pct Recovery = 89% Analysis Date = 03/13/11 Pct Recovery = 89% Analysis Date = 03/06/11 Pct Recovery = 89% Analysis Date = 03/06/11 Pct Recovery = 89% Analysis Date = 02/27/11 Pct Recovery = 89% Analysis Date = 02/27/11 Pct Recovery = 89% Analysis Date = 02/20/11 Pct Recovery = 88% Analysis Date = 02/20/11 Pct Recovery = 88% Analysis Date = 02/13/11 Pct Recovery = 88% Analysis Date = 02/13/11 Pct Recovery = 88% Analysis Date = 02/06/11 Pct Recovery = 88% Analysis Date = 02/06/11 Pct Recovery = 88% Analysis Date = 01/30/11 Pct Recovery = 88% Analysis Date = 01/30/11 Pct Recovery = 88% Analysis Date = 01/23/11 Pct Recovery = 88% Analysis Date = 01/23/11 Pct Recovery = 88% Analysis Date = 01/16/11 Pct Recovery = 88% Analysis Date = 01/16/11 Pct Recovery = 88% Analysis Date = 01/09/11 Pct Recovery = 88% Analysis Date = 01/09/11 Pct Recovery = 88% Analysis Date = 01/02/11 Pct Recovery = 88% Analysis Date = 01/02/11 Pct Recovery = 88% Analysis Date = 12/27/10 Pct Recovery = 88% Analysis Date = 12/27/10 Pct Recovery = 88% Analysis Date = 12/20/10 Pct Recovery = 88% Analysis Date = 12/20/10 Pct Recovery = 88% Analysis Date = 12/13/10 Pct Recovery = 88% Analysis Date = 12/13/10 Pct Recovery = 88% Analysis Date = 12/06/10 Pct Recovery = 88% Analysis Date = 12/06/10 Pct Recovery = 88% Analysis Date = 11/29/10 Pct Recovery = 88% Analysis Date = 11/29/10 Pct Recovery = 88% Analysis Date = 11/22/10 Pct Recovery = 88% Analysis Date = 11/22/10 Pct Recovery = 88% Analysis Date = 11/15/10 Pct Recovery = 88% Analysis Date = 11/15/10 Pct Recovery = 88% Analysis Date = 11/08/10 Pct Recovery = 88% Analysis Date = 11/08/10 Pct Recovery = 88% Analysis Date = 11/01/10 Pct Recovery = 88% Analysis Date = 11/01/10 Pct Recovery = 88% Analysis Date = 10/25/10 Pct Recovery = 88% Analysis Date = 10/25/10 Pct Recovery = 88% Analysis Date = 10/18/10 Pct Recovery = 88% Analysis Date = 10/18/10 Pct Recovery = 88% Analysis Date = 10/11/10 Pct Recovery = 88% Analysis Date = 10/11/10 Pct Recovery = 88% Analysis Date = 10/04/10 Pct Recovery = 88% Analysis Date = 10/04/10 Pct Recovery = 88% Analysis Date = 09/28/10 Pct Recovery = 88% Analysis Date = 09/28/10 Pct Recovery = 88% Analysis Date = 09/21/10 Pct Recovery = 88% Analysis Date = 09/21/10 Pct Recovery = 88% Analysis Date = 09/14/10 Pct Recovery = 88% Analysis Date = 09/14/10 Pct Recovery = 88% Analysis Date = 09/07/10 Pct Recovery = 88% Analysis Date = 09/07/10 Pct Recovery = 88% Analysis Date = 08/31/10 Pct Recovery = 88% Analysis Date = 08/31/10 Pct Recovery = 88% Analysis Date = 08/24/10 Pct Recovery = 88% Analysis Date = 08/24/10 Pct Recovery = 88% Analysis Date = 08/17/10 Pct Recovery = 88% Analysis Date = 08/17/10 Pct Recovery = 88% Analysis Date = 08/10/10 Pct Recovery = 88% Analysis Date = 08/10/10 Pct Recovery = 88% Analysis Date = 08/03/10 Pct Recovery = 88% Analysis Date = 08/03/10 Pct Recovery = 88% Analysis Date = 07/27/10 Pct Recovery = 88% Analysis Date = 07/27/10 Pct Recovery = 88% Analysis Date = 07/20/10 Pct Recovery = 88% Analysis Date = 07/20/10 Pct Recovery = 88% Analysis Date = 07/13/10 Pct Recovery = 88% Analysis Date = 07/13/10 Pct Recovery = 88% Analysis Date = 07/06/10 Pct Recovery = 88% Analysis Date = 07/06/10 Pct Recovery = 88% Analysis Date = 06/30/10 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS-O-ANALOGUE SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 106% 19% 106% 11%
>= Reporting Level 20 66% 18% 66% 20%
Total 27 76% 25% 72% 25%

Sample Statistics
TERBUFOS-O-ANALOGUE SULFONE

Characteristic N % % Basis
Plotted 27 79% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 7 21% 7 out of 34
Not Spiked 156 .  
False Positives 0 0% 0 out of 156