BQS OBSP Determination:
FIPRONIL SULFONE
METHOD: 2033 , TESTIDCODE: 62168GCM29
Open Data Set

Analysis Date = 09/20/13 SpikeMix = Spex Organics T1130514013: 100 µl & ERA 0318-13-02.2: 100 µl Pct Recovery = 73% Analysis Date = 12/06/12 SpikeMix = Abs 052412: 100 µl & ERA 0507-12-04.2: 100 µl Pct Recovery = 76% Analysis Date = 11/20/12 SpikeMix = Spex Organics T1120530013: 100 µl & Supelco LB92783: 100 µl Pct Recovery = 79% Analysis Date = 06/05/13 SpikeMix = ChemService 1473000: 50 µl & Supelco LB99392: 50 µl Pct Recovery = 169% Analysis Date = 08/19/13 SpikeMix = Supelco LB99392: 50 µl & Crescent 04CC101: 50 µl Pct Recovery = 73% Analysis Date = 09/24/13 SpikeMix = ERA 0318-13-02.2: 50 µl & Abs 042413: 50 µl & Crescent 10802AL: 10 µl Pct Recovery = 74% Analysis Date = 02/12/14 SpikeMix = Spex Organics T1130514013: 50 µl & ERA 0318-13-02.2: 50 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 78% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 01/28/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 87% Analysis Date = 05/15/12 SpikeMix = Restek A075606: 80 µl Pct Recovery = 74% Analysis Date = 11/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 72% Analysis Date = 09/13/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 44% Analysis Date = 09/01/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 62% Analysis Date = 11/17/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 83% Analysis Date = 10/02/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 90% Analysis Date = 07/14/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 84% Analysis Date = 06/20/11 SpikeMix = Restek A075606: 80 µl Pct Recovery = 69% Analysis Date = 02/09/11 SpikeMix = Supelco LB77168: 80 µl Pct Recovery = 71% Analysis Date = 09/09/10 SpikeMix = Accu 209081187: 40 µl Pct Recovery = 86% Analysis Date = 01/15/13 SpikeMix = Spex Organics T1120530013: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 78% Analysis Date = 04/22/13 SpikeMix = Abs 052412: 50 µl & ERA 0507-12-04.2: 50 µl Pct Recovery = 80% Analysis Date = 10/12/12 SpikeMix = ERA 0507-12-04.2: 50 µl Pct Recovery = 95% Analysis Date = 12/14/10 SpikeMix = Accu 209081187: 40 µl Pct Recovery = 77% Analysis Date = 01/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 90% Analysis Date = 04/02/13 SpikeMix = Spex Organics T1120530013: 50 µl & Supelco LB92783: 50 µl Pct Recovery = 87% Analysis Date = 01/17/13 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 80% Analysis Date = 10/18/12 SpikeMix = Supelco LB92783: 50 µl & Abs 052412: 50 µl Pct Recovery = 73% Analysis Date = 07/21/10 SpikeMix = Crescent 08Ll064: 40 µl Pct Recovery = 47% Analysis Date = 04/20/11 SpikeMix = NWQL PSP2SP117A: 100 µl Pct Recovery = 80% Analysis Date = 10/04/14 SpikeMix = Supelco LC06435: 60 µl & Spex Organics E1140407002: 60 µl Pct Recovery = 82% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 88% Analysis Date = 12/04/14 SpikeMix = Abs 032714: 60 µl & NSI 042814: 60 µl Pct Recovery = 75% Analysis Date = 07/09/14 SpikeMix = Spex Organics E1140407002: 60 µl & ERA 0227-14-08: 60 µl Pct Recovery = 93% Analysis Date = 11/19/14 SpikeMix = Spex Organics E1140407002: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 66% Analysis Date = 05/20/14 SpikeMix = Supelco LC06435: 60 µl & Abs 032714: 60 µl Pct Recovery = 74% Analysis Date = 08/27/14 SpikeMix = Crescent 03DD006: 60 µl & Abs 032714: 60 µl Pct Recovery = 62% Analysis Date = 06/22/11 SpikeMix = NWQL PSP2SP117A: 75 µl Pct Recovery = 64% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 88% Analysis Date = 03/08/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 114% Analysis Date = 05/25/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 80% Analysis Date = 04/23/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 72% Analysis Date = 03/05/14 SpikeMix = Supelco LB99392: 20 µl & Crescent 04CC101: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 79% Analysis Date = 11/23/13 SpikeMix = Supelco LB99392: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 131% Analysis Date = 11/09/13 SpikeMix = Spex Organics T1130514013: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 86% Analysis Date = 01/08/14 SpikeMix = ChemService 1473000: 20 µl & Supelco LB99392: 20 µl Pct Recovery = 87% Analysis Date = 02/14/12 SpikeMix = Restek A075606: 40 µl Pct Recovery = 59% Analysis Date = 12/04/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 92% Analysis Date = 08/17/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 116% Analysis Date = 03/09/12 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 81% Analysis Date = 12/22/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 90% Analysis Date = 09/24/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 86% Analysis Date = 07/20/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 113% Analysis Date = 03/30/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 70% Analysis Date = 01/10/14 SpikeMix = ERA 0318-13-02.2: 20 µl & Abs 042413: 20 µl & Crescent 10802AL: 10 µl Pct Recovery = 72% Analysis Date = 07/11/13 SpikeMix = ChemService 1473000: 20 µl & ERA 0318-13-02.2: 20 µl Pct Recovery = 84% Analysis Date = 06/11/13 SpikeMix = ERA 0318-13-02.2: 20 µl & Crescent 04CC101: 20 µl Pct Recovery = 104% Analysis Date = 01/18/11 SpikeMix = Supelco LB77168: 40 µl Pct Recovery = 56% Analysis Date = 01/09/11 SpikeMix = Restek A075606: 40 µl Pct Recovery = 96% Analysis Date = 05/07/10 SpikeMix = Accu 209081187: 20 µl Pct Recovery = 98% Analysis Date = 06/03/10 SpikeMix = Crescent 08Ll064: 20 µl Pct Recovery = 48% Analysis Date = 10/19/10 SpikeMix = Crescent 08Ll064: 20 µl Pct Recovery = 94% Analysis Date = 03/24/10 SpikeMix = Accu 209081187: 20 µl Pct Recovery = 96% Analysis Date = 07/17/14 SpikeMix = Supelco LC06435: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 72% Analysis Date = 06/30/14 SpikeMix = Crescent 03DD006: 30 µl & Spex Organics E1140407002: 30 µl Pct Recovery = 62% Analysis Date = 09/22/14 SpikeMix = Spex Organics E1140407002: 30 µl & NSI 042814: 30 µl Pct Recovery = 97% Analysis Date = 10/21/14 SpikeMix = Abs 032714: 30 µl & NSI 042814: 30 µl Pct Recovery = 108% Analysis Date = 05/28/14 SpikeMix = Spex Organics E1140407002: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 102% Analysis Date = 06/26/14 SpikeMix = Abs 032714: 30 µl & ERA 0227-14-08: 30 µl Pct Recovery = 106% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 04/29/14 SpikeMix = Crescent 03DD006: 30 µl & Abs 032714: 30 µl Pct Recovery = 59% Analysis Date = 09/05/12 SpikeMix = Spex Organics T1120530013: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 81% Analysis Date = 03/07/13 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 86% Analysis Date = 09/17/12 SpikeMix = Crescent 05BB029: 20 µl & ERA 0507-12-04.2: 20 µl Pct Recovery = 74% Analysis Date = 08/25/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 120% Analysis Date = 12/16/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 97% Analysis Date = 02/22/13 SpikeMix = Spex Organics T1120530013: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 101% Analysis Date = 07/14/12 SpikeMix = Restek A088380: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 112% Analysis Date = 08/14/12 SpikeMix = Abs 052412: 20 µl & Supelco LB92783: 20 µl Pct Recovery = 141% Analysis Date = 06/30/10 SpikeMix = NWQL PSP2SP116C: 40 µl Pct Recovery = 59% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 99% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 108% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 64% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 92% Analysis Date = 03/05/11 SpikeMix = NWQL PSP2SP117A: 25 µl Pct Recovery = 147% Analysis Date = 02/09/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/29/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/18/16 Pct Recovery = 81% Analysis Date = 01/07/16 Pct Recovery = 81% Analysis Date = 01/07/16 Pct Recovery = 81% Analysis Date = 12/28/15 Pct Recovery = 81% Analysis Date = 12/28/15 Pct Recovery = 81% Analysis Date = 12/17/15 Pct Recovery = 81% Analysis Date = 12/17/15 Pct Recovery = 81% Analysis Date = 12/06/15 Pct Recovery = 81% Analysis Date = 12/06/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/25/15 Pct Recovery = 81% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/15/15 Pct Recovery = 82% Analysis Date = 11/04/15 Pct Recovery = 82% Analysis Date = 11/04/15 Pct Recovery = 82% Analysis Date = 10/24/15 Pct Recovery = 82% Analysis Date = 10/24/15 Pct Recovery = 82% Analysis Date = 10/13/15 Pct Recovery = 82% Analysis Date = 10/13/15 Pct Recovery = 82% Analysis Date = 10/03/15 Pct Recovery = 82% Analysis Date = 10/03/15 Pct Recovery = 82% Analysis Date = 09/22/15 Pct Recovery = 82% Analysis Date = 09/22/15 Pct Recovery = 82% Analysis Date = 09/11/15 Pct Recovery = 82% Analysis Date = 09/11/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/31/15 Pct Recovery = 82% Analysis Date = 08/21/15 Pct Recovery = 82% Analysis Date = 08/21/15 Pct Recovery = 82% Analysis Date = 08/10/15 Pct Recovery = 82% Analysis Date = 08/10/15 Pct Recovery = 82% Analysis Date = 07/30/15 Pct Recovery = 82% Analysis Date = 07/30/15 Pct Recovery = 82% Analysis Date = 07/19/15 Pct Recovery = 82% Analysis Date = 07/19/15 Pct Recovery = 82% Analysis Date = 07/09/15 Pct Recovery = 82% Analysis Date = 07/09/15 Pct Recovery = 82% Analysis Date = 06/28/15 Pct Recovery = 82% Analysis Date = 06/28/15 Pct Recovery = 82% Analysis Date = 06/17/15 Pct Recovery = 82% Analysis Date = 06/17/15 Pct Recovery = 82% Analysis Date = 06/06/15 Pct Recovery = 82% Analysis Date = 06/06/15 Pct Recovery = 82% Analysis Date = 05/27/15 Pct Recovery = 82% Analysis Date = 05/27/15 Pct Recovery = 82% Analysis Date = 05/16/15 Pct Recovery = 82% Analysis Date = 05/16/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 05/05/15 Pct Recovery = 82% Analysis Date = 04/25/15 Pct Recovery = 83% Analysis Date = 04/25/15 Pct Recovery = 83% Analysis Date = 04/14/15 Pct Recovery = 83% Analysis Date = 04/14/15 Pct Recovery = 83% Analysis Date = 04/03/15 Pct Recovery = 83% Analysis Date = 04/03/15 Pct Recovery = 83% Analysis Date = 03/23/15 Pct Recovery = 83% Analysis Date = 03/23/15 Pct Recovery = 83% Analysis Date = 03/13/15 Pct Recovery = 83% Analysis Date = 03/13/15 Pct Recovery = 83% Analysis Date = 03/02/15 Pct Recovery = 83% Analysis Date = 03/02/15 Pct Recovery = 83% Analysis Date = 02/19/15 Pct Recovery = 83% Analysis Date = 02/19/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 02/08/15 Pct Recovery = 83% Analysis Date = 01/29/15 Pct Recovery = 83% Analysis Date = 01/29/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/18/15 Pct Recovery = 83% Analysis Date = 01/07/15 Pct Recovery = 83% Analysis Date = 01/07/15 Pct Recovery = 83% Analysis Date = 12/27/14 Pct Recovery = 83% Analysis Date = 12/27/14 Pct Recovery = 83% Analysis Date = 12/17/14 Pct Recovery = 83% Analysis Date = 12/17/14 Pct Recovery = 83% Analysis Date = 12/06/14 Pct Recovery = 83% Analysis Date = 12/06/14 Pct Recovery = 83% Analysis Date = 11/25/14 Pct Recovery = 83% Analysis Date = 11/25/14 Pct Recovery = 83% Analysis Date = 11/14/14 Pct Recovery = 84% Analysis Date = 11/14/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 11/04/14 Pct Recovery = 84% Analysis Date = 10/24/14 Pct Recovery = 84% Analysis Date = 10/24/14 Pct Recovery = 84% Analysis Date = 10/13/14 Pct Recovery = 84% Analysis Date = 10/13/14 Pct Recovery = 84% Analysis Date = 10/02/14 Pct Recovery = 84% Analysis Date = 10/02/14 Pct Recovery = 84% Analysis Date = 09/22/14 Pct Recovery = 84% Analysis Date = 09/22/14 Pct Recovery = 84% Analysis Date = 09/11/14 Pct Recovery = 84% Analysis Date = 09/11/14 Pct Recovery = 84% Analysis Date = 08/31/14 Pct Recovery = 84% Analysis Date = 08/31/14 Pct Recovery = 84% Analysis Date = 08/21/14 Pct Recovery = 84% Analysis Date = 08/21/14 Pct Recovery = 84% Analysis Date = 08/10/14 Pct Recovery = 84% Analysis Date = 08/10/14 Pct Recovery = 84% Analysis Date = 07/30/14 Pct Recovery = 84% Analysis Date = 07/30/14 Pct Recovery = 84% Analysis Date = 07/19/14 Pct Recovery = 84% Analysis Date = 07/19/14 Pct Recovery = 84% Analysis Date = 07/09/14 Pct Recovery = 84% Analysis Date = 07/09/14 Pct Recovery = 84% Analysis Date = 06/28/14 Pct Recovery = 84% Analysis Date = 06/28/14 Pct Recovery = 84% Analysis Date = 06/17/14 Pct Recovery = 85% Analysis Date = 06/17/14 Pct Recovery = 85% Analysis Date = 06/06/14 Pct Recovery = 85% Analysis Date = 06/06/14 Pct Recovery = 85% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/27/14 Pct Recovery = 85% Analysis Date = 05/16/14 Pct Recovery = 85% Analysis Date = 05/16/14 Pct Recovery = 85% Analysis Date = 05/05/14 Pct Recovery = 85% Analysis Date = 05/05/14 Pct Recovery = 85% Analysis Date = 04/24/14 Pct Recovery = 85% Analysis Date = 04/24/14 Pct Recovery = 85% Analysis Date = 04/14/14 Pct Recovery = 85% Analysis Date = 04/14/14 Pct Recovery = 85% Analysis Date = 04/03/14 Pct Recovery = 85% Analysis Date = 04/03/14 Pct Recovery = 85% Analysis Date = 03/23/14 Pct Recovery = 85% Analysis Date = 03/23/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 85% Analysis Date = 03/12/14 Pct Recovery = 85% Analysis Date = 03/02/14 Pct Recovery = 85% Analysis Date = 03/02/14 Pct Recovery = 85% Analysis Date = 02/19/14 Pct Recovery = 86% Analysis Date = 02/19/14 Pct Recovery = 86% Analysis Date = 02/08/14 Pct Recovery = 86% Analysis Date = 02/08/14 Pct Recovery = 86% Analysis Date = 01/28/14 Pct Recovery = 86% Analysis Date = 01/28/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/18/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 01/07/14 Pct Recovery = 86% Analysis Date = 12/27/13 Pct Recovery = 86% Analysis Date = 12/27/13 Pct Recovery = 86% Analysis Date = 12/16/13 Pct Recovery = 86% Analysis Date = 12/16/13 Pct Recovery = 86% Analysis Date = 12/06/13 Pct Recovery = 86% Analysis Date = 12/06/13 Pct Recovery = 86% Analysis Date = 11/25/13 Pct Recovery = 86% Analysis Date = 11/25/13 Pct Recovery = 86% Analysis Date = 11/14/13 Pct Recovery = 86% Analysis Date = 11/14/13 Pct Recovery = 86% Analysis Date = 11/04/13 Pct Recovery = 87% Analysis Date = 11/04/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/24/13 Pct Recovery = 87% Analysis Date = 10/13/13 Pct Recovery = 87% Analysis Date = 10/13/13 Pct Recovery = 87% Analysis Date = 10/02/13 Pct Recovery = 87% Analysis Date = 10/02/13 Pct Recovery = 87% Analysis Date = 09/22/13 Pct Recovery = 87% Analysis Date = 09/22/13 Pct Recovery = 87% Analysis Date = 09/11/13 Pct Recovery = 87% Analysis Date = 09/11/13 Pct Recovery = 87% Analysis Date = 08/31/13 Pct Recovery = 87% Analysis Date = 08/31/13 Pct Recovery = 87% Analysis Date = 08/20/13 Pct Recovery = 87% Analysis Date = 08/20/13 Pct Recovery = 87% Analysis Date = 08/10/13 Pct Recovery = 87% Analysis Date = 08/10/13 Pct Recovery = 87% Analysis Date = 07/30/13 Pct Recovery = 87% Analysis Date = 07/30/13 Pct Recovery = 87% Analysis Date = 07/19/13 Pct Recovery = 88% Analysis Date = 07/19/13 Pct Recovery = 88% Analysis Date = 07/08/13 Pct Recovery = 88% Analysis Date = 07/08/13 Pct Recovery = 88% Analysis Date = 06/28/13 Pct Recovery = 88% Analysis Date = 06/28/13 Pct Recovery = 88% Analysis Date = 06/17/13 Pct Recovery = 88% Analysis Date = 06/17/13 Pct Recovery = 88% Analysis Date = 06/06/13 Pct Recovery = 88% Analysis Date = 06/06/13 Pct Recovery = 88% Analysis Date = 05/26/13 Pct Recovery = 88% Analysis Date = 05/26/13 Pct Recovery = 88% Analysis Date = 05/16/13 Pct Recovery = 88% Analysis Date = 05/16/13 Pct Recovery = 88% Analysis Date = 05/05/13 Pct Recovery = 88% Analysis Date = 05/05/13 Pct Recovery = 88% Analysis Date = 04/24/13 Pct Recovery = 88% Analysis Date = 04/24/13 Pct Recovery = 88% Analysis Date = 04/13/13 Pct Recovery = 88% Analysis Date = 04/13/13 Pct Recovery = 88% Analysis Date = 04/03/13 Pct Recovery = 88% Analysis Date = 04/03/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/23/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/12/13 Pct Recovery = 88% Analysis Date = 03/02/13 Pct Recovery = 88% Analysis Date = 03/02/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/19/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 02/08/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/28/13 Pct Recovery = 88% Analysis Date = 01/18/13 Pct Recovery = 88% Analysis Date = 01/18/13 Pct Recovery = 88% Analysis Date = 01/07/13 Pct Recovery = 88% Analysis Date = 01/07/13 Pct Recovery = 88% Analysis Date = 12/27/12 Pct Recovery = 88% Analysis Date = 12/27/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/16/12 Pct Recovery = 88% Analysis Date = 12/06/12 Pct Recovery = 89% Analysis Date = 12/06/12 Pct Recovery = 89% Analysis Date = 11/25/12 Pct Recovery = 88% Analysis Date = 11/25/12 Pct Recovery = 88% Analysis Date = 11/14/12 Pct Recovery = 88% Analysis Date = 11/14/12 Pct Recovery = 88% Analysis Date = 11/03/12 Pct Recovery = 88% Analysis Date = 11/03/12 Pct Recovery = 88% Analysis Date = 10/24/12 Pct Recovery = 88% Analysis Date = 10/24/12 Pct Recovery = 88% Analysis Date = 10/13/12 Pct Recovery = 88% Analysis Date = 10/13/12 Pct Recovery = 88% Analysis Date = 10/02/12 Pct Recovery = 88% Analysis Date = 10/02/12 Pct Recovery = 88% Analysis Date = 09/21/12 Pct Recovery = 88% Analysis Date = 09/21/12 Pct Recovery = 88% Analysis Date = 09/11/12 Pct Recovery = 88% Analysis Date = 09/11/12 Pct Recovery = 88% Analysis Date = 08/31/12 Pct Recovery = 88% Analysis Date = 08/31/12 Pct Recovery = 88% Analysis Date = 08/20/12 Pct Recovery = 88% Analysis Date = 08/20/12 Pct Recovery = 88% Analysis Date = 08/09/12 Pct Recovery = 87% Analysis Date = 08/09/12 Pct Recovery = 87% Analysis Date = 07/30/12 Pct Recovery = 87% Analysis Date = 07/30/12 Pct Recovery = 87% Analysis Date = 07/19/12 Pct Recovery = 87% Analysis Date = 07/19/12 Pct Recovery = 87% Analysis Date = 07/08/12 Pct Recovery = 87% Analysis Date = 07/08/12 Pct Recovery = 87% Analysis Date = 06/27/12 Pct Recovery = 87% Analysis Date = 06/27/12 Pct Recovery = 87% Analysis Date = 06/17/12 Pct Recovery = 87% Analysis Date = 06/17/12 Pct Recovery = 87% Analysis Date = 06/06/12 Pct Recovery = 87% Analysis Date = 06/06/12 Pct Recovery = 87% Analysis Date = 05/26/12 Pct Recovery = 87% Analysis Date = 05/26/12 Pct Recovery = 87% Analysis Date = 05/16/12 Pct Recovery = 87% Analysis Date = 05/16/12 Pct Recovery = 87% Analysis Date = 05/05/12 Pct Recovery = 86% Analysis Date = 05/05/12 Pct Recovery = 86% Analysis Date = 04/24/12 Pct Recovery = 86% Analysis Date = 04/24/12 Pct Recovery = 86% Analysis Date = 04/13/12 Pct Recovery = 86% Analysis Date = 04/13/12 Pct Recovery = 86% Analysis Date = 04/03/12 Pct Recovery = 86% Analysis Date = 04/03/12 Pct Recovery = 86% Analysis Date = 03/23/12 Pct Recovery = 86% Analysis Date = 03/23/12 Pct Recovery = 86% Analysis Date = 03/12/12 Pct Recovery = 86% Analysis Date = 03/12/12 Pct Recovery = 86% Analysis Date = 03/01/12 Pct Recovery = 86% Analysis Date = 03/01/12 Pct Recovery = 86% Analysis Date = 02/20/12 Pct Recovery = 86% Analysis Date = 02/20/12 Pct Recovery = 86% Analysis Date = 02/09/12 Pct Recovery = 86% Analysis Date = 02/09/12 Pct Recovery = 86% Analysis Date = 01/29/12 Pct Recovery = 85% Analysis Date = 01/29/12 Pct Recovery = 85% Analysis Date = 01/18/12 Pct Recovery = 85% Analysis Date = 01/18/12 Pct Recovery = 85% Analysis Date = 01/08/12 Pct Recovery = 85% Analysis Date = 01/08/12 Pct Recovery = 85% Analysis Date = 12/28/11 Pct Recovery = 85% Analysis Date = 12/28/11 Pct Recovery = 85% Analysis Date = 12/17/11 Pct Recovery = 85% Analysis Date = 12/17/11 Pct Recovery = 85% Analysis Date = 12/06/11 Pct Recovery = 85% Analysis Date = 12/06/11 Pct Recovery = 85% Analysis Date = 11/26/11 Pct Recovery = 85% Analysis Date = 11/26/11 Pct Recovery = 85% Analysis Date = 11/15/11 Pct Recovery = 85% Analysis Date = 11/15/11 Pct Recovery = 85% Analysis Date = 11/04/11 Pct Recovery = 85% Analysis Date = 11/04/11 Pct Recovery = 85% Analysis Date = 10/24/11 Pct Recovery = 85% Analysis Date = 10/24/11 Pct Recovery = 85% Analysis Date = 10/14/11 Pct Recovery = 85% Analysis Date = 10/14/11 Pct Recovery = 85% Analysis Date = 10/03/11 Pct Recovery = 85% Analysis Date = 10/03/11 Pct Recovery = 85% Analysis Date = 09/22/11 Pct Recovery = 85% Analysis Date = 09/22/11 Pct Recovery = 85% Analysis Date = 09/12/11 Pct Recovery = 85% Analysis Date = 09/12/11 Pct Recovery = 85% Analysis Date = 09/01/11 Pct Recovery = 85% Analysis Date = 09/01/11 Pct Recovery = 85% Analysis Date = 08/21/11 Pct Recovery = 85% Analysis Date = 08/21/11 Pct Recovery = 85% Analysis Date = 08/10/11 Pct Recovery = 84% Analysis Date = 08/10/11 Pct Recovery = 84% Analysis Date = 07/31/11 Pct Recovery = 84% Analysis Date = 07/31/11 Pct Recovery = 84% Analysis Date = 07/20/11 Pct Recovery = 84% Analysis Date = 07/20/11 Pct Recovery = 84% Analysis Date = 07/09/11 Pct Recovery = 84% Analysis Date = 07/09/11 Pct Recovery = 84% Analysis Date = 06/28/11 Pct Recovery = 84% Analysis Date = 06/28/11 Pct Recovery = 84% Analysis Date = 06/18/11 Pct Recovery = 84% Analysis Date = 06/18/11 Pct Recovery = 84% Analysis Date = 06/07/11 Pct Recovery = 84% Analysis Date = 06/07/11 Pct Recovery = 84% Analysis Date = 05/27/11 Pct Recovery = 84% Analysis Date = 05/27/11 Pct Recovery = 84% Analysis Date = 05/16/11 Pct Recovery = 84% Analysis Date = 05/16/11 Pct Recovery = 84% Analysis Date = 05/06/11 Pct Recovery = 84% Analysis Date = 05/06/11 Pct Recovery = 84% Analysis Date = 04/25/11 Pct Recovery = 84% Analysis Date = 04/25/11 Pct Recovery = 84% Analysis Date = 04/14/11 Pct Recovery = 84% Analysis Date = 04/14/11 Pct Recovery = 84% Analysis Date = 04/03/11 Pct Recovery = 84% Analysis Date = 04/03/11 Pct Recovery = 84% Analysis Date = 03/24/11 Pct Recovery = 84% Analysis Date = 03/24/11 Pct Recovery = 84% Analysis Date = 03/13/11 Pct Recovery = 84% Analysis Date = 03/13/11 Pct Recovery = 84% Analysis Date = 03/02/11 Pct Recovery = 84% Analysis Date = 03/02/11 Pct Recovery = 84% Analysis Date = 02/19/11 Pct Recovery = 84% Analysis Date = 02/19/11 Pct Recovery = 84% Analysis Date = 02/09/11 Pct Recovery = 84% Analysis Date = 02/09/11 Pct Recovery = 84% Analysis Date = 01/29/11 Pct Recovery = 84% Analysis Date = 01/29/11 Pct Recovery = 84% Analysis Date = 01/18/11 Pct Recovery = 83% Analysis Date = 01/18/11 Pct Recovery = 83% Analysis Date = 01/07/11 Pct Recovery = 83% Analysis Date = 01/07/11 Pct Recovery = 83% Analysis Date = 12/28/10 Pct Recovery = 83% Analysis Date = 12/28/10 Pct Recovery = 83% Analysis Date = 12/17/10 Pct Recovery = 83% Analysis Date = 12/17/10 Pct Recovery = 83% Analysis Date = 12/06/10 Pct Recovery = 83% Analysis Date = 12/06/10 Pct Recovery = 83% Analysis Date = 11/26/10 Pct Recovery = 83% Analysis Date = 11/26/10 Pct Recovery = 83% Analysis Date = 11/15/10 Pct Recovery = 83% Analysis Date = 11/15/10 Pct Recovery = 83% Analysis Date = 11/04/10 Pct Recovery = 83% Analysis Date = 11/04/10 Pct Recovery = 83% Analysis Date = 10/24/10 Pct Recovery = 83% Analysis Date = 10/24/10 Pct Recovery = 83% Analysis Date = 10/14/10 Pct Recovery = 83% Analysis Date = 10/14/10 Pct Recovery = 83% Analysis Date = 10/03/10 Pct Recovery = 83% Analysis Date = 10/03/10 Pct Recovery = 83% Analysis Date = 09/22/10 Pct Recovery = 83% Analysis Date = 09/22/10 Pct Recovery = 83% Analysis Date = 09/11/10 Pct Recovery = 83% Analysis Date = 09/11/10 Pct Recovery = 83% Analysis Date = 09/01/10 Pct Recovery = 83% Analysis Date = 09/01/10 Pct Recovery = 83% Analysis Date = 08/21/10 Pct Recovery = 83% Analysis Date = 08/21/10 Pct Recovery = 83% Analysis Date = 08/10/10 Pct Recovery = 83% Analysis Date = 08/10/10 Pct Recovery = 83% Analysis Date = 07/30/10 Pct Recovery = 83% Analysis Date = 07/30/10 Pct Recovery = 83% Analysis Date = 07/20/10 Pct Recovery = 83% Analysis Date = 07/20/10 Pct Recovery = 83% Analysis Date = 07/09/10 Pct Recovery = 83% Analysis Date = 07/09/10 Pct Recovery = 83% Analysis Date = 06/28/10 Pct Recovery = 83% Analysis Date = 06/28/10 Pct Recovery = 83% Analysis Date = 06/17/10 Pct Recovery = 83% Analysis Date = 06/17/10 Pct Recovery = 83% Analysis Date = 06/07/10 Pct Recovery = 83% Analysis Date = 06/07/10 Pct Recovery = 83% Analysis Date = 05/27/10 Pct Recovery = 83% Analysis Date = 05/27/10 Pct Recovery = 83% Analysis Date = 05/16/10 Pct Recovery = 83% Analysis Date = 05/16/10 Pct Recovery = 83% Analysis Date = 05/05/10 Pct Recovery = 83% Analysis Date = 05/05/10 Pct Recovery = 83% Analysis Date = 04/25/10 Pct Recovery = 83% Analysis Date = 04/25/10 Pct Recovery = 83% Analysis Date = 04/14/10 Pct Recovery = 83% Analysis Date = 04/14/10 Pct Recovery = 83% Analysis Date = 04/03/10 Pct Recovery = 83% Analysis Date = 04/03/10 Pct Recovery = 83% Analysis Date = 03/24/10 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 89 85% 21% 81% 16%
Total 89 85% 21% 81% 16%

Sample Statistics
FIPRONIL SULFONE

Characteristic N % % Basis
Plotted 89 99% Spiked
Estimated Values 6 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 90 .  
False Negatives 1 1% 1 out of 90
Not Spiked 100 .  
False Positives 3 3% 3 out of 100