BQS OBSP Determination:
11-KETOTESTOSTERONE
SCHEDULE: 4434 , TESTIDCODE: 64527GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
11-KETOTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 123% 15% 123% 16%
>= Reporting Level 18 89% 18% 94% 21%
Total 20 92% 21% 95% 23%

Sample Statistics
11-KETOTESTOSTERONE

Characteristic N % % Basis
Plotted 20 80% Spiked
Estimated Values 1 4% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 2 8% Spiked
Spiked 26 .  
False Negatives 3 12% 3 out of 25
Not Spiked 99 .  
False Positives 1 1% 1 out of 98

BQS OBSP Determination:
17-ALPHA-ESTRADIOL
SCHEDULE: 4434 , TESTIDCODE: 64528GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 62 86% 14% 86% 13%
Total 62 86% 14% 86% 13%

Sample Statistics
17-ALPHA-ESTRADIOL

Characteristic N % % Basis
Plotted 62 98% Spiked
Estimated Values 0 0% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 1 2% 1 out of 63
Not Spiked 61 .  
False Positives 0 0% 0 out of 61

BQS OBSP Determination:
17-ALPHA-ETHYNYLESTRADIOL
SCHEDULE: 4434 , TESTIDCODE: 64529GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ETHYNYLESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 60 81% 16% 80% 15%
Total 60 81% 16% 80% 15%

Sample Statistics
17-ALPHA-ETHYNYLESTRADIOL

Characteristic N % % Basis
Plotted 60 95% Spiked
Estimated Values 4 6% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 3 5% 3 out of 63
Not Spiked 61 .  
False Positives 0 0% 0 out of 61

BQS OBSP Determination:
17-BETA-ESTRADIOL
SCHEDULE: 4434 , TESTIDCODE: 64530GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
17-BETA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 63 85% 15% 85% 13%
Total 63 85% 15% 85% 13%

Sample Statistics
17-BETA-ESTRADIOL

Characteristic N % % Basis
Plotted 63 100% Spiked
Estimated Values 2 3% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 0 0% 0 out of 63
Not Spiked 61 .  
False Positives 1 2% 1 out of 61

BQS OBSP Determination:
3-BETA-COPROSTANOL
SCHEDULE: 4434 , TESTIDCODE: 64532GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
3-BETA-COPROSTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 53 109% 91% 93% 17%
Total 53 109% 91% 93% 17%

Sample Statistics
3-BETA-COPROSTANOL

Characteristic N % % Basis
Plotted 53 95% Spiked
Estimated Values 2 4% Spiked
Deleted Values 5 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 59 .  
False Negatives 3 5% 3 out of 56
Not Spiked 55 .  
False Positives 4 8% 4 out of 53

BQS OBSP Determination:
4-ANDROSTENE-3,17-DIONE
SCHEDULE: 4434 , TESTIDCODE: 64533GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
4-ANDROSTENE-3,17-DIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 73% 22% 75% 21%
Total 33 73% 22% 75% 21%

Sample Statistics
4-ANDROSTENE-3,17-DIONE

Characteristic N % % Basis
Plotted 33 97% Spiked
Estimated Values 1 3% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 34
Not Spiked 90 .  
False Positives 2 2% 2 out of 89

BQS OBSP Determination:
BISPHENOL A
SCHEDULE: 4434 , TESTIDCODE: 67305GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BISPHENOL A

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 107% 10% 106% 4%
>= Reporting Level 36 78% 20% 77% 18%
Total 41 82% 22% 81% 19%

Sample Statistics
BISPHENOL A

Characteristic N % % Basis
Plotted 41 93% Spiked
Estimated Values 4 9% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 3 7% Spiked
Spiked 45 .  
False Negatives 0 0% 0 out of 44
Not Spiked 78 .  
False Positives 0 0% 0 out of 78

BQS OBSP Determination:
CHOLESTEROL
SCHEDULE: 4434 , TESTIDCODE: 64534GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CHOLESTEROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 118% 87% 99% 17%
Total 56 118% 87% 99% 17%

Sample Statistics
CHOLESTEROL

Characteristic N % % Basis
Plotted 56 100% Spiked
Estimated Values 1 2% Spiked
Deleted Values 5 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 59 .  
False Negatives 0 0% 0 out of 56
Not Spiked 55 .  
False Positives 6 11% 6 out of 53

BQS OBSP Determination:
CIS-ANDROSTERONE
SCHEDULE: 4434 , TESTIDCODE: 64535GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CIS-ANDROSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 83% 27% 80% 16%
Total 46 83% 27% 80% 16%

Sample Statistics
CIS-ANDROSTERONE

Characteristic N % % Basis
Plotted 46 96% Spiked
Estimated Values 7 15% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 48 .  
False Negatives 1 2% 1 out of 48
Not Spiked 77 .  
False Positives 0 0% 0 out of 75

BQS OBSP Determination:
DIHYDROTESTOSTERONE
SCHEDULE: 4434 , TESTIDCODE: 64544GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DIHYDROTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 168% 91% 156% 98%
>= Reporting Level 24 67% 28% 66% 11%
Total 33 95% 69% 69% 17%

Sample Statistics
DIHYDROTESTOSTERONE

Characteristic N % % Basis
Plotted 33 94% Spiked
Estimated Values 8 23% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 35 .  
False Negatives 1 3% 1 out of 35
Not Spiked 90 .  
False Positives 0 0% 0 out of 89

BQS OBSP Determination:
EPITESTOSTERONE
SCHEDULE: 4434 , TESTIDCODE: 64537GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
EPITESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 58% 18% 52% 5%
>= Reporting Level 46 82% 23% 74% 15%
Total 51 79% 23% 74% 17%

Sample Statistics
EPITESTOSTERONE

Characteristic N % % Basis
Plotted 51 100% Spiked
Estimated Values 8 16% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 53 .  
False Negatives 0 0% 0 out of 51
Not Spiked 72 .  
False Positives 2 3% 2 out of 72

BQS OBSP Determination:
EQUILENIN
SCHEDULE: 4434 , TESTIDCODE: 64538GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
EQUILENIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 75% 29% 76% 34%
Total 46 75% 29% 76% 34%

Sample Statistics
EQUILENIN

Characteristic N % % Basis
Plotted 46 94% Spiked
Estimated Values 8 16% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 3 6% 3 out of 49
Not Spiked 61 .  
False Positives 10 17% 10 out of 60

BQS OBSP Determination:
EQUILIN
SCHEDULE: 4434 , TESTIDCODE: 64539GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
EQUILIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 71% 18% 64% 1%
>= Reporting Level 51 66% 33% 64% 21%
Total 56 66% 32% 64% 19%

Sample Statistics
EQUILIN

Characteristic N % % Basis
Plotted 56 82% Spiked
Estimated Values 56 82% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 70 .  
False Negatives 11 16% 11 out of 68
Not Spiked 55 .  
False Positives 0 0% 0 out of 55

BQS OBSP Determination:
ESTRIOL
SCHEDULE: 4434 , TESTIDCODE: 64540GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ESTRIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 8 132% 149% 83% 11%
>= Reporting Level 60 79% 20% 76% 17%
Total 68 85% 55% 77% 17%

Sample Statistics
ESTRIOL

Characteristic N % % Basis
Plotted 68 91% Spiked
Estimated Values 11 15% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 76 .  
False Negatives 5 7% 5 out of 75
Not Spiked 49 .  
False Positives 3 6% 3 out of 49

BQS OBSP Determination:
ESTRONE
SCHEDULE: 4434 , TESTIDCODE: 64541GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ESTRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 67 90% 26% 85% 29%
Total 67 90% 26% 85% 29%

Sample Statistics
ESTRONE

Characteristic N % % Basis
Plotted 67 97% Spiked
Estimated Values 6 9% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 69 .  
False Negatives 1 1% 1 out of 69
Not Spiked 56 .  
False Positives 0 0% 0 out of 54

BQS OBSP Determination:
MESTRANOL
SCHEDULE: 4434 , TESTIDCODE: 64542GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
MESTRANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 143% . 143% 0%
>= Reporting Level 60 75% 50% 56% 25%
Total 61 76% 50% 56% 26%

Sample Statistics
MESTRANOL

Characteristic N % % Basis
Plotted 61 88% Spiked
Estimated Values 3 4% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 69 .  
False Negatives 7 10% 7 out of 69
Not Spiked 56 .  
False Positives 0 0% 0 out of 55

BQS OBSP Determination:
NORETHINDRONE
SCHEDULE: 4434 , TESTIDCODE: 64531GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 105% . 105% 0%
>= Reporting Level 57 81% 19% 76% 20%
Total 58 81% 19% 76% 21%

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 58 92% Spiked
Estimated Values 7 11% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 64 .  
False Negatives 5 8% 5 out of 63
Not Spiked 61 .  
False Positives 0 0% 0 out of 60

BQS OBSP Determination:
PROGESTERONE
SCHEDULE: 4434 , TESTIDCODE: 64543GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
PROGESTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 74% 34% 80% 32%
>= Reporting Level 47 52% 25% 48% 13%
Total 59 57% 28% 50% 19%

Sample Statistics
PROGESTERONE

Characteristic N % % Basis
Plotted 59 86% Spiked
Estimated Values 59 86% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 8 12% Spiked
Spiked 70 .  
False Negatives 2 3% 2 out of 69
Not Spiked 55 .  
False Positives 0 0% 0 out of 55

BQS OBSP Determination:
TESTOSTERONE
SCHEDULE: 4434 , TESTIDCODE: 64545GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 87% 14% 85% 11%
Total 36 87% 14% 85% 11%

Sample Statistics
TESTOSTERONE

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 89 .  
False Positives 0 0% 0 out of 87

BQS OBSP Determination:
TRANS-DIETHYLSTILBESTROL
SCHEDULE: 4434 , TESTIDCODE: 64536GM005
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRANS-DIETHYLSTILBESTROL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 80% . 80% 0%
>= Reporting Level 64 70% 16% 67% 17%
Total 65 70% 16% 67% 16%

Sample Statistics
TRANS-DIETHYLSTILBESTROL

Characteristic N % % Basis
Plotted 65 94% Spiked
Estimated Values 2 3% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 69 .  
False Negatives 4 6% 4 out of 69
Not Spiked 56 .  
False Positives 0 0% 0 out of 55