BQS ORGANIC BLIND SAMPLES
11-KETOTESTOSTERONE,
Schedule: 4434 Testid: 64527GM005
Measured in
06/19/08 TO 11/07/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
11-KETOTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 108% 21% 108% 22%
>= Reporting Level 8 79% 19% 72% 23%
Total 12 89% 24% 89% 30%

Miscellaneous Statistics for the Samples
11-KETOTESTOSTERONE

Characteristic N % % Basis
Plotted 12 71% Spiked
Estimated Values 1 6% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 3 18% Spiked
Spiked 17 .  
False Negatives 2 12% 2 out of 17
Not Spiked 95 .  
False Positives 1 1% 1 out of 94

BQS ORGANIC BLIND SAMPLES
17-ALPHA-ESTRADIOL,
Schedule: 4434 Testid: 64528GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
17-ALPHA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 53 87% 14% 88% 11%
Total 53 87% 14% 88% 11%

Miscellaneous Statistics for the Samples
17-ALPHA-ESTRADIOL

Characteristic N % % Basis
Plotted 53 98% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 54 .  
False Negatives 1 2% 1 out of 54
Not Spiked 58 .  
False Positives 0 0% 0 out of 58

BQS ORGANIC BLIND SAMPLES
17-ALPHA-ETHYNYLESTRADIOL,
Schedule: 4434 Testid: 64529GM005
Measured in
06/19/08 TO 12/18/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
17-ALPHA-ETHYNYLESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 82% 15% 81% 14%
Total 50 82% 15% 81% 14%

Miscellaneous Statistics for the Samples
17-ALPHA-ETHYNYLESTRADIOL

Characteristic N % % Basis
Plotted 50 93% Spiked
Estimated Values 4 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 54 .  
False Negatives 3 6% 3 out of 54
Not Spiked 58 .  
False Positives 0 0% 0 out of 58

BQS ORGANIC BLIND SAMPLES
17-BETA-ESTRADIOL,
Schedule: 4434 Testid: 64530GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
17-BETA-ESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 54 88% 15% 87% 14%
Total 54 88% 15% 87% 14%

Miscellaneous Statistics for the Samples
17-BETA-ESTRADIOL

Characteristic N % % Basis
Plotted 54 100% Spiked
Estimated Values 2 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 54 .  
False Negatives 0 0% 0 out of 54
Not Spiked 58 .  
False Positives 1 2% 1 out of 58

BQS ORGANIC BLIND SAMPLES
NORETHINDRONE,
Schedule: 4434 Testid: 64531GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
NORETHINDRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 105% . 105% 0%
>= Reporting Level 48 85% 19% 82% 19%
Total 49 85% 19% 83% 19%

Miscellaneous Statistics for the Samples
NORETHINDRONE

Characteristic N % % Basis
Plotted 49 91% Spiked
Estimated Values 7 13% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 54 .  
False Negatives 5 9% 5 out of 54
Not Spiked 58 .  
False Positives 0 0% 0 out of 57

BQS ORGANIC BLIND SAMPLES
3-BETA-COPROSTANOL,
Schedule: 4434 Testid: 64532GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
3-BETA-COPROSTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 102% 32% 94% 28%
Total 46 102% 32% 94% 28%

Miscellaneous Statistics for the Samples
3-BETA-COPROSTANOL

Characteristic N % % Basis
Plotted 46 100% Spiked
Estimated Values 3 7% Spiked
Deleted Values 7 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 46
Not Spiked 52 .  
False Positives 6 13% 6 out of 48

BQS ORGANIC BLIND SAMPLES
4-ANDROSTENE-3,17-DIONE,
Schedule: 4434 Testid: 64533GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
4-ANDROSTENE-3,17-DIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 21 90% 15% 87% 17%
Total 21 90% 15% 87% 17%

Miscellaneous Statistics for the Samples
4-ANDROSTENE-3,17-DIONE

Characteristic N % % Basis
Plotted 21 95% Spiked
Estimated Values 1 5% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 5% Spiked
Spiked 22 .  
False Negatives 0 0% 0 out of 22
Not Spiked 90 .  
False Positives 2 2% 2 out of 89

BQS ORGANIC BLIND SAMPLES
CHOLESTEROL,
Schedule: 4434 Testid: 64534GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
CHOLESTEROL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 46 108% 33% 99% 16%
Total 46 108% 33% 99% 16%

Miscellaneous Statistics for the Samples
CHOLESTEROL

Characteristic N % % Basis
Plotted 46 100% Spiked
Estimated Values 2 4% Spiked
Deleted Values 7 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 49 .  
False Negatives 0 0% 0 out of 46
Not Spiked 52 .  
False Positives 6 13% 6 out of 48

BQS ORGANIC BLIND SAMPLES
CIS-ANDROSTERONE,
Schedule: 4434 Testid: 64535GM005
Measured in
01/16/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
CIS-ANDROSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 89% 24% 83% 16%
Total 40 89% 24% 83% 16%

Miscellaneous Statistics for the Samples
CIS-ANDROSTERONE

Characteristic N % % Basis
Plotted 40 95% Spiked
Estimated Values 7 17% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 42 .  
False Negatives 1 2% 1 out of 42
Not Spiked 70 .  
False Positives 0 0% 0 out of 69

BQS ORGANIC BLIND SAMPLES
TRANS-DIETHYLSTILBESTROL,
Schedule: 4434 Testid: 64536GM005
Measured in
08/20/08 TO 12/18/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
TRANS-DIETHYLSTILBESTROL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 80% . 80% 0%
>= Reporting Level 51 70% 18% 66% 19%
Total 52 70% 18% 67% 19%

Miscellaneous Statistics for the Samples
TRANS-DIETHYLSTILBESTROL

Characteristic N % % Basis
Plotted 52 90% Spiked
Estimated Values 3 5% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 59 .  
False Negatives 6 10% 6 out of 58
Not Spiked 53 .  
False Positives 0 0% 0 out of 53

BQS ORGANIC BLIND SAMPLES
EPITESTOSTERONE,
Schedule: 4434 Testid: 64537GM005
Measured in
01/16/08 TO 12/18/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
EPITESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 58% 18% 52% 5%
>= Reporting Level 34 89% 23% 85% 18%
Total 39 85% 25% 82% 19%

Miscellaneous Statistics for the Samples
EPITESTOSTERONE

Characteristic N % % Basis
Plotted 39 100% Spiked
Estimated Values 8 21% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 40 .  
False Negatives 0 0% 0 out of 39
Not Spiked 72 .  
False Positives 2 3% 2 out of 72

BQS ORGANIC BLIND SAMPLES
EQUILENIN,
Schedule: 4434 Testid: 64538GM005
Measured in
06/09/08 TO 11/07/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
EQUILENIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 71% 29% 74% 26%
Total 38 71% 29% 74% 26%

Miscellaneous Statistics for the Samples
EQUILENIN

Characteristic N % % Basis
Plotted 38 90% Spiked
Estimated Values 10 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 42 .  
False Negatives 3 7% 3 out of 42
Not Spiked 41 .  
False Positives 4 10% 4 out of 41

BQS ORGANIC BLIND SAMPLES
EQUILIN,
Schedule: 4434 Testid: 64539GM005
Measured in
06/09/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
EQUILIN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 71% 18% 64% 1%
>= Reporting Level 42 68% 29% 68% 19%
Total 47 68% 28% 66% 19%

Miscellaneous Statistics for the Samples
EQUILIN

Characteristic N % % Basis
Plotted 47 80% Spiked
Estimated Values 47 80% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 61 .  
False Negatives 11 19% 11 out of 59
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

BQS ORGANIC BLIND SAMPLES
ESTRIOL,
Schedule: 4434 Testid: 64540GM005
Measured in
08/14/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
ESTRIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 96% 41% 84% 9%
>= Reporting Level 49 81% 21% 78% 17%
Total 58 83% 26% 80% 18%

Miscellaneous Statistics for the Samples
ESTRIOL

Characteristic N % % Basis
Plotted 58 88% Spiked
Estimated Values 11 17% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 3 5% Spiked
Spiked 67 .  
False Negatives 5 8% 5 out of 66
Not Spiked 45 .  
False Positives 3 7% 3 out of 45

BQS ORGANIC BLIND SAMPLES
ESTRONE,
Schedule: 4434 Testid: 64541GM005
Measured in
06/09/08 TO 12/18/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
ESTRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 56 98% 26% 94% 25%
Total 56 98% 26% 94% 25%

Miscellaneous Statistics for the Samples
ESTRONE

Characteristic N % % Basis
Plotted 56 95% Spiked
Estimated Values 5 8% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 59 .  
False Negatives 1 2% 1 out of 59
Not Spiked 53 .  
False Positives 0 0% 0 out of 52

BQS ORGANIC BLIND SAMPLES
MESTRANOL,
Schedule: 4434 Testid: 64542GM005
Measured in
06/09/08 TO 12/18/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
MESTRANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 143% . 143% 0%
>= Reporting Level 53 82% 46% 69% 26%
Total 54 83% 46% 69% 28%

Miscellaneous Statistics for the Samples
MESTRANOL

Characteristic N % % Basis
Plotted 54 92% Spiked
Estimated Values 3 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 3% Spiked
Spiked 59 .  
False Negatives 3 5% 3 out of 59
Not Spiked 53 .  
False Positives 0 0% 0 out of 53

BQS ORGANIC BLIND SAMPLES
PROGESTERONE,
Schedule: 4434 Testid: 64543GM005
Measured in
06/09/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
PROGESTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 15 84% 42% 87% 33%
>= Reporting Level 35 57% 26% 51% 11%
Total 50 65% 34% 52% 27%

Miscellaneous Statistics for the Samples
PROGESTERONE

Characteristic N % % Basis
Plotted 50 82% Spiked
Estimated Values 50 82% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 9 15% Spiked
Spiked 61 .  
False Negatives 2 3% 2 out of 61
Not Spiked 51 .  
False Positives 0 0% 0 out of 51

BQS ORGANIC BLIND SAMPLES
DIHYDROTESTOSTERONE,
Schedule: 4434 Testid: 64544GM005
Measured in
08/14/08 TO 02/08/13
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
DIHYDROTESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 11 142% 54% 156% 85%
>= Reporting Level 15 70% 35% 66% 8%
Total 26 100% 56% 71% 67%

Miscellaneous Statistics for the Samples
DIHYDROTESTOSTERONE

Characteristic N % % Basis
Plotted 26 96% Spiked
Estimated Values 8 30% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 4% Spiked
Spiked 27 .  
False Negatives 0 0% 0 out of 27
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

BQS ORGANIC BLIND SAMPLES
TESTOSTERONE,
Schedule: 4434 Testid: 64545GM005
Measured in
08/14/08 TO 12/18/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
TESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 25 94% 17% 90% 12%
Total 25 94% 17% 90% 12%

Miscellaneous Statistics for the Samples
TESTOSTERONE

Characteristic N % % Basis
Plotted 25 100% Spiked
Estimated Values 2 8% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 25 .  
False Negatives 0 0% 0 out of 25
Not Spiked 87 .  
False Positives 0 0% 0 out of 86

BQS ORGANIC BLIND SAMPLES
BISPHENOL A,
Schedule: 4434 Testid: 67305GM005
Measured in
02/01/10 TO 11/01/12
Open Data Set

Plot of pctrecov by newdate

Statistics for the Plotted Points
BISPHENOL A

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 107% 10% 106% 4%
>= Reporting Level 26 77% 16% 77% 16%
Total 31 82% 19% 84% 20%

Miscellaneous Statistics for the Samples
BISPHENOL A

Characteristic N % % Basis
Plotted 31 91% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 9% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 70 .  
False Positives 0 0% 0 out of 70