SAS Output

BQS ORGANIC BLIND SAMPLES

METALAXYL,

Schedule: 4433 Testid: 04254GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

METALAXYL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	5	99%	20%	104%	18%
>= Reporting Level	31	93%	16%	96%	12%
Total	36	94%	16%	96%	13%

Miscellaneous Statistics for the Samples

METALAXYL

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	7	19%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

2-METHYLNAPHTHALENE,

Schedule: 4433 Testid: 30194GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

2-METHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	72%	1%	72%	1%
>= Reporting Level	34	82%	15%	82%	13%
Total	36	82%	15%	81%	12%

Miscellaneous Statistics for the Samples

2-METHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	5	14%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

DICHLORVOS,

Schedule: 4433 Testid: 30218GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

DICHLORVOS

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	77%	14%	79%	12%
Total	36	77%	14%	79%	12%

Miscellaneous Statistics for the Samples

DICHLORVOS

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

BROMACIL,

Schedule: 4433 Testid: 30234GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

BROMACIL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	86%	13%	84%	15%
Total	34	86%	13%	84%	15%

Miscellaneous Statistics for the Samples

BROMACIL

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	5	15%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	0	0%	0 out of 34
Not Spiked	40	.
False Positives	0	0%	0 out of 40

BQS ORGANIC BLIND SAMPLES

BROMOFORM,

Schedule: 4433 Testid: 32104GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

BROMOFORM

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	67%	22%	67%	24%
>= Reporting Level	34	81%	13%	82%	10%
Total	36	81%	13%	82%	11%

Miscellaneous Statistics for the Samples

BROMOFORM

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	6	17%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

ANTHRACENE,

Schedule: 4433 Testid: 34220GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ANTHRACENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	74%	3%	74%	3%
>= Reporting Level	34	80%	13%	80%	13%
Total	36	80%	12%	79%	12%

Miscellaneous Statistics for the Samples

ANTHRACENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	5	14%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	23	.
False Positives	1	4%	1 out of 23

BQS ORGANIC BLIND SAMPLES

BENZO[A]PYRENE,

Schedule: 4433 Testid: 34247GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

BENZO[A]PYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	60%	11%	60%	11%
>= Reporting Level	34	80%	19%	85%	22%
Total	36	79%	20%	83%	22%

Miscellaneous Statistics for the Samples

BENZO[A]PYRENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	7	19%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

DIETHYL PHTHALATE,

Schedule: 4433 Testid: 34336GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

DIETHYL PHTHALATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	130%	2%	130%	2%
>= Reporting Level	34	88%	16%	90%	13%
Total	36	91%	19%	90%	13%

Miscellaneous Statistics for the Samples

DIETHYL PHTHALATE

Characteristic	N	%	% Basis
Plotted	36	97%	Spiked
Estimated Values	4	11%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	3%	Spiked
Spiked	37	.
False Negatives	0	0%	0 out of 37
Not Spiked	37	.
False Positives	8	22%	8 out of 37

BQS ORGANIC BLIND SAMPLES

FLUORANTHENE,

Schedule: 4433 Testid: 34376GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

FLUORANTHENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	81%	5%	81%	6%
>= Reporting Level	34	82%	13%	83%	13%
Total	36	82%	13%	83%	12%

Miscellaneous Statistics for the Samples

FLUORANTHENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

ISOPHORONE,

Schedule: 4433 Testid: 34408GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ISOPHORONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	119%	49%	119%	51%
>= Reporting Level	34	84%	13%	86%	10%
Total	36	86%	17%	86%	10%

Miscellaneous Statistics for the Samples

ISOPHORONE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

PHENANTHRENE,

Schedule: 4433 Testid: 34461GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

PHENANTHRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	72%	8%	72%	9%
>= Reporting Level	34	81%	15%	83%	15%
Total	36	80%	14%	80%	15%

Miscellaneous Statistics for the Samples

PHENANTHRENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	4	11%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

PYRENE,

Schedule: 4433 Testid: 34469GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

PYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	80%	4%	80%	4%
>= Reporting Level	34	82%	14%	82%	14%
Total	36	82%	14%	82%	12%

Miscellaneous Statistics for the Samples

PYRENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

TETRACHLORETHYLENE,

Schedule: 4433 Testid: 34475GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

TETRACHLORETHYLENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	44%	0%	44%	0%
>= Reporting Level	32	58%	9%	55%	9%
Total	34	57%	9%	55%	9%

Miscellaneous Statistics for the Samples

TETRACHLORETHYLENE

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	34	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	0	0%	0 out of 34
Not Spiked	40	.
False Positives	0	0%	0 out of 40

BQS ORGANIC BLIND SAMPLES

1,4-DICHLOROBENZENE,

Schedule: 4433 Testid: 34571GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

1,4-DICHLOROBENZENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	75%	3%	75%	3%
>= Reporting Level	14	75%	11%	77%	11%
Total	16	75%	10%	77%	10%

Miscellaneous Statistics for the Samples

1,4-DICHLOROBENZENE

Characteristic	N	%	% Basis
Plotted	16	100%	Spiked
Estimated Values	2	13%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	16	.
False Negatives	0	0%	0 out of 16
Not Spiked	58	.
False Positives	0	0%	0 out of 58

BQS ORGANIC BLIND SAMPLES

PHENOL,

Schedule: 4433 Testid: 34694GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

PHENOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	67%	18%	70%	16%
Total	36	67%	18%	70%	16%

Miscellaneous Statistics for the Samples

PHENOL

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	2	5%	2 out of 38

BQS ORGANIC BLIND SAMPLES

NAPHTHALENE,

Schedule: 4433 Testid: 34696GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

NAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	73%	4%	72%	4%
>= Reporting Level	32	87%	23%	85%	13%
Total	36	85%	22%	84%	13%

Miscellaneous Statistics for the Samples

NAPHTHALENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	8	22%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

CHLORPYRIFOS,

Schedule: 4433 Testid: 38932GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

CHLORPYRIFOS

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	86%	13%	88%	7%
Total	36	86%	13%	88%	7%

Miscellaneous Statistics for the Samples

CHLORPYRIFOS

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

PENTACHLOROPHENOL,

Schedule: 4433 Testid: 39032GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

PENTACHLOROPHENOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	11	76%	26%	78%	18%
>= Reporting Level	23	71%	22%	75%	22%
Total	34	73%	23%	76%	19%

Miscellaneous Statistics for the Samples

PENTACHLOROPHENOL

Characteristic	N	%	% Basis
Plotted	34	97%	Spiked
Estimated Values	34	97%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	1	3%	1 out of 35
Not Spiked	39	.
False Positives	0	0%	0 out of 39

BQS ORGANIC BLIND SAMPLES

PROMETON,

Schedule: 4433 Testid: 39056GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

PROMETON

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	106%	0%	106%	0%
>= Reporting Level	34	90%	16%	92%	15%
Total	36	90%	16%	93%	15%

Miscellaneous Statistics for the Samples

PROMETON

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	7	19%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

BIS(2-ETHYLHEXYL) PHTHALATE,

Schedule: 4433 Testid: 39100GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

BIS(2-ETHYLHEXYL) PHTHALATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	5	118%	75%	74%	104%
>= Reporting Level	23	56%	15%	56%	11%
Total	28	67%	40%	58%	10%

Miscellaneous Statistics for the Samples

BIS(2-ETHYLHEXYL) PHTHALATE

Characteristic	N	%	% Basis
Plotted	28	82%	Spiked
Estimated Values	10	29%	Spiked
Deleted Values	1	1%	Spiked + Not Spiked
Spiked, Censored	4	12%	Spiked
Spiked	35	.
False Negatives	2	6%	2 out of 34
Not Spiked	39	.
False Positives	4	10%	4 out of 39

BQS ORGANIC BLIND SAMPLES

DIAZINON,

Schedule: 4433 Testid: 39570GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

DIAZINON

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	37	87%	24%	95%	17%
Total	37	87%	24%	95%	17%

Miscellaneous Statistics for the Samples

DIAZINON

Characteristic	N	%	% Basis
Plotted	37	100%	Spiked
Estimated Values	1	3%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	37	.
False Negatives	0	0%	0 out of 37
Not Spiked	37	.
False Positives	1	3%	1 out of 37

BQS ORGANIC BLIND SAMPLES

ATRAZINE,

Schedule: 4433 Testid: 39630GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ATRAZINE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	90%	15%	92%	14%
Total	34	90%	15%	92%	14%

Miscellaneous Statistics for the Samples

ATRAZINE

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	1	3%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	0	0%	0 out of 34
Not Spiked	40	.
False Positives	1	3%	1 out of 40

BQS ORGANIC BLIND SAMPLES

CARBARYL,

Schedule: 4433 Testid: 39750GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

CARBARYL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	78%	24%	76%	18%
Total	36	78%	24%	76%	18%

Miscellaneous Statistics for the Samples

CARBARYL

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	36	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

3-TERT-BUTYL-4-HYDROXY ANISOLE (BHA),

Schedule: 4433 Testid: 61702GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

3-TERT-BUTYL-4-HYDROXY ANISOLE (BHA)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	35	47%	27%	41%	35%
Total	35	47%	27%	41%	35%

Miscellaneous Statistics for the Samples

3-TERT-BUTYL-4-HYDROXY ANISOLE (BHA)

Characteristic	N	%	% Basis
Plotted	35	97%	Spiked
Estimated Values	35	97%	Spiked
Deleted Values	2	3%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	1	3%	1 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

4-NONYLPHENOL DIETHOXYLATE, TOTAL (NPEO2),

Schedule: 4433 Testid: 61703GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/18/12

Open Data Set

Statistics for the Plotted Points

4-NONYLPHENOL DIETHOXYLATE, TOTAL (NPEO2)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	21	41%	29%	30%	10%
Total	21	41%	29%	30%	10%

Miscellaneous Statistics for the Samples

4-NONYLPHENOL DIETHOXYLATE, TOTAL (NPEO2)

Characteristic	N	%	% Basis
Plotted	21	100%	Spiked
Estimated Values	21	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	21	.
False Negatives	0	0%	0 out of 21
Not Spiked	53	.
False Positives	0	0%	0 out of 53

BQS ORGANIC BLIND SAMPLES

4-NONYLPHENOL MONOETHOXYLATE,

Schedule: 4433 Testid: 61704GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 08/24/12

Open Data Set

Statistics for the Plotted Points

4-NONYLPHENOL MONOETHOXYLATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	1	178%	.	178%	0%
>= Reporting Level	15	147%	25%	146%	20%
Total	16	149%	26%	147%	19%

Miscellaneous Statistics for the Samples

4-NONYLPHENOL MONOETHOXYLATE

Characteristic	N	%	% Basis
Plotted	16	94%	Spiked
Estimated Values	16	94%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	17	.
False Negatives	1	6%	1 out of 17
Not Spiked	57	.
False Positives	6	11%	6 out of 57

BQS ORGANIC BLIND SAMPLES

TRIS(DICHLORISOPROPYL)PHOSPHATE,

Schedule: 4433 Testid: 61707GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

TRIS(DICHLORISOPROPYL)PHOSPHATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	97%	5%	97%	5%
>= Reporting Level	35	100%	20%	101%	21%
Total	37	99%	20%	101%	15%

Miscellaneous Statistics for the Samples

TRIS(DICHLORISOPROPYL)PHOSPHATE

Characteristic	N	%	% Basis
Plotted	37	100%	Spiked
Estimated Values	6	16%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	37	.
False Negatives	0	0%	0 out of 37
Not Spiked	37	.
False Positives	1	3%	1 out of 37

BQS ORGANIC BLIND SAMPLES

TRICLOSAN,

Schedule: 4433 Testid: 61708GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

TRICLOSAN

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	37	96%	19%	97%	18%
Total	37	96%	19%	97%	18%

Miscellaneous Statistics for the Samples

TRICLOSAN

Characteristic	N	%	% Basis
Plotted	37	100%	Spiked
Estimated Values	3	8%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	37	.
False Negatives	0	0%	0 out of 37
Not Spiked	37	.
False Positives	1	3%	1 out of 37

BQS ORGANIC BLIND SAMPLES

5-METHYL-1H-BENZOTRIAZOLE,

Schedule: 4433 Testid: 61944GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

5-METHYL-1H-BENZOTRIAZOLE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	59%	22%	57%	18%
Total	34	59%	22%	57%	18%

Miscellaneous Statistics for the Samples

5-METHYL-1H-BENZOTRIAZOLE

Characteristic	N	%	% Basis
Plotted	34	97%	Spiked
Estimated Values	34	97%	Spiked
Deleted Values	4	5%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	1	3%	1 out of 35
Not Spiked	39	.
False Positives	1	3%	1 out of 35

BQS ORGANIC BLIND SAMPLES

COTININE,

Schedule: 4433 Testid: 61945GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

COTININE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	25%	16%	26%	14%
>= Reporting Level	29	43%	15%	46%	14%
Total	33	40%	16%	43%	16%

Miscellaneous Statistics for the Samples

COTININE

Characteristic	N	%	% Basis
Plotted	33	97%	Spiked
Estimated Values	33	97%	Spiked
Deleted Values	5	7%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	1	3%	1 out of 34
Not Spiked	40	.
False Positives	1	3%	1 out of 35

BQS ORGANIC BLIND SAMPLES

N,N-DIETHYL-META-TOLUAMIDE (DEET),

Schedule: 4433 Testid: 61947GCM99

Measured in MICROGRAMS PER LITER

12/02/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

N,N-DIETHYL-META-TOLUAMIDE (DEET)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	83%	16%	83%	19%
Total	36	83%	16%	83%	19%

Miscellaneous Statistics for the Samples

N,N-DIETHYL-META-TOLUAMIDE (DEET)

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	6	17%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	2	5%	2 out of 38

BQS ORGANIC BLIND SAMPLES

BETA-STIGMASTANOL,

Schedule: 4433 Testid: 61948GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

BETA-STIGMASTANOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	6	35%	14%	38%	17%
>= Reporting Level	28	52%	20%	54%	19%
Total	34	49%	20%	50%	19%

Miscellaneous Statistics for the Samples

BETA-STIGMASTANOL

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	34	100%	Spiked
Deleted Values	3	4%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	0	0%	0 out of 34
Not Spiked	39	.
False Positives	0	0%	0 out of 37

Miscellaneous Statistics for the Samples

4-TERT-OCTYLPHENOL MONOETHOXYLATES, TOTAL (OPEO1)

Characteristic	N	%	% Basis
Plotted	0	.	Spiked
Estimated Values	0	.	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	.	Spiked
Spiked	0	.
False Negatives	0	.	0 out of 0
Not Spiked	74	.
False Positives	22	30%	22 out of 74

BQS ORGANIC BLIND SAMPLES

4-TERT-OCTYLPHENOL DIETHOXYLATES, TOTAL (OPEO2),

Schedule: 4433 Testid: 62486GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/18/12

Open Data Set

Statistics for the Plotted Points

4-TERT-OCTYLPHENOL DIETHOXYLATES, TOTAL (OPEO2)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	16	29%	11%	28%	10%
Total	16	29%	11%	28%	10%

Miscellaneous Statistics for the Samples

4-TERT-OCTYLPHENOL DIETHOXYLATES, TOTAL (OPEO2)

Characteristic	N	%	% Basis
Plotted	16	94%	Spiked
Estimated Values	16	94%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	17	.
False Negatives	1	6%	1 out of 17
Not Spiked	57	.
False Positives	4	7%	4 out of 57

BQS ORGANIC BLIND SAMPLES

2,6-DIMETHYLNAPHTHALENE,

Schedule: 4433 Testid: 62805GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

2,6-DIMETHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	71%	4%	72%	6%
>= Reporting Level	35	82%	13%	83%	10%
Total	38	81%	12%	82%	10%

Miscellaneous Statistics for the Samples

2,6-DIMETHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	10	26%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

3-BETA-COPROSTANOL,

Schedule: 4433 Testid: 62806GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

3-BETA-COPROSTANOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	52%	18%	52%	16%
Total	34	52%	18%	52%	16%

Miscellaneous Statistics for the Samples

3-BETA-COPROSTANOL

Characteristic	N	%	% Basis
Plotted	34	97%	Spiked
Estimated Values	34	97%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	1	3%	1 out of 35
Not Spiked	39	.
False Positives	0	0%	0 out of 39

BQS ORGANIC BLIND SAMPLES

3-METHYL-1(H)-INDOLE (SKATOLE),

Schedule: 4433 Testid: 62807GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

3-METHYL-1(H)-INDOLE (SKATOLE)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	38	78%	18%	81%	14%
Total	38	78%	18%	81%	14%

Miscellaneous Statistics for the Samples

3-METHYL-1(H)-INDOLE (SKATOLE)

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	6	16%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

4-CUMYLPHENOL,

Schedule: 4433 Testid: 62808GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

4-CUMYLPHENOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	38	80%	19%	81%	17%
Total	38	80%	19%	81%	17%

Miscellaneous Statistics for the Samples

4-CUMYLPHENOL

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	8	21%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

4-N-OCTYLPHENOL,

Schedule: 4433 Testid: 62809GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

4-N-OCTYLPHENOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	76%	10%	76%	11%
>= Reporting Level	36	64%	17%	64%	9%
Total	38	64%	17%	64%	9%

Miscellaneous Statistics for the Samples

4-N-OCTYLPHENOL

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	38	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	1	3%	1 out of 36

BQS ORGANIC BLIND SAMPLES

4-TERT-OCTYLPHENOL,

Schedule: 4433 Testid: 62810GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

4-TERT-OCTYLPHENOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	99%	21%	96%	26%
>= Reporting Level	31	81%	11%	83%	11%
Total	35	83%	14%	84%	14%

Miscellaneous Statistics for the Samples

4-TERT-OCTYLPHENOL

Characteristic	N	%	% Basis
Plotted	35	100%	Spiked
Estimated Values	35	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	0	0%	0 out of 35
Not Spiked	39	.
False Positives	0	0%	0 out of 39

BQS ORGANIC BLIND SAMPLES

ACETOPHENONE,

Schedule: 4433 Testid: 62811GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

ACETOPHENONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	35	91%	12%	92%	12%
Total	35	91%	12%	92%	12%

Miscellaneous Statistics for the Samples

ACETOPHENONE

Characteristic	N	%	% Basis
Plotted	35	100%	Spiked
Estimated Values	3	9%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	0	0%	0 out of 35
Not Spiked	39	.
False Positives	0	0%	0 out of 39

BQS ORGANIC BLIND SAMPLES

ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN),

Schedule: 4433 Testid: 62812GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	23	84%	15%	84%	11%
Total	23	84%	15%	84%	11%

Miscellaneous Statistics for the Samples

ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN)

Characteristic	N	%	% Basis
Plotted	23	100%	Spiked
Estimated Values	1	4%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	23	.
False Negatives	0	0%	0 out of 23
Not Spiked	51	.
False Positives	0	0%	0 out of 51

BQS ORGANIC BLIND SAMPLES

ANTHRAQUINONE,

Schedule: 4433 Testid: 62813GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ANTHRAQUINONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	38	80%	16%	81%	13%
Total	38	80%	16%	81%	13%

Miscellaneous Statistics for the Samples

ANTHRAQUINONE

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	38	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

BENZOPHENONE,

Schedule: 4433 Testid: 62814GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

BENZOPHENONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	82%	5%	85%	7%
>= Reporting Level	35	88%	13%	86%	8%
Total	38	87%	13%	86%	7%

Miscellaneous Statistics for the Samples

BENZOPHENONE

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	9	24%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	1	3%	1 out of 36

BQS ORGANIC BLIND SAMPLES

BETA-SITOSTEROL,

Schedule: 4433 Testid: 62815GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

BETA-SITOSTEROL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	54%	22%	55%	22%
Total	34	54%	22%	55%	22%

Miscellaneous Statistics for the Samples

BETA-SITOSTEROL

Characteristic	N	%	% Basis
Plotted	34	97%	Spiked
Estimated Values	34	97%	Spiked
Deleted Values	1	1%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	1	3%	1 out of 35
Not Spiked	39	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

BISPHENOL A,

Schedule: 4433 Testid: 62816GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

BISPHENOL A

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	81%	10%	81%	10%
>= Reporting Level	32	86%	22%	85%	20%
Total	34	85%	22%	85%	20%

Miscellaneous Statistics for the Samples

BISPHENOL A

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	8	24%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	0	0%	0 out of 34
Not Spiked	40	.
False Positives	1	3%	1 out of 40

BQS ORGANIC BLIND SAMPLES

CAMPHOR,

Schedule: 4433 Testid: 62817GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

CAMPHOR

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	75%	3%	77%	4%
>= Reporting Level	35	86%	13%	86%	12%
Total	38	85%	12%	85%	12%

Miscellaneous Statistics for the Samples

CAMPHOR

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	8	21%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

CHOLESTEROL,

Schedule: 4433 Testid: 62818GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

CHOLESTEROL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	53%	18%	53%	18%
Total	34	53%	18%	53%	18%

Miscellaneous Statistics for the Samples

CHOLESTEROL

Characteristic	N	%	% Basis
Plotted	34	97%	Spiked
Estimated Values	34	97%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	35	.
False Negatives	1	3%	1 out of 35
Not Spiked	39	.
False Positives	0	0%	0 out of 39

BQS ORGANIC BLIND SAMPLES

D-LIMONENE,

Schedule: 4433 Testid: 62819GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

D-LIMONENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	38	77%	10%	79%	8%
Total	38	77%	10%	79%	8%

Miscellaneous Statistics for the Samples

D-LIMONENE

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	38	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB),

Schedule: 4433 Testid: 62823GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	13	84%	15%	80%	19%
Total	13	84%	15%	80%	19%

Miscellaneous Statistics for the Samples

HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)

Characteristic	N	%	% Basis
Plotted	13	100%	Spiked
Estimated Values	2	15%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	13	.
False Negatives	0	0%	0 out of 13
Not Spiked	61	.
False Positives	2	3%	2 out of 61

BQS ORGANIC BLIND SAMPLES

INDOLE,

Schedule: 4433 Testid: 62824GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

INDOLE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	78%	4%	80%	3%
>= Reporting Level	34	75%	23%	85%	18%
Total	38	75%	21%	80%	14%

Miscellaneous Statistics for the Samples

INDOLE

Characteristic	N	%	% Basis
Plotted	38	100%	Spiked
Estimated Values	11	29%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	38	.
False Negatives	0	0%	0 out of 38
Not Spiked	36	.
False Positives	0	0%	0 out of 36

BQS ORGANIC BLIND SAMPLES

ISOBORNEOL,

Schedule: 4433 Testid: 62825GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ISOBORNEOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	74%	5%	74%	6%
>= Reporting Level	33	85%	20%	82%	16%
Total	35	84%	19%	82%	19%

Miscellaneous Statistics for the Samples

ISOBORNEOL

Characteristic	N	%	% Basis
Plotted	35	97%	Spiked
Estimated Values	8	22%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	3%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

ISOQUINOLINE,

Schedule: 4433 Testid: 62826GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ISOQUINOLINE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	74%	20%	76%	17%
Total	34	74%	20%	76%	17%

Miscellaneous Statistics for the Samples

ISOQUINOLINE

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	5	15%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	0	0%	0 out of 34
Not Spiked	40	.
False Positives	1	3%	1 out of 40

BQS ORGANIC BLIND SAMPLES

MENTHOL,

Schedule: 4433 Testid: 62827GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

MENTHOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	9	104%	43%	100%	21%
>= Reporting Level	28	92%	18%	90%	15%
Total	37	95%	26%	92%	16%

Miscellaneous Statistics for the Samples

MENTHOL

Characteristic	N	%	% Basis
Plotted	37	100%	Spiked
Estimated Values	6	16%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	37	.
False Negatives	0	0%	0 out of 37
Not Spiked	37	.
False Positives	0	0%	0 out of 37

BQS ORGANIC BLIND SAMPLES

METHYL SALICYLATE,

Schedule: 4433 Testid: 62828GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

METHYL SALICYLATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	81%	14%	83%	15%
Total	36	81%	14%	83%	15%

Miscellaneous Statistics for the Samples

METHYL SALICYLATE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	2	6%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

PARA-NONYLPHENOL (TOTAL) (BRANCHED),

Schedule: 4433 Testid: 62829GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

PARA-NONYLPHENOL (TOTAL) (BRANCHED)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	27	72%	12%	70%	10%
Total	27	72%	12%	70%	10%

Miscellaneous Statistics for the Samples

PARA-NONYLPHENOL (TOTAL) (BRANCHED)

Characteristic	N	%	% Basis
Plotted	27	100%	Spiked
Estimated Values	27	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	27	.
False Negatives	0	0%	0 out of 27
Not Spiked	47	.
False Positives	0	0%	0 out of 47

BQS ORGANIC BLIND SAMPLES

TRIS(2-BUTOXYETHYL)PHOSPHATE,

Schedule: 4433 Testid: 62830GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

TRIS(2-BUTOXYETHYL)PHOSPHATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	8	117%	40%	108%	32%
>= Reporting Level	28	97%	30%	102%	21%
Total	36	101%	33%	102%	20%

Miscellaneous Statistics for the Samples

TRIS(2-BUTOXYETHYL)PHOSPHATE

Characteristic	N	%	% Basis
Plotted	36	97%	Spiked
Estimated Values	36	97%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	3%	Spiked
Spiked	37	.
False Negatives	0	0%	0 out of 37
Not Spiked	37	.
False Positives	0	0%	0 out of 37

BQS ORGANIC BLIND SAMPLES

TRIS(2-CHLOROETHYL)PHOSPHATE,

Schedule: 4433 Testid: 62831GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

TRIS(2-CHLOROETHYL)PHOSPHATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	84%	22%	72%	29%
>= Reporting Level	33	84%	20%	86%	12%
Total	36	84%	20%	85%	15%

Miscellaneous Statistics for the Samples

TRIS(2-CHLOROETHYL)PHOSPHATE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	5	14%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

TRIBUTYL PHOSPHATE,

Schedule: 4433 Testid: 62832GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

TRIBUTYL PHOSPHATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	81%	23%	82%	18%
Total	36	81%	23%	82%	18%

Miscellaneous Statistics for the Samples

TRIBUTYL PHOSPHATE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	11	31%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

TRIETHYL CITRATE (ETHYL CITRATE),

Schedule: 4433 Testid: 62833GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

TRIETHYL CITRATE (ETHYL CITRATE)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	35	74%	29%	77%	26%
Total	35	74%	29%	77%	26%

Miscellaneous Statistics for the Samples

TRIETHYL CITRATE (ETHYL CITRATE)

Characteristic	N	%	% Basis
Plotted	35	97%	Spiked
Estimated Values	8	22%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	1	3%	1 out of 36
Not Spiked	38	.
False Positives	2	5%	2 out of 38

BQS ORGANIC BLIND SAMPLES

TRIPHENYL PHOSPHATE,

Schedule: 4433 Testid: 62834GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

TRIPHENYL PHOSPHATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	79%	16%	70%	20%
>= Reporting Level	33	87%	18%	90%	13%
Total	36	87%	18%	90%	13%

Miscellaneous Statistics for the Samples

TRIPHENYL PHOSPHATE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	10	28%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	3	8%	3 out of 38

BQS ORGANIC BLIND SAMPLES

3,4-DICHLOROPHENYL ISOCYANATE,

Schedule: 4433 Testid: 63145GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/19/12

Open Data Set

Statistics for the Plotted Points

3,4-DICHLOROPHENYL ISOCYANATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	17%	8%	17%	9%
>= Reporting Level	29	19%	13%	15%	10%
Total	31	19%	12%	15%	10%

Miscellaneous Statistics for the Samples

3,4-DICHLOROPHENYL ISOCYANATE

Characteristic	N	%	% Basis
Plotted	31	97%	Spiked
Estimated Values	31	97%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	1	3%	Spiked
Spiked	32	.
False Negatives	0	0%	0 out of 32
Not Spiked	42	.
False Positives	1	2%	1 out of 42

BQS ORGANIC BLIND SAMPLES

2,2',4,4'-TETRABROMODIPHENYLETHER (PBDE 47),

Schedule: 4433 Testid: 63147GCM99

Measured in MICROGRAMS PER LITER

12/18/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

2,2',4,4'-TETRABROMODIPHENYLETHER (PBDE 47)

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	60%	7%	60%	9%
>= Reporting Level	8	84%	29%	77%	32%
Total	12	76%	26%	72%	28%

Miscellaneous Statistics for the Samples

2,2',4,4'-TETRABROMODIPHENYLETHER (PBDE 47)

Characteristic	N	%	% Basis
Plotted	12	100%	Spiked
Estimated Values	12	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 12
Not Spiked	62	.
False Positives	0	0%	0 out of 62

BQS ORGANIC BLIND SAMPLES

P-CRESOL,

Schedule: 4433 Testid: 77146GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

P-CRESOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	80%	17%	84%	18%
Total	36	80%	17%	84%	18%

Miscellaneous Statistics for the Samples

P-CRESOL

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	4	11%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

ISOPROPYLBENZENE,

Schedule: 4433 Testid: 77223GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

ISOPROPYLBENZENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	82%	10%	82%	10%
Total	36	82%	10%	82%	10%

Miscellaneous Statistics for the Samples

ISOPROPYLBENZENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	36	100%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	0	0%	0 out of 38

BQS ORGANIC BLIND SAMPLES

CARBAZOLE,

Schedule: 4433 Testid: 77571GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

CARBAZOLE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	2	81%	9%	81%	9%
>= Reporting Level	34	81%	17%	82%	16%
Total	36	81%	16%	82%	14%

Miscellaneous Statistics for the Samples

CARBAZOLE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	4	11%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	37	.
False Positives	2	5%	2 out of 37

BQS ORGANIC BLIND SAMPLES

CAFFEINE,

Schedule: 4433 Testid: 81436GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

CAFFEINE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	36	78%	14%	80%	15%
Total	36	78%	14%	80%	15%

Miscellaneous Statistics for the Samples

CAFFEINE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	1	3%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	1	3%	1 out of 38

BQS ORGANIC BLIND SAMPLES

1-METHYLNAPHTHALENE,

Schedule: 4433 Testid: 81696GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

1-METHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	73%	6%	74%	8%
>= Reporting Level	33	86%	14%	89%	16%
Total	36	85%	14%	85%	16%

Miscellaneous Statistics for the Samples

1-METHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	36	100%	Spiked
Estimated Values	8	22%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	36	.
False Negatives	0	0%	0 out of 36
Not Spiked	38	.
False Positives	5	13%	5 out of 38

BQS ORGANIC BLIND SAMPLES

METOLACHLOR,

Schedule: 4433 Testid: 82612GCM99

Measured in MICROGRAMS PER LITER

12/04/09 TO 12/20/12

Open Data Set

Statistics for the Plotted Points

METOLACHLOR

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	34	78%	11%	77%	9%
Total	34	78%	11%	77%	9%

Miscellaneous Statistics for the Samples

METOLACHLOR

Characteristic	N	%	% Basis
Plotted	34	100%	Spiked
Estimated Values	4	12%	Spiked
Deleted Values	0	0%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	34	.
False Negatives	0	0%	0 out of 34
Not Spiked	40	.
False Positives	2	5%	2 out of 40