SAS Output

False Positives Listing for TERBUTHYLAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091550184	Crescent 08HH019: 40 µl	0.006	07/23/09	0.005
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.052

False Negatives Listing for TERBUTHYLAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.04808

False Positives Listing for HEXAZINONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.008	07/20/11	0.016

False Negatives Listing for HEXAZINONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.008	07/20/11	0.02

False Positives Listing for SIMAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080150156	Crescent 07GG004: 50 µl	0.006	02/28/08	0.006
20080370105	Restek A053526: 50 µl	0.006	03/10/08	0.007
20080740016	Crescent 07GG004: 50 µl	0.006	04/09/08	0.006
20081010093	Restek A053526: 50 µl	0.006	04/28/08	0.009
20081080092	Crescent 07GG004: 50 µl	0.006	05/07/08	0.007
20081290006	Restek A053526: 50 µl	0.006	05/14/08	0.007
20081410056	Restek A053526: 50 µl	0.006	06/23/08	0.007
20081560010	Crescent 07GG004: 50 µl	0.006	07/08/08	0.006
20081780161	Restek A053526: 50 µl	0.006	08/19/08	0.006
20082040248	Crescent 07GG004: 50 µl	0.006	09/16/08	0.006
20082260232	Restek A053526: 50 µl	0.01	10/09/08	0.007
20082890058	ChemService 406-99B: 25 µl	0.01	12/11/08	0.006
20090210033	ChemService 406-99B: 40 µl	0.01	02/18/09	0.009
20090580003	ERA 0804-08-02PEST: 25 µl	0.01	03/12/09	0.006
20090920067	ChemService 406-99B: 40 µl	0.01	04/30/09	0.009
20091320001	ERA 0804-08-02PEST: 25 µl	0.01	06/18/09	0.005
20091340062	Supelco LB60731: 40 µl	0.01	07/10/09	0.214
20091620170	ChemService 406-99B: 25 µl	0.01	08/12/09	0.009
20091880135	ERA 0804-08-02PEST: 25 µl	0.01	09/16/09	0.006
20092110204	ERA 0804-08-02PEST: 40 µl	0.006	11/11/09	0.006
20092180180	ChemService 406-99B: 25 µl	0.006	12/01/09	0.008
20092460258	ERA 0804-08-02PEST: 25 µl	0.006	01/17/10	0.009
20101480005	Restek A069639: 100 µl	0.006	07/29/10	0.005
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.087

False Negatives Listing for SIMAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.01	07/10/09	0.1668161
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.08828

False Positives Listing for PROMETRYN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20082040248	Crescent 07GG004: 50 µl	0.0059	09/16/08	0.007
20091340062	Supelco LB60731: 40 µl	0.0059	07/10/09	0.070
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.046

False Negatives Listing for PROMETRYN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.0059	07/10/09	0.0796733
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.03968

False Positives Listing for PROMETON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20083110006	Protocol D1080908018: 40 µl	0.012	01/10/09	0.016
20090160003	Protocol D1080908018: 25 µl	0.012	02/11/09	0.014
20090860072	Protocol D1080908018: 25 µl	0.012	04/28/09	0.013
20091340062	Supelco LB60731: 40 µl	0.012	07/10/09	0.013
20091830169	Protocol D1080908018: 40 µl	0.012	09/15/09	0.015
20112310030	Restek A075606: 40 µl	0.012	09/13/11	0.059

False Negatives Listing for PROMETON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.012	09/13/11	0.0808

False Positives Listing for DEETHYLATRAZINE (DESETHYL ATRAZINE) (2-CHLORO-4-ISOPROPYLAMINO-6-S-TRIAZINE) CIAT

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.014	07/10/09	0.078
20112310030	Restek A075606: 40 µl	0.006	09/13/11	0.044

False Negatives Listing for DEETHYLATRAZINE (DESETHYL ATRAZINE) (2-CHLORO-4-ISOPROPYLAMINO-6-S-TRIAZINE) CIAT

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.014	07/10/09	0.0911982
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.006	09/13/11	0.05136

False Positives Listing for CYANAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.04	07/10/09	0.240
20111890005	Accu 210061341: 40 µl	0.022	07/20/11	0.069
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.022	09/13/11	0.068

False Negatives Listing for CYANAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.04	07/10/09	0.2179277
20103140135	Supelco LB77168: 40 µl	0.022	01/18/11	0.0729956
20111890004	Supelco LB77168: 40 µl	0.022	07/20/11	0.0732
20112310030	Restek A075606: 40 µl	0.022	09/13/11	0.0732

False Positives Listing for FONOFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.0048	07/20/11	0.018

False Negatives Listing for FONOFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090580003	ERA 0804-08-02PEST: 25 µl	0.01	03/12/09	0.1250664
20092110204	ERA 0804-08-02PEST: 40 µl	0.0044	11/11/09	0.1888911
20092460258	ERA 0804-08-02PEST: 25 µl	0.0044	01/17/10	0.118211
20092530080	ERA 0804-08-02PEST: 40 µl	0.0044	01/21/10	0.1820994
20111890005	Accu 210061341: 40 µl	0.0048	07/20/11	0.01996

False Positives Listing for ALPHA-ENDOSULFAN (ENDOSULFAN I)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.006	07/10/09	0.054
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.020

False Negatives Listing for ALPHA-ENDOSULFAN (ENDOSULFAN I)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.006	07/10/09	0.0522856
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.02

False Positives Listing for DICROTOPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111680035	Accu 210061341: 40 µl	0.08	07/02/11	0.004
20111890005	Accu 210061341: 40 µl	0.08	07/20/11	0.057
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.08	09/13/11	0.050

False Negatives Listing for DICROTOPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.08	07/20/11	0.1328
20112310030	Restek A075606: 40 µl	0.08	09/13/11	0.13288

False Positives Listing for DICHLOROVOS (DICHLORVOS)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.02	07/10/09	0.019
20112310030	Restek A075606: 40 µl	0.04	09/13/11	0.027

False Negatives Listing for DICHLOROVOS (DICHLORVOS)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.02	07/10/09	0.1461764
20102390088	Ultra CF-3558: 20 µl	0.04	12/01/10	0.0525306
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.04	09/13/11	0.06304

False Positives Listing for CHLORPYRIFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.01	07/10/09	0.010
20111890004	Supelco LB77168: 40 µl	0.0036	07/20/11	0.042

False Negatives Listing for CHLORPYRIFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.0036	07/20/11	0.0482

False Positives Listing for DIELDRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.008	07/20/11	0.047

False Negatives Listing for DIELDRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.008	07/20/11	0.04432

False Positives Listing for METOLACHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091210002	Crescent 08HH019: 25 µl	0.014	06/03/09	0.004
20112310030	Restek A075606: 40 µl	0.02	09/13/11	0.081

False Negatives Listing for METOLACHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.02	09/13/11	0.0984

False Positives Listing for MALATHION

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.02	07/10/09	0.081
20112310030	Restek A075606: 40 µl	0.016	09/13/11	0.053

False Negatives Listing for MALATHION

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.02	07/10/09	0.0666464
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.016	09/13/11	0.06888

False Positives Listing for DIAZINON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.005	07/10/09	0.149
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.052

False Negatives Listing for DIAZINON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.005	07/10/09	0.1444079
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.04416

False Positives Listing for ATRAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080240002	ERA 0709-07-01GC: 50 µl	0.007	03/01/08	0.007
20091340062	Supelco LB60731: 40 µl	0.007	07/10/09	0.008
20111890004	Supelco LB77168: 40 µl	0.008	07/20/11	0.156

False Negatives Listing for ATRAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.008	07/20/11	0.1484

False Positives Listing for ALACHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.008	07/10/09	0.115
20111890004	Supelco LB77168: 40 µl	0.008	07/20/11	0.049

False Negatives Listing for ALACHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.008	07/10/09	0.1045713
20111890005	Accu 210061341: 40 µl	0.008	07/20/11	0.0442

False Positives Listing for ACETOCHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.01	07/10/09	0.176
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.083

False Negatives Listing for ACETOCHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.01	07/10/09	0.1767752
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.0952

False Positives Listing for 1-NAPHTHOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.036	07/20/11	0.080
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.036	09/13/11	0.079

False Negatives Listing for 1-NAPHTHOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.036	07/20/11	0.05444
20112310030	Restek A075606: 40 µl	0.036	09/13/11	0.0544

False Positives Listing for CYFLUTHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.016	07/10/09	0.115
20112310030	Restek A075606: 40 µl	0.016	09/13/11	0.020

False Negatives Listing for CYFLUTHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.016	07/10/09	0.1608832
20102880001	Spex Organics T1100628017: 80 µl	0.016	01/11/11	0.0475389
20103350003	Spex Organics T1100628017: 40 µl	0.016	01/21/11	0.0239497
20110280004	Spex Organics T1100628017: 40 µl	0.016	02/19/11	0.0241085
20110690078	Spex Organics T1100628017: 40 µl	0.016	03/23/11	0.023511
20111260154	Spex Organics T1100628017: 40 µl	0.016	05/14/11	0.0242645
20111750006	Spex Organics T1100628017: 80 µl	0.016	07/07/11	0.048
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.016	09/13/11	0.04944
20112380055	Spex Organics T1100628017: 40 µl	0.016	09/19/11	0.024
20112520209	Spex Organics T1100628017: 80 µl	0.016	09/29/11	0.048
20113080001	Spex Organics T1100628017: 40 µl	0.016	11/17/11	0.024
20113490056	Spex Organics T1100628017: 80 µl	0.016	12/21/11	0.048

False Positives Listing for CYPERMETHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.02	07/10/09	0.103
20112310030	Restek A075606: 40 µl	0.02	09/13/11	0.026

False Negatives Listing for CYPERMETHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.02	07/10/09	0.1299706
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.02	09/13/11	0.06144

False Positives Listing for ENDOSULFAN SULFATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.016	07/20/11	0.062
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.016	09/13/11	0.058

False Negatives Listing for ENDOSULFAN SULFATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.016	07/20/11	0.0692
20112310030	Restek A075606: 40 µl	0.016	09/13/11	0.0692

False Positives Listing for FENAMIPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20101410006	Crescent 08Ll064: 40 µl	0.03	07/21/10	0.004
20111890005	Accu 210061341: 40 µl	0.03	07/20/11	0.041
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.03	09/13/11	0.037

False Negatives Listing for FENAMIPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.03	07/20/11	0.0396
20112310030	Restek A075606: 40 µl	0.03	09/13/11	0.0396

False Positives Listing for IPRODIONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112310030	Restek A075606: 40 µl	0.014	09/13/11	0.036

False Negatives Listing for IPRODIONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20081010091	Abs 071007GC: 50 µl	0.01	04/28/08	0.2026287
20082000008	Abs 071007GC: 50 µl	0.01	09/11/08	0.202226
20093520041	NSI 090109-01Pest: 40 µl	0.014	02/16/10	0.1325389
20100280077	NSI 090109-01Pest: 20 µl	0.014	03/25/10	0.0629593
20100420055	Supelco LB69639: 20 µl	0.014	04/22/10	0.0626354
20101270038	Supelco LB69639: 40 µl	0.014	07/07/10	0.1233275
20101550006	NSI 090109-01Pest: 20 µl	0.014	08/03/10	0.0655772
20101950137	Supelco LB69639: 40 µl	0.014	09/23/10	0.125816
20102250096	NSI 090109-01Pest: 100 µl	0.014	10/27/10	0.3235684
20111590005	NWQL PSP2SP117A: 75 µl	0.014	06/22/11	0.074096
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.014	09/13/11	0.05864

False Positives Listing for ISOFENPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.006	07/10/09	0.162
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.017

False Negatives Listing for ISOFENPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.006	07/10/09	0.1394283
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.01196

False Positives Listing for CYHALOTHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.01	07/10/09	0.052
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.008

False Negatives Listing for CYHALOTHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.01	07/10/09	0.0896325
20110910084	ERA 0818-10-05 LS 2033#2: 40 µl	0.01	04/13/11	0.0200402
20111960039	ERA 0818-10-05 LS 2033#2: 40 µl	0.01	07/28/11	0.01992
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.03984

False Positives Listing for METALAXYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.014	07/20/11	0.037

False Negatives Listing for METALAXYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.014	07/20/11	0.02812

False Positives Listing for METHIDATHION (SUPRACIDE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.006	07/10/09	0.138
20111890004	Supelco LB77168: 40 µl	0.012	07/20/11	0.044

False Negatives Listing for METHIDATHION (SUPRACIDE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.006	07/10/09	0.1817548
20111890005	Accu 210061341: 40 µl	0.012	07/20/11	0.04448

False Positives Listing for MYCLOBUTANIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.046

False Negatives Listing for MYCLOBUTANIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.07784

False Positives Listing for OXYFLUORFEN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.006	07/10/09	0.019
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.023

False Negatives Listing for OXYFLUORFEN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.006	07/10/09	0.0199183
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.02816

False Positives Listing for PHOSMET (IMIDAN)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.14	07/20/11	0.185
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.14	09/13/11	0.210

False Negatives Listing for PHOSMET (IMIDAN)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20080150156	Crescent 07GG004: 50 µl	0.0079	02/28/08	0.0406793
20080740016	Crescent 07GG004: 50 µl	0.0079	04/09/08	0.0404081
20081080092	Crescent 07GG004: 50 µl	0.0079	05/07/08	0.04004
20081560010	Crescent 07GG004: 50 µl	0.0079	07/08/08	0.040028
20082040248	Crescent 07GG004: 50 µl	0.0079	09/16/08	0.0392542
20101760006	Accu 209081187: 40 µl	0.034	09/09/10	0.4936544
20102500051	Accu 209081187: 40 µl	0.14	12/14/10	0.4908098
20111890004	Supelco LB77168: 40 µl	0.14	07/20/11	0.36448
20112310030	Restek A075606: 40 µl	0.14	09/13/11	0.3644

False Positives Listing for TEFLUTHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.01	07/10/09	0.139
20110620082	Abs 080610: 80 µl	0.01	03/16/11	0.006
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.020

False Negatives Listing for TEFLUTHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.0376

False Positives Listing for TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080580078	Protocol R1070723008: 50 µl	0.035	04/03/08	0.042
20080940064	Protocol R1070723008: 50 µl	0.035	04/18/08	0.027
20081340105	Protocol R1070723008: 50 µl	0.035	05/28/08	0.037
20081410056	Restek A053526: 50 µl	0.035	06/23/08	0.015
20081840006	Protocol R1070723008: 50 µl	0.035	08/20/08	0.049
20082350001	Protocol R1070723008: 50 µl	0.035	10/24/08	0.036
20111890005	Accu 210061341: 40 µl	0.018	07/20/11	0.045
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.018	09/13/11	0.039
20112520209	Spex Organics T1100628017: 80 µl	0.018	09/29/11	0.006
20112870073	ERA 0818-10-05 LS 2033#2: 40 µl	0.018	10/25/11	0.009

False Negatives Listing for TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.018	07/20/11	0.0644
20112310030	Restek A075606: 40 µl	0.018	09/13/11	0.06428

False Positives Listing for 2-CHLORO-2,6-DIETHYLACETANILIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.071

False Negatives Listing for 2-CHLORO-2,6-DIETHYLACETANILIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.0848

False Negatives Listing for 2-ETHYL-6-METHYLANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20092110204	ERA 0804-08-02PEST: 40 µl	0.0098	11/11/09	0.0633648

False Positives Listing for 3,4-DICHLOROANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.004	07/10/09	0.109
20111890004	Supelco LB77168: 40 µl	0.0042	07/20/11	0.046

False Negatives Listing for 3,4-DICHLOROANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.004	07/10/09	0.1095508
20111890005	Accu 210061341: 40 µl	0.0042	07/20/11	0.04804

False Positives Listing for 3,5-DICHLOROANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080640001	Abs 071007GC: 50 µl	0.008	04/03/08	0.006
20081010091	Abs 071007GC: 50 µl	0.008	04/28/08	0.004
20111890004	Supelco LB77168: 40 µl	0.004	07/20/11	0.021

False Negatives Listing for 3,5-DICHLOROANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.004	07/20/11	0.02016

False Positives Listing for 4-CHLORO-2-METHYLPHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.005	07/10/09	0.023
20111890004	Supelco LB77168: 40 µl	0.0046	07/20/11	0.014

False Negatives Listing for 4-CHLORO-2-METHYLPHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.005	07/10/09	0.0273877
20111890005	Accu 210061341: 40 µl	0.0046	07/20/11	0.01988

False Positives Listing for AZINPHOS-METHYL-OXON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20103430087	Restek A075606: 80 µl	0.042	01/28/11	0.406

False Negatives Listing for AZINPHOS-METHYL-OXON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111590005	NWQL PSP2SP117A: 75 µl	0.042	06/22/11	0.074096

False Positives Listing for CHLORPYRIFOS, OXYGEN ANALOG

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.06	07/20/11	0.026
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.06	09/13/11	0.015
20113490056	Spex Organics T1100628017: 80 µl	0.08	12/21/11	0.004

False Negatives Listing for CHLORPYRIFOS, OXYGEN ANALOG

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20080640001	Abs 071007GC: 50 µl	0.0562	04/03/08	0.1330917
20082000008	Abs 071007GC: 50 µl	0.0562	09/11/08	0.1276955
20082410005	Abs 071007GC: 50 µl	0.05	11/05/08	0.128835
20090780142	NWQL PSP2SP115C: 75 µl	0.05	04/17/09	0.0751654
20091130130	NWQL PSP2SP115C: 75 µl	0.05	05/27/09	0.0758265
20091410001	Abs 080408Pest: 25 µl	0.05	06/30/09	0.1017325
20091490007	NWQL PSP2SP115C: 75 µl	0.05	07/13/09	0.0748354
20091770121	NWQL PSP2SP115C: 75 µl	0.05	09/03/09	0.0744195
20092040202	Abs 080408Pest: 40 µl	0.05	10/27/09	0.1619888
20092330002	Accu B8090098: 25 µl	0.05	12/30/09	0.1012721
20092400050	Abs 080408Pest: 25 µl	0.05	01/10/10	0.1012633
20093240038	Accu 209081187: 100 µl	0.05	02/23/10	0.3646238
20100210100	Accu 209081187: 20 µl	0.05	03/24/10	0.0735309
20100570086	Accu 209081187: 20 µl	0.05	05/07/10	0.0770729
20102160002	Crescent 08Ll064: 20 µl	0.06	10/19/10	0.0722529
20102500051	Accu 209081187: 40 µl	0.06	12/14/10	0.1494287
20103140135	Supelco LB77168: 40 µl	0.06	01/18/11	0.0626247
20110980030	NWQL PSP2SP117A: 100 µl	0.06	04/20/11	0.0994827
20111590005	NWQL PSP2SP117A: 75 µl	0.06	06/22/11	0.074096
20111810004	Supelco LB77168: 80 µl	0.06	07/14/11	0.1256
20111890004	Supelco LB77168: 40 µl	0.06	07/20/11	0.0628

False Positives Listing for DIAZINON, OXYGEN ANALOG

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20083180005	Crescent 08HH019: 40 µl	0.006	01/14/09	0.003
20102880001	Spex Organics T1100628017: 80 µl	0.01	01/11/11	0.003
20111890004	Supelco LB77168: 40 µl	0.01	07/20/11	0.053

False Negatives Listing for DIAZINON, OXYGEN ANALOG

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20082970002	Supelco LB60731: 25 µl	0.006	12/17/08	0.017975
20083260002	Supelco LB60731: 40 µl	0.006	01/17/09	0.0288205
20090640123	Supelco LB60731: 25 µl	0.006	03/16/09	0.0194851
20091340062	Supelco LB60731: 40 µl	0.006	07/10/09	0.02913
20091970075	Supelco LB60731: 25 µl	0.006	09/29/09	0.0180653
20092610019	Supelco LB60731: 25 µl	0.006	01/27/10	0.0180038
20111890005	Accu 210061341: 40 µl	0.01	07/20/11	0.04768

False Positives Listing for DISULFOTON SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.014	07/10/09	0.044
20112310030	Restek A075606: 40 µl	0.014	09/13/11	0.050

False Negatives Listing for DISULFOTON SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.014	07/10/09	0.0419325
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.014	09/13/11	0.06952

False Positives Listing for ETHION MONOXON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20090580003	ERA 0804-08-02PEST: 25 µl	0.021	03/12/09	0.015
20091320001	ERA 0804-08-02PEST: 25 µl	0.021	06/18/09	0.021
20091880135	ERA 0804-08-02PEST: 25 µl	0.021	09/16/09	0.021
20092110204	ERA 0804-08-02PEST: 40 µl	0.021	11/11/09	0.036
20092460258	ERA 0804-08-02PEST: 25 µl	0.021	01/17/10	0.024
20092530080	ERA 0804-08-02PEST: 40 µl	0.021	01/21/10	0.036

False Positives Listing for FENAMIPHOS SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.054	07/20/11	0.063
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.054	09/13/11	0.078

False Negatives Listing for FENAMIPHOS SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.054	07/20/11	0.06844
20112310030	Restek A075606: 40 µl	0.054	09/13/11	0.0684

False Positives Listing for FENAMIPHOS SULFOXIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20093100007	Ultra CF-3558: 40 µl	0.08	02/17/10	0.047
20101650033	Ultra CF-3558: 40 µl	0.08	08/10/10	0.025
20102030005	Spex Organics T1090901009: 20 µl	0.08	09/30/10	0.003
20111890005	Accu 210061341: 40 µl	0.08	07/20/11	0.034
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.08	09/13/11	0.046

False Negatives Listing for FENAMIPHOS SULFOXIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20083040064	Abs 080408Pest: 25 µl	0.08	01/08/09	0.237637
20092400050	Abs 080408Pest: 25 µl	0.08	01/10/10	0.2413776
20100570086	Accu 209081187: 20 µl	0.08	05/07/10	0.1937071
20100920048	Crescent 08Ll064: 20 µl	0.08	06/03/10	0.1872169
20111890004	Supelco LB77168: 40 µl	0.08	07/20/11	0.19808
20112310030	Restek A075606: 40 µl	0.08	09/13/11	0.19796

False Positives Listing for MALAOXON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111750006	Spex Organics T1100628017: 80 µl	0.022	07/07/11	0.004
20111890005	Accu 210061341: 40 µl	0.022	07/20/11	0.086
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.022	09/13/11	0.079

False Negatives Listing for MALAOXON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.022	07/20/11	0.0972
20112310030	Restek A075606: 40 µl	0.022	09/13/11	0.09716

False Positives Listing for PARAOXON-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.01	07/10/09	0.083
20112310030	Restek A075606: 40 µl	0.014	09/13/11	0.053

False Negatives Listing for PARAOXON-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.01	07/10/09	0.1251089
20111470065	ERA 0818-10-05 LS 2033#2: 40 µl	0.014	06/20/11	0.0317768
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.014	09/13/11	0.06288

False Negatives Listing for PHOSMET OXON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20080080065	Abs 071007GC: 50 µl	0.0511	02/23/08	0.0838045
20080640001	Abs 071007GC: 50 µl	0.0511	04/03/08	0.0859658
20081010091	Abs 071007GC: 50 µl	0.0511	04/28/08	0.0826446
20081500009	Abs 071007GC: 50 µl	0.0511	07/02/08	0.0828426
20082000008	Abs 071007GC: 50 µl	0.0511	09/11/08	0.0824804
20082410005	Abs 071007GC: 50 µl	0.0511	11/05/08	0.0832164
20091490007	NWQL PSP2SP115C: 75 µl	0.0511	07/13/09	0.0748354
20091770121	NWQL PSP2SP115C: 75 µl	0.0511	09/03/09	0.0744195
20100570086	Accu 209081187: 20 µl	0.0511	05/07/10	0.107615
20101760006	Accu 209081187: 40 µl	0.0511	09/09/10	0.2098531
20102500051	Accu 209081187: 40 µl	0.0511	12/14/10	0.2086438
20110980030	NWQL PSP2SP117A: 100 µl	0.0511	04/20/11	0.0994827
20111590005	NWQL PSP2SP117A: 75 µl	0.0511	06/22/11	0.074096

False Positives Listing for FIPRONIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20110410061	ERA 0818-10-05 LS 2033#2: 80 µl	0.018	02/28/11	0.004
20111890005	Accu 210061341: 40 µl	0.018	07/20/11	0.085
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.018	09/13/11	0.093
20112870073	ERA 0818-10-05 LS 2033#2: 40 µl	0.018	10/25/11	0.005
20113220198	ERA 0818-10-05 LS 2033#2: 80 µl	0.018	12/03/11	0.006

False Negatives Listing for FIPRONIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.018	07/20/11	0.07932
20112310030	Restek A075606: 40 µl	0.018	09/13/11	0.0792

False Positives Listing for FIPRONIL SULFIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080740016	Crescent 07GG004: 50 µl	0.013	04/09/08	0.009
20082970002	Supelco LB60731: 25 µl	0.013	12/17/08	0.007
20083040064	Abs 080408Pest: 25 µl	0.013	01/08/09	0.006
20083260002	Supelco LB60731: 40 µl	0.013	01/17/09	0.007
20083400005	Accu B8090098: 40 µl	0.013	01/28/09	0.093
20083530111	Restek A063025: 40 µl	0.013	02/02/09	0.006
20090080048	Abs 080408Pest: 25 µl	0.013	02/11/09	0.007
20090300003	Restek A063025: 25 µl	0.013	02/11/09	0.007
20090370005	Accu B8090098: 25 µl	0.013	03/03/09	0.044
20090640123	Supelco LB60731: 25 µl	0.013	03/16/09	0.005
20090710012	Abs 080408Pest: 40 µl	0.013	03/25/09	0.006
20090990155	Restek A063025: 25 µl	0.013	05/06/09	0.003
20091060132	Accu B8090098: 40 µl	0.013	05/13/09	0.103
20091340062	Supelco LB60731: 40 µl	0.013	07/10/09	0.049
20091410001	Abs 080408Pest: 25 µl	0.013	06/30/09	0.004
20091770120	Accu B8090098: 25 µl	0.013	09/03/09	0.055
20092260012	Restek A063025: 25 µl	0.013	12/11/09	0.006
20092330002	Accu B8090098: 25 µl	0.013	12/30/09	0.049
20092400050	Abs 080408Pest: 25 µl	0.013	01/10/10	0.010
20102950072	Restek A075606: 40 µl	0.012	01/09/11	0.003
20103430087	Restek A075606: 80 µl	0.012	01/28/11	0.010
20110130056	Supelco LB77168: 80 µl	0.012	02/09/11	0.006
20110560005	Restek A075606: 40 µl	0.012	03/08/11	0.010
20110770001	Supelco LB77168: 40 µl	0.012	03/30/11	0.003
20111050150	Restek A075606: 40 µl	0.012	04/23/11	0.004
20111540007	Restek A075606: 80 µl	0.012	06/20/11	0.005
20111810004	Supelco LB77168: 80 µl	0.012	07/13/11	0.005
20111890005	Accu 210061341: 40 µl	0.012	07/19/11	0.006
20112220126	Restek A075606: 80 µl	0.012	09/01/11	0.008
20112310030	Restek A075606: 40 µl	0.012	09/13/11	0.092
20112450022	Supelco LB77168: 40 µl	0.012	09/24/11	0.003
20112590005	Supelco LB77168: 80 µl	0.012	10/02/11	0.008
20112930085	Restek A075606: 80 µl	0.012	11/01/11	0.005
20113130085	Supelco LB77168: 80 µl	0.012	11/17/11	0.004
20113260111	Restek A075606: 40 µl	0.012	12/04/11	0.005

False Negatives Listing for FIPRONIL SULFIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111470065	ERA 0818-10-05 LS 2033#2: 40 µl	0.012	06/20/11	0.0493228

False Positives Listing for FIPRONIL SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080580078	Protocol R1070723008: 50 µl	0.024	04/03/08	0.005
20080940064	Protocol R1070723008: 50 µl	0.024	04/18/08	0.008
20081840006	Protocol R1070723008: 50 µl	0.024	08/20/08	0.006
20082840003	Crescent 08HH019: 25 µl	0.024	12/08/08	0.005
20083040064	Abs 080408Pest: 25 µl	0.024	01/08/09	0.007
20083110006	Protocol D1080908018: 40 µl	0.024	01/10/09	0.006
20083180005	Crescent 08HH019: 40 µl	0.024	01/14/09	0.004
20083440103	Crescent 08HH019: 40 µl	0.024	01/29/09	0.008
20083460142	Crescent 08HH019: 25 µl	0.024	01/30/09	0.005
20090080048	Abs 080408Pest: 25 µl	0.024	02/11/09	0.006
20090160003	Protocol D1080908018: 25 µl	0.024	02/11/09	0.005
20090710012	Abs 080408Pest: 40 µl	0.024	03/25/09	0.007
20090860072	Protocol D1080908018: 25 µl	0.024	04/28/09	0.008
20091210002	Crescent 08HH019: 25 µl	0.024	06/03/09	0.007
20091340060	Protocol D1080908018: 25 µl	0.024	07/10/09	0.065
20091410001	Abs 080408Pest: 25 µl	0.024	06/30/09	0.006
20091550184	Crescent 08HH019: 40 µl	0.024	07/23/09	0.007
20091830169	Protocol D1080908018: 40 µl	0.024	09/15/09	0.006
20092040202	Abs 080408Pest: 40 µl	0.024	10/27/09	0.005
20111890005	Accu 210061341: 40 µl	0.024	07/20/11	0.067
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.024	09/13/11	0.052

False Negatives Listing for FIPRONIL SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.024	07/20/11	0.05964
20112310030	Restek A075606: 40 µl	0.024	09/13/11	0.05976

False Positives Listing for DESULFINYLFIPRONIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.012	07/10/09	0.050

False Positives Listing for TEBUCONAZOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.02	07/10/09	0.205

False Negatives Listing for TEBUCONAZOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.02	07/10/09	0.3126912

False Positives Listing for ETHION

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112310030	Restek A075606: 40 µl	0.008	09/13/11	0.035

False Negatives Listing for ETHION

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.008	09/13/11	0.04424

False Positives Listing for METRIBUZIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.016	07/10/09	0.235
20112310030	Restek A075606: 40 µl	0.012	09/13/11	0.028

False Negatives Listing for METRIBUZIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.016	07/10/09	0.2443837
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.012	09/13/11	0.042

False Positives Listing for 2,6-DIETHYLANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.009

False Negatives Listing for 2,6-DIETHYLANILINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090580003	ERA 0804-08-02PEST: 25 µl	0.006	03/12/09	0.0095061
20091880135	ERA 0804-08-02PEST: 25 µl	0.006	09/16/09	0.0090377
20100150090	Restek A069639: 20 µl	0.006	03/19/10	0.0080402
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.008

False Positives Listing for TRIFLURALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112310030	Restek A075606: 40 µl	0.018	09/13/11	0.050

False Negatives Listing for TRIFLURALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.018	09/13/11	0.05976

False Positives Listing for DIMETHOATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.006	07/20/11	0.019

False Negatives Listing for DIMETHOATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.006	07/20/11	0.0282

False Positives Listing for PHORATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.02	07/20/11	0.041
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.02	09/13/11	0.018

False Negatives Listing for PHORATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.02	07/20/11	0.05044
20112310030	Restek A075606: 40 µl	0.02	09/13/11	0.05056

False Positives Listing for PARATHION-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890004	Supelco LB77168: 40 µl	0.008	07/20/11	0.037

False Negatives Listing for PARATHION-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890005	Accu 210061341: 40 µl	0.008	07/20/11	0.03216

False Positives Listing for EPTC

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.002	07/10/09	0.008
20111890004	Supelco LB77168: 40 µl	0.0056	07/20/11	0.059

False Negatives Listing for EPTC

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.002	07/10/09	0.0049796
20111890005	Accu 210061341: 40 µl	0.0056	07/20/11	0.05808

False Positives Listing for TEBUTHIURON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.02	07/10/09	0.347
20111890005	Accu 210061341: 40 µl	0.028	07/20/11	0.112
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.028	09/13/11	0.097

False Negatives Listing for TEBUTHIURON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.02	07/10/09	0.2537425
20111890004	Supelco LB77168: 40 µl	0.028	07/20/11	0.0672
20112310030	Restek A075606: 40 µl	0.028	09/13/11	0.0672

False Positives Listing for MOLINATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.002	07/10/09	0.016
20111890004	Supelco LB77168: 40 µl	0.004	07/20/11	0.039

False Negatives Listing for MOLINATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.002	07/10/09	0.0174285
20111890005	Accu 210061341: 40 µl	0.004	07/20/11	0.036

False Positives Listing for ETHOPROPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.016	07/10/09	0.236
20111680035	Accu 210061341: 40 µl	0.016	07/02/11	0.014
20112310030	Restek A075606: 40 µl	0.016	09/13/11	0.083

False Negatives Listing for ETHOPROPHOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.016	07/10/09	0.2137547
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.016	09/13/11	0.0992

False Positives Listing for BENFLURALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.014	07/10/09	0.208
20112310030	Restek A075606: 40 µl	0.014	09/13/11	0.066

False Negatives Listing for BENFLURALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.014	07/10/09	0.292515
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.014	09/13/11	0.1

False Positives Listing for CARBOFURAN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.06	07/10/09	0.218
20111890005	Accu 210061341: 40 µl	0.06	07/20/11	0.105
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.06	09/13/11	0.086

False Negatives Listing for CARBOFURAN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.06	07/10/09	0.18819
20111890004	Supelco LB77168: 40 µl	0.06	07/20/11	0.0912
20112310030	Restek A075606: 40 µl	0.06	09/13/11	0.0912

False Positives Listing for TERBUFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.018	07/10/09	0.097
20112310030	Restek A075606: 40 µl	0.018	09/13/11	0.015

False Negatives Listing for TERBUFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.018	07/10/09	0.1152639
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.018	09/13/11	0.0468

False Positives Listing for PROPYZAMIDE (PRONAMIDE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.004	07/10/09	0.113
20111890004	Supelco LB77168: 40 µl	0.0036	07/20/11	0.085

False Negatives Listing for PROPYZAMIDE (PRONAMIDE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.004	07/10/09	0.1219998
20111890005	Accu 210061341: 40 µl	0.0036	07/20/11	0.07996

False Positives Listing for DISULFOTON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.04	07/20/11	0.033
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.04	09/13/11	0.012

False Negatives Listing for DISULFOTON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.04	07/20/11	0.0496
20112310030	Restek A075606: 40 µl	0.04	09/13/11	0.0498

False Positives Listing for PROPANIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.088

False Negatives Listing for PROPANIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.07928

False Positives Listing for CARBARYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091320001	ERA 0804-08-02PEST: 25 µl	0.2	06/18/09	0.006
20111890005	Accu 210061341: 40 µl	0.06	07/20/11	0.204
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.06	09/13/11	0.214

False Negatives Listing for CARBARYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.06	07/20/11	0.29696
20112310030	Restek A075606: 40 µl	0.06	09/13/11	0.2972

False Positives Listing for THIOBENCARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.016	07/10/09	0.219
20092960003	Supelco LB69639: 20 µl	0.016	02/06/10	0.007
20101950137	Supelco LB69639: 40 µl	0.016	09/23/10	0.007
20110340007	Abs 080610: 40 µl	0.016	02/22/11	0.005
20110620082	Abs 080610: 80 µl	0.016	03/16/11	0.007
20111890004	Supelco LB77168: 40 µl	0.016	07/20/11	0.004
20112310030	Restek A075606: 40 µl	0.016	09/13/11	0.063

False Negatives Listing for THIOBENCARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.016	07/10/09	0.1770485
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.016	09/13/11	0.0856

False Positives Listing for DACTHAL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340062	Supelco LB60731: 40 µl	0.006	07/10/09	0.183
20111890004	Supelco LB77168: 40 µl	0.0076	07/20/11	0.043

False Negatives Listing for DACTHAL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340060	Protocol D1080908018: 25 µl	0.006	07/10/09	0.1518773
20111890005	Accu 210061341: 40 µl	0.0076	07/20/11	0.03616

False Positives Listing for PENDIMETHALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.012	07/10/09	0.284
20112310030	Restek A075606: 40 µl	0.012	09/13/11	0.078

False Negatives Listing for PENDIMETHALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.012	07/10/09	0.3209156
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.012	09/13/11	0.084

False Positives Listing for PROPARGITE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.02	07/20/11	0.026
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.02	09/13/11	0.033

False Negatives Listing for PROPARGITE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.02	07/20/11	0.04976
20112310030	Restek A075606: 40 µl	0.02	09/13/11	0.04952

False Positives Listing for AZINPHOS-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111890005	Accu 210061341: 40 µl	0.12	07/20/11	0.103
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.12	09/13/11	0.123

False Negatives Listing for AZINPHOS-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20111890004	Supelco LB77168: 40 µl	0.12	07/20/11	0.1604
20112310030	Restek A075606: 40 µl	0.12	09/13/11	0.16036

False Positives Listing for 1RS CIS-PERMETHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091340060	Protocol D1080908018: 25 µl	0.014	07/10/09	0.051
20112310030	Restek A075606: 40 µl	0.01	09/13/11	0.019

False Negatives Listing for 1RS CIS-PERMETHRIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20091340062	Supelco LB60731: 40 µl	0.014	07/10/09	0.0650258
20112310032	ERA 0818-10-05 LS 2033#2: 80 µl	0.01	09/13/11	0.03968