SAS Output

False Negatives Listing for BROMACIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20102810021	Accu 210091144: 20 µl	0.36	12/15/10	0.8033963

False Positives Listing for ANTHRACENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20110770002	Ultra CG-2301: 20 µl	0.01	04/06/11	0.090
20112170171	Ultra CG-2301: 50 µl	0.01	08/26/11	0.190

False Negatives Listing for ANTHRACENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	1.153926

False Negatives Listing for BROMOFORM

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	09/08/06	0.7820728
20090210032	Protocol D1080815007: 40 µl	0.1	01/29/09	5.715476

False Negatives Listing for FLUORANTHENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	2.81608

False Positives Listing for ISOPHORONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.025
20081150078	Crescent 07GG011: 25 µl	0.08	05/20/08	0.019
20081290007	Supelco LB50015: 25 µl	0.08	06/03/08	0.011
20081840003	Crescent 07GG011: 25 µl	0.08	08/02/08	0.009
20082350004	Supelco LB50015: 25 µl	0.08	09/24/08	0.013
20082480189	Crescent 07GG011: 25 µl	0.08	10/08/08	0.015
20083400002	Abs 080508WW: 20 µl	0.08	01/08/09	0.008
20090300002	Supelco LB60966: 20 µl	0.08	03/05/09	0.005

False Negatives Listing for ISOPHORONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.08	01/29/09	0.2624453

False Positives Listing for NAPHTHALENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061180197	Restek A038536: 100 µl & Crescent 41224AC: 100 µl	0.5	05/16/06	0.014
20061320007	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	06/06/06	0.015
20061370129	Restek A038536: 100 µl & Abs 071805WW: 30 µl	0.5	06/06/06	0.014

False Negatives Listing for NAPHTHALENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	2.849406

False Negatives Listing for PENTACHLOROPHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20063610096	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	2	02/13/07	3.568195

False Positives Listing for PHENANTHRENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20063330003	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.08	01/31/07	0.005
20070520015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.08	03/12/07	0.006

False Negatives Listing for PHENANTHRENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	2.349511

False Positives Listing for PHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060230010	Crescent 07EE053: 30 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	03/23/06	0.200
20060370003	Restek A038536: 100 µl & Crescent 41224AC: 100 µl	0.5	03/21/06	0.400
20061180197	Restek A038536: 100 µl & Crescent 41224AC: 100 µl	0.5	05/16/06	0.259
20062910019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.4	11/22/06	0.140
20070320005	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.4	03/13/07	0.352

False Negatives Listing for PHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061650067	Supelco LB31943: 75 µl & Crescent 41208AC: 100 µl	0.5	07/06/06	0.7704703
20061740220	Supelco LB31943: 75 µl & Restek A038536: 100 µl	0.5	07/19/06	0.7715582

False Negatives Listing for PYRENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	0.7748386

False Positives Listing for TETRACHLOROETHYLENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060230010	Crescent 07EE053: 30 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	03/23/06	0.006

False Negatives Listing for TETRACHLOROETHYLENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.12	01/29/09	4.374089

False Positives Listing for 1,4-DICHLOROBENZENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.043
20093450030	Restek A070024: 10 µl	0.04	02/23/10	0.005

False Negatives Listing for 1,4-DICHLOROBENZENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	09/08/06	0.7741732
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	1.920433

False Negatives Listing for CHLORPYRIFOS

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	09/08/06	0.7346746

False Positives Listing for METOLACHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.021
20070260003	Accu B6080007: 50 µl	0.16	03/13/07	0.037

False Negatives Listing for METOLACHLOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.08	01/29/09	5.490523

False Negatives Listing for DIAZINON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	09/08/06	0.837371
20083460140	Protocol D1080815007: 20 µl	0.08	01/28/09	1.117748
20090210032	Protocol D1080815007: 40 µl	0.08	01/29/09	2.299521
20090780143	Protocol D1080815007: 20 µl	0.08	04/02/09	1.112903
20091410002	Protocol D1080815007: 20 µl	0.08	07/22/09	1.095238
20092040204	Protocol D1080815007: 20 µl	0.08	08/27/09	1.08994
20092460252	Protocol D1080815007: 40 µl	0.16	10/22/09	2.212868

False Positives Listing for CAFFEINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.129
20102160003	ChemService 480-95B: 20 µl	0.06	10/14/10	0.028

False Negatives Listing for CAFFEINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.1	01/29/09	5.898771

False Negatives Listing for METALAXYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.12	01/29/09	1.932931

False Positives Listing for OCTYLPHENOL, DIETHOXY-

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060370003	Restek A038536: 100 µl & Crescent 41224AC: 100 µl	1	03/21/06	0.600
20060620003	ChemService 346-5B: 75 µl & Restek A038536: 100 µl & Crescent 41224AC: 100 µl	1	03/30/06	0.400
20060690197	Supelco LB31943: 75 µl & Crescent 41224AC: 100 µl	1	04/03/06	1.300
20060930017	Restek A038536: 200 µl & Abs 071805WW: 60 µl & Crescent 41224AC: 200 µl	1	04/18/06	1.900
20061180197	Restek A038536: 100 µl & Crescent 41224AC: 100 µl	1	05/16/06	1.040
20061440008	ChemService 346-5B: 150 µl & Abs 071805WW: 60 µl & Crescent 41224AC: 200 µl	1	06/12/06	2.220
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	0.112
20061940016	ChemService 346-5B: 75 µl & Restek A038536: 100 µl & Crescent 41224AC: 100 µl	1	09/19/06	0.986
20062430024	Supelco LB31943: 75 µl & Restek A038536: 100 µl	1	10/13/06	0.007
20062500288	ChemService 346-5B: 150 µl & Restek A038536: 200 µl & Crescent 41224AC: 200 µl	1	10/06/06	2.320
20063180163	Accu B6080007: 50 µl	1	11/29/06	0.247
20071860015	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	1	09/06/07	0.039

False Negatives Listing for OCTYLPHENOL, DIETHOXY-

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20071710024	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	08/20/07	1.164404
20093380006	Crescent 08LL076: 20 µl	1	02/05/10	1.107724

False Positives Listing for OCTYLPHENOL, MONOETHOXY-

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060230010	Crescent 07EE053: 30 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	1	03/23/06	0.900
20060310004	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	1	03/21/06	0.600
20061000003	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	1	04/18/06	1.140
20061560046	ChemService 346-5B: 150 µl & Restek A038536: 200 µl & Crescent 41208AC: 200 µl	1	06/29/06	1.320
20061630095	Absolute 082503WW: 25 µl & Crescent 41208AC: 100 µl	1	07/03/06	0.781
20061650067	Supelco LB31943: 75 µl & Crescent 41208AC: 100 µl	1	07/06/06	0.652
20062090012	Absolute 082503WW: 50 µl & Crescent 41208AC: 200 µl	1	08/27/06	1.610
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	1	09/08/06	0.499
20062500288	ChemService 346-5B: 150 µl & Restek A038536: 200 µl & Crescent 41224AC: 200 µl	1	10/06/06	0.055
20062910019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	11/22/06	0.528
20063000064	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	11/27/06	0.265
20063330003	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	01/31/07	0.234
20063610096	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	02/13/07	0.510
20070320005	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	03/13/07	0.344
20070520015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	03/12/07	0.575
20070720045	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	04/18/07	0.547
20071010007	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	05/01/07	0.256
20071070100	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	05/01/07	0.728
20071220019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	05/22/07	0.555
20071500017	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	08/14/07	0.286
20071710024	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	08/20/07	0.684
20071920023	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	09/10/07	0.316
20072070015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/01/07	0.644
20072200100	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	10/19/07	0.300
20072290014	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/23/07	0.840
20072490002	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	11/14/07	0.651
20073110111	Crescent 07GG011: 25 µl	1	01/11/08	1.430
20080640003	Crescent 07GG011: 25 µl	1	03/31/08	1.320
20080870097	Crescent 07GG011: 25 µl	1	04/09/08	1.320
20081150078	Crescent 07GG011: 25 µl	1	05/20/08	1.510
20081500005	Crescent 07GG011: 25 µl	1	06/03/08	1.480
20081840003	Crescent 07GG011: 25 µl	1	08/02/08	1.500
20082480189	Crescent 07GG011: 25 µl	1	10/08/08	1.240
20083440104	Crescent 08HH017: 40 µl	1	01/27/09	4.000
20090580005	Crescent 08HH017: 20 µl	1	03/21/09	2.800
20090640122	Crescent 08HH017: 20 µl	1	03/24/09	2.700
20091320006	Crescent 08HH017: 20 µl	1	06/03/09	2.300
20091880137	Crescent 08HH017: 20 µl	1	08/26/09	2.400
20092400049	Crescent 08HH017: 40 µl	1	10/21/09	5.000
20092960004	Crescent 08LL076: 80 µl	1	01/20/10	4.500
20093380006	Crescent 08LL076: 20 µl	1	02/05/10	0.540
20101410008	Crescent 08LL076: 40 µl	1	08/04/10	1.800
20102390089	Crescent 08LL076: 40 µl	1	11/04/10	1.700
20111330147	Restek A075799: 50 µl	1	06/08/11	0.030

False Negatives Listing for COTININE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20072200100	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.4	10/19/07	0.7052942
20101410008	Crescent 08LL076: 40 µl	0.6	08/04/10	0.8929111

False Positives Listing for 1-METHYLNAPHTHALENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20093520065	ChemService 480-95B: 80 µl	0.022	02/23/10	0.011

False Negatives Listing for 1-METHYLNAPHTHALENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	0.3999167

False Positives Listing for 2-METHYLNAPHTHALENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20070640058	Accu B6080007: 25 µl	0.08	03/12/07	0.005

False Negatives Listing for 2-METHYLNAPHTHALENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	0.6040408

False Positives Listing for 3-BETA-COPROSTANOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	2	07/19/06	0.290

False Negatives Listing for 3-BETA-COPROSTANOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20082210030	NWQL BNA2SP053B: 75 µl	1	09/17/08	2.356175

False Positives Listing for 3-METHYL-1(H)-INDOLE (SKATOLE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20062910019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.08	11/22/06	0.004
20063610096	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.08	02/13/07	0.005
20070320005	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.08	03/13/07	0.002
20071500017	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.08	08/14/07	0.001
20071710024	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.08	08/20/07	0.006
20083260004	ERA 0804-08-02WW: 40 µl	0.04	01/28/09	0.014
20083400002	Abs 080508WW: 20 µl	0.04	01/08/09	0.007
20083530109	ERA 0804-08-02WW: 20 µl	0.04	03/05/09	0.011
20090160002	Abs 080508WW: 20 µl	0.04	01/29/09	0.006
20090920065	ERA 0804-08-02WW: 20 µl	0.04	04/23/09	0.006

False Negatives Listing for 3-METHYL-1(H)-INDOLE (SKATOLE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	1.654412
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	1.937096

False Negatives Listing for 4-CUMYLPHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	1.378676
20083460140	Protocol D1080815007: 20 µl	0.1	01/28/09	1.611825
20090210032	Protocol D1080815007: 40 µl	0.1	01/29/09	3.315976

False Negatives Listing for 4-N-OCTYLPHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	1.531863

False Negatives Listing for 4-TERT-OCTYLPHENOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	1.194853

False Positives Listing for 5-METHYL-1H-BENZOTRIAZOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111050152	Spex Organics T1100706008: 80 µl	1.2	04/28/11	0.290

False Negatives Listing for 5-METHYL-1H-BENZOTRIAZOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20071220019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1.8	05/22/07	1.961652
20090210032	Protocol D1080815007: 40 µl	2	01/29/09	3.340971
20102810021	Accu 210091144: 20 µl	1.2	12/15/10	4.012938

False Negatives Listing for ACETOPHENONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	0.5	09/08/06	0.7820728
20081630014	NWQL BNA2SP053B: 75 µl	0.4	07/12/08	0.5988024

False Positives Listing for ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.991

False Negatives Listing for ACETYL HEXAMETHYL TETRAHYDRONAPHTHALENE (AHTN)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062910019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.5	11/22/06	0.8607595

False Positives Listing for ANTHRAQUINONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20091410002	Protocol D1080815007: 20 µl	0.16	07/22/09	0.020

False Positives Listing for BENZOPHENONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20072290015	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.12	10/23/07	0.026
20072350249	Supelco LB40674: 25 µl	0.12	11/05/07	0.017
20072490006	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	0.12	11/14/07	0.013
20072560017	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.12	11/21/07	0.008
20072770005	Restek A053259: 25 µl	0.12	11/21/07	0.027
20072900074	Restek A053259: 25 µl	0.12	12/20/07	0.025
20073060021	Restek A053259: 25 µl	0.12	01/11/08	0.033
20073110111	Crescent 07GG011: 25 µl	0.12	01/11/08	0.033
20073380129	Restek A053259: 25 µl	0.12	01/23/08	0.038
20073510135	Restek A053259: 25 µl	0.12	02/01/08	0.026
20080150155	Restek A053259: 25 µl	0.12	02/27/08	0.018
20080640003	Crescent 07GG011: 25 µl	0.12	03/31/08	0.024
20080870097	Crescent 07GG011: 25 µl	0.12	04/09/08	0.034

False Positives Listing for BETA-SITOSTEROL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20111330147	Restek A075799: 50 µl	4	06/08/11	1.400

False Negatives Listing for BETA-SITOSTEROL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20081630014	NWQL BNA2SP053B: 75 µl	1.6	07/11/08	2.39521
20081840003	Crescent 07GG011: 25 µl	1.6	08/02/08	2.766798
20082210030	NWQL BNA2SP053B: 75 µl	1.6	09/17/08	2.356175

False Positives Listing for BISPHENOL A

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060930017	Restek A038536: 200 µl & Abs 071805WW: 60 µl & Crescent 41224AC: 200 µl	1	04/18/06	0.200
20062090012	Absolute 082503WW: 50 µl & Crescent 41208AC: 200 µl	1	08/27/06	0.100
20062330168	ChemService 346-5B: 75 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	1	09/08/06	0.094

False Negatives Listing for BISPHENOL A

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20082210030	NWQL BNA2SP053B: 75 µl	0.4	09/17/08	0.5890438
20103230119	Restek A075799: 20 µl	2	01/29/11	2.958012

False Positives Listing for CAMPHOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20070380003	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.1	03/13/07	0.007
20111680032	Spex Organics T1100706008: 80 µl	0.044	07/22/11	0.009
20112590003	Spex Organics T1100706008: 50 µl	0.044	11/04/11	0.020

False Negatives Listing for CAMPHOR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.8169935

False Positives Listing for CARBAZOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20093520065	ChemService 480-95B: 80 µl	0.03	02/23/10	0.012

False Negatives Listing for CARBAZOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.7659314
20090210032	Protocol D1080815007: 40 µl	0.04	01/29/09	3.940845

False Positives Listing for CHOLESTEROL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	2	07/19/06	0.714

False Negatives Listing for CHOLESTEROL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20093380006	Crescent 08LL076: 20 µl	2	02/05/10	2.004065

False Negatives Listing for D-LIMONENE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.6127451
20090210032	Protocol D1080815007: 40 µl	0.14	01/29/09	0.1583004
20092460252	Protocol D1080815007: 40 µl	0.08	10/22/09	0.1523351
20103330009	Ultra CG-2301: 20 µl	0.08	12/09/10	0.1438989

False Positives Listing for HEXAHYDROHEXAMETHYLCYCLOPENTABENZOPYRAN (HHCB)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.202
20062910019	ERA 0714-06-03: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	0.5	11/22/06	0.608
20063000064	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.5	11/27/06	0.288
20063330003	ERA 0714-06-03: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	0.5	01/31/07	0.325
20112870076	Ultra CG-2301: 20 µl	0.052	11/08/11	0.006

False Positives Listing for INDOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060580108	Crescent 07EE053: 60 µl & Abs 071805WW: 60 µl	0.5	03/30/06	0.110

False Negatives Listing for INDOLE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.7148693

False Negatives Listing for ISOBORNEOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.8169935
20090210032	Protocol D1080815007: 40 µl	0.18	01/29/09	0.1957925

False Negatives Listing for ISOPROPYLBENZENE (CUMENE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.510621

False Positives Listing for ISOQUINOLINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20112220131	NWQL BNA2SP124B: 50 µl	0.046	08/26/11	0.012

False Negatives Listing for ISOQUINOLINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.561683
20102880004	Spex Organics T1100706008: 20 µl	0.046	12/08/10	0.1956715
20103330009	Ultra CG-2301: 20 µl	0.046	12/09/10	0.1925134

False Negatives Listing for MENTHOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.7148693

False Negatives Listing for METHYL SALICYLATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	0.5	07/19/06	0.7148693
20081750161	Supelco LB50015: 25 µl	0.1	08/07/08	2.196894

False Negatives Listing for N,N-DIETHYL-META-TOLUAMIDE (DEET)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20081750161	Supelco LB50015: 25 µl	0.1	08/07/08	1.034569

False Positives Listing for NONYLPHENOL, DIETHOXY- (TOTAL)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20061440008	ChemService 346-5B: 150 µl & Abs 071805WW: 60 µl & Crescent 41224AC: 200 µl	5	06/12/06	1.360
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	5	07/19/06	2.420
20063180162	NWQL WWS1SP134A: 75 µl	5	11/29/06	7.350
20070240005	NWQL WWS1SP134A: 50 µl	5	02/13/07	3.500
20070860099	NWQL WWS1SP134A: 75 µl	5	04/25/07	7.910

False Negatives Listing for NONYLPHENOL, DIETHOXY- (TOTAL)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20063250138	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	5	01/31/07	6.12794
20070440039	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	5	03/13/07	6.037699
20071860015	Abs 091106ww: 25 µl & Crescent 08FF023: 25 µl	5	09/06/07	6.112105
20073110111	Crescent 07GG011: 25 µl	5	01/11/08	6.671384
20081500005	Crescent 07GG011: 25 µl	5	06/03/08	6.576981
20082480189	Crescent 07GG011: 25 µl	5	10/08/08	6.59868
20093380006	Crescent 08LL076: 20 µl	5	02/05/10	5.288618
20101410008	Crescent 08LL076: 40 µl	5	08/04/10	10.46556
20102390089	Crescent 08LL076: 40 µl	5	11/04/10	10.49194

False Positives Listing for P-CRESOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20063400126	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.18	01/31/07	0.165

False Positives Listing for PARA-NONYLPHENOL (TOTAL)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060230010	Crescent 07EE053: 30 µl & Abs 071805WW: 30 µl & Crescent 41208AC: 100 µl	5	03/23/06	1.000
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	5	07/19/06	1.680
20072070015	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/01/07	1.420
20072140014	Supelco LB40674: 25 µl	1	10/01/07	1.840
20072200100	Protocol F1060727002: 10 µl & Crescent 08FF020: 10 µl & Crescent 08FF021: 10 µl	1	10/19/07	0.899
20072290014	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	10/23/07	1.670
20072290015	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	1	10/23/07	2.450
20072350249	Supelco LB40674: 25 µl	1	11/05/07	1.880
20072490002	Protocol F1060727002: 25 µl & Crescent 08FF020: 25 µl & Crescent 08FF021: 25 µl	1	11/14/07	1.600
20072560017	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	1	11/21/07	0.691
20072770005	Restek A053259: 25 µl	1	11/21/07	1.760
20072900074	Restek A053259: 25 µl	1	12/20/07	2.010
20073060021	Restek A053259: 25 µl	1	01/11/08	2.020
20073240139	Restek A053259: 25 µl	1	01/14/08	1.780
20073380129	Restek A053259: 25 µl	1	01/23/08	1.930
20073510135	Restek A053259: 25 µl	1	02/01/08	1.660
20080150155	Restek A053259: 25 µl	1	02/27/08	1.400
20080580077	Supelco LB50015: 25 µl	1	03/31/08	2.200
20080800002	Supelco LB50015: 25 µl	1	04/09/08	1.760
20080940060	Supelco LB50015: 25 µl	1	04/21/08	18.200
20081290007	Supelco LB50015: 25 µl	1	06/03/08	15.400
20081750161	Supelco LB50015: 25 µl	1	08/07/08	13.100
20082040252	Supelco LB50015: 25 µl	1	09/10/08	13.200
20082350004	Supelco LB50015: 25 µl	1	09/24/08	8.160
20083110004	ChemService 406-104C: 40 µl	2	11/14/08	0.495
20090500129	Abs 080508WW: 40 µl	2	03/21/09	0.580
20090780143	Protocol D1080815007: 20 µl	2	04/02/09	0.450
20090920065	ERA 0804-08-02WW: 20 µl	2	04/23/09	0.330

False Negatives Listing for PARA-NONYLPHENOL (TOTAL)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20093100004	Accu 209081217: 20 µl	2	01/20/10	2.010488
20093380006	Crescent 08LL076: 20 µl	2	02/05/10	2.063008
20101410008	Crescent 08LL076: 40 µl	2	08/04/10	4.082454
20101480009	Accu 209081217: 20 µl	2	08/04/10	2.038114

False Negatives Listing for BETA-STIGMASTANOL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20081630014	NWQL BNA2SP053B: 75 µl	1.2	07/12/08	2.39521
20082210030	NWQL BNA2SP053B: 75 µl	1.2	09/17/08	2.356175

False Positives Listing for TRI(2-CHLOROETHYL)PHOSPHATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20072560017	Restek A046567: 25 µl & Crescent 08FF022: 25 µl	0.1	11/21/07	0.053
20082480189	Crescent 07GG011: 25 µl	0.1	10/08/08	0.108
20092960004	Crescent 08LL076: 80 µl	0.1	01/20/10	0.070

False Negatives Listing for TRICLOSAN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	1.194853

False Negatives Listing for TRIETHYL CITRATE (ETHYL CITRATE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060170046	Restek A038536: 200 µl & Crescent 07EE053: 60 µl	0.5	03/23/06	1.045151
20060620003	ChemService 346-5B: 75 µl & Restek A038536: 100 µl & Crescent 41224AC: 100 µl	0.5	03/30/06	0.5227938

False Positives Listing for TRIPHENYL PHOSPHATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20092820006	NSI 083109-01WW: 20 µl	0.12	11/04/09	0.011
20093340133	NSI 083109-01WW: 20 µl	0.12	02/03/10	0.009
20100420054	NSI 083109-01WW: 80 µl	0.12	03/25/10	0.025
20100500004	NSI 083109-01WW: 40 µl	0.12	03/25/10	0.018
20101550005	NSI 083109-01WW: 40 µl	0.12	06/29/10	0.014
20102810021	Accu 210091144: 20 µl	0.12	12/15/10	0.006

False Positives Listing for TRI(2-BUTOXYETHYL)PHOSPHATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20100420054	NSI 083109-01WW: 80 µl	0.8	03/25/10	0.100

False Positives Listing for CARBARYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20062430024	Supelco LB31943: 75 µl & Restek A038536: 100 µl	1	10/13/06	0.041
20083110004	ChemService 406-104C: 40 µl	1	11/14/08	0.280
20091130128	ChemService 406-104C: 40 µl	1	05/12/09	0.240
20103020151	Ultra CG-2301: 80 µl	0.16	12/16/10	0.074
20111680032	Spex Organics T1100706008: 80 µl	0.16	07/22/11	0.050
20112590003	Spex Organics T1100706008: 50 µl	0.16	11/04/11	0.027
20112870076	Ultra CG-2301: 20 µl	0.16	11/08/11	0.014
20113500020	Ultra CG-2301: 80 µl	0.16	02/16/12	0.069

False Negatives Listing for CARBARYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060170046	Restek A038536: 200 µl & Crescent 07EE053: 60 µl	1	03/23/06	3.135452
20060790024	Supelco LB31943: 75 µl & Crescent 07EE053: 30 µl	1	04/03/06	1.565108
20061800285	Restek A038536: 100 µl & Crescent 07EE053: 30 µl	1	07/19/06	1.531863
20093170003	ChemService 480-95B: 40 µl	0.38	01/21/10	0.5136418