SAS Output

False Positives Listing for CYCLOATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20093520062	Spex Organics T1090828008: 40 µl	0.04	12/30/09	0.006

False Negatives Listing for CYCLOATE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062160015	Ultra CB-1742: 40 µl	0.014	08/17/06	0.1625392

False Negatives Listing for TERBACIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060930014	Crescent 07EE046: 40 µl	0.026	05/01/06	0.1676095

False Negatives Listing for DEISOPROPYLATRAZINE (2-CHLORO-6-ETHYLAMINO-4-AMINO-S-TRIAZINE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20102630167	Crescent 08LL073: 80 µl	0.06	10/28/10	0.1592198

False Negatives Listing for DEETHYLDEISOPROPYLATRAZINE (CHLORODIAMINO-S-TRIAZINE)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051310013	Crescent 07DD034: 50 µl	0.04	07/07/05	0.0786658
20051460191	Crescent 07DD034: 40 µl	0.04	06/05/05	0.0630948
20051920137	Crescent 07DD034: 50 µl	0.04	07/22/05	0.0791306
20052030208	Crescent 07DD034: 40 µl	0.04	08/03/05	0.06362
20052340026	Crescent 07DD034: 50 µl	0.04	08/31/05	0.079525
20052590005	Crescent 07DD034: 50 µl	0.04	09/25/05	0.0797279
20052730081	Crescent 07DD034: 40 µl	0.04	10/13/05	0.0629129
20052900054	Crescent 07DD034: 40 µl	0.04	10/28/05	0.0635391
20060170043	Crescent 07EE046: 40 µl	0.04	01/27/06	0.1067236
20060930014	Crescent 07EE046: 40 µl	0.04	05/01/06	0.1047559
20061740222	Crescent 07EE046: 40 µl	0.04	06/27/06	0.0989315
20062330175	Crescent 07EE046: 40 µl	0.04	08/29/06	0.1060333
20062580007	Crescent 07EE046: 40 µl	0.04	09/22/06	0.1041667

False Negatives Listing for DICAMBA

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060170043	Crescent 07EE046: 40 µl	0.036	01/27/06	0.0426894
20060690198	Crescent 07EE046: 40 µl	0.036	04/07/06	0.042328
20060930014	Crescent 07EE046: 40 µl	0.036	05/01/06	0.0419024
20062330175	Crescent 07EE046: 40 µl	0.036	08/29/06	0.0424133
20062580007	Crescent 07EE046: 40 µl	0.036	09/22/06	0.0416667
20072900076	Abs 071607LC: 50 µl	0.04	11/06/07	0.279338
20080150157	Accu B7070230: 50 µl	0.04	02/12/08	0.2843157
20092400046	Supelco LB60726: 30 µl	0.04	09/30/09	0.1765857
20092820001	Accu 209081166: 40 µl	0.04	10/21/09	0.0543254
20093240039	ChemService 430-40B: 40 µl	0.04	12/03/09	0.0579885
20100360001	Accu 209081166: 40 µl	0.04	02/18/10	0.0550294
20101130051	ChemService 430-40B: 40 µl	0.04	05/05/10	0.0589681
20101900003	Accu 209081166: 40 µl	0.04	07/28/10	0.0551834
20103020153	Crescent 163162: 40 µl	0.04	11/30/10	0.0752475

False Negatives Listing for MCPB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060790022	NSI 080405-01HPLC: 25 µl	0.1	04/05/06	0.1179616
20061800284	NSI 080405-01HPLC: 25 µl	0.1	07/07/06	0.1129405
20061940014	NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl	0.1	07/20/06	0.1315928
20062230032	NWQL ABS94077: 50 µl & NWQL ABS94078: 50 µl	0.1	08/24/06	0.1258432
20062370005	NSI 080405-01HPLC: 25 µl	0.1	09/06/06	0.1181847
20062910018	Supelco LB40676: 75 µl	0.2	11/13/06	0.2223868

False Negatives Listing for METHIOCARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060580109	NSI 080405-01HPLC: 5 µl	0.01	03/10/06	0.0385306

False Negatives Listing for PROPOXUR

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20052970044	Crescent 07EE046: 10 µl	0.008	11/03/05	0.0253405

False Positives Listing for BENTAZON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20071150010	Supelco LB40676: 75 µl	0.02	05/11/07	0.001
20073060022	Ultra CD-2088: 50 µl	0.04	11/28/07	0.002

False Negatives Listing for BENTAZON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20071290015	Restek A046748: 75 µl	0.02	06/02/07	0.0671709
20101480008	Crescent 08LL073: 40 µl	0.06	06/17/10	0.0705175

False Positives Listing for 2,4-DB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20070860102	Ultra CC-2418: 75 µl	0.02	04/10/07	0.001
20071860003	Ultra CC-2418: 75 µl	0.02	07/25/07	0.001
20092260010	Restek A063332: 50 µl & Restek A062398: 50 µl	0.02	09/02/09	0.009
20102160005	Spex Organics T1090828008: 80 µl	0.02	09/01/10	0.006

False Negatives Listing for FLUOMETURON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20072200099	Accu B6070187: 75 µl	0.04	08/25/07	0.2042629

False Positives Listing for OXAMYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20092960006	Crescent 08LL073: 40 µl	0.12	11/19/09	0.002

False Negatives Listing for OXAMYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051920137	Crescent 07DD034: 50 µl	0.03	07/22/05	0.0527537
20052590005	Crescent 07DD034: 50 µl	0.03	09/25/05	0.0531519
20052730081	Crescent 07DD034: 40 µl	0.03	10/13/05	0.0419419
20052900054	Crescent 07DD034: 40 µl	0.03	10/28/05	0.0423594
20053270023	Crescent 07EE046: 200 µl	0.03	12/14/05	0.3136435
20053460080	Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl	0.03	01/07/06	0.098153
20060370004	Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl	0.03	03/04/06	0.0979876
20060440037	Ultra CB-1742: 40 µl	0.03	03/04/06	0.0419419
20060690198	Crescent 07EE046: 40 µl	0.05	04/07/06	0.0634921
20063180164	Ultra CC-2418: 20 µl	0.04	11/30/06	0.0852155

False Positives Listing for ATRAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20100630038	Crescent 08LL073: 40 µl	0.04	03/17/10	0.001

False Positives Listing for 2,4-D

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060440037	Ultra CB-1742: 40 µl	0.038	03/04/06	0.099
20060620004	Ultra CB-1742: 200 µl	0.038	04/07/06	0.150
20060860012	Ultra CB-1742: 40 µl	0.038	04/05/06	0.102
20061030077	Ultra CB-1742: 40 µl	0.038	05/01/06	0.092
20061910093	Ultra CB-1742: 200 µl	0.038	07/19/06	0.019
20062430019	Ultra CB-1742: 40 µl	0.038	09/12/06	0.008
20062430023	Ultra CB-1742: 200 µl	0.038	09/12/06	0.037

False Negatives Listing for 2,4-D

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060170043	Crescent 07EE046: 40 µl	0.038	01/27/06	0.0503735
20061740222	Crescent 07EE046: 40 µl	0.038	06/27/06	0.0466957
20073380128	Abs 071607LC: 50 µl	0.02	01/03/08	0.2015

False Negatives Listing for PROPHAM

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051920137	Crescent 07DD034: 50 µl	0.03	07/22/05	0.0527537
20072400295	Restek A046748: 50 µl	0.06	09/12/07	0.0700238

False Positives Listing for PICLORAM

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080240003	Protocol I1070803003: 50 µl	0.12	02/12/08	0.094
20100630038	Crescent 08LL073: 40 µl	0.12	03/18/10	0.016

False Negatives Listing for PICLORAM

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20071290015	Restek A046748: 75 µl	0.12	06/02/07	0.2216638
20072900076	Abs 071607LC: 50 µl	0.12	11/06/07	0.3891675
20080150157	Accu B7070230: 50 µl	0.12	02/12/08	0.4016402
20080370106	Abs 071607LC: 50 µl	0.12	02/12/08	0.3923155
20080740019	Accu B7070230: 50 µl	0.12	04/04/08	0.3995513
20080870100	Abs 071607LC: 50 µl	0.12	04/04/08	0.3914052
20082000011	Accu B7070230: 50 µl	0.12	07/31/08	0.3833285
20100920050	Restek A069890: 40 µl	0.12	04/14/10	0.2576773
20101550008	Restek A069890: 80 µl	0.12	06/17/10	0.5268971

False Negatives Listing for ORYZALIN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20080940065	Restek A053251: 50 µl	0.04	04/30/08	0.0708229

False Negatives Listing for NORFLURAZON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061180198	Crescent 07EE046: 10 µl	0.02	05/10/06	0.030284

False Negatives Listing for METHOMYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20052970044	Crescent 07EE046: 10 µl	0.02	11/03/05	0.0422342

False Negatives Listing for FENURON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062370005	NSI 080405-01HPLC: 25 µl	0.1	09/06/06	0.1076794
20063180164	Ultra CC-2418: 20 µl	0.04	11/30/06	0.0749581

False Positives Listing for DINOSEB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20080740019	Accu B7070230: 50 µl	0.04	04/04/08	0.001

False Negatives Listing for DINOSEB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20063180164	Ultra CC-2418: 20 µl	0.04	11/30/06	0.0881744

False Negatives Listing for DICHLOROPROP (DICHLORPROP)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061030077	Ultra CB-1742: 40 µl	0.028	05/01/06	0.1283834
20061320008	Ultra CB-1742: 40 µl	0.028	05/28/06	0.1274291

False Positives Listing for DACTHAL MONOACID

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060310003	NSI 080405-01HPLC: 25 µl	0.028	02/11/06	0.132

False Negatives Listing for DACTHAL MONOACID

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20071290015	Restek A046748: 75 µl	0.02	06/02/07	0.0701562
20092820001	Accu 209081166: 40 µl	0.04	10/21/09	0.0510973
20103020153	Crescent 163162: 40 µl	0.04	11/30/10	0.0514851

False Negatives Listing for CLOPYRALID

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060170043	Crescent 07EE046: 40 µl	0.024	01/27/06	0.1280683
20062330175	Crescent 07EE046: 40 µl	0.067	08/29/06	0.12724
20062910018	Supelco LB40676: 75 µl	0.06	11/13/06	0.1305048
20072140017	Supelco LB40676: 50 µl	0.06	08/23/07	0.0848953
20080290026	Crescent 07GG007: 50 µl	0.06	02/12/08	0.1583087
20092960006	Crescent 08LL073: 40 µl	0.06	11/20/09	0.0754942
20101480008	Crescent 08LL073: 40 µl	0.06	06/17/10	0.0788136
20101950136	Crescent 08LL073: 40 µl	0.06	07/28/10	0.0752252

False Negatives Listing for CHLOROTHALONIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051190007	Ultra CA-1226: 25 µl	0.035	05/06/05	0.1687961
20051540207	Ultra CA-1226: 75 µl	0.035	06/11/05	0.5155457
20051680024	Ultra CA-1226: 25 µl	0.035	08/01/05	0.1701571
20051940296	Ultra CA-1226: 25 µl	0.035	07/22/05	0.1718849
20052080326	Ultra CA-1226: 75 µl	0.035	08/13/05	0.5147292
20052410037	Ultra CA-1226: 25 µl	0.035	09/13/05	0.1702462
20052510203	Ultra CA-1226: 75 µl	0.035	09/14/05	0.5161461
20052660007	Ultra CA-1226: 25 µl	0.035	10/07/05	0.1727988
20053010004	NSI 080405-01HPLC: 25 µl	0.035	11/17/05	0.1749193

False Positives Listing for 3-HYDROXYCARBOFURAN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20092960006	Crescent 08LL073: 40 µl	0.04	11/19/09	0.003

False Negatives Listing for CARBARYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060580109	NSI 080405-01HPLC: 5 µl	0.018	03/10/06	0.025863
20061030077	Ultra CB-1742: 40 µl	0.018	05/01/06	0.085589

False Positives Listing for BROMOXYNIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20070580108	Protocol F1060804006: 20 µl	0.12	03/12/07	0.001

False Negatives Listing for BROMOXYNIL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062090016	NWQL ABS94077: 25 µl & NWQL ABS94078: 25 µl	0.044	08/09/06	0.0645995

False Positives Listing for ALDICARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060310003	NSI 080405-01HPLC: 25 µl	0.04	02/11/06	0.004

False Negatives Listing for ALDICARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20053500099	Ultra CB-1742: 10 µl	0.04	01/07/06	0.0420722
20062160015	Ultra CB-1742: 40 µl	0.15	08/17/06	0.1625392
20062430019	Ultra CB-1742: 40 µl	0.15	09/12/06	0.1699429
20063180164	Ultra CC-2418: 20 µl	0.04	11/30/06	0.0694349
20080290026	Crescent 07GG007: 50 µl	0.12	02/12/08	0.1480952

False Positives Listing for ALDICARB SULFONE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20051310013	Crescent 07DD034: 50 µl	0.018	07/07/05	0.009
20051460191	Crescent 07DD034: 40 µl	0.018	06/05/05	0.008
20051920137	Crescent 07DD034: 50 µl	0.018	07/22/05	0.007
20052030208	Crescent 07DD034: 40 µl	0.018	08/03/05	0.007
20052340026	Crescent 07DD034: 50 µl	0.018	08/31/05	0.010
20052430284	Crescent 07DD034: 40 µl	0.018	09/14/05	0.008
20052730081	Crescent 07DD034: 40 µl	0.018	10/13/05	0.007
20052900054	Crescent 07DD034: 40 µl	0.018	10/28/05	0.006
20053270023	Crescent 07EE046: 200 µl	0.018	12/14/05	0.004
20061440006	Crescent 07EE046: 200 µl	0.018	06/01/06	0.006
20062010005	Crescent 07EE046: 200 µl	0.018	07/28/06	0.021
20070240002	Ultra CC-2418: 50 µl	0.08	02/09/07	0.006
20070640064	Ultra CC-2418: 50 µl	0.08	03/28/07	0.005
20071150010	Supelco LB40676: 75 µl	0.08	05/11/07	0.007
20071220023	Supelco LB40676: 20 µl	0.08	05/11/07	0.002
20071360138	Ultra CC-2418: 75 µl	0.08	06/02/07	0.008
20071640021	Supelco LB40676: 75 µl	0.08	06/25/07	0.006
20071860003	Ultra CC-2418: 75 µl	0.08	07/25/07	0.008
20092960006	Crescent 08LL073: 40 µl	0.08	11/19/09	0.003
20093380008	NSI 090309-01HPLC: 80 µl	0.08	12/29/09	0.006

False Positives Listing for ALDICARB SULFOXIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20053080009	Ultra CB-1742: 200 µl	0.022	11/17/05	0.094
20060440037	Ultra CB-1742: 40 µl	0.022	03/04/06	0.008
20060620004	Ultra CB-1742: 200 µl	0.1	04/07/06	0.047
20060860012	Ultra CB-1742: 40 µl	0.1	04/05/06	0.017
20061030077	Ultra CB-1742: 40 µl	0.1	05/01/06	0.016
20061320008	Ultra CB-1742: 40 µl	0.1	05/28/06	0.023
20061630088	Ultra CB-1742: 10 µl	0.1	06/16/06	0.005
20061910093	Ultra CB-1742: 200 µl	0.1	07/19/06	0.062
20062160015	Ultra CB-1742: 40 µl	0.1	08/17/06	0.064
20062430019	Ultra CB-1742: 40 µl	0.1	09/12/06	0.039
20062430023	Ultra CB-1742: 200 µl	0.1	09/12/06	0.138
20093100008	Restek A069890: 40 µl	0.06	11/20/09	0.079
20093520062	Spex Organics T1090828008: 40 µl	0.06	12/30/09	0.036
20100920050	Restek A069890: 40 µl	0.06	04/14/10	0.068
20101270033	Spex Organics T1090828008: 40 µl	0.06	05/26/10	0.058
20101410004	Spex Organics T1090828008: 80 µl	0.06	06/11/10	0.082
20101550008	Restek A069890: 80 µl	0.06	06/16/10	0.063
20101760005	Restek A069890: 40 µl	0.06	07/14/10	0.055
20102160005	Spex Organics T1090828008: 80 µl	0.06	08/31/10	0.092
20102320018	Spex Organics T1090828008: 40 µl	0.06	09/02/10	0.038

False Negatives Listing for ALDICARB SULFOXIDE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20063180164	Ultra CC-2418: 20 µl	0.04	11/30/06	0.0518789

False Negatives Listing for ACIFLUORFEN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20103020153	Crescent 163162: 40 µl	0.04	11/30/10	0.0633663

False Negatives Listing for 3-KETOCARBOFURAN

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051310013	Crescent 07DD034: 50 µl	0.02	07/07/05	8.338577
20051460191	Crescent 07DD034: 40 µl	0.02	06/05/05	6.688049
20051610281	Crescent 07DD034: 10 µl	0.02	06/19/05	1.676773
20051810205	Crescent 07DD034: 10 µl	0.02	07/24/05	1.660401
20052030208	Crescent 07DD034: 40 µl	0.02	08/03/05	6.743718
20052200021	Crescent 07DD034: 10 µl	0.02	08/18/05	1.652291
20052590005	Crescent 07DD034: 50 µl	0.02	09/25/05	8.451154
20052730081	Crescent 07DD034: 40 µl	0.02	10/13/05	6.668764
20052900054	Crescent 07DD034: 40 µl	0.02	10/28/05	6.735147
20052970044	Crescent 07EE046: 10 µl	0.02	11/03/05	0.0263964

False Positives Listing for BENDIOCARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20070720033	Accu B6070187: 75 µl	0.04	03/28/07	0.037
20072200099	Accu B6070187: 75 µl	0.04	08/25/07	0.005
20083110007	NSI 081208-01Polar: 50 µl	0.04	11/19/08	0.006
20091550186	NSI 081208-01Polar: 30 µl	0.04	06/17/09	0.002

False Negatives Listing for BENDIOCARB

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051610281	Crescent 07DD034: 10 µl	0.02	06/19/05	0.0263644
20051810205	Crescent 07DD034: 10 µl	0.02	07/24/05	0.0261069
20051920137	Crescent 07DD034: 50 µl	0.02	07/22/05	0.1318844
20052200021	Crescent 07DD034: 10 µl	0.02	08/18/05	0.0259794
20052730081	Crescent 07DD034: 40 µl	0.02	10/13/05	0.1048548
20052900054	Crescent 07DD034: 40 µl	0.02	10/28/05	0.1058985
20053270023	Crescent 07EE046: 200 µl	0.02	12/14/05	0.3136435
20060480013	Crescent 07EE046: 200 µl	0.02	03/04/06	0.3202391
20063180164	Ultra CC-2418: 20 µl	0.04	11/30/06	0.0412269
20080860017	Crescent 07GG007: 50 µl	0.04	04/04/08	0.070373

False Positives Listing for CAFFEINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20092960006	Crescent 08LL073: 40 µl	0.08	11/19/09	0.252

False Negatives Listing for CHLORIMURON ETHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20050240046	NSI 100303HPLC: 100 µl	0.032	01/29/05	0.3670499
20050350094	NSI 100303HPLC: 15 µl	0.032	02/16/05	0.0549387
20050550036	NSI 100303HPLC: 100 µl	0.032	03/08/05	0.3661231
20050760050	NSI 100303HPLC: 15 µl	0.032	04/01/05	0.0549589
20051310013	Crescent 07DD034: 50 µl	0.032	07/07/05	0.2097755
20052200021	Crescent 07DD034: 10 µl	0.032	08/18/05	0.0415671
20053080009	Ultra CB-1742: 200 µl	0.032	11/17/05	0.4304778
20053270023	Crescent 07EE046: 200 µl	0.032	12/14/05	0.2090957
20060170043	Crescent 07EE046: 40 µl	0.032	01/27/06	0.0426894
20060440037	Ultra CB-1742: 40 µl	0.032	03/04/06	0.0838838
20060480013	Crescent 07EE046: 200 µl	0.032	03/04/06	0.2134928
20060620004	Ultra CB-1742: 200 µl	0.032	04/07/06	0.4154981
20060690198	Crescent 07EE046: 40 µl	0.032	04/07/06	0.042328
20060860012	Ultra CB-1742: 40 µl	0.032	04/05/06	0.0845577
20060930014	Crescent 07EE046: 40 µl	0.032	05/01/06	0.0419024
20061030077	Ultra CB-1742: 40 µl	0.032	05/01/06	0.085589
20061320008	Ultra CB-1742: 40 µl	0.032	05/28/06	0.0849527
20061440006	Crescent 07EE046: 200 µl	0.032	06/01/06	0.2134016
20061740222	Crescent 07EE046: 40 µl	0.032	06/27/06	0.0395726
20061910093	Ultra CB-1742: 200 µl	0.032	07/19/06	0.4011634
20062010005	Crescent 07EE046: 200 µl	0.032	07/28/06	0.2025727
20062160015	Ultra CB-1742: 40 µl	0.032	08/17/06	0.0808653
20062330175	Crescent 07EE046: 40 µl	0.032	08/29/06	0.0424133
20062430019	Ultra CB-1742: 40 µl	0.032	09/12/06	0.0845487
20062430023	Ultra CB-1742: 200 µl	0.032	09/12/06	0.424854
20062580007	Crescent 07EE046: 40 µl	0.032	09/22/06	0.0416667

False Negatives Listing for SULFOMETURON METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20053080009	Ultra CB-1742: 200 µl	0.038	11/17/05	0.8652604
20060170043	Crescent 07EE046: 40 µl	0.09	01/27/06	0.1280683
20060440037	Ultra CB-1742: 40 µl	0.09	03/04/06	0.1686065
20060480013	Crescent 07EE046: 200 µl	0.09	03/04/06	0.6404783
20060620004	Ultra CB-1742: 200 µl	0.09	04/07/06	0.8351511
20060860012	Ultra CB-1742: 40 µl	0.09	04/05/06	0.1699609
20061030077	Ultra CB-1742: 40 µl	0.09	05/01/06	0.1720338
20061320008	Ultra CB-1742: 40 µl	0.09	05/28/06	0.170755
20061440006	Crescent 07EE046: 200 µl	0.09	06/01/06	0.6402048
20061740222	Crescent 07EE046: 40 µl	0.09	06/27/06	0.1187178
20061910093	Ultra CB-1742: 200 µl	0.09	07/19/06	0.8063384
20062010005	Crescent 07EE046: 200 µl	0.09	07/28/06	0.607718
20062160015	Ultra CB-1742: 40 µl	0.09	08/17/06	0.1625392
20062330175	Crescent 07EE046: 40 µl	0.09	08/29/06	0.12724
20062430019	Ultra CB-1742: 40 µl	0.09	09/12/06	0.1699429
20062430023	Ultra CB-1742: 200 µl	0.09	09/12/06	0.8539565
20062580007	Crescent 07EE046: 40 µl	0.09	09/22/06	0.125

False Positives Listing for 2-HYDROXYATRAZINE

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20063060004	ChemService 363-120B: 50 µl	0.08	11/13/06	0.013
20063330002	Accu B6070187: 75 µl	0.08	01/09/07	0.007
20070720033	Accu B6070187: 75 µl	0.08	03/28/07	0.009
20070800016	ChemService 363-120B: 50 µl	0.08	04/10/07	0.008
20071500018	Accu B6070187: 50 µl	0.08	06/18/07	0.004
20072200099	Accu B6070187: 75 µl	0.08	08/25/07	0.007
20080800003	Protocol I1070803003: 50 µl	0.04	04/04/08	0.006
20081150079	Protocol I1070803003: 50 µl	0.04	05/16/08	0.002
20081840007	Restek A053251: 50 µl	0.04	07/23/08	0.011
20082130006	Protocol I1070803003: 50 µl	0.04	08/14/08	0.015
20082260236	Restek A053251: 50 µl	0.04	08/28/08	0.037
20091320004	ERA 0813-08-07Polar: 30 µl	0.06	05/28/09	0.011
20092040200	ERA 0813-08-07Polar: 30 µl	0.06	08/06/09	0.014
20092460256	ERA 0813-08-07Polar: 50 µl	0.06	09/22/09	0.018
20101340151	Accu 209081166: 80 µl	0.06	06/10/10	0.006
20101650030	ChemService 430-40B: 40 µl	0.06	06/30/10	0.004
20102180094	ChemService 430-40B: 80 µl	0.06	08/31/10	0.009
20102530004	ChemService 430-40B: 80 µl	0.06	10/27/10	0.078
20103510059	Restek A075600: 40 µl	0.06	01/04/11	0.036

False Positives Listing for METALAXYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20053460080	Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl	0.012	01/07/06	0.060

False Negatives Listing for NICOSULFURON

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062370005	NSI 080405-01HPLC: 25 µl	0.04	09/06/06	0.1575796
20073110114	Accu B7070230: 50 µl	0.1	11/28/07	0.1481026
20080150157	Accu B7070230: 50 µl	0.1	02/12/08	0.1480267
20080370106	Abs 071607LC: 50 µl	0.1	02/12/08	0.1481294
20080740019	Accu B7070230: 50 µl	0.1	04/04/08	0.1472568
20080870100	Abs 071607LC: 50 µl	0.1	04/04/08	0.1477857
20081290004	Abs 071607LC: 50 µl	0.1	05/16/08	0.1456552
20081500007	Accu B7070230: 50 µl	0.1	06/19/08	0.1469122
20081780159	Abs 071607LC: 50 µl	0.1	07/09/08	0.1446771
20082000011	Accu B7070230: 50 µl	0.1	07/30/08	0.1412778
20082350002	Abs 071607LC: 50 µl	0.1	09/09/08	0.1452797
20082480185	Accu B7070230: 50 µl	0.1	09/25/08	0.1418328
20082560003	Accu B7070230: 50 µl	0.1	09/25/08	0.1423782

False Positives Listing for 2,4-D METHYL ESTER

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20051190007	Ultra CA-1226: 25 µl	0.016	05/06/05	0.022
20051540207	Ultra CA-1226: 75 µl	0.016	06/11/05	0.033
20051680024	Ultra CA-1226: 25 µl	0.016	08/01/05	0.020
20051940296	Ultra CA-1226: 25 µl	0.016	07/22/05	0.012
20052080326	Ultra CA-1226: 75 µl	0.016	08/13/05	0.028
20052510203	Ultra CA-1226: 75 µl	0.016	09/14/05	0.032
20052660007	Ultra CA-1226: 25 µl	0.016	10/07/05	0.027
20061250009	NSI 080405-01HPLC: 75 µl	0.19	05/27/06	0.050
20062630097	NSI 080405-01HPLC: 75 µl	0.2	10/03/06	0.044
20101720152	NSI 090309-01HPLC: 80 µl	0.2	07/01/10	0.040
20101830111	NWQL LCL11SP079A: 50 µl & NWQL LCL11SP079B: 50 µl	0.2	07/27/10	0.005

False Negatives Listing for 2,4-D METHYL ESTER

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051610281	Crescent 07DD034: 10 µl	0.016	06/19/05	0.042183
20052200021	Crescent 07DD034: 10 µl	0.016	08/18/05	0.0415671
20052730081	Crescent 07DD034: 40 µl	0.016	10/13/05	0.1677676
20052900054	Crescent 07DD034: 40 µl	0.016	10/28/05	0.1694377
20052970044	Crescent 07EE046: 10 µl	0.016	11/03/05	0.0211171
20053270023	Crescent 07EE046: 200 µl	0.016	12/14/05	0.4181913
20053500099	Ultra CB-1742: 10 µl	0.016	01/07/06	0.0209314
20060440037	Ultra CB-1742: 40 µl	0.016	03/04/06	0.0838838
20060480013	Crescent 07EE046: 200 µl	0.016	03/04/06	0.4269855
20073380128	Abs 071607LC: 50 µl	0.04	01/03/08	0.319

False Negatives Listing for PROPICONAZOLE (TILT)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062160015	Ultra CB-1742: 40 µl	0.01	08/17/06	0.0808653

False Positives Listing for CHLORAMBEN, METHYL ESTER

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20093380008	NSI 090309-01HPLC: 80 µl	0.1	12/29/09	0.019
20101340151	Accu 209081166: 80 µl	0.1	06/10/10	0.062

False Negatives Listing for CHLORAMBEN, METHYL ESTER

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20060580109	NSI 080405-01HPLC: 5 µl	0.024	03/10/06	0.0274464
20061030077	Ultra CB-1742: 40 µl	0.024	05/01/06	0.085589
20061320008	Ultra CB-1742: 40 µl	0.024	05/28/06	0.0849527
20062090018	NSI 080405-01HPLC: 75 µl	0.024	08/09/06	0.4037267
20062160015	Ultra CB-1742: 40 µl	0.024	08/17/06	0.0808653
20073380128	Abs 071607LC: 50 µl	0.1	01/03/08	0.341
20080150157	Accu B7070230: 50 µl	0.1	02/12/08	0.3474628
20080740019	Accu B7070230: 50 µl	0.1	04/04/08	0.3456557
20080870100	Abs 071607LC: 50 µl	0.1	04/04/08	0.3439927
20081290004	Abs 071607LC: 50 µl	0.1	05/16/08	0.3390336
20081500007	Accu B7070230: 50 µl	0.1	06/19/08	0.3448469
20083040065	ChemService 406-113B: 50 µl	0.1	11/19/08	0.5393643
20083440101	Abs 081508Polar: 30 µl	0.1	12/30/08	0.3344064
20091060131	Abs 081508Polar: 30 µl	0.1	04/30/09	0.3347432
20091410005	ChemService 406-113B: 50 µl	0.1	06/17/09	0.5507839
20091830170	Abs 081508Polar: 30 µl	0.1	07/28/09	0.330155
20092530081	ChemService 406-113B: 30 µl	0.1	09/23/09	0.329352
20093100008	Restek A069890: 40 µl	0.1	11/20/09	0.1842234
20100920050	Restek A069890: 40 µl	0.1	04/14/10	0.1880564
20101270033	Spex Organics T1090828008: 40 µl	0.1	05/26/10	0.1907467
20101550008	Restek A069890: 80 µl	0.1	06/16/10	0.3845367
20101760005	Restek A069890: 40 µl	0.1	07/14/10	0.1879248
20103430088	ChemService 448-45B: 40 µl	0.1	01/04/11	0.1450068

False Negatives Listing for 3(4-CHLOROPHENYL) METHYL UREA

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20063180164	Ultra CC-2418: 20 µl	0.06	11/30/06	0.0678568

False Negatives Listing for BENSULFURON-METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20082350002	Abs 071607LC: 50 µl	0.06	09/09/08	0.0837961

False Positives Listing for FLUMETSULAM

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20060030004	Absolute 091202HPLC: 10 µl & Absolute 090902: 10 µl	0.04	01/09/06	0.003
20061000002	NSI 080405-01HPLC: 25 µl	0.04	05/01/06	0.007

False Negatives Listing for FLUMETSULAM

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20062330175	Crescent 07EE046: 40 µl	0.04	08/29/06	0.1060333
20072900076	Abs 071607LC: 50 µl	0.06	11/06/07	0.1760281
20092530081	ChemService 406-113B: 30 µl	0.06	09/23/09	0.0797253

False Negatives Listing for IMIDACLOPRID

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20061180198	Crescent 07EE046: 10 µl	0.02	05/10/06	0.0208855
20080740019	Accu B7070230: 50 µl	0.06	04/04/08	0.1473078
20082350002	Abs 071607LC: 50 µl	0.06	09/09/08	0.1428005

False Negatives Listing for METSULFURON METHYL

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20051190007	Ultra CA-1226: 25 µl	0.025	05/06/05	0.1947647
20051680024	Ultra CA-1226: 25 µl	0.025	08/01/05	0.1963351
20052660007	Ultra CA-1226: 25 µl	0.025	10/07/05	0.1993832
20101410004	Spex Organics T1090828008: 80 µl	0.14	06/11/10	0.4379853

False Positives Listing for 2,4-D + 2,4-D METHYL ESTER (SUM)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Result Conc.
20103020153	Crescent 163162: 40 µl	0.06	11/29/10	0.447
20103510059	Restek A075600: 40 µl	0.06	01/04/11	0.448

False Negatives Listing for 2,4-D + 2,4-D METHYL ESTER (SUM)

Lab ID	Spike Mix	Reporting Level	Analysis Date	Expected Conc.
20073380128	Abs 071607LC: 50 µl	0.02	01/03/08	0.5205