BQS OBSP Determination:
TERBUTHYLAZINE
METHOD: 2033 , TESTIDCODE: 04022GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 105% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 81% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 88% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 95% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 98% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 82% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 109% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 99% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 74% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 75% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 88% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 77% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 75% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 92% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 104% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 83% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 86% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 97% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Expected Conc. = 0.05 Median Pct Recovery = 86% Expected Conc. = 0.048 Median Pct Recovery = 86% Expected Conc. = 0.048 Median Pct Recovery = 86% Expected Conc. = 0.048 Median Pct Recovery = 86% Expected Conc. = 0.048 Median Pct Recovery = 86% Expected Conc. = 0.0414 Median Pct Recovery = 86% Expected Conc. = 0.0414 Median Pct Recovery = 86% Expected Conc. = 0.0312 Median Pct Recovery = 86% Expected Conc. = 0.0312 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.024 Median Pct Recovery = 86% Expected Conc. = 0.0207 Median Pct Recovery = 86% Expected Conc. = 0.0207 Median Pct Recovery = 86% Expected Conc. = 0.0207 Median Pct Recovery = 86% Expected Conc. = 0.0207 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.02 Median Pct Recovery = 86% Expected Conc. = 0.0159 Median Pct Recovery = 86% Expected Conc. = 0.0159 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Expected Conc. = 0.012 Median Pct Recovery = 86% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
HEXAZINONE
METHOD: 2033 , TESTIDCODE: 04025GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 77% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 29% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 64% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 19% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 56% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 48% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 60% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 89% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 68% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 61% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 63% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 90% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 63% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 147% Expected Conc. = 0.075 Median Pct Recovery = 65% Expected Conc. = 0.0725 Median Pct Recovery = 65% Expected Conc. = 0.0725 Median Pct Recovery = 65% Expected Conc. = 0.0725 Median Pct Recovery = 65% Expected Conc. = 0.0725 Median Pct Recovery = 65% Expected Conc. = 0.0597 Median Pct Recovery = 65% Expected Conc. = 0.0597 Median Pct Recovery = 65% Expected Conc. = 0.048 Median Pct Recovery = 65% Expected Conc. = 0.048 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.0362 Median Pct Recovery = 65% Expected Conc. = 0.036 Median Pct Recovery = 65% Expected Conc. = 0.036 Median Pct Recovery = 65% Expected Conc. = 0.036 Median Pct Recovery = 65% Expected Conc. = 0.036 Median Pct Recovery = 65% Expected Conc. = 0.036 Median Pct Recovery = 65% Expected Conc. = 0.036 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.03 Median Pct Recovery = 65% Expected Conc. = 0.0298 Median Pct Recovery = 65% Expected Conc. = 0.0298 Median Pct Recovery = 65% Expected Conc. = 0.0298 Median Pct Recovery = 65% Expected Conc. = 0.0298 Median Pct Recovery = 65% Expected Conc. = 0.024 Median Pct Recovery = 65% Expected Conc. = 0.024 Median Pct Recovery = 65% Expected Conc. = 0.0181 Median Pct Recovery = 65% Expected Conc. = 0.0181 Median Pct Recovery = 65% Expected Conc. = 0.0181 Median Pct Recovery = 65% Expected Conc. = 0.0181 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Expected Conc. = 0.018 Median Pct Recovery = 65% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
SIMAZINE
METHOD: 2033 , TESTIDCODE: 04035GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 111% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 96% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 84% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 68% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 104% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 87% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 86% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 118% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 85% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 118% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 100% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 101% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 76% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 93% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 92% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 113% Expected Conc. = 0.04 Median Pct Recovery = 93% Expected Conc. = 0.036 Median Pct Recovery = 93% Expected Conc. = 0.036 Median Pct Recovery = 93% Expected Conc. = 0.036 Median Pct Recovery = 93% Expected Conc. = 0.036 Median Pct Recovery = 93% Expected Conc. = 0.032 Median Pct Recovery = 93% Expected Conc. = 0.032 Median Pct Recovery = 93% Expected Conc. = 0.03 Median Pct Recovery = 93% Expected Conc. = 0.03 Median Pct Recovery = 93% Expected Conc. = 0.024 Median Pct Recovery = 93% Expected Conc. = 0.024 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.018 Median Pct Recovery = 93% Expected Conc. = 0.016 Median Pct Recovery = 93% Expected Conc. = 0.016 Median Pct Recovery = 93% Expected Conc. = 0.015 Median Pct Recovery = 93% Expected Conc. = 0.015 Median Pct Recovery = 93% Expected Conc. = 0.015 Median Pct Recovery = 93% Expected Conc. = 0.015 Median Pct Recovery = 93% Expected Conc. = 0.0121 Median Pct Recovery = 93% Expected Conc. = 0.0121 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Expected Conc. = 0.009 Median Pct Recovery = 93% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PROMETRYN
METHOD: 2033 , TESTIDCODE: 04036GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 122% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 15% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 54% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 94% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 70% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 84% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 31% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 28% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 65% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 75% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 78% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 73% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 85% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 19% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Expected Conc. = 0.06 Median Pct Recovery = 76% Expected Conc. = 0.06 Median Pct Recovery = 76% Expected Conc. = 0.06 Median Pct Recovery = 76% Expected Conc. = 0.06 Median Pct Recovery = 76% Expected Conc. = 0.06 Median Pct Recovery = 76% Expected Conc. = 0.05 Median Pct Recovery = 76% Expected Conc. = 0.05 Median Pct Recovery = 76% Expected Conc. = 0.048 Median Pct Recovery = 76% Expected Conc. = 0.048 Median Pct Recovery = 76% Expected Conc. = 0.0402 Median Pct Recovery = 76% Expected Conc. = 0.0402 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.03 Median Pct Recovery = 76% Expected Conc. = 0.025 Median Pct Recovery = 76% Expected Conc. = 0.025 Median Pct Recovery = 76% Expected Conc. = 0.025 Median Pct Recovery = 76% Expected Conc. = 0.025 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.0201 Median Pct Recovery = 76% Expected Conc. = 0.0201 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Expected Conc. = 0.015 Median Pct Recovery = 76% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PROMETON
METHOD: 2033 , TESTIDCODE: 04037GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 72% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 75% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 50% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 77% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 49% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 106% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 75% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 74% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 54% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 55% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 110% Expected Conc. = 0.0728 Median Pct Recovery = 74% Expected Conc. = 0.0728 Median Pct Recovery = 74% Expected Conc. = 0.0728 Median Pct Recovery = 74% Expected Conc. = 0.06 Median Pct Recovery = 74% Expected Conc. = 0.06 Median Pct Recovery = 74% Expected Conc. = 0.048 Median Pct Recovery = 74% Expected Conc. = 0.048 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.0364 Median Pct Recovery = 74% Expected Conc. = 0.036 Median Pct Recovery = 74% Expected Conc. = 0.036 Median Pct Recovery = 74% Expected Conc. = 0.036 Median Pct Recovery = 74% Expected Conc. = 0.036 Median Pct Recovery = 74% Expected Conc. = 0.036 Median Pct Recovery = 74% Expected Conc. = 0.036 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.03 Median Pct Recovery = 74% Expected Conc. = 0.024 Median Pct Recovery = 74% Expected Conc. = 0.024 Median Pct Recovery = 74% Expected Conc. = 0.0182 Median Pct Recovery = 74% Expected Conc. = 0.0182 Median Pct Recovery = 74% Expected Conc. = 0.0182 Median Pct Recovery = 74% Expected Conc. = 0.0182 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Expected Conc. = 0.018 Median Pct Recovery = 74% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DEETHYLATRAZINE
METHOD: 2033 , TESTIDCODE: 04040GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 52% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 33% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 38% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 50% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 33% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 16% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 47% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 44% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 50% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 51% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 50% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 58% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 62% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 55% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 64% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 61% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 54% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 69% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 64% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 73% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.05 Median Pct Recovery = 53% Expected Conc. = 0.05 Median Pct Recovery = 53% Expected Conc. = 0.048 Median Pct Recovery = 53% Expected Conc. = 0.048 Median Pct Recovery = 53% Expected Conc. = 0.0402 Median Pct Recovery = 53% Expected Conc. = 0.0402 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.03 Median Pct Recovery = 53% Expected Conc. = 0.025 Median Pct Recovery = 53% Expected Conc. = 0.025 Median Pct Recovery = 53% Expected Conc. = 0.025 Median Pct Recovery = 53% Expected Conc. = 0.025 Median Pct Recovery = 53% Expected Conc. = 0.024 Median Pct Recovery = 53% Expected Conc. = 0.024 Median Pct Recovery = 53% Expected Conc. = 0.0201 Median Pct Recovery = 53% Expected Conc. = 0.0201 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Expected Conc. = 0.015 Median Pct Recovery = 53% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CYANAZINE
METHOD: 2033 , TESTIDCODE: 04041GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 23% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 77% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 25% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 96% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 67% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 78% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 92% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 107% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 49% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 76% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 129% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 102% Expected Conc. = 0.132 Median Pct Recovery = 76% Expected Conc. = 0.132 Median Pct Recovery = 76% Expected Conc. = 0.132 Median Pct Recovery = 76% Expected Conc. = 0.1136 Median Pct Recovery = 76% Expected Conc. = 0.1136 Median Pct Recovery = 76% Expected Conc. = 0.0876 Median Pct Recovery = 76% Expected Conc. = 0.0876 Median Pct Recovery = 76% Expected Conc. = 0.068 Median Pct Recovery = 76% Expected Conc. = 0.068 Median Pct Recovery = 76% Expected Conc. = 0.068 Median Pct Recovery = 76% Expected Conc. = 0.068 Median Pct Recovery = 76% Expected Conc. = 0.068 Median Pct Recovery = 76% Expected Conc. = 0.068 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.066 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0568 Median Pct Recovery = 76% Expected Conc. = 0.0556 Median Pct Recovery = 76% Expected Conc. = 0.0556 Median Pct Recovery = 76% Expected Conc. = 0.0442 Median Pct Recovery = 76% Expected Conc. = 0.0442 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.034 Median Pct Recovery = 76% Expected Conc. = 0.033 Median Pct Recovery = 76% Expected Conc. = 0.033 Median Pct Recovery = 76% Expected Conc. = 0.033 Median Pct Recovery = 76% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FONOFOS
METHOD: 2033 , TESTIDCODE: 04095GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 55% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 51% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 59% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 78% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 82% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 77% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 84% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 84% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 71% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 32% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 72% Expected Conc. = 0.0295 Median Pct Recovery = 77% Expected Conc. = 0.0295 Median Pct Recovery = 77% Expected Conc. = 0.0295 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.0192 Median Pct Recovery = 77% Expected Conc. = 0.0192 Median Pct Recovery = 77% Expected Conc. = 0.016 Median Pct Recovery = 77% Expected Conc. = 0.016 Median Pct Recovery = 77% Expected Conc. = 0.016 Median Pct Recovery = 77% Expected Conc. = 0.016 Median Pct Recovery = 77% Expected Conc. = 0.016 Median Pct Recovery = 77% Expected Conc. = 0.016 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.0148 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.012 Median Pct Recovery = 77% Expected Conc. = 0.0096 Median Pct Recovery = 77% Expected Conc. = 0.0096 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.008 Median Pct Recovery = 77% Expected Conc. = 0.0074 Median Pct Recovery = 77% Expected Conc. = 0.0074 Median Pct Recovery = 77% Expected Conc. = 0.0074 Median Pct Recovery = 77% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ALPHA-ENDOSULFAN (ENDOSULFAN I)
METHOD: 2033 , TESTIDCODE: 34362GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 108% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 66% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 68% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 115% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 79% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 108% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 105% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 83% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 64% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 91% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 92% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 86% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 74% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 94% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 92% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 102% Expected Conc. = 0.063 Median Pct Recovery = 89% Expected Conc. = 0.05 Median Pct Recovery = 89% Expected Conc. = 0.05 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.025 Median Pct Recovery = 89% Expected Conc. = 0.025 Median Pct Recovery = 89% Expected Conc. = 0.025 Median Pct Recovery = 89% Expected Conc. = 0.025 Median Pct Recovery = 89% Expected Conc. = 0.024 Median Pct Recovery = 89% Expected Conc. = 0.024 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.012 Median Pct Recovery = 89% Expected Conc. = 0.012 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DICROTOPHOS
METHOD: 2033 , TESTIDCODE: 38454GCM39
DATES: 03/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 19% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 25% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 21% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 2% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 14% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 13% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 10% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 9% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 17% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 24% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 14% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 12% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 11% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 10% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 33% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 44% Expected Conc. = 0.502 Median Pct Recovery = 14% Expected Conc. = 0.4792 Median Pct Recovery = 14% Expected Conc. = 0.4792 Median Pct Recovery = 14% Expected Conc. = 0.4016 Median Pct Recovery = 14% Expected Conc. = 0.4016 Median Pct Recovery = 14% Expected Conc. = 0.3216 Median Pct Recovery = 14% Expected Conc. = 0.3216 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2396 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.2008 Median Pct Recovery = 14% Expected Conc. = 0.1198 Median Pct Recovery = 14% Expected Conc. = 0.1198 Median Pct Recovery = 14% Expected Conc. = 0.1198 Median Pct Recovery = 14% Expected Conc. = 0.1198 Median Pct Recovery = 14% Expected Conc. = 0.4792 Median Pct Recovery = 14% Expected Conc. = 0.4792 Median Pct Recovery = 14% Expected Conc. = 0.3192 Median Pct Recovery = 14% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DICHLOROVOS (DICHLORVOS)
METHOD: 2033 , TESTIDCODE: 38775GCM39
DATES: 02/21/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 47% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 48% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 26% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 41% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 54% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 75% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 26% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 37% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 40% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 45% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 43% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 23% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 18% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 33% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 30% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 18% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 33% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 25% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 40% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 42% Expected Conc. = 0.24 Median Pct Recovery = 41% Expected Conc. = 0.24 Median Pct Recovery = 41% Expected Conc. = 0.24 Median Pct Recovery = 41% Expected Conc. = 0.2 Median Pct Recovery = 41% Expected Conc. = 0.2 Median Pct Recovery = 41% Expected Conc. = 0.1602 Median Pct Recovery = 41% Expected Conc. = 0.1602 Median Pct Recovery = 41% Expected Conc. = 0.1578 Median Pct Recovery = 41% Expected Conc. = 0.1578 Median Pct Recovery = 41% Expected Conc. = 0.1208 Median Pct Recovery = 41% Expected Conc. = 0.1208 Median Pct Recovery = 41% Expected Conc. = 0.1208 Median Pct Recovery = 41% Expected Conc. = 0.1208 Median Pct Recovery = 41% Expected Conc. = 0.1208 Median Pct Recovery = 41% Expected Conc. = 0.1208 Median Pct Recovery = 41% Expected Conc. = 0.12 Median Pct Recovery = 41% Expected Conc. = 0.12 Median Pct Recovery = 41% Expected Conc. = 0.12 Median Pct Recovery = 41% Expected Conc. = 0.12 Median Pct Recovery = 41% Expected Conc. = 0.1004 Median Pct Recovery = 41% Expected Conc. = 0.1004 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.1 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.0604 Median Pct Recovery = 41% Expected Conc. = 0.06 Median Pct Recovery = 41% Expected Conc. = 0.06 Median Pct Recovery = 41% Expected Conc. = 0.06 Median Pct Recovery = 41% Expected Conc. = 0.06 Median Pct Recovery = 41% Expected Conc. = 0.06 Median Pct Recovery = 41% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CHLORPYRIFOS
METHOD: 2033 , TESTIDCODE: 38933GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 75% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 69% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 133% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 101% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 65% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 53% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 96% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 87% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 79% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 76% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 61% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 78% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 60% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 86% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 102% Expected Conc. = 0.0601 Median Pct Recovery = 75% Expected Conc. = 0.0601 Median Pct Recovery = 75% Expected Conc. = 0.0601 Median Pct Recovery = 75% Expected Conc. = 0.06 Median Pct Recovery = 75% Expected Conc. = 0.06 Median Pct Recovery = 75% Expected Conc. = 0.05 Median Pct Recovery = 75% Expected Conc. = 0.05 Median Pct Recovery = 75% Expected Conc. = 0.048 Median Pct Recovery = 75% Expected Conc. = 0.048 Median Pct Recovery = 75% Expected Conc. = 0.0402 Median Pct Recovery = 75% Expected Conc. = 0.0402 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.03 Median Pct Recovery = 75% Expected Conc. = 0.028 Median Pct Recovery = 75% Expected Conc. = 0.028 Median Pct Recovery = 75% Expected Conc. = 0.028 Median Pct Recovery = 75% Expected Conc. = 0.028 Median Pct Recovery = 75% Expected Conc. = 0.028 Median Pct Recovery = 75% Expected Conc. = 0.028 Median Pct Recovery = 75% Expected Conc. = 0.025 Median Pct Recovery = 75% Expected Conc. = 0.025 Median Pct Recovery = 75% Expected Conc. = 0.025 Median Pct Recovery = 75% Expected Conc. = 0.025 Median Pct Recovery = 75% Expected Conc. = 0.024 Median Pct Recovery = 75% Expected Conc. = 0.024 Median Pct Recovery = 75% Expected Conc. = 0.0201 Median Pct Recovery = 75% Expected Conc. = 0.0201 Median Pct Recovery = 75% Expected Conc. = 0.015 Median Pct Recovery = 75% Expected Conc. = 0.015 Median Pct Recovery = 75% Expected Conc. = 0.015 Median Pct Recovery = 75% Expected Conc. = 0.015 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Expected Conc. = 0.014 Median Pct Recovery = 75% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DIELDRIN
METHOD: 2033 , TESTIDCODE: 39381GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 72% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 55% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 106% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 116% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 67% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 80% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 108% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 90% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 87% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Expected Conc. = 0.074 Median Pct Recovery = 84% Expected Conc. = 0.0592 Median Pct Recovery = 84% Expected Conc. = 0.0592 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.0312 Median Pct Recovery = 84% Expected Conc. = 0.0312 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.0296 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.016 Median Pct Recovery = 84% Expected Conc. = 0.016 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
METOLACHLOR
METHOD: 2033 , TESTIDCODE: 39415GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 116% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 78% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 89% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 69% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 82% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 76% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 70% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 85% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 88% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 90% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 88% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 92% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 81% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 84% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 86% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 73% Expected Conc. = 0.074 Median Pct Recovery = 82% Expected Conc. = 0.0728 Median Pct Recovery = 82% Expected Conc. = 0.0728 Median Pct Recovery = 82% Expected Conc. = 0.0728 Median Pct Recovery = 82% Expected Conc. = 0.0728 Median Pct Recovery = 82% Expected Conc. = 0.0611 Median Pct Recovery = 82% Expected Conc. = 0.0611 Median Pct Recovery = 82% Expected Conc. = 0.048 Median Pct Recovery = 82% Expected Conc. = 0.048 Median Pct Recovery = 82% Expected Conc. = 0.0364 Median Pct Recovery = 82% Expected Conc. = 0.0364 Median Pct Recovery = 82% Expected Conc. = 0.0364 Median Pct Recovery = 82% Expected Conc. = 0.0364 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.036 Median Pct Recovery = 82% Expected Conc. = 0.0306 Median Pct Recovery = 82% Expected Conc. = 0.0306 Median Pct Recovery = 82% Expected Conc. = 0.0306 Median Pct Recovery = 82% Expected Conc. = 0.0306 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.0296 Median Pct Recovery = 82% Expected Conc. = 0.024 Median Pct Recovery = 82% Expected Conc. = 0.024 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.0182 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Expected Conc. = 0.018 Median Pct Recovery = 82% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
MALATHION
METHOD: 2033 , TESTIDCODE: 39532GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 77% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 71% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 105% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 73% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 99% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 91% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 91% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 78% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 107% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 59% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 119% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 114% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 100% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 156% Expected Conc. = 0.099 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.08 Median Pct Recovery = 91% Expected Conc. = 0.08 Median Pct Recovery = 91% Expected Conc. = 0.066 Median Pct Recovery = 91% Expected Conc. = 0.066 Median Pct Recovery = 91% Expected Conc. = 0.0484 Median Pct Recovery = 91% Expected Conc. = 0.0484 Median Pct Recovery = 91% Expected Conc. = 0.0484 Median Pct Recovery = 91% Expected Conc. = 0.0484 Median Pct Recovery = 91% Expected Conc. = 0.0484 Median Pct Recovery = 91% Expected Conc. = 0.0484 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.04 Median Pct Recovery = 91% Expected Conc. = 0.04 Median Pct Recovery = 91% Expected Conc. = 0.04 Median Pct Recovery = 91% Expected Conc. = 0.04 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0396 Median Pct Recovery = 91% Expected Conc. = 0.0324 Median Pct Recovery = 91% Expected Conc. = 0.0324 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Expected Conc. = 0.0242 Median Pct Recovery = 91% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DIAZINON
METHOD: 2033 , TESTIDCODE: 39572GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 72% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 76% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 80% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 92% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 74% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 81% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 99% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 95% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 111% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 96% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 91% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 82% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 100% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 108% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 106% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 78% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 103% Expected Conc. = 0.038 Median Pct Recovery = 94% Expected Conc. = 0.036 Median Pct Recovery = 94% Expected Conc. = 0.036 Median Pct Recovery = 94% Expected Conc. = 0.036 Median Pct Recovery = 94% Expected Conc. = 0.036 Median Pct Recovery = 94% Expected Conc. = 0.03 Median Pct Recovery = 94% Expected Conc. = 0.03 Median Pct Recovery = 94% Expected Conc. = 0.024 Median Pct Recovery = 94% Expected Conc. = 0.024 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.018 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.0152 Median Pct Recovery = 94% Expected Conc. = 0.015 Median Pct Recovery = 94% Expected Conc. = 0.015 Median Pct Recovery = 94% Expected Conc. = 0.015 Median Pct Recovery = 94% Expected Conc. = 0.015 Median Pct Recovery = 94% Expected Conc. = 0.012 Median Pct Recovery = 94% Expected Conc. = 0.012 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Expected Conc. = 0.009 Median Pct Recovery = 94% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ATRAZINE
METHOD: 2033 , TESTIDCODE: 39632GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 80% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 94% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 99% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 106% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 88% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 78% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 82% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 98% Expected Conc. = 0.0484 Median Pct Recovery = 84% Expected Conc. = 0.0484 Median Pct Recovery = 84% Expected Conc. = 0.0484 Median Pct Recovery = 84% Expected Conc. = 0.04 Median Pct Recovery = 84% Expected Conc. = 0.04 Median Pct Recovery = 84% Expected Conc. = 0.0312 Median Pct Recovery = 84% Expected Conc. = 0.0312 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.0242 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.02 Median Pct Recovery = 84% Expected Conc. = 0.016 Median Pct Recovery = 84% Expected Conc. = 0.016 Median Pct Recovery = 84% Expected Conc. = 0.0121 Median Pct Recovery = 84% Expected Conc. = 0.0121 Median Pct Recovery = 84% Expected Conc. = 0.0121 Median Pct Recovery = 84% Expected Conc. = 0.0121 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Expected Conc. = 0.012 Median Pct Recovery = 84% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ALACHLOR
METHOD: 2033 , TESTIDCODE: 46342GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 77% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 93% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 99% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 87% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 100% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 83% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 106% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 104% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 124% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 105% Expected Conc. = 0.048 Median Pct Recovery = 92% Expected Conc. = 0.048 Median Pct Recovery = 92% Expected Conc. = 0.048 Median Pct Recovery = 92% Expected Conc. = 0.04 Median Pct Recovery = 92% Expected Conc. = 0.04 Median Pct Recovery = 92% Expected Conc. = 0.0318 Median Pct Recovery = 92% Expected Conc. = 0.0318 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.02 Median Pct Recovery = 92% Expected Conc. = 0.016 Median Pct Recovery = 92% Expected Conc. = 0.016 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Expected Conc. = 0.012 Median Pct Recovery = 92% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ACETOCHLOR
METHOD: 2033 , TESTIDCODE: 49260GCM33
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 78% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 84% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 110% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 74% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 100% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 88% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 83% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 101% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 87% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 98% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 83% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 100% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 105% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 135% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 99% Expected Conc. = 0.063 Median Pct Recovery = 86% Expected Conc. = 0.06 Median Pct Recovery = 86% Expected Conc. = 0.06 Median Pct Recovery = 86% Expected Conc. = 0.06 Median Pct Recovery = 86% Expected Conc. = 0.06 Median Pct Recovery = 86% Expected Conc. = 0.0493 Median Pct Recovery = 86% Expected Conc. = 0.0493 Median Pct Recovery = 86% Expected Conc. = 0.0396 Median Pct Recovery = 86% Expected Conc. = 0.0396 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.03 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0252 Median Pct Recovery = 86% Expected Conc. = 0.0246 Median Pct Recovery = 86% Expected Conc. = 0.0246 Median Pct Recovery = 86% Expected Conc. = 0.0246 Median Pct Recovery = 86% Expected Conc. = 0.0246 Median Pct Recovery = 86% Expected Conc. = 0.0201 Median Pct Recovery = 86% Expected Conc. = 0.0201 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Expected Conc. = 0.015 Median Pct Recovery = 86% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
1-NAPHTHOL
METHOD: 2033 , TESTIDCODE: 49295GCM39
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 65% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 24% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 37% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 56% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 13% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 15% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 25% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 38% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 42% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 29% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 62% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 49% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 62% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 55% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 71% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 33% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 33% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 13% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 36% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 24% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 36% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 19% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 39% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 40% Expected Conc. = 0.313 Median Pct Recovery = 37% Expected Conc. = 0.3 Median Pct Recovery = 37% Expected Conc. = 0.3 Median Pct Recovery = 37% Expected Conc. = 0.3 Median Pct Recovery = 37% Expected Conc. = 0.3 Median Pct Recovery = 37% Expected Conc. = 0.2512 Median Pct Recovery = 37% Expected Conc. = 0.2512 Median Pct Recovery = 37% Expected Conc. = 0.1998 Median Pct Recovery = 37% Expected Conc. = 0.1998 Median Pct Recovery = 37% Expected Conc. = 0.1992 Median Pct Recovery = 37% Expected Conc. = 0.1992 Median Pct Recovery = 37% Expected Conc. = 0.15 Median Pct Recovery = 37% Expected Conc. = 0.15 Median Pct Recovery = 37% Expected Conc. = 0.15 Median Pct Recovery = 37% Expected Conc. = 0.15 Median Pct Recovery = 37% Expected Conc. = 0.1484 Median Pct Recovery = 37% Expected Conc. = 0.1484 Median Pct Recovery = 37% Expected Conc. = 0.1484 Median Pct Recovery = 37% Expected Conc. = 0.1484 Median Pct Recovery = 37% Expected Conc. = 0.1484 Median Pct Recovery = 37% Expected Conc. = 0.1484 Median Pct Recovery = 37% Expected Conc. = 0.1256 Median Pct Recovery = 37% Expected Conc. = 0.1256 Median Pct Recovery = 37% Expected Conc. = 0.1256 Median Pct Recovery = 37% Expected Conc. = 0.1256 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.1252 Median Pct Recovery = 37% Expected Conc. = 0.075 Median Pct Recovery = 37% Expected Conc. = 0.075 Median Pct Recovery = 37% Expected Conc. = 0.075 Median Pct Recovery = 37% Expected Conc. = 0.075 Median Pct Recovery = 37% Expected Conc. = 0.075 Median Pct Recovery = 37% Expected Conc. = 0.075 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Expected Conc. = 0.0742 Median Pct Recovery = 37% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CYFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61585GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 89% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 61% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 89% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 80% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 39% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 85% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 67% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 109% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 32% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 26% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Expected Conc. = 0.1 Median Pct Recovery = 73% Expected Conc. = 0.096 Median Pct Recovery = 73% Expected Conc. = 0.096 Median Pct Recovery = 73% Expected Conc. = 0.096 Median Pct Recovery = 73% Expected Conc. = 0.096 Median Pct Recovery = 73% Expected Conc. = 0.0836 Median Pct Recovery = 73% Expected Conc. = 0.0836 Median Pct Recovery = 73% Expected Conc. = 0.08 Median Pct Recovery = 73% Expected Conc. = 0.08 Median Pct Recovery = 73% Expected Conc. = 0.066 Median Pct Recovery = 73% Expected Conc. = 0.066 Median Pct Recovery = 73% Expected Conc. = 0.0484 Median Pct Recovery = 73% Expected Conc. = 0.0484 Median Pct Recovery = 73% Expected Conc. = 0.048 Median Pct Recovery = 73% Expected Conc. = 0.048 Median Pct Recovery = 73% Expected Conc. = 0.048 Median Pct Recovery = 73% Expected Conc. = 0.048 Median Pct Recovery = 73% Expected Conc. = 0.0418 Median Pct Recovery = 73% Expected Conc. = 0.0418 Median Pct Recovery = 73% Expected Conc. = 0.0418 Median Pct Recovery = 73% Expected Conc. = 0.0418 Median Pct Recovery = 73% Expected Conc. = 0.04 Median Pct Recovery = 73% Expected Conc. = 0.04 Median Pct Recovery = 73% Expected Conc. = 0.0321 Median Pct Recovery = 73% Expected Conc. = 0.0321 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.024 Median Pct Recovery = 73% Expected Conc. = 0.024 Median Pct Recovery = 73% Expected Conc. = 0.024 Median Pct Recovery = 73% Expected Conc. = 0.024 Median Pct Recovery = 73% Expected Conc. = 0.024 Median Pct Recovery = 73% Expected Conc. = 0.024 Median Pct Recovery = 73% Expected Conc. = 0.0484 Median Pct Recovery = 73% Expected Conc. = 0.0484 Median Pct Recovery = 73% Expected Conc. = 0.0484 Median Pct Recovery = 73% Expected Conc. = 0.0484 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Expected Conc. = 0.0242 Median Pct Recovery = 73% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CYPERMETHRIN
METHOD: 2033 , TESTIDCODE: 61586GCM39
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 61% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 78% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 92% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 72% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 71% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 84% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 115% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 63% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 104% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 66% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 64% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 72% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 65% Expected Conc. = 0.13 Median Pct Recovery = 69% Expected Conc. = 0.1208 Median Pct Recovery = 69% Expected Conc. = 0.1208 Median Pct Recovery = 69% Expected Conc. = 0.1208 Median Pct Recovery = 69% Expected Conc. = 0.1208 Median Pct Recovery = 69% Expected Conc. = 0.104 Median Pct Recovery = 69% Expected Conc. = 0.104 Median Pct Recovery = 69% Expected Conc. = 0.1002 Median Pct Recovery = 69% Expected Conc. = 0.1002 Median Pct Recovery = 69% Expected Conc. = 0.0804 Median Pct Recovery = 69% Expected Conc. = 0.0804 Median Pct Recovery = 69% Expected Conc. = 0.0798 Median Pct Recovery = 69% Expected Conc. = 0.0798 Median Pct Recovery = 69% Expected Conc. = 0.0604 Median Pct Recovery = 69% Expected Conc. = 0.0604 Median Pct Recovery = 69% Expected Conc. = 0.0604 Median Pct Recovery = 69% Expected Conc. = 0.0604 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.06 Median Pct Recovery = 69% Expected Conc. = 0.052 Median Pct Recovery = 69% Expected Conc. = 0.052 Median Pct Recovery = 69% Expected Conc. = 0.0501 Median Pct Recovery = 69% Expected Conc. = 0.0501 Median Pct Recovery = 69% Expected Conc. = 0.0501 Median Pct Recovery = 69% Expected Conc. = 0.0501 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.0302 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Expected Conc. = 0.03 Median Pct Recovery = 69% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ENDOSULFAN SULFATE
METHOD: 2033 , TESTIDCODE: 61590GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 96% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 62% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 100% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 79% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 65% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 83% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 81% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 117% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 71% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 71% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 76% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 66% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 69% Expected Conc. = 0.1 Median Pct Recovery = 77% Expected Conc. = 0.0968 Median Pct Recovery = 77% Expected Conc. = 0.0968 Median Pct Recovery = 77% Expected Conc. = 0.0968 Median Pct Recovery = 77% Expected Conc. = 0.0968 Median Pct Recovery = 77% Expected Conc. = 0.08 Median Pct Recovery = 77% Expected Conc. = 0.08 Median Pct Recovery = 77% Expected Conc. = 0.066 Median Pct Recovery = 77% Expected Conc. = 0.066 Median Pct Recovery = 77% Expected Conc. = 0.0484 Median Pct Recovery = 77% Expected Conc. = 0.0484 Median Pct Recovery = 77% Expected Conc. = 0.0484 Median Pct Recovery = 77% Expected Conc. = 0.0484 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.04 Median Pct Recovery = 77% Expected Conc. = 0.0324 Median Pct Recovery = 77% Expected Conc. = 0.0324 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.0242 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FENAMIPHOS
METHOD: 2033 , TESTIDCODE: 61591GCM39
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 95% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 80% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 84% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 103% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 115% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 86% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 143% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 87% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 79% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 80% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 103% Expected Conc. = 0.19 Median Pct Recovery = 85% Expected Conc. = 0.152 Median Pct Recovery = 85% Expected Conc. = 0.152 Median Pct Recovery = 85% Expected Conc. = 0.15 Median Pct Recovery = 85% Expected Conc. = 0.15 Median Pct Recovery = 85% Expected Conc. = 0.1212 Median Pct Recovery = 85% Expected Conc. = 0.1212 Median Pct Recovery = 85% Expected Conc. = 0.1206 Median Pct Recovery = 85% Expected Conc. = 0.1206 Median Pct Recovery = 85% Expected Conc. = 0.092 Median Pct Recovery = 85% Expected Conc. = 0.092 Median Pct Recovery = 85% Expected Conc. = 0.092 Median Pct Recovery = 85% Expected Conc. = 0.092 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.0908 Median Pct Recovery = 85% Expected Conc. = 0.076 Median Pct Recovery = 85% Expected Conc. = 0.076 Median Pct Recovery = 85% Expected Conc. = 0.075 Median Pct Recovery = 85% Expected Conc. = 0.075 Median Pct Recovery = 85% Expected Conc. = 0.075 Median Pct Recovery = 85% Expected Conc. = 0.075 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.1816 Median Pct Recovery = 85% Expected Conc. = 0.1816 Median Pct Recovery = 85% Expected Conc. = 0.1816 Median Pct Recovery = 85% Expected Conc. = 0.1816 Median Pct Recovery = 85% Expected Conc. = 0.092 Median Pct Recovery = 85% Expected Conc. = 0.092 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.046 Median Pct Recovery = 85% Expected Conc. = 0.0454 Median Pct Recovery = 85% Expected Conc. = 0.0454 Median Pct Recovery = 85% Expected Conc. = 0.0454 Median Pct Recovery = 85% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
IPRODIONE
METHOD: 2033 , TESTIDCODE: 61593GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 112% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 97% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 86% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 100% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 76% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 94% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 114% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 92% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 86% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 105% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 93% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 71% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 59% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 126% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 123% Expected Conc. = 0.087 Median Pct Recovery = 92% Expected Conc. = 0.0832 Median Pct Recovery = 92% Expected Conc. = 0.0832 Median Pct Recovery = 92% Expected Conc. = 0.0832 Median Pct Recovery = 92% Expected Conc. = 0.0832 Median Pct Recovery = 92% Expected Conc. = 0.0697 Median Pct Recovery = 92% Expected Conc. = 0.0697 Median Pct Recovery = 92% Expected Conc. = 0.044 Median Pct Recovery = 92% Expected Conc. = 0.044 Median Pct Recovery = 92% Expected Conc. = 0.044 Median Pct Recovery = 92% Expected Conc. = 0.044 Median Pct Recovery = 92% Expected Conc. = 0.044 Median Pct Recovery = 92% Expected Conc. = 0.044 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0416 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0348 Median Pct Recovery = 92% Expected Conc. = 0.0279 Median Pct Recovery = 92% Expected Conc. = 0.0279 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.022 Median Pct Recovery = 92% Expected Conc. = 0.0208 Median Pct Recovery = 92% Expected Conc. = 0.0208 Median Pct Recovery = 92% Expected Conc. = 0.0208 Median Pct Recovery = 92% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ISOFENPHOS
METHOD: 2033 , TESTIDCODE: 61594GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 35% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 74% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 107% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 85% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 9% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 100% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 100% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 103% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 94% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 106% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 93% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 87% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 53% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 18% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Expected Conc. = 0.09 Median Pct Recovery = 87% Expected Conc. = 0.084 Median Pct Recovery = 87% Expected Conc. = 0.084 Median Pct Recovery = 87% Expected Conc. = 0.072 Median Pct Recovery = 87% Expected Conc. = 0.072 Median Pct Recovery = 87% Expected Conc. = 0.07 Median Pct Recovery = 87% Expected Conc. = 0.07 Median Pct Recovery = 87% Expected Conc. = 0.0559 Median Pct Recovery = 87% Expected Conc. = 0.0559 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Expected Conc. = 0.036 Median Pct Recovery = 87% Expected Conc. = 0.036 Median Pct Recovery = 87% Expected Conc. = 0.035 Median Pct Recovery = 87% Expected Conc. = 0.035 Median Pct Recovery = 87% Expected Conc. = 0.035 Median Pct Recovery = 87% Expected Conc. = 0.035 Median Pct Recovery = 87% Expected Conc. = 0.0279 Median Pct Recovery = 87% Expected Conc. = 0.0279 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.021 Median Pct Recovery = 87% Expected Conc. = 0.084 Median Pct Recovery = 87% Expected Conc. = 0.084 Median Pct Recovery = 87% Expected Conc. = 0.042 Median Pct Recovery = 87% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CYHALOTHRIN
METHOD: 2033 , TESTIDCODE: 61595GCM39
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 53% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 40% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 71% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 56% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 104% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 71% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 57% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 83% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 89% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 60% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 55% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 90% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Expected Conc. = 0.084 Median Pct Recovery = 68% Expected Conc. = 0.084 Median Pct Recovery = 68% Expected Conc. = 0.084 Median Pct Recovery = 68% Expected Conc. = 0.0704 Median Pct Recovery = 68% Expected Conc. = 0.0704 Median Pct Recovery = 68% Expected Conc. = 0.0559 Median Pct Recovery = 68% Expected Conc. = 0.0559 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.042 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0352 Median Pct Recovery = 68% Expected Conc. = 0.0279 Median Pct Recovery = 68% Expected Conc. = 0.0279 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Expected Conc. = 0.021 Median Pct Recovery = 68% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
METALAXYL
METHOD: 2033 , TESTIDCODE: 61596GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 126% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 102% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 85% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 72% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 106% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 74% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 73% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 73% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 71% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 115% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 94% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 90% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 78% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 96% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 76% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 92% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 88% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 78% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 131% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 149% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Expected Conc. = 0.09 Median Pct Recovery = 88% Expected Conc. = 0.084 Median Pct Recovery = 88% Expected Conc. = 0.084 Median Pct Recovery = 88% Expected Conc. = 0.084 Median Pct Recovery = 88% Expected Conc. = 0.084 Median Pct Recovery = 88% Expected Conc. = 0.072 Median Pct Recovery = 88% Expected Conc. = 0.072 Median Pct Recovery = 88% Expected Conc. = 0.07 Median Pct Recovery = 88% Expected Conc. = 0.07 Median Pct Recovery = 88% Expected Conc. = 0.0559 Median Pct Recovery = 88% Expected Conc. = 0.0559 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.042 Median Pct Recovery = 88% Expected Conc. = 0.036 Median Pct Recovery = 88% Expected Conc. = 0.036 Median Pct Recovery = 88% Expected Conc. = 0.035 Median Pct Recovery = 88% Expected Conc. = 0.035 Median Pct Recovery = 88% Expected Conc. = 0.035 Median Pct Recovery = 88% Expected Conc. = 0.035 Median Pct Recovery = 88% Expected Conc. = 0.0282 Median Pct Recovery = 88% Expected Conc. = 0.0282 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Expected Conc. = 0.021 Median Pct Recovery = 88% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
METHIDATHION (SUPRACIDE)
METHOD: 2033 , TESTIDCODE: 61598GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 97% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 76% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 59% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 95% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 101% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 102% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 105% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 95% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 125% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 136% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 127% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 72% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 96% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 190% Expected Conc. = 0.075 Median Pct Recovery = 90% Expected Conc. = 0.0724 Median Pct Recovery = 90% Expected Conc. = 0.0724 Median Pct Recovery = 90% Expected Conc. = 0.0724 Median Pct Recovery = 90% Expected Conc. = 0.0724 Median Pct Recovery = 90% Expected Conc. = 0.0597 Median Pct Recovery = 90% Expected Conc. = 0.0597 Median Pct Recovery = 90% Expected Conc. = 0.0481 Median Pct Recovery = 90% Expected Conc. = 0.0481 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.0298 Median Pct Recovery = 90% Expected Conc. = 0.0298 Median Pct Recovery = 90% Expected Conc. = 0.0298 Median Pct Recovery = 90% Expected Conc. = 0.0298 Median Pct Recovery = 90% Expected Conc. = 0.024 Median Pct Recovery = 90% Expected Conc. = 0.024 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
MYCLOBUTANIL
METHOD: 2033 , TESTIDCODE: 61599GCM39
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 67% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 67% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 105% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 112% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 101% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 76% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 71% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 79% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 147% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 94% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.0504 Median Pct Recovery = 82% Expected Conc. = 0.0504 Median Pct Recovery = 82% Expected Conc. = 0.0402 Median Pct Recovery = 82% Expected Conc. = 0.0402 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.0256 Median Pct Recovery = 82% Expected Conc. = 0.0256 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0252 Median Pct Recovery = 82% Expected Conc. = 0.0202 Median Pct Recovery = 82% Expected Conc. = 0.0202 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Expected Conc. = 0.015 Median Pct Recovery = 82% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
OXYFLUORFEN
METHOD: 2033 , TESTIDCODE: 61600GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 103% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 84% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 73% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 102% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 95% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 103% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 81% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 82% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 93% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 94% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 178% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 111% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 93% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 71% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 105% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 106% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Expected Conc. = 0.06 Median Pct Recovery = 92% Expected Conc. = 0.06 Median Pct Recovery = 92% Expected Conc. = 0.06 Median Pct Recovery = 92% Expected Conc. = 0.06 Median Pct Recovery = 92% Expected Conc. = 0.06 Median Pct Recovery = 92% Expected Conc. = 0.05 Median Pct Recovery = 92% Expected Conc. = 0.05 Median Pct Recovery = 92% Expected Conc. = 0.048 Median Pct Recovery = 92% Expected Conc. = 0.048 Median Pct Recovery = 92% Expected Conc. = 0.0402 Median Pct Recovery = 92% Expected Conc. = 0.0402 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.03 Median Pct Recovery = 92% Expected Conc. = 0.025 Median Pct Recovery = 92% Expected Conc. = 0.025 Median Pct Recovery = 92% Expected Conc. = 0.025 Median Pct Recovery = 92% Expected Conc. = 0.025 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.024 Median Pct Recovery = 92% Expected Conc. = 0.0201 Median Pct Recovery = 92% Expected Conc. = 0.0201 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Expected Conc. = 0.015 Median Pct Recovery = 92% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PHOSMET (IMIDAN)
METHOD: 2033 , TESTIDCODE: 61601GCM39
DATES: 02/21/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 46% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 41% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 48% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 61% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 50% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 48% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 56% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 53% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 51% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 59% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 50% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 47% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 58% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 49% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 51% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 50% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 49% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 55% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 47% Expected Conc. = 0.8408 Median Pct Recovery = 50% Expected Conc. = 0.8408 Median Pct Recovery = 50% Expected Conc. = 0.8408 Median Pct Recovery = 50% Expected Conc. = 0.6984 Median Pct Recovery = 50% Expected Conc. = 0.6984 Median Pct Recovery = 50% Expected Conc. = 0.5586 Median Pct Recovery = 50% Expected Conc. = 0.5586 Median Pct Recovery = 50% Expected Conc. = 0.552 Median Pct Recovery = 50% Expected Conc. = 0.552 Median Pct Recovery = 50% Expected Conc. = 0.4204 Median Pct Recovery = 50% Expected Conc. = 0.4204 Median Pct Recovery = 50% Expected Conc. = 0.4204 Median Pct Recovery = 50% Expected Conc. = 0.4204 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.42 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Expected Conc. = 0.3488 Median Pct Recovery = 50% Expected Conc. = 0.3488 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.2102 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.21 Median Pct Recovery = 50% Expected Conc. = 0.3492 Median Pct Recovery = 50% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TEFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61606GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 73% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 52% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 52% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 40% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 63% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 61% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 45% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 56% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 65% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 73% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 59% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 53% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 58% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 56% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 61% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 56% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 56% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 41% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 61% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Expected Conc. = 0.09 Median Pct Recovery = 56% Expected Conc. = 0.084 Median Pct Recovery = 56% Expected Conc. = 0.084 Median Pct Recovery = 56% Expected Conc. = 0.084 Median Pct Recovery = 56% Expected Conc. = 0.084 Median Pct Recovery = 56% Expected Conc. = 0.072 Median Pct Recovery = 56% Expected Conc. = 0.072 Median Pct Recovery = 56% Expected Conc. = 0.0701 Median Pct Recovery = 56% Expected Conc. = 0.0701 Median Pct Recovery = 56% Expected Conc. = 0.0559 Median Pct Recovery = 56% Expected Conc. = 0.0559 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.042 Median Pct Recovery = 56% Expected Conc. = 0.036 Median Pct Recovery = 56% Expected Conc. = 0.036 Median Pct Recovery = 56% Expected Conc. = 0.035 Median Pct Recovery = 56% Expected Conc. = 0.035 Median Pct Recovery = 56% Expected Conc. = 0.035 Median Pct Recovery = 56% Expected Conc. = 0.035 Median Pct Recovery = 56% Expected Conc. = 0.0279 Median Pct Recovery = 56% Expected Conc. = 0.0279 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Expected Conc. = 0.021 Median Pct Recovery = 56% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))
METHOD: 2033 , TESTIDCODE: 61610GCM39
DATES: 02/21/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 50% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 60% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 50% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 78% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 78% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 61% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 60% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 61% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 66% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 74% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 80% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 92% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 99% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 64% Expected Conc. = 0.1088 Median Pct Recovery = 68% Expected Conc. = 0.1088 Median Pct Recovery = 68% Expected Conc. = 0.1088 Median Pct Recovery = 68% Expected Conc. = 0.0904 Median Pct Recovery = 68% Expected Conc. = 0.0904 Median Pct Recovery = 68% Expected Conc. = 0.072 Median Pct Recovery = 68% Expected Conc. = 0.072 Median Pct Recovery = 68% Expected Conc. = 0.072 Median Pct Recovery = 68% Expected Conc. = 0.072 Median Pct Recovery = 68% Expected Conc. = 0.0544 Median Pct Recovery = 68% Expected Conc. = 0.0544 Median Pct Recovery = 68% Expected Conc. = 0.0544 Median Pct Recovery = 68% Expected Conc. = 0.0544 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.054 Median Pct Recovery = 68% Expected Conc. = 0.0456 Median Pct Recovery = 68% Expected Conc. = 0.0456 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0452 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.0272 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Expected Conc. = 0.027 Median Pct Recovery = 68% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
2-CHLORO-2,6-DIETHYLACETANILIDE
METHOD: 2033 , TESTIDCODE: 61618GCM39
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 104% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 126% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 115% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 111% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 87% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 91% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 113% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 86% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 102% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 121% Expected Conc. = 0.0599 Median Pct Recovery = 89% Expected Conc. = 0.0599 Median Pct Recovery = 89% Expected Conc. = 0.0599 Median Pct Recovery = 89% Expected Conc. = 0.0401 Median Pct Recovery = 89% Expected Conc. = 0.0401 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.028 Median Pct Recovery = 89% Expected Conc. = 0.028 Median Pct Recovery = 89% Expected Conc. = 0.028 Median Pct Recovery = 89% Expected Conc. = 0.028 Median Pct Recovery = 89% Expected Conc. = 0.028 Median Pct Recovery = 89% Expected Conc. = 0.028 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0252 Median Pct Recovery = 89% Expected Conc. = 0.0201 Median Pct Recovery = 89% Expected Conc. = 0.0201 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Expected Conc. = 0.014 Median Pct Recovery = 89% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
2-ETHYL-6-METHYLANILINE
METHOD: 2033 , TESTIDCODE: 61620GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 85% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 74% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 55% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 82% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 84% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 83% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 68% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 94% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 73% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 97% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 94% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 30% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Expected Conc. = 0.06 Median Pct Recovery = 83% Expected Conc. = 0.06 Median Pct Recovery = 83% Expected Conc. = 0.06 Median Pct Recovery = 83% Expected Conc. = 0.0498 Median Pct Recovery = 83% Expected Conc. = 0.0498 Median Pct Recovery = 83% Expected Conc. = 0.048 Median Pct Recovery = 83% Expected Conc. = 0.048 Median Pct Recovery = 83% Expected Conc. = 0.0402 Median Pct Recovery = 83% Expected Conc. = 0.0402 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.03 Median Pct Recovery = 83% Expected Conc. = 0.0249 Median Pct Recovery = 83% Expected Conc. = 0.0249 Median Pct Recovery = 83% Expected Conc. = 0.0249 Median Pct Recovery = 83% Expected Conc. = 0.0249 Median Pct Recovery = 83% Expected Conc. = 0.024 Median Pct Recovery = 83% Expected Conc. = 0.024 Median Pct Recovery = 83% Expected Conc. = 0.0201 Median Pct Recovery = 83% Expected Conc. = 0.0201 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.015 Median Pct Recovery = 83% Expected Conc. = 0.06 Median Pct Recovery = 83% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
3,4-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61625GCM39
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 60% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 51% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 54% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 72% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 62% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 79% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 65% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 74% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 64% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 81% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 58% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 58% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 68% Expected Conc. = 0.0362 Median Pct Recovery = 69% Expected Conc. = 0.0362 Median Pct Recovery = 69% Expected Conc. = 0.0362 Median Pct Recovery = 69% Expected Conc. = 0.0304 Median Pct Recovery = 69% Expected Conc. = 0.0304 Median Pct Recovery = 69% Expected Conc. = 0.024 Median Pct Recovery = 69% Expected Conc. = 0.024 Median Pct Recovery = 69% Expected Conc. = 0.02 Median Pct Recovery = 69% Expected Conc. = 0.02 Median Pct Recovery = 69% Expected Conc. = 0.02 Median Pct Recovery = 69% Expected Conc. = 0.02 Median Pct Recovery = 69% Expected Conc. = 0.02 Median Pct Recovery = 69% Expected Conc. = 0.02 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0181 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.0152 Median Pct Recovery = 69% Expected Conc. = 0.012 Median Pct Recovery = 69% Expected Conc. = 0.012 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.01 Median Pct Recovery = 69% Expected Conc. = 0.0091 Median Pct Recovery = 69% Expected Conc. = 0.0091 Median Pct Recovery = 69% Expected Conc. = 0.0091 Median Pct Recovery = 69% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
3,5-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61627GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 71% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 88% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 69% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 84% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 83% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 95% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 96% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 94% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 83% Expected Conc. = 0.04 Median Pct Recovery = 84% Expected Conc. = 0.036 Median Pct Recovery = 84% Expected Conc. = 0.036 Median Pct Recovery = 84% Expected Conc. = 0.036 Median Pct Recovery = 84% Expected Conc. = 0.036 Median Pct Recovery = 84% Expected Conc. = 0.032 Median Pct Recovery = 84% Expected Conc. = 0.032 Median Pct Recovery = 84% Expected Conc. = 0.03 Median Pct Recovery = 84% Expected Conc. = 0.03 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.016 Median Pct Recovery = 84% Expected Conc. = 0.016 Median Pct Recovery = 84% Expected Conc. = 0.015 Median Pct Recovery = 84% Expected Conc. = 0.015 Median Pct Recovery = 84% Expected Conc. = 0.015 Median Pct Recovery = 84% Expected Conc. = 0.015 Median Pct Recovery = 84% Expected Conc. = 0.0121 Median Pct Recovery = 84% Expected Conc. = 0.0121 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.018 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Expected Conc. = 0.009 Median Pct Recovery = 84% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
4-CHLORO-2-METHYLPHENOL
METHOD: 2033 , TESTIDCODE: 61633GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 60% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 49% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 39% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 58% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 34% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 50% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 45% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 66% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 58% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 59% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 66% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 62% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 46% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 45% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 62% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Expected Conc. = 0.05 Median Pct Recovery = 58% Expected Conc. = 0.048 Median Pct Recovery = 58% Expected Conc. = 0.048 Median Pct Recovery = 58% Expected Conc. = 0.048 Median Pct Recovery = 58% Expected Conc. = 0.048 Median Pct Recovery = 58% Expected Conc. = 0.04 Median Pct Recovery = 58% Expected Conc. = 0.04 Median Pct Recovery = 58% Expected Conc. = 0.04 Median Pct Recovery = 58% Expected Conc. = 0.04 Median Pct Recovery = 58% Expected Conc. = 0.0318 Median Pct Recovery = 58% Expected Conc. = 0.0318 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.024 Median Pct Recovery = 58% Expected Conc. = 0.02 Median Pct Recovery = 58% Expected Conc. = 0.02 Median Pct Recovery = 58% Expected Conc. = 0.02 Median Pct Recovery = 58% Expected Conc. = 0.02 Median Pct Recovery = 58% Expected Conc. = 0.02 Median Pct Recovery = 58% Expected Conc. = 0.02 Median Pct Recovery = 58% Expected Conc. = 0.0159 Median Pct Recovery = 58% Expected Conc. = 0.0159 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Expected Conc. = 0.012 Median Pct Recovery = 58% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2033 , TESTIDCODE: 61635GCM39
DATES: 03/31/15 - 08/27/16
Open Data Set

Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 64% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 27% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 80% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 113% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 54% Expected Conc. = 0.216 Median Pct Recovery = 64% Expected Conc. = 0.1698 Median Pct Recovery = 64% Expected Conc. = 0.1698 Median Pct Recovery = 64% Expected Conc. = 0.126 Median Pct Recovery = 64% Expected Conc. = 0.126 Median Pct Recovery = 64% Expected Conc. = 0.126 Median Pct Recovery = 64% Expected Conc. = 0.126 Median Pct Recovery = 64% Expected Conc. = 0.126 Median Pct Recovery = 64% Expected Conc. = 0.126 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Expected Conc. = 0.27 Median Pct Recovery = 64% Expected Conc. = 0.27 Median Pct Recovery = 64% Expected Conc. = 0.108 Median Pct Recovery = 64% Expected Conc. = 0.108 Median Pct Recovery = 64% Expected Conc. = 0.063 Median Pct Recovery = 64% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CHLORPYRIFOS, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61636GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 50% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 24% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 41% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 39% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 28% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 23% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 46% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 45% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 39% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 30% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 31% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 63% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 54% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 50% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 46% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 63% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 66% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 58% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 29% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 56% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 28% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 20% Expected Conc. = 0.493 Median Pct Recovery = 43% Expected Conc. = 0.4816 Median Pct Recovery = 43% Expected Conc. = 0.4816 Median Pct Recovery = 43% Expected Conc. = 0.4816 Median Pct Recovery = 43% Expected Conc. = 0.4816 Median Pct Recovery = 43% Expected Conc. = 0.3168 Median Pct Recovery = 43% Expected Conc. = 0.3168 Median Pct Recovery = 43% Expected Conc. = 0.2408 Median Pct Recovery = 43% Expected Conc. = 0.2408 Median Pct Recovery = 43% Expected Conc. = 0.2408 Median Pct Recovery = 43% Expected Conc. = 0.2408 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.24 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1972 Median Pct Recovery = 43% Expected Conc. = 0.1599 Median Pct Recovery = 43% Expected Conc. = 0.1599 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.1204 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Expected Conc. = 0.12 Median Pct Recovery = 43% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DIAZINON, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61638GCM14
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 96% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 69% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 102% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 79% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 114% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 155% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 144% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 119% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 152% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 102% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 106% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 144% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 117% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 132% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 77% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 196% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 156% Expected Conc. = 0.072 Median Pct Recovery = 104% Expected Conc. = 0.0608 Median Pct Recovery = 104% Expected Conc. = 0.0608 Median Pct Recovery = 104% Expected Conc. = 0.048 Median Pct Recovery = 104% Expected Conc. = 0.048 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.036 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.0304 Median Pct Recovery = 104% Expected Conc. = 0.03 Median Pct Recovery = 104% Expected Conc. = 0.03 Median Pct Recovery = 104% Expected Conc. = 0.0239 Median Pct Recovery = 104% Expected Conc. = 0.0239 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Expected Conc. = 0.072 Median Pct Recovery = 104% Expected Conc. = 0.072 Median Pct Recovery = 104% Expected Conc. = 0.018 Median Pct Recovery = 104% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DISULFOTON SULFONE
METHOD: 2033 , TESTIDCODE: 61640GCM39
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 165% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 78% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 94% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 98% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 199% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 112% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 97% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 96% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 97% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 98% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 100% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 157% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 94% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 103% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 178% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 200% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 161% Expected Conc. = 0.0606 Median Pct Recovery = 97% Expected Conc. = 0.0606 Median Pct Recovery = 97% Expected Conc. = 0.0606 Median Pct Recovery = 97% Expected Conc. = 0.0504 Median Pct Recovery = 97% Expected Conc. = 0.0504 Median Pct Recovery = 97% Expected Conc. = 0.0401 Median Pct Recovery = 97% Expected Conc. = 0.0401 Median Pct Recovery = 97% Expected Conc. = 0.032 Median Pct Recovery = 97% Expected Conc. = 0.032 Median Pct Recovery = 97% Expected Conc. = 0.032 Median Pct Recovery = 97% Expected Conc. = 0.032 Median Pct Recovery = 97% Expected Conc. = 0.032 Median Pct Recovery = 97% Expected Conc. = 0.032 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0303 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0252 Median Pct Recovery = 97% Expected Conc. = 0.0201 Median Pct Recovery = 97% Expected Conc. = 0.0201 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.016 Median Pct Recovery = 97% Expected Conc. = 0.0152 Median Pct Recovery = 97% Expected Conc. = 0.0152 Median Pct Recovery = 97% Expected Conc. = 0.0152 Median Pct Recovery = 97% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FENAMIPHOS SULFONE
METHOD: 2033 , TESTIDCODE: 61645GCM39
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 79% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 68% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 71% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 43% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 37% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 59% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 64% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 58% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 85% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 95% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 97% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 52% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 96% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 85% Expected Conc. = 0.33 Median Pct Recovery = 76% Expected Conc. = 0.3224 Median Pct Recovery = 76% Expected Conc. = 0.3224 Median Pct Recovery = 76% Expected Conc. = 0.3224 Median Pct Recovery = 76% Expected Conc. = 0.3224 Median Pct Recovery = 76% Expected Conc. = 0.27 Median Pct Recovery = 76% Expected Conc. = 0.27 Median Pct Recovery = 76% Expected Conc. = 0.264 Median Pct Recovery = 76% Expected Conc. = 0.264 Median Pct Recovery = 76% Expected Conc. = 0.2166 Median Pct Recovery = 76% Expected Conc. = 0.2166 Median Pct Recovery = 76% Expected Conc. = 0.2148 Median Pct Recovery = 76% Expected Conc. = 0.2148 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.1612 Median Pct Recovery = 76% Expected Conc. = 0.16 Median Pct Recovery = 76% Expected Conc. = 0.16 Median Pct Recovery = 76% Expected Conc. = 0.16 Median Pct Recovery = 76% Expected Conc. = 0.16 Median Pct Recovery = 76% Expected Conc. = 0.16 Median Pct Recovery = 76% Expected Conc. = 0.16 Median Pct Recovery = 76% Expected Conc. = 0.135 Median Pct Recovery = 76% Expected Conc. = 0.135 Median Pct Recovery = 76% Expected Conc. = 0.135 Median Pct Recovery = 76% Expected Conc. = 0.135 Median Pct Recovery = 76% Expected Conc. = 0.132 Median Pct Recovery = 76% Expected Conc. = 0.132 Median Pct Recovery = 76% Expected Conc. = 0.0806 Median Pct Recovery = 76% Expected Conc. = 0.0806 Median Pct Recovery = 76% Expected Conc. = 0.0806 Median Pct Recovery = 76% Expected Conc. = 0.0806 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Expected Conc. = 0.08 Median Pct Recovery = 76% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FENAMIPHOS SULFOXIDE
METHOD: 2033 , TESTIDCODE: 61646GCM39
DATES: 02/21/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 12% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 25% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 17% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 16% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 15% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 7% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 13% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 8% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 12% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 25% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 15% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 10% Expected Conc. = 0.48 Median Pct Recovery = 14% Expected Conc. = 0.321 Median Pct Recovery = 14% Expected Conc. = 0.321 Median Pct Recovery = 14% Expected Conc. = 0.3204 Median Pct Recovery = 14% Expected Conc. = 0.3204 Median Pct Recovery = 14% Expected Conc. = 0.242 Median Pct Recovery = 14% Expected Conc. = 0.242 Median Pct Recovery = 14% Expected Conc. = 0.24 Median Pct Recovery = 14% Expected Conc. = 0.24 Median Pct Recovery = 14% Expected Conc. = 0.24 Median Pct Recovery = 14% Expected Conc. = 0.24 Median Pct Recovery = 14% Expected Conc. = 0.2 Median Pct Recovery = 14% Expected Conc. = 0.2 Median Pct Recovery = 14% Expected Conc. = 0.1988 Median Pct Recovery = 14% Expected Conc. = 0.1988 Median Pct Recovery = 14% Expected Conc. = 0.121 Median Pct Recovery = 14% Expected Conc. = 0.121 Median Pct Recovery = 14% Expected Conc. = 0.121 Median Pct Recovery = 14% Expected Conc. = 0.121 Median Pct Recovery = 14% Expected Conc. = 0.121 Median Pct Recovery = 14% Expected Conc. = 0.121 Median Pct Recovery = 14% Expected Conc. = 0.12 Median Pct Recovery = 14% Expected Conc. = 0.12 Median Pct Recovery = 14% Expected Conc. = 0.48 Median Pct Recovery = 14% Expected Conc. = 0.48 Median Pct Recovery = 14% Expected Conc. = 0.1988 Median Pct Recovery = 14% Expected Conc. = 0.1988 Median Pct Recovery = 14% Expected Conc. = 0.1988 Median Pct Recovery = 14% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
MALAOXON
METHOD: 2033 , TESTIDCODE: 61652GCM39
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 70% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 107% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 52% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 79% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 94% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 90% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 125% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 74% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 138% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 112% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 124% Expected Conc. = 0.132 Median Pct Recovery = 89% Expected Conc. = 0.132 Median Pct Recovery = 89% Expected Conc. = 0.132 Median Pct Recovery = 89% Expected Conc. = 0.1112 Median Pct Recovery = 89% Expected Conc. = 0.1112 Median Pct Recovery = 89% Expected Conc. = 0.09 Median Pct Recovery = 89% Expected Conc. = 0.09 Median Pct Recovery = 89% Expected Conc. = 0.068 Median Pct Recovery = 89% Expected Conc. = 0.068 Median Pct Recovery = 89% Expected Conc. = 0.068 Median Pct Recovery = 89% Expected Conc. = 0.068 Median Pct Recovery = 89% Expected Conc. = 0.068 Median Pct Recovery = 89% Expected Conc. = 0.068 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.066 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0556 Median Pct Recovery = 89% Expected Conc. = 0.0552 Median Pct Recovery = 89% Expected Conc. = 0.0552 Median Pct Recovery = 89% Expected Conc. = 0.0441 Median Pct Recovery = 89% Expected Conc. = 0.0441 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.034 Median Pct Recovery = 89% Expected Conc. = 0.033 Median Pct Recovery = 89% Expected Conc. = 0.033 Median Pct Recovery = 89% Expected Conc. = 0.033 Median Pct Recovery = 89% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PARAOXON-METHYL
METHOD: 2033 , TESTIDCODE: 61664GCM39
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 76% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 93% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 44% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 93% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 34% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 86% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 117% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 97% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 74% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 77% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 117% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 114% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 85% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 91% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Expected Conc. = 0.085 Median Pct Recovery = 85% Expected Conc. = 0.084 Median Pct Recovery = 85% Expected Conc. = 0.084 Median Pct Recovery = 85% Expected Conc. = 0.084 Median Pct Recovery = 85% Expected Conc. = 0.084 Median Pct Recovery = 85% Expected Conc. = 0.0702 Median Pct Recovery = 85% Expected Conc. = 0.0702 Median Pct Recovery = 85% Expected Conc. = 0.0558 Median Pct Recovery = 85% Expected Conc. = 0.0558 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.042 Median Pct Recovery = 85% Expected Conc. = 0.0351 Median Pct Recovery = 85% Expected Conc. = 0.0351 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.034 Median Pct Recovery = 85% Expected Conc. = 0.0279 Median Pct Recovery = 85% Expected Conc. = 0.0279 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Expected Conc. = 0.0351 Median Pct Recovery = 85% Expected Conc. = 0.0351 Median Pct Recovery = 85% Expected Conc. = 0.021 Median Pct Recovery = 85% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PHORATE OXON
METHOD: 2033 , TESTIDCODE: 61666GCM39
DATES: 03/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 95% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 50% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 46% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 65% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 33% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 61% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 83% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Expected Conc. = 0.167 Median Pct Recovery = 66% Expected Conc. = 0.1068 Median Pct Recovery = 66% Expected Conc. = 0.1068 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0668 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.0404 Median Pct Recovery = 66% Expected Conc. = 0.1616 Median Pct Recovery = 66% Expected Conc. = 0.1616 Median Pct Recovery = 66% Expected Conc. = 0.1616 Median Pct Recovery = 66% Expected Conc. = 0.1616 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0812 Median Pct Recovery = 66% Expected Conc. = 0.0808 Median Pct Recovery = 66% Expected Conc. = 0.0808 Median Pct Recovery = 66% Expected Conc. = 0.0808 Median Pct Recovery = 66% Expected Conc. = 0.0808 Median Pct Recovery = 66% Expected Conc. = 0.0406 Median Pct Recovery = 66% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PHOSMET OXON
METHOD: 2033 , TESTIDCODE: 61668GCM39
DATES: 03/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 35% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 29% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 61% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 63% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 63% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 56% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 76% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 93% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 50% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 65% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 83% Expected Conc. = 0.3064 Median Pct Recovery = 64% Expected Conc. = 0.3064 Median Pct Recovery = 64% Expected Conc. = 0.3064 Median Pct Recovery = 64% Expected Conc. = 0.2028 Median Pct Recovery = 64% Expected Conc. = 0.2028 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.1532 Median Pct Recovery = 64% Expected Conc. = 0.152 Median Pct Recovery = 64% Expected Conc. = 0.152 Median Pct Recovery = 64% Expected Conc. = 0.152 Median Pct Recovery = 64% Expected Conc. = 0.152 Median Pct Recovery = 64% Expected Conc. = 0.152 Median Pct Recovery = 64% Expected Conc. = 0.152 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.0766 Median Pct Recovery = 64% Expected Conc. = 0.0766 Median Pct Recovery = 64% Expected Conc. = 0.0766 Median Pct Recovery = 64% Expected Conc. = 0.0766 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.316 Median Pct Recovery = 64% Expected Conc. = 0.316 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.1264 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Expected Conc. = 0.076 Median Pct Recovery = 64% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FIPRONIL
METHOD: 2033 , TESTIDCODE: 62166GCM29
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 95% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 106% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 111% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 105% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 86% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 111% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 91% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 101% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 126% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 136% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 123% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 138% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 121% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 118% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 122% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 107% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 123% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 133% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Expected Conc. = 0.108 Median Pct Recovery = 109% Expected Conc. = 0.108 Median Pct Recovery = 109% Expected Conc. = 0.108 Median Pct Recovery = 109% Expected Conc. = 0.0896 Median Pct Recovery = 109% Expected Conc. = 0.0896 Median Pct Recovery = 109% Expected Conc. = 0.072 Median Pct Recovery = 109% Expected Conc. = 0.072 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.054 Median Pct Recovery = 109% Expected Conc. = 0.0456 Median Pct Recovery = 109% Expected Conc. = 0.0456 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0448 Median Pct Recovery = 109% Expected Conc. = 0.0363 Median Pct Recovery = 109% Expected Conc. = 0.0363 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Expected Conc. = 0.027 Median Pct Recovery = 109% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FIPRONIL SULFIDE
METHOD: 2033 , TESTIDCODE: 62167GCM29
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 91% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 103% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 90% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 81% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 68% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 101% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 92% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 94% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 110% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 104% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 88% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Expected Conc. = 0.1 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.096 Median Pct Recovery = 91% Expected Conc. = 0.0804 Median Pct Recovery = 91% Expected Conc. = 0.0804 Median Pct Recovery = 91% Expected Conc. = 0.08 Median Pct Recovery = 91% Expected Conc. = 0.08 Median Pct Recovery = 91% Expected Conc. = 0.066 Median Pct Recovery = 91% Expected Conc. = 0.066 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.048 Median Pct Recovery = 91% Expected Conc. = 0.0402 Median Pct Recovery = 91% Expected Conc. = 0.0402 Median Pct Recovery = 91% Expected Conc. = 0.0402 Median Pct Recovery = 91% Expected Conc. = 0.0402 Median Pct Recovery = 91% Expected Conc. = 0.04 Median Pct Recovery = 91% Expected Conc. = 0.04 Median Pct Recovery = 91% Expected Conc. = 0.0321 Median Pct Recovery = 91% Expected Conc. = 0.0321 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Expected Conc. = 0.024 Median Pct Recovery = 91% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
FIPRONIL SULFONE
METHOD: 2033 , TESTIDCODE: 62168GCM29
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 88% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 79% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 71% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 75% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 92% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 78% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 103% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 122% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 102% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 89% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 64% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 92% Expected Conc. = 0.149 Median Pct Recovery = 89% Expected Conc. = 0.1432 Median Pct Recovery = 89% Expected Conc. = 0.1432 Median Pct Recovery = 89% Expected Conc. = 0.1208 Median Pct Recovery = 89% Expected Conc. = 0.1208 Median Pct Recovery = 89% Expected Conc. = 0.096 Median Pct Recovery = 89% Expected Conc. = 0.096 Median Pct Recovery = 89% Expected Conc. = 0.072 Median Pct Recovery = 89% Expected Conc. = 0.072 Median Pct Recovery = 89% Expected Conc. = 0.072 Median Pct Recovery = 89% Expected Conc. = 0.072 Median Pct Recovery = 89% Expected Conc. = 0.0604 Median Pct Recovery = 89% Expected Conc. = 0.0604 Median Pct Recovery = 89% Expected Conc. = 0.0604 Median Pct Recovery = 89% Expected Conc. = 0.0604 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.0596 Median Pct Recovery = 89% Expected Conc. = 0.048 Median Pct Recovery = 89% Expected Conc. = 0.048 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.0358 Median Pct Recovery = 89% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DESULFINYLFIPRONIL
METHOD: 2033 , TESTIDCODE: 62170GCM29
DATES: 01/31/15 - 09/20/16
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 135% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 91% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 70% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 58% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 99% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 89% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 72% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 73% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 78% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 57% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Expected Conc. = 0.08 Median Pct Recovery = 75% Expected Conc. = 0.072 Median Pct Recovery = 75% Expected Conc. = 0.072 Median Pct Recovery = 75% Expected Conc. = 0.072 Median Pct Recovery = 75% Expected Conc. = 0.072 Median Pct Recovery = 75% Expected Conc. = 0.064 Median Pct Recovery = 75% Expected Conc. = 0.064 Median Pct Recovery = 75% Expected Conc. = 0.048 Median Pct Recovery = 75% Expected Conc. = 0.048 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.036 Median Pct Recovery = 75% Expected Conc. = 0.032 Median Pct Recovery = 75% Expected Conc. = 0.032 Median Pct Recovery = 75% Expected Conc. = 0.024 Median Pct Recovery = 75% Expected Conc. = 0.024 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Expected Conc. = 0.018 Median Pct Recovery = 75% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TEBUCONAZOLE
METHOD: 2033 , TESTIDCODE: 62852GCM14
DATES: 02/21/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 67% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 53% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 81% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 83% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 75% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 108% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 78% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 64% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 56% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 55% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 52% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 62% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 48% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 44% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 107% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 78% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 64% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 104% Expected Conc. = 0.12 Median Pct Recovery = 68% Expected Conc. = 0.12 Median Pct Recovery = 68% Expected Conc. = 0.12 Median Pct Recovery = 68% Expected Conc. = 0.1016 Median Pct Recovery = 68% Expected Conc. = 0.1016 Median Pct Recovery = 68% Expected Conc. = 0.0798 Median Pct Recovery = 68% Expected Conc. = 0.0798 Median Pct Recovery = 68% Expected Conc. = 0.0786 Median Pct Recovery = 68% Expected Conc. = 0.0786 Median Pct Recovery = 68% Expected Conc. = 0.0604 Median Pct Recovery = 68% Expected Conc. = 0.0604 Median Pct Recovery = 68% Expected Conc. = 0.0604 Median Pct Recovery = 68% Expected Conc. = 0.0604 Median Pct Recovery = 68% Expected Conc. = 0.0604 Median Pct Recovery = 68% Expected Conc. = 0.0604 Median Pct Recovery = 68% Expected Conc. = 0.06 Median Pct Recovery = 68% Expected Conc. = 0.06 Median Pct Recovery = 68% Expected Conc. = 0.06 Median Pct Recovery = 68% Expected Conc. = 0.06 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.0508 Median Pct Recovery = 68% Expected Conc. = 0.05 Median Pct Recovery = 68% Expected Conc. = 0.05 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.0302 Median Pct Recovery = 68% Expected Conc. = 0.03 Median Pct Recovery = 68% Expected Conc. = 0.03 Median Pct Recovery = 68% Expected Conc. = 0.03 Median Pct Recovery = 68% Expected Conc. = 0.03 Median Pct Recovery = 68% Expected Conc. = 0.03 Median Pct Recovery = 68% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ETHION
METHOD: 2033 , TESTIDCODE: 82346GCM40
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 113% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 66% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 80% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 97% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 94% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 113% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 115% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 113% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 94% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 94% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 128% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 193% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 102% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 110% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 111% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 121% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 141% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 103% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 120% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 107% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 134% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 106% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Expected Conc. = 0.03 Median Pct Recovery = 109% Expected Conc. = 0.028 Median Pct Recovery = 109% Expected Conc. = 0.028 Median Pct Recovery = 109% Expected Conc. = 0.028 Median Pct Recovery = 109% Expected Conc. = 0.028 Median Pct Recovery = 109% Expected Conc. = 0.024 Median Pct Recovery = 109% Expected Conc. = 0.024 Median Pct Recovery = 109% Expected Conc. = 0.023 Median Pct Recovery = 109% Expected Conc. = 0.023 Median Pct Recovery = 109% Expected Conc. = 0.019 Median Pct Recovery = 109% Expected Conc. = 0.019 Median Pct Recovery = 109% Expected Conc. = 0.0186 Median Pct Recovery = 109% Expected Conc. = 0.0186 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.014 Median Pct Recovery = 109% Expected Conc. = 0.012 Median Pct Recovery = 109% Expected Conc. = 0.012 Median Pct Recovery = 109% Expected Conc. = 0.0115 Median Pct Recovery = 109% Expected Conc. = 0.0115 Median Pct Recovery = 109% Expected Conc. = 0.0115 Median Pct Recovery = 109% Expected Conc. = 0.0115 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Expected Conc. = 0.007 Median Pct Recovery = 109% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
METRIBUZIN
METHOD: 2033 , TESTIDCODE: 82630GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 76% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 28% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 63% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 77% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 27% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 93% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 83% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 64% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 77% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 69% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 104% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 73% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 116% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 62% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 119% Expected Conc. = 0.075 Median Pct Recovery = 77% Expected Conc. = 0.0723 Median Pct Recovery = 77% Expected Conc. = 0.0723 Median Pct Recovery = 77% Expected Conc. = 0.0723 Median Pct Recovery = 77% Expected Conc. = 0.0723 Median Pct Recovery = 77% Expected Conc. = 0.06 Median Pct Recovery = 77% Expected Conc. = 0.06 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.048 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.0362 Median Pct Recovery = 77% Expected Conc. = 0.036 Median Pct Recovery = 77% Expected Conc. = 0.036 Median Pct Recovery = 77% Expected Conc. = 0.036 Median Pct Recovery = 77% Expected Conc. = 0.036 Median Pct Recovery = 77% Expected Conc. = 0.036 Median Pct Recovery = 77% Expected Conc. = 0.036 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.03 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.024 Median Pct Recovery = 77% Expected Conc. = 0.0181 Median Pct Recovery = 77% Expected Conc. = 0.0181 Median Pct Recovery = 77% Expected Conc. = 0.0181 Median Pct Recovery = 77% Expected Conc. = 0.0181 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Expected Conc. = 0.018 Median Pct Recovery = 77% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
2,6-DIETHYLANILINE
METHOD: 2033 , TESTIDCODE: 82660GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 29% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 90% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 91% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 59% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 92% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 89% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 62% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 96% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 104% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 78% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 94% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 103% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 84% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Expected Conc. = 0.04 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.036 Median Pct Recovery = 89% Expected Conc. = 0.032 Median Pct Recovery = 89% Expected Conc. = 0.032 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.03 Median Pct Recovery = 89% Expected Conc. = 0.024 Median Pct Recovery = 89% Expected Conc. = 0.024 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.018 Median Pct Recovery = 89% Expected Conc. = 0.016 Median Pct Recovery = 89% Expected Conc. = 0.016 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.015 Median Pct Recovery = 89% Expected Conc. = 0.0121 Median Pct Recovery = 89% Expected Conc. = 0.0121 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Expected Conc. = 0.009 Median Pct Recovery = 89% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TRIFLURALIN
METHOD: 2033 , TESTIDCODE: 82661GCM35
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 63% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 79% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 75% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 63% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 93% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 80% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 103% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 99% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 92% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 69% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 62% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Expected Conc. = 0.12 Median Pct Recovery = 79% Expected Conc. = 0.108 Median Pct Recovery = 79% Expected Conc. = 0.108 Median Pct Recovery = 79% Expected Conc. = 0.108 Median Pct Recovery = 79% Expected Conc. = 0.108 Median Pct Recovery = 79% Expected Conc. = 0.096 Median Pct Recovery = 79% Expected Conc. = 0.096 Median Pct Recovery = 79% Expected Conc. = 0.0904 Median Pct Recovery = 79% Expected Conc. = 0.0904 Median Pct Recovery = 79% Expected Conc. = 0.0726 Median Pct Recovery = 79% Expected Conc. = 0.0726 Median Pct Recovery = 79% Expected Conc. = 0.072 Median Pct Recovery = 79% Expected Conc. = 0.072 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.054 Median Pct Recovery = 79% Expected Conc. = 0.048 Median Pct Recovery = 79% Expected Conc. = 0.048 Median Pct Recovery = 79% Expected Conc. = 0.0452 Median Pct Recovery = 79% Expected Conc. = 0.0452 Median Pct Recovery = 79% Expected Conc. = 0.0452 Median Pct Recovery = 79% Expected Conc. = 0.0452 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Expected Conc. = 0.027 Median Pct Recovery = 79% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DIMETHOATE
METHOD: 2033 , TESTIDCODE: 82662GCM40
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 27% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 24% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 10% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 35% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 44% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 48% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 42% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 36% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 32% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 32% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 51% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 42% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 38% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 35% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 38% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 49% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 57% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 46% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 36% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 46% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 48% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 38% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 38% Expected Conc. = 0.0597 Median Pct Recovery = 38% Expected Conc. = 0.0504 Median Pct Recovery = 38% Expected Conc. = 0.0504 Median Pct Recovery = 38% Expected Conc. = 0.0403 Median Pct Recovery = 38% Expected Conc. = 0.0403 Median Pct Recovery = 38% Expected Conc. = 0.032 Median Pct Recovery = 38% Expected Conc. = 0.032 Median Pct Recovery = 38% Expected Conc. = 0.032 Median Pct Recovery = 38% Expected Conc. = 0.032 Median Pct Recovery = 38% Expected Conc. = 0.032 Median Pct Recovery = 38% Expected Conc. = 0.032 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0298 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0252 Median Pct Recovery = 38% Expected Conc. = 0.0201 Median Pct Recovery = 38% Expected Conc. = 0.0201 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.016 Median Pct Recovery = 38% Expected Conc. = 0.0149 Median Pct Recovery = 38% Expected Conc. = 0.0149 Median Pct Recovery = 38% Expected Conc. = 0.0149 Median Pct Recovery = 38% Expected Conc. = 0.0149 Median Pct Recovery = 38% Expected Conc. = 0.0597 Median Pct Recovery = 38% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PHORATE
METHOD: 2033 , TESTIDCODE: 82664GCM35
DATES: 03/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 88% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 33% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 55% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 43% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 52% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 80% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 80% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 78% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 63% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 50% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 40% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 63% Expected Conc. = 0.122 Median Pct Recovery = 63% Expected Conc. = 0.1 Median Pct Recovery = 63% Expected Conc. = 0.1 Median Pct Recovery = 63% Expected Conc. = 0.081 Median Pct Recovery = 63% Expected Conc. = 0.081 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.05 Median Pct Recovery = 63% Expected Conc. = 0.05 Median Pct Recovery = 63% Expected Conc. = 0.05 Median Pct Recovery = 63% Expected Conc. = 0.05 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.0488 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.12 Median Pct Recovery = 63% Expected Conc. = 0.12 Median Pct Recovery = 63% Expected Conc. = 0.12 Median Pct Recovery = 63% Expected Conc. = 0.12 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.06 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Expected Conc. = 0.03 Median Pct Recovery = 63% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PARATHION-METHYL
METHOD: 2033 , TESTIDCODE: 82667GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 133% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 104% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 79% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 123% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 90% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 107% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 96% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 80% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 84% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 148% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 103% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 108% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 135% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 130% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 116% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 112% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 106% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 176% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 158% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Expected Conc. = 0.05 Median Pct Recovery = 107% Expected Conc. = 0.048 Median Pct Recovery = 107% Expected Conc. = 0.048 Median Pct Recovery = 107% Expected Conc. = 0.048 Median Pct Recovery = 107% Expected Conc. = 0.048 Median Pct Recovery = 107% Expected Conc. = 0.0402 Median Pct Recovery = 107% Expected Conc. = 0.0402 Median Pct Recovery = 107% Expected Conc. = 0.04 Median Pct Recovery = 107% Expected Conc. = 0.04 Median Pct Recovery = 107% Expected Conc. = 0.0318 Median Pct Recovery = 107% Expected Conc. = 0.0318 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Expected Conc. = 0.0201 Median Pct Recovery = 107% Expected Conc. = 0.0201 Median Pct Recovery = 107% Expected Conc. = 0.0201 Median Pct Recovery = 107% Expected Conc. = 0.0201 Median Pct Recovery = 107% Expected Conc. = 0.02 Median Pct Recovery = 107% Expected Conc. = 0.02 Median Pct Recovery = 107% Expected Conc. = 0.016 Median Pct Recovery = 107% Expected Conc. = 0.016 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.012 Median Pct Recovery = 107% Expected Conc. = 0.024 Median Pct Recovery = 107% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
EPTC
METHOD: 2033 , TESTIDCODE: 82668GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 53% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 99% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 80% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 106% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 98% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 79% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 76% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 102% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 112% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 94% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 98% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 101% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 105% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 110% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 55% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Expected Conc. = 0.0336 Median Pct Recovery = 98% Expected Conc. = 0.0336 Median Pct Recovery = 98% Expected Conc. = 0.0336 Median Pct Recovery = 98% Expected Conc. = 0.028 Median Pct Recovery = 98% Expected Conc. = 0.028 Median Pct Recovery = 98% Expected Conc. = 0.0222 Median Pct Recovery = 98% Expected Conc. = 0.0222 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.0168 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.014 Median Pct Recovery = 98% Expected Conc. = 0.0112 Median Pct Recovery = 98% Expected Conc. = 0.0112 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Expected Conc. = 0.0084 Median Pct Recovery = 98% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TEBUTHIURON
METHOD: 2033 , TESTIDCODE: 82670GCM35
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 142% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 71% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 123% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 129% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 200% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 70% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 126% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 161% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 105% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 110% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 123% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 67% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 114% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 109% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 99% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 131% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 124% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 105% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 143% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 107% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 127% Expected Conc. = 0.18 Median Pct Recovery = 112% Expected Conc. = 0.1664 Median Pct Recovery = 112% Expected Conc. = 0.1664 Median Pct Recovery = 112% Expected Conc. = 0.1664 Median Pct Recovery = 112% Expected Conc. = 0.1664 Median Pct Recovery = 112% Expected Conc. = 0.144 Median Pct Recovery = 112% Expected Conc. = 0.144 Median Pct Recovery = 112% Expected Conc. = 0.14 Median Pct Recovery = 112% Expected Conc. = 0.14 Median Pct Recovery = 112% Expected Conc. = 0.1122 Median Pct Recovery = 112% Expected Conc. = 0.1122 Median Pct Recovery = 112% Expected Conc. = 0.1116 Median Pct Recovery = 112% Expected Conc. = 0.1116 Median Pct Recovery = 112% Expected Conc. = 0.084 Median Pct Recovery = 112% Expected Conc. = 0.084 Median Pct Recovery = 112% Expected Conc. = 0.084 Median Pct Recovery = 112% Expected Conc. = 0.084 Median Pct Recovery = 112% Expected Conc. = 0.084 Median Pct Recovery = 112% Expected Conc. = 0.084 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.0832 Median Pct Recovery = 112% Expected Conc. = 0.072 Median Pct Recovery = 112% Expected Conc. = 0.072 Median Pct Recovery = 112% Expected Conc. = 0.07 Median Pct Recovery = 112% Expected Conc. = 0.07 Median Pct Recovery = 112% Expected Conc. = 0.07 Median Pct Recovery = 112% Expected Conc. = 0.07 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.042 Median Pct Recovery = 112% Expected Conc. = 0.0416 Median Pct Recovery = 112% Expected Conc. = 0.0416 Median Pct Recovery = 112% Expected Conc. = 0.0416 Median Pct Recovery = 112% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
MOLINATE
METHOD: 2033 , TESTIDCODE: 82671GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 123% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 41% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 96% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 103% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 98% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 73% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 109% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 117% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 105% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 98% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 82% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 108% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 107% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 94% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 73% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 113% Expected Conc. = 0.05 Median Pct Recovery = 98% Expected Conc. = 0.048 Median Pct Recovery = 98% Expected Conc. = 0.048 Median Pct Recovery = 98% Expected Conc. = 0.048 Median Pct Recovery = 98% Expected Conc. = 0.048 Median Pct Recovery = 98% Expected Conc. = 0.0402 Median Pct Recovery = 98% Expected Conc. = 0.0402 Median Pct Recovery = 98% Expected Conc. = 0.04 Median Pct Recovery = 98% Expected Conc. = 0.04 Median Pct Recovery = 98% Expected Conc. = 0.0318 Median Pct Recovery = 98% Expected Conc. = 0.0318 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.0201 Median Pct Recovery = 98% Expected Conc. = 0.0201 Median Pct Recovery = 98% Expected Conc. = 0.0201 Median Pct Recovery = 98% Expected Conc. = 0.0201 Median Pct Recovery = 98% Expected Conc. = 0.02 Median Pct Recovery = 98% Expected Conc. = 0.02 Median Pct Recovery = 98% Expected Conc. = 0.0159 Median Pct Recovery = 98% Expected Conc. = 0.0159 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.024 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Expected Conc. = 0.012 Median Pct Recovery = 98% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
ETHOPROPHOS
METHOD: 2033 , TESTIDCODE: 82672GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 71% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 84% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 86% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 79% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 86% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 93% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 77% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Expected Conc. = 0.096 Median Pct Recovery = 84% Expected Conc. = 0.0808 Median Pct Recovery = 84% Expected Conc. = 0.0808 Median Pct Recovery = 84% Expected Conc. = 0.066 Median Pct Recovery = 84% Expected Conc. = 0.066 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.04 Median Pct Recovery = 84% Expected Conc. = 0.04 Median Pct Recovery = 84% Expected Conc. = 0.0321 Median Pct Recovery = 84% Expected Conc. = 0.0321 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.096 Median Pct Recovery = 84% Expected Conc. = 0.096 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.048 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.0404 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Expected Conc. = 0.024 Median Pct Recovery = 84% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
BENFLURALIN
METHOD: 2033 , TESTIDCODE: 82673GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 66% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 58% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 71% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 68% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 68% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 72% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 64% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 80% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 55% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 106% Expected Conc. = 0.084 Median Pct Recovery = 67% Expected Conc. = 0.084 Median Pct Recovery = 67% Expected Conc. = 0.084 Median Pct Recovery = 67% Expected Conc. = 0.0712 Median Pct Recovery = 67% Expected Conc. = 0.0712 Median Pct Recovery = 67% Expected Conc. = 0.0559 Median Pct Recovery = 67% Expected Conc. = 0.0559 Median Pct Recovery = 67% Expected Conc. = 0.044 Median Pct Recovery = 67% Expected Conc. = 0.044 Median Pct Recovery = 67% Expected Conc. = 0.044 Median Pct Recovery = 67% Expected Conc. = 0.044 Median Pct Recovery = 67% Expected Conc. = 0.044 Median Pct Recovery = 67% Expected Conc. = 0.044 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.042 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0356 Median Pct Recovery = 67% Expected Conc. = 0.0352 Median Pct Recovery = 67% Expected Conc. = 0.0352 Median Pct Recovery = 67% Expected Conc. = 0.0279 Median Pct Recovery = 67% Expected Conc. = 0.0279 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.022 Median Pct Recovery = 67% Expected Conc. = 0.021 Median Pct Recovery = 67% Expected Conc. = 0.021 Median Pct Recovery = 67% Expected Conc. = 0.021 Median Pct Recovery = 67% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CARBOFURAN
METHOD: 2033 , TESTIDCODE: 82674GCM35
DATES: 02/21/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 78% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 32% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 43% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 38% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 64% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 83% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 83% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 65% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 97% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 86% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 64% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 67% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 76% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 66% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Expected Conc. = 0.36 Median Pct Recovery = 71% Expected Conc. = 0.36 Median Pct Recovery = 71% Expected Conc. = 0.36 Median Pct Recovery = 71% Expected Conc. = 0.3032 Median Pct Recovery = 71% Expected Conc. = 0.3032 Median Pct Recovery = 71% Expected Conc. = 0.2406 Median Pct Recovery = 71% Expected Conc. = 0.2406 Median Pct Recovery = 71% Expected Conc. = 0.2376 Median Pct Recovery = 71% Expected Conc. = 0.2376 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.18 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1516 Median Pct Recovery = 71% Expected Conc. = 0.1484 Median Pct Recovery = 71% Expected Conc. = 0.1484 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Expected Conc. = 0.09 Median Pct Recovery = 71% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
TERBUFOS
METHOD: 2033 , TESTIDCODE: 82675GCM35
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 90% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 57% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 65% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 59% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 49% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 45% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 79% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 72% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 58% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 56% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 46% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 75% Expected Conc. = 0.0896 Median Pct Recovery = 58% Expected Conc. = 0.075 Median Pct Recovery = 58% Expected Conc. = 0.075 Median Pct Recovery = 58% Expected Conc. = 0.0726 Median Pct Recovery = 58% Expected Conc. = 0.0726 Median Pct Recovery = 58% Expected Conc. = 0.072 Median Pct Recovery = 58% Expected Conc. = 0.072 Median Pct Recovery = 58% Expected Conc. = 0.056 Median Pct Recovery = 58% Expected Conc. = 0.056 Median Pct Recovery = 58% Expected Conc. = 0.056 Median Pct Recovery = 58% Expected Conc. = 0.056 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0544 Median Pct Recovery = 58% Expected Conc. = 0.0448 Median Pct Recovery = 58% Expected Conc. = 0.0448 Median Pct Recovery = 58% Expected Conc. = 0.0448 Median Pct Recovery = 58% Expected Conc. = 0.0448 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.03 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.1088 Median Pct Recovery = 58% Expected Conc. = 0.1088 Median Pct Recovery = 58% Expected Conc. = 0.1088 Median Pct Recovery = 58% Expected Conc. = 0.1088 Median Pct Recovery = 58% Expected Conc. = 0.056 Median Pct Recovery = 58% Expected Conc. = 0.056 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.028 Median Pct Recovery = 58% Expected Conc. = 0.0272 Median Pct Recovery = 58% Expected Conc. = 0.0272 Median Pct Recovery = 58% Expected Conc. = 0.0272 Median Pct Recovery = 58% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PROPYZAMIDE (PRONAMIDE)
METHOD: 2033 , TESTIDCODE: 82676GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 101% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 73% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 77% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 89% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 70% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 100% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 77% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 71% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 84% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 72% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 84% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 88% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Expected Conc. = 0.05 Median Pct Recovery = 76% Expected Conc. = 0.0481 Median Pct Recovery = 76% Expected Conc. = 0.0481 Median Pct Recovery = 76% Expected Conc. = 0.0481 Median Pct Recovery = 76% Expected Conc. = 0.0481 Median Pct Recovery = 76% Expected Conc. = 0.04 Median Pct Recovery = 76% Expected Conc. = 0.04 Median Pct Recovery = 76% Expected Conc. = 0.0398 Median Pct Recovery = 76% Expected Conc. = 0.0398 Median Pct Recovery = 76% Expected Conc. = 0.0318 Median Pct Recovery = 76% Expected Conc. = 0.0318 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.024 Median Pct Recovery = 76% Expected Conc. = 0.02 Median Pct Recovery = 76% Expected Conc. = 0.02 Median Pct Recovery = 76% Expected Conc. = 0.0199 Median Pct Recovery = 76% Expected Conc. = 0.0199 Median Pct Recovery = 76% Expected Conc. = 0.0199 Median Pct Recovery = 76% Expected Conc. = 0.0199 Median Pct Recovery = 76% Expected Conc. = 0.0159 Median Pct Recovery = 76% Expected Conc. = 0.0159 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Expected Conc. = 0.012 Median Pct Recovery = 76% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DISULFOTON
METHOD: 2033 , TESTIDCODE: 82677GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 91% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 67% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 42% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 54% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 66% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 44% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 58% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 60% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 48% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 24% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 51% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 40% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 15% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 32% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 20% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 52% Expected Conc. = 0.247 Median Pct Recovery = 53% Expected Conc. = 0.204 Median Pct Recovery = 53% Expected Conc. = 0.204 Median Pct Recovery = 53% Expected Conc. = 0.162 Median Pct Recovery = 53% Expected Conc. = 0.162 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.102 Median Pct Recovery = 53% Expected Conc. = 0.102 Median Pct Recovery = 53% Expected Conc. = 0.102 Median Pct Recovery = 53% Expected Conc. = 0.102 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0988 Median Pct Recovery = 53% Expected Conc. = 0.0804 Median Pct Recovery = 53% Expected Conc. = 0.0804 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.0602 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Expected Conc. = 0.2408 Median Pct Recovery = 53% Expected Conc. = 0.2408 Median Pct Recovery = 53% Expected Conc. = 0.2408 Median Pct Recovery = 53% Expected Conc. = 0.2408 Median Pct Recovery = 53% Expected Conc. = 0.1204 Median Pct Recovery = 53% Expected Conc. = 0.1204 Median Pct Recovery = 53% Expected Conc. = 0.1204 Median Pct Recovery = 53% Expected Conc. = 0.1204 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.12 Median Pct Recovery = 53% Expected Conc. = 0.06 Median Pct Recovery = 53% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PROPANIL
METHOD: 2033 , TESTIDCODE: 82679GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 132% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 88% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 105% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 124% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 77% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 99% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 92% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 101% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 125% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 106% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 98% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 102% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 126% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 88% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 102% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 73% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 134% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 139% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 125% Expected Conc. = 0.06 Median Pct Recovery = 102% Expected Conc. = 0.06 Median Pct Recovery = 102% Expected Conc. = 0.06 Median Pct Recovery = 102% Expected Conc. = 0.06 Median Pct Recovery = 102% Expected Conc. = 0.06 Median Pct Recovery = 102% Expected Conc. = 0.05 Median Pct Recovery = 102% Expected Conc. = 0.05 Median Pct Recovery = 102% Expected Conc. = 0.048 Median Pct Recovery = 102% Expected Conc. = 0.048 Median Pct Recovery = 102% Expected Conc. = 0.0401 Median Pct Recovery = 102% Expected Conc. = 0.0401 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.03 Median Pct Recovery = 102% Expected Conc. = 0.025 Median Pct Recovery = 102% Expected Conc. = 0.025 Median Pct Recovery = 102% Expected Conc. = 0.025 Median Pct Recovery = 102% Expected Conc. = 0.025 Median Pct Recovery = 102% Expected Conc. = 0.024 Median Pct Recovery = 102% Expected Conc. = 0.024 Median Pct Recovery = 102% Expected Conc. = 0.0201 Median Pct Recovery = 102% Expected Conc. = 0.0201 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Expected Conc. = 0.015 Median Pct Recovery = 102% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CARBARYL
METHOD: 2033 , TESTIDCODE: 82680GCM35
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 94% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 53% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 73% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 80% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 58% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 53% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 50% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 57% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 66% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 78% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 69% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 60% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 53% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 54% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 64% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 53% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 44% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 74% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 43% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 83% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Expected Conc. = 0.373 Median Pct Recovery = 64% Expected Conc. = 0.36 Median Pct Recovery = 64% Expected Conc. = 0.36 Median Pct Recovery = 64% Expected Conc. = 0.36 Median Pct Recovery = 64% Expected Conc. = 0.36 Median Pct Recovery = 64% Expected Conc. = 0.2984 Median Pct Recovery = 64% Expected Conc. = 0.2984 Median Pct Recovery = 64% Expected Conc. = 0.243 Median Pct Recovery = 64% Expected Conc. = 0.243 Median Pct Recovery = 64% Expected Conc. = 0.24 Median Pct Recovery = 64% Expected Conc. = 0.24 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.18 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.1492 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Expected Conc. = 0.09 Median Pct Recovery = 64% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
THIOBENCARB
METHOD: 2033 , TESTIDCODE: 82681GCM35
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 61% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 102% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 78% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 96% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 61% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 66% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 68% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 93% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 74% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 71% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 62% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 56% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 64% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 72% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 73% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 53% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Expected Conc. = 0.1 Median Pct Recovery = 71% Expected Conc. = 0.096 Median Pct Recovery = 71% Expected Conc. = 0.096 Median Pct Recovery = 71% Expected Conc. = 0.096 Median Pct Recovery = 71% Expected Conc. = 0.096 Median Pct Recovery = 71% Expected Conc. = 0.0789 Median Pct Recovery = 71% Expected Conc. = 0.0789 Median Pct Recovery = 71% Expected Conc. = 0.0654 Median Pct Recovery = 71% Expected Conc. = 0.0654 Median Pct Recovery = 71% Expected Conc. = 0.0642 Median Pct Recovery = 71% Expected Conc. = 0.0642 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.048 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.04 Median Pct Recovery = 71% Expected Conc. = 0.0394 Median Pct Recovery = 71% Expected Conc. = 0.0394 Median Pct Recovery = 71% Expected Conc. = 0.0394 Median Pct Recovery = 71% Expected Conc. = 0.0394 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Expected Conc. = 0.024 Median Pct Recovery = 71% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
DACTHAL
METHOD: 2033 , TESTIDCODE: 82682GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 99% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 125% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 78% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 110% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 93% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 106% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 102% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 117% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 93% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 80% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 93% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 106% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 98% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 97% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Expected Conc. = 0.0456 Median Pct Recovery = 97% Expected Conc. = 0.0456 Median Pct Recovery = 97% Expected Conc. = 0.0456 Median Pct Recovery = 97% Expected Conc. = 0.0384 Median Pct Recovery = 97% Expected Conc. = 0.0384 Median Pct Recovery = 97% Expected Conc. = 0.03 Median Pct Recovery = 97% Expected Conc. = 0.03 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0228 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0192 Median Pct Recovery = 97% Expected Conc. = 0.0153 Median Pct Recovery = 97% Expected Conc. = 0.0153 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Expected Conc. = 0.0114 Median Pct Recovery = 97% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PENDIMETHALIN
METHOD: 2033 , TESTIDCODE: 82683GCM35
DATES: 01/31/15 - 12/20/16
Open Data Set

Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 81% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 65% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 79% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 90% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 90% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 102% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 84% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 96% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 82% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 98% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 101% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 114% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 92% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 147% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 86% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 98% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 123% Expected Conc. = 0.0725 Median Pct Recovery = 90% Expected Conc. = 0.0725 Median Pct Recovery = 90% Expected Conc. = 0.0725 Median Pct Recovery = 90% Expected Conc. = 0.052 Median Pct Recovery = 90% Expected Conc. = 0.052 Median Pct Recovery = 90% Expected Conc. = 0.0479 Median Pct Recovery = 90% Expected Conc. = 0.0479 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.0362 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.036 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.03 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.026 Median Pct Recovery = 90% Expected Conc. = 0.024 Median Pct Recovery = 90% Expected Conc. = 0.024 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.0181 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Expected Conc. = 0.018 Median Pct Recovery = 90% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
PROPARGITE
METHOD: 2033 , TESTIDCODE: 82685GCM35
DATES: 02/21/15 - 09/20/16
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 108% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 89% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 57% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 88% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 36% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 72% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 131% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 75% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 76% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 77% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 82% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Expected Conc. = 0.12 Median Pct Recovery = 82% Expected Conc. = 0.12 Median Pct Recovery = 82% Expected Conc. = 0.12 Median Pct Recovery = 82% Expected Conc. = 0.12 Median Pct Recovery = 82% Expected Conc. = 0.12 Median Pct Recovery = 82% Expected Conc. = 0.096 Median Pct Recovery = 82% Expected Conc. = 0.096 Median Pct Recovery = 82% Expected Conc. = 0.0804 Median Pct Recovery = 82% Expected Conc. = 0.0804 Median Pct Recovery = 82% Expected Conc. = 0.0798 Median Pct Recovery = 82% Expected Conc. = 0.0798 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.06 Median Pct Recovery = 82% Expected Conc. = 0.048 Median Pct Recovery = 82% Expected Conc. = 0.048 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.03 Median Pct Recovery = 82% Expected Conc. = 0.1004 Median Pct Recovery = 82% Expected Conc. = 0.1004 Median Pct Recovery = 82% Expected Conc. = 0.0502 Median Pct Recovery = 82% Expected Conc. = 0.0502 Median Pct Recovery = 82% Expected Conc. = 0.0502 Median Pct Recovery = 82% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
AZINPHOS-METHYL
METHOD: 2033 , TESTIDCODE: 82686GCM35
DATES: 02/21/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 01/21/16 SpikeMix = Abs 040615: 80 µl & Spex Organics EN150514012: 80 µl Pct Recovery = 57% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 60% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 86% Analysis Date = 03/31/15 SpikeMix = ERA 0227-14-08: 60 µl & Crescent 03DD006: 60 µl Pct Recovery = 76% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 64% Analysis Date = 09/05/15 SpikeMix = Spex Organics EN150513008: 40 µl & Abs 041415: 40 µl Pct Recovery = 63% Analysis Date = 07/21/15 SpikeMix = Abs 040615: 40 µl & Abs 041415: 40 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 61% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 81% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 56% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 77% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 45% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 59% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 60% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 63% Analysis Date = 02/02/16 SpikeMix = Spex Organics EN150513008: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 63% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 53% Expected Conc. = 0.75 Median Pct Recovery = 61% Expected Conc. = 0.72 Median Pct Recovery = 61% Expected Conc. = 0.72 Median Pct Recovery = 61% Expected Conc. = 0.72 Median Pct Recovery = 61% Expected Conc. = 0.72 Median Pct Recovery = 61% Expected Conc. = 0.6 Median Pct Recovery = 61% Expected Conc. = 0.6 Median Pct Recovery = 61% Expected Conc. = 0.6 Median Pct Recovery = 61% Expected Conc. = 0.6 Median Pct Recovery = 61% Expected Conc. = 0.4878 Median Pct Recovery = 61% Expected Conc. = 0.4878 Median Pct Recovery = 61% Expected Conc. = 0.4794 Median Pct Recovery = 61% Expected Conc. = 0.4794 Median Pct Recovery = 61% Expected Conc. = 0.3612 Median Pct Recovery = 61% Expected Conc. = 0.3612 Median Pct Recovery = 61% Expected Conc. = 0.3612 Median Pct Recovery = 61% Expected Conc. = 0.3612 Median Pct Recovery = 61% Expected Conc. = 0.3612 Median Pct Recovery = 61% Expected Conc. = 0.3612 Median Pct Recovery = 61% Expected Conc. = 0.36 Median Pct Recovery = 61% Expected Conc. = 0.36 Median Pct Recovery = 61% Expected Conc. = 0.36 Median Pct Recovery = 61% Expected Conc. = 0.36 Median Pct Recovery = 61% Expected Conc. = 0.3 Median Pct Recovery = 61% Expected Conc. = 0.3 Median Pct Recovery = 61% Expected Conc. = 0.3 Median Pct Recovery = 61% Expected Conc. = 0.3 Median Pct Recovery = 61% Expected Conc. = 0.3 Median Pct Recovery = 61% Expected Conc. = 0.3 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.1806 Median Pct Recovery = 61% Expected Conc. = 0.18 Median Pct Recovery = 61% Expected Conc. = 0.18 Median Pct Recovery = 61% Expected Conc. = 0.18 Median Pct Recovery = 61% Expected Conc. = 0.18 Median Pct Recovery = 61% Expected Conc. = 0.18 Median Pct Recovery = 61% Y = 1
The SGPlot Procedure

BQS OBSP Determination:
CIS-PERMETHRIN
METHOD: 2033 , TESTIDCODE: 82687GCM35
DATES: 01/31/15 - 01/18/17
Open Data Set

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 115% Analysis Date = 09/24/15 SpikeMix = ERA 0406-15-01: 80 µl & Abs 040615: 80 µl Pct Recovery = 63% Analysis Date = 09/17/15 SpikeMix = Spex Organics EN150514012: 80 µl & ERA 0406-15-01: 80 µl Pct Recovery = 56% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 51% Analysis Date = 02/21/15 SpikeMix = Spex Organics E1140407002: 60 µl & NSI 042814: 60 µl Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 06/17/15 SpikeMix = ChemService 3851600: 40 µl & Abs 040615: 40 µl Pct Recovery = 76% Analysis Date = 05/12/15 SpikeMix = Abs 041415: 40 µl & ChemService 3851600: 40 µl Pct Recovery = 73% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 66% Analysis Date = 02/09/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 02/08/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 54% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 42% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 38% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 78% Analysis Date = 01/31/15 SpikeMix = Supelco LC06435: 30 µl & Abs 032714: 30 µl Pct Recovery = 79% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 81% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 01/28/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 54% Analysis Date = 01/26/16 SpikeMix = ChemService 3851600: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 67% Analysis Date = 07/10/15 SpikeMix = Spex Organics EN150514012: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 139% Analysis Date = 08/19/15 SpikeMix = ERA 0406-15-01: 20 µl & Spex Organics EN150513008: 20 µl Pct Recovery = 62% Analysis Date = 07/31/15 SpikeMix = Abs 041415: 20 µl & ERA 0406-15-01: 20 µl Pct Recovery = 90% Expected Conc. = 0.062 Median Pct Recovery = 70% Expected Conc. = 0.0598 Median Pct Recovery = 70% Expected Conc. = 0.0598 Median Pct Recovery = 70% Expected Conc. = 0.0598 Median Pct Recovery = 70% Expected Conc. = 0.0598 Median Pct Recovery = 70% Expected Conc. = 0.0502 Median Pct Recovery = 70% Expected Conc. = 0.0502 Median Pct Recovery = 70% Expected Conc. = 0.0401 Median Pct Recovery = 70% Expected Conc. = 0.0401 Median Pct Recovery = 70% Expected Conc. = 0.032 Median Pct Recovery = 70% Expected Conc. = 0.032 Median Pct Recovery = 70% Expected Conc. = 0.032 Median Pct Recovery = 70% Expected Conc. = 0.032 Median Pct Recovery = 70% Expected Conc. = 0.032 Median Pct Recovery = 70% Expected Conc. = 0.032 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0299 Median Pct Recovery = 70% Expected Conc. = 0.0251 Median Pct Recovery = 70% Expected Conc. = 0.0251 Median Pct Recovery = 70% Expected Conc. = 0.0251 Median Pct Recovery = 70% Expected Conc. = 0.0251 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0248 Median Pct Recovery = 70% Expected Conc. = 0.0201 Median Pct Recovery = 70% Expected Conc. = 0.0201 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.016 Median Pct Recovery = 70% Expected Conc. = 0.0149 Median Pct Recovery = 70% Expected Conc. = 0.0149 Median Pct Recovery = 70% Expected Conc. = 0.0149 Median Pct Recovery = 70% Y = 1
The SGPlot Procedure