BQS Organic Blind Sample Program
Analytes by Multiple Methods
SITAGLIPTIN

Pct Recovery = 121% Schedule Code = 2440 Pct Recovery = 128% Schedule Code = 2440 Pct Recovery = 137% Schedule Code = 2440 Pct Recovery = 19% Schedule Code = 2440 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = LC9017 Minimum Whisker = 2% First Quartile = 3% Median = 6% Third Quartile = 41% Maximum Whisker = 82% Mean = 24% Standard Deviation = 25% Number of Observations = 19 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Schedule Code = 2440 Minimum Whisker = 37% First Quartile = 58% Median = 70% Third Quartile = 82% Maximum Whisker = 117% Mean = 72% Standard Deviation = 20% Number of Observations = 92 Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
SITAGLIPTIN

spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 195 Lab Value = 80.200 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 195 Lab Value = 4.810 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 195 Lab Value = 5.740 reportunit = ng/L spikemix = ERA 0823-11-05.2: 40 µl Expected Conc. = 389 Lab Value = 12.300 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl Expected Conc. = 194.5 Lab Value = 11.300 reportunit = ng/L spikemix = ERA 0823-11-05.2: 40 µl Expected Conc. = 389 Lab Value = 15.200 reportunit = ng/L spikemix = ERA 0823-11-05.2: 10 µl Expected Conc. = 97.25 Lab Value = 4.860 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl Expected Conc. = 194.5 Lab Value = 58.800 reportunit = ng/L spikemix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl Expected Conc. = 145.88 Lab Value = 85.900 reportunit = ng/L spikemix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl Expected Conc. = 145.88 Lab Value = 120.000 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl Expected Conc. = 194.5 Lab Value = 119.000 reportunit = ng/L spikemix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl Expected Conc. = 97.25 Lab Value = 3.420 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl Expected Conc. = 146.25 Lab Value = 50.100 reportunit = ng/L spikemix = Abs 071112: 40 µl Expected Conc. = 390 Lab Value = 8.780 reportunit = ng/L spikemix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 195 Lab Value = 68.600 reportunit = ng/L spikemix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 195 Lab Value = 5.950 reportunit = ng/L spikemix = Abs 071112: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 390 Lab Value = 9.390 reportunit = ng/L spikemix = Abs 071112: 20 µl & Abs 060112: 20 µl Expected Conc. = 195 Lab Value = 59.200 reportunit = ng/L spikemix = Abs 071112: 20 µl & Abs 053112: 20 µl Expected Conc. = 195 Lab Value = 80.300 reportunit = ng/L spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl Expected Conc. = 194.6 Lab Value = 112.000 reportunit = ng/L spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Expected Conc. = 486.5 Lab Value = 293.000 reportunit = ng/L spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Expected Conc. = 194.6 Lab Value = 111.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Expected Conc. = 194.6 Lab Value = 110.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 194.2 Lab Value = 97.200 reportunit = ng/L spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 485.5 Lab Value = 252.000 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 480.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 172.000 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 339.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 156.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 213.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 295.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 336.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 202.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 178.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Expected Conc. = 243.6 Lab Value = 133.000 reportunit = ng/L spikemix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Expected Conc. = 487.2 Lab Value = 364.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 243.6 Lab Value = 129.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 243.6 Lab Value = 167.000 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 487.2 Lab Value = 317.000 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 487.2 Lab Value = 324.000 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 609 Lab Value = 544.000 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 609 Lab Value = 498.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 243.6 Lab Value = 158.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 243.6 Lab Value = 200.000 reportunit = ng/L spikemix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 201.000 reportunit = ng/L spikemix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Expected Conc. = 585.44 Lab Value = 402.000 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 390 Lab Value = 458.000 reportunit = ng/L spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Expected Conc. = 390 Lab Value = 269.000 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 390.98 Lab Value = 273.000 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 390.98 Lab Value = 314.000 reportunit = ng/L spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Expected Conc. = 208.52 Lab Value = 157.000 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Expected Conc. = 195 Lab Value = 149.000 reportunit = ng/L spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 208 Lab Value = 203.000 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 390 Lab Value = 321.000 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Expected Conc. = 390 Lab Value = 328.000 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Expected Conc. = 390 Lab Value = 440.000 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Expected Conc. = 390 Lab Value = 209.000 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Expected Conc. = 195 Lab Value = 96.000 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 324.000 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 332.000 reportunit = ng/L spikemix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 188.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Expected Conc. = 194.6 Lab Value = 125.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Expected Conc. = 776.8 Lab Value = 648.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 485.5 Lab Value = 353.000 reportunit = ng/L spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 485.5 Lab Value = 259.000 reportunit = ng/L spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Expected Conc. = 485.5 Lab Value = 370.000 reportunit = ng/L spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Expected Conc. = 776.8 Lab Value = 631.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 194.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 169.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 205.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 243.000 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 408.000 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 402.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 182.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 200.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 89.700 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 609 Lab Value = 488.000 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 609 Lab Value = 446.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 154.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 165.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 155.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 172.000 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 370.000 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 399.000 reportunit = ng/L spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 194.2 Lab Value = 98.300 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 433.000 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 73.18 Lab Value = 58.500 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 73.18 Lab Value = 94.000 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 585.44 Lab Value = 433.000 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 585.44 Lab Value = 109.000 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 146.36 Lab Value = 72.500 reportunit = ng/L spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl Expected Conc. = 292.72 Lab Value = 159.000 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 146.36 Lab Value = 81.100 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 050115: 20 µl Expected Conc. = 146.36 Lab Value = 80.500 reportunit = ng/L spikemix = Abs 050115: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 179.000 reportunit = ng/L spikemix = Abs 050115: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 170.000 reportunit = ng/L spikemix = Abs 050115: 20 µl & Abs 051315: 20 µl Expected Conc. = 146.36 Lab Value = 80.600 reportunit = ng/L spikemix = Abs 050115: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 192.000 reportunit = ng/L spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 390 Lab Value = 388.000 reportunit = ng/L spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Expected Conc. = 208 Lab Value = 203.000 reportunit = ng/L spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Expected Conc. = 195 Lab Value = 193.000 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 195.49 Lab Value = 85.100 reportunit = ng/L spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl Expected Conc. = 390.98 Lab Value = 308.000 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 195.49 Lab Value = 82.700 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 208.52 Lab Value = 179.000 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 208.52 Lab Value = 159.000 reportunit = ng/L spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 390.98 Lab Value = 337.000 reportunit = ng/L spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Expected Conc. = 195.49 Lab Value = 121.000 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 195.49 Lab Value = 87.400 reportunit = ng/L spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl Expected Conc. = 390.98 Lab Value = 195.000 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 195.49 Lab Value = 106.000 reportunit = ng/L Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
SITAGLIPTIN

spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 195 Lab Value = 80.200 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 195 Lab Value = 4.810 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 195 Lab Value = 5.740 reportunit = ng/L spikemix = ERA 0823-11-05.2: 40 µl Expected Conc. = 389 Lab Value = 12.300 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl Expected Conc. = 194.5 Lab Value = 11.300 reportunit = ng/L spikemix = ERA 0823-11-05.2: 40 µl Expected Conc. = 389 Lab Value = 15.200 reportunit = ng/L spikemix = ERA 0823-11-05.2: 10 µl Expected Conc. = 97.25 Lab Value = 4.860 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl Expected Conc. = 194.5 Lab Value = 58.800 reportunit = ng/L spikemix = ERA 0823-11-05.2: 15 µl & ERA 0507-12-06.1: 15 µl Expected Conc. = 145.88 Lab Value = 85.900 reportunit = ng/L spikemix = ERA 0823-11-05.2: 15 µl & Abs 060112: 15 µl Expected Conc. = 145.88 Lab Value = 120.000 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl Expected Conc. = 194.5 Lab Value = 119.000 reportunit = ng/L spikemix = ERA 0823-11-05.2: 10 µl & Abs 053112: 10 µl Expected Conc. = 97.25 Lab Value = 3.420 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl Expected Conc. = 146.25 Lab Value = 50.100 reportunit = ng/L spikemix = Abs 071112: 40 µl Expected Conc. = 390 Lab Value = 8.780 reportunit = ng/L spikemix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 195 Lab Value = 68.600 reportunit = ng/L spikemix = Abs 071112: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 195 Lab Value = 5.950 reportunit = ng/L spikemix = Abs 071112: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 390 Lab Value = 9.390 reportunit = ng/L spikemix = Abs 071112: 20 µl & Abs 060112: 20 µl Expected Conc. = 195 Lab Value = 59.200 reportunit = ng/L spikemix = Abs 071112: 20 µl & Abs 053112: 20 µl Expected Conc. = 195 Lab Value = 80.300 reportunit = ng/L spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl Expected Conc. = 194.6 Lab Value = 112.000 reportunit = ng/L spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Expected Conc. = 486.5 Lab Value = 293.000 reportunit = ng/L spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Expected Conc. = 194.6 Lab Value = 111.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Expected Conc. = 194.6 Lab Value = 110.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 194.2 Lab Value = 97.200 reportunit = ng/L spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 485.5 Lab Value = 252.000 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 480.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 172.000 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 339.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 156.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 213.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 295.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 336.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 202.000 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 178.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Expected Conc. = 243.6 Lab Value = 133.000 reportunit = ng/L spikemix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Expected Conc. = 487.2 Lab Value = 364.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 243.6 Lab Value = 129.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 243.6 Lab Value = 167.000 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 487.2 Lab Value = 317.000 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 487.2 Lab Value = 324.000 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 609 Lab Value = 544.000 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 609 Lab Value = 498.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 243.6 Lab Value = 158.000 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 243.6 Lab Value = 200.000 reportunit = ng/L spikemix = ERA 0406-15-07A: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 201.000 reportunit = ng/L spikemix = ERA 0406-15-07A: 80 µl & Abs 051315: 80 µl Expected Conc. = 585.44 Lab Value = 402.000 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 390 Lab Value = 458.000 reportunit = ng/L spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Expected Conc. = 390 Lab Value = 269.000 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 390.98 Lab Value = 273.000 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 390.98 Lab Value = 314.000 reportunit = ng/L spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Expected Conc. = 208.52 Lab Value = 157.000 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Expected Conc. = 195 Lab Value = 149.000 reportunit = ng/L spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 208 Lab Value = 203.000 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 390 Lab Value = 321.000 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Expected Conc. = 390 Lab Value = 328.000 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Expected Conc. = 390 Lab Value = 440.000 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Expected Conc. = 390 Lab Value = 209.000 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Expected Conc. = 195 Lab Value = 96.000 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 324.000 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 487.2 Lab Value = 332.000 reportunit = ng/L spikemix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 188.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Expected Conc. = 194.6 Lab Value = 125.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Expected Conc. = 776.8 Lab Value = 648.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 485.5 Lab Value = 353.000 reportunit = ng/L spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 485.5 Lab Value = 259.000 reportunit = ng/L spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Expected Conc. = 485.5 Lab Value = 370.000 reportunit = ng/L spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Expected Conc. = 776.8 Lab Value = 631.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 194.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 169.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 205.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 244.6 Lab Value = 243.000 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 408.000 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 402.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 182.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 200.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 89.700 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 609 Lab Value = 488.000 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 609 Lab Value = 446.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 154.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 243.6 Lab Value = 165.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 155.000 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 244.6 Lab Value = 172.000 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 370.000 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 399.000 reportunit = ng/L spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 194.2 Lab Value = 98.300 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 489.2 Lab Value = 433.000 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 73.18 Lab Value = 58.500 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 73.18 Lab Value = 94.000 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 585.44 Lab Value = 433.000 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 585.44 Lab Value = 109.000 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 146.36 Lab Value = 72.500 reportunit = ng/L spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl Expected Conc. = 292.72 Lab Value = 159.000 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 146.36 Lab Value = 81.100 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 050115: 20 µl Expected Conc. = 146.36 Lab Value = 80.500 reportunit = ng/L spikemix = Abs 050115: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 179.000 reportunit = ng/L spikemix = Abs 050115: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 170.000 reportunit = ng/L spikemix = Abs 050115: 20 µl & Abs 051315: 20 µl Expected Conc. = 146.36 Lab Value = 80.600 reportunit = ng/L spikemix = Abs 050115: 40 µl & Abs 051315: 40 µl Expected Conc. = 292.72 Lab Value = 192.000 reportunit = ng/L spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 390 Lab Value = 388.000 reportunit = ng/L spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Expected Conc. = 208 Lab Value = 203.000 reportunit = ng/L spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Expected Conc. = 195 Lab Value = 193.000 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 195.49 Lab Value = 85.100 reportunit = ng/L spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl Expected Conc. = 390.98 Lab Value = 308.000 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 195.49 Lab Value = 82.700 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 208.52 Lab Value = 179.000 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 208.52 Lab Value = 159.000 reportunit = ng/L spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 390.98 Lab Value = 337.000 reportunit = ng/L spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Expected Conc. = 195.49 Lab Value = 121.000 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 195.49 Lab Value = 87.400 reportunit = ng/L spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl Expected Conc. = 390.98 Lab Value = 195.000 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 195.49 Lab Value = 106.000 reportunit = ng/L Y = 1
The SGPlot Procedure