BQS Organic Blind Sample Program
Analytes by Multiple Methods
FEXOFENADINE

Pct Recovery = 154% Schedule Code = LC9017 Pct Recovery = 93% Schedule Code = 2440 Pct Recovery = 94% Schedule Code = 2440 Pct Recovery = 96% Schedule Code = 2440 Pct Recovery = 97% Schedule Code = 2440 Pct Recovery = 100% Schedule Code = 2440 Pct Recovery = 104% Schedule Code = 2440 Pct Recovery = 104% Schedule Code = 2440 Pct Recovery = 31% Schedule Code = 2440 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = LC9017 Minimum Whisker = 48% First Quartile = 51% Median = 58% Third Quartile = 74% Maximum Whisker = 104% Mean = 68% Standard Deviation = 28% Number of Observations = 15 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Schedule Code = 2440 Minimum Whisker = 44% First Quartile = 59% Median = 63% Third Quartile = 71% Maximum Whisker = 87% Mean = 66% Standard Deviation = 13% Number of Observations = 101 Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
FEXOFENADINE

spikemix = Spex Organics T1120802015: 40 µl Expected Conc. = 80 Lab Value = 48.000 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 40 Lab Value = 19.400 reportunit = ng/L spikemix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 80 Lab Value = 60.300 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 40 Lab Value = 21.300 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 40 Lab Value = 28.900 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 40 Lab Value = 29.000 reportunit = ng/L spikemix = ERA 0823-11-05.1: 40 µl Expected Conc. = 78.7 Lab Value = 41.100 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl Expected Conc. = 39.35 Lab Value = 60.500 reportunit = ng/L spikemix = ERA 0823-11-05.1: 40 µl Expected Conc. = 78.7 Lab Value = 81.800 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl Expected Conc. = 39.35 Lab Value = 18.700 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 39.35 Lab Value = 19.200 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl Expected Conc. = 29.513 Lab Value = 15.100 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl Expected Conc. = 29.513 Lab Value = 15.300 reportunit = ng/L spikemix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl Expected Conc. = 78.7 Lab Value = 45.700 reportunit = ng/L spikemix = Abs 060112: 10 µl & Spex Organics T1120802015: 10 µl Expected Conc. = 20 Lab Value = 14.800 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 40 Lab Value = 23.700 reportunit = ng/L spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl Expected Conc. = 193.2 Lab Value = 179.000 reportunit = ng/L spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Expected Conc. = 483 Lab Value = 501.000 reportunit = ng/L spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Expected Conc. = 193.2 Lab Value = 181.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Expected Conc. = 193.2 Lab Value = 124.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 192.2 Lab Value = 165.000 reportunit = ng/L spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 480.5 Lab Value = 397.000 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 61.400 reportunit = ng/L spikemix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Expected Conc. = 49.6 Lab Value = 32.800 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 60.300 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 34.600 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 34.300 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 41.500 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 49.700 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 35.200 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 35.800 reportunit = ng/L spikemix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Expected Conc. = 49.6 Lab Value = 30.800 reportunit = ng/L spikemix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Expected Conc. = 99.2 Lab Value = 60.500 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.6 Lab Value = 32.100 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.6 Lab Value = 31.400 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 99.2 Lab Value = 52.300 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 99.2 Lab Value = 53.400 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 124 Lab Value = 79.400 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 124 Lab Value = 82.400 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.6 Lab Value = 30.600 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.6 Lab Value = 29.700 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 30 Lab Value = 9.300 reportunit = ng/L spikemix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Expected Conc. = 120 Lab Value = 73.100 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Expected Conc. = 30 Lab Value = 19.300 reportunit = ng/L spikemix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Expected Conc. = 60 Lab Value = 40.000 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Expected Conc. = 30 Lab Value = 14.300 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Expected Conc. = 60 Lab Value = 35.900 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Expected Conc. = 59.92 Lab Value = 39.900 reportunit = ng/L spikemix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Expected Conc. = 119.84 Lab Value = 73.800 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 20.200 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 80.7 Lab Value = 39.700 reportunit = ng/L spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Expected Conc. = 80.7 Lab Value = 56.100 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 79.965 Lab Value = 45.600 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 79.965 Lab Value = 44.500 reportunit = ng/L spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Expected Conc. = 42.648 Lab Value = 25.900 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Expected Conc. = 40.35 Lab Value = 24.000 reportunit = ng/L spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 43.04 Lab Value = 24.100 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 80.7 Lab Value = 48.400 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Expected Conc. = 80.7 Lab Value = 40.600 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Expected Conc. = 80.7 Lab Value = 54.900 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Expected Conc. = 80.7 Lab Value = 48.300 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Expected Conc. = 40.35 Lab Value = 23.000 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 57.800 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 46.500 reportunit = ng/L spikemix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 30.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Expected Conc. = 193.2 Lab Value = 200.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Expected Conc. = 768.8 Lab Value = 624.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 480.5 Lab Value = 373.000 reportunit = ng/L spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 480.5 Lab Value = 352.000 reportunit = ng/L spikemix = Abs 071817Pharm: 20 µl & ERA 06281702: 20 µl Expected Conc. = 192.2 Lab Value = 117.000 reportunit = ng/L spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Expected Conc. = 480.5 Lab Value = 362.000 reportunit = ng/L spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Expected Conc. = 768.8 Lab Value = 742.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 39.700 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 47.900 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 36.100 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 33.100 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 63.900 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 68.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 34.100 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 31.600 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 124 Lab Value = 75.700 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 124 Lab Value = 80.200 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 49.6 Lab Value = 24.400 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 49.6 Lab Value = 23.800 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 29.700 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 30.800 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 78.000 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 75.000 reportunit = ng/L spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 192.2 Lab Value = 108.000 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 71.400 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 29.96 Lab Value = 15.200 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 29.96 Lab Value = 13.600 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 29.96 Lab Value = 20.700 reportunit = ng/L spikemix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Expected Conc. = 59.92 Lab Value = 41.000 reportunit = ng/L spikemix = Abs 052215: 40 µl & Abs 050115: 40 µl Expected Conc. = 59.92 Lab Value = 37.000 reportunit = ng/L spikemix = Abs 052215: 80 µl & Abs 050115: 80 µl Expected Conc. = 119.84 Lab Value = 87.400 reportunit = ng/L spikemix = Abs 052215: 20 µl & Abs 050115: 20 µl Expected Conc. = 29.96 Lab Value = 17.000 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 15 Lab Value = 7.640 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 120 Lab Value = 69.500 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 22.300 reportunit = ng/L spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl Expected Conc. = 59.92 Lab Value = 31.300 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 16.900 reportunit = ng/L spikemix = Abs 050115: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 18.100 reportunit = ng/L spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 80.7 Lab Value = 51.500 reportunit = ng/L spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Expected Conc. = 43.04 Lab Value = 26.100 reportunit = ng/L spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Expected Conc. = 40.35 Lab Value = 17.700 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 39.983 Lab Value = 26.900 reportunit = ng/L spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl Expected Conc. = 79.965 Lab Value = 69.200 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 39.983 Lab Value = 26.500 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 42.648 Lab Value = 20.000 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 42.648 Lab Value = 26.500 reportunit = ng/L spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 79.965 Lab Value = 44.600 reportunit = ng/L spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Expected Conc. = 39.983 Lab Value = 24.400 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 39.983 Lab Value = 26.000 reportunit = ng/L spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl Expected Conc. = 79.965 Lab Value = 58.200 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 39.983 Lab Value = 30.900 reportunit = ng/L Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
FEXOFENADINE

spikemix = Spex Organics T1120802015: 40 µl Expected Conc. = 80 Lab Value = 48.000 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 40 Lab Value = 19.400 reportunit = ng/L spikemix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 80 Lab Value = 60.300 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 40 Lab Value = 21.300 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 40 Lab Value = 28.900 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & Abs 071112: 20 µl Expected Conc. = 40 Lab Value = 29.000 reportunit = ng/L spikemix = ERA 0823-11-05.1: 40 µl Expected Conc. = 78.7 Lab Value = 41.100 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl Expected Conc. = 39.35 Lab Value = 60.500 reportunit = ng/L spikemix = ERA 0823-11-05.1: 40 µl Expected Conc. = 78.7 Lab Value = 81.800 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl Expected Conc. = 39.35 Lab Value = 18.700 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 39.35 Lab Value = 19.200 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 071112: 15 µl Expected Conc. = 29.513 Lab Value = 15.100 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 060112: 15 µl Expected Conc. = 29.513 Lab Value = 15.300 reportunit = ng/L spikemix = ERA 0823-11-05.1: 40 µl & Abs 060112: 40 µl Expected Conc. = 78.7 Lab Value = 45.700 reportunit = ng/L spikemix = Abs 060112: 10 µl & Spex Organics T1120802015: 10 µl Expected Conc. = 20 Lab Value = 14.800 reportunit = ng/L spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 40 Lab Value = 23.700 reportunit = ng/L spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl Expected Conc. = 193.2 Lab Value = 179.000 reportunit = ng/L spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Expected Conc. = 483 Lab Value = 501.000 reportunit = ng/L spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Expected Conc. = 193.2 Lab Value = 181.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Expected Conc. = 193.2 Lab Value = 124.000 reportunit = ng/L spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 192.2 Lab Value = 165.000 reportunit = ng/L spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 480.5 Lab Value = 397.000 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 61.400 reportunit = ng/L spikemix = ERA 04281604: 40 µl & ERA 04281603: 40 µl Expected Conc. = 49.6 Lab Value = 32.800 reportunit = ng/L spikemix = ERA 04281604: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 60.300 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 34.600 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 34.300 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 41.500 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 49.700 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 35.200 reportunit = ng/L spikemix = ERA 04281604: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 35.800 reportunit = ng/L spikemix = ERA 04281603: 40 µl & ERA 04281604: 40 µl Expected Conc. = 49.6 Lab Value = 30.800 reportunit = ng/L spikemix = ERA 04281603: 80 µl & ERA 04281604: 80 µl Expected Conc. = 99.2 Lab Value = 60.500 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.6 Lab Value = 32.100 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.6 Lab Value = 31.400 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 99.2 Lab Value = 52.300 reportunit = ng/L spikemix = ERA 04281603: 80 µl & Crescent EN160610015: 80 µl Expected Conc. = 99.2 Lab Value = 53.400 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 124 Lab Value = 79.400 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 124 Lab Value = 82.400 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.6 Lab Value = 30.600 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.6 Lab Value = 29.700 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 30 Lab Value = 9.300 reportunit = ng/L spikemix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Expected Conc. = 120 Lab Value = 73.100 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Expected Conc. = 30 Lab Value = 19.300 reportunit = ng/L spikemix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Expected Conc. = 60 Lab Value = 40.000 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Expected Conc. = 30 Lab Value = 14.300 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Expected Conc. = 60 Lab Value = 35.900 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Expected Conc. = 59.92 Lab Value = 39.900 reportunit = ng/L spikemix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Expected Conc. = 119.84 Lab Value = 73.800 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 20.200 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 80.7 Lab Value = 39.700 reportunit = ng/L spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Expected Conc. = 80.7 Lab Value = 56.100 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 79.965 Lab Value = 45.600 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 79.965 Lab Value = 44.500 reportunit = ng/L spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Expected Conc. = 42.648 Lab Value = 25.900 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Expected Conc. = 40.35 Lab Value = 24.000 reportunit = ng/L spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 43.04 Lab Value = 24.100 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 80.7 Lab Value = 48.400 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Expected Conc. = 80.7 Lab Value = 40.600 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Expected Conc. = 80.7 Lab Value = 54.900 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Expected Conc. = 80.7 Lab Value = 48.300 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & Abs 041714: 30 µl Expected Conc. = 40.35 Lab Value = 23.000 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 57.800 reportunit = ng/L spikemix = Crescent EN160610015: 80 µl & ERA 04281603: 80 µl Expected Conc. = 99.2 Lab Value = 46.500 reportunit = ng/L spikemix = Crescent EN160610015: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 30.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Expected Conc. = 193.2 Lab Value = 200.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Expected Conc. = 768.8 Lab Value = 624.000 reportunit = ng/L spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 480.5 Lab Value = 373.000 reportunit = ng/L spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 480.5 Lab Value = 352.000 reportunit = ng/L spikemix = Abs 071817Pharm: 20 µl & ERA 06281702: 20 µl Expected Conc. = 192.2 Lab Value = 117.000 reportunit = ng/L spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Expected Conc. = 480.5 Lab Value = 362.000 reportunit = ng/L spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Expected Conc. = 768.8 Lab Value = 742.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 39.700 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 47.900 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 36.100 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Crescent EN160610015: 40 µl Expected Conc. = 49.88 Lab Value = 33.100 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 63.900 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 68.000 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 34.100 reportunit = ng/L spikemix = Abs 061516PHARM: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 31.600 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 124 Lab Value = 75.700 reportunit = ng/L spikemix = Abs 061416: 100 µl & ERA 04281603: 100 µl Expected Conc. = 124 Lab Value = 80.200 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 49.6 Lab Value = 24.400 reportunit = ng/L spikemix = Abs 061416: 40 µl & ERA 04281603: 40 µl Expected Conc. = 49.6 Lab Value = 23.800 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 29.700 reportunit = ng/L spikemix = Abs 061416: 40 µl & Abs 061516PHARM: 40 µl Expected Conc. = 49.88 Lab Value = 30.800 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 78.000 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 75.000 reportunit = ng/L spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 192.2 Lab Value = 108.000 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 99.76 Lab Value = 71.400 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 29.96 Lab Value = 15.200 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 29.96 Lab Value = 13.600 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 29.96 Lab Value = 20.700 reportunit = ng/L spikemix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Expected Conc. = 59.92 Lab Value = 41.000 reportunit = ng/L spikemix = Abs 052215: 40 µl & Abs 050115: 40 µl Expected Conc. = 59.92 Lab Value = 37.000 reportunit = ng/L spikemix = Abs 052215: 80 µl & Abs 050115: 80 µl Expected Conc. = 119.84 Lab Value = 87.400 reportunit = ng/L spikemix = Abs 052215: 20 µl & Abs 050115: 20 µl Expected Conc. = 29.96 Lab Value = 17.000 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 15 Lab Value = 7.640 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 120 Lab Value = 69.500 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 22.300 reportunit = ng/L spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl Expected Conc. = 59.92 Lab Value = 31.300 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 16.900 reportunit = ng/L spikemix = Abs 050115: 20 µl & Abs 052215: 20 µl Expected Conc. = 29.96 Lab Value = 18.100 reportunit = ng/L spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 80.7 Lab Value = 51.500 reportunit = ng/L spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Expected Conc. = 43.04 Lab Value = 26.100 reportunit = ng/L spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Expected Conc. = 40.35 Lab Value = 17.700 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 39.983 Lab Value = 26.900 reportunit = ng/L spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl Expected Conc. = 79.965 Lab Value = 69.200 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 39.983 Lab Value = 26.500 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 42.648 Lab Value = 20.000 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 42.648 Lab Value = 26.500 reportunit = ng/L spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 79.965 Lab Value = 44.600 reportunit = ng/L spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Expected Conc. = 39.983 Lab Value = 24.400 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 39.983 Lab Value = 26.000 reportunit = ng/L spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl Expected Conc. = 79.965 Lab Value = 58.200 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 39.983 Lab Value = 30.900 reportunit = ng/L Y = 1
The SGPlot Procedure