OBSP Determination:
11-KETOTESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64467GM006

The SGPlot Procedure

Sample Statistics
11-KETOTESTOSTERONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

OBSP Determination:
17-ALPHA-ESTRADIOL
METHOD: 6434 , TESTIDCODE: 64468GM006

The SGPlot Procedure

Sample Statistics
17-ALPHA-ESTRADIOL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
17-ALPHA-ETHYNYLESTRADIOL
METHOD: 6434 , TESTIDCODE: 63207GM006

Analysis Date = 04/19/17 SpikeMix = ERA 04121615: 0 µl & ERA 04121614: 0 µl Pct Recovery = 52% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
17-ALPHA-ETHYNYLESTRADIOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 52% . 52% 0%
Total 1 52% . 52% 0%

Sample Statistics
17-ALPHA-ETHYNYLESTRADIOL

Characteristic N % % Basis
Plotted 1 50% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 1 50% 1 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
17-BETA-ESTRADIOL
METHOD: 6434 , TESTIDCODE: 63164GM006

The SGPlot Procedure

Sample Statistics
17-BETA-ESTRADIOL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
3-BETA-COPROSTANOL
METHOD: 6434 , TESTIDCODE: 63170GM006

Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 50% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-BETA-COPROSTANOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 50% . 50% 0%
Total 1 50% . 50% 0%

Sample Statistics
3-BETA-COPROSTANOL

Characteristic N % % Basis
Plotted 1 50% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 1 50% 1 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
4-ANDROSTENE-3,17-DIONE
METHOD: 6434 , TESTIDCODE: 64473GM006

The SGPlot Procedure

Sample Statistics
4-ANDROSTENE-3,17-DIONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

OBSP Determination:
BISPHENOL A
METHOD: 6434 , TESTIDCODE: 63188GM006

The SGPlot Procedure

Sample Statistics
BISPHENOL A

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
CHOLESTEROL
METHOD: 6434 , TESTIDCODE: 63196GM006

The SGPlot Procedure

Sample Statistics
CHOLESTEROL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 33% Spiked
Spiked 3 .  
False Negatives 2 67% 2 out of 3
Not Spiked 1 .  
False Positives 0 0% 0 out of 1

OBSP Determination:
CIS-ANDROSTERONE
METHOD: 6434 , TESTIDCODE: 63607GM006

Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 60% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-ANDROSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 60% . 60% 0%
Total 1 60% . 60% 0%

Sample Statistics
CIS-ANDROSTERONE

Characteristic N % % Basis
Plotted 1 33% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 67% Spiked
Spiked 3 .  
False Negatives 0 0% 0 out of 3
Not Spiked 1 .  
False Positives 0 0% 0 out of 1

OBSP Determination:
DIHYDROTESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64484GM006

The SGPlot Procedure

Sample Statistics
DIHYDROTESTOSTERONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

OBSP Determination:
EPITESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64477GM006

Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 60% Analysis Date = 04/28/17 SpikeMix = ERA 04121615: 0 µl & ERA 04121613: 0 µl Pct Recovery = 71% Analysis Date = 05/24/17 SpikeMix = ERA 04121613: 0 µl Pct Recovery = 175% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EPITESTOSTERONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 3 102% 63% 71% 85%
Total 3 102% 63% 71% 85%

Sample Statistics
EPITESTOSTERONE

Characteristic N % % Basis
Plotted 3 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 3 .  
False Negatives 0 0% 0 out of 3
Not Spiked 1 .  
False Positives 0 0% 0 out of 1

OBSP Determination:
EQUILENIN
METHOD: 6434 , TESTIDCODE: 63204GM006

Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 26% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EQUILENIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 26% . 26% 0%
Total 1 26% . 26% 0%

Sample Statistics
EQUILENIN

Characteristic N % % Basis
Plotted 1 33% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 3 .  
False Negatives 2 67% 2 out of 3
Not Spiked 1 .  
False Positives 0 0% 0 out of 1

OBSP Determination:
EQUILIN
METHOD: 6434 , TESTIDCODE: 64479GM006

The SGPlot Procedure

Sample Statistics
EQUILIN

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
ESTRIOL
METHOD: 6434 , TESTIDCODE: 64480GM006

The SGPlot Procedure

Sample Statistics
ESTRIOL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
ESTRONE
METHOD: 6434 , TESTIDCODE: 63205GM006

Analysis Date = 04/19/17 SpikeMix = ERA 04121613: 0 µl & ERA 04121614: 0 µl Pct Recovery = 59% Analysis Date = 05/24/17 SpikeMix = ERA 04121613: 0 µl Pct Recovery = 125% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ESTRONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 2 92% 46% 92% 48%
Total 2 92% 46% 92% 48%

Sample Statistics
ESTRONE

Characteristic N % % Basis
Plotted 2 67% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 3 .  
False Negatives 1 33% 1 out of 3
Not Spiked 1 .  
False Positives 0 0% 0 out of 1

OBSP Determination:
MESTRANOL
METHOD: 6434 , TESTIDCODE: 63638GM006

The SGPlot Procedure

Sample Statistics
MESTRANOL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
NORETHINDRONE
METHOD: 6434 , TESTIDCODE: 63644GM006

The SGPlot Procedure

Sample Statistics
NORETHINDRONE

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 2 100% 2 out of 2
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
PROGESTERONE
METHOD: 6434 , TESTIDCODE: 63657GM006

The SGPlot Procedure

Sample Statistics
PROGESTERONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 2 50% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 2 .  
False Negatives 0 . 0 out of 0
Not Spiked 2 .  
False Positives 0 0% 0 out of 2

OBSP Determination:
TESTOSTERONE
METHOD: 6434 , TESTIDCODE: 64485GM006

The SGPlot Procedure

Sample Statistics
TESTOSTERONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 4 .  
False Positives 0 0% 0 out of 4

OBSP Determination:
TRANS-DIETHYLSTILBESTROL
METHOD: 6434 , TESTIDCODE: 63620GM006

The SGPlot Procedure

Sample Statistics
TRANS-DIETHYLSTILBESTROL

Characteristic N % % Basis
Plotted 0 0% Spiked
Estimated Values 0 0% Spiked
Deleted Values 2 50% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 1 100% 1 out of 1
Not Spiked 2 .  
False Positives 0 0% 0 out of 1