OBSP Spike Level Charts

OBSP Determination:

1,2,4-TRICHLOROBENZENE

METHOD: 5506 , TESTIDCODE: 64095GCM13

Plotted Points Statistics

1,2,4-TRICHLOROBENZENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	20%	10%	14%	6%
Total	9	20%	10%	14%	6%

Sample Statistics

1,2,4-TRICHLOROBENZENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	9	100%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	0	0%	0 out of 7

OBSP Determination:

1,2-DIMETHYLNAPHTHALENE

METHOD: 5506 , TESTIDCODE: 64097GCM13

Plotted Points Statistics

1,2-DIMETHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	33%	8%	31%	4%
Total	10	33%	8%	31%	4%

Sample Statistics

1,2-DIMETHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

1,6-DIMETHYLNAPHTHALENE

METHOD: 5506 , TESTIDCODE: 64099GCM13

Plotted Points Statistics

1,6-DIMETHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	31%	4%	30%	4%
Total	11	31%	4%	30%	4%

Sample Statistics

1,6-DIMETHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

1-METHYL-9H-FLUORENE

METHOD: 5506 , TESTIDCODE: 64100GCM13

Plotted Points Statistics

1-METHYL-9H-FLUORENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	36%	3%	35%	4%
Total	11	36%	3%	35%	4%

Sample Statistics

1-METHYL-9H-FLUORENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

1-METHYLPHENANTHRENE

METHOD: 5506 , TESTIDCODE: 64101GCM13

Plotted Points Statistics

1-METHYLPHENANTHRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	34%	4%	36%	4%
Total	11	34%	4%	36%	4%

Sample Statistics

1-METHYLPHENANTHRENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

1-METHYLPYRENE

METHOD: 5506 , TESTIDCODE: 64102GCM13

Plotted Points Statistics

1-METHYLPYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	45%	14%	43%	3%
Total	10	45%	14%	43%	3%

Sample Statistics

1-METHYLPYRENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

2,3,6-TRIMETHYLNAPHTHALENE

METHOD: 5506 , TESTIDCODE: 64103GCM13

Plotted Points Statistics

2,3,6-TRIMETHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	5	34%	2%	34%	1%
Total	5	34%	2%	34%	1%

Sample Statistics

2,3,6-TRIMETHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	5	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	6	.
False Negatives	0	0%	0 out of 5
Not Spiked	13	.
False Positives	0	0%	0 out of 11

OBSP Determination:

2,6-DIMETHYLNAPHTHALENE

METHOD: 5506 , TESTIDCODE: 63167GCM13

Plotted Points Statistics

2,6-DIMETHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	31%	4%	31%	4%
Total	11	31%	4%	31%	4%

Sample Statistics

2,6-DIMETHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

2-ETHYLNAPHTHALENE

METHOD: 5506 , TESTIDCODE: 64104GCM13

Plotted Points Statistics

2-ETHYLNAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	37%	13%	33%	8%
Total	9	37%	13%	33%	8%

Sample Statistics

2-ETHYLNAPHTHALENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	1	11%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	0	0%	0 out of 7

OBSP Determination:

2-METHYLANTHRACENE

METHOD: 5506 , TESTIDCODE: 64105GCM13

Plotted Points Statistics

2-METHYLANTHRACENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	3	31%	8%	31%	12%
Total	3	31%	8%	31%	12%

Sample Statistics

2-METHYLANTHRACENE

Characteristic	N	%	% Basis
Plotted	3	33%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	6	67%	6 out of 9
Not Spiked	7	.
False Positives	0	0%	0 out of 7

OBSP Determination:

4H-CYCLOPENTA[DEF]PHENANTHRENE

METHOD: 5506 , TESTIDCODE: 64106GCM13

Plotted Points Statistics

4H-CYCLOPENTA[DEF]PHENANTHRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	35%	12%	32%	6%
Total	10	35%	12%	32%	6%

Sample Statistics

4H-CYCLOPENTA[DEF]PHENANTHRENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

ACENAPHTHENE

METHOD: 5506 , TESTIDCODE: 64108GCM13

Plotted Points Statistics

ACENAPHTHENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	32%	7%	29%	2%
Total	10	32%	7%	29%	2%

Sample Statistics

ACENAPHTHENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	3	50%	3 out of 6

OBSP Determination:

ACENAPHTHYLENE

METHOD: 5506 , TESTIDCODE: 64109GCM13

Plotted Points Statistics

ACENAPHTHYLENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	26%	11%	22%	6%
Total	9	26%	11%	22%	6%

Sample Statistics

ACENAPHTHYLENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	0	0%	0 out of 7

OBSP Determination:

ANTHRACENE

METHOD: 5506 , TESTIDCODE: 63180GCM13

Plotted Points Statistics

ANTHRACENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	33%	4%	32%	4%
Total	11	33%	4%	32%	4%

Sample Statistics

ANTHRACENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

ANTHRAQUINONE

METHOD: 5506 , TESTIDCODE: 63181GCM13

Plotted Points Statistics

ANTHRAQUINONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	55%	26%	51%	24%
Total	10	55%	26%	51%	24%

Sample Statistics

ANTHRAQUINONE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	4	67%	4 out of 6

OBSP Determination:

BENZO[A]PYRENE

METHOD: 5506 , TESTIDCODE: 63183GCM13

Plotted Points Statistics

BENZO[A]PYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	37%	13%	36%	4%
Total	9	37%	13%	36%	4%

Sample Statistics

BENZO[A]PYRENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	5	71%	5 out of 7

OBSP Determination:

BENZO[B]FLUORANTHENE

METHOD: 5506 , TESTIDCODE: 64111GCM13

Plotted Points Statistics

BENZO[B]FLUORANTHENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	51%	17%	47%	11%
Total	9	51%	17%	47%	11%

Sample Statistics

BENZO[B]FLUORANTHENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	2	22%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	5	71%	5 out of 7

OBSP Determination:

BENZO[E]PYRENE

METHOD: 5506 , TESTIDCODE: 64112GCM13

Plotted Points Statistics

BENZO[E]PYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	44%	14%	39%	5%
Total	10	44%	14%	39%	5%

Sample Statistics

BENZO[E]PYRENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	1	10%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	3	50%	3 out of 6

OBSP Determination:

BENZO[GHI]PERYLENE

METHOD: 5506 , TESTIDCODE: 64113GCM13

Plotted Points Statistics

BENZO[GHI]PERYLENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	45%	19%	35%	7%
Total	9	45%	19%	35%	7%

Sample Statistics

BENZO[GHI]PERYLENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	6	86%	6 out of 7

OBSP Determination:

BENZO[K]FLUORANTHENE

METHOD: 5506 , TESTIDCODE: 64114GCM13

Plotted Points Statistics

BENZO[K]FLUORANTHENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	44%	16%	39%	7%
Total	10	44%	16%	39%	7%

Sample Statistics

BENZO[K]FLUORANTHENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	5	50%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	3	50%	3 out of 6

OBSP Determination:

BENZ[A]ANTHRACENE

METHOD: 5506 , TESTIDCODE: 63610GCM13

Plotted Points Statistics

BENZ[A]ANTHRACENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	44%	14%	40%	4%
Total	9	44%	14%	40%	4%

Sample Statistics

BENZ[A]ANTHRACENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	5	71%	5 out of 7

OBSP Determination:

BIS(2-ETHYLHEXYL) PHTHALATE

METHOD: 5506 , TESTIDCODE: 63187GCM13

Plotted Points Statistics

BIS(2-ETHYLHEXYL) PHTHALATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	6	108%	57%	90%	25%
Total	6	108%	57%	90%	25%

Sample Statistics

BIS(2-ETHYLHEXYL) PHTHALATE

Characteristic	N	%	% Basis
Plotted	6	60%	Spiked
Estimated Values	6	60%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	4	40%	4 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

CARBAZOLE

METHOD: 5506 , TESTIDCODE: 63194GCM13

Plotted Points Statistics

CARBAZOLE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	36%	5%	38%	6%
Total	11	36%	5%	38%	6%

Sample Statistics

CARBAZOLE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

CHRYSENE

METHOD: 5506 , TESTIDCODE: 64115GCM13

Plotted Points Statistics

CHRYSENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	41%	14%	37%	5%
Total	10	41%	14%	37%	5%

Sample Statistics

CHRYSENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	2	20%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	3	50%	3 out of 6

OBSP Determination:

DIBENZOTHIOPHENE

METHOD: 5506 , TESTIDCODE: 64117GCM13

Plotted Points Statistics

DIBENZOTHIOPHENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	6	36%	2%	37%	3%
Total	6	36%	2%	37%	3%

Sample Statistics

DIBENZOTHIOPHENE

Characteristic	N	%	% Basis
Plotted	6	55%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	5	45%	5 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

DIBENZ[A,H]ANTHRACENE

METHOD: 5506 , TESTIDCODE: 64116GCM13

Plotted Points Statistics

DIBENZ[A,H]ANTHRACENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	40%	10%	36%	13%
Total	11	40%	10%	36%	13%

Sample Statistics

DIBENZ[A,H]ANTHRACENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	11	100%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

DIETHYL PHTHALATE

METHOD: 5506 , TESTIDCODE: 63202GCM13

Plotted Points Statistics

DIETHYL PHTHALATE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	1	224%	.	224%	0%
Total	1	224%	.	224%	0%

Sample Statistics

DIETHYL PHTHALATE

Characteristic	N	%	% Basis
Plotted	1	10%	Spiked
Estimated Values	1	10%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	1	10%	Spiked
Spiked	12	.
False Negatives	8	80%	8 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

FLUORANTHENE

METHOD: 5506 , TESTIDCODE: 63208GCM13

Plotted Points Statistics

FLUORANTHENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	49%	13%	44%	12%
Total	9	49%	13%	44%	12%

Sample Statistics

FLUORANTHENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	6	86%	6 out of 7

OBSP Determination:

FLUORENE

METHOD: 5506 , TESTIDCODE: 64107GCM13

Plotted Points Statistics

FLUORENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	6	39%	14%	36%	6%
Total	6	39%	14%	36%	6%

Sample Statistics

FLUORENE

Characteristic	N	%	% Basis
Plotted	6	67%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	3	33%	3 out of 9
Not Spiked	7	.
False Positives	0	0%	0 out of 7

OBSP Determination:

HEXACHLOROBENZENE

METHOD: 5506 , TESTIDCODE: 63631GCM13

Plotted Points Statistics

HEXACHLOROBENZENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	30%	2%	30%	2%
Total	11	30%	2%	30%	2%

Sample Statistics

HEXACHLOROBENZENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

INDENO[1,2,3-CD]PYRENE

METHOD: 5506 , TESTIDCODE: 64118GCM13

Plotted Points Statistics

INDENO[1,2,3-CD]PYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	45%	20%	38%	9%
Total	9	45%	20%	38%	9%

Sample Statistics

INDENO[1,2,3-CD]PYRENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	9	100%	Spiked
Deleted Values	4	21%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	4	67%	4 out of 6

OBSP Determination:

NAPHTHALENE

METHOD: 5506 , TESTIDCODE: 63220GCM13

Plotted Points Statistics

NAPHTHALENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	9	32%	12%	28%	8%
Total	9	32%	12%	28%	8%

Sample Statistics

NAPHTHALENE

Characteristic	N	%	% Basis
Plotted	9	100%	Spiked
Estimated Values	8	89%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 9
Not Spiked	7	.
False Positives	0	0%	0 out of 7

OBSP Determination:

PENTACHLOROANISOLE

METHOD: 5506 , TESTIDCODE: 64119GCM13

Plotted Points Statistics

PENTACHLOROANISOLE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	32%	8%	30%	2%
Total	10	32%	8%	30%	2%

Sample Statistics

PENTACHLOROANISOLE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

PENTACHLORONITROBENZENE

METHOD: 5506 , TESTIDCODE: 63650GCM13

Plotted Points Statistics

PENTACHLORONITROBENZENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	7	25%	8%	24%	5%
Total	7	25%	8%	24%	5%

Sample Statistics

PENTACHLORONITROBENZENE

Characteristic	N	%	% Basis
Plotted	7	64%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	4	36%	4 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

PERYLENE

METHOD: 5506 , TESTIDCODE: 64120GCM13

Plotted Points Statistics

PERYLENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	28%	10%	24%	3%
Total	10	28%	10%	24%	3%

Sample Statistics

PERYLENE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	1	17%	1 out of 6

OBSP Determination:

PHENANTHRENE

METHOD: 5506 , TESTIDCODE: 63224GCM13

Plotted Points Statistics

PHENANTHRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	37%	4%	36%	5%
Total	11	37%	4%	36%	5%

Sample Statistics

PHENANTHRENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	2	18%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	0	0%	0 out of 5

OBSP Determination:

PHENANTHRIDINE

METHOD: 5506 , TESTIDCODE: 64121GCM13

Plotted Points Statistics

PHENANTHRIDINE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	10	39%	16%	36%	7%
Total	10	39%	16%	36%	7%

Sample Statistics

PHENANTHRIDINE

Characteristic	N	%	% Basis
Plotted	10	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 10
Not Spiked	7	.
False Positives	0	0%	0 out of 6

OBSP Determination:

PYRENE

METHOD: 5506 , TESTIDCODE: 63227GCM13

Plotted Points Statistics

PYRENE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	11	41%	5%	39%	5%
Total	11	41%	5%	39%	5%

Sample Statistics

PYRENE

Characteristic	N	%	% Basis
Plotted	11	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	3	16%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	12	.
False Negatives	0	0%	0 out of 11
Not Spiked	7	.
False Positives	3	60%	3 out of 5