OBSP Spike Level Charts

OBSP Determination:

11-KETOTESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64527GM005

Plotted Points Statistics

11-KETOTESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	102%	20%	106%	24%
>= Reporting Level	18	90%	25%	93%	15%
Total	22	92%	24%	96%	20%

Sample Statistics

11-KETOTESTOSTERONE

Characteristic	N	%	% Basis
Plotted	22	88%	Spiked
Estimated Values	2	8%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	2	8%	Spiked
Spiked	26	.
False Negatives	1	4%	1 out of 25
Not Spiked	21	.
False Positives	0	0%	0 out of 21

OBSP Determination:

17-ALPHA-ESTRADIOL

METHOD: 4434 , TESTIDCODE: 64528GM005

Plotted Points Statistics

17-ALPHA-ESTRADIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	80%	11%	78%	12%
>= Reporting Level	18	83%	12%	83%	8%
Total	22	82%	11%	82%	12%

Sample Statistics

17-ALPHA-ESTRADIOL

Characteristic	N	%	% Basis
Plotted	22	88%	Spiked
Estimated Values	2	8%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	1	4%	Spiked
Spiked	26	.
False Negatives	2	8%	2 out of 25
Not Spiked	21	.
False Positives	0	0%	0 out of 21

OBSP Determination:

17-ALPHA-ETHYNYLESTRADIOL

METHOD: 4434 , TESTIDCODE: 64529GM005

Plotted Points Statistics

17-ALPHA-ETHYNYLESTRADIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	3	71%	6%	69%	9%
>= Reporting Level	18	83%	16%	80%	16%
Total	21	81%	15%	78%	15%

Sample Statistics

17-ALPHA-ETHYNYLESTRADIOL

Characteristic	N	%	% Basis
Plotted	21	81%	Spiked
Estimated Values	2	8%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	3	12%	Spiked
Spiked	27	.
False Negatives	2	8%	2 out of 26
Not Spiked	20	.
False Positives	0	0%	0 out of 20

OBSP Determination:

17-BETA-ESTRADIOL

METHOD: 4434 , TESTIDCODE: 64530GM005

Plotted Points Statistics

17-BETA-ESTRADIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	24	80%	7%	79%	8%
Total	24	80%	7%	79%	8%

Sample Statistics

17-BETA-ESTRADIOL

Characteristic	N	%	% Basis
Plotted	24	92%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	27	.
False Negatives	2	8%	2 out of 26
Not Spiked	20	.
False Positives	3	15%	3 out of 20

OBSP Determination:

3-BETA-COPROSTANOL

METHOD: 4434 , TESTIDCODE: 64532GM005

Plotted Points Statistics

3-BETA-COPROSTANOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	21	67%	22%	71%	13%
Total	21	67%	22%	71%	13%

Sample Statistics

3-BETA-COPROSTANOL

Characteristic	N	%	% Basis
Plotted	21	84%	Spiked
Estimated Values	2	8%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	26	.
False Negatives	4	16%	4 out of 25
Not Spiked	21	.
False Positives	0	0%	0 out of 21

OBSP Determination:

4,4BISPHENOL F

METHOD: 4434 , TESTIDCODE: 51294GM005

Plotted Points Statistics

4,4BISPHENOL F

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	6	70%	19%	74%	26%
Total	6	70%	19%	74%	26%

Sample Statistics

4,4BISPHENOL F

Characteristic	N	%	% Basis
Plotted	6	100%	Spiked
Estimated Values	6	100%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	6	.
False Negatives	0	0%	0 out of 6
Not Spiked	41	.
False Positives	0	0%	0 out of 40

OBSP Determination:

4-ANDROSTENE-3,17-DIONE

METHOD: 4434 , TESTIDCODE: 64533GM005

Plotted Points Statistics

4-ANDROSTENE-3,17-DIONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	1	43%	.	43%	0%
>= Reporting Level	11	56%	13%	57%	9%
Total	12	55%	13%	56%	11%

Sample Statistics

4-ANDROSTENE-3,17-DIONE

Characteristic	N	%	% Basis
Plotted	12	71%	Spiked
Estimated Values	1	6%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	2	12%	Spiked
Spiked	17	.
False Negatives	3	18%	3 out of 17
Not Spiked	30	.
False Positives	0	0%	0 out of 29

OBSP Determination:

BISPHENOL A

METHOD: 4434 , TESTIDCODE: 67305GM005

Plotted Points Statistics

BISPHENOL A

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	27	73%	12%	72%	11%
Total	27	73%	12%	72%	11%

Sample Statistics

BISPHENOL A

Characteristic	N	%	% Basis
Plotted	27	100%	Spiked
Estimated Values	27	100%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	28	.
False Negatives	0	0%	0 out of 27
Not Spiked	19	.
False Positives	0	0%	0 out of 19

OBSP Determination:

CHOLESTEROL

METHOD: 4434 , TESTIDCODE: 64534GM005

Plotted Points Statistics

CHOLESTEROL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	27	76%	20%	81%	16%
Total	27	76%	20%	81%	16%

Sample Statistics

CHOLESTEROL

Characteristic	N	%	% Basis
Plotted	27	100%	Spiked
Estimated Values	4	15%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	28	.
False Negatives	0	0%	0 out of 27
Not Spiked	19	.
False Positives	0	0%	0 out of 19

OBSP Determination:

CIS-ANDROSTERONE

METHOD: 4434 , TESTIDCODE: 64535GM005

Plotted Points Statistics

CIS-ANDROSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	28	55%	6%	56%	5%
Total	28	55%	6%	56%	5%

Sample Statistics

CIS-ANDROSTERONE

Characteristic	N	%	% Basis
Plotted	28	97%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	29	.
False Negatives	1	3%	1 out of 29
Not Spiked	18	.
False Positives	0	0%	0 out of 17

OBSP Determination:

DIHYDROTESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64544GM005

Plotted Points Statistics

DIHYDROTESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	16	66%	18%	69%	7%
Total	16	66%	18%	69%	7%

Sample Statistics

DIHYDROTESTOSTERONE

Characteristic	N	%	% Basis
Plotted	16	89%	Spiked
Estimated Values	3	17%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	1	6%	Spiked
Spiked	18	.
False Negatives	1	6%	1 out of 18
Not Spiked	29	.
False Positives	0	0%	0 out of 28

OBSP Determination:

EPITESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64537GM005

Plotted Points Statistics

EPITESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	17	70%	24%	75%	13%
Total	17	70%	24%	75%	13%

Sample Statistics

EPITESTOSTERONE

Characteristic	N	%	% Basis
Plotted	17	94%	Spiked
Estimated Values	3	17%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	18	.
False Negatives	1	6%	1 out of 18
Not Spiked	29	.
False Positives	0	0%	0 out of 28

OBSP Determination:

EQUILENIN

METHOD: 4434 , TESTIDCODE: 64538GM005

Plotted Points Statistics

EQUILENIN

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	12	88%	57%	52%	68%
Total	12	88%	57%	52%	68%

Sample Statistics

EQUILENIN

Characteristic	N	%	% Basis
Plotted	12	100%	Spiked
Estimated Values	2	17%	Spiked
Deleted Values	1	3%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	13	.
False Negatives	0	0%	0 out of 12
Not Spiked	19	.
False Positives	5	26%	5 out of 19

OBSP Determination:

EQUILIN

METHOD: 4434 , TESTIDCODE: 64539GM005

Plotted Points Statistics

EQUILIN

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	26	47%	16%	51%	16%
Total	26	47%	16%	51%	16%

Sample Statistics

EQUILIN

Characteristic	N	%	% Basis
Plotted	26	96%	Spiked
Estimated Values	26	96%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	28	.
False Negatives	1	4%	1 out of 27
Not Spiked	19	.
False Positives	0	0%	0 out of 19

OBSP Determination:

ESTRIOL

METHOD: 4434 , TESTIDCODE: 64540GM005

Plotted Points Statistics

ESTRIOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	26	76%	12%	80%	14%
Total	26	76%	12%	80%	14%

Sample Statistics

ESTRIOL

Characteristic	N	%	% Basis
Plotted	26	100%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	27	.
False Negatives	0	0%	0 out of 26
Not Spiked	20	.
False Positives	0	0%	0 out of 20

OBSP Determination:

ESTRONE

METHOD: 4434 , TESTIDCODE: 64541GM005

Plotted Points Statistics

ESTRONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	28	66%	9%	64%	9%
Total	28	66%	9%	64%	9%

Sample Statistics

ESTRONE

Characteristic	N	%	% Basis
Plotted	28	97%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	29	.
False Negatives	1	3%	1 out of 29
Not Spiked	18	.
False Positives	0	0%	0 out of 17

OBSP Determination:

MESTRANOL

METHOD: 4434 , TESTIDCODE: 64542GM005

Plotted Points Statistics

MESTRANOL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	1	32%	.	32%	0%
>= Reporting Level	17	40%	8%	41%	6%
Total	18	40%	8%	40%	7%

Sample Statistics

MESTRANOL

Characteristic	N	%	% Basis
Plotted	18	69%	Spiked
Estimated Values	0	0%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	4	15%	Spiked
Spiked	27	.
False Negatives	4	15%	4 out of 26
Not Spiked	20	.
False Positives	0	0%	0 out of 20

OBSP Determination:

NORETHINDRONE

METHOD: 4434 , TESTIDCODE: 64531GM005

Plotted Points Statistics

NORETHINDRONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	80%	7%	79%	8%
>= Reporting Level	17	72%	18%	72%	10%
Total	21	74%	17%	74%	8%

Sample Statistics

NORETHINDRONE

Characteristic	N	%	% Basis
Plotted	21	84%	Spiked
Estimated Values	2	8%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	1	4%	Spiked
Spiked	26	.
False Negatives	3	12%	3 out of 25
Not Spiked	21	.
False Positives	0	0%	0 out of 21

OBSP Determination:

PROGESTERONE

METHOD: 4434 , TESTIDCODE: 64543GM005

Plotted Points Statistics

PROGESTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	26	38%	11%	37%	9%
Total	26	38%	11%	37%	9%

Sample Statistics

PROGESTERONE

Characteristic	N	%	% Basis
Plotted	26	90%	Spiked
Estimated Values	26	90%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	29	.
False Negatives	3	10%	3 out of 29
Not Spiked	18	.
False Positives	0	0%	0 out of 17

OBSP Determination:

TESTOSTERONE

METHOD: 4434 , TESTIDCODE: 64545GM005

Plotted Points Statistics

TESTOSTERONE

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
< Reporting Level	4	75%	18%	71%	20%
>= Reporting Level	12	70%	18%	71%	18%
Total	16	72%	17%	71%	18%

Sample Statistics

TESTOSTERONE

Characteristic	N	%	% Basis
Plotted	16	62%	Spiked
Estimated Values	1	4%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	2	8%	Spiked
Spiked	27	.
False Negatives	8	31%	8 out of 26
Not Spiked	20	.
False Positives	5	25%	5 out of 20

OBSP Determination:

TRANS-DIETHYLSTILBESTROL

METHOD: 4434 , TESTIDCODE: 64536GM005

Plotted Points Statistics

TRANS-DIETHYLSTILBESTROL

Spike Level	N	Mean	Std-Dev.	Median	F_Pseudo
>= Reporting Level	25	53%	13%	51%	8%
Total	25	53%	13%	51%	8%

Sample Statistics

TRANS-DIETHYLSTILBESTROL

Characteristic	N	%	% Basis
Plotted	25	86%	Spiked
Estimated Values	1	3%	Spiked
Deleted Values	1	2%	Spiked + Not Spiked
Spiked, Censored	0	0%	Spiked
Spiked	29	.
False Negatives	4	14%	4 out of 29
Not Spiked	18	.
False Positives	0	0%	0 out of 17