BQS OBSP Determination:
ACETONE
METHOD: 4024 , TESTIDCODE: 81552GCM60
Open Data Set

Analysis Date = 09/02/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 111% Analysis Date = 07/25/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 110% Analysis Date = 03/11/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 126% Analysis Date = 02/01/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 105% Analysis Date = 09/03/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 104% Analysis Date = 08/11/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 124% Analysis Date = 06/05/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 120% Analysis Date = 02/20/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 141% Analysis Date = 11/14/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 120% Analysis Date = 10/22/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 122% Analysis Date = 10/22/08 SpikeMix = Ultra CE-2889: 40 µl Pct Recovery = 103% Analysis Date = 09/10/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 112% Analysis Date = 03/03/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 123% Analysis Date = 02/28/13 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 110% Analysis Date = 12/03/12 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 149% Analysis Date = 03/26/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 97% Analysis Date = 01/31/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 96% Analysis Date = 08/31/05 SpikeMix = Absolute 071904VOC2: 25 µl Pct Recovery = 99% Analysis Date = 05/19/12 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 134% Analysis Date = 12/21/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 167% Analysis Date = 08/25/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 130% Analysis Date = 12/22/10 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 138% Analysis Date = 02/27/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 112% Analysis Date = 09/12/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 115% Analysis Date = 08/18/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 117% Analysis Date = 08/27/10 SpikeMix = Abs 083109VOA: 40 µl Pct Recovery = 103% Analysis Date = 08/18/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 112% Analysis Date = 07/03/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 127% Analysis Date = 05/19/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 112% Analysis Date = 03/11/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 79% Analysis Date = 11/05/04 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 110% Analysis Date = 08/25/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 110% Analysis Date = 05/18/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 112% Analysis Date = 08/29/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 114% Analysis Date = 07/28/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 104% Analysis Date = 06/09/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 114% Analysis Date = 12/19/06 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 112% Analysis Date = 06/26/13 SpikeMix = Crescent 04CC143: 20 µl Pct Recovery = 111% Analysis Date = 08/20/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 102% Analysis Date = 06/16/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 105% Analysis Date = 02/28/06 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 105% Analysis Date = 12/14/05 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 100% Analysis Date = 08/07/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 123% Analysis Date = 03/23/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 139% Analysis Date = 11/14/08 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 110% Analysis Date = 07/09/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 124% Analysis Date = 06/06/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 108% Analysis Date = 12/18/08 SpikeMix = Restek A062148: 20 µl Pct Recovery = 119% Analysis Date = 09/21/12 SpikeMix = NSI 060412-01: 10 µl Pct Recovery = 117% Analysis Date = 11/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 105% Analysis Date = 08/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 103% Analysis Date = 04/11/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 119% Analysis Date = 02/28/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 89% Analysis Date = 11/25/05 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 95% Analysis Date = 11/01/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 166% Analysis Date = 08/02/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 143% Analysis Date = 07/06/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 138% Analysis Date = 10/16/10 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 150% Analysis Date = 05/02/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 133% Analysis Date = 04/05/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 102% Analysis Date = 01/25/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 111% Analysis Date = 11/30/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 111% Analysis Date = 07/19/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 114% Analysis Date = 11/26/10 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 101% Analysis Date = 07/30/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 88% Analysis Date = 06/24/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 85% Analysis Date = 04/06/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 106% Analysis Date = 11/13/09 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 101% Analysis Date = 09/06/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 89% Analysis Date = 08/09/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 96% Analysis Date = 07/22/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 121% Analysis Date = 06/26/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 111% Analysis Date = 05/28/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 121% Analysis Date = 05/20/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 107% Analysis Date = 04/05/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 104% Analysis Date = 03/18/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 129% Analysis Date = 12/01/07 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 111% Analysis Date = 04/22/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 127% Analysis Date = 03/15/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 121% Analysis Date = 06/18/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 114% Analysis Date = 03/26/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 88% Analysis Date = 01/22/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 147% Analysis Date = 07/23/13 SpikeMix = NSI 042313VOA: 10 µl Pct Recovery = 171% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 101% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 83% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 97% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 115% Analysis Date = 04/07/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 97% Analysis Date = 11/30/04 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 110% Analysis Date = 05/04/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 95% Analysis Date = 01/12/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 100% Analysis Date = 10/29/05 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 100% Analysis Date = 08/09/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 120% Analysis Date = 04/11/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 120% Analysis Date = 02/01/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 95% Analysis Date = 10/29/05 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 95% Analysis Date = 08/21/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 112% Analysis Date = 07/11/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 102% Analysis Date = 05/24/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 112% Analysis Date = 02/15/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 122% Analysis Date = 11/18/06 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 82% Analysis Date = 09/22/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 100% Analysis Date = 07/04/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 110% Analysis Date = 03/28/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 100% Analysis Date = 02/09/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 110% Analysis Date = 07/23/13 Pct Recovery = 125% Analysis Date = 07/05/13 Pct Recovery = 125% Analysis Date = 07/05/13 Pct Recovery = 125% Analysis Date = 06/17/13 Pct Recovery = 125% Analysis Date = 06/17/13 Pct Recovery = 125% Analysis Date = 05/30/13 Pct Recovery = 125% Analysis Date = 05/30/13 Pct Recovery = 125% Analysis Date = 05/12/13 Pct Recovery = 125% Analysis Date = 05/12/13 Pct Recovery = 125% Analysis Date = 04/24/13 Pct Recovery = 125% Analysis Date = 04/24/13 Pct Recovery = 125% Analysis Date = 04/07/13 Pct Recovery = 125% Analysis Date = 04/07/13 Pct Recovery = 125% Analysis Date = 03/20/13 Pct Recovery = 124% Analysis Date = 03/20/13 Pct Recovery = 124% Analysis Date = 03/02/13 Pct Recovery = 124% Analysis Date = 03/02/13 Pct Recovery = 124% Analysis Date = 02/12/13 Pct Recovery = 124% Analysis Date = 02/12/13 Pct Recovery = 124% Analysis Date = 01/25/13 Pct Recovery = 124% Analysis Date = 01/25/13 Pct Recovery = 124% Analysis Date = 01/08/13 Pct Recovery = 124% Analysis Date = 01/08/13 Pct Recovery = 124% Analysis Date = 12/21/12 Pct Recovery = 124% Analysis Date = 12/21/12 Pct Recovery = 124% Analysis Date = 12/03/12 Pct Recovery = 124% Analysis Date = 12/03/12 Pct Recovery = 124% Analysis Date = 11/15/12 Pct Recovery = 124% Analysis Date = 11/15/12 Pct Recovery = 124% Analysis Date = 10/28/12 Pct Recovery = 124% Analysis Date = 10/28/12 Pct Recovery = 124% Analysis Date = 10/11/12 Pct Recovery = 123% Analysis Date = 10/11/12 Pct Recovery = 123% Analysis Date = 09/23/12 Pct Recovery = 123% Analysis Date = 09/23/12 Pct Recovery = 123% Analysis Date = 09/05/12 Pct Recovery = 123% Analysis Date = 09/05/12 Pct Recovery = 123% Analysis Date = 08/18/12 Pct Recovery = 123% Analysis Date = 08/18/12 Pct Recovery = 123% Analysis Date = 07/31/12 Pct Recovery = 123% Analysis Date = 07/31/12 Pct Recovery = 123% Analysis Date = 07/13/12 Pct Recovery = 123% Analysis Date = 07/13/12 Pct Recovery = 123% Analysis Date = 06/26/12 Pct Recovery = 123% Analysis Date = 06/26/12 Pct Recovery = 123% Analysis Date = 06/08/12 Pct Recovery = 123% Analysis Date = 06/08/12 Pct Recovery = 123% Analysis Date = 05/21/12 Pct Recovery = 122% Analysis Date = 05/21/12 Pct Recovery = 122% Analysis Date = 05/03/12 Pct Recovery = 122% Analysis Date = 05/03/12 Pct Recovery = 122% Analysis Date = 04/15/12 Pct Recovery = 122% Analysis Date = 04/15/12 Pct Recovery = 122% Analysis Date = 03/29/12 Pct Recovery = 122% Analysis Date = 03/29/12 Pct Recovery = 122% Analysis Date = 03/11/12 Pct Recovery = 122% Analysis Date = 03/11/12 Pct Recovery = 122% Analysis Date = 02/22/12 Pct Recovery = 122% Analysis Date = 02/22/12 Pct Recovery = 122% Analysis Date = 02/04/12 Pct Recovery = 122% Analysis Date = 02/04/12 Pct Recovery = 122% Analysis Date = 01/17/12 Pct Recovery = 122% Analysis Date = 01/17/12 Pct Recovery = 122% Analysis Date = 12/31/11 Pct Recovery = 121% Analysis Date = 12/31/11 Pct Recovery = 121% Analysis Date = 12/13/11 Pct Recovery = 121% Analysis Date = 12/13/11 Pct Recovery = 121% Analysis Date = 11/25/11 Pct Recovery = 121% Analysis Date = 11/25/11 Pct Recovery = 121% Analysis Date = 11/07/11 Pct Recovery = 121% Analysis Date = 11/07/11 Pct Recovery = 121% Analysis Date = 10/20/11 Pct Recovery = 121% Analysis Date = 10/20/11 Pct Recovery = 121% Analysis Date = 10/03/11 Pct Recovery = 121% Analysis Date = 10/03/11 Pct Recovery = 121% Analysis Date = 09/15/11 Pct Recovery = 121% Analysis Date = 09/15/11 Pct Recovery = 121% Analysis Date = 08/28/11 Pct Recovery = 121% Analysis Date = 08/28/11 Pct Recovery = 121% Analysis Date = 08/10/11 Pct Recovery = 120% Analysis Date = 08/10/11 Pct Recovery = 120% Analysis Date = 07/23/11 Pct Recovery = 120% Analysis Date = 07/23/11 Pct Recovery = 120% Analysis Date = 07/05/11 Pct Recovery = 120% Analysis Date = 07/05/11 Pct Recovery = 120% Analysis Date = 06/18/11 Pct Recovery = 120% Analysis Date = 06/18/11 Pct Recovery = 120% Analysis Date = 05/31/11 Pct Recovery = 120% Analysis Date = 05/31/11 Pct Recovery = 120% Analysis Date = 05/13/11 Pct Recovery = 120% Analysis Date = 05/13/11 Pct Recovery = 120% Analysis Date = 04/25/11 Pct Recovery = 120% Analysis Date = 04/25/11 Pct Recovery = 120% Analysis Date = 04/07/11 Pct Recovery = 120% Analysis Date = 04/07/11 Pct Recovery = 120% Analysis Date = 03/21/11 Pct Recovery = 120% Analysis Date = 03/21/11 Pct Recovery = 120% Analysis Date = 03/03/11 Pct Recovery = 119% Analysis Date = 03/03/11 Pct Recovery = 119% Analysis Date = 02/13/11 Pct Recovery = 119% Analysis Date = 02/13/11 Pct Recovery = 119% Analysis Date = 01/26/11 Pct Recovery = 119% Analysis Date = 01/26/11 Pct Recovery = 119% Analysis Date = 01/08/11 Pct Recovery = 119% Analysis Date = 01/08/11 Pct Recovery = 119% Analysis Date = 12/22/10 Pct Recovery = 119% Analysis Date = 12/22/10 Pct Recovery = 119% Analysis Date = 12/04/10 Pct Recovery = 119% Analysis Date = 12/04/10 Pct Recovery = 119% Analysis Date = 11/16/10 Pct Recovery = 119% Analysis Date = 11/16/10 Pct Recovery = 119% Analysis Date = 10/29/10 Pct Recovery = 119% Analysis Date = 10/29/10 Pct Recovery = 119% Analysis Date = 10/11/10 Pct Recovery = 119% Analysis Date = 10/11/10 Pct Recovery = 119% Analysis Date = 09/24/10 Pct Recovery = 118% Analysis Date = 09/24/10 Pct Recovery = 118% Analysis Date = 09/06/10 Pct Recovery = 118% Analysis Date = 09/06/10 Pct Recovery = 118% Analysis Date = 08/19/10 Pct Recovery = 118% Analysis Date = 08/19/10 Pct Recovery = 118% Analysis Date = 08/01/10 Pct Recovery = 118% Analysis Date = 08/01/10 Pct Recovery = 118% Analysis Date = 07/14/10 Pct Recovery = 118% Analysis Date = 07/14/10 Pct Recovery = 118% Analysis Date = 06/26/10 Pct Recovery = 118% Analysis Date = 06/26/10 Pct Recovery = 118% Analysis Date = 06/09/10 Pct Recovery = 118% Analysis Date = 06/09/10 Pct Recovery = 118% Analysis Date = 05/22/10 Pct Recovery = 118% Analysis Date = 05/22/10 Pct Recovery = 118% Analysis Date = 05/04/10 Pct Recovery = 118% Analysis Date = 05/04/10 Pct Recovery = 118% Analysis Date = 04/16/10 Pct Recovery = 117% Analysis Date = 04/16/10 Pct Recovery = 117% Analysis Date = 03/29/10 Pct Recovery = 117% Analysis Date = 03/29/10 Pct Recovery = 117% Analysis Date = 03/12/10 Pct Recovery = 117% Analysis Date = 03/12/10 Pct Recovery = 117% Analysis Date = 02/22/10 Pct Recovery = 117% Analysis Date = 02/22/10 Pct Recovery = 117% Analysis Date = 02/04/10 Pct Recovery = 117% Analysis Date = 02/04/10 Pct Recovery = 117% Analysis Date = 01/17/10 Pct Recovery = 117% Analysis Date = 01/17/10 Pct Recovery = 117% Analysis Date = 12/30/09 Pct Recovery = 116% Analysis Date = 12/30/09 Pct Recovery = 116% Analysis Date = 12/13/09 Pct Recovery = 116% Analysis Date = 12/13/09 Pct Recovery = 116% Analysis Date = 11/25/09 Pct Recovery = 116% Analysis Date = 11/25/09 Pct Recovery = 116% Analysis Date = 11/07/09 Pct Recovery = 116% Analysis Date = 11/07/09 Pct Recovery = 116% Analysis Date = 10/20/09 Pct Recovery = 116% Analysis Date = 10/20/09 Pct Recovery = 116% Analysis Date = 10/02/09 Pct Recovery = 115% Analysis Date = 10/02/09 Pct Recovery = 115% Analysis Date = 09/15/09 Pct Recovery = 115% Analysis Date = 09/15/09 Pct Recovery = 115% Analysis Date = 08/28/09 Pct Recovery = 115% Analysis Date = 08/28/09 Pct Recovery = 115% Analysis Date = 08/10/09 Pct Recovery = 115% Analysis Date = 08/10/09 Pct Recovery = 115% Analysis Date = 07/23/09 Pct Recovery = 115% Analysis Date = 07/23/09 Pct Recovery = 115% Analysis Date = 07/05/09 Pct Recovery = 114% Analysis Date = 07/05/09 Pct Recovery = 114% Analysis Date = 06/17/09 Pct Recovery = 114% Analysis Date = 06/17/09 Pct Recovery = 114% Analysis Date = 05/31/09 Pct Recovery = 114% Analysis Date = 05/31/09 Pct Recovery = 114% Analysis Date = 05/13/09 Pct Recovery = 114% Analysis Date = 05/13/09 Pct Recovery = 114% Analysis Date = 04/25/09 Pct Recovery = 114% Analysis Date = 04/25/09 Pct Recovery = 114% Analysis Date = 04/07/09 Pct Recovery = 113% Analysis Date = 04/07/09 Pct Recovery = 113% Analysis Date = 03/20/09 Pct Recovery = 113% Analysis Date = 03/20/09 Pct Recovery = 113% Analysis Date = 03/03/09 Pct Recovery = 113% Analysis Date = 03/03/09 Pct Recovery = 113% Analysis Date = 02/13/09 Pct Recovery = 113% Analysis Date = 02/13/09 Pct Recovery = 113% Analysis Date = 01/26/09 Pct Recovery = 113% Analysis Date = 01/26/09 Pct Recovery = 113% Analysis Date = 01/08/09 Pct Recovery = 113% Analysis Date = 01/08/09 Pct Recovery = 113% Analysis Date = 12/21/08 Pct Recovery = 113% Analysis Date = 12/21/08 Pct Recovery = 113% Analysis Date = 12/04/08 Pct Recovery = 113% Analysis Date = 12/04/08 Pct Recovery = 113% Analysis Date = 11/16/08 Pct Recovery = 113% Analysis Date = 11/16/08 Pct Recovery = 113% Analysis Date = 10/29/08 Pct Recovery = 112% Analysis Date = 10/29/08 Pct Recovery = 112% Analysis Date = 10/11/08 Pct Recovery = 112% Analysis Date = 10/11/08 Pct Recovery = 112% Analysis Date = 09/23/08 Pct Recovery = 112% Analysis Date = 09/23/08 Pct Recovery = 112% Analysis Date = 09/06/08 Pct Recovery = 112% Analysis Date = 09/06/08 Pct Recovery = 112% Analysis Date = 08/19/08 Pct Recovery = 112% Analysis Date = 08/19/08 Pct Recovery = 112% Analysis Date = 08/01/08 Pct Recovery = 112% Analysis Date = 08/01/08 Pct Recovery = 112% Analysis Date = 07/14/08 Pct Recovery = 112% Analysis Date = 07/14/08 Pct Recovery = 112% Analysis Date = 06/26/08 Pct Recovery = 112% Analysis Date = 06/26/08 Pct Recovery = 112% Analysis Date = 06/08/08 Pct Recovery = 112% Analysis Date = 06/08/08 Pct Recovery = 112% Analysis Date = 05/22/08 Pct Recovery = 112% Analysis Date = 05/22/08 Pct Recovery = 112% Analysis Date = 05/04/08 Pct Recovery = 112% Analysis Date = 05/04/08 Pct Recovery = 112% Analysis Date = 04/16/08 Pct Recovery = 111% Analysis Date = 04/16/08 Pct Recovery = 111% Analysis Date = 03/29/08 Pct Recovery = 111% Analysis Date = 03/29/08 Pct Recovery = 111% Analysis Date = 03/11/08 Pct Recovery = 111% Analysis Date = 03/11/08 Pct Recovery = 111% Analysis Date = 02/23/08 Pct Recovery = 111% Analysis Date = 02/23/08 Pct Recovery = 111% Analysis Date = 02/05/08 Pct Recovery = 111% Analysis Date = 02/05/08 Pct Recovery = 111% Analysis Date = 01/18/08 Pct Recovery = 111% Analysis Date = 01/18/08 Pct Recovery = 111% Analysis Date = 12/31/07 Pct Recovery = 111% Analysis Date = 12/31/07 Pct Recovery = 111% Analysis Date = 12/13/07 Pct Recovery = 111% Analysis Date = 12/13/07 Pct Recovery = 111% Analysis Date = 11/26/07 Pct Recovery = 111% Analysis Date = 11/26/07 Pct Recovery = 111% Analysis Date = 11/08/07 Pct Recovery = 110% Analysis Date = 11/08/07 Pct Recovery = 110% Analysis Date = 10/21/07 Pct Recovery = 110% Analysis Date = 10/21/07 Pct Recovery = 110% Analysis Date = 10/03/07 Pct Recovery = 110% Analysis Date = 10/03/07 Pct Recovery = 110% Analysis Date = 09/15/07 Pct Recovery = 110% Analysis Date = 09/15/07 Pct Recovery = 110% Analysis Date = 08/28/07 Pct Recovery = 110% Analysis Date = 08/28/07 Pct Recovery = 110% Analysis Date = 08/11/07 Pct Recovery = 110% Analysis Date = 08/11/07 Pct Recovery = 110% Analysis Date = 07/24/07 Pct Recovery = 109% Analysis Date = 07/24/07 Pct Recovery = 109% Analysis Date = 07/06/07 Pct Recovery = 109% Analysis Date = 07/06/07 Pct Recovery = 109% Analysis Date = 06/18/07 Pct Recovery = 109% Analysis Date = 06/18/07 Pct Recovery = 109% Analysis Date = 05/31/07 Pct Recovery = 109% Analysis Date = 05/31/07 Pct Recovery = 109% Analysis Date = 05/14/07 Pct Recovery = 109% Analysis Date = 05/14/07 Pct Recovery = 109% Analysis Date = 04/26/07 Pct Recovery = 109% Analysis Date = 04/26/07 Pct Recovery = 109% Analysis Date = 04/08/07 Pct Recovery = 109% Analysis Date = 04/08/07 Pct Recovery = 109% Analysis Date = 03/21/07 Pct Recovery = 108% Analysis Date = 03/21/07 Pct Recovery = 108% Analysis Date = 03/03/07 Pct Recovery = 108% Analysis Date = 03/03/07 Pct Recovery = 108% Analysis Date = 02/14/07 Pct Recovery = 108% Analysis Date = 02/14/07 Pct Recovery = 108% Analysis Date = 01/27/07 Pct Recovery = 108% Analysis Date = 01/27/07 Pct Recovery = 108% Analysis Date = 01/09/07 Pct Recovery = 108% Analysis Date = 01/09/07 Pct Recovery = 108% Analysis Date = 12/22/06 Pct Recovery = 108% Analysis Date = 12/22/06 Pct Recovery = 108% Analysis Date = 12/04/06 Pct Recovery = 108% Analysis Date = 12/04/06 Pct Recovery = 108% Analysis Date = 11/17/06 Pct Recovery = 107% Analysis Date = 11/17/06 Pct Recovery = 107% Analysis Date = 10/30/06 Pct Recovery = 107% Analysis Date = 10/30/06 Pct Recovery = 107% Analysis Date = 10/12/06 Pct Recovery = 107% Analysis Date = 10/12/06 Pct Recovery = 107% Analysis Date = 09/24/06 Pct Recovery = 107% Analysis Date = 09/24/06 Pct Recovery = 107% Analysis Date = 09/06/06 Pct Recovery = 107% Analysis Date = 09/06/06 Pct Recovery = 107% Analysis Date = 08/19/06 Pct Recovery = 107% Analysis Date = 08/19/06 Pct Recovery = 107% Analysis Date = 08/02/06 Pct Recovery = 107% Analysis Date = 08/02/06 Pct Recovery = 107% Analysis Date = 07/15/06 Pct Recovery = 106% Analysis Date = 07/15/06 Pct Recovery = 106% Analysis Date = 06/27/06 Pct Recovery = 106% Analysis Date = 06/27/06 Pct Recovery = 106% Analysis Date = 06/09/06 Pct Recovery = 106% Analysis Date = 06/09/06 Pct Recovery = 106% Analysis Date = 05/22/06 Pct Recovery = 106% Analysis Date = 05/22/06 Pct Recovery = 106% Analysis Date = 05/05/06 Pct Recovery = 106% Analysis Date = 05/05/06 Pct Recovery = 106% Analysis Date = 04/17/06 Pct Recovery = 106% Analysis Date = 04/17/06 Pct Recovery = 106% Analysis Date = 03/30/06 Pct Recovery = 106% Analysis Date = 03/30/06 Pct Recovery = 106% Analysis Date = 03/12/06 Pct Recovery = 106% Analysis Date = 03/12/06 Pct Recovery = 106% Analysis Date = 02/22/06 Pct Recovery = 106% Analysis Date = 02/22/06 Pct Recovery = 106% Analysis Date = 02/05/06 Pct Recovery = 106% Analysis Date = 02/05/06 Pct Recovery = 106% Analysis Date = 01/18/06 Pct Recovery = 106% Analysis Date = 01/18/06 Pct Recovery = 106% Analysis Date = 12/31/05 Pct Recovery = 106% Analysis Date = 12/31/05 Pct Recovery = 106% Analysis Date = 12/13/05 Pct Recovery = 107% Analysis Date = 12/13/05 Pct Recovery = 107% Analysis Date = 11/25/05 Pct Recovery = 107% Analysis Date = 11/25/05 Pct Recovery = 107% Analysis Date = 11/08/05 Pct Recovery = 107% Analysis Date = 11/08/05 Pct Recovery = 107% Analysis Date = 10/21/05 Pct Recovery = 107% Analysis Date = 10/21/05 Pct Recovery = 107% Analysis Date = 10/03/05 Pct Recovery = 107% Analysis Date = 10/03/05 Pct Recovery = 107% Analysis Date = 09/15/05 Pct Recovery = 107% Analysis Date = 09/15/05 Pct Recovery = 107% Analysis Date = 08/28/05 Pct Recovery = 107% Analysis Date = 08/28/05 Pct Recovery = 107% Analysis Date = 08/10/05 Pct Recovery = 108% Analysis Date = 08/10/05 Pct Recovery = 108% Analysis Date = 07/24/05 Pct Recovery = 108% Analysis Date = 07/24/05 Pct Recovery = 108% Analysis Date = 07/06/05 Pct Recovery = 108% Analysis Date = 07/06/05 Pct Recovery = 108% Analysis Date = 06/18/05 Pct Recovery = 108% Analysis Date = 06/18/05 Pct Recovery = 108% Analysis Date = 05/31/05 Pct Recovery = 108% Analysis Date = 05/31/05 Pct Recovery = 108% Analysis Date = 05/13/05 Pct Recovery = 108% Analysis Date = 05/13/05 Pct Recovery = 108% Analysis Date = 04/26/05 Pct Recovery = 109% Analysis Date = 04/26/05 Pct Recovery = 109% Analysis Date = 04/08/05 Pct Recovery = 109% Analysis Date = 04/08/05 Pct Recovery = 109% Analysis Date = 03/21/05 Pct Recovery = 109% Analysis Date = 03/21/05 Pct Recovery = 109% Analysis Date = 03/03/05 Pct Recovery = 109% Analysis Date = 03/03/05 Pct Recovery = 109% Analysis Date = 02/13/05 Pct Recovery = 109% Analysis Date = 02/13/05 Pct Recovery = 109% Analysis Date = 01/27/05 Pct Recovery = 110% Analysis Date = 01/27/05 Pct Recovery = 110% Analysis Date = 01/09/05 Pct Recovery = 110% Analysis Date = 01/09/05 Pct Recovery = 110% Analysis Date = 12/22/04 Pct Recovery = 110% Analysis Date = 12/22/04 Pct Recovery = 110% Analysis Date = 12/04/04 Pct Recovery = 110% Analysis Date = 12/04/04 Pct Recovery = 110% Analysis Date = 11/16/04 Pct Recovery = 110% Analysis Date = 11/16/04 Pct Recovery = 110% Analysis Date = 10/30/04 Pct Recovery = 111% Analysis Date = 10/30/04 Pct Recovery = 111% Analysis Date = 10/12/04 Pct Recovery = 111% Analysis Date = 10/12/04 Pct Recovery = 111% Analysis Date = 09/24/04 Pct Recovery = 111% Analysis Date = 09/24/04 Pct Recovery = 111% Analysis Date = 09/06/04 Pct Recovery = 111% Analysis Date = 09/06/04 Pct Recovery = 111% Analysis Date = 08/19/04 Pct Recovery = 111% Analysis Date = 08/19/04 Pct Recovery = 111% Analysis Date = 08/01/04 Pct Recovery = 112% Analysis Date = 08/01/04 Pct Recovery = 112% Analysis Date = 07/15/04 Pct Recovery = 112% Analysis Date = 07/15/04 Pct Recovery = 112% Analysis Date = 06/27/04 Pct Recovery = 112% Analysis Date = 06/27/04 Pct Recovery = 112% Analysis Date = 06/09/04 Pct Recovery = 112% Analysis Date = 06/09/04 Pct Recovery = 112% Analysis Date = 05/22/04 Pct Recovery = 113% Analysis Date = 05/22/04 Pct Recovery = 113% Analysis Date = 05/04/04 Pct Recovery = 113% Analysis Date = 05/04/04 Pct Recovery = 113% Analysis Date = 04/17/04 Pct Recovery = 113% Analysis Date = 04/17/04 Pct Recovery = 113% Analysis Date = 03/30/04 Pct Recovery = 113% Analysis Date = 03/30/04 Pct Recovery = 113% Analysis Date = 03/12/04 Pct Recovery = 114% Analysis Date = 03/12/04 Pct Recovery = 114% Analysis Date = 02/23/04 Pct Recovery = 114% Analysis Date = 02/23/04 Pct Recovery = 114% Analysis Date = 02/05/04 Pct Recovery = 114% Analysis Date = 02/05/04 Pct Recovery = 114% Analysis Date = 01/19/04 Pct Recovery = 114% Analysis Date = 01/19/04 Pct Recovery = 114% Analysis Date = 01/01/04 Pct Recovery = 115% Analysis Date = 01/01/04 Pct Recovery = 115% Analysis Date = 12/14/03 Pct Recovery = 115% Analysis Date = 12/14/03 Pct Recovery = 115% Analysis Date = 11/26/03 Pct Recovery = 115% Analysis Date = 11/26/03 Pct Recovery = 115% Analysis Date = 11/08/03 Pct Recovery = 115% Analysis Date = 11/08/03 Pct Recovery = 115% Analysis Date = 10/22/03 Pct Recovery = 115% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 105% 6% 105% 7%
>= Reporting Level 101 113% 18% 111% 14%
Total 105 113% 17% 111% 14%

Sample Statistics
ACETONE

Characteristic N % % Basis
Plotted 105 99% Spiked
Estimated Values 4 4% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 106 .  
False Negatives 1 1% 1 out of 106
Not Spiked 87 .  
False Positives 18 21% 18 out of 86

BQS OBSP Determination:
DIISOPROPYL ETHER
METHOD: 4024 , TESTIDCODE: 81577GCM60
Open Data Set

Analysis Date = 09/02/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 137% Analysis Date = 07/25/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 133% Analysis Date = 07/22/05 SpikeMix = Supelco LB22063: 25 µl Pct Recovery = 116% Analysis Date = 03/11/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 107% Analysis Date = 02/01/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 116% Analysis Date = 06/03/05 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 115% Analysis Date = 11/30/04 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 104% Analysis Date = 06/17/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 106% Analysis Date = 03/11/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 127% Analysis Date = 01/14/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 128% Analysis Date = 08/20/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 123% Analysis Date = 06/16/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 125% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 101% Analysis Date = 02/04/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 103% Analysis Date = 04/11/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 114% Analysis Date = 02/28/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 100% Analysis Date = 11/25/05 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 115% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 109% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 99% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 102% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 100% Analysis Date = 08/31/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 126% Analysis Date = 04/15/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 108% Analysis Date = 12/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 105% Analysis Date = 10/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 116% Analysis Date = 08/24/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 101% Analysis Date = 06/05/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 98% Analysis Date = 04/14/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 127% Analysis Date = 02/07/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 126% Analysis Date = 12/06/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 127% Analysis Date = 10/09/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 109% Analysis Date = 05/04/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 111% Analysis Date = 01/12/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 118% Analysis Date = 10/29/05 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 115% Analysis Date = 07/16/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 98% Analysis Date = 05/06/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 111% Analysis Date = 11/07/03 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 110% Analysis Date = 09/24/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 95% Analysis Date = 07/02/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 93% Analysis Date = 06/05/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 90% Analysis Date = 04/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 88% Analysis Date = 01/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 97% Analysis Date = 12/13/03 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 92% Analysis Date = 06/30/12 SpikeMix = Accu 212051187: 25 µl Pct Recovery = 79% Analysis Date = 03/26/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 101% Analysis Date = 02/19/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 99% Analysis Date = 01/03/13 SpikeMix = Accu 212051187: 20 µl Pct Recovery = 87% Analysis Date = 08/28/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 96% Analysis Date = 08/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 113% Analysis Date = 07/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 104% Analysis Date = 06/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 113% Analysis Date = 05/06/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 104% Analysis Date = 04/15/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 117% Analysis Date = 03/27/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 104% Analysis Date = 03/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 11/19/07 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 108% Analysis Date = 07/19/10 SpikeMix = Ultra CF-3592: 40 µl Pct Recovery = 107% Analysis Date = 08/27/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 103% Analysis Date = 08/17/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 98% Analysis Date = 03/10/12 SpikeMix = Restek A075544: 40 µl Pct Recovery = 106% Analysis Date = 09/13/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 101% Analysis Date = 08/18/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 118% Analysis Date = 11/15/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 100% Analysis Date = 08/02/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 104% Analysis Date = 11/09/10 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 94% Analysis Date = 07/25/09 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 94% Analysis Date = 12/11/08 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 100% Analysis Date = 07/01/09 SpikeMix = Accu B8080231: 40 µl Pct Recovery = 100% Analysis Date = 11/27/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 104% Analysis Date = 09/08/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 97% Analysis Date = 10/22/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 105% Analysis Date = 07/11/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 100% Analysis Date = 09/18/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 94% Analysis Date = 08/29/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 101% Analysis Date = 08/02/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 109% Analysis Date = 07/14/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 123% Analysis Date = 06/22/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 109% Analysis Date = 05/31/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 94% Analysis Date = 03/23/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 101% Analysis Date = 12/29/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 87% Analysis Date = 12/01/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 109% Analysis Date = 05/06/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 106% Analysis Date = 03/26/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 112% Analysis Date = 10/26/09 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 111% Analysis Date = 06/24/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 110% Analysis Date = 04/22/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 94% Analysis Date = 02/09/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 108% Analysis Date = 02/10/12 SpikeMix = Restek A075544: 20 µl Pct Recovery = 95% Analysis Date = 10/15/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 104% Analysis Date = 06/21/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 100% Analysis Date = 10/09/10 SpikeMix = Restek A075544: 20 µl Pct Recovery = 100% Analysis Date = 06/07/12 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 89% Analysis Date = 08/26/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 86% Analysis Date = 07/19/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 92% Analysis Date = 12/10/10 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 100% Analysis Date = 04/07/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 100% Analysis Date = 02/21/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 113% Analysis Date = 10/22/08 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 100% Analysis Date = 08/25/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 126% Analysis Date = 03/09/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 100% Analysis Date = 10/29/08 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 126% Analysis Date = 06/07/13 SpikeMix = ChemService 1448500: 10 µl Pct Recovery = 109% Analysis Date = 06/07/13 Pct Recovery = 97% Analysis Date = 05/20/13 Pct Recovery = 97% Analysis Date = 05/20/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 05/02/13 Pct Recovery = 97% Analysis Date = 04/15/13 Pct Recovery = 97% Analysis Date = 04/15/13 Pct Recovery = 97% Analysis Date = 03/28/13 Pct Recovery = 97% Analysis Date = 03/28/13 Pct Recovery = 97% Analysis Date = 03/10/13 Pct Recovery = 97% Analysis Date = 03/10/13 Pct Recovery = 97% Analysis Date = 02/21/13 Pct Recovery = 97% Analysis Date = 02/21/13 Pct Recovery = 97% Analysis Date = 02/03/13 Pct Recovery = 97% Analysis Date = 02/03/13 Pct Recovery = 97% Analysis Date = 01/16/13 Pct Recovery = 97% Analysis Date = 01/16/13 Pct Recovery = 97% Analysis Date = 12/30/12 Pct Recovery = 97% Analysis Date = 12/30/12 Pct Recovery = 97% Analysis Date = 12/12/12 Pct Recovery = 98% Analysis Date = 12/12/12 Pct Recovery = 98% Analysis Date = 11/24/12 Pct Recovery = 98% Analysis Date = 11/24/12 Pct Recovery = 98% Analysis Date = 11/07/12 Pct Recovery = 98% Analysis Date = 11/07/12 Pct Recovery = 98% Analysis Date = 10/20/12 Pct Recovery = 98% Analysis Date = 10/20/12 Pct Recovery = 98% Analysis Date = 10/02/12 Pct Recovery = 98% Analysis Date = 10/02/12 Pct Recovery = 98% Analysis Date = 09/15/12 Pct Recovery = 98% Analysis Date = 09/15/12 Pct Recovery = 98% Analysis Date = 08/28/12 Pct Recovery = 98% Analysis Date = 08/28/12 Pct Recovery = 98% Analysis Date = 08/11/12 Pct Recovery = 98% Analysis Date = 08/11/12 Pct Recovery = 98% Analysis Date = 07/24/12 Pct Recovery = 98% Analysis Date = 07/24/12 Pct Recovery = 98% Analysis Date = 07/06/12 Pct Recovery = 99% Analysis Date = 07/06/12 Pct Recovery = 99% Analysis Date = 06/19/12 Pct Recovery = 99% Analysis Date = 06/19/12 Pct Recovery = 99% Analysis Date = 06/01/12 Pct Recovery = 99% Analysis Date = 06/01/12 Pct Recovery = 99% Analysis Date = 05/14/12 Pct Recovery = 99% Analysis Date = 05/14/12 Pct Recovery = 99% Analysis Date = 04/27/12 Pct Recovery = 99% Analysis Date = 04/27/12 Pct Recovery = 99% Analysis Date = 04/09/12 Pct Recovery = 99% Analysis Date = 04/09/12 Pct Recovery = 99% Analysis Date = 03/22/12 Pct Recovery = 99% Analysis Date = 03/22/12 Pct Recovery = 99% Analysis Date = 03/05/12 Pct Recovery = 99% Analysis Date = 03/05/12 Pct Recovery = 99% Analysis Date = 02/16/12 Pct Recovery = 99% Analysis Date = 02/16/12 Pct Recovery = 99% Analysis Date = 01/29/12 Pct Recovery = 99% Analysis Date = 01/29/12 Pct Recovery = 99% Analysis Date = 01/12/12 Pct Recovery = 100% Analysis Date = 01/12/12 Pct Recovery = 100% Analysis Date = 12/25/11 Pct Recovery = 100% Analysis Date = 12/25/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 100% Analysis Date = 12/08/11 Pct Recovery = 100% Analysis Date = 11/20/11 Pct Recovery = 100% Analysis Date = 11/20/11 Pct Recovery = 100% Analysis Date = 11/02/11 Pct Recovery = 100% Analysis Date = 11/02/11 Pct Recovery = 100% Analysis Date = 10/16/11 Pct Recovery = 100% Analysis Date = 10/16/11 Pct Recovery = 100% Analysis Date = 09/28/11 Pct Recovery = 100% Analysis Date = 09/28/11 Pct Recovery = 100% Analysis Date = 09/10/11 Pct Recovery = 100% Analysis Date = 09/10/11 Pct Recovery = 100% Analysis Date = 08/24/11 Pct Recovery = 100% Analysis Date = 08/24/11 Pct Recovery = 100% Analysis Date = 08/06/11 Pct Recovery = 100% Analysis Date = 08/06/11 Pct Recovery = 100% Analysis Date = 07/19/11 Pct Recovery = 101% Analysis Date = 07/19/11 Pct Recovery = 101% Analysis Date = 07/02/11 Pct Recovery = 101% Analysis Date = 07/02/11 Pct Recovery = 101% Analysis Date = 06/14/11 Pct Recovery = 101% Analysis Date = 06/14/11 Pct Recovery = 101% Analysis Date = 05/27/11 Pct Recovery = 101% Analysis Date = 05/27/11 Pct Recovery = 101% Analysis Date = 05/10/11 Pct Recovery = 101% Analysis Date = 05/10/11 Pct Recovery = 101% Analysis Date = 04/22/11 Pct Recovery = 101% Analysis Date = 04/22/11 Pct Recovery = 101% Analysis Date = 04/04/11 Pct Recovery = 101% Analysis Date = 04/04/11 Pct Recovery = 101% Analysis Date = 03/18/11 Pct Recovery = 101% Analysis Date = 03/18/11 Pct Recovery = 101% Analysis Date = 02/28/11 Pct Recovery = 101% Analysis Date = 02/28/11 Pct Recovery = 101% Analysis Date = 02/11/11 Pct Recovery = 101% Analysis Date = 02/11/11 Pct Recovery = 101% Analysis Date = 01/24/11 Pct Recovery = 102% Analysis Date = 01/24/11 Pct Recovery = 102% Analysis Date = 01/06/11 Pct Recovery = 102% Analysis Date = 01/06/11 Pct Recovery = 102% Analysis Date = 12/20/10 Pct Recovery = 102% Analysis Date = 12/20/10 Pct Recovery = 102% Analysis Date = 12/02/10 Pct Recovery = 102% Analysis Date = 12/02/10 Pct Recovery = 102% Analysis Date = 11/14/10 Pct Recovery = 102% Analysis Date = 11/14/10 Pct Recovery = 102% Analysis Date = 10/28/10 Pct Recovery = 102% Analysis Date = 10/28/10 Pct Recovery = 102% Analysis Date = 10/10/10 Pct Recovery = 102% Analysis Date = 10/10/10 Pct Recovery = 102% Analysis Date = 09/22/10 Pct Recovery = 102% Analysis Date = 09/22/10 Pct Recovery = 102% Analysis Date = 09/05/10 Pct Recovery = 102% Analysis Date = 09/05/10 Pct Recovery = 102% Analysis Date = 08/18/10 Pct Recovery = 102% Analysis Date = 08/18/10 Pct Recovery = 102% Analysis Date = 07/31/10 Pct Recovery = 102% Analysis Date = 07/31/10 Pct Recovery = 102% Analysis Date = 07/14/10 Pct Recovery = 103% Analysis Date = 07/14/10 Pct Recovery = 103% Analysis Date = 06/26/10 Pct Recovery = 103% Analysis Date = 06/26/10 Pct Recovery = 103% Analysis Date = 06/09/10 Pct Recovery = 103% Analysis Date = 06/09/10 Pct Recovery = 103% Analysis Date = 05/22/10 Pct Recovery = 103% Analysis Date = 05/22/10 Pct Recovery = 103% Analysis Date = 05/04/10 Pct Recovery = 103% Analysis Date = 05/04/10 Pct Recovery = 103% Analysis Date = 04/17/10 Pct Recovery = 103% Analysis Date = 04/17/10 Pct Recovery = 103% Analysis Date = 03/30/10 Pct Recovery = 103% Analysis Date = 03/30/10 Pct Recovery = 103% Analysis Date = 03/12/10 Pct Recovery = 103% Analysis Date = 03/12/10 Pct Recovery = 103% Analysis Date = 02/23/10 Pct Recovery = 103% Analysis Date = 02/23/10 Pct Recovery = 103% Analysis Date = 02/05/10 Pct Recovery = 104% Analysis Date = 02/05/10 Pct Recovery = 104% Analysis Date = 01/18/10 Pct Recovery = 104% Analysis Date = 01/18/10 Pct Recovery = 104% Analysis Date = 01/01/10 Pct Recovery = 104% Analysis Date = 01/01/10 Pct Recovery = 104% Analysis Date = 12/14/09 Pct Recovery = 104% Analysis Date = 12/14/09 Pct Recovery = 104% Analysis Date = 11/26/09 Pct Recovery = 104% Analysis Date = 11/26/09 Pct Recovery = 104% Analysis Date = 11/09/09 Pct Recovery = 104% Analysis Date = 11/09/09 Pct Recovery = 104% Analysis Date = 10/22/09 Pct Recovery = 104% Analysis Date = 10/22/09 Pct Recovery = 104% Analysis Date = 10/04/09 Pct Recovery = 104% Analysis Date = 10/04/09 Pct Recovery = 104% Analysis Date = 09/17/09 Pct Recovery = 104% Analysis Date = 09/17/09 Pct Recovery = 104% Analysis Date = 08/30/09 Pct Recovery = 104% Analysis Date = 08/30/09 Pct Recovery = 104% Analysis Date = 08/13/09 Pct Recovery = 105% Analysis Date = 08/13/09 Pct Recovery = 105% Analysis Date = 07/26/09 Pct Recovery = 105% Analysis Date = 07/26/09 Pct Recovery = 105% Analysis Date = 07/08/09 Pct Recovery = 105% Analysis Date = 07/08/09 Pct Recovery = 105% Analysis Date = 06/21/09 Pct Recovery = 105% Analysis Date = 06/21/09 Pct Recovery = 105% Analysis Date = 06/03/09 Pct Recovery = 105% Analysis Date = 06/03/09 Pct Recovery = 105% Analysis Date = 05/16/09 Pct Recovery = 105% Analysis Date = 05/16/09 Pct Recovery = 105% Analysis Date = 04/29/09 Pct Recovery = 105% Analysis Date = 04/29/09 Pct Recovery = 105% Analysis Date = 04/11/09 Pct Recovery = 105% Analysis Date = 04/11/09 Pct Recovery = 105% Analysis Date = 03/24/09 Pct Recovery = 105% Analysis Date = 03/24/09 Pct Recovery = 105% Analysis Date = 03/07/09 Pct Recovery = 105% Analysis Date = 03/07/09 Pct Recovery = 105% Analysis Date = 02/17/09 Pct Recovery = 106% Analysis Date = 02/17/09 Pct Recovery = 106% Analysis Date = 01/30/09 Pct Recovery = 106% Analysis Date = 01/30/09 Pct Recovery = 106% Analysis Date = 01/13/09 Pct Recovery = 106% Analysis Date = 01/13/09 Pct Recovery = 106% Analysis Date = 12/26/08 Pct Recovery = 106% Analysis Date = 12/26/08 Pct Recovery = 106% Analysis Date = 12/09/08 Pct Recovery = 106% Analysis Date = 12/09/08 Pct Recovery = 106% Analysis Date = 11/21/08 Pct Recovery = 106% Analysis Date = 11/21/08 Pct Recovery = 106% Analysis Date = 11/03/08 Pct Recovery = 106% Analysis Date = 11/03/08 Pct Recovery = 106% Analysis Date = 10/17/08 Pct Recovery = 106% Analysis Date = 10/17/08 Pct Recovery = 106% Analysis Date = 09/29/08 Pct Recovery = 106% Analysis Date = 09/29/08 Pct Recovery = 106% Analysis Date = 09/11/08 Pct Recovery = 107% Analysis Date = 09/11/08 Pct Recovery = 107% Analysis Date = 08/25/08 Pct Recovery = 107% Analysis Date = 08/25/08 Pct Recovery = 107% Analysis Date = 08/07/08 Pct Recovery = 107% Analysis Date = 08/07/08 Pct Recovery = 107% Analysis Date = 07/20/08 Pct Recovery = 107% Analysis Date = 07/20/08 Pct Recovery = 107% Analysis Date = 07/03/08 Pct Recovery = 107% Analysis Date = 07/03/08 Pct Recovery = 107% Analysis Date = 06/15/08 Pct Recovery = 107% Analysis Date = 06/15/08 Pct Recovery = 107% Analysis Date = 05/28/08 Pct Recovery = 107% Analysis Date = 05/28/08 Pct Recovery = 107% Analysis Date = 05/11/08 Pct Recovery = 107% Analysis Date = 05/11/08 Pct Recovery = 107% Analysis Date = 04/23/08 Pct Recovery = 107% Analysis Date = 04/23/08 Pct Recovery = 107% Analysis Date = 04/05/08 Pct Recovery = 108% Analysis Date = 04/05/08 Pct Recovery = 108% Analysis Date = 03/19/08 Pct Recovery = 108% Analysis Date = 03/19/08 Pct Recovery = 108% Analysis Date = 03/01/08 Pct Recovery = 108% Analysis Date = 03/01/08 Pct Recovery = 108% Analysis Date = 02/13/08 Pct Recovery = 108% Analysis Date = 02/13/08 Pct Recovery = 108% Analysis Date = 01/26/08 Pct Recovery = 108% Analysis Date = 01/26/08 Pct Recovery = 108% Analysis Date = 01/08/08 Pct Recovery = 108% Analysis Date = 01/08/08 Pct Recovery = 108% Analysis Date = 12/22/07 Pct Recovery = 108% Analysis Date = 12/22/07 Pct Recovery = 108% Analysis Date = 12/04/07 Pct Recovery = 108% Analysis Date = 12/04/07 Pct Recovery = 108% Analysis Date = 11/16/07 Pct Recovery = 108% Analysis Date = 11/16/07 Pct Recovery = 108% Analysis Date = 10/30/07 Pct Recovery = 108% Analysis Date = 10/30/07 Pct Recovery = 108% Analysis Date = 10/12/07 Pct Recovery = 109% Analysis Date = 10/12/07 Pct Recovery = 109% Analysis Date = 09/24/07 Pct Recovery = 109% Analysis Date = 09/24/07 Pct Recovery = 109% Analysis Date = 09/07/07 Pct Recovery = 109% Analysis Date = 09/07/07 Pct Recovery = 109% Analysis Date = 08/20/07 Pct Recovery = 109% Analysis Date = 08/20/07 Pct Recovery = 109% Analysis Date = 08/02/07 Pct Recovery = 109% Analysis Date = 08/02/07 Pct Recovery = 109% Analysis Date = 07/16/07 Pct Recovery = 109% Analysis Date = 07/16/07 Pct Recovery = 109% Analysis Date = 06/28/07 Pct Recovery = 109% Analysis Date = 06/28/07 Pct Recovery = 109% Analysis Date = 06/11/07 Pct Recovery = 109% Analysis Date = 06/11/07 Pct Recovery = 109% Analysis Date = 05/24/07 Pct Recovery = 109% Analysis Date = 05/24/07 Pct Recovery = 109% Analysis Date = 05/06/07 Pct Recovery = 109% Analysis Date = 05/06/07 Pct Recovery = 109% Analysis Date = 04/19/07 Pct Recovery = 109% Analysis Date = 04/19/07 Pct Recovery = 109% Analysis Date = 04/01/07 Pct Recovery = 109% Analysis Date = 04/01/07 Pct Recovery = 109% Analysis Date = 03/14/07 Pct Recovery = 109% Analysis Date = 03/14/07 Pct Recovery = 109% Analysis Date = 02/25/07 Pct Recovery = 109% Analysis Date = 02/25/07 Pct Recovery = 109% Analysis Date = 02/07/07 Pct Recovery = 109% Analysis Date = 02/07/07 Pct Recovery = 109% Analysis Date = 01/20/07 Pct Recovery = 110% Analysis Date = 01/20/07 Pct Recovery = 110% Analysis Date = 01/03/07 Pct Recovery = 110% Analysis Date = 01/03/07 Pct Recovery = 110% Analysis Date = 12/16/06 Pct Recovery = 110% Analysis Date = 12/16/06 Pct Recovery = 110% Analysis Date = 11/28/06 Pct Recovery = 110% Analysis Date = 11/28/06 Pct Recovery = 110% Analysis Date = 11/11/06 Pct Recovery = 110% Analysis Date = 11/11/06 Pct Recovery = 110% Analysis Date = 10/24/06 Pct Recovery = 110% Analysis Date = 10/24/06 Pct Recovery = 110% Analysis Date = 10/06/06 Pct Recovery = 110% Analysis Date = 10/06/06 Pct Recovery = 110% Analysis Date = 09/19/06 Pct Recovery = 110% Analysis Date = 09/19/06 Pct Recovery = 110% Analysis Date = 09/01/06 Pct Recovery = 110% Analysis Date = 09/01/06 Pct Recovery = 110% Analysis Date = 08/15/06 Pct Recovery = 110% Analysis Date = 08/15/06 Pct Recovery = 110% Analysis Date = 07/28/06 Pct Recovery = 110% Analysis Date = 07/28/06 Pct Recovery = 110% Analysis Date = 07/10/06 Pct Recovery = 110% Analysis Date = 07/10/06 Pct Recovery = 110% Analysis Date = 06/23/06 Pct Recovery = 110% Analysis Date = 06/23/06 Pct Recovery = 110% Analysis Date = 06/05/06 Pct Recovery = 110% Analysis Date = 06/05/06 Pct Recovery = 110% Analysis Date = 05/18/06 Pct Recovery = 110% Analysis Date = 05/18/06 Pct Recovery = 110% Analysis Date = 05/01/06 Pct Recovery = 110% Analysis Date = 05/01/06 Pct Recovery = 110% Analysis Date = 04/13/06 Pct Recovery = 110% Analysis Date = 04/13/06 Pct Recovery = 110% Analysis Date = 03/26/06 Pct Recovery = 110% Analysis Date = 03/26/06 Pct Recovery = 110% Analysis Date = 03/09/06 Pct Recovery = 110% Analysis Date = 03/09/06 Pct Recovery = 110% Analysis Date = 02/19/06 Pct Recovery = 110% Analysis Date = 02/19/06 Pct Recovery = 110% Analysis Date = 02/01/06 Pct Recovery = 110% Analysis Date = 02/01/06 Pct Recovery = 110% Analysis Date = 01/15/06 Pct Recovery = 110% Analysis Date = 01/15/06 Pct Recovery = 110% Analysis Date = 12/28/05 Pct Recovery = 110% Analysis Date = 12/28/05 Pct Recovery = 110% Analysis Date = 12/11/05 Pct Recovery = 110% Analysis Date = 12/11/05 Pct Recovery = 110% Analysis Date = 11/23/05 Pct Recovery = 110% Analysis Date = 11/23/05 Pct Recovery = 110% Analysis Date = 11/05/05 Pct Recovery = 110% Analysis Date = 11/05/05 Pct Recovery = 110% Analysis Date = 10/19/05 Pct Recovery = 110% Analysis Date = 10/19/05 Pct Recovery = 110% Analysis Date = 10/01/05 Pct Recovery = 110% Analysis Date = 10/01/05 Pct Recovery = 110% Analysis Date = 09/13/05 Pct Recovery = 110% Analysis Date = 09/13/05 Pct Recovery = 110% Analysis Date = 08/27/05 Pct Recovery = 110% Analysis Date = 08/27/05 Pct Recovery = 110% Analysis Date = 08/09/05 Pct Recovery = 110% Analysis Date = 08/09/05 Pct Recovery = 110% Analysis Date = 07/22/05 Pct Recovery = 109% Analysis Date = 07/22/05 Pct Recovery = 109% Analysis Date = 07/05/05 Pct Recovery = 109% Analysis Date = 07/05/05 Pct Recovery = 109% Analysis Date = 06/17/05 Pct Recovery = 109% Analysis Date = 06/17/05 Pct Recovery = 109% Analysis Date = 05/30/05 Pct Recovery = 109% Analysis Date = 05/30/05 Pct Recovery = 109% Analysis Date = 05/13/05 Pct Recovery = 109% Analysis Date = 05/13/05 Pct Recovery = 109% Analysis Date = 04/25/05 Pct Recovery = 109% Analysis Date = 04/25/05 Pct Recovery = 109% Analysis Date = 04/07/05 Pct Recovery = 109% Analysis Date = 04/07/05 Pct Recovery = 109% Analysis Date = 03/21/05 Pct Recovery = 109% Analysis Date = 03/21/05 Pct Recovery = 109% Analysis Date = 03/03/05 Pct Recovery = 109% Analysis Date = 03/03/05 Pct Recovery = 109% Analysis Date = 02/14/05 Pct Recovery = 109% Analysis Date = 02/14/05 Pct Recovery = 109% Analysis Date = 01/27/05 Pct Recovery = 109% Analysis Date = 01/27/05 Pct Recovery = 109% Analysis Date = 01/09/05 Pct Recovery = 109% Analysis Date = 01/09/05 Pct Recovery = 109% Analysis Date = 12/23/04 Pct Recovery = 109% Analysis Date = 12/23/04 Pct Recovery = 109% Analysis Date = 12/05/04 Pct Recovery = 109% Analysis Date = 12/05/04 Pct Recovery = 109% Analysis Date = 11/17/04 Pct Recovery = 109% Analysis Date = 11/17/04 Pct Recovery = 109% Analysis Date = 10/31/04 Pct Recovery = 108% Analysis Date = 10/31/04 Pct Recovery = 108% Analysis Date = 10/13/04 Pct Recovery = 108% Analysis Date = 10/13/04 Pct Recovery = 108% Analysis Date = 09/25/04 Pct Recovery = 108% Analysis Date = 09/25/04 Pct Recovery = 108% Analysis Date = 09/08/04 Pct Recovery = 108% Analysis Date = 09/08/04 Pct Recovery = 108% Analysis Date = 08/21/04 Pct Recovery = 108% Analysis Date = 08/21/04 Pct Recovery = 108% Analysis Date = 08/03/04 Pct Recovery = 108% Analysis Date = 08/03/04 Pct Recovery = 108% Analysis Date = 07/17/04 Pct Recovery = 108% Analysis Date = 07/17/04 Pct Recovery = 108% Analysis Date = 06/29/04 Pct Recovery = 108% Analysis Date = 06/29/04 Pct Recovery = 108% Analysis Date = 06/12/04 Pct Recovery = 108% Analysis Date = 06/12/04 Pct Recovery = 108% Analysis Date = 05/25/04 Pct Recovery = 108% Analysis Date = 05/25/04 Pct Recovery = 108% Analysis Date = 05/07/04 Pct Recovery = 108% Analysis Date = 05/07/04 Pct Recovery = 108% Analysis Date = 04/20/04 Pct Recovery = 107% Analysis Date = 04/20/04 Pct Recovery = 107% Analysis Date = 04/02/04 Pct Recovery = 107% Analysis Date = 04/02/04 Pct Recovery = 107% Analysis Date = 03/15/04 Pct Recovery = 107% Analysis Date = 03/15/04 Pct Recovery = 107% Analysis Date = 02/27/04 Pct Recovery = 107% Analysis Date = 02/27/04 Pct Recovery = 107% Analysis Date = 02/09/04 Pct Recovery = 107% Analysis Date = 02/09/04 Pct Recovery = 107% Analysis Date = 01/22/04 Pct Recovery = 107% Analysis Date = 01/22/04 Pct Recovery = 107% Analysis Date = 01/05/04 Pct Recovery = 107% Analysis Date = 01/05/04 Pct Recovery = 107% Analysis Date = 12/18/03 Pct Recovery = 107% Analysis Date = 12/18/03 Pct Recovery = 107% Analysis Date = 11/30/03 Pct Recovery = 107% Analysis Date = 11/30/03 Pct Recovery = 107% Analysis Date = 11/13/03 Pct Recovery = 107% Analysis Date = 11/13/03 Pct Recovery = 107% Analysis Date = 10/26/03 Pct Recovery = 107% Analysis Date = 10/26/03 Pct Recovery = 107% Analysis Date = 10/09/03 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIISOPROPYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 102 106% 11% 104% 10%
Total 102 106% 11% 104% 10%

Sample Statistics
DIISOPROPYL ETHER

Characteristic N % % Basis
Plotted 102 100% Spiked
Estimated Values 4 4% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 103 .  
False Negatives 0 0% 0 out of 102
Not Spiked 90 .  
False Positives 0 0% 0 out of 90

BQS OBSP Determination:
ETHYL TERT-BUTYL ETHER
METHOD: 4024 , TESTIDCODE: 50004GCM60
Open Data Set

Analysis Date = 07/22/05 SpikeMix = Supelco LB22063: 25 µl Pct Recovery = 124% Analysis Date = 09/02/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 137% Analysis Date = 07/25/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 137% Analysis Date = 06/17/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 91% Analysis Date = 03/11/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 126% Analysis Date = 01/14/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 125% Analysis Date = 06/03/05 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 124% Analysis Date = 11/30/04 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 103% Analysis Date = 03/11/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 116% Analysis Date = 02/01/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 123% Analysis Date = 08/24/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 107% Analysis Date = 06/05/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 106% Analysis Date = 04/14/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 141% Analysis Date = 02/07/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 133% Analysis Date = 12/06/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 135% Analysis Date = 10/09/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 110% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 102% Analysis Date = 02/04/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 102% Analysis Date = 08/20/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 122% Analysis Date = 06/16/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 124% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 119% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 102% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 99% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 102% Analysis Date = 08/31/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 128% Analysis Date = 04/15/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 110% Analysis Date = 12/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 109% Analysis Date = 10/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 114% Analysis Date = 07/16/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 100% Analysis Date = 05/06/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 119% Analysis Date = 11/07/03 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 114% Analysis Date = 04/11/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 114% Analysis Date = 02/28/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 101% Analysis Date = 11/25/05 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 111% Analysis Date = 05/04/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 116% Analysis Date = 01/12/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 118% Analysis Date = 10/29/05 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 111% Analysis Date = 09/18/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 92% Analysis Date = 08/29/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 90% Analysis Date = 08/02/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 96% Analysis Date = 07/14/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 102% Analysis Date = 06/22/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 100% Analysis Date = 05/31/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 98% Analysis Date = 03/23/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 108% Analysis Date = 12/29/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 102% Analysis Date = 12/01/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 110% Analysis Date = 09/24/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 98% Analysis Date = 07/02/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 98% Analysis Date = 06/05/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 95% Analysis Date = 04/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 95% Analysis Date = 01/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 105% Analysis Date = 12/13/03 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 95% Analysis Date = 06/30/12 SpikeMix = Accu 212051187: 25 µl Pct Recovery = 76% Analysis Date = 07/19/10 SpikeMix = Ultra CF-3592: 40 µl Pct Recovery = 107% Analysis Date = 08/27/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 103% Analysis Date = 08/17/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 101% Analysis Date = 01/03/13 SpikeMix = Accu 212051187: 20 µl Pct Recovery = 94% Analysis Date = 03/26/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 106% Analysis Date = 02/19/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 90% Analysis Date = 07/01/09 SpikeMix = Accu B8080231: 40 µl Pct Recovery = 116% Analysis Date = 07/25/09 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 117% Analysis Date = 12/11/08 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 100% Analysis Date = 03/10/12 SpikeMix = Restek A075544: 40 µl Pct Recovery = 98% Analysis Date = 09/13/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 102% Analysis Date = 08/18/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 117% Analysis Date = 11/15/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 113% Analysis Date = 08/02/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 121% Analysis Date = 11/09/10 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 98% Analysis Date = 08/28/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 95% Analysis Date = 08/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 95% Analysis Date = 07/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 107% Analysis Date = 06/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 119% Analysis Date = 05/06/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 107% Analysis Date = 04/15/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 119% Analysis Date = 03/27/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 119% Analysis Date = 03/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 107% Analysis Date = 11/19/07 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 107% Analysis Date = 05/06/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 104% Analysis Date = 03/26/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 106% Analysis Date = 10/26/09 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 110% Analysis Date = 06/07/13 SpikeMix = ChemService 1448500: 10 µl Pct Recovery = 101% Analysis Date = 06/24/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 104% Analysis Date = 04/22/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 97% Analysis Date = 02/09/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 105% Analysis Date = 10/22/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 100% Analysis Date = 07/11/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 100% Analysis Date = 11/27/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 92% Analysis Date = 09/08/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 112% Analysis Date = 08/25/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 150% Analysis Date = 03/09/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 83% Analysis Date = 10/29/08 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 100% Analysis Date = 04/07/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 117% Analysis Date = 02/21/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 100% Analysis Date = 10/22/08 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 100% Analysis Date = 02/10/12 SpikeMix = Restek A075544: 20 µl Pct Recovery = 77% Analysis Date = 10/15/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 111% Analysis Date = 06/21/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 114% Analysis Date = 10/09/10 SpikeMix = Restek A075544: 20 µl Pct Recovery = 96% Analysis Date = 06/07/12 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 91% Analysis Date = 08/26/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 106% Analysis Date = 07/19/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 108% Analysis Date = 12/10/10 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 100% Analysis Date = 06/07/13 Pct Recovery = 98% Analysis Date = 05/20/13 Pct Recovery = 98% Analysis Date = 05/20/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 05/02/13 Pct Recovery = 98% Analysis Date = 04/15/13 Pct Recovery = 98% Analysis Date = 04/15/13 Pct Recovery = 98% Analysis Date = 03/28/13 Pct Recovery = 98% Analysis Date = 03/28/13 Pct Recovery = 98% Analysis Date = 03/10/13 Pct Recovery = 98% Analysis Date = 03/10/13 Pct Recovery = 98% Analysis Date = 02/21/13 Pct Recovery = 98% Analysis Date = 02/21/13 Pct Recovery = 98% Analysis Date = 02/03/13 Pct Recovery = 98% Analysis Date = 02/03/13 Pct Recovery = 98% Analysis Date = 01/16/13 Pct Recovery = 99% Analysis Date = 01/16/13 Pct Recovery = 99% Analysis Date = 12/30/12 Pct Recovery = 99% Analysis Date = 12/30/12 Pct Recovery = 99% Analysis Date = 12/12/12 Pct Recovery = 99% Analysis Date = 12/12/12 Pct Recovery = 99% Analysis Date = 11/24/12 Pct Recovery = 99% Analysis Date = 11/24/12 Pct Recovery = 99% Analysis Date = 11/07/12 Pct Recovery = 99% Analysis Date = 11/07/12 Pct Recovery = 99% Analysis Date = 10/20/12 Pct Recovery = 99% Analysis Date = 10/20/12 Pct Recovery = 99% Analysis Date = 10/02/12 Pct Recovery = 99% Analysis Date = 10/02/12 Pct Recovery = 99% Analysis Date = 09/15/12 Pct Recovery = 99% Analysis Date = 09/15/12 Pct Recovery = 99% Analysis Date = 08/28/12 Pct Recovery = 100% Analysis Date = 08/28/12 Pct Recovery = 100% Analysis Date = 08/11/12 Pct Recovery = 100% Analysis Date = 08/11/12 Pct Recovery = 100% Analysis Date = 07/24/12 Pct Recovery = 100% Analysis Date = 07/24/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 07/06/12 Pct Recovery = 100% Analysis Date = 06/19/12 Pct Recovery = 100% Analysis Date = 06/19/12 Pct Recovery = 100% Analysis Date = 06/01/12 Pct Recovery = 100% Analysis Date = 06/01/12 Pct Recovery = 100% Analysis Date = 05/14/12 Pct Recovery = 100% Analysis Date = 05/14/12 Pct Recovery = 100% Analysis Date = 04/27/12 Pct Recovery = 100% Analysis Date = 04/27/12 Pct Recovery = 100% Analysis Date = 04/09/12 Pct Recovery = 101% Analysis Date = 04/09/12 Pct Recovery = 101% Analysis Date = 03/22/12 Pct Recovery = 101% Analysis Date = 03/22/12 Pct Recovery = 101% Analysis Date = 03/05/12 Pct Recovery = 101% Analysis Date = 03/05/12 Pct Recovery = 101% Analysis Date = 02/16/12 Pct Recovery = 101% Analysis Date = 02/16/12 Pct Recovery = 101% Analysis Date = 01/29/12 Pct Recovery = 101% Analysis Date = 01/29/12 Pct Recovery = 101% Analysis Date = 01/12/12 Pct Recovery = 101% Analysis Date = 01/12/12 Pct Recovery = 101% Analysis Date = 12/25/11 Pct Recovery = 101% Analysis Date = 12/25/11 Pct Recovery = 101% Analysis Date = 12/08/11 Pct Recovery = 101% Analysis Date = 12/08/11 Pct Recovery = 101% Analysis Date = 11/20/11 Pct Recovery = 102% Analysis Date = 11/20/11 Pct Recovery = 102% Analysis Date = 11/02/11 Pct Recovery = 102% Analysis Date = 11/02/11 Pct Recovery = 102% Analysis Date = 10/16/11 Pct Recovery = 102% Analysis Date = 10/16/11 Pct Recovery = 102% Analysis Date = 09/28/11 Pct Recovery = 102% Analysis Date = 09/28/11 Pct Recovery = 102% Analysis Date = 09/10/11 Pct Recovery = 102% Analysis Date = 09/10/11 Pct Recovery = 102% Analysis Date = 08/24/11 Pct Recovery = 102% Analysis Date = 08/24/11 Pct Recovery = 102% Analysis Date = 08/06/11 Pct Recovery = 102% Analysis Date = 08/06/11 Pct Recovery = 102% Analysis Date = 07/19/11 Pct Recovery = 102% Analysis Date = 07/19/11 Pct Recovery = 102% Analysis Date = 07/02/11 Pct Recovery = 102% Analysis Date = 07/02/11 Pct Recovery = 102% Analysis Date = 06/14/11 Pct Recovery = 103% Analysis Date = 06/14/11 Pct Recovery = 103% Analysis Date = 05/27/11 Pct Recovery = 103% Analysis Date = 05/27/11 Pct Recovery = 103% Analysis Date = 05/10/11 Pct Recovery = 103% Analysis Date = 05/10/11 Pct Recovery = 103% Analysis Date = 04/22/11 Pct Recovery = 103% Analysis Date = 04/22/11 Pct Recovery = 103% Analysis Date = 04/04/11 Pct Recovery = 103% Analysis Date = 04/04/11 Pct Recovery = 103% Analysis Date = 03/18/11 Pct Recovery = 103% Analysis Date = 03/18/11 Pct Recovery = 103% Analysis Date = 02/28/11 Pct Recovery = 103% Analysis Date = 02/28/11 Pct Recovery = 103% Analysis Date = 02/11/11 Pct Recovery = 103% Analysis Date = 02/11/11 Pct Recovery = 103% Analysis Date = 01/24/11 Pct Recovery = 103% Analysis Date = 01/24/11 Pct Recovery = 103% Analysis Date = 01/06/11 Pct Recovery = 104% Analysis Date = 01/06/11 Pct Recovery = 104% Analysis Date = 12/20/10 Pct Recovery = 104% Analysis Date = 12/20/10 Pct Recovery = 104% Analysis Date = 12/02/10 Pct Recovery = 104% Analysis Date = 12/02/10 Pct Recovery = 104% Analysis Date = 11/14/10 Pct Recovery = 104% Analysis Date = 11/14/10 Pct Recovery = 104% Analysis Date = 10/28/10 Pct Recovery = 104% Analysis Date = 10/28/10 Pct Recovery = 104% Analysis Date = 10/10/10 Pct Recovery = 104% Analysis Date = 10/10/10 Pct Recovery = 104% Analysis Date = 09/22/10 Pct Recovery = 104% Analysis Date = 09/22/10 Pct Recovery = 104% Analysis Date = 09/05/10 Pct Recovery = 104% Analysis Date = 09/05/10 Pct Recovery = 104% Analysis Date = 08/18/10 Pct Recovery = 104% Analysis Date = 08/18/10 Pct Recovery = 104% Analysis Date = 07/31/10 Pct Recovery = 104% Analysis Date = 07/31/10 Pct Recovery = 104% Analysis Date = 07/14/10 Pct Recovery = 105% Analysis Date = 07/14/10 Pct Recovery = 105% Analysis Date = 06/26/10 Pct Recovery = 105% Analysis Date = 06/26/10 Pct Recovery = 105% Analysis Date = 06/09/10 Pct Recovery = 105% Analysis Date = 06/09/10 Pct Recovery = 105% Analysis Date = 05/22/10 Pct Recovery = 105% Analysis Date = 05/22/10 Pct Recovery = 105% Analysis Date = 05/04/10 Pct Recovery = 105% Analysis Date = 05/04/10 Pct Recovery = 105% Analysis Date = 04/17/10 Pct Recovery = 105% Analysis Date = 04/17/10 Pct Recovery = 105% Analysis Date = 03/30/10 Pct Recovery = 105% Analysis Date = 03/30/10 Pct Recovery = 105% Analysis Date = 03/12/10 Pct Recovery = 105% Analysis Date = 03/12/10 Pct Recovery = 105% Analysis Date = 02/23/10 Pct Recovery = 105% Analysis Date = 02/23/10 Pct Recovery = 105% Analysis Date = 02/05/10 Pct Recovery = 105% Analysis Date = 02/05/10 Pct Recovery = 105% Analysis Date = 01/18/10 Pct Recovery = 105% Analysis Date = 01/18/10 Pct Recovery = 105% Analysis Date = 01/01/10 Pct Recovery = 106% Analysis Date = 01/01/10 Pct Recovery = 106% Analysis Date = 12/14/09 Pct Recovery = 106% Analysis Date = 12/14/09 Pct Recovery = 106% Analysis Date = 11/26/09 Pct Recovery = 106% Analysis Date = 11/26/09 Pct Recovery = 106% Analysis Date = 11/09/09 Pct Recovery = 106% Analysis Date = 11/09/09 Pct Recovery = 106% Analysis Date = 10/22/09 Pct Recovery = 106% Analysis Date = 10/22/09 Pct Recovery = 106% Analysis Date = 10/04/09 Pct Recovery = 106% Analysis Date = 10/04/09 Pct Recovery = 106% Analysis Date = 09/17/09 Pct Recovery = 106% Analysis Date = 09/17/09 Pct Recovery = 106% Analysis Date = 08/30/09 Pct Recovery = 106% Analysis Date = 08/30/09 Pct Recovery = 106% Analysis Date = 08/13/09 Pct Recovery = 106% Analysis Date = 08/13/09 Pct Recovery = 106% Analysis Date = 07/26/09 Pct Recovery = 106% Analysis Date = 07/26/09 Pct Recovery = 106% Analysis Date = 07/08/09 Pct Recovery = 106% Analysis Date = 07/08/09 Pct Recovery = 106% Analysis Date = 06/21/09 Pct Recovery = 106% Analysis Date = 06/21/09 Pct Recovery = 106% Analysis Date = 06/03/09 Pct Recovery = 106% Analysis Date = 06/03/09 Pct Recovery = 106% Analysis Date = 05/16/09 Pct Recovery = 106% Analysis Date = 05/16/09 Pct Recovery = 106% Analysis Date = 04/29/09 Pct Recovery = 106% Analysis Date = 04/29/09 Pct Recovery = 106% Analysis Date = 04/11/09 Pct Recovery = 106% Analysis Date = 04/11/09 Pct Recovery = 106% Analysis Date = 03/24/09 Pct Recovery = 106% Analysis Date = 03/24/09 Pct Recovery = 106% Analysis Date = 03/07/09 Pct Recovery = 106% Analysis Date = 03/07/09 Pct Recovery = 106% Analysis Date = 02/17/09 Pct Recovery = 106% Analysis Date = 02/17/09 Pct Recovery = 106% Analysis Date = 01/30/09 Pct Recovery = 106% Analysis Date = 01/30/09 Pct Recovery = 106% Analysis Date = 01/13/09 Pct Recovery = 106% Analysis Date = 01/13/09 Pct Recovery = 106% Analysis Date = 12/26/08 Pct Recovery = 106% Analysis Date = 12/26/08 Pct Recovery = 106% Analysis Date = 12/09/08 Pct Recovery = 106% Analysis Date = 12/09/08 Pct Recovery = 106% Analysis Date = 11/21/08 Pct Recovery = 106% Analysis Date = 11/21/08 Pct Recovery = 106% Analysis Date = 11/03/08 Pct Recovery = 106% Analysis Date = 11/03/08 Pct Recovery = 106% Analysis Date = 10/17/08 Pct Recovery = 107% Analysis Date = 10/17/08 Pct Recovery = 107% Analysis Date = 09/29/08 Pct Recovery = 107% Analysis Date = 09/29/08 Pct Recovery = 107% Analysis Date = 09/11/08 Pct Recovery = 107% Analysis Date = 09/11/08 Pct Recovery = 107% Analysis Date = 08/25/08 Pct Recovery = 107% Analysis Date = 08/25/08 Pct Recovery = 107% Analysis Date = 08/07/08 Pct Recovery = 107% Analysis Date = 08/07/08 Pct Recovery = 107% Analysis Date = 07/20/08 Pct Recovery = 107% Analysis Date = 07/20/08 Pct Recovery = 107% Analysis Date = 07/03/08 Pct Recovery = 107% Analysis Date = 07/03/08 Pct Recovery = 107% Analysis Date = 06/15/08 Pct Recovery = 107% Analysis Date = 06/15/08 Pct Recovery = 107% Analysis Date = 05/28/08 Pct Recovery = 107% Analysis Date = 05/28/08 Pct Recovery = 107% Analysis Date = 05/11/08 Pct Recovery = 107% Analysis Date = 05/11/08 Pct Recovery = 107% Analysis Date = 04/23/08 Pct Recovery = 107% Analysis Date = 04/23/08 Pct Recovery = 107% Analysis Date = 04/05/08 Pct Recovery = 108% Analysis Date = 04/05/08 Pct Recovery = 108% Analysis Date = 03/19/08 Pct Recovery = 108% Analysis Date = 03/19/08 Pct Recovery = 108% Analysis Date = 03/01/08 Pct Recovery = 108% Analysis Date = 03/01/08 Pct Recovery = 108% Analysis Date = 02/13/08 Pct Recovery = 108% Analysis Date = 02/13/08 Pct Recovery = 108% Analysis Date = 01/26/08 Pct Recovery = 108% Analysis Date = 01/26/08 Pct Recovery = 108% Analysis Date = 01/08/08 Pct Recovery = 108% Analysis Date = 01/08/08 Pct Recovery = 108% Analysis Date = 12/22/07 Pct Recovery = 108% Analysis Date = 12/22/07 Pct Recovery = 108% Analysis Date = 12/04/07 Pct Recovery = 108% Analysis Date = 12/04/07 Pct Recovery = 108% Analysis Date = 11/16/07 Pct Recovery = 108% Analysis Date = 11/16/07 Pct Recovery = 108% Analysis Date = 10/30/07 Pct Recovery = 109% Analysis Date = 10/30/07 Pct Recovery = 109% Analysis Date = 10/12/07 Pct Recovery = 109% Analysis Date = 10/12/07 Pct Recovery = 109% Analysis Date = 09/24/07 Pct Recovery = 109% Analysis Date = 09/24/07 Pct Recovery = 109% Analysis Date = 09/07/07 Pct Recovery = 109% Analysis Date = 09/07/07 Pct Recovery = 109% Analysis Date = 08/20/07 Pct Recovery = 109% Analysis Date = 08/20/07 Pct Recovery = 109% Analysis Date = 08/02/07 Pct Recovery = 109% Analysis Date = 08/02/07 Pct Recovery = 109% Analysis Date = 07/16/07 Pct Recovery = 109% Analysis Date = 07/16/07 Pct Recovery = 109% Analysis Date = 06/28/07 Pct Recovery = 109% Analysis Date = 06/28/07 Pct Recovery = 109% Analysis Date = 06/11/07 Pct Recovery = 109% Analysis Date = 06/11/07 Pct Recovery = 109% Analysis Date = 05/24/07 Pct Recovery = 109% Analysis Date = 05/24/07 Pct Recovery = 109% Analysis Date = 05/06/07 Pct Recovery = 109% Analysis Date = 05/06/07 Pct Recovery = 109% Analysis Date = 04/19/07 Pct Recovery = 110% Analysis Date = 04/19/07 Pct Recovery = 110% Analysis Date = 04/01/07 Pct Recovery = 110% Analysis Date = 04/01/07 Pct Recovery = 110% Analysis Date = 03/14/07 Pct Recovery = 110% Analysis Date = 03/14/07 Pct Recovery = 110% Analysis Date = 02/25/07 Pct Recovery = 110% Analysis Date = 02/25/07 Pct Recovery = 110% Analysis Date = 02/07/07 Pct Recovery = 110% Analysis Date = 02/07/07 Pct Recovery = 110% Analysis Date = 01/20/07 Pct Recovery = 110% Analysis Date = 01/20/07 Pct Recovery = 110% Analysis Date = 01/03/07 Pct Recovery = 110% Analysis Date = 01/03/07 Pct Recovery = 110% Analysis Date = 12/16/06 Pct Recovery = 110% Analysis Date = 12/16/06 Pct Recovery = 110% Analysis Date = 11/28/06 Pct Recovery = 110% Analysis Date = 11/28/06 Pct Recovery = 110% Analysis Date = 11/11/06 Pct Recovery = 110% Analysis Date = 11/11/06 Pct Recovery = 110% Analysis Date = 10/24/06 Pct Recovery = 111% Analysis Date = 10/24/06 Pct Recovery = 111% Analysis Date = 10/06/06 Pct Recovery = 111% Analysis Date = 10/06/06 Pct Recovery = 111% Analysis Date = 09/19/06 Pct Recovery = 111% Analysis Date = 09/19/06 Pct Recovery = 111% Analysis Date = 09/01/06 Pct Recovery = 111% Analysis Date = 09/01/06 Pct Recovery = 111% Analysis Date = 08/15/06 Pct Recovery = 111% Analysis Date = 08/15/06 Pct Recovery = 111% Analysis Date = 07/28/06 Pct Recovery = 111% Analysis Date = 07/28/06 Pct Recovery = 111% Analysis Date = 07/10/06 Pct Recovery = 111% Analysis Date = 07/10/06 Pct Recovery = 111% Analysis Date = 06/23/06 Pct Recovery = 111% Analysis Date = 06/23/06 Pct Recovery = 111% Analysis Date = 06/05/06 Pct Recovery = 111% Analysis Date = 06/05/06 Pct Recovery = 111% Analysis Date = 05/18/06 Pct Recovery = 111% Analysis Date = 05/18/06 Pct Recovery = 111% Analysis Date = 05/01/06 Pct Recovery = 111% Analysis Date = 05/01/06 Pct Recovery = 111% Analysis Date = 04/13/06 Pct Recovery = 111% Analysis Date = 04/13/06 Pct Recovery = 111% Analysis Date = 03/26/06 Pct Recovery = 111% Analysis Date = 03/26/06 Pct Recovery = 111% Analysis Date = 03/09/06 Pct Recovery = 112% Analysis Date = 03/09/06 Pct Recovery = 112% Analysis Date = 02/19/06 Pct Recovery = 112% Analysis Date = 02/19/06 Pct Recovery = 112% Analysis Date = 02/01/06 Pct Recovery = 112% Analysis Date = 02/01/06 Pct Recovery = 112% Analysis Date = 01/15/06 Pct Recovery = 112% Analysis Date = 01/15/06 Pct Recovery = 112% Analysis Date = 12/28/05 Pct Recovery = 112% Analysis Date = 12/28/05 Pct Recovery = 112% Analysis Date = 12/11/05 Pct Recovery = 112% Analysis Date = 12/11/05 Pct Recovery = 112% Analysis Date = 11/23/05 Pct Recovery = 112% Analysis Date = 11/23/05 Pct Recovery = 112% Analysis Date = 11/05/05 Pct Recovery = 112% Analysis Date = 11/05/05 Pct Recovery = 112% Analysis Date = 10/19/05 Pct Recovery = 112% Analysis Date = 10/19/05 Pct Recovery = 112% Analysis Date = 10/01/05 Pct Recovery = 112% Analysis Date = 10/01/05 Pct Recovery = 112% Analysis Date = 09/13/05 Pct Recovery = 112% Analysis Date = 09/13/05 Pct Recovery = 112% Analysis Date = 08/27/05 Pct Recovery = 112% Analysis Date = 08/27/05 Pct Recovery = 112% Analysis Date = 08/09/05 Pct Recovery = 112% Analysis Date = 08/09/05 Pct Recovery = 112% Analysis Date = 07/22/05 Pct Recovery = 112% Analysis Date = 07/22/05 Pct Recovery = 112% Analysis Date = 07/05/05 Pct Recovery = 112% Analysis Date = 07/05/05 Pct Recovery = 112% Analysis Date = 06/17/05 Pct Recovery = 112% Analysis Date = 06/17/05 Pct Recovery = 112% Analysis Date = 05/30/05 Pct Recovery = 112% Analysis Date = 05/30/05 Pct Recovery = 112% Analysis Date = 05/13/05 Pct Recovery = 112% Analysis Date = 05/13/05 Pct Recovery = 112% Analysis Date = 04/25/05 Pct Recovery = 112% Analysis Date = 04/25/05 Pct Recovery = 112% Analysis Date = 04/07/05 Pct Recovery = 112% Analysis Date = 04/07/05 Pct Recovery = 112% Analysis Date = 03/21/05 Pct Recovery = 112% Analysis Date = 03/21/05 Pct Recovery = 112% Analysis Date = 03/03/05 Pct Recovery = 112% Analysis Date = 03/03/05 Pct Recovery = 112% Analysis Date = 02/14/05 Pct Recovery = 112% Analysis Date = 02/14/05 Pct Recovery = 112% Analysis Date = 01/27/05 Pct Recovery = 112% Analysis Date = 01/27/05 Pct Recovery = 112% Analysis Date = 01/09/05 Pct Recovery = 112% Analysis Date = 01/09/05 Pct Recovery = 112% Analysis Date = 12/23/04 Pct Recovery = 112% Analysis Date = 12/23/04 Pct Recovery = 112% Analysis Date = 12/05/04 Pct Recovery = 112% Analysis Date = 12/05/04 Pct Recovery = 112% Analysis Date = 11/17/04 Pct Recovery = 112% Analysis Date = 11/17/04 Pct Recovery = 112% Analysis Date = 10/31/04 Pct Recovery = 112% Analysis Date = 10/31/04 Pct Recovery = 112% Analysis Date = 10/13/04 Pct Recovery = 112% Analysis Date = 10/13/04 Pct Recovery = 112% Analysis Date = 09/25/04 Pct Recovery = 111% Analysis Date = 09/25/04 Pct Recovery = 111% Analysis Date = 09/08/04 Pct Recovery = 111% Analysis Date = 09/08/04 Pct Recovery = 111% Analysis Date = 08/21/04 Pct Recovery = 111% Analysis Date = 08/21/04 Pct Recovery = 111% Analysis Date = 08/03/04 Pct Recovery = 111% Analysis Date = 08/03/04 Pct Recovery = 111% Analysis Date = 07/17/04 Pct Recovery = 111% Analysis Date = 07/17/04 Pct Recovery = 111% Analysis Date = 06/29/04 Pct Recovery = 111% Analysis Date = 06/29/04 Pct Recovery = 111% Analysis Date = 06/12/04 Pct Recovery = 111% Analysis Date = 06/12/04 Pct Recovery = 111% Analysis Date = 05/25/04 Pct Recovery = 111% Analysis Date = 05/25/04 Pct Recovery = 111% Analysis Date = 05/07/04 Pct Recovery = 111% Analysis Date = 05/07/04 Pct Recovery = 111% Analysis Date = 04/20/04 Pct Recovery = 111% Analysis Date = 04/20/04 Pct Recovery = 111% Analysis Date = 04/02/04 Pct Recovery = 111% Analysis Date = 04/02/04 Pct Recovery = 111% Analysis Date = 03/15/04 Pct Recovery = 111% Analysis Date = 03/15/04 Pct Recovery = 111% Analysis Date = 02/27/04 Pct Recovery = 111% Analysis Date = 02/27/04 Pct Recovery = 111% Analysis Date = 02/09/04 Pct Recovery = 111% Analysis Date = 02/09/04 Pct Recovery = 111% Analysis Date = 01/22/04 Pct Recovery = 111% Analysis Date = 01/22/04 Pct Recovery = 111% Analysis Date = 01/05/04 Pct Recovery = 111% Analysis Date = 01/05/04 Pct Recovery = 111% Analysis Date = 12/18/03 Pct Recovery = 111% Analysis Date = 12/18/03 Pct Recovery = 111% Analysis Date = 11/30/03 Pct Recovery = 111% Analysis Date = 11/30/03 Pct Recovery = 111% Analysis Date = 11/13/03 Pct Recovery = 111% Analysis Date = 11/13/03 Pct Recovery = 111% Analysis Date = 10/26/03 Pct Recovery = 111% Analysis Date = 10/26/03 Pct Recovery = 111% Analysis Date = 10/09/03 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHYL TERT-BUTYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 102 108% 13% 106% 12%
Total 102 108% 13% 106% 12%

Sample Statistics
ETHYL TERT-BUTYL ETHER

Characteristic N % % Basis
Plotted 102 100% Spiked
Estimated Values 13 13% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 103 .  
False Negatives 0 0% 0 out of 102
Not Spiked 90 .  
False Positives 0 0% 0 out of 90

BQS OBSP Determination:
METHYL ACETATE
METHOD: 4024 , TESTIDCODE: 77032GCM60
Open Data Set

Analysis Date = 09/03/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 130% Analysis Date = 08/11/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 107% Analysis Date = 06/05/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 77% Analysis Date = 02/20/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 145% Analysis Date = 11/14/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 136% Analysis Date = 10/22/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 133% Analysis Date = 08/25/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 105% Analysis Date = 05/18/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 97% Analysis Date = 08/31/05 SpikeMix = Absolute 071904VOC2: 25 µl Pct Recovery = 107% Analysis Date = 02/28/06 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 94% Analysis Date = 12/14/05 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 101% Analysis Date = 05/19/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 93% Analysis Date = 03/11/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 103% Analysis Date = 11/05/04 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 105% Analysis Date = 06/17/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 94% Analysis Date = 03/11/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 113% Analysis Date = 01/14/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 113% Analysis Date = 08/09/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 98% Analysis Date = 04/11/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 107% Analysis Date = 02/01/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 88% Analysis Date = 10/29/05 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 85% Analysis Date = 08/29/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 97% Analysis Date = 07/28/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 93% Analysis Date = 06/09/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 91% Analysis Date = 12/19/06 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 101% Analysis Date = 06/18/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 106% Analysis Date = 03/26/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 88% Analysis Date = 01/22/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 115% Analysis Date = 08/24/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 116% Analysis Date = 06/05/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 162% Analysis Date = 04/14/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 112% Analysis Date = 02/07/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 114% Analysis Date = 12/06/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 110% Analysis Date = 10/09/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 98% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 91% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 84% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 98% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 112% Analysis Date = 08/10/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 93% Analysis Date = 04/07/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 101% Analysis Date = 11/30/04 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 135% Analysis Date = 07/16/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 113% Analysis Date = 05/06/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 100% Analysis Date = 11/07/03 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 103% Analysis Date = 09/22/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 107% Analysis Date = 07/04/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 109% Analysis Date = 03/28/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 97% Analysis Date = 02/09/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 89% Analysis Date = 09/10/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 106% Analysis Date = 03/03/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 114% Analysis Date = 10/22/08 SpikeMix = Ultra CE-2889: 40 µl Pct Recovery = 109% Analysis Date = 02/27/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 124% Analysis Date = 09/12/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 116% Analysis Date = 08/18/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 108% Analysis Date = 06/26/13 SpikeMix = Crescent 04CC143: 20 µl Pct Recovery = 80% Analysis Date = 05/19/12 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 101% Analysis Date = 12/21/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 108% Analysis Date = 08/25/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 95% Analysis Date = 12/22/10 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 100% Analysis Date = 08/27/10 SpikeMix = Abs 083109VOA: 40 µl Pct Recovery = 103% Analysis Date = 08/18/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 103% Analysis Date = 07/03/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 111% Analysis Date = 08/21/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 87% Analysis Date = 07/11/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 95% Analysis Date = 05/24/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 97% Analysis Date = 02/15/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 97% Analysis Date = 11/18/06 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 98% Analysis Date = 02/28/13 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 81% Analysis Date = 12/03/12 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 108% Analysis Date = 03/26/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 82% Analysis Date = 01/31/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 80% Analysis Date = 09/06/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 116% Analysis Date = 08/09/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 115% Analysis Date = 07/22/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 117% Analysis Date = 06/26/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 103% Analysis Date = 05/28/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 88% Analysis Date = 05/20/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 116% Analysis Date = 04/05/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 101% Analysis Date = 03/18/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 129% Analysis Date = 12/01/07 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 114% Analysis Date = 07/09/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 116% Analysis Date = 06/06/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 111% Analysis Date = 12/18/08 SpikeMix = Restek A062148: 20 µl Pct Recovery = 110% Analysis Date = 08/07/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 125% Analysis Date = 03/23/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 145% Analysis Date = 11/14/08 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 117% Analysis Date = 07/23/13 SpikeMix = NSI 042313VOA: 10 µl Pct Recovery = 83% Analysis Date = 05/02/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 84% Analysis Date = 04/05/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 99% Analysis Date = 01/25/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 137% Analysis Date = 11/30/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 112% Analysis Date = 07/19/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 109% Analysis Date = 11/26/10 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 110% Analysis Date = 11/01/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 105% Analysis Date = 08/02/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 106% Analysis Date = 07/06/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 95% Analysis Date = 10/16/10 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 100% Analysis Date = 07/30/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 86% Analysis Date = 06/24/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 80% Analysis Date = 04/06/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 95% Analysis Date = 11/13/09 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 94% Analysis Date = 04/22/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 100% Analysis Date = 03/15/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 87% Analysis Date = 09/21/12 SpikeMix = NSI 060412-01: 10 µl Pct Recovery = 92% Analysis Date = 11/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 96% Analysis Date = 08/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 84% Analysis Date = 07/23/13 Pct Recovery = 92% Analysis Date = 07/05/13 Pct Recovery = 92% Analysis Date = 07/05/13 Pct Recovery = 92% Analysis Date = 06/17/13 Pct Recovery = 92% Analysis Date = 06/17/13 Pct Recovery = 92% Analysis Date = 05/30/13 Pct Recovery = 92% Analysis Date = 05/30/13 Pct Recovery = 92% Analysis Date = 05/12/13 Pct Recovery = 93% Analysis Date = 05/12/13 Pct Recovery = 93% Analysis Date = 04/24/13 Pct Recovery = 93% Analysis Date = 04/24/13 Pct Recovery = 93% Analysis Date = 04/06/13 Pct Recovery = 93% Analysis Date = 04/06/13 Pct Recovery = 93% Analysis Date = 03/19/13 Pct Recovery = 93% Analysis Date = 03/19/13 Pct Recovery = 93% Analysis Date = 03/02/13 Pct Recovery = 94% Analysis Date = 03/02/13 Pct Recovery = 94% Analysis Date = 02/12/13 Pct Recovery = 94% Analysis Date = 02/12/13 Pct Recovery = 94% Analysis Date = 01/25/13 Pct Recovery = 94% Analysis Date = 01/25/13 Pct Recovery = 94% Analysis Date = 01/07/13 Pct Recovery = 94% Analysis Date = 01/07/13 Pct Recovery = 94% Analysis Date = 12/20/12 Pct Recovery = 94% Analysis Date = 12/20/12 Pct Recovery = 94% Analysis Date = 12/02/12 Pct Recovery = 95% Analysis Date = 12/02/12 Pct Recovery = 95% Analysis Date = 11/14/12 Pct Recovery = 95% Analysis Date = 11/14/12 Pct Recovery = 95% Analysis Date = 10/27/12 Pct Recovery = 95% Analysis Date = 10/27/12 Pct Recovery = 95% Analysis Date = 10/10/12 Pct Recovery = 95% Analysis Date = 10/10/12 Pct Recovery = 95% Analysis Date = 09/22/12 Pct Recovery = 96% Analysis Date = 09/22/12 Pct Recovery = 96% Analysis Date = 09/04/12 Pct Recovery = 96% Analysis Date = 09/04/12 Pct Recovery = 96% Analysis Date = 08/17/12 Pct Recovery = 96% Analysis Date = 08/17/12 Pct Recovery = 96% Analysis Date = 07/30/12 Pct Recovery = 96% Analysis Date = 07/30/12 Pct Recovery = 96% Analysis Date = 07/12/12 Pct Recovery = 96% Analysis Date = 07/12/12 Pct Recovery = 96% Analysis Date = 06/24/12 Pct Recovery = 97% Analysis Date = 06/24/12 Pct Recovery = 97% Analysis Date = 06/06/12 Pct Recovery = 97% Analysis Date = 06/06/12 Pct Recovery = 97% Analysis Date = 05/20/12 Pct Recovery = 97% Analysis Date = 05/20/12 Pct Recovery = 97% Analysis Date = 05/02/12 Pct Recovery = 97% Analysis Date = 05/02/12 Pct Recovery = 97% Analysis Date = 04/14/12 Pct Recovery = 97% Analysis Date = 04/14/12 Pct Recovery = 97% Analysis Date = 03/27/12 Pct Recovery = 98% Analysis Date = 03/27/12 Pct Recovery = 98% Analysis Date = 03/09/12 Pct Recovery = 98% Analysis Date = 03/09/12 Pct Recovery = 98% Analysis Date = 02/20/12 Pct Recovery = 98% Analysis Date = 02/20/12 Pct Recovery = 98% Analysis Date = 02/02/12 Pct Recovery = 98% Analysis Date = 02/02/12 Pct Recovery = 98% Analysis Date = 01/15/12 Pct Recovery = 98% Analysis Date = 01/15/12 Pct Recovery = 98% Analysis Date = 12/29/11 Pct Recovery = 99% Analysis Date = 12/29/11 Pct Recovery = 99% Analysis Date = 12/11/11 Pct Recovery = 99% Analysis Date = 12/11/11 Pct Recovery = 99% Analysis Date = 11/23/11 Pct Recovery = 99% Analysis Date = 11/23/11 Pct Recovery = 99% Analysis Date = 11/05/11 Pct Recovery = 99% Analysis Date = 11/05/11 Pct Recovery = 99% Analysis Date = 10/18/11 Pct Recovery = 100% Analysis Date = 10/18/11 Pct Recovery = 100% Analysis Date = 09/30/11 Pct Recovery = 100% Analysis Date = 09/30/11 Pct Recovery = 100% Analysis Date = 09/12/11 Pct Recovery = 100% Analysis Date = 09/12/11 Pct Recovery = 100% Analysis Date = 08/25/11 Pct Recovery = 100% Analysis Date = 08/25/11 Pct Recovery = 100% Analysis Date = 08/08/11 Pct Recovery = 100% Analysis Date = 08/08/11 Pct Recovery = 100% Analysis Date = 07/21/11 Pct Recovery = 101% Analysis Date = 07/21/11 Pct Recovery = 101% Analysis Date = 07/03/11 Pct Recovery = 101% Analysis Date = 07/03/11 Pct Recovery = 101% Analysis Date = 06/15/11 Pct Recovery = 101% Analysis Date = 06/15/11 Pct Recovery = 101% Analysis Date = 05/28/11 Pct Recovery = 101% Analysis Date = 05/28/11 Pct Recovery = 101% Analysis Date = 05/10/11 Pct Recovery = 101% Analysis Date = 05/10/11 Pct Recovery = 101% Analysis Date = 04/22/11 Pct Recovery = 102% Analysis Date = 04/22/11 Pct Recovery = 102% Analysis Date = 04/04/11 Pct Recovery = 102% Analysis Date = 04/04/11 Pct Recovery = 102% Analysis Date = 03/18/11 Pct Recovery = 102% Analysis Date = 03/18/11 Pct Recovery = 102% Analysis Date = 02/28/11 Pct Recovery = 102% Analysis Date = 02/28/11 Pct Recovery = 102% Analysis Date = 02/10/11 Pct Recovery = 103% Analysis Date = 02/10/11 Pct Recovery = 103% Analysis Date = 01/23/11 Pct Recovery = 103% Analysis Date = 01/23/11 Pct Recovery = 103% Analysis Date = 01/05/11 Pct Recovery = 103% Analysis Date = 01/05/11 Pct Recovery = 103% Analysis Date = 12/18/10 Pct Recovery = 103% Analysis Date = 12/18/10 Pct Recovery = 103% Analysis Date = 11/30/10 Pct Recovery = 103% Analysis Date = 11/30/10 Pct Recovery = 103% Analysis Date = 11/12/10 Pct Recovery = 104% Analysis Date = 11/12/10 Pct Recovery = 104% Analysis Date = 10/26/10 Pct Recovery = 104% Analysis Date = 10/26/10 Pct Recovery = 104% Analysis Date = 10/08/10 Pct Recovery = 104% Analysis Date = 10/08/10 Pct Recovery = 104% Analysis Date = 09/20/10 Pct Recovery = 104% Analysis Date = 09/20/10 Pct Recovery = 104% Analysis Date = 09/02/10 Pct Recovery = 104% Analysis Date = 09/02/10 Pct Recovery = 104% Analysis Date = 08/15/10 Pct Recovery = 105% Analysis Date = 08/15/10 Pct Recovery = 105% Analysis Date = 07/28/10 Pct Recovery = 105% Analysis Date = 07/28/10 Pct Recovery = 105% Analysis Date = 07/10/10 Pct Recovery = 105% Analysis Date = 07/10/10 Pct Recovery = 105% Analysis Date = 06/22/10 Pct Recovery = 105% Analysis Date = 06/22/10 Pct Recovery = 105% Analysis Date = 06/05/10 Pct Recovery = 105% Analysis Date = 06/05/10 Pct Recovery = 105% Analysis Date = 05/18/10 Pct Recovery = 105% Analysis Date = 05/18/10 Pct Recovery = 105% Analysis Date = 04/30/10 Pct Recovery = 106% Analysis Date = 04/30/10 Pct Recovery = 106% Analysis Date = 04/12/10 Pct Recovery = 106% Analysis Date = 04/12/10 Pct Recovery = 106% Analysis Date = 03/25/10 Pct Recovery = 106% Analysis Date = 03/25/10 Pct Recovery = 106% Analysis Date = 03/07/10 Pct Recovery = 106% Analysis Date = 03/07/10 Pct Recovery = 106% Analysis Date = 02/17/10 Pct Recovery = 106% Analysis Date = 02/17/10 Pct Recovery = 106% Analysis Date = 01/30/10 Pct Recovery = 106% Analysis Date = 01/30/10 Pct Recovery = 106% Analysis Date = 01/13/10 Pct Recovery = 106% Analysis Date = 01/13/10 Pct Recovery = 106% Analysis Date = 12/26/09 Pct Recovery = 106% Analysis Date = 12/26/09 Pct Recovery = 106% Analysis Date = 12/08/09 Pct Recovery = 106% Analysis Date = 12/08/09 Pct Recovery = 106% Analysis Date = 11/20/09 Pct Recovery = 106% Analysis Date = 11/20/09 Pct Recovery = 106% Analysis Date = 11/02/09 Pct Recovery = 106% Analysis Date = 11/02/09 Pct Recovery = 106% Analysis Date = 10/15/09 Pct Recovery = 106% Analysis Date = 10/15/09 Pct Recovery = 106% Analysis Date = 09/27/09 Pct Recovery = 106% Analysis Date = 09/27/09 Pct Recovery = 106% Analysis Date = 09/09/09 Pct Recovery = 106% Analysis Date = 09/09/09 Pct Recovery = 106% Analysis Date = 08/23/09 Pct Recovery = 106% Analysis Date = 08/23/09 Pct Recovery = 106% Analysis Date = 08/05/09 Pct Recovery = 106% Analysis Date = 08/05/09 Pct Recovery = 106% Analysis Date = 07/18/09 Pct Recovery = 106% Analysis Date = 07/18/09 Pct Recovery = 106% Analysis Date = 06/30/09 Pct Recovery = 106% Analysis Date = 06/30/09 Pct Recovery = 106% Analysis Date = 06/12/09 Pct Recovery = 106% Analysis Date = 06/12/09 Pct Recovery = 106% Analysis Date = 05/25/09 Pct Recovery = 106% Analysis Date = 05/25/09 Pct Recovery = 106% Analysis Date = 05/07/09 Pct Recovery = 106% Analysis Date = 05/07/09 Pct Recovery = 106% Analysis Date = 04/19/09 Pct Recovery = 106% Analysis Date = 04/19/09 Pct Recovery = 106% Analysis Date = 04/02/09 Pct Recovery = 106% Analysis Date = 04/02/09 Pct Recovery = 106% Analysis Date = 03/15/09 Pct Recovery = 106% Analysis Date = 03/15/09 Pct Recovery = 106% Analysis Date = 02/25/09 Pct Recovery = 106% Analysis Date = 02/25/09 Pct Recovery = 106% Analysis Date = 02/07/09 Pct Recovery = 106% Analysis Date = 02/07/09 Pct Recovery = 106% Analysis Date = 01/20/09 Pct Recovery = 106% Analysis Date = 01/20/09 Pct Recovery = 106% Analysis Date = 01/02/09 Pct Recovery = 106% Analysis Date = 01/02/09 Pct Recovery = 106% Analysis Date = 12/15/08 Pct Recovery = 106% Analysis Date = 12/15/08 Pct Recovery = 106% Analysis Date = 11/27/08 Pct Recovery = 106% Analysis Date = 11/27/08 Pct Recovery = 106% Analysis Date = 11/10/08 Pct Recovery = 106% Analysis Date = 11/10/08 Pct Recovery = 106% Analysis Date = 10/23/08 Pct Recovery = 106% Analysis Date = 10/23/08 Pct Recovery = 106% Analysis Date = 10/05/08 Pct Recovery = 106% Analysis Date = 10/05/08 Pct Recovery = 106% Analysis Date = 09/17/08 Pct Recovery = 106% Analysis Date = 09/17/08 Pct Recovery = 106% Analysis Date = 08/30/08 Pct Recovery = 106% Analysis Date = 08/30/08 Pct Recovery = 106% Analysis Date = 08/12/08 Pct Recovery = 106% Analysis Date = 08/12/08 Pct Recovery = 106% Analysis Date = 07/25/08 Pct Recovery = 106% Analysis Date = 07/25/08 Pct Recovery = 106% Analysis Date = 07/07/08 Pct Recovery = 106% Analysis Date = 07/07/08 Pct Recovery = 106% Analysis Date = 06/20/08 Pct Recovery = 105% Analysis Date = 06/20/08 Pct Recovery = 105% Analysis Date = 06/02/08 Pct Recovery = 105% Analysis Date = 06/02/08 Pct Recovery = 105% Analysis Date = 05/15/08 Pct Recovery = 105% Analysis Date = 05/15/08 Pct Recovery = 105% Analysis Date = 04/27/08 Pct Recovery = 105% Analysis Date = 04/27/08 Pct Recovery = 105% Analysis Date = 04/09/08 Pct Recovery = 105% Analysis Date = 04/09/08 Pct Recovery = 105% Analysis Date = 03/22/08 Pct Recovery = 105% Analysis Date = 03/22/08 Pct Recovery = 105% Analysis Date = 03/04/08 Pct Recovery = 105% Analysis Date = 03/04/08 Pct Recovery = 105% Analysis Date = 02/15/08 Pct Recovery = 105% Analysis Date = 02/15/08 Pct Recovery = 105% Analysis Date = 01/29/08 Pct Recovery = 105% Analysis Date = 01/29/08 Pct Recovery = 105% Analysis Date = 01/11/08 Pct Recovery = 105% Analysis Date = 01/11/08 Pct Recovery = 105% Analysis Date = 12/24/07 Pct Recovery = 105% Analysis Date = 12/24/07 Pct Recovery = 105% Analysis Date = 12/06/07 Pct Recovery = 105% Analysis Date = 12/06/07 Pct Recovery = 105% Analysis Date = 11/18/07 Pct Recovery = 105% Analysis Date = 11/18/07 Pct Recovery = 105% Analysis Date = 10/31/07 Pct Recovery = 105% Analysis Date = 10/31/07 Pct Recovery = 105% Analysis Date = 10/13/07 Pct Recovery = 104% Analysis Date = 10/13/07 Pct Recovery = 104% Analysis Date = 09/25/07 Pct Recovery = 104% Analysis Date = 09/25/07 Pct Recovery = 104% Analysis Date = 09/08/07 Pct Recovery = 104% Analysis Date = 09/08/07 Pct Recovery = 104% Analysis Date = 08/21/07 Pct Recovery = 104% Analysis Date = 08/21/07 Pct Recovery = 104% Analysis Date = 08/03/07 Pct Recovery = 104% Analysis Date = 08/03/07 Pct Recovery = 104% Analysis Date = 07/16/07 Pct Recovery = 104% Analysis Date = 07/16/07 Pct Recovery = 104% Analysis Date = 06/28/07 Pct Recovery = 104% Analysis Date = 06/28/07 Pct Recovery = 104% Analysis Date = 06/10/07 Pct Recovery = 103% Analysis Date = 06/10/07 Pct Recovery = 103% Analysis Date = 05/23/07 Pct Recovery = 103% Analysis Date = 05/23/07 Pct Recovery = 103% Analysis Date = 05/05/07 Pct Recovery = 103% Analysis Date = 05/05/07 Pct Recovery = 103% Analysis Date = 04/18/07 Pct Recovery = 103% Analysis Date = 04/18/07 Pct Recovery = 103% Analysis Date = 03/31/07 Pct Recovery = 102% Analysis Date = 03/31/07 Pct Recovery = 102% Analysis Date = 03/13/07 Pct Recovery = 102% Analysis Date = 03/13/07 Pct Recovery = 102% Analysis Date = 02/23/07 Pct Recovery = 102% Analysis Date = 02/23/07 Pct Recovery = 102% Analysis Date = 02/05/07 Pct Recovery = 102% Analysis Date = 02/05/07 Pct Recovery = 102% Analysis Date = 01/18/07 Pct Recovery = 102% Analysis Date = 01/18/07 Pct Recovery = 102% Analysis Date = 12/31/06 Pct Recovery = 101% Analysis Date = 12/31/06 Pct Recovery = 101% Analysis Date = 12/13/06 Pct Recovery = 101% Analysis Date = 12/13/06 Pct Recovery = 101% Analysis Date = 11/26/06 Pct Recovery = 101% Analysis Date = 11/26/06 Pct Recovery = 101% Analysis Date = 11/08/06 Pct Recovery = 101% Analysis Date = 11/08/06 Pct Recovery = 101% Analysis Date = 10/21/06 Pct Recovery = 101% Analysis Date = 10/21/06 Pct Recovery = 101% Analysis Date = 10/03/06 Pct Recovery = 101% Analysis Date = 10/03/06 Pct Recovery = 101% Analysis Date = 09/15/06 Pct Recovery = 101% Analysis Date = 09/15/06 Pct Recovery = 101% Analysis Date = 08/28/06 Pct Recovery = 100% Analysis Date = 08/28/06 Pct Recovery = 100% Analysis Date = 08/10/06 Pct Recovery = 100% Analysis Date = 08/10/06 Pct Recovery = 100% Analysis Date = 07/23/06 Pct Recovery = 100% Analysis Date = 07/23/06 Pct Recovery = 100% Analysis Date = 07/06/06 Pct Recovery = 100% Analysis Date = 07/06/06 Pct Recovery = 100% Analysis Date = 06/18/06 Pct Recovery = 100% Analysis Date = 06/18/06 Pct Recovery = 100% Analysis Date = 05/31/06 Pct Recovery = 100% Analysis Date = 05/31/06 Pct Recovery = 100% Analysis Date = 05/13/06 Pct Recovery = 100% Analysis Date = 05/13/06 Pct Recovery = 100% Analysis Date = 04/25/06 Pct Recovery = 100% Analysis Date = 04/25/06 Pct Recovery = 100% Analysis Date = 04/07/06 Pct Recovery = 100% Analysis Date = 04/07/06 Pct Recovery = 100% Analysis Date = 03/20/06 Pct Recovery = 100% Analysis Date = 03/20/06 Pct Recovery = 100% Analysis Date = 03/02/06 Pct Recovery = 101% Analysis Date = 03/02/06 Pct Recovery = 101% Analysis Date = 02/13/06 Pct Recovery = 101% Analysis Date = 02/13/06 Pct Recovery = 101% Analysis Date = 01/26/06 Pct Recovery = 101% Analysis Date = 01/26/06 Pct Recovery = 101% Analysis Date = 01/08/06 Pct Recovery = 101% Analysis Date = 01/08/06 Pct Recovery = 101% Analysis Date = 12/21/05 Pct Recovery = 101% Analysis Date = 12/21/05 Pct Recovery = 101% Analysis Date = 12/03/05 Pct Recovery = 102% Analysis Date = 12/03/05 Pct Recovery = 102% Analysis Date = 11/15/05 Pct Recovery = 102% Analysis Date = 11/15/05 Pct Recovery = 102% Analysis Date = 10/28/05 Pct Recovery = 102% Analysis Date = 10/28/05 Pct Recovery = 102% Analysis Date = 10/10/05 Pct Recovery = 103% Analysis Date = 10/10/05 Pct Recovery = 103% Analysis Date = 09/23/05 Pct Recovery = 103% Analysis Date = 09/23/05 Pct Recovery = 103% Analysis Date = 09/05/05 Pct Recovery = 103% Analysis Date = 09/05/05 Pct Recovery = 103% Analysis Date = 08/18/05 Pct Recovery = 104% Analysis Date = 08/18/05 Pct Recovery = 104% Analysis Date = 07/31/05 Pct Recovery = 104% Analysis Date = 07/31/05 Pct Recovery = 104% Analysis Date = 07/13/05 Pct Recovery = 104% Analysis Date = 07/13/05 Pct Recovery = 104% Analysis Date = 06/25/05 Pct Recovery = 105% Analysis Date = 06/25/05 Pct Recovery = 105% Analysis Date = 06/07/05 Pct Recovery = 105% Analysis Date = 06/07/05 Pct Recovery = 105% Analysis Date = 05/20/05 Pct Recovery = 105% Analysis Date = 05/20/05 Pct Recovery = 105% Analysis Date = 05/03/05 Pct Recovery = 105% Analysis Date = 05/03/05 Pct Recovery = 105% Analysis Date = 04/15/05 Pct Recovery = 106% Analysis Date = 04/15/05 Pct Recovery = 106% Analysis Date = 03/28/05 Pct Recovery = 106% Analysis Date = 03/28/05 Pct Recovery = 106% Analysis Date = 03/10/05 Pct Recovery = 106% Analysis Date = 03/10/05 Pct Recovery = 106% Analysis Date = 02/20/05 Pct Recovery = 107% Analysis Date = 02/20/05 Pct Recovery = 107% Analysis Date = 02/02/05 Pct Recovery = 107% Analysis Date = 02/02/05 Pct Recovery = 107% Analysis Date = 01/15/05 Pct Recovery = 107% Analysis Date = 01/15/05 Pct Recovery = 107% Analysis Date = 12/28/04 Pct Recovery = 108% Analysis Date = 12/28/04 Pct Recovery = 108% Analysis Date = 12/11/04 Pct Recovery = 108% Analysis Date = 12/11/04 Pct Recovery = 108% Analysis Date = 11/23/04 Pct Recovery = 108% Analysis Date = 11/23/04 Pct Recovery = 108% Analysis Date = 11/05/04 Pct Recovery = 109% Analysis Date = 11/05/04 Pct Recovery = 109% Analysis Date = 10/18/04 Pct Recovery = 109% Analysis Date = 10/18/04 Pct Recovery = 109% Analysis Date = 09/30/04 Pct Recovery = 110% Analysis Date = 09/30/04 Pct Recovery = 110% Analysis Date = 09/12/04 Pct Recovery = 110% Analysis Date = 09/12/04 Pct Recovery = 110% Analysis Date = 08/25/04 Pct Recovery = 110% Analysis Date = 08/25/04 Pct Recovery = 110% Analysis Date = 08/07/04 Pct Recovery = 111% Analysis Date = 08/07/04 Pct Recovery = 111% Analysis Date = 07/21/04 Pct Recovery = 111% Analysis Date = 07/21/04 Pct Recovery = 111% Analysis Date = 07/03/04 Pct Recovery = 111% Analysis Date = 07/03/04 Pct Recovery = 111% Analysis Date = 06/15/04 Pct Recovery = 112% Analysis Date = 06/15/04 Pct Recovery = 112% Analysis Date = 05/28/04 Pct Recovery = 112% Analysis Date = 05/28/04 Pct Recovery = 112% Analysis Date = 05/10/04 Pct Recovery = 112% Analysis Date = 05/10/04 Pct Recovery = 112% Analysis Date = 04/22/04 Pct Recovery = 113% Analysis Date = 04/22/04 Pct Recovery = 113% Analysis Date = 04/04/04 Pct Recovery = 113% Analysis Date = 04/04/04 Pct Recovery = 113% Analysis Date = 03/17/04 Pct Recovery = 113% Analysis Date = 03/17/04 Pct Recovery = 113% Analysis Date = 02/29/04 Pct Recovery = 114% Analysis Date = 02/29/04 Pct Recovery = 114% Analysis Date = 02/11/04 Pct Recovery = 114% Analysis Date = 02/11/04 Pct Recovery = 114% Analysis Date = 01/24/04 Pct Recovery = 115% Analysis Date = 01/24/04 Pct Recovery = 115% Analysis Date = 01/06/04 Pct Recovery = 115% Analysis Date = 01/06/04 Pct Recovery = 115% Analysis Date = 12/19/03 Pct Recovery = 115% Analysis Date = 12/19/03 Pct Recovery = 115% Analysis Date = 12/01/03 Pct Recovery = 116% Analysis Date = 12/01/03 Pct Recovery = 116% Analysis Date = 11/13/03 Pct Recovery = 116% Analysis Date = 11/13/03 Pct Recovery = 116% Analysis Date = 10/26/03 Pct Recovery = 117% Analysis Date = 10/26/03 Pct Recovery = 117% Analysis Date = 10/09/03 Pct Recovery = 117% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL ACETATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 106 104% 15% 103% 14%
Total 106 104% 15% 103% 14%

Sample Statistics
METHYL ACETATE

Characteristic N % % Basis
Plotted 106 100% Spiked
Estimated Values 5 5% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 106 .  
False Negatives 0 0% 0 out of 106
Not Spiked 87 .  
False Positives 1 1% 1 out of 86

BQS OBSP Determination:
TERT-AMYL ALCOHOL
METHOD: 4024 , TESTIDCODE: 77073GCM60
Open Data Set

Analysis Date = 09/03/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 102% Analysis Date = 08/11/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 103% Analysis Date = 06/05/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 121% Analysis Date = 02/20/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 112% Analysis Date = 11/14/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 111% Analysis Date = 10/22/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 130% Analysis Date = 03/26/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 96% Analysis Date = 01/31/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 100% Analysis Date = 08/25/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 96% Analysis Date = 05/18/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 102% Analysis Date = 02/28/13 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 95% Analysis Date = 12/03/12 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 99% Analysis Date = 08/31/05 SpikeMix = Absolute 071904VOC2: 25 µl Pct Recovery = 99% Analysis Date = 02/28/06 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 95% Analysis Date = 12/14/05 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 100% Analysis Date = 05/19/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 89% Analysis Date = 03/11/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 86% Analysis Date = 11/05/04 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 89% Analysis Date = 08/29/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 105% Analysis Date = 07/28/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 109% Analysis Date = 06/09/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 100% Analysis Date = 12/19/06 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 118% Analysis Date = 11/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 100% Analysis Date = 08/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 108% Analysis Date = 09/21/12 SpikeMix = NSI 060412-01: 10 µl Pct Recovery = 116% Analysis Date = 08/09/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 99% Analysis Date = 04/11/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 99% Analysis Date = 02/01/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 98% Analysis Date = 10/29/05 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 81% Analysis Date = 06/18/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 97% Analysis Date = 03/26/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 81% Analysis Date = 01/22/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 91% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 92% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 96% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 83% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 94% Analysis Date = 08/10/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 96% Analysis Date = 04/07/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 85% Analysis Date = 11/30/04 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 111% Analysis Date = 06/26/13 SpikeMix = Crescent 04CC143: 20 µl Pct Recovery = 113% Analysis Date = 05/19/12 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 91% Analysis Date = 12/21/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 77% Analysis Date = 08/25/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 101% Analysis Date = 12/22/10 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 100% Analysis Date = 02/27/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 89% Analysis Date = 09/12/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 98% Analysis Date = 08/18/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 100% Analysis Date = 09/10/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 99% Analysis Date = 03/03/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 87% Analysis Date = 10/22/08 SpikeMix = Ultra CE-2889: 40 µl Pct Recovery = 94% Analysis Date = 08/21/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 101% Analysis Date = 07/11/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 113% Analysis Date = 05/24/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 122% Analysis Date = 02/15/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 121% Analysis Date = 11/18/06 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 99% Analysis Date = 08/27/10 SpikeMix = Abs 083109VOA: 40 µl Pct Recovery = 104% Analysis Date = 08/18/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 95% Analysis Date = 07/03/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 97% Analysis Date = 09/22/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 60% Analysis Date = 07/04/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 116% Analysis Date = 03/28/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 82% Analysis Date = 02/09/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 116% Analysis Date = 09/06/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 96% Analysis Date = 08/09/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 100% Analysis Date = 07/22/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 103% Analysis Date = 06/26/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 102% Analysis Date = 05/28/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 95% Analysis Date = 05/20/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 101% Analysis Date = 04/05/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 95% Analysis Date = 03/18/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 85% Analysis Date = 12/01/07 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 95% Analysis Date = 07/23/13 SpikeMix = NSI 042313VOA: 10 µl Pct Recovery = 169% Analysis Date = 11/01/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 103% Analysis Date = 08/02/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 107% Analysis Date = 07/06/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 102% Analysis Date = 10/16/10 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 78% Analysis Date = 05/02/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 86% Analysis Date = 04/05/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 103% Analysis Date = 01/25/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 117% Analysis Date = 11/30/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 108% Analysis Date = 07/19/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 103% Analysis Date = 11/26/10 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 99% Analysis Date = 07/09/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 102% Analysis Date = 06/06/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 123% Analysis Date = 12/18/08 SpikeMix = Restek A062148: 20 µl Pct Recovery = 110% Analysis Date = 08/07/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 99% Analysis Date = 03/23/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 94% Analysis Date = 11/14/08 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 108% Analysis Date = 07/30/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 108% Analysis Date = 06/24/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 102% Analysis Date = 04/06/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 98% Analysis Date = 11/13/09 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 102% Analysis Date = 04/22/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 93% Analysis Date = 03/15/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 87% Analysis Date = 07/23/13 Pct Recovery = 108% Analysis Date = 07/05/13 Pct Recovery = 108% Analysis Date = 07/05/13 Pct Recovery = 108% Analysis Date = 06/17/13 Pct Recovery = 108% Analysis Date = 06/17/13 Pct Recovery = 108% Analysis Date = 05/30/13 Pct Recovery = 108% Analysis Date = 05/30/13 Pct Recovery = 108% Analysis Date = 05/12/13 Pct Recovery = 108% Analysis Date = 05/12/13 Pct Recovery = 108% Analysis Date = 04/24/13 Pct Recovery = 107% Analysis Date = 04/24/13 Pct Recovery = 107% Analysis Date = 04/07/13 Pct Recovery = 107% Analysis Date = 04/07/13 Pct Recovery = 107% Analysis Date = 03/20/13 Pct Recovery = 107% Analysis Date = 03/20/13 Pct Recovery = 107% Analysis Date = 03/02/13 Pct Recovery = 107% Analysis Date = 03/02/13 Pct Recovery = 107% Analysis Date = 02/12/13 Pct Recovery = 107% Analysis Date = 02/12/13 Pct Recovery = 107% Analysis Date = 01/25/13 Pct Recovery = 106% Analysis Date = 01/25/13 Pct Recovery = 106% Analysis Date = 01/08/13 Pct Recovery = 106% Analysis Date = 01/08/13 Pct Recovery = 106% Analysis Date = 12/21/12 Pct Recovery = 106% Analysis Date = 12/21/12 Pct Recovery = 106% Analysis Date = 12/03/12 Pct Recovery = 106% Analysis Date = 12/03/12 Pct Recovery = 106% Analysis Date = 11/15/12 Pct Recovery = 106% Analysis Date = 11/15/12 Pct Recovery = 106% Analysis Date = 10/28/12 Pct Recovery = 106% Analysis Date = 10/28/12 Pct Recovery = 106% Analysis Date = 10/11/12 Pct Recovery = 105% Analysis Date = 10/11/12 Pct Recovery = 105% Analysis Date = 09/23/12 Pct Recovery = 105% Analysis Date = 09/23/12 Pct Recovery = 105% Analysis Date = 09/05/12 Pct Recovery = 105% Analysis Date = 09/05/12 Pct Recovery = 105% Analysis Date = 08/18/12 Pct Recovery = 105% Analysis Date = 08/18/12 Pct Recovery = 105% Analysis Date = 07/31/12 Pct Recovery = 105% Analysis Date = 07/31/12 Pct Recovery = 105% Analysis Date = 07/13/12 Pct Recovery = 104% Analysis Date = 07/13/12 Pct Recovery = 104% Analysis Date = 06/26/12 Pct Recovery = 104% Analysis Date = 06/26/12 Pct Recovery = 104% Analysis Date = 06/08/12 Pct Recovery = 104% Analysis Date = 06/08/12 Pct Recovery = 104% Analysis Date = 05/21/12 Pct Recovery = 104% Analysis Date = 05/21/12 Pct Recovery = 104% Analysis Date = 05/03/12 Pct Recovery = 104% Analysis Date = 05/03/12 Pct Recovery = 104% Analysis Date = 04/15/12 Pct Recovery = 104% Analysis Date = 04/15/12 Pct Recovery = 104% Analysis Date = 03/29/12 Pct Recovery = 103% Analysis Date = 03/29/12 Pct Recovery = 103% Analysis Date = 03/11/12 Pct Recovery = 103% Analysis Date = 03/11/12 Pct Recovery = 103% Analysis Date = 02/22/12 Pct Recovery = 103% Analysis Date = 02/22/12 Pct Recovery = 103% Analysis Date = 02/04/12 Pct Recovery = 103% Analysis Date = 02/04/12 Pct Recovery = 103% Analysis Date = 01/17/12 Pct Recovery = 103% Analysis Date = 01/17/12 Pct Recovery = 103% Analysis Date = 12/31/11 Pct Recovery = 103% Analysis Date = 12/31/11 Pct Recovery = 103% Analysis Date = 12/13/11 Pct Recovery = 102% Analysis Date = 12/13/11 Pct Recovery = 102% Analysis Date = 11/25/11 Pct Recovery = 102% Analysis Date = 11/25/11 Pct Recovery = 102% Analysis Date = 11/07/11 Pct Recovery = 102% Analysis Date = 11/07/11 Pct Recovery = 102% Analysis Date = 10/20/11 Pct Recovery = 102% Analysis Date = 10/20/11 Pct Recovery = 102% Analysis Date = 10/03/11 Pct Recovery = 102% Analysis Date = 10/03/11 Pct Recovery = 102% Analysis Date = 09/15/11 Pct Recovery = 102% Analysis Date = 09/15/11 Pct Recovery = 102% Analysis Date = 08/28/11 Pct Recovery = 101% Analysis Date = 08/28/11 Pct Recovery = 101% Analysis Date = 08/10/11 Pct Recovery = 101% Analysis Date = 08/10/11 Pct Recovery = 101% Analysis Date = 07/23/11 Pct Recovery = 101% Analysis Date = 07/23/11 Pct Recovery = 101% Analysis Date = 07/05/11 Pct Recovery = 101% Analysis Date = 07/05/11 Pct Recovery = 101% Analysis Date = 06/18/11 Pct Recovery = 101% Analysis Date = 06/18/11 Pct Recovery = 101% Analysis Date = 05/31/11 Pct Recovery = 101% Analysis Date = 05/31/11 Pct Recovery = 101% Analysis Date = 05/13/11 Pct Recovery = 101% Analysis Date = 05/13/11 Pct Recovery = 101% Analysis Date = 04/25/11 Pct Recovery = 101% Analysis Date = 04/25/11 Pct Recovery = 101% Analysis Date = 04/07/11 Pct Recovery = 100% Analysis Date = 04/07/11 Pct Recovery = 100% Analysis Date = 03/21/11 Pct Recovery = 100% Analysis Date = 03/21/11 Pct Recovery = 100% Analysis Date = 03/03/11 Pct Recovery = 100% Analysis Date = 03/03/11 Pct Recovery = 100% Analysis Date = 02/13/11 Pct Recovery = 100% Analysis Date = 02/13/11 Pct Recovery = 100% Analysis Date = 01/26/11 Pct Recovery = 100% Analysis Date = 01/26/11 Pct Recovery = 100% Analysis Date = 01/08/11 Pct Recovery = 100% Analysis Date = 01/08/11 Pct Recovery = 100% Analysis Date = 12/22/10 Pct Recovery = 100% Analysis Date = 12/22/10 Pct Recovery = 100% Analysis Date = 12/04/10 Pct Recovery = 100% Analysis Date = 12/04/10 Pct Recovery = 100% Analysis Date = 11/16/10 Pct Recovery = 99% Analysis Date = 11/16/10 Pct Recovery = 99% Analysis Date = 10/29/10 Pct Recovery = 99% Analysis Date = 10/29/10 Pct Recovery = 99% Analysis Date = 10/11/10 Pct Recovery = 99% Analysis Date = 10/11/10 Pct Recovery = 99% Analysis Date = 09/24/10 Pct Recovery = 99% Analysis Date = 09/24/10 Pct Recovery = 99% Analysis Date = 09/06/10 Pct Recovery = 99% Analysis Date = 09/06/10 Pct Recovery = 99% Analysis Date = 08/19/10 Pct Recovery = 99% Analysis Date = 08/19/10 Pct Recovery = 99% Analysis Date = 08/01/10 Pct Recovery = 99% Analysis Date = 08/01/10 Pct Recovery = 99% Analysis Date = 07/14/10 Pct Recovery = 99% Analysis Date = 07/14/10 Pct Recovery = 99% Analysis Date = 06/26/10 Pct Recovery = 99% Analysis Date = 06/26/10 Pct Recovery = 99% Analysis Date = 06/09/10 Pct Recovery = 99% Analysis Date = 06/09/10 Pct Recovery = 99% Analysis Date = 05/22/10 Pct Recovery = 99% Analysis Date = 05/22/10 Pct Recovery = 99% Analysis Date = 05/04/10 Pct Recovery = 99% Analysis Date = 05/04/10 Pct Recovery = 99% Analysis Date = 04/16/10 Pct Recovery = 99% Analysis Date = 04/16/10 Pct Recovery = 99% Analysis Date = 03/29/10 Pct Recovery = 99% Analysis Date = 03/29/10 Pct Recovery = 99% Analysis Date = 03/12/10 Pct Recovery = 99% Analysis Date = 03/12/10 Pct Recovery = 99% Analysis Date = 02/22/10 Pct Recovery = 99% Analysis Date = 02/22/10 Pct Recovery = 99% Analysis Date = 02/04/10 Pct Recovery = 99% Analysis Date = 02/04/10 Pct Recovery = 99% Analysis Date = 01/17/10 Pct Recovery = 99% Analysis Date = 01/17/10 Pct Recovery = 99% Analysis Date = 12/30/09 Pct Recovery = 99% Analysis Date = 12/30/09 Pct Recovery = 99% Analysis Date = 12/13/09 Pct Recovery = 99% Analysis Date = 12/13/09 Pct Recovery = 99% Analysis Date = 11/25/09 Pct Recovery = 99% Analysis Date = 11/25/09 Pct Recovery = 99% Analysis Date = 11/07/09 Pct Recovery = 99% Analysis Date = 11/07/09 Pct Recovery = 99% Analysis Date = 10/20/09 Pct Recovery = 99% Analysis Date = 10/20/09 Pct Recovery = 99% Analysis Date = 10/02/09 Pct Recovery = 99% Analysis Date = 10/02/09 Pct Recovery = 99% Analysis Date = 09/15/09 Pct Recovery = 99% Analysis Date = 09/15/09 Pct Recovery = 99% Analysis Date = 08/28/09 Pct Recovery = 99% Analysis Date = 08/28/09 Pct Recovery = 99% Analysis Date = 08/10/09 Pct Recovery = 99% Analysis Date = 08/10/09 Pct Recovery = 99% Analysis Date = 07/23/09 Pct Recovery = 99% Analysis Date = 07/23/09 Pct Recovery = 99% Analysis Date = 07/05/09 Pct Recovery = 100% Analysis Date = 07/05/09 Pct Recovery = 100% Analysis Date = 06/17/09 Pct Recovery = 100% Analysis Date = 06/17/09 Pct Recovery = 100% Analysis Date = 05/31/09 Pct Recovery = 100% Analysis Date = 05/31/09 Pct Recovery = 100% Analysis Date = 05/13/09 Pct Recovery = 100% Analysis Date = 05/13/09 Pct Recovery = 100% Analysis Date = 04/25/09 Pct Recovery = 100% Analysis Date = 04/25/09 Pct Recovery = 100% Analysis Date = 04/07/09 Pct Recovery = 100% Analysis Date = 04/07/09 Pct Recovery = 100% Analysis Date = 03/20/09 Pct Recovery = 100% Analysis Date = 03/20/09 Pct Recovery = 100% Analysis Date = 03/03/09 Pct Recovery = 100% Analysis Date = 03/03/09 Pct Recovery = 100% Analysis Date = 02/13/09 Pct Recovery = 100% Analysis Date = 02/13/09 Pct Recovery = 100% Analysis Date = 01/26/09 Pct Recovery = 100% Analysis Date = 01/26/09 Pct Recovery = 100% Analysis Date = 01/08/09 Pct Recovery = 100% Analysis Date = 01/08/09 Pct Recovery = 100% Analysis Date = 12/21/08 Pct Recovery = 100% Analysis Date = 12/21/08 Pct Recovery = 100% Analysis Date = 12/04/08 Pct Recovery = 100% Analysis Date = 12/04/08 Pct Recovery = 100% Analysis Date = 11/16/08 Pct Recovery = 100% Analysis Date = 11/16/08 Pct Recovery = 100% Analysis Date = 10/29/08 Pct Recovery = 100% Analysis Date = 10/29/08 Pct Recovery = 100% Analysis Date = 10/11/08 Pct Recovery = 100% Analysis Date = 10/11/08 Pct Recovery = 100% Analysis Date = 09/23/08 Pct Recovery = 100% Analysis Date = 09/23/08 Pct Recovery = 100% Analysis Date = 09/06/08 Pct Recovery = 100% Analysis Date = 09/06/08 Pct Recovery = 100% Analysis Date = 08/19/08 Pct Recovery = 101% Analysis Date = 08/19/08 Pct Recovery = 101% Analysis Date = 08/01/08 Pct Recovery = 101% Analysis Date = 08/01/08 Pct Recovery = 101% Analysis Date = 07/14/08 Pct Recovery = 101% Analysis Date = 07/14/08 Pct Recovery = 101% Analysis Date = 06/26/08 Pct Recovery = 101% Analysis Date = 06/26/08 Pct Recovery = 101% Analysis Date = 06/08/08 Pct Recovery = 101% Analysis Date = 06/08/08 Pct Recovery = 101% Analysis Date = 05/22/08 Pct Recovery = 101% Analysis Date = 05/22/08 Pct Recovery = 101% Analysis Date = 05/04/08 Pct Recovery = 101% Analysis Date = 05/04/08 Pct Recovery = 101% Analysis Date = 04/16/08 Pct Recovery = 101% Analysis Date = 04/16/08 Pct Recovery = 101% Analysis Date = 03/29/08 Pct Recovery = 101% Analysis Date = 03/29/08 Pct Recovery = 101% Analysis Date = 03/11/08 Pct Recovery = 101% Analysis Date = 03/11/08 Pct Recovery = 101% Analysis Date = 02/23/08 Pct Recovery = 101% Analysis Date = 02/23/08 Pct Recovery = 101% Analysis Date = 02/05/08 Pct Recovery = 100% Analysis Date = 02/05/08 Pct Recovery = 100% Analysis Date = 01/18/08 Pct Recovery = 100% Analysis Date = 01/18/08 Pct Recovery = 100% Analysis Date = 12/31/07 Pct Recovery = 100% Analysis Date = 12/31/07 Pct Recovery = 100% Analysis Date = 12/13/07 Pct Recovery = 100% Analysis Date = 12/13/07 Pct Recovery = 100% Analysis Date = 11/26/07 Pct Recovery = 100% Analysis Date = 11/26/07 Pct Recovery = 100% Analysis Date = 11/08/07 Pct Recovery = 100% Analysis Date = 11/08/07 Pct Recovery = 100% Analysis Date = 10/21/07 Pct Recovery = 100% Analysis Date = 10/21/07 Pct Recovery = 100% Analysis Date = 10/03/07 Pct Recovery = 100% Analysis Date = 10/03/07 Pct Recovery = 100% Analysis Date = 09/15/07 Pct Recovery = 100% Analysis Date = 09/15/07 Pct Recovery = 100% Analysis Date = 08/28/07 Pct Recovery = 100% Analysis Date = 08/28/07 Pct Recovery = 100% Analysis Date = 08/11/07 Pct Recovery = 100% Analysis Date = 08/11/07 Pct Recovery = 100% Analysis Date = 07/24/07 Pct Recovery = 100% Analysis Date = 07/24/07 Pct Recovery = 100% Analysis Date = 07/06/07 Pct Recovery = 100% Analysis Date = 07/06/07 Pct Recovery = 100% Analysis Date = 06/18/07 Pct Recovery = 100% Analysis Date = 06/18/07 Pct Recovery = 100% Analysis Date = 05/31/07 Pct Recovery = 100% Analysis Date = 05/31/07 Pct Recovery = 100% Analysis Date = 05/14/07 Pct Recovery = 100% Analysis Date = 05/14/07 Pct Recovery = 100% Analysis Date = 04/26/07 Pct Recovery = 100% Analysis Date = 04/26/07 Pct Recovery = 100% Analysis Date = 04/08/07 Pct Recovery = 100% Analysis Date = 04/08/07 Pct Recovery = 100% Analysis Date = 03/21/07 Pct Recovery = 100% Analysis Date = 03/21/07 Pct Recovery = 100% Analysis Date = 03/03/07 Pct Recovery = 100% Analysis Date = 03/03/07 Pct Recovery = 100% Analysis Date = 02/14/07 Pct Recovery = 100% Analysis Date = 02/14/07 Pct Recovery = 100% Analysis Date = 01/27/07 Pct Recovery = 100% Analysis Date = 01/27/07 Pct Recovery = 100% Analysis Date = 01/09/07 Pct Recovery = 99% Analysis Date = 01/09/07 Pct Recovery = 99% Analysis Date = 12/22/06 Pct Recovery = 99% Analysis Date = 12/22/06 Pct Recovery = 99% Analysis Date = 12/04/06 Pct Recovery = 99% Analysis Date = 12/04/06 Pct Recovery = 99% Analysis Date = 11/17/06 Pct Recovery = 99% Analysis Date = 11/17/06 Pct Recovery = 99% Analysis Date = 10/30/06 Pct Recovery = 99% Analysis Date = 10/30/06 Pct Recovery = 99% Analysis Date = 10/12/06 Pct Recovery = 99% Analysis Date = 10/12/06 Pct Recovery = 99% Analysis Date = 09/24/06 Pct Recovery = 99% Analysis Date = 09/24/06 Pct Recovery = 99% Analysis Date = 09/06/06 Pct Recovery = 99% Analysis Date = 09/06/06 Pct Recovery = 99% Analysis Date = 08/19/06 Pct Recovery = 99% Analysis Date = 08/19/06 Pct Recovery = 99% Analysis Date = 08/02/06 Pct Recovery = 99% Analysis Date = 08/02/06 Pct Recovery = 99% Analysis Date = 07/15/06 Pct Recovery = 99% Analysis Date = 07/15/06 Pct Recovery = 99% Analysis Date = 06/27/06 Pct Recovery = 99% Analysis Date = 06/27/06 Pct Recovery = 99% Analysis Date = 06/09/06 Pct Recovery = 99% Analysis Date = 06/09/06 Pct Recovery = 99% Analysis Date = 05/22/06 Pct Recovery = 99% Analysis Date = 05/22/06 Pct Recovery = 99% Analysis Date = 05/05/06 Pct Recovery = 99% Analysis Date = 05/05/06 Pct Recovery = 99% Analysis Date = 04/17/06 Pct Recovery = 99% Analysis Date = 04/17/06 Pct Recovery = 99% Analysis Date = 03/30/06 Pct Recovery = 99% Analysis Date = 03/30/06 Pct Recovery = 99% Analysis Date = 03/12/06 Pct Recovery = 98% Analysis Date = 03/12/06 Pct Recovery = 98% Analysis Date = 02/22/06 Pct Recovery = 98% Analysis Date = 02/22/06 Pct Recovery = 98% Analysis Date = 02/05/06 Pct Recovery = 98% Analysis Date = 02/05/06 Pct Recovery = 98% Analysis Date = 01/18/06 Pct Recovery = 99% Analysis Date = 01/18/06 Pct Recovery = 99% Analysis Date = 12/31/05 Pct Recovery = 99% Analysis Date = 12/31/05 Pct Recovery = 99% Analysis Date = 12/13/05 Pct Recovery = 99% Analysis Date = 12/13/05 Pct Recovery = 99% Analysis Date = 11/25/05 Pct Recovery = 99% Analysis Date = 11/25/05 Pct Recovery = 99% Analysis Date = 11/08/05 Pct Recovery = 99% Analysis Date = 11/08/05 Pct Recovery = 99% Analysis Date = 10/21/05 Pct Recovery = 99% Analysis Date = 10/21/05 Pct Recovery = 99% Analysis Date = 10/03/05 Pct Recovery = 99% Analysis Date = 10/03/05 Pct Recovery = 99% Analysis Date = 09/15/05 Pct Recovery = 99% Analysis Date = 09/15/05 Pct Recovery = 99% Analysis Date = 08/28/05 Pct Recovery = 99% Analysis Date = 08/28/05 Pct Recovery = 99% Analysis Date = 08/10/05 Pct Recovery = 99% Analysis Date = 08/10/05 Pct Recovery = 99% Analysis Date = 07/24/05 Pct Recovery = 99% Analysis Date = 07/24/05 Pct Recovery = 99% Analysis Date = 07/06/05 Pct Recovery = 99% Analysis Date = 07/06/05 Pct Recovery = 99% Analysis Date = 06/18/05 Pct Recovery = 99% Analysis Date = 06/18/05 Pct Recovery = 99% Analysis Date = 05/31/05 Pct Recovery = 99% Analysis Date = 05/31/05 Pct Recovery = 99% Analysis Date = 05/13/05 Pct Recovery = 99% Analysis Date = 05/13/05 Pct Recovery = 99% Analysis Date = 04/26/05 Pct Recovery = 99% Analysis Date = 04/26/05 Pct Recovery = 99% Analysis Date = 04/08/05 Pct Recovery = 99% Analysis Date = 04/08/05 Pct Recovery = 99% Analysis Date = 03/21/05 Pct Recovery = 99% Analysis Date = 03/21/05 Pct Recovery = 99% Analysis Date = 03/03/05 Pct Recovery = 100% Analysis Date = 03/03/05 Pct Recovery = 100% Analysis Date = 02/13/05 Pct Recovery = 100% Analysis Date = 02/13/05 Pct Recovery = 100% Analysis Date = 01/27/05 Pct Recovery = 100% Analysis Date = 01/27/05 Pct Recovery = 100% Analysis Date = 01/09/05 Pct Recovery = 100% Analysis Date = 01/09/05 Pct Recovery = 100% Analysis Date = 12/22/04 Pct Recovery = 100% Analysis Date = 12/22/04 Pct Recovery = 100% Analysis Date = 12/04/04 Pct Recovery = 100% Analysis Date = 12/04/04 Pct Recovery = 100% Analysis Date = 11/16/04 Pct Recovery = 100% Analysis Date = 11/16/04 Pct Recovery = 100% Analysis Date = 10/30/04 Pct Recovery = 100% Analysis Date = 10/30/04 Pct Recovery = 100% Analysis Date = 10/12/04 Pct Recovery = 100% Analysis Date = 10/12/04 Pct Recovery = 100% Analysis Date = 09/24/04 Pct Recovery = 100% Analysis Date = 09/24/04 Pct Recovery = 100% Analysis Date = 09/06/04 Pct Recovery = 100% Analysis Date = 09/06/04 Pct Recovery = 100% Analysis Date = 08/19/04 Pct Recovery = 100% Analysis Date = 08/19/04 Pct Recovery = 100% Analysis Date = 08/01/04 Pct Recovery = 100% Analysis Date = 08/01/04 Pct Recovery = 100% Analysis Date = 07/15/04 Pct Recovery = 101% Analysis Date = 07/15/04 Pct Recovery = 101% Analysis Date = 06/27/04 Pct Recovery = 101% Analysis Date = 06/27/04 Pct Recovery = 101% Analysis Date = 06/09/04 Pct Recovery = 101% Analysis Date = 06/09/04 Pct Recovery = 101% Analysis Date = 05/22/04 Pct Recovery = 101% Analysis Date = 05/22/04 Pct Recovery = 101% Analysis Date = 05/04/04 Pct Recovery = 101% Analysis Date = 05/04/04 Pct Recovery = 101% Analysis Date = 04/17/04 Pct Recovery = 101% Analysis Date = 04/17/04 Pct Recovery = 101% Analysis Date = 03/30/04 Pct Recovery = 101% Analysis Date = 03/30/04 Pct Recovery = 101% Analysis Date = 03/12/04 Pct Recovery = 101% Analysis Date = 03/12/04 Pct Recovery = 101% Analysis Date = 02/23/04 Pct Recovery = 101% Analysis Date = 02/23/04 Pct Recovery = 101% Analysis Date = 02/05/04 Pct Recovery = 102% Analysis Date = 02/05/04 Pct Recovery = 102% Analysis Date = 01/19/04 Pct Recovery = 102% Analysis Date = 01/19/04 Pct Recovery = 102% Analysis Date = 01/01/04 Pct Recovery = 102% Analysis Date = 01/01/04 Pct Recovery = 102% Analysis Date = 12/14/03 Pct Recovery = 102% Analysis Date = 12/14/03 Pct Recovery = 102% Analysis Date = 11/26/03 Pct Recovery = 102% Analysis Date = 11/26/03 Pct Recovery = 102% Analysis Date = 11/08/03 Pct Recovery = 102% Analysis Date = 11/08/03 Pct Recovery = 102% Analysis Date = 10/22/03 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-AMYL ALCOHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 94 100% 13% 100% 8%
Total 94 100% 13% 100% 8%

Sample Statistics
TERT-AMYL ALCOHOL

Characteristic N % % Basis
Plotted 94 100% Spiked
Estimated Values 5 5% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 94 .  
False Negatives 0 0% 0 out of 94
Not Spiked 99 .  
False Positives 0 0% 0 out of 98

BQS OBSP Determination:
TERT-BUTYL ALCOHOL
METHOD: 4024 , TESTIDCODE: 77035GCM60
Open Data Set

Analysis Date = 09/03/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 102% Analysis Date = 08/11/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 108% Analysis Date = 06/05/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 125% Analysis Date = 02/20/04 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 130% Analysis Date = 11/14/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 123% Analysis Date = 10/22/03 SpikeMix = AccuStandard B3090068: 25 µl Pct Recovery = 135% Analysis Date = 02/28/13 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 93% Analysis Date = 12/03/12 SpikeMix = NSI 060412-01: 20 µl Pct Recovery = 98% Analysis Date = 03/26/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 89% Analysis Date = 01/31/13 SpikeMix = Crescent 05BB024: 20 µl Pct Recovery = 89% Analysis Date = 08/25/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 94% Analysis Date = 05/18/06 SpikeMix = Supelco LB31916: 25 µl Pct Recovery = 102% Analysis Date = 08/31/05 SpikeMix = Absolute 071904VOC2: 25 µl Pct Recovery = 98% Analysis Date = 06/17/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 183% Analysis Date = 03/11/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 154% Analysis Date = 01/14/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 160% Analysis Date = 02/28/06 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 104% Analysis Date = 12/14/05 SpikeMix = Supelco LB31916: 20 µl Pct Recovery = 111% Analysis Date = 10/22/08 SpikeMix = Ultra CE-2889: 40 µl Pct Recovery = 92% Analysis Date = 05/19/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 93% Analysis Date = 03/11/05 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 109% Analysis Date = 11/05/04 SpikeMix = Absolute 071904VOC2: 20 µl Pct Recovery = 100% Analysis Date = 09/10/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 86% Analysis Date = 03/03/09 SpikeMix = Restek A062148: 40 µl Pct Recovery = 102% Analysis Date = 02/27/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 101% Analysis Date = 09/12/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 99% Analysis Date = 08/18/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 40 µl Pct Recovery = 103% Analysis Date = 05/19/12 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 98% Analysis Date = 12/21/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 102% Analysis Date = 08/25/11 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 93% Analysis Date = 12/22/10 SpikeMix = ChemService 443-149B: 40 µl Pct Recovery = 106% Analysis Date = 08/29/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 99% Analysis Date = 07/28/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 93% Analysis Date = 06/09/07 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 88% Analysis Date = 12/19/06 SpikeMix = Crescent 07FF044: 25 µl Pct Recovery = 104% Analysis Date = 08/27/10 SpikeMix = Abs 083109VOA: 40 µl Pct Recovery = 101% Analysis Date = 09/21/12 SpikeMix = NSI 060412-01: 10 µl Pct Recovery = 98% Analysis Date = 11/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 93% Analysis Date = 08/02/12 SpikeMix = Crescent 05BB024: 10 µl Pct Recovery = 77% Analysis Date = 08/18/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 105% Analysis Date = 07/03/10 SpikeMix = ChemService 430-41B: 40 µl Pct Recovery = 106% Analysis Date = 06/26/13 SpikeMix = Crescent 04CC143: 20 µl Pct Recovery = 101% Analysis Date = 08/24/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 92% Analysis Date = 06/05/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 121% Analysis Date = 04/14/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 104% Analysis Date = 02/07/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 158% Analysis Date = 12/06/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 158% Analysis Date = 10/09/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 142% Analysis Date = 08/09/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 100% Analysis Date = 04/11/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 86% Analysis Date = 02/01/06 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 95% Analysis Date = 10/29/05 SpikeMix = Supelco LB31916: 10 µl Pct Recovery = 73% Analysis Date = 08/07/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 115% Analysis Date = 03/23/09 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 111% Analysis Date = 11/14/08 SpikeMix = Ultra CE-2889: 20 µl Pct Recovery = 97% Analysis Date = 06/18/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 102% Analysis Date = 03/26/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 88% Analysis Date = 01/22/05 SpikeMix = Absolute 071904VOC2: 10 µl Pct Recovery = 116% Analysis Date = 07/09/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 98% Analysis Date = 06/06/09 SpikeMix = Restek A062148: 20 µl Pct Recovery = 93% Analysis Date = 12/18/08 SpikeMix = Restek A062148: 20 µl Pct Recovery = 102% Analysis Date = 05/02/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 92% Analysis Date = 04/05/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 103% Analysis Date = 01/25/12 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 108% Analysis Date = 11/30/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 114% Analysis Date = 07/19/11 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 100% Analysis Date = 11/26/10 SpikeMix = ERA 0618-10-02 LS4024 #2: 20 µl Pct Recovery = 99% Analysis Date = 11/01/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 110% Analysis Date = 08/02/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 110% Analysis Date = 07/06/11 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 101% Analysis Date = 10/16/10 SpikeMix = ChemService 443-149B: 20 µl Pct Recovery = 94% Analysis Date = 07/16/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 94% Analysis Date = 05/06/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 131% Analysis Date = 11/07/03 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 137% Analysis Date = 07/30/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 92% Analysis Date = 06/24/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 101% Analysis Date = 04/06/10 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 98% Analysis Date = 11/13/09 SpikeMix = Abs 083109VOA: 20 µl Pct Recovery = 92% Analysis Date = 04/22/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 98% Analysis Date = 03/15/10 SpikeMix = ChemService 430-41B: 20 µl Pct Recovery = 98% Analysis Date = 07/23/13 SpikeMix = NSI 042313VOA: 10 µl Pct Recovery = 124% Analysis Date = 09/06/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 77% Analysis Date = 08/09/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 77% Analysis Date = 07/22/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 98% Analysis Date = 06/26/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 98% Analysis Date = 05/28/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 88% Analysis Date = 05/20/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 88% Analysis Date = 04/05/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 88% Analysis Date = 03/18/08 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 88% Analysis Date = 12/01/07 SpikeMix = Protocol R1070705003: 20 µl Pct Recovery = 83% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 116% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 104% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 116% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 110% Analysis Date = 08/10/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 87% Analysis Date = 04/07/05 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 93% Analysis Date = 11/30/04 SpikeMix = Absolute 071904VOC2: 8 µl Pct Recovery = 87% Analysis Date = 08/21/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 93% Analysis Date = 07/11/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 100% Analysis Date = 05/24/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 113% Analysis Date = 02/15/07 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 100% Analysis Date = 11/18/06 SpikeMix = Crescent 07FF044: 10 µl Pct Recovery = 93% Analysis Date = 09/22/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 64% Analysis Date = 07/04/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 109% Analysis Date = 03/28/06 SpikeMix = Supelco LB31916: 5 µl Pct Recovery = 82% Analysis Date = 07/23/13 Pct Recovery = 100% Analysis Date = 07/05/13 Pct Recovery = 100% Analysis Date = 07/05/13 Pct Recovery = 100% Analysis Date = 06/17/13 Pct Recovery = 100% Analysis Date = 06/17/13 Pct Recovery = 100% Analysis Date = 05/30/13 Pct Recovery = 100% Analysis Date = 05/30/13 Pct Recovery = 100% Analysis Date = 05/12/13 Pct Recovery = 100% Analysis Date = 05/12/13 Pct Recovery = 100% Analysis Date = 04/24/13 Pct Recovery = 100% Analysis Date = 04/24/13 Pct Recovery = 100% Analysis Date = 04/06/13 Pct Recovery = 100% Analysis Date = 04/06/13 Pct Recovery = 100% Analysis Date = 03/19/13 Pct Recovery = 100% Analysis Date = 03/19/13 Pct Recovery = 100% Analysis Date = 03/02/13 Pct Recovery = 100% Analysis Date = 03/02/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 02/12/13 Pct Recovery = 100% Analysis Date = 01/25/13 Pct Recovery = 100% Analysis Date = 01/25/13 Pct Recovery = 100% Analysis Date = 01/07/13 Pct Recovery = 100% Analysis Date = 01/07/13 Pct Recovery = 100% Analysis Date = 12/20/12 Pct Recovery = 100% Analysis Date = 12/20/12 Pct Recovery = 100% Analysis Date = 12/02/12 Pct Recovery = 100% Analysis Date = 12/02/12 Pct Recovery = 100% Analysis Date = 11/14/12 Pct Recovery = 100% Analysis Date = 11/14/12 Pct Recovery = 100% Analysis Date = 10/27/12 Pct Recovery = 100% Analysis Date = 10/27/12 Pct Recovery = 100% Analysis Date = 10/10/12 Pct Recovery = 100% Analysis Date = 10/10/12 Pct Recovery = 100% Analysis Date = 09/22/12 Pct Recovery = 100% Analysis Date = 09/22/12 Pct Recovery = 100% Analysis Date = 09/04/12 Pct Recovery = 100% Analysis Date = 09/04/12 Pct Recovery = 100% Analysis Date = 08/17/12 Pct Recovery = 100% Analysis Date = 08/17/12 Pct Recovery = 100% Analysis Date = 07/30/12 Pct Recovery = 100% Analysis Date = 07/30/12 Pct Recovery = 100% Analysis Date = 07/12/12 Pct Recovery = 100% Analysis Date = 07/12/12 Pct Recovery = 100% Analysis Date = 06/24/12 Pct Recovery = 100% Analysis Date = 06/24/12 Pct Recovery = 100% Analysis Date = 06/06/12 Pct Recovery = 100% Analysis Date = 06/06/12 Pct Recovery = 100% Analysis Date = 05/20/12 Pct Recovery = 100% Analysis Date = 05/20/12 Pct Recovery = 100% Analysis Date = 05/02/12 Pct Recovery = 100% Analysis Date = 05/02/12 Pct Recovery = 100% Analysis Date = 04/14/12 Pct Recovery = 100% Analysis Date = 04/14/12 Pct Recovery = 100% Analysis Date = 03/27/12 Pct Recovery = 100% Analysis Date = 03/27/12 Pct Recovery = 100% Analysis Date = 03/09/12 Pct Recovery = 100% Analysis Date = 03/09/12 Pct Recovery = 100% Analysis Date = 02/20/12 Pct Recovery = 100% Analysis Date = 02/20/12 Pct Recovery = 100% Analysis Date = 02/02/12 Pct Recovery = 99% Analysis Date = 02/02/12 Pct Recovery = 99% Analysis Date = 01/15/12 Pct Recovery = 99% Analysis Date = 01/15/12 Pct Recovery = 99% Analysis Date = 12/29/11 Pct Recovery = 99% Analysis Date = 12/29/11 Pct Recovery = 99% Analysis Date = 12/11/11 Pct Recovery = 99% Analysis Date = 12/11/11 Pct Recovery = 99% Analysis Date = 11/23/11 Pct Recovery = 99% Analysis Date = 11/23/11 Pct Recovery = 99% Analysis Date = 11/05/11 Pct Recovery = 99% Analysis Date = 11/05/11 Pct Recovery = 99% Analysis Date = 10/18/11 Pct Recovery = 99% Analysis Date = 10/18/11 Pct Recovery = 99% Analysis Date = 09/30/11 Pct Recovery = 99% Analysis Date = 09/30/11 Pct Recovery = 99% Analysis Date = 09/12/11 Pct Recovery = 99% Analysis Date = 09/12/11 Pct Recovery = 99% Analysis Date = 08/25/11 Pct Recovery = 99% Analysis Date = 08/25/11 Pct Recovery = 99% Analysis Date = 08/08/11 Pct Recovery = 99% Analysis Date = 08/08/11 Pct Recovery = 99% Analysis Date = 07/21/11 Pct Recovery = 99% Analysis Date = 07/21/11 Pct Recovery = 99% Analysis Date = 07/03/11 Pct Recovery = 99% Analysis Date = 07/03/11 Pct Recovery = 99% Analysis Date = 06/15/11 Pct Recovery = 99% Analysis Date = 06/15/11 Pct Recovery = 99% Analysis Date = 05/28/11 Pct Recovery = 99% Analysis Date = 05/28/11 Pct Recovery = 99% Analysis Date = 05/10/11 Pct Recovery = 99% Analysis Date = 05/10/11 Pct Recovery = 99% Analysis Date = 04/22/11 Pct Recovery = 99% Analysis Date = 04/22/11 Pct Recovery = 99% Analysis Date = 04/04/11 Pct Recovery = 99% Analysis Date = 04/04/11 Pct Recovery = 99% Analysis Date = 03/18/11 Pct Recovery = 99% Analysis Date = 03/18/11 Pct Recovery = 99% Analysis Date = 02/28/11 Pct Recovery = 99% Analysis Date = 02/28/11 Pct Recovery = 99% Analysis Date = 02/10/11 Pct Recovery = 99% Analysis Date = 02/10/11 Pct Recovery = 99% Analysis Date = 01/23/11 Pct Recovery = 99% Analysis Date = 01/23/11 Pct Recovery = 99% Analysis Date = 01/05/11 Pct Recovery = 99% Analysis Date = 01/05/11 Pct Recovery = 99% Analysis Date = 12/18/10 Pct Recovery = 99% Analysis Date = 12/18/10 Pct Recovery = 99% Analysis Date = 11/30/10 Pct Recovery = 98% Analysis Date = 11/30/10 Pct Recovery = 98% Analysis Date = 11/12/10 Pct Recovery = 98% Analysis Date = 11/12/10 Pct Recovery = 98% Analysis Date = 10/26/10 Pct Recovery = 98% Analysis Date = 10/26/10 Pct Recovery = 98% Analysis Date = 10/08/10 Pct Recovery = 98% Analysis Date = 10/08/10 Pct Recovery = 98% Analysis Date = 09/20/10 Pct Recovery = 98% Analysis Date = 09/20/10 Pct Recovery = 98% Analysis Date = 09/02/10 Pct Recovery = 98% Analysis Date = 09/02/10 Pct Recovery = 98% Analysis Date = 08/15/10 Pct Recovery = 98% Analysis Date = 08/15/10 Pct Recovery = 98% Analysis Date = 07/28/10 Pct Recovery = 98% Analysis Date = 07/28/10 Pct Recovery = 98% Analysis Date = 07/10/10 Pct Recovery = 98% Analysis Date = 07/10/10 Pct Recovery = 98% Analysis Date = 06/22/10 Pct Recovery = 98% Analysis Date = 06/22/10 Pct Recovery = 98% Analysis Date = 06/05/10 Pct Recovery = 98% Analysis Date = 06/05/10 Pct Recovery = 98% Analysis Date = 05/18/10 Pct Recovery = 98% Analysis Date = 05/18/10 Pct Recovery = 98% Analysis Date = 04/30/10 Pct Recovery = 98% Analysis Date = 04/30/10 Pct Recovery = 98% Analysis Date = 04/12/10 Pct Recovery = 98% Analysis Date = 04/12/10 Pct Recovery = 98% Analysis Date = 03/25/10 Pct Recovery = 98% Analysis Date = 03/25/10 Pct Recovery = 98% Analysis Date = 03/07/10 Pct Recovery = 98% Analysis Date = 03/07/10 Pct Recovery = 98% Analysis Date = 02/17/10 Pct Recovery = 98% Analysis Date = 02/17/10 Pct Recovery = 98% Analysis Date = 01/30/10 Pct Recovery = 98% Analysis Date = 01/30/10 Pct Recovery = 98% Analysis Date = 01/13/10 Pct Recovery = 98% Analysis Date = 01/13/10 Pct Recovery = 98% Analysis Date = 12/26/09 Pct Recovery = 98% Analysis Date = 12/26/09 Pct Recovery = 98% Analysis Date = 12/08/09 Pct Recovery = 97% Analysis Date = 12/08/09 Pct Recovery = 97% Analysis Date = 11/20/09 Pct Recovery = 97% Analysis Date = 11/20/09 Pct Recovery = 97% Analysis Date = 11/02/09 Pct Recovery = 97% Analysis Date = 11/02/09 Pct Recovery = 97% Analysis Date = 10/15/09 Pct Recovery = 97% Analysis Date = 10/15/09 Pct Recovery = 97% Analysis Date = 09/27/09 Pct Recovery = 97% Analysis Date = 09/27/09 Pct Recovery = 97% Analysis Date = 09/09/09 Pct Recovery = 97% Analysis Date = 09/09/09 Pct Recovery = 97% Analysis Date = 08/23/09 Pct Recovery = 97% Analysis Date = 08/23/09 Pct Recovery = 97% Analysis Date = 08/05/09 Pct Recovery = 97% Analysis Date = 08/05/09 Pct Recovery = 97% Analysis Date = 07/18/09 Pct Recovery = 97% Analysis Date = 07/18/09 Pct Recovery = 97% Analysis Date = 06/30/09 Pct Recovery = 97% Analysis Date = 06/30/09 Pct Recovery = 97% Analysis Date = 06/12/09 Pct Recovery = 97% Analysis Date = 06/12/09 Pct Recovery = 97% Analysis Date = 05/25/09 Pct Recovery = 96% Analysis Date = 05/25/09 Pct Recovery = 96% Analysis Date = 05/07/09 Pct Recovery = 96% Analysis Date = 05/07/09 Pct Recovery = 96% Analysis Date = 04/19/09 Pct Recovery = 96% Analysis Date = 04/19/09 Pct Recovery = 96% Analysis Date = 04/02/09 Pct Recovery = 96% Analysis Date = 04/02/09 Pct Recovery = 96% Analysis Date = 03/15/09 Pct Recovery = 96% Analysis Date = 03/15/09 Pct Recovery = 96% Analysis Date = 02/25/09 Pct Recovery = 96% Analysis Date = 02/25/09 Pct Recovery = 96% Analysis Date = 02/07/09 Pct Recovery = 96% Analysis Date = 02/07/09 Pct Recovery = 96% Analysis Date = 01/20/09 Pct Recovery = 96% Analysis Date = 01/20/09 Pct Recovery = 96% Analysis Date = 01/02/09 Pct Recovery = 96% Analysis Date = 01/02/09 Pct Recovery = 96% Analysis Date = 12/15/08 Pct Recovery = 96% Analysis Date = 12/15/08 Pct Recovery = 96% Analysis Date = 11/27/08 Pct Recovery = 96% Analysis Date = 11/27/08 Pct Recovery = 96% Analysis Date = 11/10/08 Pct Recovery = 96% Analysis Date = 11/10/08 Pct Recovery = 96% Analysis Date = 10/23/08 Pct Recovery = 96% Analysis Date = 10/23/08 Pct Recovery = 96% Analysis Date = 10/05/08 Pct Recovery = 95% Analysis Date = 10/05/08 Pct Recovery = 95% Analysis Date = 09/17/08 Pct Recovery = 95% Analysis Date = 09/17/08 Pct Recovery = 95% Analysis Date = 08/30/08 Pct Recovery = 95% Analysis Date = 08/30/08 Pct Recovery = 95% Analysis Date = 08/12/08 Pct Recovery = 95% Analysis Date = 08/12/08 Pct Recovery = 95% Analysis Date = 07/25/08 Pct Recovery = 95% Analysis Date = 07/25/08 Pct Recovery = 95% Analysis Date = 07/07/08 Pct Recovery = 95% Analysis Date = 07/07/08 Pct Recovery = 95% Analysis Date = 06/20/08 Pct Recovery = 95% Analysis Date = 06/20/08 Pct Recovery = 95% Analysis Date = 06/02/08 Pct Recovery = 95% Analysis Date = 06/02/08 Pct Recovery = 95% Analysis Date = 05/15/08 Pct Recovery = 95% Analysis Date = 05/15/08 Pct Recovery = 95% Analysis Date = 04/27/08 Pct Recovery = 95% Analysis Date = 04/27/08 Pct Recovery = 95% Analysis Date = 04/09/08 Pct Recovery = 95% Analysis Date = 04/09/08 Pct Recovery = 95% Analysis Date = 03/22/08 Pct Recovery = 95% Analysis Date = 03/22/08 Pct Recovery = 95% Analysis Date = 03/04/08 Pct Recovery = 95% Analysis Date = 03/04/08 Pct Recovery = 95% Analysis Date = 02/15/08 Pct Recovery = 95% Analysis Date = 02/15/08 Pct Recovery = 95% Analysis Date = 01/29/08 Pct Recovery = 95% Analysis Date = 01/29/08 Pct Recovery = 95% Analysis Date = 01/11/08 Pct Recovery = 95% Analysis Date = 01/11/08 Pct Recovery = 95% Analysis Date = 12/24/07 Pct Recovery = 95% Analysis Date = 12/24/07 Pct Recovery = 95% Analysis Date = 12/06/07 Pct Recovery = 94% Analysis Date = 12/06/07 Pct Recovery = 94% Analysis Date = 11/18/07 Pct Recovery = 94% Analysis Date = 11/18/07 Pct Recovery = 94% Analysis Date = 10/31/07 Pct Recovery = 94% Analysis Date = 10/31/07 Pct Recovery = 94% Analysis Date = 10/13/07 Pct Recovery = 94% Analysis Date = 10/13/07 Pct Recovery = 94% Analysis Date = 09/25/07 Pct Recovery = 94% Analysis Date = 09/25/07 Pct Recovery = 94% Analysis Date = 09/08/07 Pct Recovery = 94% Analysis Date = 09/08/07 Pct Recovery = 94% Analysis Date = 08/21/07 Pct Recovery = 94% Analysis Date = 08/21/07 Pct Recovery = 94% Analysis Date = 08/03/07 Pct Recovery = 94% Analysis Date = 08/03/07 Pct Recovery = 94% Analysis Date = 07/16/07 Pct Recovery = 94% Analysis Date = 07/16/07 Pct Recovery = 94% Analysis Date = 06/28/07 Pct Recovery = 94% Analysis Date = 06/28/07 Pct Recovery = 94% Analysis Date = 06/10/07 Pct Recovery = 94% Analysis Date = 06/10/07 Pct Recovery = 94% Analysis Date = 05/23/07 Pct Recovery = 94% Analysis Date = 05/23/07 Pct Recovery = 94% Analysis Date = 05/05/07 Pct Recovery = 95% Analysis Date = 05/05/07 Pct Recovery = 95% Analysis Date = 04/18/07 Pct Recovery = 95% Analysis Date = 04/18/07 Pct Recovery = 95% Analysis Date = 03/31/07 Pct Recovery = 95% Analysis Date = 03/31/07 Pct Recovery = 95% Analysis Date = 03/13/07 Pct Recovery = 95% Analysis Date = 03/13/07 Pct Recovery = 95% Analysis Date = 02/23/07 Pct Recovery = 95% Analysis Date = 02/23/07 Pct Recovery = 95% Analysis Date = 02/05/07 Pct Recovery = 95% Analysis Date = 02/05/07 Pct Recovery = 95% Analysis Date = 01/18/07 Pct Recovery = 95% Analysis Date = 01/18/07 Pct Recovery = 95% Analysis Date = 12/31/06 Pct Recovery = 95% Analysis Date = 12/31/06 Pct Recovery = 95% Analysis Date = 12/13/06 Pct Recovery = 96% Analysis Date = 12/13/06 Pct Recovery = 96% Analysis Date = 11/26/06 Pct Recovery = 96% Analysis Date = 11/26/06 Pct Recovery = 96% Analysis Date = 11/08/06 Pct Recovery = 96% Analysis Date = 11/08/06 Pct Recovery = 96% Analysis Date = 10/21/06 Pct Recovery = 96% Analysis Date = 10/21/06 Pct Recovery = 96% Analysis Date = 10/03/06 Pct Recovery = 96% Analysis Date = 10/03/06 Pct Recovery = 96% Analysis Date = 09/15/06 Pct Recovery = 96% Analysis Date = 09/15/06 Pct Recovery = 96% Analysis Date = 08/28/06 Pct Recovery = 96% Analysis Date = 08/28/06 Pct Recovery = 96% Analysis Date = 08/10/06 Pct Recovery = 96% Analysis Date = 08/10/06 Pct Recovery = 96% Analysis Date = 07/23/06 Pct Recovery = 96% Analysis Date = 07/23/06 Pct Recovery = 96% Analysis Date = 07/06/06 Pct Recovery = 97% Analysis Date = 07/06/06 Pct Recovery = 97% Analysis Date = 06/18/06 Pct Recovery = 97% Analysis Date = 06/18/06 Pct Recovery = 97% Analysis Date = 05/31/06 Pct Recovery = 97% Analysis Date = 05/31/06 Pct Recovery = 97% Analysis Date = 05/13/06 Pct Recovery = 98% Analysis Date = 05/13/06 Pct Recovery = 98% Analysis Date = 04/25/06 Pct Recovery = 98% Analysis Date = 04/25/06 Pct Recovery = 98% Analysis Date = 04/07/06 Pct Recovery = 99% Analysis Date = 04/07/06 Pct Recovery = 99% Analysis Date = 03/20/06 Pct Recovery = 99% Analysis Date = 03/20/06 Pct Recovery = 99% Analysis Date = 03/02/06 Pct Recovery = 100% Analysis Date = 03/02/06 Pct Recovery = 100% Analysis Date = 02/13/06 Pct Recovery = 100% Analysis Date = 02/13/06 Pct Recovery = 100% Analysis Date = 01/26/06 Pct Recovery = 100% Analysis Date = 01/26/06 Pct Recovery = 100% Analysis Date = 01/08/06 Pct Recovery = 101% Analysis Date = 01/08/06 Pct Recovery = 101% Analysis Date = 12/21/05 Pct Recovery = 101% Analysis Date = 12/21/05 Pct Recovery = 101% Analysis Date = 12/03/05 Pct Recovery = 102% Analysis Date = 12/03/05 Pct Recovery = 102% Analysis Date = 11/15/05 Pct Recovery = 103% Analysis Date = 11/15/05 Pct Recovery = 103% Analysis Date = 10/28/05 Pct Recovery = 103% Analysis Date = 10/28/05 Pct Recovery = 103% Analysis Date = 10/10/05 Pct Recovery = 104% Analysis Date = 10/10/05 Pct Recovery = 104% Analysis Date = 09/23/05 Pct Recovery = 105% Analysis Date = 09/23/05 Pct Recovery = 105% Analysis Date = 09/05/05 Pct Recovery = 105% Analysis Date = 09/05/05 Pct Recovery = 105% Analysis Date = 08/18/05 Pct Recovery = 106% Analysis Date = 08/18/05 Pct Recovery = 106% Analysis Date = 07/31/05 Pct Recovery = 106% Analysis Date = 07/31/05 Pct Recovery = 106% Analysis Date = 07/13/05 Pct Recovery = 107% Analysis Date = 07/13/05 Pct Recovery = 107% Analysis Date = 06/25/05 Pct Recovery = 108% Analysis Date = 06/25/05 Pct Recovery = 108% Analysis Date = 06/07/05 Pct Recovery = 108% Analysis Date = 06/07/05 Pct Recovery = 108% Analysis Date = 05/20/05 Pct Recovery = 109% Analysis Date = 05/20/05 Pct Recovery = 109% Analysis Date = 05/03/05 Pct Recovery = 110% Analysis Date = 05/03/05 Pct Recovery = 110% Analysis Date = 04/15/05 Pct Recovery = 110% Analysis Date = 04/15/05 Pct Recovery = 110% Analysis Date = 03/28/05 Pct Recovery = 111% Analysis Date = 03/28/05 Pct Recovery = 111% Analysis Date = 03/10/05 Pct Recovery = 112% Analysis Date = 03/10/05 Pct Recovery = 112% Analysis Date = 02/20/05 Pct Recovery = 113% Analysis Date = 02/20/05 Pct Recovery = 113% Analysis Date = 02/02/05 Pct Recovery = 113% Analysis Date = 02/02/05 Pct Recovery = 113% Analysis Date = 01/15/05 Pct Recovery = 114% Analysis Date = 01/15/05 Pct Recovery = 114% Analysis Date = 12/28/04 Pct Recovery = 115% Analysis Date = 12/28/04 Pct Recovery = 115% Analysis Date = 12/11/04 Pct Recovery = 115% Analysis Date = 12/11/04 Pct Recovery = 115% Analysis Date = 11/23/04 Pct Recovery = 116% Analysis Date = 11/23/04 Pct Recovery = 116% Analysis Date = 11/05/04 Pct Recovery = 117% Analysis Date = 11/05/04 Pct Recovery = 117% Analysis Date = 10/18/04 Pct Recovery = 118% Analysis Date = 10/18/04 Pct Recovery = 118% Analysis Date = 09/30/04 Pct Recovery = 118% Analysis Date = 09/30/04 Pct Recovery = 118% Analysis Date = 09/12/04 Pct Recovery = 119% Analysis Date = 09/12/04 Pct Recovery = 119% Analysis Date = 08/25/04 Pct Recovery = 120% Analysis Date = 08/25/04 Pct Recovery = 120% Analysis Date = 08/07/04 Pct Recovery = 121% Analysis Date = 08/07/04 Pct Recovery = 121% Analysis Date = 07/21/04 Pct Recovery = 121% Analysis Date = 07/21/04 Pct Recovery = 121% Analysis Date = 07/03/04 Pct Recovery = 122% Analysis Date = 07/03/04 Pct Recovery = 122% Analysis Date = 06/15/04 Pct Recovery = 123% Analysis Date = 06/15/04 Pct Recovery = 123% Analysis Date = 05/28/04 Pct Recovery = 124% Analysis Date = 05/28/04 Pct Recovery = 124% Analysis Date = 05/10/04 Pct Recovery = 124% Analysis Date = 05/10/04 Pct Recovery = 124% Analysis Date = 04/22/04 Pct Recovery = 125% Analysis Date = 04/22/04 Pct Recovery = 125% Analysis Date = 04/04/04 Pct Recovery = 126% Analysis Date = 04/04/04 Pct Recovery = 126% Analysis Date = 03/17/04 Pct Recovery = 127% Analysis Date = 03/17/04 Pct Recovery = 127% Analysis Date = 02/29/04 Pct Recovery = 127% Analysis Date = 02/29/04 Pct Recovery = 127% Analysis Date = 02/11/04 Pct Recovery = 128% Analysis Date = 02/11/04 Pct Recovery = 128% Analysis Date = 01/24/04 Pct Recovery = 129% Analysis Date = 01/24/04 Pct Recovery = 129% Analysis Date = 01/06/04 Pct Recovery = 130% Analysis Date = 01/06/04 Pct Recovery = 130% Analysis Date = 12/19/03 Pct Recovery = 131% Analysis Date = 12/19/03 Pct Recovery = 131% Analysis Date = 12/01/03 Pct Recovery = 132% Analysis Date = 12/01/03 Pct Recovery = 132% Analysis Date = 11/13/03 Pct Recovery = 132% Analysis Date = 11/13/03 Pct Recovery = 132% Analysis Date = 10/26/03 Pct Recovery = 133% Analysis Date = 10/26/03 Pct Recovery = 133% Analysis Date = 10/09/03 Pct Recovery = 134% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYL ALCOHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 24 94% 13% 93% 11%
>= Reporting Level 81 106% 19% 101% 11%
Total 105 103% 19% 100% 12%

Sample Statistics
TERT-BUTYL ALCOHOL

Characteristic N % % Basis
Plotted 105 99% Spiked
Estimated Values 20 19% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 106 .  
False Negatives 0 0% 0 out of 106
Not Spiked 87 .  
False Positives 0 0% 0 out of 86

BQS OBSP Determination:
TERT-BUTYL METHYL ETHER (MTBE)
METHOD: 4024 , TESTIDCODE: 78032GCM60
Open Data Set

Analysis Date = 09/02/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 128% Analysis Date = 07/25/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 132% Analysis Date = 03/11/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 110% Analysis Date = 02/01/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 118% Analysis Date = 07/22/05 SpikeMix = Supelco LB22063: 25 µl Pct Recovery = 112% Analysis Date = 06/03/05 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 103% Analysis Date = 11/30/04 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 97% Analysis Date = 06/17/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 97% Analysis Date = 03/11/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 128% Analysis Date = 01/14/04 SpikeMix = Supelco LB14634: 30 µl Pct Recovery = 126% Analysis Date = 08/20/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 112% Analysis Date = 06/16/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 115% Analysis Date = 04/11/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 107% Analysis Date = 02/28/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 100% Analysis Date = 11/25/05 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 106% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 98% Analysis Date = 02/04/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 89% Analysis Date = 08/24/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 104% Analysis Date = 06/05/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 106% Analysis Date = 04/14/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 134% Analysis Date = 02/07/04 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 128% Analysis Date = 12/06/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 128% Analysis Date = 10/09/03 SpikeMix = ChemService 309-107A: 15 µl Pct Recovery = 111% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 103% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 97% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 97% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 99% Analysis Date = 08/31/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 112% Analysis Date = 04/15/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 104% Analysis Date = 12/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 106% Analysis Date = 10/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 109% Analysis Date = 05/04/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 106% Analysis Date = 01/12/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 108% Analysis Date = 10/29/05 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 109% Analysis Date = 07/16/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 102% Analysis Date = 05/06/04 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 108% Analysis Date = 11/07/03 SpikeMix = Supelco LB14634: 10 µl Pct Recovery = 111% Analysis Date = 07/25/09 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 108% Analysis Date = 12/11/08 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 105% Analysis Date = 07/01/09 SpikeMix = Accu B8080231: 40 µl Pct Recovery = 100% Analysis Date = 06/30/12 SpikeMix = Accu 212051187: 25 µl Pct Recovery = 75% Analysis Date = 09/18/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 79% Analysis Date = 08/29/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 93% Analysis Date = 08/02/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 96% Analysis Date = 07/14/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 111% Analysis Date = 06/22/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 96% Analysis Date = 05/31/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 93% Analysis Date = 03/23/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 104% Analysis Date = 12/29/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 93% Analysis Date = 12/01/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 104% Analysis Date = 03/26/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 137% Analysis Date = 02/19/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 126% Analysis Date = 01/03/13 SpikeMix = Accu 212051187: 20 µl Pct Recovery = 83% Analysis Date = 09/24/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 95% Analysis Date = 07/02/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 90% Analysis Date = 06/05/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 90% Analysis Date = 04/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 90% Analysis Date = 01/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 95% Analysis Date = 12/13/03 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 90% Analysis Date = 03/10/12 SpikeMix = Restek A075544: 40 µl Pct Recovery = 111% Analysis Date = 09/13/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 108% Analysis Date = 08/18/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 115% Analysis Date = 11/15/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 105% Analysis Date = 08/02/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 100% Analysis Date = 11/09/10 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 96% Analysis Date = 04/07/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 110% Analysis Date = 02/21/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 100% Analysis Date = 10/22/08 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 105% Analysis Date = 08/25/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 100% Analysis Date = 03/09/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 105% Analysis Date = 10/29/08 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 105% Analysis Date = 08/28/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 116% Analysis Date = 08/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 110% Analysis Date = 07/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 128% Analysis Date = 06/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 134% Analysis Date = 05/06/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 116% Analysis Date = 04/15/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 128% Analysis Date = 03/27/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 122% Analysis Date = 03/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 110% Analysis Date = 11/19/07 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 116% Analysis Date = 11/27/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 133% Analysis Date = 09/08/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 141% Analysis Date = 10/22/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 93% Analysis Date = 07/11/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 87% Analysis Date = 08/27/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 108% Analysis Date = 08/17/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 102% Analysis Date = 07/19/10 SpikeMix = Ultra CF-3592: 40 µl Pct Recovery = 117% Analysis Date = 02/10/12 SpikeMix = Restek A075544: 20 µl Pct Recovery = 102% Analysis Date = 10/15/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 94% Analysis Date = 06/21/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 104% Analysis Date = 10/09/10 SpikeMix = Restek A075544: 20 µl Pct Recovery = 99% Analysis Date = 06/07/12 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 86% Analysis Date = 08/26/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 94% Analysis Date = 07/19/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 92% Analysis Date = 12/10/10 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 89% Analysis Date = 06/07/13 SpikeMix = ChemService 1448500: 10 µl Pct Recovery = 114% Analysis Date = 06/24/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 116% Analysis Date = 04/22/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 108% Analysis Date = 02/09/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 104% Analysis Date = 05/06/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 102% Analysis Date = 03/26/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 112% Analysis Date = 10/26/09 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 96% Analysis Date = 06/07/13 Pct Recovery = 106% Analysis Date = 05/20/13 Pct Recovery = 106% Analysis Date = 05/20/13 Pct Recovery = 106% Analysis Date = 05/02/13 Pct Recovery = 106% Analysis Date = 05/02/13 Pct Recovery = 106% Analysis Date = 04/15/13 Pct Recovery = 106% Analysis Date = 04/15/13 Pct Recovery = 106% Analysis Date = 03/28/13 Pct Recovery = 106% Analysis Date = 03/28/13 Pct Recovery = 106% Analysis Date = 03/10/13 Pct Recovery = 106% Analysis Date = 03/10/13 Pct Recovery = 106% Analysis Date = 02/21/13 Pct Recovery = 106% Analysis Date = 02/21/13 Pct Recovery = 106% Analysis Date = 02/03/13 Pct Recovery = 106% Analysis Date = 02/03/13 Pct Recovery = 106% Analysis Date = 01/16/13 Pct Recovery = 106% Analysis Date = 01/16/13 Pct Recovery = 106% Analysis Date = 12/30/12 Pct Recovery = 106% Analysis Date = 12/30/12 Pct Recovery = 106% Analysis Date = 12/12/12 Pct Recovery = 106% Analysis Date = 12/12/12 Pct Recovery = 106% Analysis Date = 11/24/12 Pct Recovery = 106% Analysis Date = 11/24/12 Pct Recovery = 106% Analysis Date = 11/07/12 Pct Recovery = 106% Analysis Date = 11/07/12 Pct Recovery = 106% Analysis Date = 10/20/12 Pct Recovery = 105% Analysis Date = 10/20/12 Pct Recovery = 105% Analysis Date = 10/02/12 Pct Recovery = 105% Analysis Date = 10/02/12 Pct Recovery = 105% Analysis Date = 09/15/12 Pct Recovery = 105% Analysis Date = 09/15/12 Pct Recovery = 105% Analysis Date = 08/28/12 Pct Recovery = 105% Analysis Date = 08/28/12 Pct Recovery = 105% Analysis Date = 08/11/12 Pct Recovery = 105% Analysis Date = 08/11/12 Pct Recovery = 105% Analysis Date = 07/24/12 Pct Recovery = 105% Analysis Date = 07/24/12 Pct Recovery = 105% Analysis Date = 07/06/12 Pct Recovery = 105% Analysis Date = 07/06/12 Pct Recovery = 105% Analysis Date = 06/19/12 Pct Recovery = 105% Analysis Date = 06/19/12 Pct Recovery = 105% Analysis Date = 06/01/12 Pct Recovery = 105% Analysis Date = 06/01/12 Pct Recovery = 105% Analysis Date = 05/14/12 Pct Recovery = 105% Analysis Date = 05/14/12 Pct Recovery = 105% Analysis Date = 04/27/12 Pct Recovery = 105% Analysis Date = 04/27/12 Pct Recovery = 105% Analysis Date = 04/09/12 Pct Recovery = 105% Analysis Date = 04/09/12 Pct Recovery = 105% Analysis Date = 03/22/12 Pct Recovery = 105% Analysis Date = 03/22/12 Pct Recovery = 105% Analysis Date = 03/05/12 Pct Recovery = 105% Analysis Date = 03/05/12 Pct Recovery = 105% Analysis Date = 02/16/12 Pct Recovery = 105% Analysis Date = 02/16/12 Pct Recovery = 105% Analysis Date = 01/29/12 Pct Recovery = 105% Analysis Date = 01/29/12 Pct Recovery = 105% Analysis Date = 01/12/12 Pct Recovery = 105% Analysis Date = 01/12/12 Pct Recovery = 105% Analysis Date = 12/25/11 Pct Recovery = 105% Analysis Date = 12/25/11 Pct Recovery = 105% Analysis Date = 12/08/11 Pct Recovery = 105% Analysis Date = 12/08/11 Pct Recovery = 105% Analysis Date = 11/20/11 Pct Recovery = 105% Analysis Date = 11/20/11 Pct Recovery = 105% Analysis Date = 11/02/11 Pct Recovery = 105% Analysis Date = 11/02/11 Pct Recovery = 105% Analysis Date = 10/16/11 Pct Recovery = 105% Analysis Date = 10/16/11 Pct Recovery = 105% Analysis Date = 09/28/11 Pct Recovery = 105% Analysis Date = 09/28/11 Pct Recovery = 105% Analysis Date = 09/10/11 Pct Recovery = 105% Analysis Date = 09/10/11 Pct Recovery = 105% Analysis Date = 08/24/11 Pct Recovery = 105% Analysis Date = 08/24/11 Pct Recovery = 105% Analysis Date = 08/06/11 Pct Recovery = 105% Analysis Date = 08/06/11 Pct Recovery = 105% Analysis Date = 07/19/11 Pct Recovery = 105% Analysis Date = 07/19/11 Pct Recovery = 105% Analysis Date = 07/02/11 Pct Recovery = 105% Analysis Date = 07/02/11 Pct Recovery = 105% Analysis Date = 06/14/11 Pct Recovery = 105% Analysis Date = 06/14/11 Pct Recovery = 105% Analysis Date = 05/27/11 Pct Recovery = 105% Analysis Date = 05/27/11 Pct Recovery = 105% Analysis Date = 05/10/11 Pct Recovery = 105% Analysis Date = 05/10/11 Pct Recovery = 105% Analysis Date = 04/22/11 Pct Recovery = 105% Analysis Date = 04/22/11 Pct Recovery = 105% Analysis Date = 04/04/11 Pct Recovery = 105% Analysis Date = 04/04/11 Pct Recovery = 105% Analysis Date = 03/18/11 Pct Recovery = 105% Analysis Date = 03/18/11 Pct Recovery = 105% Analysis Date = 02/28/11 Pct Recovery = 105% Analysis Date = 02/28/11 Pct Recovery = 105% Analysis Date = 02/11/11 Pct Recovery = 105% Analysis Date = 02/11/11 Pct Recovery = 105% Analysis Date = 01/24/11 Pct Recovery = 105% Analysis Date = 01/24/11 Pct Recovery = 105% Analysis Date = 01/06/11 Pct Recovery = 105% Analysis Date = 01/06/11 Pct Recovery = 105% Analysis Date = 12/20/10 Pct Recovery = 105% Analysis Date = 12/20/10 Pct Recovery = 105% Analysis Date = 12/02/10 Pct Recovery = 105% Analysis Date = 12/02/10 Pct Recovery = 105% Analysis Date = 11/14/10 Pct Recovery = 105% Analysis Date = 11/14/10 Pct Recovery = 105% Analysis Date = 10/28/10 Pct Recovery = 105% Analysis Date = 10/28/10 Pct Recovery = 105% Analysis Date = 10/10/10 Pct Recovery = 105% Analysis Date = 10/10/10 Pct Recovery = 105% Analysis Date = 09/22/10 Pct Recovery = 105% Analysis Date = 09/22/10 Pct Recovery = 105% Analysis Date = 09/05/10 Pct Recovery = 105% Analysis Date = 09/05/10 Pct Recovery = 105% Analysis Date = 08/18/10 Pct Recovery = 105% Analysis Date = 08/18/10 Pct Recovery = 105% Analysis Date = 07/31/10 Pct Recovery = 105% Analysis Date = 07/31/10 Pct Recovery = 105% Analysis Date = 07/14/10 Pct Recovery = 105% Analysis Date = 07/14/10 Pct Recovery = 105% Analysis Date = 06/26/10 Pct Recovery = 105% Analysis Date = 06/26/10 Pct Recovery = 105% Analysis Date = 06/09/10 Pct Recovery = 105% Analysis Date = 06/09/10 Pct Recovery = 105% Analysis Date = 05/22/10 Pct Recovery = 105% Analysis Date = 05/22/10 Pct Recovery = 105% Analysis Date = 05/04/10 Pct Recovery = 105% Analysis Date = 05/04/10 Pct Recovery = 105% Analysis Date = 04/17/10 Pct Recovery = 105% Analysis Date = 04/17/10 Pct Recovery = 105% Analysis Date = 03/30/10 Pct Recovery = 106% Analysis Date = 03/30/10 Pct Recovery = 106% Analysis Date = 03/12/10 Pct Recovery = 106% Analysis Date = 03/12/10 Pct Recovery = 106% Analysis Date = 02/23/10 Pct Recovery = 106% Analysis Date = 02/23/10 Pct Recovery = 106% Analysis Date = 02/05/10 Pct Recovery = 106% Analysis Date = 02/05/10 Pct Recovery = 106% Analysis Date = 01/18/10 Pct Recovery = 106% Analysis Date = 01/18/10 Pct Recovery = 106% Analysis Date = 01/01/10 Pct Recovery = 106% Analysis Date = 01/01/10 Pct Recovery = 106% Analysis Date = 12/14/09 Pct Recovery = 106% Analysis Date = 12/14/09 Pct Recovery = 106% Analysis Date = 11/26/09 Pct Recovery = 106% Analysis Date = 11/26/09 Pct Recovery = 106% Analysis Date = 11/09/09 Pct Recovery = 106% Analysis Date = 11/09/09 Pct Recovery = 106% Analysis Date = 10/22/09 Pct Recovery = 106% Analysis Date = 10/22/09 Pct Recovery = 106% Analysis Date = 10/04/09 Pct Recovery = 106% Analysis Date = 10/04/09 Pct Recovery = 106% Analysis Date = 09/17/09 Pct Recovery = 106% Analysis Date = 09/17/09 Pct Recovery = 106% Analysis Date = 08/30/09 Pct Recovery = 106% Analysis Date = 08/30/09 Pct Recovery = 106% Analysis Date = 08/13/09 Pct Recovery = 106% Analysis Date = 08/13/09 Pct Recovery = 106% Analysis Date = 07/26/09 Pct Recovery = 106% Analysis Date = 07/26/09 Pct Recovery = 106% Analysis Date = 07/08/09 Pct Recovery = 106% Analysis Date = 07/08/09 Pct Recovery = 106% Analysis Date = 06/21/09 Pct Recovery = 107% Analysis Date = 06/21/09 Pct Recovery = 107% Analysis Date = 06/03/09 Pct Recovery = 107% Analysis Date = 06/03/09 Pct Recovery = 107% Analysis Date = 05/16/09 Pct Recovery = 107% Analysis Date = 05/16/09 Pct Recovery = 107% Analysis Date = 04/29/09 Pct Recovery = 107% Analysis Date = 04/29/09 Pct Recovery = 107% Analysis Date = 04/11/09 Pct Recovery = 107% Analysis Date = 04/11/09 Pct Recovery = 107% Analysis Date = 03/24/09 Pct Recovery = 107% Analysis Date = 03/24/09 Pct Recovery = 107% Analysis Date = 03/07/09 Pct Recovery = 107% Analysis Date = 03/07/09 Pct Recovery = 107% Analysis Date = 02/17/09 Pct Recovery = 107% Analysis Date = 02/17/09 Pct Recovery = 107% Analysis Date = 01/30/09 Pct Recovery = 107% Analysis Date = 01/30/09 Pct Recovery = 107% Analysis Date = 01/13/09 Pct Recovery = 107% Analysis Date = 01/13/09 Pct Recovery = 107% Analysis Date = 12/26/08 Pct Recovery = 107% Analysis Date = 12/26/08 Pct Recovery = 107% Analysis Date = 12/09/08 Pct Recovery = 107% Analysis Date = 12/09/08 Pct Recovery = 107% Analysis Date = 11/21/08 Pct Recovery = 107% Analysis Date = 11/21/08 Pct Recovery = 107% Analysis Date = 11/03/08 Pct Recovery = 107% Analysis Date = 11/03/08 Pct Recovery = 107% Analysis Date = 10/17/08 Pct Recovery = 107% Analysis Date = 10/17/08 Pct Recovery = 107% Analysis Date = 09/29/08 Pct Recovery = 108% Analysis Date = 09/29/08 Pct Recovery = 108% Analysis Date = 09/11/08 Pct Recovery = 108% Analysis Date = 09/11/08 Pct Recovery = 108% Analysis Date = 08/25/08 Pct Recovery = 108% Analysis Date = 08/25/08 Pct Recovery = 108% Analysis Date = 08/07/08 Pct Recovery = 108% Analysis Date = 08/07/08 Pct Recovery = 108% Analysis Date = 07/20/08 Pct Recovery = 108% Analysis Date = 07/20/08 Pct Recovery = 108% Analysis Date = 07/03/08 Pct Recovery = 108% Analysis Date = 07/03/08 Pct Recovery = 108% Analysis Date = 06/15/08 Pct Recovery = 108% Analysis Date = 06/15/08 Pct Recovery = 108% Analysis Date = 05/28/08 Pct Recovery = 108% Analysis Date = 05/28/08 Pct Recovery = 108% Analysis Date = 05/11/08 Pct Recovery = 108% Analysis Date = 05/11/08 Pct Recovery = 108% Analysis Date = 04/23/08 Pct Recovery = 108% Analysis Date = 04/23/08 Pct Recovery = 108% Analysis Date = 04/05/08 Pct Recovery = 108% Analysis Date = 04/05/08 Pct Recovery = 108% Analysis Date = 03/19/08 Pct Recovery = 108% Analysis Date = 03/19/08 Pct Recovery = 108% Analysis Date = 03/01/08 Pct Recovery = 108% Analysis Date = 03/01/08 Pct Recovery = 108% Analysis Date = 02/13/08 Pct Recovery = 108% Analysis Date = 02/13/08 Pct Recovery = 108% Analysis Date = 01/26/08 Pct Recovery = 108% Analysis Date = 01/26/08 Pct Recovery = 108% Analysis Date = 01/08/08 Pct Recovery = 108% Analysis Date = 01/08/08 Pct Recovery = 108% Analysis Date = 12/22/07 Pct Recovery = 108% Analysis Date = 12/22/07 Pct Recovery = 108% Analysis Date = 12/04/07 Pct Recovery = 108% Analysis Date = 12/04/07 Pct Recovery = 108% Analysis Date = 11/16/07 Pct Recovery = 108% Analysis Date = 11/16/07 Pct Recovery = 108% Analysis Date = 10/30/07 Pct Recovery = 108% Analysis Date = 10/30/07 Pct Recovery = 108% Analysis Date = 10/12/07 Pct Recovery = 108% Analysis Date = 10/12/07 Pct Recovery = 108% Analysis Date = 09/24/07 Pct Recovery = 109% Analysis Date = 09/24/07 Pct Recovery = 109% Analysis Date = 09/07/07 Pct Recovery = 109% Analysis Date = 09/07/07 Pct Recovery = 109% Analysis Date = 08/20/07 Pct Recovery = 109% Analysis Date = 08/20/07 Pct Recovery = 109% Analysis Date = 08/02/07 Pct Recovery = 108% Analysis Date = 08/02/07 Pct Recovery = 108% Analysis Date = 07/16/07 Pct Recovery = 108% Analysis Date = 07/16/07 Pct Recovery = 108% Analysis Date = 06/28/07 Pct Recovery = 108% Analysis Date = 06/28/07 Pct Recovery = 108% Analysis Date = 06/11/07 Pct Recovery = 108% Analysis Date = 06/11/07 Pct Recovery = 108% Analysis Date = 05/24/07 Pct Recovery = 108% Analysis Date = 05/24/07 Pct Recovery = 108% Analysis Date = 05/06/07 Pct Recovery = 108% Analysis Date = 05/06/07 Pct Recovery = 108% Analysis Date = 04/19/07 Pct Recovery = 108% Analysis Date = 04/19/07 Pct Recovery = 108% Analysis Date = 04/01/07 Pct Recovery = 108% Analysis Date = 04/01/07 Pct Recovery = 108% Analysis Date = 03/14/07 Pct Recovery = 108% Analysis Date = 03/14/07 Pct Recovery = 108% Analysis Date = 02/25/07 Pct Recovery = 107% Analysis Date = 02/25/07 Pct Recovery = 107% Analysis Date = 02/07/07 Pct Recovery = 107% Analysis Date = 02/07/07 Pct Recovery = 107% Analysis Date = 01/20/07 Pct Recovery = 107% Analysis Date = 01/20/07 Pct Recovery = 107% Analysis Date = 01/03/07 Pct Recovery = 107% Analysis Date = 01/03/07 Pct Recovery = 107% Analysis Date = 12/16/06 Pct Recovery = 107% Analysis Date = 12/16/06 Pct Recovery = 107% Analysis Date = 11/28/06 Pct Recovery = 107% Analysis Date = 11/28/06 Pct Recovery = 107% Analysis Date = 11/11/06 Pct Recovery = 107% Analysis Date = 11/11/06 Pct Recovery = 107% Analysis Date = 10/24/06 Pct Recovery = 107% Analysis Date = 10/24/06 Pct Recovery = 107% Analysis Date = 10/06/06 Pct Recovery = 107% Analysis Date = 10/06/06 Pct Recovery = 107% Analysis Date = 09/19/06 Pct Recovery = 107% Analysis Date = 09/19/06 Pct Recovery = 107% Analysis Date = 09/01/06 Pct Recovery = 106% Analysis Date = 09/01/06 Pct Recovery = 106% Analysis Date = 08/15/06 Pct Recovery = 106% Analysis Date = 08/15/06 Pct Recovery = 106% Analysis Date = 07/28/06 Pct Recovery = 106% Analysis Date = 07/28/06 Pct Recovery = 106% Analysis Date = 07/10/06 Pct Recovery = 106% Analysis Date = 07/10/06 Pct Recovery = 106% Analysis Date = 06/23/06 Pct Recovery = 106% Analysis Date = 06/23/06 Pct Recovery = 106% Analysis Date = 06/05/06 Pct Recovery = 106% Analysis Date = 06/05/06 Pct Recovery = 106% Analysis Date = 05/18/06 Pct Recovery = 106% Analysis Date = 05/18/06 Pct Recovery = 106% Analysis Date = 05/01/06 Pct Recovery = 106% Analysis Date = 05/01/06 Pct Recovery = 106% Analysis Date = 04/13/06 Pct Recovery = 106% Analysis Date = 04/13/06 Pct Recovery = 106% Analysis Date = 03/26/06 Pct Recovery = 106% Analysis Date = 03/26/06 Pct Recovery = 106% Analysis Date = 03/09/06 Pct Recovery = 106% Analysis Date = 03/09/06 Pct Recovery = 106% Analysis Date = 02/19/06 Pct Recovery = 106% Analysis Date = 02/19/06 Pct Recovery = 106% Analysis Date = 02/01/06 Pct Recovery = 106% Analysis Date = 02/01/06 Pct Recovery = 106% Analysis Date = 01/15/06 Pct Recovery = 106% Analysis Date = 01/15/06 Pct Recovery = 106% Analysis Date = 12/28/05 Pct Recovery = 106% Analysis Date = 12/28/05 Pct Recovery = 106% Analysis Date = 12/11/05 Pct Recovery = 106% Analysis Date = 12/11/05 Pct Recovery = 106% Analysis Date = 11/23/05 Pct Recovery = 106% Analysis Date = 11/23/05 Pct Recovery = 106% Analysis Date = 11/05/05 Pct Recovery = 106% Analysis Date = 11/05/05 Pct Recovery = 106% Analysis Date = 10/19/05 Pct Recovery = 106% Analysis Date = 10/19/05 Pct Recovery = 106% Analysis Date = 10/01/05 Pct Recovery = 106% Analysis Date = 10/01/05 Pct Recovery = 106% Analysis Date = 09/13/05 Pct Recovery = 106% Analysis Date = 09/13/05 Pct Recovery = 106% Analysis Date = 08/27/05 Pct Recovery = 106% Analysis Date = 08/27/05 Pct Recovery = 106% Analysis Date = 08/09/05 Pct Recovery = 106% Analysis Date = 08/09/05 Pct Recovery = 106% Analysis Date = 07/22/05 Pct Recovery = 106% Analysis Date = 07/22/05 Pct Recovery = 106% Analysis Date = 07/05/05 Pct Recovery = 106% Analysis Date = 07/05/05 Pct Recovery = 106% Analysis Date = 06/17/05 Pct Recovery = 106% Analysis Date = 06/17/05 Pct Recovery = 106% Analysis Date = 05/30/05 Pct Recovery = 106% Analysis Date = 05/30/05 Pct Recovery = 106% Analysis Date = 05/13/05 Pct Recovery = 106% Analysis Date = 05/13/05 Pct Recovery = 106% Analysis Date = 04/25/05 Pct Recovery = 106% Analysis Date = 04/25/05 Pct Recovery = 106% Analysis Date = 04/07/05 Pct Recovery = 106% Analysis Date = 04/07/05 Pct Recovery = 106% Analysis Date = 03/21/05 Pct Recovery = 106% Analysis Date = 03/21/05 Pct Recovery = 106% Analysis Date = 03/03/05 Pct Recovery = 106% Analysis Date = 03/03/05 Pct Recovery = 106% Analysis Date = 02/14/05 Pct Recovery = 106% Analysis Date = 02/14/05 Pct Recovery = 106% Analysis Date = 01/27/05 Pct Recovery = 106% Analysis Date = 01/27/05 Pct Recovery = 106% Analysis Date = 01/09/05 Pct Recovery = 106% Analysis Date = 01/09/05 Pct Recovery = 106% Analysis Date = 12/23/04 Pct Recovery = 106% Analysis Date = 12/23/04 Pct Recovery = 106% Analysis Date = 12/05/04 Pct Recovery = 106% Analysis Date = 12/05/04 Pct Recovery = 106% Analysis Date = 11/17/04 Pct Recovery = 106% Analysis Date = 11/17/04 Pct Recovery = 106% Analysis Date = 10/31/04 Pct Recovery = 106% Analysis Date = 10/31/04 Pct Recovery = 106% Analysis Date = 10/13/04 Pct Recovery = 106% Analysis Date = 10/13/04 Pct Recovery = 106% Analysis Date = 09/25/04 Pct Recovery = 106% Analysis Date = 09/25/04 Pct Recovery = 106% Analysis Date = 09/08/04 Pct Recovery = 106% Analysis Date = 09/08/04 Pct Recovery = 106% Analysis Date = 08/21/04 Pct Recovery = 106% Analysis Date = 08/21/04 Pct Recovery = 106% Analysis Date = 08/03/04 Pct Recovery = 106% Analysis Date = 08/03/04 Pct Recovery = 106% Analysis Date = 07/17/04 Pct Recovery = 106% Analysis Date = 07/17/04 Pct Recovery = 106% Analysis Date = 06/29/04 Pct Recovery = 106% Analysis Date = 06/29/04 Pct Recovery = 106% Analysis Date = 06/12/04 Pct Recovery = 106% Analysis Date = 06/12/04 Pct Recovery = 106% Analysis Date = 05/25/04 Pct Recovery = 106% Analysis Date = 05/25/04 Pct Recovery = 106% Analysis Date = 05/07/04 Pct Recovery = 107% Analysis Date = 05/07/04 Pct Recovery = 107% Analysis Date = 04/20/04 Pct Recovery = 107% Analysis Date = 04/20/04 Pct Recovery = 107% Analysis Date = 04/02/04 Pct Recovery = 107% Analysis Date = 04/02/04 Pct Recovery = 107% Analysis Date = 03/15/04 Pct Recovery = 107% Analysis Date = 03/15/04 Pct Recovery = 107% Analysis Date = 02/27/04 Pct Recovery = 107% Analysis Date = 02/27/04 Pct Recovery = 107% Analysis Date = 02/09/04 Pct Recovery = 107% Analysis Date = 02/09/04 Pct Recovery = 107% Analysis Date = 01/22/04 Pct Recovery = 107% Analysis Date = 01/22/04 Pct Recovery = 107% Analysis Date = 01/05/04 Pct Recovery = 107% Analysis Date = 01/05/04 Pct Recovery = 107% Analysis Date = 12/18/03 Pct Recovery = 107% Analysis Date = 12/18/03 Pct Recovery = 107% Analysis Date = 11/30/03 Pct Recovery = 107% Analysis Date = 11/30/03 Pct Recovery = 107% Analysis Date = 11/13/03 Pct Recovery = 107% Analysis Date = 11/13/03 Pct Recovery = 107% Analysis Date = 10/26/03 Pct Recovery = 107% Analysis Date = 10/26/03 Pct Recovery = 107% Analysis Date = 10/09/03 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 6 106% 7% 106% 7%
>= Reporting Level 96 106% 14% 105% 12%
Total 102 106% 13% 105% 11%

Sample Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Characteristic N % % Basis
Plotted 102 100% Spiked
Estimated Values 5 5% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 103 .  
False Negatives 0 0% 0 out of 102
Not Spiked 90 .  
False Positives 0 0% 0 out of 90

BQS OBSP Determination:
TERT-PENTYL METHYL ETHER (TAME)
METHOD: 4024 , TESTIDCODE: 50005GCM60
Open Data Set

Analysis Date = 07/22/05 SpikeMix = Supelco LB22063: 25 µl Pct Recovery = 110% Analysis Date = 06/03/05 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 118% Analysis Date = 11/30/04 SpikeMix = Supelco LB22063: 20 µl Pct Recovery = 103% Analysis Date = 09/02/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 126% Analysis Date = 07/25/06 SpikeMix = Ultra CB-1580: 25 µl Pct Recovery = 126% Analysis Date = 03/11/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 111% Analysis Date = 02/01/06 SpikeMix = Ultra CB-1580: 20 µl Pct Recovery = 116% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 101% Analysis Date = 02/04/05 SpikeMix = Supelco LB22063: 10 µl Pct Recovery = 101% Analysis Date = 09/10/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 110% Analysis Date = 05/05/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 100% Analysis Date = 03/03/05 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 95% Analysis Date = 12/31/04 SpikeMix = Supelco LB22063: 8 µl & Absolute 071904VOC2: 8 µl Pct Recovery = 100% Analysis Date = 08/31/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 116% Analysis Date = 04/15/05 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 104% Analysis Date = 12/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 105% Analysis Date = 10/15/04 SpikeMix = Supelco LB22063: 8 µl Pct Recovery = 108% Analysis Date = 08/20/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 115% Analysis Date = 06/16/06 SpikeMix = Ultra CB-1580: 10 µl Pct Recovery = 123% Analysis Date = 04/11/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 113% Analysis Date = 02/28/06 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 100% Analysis Date = 11/25/05 SpikeMix = Ultra CB-1580: 8 µl Pct Recovery = 111% Analysis Date = 05/04/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 111% Analysis Date = 01/12/06 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 113% Analysis Date = 10/29/05 SpikeMix = Ultra CB-1580: 5 µl Pct Recovery = 110% Analysis Date = 09/24/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 101% Analysis Date = 07/02/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 105% Analysis Date = 06/05/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 103% Analysis Date = 04/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 101% Analysis Date = 01/22/04 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 109% Analysis Date = 12/13/03 SpikeMix = Ultra U1734: 10 µl Pct Recovery = 98% Analysis Date = 09/18/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 93% Analysis Date = 08/29/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 91% Analysis Date = 08/02/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 99% Analysis Date = 07/14/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 108% Analysis Date = 06/22/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 99% Analysis Date = 05/31/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 98% Analysis Date = 03/23/07 SpikeMix = Restek A046458: 10 µl Pct Recovery = 108% Analysis Date = 12/29/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 101% Analysis Date = 12/01/06 SpikeMix = Restek A046458: 10 µl Pct Recovery = 110% Analysis Date = 06/30/12 SpikeMix = Accu 212051187: 25 µl Pct Recovery = 80% Analysis Date = 03/26/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 102% Analysis Date = 02/19/13 SpikeMix = ChemService 426000: 20 µl Pct Recovery = 96% Analysis Date = 01/03/13 SpikeMix = Accu 212051187: 20 µl Pct Recovery = 85% Analysis Date = 07/25/09 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 104% Analysis Date = 12/11/08 SpikeMix = Crescent 08HH020: 40 µl Pct Recovery = 109% Analysis Date = 07/01/09 SpikeMix = Accu B8080231: 40 µl Pct Recovery = 105% Analysis Date = 11/27/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 108% Analysis Date = 09/08/12 SpikeMix = ChemService 426000: 10 µl Pct Recovery = 96% Analysis Date = 10/22/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 112% Analysis Date = 07/11/12 SpikeMix = Accu 212051187: 10 µl Pct Recovery = 101% Analysis Date = 07/19/10 SpikeMix = Ultra CF-3592: 40 µl Pct Recovery = 111% Analysis Date = 03/10/12 SpikeMix = Restek A075544: 40 µl Pct Recovery = 98% Analysis Date = 09/13/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 103% Analysis Date = 08/18/11 SpikeMix = Restek A075544: 40 µl Pct Recovery = 102% Analysis Date = 11/15/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 121% Analysis Date = 08/02/11 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 128% Analysis Date = 11/09/10 SpikeMix = NSI 062210-01: 40 µl Pct Recovery = 122% Analysis Date = 08/27/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 103% Analysis Date = 08/17/10 SpikeMix = ERA 0817-09-02VOA: 40 µl Pct Recovery = 100% Analysis Date = 08/28/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 90% Analysis Date = 08/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 07/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 06/10/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 120% Analysis Date = 05/06/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 04/15/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 110% Analysis Date = 03/27/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 03/08/08 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 11/19/07 SpikeMix = ChemService 385-17C: 20 µl Pct Recovery = 100% Analysis Date = 04/07/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 115% Analysis Date = 02/21/09 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 115% Analysis Date = 10/22/08 SpikeMix = Crescent 08HH020: 20 µl Pct Recovery = 104% Analysis Date = 08/25/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 126% Analysis Date = 03/09/09 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 105% Analysis Date = 10/29/08 SpikeMix = Accu B8080231: 20 µl Pct Recovery = 105% Analysis Date = 05/06/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 104% Analysis Date = 03/26/10 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 110% Analysis Date = 10/26/09 SpikeMix = Ultra CF-3592: 20 µl Pct Recovery = 109% Analysis Date = 02/10/12 SpikeMix = Restek A075544: 20 µl Pct Recovery = 105% Analysis Date = 10/15/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 88% Analysis Date = 06/21/11 SpikeMix = Restek A075544: 20 µl Pct Recovery = 82% Analysis Date = 10/09/10 SpikeMix = Restek A075544: 20 µl Pct Recovery = 97% Analysis Date = 06/07/12 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 121% Analysis Date = 08/26/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 125% Analysis Date = 07/19/11 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 125% Analysis Date = 12/10/10 SpikeMix = NSI 062210-01: 20 µl Pct Recovery = 124% Analysis Date = 06/24/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 105% Analysis Date = 04/22/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 96% Analysis Date = 02/09/10 SpikeMix = ERA 0817-09-02VOA: 20 µl Pct Recovery = 104% Analysis Date = 06/07/13 SpikeMix = ChemService 1448500: 10 µl Pct Recovery = 131% Analysis Date = 06/06/13 Pct Recovery = 104% Analysis Date = 05/20/13 Pct Recovery = 104% Analysis Date = 05/20/13 Pct Recovery = 104% Analysis Date = 05/03/13 Pct Recovery = 104% Analysis Date = 05/03/13 Pct Recovery = 104% Analysis Date = 04/16/13 Pct Recovery = 104% Analysis Date = 04/16/13 Pct Recovery = 104% Analysis Date = 03/29/13 Pct Recovery = 104% Analysis Date = 03/29/13 Pct Recovery = 104% Analysis Date = 03/12/13 Pct Recovery = 105% Analysis Date = 03/12/13 Pct Recovery = 105% Analysis Date = 02/23/13 Pct Recovery = 105% Analysis Date = 02/23/13 Pct Recovery = 105% Analysis Date = 02/05/13 Pct Recovery = 105% Analysis Date = 02/05/13 Pct Recovery = 105% Analysis Date = 01/19/13 Pct Recovery = 105% Analysis Date = 01/19/13 Pct Recovery = 105% Analysis Date = 01/02/13 Pct Recovery = 105% Analysis Date = 01/02/13 Pct Recovery = 105% Analysis Date = 12/15/12 Pct Recovery = 105% Analysis Date = 12/15/12 Pct Recovery = 105% Analysis Date = 11/28/12 Pct Recovery = 105% Analysis Date = 11/28/12 Pct Recovery = 105% Analysis Date = 11/11/12 Pct Recovery = 105% Analysis Date = 11/11/12 Pct Recovery = 105% Analysis Date = 10/24/12 Pct Recovery = 105% Analysis Date = 10/24/12 Pct Recovery = 105% Analysis Date = 10/07/12 Pct Recovery = 105% Analysis Date = 10/07/12 Pct Recovery = 105% Analysis Date = 09/20/12 Pct Recovery = 105% Analysis Date = 09/20/12 Pct Recovery = 105% Analysis Date = 09/02/12 Pct Recovery = 105% Analysis Date = 09/02/12 Pct Recovery = 105% Analysis Date = 08/16/12 Pct Recovery = 105% Analysis Date = 08/16/12 Pct Recovery = 105% Analysis Date = 07/30/12 Pct Recovery = 105% Analysis Date = 07/30/12 Pct Recovery = 105% Analysis Date = 07/12/12 Pct Recovery = 105% Analysis Date = 07/12/12 Pct Recovery = 105% Analysis Date = 06/25/12 Pct Recovery = 105% Analysis Date = 06/25/12 Pct Recovery = 105% Analysis Date = 06/08/12 Pct Recovery = 105% Analysis Date = 06/08/12 Pct Recovery = 105% Analysis Date = 05/21/12 Pct Recovery = 105% Analysis Date = 05/21/12 Pct Recovery = 105% Analysis Date = 05/04/12 Pct Recovery = 105% Analysis Date = 05/04/12 Pct Recovery = 105% Analysis Date = 04/17/12 Pct Recovery = 105% Analysis Date = 04/17/12 Pct Recovery = 105% Analysis Date = 03/30/12 Pct Recovery = 106% Analysis Date = 03/30/12 Pct Recovery = 106% Analysis Date = 03/13/12 Pct Recovery = 106% Analysis Date = 03/13/12 Pct Recovery = 106% Analysis Date = 02/25/12 Pct Recovery = 106% Analysis Date = 02/25/12 Pct Recovery = 106% Analysis Date = 02/08/12 Pct Recovery = 106% Analysis Date = 02/08/12 Pct Recovery = 106% Analysis Date = 01/21/12 Pct Recovery = 106% Analysis Date = 01/21/12 Pct Recovery = 106% Analysis Date = 01/04/12 Pct Recovery = 106% Analysis Date = 01/04/12 Pct Recovery = 106% Analysis Date = 12/18/11 Pct Recovery = 106% Analysis Date = 12/18/11 Pct Recovery = 106% Analysis Date = 11/30/11 Pct Recovery = 106% Analysis Date = 11/30/11 Pct Recovery = 106% Analysis Date = 11/13/11 Pct Recovery = 106% Analysis Date = 11/13/11 Pct Recovery = 106% Analysis Date = 10/27/11 Pct Recovery = 106% Analysis Date = 10/27/11 Pct Recovery = 106% Analysis Date = 10/09/11 Pct Recovery = 106% Analysis Date = 10/09/11 Pct Recovery = 106% Analysis Date = 09/22/11 Pct Recovery = 106% Analysis Date = 09/22/11 Pct Recovery = 106% Analysis Date = 09/05/11 Pct Recovery = 106% Analysis Date = 09/05/11 Pct Recovery = 106% Analysis Date = 08/18/11 Pct Recovery = 106% Analysis Date = 08/18/11 Pct Recovery = 106% Analysis Date = 08/01/11 Pct Recovery = 106% Analysis Date = 08/01/11 Pct Recovery = 106% Analysis Date = 07/15/11 Pct Recovery = 106% Analysis Date = 07/15/11 Pct Recovery = 106% Analysis Date = 06/27/11 Pct Recovery = 106% Analysis Date = 06/27/11 Pct Recovery = 106% Analysis Date = 06/10/11 Pct Recovery = 106% Analysis Date = 06/10/11 Pct Recovery = 106% Analysis Date = 05/24/11 Pct Recovery = 106% Analysis Date = 05/24/11 Pct Recovery = 106% Analysis Date = 05/06/11 Pct Recovery = 106% Analysis Date = 05/06/11 Pct Recovery = 106% Analysis Date = 04/19/11 Pct Recovery = 106% Analysis Date = 04/19/11 Pct Recovery = 106% Analysis Date = 04/02/11 Pct Recovery = 106% Analysis Date = 04/02/11 Pct Recovery = 106% Analysis Date = 03/15/11 Pct Recovery = 106% Analysis Date = 03/15/11 Pct Recovery = 106% Analysis Date = 02/26/11 Pct Recovery = 106% Analysis Date = 02/26/11 Pct Recovery = 106% Analysis Date = 02/09/11 Pct Recovery = 107% Analysis Date = 02/09/11 Pct Recovery = 107% Analysis Date = 01/22/11 Pct Recovery = 107% Analysis Date = 01/22/11 Pct Recovery = 107% Analysis Date = 01/05/11 Pct Recovery = 107% Analysis Date = 01/05/11 Pct Recovery = 107% Analysis Date = 12/19/10 Pct Recovery = 107% Analysis Date = 12/19/10 Pct Recovery = 107% Analysis Date = 12/02/10 Pct Recovery = 107% Analysis Date = 12/02/10 Pct Recovery = 107% Analysis Date = 11/14/10 Pct Recovery = 107% Analysis Date = 11/14/10 Pct Recovery = 107% Analysis Date = 10/28/10 Pct Recovery = 107% Analysis Date = 10/28/10 Pct Recovery = 107% Analysis Date = 10/11/10 Pct Recovery = 107% Analysis Date = 10/11/10 Pct Recovery = 107% Analysis Date = 09/23/10 Pct Recovery = 107% Analysis Date = 09/23/10 Pct Recovery = 107% Analysis Date = 09/06/10 Pct Recovery = 107% Analysis Date = 09/06/10 Pct Recovery = 107% Analysis Date = 08/20/10 Pct Recovery = 107% Analysis Date = 08/20/10 Pct Recovery = 107% Analysis Date = 08/02/10 Pct Recovery = 107% Analysis Date = 08/02/10 Pct Recovery = 107% Analysis Date = 07/16/10 Pct Recovery = 107% Analysis Date = 07/16/10 Pct Recovery = 107% Analysis Date = 06/29/10 Pct Recovery = 107% Analysis Date = 06/29/10 Pct Recovery = 107% Analysis Date = 06/11/10 Pct Recovery = 107% Analysis Date = 06/11/10 Pct Recovery = 107% Analysis Date = 05/25/10 Pct Recovery = 107% Analysis Date = 05/25/10 Pct Recovery = 107% Analysis Date = 05/08/10 Pct Recovery = 107% Analysis Date = 05/08/10 Pct Recovery = 107% Analysis Date = 04/20/10 Pct Recovery = 107% Analysis Date = 04/20/10 Pct Recovery = 107% Analysis Date = 04/03/10 Pct Recovery = 107% Analysis Date = 04/03/10 Pct Recovery = 107% Analysis Date = 03/17/10 Pct Recovery = 107% Analysis Date = 03/17/10 Pct Recovery = 107% Analysis Date = 02/27/10 Pct Recovery = 107% Analysis Date = 02/27/10 Pct Recovery = 107% Analysis Date = 02/10/10 Pct Recovery = 107% Analysis Date = 02/10/10 Pct Recovery = 107% Analysis Date = 01/24/10 Pct Recovery = 107% Analysis Date = 01/24/10 Pct Recovery = 107% Analysis Date = 01/06/10 Pct Recovery = 107% Analysis Date = 01/06/10 Pct Recovery = 107% Analysis Date = 12/20/09 Pct Recovery = 107% Analysis Date = 12/20/09 Pct Recovery = 107% Analysis Date = 12/03/09 Pct Recovery = 107% Analysis Date = 12/03/09 Pct Recovery = 107% Analysis Date = 11/15/09 Pct Recovery = 107% Analysis Date = 11/15/09 Pct Recovery = 107% Analysis Date = 10/29/09 Pct Recovery = 107% Analysis Date = 10/29/09 Pct Recovery = 107% Analysis Date = 10/12/09 Pct Recovery = 107% Analysis Date = 10/12/09 Pct Recovery = 107% Analysis Date = 09/25/09 Pct Recovery = 106% Analysis Date = 09/25/09 Pct Recovery = 106% Analysis Date = 09/07/09 Pct Recovery = 106% Analysis Date = 09/07/09 Pct Recovery = 106% Analysis Date = 08/21/09 Pct Recovery = 106% Analysis Date = 08/21/09 Pct Recovery = 106% Analysis Date = 08/04/09 Pct Recovery = 106% Analysis Date = 08/04/09 Pct Recovery = 106% Analysis Date = 07/17/09 Pct Recovery = 106% Analysis Date = 07/17/09 Pct Recovery = 106% Analysis Date = 06/30/09 Pct Recovery = 106% Analysis Date = 06/30/09 Pct Recovery = 106% Analysis Date = 06/13/09 Pct Recovery = 106% Analysis Date = 06/13/09 Pct Recovery = 106% Analysis Date = 05/26/09 Pct Recovery = 106% Analysis Date = 05/26/09 Pct Recovery = 106% Analysis Date = 05/09/09 Pct Recovery = 106% Analysis Date = 05/09/09 Pct Recovery = 106% Analysis Date = 04/22/09 Pct Recovery = 106% Analysis Date = 04/22/09 Pct Recovery = 106% Analysis Date = 04/04/09 Pct Recovery = 106% Analysis Date = 04/04/09 Pct Recovery = 106% Analysis Date = 03/18/09 Pct Recovery = 106% Analysis Date = 03/18/09 Pct Recovery = 106% Analysis Date = 03/01/09 Pct Recovery = 106% Analysis Date = 03/01/09 Pct Recovery = 106% Analysis Date = 02/11/09 Pct Recovery = 106% Analysis Date = 02/11/09 Pct Recovery = 106% Analysis Date = 01/25/09 Pct Recovery = 105% Analysis Date = 01/25/09 Pct Recovery = 105% Analysis Date = 01/08/09 Pct Recovery = 105% Analysis Date = 01/08/09 Pct Recovery = 105% Analysis Date = 12/21/08 Pct Recovery = 105% Analysis Date = 12/21/08 Pct Recovery = 105% Analysis Date = 12/04/08 Pct Recovery = 105% Analysis Date = 12/04/08 Pct Recovery = 105% Analysis Date = 11/17/08 Pct Recovery = 105% Analysis Date = 11/17/08 Pct Recovery = 105% Analysis Date = 10/30/08 Pct Recovery = 105% Analysis Date = 10/30/08 Pct Recovery = 105% Analysis Date = 10/13/08 Pct Recovery = 105% Analysis Date = 10/13/08 Pct Recovery = 105% Analysis Date = 09/26/08 Pct Recovery = 105% Analysis Date = 09/26/08 Pct Recovery = 105% Analysis Date = 09/08/08 Pct Recovery = 105% Analysis Date = 09/08/08 Pct Recovery = 105% Analysis Date = 08/22/08 Pct Recovery = 105% Analysis Date = 08/22/08 Pct Recovery = 105% Analysis Date = 08/05/08 Pct Recovery = 105% Analysis Date = 08/05/08 Pct Recovery = 105% Analysis Date = 07/19/08 Pct Recovery = 105% Analysis Date = 07/19/08 Pct Recovery = 105% Analysis Date = 07/01/08 Pct Recovery = 105% Analysis Date = 07/01/08 Pct Recovery = 105% Analysis Date = 06/14/08 Pct Recovery = 105% Analysis Date = 06/14/08 Pct Recovery = 105% Analysis Date = 05/28/08 Pct Recovery = 105% Analysis Date = 05/28/08 Pct Recovery = 105% Analysis Date = 05/10/08 Pct Recovery = 105% Analysis Date = 05/10/08 Pct Recovery = 105% Analysis Date = 04/23/08 Pct Recovery = 105% Analysis Date = 04/23/08 Pct Recovery = 105% Analysis Date = 04/06/08 Pct Recovery = 105% Analysis Date = 04/06/08 Pct Recovery = 105% Analysis Date = 03/19/08 Pct Recovery = 105% Analysis Date = 03/19/08 Pct Recovery = 105% Analysis Date = 03/02/08 Pct Recovery = 106% Analysis Date = 03/02/08 Pct Recovery = 106% Analysis Date = 02/14/08 Pct Recovery = 106% Analysis Date = 02/14/08 Pct Recovery = 106% Analysis Date = 01/27/08 Pct Recovery = 106% Analysis Date = 01/27/08 Pct Recovery = 106% Analysis Date = 01/10/08 Pct Recovery = 106% Analysis Date = 01/10/08 Pct Recovery = 106% Analysis Date = 12/24/07 Pct Recovery = 106% Analysis Date = 12/24/07 Pct Recovery = 106% Analysis Date = 12/06/07 Pct Recovery = 106% Analysis Date = 12/06/07 Pct Recovery = 106% Analysis Date = 11/19/07 Pct Recovery = 106% Analysis Date = 11/19/07 Pct Recovery = 106% Analysis Date = 11/02/07 Pct Recovery = 106% Analysis Date = 11/02/07 Pct Recovery = 106% Analysis Date = 10/15/07 Pct Recovery = 106% Analysis Date = 10/15/07 Pct Recovery = 106% Analysis Date = 09/28/07 Pct Recovery = 106% Analysis Date = 09/28/07 Pct Recovery = 106% Analysis Date = 09/11/07 Pct Recovery = 106% Analysis Date = 09/11/07 Pct Recovery = 106% Analysis Date = 08/24/07 Pct Recovery = 106% Analysis Date = 08/24/07 Pct Recovery = 106% Analysis Date = 08/07/07 Pct Recovery = 106% Analysis Date = 08/07/07 Pct Recovery = 106% Analysis Date = 07/21/07 Pct Recovery = 106% Analysis Date = 07/21/07 Pct Recovery = 106% Analysis Date = 07/03/07 Pct Recovery = 106% Analysis Date = 07/03/07 Pct Recovery = 106% Analysis Date = 06/16/07 Pct Recovery = 106% Analysis Date = 06/16/07 Pct Recovery = 106% Analysis Date = 05/30/07 Pct Recovery = 107% Analysis Date = 05/30/07 Pct Recovery = 107% Analysis Date = 05/13/07 Pct Recovery = 107% Analysis Date = 05/13/07 Pct Recovery = 107% Analysis Date = 04/25/07 Pct Recovery = 107% Analysis Date = 04/25/07 Pct Recovery = 107% Analysis Date = 04/08/07 Pct Recovery = 107% Analysis Date = 04/08/07 Pct Recovery = 107% Analysis Date = 03/22/07 Pct Recovery = 107% Analysis Date = 03/22/07 Pct Recovery = 107% Analysis Date = 03/04/07 Pct Recovery = 107% Analysis Date = 03/04/07 Pct Recovery = 107% Analysis Date = 02/15/07 Pct Recovery = 107% Analysis Date = 02/15/07 Pct Recovery = 107% Analysis Date = 01/29/07 Pct Recovery = 107% Analysis Date = 01/29/07 Pct Recovery = 107% Analysis Date = 01/11/07 Pct Recovery = 107% Analysis Date = 01/11/07 Pct Recovery = 107% Analysis Date = 12/25/06 Pct Recovery = 107% Analysis Date = 12/25/06 Pct Recovery = 107% Analysis Date = 12/08/06 Pct Recovery = 107% Analysis Date = 12/08/06 Pct Recovery = 107% Analysis Date = 11/20/06 Pct Recovery = 107% Analysis Date = 11/20/06 Pct Recovery = 107% Analysis Date = 11/03/06 Pct Recovery = 107% Analysis Date = 11/03/06 Pct Recovery = 107% Analysis Date = 10/17/06 Pct Recovery = 107% Analysis Date = 10/17/06 Pct Recovery = 107% Analysis Date = 09/29/06 Pct Recovery = 107% Analysis Date = 09/29/06 Pct Recovery = 107% Analysis Date = 09/12/06 Pct Recovery = 107% Analysis Date = 09/12/06 Pct Recovery = 107% Analysis Date = 08/26/06 Pct Recovery = 107% Analysis Date = 08/26/06 Pct Recovery = 107% Analysis Date = 08/08/06 Pct Recovery = 107% Analysis Date = 08/08/06 Pct Recovery = 107% Analysis Date = 07/22/06 Pct Recovery = 107% Analysis Date = 07/22/06 Pct Recovery = 107% Analysis Date = 07/05/06 Pct Recovery = 107% Analysis Date = 07/05/06 Pct Recovery = 107% Analysis Date = 06/17/06 Pct Recovery = 107% Analysis Date = 06/17/06 Pct Recovery = 107% Analysis Date = 05/31/06 Pct Recovery = 107% Analysis Date = 05/31/06 Pct Recovery = 107% Analysis Date = 05/14/06 Pct Recovery = 107% Analysis Date = 05/14/06 Pct Recovery = 107% Analysis Date = 04/26/06 Pct Recovery = 107% Analysis Date = 04/26/06 Pct Recovery = 107% Analysis Date = 04/09/06 Pct Recovery = 107% Analysis Date = 04/09/06 Pct Recovery = 107% Analysis Date = 03/23/06 Pct Recovery = 107% Analysis Date = 03/23/06 Pct Recovery = 107% Analysis Date = 03/06/06 Pct Recovery = 107% Analysis Date = 03/06/06 Pct Recovery = 107% Analysis Date = 02/16/06 Pct Recovery = 107% Analysis Date = 02/16/06 Pct Recovery = 107% Analysis Date = 01/30/06 Pct Recovery = 107% Analysis Date = 01/30/06 Pct Recovery = 107% Analysis Date = 01/13/06 Pct Recovery = 107% Analysis Date = 01/13/06 Pct Recovery = 107% Analysis Date = 12/26/05 Pct Recovery = 107% Analysis Date = 12/26/05 Pct Recovery = 107% Analysis Date = 12/09/05 Pct Recovery = 107% Analysis Date = 12/09/05 Pct Recovery = 107% Analysis Date = 11/22/05 Pct Recovery = 107% Analysis Date = 11/22/05 Pct Recovery = 107% Analysis Date = 11/04/05 Pct Recovery = 107% Analysis Date = 11/04/05 Pct Recovery = 107% Analysis Date = 10/18/05 Pct Recovery = 107% Analysis Date = 10/18/05 Pct Recovery = 107% Analysis Date = 10/01/05 Pct Recovery = 107% Analysis Date = 10/01/05 Pct Recovery = 107% Analysis Date = 09/13/05 Pct Recovery = 107% Analysis Date = 09/13/05 Pct Recovery = 107% Analysis Date = 08/27/05 Pct Recovery = 107% Analysis Date = 08/27/05 Pct Recovery = 107% Analysis Date = 08/10/05 Pct Recovery = 107% Analysis Date = 08/10/05 Pct Recovery = 107% Analysis Date = 07/23/05 Pct Recovery = 107% Analysis Date = 07/23/05 Pct Recovery = 107% Analysis Date = 07/06/05 Pct Recovery = 107% Analysis Date = 07/06/05 Pct Recovery = 107% Analysis Date = 06/19/05 Pct Recovery = 107% Analysis Date = 06/19/05 Pct Recovery = 107% Analysis Date = 06/01/05 Pct Recovery = 107% Analysis Date = 06/01/05 Pct Recovery = 107% Analysis Date = 05/15/05 Pct Recovery = 107% Analysis Date = 05/15/05 Pct Recovery = 107% Analysis Date = 04/28/05 Pct Recovery = 106% Analysis Date = 04/28/05 Pct Recovery = 106% Analysis Date = 04/10/05 Pct Recovery = 106% Analysis Date = 04/10/05 Pct Recovery = 106% Analysis Date = 03/24/05 Pct Recovery = 106% Analysis Date = 03/24/05 Pct Recovery = 106% Analysis Date = 03/07/05 Pct Recovery = 106% Analysis Date = 03/07/05 Pct Recovery = 106% Analysis Date = 02/17/05 Pct Recovery = 106% Analysis Date = 02/17/05 Pct Recovery = 106% Analysis Date = 01/31/05 Pct Recovery = 106% Analysis Date = 01/31/05 Pct Recovery = 106% Analysis Date = 01/14/05 Pct Recovery = 106% Analysis Date = 01/14/05 Pct Recovery = 106% Analysis Date = 12/28/04 Pct Recovery = 106% Analysis Date = 12/28/04 Pct Recovery = 106% Analysis Date = 12/10/04 Pct Recovery = 106% Analysis Date = 12/10/04 Pct Recovery = 106% Analysis Date = 11/23/04 Pct Recovery = 106% Analysis Date = 11/23/04 Pct Recovery = 106% Analysis Date = 11/06/04 Pct Recovery = 106% Analysis Date = 11/06/04 Pct Recovery = 106% Analysis Date = 10/19/04 Pct Recovery = 106% Analysis Date = 10/19/04 Pct Recovery = 106% Analysis Date = 10/02/04 Pct Recovery = 106% Analysis Date = 10/02/04 Pct Recovery = 106% Analysis Date = 09/15/04 Pct Recovery = 105% Analysis Date = 09/15/04 Pct Recovery = 105% Analysis Date = 08/28/04 Pct Recovery = 105% Analysis Date = 08/28/04 Pct Recovery = 105% Analysis Date = 08/11/04 Pct Recovery = 105% Analysis Date = 08/11/04 Pct Recovery = 105% Analysis Date = 07/25/04 Pct Recovery = 105% Analysis Date = 07/25/04 Pct Recovery = 105% Analysis Date = 07/07/04 Pct Recovery = 105% Analysis Date = 07/07/04 Pct Recovery = 105% Analysis Date = 06/20/04 Pct Recovery = 105% Analysis Date = 06/20/04 Pct Recovery = 105% Analysis Date = 06/03/04 Pct Recovery = 105% Analysis Date = 06/03/04 Pct Recovery = 105% Analysis Date = 05/16/04 Pct Recovery = 105% Analysis Date = 05/16/04 Pct Recovery = 105% Analysis Date = 04/29/04 Pct Recovery = 105% Analysis Date = 04/29/04 Pct Recovery = 105% Analysis Date = 04/12/04 Pct Recovery = 104% Analysis Date = 04/12/04 Pct Recovery = 104% Analysis Date = 03/25/04 Pct Recovery = 104% Analysis Date = 03/25/04 Pct Recovery = 104% Analysis Date = 03/08/04 Pct Recovery = 104% Analysis Date = 03/08/04 Pct Recovery = 104% Analysis Date = 02/20/04 Pct Recovery = 104% Analysis Date = 02/20/04 Pct Recovery = 104% Analysis Date = 02/02/04 Pct Recovery = 104% Analysis Date = 02/02/04 Pct Recovery = 104% Analysis Date = 01/16/04 Pct Recovery = 104% Analysis Date = 01/16/04 Pct Recovery = 104% Analysis Date = 12/30/03 Pct Recovery = 104% Analysis Date = 12/30/03 Pct Recovery = 104% Analysis Date = 12/13/03 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERT-PENTYL METHYL ETHER (TAME)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 90 106% 10% 105% 8%
Total 90 106% 10% 105% 8%

Sample Statistics
TERT-PENTYL METHYL ETHER (TAME)

Characteristic N % % Basis
Plotted 90 100% Spiked
Estimated Values 7 8% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 91 .  
False Negatives 0 0% 0 out of 90
Not Spiked 102 .  
False Positives 0 0% 0 out of 102