OBSP Determination:
1H-1,2,4-TRIAZOLE
METHOD: 2447 , TESTIDCODE: 68498LCM60

Laboratory ID = 20202590106 Lab Value = 199.360 Expected Conc. = 276 Report level label = 22 Pct Recovery = 72% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 214.044 Expected Conc. = 276 Report level label = 22 Pct Recovery = 78% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202110006 Lab Value = 243.640 Expected Conc. = 274.6 Report level label = 22 Pct Recovery = 89% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20221940195 Lab Value = 130.091 Expected Conc. = 222.88 Report level label = 22 Pct Recovery = 58% Analysis Date = 07/23/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20222640086 Lab Value = 138.704 Expected Conc. = 218 Report level label = 22 Pct Recovery = 64% Analysis Date = 09/29/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20203230018 Lab Value = 83.235 Expected Conc. = 138 Report level label = 22 Pct Recovery = 60% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 82.109 Expected Conc. = 138 Report level label = 22 Pct Recovery = 59% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 116.933 Expected Conc. = 138 Report level label = 22 Pct Recovery = 85% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221870197 Lab Value = 91.447 Expected Conc. = 137.5 Report level label = 22 Pct Recovery = 67% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20221730293 Lab Value = 96.953 Expected Conc. = 137.5 Report level label = 22 Pct Recovery = 71% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20201680155 Lab Value = 134.626 Expected Conc. = 137.3 Report level label = 22 Pct Recovery = 98% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20210970035 Lab Value = 56.450 Expected Conc. = 55.2 Report level label = 22 Pct Recovery = 102% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 38.106 Expected Conc. = 55.2 Report level label = 22 Pct Recovery = 69% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 47.740 Expected Conc. = 55.2 Report level label = 22 Pct Recovery = 86% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 49.751 Expected Conc. = 55.2 Report level label = 22 Pct Recovery = 90% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 45.679 Expected Conc. = 55.2 Report level label = 22 Pct Recovery = 83% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 47.756 Expected Conc. = 55.2 Report level label = 22 Pct Recovery = 87% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222500483 Lab Value = 32.718 Expected Conc. = 55 Report level label = 22 Pct Recovery = 59% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Laboratory ID = 20201610160 Lab Value = 53.087 Expected Conc. = 54.92 Report level label = 22 Pct Recovery = 97% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Analysis Date = 09/28/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 62% Analysis Date = 09/20/22 Pct Recovery = 62% Analysis Date = 09/16/22 Pct Recovery = 62% Analysis Date = 09/16/22 Pct Recovery = 62% Analysis Date = 09/12/22 Pct Recovery = 62% Analysis Date = 09/12/22 Pct Recovery = 62% Analysis Date = 09/08/22 Pct Recovery = 62% Analysis Date = 09/08/22 Pct Recovery = 62% Analysis Date = 09/03/22 Pct Recovery = 62% Analysis Date = 09/03/22 Pct Recovery = 62% Analysis Date = 08/30/22 Pct Recovery = 63% Analysis Date = 08/30/22 Pct Recovery = 63% Analysis Date = 08/26/22 Pct Recovery = 63% Analysis Date = 08/26/22 Pct Recovery = 63% Analysis Date = 08/22/22 Pct Recovery = 63% Analysis Date = 08/22/22 Pct Recovery = 63% Analysis Date = 08/18/22 Pct Recovery = 63% Analysis Date = 08/18/22 Pct Recovery = 63% Analysis Date = 08/14/22 Pct Recovery = 64% Analysis Date = 08/14/22 Pct Recovery = 64% Analysis Date = 08/09/22 Pct Recovery = 64% Analysis Date = 08/09/22 Pct Recovery = 64% Analysis Date = 08/05/22 Pct Recovery = 64% Analysis Date = 08/05/22 Pct Recovery = 64% Analysis Date = 08/01/22 Pct Recovery = 64% Analysis Date = 08/01/22 Pct Recovery = 64% Analysis Date = 07/28/22 Pct Recovery = 64% Analysis Date = 07/28/22 Pct Recovery = 64% Analysis Date = 07/24/22 Pct Recovery = 65% Analysis Date = 07/24/22 Pct Recovery = 65% Analysis Date = 07/20/22 Pct Recovery = 65% Analysis Date = 07/20/22 Pct Recovery = 65% Analysis Date = 07/15/22 Pct Recovery = 65% Analysis Date = 07/15/22 Pct Recovery = 65% Analysis Date = 07/11/22 Pct Recovery = 65% Analysis Date = 07/11/22 Pct Recovery = 65% Analysis Date = 07/07/22 Pct Recovery = 65% Analysis Date = 07/07/22 Pct Recovery = 65% Analysis Date = 07/03/22 Pct Recovery = 66% Analysis Date = 07/03/22 Pct Recovery = 66% Analysis Date = 06/29/22 Pct Recovery = 66% Analysis Date = 06/29/22 Pct Recovery = 66% Analysis Date = 06/25/22 Pct Recovery = 66% Analysis Date = 06/25/22 Pct Recovery = 66% Analysis Date = 06/20/22 Pct Recovery = 66% Analysis Date = 06/20/22 Pct Recovery = 66% Analysis Date = 06/16/22 Pct Recovery = 66% Analysis Date = 06/16/22 Pct Recovery = 66% Analysis Date = 06/12/22 Pct Recovery = 66% Analysis Date = 06/12/22 Pct Recovery = 66% Analysis Date = 06/08/22 Pct Recovery = 66% Analysis Date = 06/08/22 Pct Recovery = 66% Analysis Date = 06/04/22 Pct Recovery = 67% Analysis Date = 06/04/22 Pct Recovery = 67% Analysis Date = 05/31/22 Pct Recovery = 67% Analysis Date = 05/31/22 Pct Recovery = 67% Analysis Date = 05/26/22 Pct Recovery = 67% Analysis Date = 05/26/22 Pct Recovery = 67% Analysis Date = 05/22/22 Pct Recovery = 67% Analysis Date = 05/22/22 Pct Recovery = 67% Analysis Date = 05/18/22 Pct Recovery = 67% Analysis Date = 05/18/22 Pct Recovery = 67% Analysis Date = 05/14/22 Pct Recovery = 67% Analysis Date = 05/14/22 Pct Recovery = 67% Analysis Date = 05/10/22 Pct Recovery = 67% Analysis Date = 05/10/22 Pct Recovery = 67% Analysis Date = 05/06/22 Pct Recovery = 67% Analysis Date = 05/06/22 Pct Recovery = 67% Analysis Date = 05/01/22 Pct Recovery = 67% Analysis Date = 05/01/22 Pct Recovery = 67% Analysis Date = 04/27/22 Pct Recovery = 67% Analysis Date = 04/27/22 Pct Recovery = 67% Analysis Date = 04/23/22 Pct Recovery = 68% Analysis Date = 04/23/22 Pct Recovery = 68% Analysis Date = 04/19/22 Pct Recovery = 68% Analysis Date = 04/19/22 Pct Recovery = 68% Analysis Date = 04/15/22 Pct Recovery = 68% Analysis Date = 04/15/22 Pct Recovery = 68% Analysis Date = 04/11/22 Pct Recovery = 68% Analysis Date = 04/11/22 Pct Recovery = 68% Analysis Date = 04/06/22 Pct Recovery = 68% Analysis Date = 04/06/22 Pct Recovery = 68% Analysis Date = 04/02/22 Pct Recovery = 68% Analysis Date = 04/02/22 Pct Recovery = 68% Analysis Date = 03/29/22 Pct Recovery = 68% Analysis Date = 03/29/22 Pct Recovery = 68% Analysis Date = 03/25/22 Pct Recovery = 68% Analysis Date = 03/25/22 Pct Recovery = 68% Analysis Date = 03/21/22 Pct Recovery = 68% Analysis Date = 03/21/22 Pct Recovery = 68% Analysis Date = 03/17/22 Pct Recovery = 69% Analysis Date = 03/17/22 Pct Recovery = 69% Analysis Date = 03/12/22 Pct Recovery = 69% Analysis Date = 03/12/22 Pct Recovery = 69% Analysis Date = 03/08/22 Pct Recovery = 69% Analysis Date = 03/08/22 Pct Recovery = 69% Analysis Date = 03/04/22 Pct Recovery = 69% Analysis Date = 03/04/22 Pct Recovery = 69% Analysis Date = 02/28/22 Pct Recovery = 69% Analysis Date = 02/28/22 Pct Recovery = 69% Analysis Date = 02/24/22 Pct Recovery = 69% Analysis Date = 02/24/22 Pct Recovery = 69% Analysis Date = 02/19/22 Pct Recovery = 69% Analysis Date = 02/19/22 Pct Recovery = 69% Analysis Date = 02/15/22 Pct Recovery = 69% Analysis Date = 02/15/22 Pct Recovery = 69% Analysis Date = 02/11/22 Pct Recovery = 69% Analysis Date = 02/11/22 Pct Recovery = 69% Analysis Date = 02/07/22 Pct Recovery = 69% Analysis Date = 02/07/22 Pct Recovery = 69% Analysis Date = 02/03/22 Pct Recovery = 70% Analysis Date = 02/03/22 Pct Recovery = 70% Analysis Date = 01/30/22 Pct Recovery = 70% Analysis Date = 01/30/22 Pct Recovery = 70% Analysis Date = 01/25/22 Pct Recovery = 70% Analysis Date = 01/25/22 Pct Recovery = 70% Analysis Date = 01/21/22 Pct Recovery = 70% Analysis Date = 01/21/22 Pct Recovery = 70% Analysis Date = 01/17/22 Pct Recovery = 70% Analysis Date = 01/17/22 Pct Recovery = 70% Analysis Date = 01/13/22 Pct Recovery = 70% Analysis Date = 01/13/22 Pct Recovery = 70% Analysis Date = 01/09/22 Pct Recovery = 70% Analysis Date = 01/09/22 Pct Recovery = 70% Analysis Date = 01/05/22 Pct Recovery = 70% Analysis Date = 01/05/22 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 70% Analysis Date = 12/27/21 Pct Recovery = 71% Analysis Date = 12/27/21 Pct Recovery = 71% Analysis Date = 12/23/21 Pct Recovery = 71% Analysis Date = 12/23/21 Pct Recovery = 71% Analysis Date = 12/19/21 Pct Recovery = 71% Analysis Date = 12/19/21 Pct Recovery = 71% Analysis Date = 12/15/21 Pct Recovery = 71% Analysis Date = 12/15/21 Pct Recovery = 71% Analysis Date = 12/11/21 Pct Recovery = 71% Analysis Date = 12/11/21 Pct Recovery = 71% Analysis Date = 12/06/21 Pct Recovery = 71% Analysis Date = 12/06/21 Pct Recovery = 71% Analysis Date = 12/02/21 Pct Recovery = 71% Analysis Date = 12/02/21 Pct Recovery = 71% Analysis Date = 11/28/21 Pct Recovery = 71% Analysis Date = 11/28/21 Pct Recovery = 71% Analysis Date = 11/24/21 Pct Recovery = 71% Analysis Date = 11/24/21 Pct Recovery = 71% Analysis Date = 11/20/21 Pct Recovery = 71% Analysis Date = 11/20/21 Pct Recovery = 71% Analysis Date = 11/16/21 Pct Recovery = 72% Analysis Date = 11/16/21 Pct Recovery = 72% Analysis Date = 11/11/21 Pct Recovery = 72% Analysis Date = 11/11/21 Pct Recovery = 72% Analysis Date = 11/07/21 Pct Recovery = 72% Analysis Date = 11/07/21 Pct Recovery = 72% Analysis Date = 11/03/21 Pct Recovery = 72% Analysis Date = 11/03/21 Pct Recovery = 72% Analysis Date = 10/30/21 Pct Recovery = 72% Analysis Date = 10/30/21 Pct Recovery = 72% Analysis Date = 10/26/21 Pct Recovery = 72% Analysis Date = 10/26/21 Pct Recovery = 72% Analysis Date = 10/22/21 Pct Recovery = 72% Analysis Date = 10/22/21 Pct Recovery = 72% Analysis Date = 10/17/21 Pct Recovery = 72% Analysis Date = 10/17/21 Pct Recovery = 72% Analysis Date = 10/13/21 Pct Recovery = 72% Analysis Date = 10/13/21 Pct Recovery = 72% Analysis Date = 10/09/21 Pct Recovery = 72% Analysis Date = 10/09/21 Pct Recovery = 72% Analysis Date = 10/05/21 Pct Recovery = 73% Analysis Date = 10/05/21 Pct Recovery = 73% Analysis Date = 10/01/21 Pct Recovery = 73% Analysis Date = 10/01/21 Pct Recovery = 73% Analysis Date = 09/27/21 Pct Recovery = 73% Analysis Date = 09/27/21 Pct Recovery = 73% Analysis Date = 09/22/21 Pct Recovery = 73% Analysis Date = 09/22/21 Pct Recovery = 73% Analysis Date = 09/18/21 Pct Recovery = 73% Analysis Date = 09/18/21 Pct Recovery = 73% Analysis Date = 09/14/21 Pct Recovery = 73% Analysis Date = 09/14/21 Pct Recovery = 73% Analysis Date = 09/10/21 Pct Recovery = 73% Analysis Date = 09/10/21 Pct Recovery = 73% Analysis Date = 09/06/21 Pct Recovery = 73% Analysis Date = 09/06/21 Pct Recovery = 73% Analysis Date = 09/02/21 Pct Recovery = 73% Analysis Date = 09/02/21 Pct Recovery = 73% Analysis Date = 08/28/21 Pct Recovery = 74% Analysis Date = 08/28/21 Pct Recovery = 74% Analysis Date = 08/24/21 Pct Recovery = 74% Analysis Date = 08/24/21 Pct Recovery = 74% Analysis Date = 08/20/21 Pct Recovery = 74% Analysis Date = 08/20/21 Pct Recovery = 74% Analysis Date = 08/16/21 Pct Recovery = 74% Analysis Date = 08/16/21 Pct Recovery = 74% Analysis Date = 08/12/21 Pct Recovery = 74% Analysis Date = 08/12/21 Pct Recovery = 74% Analysis Date = 08/07/21 Pct Recovery = 74% Analysis Date = 08/07/21 Pct Recovery = 74% Analysis Date = 08/03/21 Pct Recovery = 74% Analysis Date = 08/03/21 Pct Recovery = 74% Analysis Date = 07/30/21 Pct Recovery = 74% Analysis Date = 07/30/21 Pct Recovery = 74% Analysis Date = 07/26/21 Pct Recovery = 74% Analysis Date = 07/26/21 Pct Recovery = 74% Analysis Date = 07/22/21 Pct Recovery = 74% Analysis Date = 07/22/21 Pct Recovery = 74% Analysis Date = 07/18/21 Pct Recovery = 75% Analysis Date = 07/18/21 Pct Recovery = 75% Analysis Date = 07/13/21 Pct Recovery = 75% Analysis Date = 07/13/21 Pct Recovery = 75% Analysis Date = 07/09/21 Pct Recovery = 75% Analysis Date = 07/09/21 Pct Recovery = 75% Analysis Date = 07/05/21 Pct Recovery = 75% Analysis Date = 07/05/21 Pct Recovery = 75% Analysis Date = 07/01/21 Pct Recovery = 75% Analysis Date = 07/01/21 Pct Recovery = 75% Analysis Date = 06/27/21 Pct Recovery = 75% Analysis Date = 06/27/21 Pct Recovery = 75% Analysis Date = 06/23/21 Pct Recovery = 75% Analysis Date = 06/23/21 Pct Recovery = 75% Analysis Date = 06/18/21 Pct Recovery = 75% Analysis Date = 06/18/21 Pct Recovery = 75% Analysis Date = 06/14/21 Pct Recovery = 75% Analysis Date = 06/14/21 Pct Recovery = 75% Analysis Date = 06/10/21 Pct Recovery = 75% Analysis Date = 06/10/21 Pct Recovery = 75% Analysis Date = 06/06/21 Pct Recovery = 76% Analysis Date = 06/06/21 Pct Recovery = 76% Analysis Date = 06/02/21 Pct Recovery = 76% Analysis Date = 06/02/21 Pct Recovery = 76% Analysis Date = 05/29/21 Pct Recovery = 76% Analysis Date = 05/29/21 Pct Recovery = 76% Analysis Date = 05/24/21 Pct Recovery = 76% Analysis Date = 05/24/21 Pct Recovery = 76% Analysis Date = 05/20/21 Pct Recovery = 76% Analysis Date = 05/20/21 Pct Recovery = 76% Analysis Date = 05/16/21 Pct Recovery = 76% Analysis Date = 05/16/21 Pct Recovery = 76% Analysis Date = 05/12/21 Pct Recovery = 76% Analysis Date = 05/12/21 Pct Recovery = 76% Analysis Date = 05/08/21 Pct Recovery = 76% Analysis Date = 05/08/21 Pct Recovery = 76% Analysis Date = 05/04/21 Pct Recovery = 76% Analysis Date = 05/04/21 Pct Recovery = 76% Analysis Date = 04/29/21 Pct Recovery = 77% Analysis Date = 04/29/21 Pct Recovery = 77% Analysis Date = 04/25/21 Pct Recovery = 77% Analysis Date = 04/25/21 Pct Recovery = 77% Analysis Date = 04/21/21 Pct Recovery = 77% Analysis Date = 04/21/21 Pct Recovery = 77% Analysis Date = 04/17/21 Pct Recovery = 77% Analysis Date = 04/17/21 Pct Recovery = 77% Analysis Date = 04/13/21 Pct Recovery = 77% Analysis Date = 04/13/21 Pct Recovery = 77% Analysis Date = 04/09/21 Pct Recovery = 77% Analysis Date = 04/09/21 Pct Recovery = 77% Analysis Date = 04/04/21 Pct Recovery = 77% Analysis Date = 04/04/21 Pct Recovery = 77% Analysis Date = 03/31/21 Pct Recovery = 77% Analysis Date = 03/31/21 Pct Recovery = 77% Analysis Date = 03/27/21 Pct Recovery = 77% Analysis Date = 03/27/21 Pct Recovery = 77% Analysis Date = 03/23/21 Pct Recovery = 77% Analysis Date = 03/23/21 Pct Recovery = 77% Analysis Date = 03/19/21 Pct Recovery = 78% Analysis Date = 03/19/21 Pct Recovery = 78% Analysis Date = 03/15/21 Pct Recovery = 78% Analysis Date = 03/15/21 Pct Recovery = 78% Analysis Date = 03/10/21 Pct Recovery = 78% Analysis Date = 03/10/21 Pct Recovery = 78% Analysis Date = 03/06/21 Pct Recovery = 78% Analysis Date = 03/06/21 Pct Recovery = 78% Analysis Date = 03/02/21 Pct Recovery = 78% Analysis Date = 03/02/21 Pct Recovery = 78% Analysis Date = 02/26/21 Pct Recovery = 78% Analysis Date = 02/26/21 Pct Recovery = 78% Analysis Date = 02/22/21 Pct Recovery = 78% Analysis Date = 02/22/21 Pct Recovery = 78% Analysis Date = 02/18/21 Pct Recovery = 78% Analysis Date = 02/18/21 Pct Recovery = 78% Analysis Date = 02/13/21 Pct Recovery = 78% Analysis Date = 02/13/21 Pct Recovery = 78% Analysis Date = 02/09/21 Pct Recovery = 78% Analysis Date = 02/09/21 Pct Recovery = 78% Analysis Date = 02/05/21 Pct Recovery = 78% Analysis Date = 02/05/21 Pct Recovery = 78% Analysis Date = 02/01/21 Pct Recovery = 77% Analysis Date = 02/01/21 Pct Recovery = 77% Analysis Date = 01/28/21 Pct Recovery = 76% Analysis Date = 01/28/21 Pct Recovery = 76% Analysis Date = 01/24/21 Pct Recovery = 76% Analysis Date = 01/24/21 Pct Recovery = 76% Analysis Date = 01/19/21 Pct Recovery = 76% Analysis Date = 01/19/21 Pct Recovery = 76% Analysis Date = 01/15/21 Pct Recovery = 76% Analysis Date = 01/15/21 Pct Recovery = 76% Analysis Date = 01/11/21 Pct Recovery = 76% Analysis Date = 01/11/21 Pct Recovery = 76% Analysis Date = 01/07/21 Pct Recovery = 76% Analysis Date = 01/07/21 Pct Recovery = 76% Analysis Date = 01/03/21 Pct Recovery = 76% Analysis Date = 01/03/21 Pct Recovery = 76% Analysis Date = 12/29/20 Pct Recovery = 76% Analysis Date = 12/29/20 Pct Recovery = 76% Analysis Date = 12/25/20 Pct Recovery = 75% Analysis Date = 12/25/20 Pct Recovery = 75% Analysis Date = 12/21/20 Pct Recovery = 75% Analysis Date = 12/21/20 Pct Recovery = 75% Analysis Date = 12/17/20 Pct Recovery = 75% Analysis Date = 12/17/20 Pct Recovery = 75% Analysis Date = 12/13/20 Pct Recovery = 75% Analysis Date = 12/13/20 Pct Recovery = 75% Analysis Date = 12/09/20 Pct Recovery = 76% Analysis Date = 12/09/20 Pct Recovery = 76% Analysis Date = 12/04/20 Pct Recovery = 77% Analysis Date = 12/04/20 Pct Recovery = 77% Analysis Date = 11/30/20 Pct Recovery = 77% Analysis Date = 11/30/20 Pct Recovery = 77% Analysis Date = 11/26/20 Pct Recovery = 78% Analysis Date = 11/26/20 Pct Recovery = 78% Analysis Date = 11/22/20 Pct Recovery = 78% Analysis Date = 11/22/20 Pct Recovery = 78% Analysis Date = 11/18/20 Pct Recovery = 79% Analysis Date = 11/18/20 Pct Recovery = 79% Analysis Date = 11/14/20 Pct Recovery = 79% Analysis Date = 11/14/20 Pct Recovery = 79% Analysis Date = 11/09/20 Pct Recovery = 80% Analysis Date = 11/09/20 Pct Recovery = 80% Analysis Date = 11/05/20 Pct Recovery = 80% Analysis Date = 11/05/20 Pct Recovery = 80% Analysis Date = 11/01/20 Pct Recovery = 81% Analysis Date = 11/01/20 Pct Recovery = 81% Analysis Date = 10/28/20 Pct Recovery = 81% Analysis Date = 10/28/20 Pct Recovery = 81% Analysis Date = 10/24/20 Pct Recovery = 81% Analysis Date = 10/24/20 Pct Recovery = 81% Analysis Date = 10/20/20 Pct Recovery = 81% Analysis Date = 10/20/20 Pct Recovery = 81% Analysis Date = 10/15/20 Pct Recovery = 81% Analysis Date = 10/15/20 Pct Recovery = 81% Analysis Date = 10/11/20 Pct Recovery = 81% Analysis Date = 10/11/20 Pct Recovery = 81% Analysis Date = 10/07/20 Pct Recovery = 81% Analysis Date = 10/07/20 Pct Recovery = 81% Analysis Date = 10/03/20 Pct Recovery = 82% Analysis Date = 10/03/20 Pct Recovery = 82% Analysis Date = 09/29/20 Pct Recovery = 82% Analysis Date = 09/29/20 Pct Recovery = 82% Analysis Date = 09/25/20 Pct Recovery = 82% Analysis Date = 09/25/20 Pct Recovery = 82% Analysis Date = 09/20/20 Pct Recovery = 82% Analysis Date = 09/20/20 Pct Recovery = 82% Analysis Date = 09/16/20 Pct Recovery = 83% Analysis Date = 09/16/20 Pct Recovery = 83% Analysis Date = 09/12/20 Pct Recovery = 83% Analysis Date = 09/12/20 Pct Recovery = 83% Analysis Date = 09/08/20 Pct Recovery = 84% Analysis Date = 09/08/20 Pct Recovery = 84% Analysis Date = 09/04/20 Pct Recovery = 85% Analysis Date = 09/04/20 Pct Recovery = 85% Analysis Date = 08/31/20 Pct Recovery = 85% Analysis Date = 08/31/20 Pct Recovery = 85% Analysis Date = 08/26/20 Pct Recovery = 86% Analysis Date = 08/26/20 Pct Recovery = 86% Analysis Date = 08/22/20 Pct Recovery = 87% Analysis Date = 08/22/20 Pct Recovery = 87% Analysis Date = 08/18/20 Pct Recovery = 87% Analysis Date = 08/18/20 Pct Recovery = 87% Analysis Date = 08/14/20 Pct Recovery = 88% Analysis Date = 08/14/20 Pct Recovery = 88% Analysis Date = 08/10/20 Pct Recovery = 89% Analysis Date = 08/10/20 Pct Recovery = 89% Analysis Date = 08/06/20 Pct Recovery = 89% Analysis Date = 08/06/20 Pct Recovery = 89% Analysis Date = 08/01/20 Pct Recovery = 90% Analysis Date = 08/01/20 Pct Recovery = 90% Analysis Date = 07/28/20 Pct Recovery = 90% Analysis Date = 07/28/20 Pct Recovery = 90% Analysis Date = 07/24/20 Pct Recovery = 91% Analysis Date = 07/24/20 Pct Recovery = 91% Analysis Date = 07/20/20 Pct Recovery = 92% Analysis Date = 07/20/20 Pct Recovery = 92% Analysis Date = 07/16/20 Pct Recovery = 92% Analysis Date = 07/16/20 Pct Recovery = 92% Analysis Date = 07/12/20 Pct Recovery = 93% Analysis Date = 07/12/20 Pct Recovery = 93% Analysis Date = 07/07/20 Pct Recovery = 93% Analysis Date = 07/07/20 Pct Recovery = 93% Analysis Date = 07/03/20 Pct Recovery = 94% Analysis Date = 07/03/20 Pct Recovery = 94% Analysis Date = 06/29/20 Pct Recovery = 94% Analysis Date = 06/29/20 Pct Recovery = 94% Analysis Date = 06/25/20 Pct Recovery = 95% Analysis Date = 06/25/20 Pct Recovery = 95% Analysis Date = 06/21/20 Pct Recovery = 96% Analysis Date = 06/21/20 Pct Recovery = 96% Analysis Date = 06/17/20 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1H-1,2,4-TRIAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 78% 14% 78% 19%
Total 19 78% 14% 78% 19%

Sample Statistics
1H-1,2,4-TRIAZOLE

Characteristic N % % Basis
Plotted 19 86% Spiked
Estimated Values 19 86% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 22 .  
False Negatives 3 14% 3 out of 22
Not Spiked 94 .  
False Positives 0 0% 0 out of 94

OBSP Determination:
2,4-D
METHOD: 2447 , TESTIDCODE: 68500LCM60

Laboratory ID = 20202390020 Lab Value = 1079.339 Expected Conc. = 778.2 Report level label = 62 Pct Recovery = 139% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20201820155 Lab Value = 918.948 Expected Conc. = 776.5 Report level label = 62 Pct Recovery = 118% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 549.817 Expected Conc. = 776.5 Report level label = 62 Pct Recovery = 71% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202590107 Lab Value = 883.259 Expected Conc. = 775.2 Report level label = 62 Pct Recovery = 114% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 1028.609 Expected Conc. = 775.2 Report level label = 62 Pct Recovery = 133% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 734.825 Expected Conc. = 764.1 Report level label = 62 Pct Recovery = 96% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 747.547 Expected Conc. = 764.1 Report level label = 62 Pct Recovery = 98% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20220810134 Lab Value = 505.647 Expected Conc. = 626.4 Report level label = 62 Pct Recovery = 81% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20212990174 Lab Value = 286.724 Expected Conc. = 621.36 Report level label = 62 Pct Recovery = 46% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222150193 Lab Value = 446.257 Expected Conc. = 620 Report level label = 62 Pct Recovery = 72% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20222010132 Lab Value = 466.947 Expected Conc. = 620 Report level label = 62 Pct Recovery = 75% Analysis Date = 07/22/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220190116 Lab Value = 429.728 Expected Conc. = 617.6 Report level label = 62 Pct Recovery = 70% Analysis Date = 02/01/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 484.112 Expected Conc. = 617.6 Report level label = 62 Pct Recovery = 78% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20220810133 Lab Value = 375.066 Expected Conc. = 391.5 Report level label = 62 Pct Recovery = 96% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201960104 Lab Value = 477.761 Expected Conc. = 389.1 Report level label = 62 Pct Recovery = 123% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20213340027 Lab Value = 336.044 Expected Conc. = 388.35 Report level label = 62 Pct Recovery = 87% Analysis Date = 12/04/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 775.333 Expected Conc. = 388.35 Report level label = 62 Pct Recovery = 200% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 243.851 Expected Conc. = 388.35 Report level label = 62 Pct Recovery = 63% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202530029 Lab Value = 445.763 Expected Conc. = 388.25 Report level label = 62 Pct Recovery = 115% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 355.666 Expected Conc. = 388.25 Report level label = 62 Pct Recovery = 92% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 297.429 Expected Conc. = 388.25 Report level label = 62 Pct Recovery = 77% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20203360042 Lab Value = 450.758 Expected Conc. = 387.6 Report level label = 62 Pct Recovery = 116% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 494.504 Expected Conc. = 387.6 Report level label = 62 Pct Recovery = 128% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 503.662 Expected Conc. = 387.6 Report level label = 62 Pct Recovery = 130% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221730293 Lab Value = 251.305 Expected Conc. = 386 Report level label = 62 Pct Recovery = 65% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 300.949 Expected Conc. = 386 Report level label = 62 Pct Recovery = 78% Analysis Date = 02/02/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20222630205 Lab Value = 117.358 Expected Conc. = 156.6 Report level label = 62 Pct Recovery = 75% Analysis Date = 09/30/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20201610160 Lab Value = 109.606 Expected Conc. = 155.64 Report level label = 62 Pct Recovery = 70% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20213060210 Lab Value = 95.149 Expected Conc. = 155.34 Report level label = 62 Pct Recovery = 61% Analysis Date = 11/09/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20202180001 Lab Value = 149.392 Expected Conc. = 155.3 Report level label = 62 Pct Recovery = 96% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 191.152 Expected Conc. = 155.3 Report level label = 62 Pct Recovery = 123% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 169.969 Expected Conc. = 155.3 Report level label = 62 Pct Recovery = 109% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210970035 Lab Value = 178.622 Expected Conc. = 155.04 Report level label = 62 Pct Recovery = 115% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 167.552 Expected Conc. = 155.04 Report level label = 62 Pct Recovery = 108% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 114.094 Expected Conc. = 155.04 Report level label = 62 Pct Recovery = 74% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 148.795 Expected Conc. = 155.04 Report level label = 62 Pct Recovery = 96% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222500483 Lab Value = 133.051 Expected Conc. = 154.4 Report level label = 62 Pct Recovery = 86% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 98.430 Expected Conc. = 154.4 Report level label = 62 Pct Recovery = 64% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210830019 Lab Value = 97.569 Expected Conc. = 152.82 Report level label = 62 Pct Recovery = 64% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 10/13/22 Pct Recovery = 75% Analysis Date = 10/09/22 Pct Recovery = 75% Analysis Date = 10/09/22 Pct Recovery = 75% Analysis Date = 10/05/22 Pct Recovery = 75% Analysis Date = 10/05/22 Pct Recovery = 75% Analysis Date = 09/30/22 Pct Recovery = 75% Analysis Date = 09/30/22 Pct Recovery = 75% Analysis Date = 09/26/22 Pct Recovery = 76% Analysis Date = 09/26/22 Pct Recovery = 76% Analysis Date = 09/22/22 Pct Recovery = 76% Analysis Date = 09/22/22 Pct Recovery = 76% Analysis Date = 09/17/22 Pct Recovery = 76% Analysis Date = 09/17/22 Pct Recovery = 76% Analysis Date = 09/13/22 Pct Recovery = 76% Analysis Date = 09/13/22 Pct Recovery = 76% Analysis Date = 09/08/22 Pct Recovery = 76% Analysis Date = 09/08/22 Pct Recovery = 76% Analysis Date = 09/04/22 Pct Recovery = 76% Analysis Date = 09/04/22 Pct Recovery = 76% Analysis Date = 08/31/22 Pct Recovery = 76% Analysis Date = 08/31/22 Pct Recovery = 76% Analysis Date = 08/26/22 Pct Recovery = 76% Analysis Date = 08/26/22 Pct Recovery = 76% Analysis Date = 08/22/22 Pct Recovery = 77% Analysis Date = 08/22/22 Pct Recovery = 77% Analysis Date = 08/17/22 Pct Recovery = 77% Analysis Date = 08/17/22 Pct Recovery = 77% Analysis Date = 08/13/22 Pct Recovery = 77% Analysis Date = 08/13/22 Pct Recovery = 77% Analysis Date = 08/09/22 Pct Recovery = 77% Analysis Date = 08/09/22 Pct Recovery = 77% Analysis Date = 08/04/22 Pct Recovery = 77% Analysis Date = 08/04/22 Pct Recovery = 77% Analysis Date = 07/31/22 Pct Recovery = 77% Analysis Date = 07/31/22 Pct Recovery = 77% Analysis Date = 07/27/22 Pct Recovery = 77% Analysis Date = 07/27/22 Pct Recovery = 77% Analysis Date = 07/22/22 Pct Recovery = 77% Analysis Date = 07/22/22 Pct Recovery = 77% Analysis Date = 07/18/22 Pct Recovery = 78% Analysis Date = 07/18/22 Pct Recovery = 78% Analysis Date = 07/13/22 Pct Recovery = 78% Analysis Date = 07/13/22 Pct Recovery = 78% Analysis Date = 07/09/22 Pct Recovery = 78% Analysis Date = 07/09/22 Pct Recovery = 78% Analysis Date = 07/05/22 Pct Recovery = 78% Analysis Date = 07/05/22 Pct Recovery = 78% Analysis Date = 06/30/22 Pct Recovery = 78% Analysis Date = 06/30/22 Pct Recovery = 78% Analysis Date = 06/26/22 Pct Recovery = 78% Analysis Date = 06/26/22 Pct Recovery = 78% Analysis Date = 06/21/22 Pct Recovery = 78% Analysis Date = 06/21/22 Pct Recovery = 78% Analysis Date = 06/17/22 Pct Recovery = 78% Analysis Date = 06/17/22 Pct Recovery = 78% Analysis Date = 06/13/22 Pct Recovery = 78% Analysis Date = 06/13/22 Pct Recovery = 78% Analysis Date = 06/08/22 Pct Recovery = 79% Analysis Date = 06/08/22 Pct Recovery = 79% Analysis Date = 06/04/22 Pct Recovery = 79% Analysis Date = 06/04/22 Pct Recovery = 79% Analysis Date = 05/31/22 Pct Recovery = 79% Analysis Date = 05/31/22 Pct Recovery = 79% Analysis Date = 05/26/22 Pct Recovery = 79% Analysis Date = 05/26/22 Pct Recovery = 79% Analysis Date = 05/22/22 Pct Recovery = 79% Analysis Date = 05/22/22 Pct Recovery = 79% Analysis Date = 05/17/22 Pct Recovery = 79% Analysis Date = 05/17/22 Pct Recovery = 79% Analysis Date = 05/13/22 Pct Recovery = 79% Analysis Date = 05/13/22 Pct Recovery = 79% Analysis Date = 05/09/22 Pct Recovery = 79% Analysis Date = 05/09/22 Pct Recovery = 79% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/25/22 Pct Recovery = 80% Analysis Date = 04/25/22 Pct Recovery = 80% Analysis Date = 04/21/22 Pct Recovery = 80% Analysis Date = 04/21/22 Pct Recovery = 80% Analysis Date = 04/17/22 Pct Recovery = 80% Analysis Date = 04/17/22 Pct Recovery = 80% Analysis Date = 04/12/22 Pct Recovery = 80% Analysis Date = 04/12/22 Pct Recovery = 80% Analysis Date = 04/08/22 Pct Recovery = 80% Analysis Date = 04/08/22 Pct Recovery = 80% Analysis Date = 04/04/22 Pct Recovery = 80% Analysis Date = 04/04/22 Pct Recovery = 80% Analysis Date = 03/30/22 Pct Recovery = 81% Analysis Date = 03/30/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/21/22 Pct Recovery = 81% Analysis Date = 03/21/22 Pct Recovery = 81% Analysis Date = 03/17/22 Pct Recovery = 81% Analysis Date = 03/17/22 Pct Recovery = 81% Analysis Date = 03/13/22 Pct Recovery = 81% Analysis Date = 03/13/22 Pct Recovery = 81% Analysis Date = 03/08/22 Pct Recovery = 81% Analysis Date = 03/08/22 Pct Recovery = 81% Analysis Date = 03/04/22 Pct Recovery = 81% Analysis Date = 03/04/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/23/22 Pct Recovery = 82% Analysis Date = 02/23/22 Pct Recovery = 82% Analysis Date = 02/19/22 Pct Recovery = 82% Analysis Date = 02/19/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/01/22 Pct Recovery = 82% Analysis Date = 02/01/22 Pct Recovery = 82% Analysis Date = 01/28/22 Pct Recovery = 82% Analysis Date = 01/28/22 Pct Recovery = 82% Analysis Date = 01/23/22 Pct Recovery = 82% Analysis Date = 01/23/22 Pct Recovery = 82% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 83% Analysis Date = 01/01/22 Pct Recovery = 83% Analysis Date = 01/01/22 Pct Recovery = 83% Analysis Date = 12/28/21 Pct Recovery = 83% Analysis Date = 12/28/21 Pct Recovery = 83% Analysis Date = 12/24/21 Pct Recovery = 83% Analysis Date = 12/24/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 84% Analysis Date = 12/19/21 Pct Recovery = 84% Analysis Date = 12/15/21 Pct Recovery = 84% Analysis Date = 12/15/21 Pct Recovery = 84% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/06/21 Pct Recovery = 84% Analysis Date = 12/06/21 Pct Recovery = 84% Analysis Date = 12/02/21 Pct Recovery = 84% Analysis Date = 12/02/21 Pct Recovery = 84% Analysis Date = 11/27/21 Pct Recovery = 84% Analysis Date = 11/27/21 Pct Recovery = 84% Analysis Date = 11/23/21 Pct Recovery = 84% Analysis Date = 11/23/21 Pct Recovery = 84% Analysis Date = 11/19/21 Pct Recovery = 85% Analysis Date = 11/19/21 Pct Recovery = 85% Analysis Date = 11/14/21 Pct Recovery = 85% Analysis Date = 11/14/21 Pct Recovery = 85% Analysis Date = 11/10/21 Pct Recovery = 85% Analysis Date = 11/10/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/23/21 Pct Recovery = 85% Analysis Date = 10/23/21 Pct Recovery = 85% Analysis Date = 10/19/21 Pct Recovery = 85% Analysis Date = 10/19/21 Pct Recovery = 85% Analysis Date = 10/15/21 Pct Recovery = 86% Analysis Date = 10/15/21 Pct Recovery = 86% Analysis Date = 10/10/21 Pct Recovery = 86% Analysis Date = 10/10/21 Pct Recovery = 86% Analysis Date = 10/06/21 Pct Recovery = 86% Analysis Date = 10/06/21 Pct Recovery = 86% Analysis Date = 10/01/21 Pct Recovery = 86% Analysis Date = 10/01/21 Pct Recovery = 86% Analysis Date = 09/27/21 Pct Recovery = 86% Analysis Date = 09/27/21 Pct Recovery = 86% Analysis Date = 09/23/21 Pct Recovery = 86% Analysis Date = 09/23/21 Pct Recovery = 86% Analysis Date = 09/18/21 Pct Recovery = 86% Analysis Date = 09/18/21 Pct Recovery = 86% Analysis Date = 09/14/21 Pct Recovery = 87% Analysis Date = 09/14/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 87% Analysis Date = 09/05/21 Pct Recovery = 87% Analysis Date = 09/05/21 Pct Recovery = 87% Analysis Date = 09/01/21 Pct Recovery = 87% Analysis Date = 09/01/21 Pct Recovery = 87% Analysis Date = 08/27/21 Pct Recovery = 87% Analysis Date = 08/27/21 Pct Recovery = 87% Analysis Date = 08/23/21 Pct Recovery = 87% Analysis Date = 08/23/21 Pct Recovery = 87% Analysis Date = 08/19/21 Pct Recovery = 87% Analysis Date = 08/19/21 Pct Recovery = 87% Analysis Date = 08/14/21 Pct Recovery = 87% Analysis Date = 08/14/21 Pct Recovery = 87% Analysis Date = 08/10/21 Pct Recovery = 88% Analysis Date = 08/10/21 Pct Recovery = 88% Analysis Date = 08/05/21 Pct Recovery = 88% Analysis Date = 08/05/21 Pct Recovery = 88% Analysis Date = 08/01/21 Pct Recovery = 88% Analysis Date = 08/01/21 Pct Recovery = 88% Analysis Date = 07/28/21 Pct Recovery = 88% Analysis Date = 07/28/21 Pct Recovery = 88% Analysis Date = 07/23/21 Pct Recovery = 88% Analysis Date = 07/23/21 Pct Recovery = 88% Analysis Date = 07/19/21 Pct Recovery = 88% Analysis Date = 07/19/21 Pct Recovery = 88% Analysis Date = 07/14/21 Pct Recovery = 88% Analysis Date = 07/14/21 Pct Recovery = 88% Analysis Date = 07/10/21 Pct Recovery = 89% Analysis Date = 07/10/21 Pct Recovery = 89% Analysis Date = 07/06/21 Pct Recovery = 89% Analysis Date = 07/06/21 Pct Recovery = 89% Analysis Date = 07/01/21 Pct Recovery = 89% Analysis Date = 07/01/21 Pct Recovery = 89% Analysis Date = 06/27/21 Pct Recovery = 89% Analysis Date = 06/27/21 Pct Recovery = 89% Analysis Date = 06/23/21 Pct Recovery = 89% Analysis Date = 06/23/21 Pct Recovery = 89% Analysis Date = 06/18/21 Pct Recovery = 89% Analysis Date = 06/18/21 Pct Recovery = 89% Analysis Date = 06/14/21 Pct Recovery = 89% Analysis Date = 06/14/21 Pct Recovery = 89% Analysis Date = 06/09/21 Pct Recovery = 89% Analysis Date = 06/09/21 Pct Recovery = 89% Analysis Date = 06/05/21 Pct Recovery = 90% Analysis Date = 06/05/21 Pct Recovery = 90% Analysis Date = 06/01/21 Pct Recovery = 90% Analysis Date = 06/01/21 Pct Recovery = 90% Analysis Date = 05/27/21 Pct Recovery = 90% Analysis Date = 05/27/21 Pct Recovery = 90% Analysis Date = 05/23/21 Pct Recovery = 90% Analysis Date = 05/23/21 Pct Recovery = 90% Analysis Date = 05/18/21 Pct Recovery = 90% Analysis Date = 05/18/21 Pct Recovery = 90% Analysis Date = 05/14/21 Pct Recovery = 90% Analysis Date = 05/14/21 Pct Recovery = 90% Analysis Date = 05/10/21 Pct Recovery = 90% Analysis Date = 05/10/21 Pct Recovery = 90% Analysis Date = 05/05/21 Pct Recovery = 91% Analysis Date = 05/05/21 Pct Recovery = 91% Analysis Date = 05/01/21 Pct Recovery = 91% Analysis Date = 05/01/21 Pct Recovery = 91% Analysis Date = 04/27/21 Pct Recovery = 91% Analysis Date = 04/27/21 Pct Recovery = 91% Analysis Date = 04/22/21 Pct Recovery = 91% Analysis Date = 04/22/21 Pct Recovery = 91% Analysis Date = 04/18/21 Pct Recovery = 91% Analysis Date = 04/18/21 Pct Recovery = 91% Analysis Date = 04/13/21 Pct Recovery = 91% Analysis Date = 04/13/21 Pct Recovery = 91% Analysis Date = 04/09/21 Pct Recovery = 92% Analysis Date = 04/09/21 Pct Recovery = 92% Analysis Date = 04/05/21 Pct Recovery = 92% Analysis Date = 04/05/21 Pct Recovery = 92% Analysis Date = 03/31/21 Pct Recovery = 93% Analysis Date = 03/31/21 Pct Recovery = 93% Analysis Date = 03/27/21 Pct Recovery = 93% Analysis Date = 03/27/21 Pct Recovery = 93% Analysis Date = 03/22/21 Pct Recovery = 94% Analysis Date = 03/22/21 Pct Recovery = 94% Analysis Date = 03/18/21 Pct Recovery = 94% Analysis Date = 03/18/21 Pct Recovery = 94% Analysis Date = 03/14/21 Pct Recovery = 95% Analysis Date = 03/14/21 Pct Recovery = 95% Analysis Date = 03/09/21 Pct Recovery = 95% Analysis Date = 03/09/21 Pct Recovery = 95% Analysis Date = 03/05/21 Pct Recovery = 96% Analysis Date = 03/05/21 Pct Recovery = 96% Analysis Date = 03/01/21 Pct Recovery = 96% Analysis Date = 03/01/21 Pct Recovery = 96% Analysis Date = 02/24/21 Pct Recovery = 97% Analysis Date = 02/24/21 Pct Recovery = 97% Analysis Date = 02/20/21 Pct Recovery = 97% Analysis Date = 02/20/21 Pct Recovery = 97% Analysis Date = 02/15/21 Pct Recovery = 98% Analysis Date = 02/15/21 Pct Recovery = 98% Analysis Date = 02/11/21 Pct Recovery = 98% Analysis Date = 02/11/21 Pct Recovery = 98% Analysis Date = 02/07/21 Pct Recovery = 99% Analysis Date = 02/07/21 Pct Recovery = 99% Analysis Date = 02/02/21 Pct Recovery = 99% Analysis Date = 02/02/21 Pct Recovery = 99% Analysis Date = 01/29/21 Pct Recovery = 100% Analysis Date = 01/29/21 Pct Recovery = 100% Analysis Date = 01/24/21 Pct Recovery = 100% Analysis Date = 01/24/21 Pct Recovery = 100% Analysis Date = 01/20/21 Pct Recovery = 101% Analysis Date = 01/20/21 Pct Recovery = 101% Analysis Date = 01/16/21 Pct Recovery = 101% Analysis Date = 01/16/21 Pct Recovery = 101% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 103% Analysis Date = 12/29/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/20/20 Pct Recovery = 104% Analysis Date = 12/20/20 Pct Recovery = 104% Analysis Date = 12/16/20 Pct Recovery = 104% Analysis Date = 12/16/20 Pct Recovery = 104% Analysis Date = 12/12/20 Pct Recovery = 105% Analysis Date = 12/12/20 Pct Recovery = 105% Analysis Date = 12/07/20 Pct Recovery = 105% Analysis Date = 12/07/20 Pct Recovery = 105% Analysis Date = 12/03/20 Pct Recovery = 106% Analysis Date = 12/03/20 Pct Recovery = 106% Analysis Date = 11/28/20 Pct Recovery = 106% Analysis Date = 11/28/20 Pct Recovery = 106% Analysis Date = 11/24/20 Pct Recovery = 107% Analysis Date = 11/24/20 Pct Recovery = 107% Analysis Date = 11/20/20 Pct Recovery = 107% Analysis Date = 11/20/20 Pct Recovery = 107% Analysis Date = 11/15/20 Pct Recovery = 108% Analysis Date = 11/15/20 Pct Recovery = 108% Analysis Date = 11/11/20 Pct Recovery = 108% Analysis Date = 11/11/20 Pct Recovery = 108% Analysis Date = 11/07/20 Pct Recovery = 109% Analysis Date = 11/07/20 Pct Recovery = 109% Analysis Date = 11/02/20 Pct Recovery = 109% Analysis Date = 11/02/20 Pct Recovery = 109% Analysis Date = 10/29/20 Pct Recovery = 110% Analysis Date = 10/29/20 Pct Recovery = 110% Analysis Date = 10/24/20 Pct Recovery = 110% Analysis Date = 10/24/20 Pct Recovery = 110% Analysis Date = 10/20/20 Pct Recovery = 110% Analysis Date = 10/20/20 Pct Recovery = 110% Analysis Date = 10/16/20 Pct Recovery = 109% Analysis Date = 10/16/20 Pct Recovery = 109% Analysis Date = 10/11/20 Pct Recovery = 109% Analysis Date = 10/11/20 Pct Recovery = 109% Analysis Date = 10/07/20 Pct Recovery = 109% Analysis Date = 10/07/20 Pct Recovery = 109% Analysis Date = 10/02/20 Pct Recovery = 109% Analysis Date = 10/02/20 Pct Recovery = 109% Analysis Date = 09/28/20 Pct Recovery = 109% Analysis Date = 09/28/20 Pct Recovery = 109% Analysis Date = 09/24/20 Pct Recovery = 108% Analysis Date = 09/24/20 Pct Recovery = 108% Analysis Date = 09/19/20 Pct Recovery = 108% Analysis Date = 09/19/20 Pct Recovery = 108% Analysis Date = 09/15/20 Pct Recovery = 107% Analysis Date = 09/15/20 Pct Recovery = 107% Analysis Date = 09/11/20 Pct Recovery = 107% Analysis Date = 09/11/20 Pct Recovery = 107% Analysis Date = 09/06/20 Pct Recovery = 106% Analysis Date = 09/06/20 Pct Recovery = 106% Analysis Date = 09/02/20 Pct Recovery = 106% Analysis Date = 09/02/20 Pct Recovery = 106% Analysis Date = 08/28/20 Pct Recovery = 106% Analysis Date = 08/28/20 Pct Recovery = 106% Analysis Date = 08/24/20 Pct Recovery = 105% Analysis Date = 08/24/20 Pct Recovery = 105% Analysis Date = 08/20/20 Pct Recovery = 105% Analysis Date = 08/20/20 Pct Recovery = 105% Analysis Date = 08/15/20 Pct Recovery = 104% Analysis Date = 08/15/20 Pct Recovery = 104% Analysis Date = 08/11/20 Pct Recovery = 104% Analysis Date = 08/11/20 Pct Recovery = 104% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 103% Analysis Date = 07/29/20 Pct Recovery = 102% Analysis Date = 07/29/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 102% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/11/20 Pct Recovery = 100% Analysis Date = 07/11/20 Pct Recovery = 100% Analysis Date = 07/07/20 Pct Recovery = 99% Analysis Date = 07/07/20 Pct Recovery = 99% Analysis Date = 07/02/20 Pct Recovery = 99% Analysis Date = 07/02/20 Pct Recovery = 99% Analysis Date = 06/28/20 Pct Recovery = 98% Analysis Date = 06/28/20 Pct Recovery = 98% Analysis Date = 06/24/20 Pct Recovery = 98% Analysis Date = 06/24/20 Pct Recovery = 98% Analysis Date = 06/19/20 Pct Recovery = 97% Analysis Date = 06/19/20 Pct Recovery = 97% Analysis Date = 06/15/20 Pct Recovery = 97% Analysis Date = 06/15/20 Pct Recovery = 97% Analysis Date = 06/10/20 Pct Recovery = 96% Analysis Date = 06/10/20 Pct Recovery = 96% Analysis Date = 06/06/20 Pct Recovery = 95% Analysis Date = 06/06/20 Pct Recovery = 95% Analysis Date = 06/02/20 Pct Recovery = 95% Analysis Date = 06/02/20 Pct Recovery = 95% Analysis Date = 05/28/20 Pct Recovery = 94% Analysis Date = 05/28/20 Pct Recovery = 94% Analysis Date = 05/24/20 Pct Recovery = 94% Analysis Date = 05/24/20 Pct Recovery = 94% Analysis Date = 05/20/20 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,4-D

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 39 95% 29% 92% 32%
Total 39 95% 29% 92% 32%

Sample Statistics
2,4-D

Characteristic N % % Basis
Plotted 39 93% Spiked
Estimated Values 7 17% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 7% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

OBSP Determination:
2-HYDROXY-4-ISOPROPYLAMINO-6-AMINO-S-TRIAZINE
METHOD: 2447 , TESTIDCODE: 68659LCM60

Laboratory ID = 20202590106 Lab Value = 45.113 Expected Conc. = 50 Report level label = 4 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 42.332 Expected Conc. = 50 Report level label = 4 Pct Recovery = 85% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221370164 Lab Value = 48.842 Expected Conc. = 40.8 Report level label = 4 Pct Recovery = 120% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20222210250 Lab Value = 19.723 Expected Conc. = 40 Report level label = 4 Pct Recovery = 49% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 30.203 Expected Conc. = 40 Report level label = 4 Pct Recovery = 76% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 22.597 Expected Conc. = 40 Report level label = 4 Pct Recovery = 56% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20202390020 Lab Value = 25.476 Expected Conc. = 25.15 Report level label = 4 Pct Recovery = 101% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 18.171 Expected Conc. = 25.15 Report level label = 4 Pct Recovery = 72% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20222070177 Lab Value = 12.230 Expected Conc. = 25 Report level label = 4 Pct Recovery = 49% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20203230018 Lab Value = 22.991 Expected Conc. = 25 Report level label = 4 Pct Recovery = 92% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 21.436 Expected Conc. = 25 Report level label = 4 Pct Recovery = 86% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 27.150 Expected Conc. = 25 Report level label = 4 Pct Recovery = 109% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201550031 Lab Value = 28.117 Expected Conc. = 24.85 Report level label = 4 Pct Recovery = 113% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20201960104 Lab Value = 20.359 Expected Conc. = 20.12 Report level label = 4 Pct Recovery = 101% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 18.204 Expected Conc. = 20.12 Report level label = 4 Pct Recovery = 90% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20221160208 Lab Value = 7.410 Expected Conc. = 10.2 Report level label = 4 Pct Recovery = 73% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20222000207 Lab Value = 5.998 Expected Conc. = 10 Report level label = 4 Pct Recovery = 60% Analysis Date = 07/27/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20210970035 Lab Value = 7.241 Expected Conc. = 10 Report level label = 4 Pct Recovery = 72% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 9.134 Expected Conc. = 10 Report level label = 4 Pct Recovery = 91% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 8.666 Expected Conc. = 10 Report level label = 4 Pct Recovery = 87% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 10.202 Expected Conc. = 10 Report level label = 4 Pct Recovery = 102% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 7.465 Expected Conc. = 10 Report level label = 4 Pct Recovery = 75% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 7.961 Expected Conc. = 10 Report level label = 4 Pct Recovery = 80% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 9.425 Expected Conc. = 9.94 Report level label = 4 Pct Recovery = 95% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 7.520 Expected Conc. = 9.94 Report level label = 4 Pct Recovery = 76% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 10.426 Expected Conc. = 9.94 Report level label = 4 Pct Recovery = 105% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 9.390 Expected Conc. = 9.94 Report level label = 4 Pct Recovery = 94% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 8.339 Expected Conc. = 9.94 Report level label = 4 Pct Recovery = 84% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Analysis Date = 08/15/22 Pct Recovery = 65% Analysis Date = 08/11/22 Pct Recovery = 66% Analysis Date = 08/11/22 Pct Recovery = 66% Analysis Date = 08/07/22 Pct Recovery = 66% Analysis Date = 08/07/22 Pct Recovery = 66% Analysis Date = 08/03/22 Pct Recovery = 66% Analysis Date = 08/03/22 Pct Recovery = 66% Analysis Date = 07/30/22 Pct Recovery = 66% Analysis Date = 07/30/22 Pct Recovery = 66% Analysis Date = 07/26/22 Pct Recovery = 67% Analysis Date = 07/26/22 Pct Recovery = 67% Analysis Date = 07/22/22 Pct Recovery = 67% Analysis Date = 07/22/22 Pct Recovery = 67% Analysis Date = 07/18/22 Pct Recovery = 67% Analysis Date = 07/18/22 Pct Recovery = 67% Analysis Date = 07/14/22 Pct Recovery = 67% Analysis Date = 07/14/22 Pct Recovery = 67% Analysis Date = 07/10/22 Pct Recovery = 68% Analysis Date = 07/10/22 Pct Recovery = 68% Analysis Date = 07/06/22 Pct Recovery = 68% Analysis Date = 07/06/22 Pct Recovery = 68% Analysis Date = 07/02/22 Pct Recovery = 68% Analysis Date = 07/02/22 Pct Recovery = 68% Analysis Date = 06/28/22 Pct Recovery = 68% Analysis Date = 06/28/22 Pct Recovery = 68% Analysis Date = 06/24/22 Pct Recovery = 68% Analysis Date = 06/24/22 Pct Recovery = 68% Analysis Date = 06/20/22 Pct Recovery = 69% Analysis Date = 06/20/22 Pct Recovery = 69% Analysis Date = 06/16/22 Pct Recovery = 69% Analysis Date = 06/16/22 Pct Recovery = 69% Analysis Date = 06/12/22 Pct Recovery = 69% Analysis Date = 06/12/22 Pct Recovery = 69% Analysis Date = 06/08/22 Pct Recovery = 69% Analysis Date = 06/08/22 Pct Recovery = 69% Analysis Date = 06/04/22 Pct Recovery = 70% Analysis Date = 06/04/22 Pct Recovery = 70% Analysis Date = 05/31/22 Pct Recovery = 70% Analysis Date = 05/31/22 Pct Recovery = 70% Analysis Date = 05/27/22 Pct Recovery = 70% Analysis Date = 05/27/22 Pct Recovery = 70% Analysis Date = 05/23/22 Pct Recovery = 70% Analysis Date = 05/23/22 Pct Recovery = 70% Analysis Date = 05/19/22 Pct Recovery = 70% Analysis Date = 05/19/22 Pct Recovery = 70% Analysis Date = 05/14/22 Pct Recovery = 70% Analysis Date = 05/14/22 Pct Recovery = 70% Analysis Date = 05/10/22 Pct Recovery = 70% Analysis Date = 05/10/22 Pct Recovery = 70% Analysis Date = 05/06/22 Pct Recovery = 71% Analysis Date = 05/06/22 Pct Recovery = 71% Analysis Date = 05/02/22 Pct Recovery = 71% Analysis Date = 05/02/22 Pct Recovery = 71% Analysis Date = 04/28/22 Pct Recovery = 71% Analysis Date = 04/28/22 Pct Recovery = 71% Analysis Date = 04/24/22 Pct Recovery = 71% Analysis Date = 04/24/22 Pct Recovery = 71% Analysis Date = 04/20/22 Pct Recovery = 71% Analysis Date = 04/20/22 Pct Recovery = 71% Analysis Date = 04/16/22 Pct Recovery = 71% Analysis Date = 04/16/22 Pct Recovery = 71% Analysis Date = 04/12/22 Pct Recovery = 71% Analysis Date = 04/12/22 Pct Recovery = 71% Analysis Date = 04/08/22 Pct Recovery = 71% Analysis Date = 04/08/22 Pct Recovery = 71% Analysis Date = 04/04/22 Pct Recovery = 71% Analysis Date = 04/04/22 Pct Recovery = 71% Analysis Date = 03/31/22 Pct Recovery = 71% Analysis Date = 03/31/22 Pct Recovery = 71% Analysis Date = 03/27/22 Pct Recovery = 72% Analysis Date = 03/27/22 Pct Recovery = 72% Analysis Date = 03/23/22 Pct Recovery = 72% Analysis Date = 03/23/22 Pct Recovery = 72% Analysis Date = 03/19/22 Pct Recovery = 72% Analysis Date = 03/19/22 Pct Recovery = 72% Analysis Date = 03/15/22 Pct Recovery = 72% Analysis Date = 03/15/22 Pct Recovery = 72% Analysis Date = 03/11/22 Pct Recovery = 72% Analysis Date = 03/11/22 Pct Recovery = 72% Analysis Date = 03/07/22 Pct Recovery = 72% Analysis Date = 03/07/22 Pct Recovery = 72% Analysis Date = 03/03/22 Pct Recovery = 72% Analysis Date = 03/03/22 Pct Recovery = 72% Analysis Date = 02/27/22 Pct Recovery = 72% Analysis Date = 02/27/22 Pct Recovery = 72% Analysis Date = 02/23/22 Pct Recovery = 72% Analysis Date = 02/23/22 Pct Recovery = 72% Analysis Date = 02/19/22 Pct Recovery = 73% Analysis Date = 02/19/22 Pct Recovery = 73% Analysis Date = 02/14/22 Pct Recovery = 73% Analysis Date = 02/14/22 Pct Recovery = 73% Analysis Date = 02/10/22 Pct Recovery = 73% Analysis Date = 02/10/22 Pct Recovery = 73% Analysis Date = 02/06/22 Pct Recovery = 73% Analysis Date = 02/06/22 Pct Recovery = 73% Analysis Date = 02/02/22 Pct Recovery = 73% Analysis Date = 02/02/22 Pct Recovery = 73% Analysis Date = 01/29/22 Pct Recovery = 73% Analysis Date = 01/29/22 Pct Recovery = 73% Analysis Date = 01/25/22 Pct Recovery = 73% Analysis Date = 01/25/22 Pct Recovery = 73% Analysis Date = 01/21/22 Pct Recovery = 73% Analysis Date = 01/21/22 Pct Recovery = 73% Analysis Date = 01/17/22 Pct Recovery = 73% Analysis Date = 01/17/22 Pct Recovery = 73% Analysis Date = 01/13/22 Pct Recovery = 73% Analysis Date = 01/13/22 Pct Recovery = 73% Analysis Date = 01/09/22 Pct Recovery = 74% Analysis Date = 01/09/22 Pct Recovery = 74% Analysis Date = 01/05/22 Pct Recovery = 74% Analysis Date = 01/05/22 Pct Recovery = 74% Analysis Date = 01/01/22 Pct Recovery = 74% Analysis Date = 01/01/22 Pct Recovery = 74% Analysis Date = 12/28/21 Pct Recovery = 74% Analysis Date = 12/28/21 Pct Recovery = 74% Analysis Date = 12/24/21 Pct Recovery = 74% Analysis Date = 12/24/21 Pct Recovery = 74% Analysis Date = 12/20/21 Pct Recovery = 74% Analysis Date = 12/20/21 Pct Recovery = 74% Analysis Date = 12/16/21 Pct Recovery = 74% Analysis Date = 12/16/21 Pct Recovery = 74% Analysis Date = 12/12/21 Pct Recovery = 74% Analysis Date = 12/12/21 Pct Recovery = 74% Analysis Date = 12/08/21 Pct Recovery = 74% Analysis Date = 12/08/21 Pct Recovery = 74% Analysis Date = 12/04/21 Pct Recovery = 74% Analysis Date = 12/04/21 Pct Recovery = 74% Analysis Date = 11/30/21 Pct Recovery = 75% Analysis Date = 11/30/21 Pct Recovery = 75% Analysis Date = 11/26/21 Pct Recovery = 75% Analysis Date = 11/26/21 Pct Recovery = 75% Analysis Date = 11/22/21 Pct Recovery = 75% Analysis Date = 11/22/21 Pct Recovery = 75% Analysis Date = 11/17/21 Pct Recovery = 75% Analysis Date = 11/17/21 Pct Recovery = 75% Analysis Date = 11/13/21 Pct Recovery = 75% Analysis Date = 11/13/21 Pct Recovery = 75% Analysis Date = 11/09/21 Pct Recovery = 75% Analysis Date = 11/09/21 Pct Recovery = 75% Analysis Date = 11/05/21 Pct Recovery = 75% Analysis Date = 11/05/21 Pct Recovery = 75% Analysis Date = 11/01/21 Pct Recovery = 75% Analysis Date = 11/01/21 Pct Recovery = 75% Analysis Date = 10/28/21 Pct Recovery = 75% Analysis Date = 10/28/21 Pct Recovery = 75% Analysis Date = 10/24/21 Pct Recovery = 75% Analysis Date = 10/24/21 Pct Recovery = 75% Analysis Date = 10/20/21 Pct Recovery = 76% Analysis Date = 10/20/21 Pct Recovery = 76% Analysis Date = 10/16/21 Pct Recovery = 76% Analysis Date = 10/16/21 Pct Recovery = 76% Analysis Date = 10/12/21 Pct Recovery = 76% Analysis Date = 10/12/21 Pct Recovery = 76% Analysis Date = 10/08/21 Pct Recovery = 76% Analysis Date = 10/08/21 Pct Recovery = 76% Analysis Date = 10/04/21 Pct Recovery = 76% Analysis Date = 10/04/21 Pct Recovery = 76% Analysis Date = 09/30/21 Pct Recovery = 76% Analysis Date = 09/30/21 Pct Recovery = 76% Analysis Date = 09/26/21 Pct Recovery = 76% Analysis Date = 09/26/21 Pct Recovery = 76% Analysis Date = 09/22/21 Pct Recovery = 76% Analysis Date = 09/22/21 Pct Recovery = 76% Analysis Date = 09/18/21 Pct Recovery = 76% Analysis Date = 09/18/21 Pct Recovery = 76% Analysis Date = 09/14/21 Pct Recovery = 77% Analysis Date = 09/14/21 Pct Recovery = 77% Analysis Date = 09/10/21 Pct Recovery = 77% Analysis Date = 09/10/21 Pct Recovery = 77% Analysis Date = 09/06/21 Pct Recovery = 77% Analysis Date = 09/06/21 Pct Recovery = 77% Analysis Date = 09/02/21 Pct Recovery = 77% Analysis Date = 09/02/21 Pct Recovery = 77% Analysis Date = 08/29/21 Pct Recovery = 77% Analysis Date = 08/29/21 Pct Recovery = 77% Analysis Date = 08/25/21 Pct Recovery = 77% Analysis Date = 08/25/21 Pct Recovery = 77% Analysis Date = 08/20/21 Pct Recovery = 77% Analysis Date = 08/20/21 Pct Recovery = 77% Analysis Date = 08/16/21 Pct Recovery = 77% Analysis Date = 08/16/21 Pct Recovery = 77% Analysis Date = 08/12/21 Pct Recovery = 77% Analysis Date = 08/12/21 Pct Recovery = 77% Analysis Date = 08/08/21 Pct Recovery = 77% Analysis Date = 08/08/21 Pct Recovery = 77% Analysis Date = 08/04/21 Pct Recovery = 78% Analysis Date = 08/04/21 Pct Recovery = 78% Analysis Date = 07/31/21 Pct Recovery = 78% Analysis Date = 07/31/21 Pct Recovery = 78% Analysis Date = 07/27/21 Pct Recovery = 78% Analysis Date = 07/27/21 Pct Recovery = 78% Analysis Date = 07/23/21 Pct Recovery = 78% Analysis Date = 07/23/21 Pct Recovery = 78% Analysis Date = 07/19/21 Pct Recovery = 78% Analysis Date = 07/19/21 Pct Recovery = 78% Analysis Date = 07/15/21 Pct Recovery = 78% Analysis Date = 07/15/21 Pct Recovery = 78% Analysis Date = 07/11/21 Pct Recovery = 78% Analysis Date = 07/11/21 Pct Recovery = 78% Analysis Date = 07/07/21 Pct Recovery = 78% Analysis Date = 07/07/21 Pct Recovery = 78% Analysis Date = 07/03/21 Pct Recovery = 78% Analysis Date = 07/03/21 Pct Recovery = 78% Analysis Date = 06/29/21 Pct Recovery = 78% Analysis Date = 06/29/21 Pct Recovery = 78% Analysis Date = 06/25/21 Pct Recovery = 79% Analysis Date = 06/25/21 Pct Recovery = 79% Analysis Date = 06/21/21 Pct Recovery = 79% Analysis Date = 06/21/21 Pct Recovery = 79% Analysis Date = 06/17/21 Pct Recovery = 79% Analysis Date = 06/17/21 Pct Recovery = 79% Analysis Date = 06/13/21 Pct Recovery = 79% Analysis Date = 06/13/21 Pct Recovery = 79% Analysis Date = 06/09/21 Pct Recovery = 79% Analysis Date = 06/09/21 Pct Recovery = 79% Analysis Date = 06/05/21 Pct Recovery = 79% Analysis Date = 06/05/21 Pct Recovery = 79% Analysis Date = 06/01/21 Pct Recovery = 79% Analysis Date = 06/01/21 Pct Recovery = 79% Analysis Date = 05/28/21 Pct Recovery = 79% Analysis Date = 05/28/21 Pct Recovery = 79% Analysis Date = 05/24/21 Pct Recovery = 79% Analysis Date = 05/24/21 Pct Recovery = 79% Analysis Date = 05/19/21 Pct Recovery = 80% Analysis Date = 05/19/21 Pct Recovery = 80% Analysis Date = 05/15/21 Pct Recovery = 80% Analysis Date = 05/15/21 Pct Recovery = 80% Analysis Date = 05/11/21 Pct Recovery = 80% Analysis Date = 05/11/21 Pct Recovery = 80% Analysis Date = 05/07/21 Pct Recovery = 80% Analysis Date = 05/07/21 Pct Recovery = 80% Analysis Date = 05/03/21 Pct Recovery = 80% Analysis Date = 05/03/21 Pct Recovery = 80% Analysis Date = 04/29/21 Pct Recovery = 80% Analysis Date = 04/29/21 Pct Recovery = 80% Analysis Date = 04/25/21 Pct Recovery = 80% Analysis Date = 04/25/21 Pct Recovery = 80% Analysis Date = 04/21/21 Pct Recovery = 80% Analysis Date = 04/21/21 Pct Recovery = 80% Analysis Date = 04/17/21 Pct Recovery = 80% Analysis Date = 04/17/21 Pct Recovery = 80% Analysis Date = 04/13/21 Pct Recovery = 80% Analysis Date = 04/13/21 Pct Recovery = 80% Analysis Date = 04/09/21 Pct Recovery = 81% Analysis Date = 04/09/21 Pct Recovery = 81% Analysis Date = 04/05/21 Pct Recovery = 81% Analysis Date = 04/05/21 Pct Recovery = 81% Analysis Date = 04/01/21 Pct Recovery = 81% Analysis Date = 04/01/21 Pct Recovery = 81% Analysis Date = 03/28/21 Pct Recovery = 82% Analysis Date = 03/28/21 Pct Recovery = 82% Analysis Date = 03/24/21 Pct Recovery = 82% Analysis Date = 03/24/21 Pct Recovery = 82% Analysis Date = 03/20/21 Pct Recovery = 82% Analysis Date = 03/20/21 Pct Recovery = 82% Analysis Date = 03/16/21 Pct Recovery = 83% Analysis Date = 03/16/21 Pct Recovery = 83% Analysis Date = 03/12/21 Pct Recovery = 83% Analysis Date = 03/12/21 Pct Recovery = 83% Analysis Date = 03/08/21 Pct Recovery = 83% Analysis Date = 03/08/21 Pct Recovery = 83% Analysis Date = 03/04/21 Pct Recovery = 84% Analysis Date = 03/04/21 Pct Recovery = 84% Analysis Date = 02/28/21 Pct Recovery = 84% Analysis Date = 02/28/21 Pct Recovery = 84% Analysis Date = 02/24/21 Pct Recovery = 84% Analysis Date = 02/24/21 Pct Recovery = 84% Analysis Date = 02/19/21 Pct Recovery = 85% Analysis Date = 02/19/21 Pct Recovery = 85% Analysis Date = 02/15/21 Pct Recovery = 85% Analysis Date = 02/15/21 Pct Recovery = 85% Analysis Date = 02/11/21 Pct Recovery = 85% Analysis Date = 02/11/21 Pct Recovery = 85% Analysis Date = 02/07/21 Pct Recovery = 86% Analysis Date = 02/07/21 Pct Recovery = 86% Analysis Date = 02/03/21 Pct Recovery = 86% Analysis Date = 02/03/21 Pct Recovery = 86% Analysis Date = 01/30/21 Pct Recovery = 86% Analysis Date = 01/30/21 Pct Recovery = 86% Analysis Date = 01/26/21 Pct Recovery = 87% Analysis Date = 01/26/21 Pct Recovery = 87% Analysis Date = 01/22/21 Pct Recovery = 87% Analysis Date = 01/22/21 Pct Recovery = 87% Analysis Date = 01/18/21 Pct Recovery = 87% Analysis Date = 01/18/21 Pct Recovery = 87% Analysis Date = 01/14/21 Pct Recovery = 88% Analysis Date = 01/14/21 Pct Recovery = 88% Analysis Date = 01/10/21 Pct Recovery = 88% Analysis Date = 01/10/21 Pct Recovery = 88% Analysis Date = 01/06/21 Pct Recovery = 88% Analysis Date = 01/06/21 Pct Recovery = 88% Analysis Date = 01/02/21 Pct Recovery = 89% Analysis Date = 01/02/21 Pct Recovery = 89% Analysis Date = 12/29/20 Pct Recovery = 89% Analysis Date = 12/29/20 Pct Recovery = 89% Analysis Date = 12/25/20 Pct Recovery = 89% Analysis Date = 12/25/20 Pct Recovery = 89% Analysis Date = 12/21/20 Pct Recovery = 90% Analysis Date = 12/21/20 Pct Recovery = 90% Analysis Date = 12/17/20 Pct Recovery = 90% Analysis Date = 12/17/20 Pct Recovery = 90% Analysis Date = 12/13/20 Pct Recovery = 90% Analysis Date = 12/13/20 Pct Recovery = 90% Analysis Date = 12/09/20 Pct Recovery = 90% Analysis Date = 12/09/20 Pct Recovery = 90% Analysis Date = 12/05/20 Pct Recovery = 90% Analysis Date = 12/05/20 Pct Recovery = 90% Analysis Date = 12/01/20 Pct Recovery = 90% Analysis Date = 12/01/20 Pct Recovery = 90% Analysis Date = 11/27/20 Pct Recovery = 90% Analysis Date = 11/27/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 90% Analysis Date = 11/18/20 Pct Recovery = 90% Analysis Date = 11/18/20 Pct Recovery = 90% Analysis Date = 11/14/20 Pct Recovery = 90% Analysis Date = 11/14/20 Pct Recovery = 90% Analysis Date = 11/10/20 Pct Recovery = 90% Analysis Date = 11/10/20 Pct Recovery = 90% Analysis Date = 11/06/20 Pct Recovery = 90% Analysis Date = 11/06/20 Pct Recovery = 90% Analysis Date = 11/02/20 Pct Recovery = 90% Analysis Date = 11/02/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/25/20 Pct Recovery = 90% Analysis Date = 10/25/20 Pct Recovery = 90% Analysis Date = 10/21/20 Pct Recovery = 90% Analysis Date = 10/21/20 Pct Recovery = 90% Analysis Date = 10/17/20 Pct Recovery = 90% Analysis Date = 10/17/20 Pct Recovery = 90% Analysis Date = 10/13/20 Pct Recovery = 90% Analysis Date = 10/13/20 Pct Recovery = 90% Analysis Date = 10/09/20 Pct Recovery = 89% Analysis Date = 10/09/20 Pct Recovery = 89% Analysis Date = 10/05/20 Pct Recovery = 89% Analysis Date = 10/05/20 Pct Recovery = 89% Analysis Date = 10/01/20 Pct Recovery = 89% Analysis Date = 10/01/20 Pct Recovery = 89% Analysis Date = 09/27/20 Pct Recovery = 89% Analysis Date = 09/27/20 Pct Recovery = 89% Analysis Date = 09/23/20 Pct Recovery = 89% Analysis Date = 09/23/20 Pct Recovery = 89% Analysis Date = 09/19/20 Pct Recovery = 89% Analysis Date = 09/19/20 Pct Recovery = 89% Analysis Date = 09/15/20 Pct Recovery = 89% Analysis Date = 09/15/20 Pct Recovery = 89% Analysis Date = 09/11/20 Pct Recovery = 89% Analysis Date = 09/11/20 Pct Recovery = 89% Analysis Date = 09/07/20 Pct Recovery = 89% Analysis Date = 09/07/20 Pct Recovery = 89% Analysis Date = 09/03/20 Pct Recovery = 89% Analysis Date = 09/03/20 Pct Recovery = 89% Analysis Date = 08/30/20 Pct Recovery = 90% Analysis Date = 08/30/20 Pct Recovery = 90% Analysis Date = 08/25/20 Pct Recovery = 90% Analysis Date = 08/25/20 Pct Recovery = 90% Analysis Date = 08/21/20 Pct Recovery = 90% Analysis Date = 08/21/20 Pct Recovery = 90% Analysis Date = 08/17/20 Pct Recovery = 91% Analysis Date = 08/17/20 Pct Recovery = 91% Analysis Date = 08/13/20 Pct Recovery = 91% Analysis Date = 08/13/20 Pct Recovery = 91% Analysis Date = 08/09/20 Pct Recovery = 91% Analysis Date = 08/09/20 Pct Recovery = 91% Analysis Date = 08/05/20 Pct Recovery = 91% Analysis Date = 08/05/20 Pct Recovery = 91% Analysis Date = 08/01/20 Pct Recovery = 92% Analysis Date = 08/01/20 Pct Recovery = 92% Analysis Date = 07/28/20 Pct Recovery = 92% Analysis Date = 07/28/20 Pct Recovery = 92% Analysis Date = 07/24/20 Pct Recovery = 93% Analysis Date = 07/24/20 Pct Recovery = 93% Analysis Date = 07/20/20 Pct Recovery = 93% Analysis Date = 07/20/20 Pct Recovery = 93% Analysis Date = 07/16/20 Pct Recovery = 93% Analysis Date = 07/16/20 Pct Recovery = 93% Analysis Date = 07/12/20 Pct Recovery = 94% Analysis Date = 07/12/20 Pct Recovery = 94% Analysis Date = 07/08/20 Pct Recovery = 94% Analysis Date = 07/08/20 Pct Recovery = 94% Analysis Date = 07/04/20 Pct Recovery = 94% Analysis Date = 07/04/20 Pct Recovery = 94% Analysis Date = 06/30/20 Pct Recovery = 95% Analysis Date = 06/30/20 Pct Recovery = 95% Analysis Date = 06/26/20 Pct Recovery = 95% Analysis Date = 06/26/20 Pct Recovery = 95% Analysis Date = 06/22/20 Pct Recovery = 95% Analysis Date = 06/22/20 Pct Recovery = 95% Analysis Date = 06/18/20 Pct Recovery = 96% Analysis Date = 06/18/20 Pct Recovery = 96% Analysis Date = 06/14/20 Pct Recovery = 96% Analysis Date = 06/14/20 Pct Recovery = 96% Analysis Date = 06/10/20 Pct Recovery = 97% Analysis Date = 06/10/20 Pct Recovery = 97% Analysis Date = 06/06/20 Pct Recovery = 97% Analysis Date = 06/06/20 Pct Recovery = 97% Analysis Date = 06/02/20 Pct Recovery = 97% Analysis Date = 06/02/20 Pct Recovery = 97% Analysis Date = 05/29/20 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-HYDROXY-4-ISOPROPYLAMINO-6-AMINO-S-TRIAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 85% 18% 86% 18%
Total 28 85% 18% 86% 18%

Sample Statistics
2-HYDROXY-4-ISOPROPYLAMINO-6-AMINO-S-TRIAZINE

Characteristic N % % Basis
Plotted 28 100% Spiked
Estimated Values 15 54% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 28 .  
False Negatives 0 0% 0 out of 28
Not Spiked 86 .  
False Positives 3 3% 3 out of 86

OBSP Determination:
2-HYDROXY-4-ISOPROPYLAMINO-6-ETHYLAMINO-S-TRIAZINE (OIET)
METHOD: 2447 , TESTIDCODE: 68660LCM60

Laboratory ID = 20210620008 Lab Value = 219.743 Expected Conc. = 100.4 Report level label = 8 Pct Recovery = 219% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810053 Lab Value = 237.646 Expected Conc. = 100.4 Report level label = 8 Pct Recovery = 237% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810052 Lab Value = 266.406 Expected Conc. = 100.4 Report level label = 8 Pct Recovery = 265% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202590106 Lab Value = 245.580 Expected Conc. = 99.7 Report level label = 8 Pct Recovery = 246% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 221.483 Expected Conc. = 99.7 Report level label = 8 Pct Recovery = 222% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210400070 Lab Value = 119.986 Expected Conc. = 50.2 Report level label = 8 Pct Recovery = 239% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202390020 Lab Value = 109.247 Expected Conc. = 50.05 Report level label = 8 Pct Recovery = 218% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20203230018 Lab Value = 114.717 Expected Conc. = 49.85 Report level label = 8 Pct Recovery = 230% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 116.077 Expected Conc. = 49.85 Report level label = 8 Pct Recovery = 233% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 118.073 Expected Conc. = 49.85 Report level label = 8 Pct Recovery = 237% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 41.364 Expected Conc. = 19.94 Report level label = 8 Pct Recovery = 207% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 53.686 Expected Conc. = 19.94 Report level label = 8 Pct Recovery = 269% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 42.787 Expected Conc. = 19.94 Report level label = 8 Pct Recovery = 215% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210620007 Lab Value = 194.143 Expected Conc. = 100.4 Report level label = 8 Pct Recovery = 193% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20222210250 Lab Value = 18.343 Expected Conc. = 80 Report level label = 8 Pct Recovery = 23% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 40.586 Expected Conc. = 80 Report level label = 8 Pct Recovery = 51% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 21.042 Expected Conc. = 80 Report level label = 8 Pct Recovery = 26% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221370164 Lab Value = 80.425 Expected Conc. = 80 Report level label = 8 Pct Recovery = 101% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20202110006 Lab Value = 64.225 Expected Conc. = 50.05 Report level label = 8 Pct Recovery = 128% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20222070177 Lab Value = 13.289 Expected Conc. = 50 Report level label = 8 Pct Recovery = 27% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20201960104 Lab Value = 74.888 Expected Conc. = 40.04 Report level label = 8 Pct Recovery = 187% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 34.667 Expected Conc. = 40.04 Report level label = 8 Pct Recovery = 87% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20222000207 Lab Value = 9.058 Expected Conc. = 20 Report level label = 8 Pct Recovery = 45% Analysis Date = 07/27/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20221160208 Lab Value = 19.735 Expected Conc. = 20 Report level label = 8 Pct Recovery = 99% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20210970035 Lab Value = 30.529 Expected Conc. = 19.94 Report level label = 8 Pct Recovery = 153% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 37.594 Expected Conc. = 19.94 Report level label = 8 Pct Recovery = 189% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 33.275 Expected Conc. = 19.94 Report level label = 8 Pct Recovery = 167% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 08/15/22 Pct Recovery = 37% Analysis Date = 08/12/22 Pct Recovery = 39% Analysis Date = 08/12/22 Pct Recovery = 39% Analysis Date = 08/08/22 Pct Recovery = 40% Analysis Date = 08/08/22 Pct Recovery = 40% Analysis Date = 08/04/22 Pct Recovery = 41% Analysis Date = 08/04/22 Pct Recovery = 41% Analysis Date = 07/31/22 Pct Recovery = 43% Analysis Date = 07/31/22 Pct Recovery = 43% Analysis Date = 07/27/22 Pct Recovery = 44% Analysis Date = 07/27/22 Pct Recovery = 44% Analysis Date = 07/23/22 Pct Recovery = 45% Analysis Date = 07/23/22 Pct Recovery = 45% Analysis Date = 07/19/22 Pct Recovery = 47% Analysis Date = 07/19/22 Pct Recovery = 47% Analysis Date = 07/15/22 Pct Recovery = 48% Analysis Date = 07/15/22 Pct Recovery = 48% Analysis Date = 07/11/22 Pct Recovery = 49% Analysis Date = 07/11/22 Pct Recovery = 49% Analysis Date = 07/07/22 Pct Recovery = 50% Analysis Date = 07/07/22 Pct Recovery = 50% Analysis Date = 07/03/22 Pct Recovery = 52% Analysis Date = 07/03/22 Pct Recovery = 52% Analysis Date = 06/30/22 Pct Recovery = 53% Analysis Date = 06/30/22 Pct Recovery = 53% Analysis Date = 06/26/22 Pct Recovery = 54% Analysis Date = 06/26/22 Pct Recovery = 54% Analysis Date = 06/22/22 Pct Recovery = 56% Analysis Date = 06/22/22 Pct Recovery = 56% Analysis Date = 06/18/22 Pct Recovery = 57% Analysis Date = 06/18/22 Pct Recovery = 57% Analysis Date = 06/14/22 Pct Recovery = 58% Analysis Date = 06/14/22 Pct Recovery = 58% Analysis Date = 06/10/22 Pct Recovery = 59% Analysis Date = 06/10/22 Pct Recovery = 59% Analysis Date = 06/06/22 Pct Recovery = 61% Analysis Date = 06/06/22 Pct Recovery = 61% Analysis Date = 06/02/22 Pct Recovery = 62% Analysis Date = 06/02/22 Pct Recovery = 62% Analysis Date = 05/29/22 Pct Recovery = 63% Analysis Date = 05/29/22 Pct Recovery = 63% Analysis Date = 05/25/22 Pct Recovery = 64% Analysis Date = 05/25/22 Pct Recovery = 64% Analysis Date = 05/21/22 Pct Recovery = 66% Analysis Date = 05/21/22 Pct Recovery = 66% Analysis Date = 05/18/22 Pct Recovery = 67% Analysis Date = 05/18/22 Pct Recovery = 67% Analysis Date = 05/14/22 Pct Recovery = 68% Analysis Date = 05/14/22 Pct Recovery = 68% Analysis Date = 05/10/22 Pct Recovery = 69% Analysis Date = 05/10/22 Pct Recovery = 69% Analysis Date = 05/06/22 Pct Recovery = 71% Analysis Date = 05/06/22 Pct Recovery = 71% Analysis Date = 05/02/22 Pct Recovery = 72% Analysis Date = 05/02/22 Pct Recovery = 72% Analysis Date = 04/28/22 Pct Recovery = 73% Analysis Date = 04/28/22 Pct Recovery = 73% Analysis Date = 04/24/22 Pct Recovery = 74% Analysis Date = 04/24/22 Pct Recovery = 74% Analysis Date = 04/20/22 Pct Recovery = 76% Analysis Date = 04/20/22 Pct Recovery = 76% Analysis Date = 04/16/22 Pct Recovery = 77% Analysis Date = 04/16/22 Pct Recovery = 77% Analysis Date = 04/12/22 Pct Recovery = 78% Analysis Date = 04/12/22 Pct Recovery = 78% Analysis Date = 04/08/22 Pct Recovery = 79% Analysis Date = 04/08/22 Pct Recovery = 79% Analysis Date = 04/05/22 Pct Recovery = 80% Analysis Date = 04/05/22 Pct Recovery = 80% Analysis Date = 04/01/22 Pct Recovery = 82% Analysis Date = 04/01/22 Pct Recovery = 82% Analysis Date = 03/28/22 Pct Recovery = 83% Analysis Date = 03/28/22 Pct Recovery = 83% Analysis Date = 03/24/22 Pct Recovery = 84% Analysis Date = 03/24/22 Pct Recovery = 84% Analysis Date = 03/20/22 Pct Recovery = 85% Analysis Date = 03/20/22 Pct Recovery = 85% Analysis Date = 03/16/22 Pct Recovery = 86% Analysis Date = 03/16/22 Pct Recovery = 86% Analysis Date = 03/12/22 Pct Recovery = 87% Analysis Date = 03/12/22 Pct Recovery = 87% Analysis Date = 03/08/22 Pct Recovery = 89% Analysis Date = 03/08/22 Pct Recovery = 89% Analysis Date = 03/04/22 Pct Recovery = 90% Analysis Date = 03/04/22 Pct Recovery = 90% Analysis Date = 02/28/22 Pct Recovery = 91% Analysis Date = 02/28/22 Pct Recovery = 91% Analysis Date = 02/24/22 Pct Recovery = 92% Analysis Date = 02/24/22 Pct Recovery = 92% Analysis Date = 02/21/22 Pct Recovery = 93% Analysis Date = 02/21/22 Pct Recovery = 93% Analysis Date = 02/17/22 Pct Recovery = 95% Analysis Date = 02/17/22 Pct Recovery = 95% Analysis Date = 02/13/22 Pct Recovery = 96% Analysis Date = 02/13/22 Pct Recovery = 96% Analysis Date = 02/09/22 Pct Recovery = 97% Analysis Date = 02/09/22 Pct Recovery = 97% Analysis Date = 02/05/22 Pct Recovery = 98% Analysis Date = 02/05/22 Pct Recovery = 98% Analysis Date = 02/01/22 Pct Recovery = 99% Analysis Date = 02/01/22 Pct Recovery = 99% Analysis Date = 01/28/22 Pct Recovery = 101% Analysis Date = 01/28/22 Pct Recovery = 101% Analysis Date = 01/24/22 Pct Recovery = 102% Analysis Date = 01/24/22 Pct Recovery = 102% Analysis Date = 01/20/22 Pct Recovery = 103% Analysis Date = 01/20/22 Pct Recovery = 103% Analysis Date = 01/16/22 Pct Recovery = 104% Analysis Date = 01/16/22 Pct Recovery = 104% Analysis Date = 01/12/22 Pct Recovery = 105% Analysis Date = 01/12/22 Pct Recovery = 105% Analysis Date = 01/09/22 Pct Recovery = 107% Analysis Date = 01/09/22 Pct Recovery = 107% Analysis Date = 01/05/22 Pct Recovery = 108% Analysis Date = 01/05/22 Pct Recovery = 108% Analysis Date = 01/01/22 Pct Recovery = 109% Analysis Date = 01/01/22 Pct Recovery = 109% Analysis Date = 12/28/21 Pct Recovery = 110% Analysis Date = 12/28/21 Pct Recovery = 110% Analysis Date = 12/24/21 Pct Recovery = 111% Analysis Date = 12/24/21 Pct Recovery = 111% Analysis Date = 12/20/21 Pct Recovery = 112% Analysis Date = 12/20/21 Pct Recovery = 112% Analysis Date = 12/16/21 Pct Recovery = 114% Analysis Date = 12/16/21 Pct Recovery = 114% Analysis Date = 12/12/21 Pct Recovery = 115% Analysis Date = 12/12/21 Pct Recovery = 115% Analysis Date = 12/08/21 Pct Recovery = 116% Analysis Date = 12/08/21 Pct Recovery = 116% Analysis Date = 12/04/21 Pct Recovery = 117% Analysis Date = 12/04/21 Pct Recovery = 117% Analysis Date = 11/30/21 Pct Recovery = 118% Analysis Date = 11/30/21 Pct Recovery = 118% Analysis Date = 11/27/21 Pct Recovery = 120% Analysis Date = 11/27/21 Pct Recovery = 120% Analysis Date = 11/23/21 Pct Recovery = 121% Analysis Date = 11/23/21 Pct Recovery = 121% Analysis Date = 11/19/21 Pct Recovery = 122% Analysis Date = 11/19/21 Pct Recovery = 122% Analysis Date = 11/15/21 Pct Recovery = 123% Analysis Date = 11/15/21 Pct Recovery = 123% Analysis Date = 11/11/21 Pct Recovery = 124% Analysis Date = 11/11/21 Pct Recovery = 124% Analysis Date = 11/07/21 Pct Recovery = 126% Analysis Date = 11/07/21 Pct Recovery = 126% Analysis Date = 11/03/21 Pct Recovery = 127% Analysis Date = 11/03/21 Pct Recovery = 127% Analysis Date = 10/30/21 Pct Recovery = 128% Analysis Date = 10/30/21 Pct Recovery = 128% Analysis Date = 10/26/21 Pct Recovery = 129% Analysis Date = 10/26/21 Pct Recovery = 129% Analysis Date = 10/22/21 Pct Recovery = 130% Analysis Date = 10/22/21 Pct Recovery = 130% Analysis Date = 10/18/21 Pct Recovery = 132% Analysis Date = 10/18/21 Pct Recovery = 132% Analysis Date = 10/15/21 Pct Recovery = 133% Analysis Date = 10/15/21 Pct Recovery = 133% Analysis Date = 10/11/21 Pct Recovery = 134% Analysis Date = 10/11/21 Pct Recovery = 134% Analysis Date = 10/07/21 Pct Recovery = 135% Analysis Date = 10/07/21 Pct Recovery = 135% Analysis Date = 10/03/21 Pct Recovery = 136% Analysis Date = 10/03/21 Pct Recovery = 136% Analysis Date = 09/29/21 Pct Recovery = 138% Analysis Date = 09/29/21 Pct Recovery = 138% Analysis Date = 09/25/21 Pct Recovery = 139% Analysis Date = 09/25/21 Pct Recovery = 139% Analysis Date = 09/21/21 Pct Recovery = 140% Analysis Date = 09/21/21 Pct Recovery = 140% Analysis Date = 09/17/21 Pct Recovery = 141% Analysis Date = 09/17/21 Pct Recovery = 141% Analysis Date = 09/13/21 Pct Recovery = 142% Analysis Date = 09/13/21 Pct Recovery = 142% Analysis Date = 09/09/21 Pct Recovery = 143% Analysis Date = 09/09/21 Pct Recovery = 143% Analysis Date = 09/05/21 Pct Recovery = 145% Analysis Date = 09/05/21 Pct Recovery = 145% Analysis Date = 09/02/21 Pct Recovery = 146% Analysis Date = 09/02/21 Pct Recovery = 146% Analysis Date = 08/29/21 Pct Recovery = 147% Analysis Date = 08/29/21 Pct Recovery = 147% Analysis Date = 08/25/21 Pct Recovery = 148% Analysis Date = 08/25/21 Pct Recovery = 148% Analysis Date = 08/21/21 Pct Recovery = 149% Analysis Date = 08/21/21 Pct Recovery = 149% Analysis Date = 08/17/21 Pct Recovery = 151% Analysis Date = 08/17/21 Pct Recovery = 151% Analysis Date = 08/13/21 Pct Recovery = 152% Analysis Date = 08/13/21 Pct Recovery = 152% Analysis Date = 08/09/21 Pct Recovery = 153% Analysis Date = 08/09/21 Pct Recovery = 153% Analysis Date = 08/05/21 Pct Recovery = 154% Analysis Date = 08/05/21 Pct Recovery = 154% Analysis Date = 08/01/21 Pct Recovery = 155% Analysis Date = 08/01/21 Pct Recovery = 155% Analysis Date = 07/28/21 Pct Recovery = 157% Analysis Date = 07/28/21 Pct Recovery = 157% Analysis Date = 07/24/21 Pct Recovery = 158% Analysis Date = 07/24/21 Pct Recovery = 158% Analysis Date = 07/20/21 Pct Recovery = 159% Analysis Date = 07/20/21 Pct Recovery = 159% Analysis Date = 07/17/21 Pct Recovery = 160% Analysis Date = 07/17/21 Pct Recovery = 160% Analysis Date = 07/13/21 Pct Recovery = 161% Analysis Date = 07/13/21 Pct Recovery = 161% Analysis Date = 07/09/21 Pct Recovery = 163% Analysis Date = 07/09/21 Pct Recovery = 163% Analysis Date = 07/05/21 Pct Recovery = 164% Analysis Date = 07/05/21 Pct Recovery = 164% Analysis Date = 07/01/21 Pct Recovery = 165% Analysis Date = 07/01/21 Pct Recovery = 165% Analysis Date = 06/27/21 Pct Recovery = 166% Analysis Date = 06/27/21 Pct Recovery = 166% Analysis Date = 06/23/21 Pct Recovery = 167% Analysis Date = 06/23/21 Pct Recovery = 167% Analysis Date = 06/19/21 Pct Recovery = 168% Analysis Date = 06/19/21 Pct Recovery = 168% Analysis Date = 06/15/21 Pct Recovery = 170% Analysis Date = 06/15/21 Pct Recovery = 170% Analysis Date = 06/11/21 Pct Recovery = 171% Analysis Date = 06/11/21 Pct Recovery = 171% Analysis Date = 06/07/21 Pct Recovery = 172% Analysis Date = 06/07/21 Pct Recovery = 172% Analysis Date = 06/04/21 Pct Recovery = 173% Analysis Date = 06/04/21 Pct Recovery = 173% Analysis Date = 05/31/21 Pct Recovery = 174% Analysis Date = 05/31/21 Pct Recovery = 174% Analysis Date = 05/27/21 Pct Recovery = 176% Analysis Date = 05/27/21 Pct Recovery = 176% Analysis Date = 05/23/21 Pct Recovery = 177% Analysis Date = 05/23/21 Pct Recovery = 177% Analysis Date = 05/19/21 Pct Recovery = 178% Analysis Date = 05/19/21 Pct Recovery = 178% Analysis Date = 05/15/21 Pct Recovery = 179% Analysis Date = 05/15/21 Pct Recovery = 179% Analysis Date = 05/11/21 Pct Recovery = 180% Analysis Date = 05/11/21 Pct Recovery = 180% Analysis Date = 05/07/21 Pct Recovery = 182% Analysis Date = 05/07/21 Pct Recovery = 182% Analysis Date = 05/03/21 Pct Recovery = 183% Analysis Date = 05/03/21 Pct Recovery = 183% Analysis Date = 04/29/21 Pct Recovery = 184% Analysis Date = 04/29/21 Pct Recovery = 184% Analysis Date = 04/25/21 Pct Recovery = 185% Analysis Date = 04/25/21 Pct Recovery = 185% Analysis Date = 04/22/21 Pct Recovery = 186% Analysis Date = 04/22/21 Pct Recovery = 186% Analysis Date = 04/18/21 Pct Recovery = 188% Analysis Date = 04/18/21 Pct Recovery = 188% Analysis Date = 04/14/21 Pct Recovery = 189% Analysis Date = 04/14/21 Pct Recovery = 189% Analysis Date = 04/10/21 Pct Recovery = 190% Analysis Date = 04/10/21 Pct Recovery = 190% Analysis Date = 04/06/21 Pct Recovery = 191% Analysis Date = 04/06/21 Pct Recovery = 191% Analysis Date = 04/02/21 Pct Recovery = 192% Analysis Date = 04/02/21 Pct Recovery = 192% Analysis Date = 03/29/21 Pct Recovery = 194% Analysis Date = 03/29/21 Pct Recovery = 194% Analysis Date = 03/25/21 Pct Recovery = 195% Analysis Date = 03/25/21 Pct Recovery = 195% Analysis Date = 03/21/21 Pct Recovery = 196% Analysis Date = 03/21/21 Pct Recovery = 196% Analysis Date = 03/17/21 Pct Recovery = 197% Analysis Date = 03/17/21 Pct Recovery = 197% Analysis Date = 03/13/21 Pct Recovery = 198% Analysis Date = 03/13/21 Pct Recovery = 198% Analysis Date = 03/10/21 Pct Recovery = 199% Analysis Date = 03/10/21 Pct Recovery = 199% Analysis Date = 03/06/21 Pct Recovery = 201% Analysis Date = 03/06/21 Pct Recovery = 201% Analysis Date = 03/02/21 Pct Recovery = 202% Analysis Date = 03/02/21 Pct Recovery = 202% Analysis Date = 02/26/21 Pct Recovery = 203% Analysis Date = 02/26/21 Pct Recovery = 203% Analysis Date = 02/22/21 Pct Recovery = 204% Analysis Date = 02/22/21 Pct Recovery = 204% Analysis Date = 02/18/21 Pct Recovery = 205% Analysis Date = 02/18/21 Pct Recovery = 205% Analysis Date = 09/19/20 Pct Recovery = 205% Analysis Date = 09/19/20 Pct Recovery = 205% Analysis Date = 09/15/20 Pct Recovery = 202% Analysis Date = 09/15/20 Pct Recovery = 202% Analysis Date = 09/11/20 Pct Recovery = 199% Analysis Date = 09/11/20 Pct Recovery = 199% Analysis Date = 09/07/20 Pct Recovery = 196% Analysis Date = 09/07/20 Pct Recovery = 196% Analysis Date = 09/03/20 Pct Recovery = 193% Analysis Date = 09/03/20 Pct Recovery = 193% Analysis Date = 08/30/20 Pct Recovery = 190% Analysis Date = 08/30/20 Pct Recovery = 190% Analysis Date = 08/26/20 Pct Recovery = 186% Analysis Date = 08/26/20 Pct Recovery = 186% Analysis Date = 08/22/20 Pct Recovery = 183% Analysis Date = 08/22/20 Pct Recovery = 183% Analysis Date = 08/18/20 Pct Recovery = 180% Analysis Date = 08/18/20 Pct Recovery = 180% Analysis Date = 08/14/20 Pct Recovery = 176% Analysis Date = 08/14/20 Pct Recovery = 176% Analysis Date = 08/10/20 Pct Recovery = 173% Analysis Date = 08/10/20 Pct Recovery = 173% Analysis Date = 08/07/20 Pct Recovery = 169% Analysis Date = 08/07/20 Pct Recovery = 169% Analysis Date = 08/03/20 Pct Recovery = 166% Analysis Date = 08/03/20 Pct Recovery = 166% Analysis Date = 07/30/20 Pct Recovery = 163% Analysis Date = 07/30/20 Pct Recovery = 163% Analysis Date = 07/26/20 Pct Recovery = 159% Analysis Date = 07/26/20 Pct Recovery = 159% Analysis Date = 07/22/20 Pct Recovery = 156% Analysis Date = 07/22/20 Pct Recovery = 156% Analysis Date = 07/18/20 Pct Recovery = 152% Analysis Date = 07/18/20 Pct Recovery = 152% Analysis Date = 07/14/20 Pct Recovery = 149% Analysis Date = 07/14/20 Pct Recovery = 149% Analysis Date = 07/10/20 Pct Recovery = 145% Analysis Date = 07/10/20 Pct Recovery = 145% Analysis Date = 07/06/20 Pct Recovery = 141% Analysis Date = 07/06/20 Pct Recovery = 141% Analysis Date = 07/02/20 Pct Recovery = 138% Analysis Date = 07/02/20 Pct Recovery = 138% Analysis Date = 06/28/20 Pct Recovery = 134% Analysis Date = 06/28/20 Pct Recovery = 134% Analysis Date = 06/25/20 Pct Recovery = 130% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-HYDROXY-4-ISOPROPYLAMINO-6-ETHYLAMINO-S-TRIAZINE (OIET)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 27 167% 81% 193% 99%
Total 27 167% 81% 193% 99%

Sample Statistics
2-HYDROXY-4-ISOPROPYLAMINO-6-ETHYLAMINO-S-TRIAZINE (OIET)

Characteristic N % % Basis
Plotted 27 100% Spiked
Estimated Values 20 74% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 27 .  
False Negatives 0 0% 0 out of 27
Not Spiked 79 .  
False Positives 2 3% 2 out of 79

OBSP Determination:
3-PHENOXYBENZOIC ACID
METHOD: 2447 , TESTIDCODE: 68873LCM60

Laboratory ID = 20201820155 Lab Value = 791.588 Expected Conc. = 765 Report level label = 61 Pct Recovery = 103% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 795.639 Expected Conc. = 765 Report level label = 61 Pct Recovery = 104% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 880.019 Expected Conc. = 756.4 Report level label = 61 Pct Recovery = 116% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20202590107 Lab Value = 820.181 Expected Conc. = 752 Report level label = 61 Pct Recovery = 109% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 738.413 Expected Conc. = 752 Report level label = 61 Pct Recovery = 98% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221940195 Lab Value = 361.935 Expected Conc. = 612.92 Report level label = 61 Pct Recovery = 59% Analysis Date = 07/21/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20222010133 Lab Value = 383.672 Expected Conc. = 610 Report level label = 61 Pct Recovery = 63% Analysis Date = 07/22/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20222640086 Lab Value = 470.852 Expected Conc. = 609.6 Report level label = 61 Pct Recovery = 77% Analysis Date = 09/30/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20202530029 Lab Value = 390.378 Expected Conc. = 382.5 Report level label = 61 Pct Recovery = 102% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 332.055 Expected Conc. = 382.5 Report level label = 61 Pct Recovery = 87% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 468.842 Expected Conc. = 382.5 Report level label = 61 Pct Recovery = 123% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20221870197 Lab Value = 242.349 Expected Conc. = 381.25 Report level label = 61 Pct Recovery = 64% Analysis Date = 07/14/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20221730293 Lab Value = 236.200 Expected Conc. = 381.25 Report level label = 61 Pct Recovery = 62% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20201960104 Lab Value = 451.802 Expected Conc. = 378.2 Report level label = 61 Pct Recovery = 119% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20203360042 Lab Value = 272.605 Expected Conc. = 376 Report level label = 61 Pct Recovery = 73% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 393.318 Expected Conc. = 376 Report level label = 61 Pct Recovery = 105% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 441.855 Expected Conc. = 376 Report level label = 61 Pct Recovery = 118% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202180001 Lab Value = 191.394 Expected Conc. = 153 Report level label = 61 Pct Recovery = 125% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 120.051 Expected Conc. = 153 Report level label = 61 Pct Recovery = 78% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 145.165 Expected Conc. = 153 Report level label = 61 Pct Recovery = 95% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20222500483 Lab Value = 154.354 Expected Conc. = 152.5 Report level label = 61 Pct Recovery = 101% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Laboratory ID = 20201610160 Lab Value = 156.569 Expected Conc. = 151.28 Report level label = 61 Pct Recovery = 103% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210970035 Lab Value = 159.006 Expected Conc. = 150.4 Report level label = 61 Pct Recovery = 106% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 173.402 Expected Conc. = 150.4 Report level label = 61 Pct Recovery = 115% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 147.060 Expected Conc. = 150.4 Report level label = 61 Pct Recovery = 98% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 166.812 Expected Conc. = 150.4 Report level label = 61 Pct Recovery = 111% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 152.070 Expected Conc. = 150.4 Report level label = 61 Pct Recovery = 101% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 143.488 Expected Conc. = 150.4 Report level label = 61 Pct Recovery = 95% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 10/13/22 Pct Recovery = 70% Analysis Date = 10/09/22 Pct Recovery = 70% Analysis Date = 10/09/22 Pct Recovery = 70% Analysis Date = 10/05/22 Pct Recovery = 70% Analysis Date = 10/05/22 Pct Recovery = 70% Analysis Date = 09/30/22 Pct Recovery = 71% Analysis Date = 09/30/22 Pct Recovery = 71% Analysis Date = 09/26/22 Pct Recovery = 71% Analysis Date = 09/26/22 Pct Recovery = 71% Analysis Date = 09/22/22 Pct Recovery = 71% Analysis Date = 09/22/22 Pct Recovery = 71% Analysis Date = 09/17/22 Pct Recovery = 71% Analysis Date = 09/17/22 Pct Recovery = 71% Analysis Date = 09/13/22 Pct Recovery = 71% Analysis Date = 09/13/22 Pct Recovery = 71% Analysis Date = 09/08/22 Pct Recovery = 71% Analysis Date = 09/08/22 Pct Recovery = 71% Analysis Date = 09/04/22 Pct Recovery = 71% Analysis Date = 09/04/22 Pct Recovery = 71% Analysis Date = 08/31/22 Pct Recovery = 72% Analysis Date = 08/31/22 Pct Recovery = 72% Analysis Date = 08/26/22 Pct Recovery = 72% Analysis Date = 08/26/22 Pct Recovery = 72% Analysis Date = 08/22/22 Pct Recovery = 72% Analysis Date = 08/22/22 Pct Recovery = 72% Analysis Date = 08/17/22 Pct Recovery = 72% Analysis Date = 08/17/22 Pct Recovery = 72% Analysis Date = 08/13/22 Pct Recovery = 72% Analysis Date = 08/13/22 Pct Recovery = 72% Analysis Date = 08/09/22 Pct Recovery = 72% Analysis Date = 08/09/22 Pct Recovery = 72% Analysis Date = 08/04/22 Pct Recovery = 72% Analysis Date = 08/04/22 Pct Recovery = 72% Analysis Date = 07/31/22 Pct Recovery = 73% Analysis Date = 07/31/22 Pct Recovery = 73% Analysis Date = 07/27/22 Pct Recovery = 73% Analysis Date = 07/27/22 Pct Recovery = 73% Analysis Date = 07/22/22 Pct Recovery = 73% Analysis Date = 07/22/22 Pct Recovery = 73% Analysis Date = 07/18/22 Pct Recovery = 73% Analysis Date = 07/18/22 Pct Recovery = 73% Analysis Date = 07/13/22 Pct Recovery = 73% Analysis Date = 07/13/22 Pct Recovery = 73% Analysis Date = 07/09/22 Pct Recovery = 73% Analysis Date = 07/09/22 Pct Recovery = 73% Analysis Date = 07/05/22 Pct Recovery = 74% Analysis Date = 07/05/22 Pct Recovery = 74% Analysis Date = 06/30/22 Pct Recovery = 74% Analysis Date = 06/30/22 Pct Recovery = 74% Analysis Date = 06/26/22 Pct Recovery = 74% Analysis Date = 06/26/22 Pct Recovery = 74% Analysis Date = 06/21/22 Pct Recovery = 74% Analysis Date = 06/21/22 Pct Recovery = 74% Analysis Date = 06/17/22 Pct Recovery = 75% Analysis Date = 06/17/22 Pct Recovery = 75% Analysis Date = 06/13/22 Pct Recovery = 75% Analysis Date = 06/13/22 Pct Recovery = 75% Analysis Date = 06/08/22 Pct Recovery = 75% Analysis Date = 06/08/22 Pct Recovery = 75% Analysis Date = 06/04/22 Pct Recovery = 75% Analysis Date = 06/04/22 Pct Recovery = 75% Analysis Date = 05/31/22 Pct Recovery = 76% Analysis Date = 05/31/22 Pct Recovery = 76% Analysis Date = 05/26/22 Pct Recovery = 76% Analysis Date = 05/26/22 Pct Recovery = 76% Analysis Date = 05/22/22 Pct Recovery = 76% Analysis Date = 05/22/22 Pct Recovery = 76% Analysis Date = 05/17/22 Pct Recovery = 76% Analysis Date = 05/17/22 Pct Recovery = 76% Analysis Date = 05/13/22 Pct Recovery = 77% Analysis Date = 05/13/22 Pct Recovery = 77% Analysis Date = 05/09/22 Pct Recovery = 77% Analysis Date = 05/09/22 Pct Recovery = 77% Analysis Date = 05/04/22 Pct Recovery = 77% Analysis Date = 05/04/22 Pct Recovery = 77% Analysis Date = 04/30/22 Pct Recovery = 77% Analysis Date = 04/30/22 Pct Recovery = 77% Analysis Date = 04/25/22 Pct Recovery = 78% Analysis Date = 04/25/22 Pct Recovery = 78% Analysis Date = 04/21/22 Pct Recovery = 78% Analysis Date = 04/21/22 Pct Recovery = 78% Analysis Date = 04/17/22 Pct Recovery = 78% Analysis Date = 04/17/22 Pct Recovery = 78% Analysis Date = 04/12/22 Pct Recovery = 78% Analysis Date = 04/12/22 Pct Recovery = 78% Analysis Date = 04/08/22 Pct Recovery = 79% Analysis Date = 04/08/22 Pct Recovery = 79% Analysis Date = 04/04/22 Pct Recovery = 79% Analysis Date = 04/04/22 Pct Recovery = 79% Analysis Date = 03/30/22 Pct Recovery = 79% Analysis Date = 03/30/22 Pct Recovery = 79% Analysis Date = 03/26/22 Pct Recovery = 79% Analysis Date = 03/26/22 Pct Recovery = 79% Analysis Date = 03/21/22 Pct Recovery = 80% Analysis Date = 03/21/22 Pct Recovery = 80% Analysis Date = 03/17/22 Pct Recovery = 80% Analysis Date = 03/17/22 Pct Recovery = 80% Analysis Date = 03/13/22 Pct Recovery = 80% Analysis Date = 03/13/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 81% Analysis Date = 03/04/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/23/22 Pct Recovery = 81% Analysis Date = 02/23/22 Pct Recovery = 81% Analysis Date = 02/19/22 Pct Recovery = 81% Analysis Date = 02/19/22 Pct Recovery = 81% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/01/22 Pct Recovery = 82% Analysis Date = 02/01/22 Pct Recovery = 82% Analysis Date = 01/28/22 Pct Recovery = 83% Analysis Date = 01/28/22 Pct Recovery = 83% Analysis Date = 01/23/22 Pct Recovery = 83% Analysis Date = 01/23/22 Pct Recovery = 83% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 84% Analysis Date = 01/10/22 Pct Recovery = 84% Analysis Date = 01/06/22 Pct Recovery = 84% Analysis Date = 01/06/22 Pct Recovery = 84% Analysis Date = 01/01/22 Pct Recovery = 84% Analysis Date = 01/01/22 Pct Recovery = 84% Analysis Date = 12/28/21 Pct Recovery = 85% Analysis Date = 12/28/21 Pct Recovery = 85% Analysis Date = 12/24/21 Pct Recovery = 85% Analysis Date = 12/24/21 Pct Recovery = 85% Analysis Date = 12/19/21 Pct Recovery = 85% Analysis Date = 12/19/21 Pct Recovery = 85% Analysis Date = 12/15/21 Pct Recovery = 85% Analysis Date = 12/15/21 Pct Recovery = 85% Analysis Date = 12/11/21 Pct Recovery = 86% Analysis Date = 12/11/21 Pct Recovery = 86% Analysis Date = 12/06/21 Pct Recovery = 86% Analysis Date = 12/06/21 Pct Recovery = 86% Analysis Date = 12/02/21 Pct Recovery = 86% Analysis Date = 12/02/21 Pct Recovery = 86% Analysis Date = 11/27/21 Pct Recovery = 86% Analysis Date = 11/27/21 Pct Recovery = 86% Analysis Date = 11/23/21 Pct Recovery = 87% Analysis Date = 11/23/21 Pct Recovery = 87% Analysis Date = 11/19/21 Pct Recovery = 87% Analysis Date = 11/19/21 Pct Recovery = 87% Analysis Date = 11/14/21 Pct Recovery = 87% Analysis Date = 11/14/21 Pct Recovery = 87% Analysis Date = 11/10/21 Pct Recovery = 87% Analysis Date = 11/10/21 Pct Recovery = 87% Analysis Date = 11/05/21 Pct Recovery = 88% Analysis Date = 11/05/21 Pct Recovery = 88% Analysis Date = 11/01/21 Pct Recovery = 88% Analysis Date = 11/01/21 Pct Recovery = 88% Analysis Date = 10/28/21 Pct Recovery = 88% Analysis Date = 10/28/21 Pct Recovery = 88% Analysis Date = 10/23/21 Pct Recovery = 88% Analysis Date = 10/23/21 Pct Recovery = 88% Analysis Date = 10/19/21 Pct Recovery = 89% Analysis Date = 10/19/21 Pct Recovery = 89% Analysis Date = 10/15/21 Pct Recovery = 89% Analysis Date = 10/15/21 Pct Recovery = 89% Analysis Date = 10/10/21 Pct Recovery = 89% Analysis Date = 10/10/21 Pct Recovery = 89% Analysis Date = 10/06/21 Pct Recovery = 89% Analysis Date = 10/06/21 Pct Recovery = 89% Analysis Date = 10/01/21 Pct Recovery = 90% Analysis Date = 10/01/21 Pct Recovery = 90% Analysis Date = 09/27/21 Pct Recovery = 90% Analysis Date = 09/27/21 Pct Recovery = 90% Analysis Date = 09/23/21 Pct Recovery = 90% Analysis Date = 09/23/21 Pct Recovery = 90% Analysis Date = 09/18/21 Pct Recovery = 90% Analysis Date = 09/18/21 Pct Recovery = 90% Analysis Date = 09/14/21 Pct Recovery = 91% Analysis Date = 09/14/21 Pct Recovery = 91% Analysis Date = 09/09/21 Pct Recovery = 91% Analysis Date = 09/09/21 Pct Recovery = 91% Analysis Date = 09/05/21 Pct Recovery = 91% Analysis Date = 09/05/21 Pct Recovery = 91% Analysis Date = 09/01/21 Pct Recovery = 91% Analysis Date = 09/01/21 Pct Recovery = 91% Analysis Date = 08/27/21 Pct Recovery = 92% Analysis Date = 08/27/21 Pct Recovery = 92% Analysis Date = 08/23/21 Pct Recovery = 92% Analysis Date = 08/23/21 Pct Recovery = 92% Analysis Date = 08/19/21 Pct Recovery = 92% Analysis Date = 08/19/21 Pct Recovery = 92% Analysis Date = 08/14/21 Pct Recovery = 92% Analysis Date = 08/14/21 Pct Recovery = 92% Analysis Date = 08/10/21 Pct Recovery = 93% Analysis Date = 08/10/21 Pct Recovery = 93% Analysis Date = 08/05/21 Pct Recovery = 93% Analysis Date = 08/05/21 Pct Recovery = 93% Analysis Date = 08/01/21 Pct Recovery = 93% Analysis Date = 08/01/21 Pct Recovery = 93% Analysis Date = 07/28/21 Pct Recovery = 93% Analysis Date = 07/28/21 Pct Recovery = 93% Analysis Date = 07/23/21 Pct Recovery = 94% Analysis Date = 07/23/21 Pct Recovery = 94% Analysis Date = 07/19/21 Pct Recovery = 94% Analysis Date = 07/19/21 Pct Recovery = 94% Analysis Date = 07/14/21 Pct Recovery = 94% Analysis Date = 07/14/21 Pct Recovery = 94% Analysis Date = 07/10/21 Pct Recovery = 94% Analysis Date = 07/10/21 Pct Recovery = 94% Analysis Date = 07/06/21 Pct Recovery = 95% Analysis Date = 07/06/21 Pct Recovery = 95% Analysis Date = 07/01/21 Pct Recovery = 95% Analysis Date = 07/01/21 Pct Recovery = 95% Analysis Date = 06/27/21 Pct Recovery = 95% Analysis Date = 06/27/21 Pct Recovery = 95% Analysis Date = 06/23/21 Pct Recovery = 96% Analysis Date = 06/23/21 Pct Recovery = 96% Analysis Date = 06/18/21 Pct Recovery = 96% Analysis Date = 06/18/21 Pct Recovery = 96% Analysis Date = 06/14/21 Pct Recovery = 96% Analysis Date = 06/14/21 Pct Recovery = 96% Analysis Date = 06/09/21 Pct Recovery = 96% Analysis Date = 06/09/21 Pct Recovery = 96% Analysis Date = 06/05/21 Pct Recovery = 97% Analysis Date = 06/05/21 Pct Recovery = 97% Analysis Date = 06/01/21 Pct Recovery = 97% Analysis Date = 06/01/21 Pct Recovery = 97% Analysis Date = 05/27/21 Pct Recovery = 97% Analysis Date = 05/27/21 Pct Recovery = 97% Analysis Date = 05/23/21 Pct Recovery = 97% Analysis Date = 05/23/21 Pct Recovery = 97% Analysis Date = 05/18/21 Pct Recovery = 98% Analysis Date = 05/18/21 Pct Recovery = 98% Analysis Date = 05/14/21 Pct Recovery = 98% Analysis Date = 05/14/21 Pct Recovery = 98% Analysis Date = 05/10/21 Pct Recovery = 98% Analysis Date = 05/10/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/01/21 Pct Recovery = 99% Analysis Date = 05/01/21 Pct Recovery = 99% Analysis Date = 04/27/21 Pct Recovery = 99% Analysis Date = 04/27/21 Pct Recovery = 99% Analysis Date = 04/22/21 Pct Recovery = 99% Analysis Date = 04/22/21 Pct Recovery = 99% Analysis Date = 04/18/21 Pct Recovery = 99% Analysis Date = 04/18/21 Pct Recovery = 99% Analysis Date = 04/13/21 Pct Recovery = 100% Analysis Date = 04/13/21 Pct Recovery = 100% Analysis Date = 04/09/21 Pct Recovery = 100% Analysis Date = 04/09/21 Pct Recovery = 100% Analysis Date = 04/05/21 Pct Recovery = 100% Analysis Date = 04/05/21 Pct Recovery = 100% Analysis Date = 03/31/21 Pct Recovery = 100% Analysis Date = 03/31/21 Pct Recovery = 100% Analysis Date = 03/27/21 Pct Recovery = 101% Analysis Date = 03/27/21 Pct Recovery = 101% Analysis Date = 03/22/21 Pct Recovery = 101% Analysis Date = 03/22/21 Pct Recovery = 101% Analysis Date = 03/18/21 Pct Recovery = 101% Analysis Date = 03/18/21 Pct Recovery = 101% Analysis Date = 03/14/21 Pct Recovery = 101% Analysis Date = 03/14/21 Pct Recovery = 101% Analysis Date = 03/09/21 Pct Recovery = 102% Analysis Date = 03/09/21 Pct Recovery = 102% Analysis Date = 03/05/21 Pct Recovery = 102% Analysis Date = 03/05/21 Pct Recovery = 102% Analysis Date = 03/01/21 Pct Recovery = 102% Analysis Date = 03/01/21 Pct Recovery = 102% Analysis Date = 02/24/21 Pct Recovery = 102% Analysis Date = 02/24/21 Pct Recovery = 102% Analysis Date = 02/20/21 Pct Recovery = 103% Analysis Date = 02/20/21 Pct Recovery = 103% Analysis Date = 02/15/21 Pct Recovery = 103% Analysis Date = 02/15/21 Pct Recovery = 103% Analysis Date = 02/11/21 Pct Recovery = 103% Analysis Date = 02/11/21 Pct Recovery = 103% Analysis Date = 02/07/21 Pct Recovery = 103% Analysis Date = 02/07/21 Pct Recovery = 103% Analysis Date = 02/02/21 Pct Recovery = 103% Analysis Date = 02/02/21 Pct Recovery = 103% Analysis Date = 01/29/21 Pct Recovery = 103% Analysis Date = 01/29/21 Pct Recovery = 103% Analysis Date = 01/24/21 Pct Recovery = 103% Analysis Date = 01/24/21 Pct Recovery = 103% Analysis Date = 01/20/21 Pct Recovery = 103% Analysis Date = 01/20/21 Pct Recovery = 103% Analysis Date = 01/16/21 Pct Recovery = 102% Analysis Date = 01/16/21 Pct Recovery = 102% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/25/20 Pct Recovery = 102% Analysis Date = 12/25/20 Pct Recovery = 102% Analysis Date = 12/20/20 Pct Recovery = 102% Analysis Date = 12/20/20 Pct Recovery = 102% Analysis Date = 12/16/20 Pct Recovery = 101% Analysis Date = 12/16/20 Pct Recovery = 101% Analysis Date = 12/12/20 Pct Recovery = 101% Analysis Date = 12/12/20 Pct Recovery = 101% Analysis Date = 12/07/20 Pct Recovery = 101% Analysis Date = 12/07/20 Pct Recovery = 101% Analysis Date = 12/03/20 Pct Recovery = 101% Analysis Date = 12/03/20 Pct Recovery = 101% Analysis Date = 11/28/20 Pct Recovery = 101% Analysis Date = 11/28/20 Pct Recovery = 101% Analysis Date = 11/24/20 Pct Recovery = 101% Analysis Date = 11/24/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 101% Analysis Date = 11/11/20 Pct Recovery = 101% Analysis Date = 11/11/20 Pct Recovery = 101% Analysis Date = 11/07/20 Pct Recovery = 101% Analysis Date = 11/07/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 102% Analysis Date = 11/02/20 Pct Recovery = 102% Analysis Date = 10/29/20 Pct Recovery = 102% Analysis Date = 10/29/20 Pct Recovery = 102% Analysis Date = 10/24/20 Pct Recovery = 103% Analysis Date = 10/24/20 Pct Recovery = 103% Analysis Date = 10/20/20 Pct Recovery = 103% Analysis Date = 10/20/20 Pct Recovery = 103% Analysis Date = 10/16/20 Pct Recovery = 103% Analysis Date = 10/16/20 Pct Recovery = 103% Analysis Date = 10/11/20 Pct Recovery = 104% Analysis Date = 10/11/20 Pct Recovery = 104% Analysis Date = 10/07/20 Pct Recovery = 104% Analysis Date = 10/07/20 Pct Recovery = 104% Analysis Date = 10/02/20 Pct Recovery = 104% Analysis Date = 10/02/20 Pct Recovery = 104% Analysis Date = 09/28/20 Pct Recovery = 104% Analysis Date = 09/28/20 Pct Recovery = 104% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/06/20 Pct Recovery = 104% Analysis Date = 09/06/20 Pct Recovery = 104% Analysis Date = 09/02/20 Pct Recovery = 104% Analysis Date = 09/02/20 Pct Recovery = 104% Analysis Date = 08/28/20 Pct Recovery = 104% Analysis Date = 08/28/20 Pct Recovery = 104% Analysis Date = 08/24/20 Pct Recovery = 104% Analysis Date = 08/24/20 Pct Recovery = 104% Analysis Date = 08/20/20 Pct Recovery = 103% Analysis Date = 08/20/20 Pct Recovery = 103% Analysis Date = 08/15/20 Pct Recovery = 103% Analysis Date = 08/15/20 Pct Recovery = 103% Analysis Date = 08/11/20 Pct Recovery = 103% Analysis Date = 08/11/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 104% Analysis Date = 08/02/20 Pct Recovery = 104% Analysis Date = 07/29/20 Pct Recovery = 104% Analysis Date = 07/29/20 Pct Recovery = 104% Analysis Date = 07/24/20 Pct Recovery = 104% Analysis Date = 07/24/20 Pct Recovery = 104% Analysis Date = 07/20/20 Pct Recovery = 104% Analysis Date = 07/20/20 Pct Recovery = 104% Analysis Date = 07/16/20 Pct Recovery = 105% Analysis Date = 07/16/20 Pct Recovery = 105% Analysis Date = 07/11/20 Pct Recovery = 105% Analysis Date = 07/11/20 Pct Recovery = 105% Analysis Date = 07/07/20 Pct Recovery = 105% Analysis Date = 07/07/20 Pct Recovery = 105% Analysis Date = 07/02/20 Pct Recovery = 105% Analysis Date = 07/02/20 Pct Recovery = 105% Analysis Date = 06/28/20 Pct Recovery = 106% Analysis Date = 06/28/20 Pct Recovery = 106% Analysis Date = 06/24/20 Pct Recovery = 106% Analysis Date = 06/24/20 Pct Recovery = 106% Analysis Date = 06/19/20 Pct Recovery = 106% Analysis Date = 06/19/20 Pct Recovery = 106% Analysis Date = 06/15/20 Pct Recovery = 107% Analysis Date = 06/15/20 Pct Recovery = 107% Analysis Date = 06/10/20 Pct Recovery = 107% Analysis Date = 06/10/20 Pct Recovery = 107% Analysis Date = 06/06/20 Pct Recovery = 107% Analysis Date = 06/06/20 Pct Recovery = 107% Analysis Date = 06/02/20 Pct Recovery = 108% Analysis Date = 06/02/20 Pct Recovery = 108% Analysis Date = 05/28/20 Pct Recovery = 108% Analysis Date = 05/28/20 Pct Recovery = 108% Analysis Date = 05/24/20 Pct Recovery = 108% Analysis Date = 05/24/20 Pct Recovery = 108% Analysis Date = 05/20/20 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-PHENOXYBENZOIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 97% 19% 102% 20%
Total 28 97% 19% 102% 20%

Sample Statistics
3-PHENOXYBENZOIC ACID

Characteristic N % % Basis
Plotted 28 93% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 30 .  
False Negatives 1 3% 1 out of 30
Not Spiked 86 .  
False Positives 0 0% 0 out of 86

OBSP Determination:
4-HYDROXYCHLOROTHALONIL
METHOD: 2447 , TESTIDCODE: 68336LCM60

Laboratory ID = 20201820155 Lab Value = 1260.134 Expected Conc. = 1244.2 Report level label = 42 Pct Recovery = 101% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 1145.638 Expected Conc. = 1244.2 Report level label = 42 Pct Recovery = 92% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 1520.620 Expected Conc. = 1228.3 Report level label = 42 Pct Recovery = 124% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20222640086 Lab Value = 937.279 Expected Conc. = 1154 Report level label = 42 Pct Recovery = 81% Analysis Date = 09/30/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20221940195 Lab Value = 871.863 Expected Conc. = 1149.4 Report level label = 42 Pct Recovery = 76% Analysis Date = 07/21/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20222010133 Lab Value = 261.065 Expected Conc. = 1140 Report level label = 42 Pct Recovery = 23% Analysis Date = 07/22/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20221870197 Lab Value = 355.837 Expected Conc. = 712.5 Report level label = 42 Pct Recovery = 50% Analysis Date = 07/14/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20221730293 Lab Value = 369.690 Expected Conc. = 712.5 Report level label = 42 Pct Recovery = 52% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20202530029 Lab Value = 556.965 Expected Conc. = 622.1 Report level label = 42 Pct Recovery = 90% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 545.882 Expected Conc. = 622.1 Report level label = 42 Pct Recovery = 88% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 751.109 Expected Conc. = 622.1 Report level label = 42 Pct Recovery = 121% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201960104 Lab Value = 670.990 Expected Conc. = 614.15 Report level label = 42 Pct Recovery = 109% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202590107 Lab Value = 561.644 Expected Conc. = 534 Report level label = 42 Pct Recovery = 105% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 512.642 Expected Conc. = 534 Report level label = 42 Pct Recovery = 96% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 493.176 Expected Conc. = 526.4 Report level label = 42 Pct Recovery = 94% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 543.819 Expected Conc. = 526.4 Report level label = 42 Pct Recovery = 103% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222500483 Lab Value = 139.825 Expected Conc. = 285 Report level label = 42 Pct Recovery = 49% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Laboratory ID = 20203360042 Lab Value = 227.932 Expected Conc. = 267 Report level label = 42 Pct Recovery = 85% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 239.272 Expected Conc. = 267 Report level label = 42 Pct Recovery = 90% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 286.208 Expected Conc. = 267 Report level label = 42 Pct Recovery = 107% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202180001 Lab Value = 215.538 Expected Conc. = 248.84 Report level label = 42 Pct Recovery = 87% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 281.671 Expected Conc. = 248.84 Report level label = 42 Pct Recovery = 113% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 233.158 Expected Conc. = 248.84 Report level label = 42 Pct Recovery = 94% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201610160 Lab Value = 270.379 Expected Conc. = 245.66 Report level label = 42 Pct Recovery = 110% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210970035 Lab Value = 105.415 Expected Conc. = 106.8 Report level label = 42 Pct Recovery = 99% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 87.595 Expected Conc. = 106.8 Report level label = 42 Pct Recovery = 82% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 100.983 Expected Conc. = 106.8 Report level label = 42 Pct Recovery = 95% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 102.403 Expected Conc. = 106.8 Report level label = 42 Pct Recovery = 96% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 93.007 Expected Conc. = 106.8 Report level label = 42 Pct Recovery = 87% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 150.512 Expected Conc. = 106.8 Report level label = 42 Pct Recovery = 141% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210830019 Lab Value = 44.425 Expected Conc. = 105.28 Report level label = 42 Pct Recovery = 42% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 98.491 Expected Conc. = 105.28 Report level label = 42 Pct Recovery = 94% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 10/13/22 Pct Recovery = 54% Analysis Date = 10/09/22 Pct Recovery = 54% Analysis Date = 10/09/22 Pct Recovery = 54% Analysis Date = 10/05/22 Pct Recovery = 54% Analysis Date = 10/05/22 Pct Recovery = 54% Analysis Date = 09/30/22 Pct Recovery = 54% Analysis Date = 09/30/22 Pct Recovery = 54% Analysis Date = 09/26/22 Pct Recovery = 54% Analysis Date = 09/26/22 Pct Recovery = 54% Analysis Date = 09/22/22 Pct Recovery = 54% Analysis Date = 09/22/22 Pct Recovery = 54% Analysis Date = 09/17/22 Pct Recovery = 55% Analysis Date = 09/17/22 Pct Recovery = 55% Analysis Date = 09/13/22 Pct Recovery = 55% Analysis Date = 09/13/22 Pct Recovery = 55% Analysis Date = 09/08/22 Pct Recovery = 55% Analysis Date = 09/08/22 Pct Recovery = 55% Analysis Date = 09/04/22 Pct Recovery = 55% Analysis Date = 09/04/22 Pct Recovery = 55% Analysis Date = 08/31/22 Pct Recovery = 55% Analysis Date = 08/31/22 Pct Recovery = 55% Analysis Date = 08/26/22 Pct Recovery = 55% Analysis Date = 08/26/22 Pct Recovery = 55% Analysis Date = 08/22/22 Pct Recovery = 55% Analysis Date = 08/22/22 Pct Recovery = 55% Analysis Date = 08/17/22 Pct Recovery = 56% Analysis Date = 08/17/22 Pct Recovery = 56% Analysis Date = 08/13/22 Pct Recovery = 56% Analysis Date = 08/13/22 Pct Recovery = 56% Analysis Date = 08/09/22 Pct Recovery = 56% Analysis Date = 08/09/22 Pct Recovery = 56% Analysis Date = 08/04/22 Pct Recovery = 56% Analysis Date = 08/04/22 Pct Recovery = 56% Analysis Date = 07/31/22 Pct Recovery = 56% Analysis Date = 07/31/22 Pct Recovery = 56% Analysis Date = 07/27/22 Pct Recovery = 56% Analysis Date = 07/27/22 Pct Recovery = 56% Analysis Date = 07/22/22 Pct Recovery = 56% Analysis Date = 07/22/22 Pct Recovery = 56% Analysis Date = 07/18/22 Pct Recovery = 57% Analysis Date = 07/18/22 Pct Recovery = 57% Analysis Date = 07/13/22 Pct Recovery = 57% Analysis Date = 07/13/22 Pct Recovery = 57% Analysis Date = 07/09/22 Pct Recovery = 57% Analysis Date = 07/09/22 Pct Recovery = 57% Analysis Date = 07/05/22 Pct Recovery = 57% Analysis Date = 07/05/22 Pct Recovery = 57% Analysis Date = 06/30/22 Pct Recovery = 57% Analysis Date = 06/30/22 Pct Recovery = 57% Analysis Date = 06/26/22 Pct Recovery = 57% Analysis Date = 06/26/22 Pct Recovery = 57% Analysis Date = 06/21/22 Pct Recovery = 57% Analysis Date = 06/21/22 Pct Recovery = 57% Analysis Date = 06/17/22 Pct Recovery = 58% Analysis Date = 06/17/22 Pct Recovery = 58% Analysis Date = 06/13/22 Pct Recovery = 58% Analysis Date = 06/13/22 Pct Recovery = 58% Analysis Date = 06/08/22 Pct Recovery = 58% Analysis Date = 06/08/22 Pct Recovery = 58% Analysis Date = 06/04/22 Pct Recovery = 58% Analysis Date = 06/04/22 Pct Recovery = 58% Analysis Date = 05/31/22 Pct Recovery = 58% Analysis Date = 05/31/22 Pct Recovery = 58% Analysis Date = 05/26/22 Pct Recovery = 58% Analysis Date = 05/26/22 Pct Recovery = 58% Analysis Date = 05/22/22 Pct Recovery = 58% Analysis Date = 05/22/22 Pct Recovery = 58% Analysis Date = 05/17/22 Pct Recovery = 59% Analysis Date = 05/17/22 Pct Recovery = 59% Analysis Date = 05/13/22 Pct Recovery = 59% Analysis Date = 05/13/22 Pct Recovery = 59% Analysis Date = 05/09/22 Pct Recovery = 59% Analysis Date = 05/09/22 Pct Recovery = 59% Analysis Date = 05/04/22 Pct Recovery = 59% Analysis Date = 05/04/22 Pct Recovery = 59% Analysis Date = 04/30/22 Pct Recovery = 59% Analysis Date = 04/30/22 Pct Recovery = 59% Analysis Date = 04/25/22 Pct Recovery = 59% Analysis Date = 04/25/22 Pct Recovery = 59% Analysis Date = 04/21/22 Pct Recovery = 59% Analysis Date = 04/21/22 Pct Recovery = 59% Analysis Date = 04/17/22 Pct Recovery = 60% Analysis Date = 04/17/22 Pct Recovery = 60% Analysis Date = 04/12/22 Pct Recovery = 60% Analysis Date = 04/12/22 Pct Recovery = 60% Analysis Date = 04/08/22 Pct Recovery = 60% Analysis Date = 04/08/22 Pct Recovery = 60% Analysis Date = 04/04/22 Pct Recovery = 60% Analysis Date = 04/04/22 Pct Recovery = 60% Analysis Date = 03/30/22 Pct Recovery = 60% Analysis Date = 03/30/22 Pct Recovery = 60% Analysis Date = 03/26/22 Pct Recovery = 60% Analysis Date = 03/26/22 Pct Recovery = 60% Analysis Date = 03/21/22 Pct Recovery = 60% Analysis Date = 03/21/22 Pct Recovery = 60% Analysis Date = 03/17/22 Pct Recovery = 61% Analysis Date = 03/17/22 Pct Recovery = 61% Analysis Date = 03/13/22 Pct Recovery = 61% Analysis Date = 03/13/22 Pct Recovery = 61% Analysis Date = 03/08/22 Pct Recovery = 61% Analysis Date = 03/08/22 Pct Recovery = 61% Analysis Date = 03/04/22 Pct Recovery = 61% Analysis Date = 03/04/22 Pct Recovery = 61% Analysis Date = 02/27/22 Pct Recovery = 61% Analysis Date = 02/27/22 Pct Recovery = 61% Analysis Date = 02/23/22 Pct Recovery = 61% Analysis Date = 02/23/22 Pct Recovery = 61% Analysis Date = 02/19/22 Pct Recovery = 61% Analysis Date = 02/19/22 Pct Recovery = 61% Analysis Date = 02/14/22 Pct Recovery = 62% Analysis Date = 02/14/22 Pct Recovery = 62% Analysis Date = 02/10/22 Pct Recovery = 62% Analysis Date = 02/10/22 Pct Recovery = 62% Analysis Date = 02/06/22 Pct Recovery = 62% Analysis Date = 02/06/22 Pct Recovery = 62% Analysis Date = 02/01/22 Pct Recovery = 62% Analysis Date = 02/01/22 Pct Recovery = 62% Analysis Date = 01/28/22 Pct Recovery = 62% Analysis Date = 01/28/22 Pct Recovery = 62% Analysis Date = 01/23/22 Pct Recovery = 62% Analysis Date = 01/23/22 Pct Recovery = 62% Analysis Date = 01/19/22 Pct Recovery = 63% Analysis Date = 01/19/22 Pct Recovery = 63% Analysis Date = 01/15/22 Pct Recovery = 63% Analysis Date = 01/15/22 Pct Recovery = 63% Analysis Date = 01/10/22 Pct Recovery = 63% Analysis Date = 01/10/22 Pct Recovery = 63% Analysis Date = 01/06/22 Pct Recovery = 63% Analysis Date = 01/06/22 Pct Recovery = 63% Analysis Date = 01/01/22 Pct Recovery = 63% Analysis Date = 01/01/22 Pct Recovery = 63% Analysis Date = 12/28/21 Pct Recovery = 63% Analysis Date = 12/28/21 Pct Recovery = 63% Analysis Date = 12/24/21 Pct Recovery = 63% Analysis Date = 12/24/21 Pct Recovery = 63% Analysis Date = 12/19/21 Pct Recovery = 64% Analysis Date = 12/19/21 Pct Recovery = 64% Analysis Date = 12/15/21 Pct Recovery = 64% Analysis Date = 12/15/21 Pct Recovery = 64% Analysis Date = 12/11/21 Pct Recovery = 64% Analysis Date = 12/11/21 Pct Recovery = 64% Analysis Date = 12/06/21 Pct Recovery = 64% Analysis Date = 12/06/21 Pct Recovery = 64% Analysis Date = 12/02/21 Pct Recovery = 64% Analysis Date = 12/02/21 Pct Recovery = 64% Analysis Date = 11/27/21 Pct Recovery = 64% Analysis Date = 11/27/21 Pct Recovery = 64% Analysis Date = 11/23/21 Pct Recovery = 64% Analysis Date = 11/23/21 Pct Recovery = 64% Analysis Date = 11/19/21 Pct Recovery = 65% Analysis Date = 11/19/21 Pct Recovery = 65% Analysis Date = 11/14/21 Pct Recovery = 65% Analysis Date = 11/14/21 Pct Recovery = 65% Analysis Date = 11/10/21 Pct Recovery = 65% Analysis Date = 11/10/21 Pct Recovery = 65% Analysis Date = 11/05/21 Pct Recovery = 65% Analysis Date = 11/05/21 Pct Recovery = 65% Analysis Date = 11/01/21 Pct Recovery = 65% Analysis Date = 11/01/21 Pct Recovery = 65% Analysis Date = 10/28/21 Pct Recovery = 65% Analysis Date = 10/28/21 Pct Recovery = 65% Analysis Date = 10/23/21 Pct Recovery = 65% Analysis Date = 10/23/21 Pct Recovery = 65% Analysis Date = 10/19/21 Pct Recovery = 66% Analysis Date = 10/19/21 Pct Recovery = 66% Analysis Date = 10/15/21 Pct Recovery = 66% Analysis Date = 10/15/21 Pct Recovery = 66% Analysis Date = 10/10/21 Pct Recovery = 66% Analysis Date = 10/10/21 Pct Recovery = 66% Analysis Date = 10/06/21 Pct Recovery = 66% Analysis Date = 10/06/21 Pct Recovery = 66% Analysis Date = 10/01/21 Pct Recovery = 66% Analysis Date = 10/01/21 Pct Recovery = 66% Analysis Date = 09/27/21 Pct Recovery = 66% Analysis Date = 09/27/21 Pct Recovery = 66% Analysis Date = 09/23/21 Pct Recovery = 66% Analysis Date = 09/23/21 Pct Recovery = 66% Analysis Date = 09/18/21 Pct Recovery = 67% Analysis Date = 09/18/21 Pct Recovery = 67% Analysis Date = 09/14/21 Pct Recovery = 67% Analysis Date = 09/14/21 Pct Recovery = 67% Analysis Date = 09/09/21 Pct Recovery = 67% Analysis Date = 09/09/21 Pct Recovery = 67% Analysis Date = 09/05/21 Pct Recovery = 67% Analysis Date = 09/05/21 Pct Recovery = 67% Analysis Date = 09/01/21 Pct Recovery = 67% Analysis Date = 09/01/21 Pct Recovery = 67% Analysis Date = 08/27/21 Pct Recovery = 67% Analysis Date = 08/27/21 Pct Recovery = 67% Analysis Date = 08/23/21 Pct Recovery = 67% Analysis Date = 08/23/21 Pct Recovery = 67% Analysis Date = 08/19/21 Pct Recovery = 68% Analysis Date = 08/19/21 Pct Recovery = 68% Analysis Date = 08/14/21 Pct Recovery = 68% Analysis Date = 08/14/21 Pct Recovery = 68% Analysis Date = 08/10/21 Pct Recovery = 68% Analysis Date = 08/10/21 Pct Recovery = 68% Analysis Date = 08/05/21 Pct Recovery = 68% Analysis Date = 08/05/21 Pct Recovery = 68% Analysis Date = 08/01/21 Pct Recovery = 68% Analysis Date = 08/01/21 Pct Recovery = 68% Analysis Date = 07/28/21 Pct Recovery = 68% Analysis Date = 07/28/21 Pct Recovery = 68% Analysis Date = 07/23/21 Pct Recovery = 68% Analysis Date = 07/23/21 Pct Recovery = 68% Analysis Date = 07/19/21 Pct Recovery = 69% Analysis Date = 07/19/21 Pct Recovery = 69% Analysis Date = 07/14/21 Pct Recovery = 69% Analysis Date = 07/14/21 Pct Recovery = 69% Analysis Date = 07/10/21 Pct Recovery = 69% Analysis Date = 07/10/21 Pct Recovery = 69% Analysis Date = 07/06/21 Pct Recovery = 69% Analysis Date = 07/06/21 Pct Recovery = 69% Analysis Date = 07/01/21 Pct Recovery = 69% Analysis Date = 07/01/21 Pct Recovery = 69% Analysis Date = 06/27/21 Pct Recovery = 69% Analysis Date = 06/27/21 Pct Recovery = 69% Analysis Date = 06/23/21 Pct Recovery = 69% Analysis Date = 06/23/21 Pct Recovery = 69% Analysis Date = 06/18/21 Pct Recovery = 70% Analysis Date = 06/18/21 Pct Recovery = 70% Analysis Date = 06/14/21 Pct Recovery = 70% Analysis Date = 06/14/21 Pct Recovery = 70% Analysis Date = 06/09/21 Pct Recovery = 70% Analysis Date = 06/09/21 Pct Recovery = 70% Analysis Date = 06/05/21 Pct Recovery = 70% Analysis Date = 06/05/21 Pct Recovery = 70% Analysis Date = 06/01/21 Pct Recovery = 70% Analysis Date = 06/01/21 Pct Recovery = 70% Analysis Date = 05/27/21 Pct Recovery = 70% Analysis Date = 05/27/21 Pct Recovery = 70% Analysis Date = 05/23/21 Pct Recovery = 71% Analysis Date = 05/23/21 Pct Recovery = 71% Analysis Date = 05/18/21 Pct Recovery = 71% Analysis Date = 05/18/21 Pct Recovery = 71% Analysis Date = 05/14/21 Pct Recovery = 71% Analysis Date = 05/14/21 Pct Recovery = 71% Analysis Date = 05/10/21 Pct Recovery = 71% Analysis Date = 05/10/21 Pct Recovery = 71% Analysis Date = 05/05/21 Pct Recovery = 71% Analysis Date = 05/05/21 Pct Recovery = 71% Analysis Date = 05/01/21 Pct Recovery = 71% Analysis Date = 05/01/21 Pct Recovery = 71% Analysis Date = 04/27/21 Pct Recovery = 71% Analysis Date = 04/27/21 Pct Recovery = 71% Analysis Date = 04/22/21 Pct Recovery = 72% Analysis Date = 04/22/21 Pct Recovery = 72% Analysis Date = 04/18/21 Pct Recovery = 72% Analysis Date = 04/18/21 Pct Recovery = 72% Analysis Date = 04/13/21 Pct Recovery = 72% Analysis Date = 04/13/21 Pct Recovery = 72% Analysis Date = 04/09/21 Pct Recovery = 73% Analysis Date = 04/09/21 Pct Recovery = 73% Analysis Date = 04/05/21 Pct Recovery = 74% Analysis Date = 04/05/21 Pct Recovery = 74% Analysis Date = 03/31/21 Pct Recovery = 74% Analysis Date = 03/31/21 Pct Recovery = 74% Analysis Date = 03/27/21 Pct Recovery = 75% Analysis Date = 03/27/21 Pct Recovery = 75% Analysis Date = 03/22/21 Pct Recovery = 76% Analysis Date = 03/22/21 Pct Recovery = 76% Analysis Date = 03/18/21 Pct Recovery = 77% Analysis Date = 03/18/21 Pct Recovery = 77% Analysis Date = 03/14/21 Pct Recovery = 77% Analysis Date = 03/14/21 Pct Recovery = 77% Analysis Date = 03/09/21 Pct Recovery = 78% Analysis Date = 03/09/21 Pct Recovery = 78% Analysis Date = 03/05/21 Pct Recovery = 79% Analysis Date = 03/05/21 Pct Recovery = 79% Analysis Date = 03/01/21 Pct Recovery = 80% Analysis Date = 03/01/21 Pct Recovery = 80% Analysis Date = 02/24/21 Pct Recovery = 80% Analysis Date = 02/24/21 Pct Recovery = 80% Analysis Date = 02/20/21 Pct Recovery = 81% Analysis Date = 02/20/21 Pct Recovery = 81% Analysis Date = 02/15/21 Pct Recovery = 82% Analysis Date = 02/15/21 Pct Recovery = 82% Analysis Date = 02/11/21 Pct Recovery = 83% Analysis Date = 02/11/21 Pct Recovery = 83% Analysis Date = 02/07/21 Pct Recovery = 84% Analysis Date = 02/07/21 Pct Recovery = 84% Analysis Date = 02/02/21 Pct Recovery = 84% Analysis Date = 02/02/21 Pct Recovery = 84% Analysis Date = 01/29/21 Pct Recovery = 85% Analysis Date = 01/29/21 Pct Recovery = 85% Analysis Date = 01/24/21 Pct Recovery = 86% Analysis Date = 01/24/21 Pct Recovery = 86% Analysis Date = 01/20/21 Pct Recovery = 87% Analysis Date = 01/20/21 Pct Recovery = 87% Analysis Date = 01/16/21 Pct Recovery = 88% Analysis Date = 01/16/21 Pct Recovery = 88% Analysis Date = 01/11/21 Pct Recovery = 88% Analysis Date = 01/11/21 Pct Recovery = 88% Analysis Date = 01/07/21 Pct Recovery = 89% Analysis Date = 01/07/21 Pct Recovery = 89% Analysis Date = 01/03/21 Pct Recovery = 90% Analysis Date = 01/03/21 Pct Recovery = 90% Analysis Date = 12/29/20 Pct Recovery = 91% Analysis Date = 12/29/20 Pct Recovery = 91% Analysis Date = 12/25/20 Pct Recovery = 92% Analysis Date = 12/25/20 Pct Recovery = 92% Analysis Date = 12/20/20 Pct Recovery = 93% Analysis Date = 12/20/20 Pct Recovery = 93% Analysis Date = 12/16/20 Pct Recovery = 94% Analysis Date = 12/16/20 Pct Recovery = 94% Analysis Date = 12/12/20 Pct Recovery = 95% Analysis Date = 12/12/20 Pct Recovery = 95% Analysis Date = 12/07/20 Pct Recovery = 96% Analysis Date = 12/07/20 Pct Recovery = 96% Analysis Date = 12/03/20 Pct Recovery = 96% Analysis Date = 12/03/20 Pct Recovery = 96% Analysis Date = 11/28/20 Pct Recovery = 97% Analysis Date = 11/28/20 Pct Recovery = 97% Analysis Date = 11/24/20 Pct Recovery = 98% Analysis Date = 11/24/20 Pct Recovery = 98% Analysis Date = 11/20/20 Pct Recovery = 98% Analysis Date = 11/20/20 Pct Recovery = 98% Analysis Date = 11/15/20 Pct Recovery = 99% Analysis Date = 11/15/20 Pct Recovery = 99% Analysis Date = 11/11/20 Pct Recovery = 100% Analysis Date = 11/11/20 Pct Recovery = 100% Analysis Date = 11/07/20 Pct Recovery = 100% Analysis Date = 11/07/20 Pct Recovery = 100% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/24/20 Pct Recovery = 101% Analysis Date = 10/24/20 Pct Recovery = 101% Analysis Date = 10/20/20 Pct Recovery = 101% Analysis Date = 10/20/20 Pct Recovery = 101% Analysis Date = 10/16/20 Pct Recovery = 102% Analysis Date = 10/16/20 Pct Recovery = 102% Analysis Date = 10/11/20 Pct Recovery = 102% Analysis Date = 10/11/20 Pct Recovery = 102% Analysis Date = 10/07/20 Pct Recovery = 103% Analysis Date = 10/07/20 Pct Recovery = 103% Analysis Date = 10/02/20 Pct Recovery = 103% Analysis Date = 10/02/20 Pct Recovery = 103% Analysis Date = 09/28/20 Pct Recovery = 103% Analysis Date = 09/28/20 Pct Recovery = 103% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/19/20 Pct Recovery = 104% Analysis Date = 09/19/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/06/20 Pct Recovery = 103% Analysis Date = 09/06/20 Pct Recovery = 103% Analysis Date = 09/02/20 Pct Recovery = 103% Analysis Date = 09/02/20 Pct Recovery = 103% Analysis Date = 08/28/20 Pct Recovery = 103% Analysis Date = 08/28/20 Pct Recovery = 103% Analysis Date = 08/24/20 Pct Recovery = 103% Analysis Date = 08/24/20 Pct Recovery = 103% Analysis Date = 08/20/20 Pct Recovery = 103% Analysis Date = 08/20/20 Pct Recovery = 103% Analysis Date = 08/15/20 Pct Recovery = 103% Analysis Date = 08/15/20 Pct Recovery = 103% Analysis Date = 08/11/20 Pct Recovery = 103% Analysis Date = 08/11/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 103% Analysis Date = 07/29/20 Pct Recovery = 103% Analysis Date = 07/29/20 Pct Recovery = 103% Analysis Date = 07/24/20 Pct Recovery = 103% Analysis Date = 07/24/20 Pct Recovery = 103% Analysis Date = 07/20/20 Pct Recovery = 103% Analysis Date = 07/20/20 Pct Recovery = 103% Analysis Date = 07/16/20 Pct Recovery = 103% Analysis Date = 07/16/20 Pct Recovery = 103% Analysis Date = 07/11/20 Pct Recovery = 103% Analysis Date = 07/11/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/02/20 Pct Recovery = 103% Analysis Date = 07/02/20 Pct Recovery = 103% Analysis Date = 06/28/20 Pct Recovery = 104% Analysis Date = 06/28/20 Pct Recovery = 104% Analysis Date = 06/24/20 Pct Recovery = 104% Analysis Date = 06/24/20 Pct Recovery = 104% Analysis Date = 06/19/20 Pct Recovery = 104% Analysis Date = 06/19/20 Pct Recovery = 104% Analysis Date = 06/15/20 Pct Recovery = 104% Analysis Date = 06/15/20 Pct Recovery = 104% Analysis Date = 06/10/20 Pct Recovery = 104% Analysis Date = 06/10/20 Pct Recovery = 104% Analysis Date = 06/06/20 Pct Recovery = 104% Analysis Date = 06/06/20 Pct Recovery = 104% Analysis Date = 06/02/20 Pct Recovery = 104% Analysis Date = 06/02/20 Pct Recovery = 104% Analysis Date = 05/28/20 Pct Recovery = 104% Analysis Date = 05/28/20 Pct Recovery = 104% Analysis Date = 05/24/20 Pct Recovery = 105% Analysis Date = 05/24/20 Pct Recovery = 105% Analysis Date = 05/20/20 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-HYDROXYCHLOROTHALONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 90% 25% 94% 15%
Total 32 90% 25% 94% 15%

Sample Statistics
4-HYDROXYCHLOROTHALONIL

Characteristic N % % Basis
Plotted 32 94% Spiked
Estimated Values 32 94% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 2 6% 2 out of 34
Not Spiked 82 .  
False Positives 0 0% 0 out of 80

OBSP Determination:
ACEPHATE (ORTHENE)
METHOD: 2447 , TESTIDCODE: 68519LCM60

Laboratory ID = 20202110006 Lab Value = 117.129 Expected Conc. = 126.6 Report level label = 10 Pct Recovery = 93% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203230021 Lab Value = 100.690 Expected Conc. = 125.2 Report level label = 10 Pct Recovery = 80% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 96.242 Expected Conc. = 125.2 Report level label = 10 Pct Recovery = 77% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 113.795 Expected Conc. = 125.2 Report level label = 10 Pct Recovery = 91% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 113.736 Expected Conc. = 125.2 Report level label = 10 Pct Recovery = 91% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201820155 Lab Value = 115.362 Expected Conc. = 125.1 Report level label = 10 Pct Recovery = 92% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20212990174 Lab Value = 61.811 Expected Conc. = 101.44 Report level label = 10 Pct Recovery = 61% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 61.355 Expected Conc. = 101.12 Report level label = 10 Pct Recovery = 61% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 65.705 Expected Conc. = 101.12 Report level label = 10 Pct Recovery = 65% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20220810134 Lab Value = 94.806 Expected Conc. = 100.4 Report level label = 10 Pct Recovery = 94% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222010132 Lab Value = 51.771 Expected Conc. = 100 Report level label = 10 Pct Recovery = 52% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20222150193 Lab Value = 56.667 Expected Conc. = 98.8 Report level label = 10 Pct Recovery = 57% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20213340027 Lab Value = 46.029 Expected Conc. = 63.4 Report level label = 10 Pct Recovery = 73% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 120.405 Expected Conc. = 63.4 Report level label = 10 Pct Recovery = 190% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 37.786 Expected Conc. = 63.4 Report level label = 10 Pct Recovery = 60% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20201680155 Lab Value = 68.277 Expected Conc. = 63.3 Report level label = 10 Pct Recovery = 108% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20221730293 Lab Value = 41.000 Expected Conc. = 63.2 Report level label = 10 Pct Recovery = 65% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 37.725 Expected Conc. = 63.2 Report level label = 10 Pct Recovery = 60% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220810133 Lab Value = 64.165 Expected Conc. = 62.75 Report level label = 10 Pct Recovery = 102% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20203230018 Lab Value = 50.782 Expected Conc. = 62.6 Report level label = 10 Pct Recovery = 81% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 56.535 Expected Conc. = 62.6 Report level label = 10 Pct Recovery = 90% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 58.817 Expected Conc. = 62.6 Report level label = 10 Pct Recovery = 94% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 55.190 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 88% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 51.668 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 83% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 46.152 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 74% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20213060210 Lab Value = 11.647 Expected Conc. = 25.36 Report level label = 10 Pct Recovery = 46% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20201610160 Lab Value = 26.568 Expected Conc. = 25.32 Report level label = 10 Pct Recovery = 105% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20222500483 Lab Value = 20.738 Expected Conc. = 25.28 Report level label = 10 Pct Recovery = 82% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20222630205 Lab Value = 18.573 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 74% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210970035 Lab Value = 22.071 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 88% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210830019 Lab Value = 24.462 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 98% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 25.161 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 100% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210340007 Lab Value = 21.383 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 85% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 26.955 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 108% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 19.273 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 77% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 24.589 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 98% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 28.004 Expected Conc. = 25.04 Report level label = 10 Pct Recovery = 112% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 20.225 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 81% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 27.763 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 111% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 36.018 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 144% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 22.119 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 88% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Analysis Date = 09/28/22 Pct Recovery = 68% Analysis Date = 09/24/22 Pct Recovery = 68% Analysis Date = 09/24/22 Pct Recovery = 68% Analysis Date = 09/20/22 Pct Recovery = 68% Analysis Date = 09/20/22 Pct Recovery = 68% Analysis Date = 09/16/22 Pct Recovery = 69% Analysis Date = 09/16/22 Pct Recovery = 69% Analysis Date = 09/11/22 Pct Recovery = 69% Analysis Date = 09/11/22 Pct Recovery = 69% Analysis Date = 09/07/22 Pct Recovery = 69% Analysis Date = 09/07/22 Pct Recovery = 69% Analysis Date = 09/03/22 Pct Recovery = 69% Analysis Date = 09/03/22 Pct Recovery = 69% Analysis Date = 08/29/22 Pct Recovery = 69% Analysis Date = 08/29/22 Pct Recovery = 69% Analysis Date = 08/25/22 Pct Recovery = 69% Analysis Date = 08/25/22 Pct Recovery = 69% Analysis Date = 08/21/22 Pct Recovery = 70% Analysis Date = 08/21/22 Pct Recovery = 70% Analysis Date = 08/16/22 Pct Recovery = 70% Analysis Date = 08/16/22 Pct Recovery = 70% Analysis Date = 08/12/22 Pct Recovery = 70% Analysis Date = 08/12/22 Pct Recovery = 70% Analysis Date = 08/08/22 Pct Recovery = 70% Analysis Date = 08/08/22 Pct Recovery = 70% Analysis Date = 08/03/22 Pct Recovery = 70% Analysis Date = 08/03/22 Pct Recovery = 70% Analysis Date = 07/30/22 Pct Recovery = 71% Analysis Date = 07/30/22 Pct Recovery = 71% Analysis Date = 07/26/22 Pct Recovery = 71% Analysis Date = 07/26/22 Pct Recovery = 71% Analysis Date = 07/21/22 Pct Recovery = 71% Analysis Date = 07/21/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/04/22 Pct Recovery = 72% Analysis Date = 07/04/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/21/22 Pct Recovery = 72% Analysis Date = 06/21/22 Pct Recovery = 72% Analysis Date = 06/17/22 Pct Recovery = 72% Analysis Date = 06/17/22 Pct Recovery = 72% Analysis Date = 06/13/22 Pct Recovery = 72% Analysis Date = 06/13/22 Pct Recovery = 72% Analysis Date = 06/08/22 Pct Recovery = 73% Analysis Date = 06/08/22 Pct Recovery = 73% Analysis Date = 06/04/22 Pct Recovery = 73% Analysis Date = 06/04/22 Pct Recovery = 73% Analysis Date = 05/31/22 Pct Recovery = 73% Analysis Date = 05/31/22 Pct Recovery = 73% Analysis Date = 05/26/22 Pct Recovery = 73% Analysis Date = 05/26/22 Pct Recovery = 73% Analysis Date = 05/22/22 Pct Recovery = 73% Analysis Date = 05/22/22 Pct Recovery = 73% Analysis Date = 05/18/22 Pct Recovery = 74% Analysis Date = 05/18/22 Pct Recovery = 74% Analysis Date = 05/13/22 Pct Recovery = 74% Analysis Date = 05/13/22 Pct Recovery = 74% Analysis Date = 05/09/22 Pct Recovery = 74% Analysis Date = 05/09/22 Pct Recovery = 74% Analysis Date = 05/05/22 Pct Recovery = 74% Analysis Date = 05/05/22 Pct Recovery = 74% Analysis Date = 04/30/22 Pct Recovery = 74% Analysis Date = 04/30/22 Pct Recovery = 74% Analysis Date = 04/26/22 Pct Recovery = 74% Analysis Date = 04/26/22 Pct Recovery = 74% Analysis Date = 04/22/22 Pct Recovery = 75% Analysis Date = 04/22/22 Pct Recovery = 75% Analysis Date = 04/18/22 Pct Recovery = 75% Analysis Date = 04/18/22 Pct Recovery = 75% Analysis Date = 04/13/22 Pct Recovery = 75% Analysis Date = 04/13/22 Pct Recovery = 75% Analysis Date = 04/09/22 Pct Recovery = 75% Analysis Date = 04/09/22 Pct Recovery = 75% Analysis Date = 04/05/22 Pct Recovery = 75% Analysis Date = 04/05/22 Pct Recovery = 75% Analysis Date = 03/31/22 Pct Recovery = 75% Analysis Date = 03/31/22 Pct Recovery = 75% Analysis Date = 03/27/22 Pct Recovery = 76% Analysis Date = 03/27/22 Pct Recovery = 76% Analysis Date = 03/23/22 Pct Recovery = 76% Analysis Date = 03/23/22 Pct Recovery = 76% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/05/22 Pct Recovery = 77% Analysis Date = 03/05/22 Pct Recovery = 77% Analysis Date = 03/01/22 Pct Recovery = 77% Analysis Date = 03/01/22 Pct Recovery = 77% Analysis Date = 02/25/22 Pct Recovery = 77% Analysis Date = 02/25/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 77% Analysis Date = 02/12/22 Pct Recovery = 77% Analysis Date = 02/12/22 Pct Recovery = 77% Analysis Date = 02/07/22 Pct Recovery = 78% Analysis Date = 02/07/22 Pct Recovery = 78% Analysis Date = 02/03/22 Pct Recovery = 78% Analysis Date = 02/03/22 Pct Recovery = 78% Analysis Date = 01/30/22 Pct Recovery = 78% Analysis Date = 01/30/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/21/22 Pct Recovery = 78% Analysis Date = 01/21/22 Pct Recovery = 78% Analysis Date = 01/17/22 Pct Recovery = 79% Analysis Date = 01/17/22 Pct Recovery = 79% Analysis Date = 01/13/22 Pct Recovery = 79% Analysis Date = 01/13/22 Pct Recovery = 79% Analysis Date = 01/08/22 Pct Recovery = 79% Analysis Date = 01/08/22 Pct Recovery = 79% Analysis Date = 01/04/22 Pct Recovery = 79% Analysis Date = 01/04/22 Pct Recovery = 79% Analysis Date = 12/31/21 Pct Recovery = 79% Analysis Date = 12/31/21 Pct Recovery = 79% Analysis Date = 12/26/21 Pct Recovery = 80% Analysis Date = 12/26/21 Pct Recovery = 80% Analysis Date = 12/22/21 Pct Recovery = 80% Analysis Date = 12/22/21 Pct Recovery = 80% Analysis Date = 12/18/21 Pct Recovery = 80% Analysis Date = 12/18/21 Pct Recovery = 80% Analysis Date = 12/13/21 Pct Recovery = 80% Analysis Date = 12/13/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/05/21 Pct Recovery = 81% Analysis Date = 12/05/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/26/21 Pct Recovery = 81% Analysis Date = 11/26/21 Pct Recovery = 81% Analysis Date = 11/22/21 Pct Recovery = 81% Analysis Date = 11/22/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/13/21 Pct Recovery = 81% Analysis Date = 11/13/21 Pct Recovery = 81% Analysis Date = 11/09/21 Pct Recovery = 81% Analysis Date = 11/09/21 Pct Recovery = 81% Analysis Date = 11/05/21 Pct Recovery = 82% Analysis Date = 11/05/21 Pct Recovery = 82% Analysis Date = 10/31/21 Pct Recovery = 82% Analysis Date = 10/31/21 Pct Recovery = 82% Analysis Date = 10/27/21 Pct Recovery = 82% Analysis Date = 10/27/21 Pct Recovery = 82% Analysis Date = 10/23/21 Pct Recovery = 82% Analysis Date = 10/23/21 Pct Recovery = 82% Analysis Date = 10/18/21 Pct Recovery = 82% Analysis Date = 10/18/21 Pct Recovery = 82% Analysis Date = 10/14/21 Pct Recovery = 82% Analysis Date = 10/14/21 Pct Recovery = 82% Analysis Date = 10/10/21 Pct Recovery = 82% Analysis Date = 10/10/21 Pct Recovery = 82% Analysis Date = 10/05/21 Pct Recovery = 82% Analysis Date = 10/05/21 Pct Recovery = 82% Analysis Date = 10/01/21 Pct Recovery = 82% Analysis Date = 10/01/21 Pct Recovery = 82% Analysis Date = 09/27/21 Pct Recovery = 83% Analysis Date = 09/27/21 Pct Recovery = 83% Analysis Date = 09/22/21 Pct Recovery = 83% Analysis Date = 09/22/21 Pct Recovery = 83% Analysis Date = 09/18/21 Pct Recovery = 83% Analysis Date = 09/18/21 Pct Recovery = 83% Analysis Date = 09/14/21 Pct Recovery = 83% Analysis Date = 09/14/21 Pct Recovery = 83% Analysis Date = 09/09/21 Pct Recovery = 83% Analysis Date = 09/09/21 Pct Recovery = 83% Analysis Date = 09/05/21 Pct Recovery = 83% Analysis Date = 09/05/21 Pct Recovery = 83% Analysis Date = 09/01/21 Pct Recovery = 83% Analysis Date = 09/01/21 Pct Recovery = 83% Analysis Date = 08/28/21 Pct Recovery = 83% Analysis Date = 08/28/21 Pct Recovery = 83% Analysis Date = 08/23/21 Pct Recovery = 83% Analysis Date = 08/23/21 Pct Recovery = 83% Analysis Date = 08/19/21 Pct Recovery = 83% Analysis Date = 08/19/21 Pct Recovery = 83% Analysis Date = 08/15/21 Pct Recovery = 84% Analysis Date = 08/15/21 Pct Recovery = 84% Analysis Date = 08/10/21 Pct Recovery = 84% Analysis Date = 08/10/21 Pct Recovery = 84% Analysis Date = 08/06/21 Pct Recovery = 84% Analysis Date = 08/06/21 Pct Recovery = 84% Analysis Date = 08/02/21 Pct Recovery = 84% Analysis Date = 08/02/21 Pct Recovery = 84% Analysis Date = 07/28/21 Pct Recovery = 84% Analysis Date = 07/28/21 Pct Recovery = 84% Analysis Date = 07/24/21 Pct Recovery = 84% Analysis Date = 07/24/21 Pct Recovery = 84% Analysis Date = 07/20/21 Pct Recovery = 84% Analysis Date = 07/20/21 Pct Recovery = 84% Analysis Date = 07/15/21 Pct Recovery = 84% Analysis Date = 07/15/21 Pct Recovery = 84% Analysis Date = 07/11/21 Pct Recovery = 84% Analysis Date = 07/11/21 Pct Recovery = 84% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/02/21 Pct Recovery = 85% Analysis Date = 07/02/21 Pct Recovery = 85% Analysis Date = 06/28/21 Pct Recovery = 85% Analysis Date = 06/28/21 Pct Recovery = 85% Analysis Date = 06/24/21 Pct Recovery = 85% Analysis Date = 06/24/21 Pct Recovery = 85% Analysis Date = 06/19/21 Pct Recovery = 85% Analysis Date = 06/19/21 Pct Recovery = 85% Analysis Date = 06/15/21 Pct Recovery = 85% Analysis Date = 06/15/21 Pct Recovery = 85% Analysis Date = 06/11/21 Pct Recovery = 85% Analysis Date = 06/11/21 Pct Recovery = 85% Analysis Date = 06/07/21 Pct Recovery = 85% Analysis Date = 06/07/21 Pct Recovery = 85% Analysis Date = 06/02/21 Pct Recovery = 85% Analysis Date = 06/02/21 Pct Recovery = 85% Analysis Date = 05/29/21 Pct Recovery = 86% Analysis Date = 05/29/21 Pct Recovery = 86% Analysis Date = 05/25/21 Pct Recovery = 86% Analysis Date = 05/25/21 Pct Recovery = 86% Analysis Date = 05/20/21 Pct Recovery = 86% Analysis Date = 05/20/21 Pct Recovery = 86% Analysis Date = 05/16/21 Pct Recovery = 86% Analysis Date = 05/16/21 Pct Recovery = 86% Analysis Date = 05/12/21 Pct Recovery = 86% Analysis Date = 05/12/21 Pct Recovery = 86% Analysis Date = 05/07/21 Pct Recovery = 86% Analysis Date = 05/07/21 Pct Recovery = 86% Analysis Date = 05/03/21 Pct Recovery = 86% Analysis Date = 05/03/21 Pct Recovery = 86% Analysis Date = 04/29/21 Pct Recovery = 86% Analysis Date = 04/29/21 Pct Recovery = 86% Analysis Date = 04/24/21 Pct Recovery = 86% Analysis Date = 04/24/21 Pct Recovery = 86% Analysis Date = 04/20/21 Pct Recovery = 86% Analysis Date = 04/20/21 Pct Recovery = 86% Analysis Date = 04/16/21 Pct Recovery = 87% Analysis Date = 04/16/21 Pct Recovery = 87% Analysis Date = 04/11/21 Pct Recovery = 87% Analysis Date = 04/11/21 Pct Recovery = 87% Analysis Date = 04/07/21 Pct Recovery = 87% Analysis Date = 04/07/21 Pct Recovery = 87% Analysis Date = 04/03/21 Pct Recovery = 87% Analysis Date = 04/03/21 Pct Recovery = 87% Analysis Date = 03/29/21 Pct Recovery = 87% Analysis Date = 03/29/21 Pct Recovery = 87% Analysis Date = 03/25/21 Pct Recovery = 88% Analysis Date = 03/25/21 Pct Recovery = 88% Analysis Date = 03/21/21 Pct Recovery = 88% Analysis Date = 03/21/21 Pct Recovery = 88% Analysis Date = 03/17/21 Pct Recovery = 88% Analysis Date = 03/17/21 Pct Recovery = 88% Analysis Date = 03/12/21 Pct Recovery = 88% Analysis Date = 03/12/21 Pct Recovery = 88% Analysis Date = 03/08/21 Pct Recovery = 88% Analysis Date = 03/08/21 Pct Recovery = 88% Analysis Date = 03/04/21 Pct Recovery = 88% Analysis Date = 03/04/21 Pct Recovery = 88% Analysis Date = 02/27/21 Pct Recovery = 89% Analysis Date = 02/27/21 Pct Recovery = 89% Analysis Date = 02/23/21 Pct Recovery = 89% Analysis Date = 02/23/21 Pct Recovery = 89% Analysis Date = 02/19/21 Pct Recovery = 89% Analysis Date = 02/19/21 Pct Recovery = 89% Analysis Date = 02/14/21 Pct Recovery = 89% Analysis Date = 02/14/21 Pct Recovery = 89% Analysis Date = 02/10/21 Pct Recovery = 89% Analysis Date = 02/10/21 Pct Recovery = 89% Analysis Date = 02/06/21 Pct Recovery = 90% Analysis Date = 02/06/21 Pct Recovery = 90% Analysis Date = 02/01/21 Pct Recovery = 90% Analysis Date = 02/01/21 Pct Recovery = 90% Analysis Date = 01/28/21 Pct Recovery = 90% Analysis Date = 01/28/21 Pct Recovery = 90% Analysis Date = 01/24/21 Pct Recovery = 90% Analysis Date = 01/24/21 Pct Recovery = 90% Analysis Date = 01/19/21 Pct Recovery = 90% Analysis Date = 01/19/21 Pct Recovery = 90% Analysis Date = 01/15/21 Pct Recovery = 90% Analysis Date = 01/15/21 Pct Recovery = 90% Analysis Date = 01/11/21 Pct Recovery = 90% Analysis Date = 01/11/21 Pct Recovery = 90% Analysis Date = 01/07/21 Pct Recovery = 90% Analysis Date = 01/07/21 Pct Recovery = 90% Analysis Date = 01/02/21 Pct Recovery = 90% Analysis Date = 01/02/21 Pct Recovery = 90% Analysis Date = 12/29/20 Pct Recovery = 90% Analysis Date = 12/29/20 Pct Recovery = 90% Analysis Date = 12/25/20 Pct Recovery = 90% Analysis Date = 12/25/20 Pct Recovery = 90% Analysis Date = 12/20/20 Pct Recovery = 90% Analysis Date = 12/20/20 Pct Recovery = 90% Analysis Date = 12/16/20 Pct Recovery = 91% Analysis Date = 12/16/20 Pct Recovery = 91% Analysis Date = 12/12/20 Pct Recovery = 91% Analysis Date = 12/12/20 Pct Recovery = 91% Analysis Date = 12/07/20 Pct Recovery = 91% Analysis Date = 12/07/20 Pct Recovery = 91% Analysis Date = 12/03/20 Pct Recovery = 91% Analysis Date = 12/03/20 Pct Recovery = 91% Analysis Date = 11/29/20 Pct Recovery = 91% Analysis Date = 11/29/20 Pct Recovery = 91% Analysis Date = 11/24/20 Pct Recovery = 91% Analysis Date = 11/24/20 Pct Recovery = 91% Analysis Date = 11/20/20 Pct Recovery = 92% Analysis Date = 11/20/20 Pct Recovery = 92% Analysis Date = 11/16/20 Pct Recovery = 92% Analysis Date = 11/16/20 Pct Recovery = 92% Analysis Date = 11/11/20 Pct Recovery = 92% Analysis Date = 11/11/20 Pct Recovery = 92% Analysis Date = 11/07/20 Pct Recovery = 92% Analysis Date = 11/07/20 Pct Recovery = 92% Analysis Date = 11/03/20 Pct Recovery = 92% Analysis Date = 11/03/20 Pct Recovery = 92% Analysis Date = 10/29/20 Pct Recovery = 93% Analysis Date = 10/29/20 Pct Recovery = 93% Analysis Date = 10/25/20 Pct Recovery = 93% Analysis Date = 10/25/20 Pct Recovery = 93% Analysis Date = 10/21/20 Pct Recovery = 93% Analysis Date = 10/21/20 Pct Recovery = 93% Analysis Date = 10/17/20 Pct Recovery = 94% Analysis Date = 10/17/20 Pct Recovery = 94% Analysis Date = 10/12/20 Pct Recovery = 94% Analysis Date = 10/12/20 Pct Recovery = 94% Analysis Date = 10/08/20 Pct Recovery = 94% Analysis Date = 10/08/20 Pct Recovery = 94% Analysis Date = 10/04/20 Pct Recovery = 95% Analysis Date = 10/04/20 Pct Recovery = 95% Analysis Date = 09/29/20 Pct Recovery = 95% Analysis Date = 09/29/20 Pct Recovery = 95% Analysis Date = 09/25/20 Pct Recovery = 95% Analysis Date = 09/25/20 Pct Recovery = 95% Analysis Date = 09/21/20 Pct Recovery = 96% Analysis Date = 09/21/20 Pct Recovery = 96% Analysis Date = 09/16/20 Pct Recovery = 96% Analysis Date = 09/16/20 Pct Recovery = 96% Analysis Date = 09/12/20 Pct Recovery = 96% Analysis Date = 09/12/20 Pct Recovery = 96% Analysis Date = 09/08/20 Pct Recovery = 96% Analysis Date = 09/08/20 Pct Recovery = 96% Analysis Date = 09/03/20 Pct Recovery = 97% Analysis Date = 09/03/20 Pct Recovery = 97% Analysis Date = 08/30/20 Pct Recovery = 97% Analysis Date = 08/30/20 Pct Recovery = 97% Analysis Date = 08/26/20 Pct Recovery = 97% Analysis Date = 08/26/20 Pct Recovery = 97% Analysis Date = 08/21/20 Pct Recovery = 97% Analysis Date = 08/21/20 Pct Recovery = 97% Analysis Date = 08/17/20 Pct Recovery = 97% Analysis Date = 08/17/20 Pct Recovery = 97% Analysis Date = 08/13/20 Pct Recovery = 97% Analysis Date = 08/13/20 Pct Recovery = 97% Analysis Date = 08/08/20 Pct Recovery = 97% Analysis Date = 08/08/20 Pct Recovery = 97% Analysis Date = 08/04/20 Pct Recovery = 97% Analysis Date = 08/04/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/22/20 Pct Recovery = 97% Analysis Date = 07/22/20 Pct Recovery = 97% Analysis Date = 07/18/20 Pct Recovery = 97% Analysis Date = 07/18/20 Pct Recovery = 97% Analysis Date = 07/14/20 Pct Recovery = 97% Analysis Date = 07/14/20 Pct Recovery = 97% Analysis Date = 07/09/20 Pct Recovery = 98% Analysis Date = 07/09/20 Pct Recovery = 98% Analysis Date = 07/05/20 Pct Recovery = 98% Analysis Date = 07/05/20 Pct Recovery = 98% Analysis Date = 07/01/20 Pct Recovery = 98% Analysis Date = 07/01/20 Pct Recovery = 98% Analysis Date = 06/26/20 Pct Recovery = 98% Analysis Date = 06/26/20 Pct Recovery = 98% Analysis Date = 06/22/20 Pct Recovery = 98% Analysis Date = 06/22/20 Pct Recovery = 98% Analysis Date = 06/18/20 Pct Recovery = 98% Analysis Date = 06/18/20 Pct Recovery = 98% Analysis Date = 06/13/20 Pct Recovery = 98% Analysis Date = 06/13/20 Pct Recovery = 98% Analysis Date = 06/09/20 Pct Recovery = 98% Analysis Date = 06/09/20 Pct Recovery = 98% Analysis Date = 06/05/20 Pct Recovery = 98% Analysis Date = 06/05/20 Pct Recovery = 98% Analysis Date = 05/31/20 Pct Recovery = 98% Analysis Date = 05/31/20 Pct Recovery = 98% Analysis Date = 05/27/20 Pct Recovery = 98% Analysis Date = 05/27/20 Pct Recovery = 98% Analysis Date = 05/23/20 Pct Recovery = 99% Analysis Date = 05/23/20 Pct Recovery = 99% Analysis Date = 05/19/20 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACEPHATE (ORTHENE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 87% 25% 88% 18%
Total 41 87% 25% 88% 18%

Sample Statistics
ACEPHATE (ORTHENE)

Characteristic N % % Basis
Plotted 41 98% Spiked
Estimated Values 5 12% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 1 2% 1 out of 42
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

OBSP Determination:
ACETOCHLOR
METHOD: 2447 , TESTIDCODE: 68520LCM60

Laboratory ID = 20213200091 Lab Value = 157.105 Expected Conc. = 62.45 Report level label = 10 Pct Recovery = 252% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202110006 Lab Value = 141.210 Expected Conc. = 126.4 Report level label = 10 Pct Recovery = 112% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20202590106 Lab Value = 139.317 Expected Conc. = 125.7 Report level label = 10 Pct Recovery = 111% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 149.813 Expected Conc. = 125.7 Report level label = 10 Pct Recovery = 119% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201820155 Lab Value = 135.985 Expected Conc. = 125.6 Report level label = 10 Pct Recovery = 108% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203230021 Lab Value = 94.401 Expected Conc. = 124.9 Report level label = 10 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 126.799 Expected Conc. = 124.9 Report level label = 10 Pct Recovery = 102% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20220190116 Lab Value = 52.591 Expected Conc. = 100.08 Report level label = 10 Pct Recovery = 53% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 74.139 Expected Conc. = 100.08 Report level label = 10 Pct Recovery = 74% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 71.280 Expected Conc. = 100 Report level label = 10 Pct Recovery = 71% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20212990174 Lab Value = 69.428 Expected Conc. = 99.92 Report level label = 10 Pct Recovery = 69% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222150193 Lab Value = 69.043 Expected Conc. = 99.6 Report level label = 10 Pct Recovery = 69% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220810134 Lab Value = 92.360 Expected Conc. = 99.6 Report level label = 10 Pct Recovery = 93% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20201680155 Lab Value = 66.471 Expected Conc. = 63.2 Report level label = 10 Pct Recovery = 105% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20203230018 Lab Value = 73.190 Expected Conc. = 62.85 Report level label = 10 Pct Recovery = 116% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 55.633 Expected Conc. = 62.85 Report level label = 10 Pct Recovery = 89% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 63.201 Expected Conc. = 62.85 Report level label = 10 Pct Recovery = 101% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 72.053 Expected Conc. = 62.8 Report level label = 10 Pct Recovery = 115% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 68.768 Expected Conc. = 62.8 Report level label = 10 Pct Recovery = 110% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 73.693 Expected Conc. = 62.8 Report level label = 10 Pct Recovery = 117% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20221730293 Lab Value = 48.871 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 78% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 41.485 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 66% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20213340027 Lab Value = 51.087 Expected Conc. = 62.45 Report level label = 10 Pct Recovery = 82% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 30.093 Expected Conc. = 62.45 Report level label = 10 Pct Recovery = 48% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20220810133 Lab Value = 52.008 Expected Conc. = 62.25 Report level label = 10 Pct Recovery = 84% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201610160 Lab Value = 29.747 Expected Conc. = 25.28 Report level label = 10 Pct Recovery = 118% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210970035 Lab Value = 30.640 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 122% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 23.959 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 95% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 24.633 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 98% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 46.298 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 184% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 24.131 Expected Conc. = 25.12 Report level label = 10 Pct Recovery = 96% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 29.422 Expected Conc. = 25.12 Report level label = 10 Pct Recovery = 117% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 42.060 Expected Conc. = 25.12 Report level label = 10 Pct Recovery = 167% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 26.306 Expected Conc. = 25.12 Report level label = 10 Pct Recovery = 105% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20222500483 Lab Value = 13.582 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 54% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 16.811 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 67% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213060210 Lab Value = 10.500 Expected Conc. = 24.98 Report level label = 10 Pct Recovery = 42% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210270007 Lab Value = 24.842 Expected Conc. = 24.98 Report level label = 10 Pct Recovery = 99% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222630205 Lab Value = 14.618 Expected Conc. = 24.9 Report level label = 10 Pct Recovery = 59% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Analysis Date = 09/28/22 Pct Recovery = 62% Analysis Date = 09/24/22 Pct Recovery = 62% Analysis Date = 09/24/22 Pct Recovery = 62% Analysis Date = 09/20/22 Pct Recovery = 63% Analysis Date = 09/20/22 Pct Recovery = 63% Analysis Date = 09/16/22 Pct Recovery = 63% Analysis Date = 09/16/22 Pct Recovery = 63% Analysis Date = 09/11/22 Pct Recovery = 63% Analysis Date = 09/11/22 Pct Recovery = 63% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 08/29/22 Pct Recovery = 64% Analysis Date = 08/29/22 Pct Recovery = 64% Analysis Date = 08/25/22 Pct Recovery = 65% Analysis Date = 08/25/22 Pct Recovery = 65% Analysis Date = 08/21/22 Pct Recovery = 65% Analysis Date = 08/21/22 Pct Recovery = 65% Analysis Date = 08/16/22 Pct Recovery = 65% Analysis Date = 08/16/22 Pct Recovery = 65% Analysis Date = 08/12/22 Pct Recovery = 66% Analysis Date = 08/12/22 Pct Recovery = 66% Analysis Date = 08/08/22 Pct Recovery = 66% Analysis Date = 08/08/22 Pct Recovery = 66% Analysis Date = 08/03/22 Pct Recovery = 67% Analysis Date = 08/03/22 Pct Recovery = 67% Analysis Date = 07/30/22 Pct Recovery = 67% Analysis Date = 07/30/22 Pct Recovery = 67% Analysis Date = 07/26/22 Pct Recovery = 67% Analysis Date = 07/26/22 Pct Recovery = 67% Analysis Date = 07/21/22 Pct Recovery = 68% Analysis Date = 07/21/22 Pct Recovery = 68% Analysis Date = 07/17/22 Pct Recovery = 68% Analysis Date = 07/17/22 Pct Recovery = 68% Analysis Date = 07/13/22 Pct Recovery = 68% Analysis Date = 07/13/22 Pct Recovery = 68% Analysis Date = 07/09/22 Pct Recovery = 69% Analysis Date = 07/09/22 Pct Recovery = 69% Analysis Date = 07/04/22 Pct Recovery = 69% Analysis Date = 07/04/22 Pct Recovery = 69% Analysis Date = 06/30/22 Pct Recovery = 70% Analysis Date = 06/30/22 Pct Recovery = 70% Analysis Date = 06/26/22 Pct Recovery = 70% Analysis Date = 06/26/22 Pct Recovery = 70% Analysis Date = 06/21/22 Pct Recovery = 70% Analysis Date = 06/21/22 Pct Recovery = 70% Analysis Date = 06/17/22 Pct Recovery = 71% Analysis Date = 06/17/22 Pct Recovery = 71% Analysis Date = 06/13/22 Pct Recovery = 71% Analysis Date = 06/13/22 Pct Recovery = 71% Analysis Date = 06/08/22 Pct Recovery = 71% Analysis Date = 06/08/22 Pct Recovery = 71% Analysis Date = 06/04/22 Pct Recovery = 72% Analysis Date = 06/04/22 Pct Recovery = 72% Analysis Date = 05/31/22 Pct Recovery = 72% Analysis Date = 05/31/22 Pct Recovery = 72% Analysis Date = 05/26/22 Pct Recovery = 73% Analysis Date = 05/26/22 Pct Recovery = 73% Analysis Date = 05/22/22 Pct Recovery = 73% Analysis Date = 05/22/22 Pct Recovery = 73% Analysis Date = 05/18/22 Pct Recovery = 73% Analysis Date = 05/18/22 Pct Recovery = 73% Analysis Date = 05/13/22 Pct Recovery = 74% Analysis Date = 05/13/22 Pct Recovery = 74% Analysis Date = 05/09/22 Pct Recovery = 74% Analysis Date = 05/09/22 Pct Recovery = 74% Analysis Date = 05/05/22 Pct Recovery = 74% Analysis Date = 05/05/22 Pct Recovery = 74% Analysis Date = 04/30/22 Pct Recovery = 75% Analysis Date = 04/30/22 Pct Recovery = 75% Analysis Date = 04/26/22 Pct Recovery = 75% Analysis Date = 04/26/22 Pct Recovery = 75% Analysis Date = 04/22/22 Pct Recovery = 76% Analysis Date = 04/22/22 Pct Recovery = 76% Analysis Date = 04/18/22 Pct Recovery = 76% Analysis Date = 04/18/22 Pct Recovery = 76% Analysis Date = 04/13/22 Pct Recovery = 76% Analysis Date = 04/13/22 Pct Recovery = 76% Analysis Date = 04/09/22 Pct Recovery = 77% Analysis Date = 04/09/22 Pct Recovery = 77% Analysis Date = 04/05/22 Pct Recovery = 77% Analysis Date = 04/05/22 Pct Recovery = 77% Analysis Date = 03/31/22 Pct Recovery = 77% Analysis Date = 03/31/22 Pct Recovery = 77% Analysis Date = 03/27/22 Pct Recovery = 78% Analysis Date = 03/27/22 Pct Recovery = 78% Analysis Date = 03/23/22 Pct Recovery = 78% Analysis Date = 03/23/22 Pct Recovery = 78% Analysis Date = 03/18/22 Pct Recovery = 78% Analysis Date = 03/18/22 Pct Recovery = 78% Analysis Date = 03/14/22 Pct Recovery = 79% Analysis Date = 03/14/22 Pct Recovery = 79% Analysis Date = 03/10/22 Pct Recovery = 79% Analysis Date = 03/10/22 Pct Recovery = 79% Analysis Date = 03/05/22 Pct Recovery = 80% Analysis Date = 03/05/22 Pct Recovery = 80% Analysis Date = 03/01/22 Pct Recovery = 80% Analysis Date = 03/01/22 Pct Recovery = 80% Analysis Date = 02/25/22 Pct Recovery = 80% Analysis Date = 02/25/22 Pct Recovery = 80% Analysis Date = 02/20/22 Pct Recovery = 81% Analysis Date = 02/20/22 Pct Recovery = 81% Analysis Date = 02/16/22 Pct Recovery = 81% Analysis Date = 02/16/22 Pct Recovery = 81% Analysis Date = 02/12/22 Pct Recovery = 81% Analysis Date = 02/12/22 Pct Recovery = 81% Analysis Date = 02/07/22 Pct Recovery = 82% Analysis Date = 02/07/22 Pct Recovery = 82% Analysis Date = 02/03/22 Pct Recovery = 82% Analysis Date = 02/03/22 Pct Recovery = 82% Analysis Date = 01/30/22 Pct Recovery = 83% Analysis Date = 01/30/22 Pct Recovery = 83% Analysis Date = 01/26/22 Pct Recovery = 83% Analysis Date = 01/26/22 Pct Recovery = 83% Analysis Date = 01/21/22 Pct Recovery = 83% Analysis Date = 01/21/22 Pct Recovery = 83% Analysis Date = 01/17/22 Pct Recovery = 84% Analysis Date = 01/17/22 Pct Recovery = 84% Analysis Date = 01/13/22 Pct Recovery = 84% Analysis Date = 01/13/22 Pct Recovery = 84% Analysis Date = 01/08/22 Pct Recovery = 84% Analysis Date = 01/08/22 Pct Recovery = 84% Analysis Date = 01/04/22 Pct Recovery = 85% Analysis Date = 01/04/22 Pct Recovery = 85% Analysis Date = 12/31/21 Pct Recovery = 85% Analysis Date = 12/31/21 Pct Recovery = 85% Analysis Date = 12/26/21 Pct Recovery = 85% Analysis Date = 12/26/21 Pct Recovery = 85% Analysis Date = 12/22/21 Pct Recovery = 86% Analysis Date = 12/22/21 Pct Recovery = 86% Analysis Date = 12/18/21 Pct Recovery = 86% Analysis Date = 12/18/21 Pct Recovery = 86% Analysis Date = 12/13/21 Pct Recovery = 87% Analysis Date = 12/13/21 Pct Recovery = 87% Analysis Date = 12/09/21 Pct Recovery = 87% Analysis Date = 12/09/21 Pct Recovery = 87% Analysis Date = 12/05/21 Pct Recovery = 87% Analysis Date = 12/05/21 Pct Recovery = 87% Analysis Date = 11/30/21 Pct Recovery = 88% Analysis Date = 11/30/21 Pct Recovery = 88% Analysis Date = 11/26/21 Pct Recovery = 88% Analysis Date = 11/26/21 Pct Recovery = 88% Analysis Date = 11/22/21 Pct Recovery = 88% Analysis Date = 11/22/21 Pct Recovery = 88% Analysis Date = 11/18/21 Pct Recovery = 89% Analysis Date = 11/18/21 Pct Recovery = 89% Analysis Date = 11/13/21 Pct Recovery = 89% Analysis Date = 11/13/21 Pct Recovery = 89% Analysis Date = 11/09/21 Pct Recovery = 89% Analysis Date = 11/09/21 Pct Recovery = 89% Analysis Date = 11/05/21 Pct Recovery = 89% Analysis Date = 11/05/21 Pct Recovery = 89% Analysis Date = 10/31/21 Pct Recovery = 90% Analysis Date = 10/31/21 Pct Recovery = 90% Analysis Date = 10/27/21 Pct Recovery = 90% Analysis Date = 10/27/21 Pct Recovery = 90% Analysis Date = 10/23/21 Pct Recovery = 90% Analysis Date = 10/23/21 Pct Recovery = 90% Analysis Date = 10/18/21 Pct Recovery = 90% Analysis Date = 10/18/21 Pct Recovery = 90% Analysis Date = 10/14/21 Pct Recovery = 90% Analysis Date = 10/14/21 Pct Recovery = 90% Analysis Date = 10/10/21 Pct Recovery = 91% Analysis Date = 10/10/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/01/21 Pct Recovery = 91% Analysis Date = 10/01/21 Pct Recovery = 91% Analysis Date = 09/27/21 Pct Recovery = 91% Analysis Date = 09/27/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 91% Analysis Date = 09/18/21 Pct Recovery = 91% Analysis Date = 09/18/21 Pct Recovery = 91% Analysis Date = 09/14/21 Pct Recovery = 92% Analysis Date = 09/14/21 Pct Recovery = 92% Analysis Date = 09/09/21 Pct Recovery = 92% Analysis Date = 09/09/21 Pct Recovery = 92% Analysis Date = 09/05/21 Pct Recovery = 92% Analysis Date = 09/05/21 Pct Recovery = 92% Analysis Date = 09/01/21 Pct Recovery = 92% Analysis Date = 09/01/21 Pct Recovery = 92% Analysis Date = 08/28/21 Pct Recovery = 92% Analysis Date = 08/28/21 Pct Recovery = 92% Analysis Date = 08/23/21 Pct Recovery = 93% Analysis Date = 08/23/21 Pct Recovery = 93% Analysis Date = 08/19/21 Pct Recovery = 93% Analysis Date = 08/19/21 Pct Recovery = 93% Analysis Date = 08/15/21 Pct Recovery = 93% Analysis Date = 08/15/21 Pct Recovery = 93% Analysis Date = 08/10/21 Pct Recovery = 93% Analysis Date = 08/10/21 Pct Recovery = 93% Analysis Date = 08/06/21 Pct Recovery = 93% Analysis Date = 08/06/21 Pct Recovery = 93% Analysis Date = 08/02/21 Pct Recovery = 94% Analysis Date = 08/02/21 Pct Recovery = 94% Analysis Date = 07/28/21 Pct Recovery = 94% Analysis Date = 07/28/21 Pct Recovery = 94% Analysis Date = 07/24/21 Pct Recovery = 94% Analysis Date = 07/24/21 Pct Recovery = 94% Analysis Date = 07/20/21 Pct Recovery = 94% Analysis Date = 07/20/21 Pct Recovery = 94% Analysis Date = 07/15/21 Pct Recovery = 94% Analysis Date = 07/15/21 Pct Recovery = 94% Analysis Date = 07/11/21 Pct Recovery = 95% Analysis Date = 07/11/21 Pct Recovery = 95% Analysis Date = 07/07/21 Pct Recovery = 95% Analysis Date = 07/07/21 Pct Recovery = 95% Analysis Date = 07/02/21 Pct Recovery = 95% Analysis Date = 07/02/21 Pct Recovery = 95% Analysis Date = 06/28/21 Pct Recovery = 95% Analysis Date = 06/28/21 Pct Recovery = 95% Analysis Date = 06/24/21 Pct Recovery = 95% Analysis Date = 06/24/21 Pct Recovery = 95% Analysis Date = 06/19/21 Pct Recovery = 96% Analysis Date = 06/19/21 Pct Recovery = 96% Analysis Date = 06/15/21 Pct Recovery = 96% Analysis Date = 06/15/21 Pct Recovery = 96% Analysis Date = 06/11/21 Pct Recovery = 96% Analysis Date = 06/11/21 Pct Recovery = 96% Analysis Date = 06/07/21 Pct Recovery = 96% Analysis Date = 06/07/21 Pct Recovery = 96% Analysis Date = 06/02/21 Pct Recovery = 96% Analysis Date = 06/02/21 Pct Recovery = 96% Analysis Date = 05/29/21 Pct Recovery = 97% Analysis Date = 05/29/21 Pct Recovery = 97% Analysis Date = 05/25/21 Pct Recovery = 97% Analysis Date = 05/25/21 Pct Recovery = 97% Analysis Date = 05/20/21 Pct Recovery = 97% Analysis Date = 05/20/21 Pct Recovery = 97% Analysis Date = 05/16/21 Pct Recovery = 97% Analysis Date = 05/16/21 Pct Recovery = 97% Analysis Date = 05/12/21 Pct Recovery = 97% Analysis Date = 05/12/21 Pct Recovery = 97% Analysis Date = 05/07/21 Pct Recovery = 97% Analysis Date = 05/07/21 Pct Recovery = 97% Analysis Date = 05/03/21 Pct Recovery = 98% Analysis Date = 05/03/21 Pct Recovery = 98% Analysis Date = 04/29/21 Pct Recovery = 98% Analysis Date = 04/29/21 Pct Recovery = 98% Analysis Date = 04/24/21 Pct Recovery = 98% Analysis Date = 04/24/21 Pct Recovery = 98% Analysis Date = 04/20/21 Pct Recovery = 98% Analysis Date = 04/20/21 Pct Recovery = 98% Analysis Date = 04/16/21 Pct Recovery = 98% Analysis Date = 04/16/21 Pct Recovery = 98% Analysis Date = 04/11/21 Pct Recovery = 99% Analysis Date = 04/11/21 Pct Recovery = 99% Analysis Date = 04/07/21 Pct Recovery = 99% Analysis Date = 04/07/21 Pct Recovery = 99% Analysis Date = 04/03/21 Pct Recovery = 99% Analysis Date = 04/03/21 Pct Recovery = 99% Analysis Date = 03/29/21 Pct Recovery = 100% Analysis Date = 03/29/21 Pct Recovery = 100% Analysis Date = 03/25/21 Pct Recovery = 100% Analysis Date = 03/25/21 Pct Recovery = 100% Analysis Date = 03/21/21 Pct Recovery = 100% Analysis Date = 03/21/21 Pct Recovery = 100% Analysis Date = 03/17/21 Pct Recovery = 100% Analysis Date = 03/17/21 Pct Recovery = 100% Analysis Date = 03/12/21 Pct Recovery = 101% Analysis Date = 03/12/21 Pct Recovery = 101% Analysis Date = 03/08/21 Pct Recovery = 101% Analysis Date = 03/08/21 Pct Recovery = 101% Analysis Date = 03/04/21 Pct Recovery = 101% Analysis Date = 03/04/21 Pct Recovery = 101% Analysis Date = 02/27/21 Pct Recovery = 101% Analysis Date = 02/27/21 Pct Recovery = 101% Analysis Date = 02/23/21 Pct Recovery = 102% Analysis Date = 02/23/21 Pct Recovery = 102% Analysis Date = 02/19/21 Pct Recovery = 102% Analysis Date = 02/19/21 Pct Recovery = 102% Analysis Date = 02/14/21 Pct Recovery = 102% Analysis Date = 02/14/21 Pct Recovery = 102% Analysis Date = 02/10/21 Pct Recovery = 103% Analysis Date = 02/10/21 Pct Recovery = 103% Analysis Date = 02/06/21 Pct Recovery = 103% Analysis Date = 02/06/21 Pct Recovery = 103% Analysis Date = 02/01/21 Pct Recovery = 103% Analysis Date = 02/01/21 Pct Recovery = 103% Analysis Date = 01/28/21 Pct Recovery = 103% Analysis Date = 01/28/21 Pct Recovery = 103% Analysis Date = 01/24/21 Pct Recovery = 104% Analysis Date = 01/24/21 Pct Recovery = 104% Analysis Date = 01/19/21 Pct Recovery = 104% Analysis Date = 01/19/21 Pct Recovery = 104% Analysis Date = 01/15/21 Pct Recovery = 104% Analysis Date = 01/15/21 Pct Recovery = 104% Analysis Date = 01/11/21 Pct Recovery = 105% Analysis Date = 01/11/21 Pct Recovery = 105% Analysis Date = 01/07/21 Pct Recovery = 105% Analysis Date = 01/07/21 Pct Recovery = 105% Analysis Date = 01/02/21 Pct Recovery = 106% Analysis Date = 01/02/21 Pct Recovery = 106% Analysis Date = 12/29/20 Pct Recovery = 106% Analysis Date = 12/29/20 Pct Recovery = 106% Analysis Date = 12/25/20 Pct Recovery = 106% Analysis Date = 12/25/20 Pct Recovery = 106% Analysis Date = 12/20/20 Pct Recovery = 107% Analysis Date = 12/20/20 Pct Recovery = 107% Analysis Date = 12/16/20 Pct Recovery = 107% Analysis Date = 12/16/20 Pct Recovery = 107% Analysis Date = 12/12/20 Pct Recovery = 107% Analysis Date = 12/12/20 Pct Recovery = 107% Analysis Date = 12/07/20 Pct Recovery = 108% Analysis Date = 12/07/20 Pct Recovery = 108% Analysis Date = 12/03/20 Pct Recovery = 108% Analysis Date = 12/03/20 Pct Recovery = 108% Analysis Date = 11/29/20 Pct Recovery = 108% Analysis Date = 11/29/20 Pct Recovery = 108% Analysis Date = 11/24/20 Pct Recovery = 109% Analysis Date = 11/24/20 Pct Recovery = 109% Analysis Date = 11/20/20 Pct Recovery = 109% Analysis Date = 11/20/20 Pct Recovery = 109% Analysis Date = 11/16/20 Pct Recovery = 110% Analysis Date = 11/16/20 Pct Recovery = 110% Analysis Date = 11/11/20 Pct Recovery = 110% Analysis Date = 11/11/20 Pct Recovery = 110% Analysis Date = 11/07/20 Pct Recovery = 110% Analysis Date = 11/07/20 Pct Recovery = 110% Analysis Date = 11/03/20 Pct Recovery = 111% Analysis Date = 11/03/20 Pct Recovery = 111% Analysis Date = 10/29/20 Pct Recovery = 111% Analysis Date = 10/29/20 Pct Recovery = 111% Analysis Date = 10/25/20 Pct Recovery = 111% Analysis Date = 10/25/20 Pct Recovery = 111% Analysis Date = 10/21/20 Pct Recovery = 112% Analysis Date = 10/21/20 Pct Recovery = 112% Analysis Date = 10/17/20 Pct Recovery = 112% Analysis Date = 10/17/20 Pct Recovery = 112% Analysis Date = 10/12/20 Pct Recovery = 112% Analysis Date = 10/12/20 Pct Recovery = 112% Analysis Date = 10/08/20 Pct Recovery = 113% Analysis Date = 10/08/20 Pct Recovery = 113% Analysis Date = 10/04/20 Pct Recovery = 113% Analysis Date = 10/04/20 Pct Recovery = 113% Analysis Date = 09/29/20 Pct Recovery = 114% Analysis Date = 09/29/20 Pct Recovery = 114% Analysis Date = 09/25/20 Pct Recovery = 114% Analysis Date = 09/25/20 Pct Recovery = 114% Analysis Date = 09/21/20 Pct Recovery = 114% Analysis Date = 09/21/20 Pct Recovery = 114% Analysis Date = 09/16/20 Pct Recovery = 115% Analysis Date = 09/16/20 Pct Recovery = 115% Analysis Date = 09/12/20 Pct Recovery = 115% Analysis Date = 09/12/20 Pct Recovery = 115% Analysis Date = 09/08/20 Pct Recovery = 115% Analysis Date = 09/08/20 Pct Recovery = 115% Analysis Date = 09/03/20 Pct Recovery = 115% Analysis Date = 09/03/20 Pct Recovery = 115% Analysis Date = 08/30/20 Pct Recovery = 116% Analysis Date = 08/30/20 Pct Recovery = 116% Analysis Date = 08/26/20 Pct Recovery = 116% Analysis Date = 08/26/20 Pct Recovery = 116% Analysis Date = 08/21/20 Pct Recovery = 116% Analysis Date = 08/21/20 Pct Recovery = 116% Analysis Date = 08/17/20 Pct Recovery = 116% Analysis Date = 08/17/20 Pct Recovery = 116% Analysis Date = 08/13/20 Pct Recovery = 117% Analysis Date = 08/13/20 Pct Recovery = 117% Analysis Date = 08/08/20 Pct Recovery = 117% Analysis Date = 08/08/20 Pct Recovery = 117% Analysis Date = 08/04/20 Pct Recovery = 117% Analysis Date = 08/04/20 Pct Recovery = 117% Analysis Date = 07/31/20 Pct Recovery = 117% Analysis Date = 07/31/20 Pct Recovery = 117% Analysis Date = 07/27/20 Pct Recovery = 118% Analysis Date = 07/27/20 Pct Recovery = 118% Analysis Date = 07/22/20 Pct Recovery = 118% Analysis Date = 07/22/20 Pct Recovery = 118% Analysis Date = 07/18/20 Pct Recovery = 118% Analysis Date = 07/18/20 Pct Recovery = 118% Analysis Date = 07/14/20 Pct Recovery = 118% Analysis Date = 07/14/20 Pct Recovery = 118% Analysis Date = 07/09/20 Pct Recovery = 118% Analysis Date = 07/09/20 Pct Recovery = 118% Analysis Date = 07/05/20 Pct Recovery = 119% Analysis Date = 07/05/20 Pct Recovery = 119% Analysis Date = 07/01/20 Pct Recovery = 119% Analysis Date = 07/01/20 Pct Recovery = 119% Analysis Date = 06/26/20 Pct Recovery = 119% Analysis Date = 06/26/20 Pct Recovery = 119% Analysis Date = 06/22/20 Pct Recovery = 119% Analysis Date = 06/22/20 Pct Recovery = 119% Analysis Date = 06/18/20 Pct Recovery = 119% Analysis Date = 06/18/20 Pct Recovery = 119% Analysis Date = 06/13/20 Pct Recovery = 119% Analysis Date = 06/13/20 Pct Recovery = 119% Analysis Date = 06/09/20 Pct Recovery = 119% Analysis Date = 06/09/20 Pct Recovery = 119% Analysis Date = 06/05/20 Pct Recovery = 120% Analysis Date = 06/05/20 Pct Recovery = 120% Analysis Date = 05/31/20 Pct Recovery = 120% Analysis Date = 05/31/20 Pct Recovery = 120% Analysis Date = 05/27/20 Pct Recovery = 120% Analysis Date = 05/27/20 Pct Recovery = 120% Analysis Date = 05/23/20 Pct Recovery = 120% Analysis Date = 05/23/20 Pct Recovery = 120% Analysis Date = 05/19/20 Pct Recovery = 120% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 39 99% 39% 98% 32%
Total 39 99% 39% 98% 32%

Sample Statistics
ACETOCHLOR

Characteristic N % % Basis
Plotted 39 93% Spiked
Estimated Values 4 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 7% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 72 .  
False Positives 0 0% 0 out of 72

OBSP Determination:
ACETOCHLOR OXANILIC ACID
METHOD: 2447 , TESTIDCODE: 68522LCM60

Laboratory ID = 20201820155 Lab Value = 1004.012 Expected Conc. = 821.1 Report level label = 65 Pct Recovery = 122% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20210760015 Lab Value = 443.837 Expected Conc. = 805.3 Report level label = 65 Pct Recovery = 55% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 559.338 Expected Conc. = 805.3 Report level label = 65 Pct Recovery = 69% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 936.221 Expected Conc. = 805.3 Report level label = 65 Pct Recovery = 116% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 701.219 Expected Conc. = 805.3 Report level label = 65 Pct Recovery = 87% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202110006 Lab Value = 1055.497 Expected Conc. = 802.5 Report level label = 65 Pct Recovery = 132% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203080100 Lab Value = 1273.635 Expected Conc. = 800.7 Report level label = 65 Pct Recovery = 159% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 1072.617 Expected Conc. = 800.7 Report level label = 65 Pct Recovery = 134% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 1091.055 Expected Conc. = 800.7 Report level label = 65 Pct Recovery = 136% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221370164 Lab Value = 575.795 Expected Conc. = 650.92 Report level label = 65 Pct Recovery = 88% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20202530029 Lab Value = 517.249 Expected Conc. = 410.55 Report level label = 65 Pct Recovery = 126% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 456.364 Expected Conc. = 410.55 Report level label = 65 Pct Recovery = 111% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 520.025 Expected Conc. = 410.55 Report level label = 65 Pct Recovery = 127% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20210480001 Lab Value = 360.062 Expected Conc. = 402.65 Report level label = 65 Pct Recovery = 89% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201680155 Lab Value = 483.249 Expected Conc. = 401.25 Report level label = 65 Pct Recovery = 120% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202880004 Lab Value = 458.889 Expected Conc. = 400.35 Report level label = 65 Pct Recovery = 115% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210620006 Lab Value = 425.881 Expected Conc. = 320.28 Report level label = 65 Pct Recovery = 133% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 509.155 Expected Conc. = 320.28 Report level label = 65 Pct Recovery = 159% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202330309 Lab Value = 231.773 Expected Conc. = 164.22 Report level label = 65 Pct Recovery = 141% Analysis Date = 09/01/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 211.517 Expected Conc. = 164.22 Report level label = 65 Pct Recovery = 129% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 285.815 Expected Conc. = 164.22 Report level label = 65 Pct Recovery = 174% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 135.270 Expected Conc. = 164.22 Report level label = 65 Pct Recovery = 82% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20221160208 Lab Value = 110.821 Expected Conc. = 162.73 Report level label = 65 Pct Recovery = 68% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20210690067 Lab Value = 148.675 Expected Conc. = 161.06 Report level label = 65 Pct Recovery = 92% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 218.687 Expected Conc. = 160.5 Report level label = 65 Pct Recovery = 136% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210120050 Lab Value = 142.306 Expected Conc. = 160.14 Report level label = 65 Pct Recovery = 89% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 214.098 Expected Conc. = 160.14 Report level label = 65 Pct Recovery = 134% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 203.510 Expected Conc. = 160.14 Report level label = 65 Pct Recovery = 127% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 215.665 Expected Conc. = 160.14 Report level label = 65 Pct Recovery = 135% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 166.509 Expected Conc. = 160.14 Report level label = 65 Pct Recovery = 104% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 05/23/22 Pct Recovery = 77% Analysis Date = 05/20/22 Pct Recovery = 78% Analysis Date = 05/20/22 Pct Recovery = 78% Analysis Date = 05/16/22 Pct Recovery = 78% Analysis Date = 05/16/22 Pct Recovery = 78% Analysis Date = 05/12/22 Pct Recovery = 78% Analysis Date = 05/12/22 Pct Recovery = 78% Analysis Date = 05/09/22 Pct Recovery = 78% Analysis Date = 05/09/22 Pct Recovery = 78% Analysis Date = 05/05/22 Pct Recovery = 78% Analysis Date = 05/05/22 Pct Recovery = 78% Analysis Date = 05/01/22 Pct Recovery = 78% Analysis Date = 05/01/22 Pct Recovery = 78% Analysis Date = 04/28/22 Pct Recovery = 78% Analysis Date = 04/28/22 Pct Recovery = 78% Analysis Date = 04/24/22 Pct Recovery = 78% Analysis Date = 04/24/22 Pct Recovery = 78% Analysis Date = 04/20/22 Pct Recovery = 78% Analysis Date = 04/20/22 Pct Recovery = 78% Analysis Date = 04/17/22 Pct Recovery = 78% Analysis Date = 04/17/22 Pct Recovery = 78% Analysis Date = 04/13/22 Pct Recovery = 78% Analysis Date = 04/13/22 Pct Recovery = 78% Analysis Date = 04/09/22 Pct Recovery = 78% Analysis Date = 04/09/22 Pct Recovery = 78% Analysis Date = 04/06/22 Pct Recovery = 78% Analysis Date = 04/06/22 Pct Recovery = 78% Analysis Date = 04/02/22 Pct Recovery = 78% Analysis Date = 04/02/22 Pct Recovery = 78% Analysis Date = 03/29/22 Pct Recovery = 78% Analysis Date = 03/29/22 Pct Recovery = 78% Analysis Date = 03/26/22 Pct Recovery = 78% Analysis Date = 03/26/22 Pct Recovery = 78% Analysis Date = 03/22/22 Pct Recovery = 78% Analysis Date = 03/22/22 Pct Recovery = 78% Analysis Date = 03/18/22 Pct Recovery = 78% Analysis Date = 03/18/22 Pct Recovery = 78% Analysis Date = 03/15/22 Pct Recovery = 78% Analysis Date = 03/15/22 Pct Recovery = 78% Analysis Date = 03/11/22 Pct Recovery = 79% Analysis Date = 03/11/22 Pct Recovery = 79% Analysis Date = 03/07/22 Pct Recovery = 79% Analysis Date = 03/07/22 Pct Recovery = 79% Analysis Date = 03/04/22 Pct Recovery = 79% Analysis Date = 03/04/22 Pct Recovery = 79% Analysis Date = 02/28/22 Pct Recovery = 79% Analysis Date = 02/28/22 Pct Recovery = 79% Analysis Date = 02/24/22 Pct Recovery = 79% Analysis Date = 02/24/22 Pct Recovery = 79% Analysis Date = 02/21/22 Pct Recovery = 79% Analysis Date = 02/21/22 Pct Recovery = 79% Analysis Date = 02/17/22 Pct Recovery = 79% Analysis Date = 02/17/22 Pct Recovery = 79% Analysis Date = 02/13/22 Pct Recovery = 79% Analysis Date = 02/13/22 Pct Recovery = 79% Analysis Date = 02/10/22 Pct Recovery = 79% Analysis Date = 02/10/22 Pct Recovery = 79% Analysis Date = 02/06/22 Pct Recovery = 79% Analysis Date = 02/06/22 Pct Recovery = 79% Analysis Date = 02/02/22 Pct Recovery = 79% Analysis Date = 02/02/22 Pct Recovery = 79% Analysis Date = 01/30/22 Pct Recovery = 79% Analysis Date = 01/30/22 Pct Recovery = 79% Analysis Date = 01/26/22 Pct Recovery = 79% Analysis Date = 01/26/22 Pct Recovery = 79% Analysis Date = 01/22/22 Pct Recovery = 79% Analysis Date = 01/22/22 Pct Recovery = 79% Analysis Date = 01/19/22 Pct Recovery = 79% Analysis Date = 01/19/22 Pct Recovery = 79% Analysis Date = 01/15/22 Pct Recovery = 79% Analysis Date = 01/15/22 Pct Recovery = 79% Analysis Date = 01/11/22 Pct Recovery = 79% Analysis Date = 01/11/22 Pct Recovery = 79% Analysis Date = 01/08/22 Pct Recovery = 79% Analysis Date = 01/08/22 Pct Recovery = 79% Analysis Date = 01/04/22 Pct Recovery = 79% Analysis Date = 01/04/22 Pct Recovery = 79% Analysis Date = 12/31/21 Pct Recovery = 80% Analysis Date = 12/31/21 Pct Recovery = 80% Analysis Date = 12/28/21 Pct Recovery = 80% Analysis Date = 12/28/21 Pct Recovery = 80% Analysis Date = 12/24/21 Pct Recovery = 80% Analysis Date = 12/24/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/17/21 Pct Recovery = 80% Analysis Date = 12/17/21 Pct Recovery = 80% Analysis Date = 12/13/21 Pct Recovery = 80% Analysis Date = 12/13/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/06/21 Pct Recovery = 80% Analysis Date = 12/06/21 Pct Recovery = 80% Analysis Date = 12/02/21 Pct Recovery = 80% Analysis Date = 12/02/21 Pct Recovery = 80% Analysis Date = 11/28/21 Pct Recovery = 80% Analysis Date = 11/28/21 Pct Recovery = 80% Analysis Date = 11/25/21 Pct Recovery = 80% Analysis Date = 11/25/21 Pct Recovery = 80% Analysis Date = 11/21/21 Pct Recovery = 80% Analysis Date = 11/21/21 Pct Recovery = 80% Analysis Date = 11/17/21 Pct Recovery = 80% Analysis Date = 11/17/21 Pct Recovery = 80% Analysis Date = 11/14/21 Pct Recovery = 80% Analysis Date = 11/14/21 Pct Recovery = 80% Analysis Date = 11/10/21 Pct Recovery = 80% Analysis Date = 11/10/21 Pct Recovery = 80% Analysis Date = 11/06/21 Pct Recovery = 80% Analysis Date = 11/06/21 Pct Recovery = 80% Analysis Date = 11/03/21 Pct Recovery = 80% Analysis Date = 11/03/21 Pct Recovery = 80% Analysis Date = 10/30/21 Pct Recovery = 80% Analysis Date = 10/30/21 Pct Recovery = 80% Analysis Date = 10/26/21 Pct Recovery = 80% Analysis Date = 10/26/21 Pct Recovery = 80% Analysis Date = 10/23/21 Pct Recovery = 81% Analysis Date = 10/23/21 Pct Recovery = 81% Analysis Date = 10/19/21 Pct Recovery = 81% Analysis Date = 10/19/21 Pct Recovery = 81% Analysis Date = 10/15/21 Pct Recovery = 81% Analysis Date = 10/15/21 Pct Recovery = 81% Analysis Date = 10/12/21 Pct Recovery = 81% Analysis Date = 10/12/21 Pct Recovery = 81% Analysis Date = 10/08/21 Pct Recovery = 81% Analysis Date = 10/08/21 Pct Recovery = 81% Analysis Date = 10/04/21 Pct Recovery = 81% Analysis Date = 10/04/21 Pct Recovery = 81% Analysis Date = 10/01/21 Pct Recovery = 81% Analysis Date = 10/01/21 Pct Recovery = 81% Analysis Date = 09/27/21 Pct Recovery = 81% Analysis Date = 09/27/21 Pct Recovery = 81% Analysis Date = 09/23/21 Pct Recovery = 81% Analysis Date = 09/23/21 Pct Recovery = 81% Analysis Date = 09/20/21 Pct Recovery = 81% Analysis Date = 09/20/21 Pct Recovery = 81% Analysis Date = 09/16/21 Pct Recovery = 81% Analysis Date = 09/16/21 Pct Recovery = 81% Analysis Date = 09/12/21 Pct Recovery = 81% Analysis Date = 09/12/21 Pct Recovery = 81% Analysis Date = 09/09/21 Pct Recovery = 81% Analysis Date = 09/09/21 Pct Recovery = 81% Analysis Date = 09/05/21 Pct Recovery = 81% Analysis Date = 09/05/21 Pct Recovery = 81% Analysis Date = 09/01/21 Pct Recovery = 81% Analysis Date = 09/01/21 Pct Recovery = 81% Analysis Date = 08/29/21 Pct Recovery = 81% Analysis Date = 08/29/21 Pct Recovery = 81% Analysis Date = 08/25/21 Pct Recovery = 81% Analysis Date = 08/25/21 Pct Recovery = 81% Analysis Date = 08/21/21 Pct Recovery = 81% Analysis Date = 08/21/21 Pct Recovery = 81% Analysis Date = 08/18/21 Pct Recovery = 81% Analysis Date = 08/18/21 Pct Recovery = 81% Analysis Date = 08/14/21 Pct Recovery = 82% Analysis Date = 08/14/21 Pct Recovery = 82% Analysis Date = 08/10/21 Pct Recovery = 82% Analysis Date = 08/10/21 Pct Recovery = 82% Analysis Date = 08/07/21 Pct Recovery = 82% Analysis Date = 08/07/21 Pct Recovery = 82% Analysis Date = 08/03/21 Pct Recovery = 82% Analysis Date = 08/03/21 Pct Recovery = 82% Analysis Date = 07/30/21 Pct Recovery = 82% Analysis Date = 07/30/21 Pct Recovery = 82% Analysis Date = 07/27/21 Pct Recovery = 82% Analysis Date = 07/27/21 Pct Recovery = 82% Analysis Date = 07/23/21 Pct Recovery = 82% Analysis Date = 07/23/21 Pct Recovery = 82% Analysis Date = 07/19/21 Pct Recovery = 82% Analysis Date = 07/19/21 Pct Recovery = 82% Analysis Date = 07/16/21 Pct Recovery = 82% Analysis Date = 07/16/21 Pct Recovery = 82% Analysis Date = 07/12/21 Pct Recovery = 82% Analysis Date = 07/12/21 Pct Recovery = 82% Analysis Date = 07/08/21 Pct Recovery = 82% Analysis Date = 07/08/21 Pct Recovery = 82% Analysis Date = 07/05/21 Pct Recovery = 82% Analysis Date = 07/05/21 Pct Recovery = 82% Analysis Date = 07/01/21 Pct Recovery = 82% Analysis Date = 07/01/21 Pct Recovery = 82% Analysis Date = 06/27/21 Pct Recovery = 82% Analysis Date = 06/27/21 Pct Recovery = 82% Analysis Date = 06/24/21 Pct Recovery = 82% Analysis Date = 06/24/21 Pct Recovery = 82% Analysis Date = 06/20/21 Pct Recovery = 82% Analysis Date = 06/20/21 Pct Recovery = 82% Analysis Date = 06/16/21 Pct Recovery = 82% Analysis Date = 06/16/21 Pct Recovery = 82% Analysis Date = 06/13/21 Pct Recovery = 82% Analysis Date = 06/13/21 Pct Recovery = 82% Analysis Date = 06/09/21 Pct Recovery = 83% Analysis Date = 06/09/21 Pct Recovery = 83% Analysis Date = 06/05/21 Pct Recovery = 83% Analysis Date = 06/05/21 Pct Recovery = 83% Analysis Date = 06/02/21 Pct Recovery = 83% Analysis Date = 06/02/21 Pct Recovery = 83% Analysis Date = 05/29/21 Pct Recovery = 83% Analysis Date = 05/29/21 Pct Recovery = 83% Analysis Date = 05/25/21 Pct Recovery = 83% Analysis Date = 05/25/21 Pct Recovery = 83% Analysis Date = 05/21/21 Pct Recovery = 83% Analysis Date = 05/21/21 Pct Recovery = 83% Analysis Date = 05/18/21 Pct Recovery = 83% Analysis Date = 05/18/21 Pct Recovery = 83% Analysis Date = 05/14/21 Pct Recovery = 83% Analysis Date = 05/14/21 Pct Recovery = 83% Analysis Date = 05/10/21 Pct Recovery = 83% Analysis Date = 05/10/21 Pct Recovery = 83% Analysis Date = 05/07/21 Pct Recovery = 83% Analysis Date = 05/07/21 Pct Recovery = 83% Analysis Date = 05/03/21 Pct Recovery = 83% Analysis Date = 05/03/21 Pct Recovery = 83% Analysis Date = 04/29/21 Pct Recovery = 83% Analysis Date = 04/29/21 Pct Recovery = 83% Analysis Date = 04/26/21 Pct Recovery = 83% Analysis Date = 04/26/21 Pct Recovery = 83% Analysis Date = 04/22/21 Pct Recovery = 83% Analysis Date = 04/22/21 Pct Recovery = 83% Analysis Date = 04/18/21 Pct Recovery = 83% Analysis Date = 04/18/21 Pct Recovery = 83% Analysis Date = 04/15/21 Pct Recovery = 83% Analysis Date = 04/15/21 Pct Recovery = 83% Analysis Date = 04/11/21 Pct Recovery = 83% Analysis Date = 04/11/21 Pct Recovery = 83% Analysis Date = 04/07/21 Pct Recovery = 83% Analysis Date = 04/07/21 Pct Recovery = 83% Analysis Date = 04/04/21 Pct Recovery = 83% Analysis Date = 04/04/21 Pct Recovery = 83% Analysis Date = 03/31/21 Pct Recovery = 84% Analysis Date = 03/31/21 Pct Recovery = 84% Analysis Date = 03/27/21 Pct Recovery = 84% Analysis Date = 03/27/21 Pct Recovery = 84% Analysis Date = 03/24/21 Pct Recovery = 84% Analysis Date = 03/24/21 Pct Recovery = 84% Analysis Date = 03/20/21 Pct Recovery = 84% Analysis Date = 03/20/21 Pct Recovery = 84% Analysis Date = 03/16/21 Pct Recovery = 84% Analysis Date = 03/16/21 Pct Recovery = 84% Analysis Date = 03/13/21 Pct Recovery = 86% Analysis Date = 03/13/21 Pct Recovery = 86% Analysis Date = 03/09/21 Pct Recovery = 87% Analysis Date = 03/09/21 Pct Recovery = 87% Analysis Date = 03/05/21 Pct Recovery = 88% Analysis Date = 03/05/21 Pct Recovery = 88% Analysis Date = 03/02/21 Pct Recovery = 90% Analysis Date = 03/02/21 Pct Recovery = 90% Analysis Date = 02/26/21 Pct Recovery = 91% Analysis Date = 02/26/21 Pct Recovery = 91% Analysis Date = 02/22/21 Pct Recovery = 93% Analysis Date = 02/22/21 Pct Recovery = 93% Analysis Date = 02/19/21 Pct Recovery = 94% Analysis Date = 02/19/21 Pct Recovery = 94% Analysis Date = 02/15/21 Pct Recovery = 95% Analysis Date = 02/15/21 Pct Recovery = 95% Analysis Date = 02/11/21 Pct Recovery = 97% Analysis Date = 02/11/21 Pct Recovery = 97% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/04/21 Pct Recovery = 100% Analysis Date = 02/04/21 Pct Recovery = 100% Analysis Date = 01/31/21 Pct Recovery = 101% Analysis Date = 01/31/21 Pct Recovery = 101% Analysis Date = 01/28/21 Pct Recovery = 103% Analysis Date = 01/28/21 Pct Recovery = 103% Analysis Date = 01/24/21 Pct Recovery = 104% Analysis Date = 01/24/21 Pct Recovery = 104% Analysis Date = 01/20/21 Pct Recovery = 105% Analysis Date = 01/20/21 Pct Recovery = 105% Analysis Date = 01/17/21 Pct Recovery = 107% Analysis Date = 01/17/21 Pct Recovery = 107% Analysis Date = 01/13/21 Pct Recovery = 108% Analysis Date = 01/13/21 Pct Recovery = 108% Analysis Date = 01/09/21 Pct Recovery = 109% Analysis Date = 01/09/21 Pct Recovery = 109% Analysis Date = 01/06/21 Pct Recovery = 110% Analysis Date = 01/06/21 Pct Recovery = 110% Analysis Date = 01/02/21 Pct Recovery = 111% Analysis Date = 01/02/21 Pct Recovery = 111% Analysis Date = 12/29/20 Pct Recovery = 112% Analysis Date = 12/29/20 Pct Recovery = 112% Analysis Date = 12/26/20 Pct Recovery = 113% Analysis Date = 12/26/20 Pct Recovery = 113% Analysis Date = 12/22/20 Pct Recovery = 115% Analysis Date = 12/22/20 Pct Recovery = 115% Analysis Date = 12/18/20 Pct Recovery = 116% Analysis Date = 12/18/20 Pct Recovery = 116% Analysis Date = 12/15/20 Pct Recovery = 117% Analysis Date = 12/15/20 Pct Recovery = 117% Analysis Date = 12/11/20 Pct Recovery = 118% Analysis Date = 12/11/20 Pct Recovery = 118% Analysis Date = 12/07/20 Pct Recovery = 119% Analysis Date = 12/07/20 Pct Recovery = 119% Analysis Date = 12/04/20 Pct Recovery = 120% Analysis Date = 12/04/20 Pct Recovery = 120% Analysis Date = 11/30/20 Pct Recovery = 121% Analysis Date = 11/30/20 Pct Recovery = 121% Analysis Date = 11/26/20 Pct Recovery = 122% Analysis Date = 11/26/20 Pct Recovery = 122% Analysis Date = 11/23/20 Pct Recovery = 123% Analysis Date = 11/23/20 Pct Recovery = 123% Analysis Date = 11/19/20 Pct Recovery = 124% Analysis Date = 11/19/20 Pct Recovery = 124% Analysis Date = 11/15/20 Pct Recovery = 125% Analysis Date = 11/15/20 Pct Recovery = 125% Analysis Date = 11/12/20 Pct Recovery = 126% Analysis Date = 11/12/20 Pct Recovery = 126% Analysis Date = 11/08/20 Pct Recovery = 126% Analysis Date = 11/08/20 Pct Recovery = 126% Analysis Date = 11/04/20 Pct Recovery = 126% Analysis Date = 11/04/20 Pct Recovery = 126% Analysis Date = 11/01/20 Pct Recovery = 127% Analysis Date = 11/01/20 Pct Recovery = 127% Analysis Date = 10/28/20 Pct Recovery = 127% Analysis Date = 10/28/20 Pct Recovery = 127% Analysis Date = 10/24/20 Pct Recovery = 128% Analysis Date = 10/24/20 Pct Recovery = 128% Analysis Date = 10/21/20 Pct Recovery = 128% Analysis Date = 10/21/20 Pct Recovery = 128% Analysis Date = 10/17/20 Pct Recovery = 128% Analysis Date = 10/17/20 Pct Recovery = 128% Analysis Date = 10/13/20 Pct Recovery = 128% Analysis Date = 10/13/20 Pct Recovery = 128% Analysis Date = 10/10/20 Pct Recovery = 128% Analysis Date = 10/10/20 Pct Recovery = 128% Analysis Date = 10/06/20 Pct Recovery = 128% Analysis Date = 10/06/20 Pct Recovery = 128% Analysis Date = 10/02/20 Pct Recovery = 128% Analysis Date = 10/02/20 Pct Recovery = 128% Analysis Date = 09/29/20 Pct Recovery = 128% Analysis Date = 09/29/20 Pct Recovery = 128% Analysis Date = 09/25/20 Pct Recovery = 128% Analysis Date = 09/25/20 Pct Recovery = 128% Analysis Date = 09/21/20 Pct Recovery = 129% Analysis Date = 09/21/20 Pct Recovery = 129% Analysis Date = 09/18/20 Pct Recovery = 129% Analysis Date = 09/18/20 Pct Recovery = 129% Analysis Date = 09/14/20 Pct Recovery = 129% Analysis Date = 09/14/20 Pct Recovery = 129% Analysis Date = 09/10/20 Pct Recovery = 130% Analysis Date = 09/10/20 Pct Recovery = 130% Analysis Date = 09/07/20 Pct Recovery = 130% Analysis Date = 09/07/20 Pct Recovery = 130% Analysis Date = 09/03/20 Pct Recovery = 130% Analysis Date = 09/03/20 Pct Recovery = 130% Analysis Date = 08/30/20 Pct Recovery = 130% Analysis Date = 08/30/20 Pct Recovery = 130% Analysis Date = 08/27/20 Pct Recovery = 130% Analysis Date = 08/27/20 Pct Recovery = 130% Analysis Date = 08/23/20 Pct Recovery = 130% Analysis Date = 08/23/20 Pct Recovery = 130% Analysis Date = 08/19/20 Pct Recovery = 130% Analysis Date = 08/19/20 Pct Recovery = 130% Analysis Date = 08/16/20 Pct Recovery = 129% Analysis Date = 08/16/20 Pct Recovery = 129% Analysis Date = 08/12/20 Pct Recovery = 129% Analysis Date = 08/12/20 Pct Recovery = 129% Analysis Date = 08/08/20 Pct Recovery = 129% Analysis Date = 08/08/20 Pct Recovery = 129% Analysis Date = 08/05/20 Pct Recovery = 129% Analysis Date = 08/05/20 Pct Recovery = 129% Analysis Date = 08/01/20 Pct Recovery = 128% Analysis Date = 08/01/20 Pct Recovery = 128% Analysis Date = 07/28/20 Pct Recovery = 128% Analysis Date = 07/28/20 Pct Recovery = 128% Analysis Date = 07/25/20 Pct Recovery = 128% Analysis Date = 07/25/20 Pct Recovery = 128% Analysis Date = 07/21/20 Pct Recovery = 127% Analysis Date = 07/21/20 Pct Recovery = 127% Analysis Date = 07/17/20 Pct Recovery = 127% Analysis Date = 07/17/20 Pct Recovery = 127% Analysis Date = 07/14/20 Pct Recovery = 127% Analysis Date = 07/14/20 Pct Recovery = 127% Analysis Date = 07/10/20 Pct Recovery = 126% Analysis Date = 07/10/20 Pct Recovery = 126% Analysis Date = 07/06/20 Pct Recovery = 126% Analysis Date = 07/06/20 Pct Recovery = 126% Analysis Date = 07/03/20 Pct Recovery = 126% Analysis Date = 07/03/20 Pct Recovery = 126% Analysis Date = 06/29/20 Pct Recovery = 125% Analysis Date = 06/29/20 Pct Recovery = 125% Analysis Date = 06/25/20 Pct Recovery = 125% Analysis Date = 06/25/20 Pct Recovery = 125% Analysis Date = 06/22/20 Pct Recovery = 125% Analysis Date = 06/22/20 Pct Recovery = 125% Analysis Date = 06/18/20 Pct Recovery = 124% Analysis Date = 06/18/20 Pct Recovery = 124% Analysis Date = 06/14/20 Pct Recovery = 124% Analysis Date = 06/14/20 Pct Recovery = 124% Analysis Date = 06/11/20 Pct Recovery = 123% Analysis Date = 06/11/20 Pct Recovery = 123% Analysis Date = 06/07/20 Pct Recovery = 123% Analysis Date = 06/07/20 Pct Recovery = 123% Analysis Date = 06/03/20 Pct Recovery = 123% Analysis Date = 06/03/20 Pct Recovery = 123% Analysis Date = 05/31/20 Pct Recovery = 122% Analysis Date = 05/31/20 Pct Recovery = 122% Analysis Date = 05/27/20 Pct Recovery = 122% Analysis Date = 05/27/20 Pct Recovery = 122% Analysis Date = 05/23/20 Pct Recovery = 121% Analysis Date = 05/23/20 Pct Recovery = 121% Analysis Date = 05/20/20 Pct Recovery = 121% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR OXANILIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 116% 29% 124% 33%
Total 30 116% 29% 124% 33%

Sample Statistics
ACETOCHLOR OXANILIC ACID

Characteristic N % % Basis
Plotted 30 97% Spiked
Estimated Values 30 97% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 1 3% 1 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
ACETOCHLOR SULFONIC ACID
METHOD: 2447 , TESTIDCODE: 68523LCM60

Laboratory ID = 20202110006 Lab Value = 3721.755 Expected Conc. = 4030.4 Report level label = 320 Pct Recovery = 92% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203080100 Lab Value = 4637.156 Expected Conc. = 4026.8 Report level label = 320 Pct Recovery = 115% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 4183.781 Expected Conc. = 4026.8 Report level label = 320 Pct Recovery = 104% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 4383.011 Expected Conc. = 4026.8 Report level label = 320 Pct Recovery = 109% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201820155 Lab Value = 3798.460 Expected Conc. = 4002.9 Report level label = 320 Pct Recovery = 95% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20210760015 Lab Value = 3047.738 Expected Conc. = 3986 Report level label = 320 Pct Recovery = 76% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 3298.428 Expected Conc. = 3986 Report level label = 320 Pct Recovery = 83% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 4632.402 Expected Conc. = 3986 Report level label = 320 Pct Recovery = 116% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 4236.173 Expected Conc. = 3986 Report level label = 320 Pct Recovery = 106% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221370164 Lab Value = 2609.468 Expected Conc. = 3201.9 Report level label = 320 Pct Recovery = 81% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20201680155 Lab Value = 2064.424 Expected Conc. = 2015.2 Report level label = 320 Pct Recovery = 102% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202880004 Lab Value = 1837.887 Expected Conc. = 2013.4 Report level label = 320 Pct Recovery = 91% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202530029 Lab Value = 1556.830 Expected Conc. = 2001.5 Report level label = 320 Pct Recovery = 78% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 1588.570 Expected Conc. = 2001.5 Report level label = 320 Pct Recovery = 79% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 2104.942 Expected Conc. = 2001.5 Report level label = 320 Pct Recovery = 105% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20210480001 Lab Value = 1546.013 Expected Conc. = 1993 Report level label = 320 Pct Recovery = 78% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 1526.130 Expected Conc. = 1610.7 Report level label = 320 Pct Recovery = 95% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 1862.799 Expected Conc. = 1610.7 Report level label = 320 Pct Recovery = 116% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 1426.406 Expected Conc. = 1594.4 Report level label = 320 Pct Recovery = 89% Analysis Date = 04/06/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 1061.161 Expected Conc. = 806.08 Report level label = 320 Pct Recovery = 132% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210120050 Lab Value = 630.616 Expected Conc. = 805.36 Report level label = 320 Pct Recovery = 78% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 1131.305 Expected Conc. = 805.36 Report level label = 320 Pct Recovery = 140% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 806.013 Expected Conc. = 805.36 Report level label = 320 Pct Recovery = 100% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 794.205 Expected Conc. = 805.36 Report level label = 320 Pct Recovery = 99% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 892.359 Expected Conc. = 805.36 Report level label = 320 Pct Recovery = 111% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202040027 Lab Value = 747.243 Expected Conc. = 800.58 Report level label = 320 Pct Recovery = 93% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 937.024 Expected Conc. = 800.58 Report level label = 320 Pct Recovery = 117% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 904.681 Expected Conc. = 800.58 Report level label = 320 Pct Recovery = 113% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20221160208 Lab Value = 484.529 Expected Conc. = 800.48 Report level label = 320 Pct Recovery = 61% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20210690067 Lab Value = 705.423 Expected Conc. = 797.2 Report level label = 320 Pct Recovery = 88% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 05/23/22 Pct Recovery = 71% Analysis Date = 05/20/22 Pct Recovery = 71% Analysis Date = 05/20/22 Pct Recovery = 71% Analysis Date = 05/16/22 Pct Recovery = 71% Analysis Date = 05/16/22 Pct Recovery = 71% Analysis Date = 05/12/22 Pct Recovery = 71% Analysis Date = 05/12/22 Pct Recovery = 71% Analysis Date = 05/09/22 Pct Recovery = 71% Analysis Date = 05/09/22 Pct Recovery = 71% Analysis Date = 05/05/22 Pct Recovery = 71% Analysis Date = 05/05/22 Pct Recovery = 71% Analysis Date = 05/01/22 Pct Recovery = 71% Analysis Date = 05/01/22 Pct Recovery = 71% Analysis Date = 04/28/22 Pct Recovery = 71% Analysis Date = 04/28/22 Pct Recovery = 71% Analysis Date = 04/24/22 Pct Recovery = 72% Analysis Date = 04/24/22 Pct Recovery = 72% Analysis Date = 04/20/22 Pct Recovery = 72% Analysis Date = 04/20/22 Pct Recovery = 72% Analysis Date = 04/17/22 Pct Recovery = 72% Analysis Date = 04/17/22 Pct Recovery = 72% Analysis Date = 04/13/22 Pct Recovery = 72% Analysis Date = 04/13/22 Pct Recovery = 72% Analysis Date = 04/09/22 Pct Recovery = 72% Analysis Date = 04/09/22 Pct Recovery = 72% Analysis Date = 04/06/22 Pct Recovery = 72% Analysis Date = 04/06/22 Pct Recovery = 72% Analysis Date = 04/02/22 Pct Recovery = 72% Analysis Date = 04/02/22 Pct Recovery = 72% Analysis Date = 03/29/22 Pct Recovery = 72% Analysis Date = 03/29/22 Pct Recovery = 72% Analysis Date = 03/26/22 Pct Recovery = 72% Analysis Date = 03/26/22 Pct Recovery = 72% Analysis Date = 03/22/22 Pct Recovery = 72% Analysis Date = 03/22/22 Pct Recovery = 72% Analysis Date = 03/18/22 Pct Recovery = 73% Analysis Date = 03/18/22 Pct Recovery = 73% Analysis Date = 03/15/22 Pct Recovery = 73% Analysis Date = 03/15/22 Pct Recovery = 73% Analysis Date = 03/11/22 Pct Recovery = 73% Analysis Date = 03/11/22 Pct Recovery = 73% Analysis Date = 03/07/22 Pct Recovery = 73% Analysis Date = 03/07/22 Pct Recovery = 73% Analysis Date = 03/04/22 Pct Recovery = 73% Analysis Date = 03/04/22 Pct Recovery = 73% Analysis Date = 02/28/22 Pct Recovery = 73% Analysis Date = 02/28/22 Pct Recovery = 73% Analysis Date = 02/24/22 Pct Recovery = 73% Analysis Date = 02/24/22 Pct Recovery = 73% Analysis Date = 02/21/22 Pct Recovery = 73% Analysis Date = 02/21/22 Pct Recovery = 73% Analysis Date = 02/17/22 Pct Recovery = 73% Analysis Date = 02/17/22 Pct Recovery = 73% Analysis Date = 02/13/22 Pct Recovery = 73% Analysis Date = 02/13/22 Pct Recovery = 73% Analysis Date = 02/10/22 Pct Recovery = 74% Analysis Date = 02/10/22 Pct Recovery = 74% Analysis Date = 02/06/22 Pct Recovery = 74% Analysis Date = 02/06/22 Pct Recovery = 74% Analysis Date = 02/02/22 Pct Recovery = 74% Analysis Date = 02/02/22 Pct Recovery = 74% Analysis Date = 01/30/22 Pct Recovery = 74% Analysis Date = 01/30/22 Pct Recovery = 74% Analysis Date = 01/26/22 Pct Recovery = 74% Analysis Date = 01/26/22 Pct Recovery = 74% Analysis Date = 01/22/22 Pct Recovery = 74% Analysis Date = 01/22/22 Pct Recovery = 74% Analysis Date = 01/19/22 Pct Recovery = 74% Analysis Date = 01/19/22 Pct Recovery = 74% Analysis Date = 01/15/22 Pct Recovery = 74% Analysis Date = 01/15/22 Pct Recovery = 74% Analysis Date = 01/11/22 Pct Recovery = 74% Analysis Date = 01/11/22 Pct Recovery = 74% Analysis Date = 01/08/22 Pct Recovery = 74% Analysis Date = 01/08/22 Pct Recovery = 74% Analysis Date = 01/04/22 Pct Recovery = 75% Analysis Date = 01/04/22 Pct Recovery = 75% Analysis Date = 12/31/21 Pct Recovery = 75% Analysis Date = 12/31/21 Pct Recovery = 75% Analysis Date = 12/28/21 Pct Recovery = 75% Analysis Date = 12/28/21 Pct Recovery = 75% Analysis Date = 12/24/21 Pct Recovery = 75% Analysis Date = 12/24/21 Pct Recovery = 75% Analysis Date = 12/20/21 Pct Recovery = 75% Analysis Date = 12/20/21 Pct Recovery = 75% Analysis Date = 12/17/21 Pct Recovery = 75% Analysis Date = 12/17/21 Pct Recovery = 75% Analysis Date = 12/13/21 Pct Recovery = 75% Analysis Date = 12/13/21 Pct Recovery = 75% Analysis Date = 12/09/21 Pct Recovery = 75% Analysis Date = 12/09/21 Pct Recovery = 75% Analysis Date = 12/06/21 Pct Recovery = 75% Analysis Date = 12/06/21 Pct Recovery = 75% Analysis Date = 12/02/21 Pct Recovery = 75% Analysis Date = 12/02/21 Pct Recovery = 75% Analysis Date = 11/28/21 Pct Recovery = 76% Analysis Date = 11/28/21 Pct Recovery = 76% Analysis Date = 11/25/21 Pct Recovery = 76% Analysis Date = 11/25/21 Pct Recovery = 76% Analysis Date = 11/21/21 Pct Recovery = 76% Analysis Date = 11/21/21 Pct Recovery = 76% Analysis Date = 11/17/21 Pct Recovery = 76% Analysis Date = 11/17/21 Pct Recovery = 76% Analysis Date = 11/14/21 Pct Recovery = 76% Analysis Date = 11/14/21 Pct Recovery = 76% Analysis Date = 11/10/21 Pct Recovery = 76% Analysis Date = 11/10/21 Pct Recovery = 76% Analysis Date = 11/06/21 Pct Recovery = 76% Analysis Date = 11/06/21 Pct Recovery = 76% Analysis Date = 11/03/21 Pct Recovery = 76% Analysis Date = 11/03/21 Pct Recovery = 76% Analysis Date = 10/30/21 Pct Recovery = 76% Analysis Date = 10/30/21 Pct Recovery = 76% Analysis Date = 10/26/21 Pct Recovery = 77% Analysis Date = 10/26/21 Pct Recovery = 77% Analysis Date = 10/23/21 Pct Recovery = 77% Analysis Date = 10/23/21 Pct Recovery = 77% Analysis Date = 10/19/21 Pct Recovery = 77% Analysis Date = 10/19/21 Pct Recovery = 77% Analysis Date = 10/15/21 Pct Recovery = 77% Analysis Date = 10/15/21 Pct Recovery = 77% Analysis Date = 10/12/21 Pct Recovery = 77% Analysis Date = 10/12/21 Pct Recovery = 77% Analysis Date = 10/08/21 Pct Recovery = 77% Analysis Date = 10/08/21 Pct Recovery = 77% Analysis Date = 10/04/21 Pct Recovery = 77% Analysis Date = 10/04/21 Pct Recovery = 77% Analysis Date = 10/01/21 Pct Recovery = 77% Analysis Date = 10/01/21 Pct Recovery = 77% Analysis Date = 09/27/21 Pct Recovery = 77% Analysis Date = 09/27/21 Pct Recovery = 77% Analysis Date = 09/23/21 Pct Recovery = 77% Analysis Date = 09/23/21 Pct Recovery = 77% Analysis Date = 09/20/21 Pct Recovery = 78% Analysis Date = 09/20/21 Pct Recovery = 78% Analysis Date = 09/16/21 Pct Recovery = 78% Analysis Date = 09/16/21 Pct Recovery = 78% Analysis Date = 09/12/21 Pct Recovery = 78% Analysis Date = 09/12/21 Pct Recovery = 78% Analysis Date = 09/09/21 Pct Recovery = 78% Analysis Date = 09/09/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 78% Analysis Date = 09/01/21 Pct Recovery = 78% Analysis Date = 09/01/21 Pct Recovery = 78% Analysis Date = 08/29/21 Pct Recovery = 78% Analysis Date = 08/29/21 Pct Recovery = 78% Analysis Date = 08/25/21 Pct Recovery = 78% Analysis Date = 08/25/21 Pct Recovery = 78% Analysis Date = 08/21/21 Pct Recovery = 78% Analysis Date = 08/21/21 Pct Recovery = 78% Analysis Date = 08/18/21 Pct Recovery = 78% Analysis Date = 08/18/21 Pct Recovery = 78% Analysis Date = 08/14/21 Pct Recovery = 79% Analysis Date = 08/14/21 Pct Recovery = 79% Analysis Date = 08/10/21 Pct Recovery = 79% Analysis Date = 08/10/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/27/21 Pct Recovery = 79% Analysis Date = 07/27/21 Pct Recovery = 79% Analysis Date = 07/23/21 Pct Recovery = 79% Analysis Date = 07/23/21 Pct Recovery = 79% Analysis Date = 07/19/21 Pct Recovery = 79% Analysis Date = 07/19/21 Pct Recovery = 79% Analysis Date = 07/16/21 Pct Recovery = 79% Analysis Date = 07/16/21 Pct Recovery = 79% Analysis Date = 07/12/21 Pct Recovery = 79% Analysis Date = 07/12/21 Pct Recovery = 79% Analysis Date = 07/08/21 Pct Recovery = 80% Analysis Date = 07/08/21 Pct Recovery = 80% Analysis Date = 07/05/21 Pct Recovery = 80% Analysis Date = 07/05/21 Pct Recovery = 80% Analysis Date = 07/01/21 Pct Recovery = 80% Analysis Date = 07/01/21 Pct Recovery = 80% Analysis Date = 06/27/21 Pct Recovery = 80% Analysis Date = 06/27/21 Pct Recovery = 80% Analysis Date = 06/24/21 Pct Recovery = 80% Analysis Date = 06/24/21 Pct Recovery = 80% Analysis Date = 06/20/21 Pct Recovery = 80% Analysis Date = 06/20/21 Pct Recovery = 80% Analysis Date = 06/16/21 Pct Recovery = 80% Analysis Date = 06/16/21 Pct Recovery = 80% Analysis Date = 06/13/21 Pct Recovery = 80% Analysis Date = 06/13/21 Pct Recovery = 80% Analysis Date = 06/09/21 Pct Recovery = 80% Analysis Date = 06/09/21 Pct Recovery = 80% Analysis Date = 06/05/21 Pct Recovery = 80% Analysis Date = 06/05/21 Pct Recovery = 80% Analysis Date = 06/02/21 Pct Recovery = 81% Analysis Date = 06/02/21 Pct Recovery = 81% Analysis Date = 05/29/21 Pct Recovery = 81% Analysis Date = 05/29/21 Pct Recovery = 81% Analysis Date = 05/25/21 Pct Recovery = 81% Analysis Date = 05/25/21 Pct Recovery = 81% Analysis Date = 05/21/21 Pct Recovery = 81% Analysis Date = 05/21/21 Pct Recovery = 81% Analysis Date = 05/18/21 Pct Recovery = 81% Analysis Date = 05/18/21 Pct Recovery = 81% Analysis Date = 05/14/21 Pct Recovery = 81% Analysis Date = 05/14/21 Pct Recovery = 81% Analysis Date = 05/10/21 Pct Recovery = 81% Analysis Date = 05/10/21 Pct Recovery = 81% Analysis Date = 05/07/21 Pct Recovery = 81% Analysis Date = 05/07/21 Pct Recovery = 81% Analysis Date = 05/03/21 Pct Recovery = 81% Analysis Date = 05/03/21 Pct Recovery = 81% Analysis Date = 04/29/21 Pct Recovery = 82% Analysis Date = 04/29/21 Pct Recovery = 82% Analysis Date = 04/26/21 Pct Recovery = 82% Analysis Date = 04/26/21 Pct Recovery = 82% Analysis Date = 04/22/21 Pct Recovery = 82% Analysis Date = 04/22/21 Pct Recovery = 82% Analysis Date = 04/18/21 Pct Recovery = 82% Analysis Date = 04/18/21 Pct Recovery = 82% Analysis Date = 04/15/21 Pct Recovery = 82% Analysis Date = 04/15/21 Pct Recovery = 82% Analysis Date = 04/11/21 Pct Recovery = 82% Analysis Date = 04/11/21 Pct Recovery = 82% Analysis Date = 04/07/21 Pct Recovery = 82% Analysis Date = 04/07/21 Pct Recovery = 82% Analysis Date = 04/04/21 Pct Recovery = 82% Analysis Date = 04/04/21 Pct Recovery = 82% Analysis Date = 03/31/21 Pct Recovery = 82% Analysis Date = 03/31/21 Pct Recovery = 82% Analysis Date = 03/27/21 Pct Recovery = 82% Analysis Date = 03/27/21 Pct Recovery = 82% Analysis Date = 03/24/21 Pct Recovery = 83% Analysis Date = 03/24/21 Pct Recovery = 83% Analysis Date = 03/20/21 Pct Recovery = 83% Analysis Date = 03/20/21 Pct Recovery = 83% Analysis Date = 03/16/21 Pct Recovery = 84% Analysis Date = 03/16/21 Pct Recovery = 84% Analysis Date = 03/13/21 Pct Recovery = 85% Analysis Date = 03/13/21 Pct Recovery = 85% Analysis Date = 03/09/21 Pct Recovery = 86% Analysis Date = 03/09/21 Pct Recovery = 86% Analysis Date = 03/05/21 Pct Recovery = 87% Analysis Date = 03/05/21 Pct Recovery = 87% Analysis Date = 03/02/21 Pct Recovery = 88% Analysis Date = 03/02/21 Pct Recovery = 88% Analysis Date = 02/26/21 Pct Recovery = 89% Analysis Date = 02/26/21 Pct Recovery = 89% Analysis Date = 02/22/21 Pct Recovery = 89% Analysis Date = 02/22/21 Pct Recovery = 89% Analysis Date = 02/19/21 Pct Recovery = 90% Analysis Date = 02/19/21 Pct Recovery = 90% Analysis Date = 02/15/21 Pct Recovery = 91% Analysis Date = 02/15/21 Pct Recovery = 91% Analysis Date = 02/11/21 Pct Recovery = 92% Analysis Date = 02/11/21 Pct Recovery = 92% Analysis Date = 02/08/21 Pct Recovery = 93% Analysis Date = 02/08/21 Pct Recovery = 93% Analysis Date = 02/04/21 Pct Recovery = 94% Analysis Date = 02/04/21 Pct Recovery = 94% Analysis Date = 01/31/21 Pct Recovery = 95% Analysis Date = 01/31/21 Pct Recovery = 95% Analysis Date = 01/28/21 Pct Recovery = 96% Analysis Date = 01/28/21 Pct Recovery = 96% Analysis Date = 01/24/21 Pct Recovery = 96% Analysis Date = 01/24/21 Pct Recovery = 96% Analysis Date = 01/20/21 Pct Recovery = 97% Analysis Date = 01/20/21 Pct Recovery = 97% Analysis Date = 01/17/21 Pct Recovery = 98% Analysis Date = 01/17/21 Pct Recovery = 98% Analysis Date = 01/13/21 Pct Recovery = 99% Analysis Date = 01/13/21 Pct Recovery = 99% Analysis Date = 01/09/21 Pct Recovery = 100% Analysis Date = 01/09/21 Pct Recovery = 100% Analysis Date = 01/06/21 Pct Recovery = 100% Analysis Date = 01/06/21 Pct Recovery = 100% Analysis Date = 01/02/21 Pct Recovery = 101% Analysis Date = 01/02/21 Pct Recovery = 101% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/26/20 Pct Recovery = 103% Analysis Date = 12/26/20 Pct Recovery = 103% Analysis Date = 12/22/20 Pct Recovery = 104% Analysis Date = 12/22/20 Pct Recovery = 104% Analysis Date = 12/18/20 Pct Recovery = 104% Analysis Date = 12/18/20 Pct Recovery = 104% Analysis Date = 12/15/20 Pct Recovery = 104% Analysis Date = 12/15/20 Pct Recovery = 104% Analysis Date = 12/11/20 Pct Recovery = 105% Analysis Date = 12/11/20 Pct Recovery = 105% Analysis Date = 12/07/20 Pct Recovery = 105% Analysis Date = 12/07/20 Pct Recovery = 105% Analysis Date = 12/04/20 Pct Recovery = 105% Analysis Date = 12/04/20 Pct Recovery = 105% Analysis Date = 11/30/20 Pct Recovery = 105% Analysis Date = 11/30/20 Pct Recovery = 105% Analysis Date = 11/26/20 Pct Recovery = 105% Analysis Date = 11/26/20 Pct Recovery = 105% Analysis Date = 11/23/20 Pct Recovery = 105% Analysis Date = 11/23/20 Pct Recovery = 105% Analysis Date = 11/19/20 Pct Recovery = 105% Analysis Date = 11/19/20 Pct Recovery = 105% Analysis Date = 11/15/20 Pct Recovery = 105% Analysis Date = 11/15/20 Pct Recovery = 105% Analysis Date = 11/12/20 Pct Recovery = 105% Analysis Date = 11/12/20 Pct Recovery = 105% Analysis Date = 11/08/20 Pct Recovery = 105% Analysis Date = 11/08/20 Pct Recovery = 105% Analysis Date = 11/04/20 Pct Recovery = 105% Analysis Date = 11/04/20 Pct Recovery = 105% Analysis Date = 11/01/20 Pct Recovery = 104% Analysis Date = 11/01/20 Pct Recovery = 104% Analysis Date = 10/28/20 Pct Recovery = 103% Analysis Date = 10/28/20 Pct Recovery = 103% Analysis Date = 10/24/20 Pct Recovery = 103% Analysis Date = 10/24/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 102% Analysis Date = 10/13/20 Pct Recovery = 101% Analysis Date = 10/13/20 Pct Recovery = 101% Analysis Date = 10/10/20 Pct Recovery = 100% Analysis Date = 10/10/20 Pct Recovery = 100% Analysis Date = 10/06/20 Pct Recovery = 100% Analysis Date = 10/06/20 Pct Recovery = 100% Analysis Date = 10/02/20 Pct Recovery = 99% Analysis Date = 10/02/20 Pct Recovery = 99% Analysis Date = 09/29/20 Pct Recovery = 99% Analysis Date = 09/29/20 Pct Recovery = 99% Analysis Date = 09/25/20 Pct Recovery = 98% Analysis Date = 09/25/20 Pct Recovery = 98% Analysis Date = 09/21/20 Pct Recovery = 98% Analysis Date = 09/21/20 Pct Recovery = 98% Analysis Date = 09/18/20 Pct Recovery = 97% Analysis Date = 09/18/20 Pct Recovery = 97% Analysis Date = 09/14/20 Pct Recovery = 98% Analysis Date = 09/14/20 Pct Recovery = 98% Analysis Date = 09/10/20 Pct Recovery = 98% Analysis Date = 09/10/20 Pct Recovery = 98% Analysis Date = 09/07/20 Pct Recovery = 98% Analysis Date = 09/07/20 Pct Recovery = 98% Analysis Date = 09/03/20 Pct Recovery = 98% Analysis Date = 09/03/20 Pct Recovery = 98% Analysis Date = 08/30/20 Pct Recovery = 99% Analysis Date = 08/30/20 Pct Recovery = 99% Analysis Date = 08/27/20 Pct Recovery = 99% Analysis Date = 08/27/20 Pct Recovery = 99% Analysis Date = 08/23/20 Pct Recovery = 99% Analysis Date = 08/23/20 Pct Recovery = 99% Analysis Date = 08/19/20 Pct Recovery = 100% Analysis Date = 08/19/20 Pct Recovery = 100% Analysis Date = 08/16/20 Pct Recovery = 100% Analysis Date = 08/16/20 Pct Recovery = 100% Analysis Date = 08/12/20 Pct Recovery = 100% Analysis Date = 08/12/20 Pct Recovery = 100% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/05/20 Pct Recovery = 101% Analysis Date = 08/05/20 Pct Recovery = 101% Analysis Date = 08/01/20 Pct Recovery = 101% Analysis Date = 08/01/20 Pct Recovery = 101% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/25/20 Pct Recovery = 102% Analysis Date = 07/25/20 Pct Recovery = 102% Analysis Date = 07/21/20 Pct Recovery = 103% Analysis Date = 07/21/20 Pct Recovery = 103% Analysis Date = 07/17/20 Pct Recovery = 103% Analysis Date = 07/17/20 Pct Recovery = 103% Analysis Date = 07/14/20 Pct Recovery = 104% Analysis Date = 07/14/20 Pct Recovery = 104% Analysis Date = 07/10/20 Pct Recovery = 104% Analysis Date = 07/10/20 Pct Recovery = 104% Analysis Date = 07/06/20 Pct Recovery = 105% Analysis Date = 07/06/20 Pct Recovery = 105% Analysis Date = 07/03/20 Pct Recovery = 105% Analysis Date = 07/03/20 Pct Recovery = 105% Analysis Date = 06/29/20 Pct Recovery = 106% Analysis Date = 06/29/20 Pct Recovery = 106% Analysis Date = 06/25/20 Pct Recovery = 106% Analysis Date = 06/25/20 Pct Recovery = 106% Analysis Date = 06/22/20 Pct Recovery = 107% Analysis Date = 06/22/20 Pct Recovery = 107% Analysis Date = 06/18/20 Pct Recovery = 107% Analysis Date = 06/18/20 Pct Recovery = 107% Analysis Date = 06/14/20 Pct Recovery = 108% Analysis Date = 06/14/20 Pct Recovery = 108% Analysis Date = 06/11/20 Pct Recovery = 109% Analysis Date = 06/11/20 Pct Recovery = 109% Analysis Date = 06/07/20 Pct Recovery = 109% Analysis Date = 06/07/20 Pct Recovery = 109% Analysis Date = 06/03/20 Pct Recovery = 110% Analysis Date = 06/03/20 Pct Recovery = 110% Analysis Date = 05/31/20 Pct Recovery = 110% Analysis Date = 05/31/20 Pct Recovery = 110% Analysis Date = 05/27/20 Pct Recovery = 111% Analysis Date = 05/27/20 Pct Recovery = 111% Analysis Date = 05/23/20 Pct Recovery = 112% Analysis Date = 05/23/20 Pct Recovery = 112% Analysis Date = 05/20/20 Pct Recovery = 112% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR SULFONIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 98% 18% 97% 21%
Total 30 98% 18% 97% 21%

Sample Statistics
ACETOCHLOR SULFONIC ACID

Characteristic N % % Basis
Plotted 30 97% Spiked
Estimated Values 30 97% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 31 .  
False Negatives 0 0% 0 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
ATRAZINE
METHOD: 2447 , TESTIDCODE: 65065LCM60

Laboratory ID = 20213200091 Lab Value = 90.425 Expected Conc. = 42.9 Report level label = 6.8 Pct Recovery = 211% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20203080100 Lab Value = 64.239 Expected Conc. = 85.1 Report level label = 6.8 Pct Recovery = 75% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 81.918 Expected Conc. = 85.1 Report level label = 6.8 Pct Recovery = 96% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 90.235 Expected Conc. = 85.1 Report level label = 6.8 Pct Recovery = 106% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 69.455 Expected Conc. = 85 Report level label = 6.8 Pct Recovery = 82% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 64.624 Expected Conc. = 85 Report level label = 6.8 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 70.350 Expected Conc. = 85 Report level label = 6.8 Pct Recovery = 83% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 88.517 Expected Conc. = 85 Report level label = 6.8 Pct Recovery = 104% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20212990174 Lab Value = 45.455 Expected Conc. = 68.64 Report level label = 6.8 Pct Recovery = 66% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 35.204 Expected Conc. = 68 Report level label = 6.8 Pct Recovery = 52% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220190116 Lab Value = 33.087 Expected Conc. = 68 Report level label = 6.8 Pct Recovery = 49% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 47.861 Expected Conc. = 68 Report level label = 6.8 Pct Recovery = 70% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 37.325 Expected Conc. = 67.6 Report level label = 6.8 Pct Recovery = 55% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220810134 Lab Value = 54.044 Expected Conc. = 66.8 Report level label = 6.8 Pct Recovery = 81% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20213340027 Lab Value = 26.681 Expected Conc. = 42.9 Report level label = 6.8 Pct Recovery = 62% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 27.074 Expected Conc. = 42.9 Report level label = 6.8 Pct Recovery = 63% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202390020 Lab Value = 67.976 Expected Conc. = 42.7 Report level label = 6.8 Pct Recovery = 159% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 42.147 Expected Conc. = 42.7 Report level label = 6.8 Pct Recovery = 99% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202880004 Lab Value = 38.522 Expected Conc. = 42.55 Report level label = 6.8 Pct Recovery = 91% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221730293 Lab Value = 27.273 Expected Conc. = 42.5 Report level label = 6.8 Pct Recovery = 64% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 22.431 Expected Conc. = 42.5 Report level label = 6.8 Pct Recovery = 53% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20210480001 Lab Value = 30.936 Expected Conc. = 42.5 Report level label = 6.8 Pct Recovery = 73% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201550031 Lab Value = 43.769 Expected Conc. = 42.5 Report level label = 6.8 Pct Recovery = 103% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20220810133 Lab Value = 31.711 Expected Conc. = 41.75 Report level label = 6.8 Pct Recovery = 76% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201960104 Lab Value = 41.672 Expected Conc. = 34.16 Report level label = 6.8 Pct Recovery = 122% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 34.957 Expected Conc. = 34.16 Report level label = 6.8 Pct Recovery = 102% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210620006 Lab Value = 29.544 Expected Conc. = 34.04 Report level label = 6.8 Pct Recovery = 87% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 27.227 Expected Conc. = 34.04 Report level label = 6.8 Pct Recovery = 80% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 28.857 Expected Conc. = 34 Report level label = 6.8 Pct Recovery = 85% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20213060210 Lab Value = 13.488 Expected Conc. = 17.16 Report level label = 6.8 Pct Recovery = 79% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210120050 Lab Value = 17.156 Expected Conc. = 17.02 Report level label = 6.8 Pct Recovery = 101% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 19.915 Expected Conc. = 17.02 Report level label = 6.8 Pct Recovery = 117% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 18.548 Expected Conc. = 17.02 Report level label = 6.8 Pct Recovery = 109% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 19.035 Expected Conc. = 17.02 Report level label = 6.8 Pct Recovery = 112% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 16.662 Expected Conc. = 17.02 Report level label = 6.8 Pct Recovery = 98% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222500483 Lab Value = 16.033 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 94% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 13.368 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 79% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210690067 Lab Value = 17.232 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 101% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202330309 Lab Value = 17.310 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 102% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 15.024 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 88% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 18.559 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 109% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 16.612 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 98% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 18.953 Expected Conc. = 17 Report level label = 6.8 Pct Recovery = 111% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20222630205 Lab Value = 14.037 Expected Conc. = 16.7 Report level label = 6.8 Pct Recovery = 84% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Analysis Date = 09/28/22 Pct Recovery = 68% Analysis Date = 09/24/22 Pct Recovery = 68% Analysis Date = 09/24/22 Pct Recovery = 68% Analysis Date = 09/20/22 Pct Recovery = 68% Analysis Date = 09/20/22 Pct Recovery = 68% Analysis Date = 09/16/22 Pct Recovery = 68% Analysis Date = 09/16/22 Pct Recovery = 68% Analysis Date = 09/11/22 Pct Recovery = 69% Analysis Date = 09/11/22 Pct Recovery = 69% Analysis Date = 09/07/22 Pct Recovery = 69% Analysis Date = 09/07/22 Pct Recovery = 69% Analysis Date = 09/03/22 Pct Recovery = 69% Analysis Date = 09/03/22 Pct Recovery = 69% Analysis Date = 08/30/22 Pct Recovery = 69% Analysis Date = 08/30/22 Pct Recovery = 69% Analysis Date = 08/25/22 Pct Recovery = 69% Analysis Date = 08/25/22 Pct Recovery = 69% Analysis Date = 08/21/22 Pct Recovery = 69% Analysis Date = 08/21/22 Pct Recovery = 69% Analysis Date = 08/17/22 Pct Recovery = 70% Analysis Date = 08/17/22 Pct Recovery = 70% Analysis Date = 08/13/22 Pct Recovery = 70% Analysis Date = 08/13/22 Pct Recovery = 70% Analysis Date = 08/08/22 Pct Recovery = 70% Analysis Date = 08/08/22 Pct Recovery = 70% Analysis Date = 08/04/22 Pct Recovery = 70% Analysis Date = 08/04/22 Pct Recovery = 70% Analysis Date = 07/31/22 Pct Recovery = 70% Analysis Date = 07/31/22 Pct Recovery = 70% Analysis Date = 07/27/22 Pct Recovery = 71% Analysis Date = 07/27/22 Pct Recovery = 71% Analysis Date = 07/22/22 Pct Recovery = 71% Analysis Date = 07/22/22 Pct Recovery = 71% Analysis Date = 07/18/22 Pct Recovery = 71% Analysis Date = 07/18/22 Pct Recovery = 71% Analysis Date = 07/14/22 Pct Recovery = 71% Analysis Date = 07/14/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/05/22 Pct Recovery = 71% Analysis Date = 07/05/22 Pct Recovery = 71% Analysis Date = 07/01/22 Pct Recovery = 72% Analysis Date = 07/01/22 Pct Recovery = 72% Analysis Date = 06/27/22 Pct Recovery = 72% Analysis Date = 06/27/22 Pct Recovery = 72% Analysis Date = 06/22/22 Pct Recovery = 72% Analysis Date = 06/22/22 Pct Recovery = 72% Analysis Date = 06/18/22 Pct Recovery = 72% Analysis Date = 06/18/22 Pct Recovery = 72% Analysis Date = 06/14/22 Pct Recovery = 72% Analysis Date = 06/14/22 Pct Recovery = 72% Analysis Date = 06/10/22 Pct Recovery = 73% Analysis Date = 06/10/22 Pct Recovery = 73% Analysis Date = 06/05/22 Pct Recovery = 73% Analysis Date = 06/05/22 Pct Recovery = 73% Analysis Date = 06/01/22 Pct Recovery = 73% Analysis Date = 06/01/22 Pct Recovery = 73% Analysis Date = 05/28/22 Pct Recovery = 73% Analysis Date = 05/28/22 Pct Recovery = 73% Analysis Date = 05/24/22 Pct Recovery = 73% Analysis Date = 05/24/22 Pct Recovery = 73% Analysis Date = 05/19/22 Pct Recovery = 73% Analysis Date = 05/19/22 Pct Recovery = 73% Analysis Date = 05/15/22 Pct Recovery = 74% Analysis Date = 05/15/22 Pct Recovery = 74% Analysis Date = 05/11/22 Pct Recovery = 74% Analysis Date = 05/11/22 Pct Recovery = 74% Analysis Date = 05/06/22 Pct Recovery = 74% Analysis Date = 05/06/22 Pct Recovery = 74% Analysis Date = 05/02/22 Pct Recovery = 74% Analysis Date = 05/02/22 Pct Recovery = 74% Analysis Date = 04/28/22 Pct Recovery = 74% Analysis Date = 04/28/22 Pct Recovery = 74% Analysis Date = 04/24/22 Pct Recovery = 75% Analysis Date = 04/24/22 Pct Recovery = 75% Analysis Date = 04/19/22 Pct Recovery = 75% Analysis Date = 04/19/22 Pct Recovery = 75% Analysis Date = 04/15/22 Pct Recovery = 75% Analysis Date = 04/15/22 Pct Recovery = 75% Analysis Date = 04/11/22 Pct Recovery = 75% Analysis Date = 04/11/22 Pct Recovery = 75% Analysis Date = 04/07/22 Pct Recovery = 75% Analysis Date = 04/07/22 Pct Recovery = 75% Analysis Date = 04/02/22 Pct Recovery = 75% Analysis Date = 04/02/22 Pct Recovery = 75% Analysis Date = 03/29/22 Pct Recovery = 76% Analysis Date = 03/29/22 Pct Recovery = 76% Analysis Date = 03/25/22 Pct Recovery = 76% Analysis Date = 03/25/22 Pct Recovery = 76% Analysis Date = 03/21/22 Pct Recovery = 76% Analysis Date = 03/21/22 Pct Recovery = 76% Analysis Date = 03/16/22 Pct Recovery = 76% Analysis Date = 03/16/22 Pct Recovery = 76% Analysis Date = 03/12/22 Pct Recovery = 77% Analysis Date = 03/12/22 Pct Recovery = 77% Analysis Date = 03/08/22 Pct Recovery = 77% Analysis Date = 03/08/22 Pct Recovery = 77% Analysis Date = 03/04/22 Pct Recovery = 77% Analysis Date = 03/04/22 Pct Recovery = 77% Analysis Date = 02/27/22 Pct Recovery = 77% Analysis Date = 02/27/22 Pct Recovery = 77% Analysis Date = 02/23/22 Pct Recovery = 77% Analysis Date = 02/23/22 Pct Recovery = 77% Analysis Date = 02/19/22 Pct Recovery = 78% Analysis Date = 02/19/22 Pct Recovery = 78% Analysis Date = 02/14/22 Pct Recovery = 78% Analysis Date = 02/14/22 Pct Recovery = 78% Analysis Date = 02/10/22 Pct Recovery = 78% Analysis Date = 02/10/22 Pct Recovery = 78% Analysis Date = 02/06/22 Pct Recovery = 78% Analysis Date = 02/06/22 Pct Recovery = 78% Analysis Date = 02/02/22 Pct Recovery = 78% Analysis Date = 02/02/22 Pct Recovery = 78% Analysis Date = 01/28/22 Pct Recovery = 79% Analysis Date = 01/28/22 Pct Recovery = 79% Analysis Date = 01/24/22 Pct Recovery = 79% Analysis Date = 01/24/22 Pct Recovery = 79% Analysis Date = 01/20/22 Pct Recovery = 79% Analysis Date = 01/20/22 Pct Recovery = 79% Analysis Date = 01/16/22 Pct Recovery = 80% Analysis Date = 01/16/22 Pct Recovery = 80% Analysis Date = 01/11/22 Pct Recovery = 80% Analysis Date = 01/11/22 Pct Recovery = 80% Analysis Date = 01/07/22 Pct Recovery = 80% Analysis Date = 01/07/22 Pct Recovery = 80% Analysis Date = 01/03/22 Pct Recovery = 81% Analysis Date = 01/03/22 Pct Recovery = 81% Analysis Date = 12/30/21 Pct Recovery = 81% Analysis Date = 12/30/21 Pct Recovery = 81% Analysis Date = 12/25/21 Pct Recovery = 81% Analysis Date = 12/25/21 Pct Recovery = 81% Analysis Date = 12/21/21 Pct Recovery = 81% Analysis Date = 12/21/21 Pct Recovery = 81% Analysis Date = 12/17/21 Pct Recovery = 82% Analysis Date = 12/17/21 Pct Recovery = 82% Analysis Date = 12/12/21 Pct Recovery = 82% Analysis Date = 12/12/21 Pct Recovery = 82% Analysis Date = 12/08/21 Pct Recovery = 82% Analysis Date = 12/08/21 Pct Recovery = 82% Analysis Date = 12/04/21 Pct Recovery = 82% Analysis Date = 12/04/21 Pct Recovery = 82% Analysis Date = 11/30/21 Pct Recovery = 82% Analysis Date = 11/30/21 Pct Recovery = 82% Analysis Date = 11/25/21 Pct Recovery = 83% Analysis Date = 11/25/21 Pct Recovery = 83% Analysis Date = 11/21/21 Pct Recovery = 83% Analysis Date = 11/21/21 Pct Recovery = 83% Analysis Date = 11/17/21 Pct Recovery = 83% Analysis Date = 11/17/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/08/21 Pct Recovery = 83% Analysis Date = 11/08/21 Pct Recovery = 83% Analysis Date = 11/04/21 Pct Recovery = 83% Analysis Date = 11/04/21 Pct Recovery = 83% Analysis Date = 10/31/21 Pct Recovery = 83% Analysis Date = 10/31/21 Pct Recovery = 83% Analysis Date = 10/27/21 Pct Recovery = 83% Analysis Date = 10/27/21 Pct Recovery = 83% Analysis Date = 10/22/21 Pct Recovery = 83% Analysis Date = 10/22/21 Pct Recovery = 83% Analysis Date = 10/18/21 Pct Recovery = 83% Analysis Date = 10/18/21 Pct Recovery = 83% Analysis Date = 10/14/21 Pct Recovery = 83% Analysis Date = 10/14/21 Pct Recovery = 83% Analysis Date = 10/10/21 Pct Recovery = 83% Analysis Date = 10/10/21 Pct Recovery = 83% Analysis Date = 10/05/21 Pct Recovery = 83% Analysis Date = 10/05/21 Pct Recovery = 83% Analysis Date = 10/01/21 Pct Recovery = 83% Analysis Date = 10/01/21 Pct Recovery = 83% Analysis Date = 09/27/21 Pct Recovery = 83% Analysis Date = 09/27/21 Pct Recovery = 83% Analysis Date = 09/22/21 Pct Recovery = 83% Analysis Date = 09/22/21 Pct Recovery = 83% Analysis Date = 09/18/21 Pct Recovery = 83% Analysis Date = 09/18/21 Pct Recovery = 83% Analysis Date = 09/14/21 Pct Recovery = 83% Analysis Date = 09/14/21 Pct Recovery = 83% Analysis Date = 09/10/21 Pct Recovery = 83% Analysis Date = 09/10/21 Pct Recovery = 83% Analysis Date = 09/05/21 Pct Recovery = 83% Analysis Date = 09/05/21 Pct Recovery = 83% Analysis Date = 09/01/21 Pct Recovery = 83% Analysis Date = 09/01/21 Pct Recovery = 83% Analysis Date = 08/28/21 Pct Recovery = 83% Analysis Date = 08/28/21 Pct Recovery = 83% Analysis Date = 08/24/21 Pct Recovery = 83% Analysis Date = 08/24/21 Pct Recovery = 83% Analysis Date = 08/19/21 Pct Recovery = 83% Analysis Date = 08/19/21 Pct Recovery = 83% Analysis Date = 08/15/21 Pct Recovery = 83% Analysis Date = 08/15/21 Pct Recovery = 83% Analysis Date = 08/11/21 Pct Recovery = 83% Analysis Date = 08/11/21 Pct Recovery = 83% Analysis Date = 08/07/21 Pct Recovery = 83% Analysis Date = 08/07/21 Pct Recovery = 83% Analysis Date = 08/02/21 Pct Recovery = 84% Analysis Date = 08/02/21 Pct Recovery = 84% Analysis Date = 07/29/21 Pct Recovery = 84% Analysis Date = 07/29/21 Pct Recovery = 84% Analysis Date = 07/25/21 Pct Recovery = 84% Analysis Date = 07/25/21 Pct Recovery = 84% Analysis Date = 07/20/21 Pct Recovery = 84% Analysis Date = 07/20/21 Pct Recovery = 84% Analysis Date = 07/16/21 Pct Recovery = 84% Analysis Date = 07/16/21 Pct Recovery = 84% Analysis Date = 07/12/21 Pct Recovery = 84% Analysis Date = 07/12/21 Pct Recovery = 84% Analysis Date = 07/08/21 Pct Recovery = 84% Analysis Date = 07/08/21 Pct Recovery = 84% Analysis Date = 07/03/21 Pct Recovery = 84% Analysis Date = 07/03/21 Pct Recovery = 84% Analysis Date = 06/29/21 Pct Recovery = 84% Analysis Date = 06/29/21 Pct Recovery = 84% Analysis Date = 06/25/21 Pct Recovery = 84% Analysis Date = 06/25/21 Pct Recovery = 84% Analysis Date = 06/21/21 Pct Recovery = 84% Analysis Date = 06/21/21 Pct Recovery = 84% Analysis Date = 06/16/21 Pct Recovery = 84% Analysis Date = 06/16/21 Pct Recovery = 84% Analysis Date = 06/12/21 Pct Recovery = 84% Analysis Date = 06/12/21 Pct Recovery = 84% Analysis Date = 06/08/21 Pct Recovery = 84% Analysis Date = 06/08/21 Pct Recovery = 84% Analysis Date = 06/04/21 Pct Recovery = 84% Analysis Date = 06/04/21 Pct Recovery = 84% Analysis Date = 05/30/21 Pct Recovery = 84% Analysis Date = 05/30/21 Pct Recovery = 84% Analysis Date = 05/26/21 Pct Recovery = 84% Analysis Date = 05/26/21 Pct Recovery = 84% Analysis Date = 05/22/21 Pct Recovery = 84% Analysis Date = 05/22/21 Pct Recovery = 84% Analysis Date = 05/17/21 Pct Recovery = 84% Analysis Date = 05/17/21 Pct Recovery = 84% Analysis Date = 05/13/21 Pct Recovery = 84% Analysis Date = 05/13/21 Pct Recovery = 84% Analysis Date = 05/09/21 Pct Recovery = 84% Analysis Date = 05/09/21 Pct Recovery = 84% Analysis Date = 05/05/21 Pct Recovery = 84% Analysis Date = 05/05/21 Pct Recovery = 84% Analysis Date = 04/30/21 Pct Recovery = 84% Analysis Date = 04/30/21 Pct Recovery = 84% Analysis Date = 04/26/21 Pct Recovery = 84% Analysis Date = 04/26/21 Pct Recovery = 84% Analysis Date = 04/22/21 Pct Recovery = 84% Analysis Date = 04/22/21 Pct Recovery = 84% Analysis Date = 04/18/21 Pct Recovery = 84% Analysis Date = 04/18/21 Pct Recovery = 84% Analysis Date = 04/13/21 Pct Recovery = 84% Analysis Date = 04/13/21 Pct Recovery = 84% Analysis Date = 04/09/21 Pct Recovery = 85% Analysis Date = 04/09/21 Pct Recovery = 85% Analysis Date = 04/05/21 Pct Recovery = 85% Analysis Date = 04/05/21 Pct Recovery = 85% Analysis Date = 04/01/21 Pct Recovery = 85% Analysis Date = 04/01/21 Pct Recovery = 85% Analysis Date = 03/27/21 Pct Recovery = 86% Analysis Date = 03/27/21 Pct Recovery = 86% Analysis Date = 03/23/21 Pct Recovery = 86% Analysis Date = 03/23/21 Pct Recovery = 86% Analysis Date = 03/19/21 Pct Recovery = 86% Analysis Date = 03/19/21 Pct Recovery = 86% Analysis Date = 03/15/21 Pct Recovery = 87% Analysis Date = 03/15/21 Pct Recovery = 87% Analysis Date = 03/10/21 Pct Recovery = 87% Analysis Date = 03/10/21 Pct Recovery = 87% Analysis Date = 03/06/21 Pct Recovery = 87% Analysis Date = 03/06/21 Pct Recovery = 87% Analysis Date = 03/02/21 Pct Recovery = 88% Analysis Date = 03/02/21 Pct Recovery = 88% Analysis Date = 02/25/21 Pct Recovery = 88% Analysis Date = 02/25/21 Pct Recovery = 88% Analysis Date = 02/21/21 Pct Recovery = 89% Analysis Date = 02/21/21 Pct Recovery = 89% Analysis Date = 02/17/21 Pct Recovery = 89% Analysis Date = 02/17/21 Pct Recovery = 89% Analysis Date = 02/13/21 Pct Recovery = 90% Analysis Date = 02/13/21 Pct Recovery = 90% Analysis Date = 02/08/21 Pct Recovery = 90% Analysis Date = 02/08/21 Pct Recovery = 90% Analysis Date = 02/04/21 Pct Recovery = 91% Analysis Date = 02/04/21 Pct Recovery = 91% Analysis Date = 01/31/21 Pct Recovery = 91% Analysis Date = 01/31/21 Pct Recovery = 91% Analysis Date = 01/27/21 Pct Recovery = 92% Analysis Date = 01/27/21 Pct Recovery = 92% Analysis Date = 01/22/21 Pct Recovery = 92% Analysis Date = 01/22/21 Pct Recovery = 92% Analysis Date = 01/18/21 Pct Recovery = 92% Analysis Date = 01/18/21 Pct Recovery = 92% Analysis Date = 01/14/21 Pct Recovery = 93% Analysis Date = 01/14/21 Pct Recovery = 93% Analysis Date = 01/10/21 Pct Recovery = 93% Analysis Date = 01/10/21 Pct Recovery = 93% Analysis Date = 01/05/21 Pct Recovery = 94% Analysis Date = 01/05/21 Pct Recovery = 94% Analysis Date = 01/01/21 Pct Recovery = 94% Analysis Date = 01/01/21 Pct Recovery = 94% Analysis Date = 12/28/20 Pct Recovery = 95% Analysis Date = 12/28/20 Pct Recovery = 95% Analysis Date = 12/23/20 Pct Recovery = 95% Analysis Date = 12/23/20 Pct Recovery = 95% Analysis Date = 12/19/20 Pct Recovery = 96% Analysis Date = 12/19/20 Pct Recovery = 96% Analysis Date = 12/15/20 Pct Recovery = 96% Analysis Date = 12/15/20 Pct Recovery = 96% Analysis Date = 12/11/20 Pct Recovery = 97% Analysis Date = 12/11/20 Pct Recovery = 97% Analysis Date = 12/06/20 Pct Recovery = 97% Analysis Date = 12/06/20 Pct Recovery = 97% Analysis Date = 12/02/20 Pct Recovery = 98% Analysis Date = 12/02/20 Pct Recovery = 98% Analysis Date = 11/28/20 Pct Recovery = 98% Analysis Date = 11/28/20 Pct Recovery = 98% Analysis Date = 11/24/20 Pct Recovery = 99% Analysis Date = 11/24/20 Pct Recovery = 99% Analysis Date = 11/19/20 Pct Recovery = 99% Analysis Date = 11/19/20 Pct Recovery = 99% Analysis Date = 11/15/20 Pct Recovery = 99% Analysis Date = 11/15/20 Pct Recovery = 99% Analysis Date = 11/11/20 Pct Recovery = 100% Analysis Date = 11/11/20 Pct Recovery = 100% Analysis Date = 11/07/20 Pct Recovery = 100% Analysis Date = 11/07/20 Pct Recovery = 100% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/25/20 Pct Recovery = 102% Analysis Date = 10/25/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/16/20 Pct Recovery = 103% Analysis Date = 10/16/20 Pct Recovery = 103% Analysis Date = 10/12/20 Pct Recovery = 103% Analysis Date = 10/12/20 Pct Recovery = 103% Analysis Date = 10/08/20 Pct Recovery = 103% Analysis Date = 10/08/20 Pct Recovery = 103% Analysis Date = 10/03/20 Pct Recovery = 103% Analysis Date = 10/03/20 Pct Recovery = 103% Analysis Date = 09/29/20 Pct Recovery = 103% Analysis Date = 09/29/20 Pct Recovery = 103% Analysis Date = 09/25/20 Pct Recovery = 104% Analysis Date = 09/25/20 Pct Recovery = 104% Analysis Date = 09/21/20 Pct Recovery = 104% Analysis Date = 09/21/20 Pct Recovery = 104% Analysis Date = 09/16/20 Pct Recovery = 104% Analysis Date = 09/16/20 Pct Recovery = 104% Analysis Date = 09/12/20 Pct Recovery = 104% Analysis Date = 09/12/20 Pct Recovery = 104% Analysis Date = 09/08/20 Pct Recovery = 104% Analysis Date = 09/08/20 Pct Recovery = 104% Analysis Date = 09/04/20 Pct Recovery = 105% Analysis Date = 09/04/20 Pct Recovery = 105% Analysis Date = 08/30/20 Pct Recovery = 105% Analysis Date = 08/30/20 Pct Recovery = 105% Analysis Date = 08/26/20 Pct Recovery = 105% Analysis Date = 08/26/20 Pct Recovery = 105% Analysis Date = 08/22/20 Pct Recovery = 105% Analysis Date = 08/22/20 Pct Recovery = 105% Analysis Date = 08/18/20 Pct Recovery = 105% Analysis Date = 08/18/20 Pct Recovery = 105% Analysis Date = 08/13/20 Pct Recovery = 106% Analysis Date = 08/13/20 Pct Recovery = 106% Analysis Date = 08/09/20 Pct Recovery = 106% Analysis Date = 08/09/20 Pct Recovery = 106% Analysis Date = 08/05/20 Pct Recovery = 106% Analysis Date = 08/05/20 Pct Recovery = 106% Analysis Date = 07/31/20 Pct Recovery = 106% Analysis Date = 07/31/20 Pct Recovery = 106% Analysis Date = 07/27/20 Pct Recovery = 106% Analysis Date = 07/27/20 Pct Recovery = 106% Analysis Date = 07/23/20 Pct Recovery = 107% Analysis Date = 07/23/20 Pct Recovery = 107% Analysis Date = 07/19/20 Pct Recovery = 107% Analysis Date = 07/19/20 Pct Recovery = 107% Analysis Date = 07/14/20 Pct Recovery = 107% Analysis Date = 07/14/20 Pct Recovery = 107% Analysis Date = 07/10/20 Pct Recovery = 107% Analysis Date = 07/10/20 Pct Recovery = 107% Analysis Date = 07/06/20 Pct Recovery = 107% Analysis Date = 07/06/20 Pct Recovery = 107% Analysis Date = 07/02/20 Pct Recovery = 108% Analysis Date = 07/02/20 Pct Recovery = 108% Analysis Date = 06/27/20 Pct Recovery = 108% Analysis Date = 06/27/20 Pct Recovery = 108% Analysis Date = 06/23/20 Pct Recovery = 108% Analysis Date = 06/23/20 Pct Recovery = 108% Analysis Date = 06/19/20 Pct Recovery = 108% Analysis Date = 06/19/20 Pct Recovery = 108% Analysis Date = 06/15/20 Pct Recovery = 108% Analysis Date = 06/15/20 Pct Recovery = 108% Analysis Date = 06/10/20 Pct Recovery = 108% Analysis Date = 06/10/20 Pct Recovery = 108% Analysis Date = 06/06/20 Pct Recovery = 109% Analysis Date = 06/06/20 Pct Recovery = 109% Analysis Date = 06/02/20 Pct Recovery = 109% Analysis Date = 06/02/20 Pct Recovery = 109% Analysis Date = 05/29/20 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 91% 28% 88% 20%
Total 44 91% 28% 88% 20%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 8 18% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 72 .  
False Positives 2 3% 2 out of 72

OBSP Determination:
AZOXYSTROBIN
METHOD: 2447 , TESTIDCODE: 66589LCM60

Laboratory ID = 20210760015 Lab Value = 28.261 Expected Conc. = 37.43 Report level label = 3 Pct Recovery = 76% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 29.569 Expected Conc. = 37.43 Report level label = 3 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 33.082 Expected Conc. = 37.43 Report level label = 3 Pct Recovery = 88% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 37.512 Expected Conc. = 37.43 Report level label = 3 Pct Recovery = 100% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 27.630 Expected Conc. = 37 Report level label = 3 Pct Recovery = 75% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 38.290 Expected Conc. = 37 Report level label = 3 Pct Recovery = 103% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 37.910 Expected Conc. = 37 Report level label = 3 Pct Recovery = 102% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20220190116 Lab Value = 16.316 Expected Conc. = 30.4 Report level label = 3 Pct Recovery = 54% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 20.240 Expected Conc. = 30.4 Report level label = 3 Pct Recovery = 67% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 14.626 Expected Conc. = 30.32 Report level label = 3 Pct Recovery = 48% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20212990174 Lab Value = 19.306 Expected Conc. = 30.08 Report level label = 3 Pct Recovery = 64% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 11.159 Expected Conc. = 30 Report level label = 3 Pct Recovery = 37% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 21.936 Expected Conc. = 30 Report level label = 3 Pct Recovery = 73% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20221730293 Lab Value = 14.342 Expected Conc. = 19 Report level label = 3 Pct Recovery = 75% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 10.557 Expected Conc. = 19 Report level label = 3 Pct Recovery = 56% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20201550031 Lab Value = 19.824 Expected Conc. = 18.95 Report level label = 3 Pct Recovery = 105% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20213340027 Lab Value = 11.738 Expected Conc. = 18.8 Report level label = 3 Pct Recovery = 62% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 32.256 Expected Conc. = 18.8 Report level label = 3 Pct Recovery = 172% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 11.344 Expected Conc. = 18.8 Report level label = 3 Pct Recovery = 60% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20220810133 Lab Value = 12.766 Expected Conc. = 18.75 Report level label = 3 Pct Recovery = 68% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20210480001 Lab Value = 15.054 Expected Conc. = 18.715 Report level label = 3 Pct Recovery = 80% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202880004 Lab Value = 18.351 Expected Conc. = 18.5 Report level label = 3 Pct Recovery = 99% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202390020 Lab Value = 22.821 Expected Conc. = 18.45 Report level label = 3 Pct Recovery = 124% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 17.040 Expected Conc. = 18.45 Report level label = 3 Pct Recovery = 92% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20210900005 Lab Value = 11.880 Expected Conc. = 14.972 Report level label = 3 Pct Recovery = 79% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 12.106 Expected Conc. = 14.8 Report level label = 3 Pct Recovery = 82% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 14.324 Expected Conc. = 14.8 Report level label = 3 Pct Recovery = 97% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 18.182 Expected Conc. = 14.76 Report level label = 3 Pct Recovery = 123% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 16.622 Expected Conc. = 14.76 Report level label = 3 Pct Recovery = 113% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20222500483 Lab Value = 5.293 Expected Conc. = 7.6 Report level label = 3 Pct Recovery = 70% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 4.761 Expected Conc. = 7.6 Report level label = 3 Pct Recovery = 63% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20202330309 Lab Value = 6.136 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 81% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 6.095 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 80% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 8.672 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 114% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 8.379 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 111% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 7.789 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 103% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20213060210 Lab Value = 3.975 Expected Conc. = 7.52 Report level label = 3 Pct Recovery = 53% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222630205 Lab Value = 6.036 Expected Conc. = 7.5 Report level label = 3 Pct Recovery = 80% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210690067 Lab Value = 6.951 Expected Conc. = 7.486 Report level label = 3 Pct Recovery = 93% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203530076 Lab Value = 7.106 Expected Conc. = 7.4 Report level label = 3 Pct Recovery = 96% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.663 Expected Conc. = 7.4 Report level label = 3 Pct Recovery = 104% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 7.451 Expected Conc. = 7.4 Report level label = 3 Pct Recovery = 101% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 7.465 Expected Conc. = 7.4 Report level label = 3 Pct Recovery = 101% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 09/28/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 61% Analysis Date = 09/16/22 Pct Recovery = 61% Analysis Date = 09/16/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 62% Analysis Date = 09/03/22 Pct Recovery = 62% Analysis Date = 08/30/22 Pct Recovery = 62% Analysis Date = 08/30/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/17/22 Pct Recovery = 62% Analysis Date = 08/17/22 Pct Recovery = 62% Analysis Date = 08/13/22 Pct Recovery = 62% Analysis Date = 08/13/22 Pct Recovery = 62% Analysis Date = 08/08/22 Pct Recovery = 63% Analysis Date = 08/08/22 Pct Recovery = 63% Analysis Date = 08/04/22 Pct Recovery = 63% Analysis Date = 08/04/22 Pct Recovery = 63% Analysis Date = 07/31/22 Pct Recovery = 63% Analysis Date = 07/31/22 Pct Recovery = 63% Analysis Date = 07/27/22 Pct Recovery = 63% Analysis Date = 07/27/22 Pct Recovery = 63% Analysis Date = 07/22/22 Pct Recovery = 63% Analysis Date = 07/22/22 Pct Recovery = 63% Analysis Date = 07/18/22 Pct Recovery = 63% Analysis Date = 07/18/22 Pct Recovery = 63% Analysis Date = 07/14/22 Pct Recovery = 64% Analysis Date = 07/14/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/05/22 Pct Recovery = 64% Analysis Date = 07/05/22 Pct Recovery = 64% Analysis Date = 07/01/22 Pct Recovery = 64% Analysis Date = 07/01/22 Pct Recovery = 64% Analysis Date = 06/27/22 Pct Recovery = 64% Analysis Date = 06/27/22 Pct Recovery = 64% Analysis Date = 06/22/22 Pct Recovery = 64% Analysis Date = 06/22/22 Pct Recovery = 64% Analysis Date = 06/18/22 Pct Recovery = 65% Analysis Date = 06/18/22 Pct Recovery = 65% Analysis Date = 06/14/22 Pct Recovery = 65% Analysis Date = 06/14/22 Pct Recovery = 65% Analysis Date = 06/10/22 Pct Recovery = 65% Analysis Date = 06/10/22 Pct Recovery = 65% Analysis Date = 06/05/22 Pct Recovery = 65% Analysis Date = 06/05/22 Pct Recovery = 65% Analysis Date = 06/01/22 Pct Recovery = 65% Analysis Date = 06/01/22 Pct Recovery = 65% Analysis Date = 05/28/22 Pct Recovery = 65% Analysis Date = 05/28/22 Pct Recovery = 65% Analysis Date = 05/24/22 Pct Recovery = 66% Analysis Date = 05/24/22 Pct Recovery = 66% Analysis Date = 05/19/22 Pct Recovery = 66% Analysis Date = 05/19/22 Pct Recovery = 66% Analysis Date = 05/15/22 Pct Recovery = 66% Analysis Date = 05/15/22 Pct Recovery = 66% Analysis Date = 05/11/22 Pct Recovery = 66% Analysis Date = 05/11/22 Pct Recovery = 66% Analysis Date = 05/06/22 Pct Recovery = 66% Analysis Date = 05/06/22 Pct Recovery = 66% Analysis Date = 05/02/22 Pct Recovery = 66% Analysis Date = 05/02/22 Pct Recovery = 66% Analysis Date = 04/28/22 Pct Recovery = 67% Analysis Date = 04/28/22 Pct Recovery = 67% Analysis Date = 04/24/22 Pct Recovery = 67% Analysis Date = 04/24/22 Pct Recovery = 67% Analysis Date = 04/19/22 Pct Recovery = 67% Analysis Date = 04/19/22 Pct Recovery = 67% Analysis Date = 04/15/22 Pct Recovery = 67% Analysis Date = 04/15/22 Pct Recovery = 67% Analysis Date = 04/11/22 Pct Recovery = 67% Analysis Date = 04/11/22 Pct Recovery = 67% Analysis Date = 04/07/22 Pct Recovery = 67% Analysis Date = 04/07/22 Pct Recovery = 67% Analysis Date = 04/02/22 Pct Recovery = 68% Analysis Date = 04/02/22 Pct Recovery = 68% Analysis Date = 03/29/22 Pct Recovery = 68% Analysis Date = 03/29/22 Pct Recovery = 68% Analysis Date = 03/25/22 Pct Recovery = 68% Analysis Date = 03/25/22 Pct Recovery = 68% Analysis Date = 03/21/22 Pct Recovery = 68% Analysis Date = 03/21/22 Pct Recovery = 68% Analysis Date = 03/16/22 Pct Recovery = 68% Analysis Date = 03/16/22 Pct Recovery = 68% Analysis Date = 03/12/22 Pct Recovery = 69% Analysis Date = 03/12/22 Pct Recovery = 69% Analysis Date = 03/08/22 Pct Recovery = 69% Analysis Date = 03/08/22 Pct Recovery = 69% Analysis Date = 03/04/22 Pct Recovery = 69% Analysis Date = 03/04/22 Pct Recovery = 69% Analysis Date = 02/27/22 Pct Recovery = 69% Analysis Date = 02/27/22 Pct Recovery = 69% Analysis Date = 02/23/22 Pct Recovery = 69% Analysis Date = 02/23/22 Pct Recovery = 69% Analysis Date = 02/19/22 Pct Recovery = 70% Analysis Date = 02/19/22 Pct Recovery = 70% Analysis Date = 02/14/22 Pct Recovery = 70% Analysis Date = 02/14/22 Pct Recovery = 70% Analysis Date = 02/10/22 Pct Recovery = 70% Analysis Date = 02/10/22 Pct Recovery = 70% Analysis Date = 02/06/22 Pct Recovery = 70% Analysis Date = 02/06/22 Pct Recovery = 70% Analysis Date = 02/02/22 Pct Recovery = 70% Analysis Date = 02/02/22 Pct Recovery = 70% Analysis Date = 01/28/22 Pct Recovery = 71% Analysis Date = 01/28/22 Pct Recovery = 71% Analysis Date = 01/24/22 Pct Recovery = 71% Analysis Date = 01/24/22 Pct Recovery = 71% Analysis Date = 01/20/22 Pct Recovery = 71% Analysis Date = 01/20/22 Pct Recovery = 71% Analysis Date = 01/16/22 Pct Recovery = 71% Analysis Date = 01/16/22 Pct Recovery = 71% Analysis Date = 01/11/22 Pct Recovery = 71% Analysis Date = 01/11/22 Pct Recovery = 71% Analysis Date = 01/07/22 Pct Recovery = 72% Analysis Date = 01/07/22 Pct Recovery = 72% Analysis Date = 01/03/22 Pct Recovery = 72% Analysis Date = 01/03/22 Pct Recovery = 72% Analysis Date = 12/30/21 Pct Recovery = 72% Analysis Date = 12/30/21 Pct Recovery = 72% Analysis Date = 12/25/21 Pct Recovery = 72% Analysis Date = 12/25/21 Pct Recovery = 72% Analysis Date = 12/21/21 Pct Recovery = 73% Analysis Date = 12/21/21 Pct Recovery = 73% Analysis Date = 12/17/21 Pct Recovery = 73% Analysis Date = 12/17/21 Pct Recovery = 73% Analysis Date = 12/12/21 Pct Recovery = 73% Analysis Date = 12/12/21 Pct Recovery = 73% Analysis Date = 12/08/21 Pct Recovery = 73% Analysis Date = 12/08/21 Pct Recovery = 73% Analysis Date = 12/04/21 Pct Recovery = 73% Analysis Date = 12/04/21 Pct Recovery = 73% Analysis Date = 11/30/21 Pct Recovery = 73% Analysis Date = 11/30/21 Pct Recovery = 73% Analysis Date = 11/25/21 Pct Recovery = 74% Analysis Date = 11/25/21 Pct Recovery = 74% Analysis Date = 11/21/21 Pct Recovery = 74% Analysis Date = 11/21/21 Pct Recovery = 74% Analysis Date = 11/17/21 Pct Recovery = 74% Analysis Date = 11/17/21 Pct Recovery = 74% Analysis Date = 11/13/21 Pct Recovery = 74% Analysis Date = 11/13/21 Pct Recovery = 74% Analysis Date = 11/08/21 Pct Recovery = 74% Analysis Date = 11/08/21 Pct Recovery = 74% Analysis Date = 11/04/21 Pct Recovery = 74% Analysis Date = 11/04/21 Pct Recovery = 74% Analysis Date = 10/31/21 Pct Recovery = 75% Analysis Date = 10/31/21 Pct Recovery = 75% Analysis Date = 10/27/21 Pct Recovery = 75% Analysis Date = 10/27/21 Pct Recovery = 75% Analysis Date = 10/22/21 Pct Recovery = 75% Analysis Date = 10/22/21 Pct Recovery = 75% Analysis Date = 10/18/21 Pct Recovery = 75% Analysis Date = 10/18/21 Pct Recovery = 75% Analysis Date = 10/14/21 Pct Recovery = 75% Analysis Date = 10/14/21 Pct Recovery = 75% Analysis Date = 10/10/21 Pct Recovery = 76% Analysis Date = 10/10/21 Pct Recovery = 76% Analysis Date = 10/05/21 Pct Recovery = 76% Analysis Date = 10/05/21 Pct Recovery = 76% Analysis Date = 10/01/21 Pct Recovery = 76% Analysis Date = 10/01/21 Pct Recovery = 76% Analysis Date = 09/27/21 Pct Recovery = 76% Analysis Date = 09/27/21 Pct Recovery = 76% Analysis Date = 09/22/21 Pct Recovery = 76% Analysis Date = 09/22/21 Pct Recovery = 76% Analysis Date = 09/18/21 Pct Recovery = 76% Analysis Date = 09/18/21 Pct Recovery = 76% Analysis Date = 09/14/21 Pct Recovery = 77% Analysis Date = 09/14/21 Pct Recovery = 77% Analysis Date = 09/10/21 Pct Recovery = 77% Analysis Date = 09/10/21 Pct Recovery = 77% Analysis Date = 09/05/21 Pct Recovery = 77% Analysis Date = 09/05/21 Pct Recovery = 77% Analysis Date = 09/01/21 Pct Recovery = 77% Analysis Date = 09/01/21 Pct Recovery = 77% Analysis Date = 08/28/21 Pct Recovery = 77% Analysis Date = 08/28/21 Pct Recovery = 77% Analysis Date = 08/24/21 Pct Recovery = 77% Analysis Date = 08/24/21 Pct Recovery = 77% Analysis Date = 08/19/21 Pct Recovery = 78% Analysis Date = 08/19/21 Pct Recovery = 78% Analysis Date = 08/15/21 Pct Recovery = 78% Analysis Date = 08/15/21 Pct Recovery = 78% Analysis Date = 08/11/21 Pct Recovery = 78% Analysis Date = 08/11/21 Pct Recovery = 78% Analysis Date = 08/07/21 Pct Recovery = 78% Analysis Date = 08/07/21 Pct Recovery = 78% Analysis Date = 08/02/21 Pct Recovery = 78% Analysis Date = 08/02/21 Pct Recovery = 78% Analysis Date = 07/29/21 Pct Recovery = 78% Analysis Date = 07/29/21 Pct Recovery = 78% Analysis Date = 07/25/21 Pct Recovery = 79% Analysis Date = 07/25/21 Pct Recovery = 79% Analysis Date = 07/20/21 Pct Recovery = 79% Analysis Date = 07/20/21 Pct Recovery = 79% Analysis Date = 07/16/21 Pct Recovery = 79% Analysis Date = 07/16/21 Pct Recovery = 79% Analysis Date = 07/12/21 Pct Recovery = 79% Analysis Date = 07/12/21 Pct Recovery = 79% Analysis Date = 07/08/21 Pct Recovery = 79% Analysis Date = 07/08/21 Pct Recovery = 79% Analysis Date = 07/03/21 Pct Recovery = 79% Analysis Date = 07/03/21 Pct Recovery = 79% Analysis Date = 06/29/21 Pct Recovery = 80% Analysis Date = 06/29/21 Pct Recovery = 80% Analysis Date = 06/25/21 Pct Recovery = 80% Analysis Date = 06/25/21 Pct Recovery = 80% Analysis Date = 06/21/21 Pct Recovery = 80% Analysis Date = 06/21/21 Pct Recovery = 80% Analysis Date = 06/16/21 Pct Recovery = 80% Analysis Date = 06/16/21 Pct Recovery = 80% Analysis Date = 06/12/21 Pct Recovery = 80% Analysis Date = 06/12/21 Pct Recovery = 80% Analysis Date = 06/08/21 Pct Recovery = 81% Analysis Date = 06/08/21 Pct Recovery = 81% Analysis Date = 06/04/21 Pct Recovery = 81% Analysis Date = 06/04/21 Pct Recovery = 81% Analysis Date = 05/30/21 Pct Recovery = 81% Analysis Date = 05/30/21 Pct Recovery = 81% Analysis Date = 05/26/21 Pct Recovery = 81% Analysis Date = 05/26/21 Pct Recovery = 81% Analysis Date = 05/22/21 Pct Recovery = 81% Analysis Date = 05/22/21 Pct Recovery = 81% Analysis Date = 05/17/21 Pct Recovery = 81% Analysis Date = 05/17/21 Pct Recovery = 81% Analysis Date = 05/13/21 Pct Recovery = 82% Analysis Date = 05/13/21 Pct Recovery = 82% Analysis Date = 05/09/21 Pct Recovery = 82% Analysis Date = 05/09/21 Pct Recovery = 82% Analysis Date = 05/05/21 Pct Recovery = 82% Analysis Date = 05/05/21 Pct Recovery = 82% Analysis Date = 04/30/21 Pct Recovery = 82% Analysis Date = 04/30/21 Pct Recovery = 82% Analysis Date = 04/26/21 Pct Recovery = 82% Analysis Date = 04/26/21 Pct Recovery = 82% Analysis Date = 04/22/21 Pct Recovery = 82% Analysis Date = 04/22/21 Pct Recovery = 82% Analysis Date = 04/18/21 Pct Recovery = 83% Analysis Date = 04/18/21 Pct Recovery = 83% Analysis Date = 04/13/21 Pct Recovery = 83% Analysis Date = 04/13/21 Pct Recovery = 83% Analysis Date = 04/09/21 Pct Recovery = 83% Analysis Date = 04/09/21 Pct Recovery = 83% Analysis Date = 04/05/21 Pct Recovery = 83% Analysis Date = 04/05/21 Pct Recovery = 83% Analysis Date = 04/01/21 Pct Recovery = 83% Analysis Date = 04/01/21 Pct Recovery = 83% Analysis Date = 03/27/21 Pct Recovery = 83% Analysis Date = 03/27/21 Pct Recovery = 83% Analysis Date = 03/23/21 Pct Recovery = 84% Analysis Date = 03/23/21 Pct Recovery = 84% Analysis Date = 03/19/21 Pct Recovery = 84% Analysis Date = 03/19/21 Pct Recovery = 84% Analysis Date = 03/15/21 Pct Recovery = 84% Analysis Date = 03/15/21 Pct Recovery = 84% Analysis Date = 03/10/21 Pct Recovery = 85% Analysis Date = 03/10/21 Pct Recovery = 85% Analysis Date = 03/06/21 Pct Recovery = 85% Analysis Date = 03/06/21 Pct Recovery = 85% Analysis Date = 03/02/21 Pct Recovery = 85% Analysis Date = 03/02/21 Pct Recovery = 85% Analysis Date = 02/25/21 Pct Recovery = 86% Analysis Date = 02/25/21 Pct Recovery = 86% Analysis Date = 02/21/21 Pct Recovery = 86% Analysis Date = 02/21/21 Pct Recovery = 86% Analysis Date = 02/17/21 Pct Recovery = 87% Analysis Date = 02/17/21 Pct Recovery = 87% Analysis Date = 02/13/21 Pct Recovery = 87% Analysis Date = 02/13/21 Pct Recovery = 87% Analysis Date = 02/08/21 Pct Recovery = 88% Analysis Date = 02/08/21 Pct Recovery = 88% Analysis Date = 02/04/21 Pct Recovery = 88% Analysis Date = 02/04/21 Pct Recovery = 88% Analysis Date = 01/31/21 Pct Recovery = 88% Analysis Date = 01/31/21 Pct Recovery = 88% Analysis Date = 01/27/21 Pct Recovery = 89% Analysis Date = 01/27/21 Pct Recovery = 89% Analysis Date = 01/22/21 Pct Recovery = 89% Analysis Date = 01/22/21 Pct Recovery = 89% Analysis Date = 01/18/21 Pct Recovery = 90% Analysis Date = 01/18/21 Pct Recovery = 90% Analysis Date = 01/14/21 Pct Recovery = 90% Analysis Date = 01/14/21 Pct Recovery = 90% Analysis Date = 01/10/21 Pct Recovery = 90% Analysis Date = 01/10/21 Pct Recovery = 90% Analysis Date = 01/05/21 Pct Recovery = 91% Analysis Date = 01/05/21 Pct Recovery = 91% Analysis Date = 01/01/21 Pct Recovery = 91% Analysis Date = 01/01/21 Pct Recovery = 91% Analysis Date = 12/28/20 Pct Recovery = 92% Analysis Date = 12/28/20 Pct Recovery = 92% Analysis Date = 12/23/20 Pct Recovery = 92% Analysis Date = 12/23/20 Pct Recovery = 92% Analysis Date = 12/19/20 Pct Recovery = 92% Analysis Date = 12/19/20 Pct Recovery = 92% Analysis Date = 12/15/20 Pct Recovery = 93% Analysis Date = 12/15/20 Pct Recovery = 93% Analysis Date = 12/11/20 Pct Recovery = 93% Analysis Date = 12/11/20 Pct Recovery = 93% Analysis Date = 12/06/20 Pct Recovery = 94% Analysis Date = 12/06/20 Pct Recovery = 94% Analysis Date = 12/02/20 Pct Recovery = 94% Analysis Date = 12/02/20 Pct Recovery = 94% Analysis Date = 11/28/20 Pct Recovery = 94% Analysis Date = 11/28/20 Pct Recovery = 94% Analysis Date = 11/24/20 Pct Recovery = 95% Analysis Date = 11/24/20 Pct Recovery = 95% Analysis Date = 11/19/20 Pct Recovery = 95% Analysis Date = 11/19/20 Pct Recovery = 95% Analysis Date = 11/15/20 Pct Recovery = 95% Analysis Date = 11/15/20 Pct Recovery = 95% Analysis Date = 11/11/20 Pct Recovery = 96% Analysis Date = 11/11/20 Pct Recovery = 96% Analysis Date = 11/07/20 Pct Recovery = 96% Analysis Date = 11/07/20 Pct Recovery = 96% Analysis Date = 11/02/20 Pct Recovery = 96% Analysis Date = 11/02/20 Pct Recovery = 96% Analysis Date = 10/29/20 Pct Recovery = 97% Analysis Date = 10/29/20 Pct Recovery = 97% Analysis Date = 10/25/20 Pct Recovery = 97% Analysis Date = 10/25/20 Pct Recovery = 97% Analysis Date = 10/21/20 Pct Recovery = 97% Analysis Date = 10/21/20 Pct Recovery = 97% Analysis Date = 10/16/20 Pct Recovery = 98% Analysis Date = 10/16/20 Pct Recovery = 98% Analysis Date = 10/12/20 Pct Recovery = 98% Analysis Date = 10/12/20 Pct Recovery = 98% Analysis Date = 10/08/20 Pct Recovery = 99% Analysis Date = 10/08/20 Pct Recovery = 99% Analysis Date = 10/03/20 Pct Recovery = 99% Analysis Date = 10/03/20 Pct Recovery = 99% Analysis Date = 09/29/20 Pct Recovery = 99% Analysis Date = 09/29/20 Pct Recovery = 99% Analysis Date = 09/25/20 Pct Recovery = 100% Analysis Date = 09/25/20 Pct Recovery = 100% Analysis Date = 09/21/20 Pct Recovery = 100% Analysis Date = 09/21/20 Pct Recovery = 100% Analysis Date = 09/16/20 Pct Recovery = 100% Analysis Date = 09/16/20 Pct Recovery = 100% Analysis Date = 09/12/20 Pct Recovery = 101% Analysis Date = 09/12/20 Pct Recovery = 101% Analysis Date = 09/08/20 Pct Recovery = 101% Analysis Date = 09/08/20 Pct Recovery = 101% Analysis Date = 09/04/20 Pct Recovery = 101% Analysis Date = 09/04/20 Pct Recovery = 101% Analysis Date = 08/30/20 Pct Recovery = 102% Analysis Date = 08/30/20 Pct Recovery = 102% Analysis Date = 08/26/20 Pct Recovery = 102% Analysis Date = 08/26/20 Pct Recovery = 102% Analysis Date = 08/22/20 Pct Recovery = 102% Analysis Date = 08/22/20 Pct Recovery = 102% Analysis Date = 08/18/20 Pct Recovery = 103% Analysis Date = 08/18/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/05/20 Pct Recovery = 104% Analysis Date = 08/05/20 Pct Recovery = 104% Analysis Date = 07/31/20 Pct Recovery = 104% Analysis Date = 07/31/20 Pct Recovery = 104% Analysis Date = 07/27/20 Pct Recovery = 104% Analysis Date = 07/27/20 Pct Recovery = 104% Analysis Date = 07/23/20 Pct Recovery = 105% Analysis Date = 07/23/20 Pct Recovery = 105% Analysis Date = 07/19/20 Pct Recovery = 105% Analysis Date = 07/19/20 Pct Recovery = 105% Analysis Date = 07/14/20 Pct Recovery = 105% Analysis Date = 07/14/20 Pct Recovery = 105% Analysis Date = 07/10/20 Pct Recovery = 106% Analysis Date = 07/10/20 Pct Recovery = 106% Analysis Date = 07/06/20 Pct Recovery = 106% Analysis Date = 07/06/20 Pct Recovery = 106% Analysis Date = 07/02/20 Pct Recovery = 106% Analysis Date = 07/02/20 Pct Recovery = 106% Analysis Date = 06/27/20 Pct Recovery = 107% Analysis Date = 06/27/20 Pct Recovery = 107% Analysis Date = 06/23/20 Pct Recovery = 107% Analysis Date = 06/23/20 Pct Recovery = 107% Analysis Date = 06/19/20 Pct Recovery = 107% Analysis Date = 06/19/20 Pct Recovery = 107% Analysis Date = 06/15/20 Pct Recovery = 108% Analysis Date = 06/15/20 Pct Recovery = 108% Analysis Date = 06/10/20 Pct Recovery = 108% Analysis Date = 06/10/20 Pct Recovery = 108% Analysis Date = 06/06/20 Pct Recovery = 109% Analysis Date = 06/06/20 Pct Recovery = 109% Analysis Date = 06/02/20 Pct Recovery = 109% Analysis Date = 06/02/20 Pct Recovery = 109% Analysis Date = 05/29/20 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZOXYSTROBIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 43 86% 25% 81% 25%
Total 43 86% 25% 81% 25%

Sample Statistics
AZOXYSTROBIN

Characteristic N % % Basis
Plotted 43 98% Spiked
Estimated Values 3 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 1 2% 1 out of 44
Not Spiked 72 .  
False Positives 0 0% 0 out of 72

OBSP Determination:
BENTAZONE
METHOD: 2447 , TESTIDCODE: 68538LCM60

Laboratory ID = 20201820155 Lab Value = 103.827 Expected Conc. = 114.1 Report level label = 9 Pct Recovery = 91% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 65.007 Expected Conc. = 114.1 Report level label = 9 Pct Recovery = 57% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 151.553 Expected Conc. = 113 Report level label = 9 Pct Recovery = 134% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203230021 Lab Value = 112.142 Expected Conc. = 112.2 Report level label = 9 Pct Recovery = 100% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 116.075 Expected Conc. = 112.2 Report level label = 9 Pct Recovery = 103% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590107 Lab Value = 119.981 Expected Conc. = 110.4 Report level label = 9 Pct Recovery = 109% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 125.023 Expected Conc. = 110.4 Report level label = 9 Pct Recovery = 113% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222150193 Lab Value = 69.770 Expected Conc. = 90 Report level label = 9 Pct Recovery = 78% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20222010132 Lab Value = 68.547 Expected Conc. = 90 Report level label = 9 Pct Recovery = 76% Analysis Date = 07/22/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 67.877 Expected Conc. = 90 Report level label = 9 Pct Recovery = 75% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20212990174 Lab Value = 45.322 Expected Conc. = 89.92 Report level label = 9 Pct Recovery = 50% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 51.097 Expected Conc. = 89.68 Report level label = 9 Pct Recovery = 57% Analysis Date = 02/01/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 70.342 Expected Conc. = 89.68 Report level label = 9 Pct Recovery = 78% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20202530029 Lab Value = 46.178 Expected Conc. = 57.05 Report level label = 9 Pct Recovery = 81% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 47.087 Expected Conc. = 57.05 Report level label = 9 Pct Recovery = 83% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 42.969 Expected Conc. = 57.05 Report level label = 9 Pct Recovery = 75% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201960104 Lab Value = 56.288 Expected Conc. = 56.5 Report level label = 9 Pct Recovery = 100% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20220810133 Lab Value = 52.358 Expected Conc. = 56.25 Report level label = 9 Pct Recovery = 93% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20213340027 Lab Value = 46.116 Expected Conc. = 56.2 Report level label = 9 Pct Recovery = 82% Analysis Date = 12/04/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 104.483 Expected Conc. = 56.2 Report level label = 9 Pct Recovery = 186% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 31.436 Expected Conc. = 56.2 Report level label = 9 Pct Recovery = 56% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 45.129 Expected Conc. = 56.05 Report level label = 9 Pct Recovery = 81% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 47.484 Expected Conc. = 56.05 Report level label = 9 Pct Recovery = 85% Analysis Date = 02/02/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20203360042 Lab Value = 50.380 Expected Conc. = 55.2 Report level label = 9 Pct Recovery = 91% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 48.350 Expected Conc. = 55.2 Report level label = 9 Pct Recovery = 88% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 66.193 Expected Conc. = 55.2 Report level label = 9 Pct Recovery = 120% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202180001 Lab Value = 29.305 Expected Conc. = 22.82 Report level label = 9 Pct Recovery = 128% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 17.526 Expected Conc. = 22.82 Report level label = 9 Pct Recovery = 77% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 17.084 Expected Conc. = 22.82 Report level label = 9 Pct Recovery = 75% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201610160 Lab Value = 13.759 Expected Conc. = 22.6 Report level label = 9 Pct Recovery = 61% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20222630205 Lab Value = 16.836 Expected Conc. = 22.5 Report level label = 9 Pct Recovery = 75% Analysis Date = 09/30/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20213060210 Lab Value = 10.846 Expected Conc. = 22.48 Report level label = 9 Pct Recovery = 48% Analysis Date = 11/09/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210830019 Lab Value = 26.467 Expected Conc. = 22.44 Report level label = 9 Pct Recovery = 118% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 18.966 Expected Conc. = 22.44 Report level label = 9 Pct Recovery = 85% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222500483 Lab Value = 19.913 Expected Conc. = 22.42 Report level label = 9 Pct Recovery = 89% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 17.387 Expected Conc. = 22.42 Report level label = 9 Pct Recovery = 78% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210970035 Lab Value = 25.537 Expected Conc. = 22.08 Report level label = 9 Pct Recovery = 116% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 20.238 Expected Conc. = 22.08 Report level label = 9 Pct Recovery = 92% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 20.603 Expected Conc. = 22.08 Report level label = 9 Pct Recovery = 93% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 22.633 Expected Conc. = 22.08 Report level label = 9 Pct Recovery = 103% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 29.175 Expected Conc. = 22.08 Report level label = 9 Pct Recovery = 132% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 18.671 Expected Conc. = 22.08 Report level label = 9 Pct Recovery = 85% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 10/13/22 Pct Recovery = 79% Analysis Date = 10/09/22 Pct Recovery = 79% Analysis Date = 10/09/22 Pct Recovery = 79% Analysis Date = 10/05/22 Pct Recovery = 79% Analysis Date = 10/05/22 Pct Recovery = 79% Analysis Date = 09/30/22 Pct Recovery = 79% Analysis Date = 09/30/22 Pct Recovery = 79% Analysis Date = 09/26/22 Pct Recovery = 79% Analysis Date = 09/26/22 Pct Recovery = 79% Analysis Date = 09/22/22 Pct Recovery = 79% Analysis Date = 09/22/22 Pct Recovery = 79% Analysis Date = 09/17/22 Pct Recovery = 79% Analysis Date = 09/17/22 Pct Recovery = 79% Analysis Date = 09/13/22 Pct Recovery = 79% Analysis Date = 09/13/22 Pct Recovery = 79% Analysis Date = 09/08/22 Pct Recovery = 79% Analysis Date = 09/08/22 Pct Recovery = 79% Analysis Date = 09/04/22 Pct Recovery = 79% Analysis Date = 09/04/22 Pct Recovery = 79% Analysis Date = 08/31/22 Pct Recovery = 79% Analysis Date = 08/31/22 Pct Recovery = 79% Analysis Date = 08/26/22 Pct Recovery = 79% Analysis Date = 08/26/22 Pct Recovery = 79% Analysis Date = 08/22/22 Pct Recovery = 79% Analysis Date = 08/22/22 Pct Recovery = 79% Analysis Date = 08/17/22 Pct Recovery = 79% Analysis Date = 08/17/22 Pct Recovery = 79% Analysis Date = 08/13/22 Pct Recovery = 79% Analysis Date = 08/13/22 Pct Recovery = 79% Analysis Date = 08/09/22 Pct Recovery = 79% Analysis Date = 08/09/22 Pct Recovery = 79% Analysis Date = 08/04/22 Pct Recovery = 79% Analysis Date = 08/04/22 Pct Recovery = 79% Analysis Date = 07/31/22 Pct Recovery = 79% Analysis Date = 07/31/22 Pct Recovery = 79% Analysis Date = 07/27/22 Pct Recovery = 79% Analysis Date = 07/27/22 Pct Recovery = 79% Analysis Date = 07/22/22 Pct Recovery = 79% Analysis Date = 07/22/22 Pct Recovery = 79% Analysis Date = 07/18/22 Pct Recovery = 80% Analysis Date = 07/18/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 06/30/22 Pct Recovery = 80% Analysis Date = 06/30/22 Pct Recovery = 80% Analysis Date = 06/26/22 Pct Recovery = 80% Analysis Date = 06/26/22 Pct Recovery = 80% Analysis Date = 06/21/22 Pct Recovery = 80% Analysis Date = 06/21/22 Pct Recovery = 80% Analysis Date = 06/17/22 Pct Recovery = 80% Analysis Date = 06/17/22 Pct Recovery = 80% Analysis Date = 06/13/22 Pct Recovery = 80% Analysis Date = 06/13/22 Pct Recovery = 80% Analysis Date = 06/08/22 Pct Recovery = 80% Analysis Date = 06/08/22 Pct Recovery = 80% Analysis Date = 06/04/22 Pct Recovery = 80% Analysis Date = 06/04/22 Pct Recovery = 80% Analysis Date = 05/31/22 Pct Recovery = 80% Analysis Date = 05/31/22 Pct Recovery = 80% Analysis Date = 05/26/22 Pct Recovery = 80% Analysis Date = 05/26/22 Pct Recovery = 80% Analysis Date = 05/22/22 Pct Recovery = 80% Analysis Date = 05/22/22 Pct Recovery = 80% Analysis Date = 05/17/22 Pct Recovery = 80% Analysis Date = 05/17/22 Pct Recovery = 80% Analysis Date = 05/13/22 Pct Recovery = 80% Analysis Date = 05/13/22 Pct Recovery = 80% Analysis Date = 05/09/22 Pct Recovery = 80% Analysis Date = 05/09/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/25/22 Pct Recovery = 80% Analysis Date = 04/25/22 Pct Recovery = 80% Analysis Date = 04/21/22 Pct Recovery = 81% Analysis Date = 04/21/22 Pct Recovery = 81% Analysis Date = 04/17/22 Pct Recovery = 81% Analysis Date = 04/17/22 Pct Recovery = 81% Analysis Date = 04/12/22 Pct Recovery = 81% Analysis Date = 04/12/22 Pct Recovery = 81% Analysis Date = 04/08/22 Pct Recovery = 81% Analysis Date = 04/08/22 Pct Recovery = 81% Analysis Date = 04/04/22 Pct Recovery = 81% Analysis Date = 04/04/22 Pct Recovery = 81% Analysis Date = 03/30/22 Pct Recovery = 81% Analysis Date = 03/30/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/21/22 Pct Recovery = 81% Analysis Date = 03/21/22 Pct Recovery = 81% Analysis Date = 03/17/22 Pct Recovery = 81% Analysis Date = 03/17/22 Pct Recovery = 81% Analysis Date = 03/13/22 Pct Recovery = 81% Analysis Date = 03/13/22 Pct Recovery = 81% Analysis Date = 03/08/22 Pct Recovery = 81% Analysis Date = 03/08/22 Pct Recovery = 81% Analysis Date = 03/04/22 Pct Recovery = 81% Analysis Date = 03/04/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 82% Analysis Date = 02/27/22 Pct Recovery = 82% Analysis Date = 02/23/22 Pct Recovery = 82% Analysis Date = 02/23/22 Pct Recovery = 82% Analysis Date = 02/19/22 Pct Recovery = 82% Analysis Date = 02/19/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/01/22 Pct Recovery = 82% Analysis Date = 02/01/22 Pct Recovery = 82% Analysis Date = 01/28/22 Pct Recovery = 82% Analysis Date = 01/28/22 Pct Recovery = 82% Analysis Date = 01/23/22 Pct Recovery = 82% Analysis Date = 01/23/22 Pct Recovery = 82% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 83% Analysis Date = 01/01/22 Pct Recovery = 83% Analysis Date = 01/01/22 Pct Recovery = 83% Analysis Date = 12/28/21 Pct Recovery = 83% Analysis Date = 12/28/21 Pct Recovery = 83% Analysis Date = 12/24/21 Pct Recovery = 83% Analysis Date = 12/24/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 83% Analysis Date = 12/15/21 Pct Recovery = 83% Analysis Date = 12/15/21 Pct Recovery = 83% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/06/21 Pct Recovery = 84% Analysis Date = 12/06/21 Pct Recovery = 84% Analysis Date = 12/02/21 Pct Recovery = 84% Analysis Date = 12/02/21 Pct Recovery = 84% Analysis Date = 11/27/21 Pct Recovery = 84% Analysis Date = 11/27/21 Pct Recovery = 84% Analysis Date = 11/23/21 Pct Recovery = 85% Analysis Date = 11/23/21 Pct Recovery = 85% Analysis Date = 11/19/21 Pct Recovery = 85% Analysis Date = 11/19/21 Pct Recovery = 85% Analysis Date = 11/14/21 Pct Recovery = 85% Analysis Date = 11/14/21 Pct Recovery = 85% Analysis Date = 11/10/21 Pct Recovery = 85% Analysis Date = 11/10/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 86% Analysis Date = 11/05/21 Pct Recovery = 86% Analysis Date = 11/01/21 Pct Recovery = 86% Analysis Date = 11/01/21 Pct Recovery = 86% Analysis Date = 10/28/21 Pct Recovery = 86% Analysis Date = 10/28/21 Pct Recovery = 86% Analysis Date = 10/23/21 Pct Recovery = 86% Analysis Date = 10/23/21 Pct Recovery = 86% Analysis Date = 10/19/21 Pct Recovery = 87% Analysis Date = 10/19/21 Pct Recovery = 87% Analysis Date = 10/15/21 Pct Recovery = 87% Analysis Date = 10/15/21 Pct Recovery = 87% Analysis Date = 10/10/21 Pct Recovery = 87% Analysis Date = 10/10/21 Pct Recovery = 87% Analysis Date = 10/06/21 Pct Recovery = 87% Analysis Date = 10/06/21 Pct Recovery = 87% Analysis Date = 10/01/21 Pct Recovery = 88% Analysis Date = 10/01/21 Pct Recovery = 88% Analysis Date = 09/27/21 Pct Recovery = 88% Analysis Date = 09/27/21 Pct Recovery = 88% Analysis Date = 09/23/21 Pct Recovery = 88% Analysis Date = 09/23/21 Pct Recovery = 88% Analysis Date = 09/18/21 Pct Recovery = 89% Analysis Date = 09/18/21 Pct Recovery = 89% Analysis Date = 09/14/21 Pct Recovery = 89% Analysis Date = 09/14/21 Pct Recovery = 89% Analysis Date = 09/09/21 Pct Recovery = 89% Analysis Date = 09/09/21 Pct Recovery = 89% Analysis Date = 09/05/21 Pct Recovery = 89% Analysis Date = 09/05/21 Pct Recovery = 89% Analysis Date = 09/01/21 Pct Recovery = 90% Analysis Date = 09/01/21 Pct Recovery = 90% Analysis Date = 08/27/21 Pct Recovery = 90% Analysis Date = 08/27/21 Pct Recovery = 90% Analysis Date = 08/23/21 Pct Recovery = 90% Analysis Date = 08/23/21 Pct Recovery = 90% Analysis Date = 08/19/21 Pct Recovery = 91% Analysis Date = 08/19/21 Pct Recovery = 91% Analysis Date = 08/14/21 Pct Recovery = 91% Analysis Date = 08/14/21 Pct Recovery = 91% Analysis Date = 08/10/21 Pct Recovery = 91% Analysis Date = 08/10/21 Pct Recovery = 91% Analysis Date = 08/05/21 Pct Recovery = 91% Analysis Date = 08/05/21 Pct Recovery = 91% Analysis Date = 08/01/21 Pct Recovery = 92% Analysis Date = 08/01/21 Pct Recovery = 92% Analysis Date = 07/28/21 Pct Recovery = 92% Analysis Date = 07/28/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/10/21 Pct Recovery = 93% Analysis Date = 07/10/21 Pct Recovery = 93% Analysis Date = 07/06/21 Pct Recovery = 93% Analysis Date = 07/06/21 Pct Recovery = 93% Analysis Date = 07/01/21 Pct Recovery = 94% Analysis Date = 07/01/21 Pct Recovery = 94% Analysis Date = 06/27/21 Pct Recovery = 94% Analysis Date = 06/27/21 Pct Recovery = 94% Analysis Date = 06/23/21 Pct Recovery = 94% Analysis Date = 06/23/21 Pct Recovery = 94% Analysis Date = 06/18/21 Pct Recovery = 94% Analysis Date = 06/18/21 Pct Recovery = 94% Analysis Date = 06/14/21 Pct Recovery = 95% Analysis Date = 06/14/21 Pct Recovery = 95% Analysis Date = 06/09/21 Pct Recovery = 95% Analysis Date = 06/09/21 Pct Recovery = 95% Analysis Date = 06/05/21 Pct Recovery = 95% Analysis Date = 06/05/21 Pct Recovery = 95% Analysis Date = 06/01/21 Pct Recovery = 96% Analysis Date = 06/01/21 Pct Recovery = 96% Analysis Date = 05/27/21 Pct Recovery = 96% Analysis Date = 05/27/21 Pct Recovery = 96% Analysis Date = 05/23/21 Pct Recovery = 96% Analysis Date = 05/23/21 Pct Recovery = 96% Analysis Date = 05/18/21 Pct Recovery = 96% Analysis Date = 05/18/21 Pct Recovery = 96% Analysis Date = 05/14/21 Pct Recovery = 97% Analysis Date = 05/14/21 Pct Recovery = 97% Analysis Date = 05/10/21 Pct Recovery = 97% Analysis Date = 05/10/21 Pct Recovery = 97% Analysis Date = 05/05/21 Pct Recovery = 97% Analysis Date = 05/05/21 Pct Recovery = 97% Analysis Date = 05/01/21 Pct Recovery = 98% Analysis Date = 05/01/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/22/21 Pct Recovery = 98% Analysis Date = 04/22/21 Pct Recovery = 98% Analysis Date = 04/18/21 Pct Recovery = 98% Analysis Date = 04/18/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 99% Analysis Date = 04/13/21 Pct Recovery = 99% Analysis Date = 04/09/21 Pct Recovery = 99% Analysis Date = 04/09/21 Pct Recovery = 99% Analysis Date = 04/05/21 Pct Recovery = 99% Analysis Date = 04/05/21 Pct Recovery = 99% Analysis Date = 03/31/21 Pct Recovery = 99% Analysis Date = 03/31/21 Pct Recovery = 99% Analysis Date = 03/27/21 Pct Recovery = 100% Analysis Date = 03/27/21 Pct Recovery = 100% Analysis Date = 03/22/21 Pct Recovery = 100% Analysis Date = 03/22/21 Pct Recovery = 100% Analysis Date = 03/18/21 Pct Recovery = 100% Analysis Date = 03/18/21 Pct Recovery = 100% Analysis Date = 03/14/21 Pct Recovery = 101% Analysis Date = 03/14/21 Pct Recovery = 101% Analysis Date = 03/09/21 Pct Recovery = 101% Analysis Date = 03/09/21 Pct Recovery = 101% Analysis Date = 03/05/21 Pct Recovery = 101% Analysis Date = 03/05/21 Pct Recovery = 101% Analysis Date = 03/01/21 Pct Recovery = 101% Analysis Date = 03/01/21 Pct Recovery = 101% Analysis Date = 02/24/21 Pct Recovery = 102% Analysis Date = 02/24/21 Pct Recovery = 102% Analysis Date = 02/20/21 Pct Recovery = 102% Analysis Date = 02/20/21 Pct Recovery = 102% Analysis Date = 02/15/21 Pct Recovery = 102% Analysis Date = 02/15/21 Pct Recovery = 102% Analysis Date = 02/11/21 Pct Recovery = 103% Analysis Date = 02/11/21 Pct Recovery = 103% Analysis Date = 02/07/21 Pct Recovery = 102% Analysis Date = 02/07/21 Pct Recovery = 102% Analysis Date = 02/02/21 Pct Recovery = 102% Analysis Date = 02/02/21 Pct Recovery = 102% Analysis Date = 01/29/21 Pct Recovery = 102% Analysis Date = 01/29/21 Pct Recovery = 102% Analysis Date = 01/24/21 Pct Recovery = 102% Analysis Date = 01/24/21 Pct Recovery = 102% Analysis Date = 01/20/21 Pct Recovery = 102% Analysis Date = 01/20/21 Pct Recovery = 102% Analysis Date = 01/16/21 Pct Recovery = 102% Analysis Date = 01/16/21 Pct Recovery = 102% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/25/20 Pct Recovery = 102% Analysis Date = 12/25/20 Pct Recovery = 102% Analysis Date = 12/20/20 Pct Recovery = 102% Analysis Date = 12/20/20 Pct Recovery = 102% Analysis Date = 12/16/20 Pct Recovery = 101% Analysis Date = 12/16/20 Pct Recovery = 101% Analysis Date = 12/12/20 Pct Recovery = 101% Analysis Date = 12/12/20 Pct Recovery = 101% Analysis Date = 12/07/20 Pct Recovery = 101% Analysis Date = 12/07/20 Pct Recovery = 101% Analysis Date = 12/03/20 Pct Recovery = 101% Analysis Date = 12/03/20 Pct Recovery = 101% Analysis Date = 11/28/20 Pct Recovery = 101% Analysis Date = 11/28/20 Pct Recovery = 101% Analysis Date = 11/24/20 Pct Recovery = 101% Analysis Date = 11/24/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 101% Analysis Date = 11/11/20 Pct Recovery = 101% Analysis Date = 11/11/20 Pct Recovery = 101% Analysis Date = 11/07/20 Pct Recovery = 101% Analysis Date = 11/07/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/24/20 Pct Recovery = 100% Analysis Date = 10/24/20 Pct Recovery = 100% Analysis Date = 10/20/20 Pct Recovery = 100% Analysis Date = 10/20/20 Pct Recovery = 100% Analysis Date = 10/16/20 Pct Recovery = 99% Analysis Date = 10/16/20 Pct Recovery = 99% Analysis Date = 10/11/20 Pct Recovery = 99% Analysis Date = 10/11/20 Pct Recovery = 99% Analysis Date = 10/07/20 Pct Recovery = 99% Analysis Date = 10/07/20 Pct Recovery = 99% Analysis Date = 10/02/20 Pct Recovery = 98% Analysis Date = 10/02/20 Pct Recovery = 98% Analysis Date = 09/28/20 Pct Recovery = 98% Analysis Date = 09/28/20 Pct Recovery = 98% Analysis Date = 09/24/20 Pct Recovery = 97% Analysis Date = 09/24/20 Pct Recovery = 97% Analysis Date = 09/19/20 Pct Recovery = 97% Analysis Date = 09/19/20 Pct Recovery = 97% Analysis Date = 09/15/20 Pct Recovery = 96% Analysis Date = 09/15/20 Pct Recovery = 96% Analysis Date = 09/11/20 Pct Recovery = 96% Analysis Date = 09/11/20 Pct Recovery = 96% Analysis Date = 09/06/20 Pct Recovery = 95% Analysis Date = 09/06/20 Pct Recovery = 95% Analysis Date = 09/02/20 Pct Recovery = 94% Analysis Date = 09/02/20 Pct Recovery = 94% Analysis Date = 08/28/20 Pct Recovery = 93% Analysis Date = 08/28/20 Pct Recovery = 93% Analysis Date = 08/24/20 Pct Recovery = 93% Analysis Date = 08/24/20 Pct Recovery = 93% Analysis Date = 08/20/20 Pct Recovery = 92% Analysis Date = 08/20/20 Pct Recovery = 92% Analysis Date = 08/15/20 Pct Recovery = 91% Analysis Date = 08/15/20 Pct Recovery = 91% Analysis Date = 08/11/20 Pct Recovery = 91% Analysis Date = 08/11/20 Pct Recovery = 91% Analysis Date = 08/06/20 Pct Recovery = 90% Analysis Date = 08/06/20 Pct Recovery = 90% Analysis Date = 08/02/20 Pct Recovery = 89% Analysis Date = 08/02/20 Pct Recovery = 89% Analysis Date = 07/29/20 Pct Recovery = 88% Analysis Date = 07/29/20 Pct Recovery = 88% Analysis Date = 07/24/20 Pct Recovery = 88% Analysis Date = 07/24/20 Pct Recovery = 88% Analysis Date = 07/20/20 Pct Recovery = 87% Analysis Date = 07/20/20 Pct Recovery = 87% Analysis Date = 07/16/20 Pct Recovery = 86% Analysis Date = 07/16/20 Pct Recovery = 86% Analysis Date = 07/11/20 Pct Recovery = 85% Analysis Date = 07/11/20 Pct Recovery = 85% Analysis Date = 07/07/20 Pct Recovery = 85% Analysis Date = 07/07/20 Pct Recovery = 85% Analysis Date = 07/02/20 Pct Recovery = 84% Analysis Date = 07/02/20 Pct Recovery = 84% Analysis Date = 06/28/20 Pct Recovery = 83% Analysis Date = 06/28/20 Pct Recovery = 83% Analysis Date = 06/24/20 Pct Recovery = 82% Analysis Date = 06/24/20 Pct Recovery = 82% Analysis Date = 06/19/20 Pct Recovery = 81% Analysis Date = 06/19/20 Pct Recovery = 81% Analysis Date = 06/15/20 Pct Recovery = 81% Analysis Date = 06/15/20 Pct Recovery = 81% Analysis Date = 06/10/20 Pct Recovery = 80% Analysis Date = 06/10/20 Pct Recovery = 80% Analysis Date = 06/06/20 Pct Recovery = 79% Analysis Date = 06/06/20 Pct Recovery = 79% Analysis Date = 06/02/20 Pct Recovery = 78% Analysis Date = 06/02/20 Pct Recovery = 78% Analysis Date = 05/28/20 Pct Recovery = 77% Analysis Date = 05/28/20 Pct Recovery = 77% Analysis Date = 05/24/20 Pct Recovery = 76% Analysis Date = 05/24/20 Pct Recovery = 76% Analysis Date = 05/20/20 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENTAZONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 90% 26% 85% 20%
Total 42 90% 26% 85% 20%

Sample Statistics
BENTAZONE

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 9 21% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 74 .  
False Positives 0 0% 0 out of 72

OBSP Determination:
BROMACIL
METHOD: 2447 , TESTIDCODE: 68542LCM60

Laboratory ID = 20201820155 Lab Value = 70.186 Expected Conc. = 70.6 Report level label = 5.6 Pct Recovery = 99% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 73.493 Expected Conc. = 70.6 Report level label = 5.6 Pct Recovery = 104% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 95.514 Expected Conc. = 70.5 Report level label = 5.6 Pct Recovery = 135% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20210760015 Lab Value = 49.494 Expected Conc. = 70.49 Report level label = 5.6 Pct Recovery = 70% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 65.934 Expected Conc. = 70.49 Report level label = 5.6 Pct Recovery = 94% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 70.432 Expected Conc. = 70.49 Report level label = 5.6 Pct Recovery = 100% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 70.429 Expected Conc. = 70.49 Report level label = 5.6 Pct Recovery = 100% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 62.605 Expected Conc. = 70 Report level label = 5.6 Pct Recovery = 89% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 79.718 Expected Conc. = 70 Report level label = 5.6 Pct Recovery = 114% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 71.800 Expected Conc. = 70 Report level label = 5.6 Pct Recovery = 103% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150192 Lab Value = 45.041 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 80% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 38.516 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 69% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221520237 Lab Value = 52.707 Expected Conc. = 55.68 Report level label = 5.6 Pct Recovery = 95% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20202530029 Lab Value = 32.802 Expected Conc. = 35.3 Report level label = 5.6 Pct Recovery = 93% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 34.375 Expected Conc. = 35.3 Report level label = 5.6 Pct Recovery = 97% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 36.322 Expected Conc. = 35.3 Report level label = 5.6 Pct Recovery = 103% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20220740064 Lab Value = 27.135 Expected Conc. = 35.25 Report level label = 5.6 Pct Recovery = 77% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20201960104 Lab Value = 47.860 Expected Conc. = 35.25 Report level label = 5.6 Pct Recovery = 136% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20210480001 Lab Value = 30.757 Expected Conc. = 35.245 Report level label = 5.6 Pct Recovery = 87% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202880004 Lab Value = 39.742 Expected Conc. = 35 Report level label = 5.6 Pct Recovery = 114% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221870197 Lab Value = 24.266 Expected Conc. = 34.8 Report level label = 5.6 Pct Recovery = 70% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210900005 Lab Value = 28.467 Expected Conc. = 28.196 Report level label = 5.6 Pct Recovery = 101% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 28.546 Expected Conc. = 28 Report level label = 5.6 Pct Recovery = 102% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 31.987 Expected Conc. = 28 Report level label = 5.6 Pct Recovery = 114% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202180001 Lab Value = 11.394 Expected Conc. = 14.12 Report level label = 5.6 Pct Recovery = 81% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 17.471 Expected Conc. = 14.12 Report level label = 5.6 Pct Recovery = 124% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201610160 Lab Value = 17.822 Expected Conc. = 14.1 Report level label = 5.6 Pct Recovery = 126% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210690067 Lab Value = 14.386 Expected Conc. = 14.098 Report level label = 5.6 Pct Recovery = 102% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210120050 Lab Value = 15.576 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 111% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 15.187 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 108% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 15.057 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 108% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/02/22 Pct Recovery = 77% Analysis Date = 08/02/22 Pct Recovery = 77% Analysis Date = 07/29/22 Pct Recovery = 77% Analysis Date = 07/29/22 Pct Recovery = 77% Analysis Date = 07/25/22 Pct Recovery = 77% Analysis Date = 07/25/22 Pct Recovery = 77% Analysis Date = 07/21/22 Pct Recovery = 77% Analysis Date = 07/21/22 Pct Recovery = 77% Analysis Date = 07/17/22 Pct Recovery = 77% Analysis Date = 07/17/22 Pct Recovery = 77% Analysis Date = 07/13/22 Pct Recovery = 77% Analysis Date = 07/13/22 Pct Recovery = 77% Analysis Date = 07/09/22 Pct Recovery = 77% Analysis Date = 07/09/22 Pct Recovery = 77% Analysis Date = 07/05/22 Pct Recovery = 78% Analysis Date = 07/05/22 Pct Recovery = 78% Analysis Date = 07/01/22 Pct Recovery = 78% Analysis Date = 07/01/22 Pct Recovery = 78% Analysis Date = 06/26/22 Pct Recovery = 78% Analysis Date = 06/26/22 Pct Recovery = 78% Analysis Date = 06/22/22 Pct Recovery = 78% Analysis Date = 06/22/22 Pct Recovery = 78% Analysis Date = 06/18/22 Pct Recovery = 78% Analysis Date = 06/18/22 Pct Recovery = 78% Analysis Date = 06/14/22 Pct Recovery = 78% Analysis Date = 06/14/22 Pct Recovery = 78% Analysis Date = 06/10/22 Pct Recovery = 79% Analysis Date = 06/10/22 Pct Recovery = 79% Analysis Date = 06/06/22 Pct Recovery = 79% Analysis Date = 06/06/22 Pct Recovery = 79% Analysis Date = 06/02/22 Pct Recovery = 79% Analysis Date = 06/02/22 Pct Recovery = 79% Analysis Date = 05/29/22 Pct Recovery = 79% Analysis Date = 05/29/22 Pct Recovery = 79% Analysis Date = 05/25/22 Pct Recovery = 79% Analysis Date = 05/25/22 Pct Recovery = 79% Analysis Date = 05/21/22 Pct Recovery = 79% Analysis Date = 05/21/22 Pct Recovery = 79% Analysis Date = 05/17/22 Pct Recovery = 79% Analysis Date = 05/17/22 Pct Recovery = 79% Analysis Date = 05/12/22 Pct Recovery = 79% Analysis Date = 05/12/22 Pct Recovery = 79% Analysis Date = 05/08/22 Pct Recovery = 80% Analysis Date = 05/08/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/26/22 Pct Recovery = 80% Analysis Date = 04/26/22 Pct Recovery = 80% Analysis Date = 04/22/22 Pct Recovery = 80% Analysis Date = 04/22/22 Pct Recovery = 80% Analysis Date = 04/18/22 Pct Recovery = 80% Analysis Date = 04/18/22 Pct Recovery = 80% Analysis Date = 04/14/22 Pct Recovery = 80% Analysis Date = 04/14/22 Pct Recovery = 80% Analysis Date = 04/10/22 Pct Recovery = 80% Analysis Date = 04/10/22 Pct Recovery = 80% Analysis Date = 04/06/22 Pct Recovery = 81% Analysis Date = 04/06/22 Pct Recovery = 81% Analysis Date = 04/02/22 Pct Recovery = 81% Analysis Date = 04/02/22 Pct Recovery = 81% Analysis Date = 03/28/22 Pct Recovery = 81% Analysis Date = 03/28/22 Pct Recovery = 81% Analysis Date = 03/24/22 Pct Recovery = 81% Analysis Date = 03/24/22 Pct Recovery = 81% Analysis Date = 03/20/22 Pct Recovery = 81% Analysis Date = 03/20/22 Pct Recovery = 81% Analysis Date = 03/16/22 Pct Recovery = 81% Analysis Date = 03/16/22 Pct Recovery = 81% Analysis Date = 03/12/22 Pct Recovery = 81% Analysis Date = 03/12/22 Pct Recovery = 81% Analysis Date = 03/08/22 Pct Recovery = 82% Analysis Date = 03/08/22 Pct Recovery = 82% Analysis Date = 03/04/22 Pct Recovery = 82% Analysis Date = 03/04/22 Pct Recovery = 82% Analysis Date = 02/28/22 Pct Recovery = 82% Analysis Date = 02/28/22 Pct Recovery = 82% Analysis Date = 02/24/22 Pct Recovery = 82% Analysis Date = 02/24/22 Pct Recovery = 82% Analysis Date = 02/20/22 Pct Recovery = 82% Analysis Date = 02/20/22 Pct Recovery = 82% Analysis Date = 02/16/22 Pct Recovery = 82% Analysis Date = 02/16/22 Pct Recovery = 82% Analysis Date = 02/11/22 Pct Recovery = 82% Analysis Date = 02/11/22 Pct Recovery = 82% Analysis Date = 02/07/22 Pct Recovery = 82% Analysis Date = 02/07/22 Pct Recovery = 82% Analysis Date = 02/03/22 Pct Recovery = 83% Analysis Date = 02/03/22 Pct Recovery = 83% Analysis Date = 01/30/22 Pct Recovery = 83% Analysis Date = 01/30/22 Pct Recovery = 83% Analysis Date = 01/26/22 Pct Recovery = 83% Analysis Date = 01/26/22 Pct Recovery = 83% Analysis Date = 01/22/22 Pct Recovery = 83% Analysis Date = 01/22/22 Pct Recovery = 83% Analysis Date = 01/18/22 Pct Recovery = 83% Analysis Date = 01/18/22 Pct Recovery = 83% Analysis Date = 01/14/22 Pct Recovery = 83% Analysis Date = 01/14/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 83% Analysis Date = 01/02/22 Pct Recovery = 84% Analysis Date = 01/02/22 Pct Recovery = 84% Analysis Date = 12/28/21 Pct Recovery = 84% Analysis Date = 12/28/21 Pct Recovery = 84% Analysis Date = 12/24/21 Pct Recovery = 84% Analysis Date = 12/24/21 Pct Recovery = 84% Analysis Date = 12/20/21 Pct Recovery = 84% Analysis Date = 12/20/21 Pct Recovery = 84% Analysis Date = 12/16/21 Pct Recovery = 84% Analysis Date = 12/16/21 Pct Recovery = 84% Analysis Date = 12/12/21 Pct Recovery = 84% Analysis Date = 12/12/21 Pct Recovery = 84% Analysis Date = 12/08/21 Pct Recovery = 84% Analysis Date = 12/08/21 Pct Recovery = 84% Analysis Date = 12/04/21 Pct Recovery = 85% Analysis Date = 12/04/21 Pct Recovery = 85% Analysis Date = 11/30/21 Pct Recovery = 85% Analysis Date = 11/30/21 Pct Recovery = 85% Analysis Date = 11/26/21 Pct Recovery = 85% Analysis Date = 11/26/21 Pct Recovery = 85% Analysis Date = 11/22/21 Pct Recovery = 85% Analysis Date = 11/22/21 Pct Recovery = 85% Analysis Date = 11/18/21 Pct Recovery = 85% Analysis Date = 11/18/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 86% Analysis Date = 11/01/21 Pct Recovery = 86% Analysis Date = 10/28/21 Pct Recovery = 86% Analysis Date = 10/28/21 Pct Recovery = 86% Analysis Date = 10/24/21 Pct Recovery = 86% Analysis Date = 10/24/21 Pct Recovery = 86% Analysis Date = 10/20/21 Pct Recovery = 86% Analysis Date = 10/20/21 Pct Recovery = 86% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/12/21 Pct Recovery = 86% Analysis Date = 10/12/21 Pct Recovery = 86% Analysis Date = 10/08/21 Pct Recovery = 86% Analysis Date = 10/08/21 Pct Recovery = 86% Analysis Date = 10/04/21 Pct Recovery = 87% Analysis Date = 10/04/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 87% Analysis Date = 09/13/21 Pct Recovery = 87% Analysis Date = 09/13/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 87% Analysis Date = 09/05/21 Pct Recovery = 87% Analysis Date = 09/05/21 Pct Recovery = 87% Analysis Date = 09/01/21 Pct Recovery = 88% Analysis Date = 09/01/21 Pct Recovery = 88% Analysis Date = 08/28/21 Pct Recovery = 88% Analysis Date = 08/28/21 Pct Recovery = 88% Analysis Date = 08/24/21 Pct Recovery = 88% Analysis Date = 08/24/21 Pct Recovery = 88% Analysis Date = 08/20/21 Pct Recovery = 88% Analysis Date = 08/20/21 Pct Recovery = 88% Analysis Date = 08/15/21 Pct Recovery = 88% Analysis Date = 08/15/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 88% Analysis Date = 08/03/21 Pct Recovery = 88% Analysis Date = 08/03/21 Pct Recovery = 88% Analysis Date = 07/30/21 Pct Recovery = 89% Analysis Date = 07/30/21 Pct Recovery = 89% Analysis Date = 07/26/21 Pct Recovery = 89% Analysis Date = 07/26/21 Pct Recovery = 89% Analysis Date = 07/22/21 Pct Recovery = 89% Analysis Date = 07/22/21 Pct Recovery = 89% Analysis Date = 07/18/21 Pct Recovery = 89% Analysis Date = 07/18/21 Pct Recovery = 89% Analysis Date = 07/14/21 Pct Recovery = 89% Analysis Date = 07/14/21 Pct Recovery = 89% Analysis Date = 07/10/21 Pct Recovery = 89% Analysis Date = 07/10/21 Pct Recovery = 89% Analysis Date = 07/06/21 Pct Recovery = 89% Analysis Date = 07/06/21 Pct Recovery = 89% Analysis Date = 07/02/21 Pct Recovery = 90% Analysis Date = 07/02/21 Pct Recovery = 90% Analysis Date = 06/27/21 Pct Recovery = 90% Analysis Date = 06/27/21 Pct Recovery = 90% Analysis Date = 06/23/21 Pct Recovery = 90% Analysis Date = 06/23/21 Pct Recovery = 90% Analysis Date = 06/19/21 Pct Recovery = 90% Analysis Date = 06/19/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/07/21 Pct Recovery = 90% Analysis Date = 06/07/21 Pct Recovery = 90% Analysis Date = 06/03/21 Pct Recovery = 90% Analysis Date = 06/03/21 Pct Recovery = 90% Analysis Date = 05/30/21 Pct Recovery = 91% Analysis Date = 05/30/21 Pct Recovery = 91% Analysis Date = 05/26/21 Pct Recovery = 91% Analysis Date = 05/26/21 Pct Recovery = 91% Analysis Date = 05/22/21 Pct Recovery = 91% Analysis Date = 05/22/21 Pct Recovery = 91% Analysis Date = 05/18/21 Pct Recovery = 91% Analysis Date = 05/18/21 Pct Recovery = 91% Analysis Date = 05/13/21 Pct Recovery = 91% Analysis Date = 05/13/21 Pct Recovery = 91% Analysis Date = 05/09/21 Pct Recovery = 91% Analysis Date = 05/09/21 Pct Recovery = 91% Analysis Date = 05/05/21 Pct Recovery = 91% Analysis Date = 05/05/21 Pct Recovery = 91% Analysis Date = 05/01/21 Pct Recovery = 91% Analysis Date = 05/01/21 Pct Recovery = 91% Analysis Date = 04/27/21 Pct Recovery = 92% Analysis Date = 04/27/21 Pct Recovery = 92% Analysis Date = 04/23/21 Pct Recovery = 92% Analysis Date = 04/23/21 Pct Recovery = 92% Analysis Date = 04/19/21 Pct Recovery = 92% Analysis Date = 04/19/21 Pct Recovery = 92% Analysis Date = 04/15/21 Pct Recovery = 92% Analysis Date = 04/15/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 92% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/25/21 Pct Recovery = 94% Analysis Date = 03/25/21 Pct Recovery = 94% Analysis Date = 03/21/21 Pct Recovery = 95% Analysis Date = 03/21/21 Pct Recovery = 95% Analysis Date = 03/17/21 Pct Recovery = 95% Analysis Date = 03/17/21 Pct Recovery = 95% Analysis Date = 03/13/21 Pct Recovery = 95% Analysis Date = 03/13/21 Pct Recovery = 95% Analysis Date = 03/09/21 Pct Recovery = 96% Analysis Date = 03/09/21 Pct Recovery = 96% Analysis Date = 03/05/21 Pct Recovery = 96% Analysis Date = 03/05/21 Pct Recovery = 96% Analysis Date = 03/01/21 Pct Recovery = 97% Analysis Date = 03/01/21 Pct Recovery = 97% Analysis Date = 02/25/21 Pct Recovery = 97% Analysis Date = 02/25/21 Pct Recovery = 97% Analysis Date = 02/21/21 Pct Recovery = 98% Analysis Date = 02/21/21 Pct Recovery = 98% Analysis Date = 02/17/21 Pct Recovery = 98% Analysis Date = 02/17/21 Pct Recovery = 98% Analysis Date = 02/12/21 Pct Recovery = 99% Analysis Date = 02/12/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/04/21 Pct Recovery = 100% Analysis Date = 02/04/21 Pct Recovery = 100% Analysis Date = 01/31/21 Pct Recovery = 100% Analysis Date = 01/31/21 Pct Recovery = 100% Analysis Date = 01/27/21 Pct Recovery = 100% Analysis Date = 01/27/21 Pct Recovery = 100% Analysis Date = 01/23/21 Pct Recovery = 101% Analysis Date = 01/23/21 Pct Recovery = 101% Analysis Date = 01/19/21 Pct Recovery = 101% Analysis Date = 01/19/21 Pct Recovery = 101% Analysis Date = 01/15/21 Pct Recovery = 101% Analysis Date = 01/15/21 Pct Recovery = 101% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/11/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/07/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 01/03/21 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 103% Analysis Date = 12/29/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/21/20 Pct Recovery = 103% Analysis Date = 12/21/20 Pct Recovery = 103% Analysis Date = 12/17/20 Pct Recovery = 104% Analysis Date = 12/17/20 Pct Recovery = 104% Analysis Date = 12/13/20 Pct Recovery = 104% Analysis Date = 12/13/20 Pct Recovery = 104% Analysis Date = 12/09/20 Pct Recovery = 104% Analysis Date = 12/09/20 Pct Recovery = 104% Analysis Date = 12/05/20 Pct Recovery = 104% Analysis Date = 12/05/20 Pct Recovery = 104% Analysis Date = 12/01/20 Pct Recovery = 104% Analysis Date = 12/01/20 Pct Recovery = 104% Analysis Date = 11/27/20 Pct Recovery = 104% Analysis Date = 11/27/20 Pct Recovery = 104% Analysis Date = 11/23/20 Pct Recovery = 104% Analysis Date = 11/23/20 Pct Recovery = 104% Analysis Date = 11/19/20 Pct Recovery = 105% Analysis Date = 11/19/20 Pct Recovery = 105% Analysis Date = 11/14/20 Pct Recovery = 105% Analysis Date = 11/14/20 Pct Recovery = 105% Analysis Date = 11/10/20 Pct Recovery = 105% Analysis Date = 11/10/20 Pct Recovery = 105% Analysis Date = 11/06/20 Pct Recovery = 105% Analysis Date = 11/06/20 Pct Recovery = 105% Analysis Date = 11/02/20 Pct Recovery = 105% Analysis Date = 11/02/20 Pct Recovery = 105% Analysis Date = 10/29/20 Pct Recovery = 105% Analysis Date = 10/29/20 Pct Recovery = 105% Analysis Date = 10/25/20 Pct Recovery = 105% Analysis Date = 10/25/20 Pct Recovery = 105% Analysis Date = 10/21/20 Pct Recovery = 106% Analysis Date = 10/21/20 Pct Recovery = 106% Analysis Date = 10/17/20 Pct Recovery = 106% Analysis Date = 10/17/20 Pct Recovery = 106% Analysis Date = 10/13/20 Pct Recovery = 106% Analysis Date = 10/13/20 Pct Recovery = 106% Analysis Date = 10/09/20 Pct Recovery = 106% Analysis Date = 10/09/20 Pct Recovery = 106% Analysis Date = 10/05/20 Pct Recovery = 106% Analysis Date = 10/05/20 Pct Recovery = 106% Analysis Date = 09/30/20 Pct Recovery = 106% Analysis Date = 09/30/20 Pct Recovery = 106% Analysis Date = 09/26/20 Pct Recovery = 106% Analysis Date = 09/26/20 Pct Recovery = 106% Analysis Date = 09/22/20 Pct Recovery = 106% Analysis Date = 09/22/20 Pct Recovery = 106% Analysis Date = 09/18/20 Pct Recovery = 107% Analysis Date = 09/18/20 Pct Recovery = 107% Analysis Date = 09/14/20 Pct Recovery = 107% Analysis Date = 09/14/20 Pct Recovery = 107% Analysis Date = 09/10/20 Pct Recovery = 107% Analysis Date = 09/10/20 Pct Recovery = 107% Analysis Date = 09/06/20 Pct Recovery = 108% Analysis Date = 09/06/20 Pct Recovery = 108% Analysis Date = 09/02/20 Pct Recovery = 108% Analysis Date = 09/02/20 Pct Recovery = 108% Analysis Date = 08/29/20 Pct Recovery = 108% Analysis Date = 08/29/20 Pct Recovery = 108% Analysis Date = 08/25/20 Pct Recovery = 108% Analysis Date = 08/25/20 Pct Recovery = 108% Analysis Date = 08/21/20 Pct Recovery = 109% Analysis Date = 08/21/20 Pct Recovery = 109% Analysis Date = 08/16/20 Pct Recovery = 109% Analysis Date = 08/16/20 Pct Recovery = 109% Analysis Date = 08/12/20 Pct Recovery = 109% Analysis Date = 08/12/20 Pct Recovery = 109% Analysis Date = 08/08/20 Pct Recovery = 109% Analysis Date = 08/08/20 Pct Recovery = 109% Analysis Date = 08/04/20 Pct Recovery = 110% Analysis Date = 08/04/20 Pct Recovery = 110% Analysis Date = 07/31/20 Pct Recovery = 110% Analysis Date = 07/31/20 Pct Recovery = 110% Analysis Date = 07/27/20 Pct Recovery = 110% Analysis Date = 07/27/20 Pct Recovery = 110% Analysis Date = 07/23/20 Pct Recovery = 110% Analysis Date = 07/23/20 Pct Recovery = 110% Analysis Date = 07/19/20 Pct Recovery = 110% Analysis Date = 07/19/20 Pct Recovery = 110% Analysis Date = 07/15/20 Pct Recovery = 111% Analysis Date = 07/15/20 Pct Recovery = 111% Analysis Date = 07/11/20 Pct Recovery = 111% Analysis Date = 07/11/20 Pct Recovery = 111% Analysis Date = 07/07/20 Pct Recovery = 111% Analysis Date = 07/07/20 Pct Recovery = 111% Analysis Date = 07/02/20 Pct Recovery = 111% Analysis Date = 07/02/20 Pct Recovery = 111% Analysis Date = 06/28/20 Pct Recovery = 112% Analysis Date = 06/28/20 Pct Recovery = 112% Analysis Date = 06/24/20 Pct Recovery = 112% Analysis Date = 06/24/20 Pct Recovery = 112% Analysis Date = 06/20/20 Pct Recovery = 112% Analysis Date = 06/20/20 Pct Recovery = 112% Analysis Date = 06/16/20 Pct Recovery = 112% Analysis Date = 06/16/20 Pct Recovery = 112% Analysis Date = 06/12/20 Pct Recovery = 112% Analysis Date = 06/12/20 Pct Recovery = 112% Analysis Date = 06/08/20 Pct Recovery = 113% Analysis Date = 06/08/20 Pct Recovery = 113% Analysis Date = 06/04/20 Pct Recovery = 113% Analysis Date = 06/04/20 Pct Recovery = 113% Analysis Date = 05/31/20 Pct Recovery = 113% Analysis Date = 05/31/20 Pct Recovery = 113% Analysis Date = 05/27/20 Pct Recovery = 113% Analysis Date = 05/27/20 Pct Recovery = 113% Analysis Date = 05/23/20 Pct Recovery = 114% Analysis Date = 05/23/20 Pct Recovery = 114% Analysis Date = 05/19/20 Pct Recovery = 114% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMACIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 100% 17% 101% 16%
Total 31 100% 17% 101% 16%

Sample Statistics
BROMACIL

Characteristic N % % Basis
Plotted 31 89% Spiked
Estimated Values 3 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 9% Spiked
Spiked 35 .  
False Negatives 1 3% 1 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
BROMOXYNIL
METHOD: 2447 , TESTIDCODE: 68543LCM60

Laboratory ID = 20210760015 Lab Value = 580.343 Expected Conc. = 749.2 Report level label = 60 Pct Recovery = 77% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 431.756 Expected Conc. = 749.2 Report level label = 60 Pct Recovery = 58% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 648.842 Expected Conc. = 749.2 Report level label = 60 Pct Recovery = 87% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 687.721 Expected Conc. = 749.2 Report level label = 60 Pct Recovery = 92% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 749.614 Expected Conc. = 747.2 Report level label = 60 Pct Recovery = 100% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 582.426 Expected Conc. = 747.2 Report level label = 60 Pct Recovery = 78% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 628.617 Expected Conc. = 747.2 Report level label = 60 Pct Recovery = 84% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150193 Lab Value = 462.814 Expected Conc. = 609.6 Report level label = 60 Pct Recovery = 76% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220810134 Lab Value = 420.836 Expected Conc. = 604 Report level label = 60 Pct Recovery = 70% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222010132 Lab Value = 429.077 Expected Conc. = 600 Report level label = 60 Pct Recovery = 72% Analysis Date = 07/22/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20212990174 Lab Value = 267.512 Expected Conc. = 599.84 Report level label = 60 Pct Recovery = 45% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 255.660 Expected Conc. = 402.8 Report level label = 60 Pct Recovery = 63% Analysis Date = 02/01/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 277.220 Expected Conc. = 402.8 Report level label = 60 Pct Recovery = 69% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20220810133 Lab Value = 285.285 Expected Conc. = 377.5 Report level label = 60 Pct Recovery = 76% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201550031 Lab Value = 249.165 Expected Conc. = 375.9 Report level label = 60 Pct Recovery = 66% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20202390020 Lab Value = 400.163 Expected Conc. = 375.4 Report level label = 60 Pct Recovery = 107% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 327.157 Expected Conc. = 375.4 Report level label = 60 Pct Recovery = 87% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20213340027 Lab Value = 262.790 Expected Conc. = 374.9 Report level label = 60 Pct Recovery = 70% Analysis Date = 12/04/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 748.607 Expected Conc. = 374.9 Report level label = 60 Pct Recovery = 200% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 228.982 Expected Conc. = 374.9 Report level label = 60 Pct Recovery = 61% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20210480001 Lab Value = 255.288 Expected Conc. = 374.6 Report level label = 60 Pct Recovery = 68% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202880004 Lab Value = 268.386 Expected Conc. = 373.6 Report level label = 60 Pct Recovery = 72% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 236.019 Expected Conc. = 300.32 Report level label = 60 Pct Recovery = 79% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 178.648 Expected Conc. = 300.32 Report level label = 60 Pct Recovery = 59% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210900005 Lab Value = 283.205 Expected Conc. = 299.68 Report level label = 60 Pct Recovery = 95% Analysis Date = 04/06/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 407.099 Expected Conc. = 298.88 Report level label = 60 Pct Recovery = 136% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 263.595 Expected Conc. = 298.88 Report level label = 60 Pct Recovery = 88% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221730293 Lab Value = 179.797 Expected Conc. = 251.75 Report level label = 60 Pct Recovery = 71% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 152.100 Expected Conc. = 251.75 Report level label = 60 Pct Recovery = 60% Analysis Date = 02/02/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20222630205 Lab Value = 124.513 Expected Conc. = 151 Report level label = 60 Pct Recovery = 82% Analysis Date = 09/30/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20202330309 Lab Value = 96.374 Expected Conc. = 150.36 Report level label = 60 Pct Recovery = 64% Analysis Date = 09/01/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 157.364 Expected Conc. = 150.36 Report level label = 60 Pct Recovery = 105% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 127.225 Expected Conc. = 150.36 Report level label = 60 Pct Recovery = 85% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 100.782 Expected Conc. = 150.36 Report level label = 60 Pct Recovery = 67% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 74.250 Expected Conc. = 150.36 Report level label = 60 Pct Recovery = 49% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20213060210 Lab Value = 101.667 Expected Conc. = 149.96 Report level label = 60 Pct Recovery = 68% Analysis Date = 11/09/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210690067 Lab Value = 193.931 Expected Conc. = 149.84 Report level label = 60 Pct Recovery = 129% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210120050 Lab Value = 96.114 Expected Conc. = 149.44 Report level label = 60 Pct Recovery = 64% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 101.171 Expected Conc. = 149.44 Report level label = 60 Pct Recovery = 68% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 105.130 Expected Conc. = 149.44 Report level label = 60 Pct Recovery = 70% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 118.947 Expected Conc. = 149.44 Report level label = 60 Pct Recovery = 80% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 107.561 Expected Conc. = 149.44 Report level label = 60 Pct Recovery = 72% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222500483 Lab Value = 88.756 Expected Conc. = 100.7 Report level label = 60 Pct Recovery = 88% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 56.628 Expected Conc. = 100.7 Report level label = 60 Pct Recovery = 56% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Analysis Date = 10/13/22 Pct Recovery = 75% Analysis Date = 10/09/22 Pct Recovery = 75% Analysis Date = 10/09/22 Pct Recovery = 75% Analysis Date = 10/05/22 Pct Recovery = 76% Analysis Date = 10/05/22 Pct Recovery = 76% Analysis Date = 09/30/22 Pct Recovery = 76% Analysis Date = 09/30/22 Pct Recovery = 76% Analysis Date = 09/26/22 Pct Recovery = 76% Analysis Date = 09/26/22 Pct Recovery = 76% Analysis Date = 09/22/22 Pct Recovery = 76% Analysis Date = 09/22/22 Pct Recovery = 76% Analysis Date = 09/17/22 Pct Recovery = 76% Analysis Date = 09/17/22 Pct Recovery = 76% Analysis Date = 09/13/22 Pct Recovery = 76% Analysis Date = 09/13/22 Pct Recovery = 76% Analysis Date = 09/09/22 Pct Recovery = 76% Analysis Date = 09/09/22 Pct Recovery = 76% Analysis Date = 09/04/22 Pct Recovery = 76% Analysis Date = 09/04/22 Pct Recovery = 76% Analysis Date = 08/31/22 Pct Recovery = 76% Analysis Date = 08/31/22 Pct Recovery = 76% Analysis Date = 08/27/22 Pct Recovery = 76% Analysis Date = 08/27/22 Pct Recovery = 76% Analysis Date = 08/22/22 Pct Recovery = 76% Analysis Date = 08/22/22 Pct Recovery = 76% Analysis Date = 08/18/22 Pct Recovery = 76% Analysis Date = 08/18/22 Pct Recovery = 76% Analysis Date = 08/14/22 Pct Recovery = 76% Analysis Date = 08/14/22 Pct Recovery = 76% Analysis Date = 08/09/22 Pct Recovery = 76% Analysis Date = 08/09/22 Pct Recovery = 76% Analysis Date = 08/05/22 Pct Recovery = 76% Analysis Date = 08/05/22 Pct Recovery = 76% Analysis Date = 08/01/22 Pct Recovery = 76% Analysis Date = 08/01/22 Pct Recovery = 76% Analysis Date = 07/27/22 Pct Recovery = 76% Analysis Date = 07/27/22 Pct Recovery = 76% Analysis Date = 07/23/22 Pct Recovery = 76% Analysis Date = 07/23/22 Pct Recovery = 76% Analysis Date = 07/19/22 Pct Recovery = 76% Analysis Date = 07/19/22 Pct Recovery = 76% Analysis Date = 07/14/22 Pct Recovery = 76% Analysis Date = 07/14/22 Pct Recovery = 76% Analysis Date = 07/10/22 Pct Recovery = 76% Analysis Date = 07/10/22 Pct Recovery = 76% Analysis Date = 07/06/22 Pct Recovery = 76% Analysis Date = 07/06/22 Pct Recovery = 76% Analysis Date = 07/01/22 Pct Recovery = 76% Analysis Date = 07/01/22 Pct Recovery = 76% Analysis Date = 06/27/22 Pct Recovery = 76% Analysis Date = 06/27/22 Pct Recovery = 76% Analysis Date = 06/23/22 Pct Recovery = 76% Analysis Date = 06/23/22 Pct Recovery = 76% Analysis Date = 06/18/22 Pct Recovery = 76% Analysis Date = 06/18/22 Pct Recovery = 76% Analysis Date = 06/14/22 Pct Recovery = 76% Analysis Date = 06/14/22 Pct Recovery = 76% Analysis Date = 06/10/22 Pct Recovery = 76% Analysis Date = 06/10/22 Pct Recovery = 76% Analysis Date = 06/05/22 Pct Recovery = 76% Analysis Date = 06/05/22 Pct Recovery = 76% Analysis Date = 06/01/22 Pct Recovery = 76% Analysis Date = 06/01/22 Pct Recovery = 76% Analysis Date = 05/28/22 Pct Recovery = 76% Analysis Date = 05/28/22 Pct Recovery = 76% Analysis Date = 05/23/22 Pct Recovery = 76% Analysis Date = 05/23/22 Pct Recovery = 76% Analysis Date = 05/19/22 Pct Recovery = 76% Analysis Date = 05/19/22 Pct Recovery = 76% Analysis Date = 05/15/22 Pct Recovery = 76% Analysis Date = 05/15/22 Pct Recovery = 76% Analysis Date = 05/10/22 Pct Recovery = 76% Analysis Date = 05/10/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 04/27/22 Pct Recovery = 77% Analysis Date = 04/27/22 Pct Recovery = 77% Analysis Date = 04/23/22 Pct Recovery = 77% Analysis Date = 04/23/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/14/22 Pct Recovery = 77% Analysis Date = 04/14/22 Pct Recovery = 77% Analysis Date = 04/10/22 Pct Recovery = 77% Analysis Date = 04/10/22 Pct Recovery = 77% Analysis Date = 04/06/22 Pct Recovery = 77% Analysis Date = 04/06/22 Pct Recovery = 77% Analysis Date = 04/01/22 Pct Recovery = 77% Analysis Date = 04/01/22 Pct Recovery = 77% Analysis Date = 03/28/22 Pct Recovery = 77% Analysis Date = 03/28/22 Pct Recovery = 77% Analysis Date = 03/24/22 Pct Recovery = 77% Analysis Date = 03/24/22 Pct Recovery = 77% Analysis Date = 03/19/22 Pct Recovery = 77% Analysis Date = 03/19/22 Pct Recovery = 77% Analysis Date = 03/15/22 Pct Recovery = 77% Analysis Date = 03/15/22 Pct Recovery = 77% Analysis Date = 03/11/22 Pct Recovery = 77% Analysis Date = 03/11/22 Pct Recovery = 77% Analysis Date = 03/06/22 Pct Recovery = 77% Analysis Date = 03/06/22 Pct Recovery = 77% Analysis Date = 03/02/22 Pct Recovery = 77% Analysis Date = 03/02/22 Pct Recovery = 77% Analysis Date = 02/26/22 Pct Recovery = 77% Analysis Date = 02/26/22 Pct Recovery = 77% Analysis Date = 02/21/22 Pct Recovery = 77% Analysis Date = 02/21/22 Pct Recovery = 77% Analysis Date = 02/17/22 Pct Recovery = 77% Analysis Date = 02/17/22 Pct Recovery = 77% Analysis Date = 02/13/22 Pct Recovery = 77% Analysis Date = 02/13/22 Pct Recovery = 77% Analysis Date = 02/08/22 Pct Recovery = 77% Analysis Date = 02/08/22 Pct Recovery = 77% Analysis Date = 02/04/22 Pct Recovery = 78% Analysis Date = 02/04/22 Pct Recovery = 78% Analysis Date = 01/31/22 Pct Recovery = 78% Analysis Date = 01/31/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/22/22 Pct Recovery = 78% Analysis Date = 01/22/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/13/22 Pct Recovery = 78% Analysis Date = 01/13/22 Pct Recovery = 78% Analysis Date = 01/09/22 Pct Recovery = 78% Analysis Date = 01/09/22 Pct Recovery = 78% Analysis Date = 01/05/22 Pct Recovery = 78% Analysis Date = 01/05/22 Pct Recovery = 78% Analysis Date = 12/31/21 Pct Recovery = 78% Analysis Date = 12/31/21 Pct Recovery = 78% Analysis Date = 12/27/21 Pct Recovery = 79% Analysis Date = 12/27/21 Pct Recovery = 79% Analysis Date = 12/23/21 Pct Recovery = 79% Analysis Date = 12/23/21 Pct Recovery = 79% Analysis Date = 12/18/21 Pct Recovery = 79% Analysis Date = 12/18/21 Pct Recovery = 79% Analysis Date = 12/14/21 Pct Recovery = 79% Analysis Date = 12/14/21 Pct Recovery = 79% Analysis Date = 12/10/21 Pct Recovery = 79% Analysis Date = 12/10/21 Pct Recovery = 79% Analysis Date = 12/05/21 Pct Recovery = 79% Analysis Date = 12/05/21 Pct Recovery = 79% Analysis Date = 12/01/21 Pct Recovery = 79% Analysis Date = 12/01/21 Pct Recovery = 79% Analysis Date = 11/27/21 Pct Recovery = 80% Analysis Date = 11/27/21 Pct Recovery = 80% Analysis Date = 11/22/21 Pct Recovery = 80% Analysis Date = 11/22/21 Pct Recovery = 80% Analysis Date = 11/18/21 Pct Recovery = 80% Analysis Date = 11/18/21 Pct Recovery = 80% Analysis Date = 11/14/21 Pct Recovery = 80% Analysis Date = 11/14/21 Pct Recovery = 80% Analysis Date = 11/09/21 Pct Recovery = 81% Analysis Date = 11/09/21 Pct Recovery = 81% Analysis Date = 11/05/21 Pct Recovery = 81% Analysis Date = 11/05/21 Pct Recovery = 81% Analysis Date = 11/01/21 Pct Recovery = 81% Analysis Date = 11/01/21 Pct Recovery = 81% Analysis Date = 10/27/21 Pct Recovery = 82% Analysis Date = 10/27/21 Pct Recovery = 82% Analysis Date = 10/23/21 Pct Recovery = 82% Analysis Date = 10/23/21 Pct Recovery = 82% Analysis Date = 10/19/21 Pct Recovery = 82% Analysis Date = 10/19/21 Pct Recovery = 82% Analysis Date = 10/14/21 Pct Recovery = 82% Analysis Date = 10/14/21 Pct Recovery = 82% Analysis Date = 10/10/21 Pct Recovery = 83% Analysis Date = 10/10/21 Pct Recovery = 83% Analysis Date = 10/06/21 Pct Recovery = 83% Analysis Date = 10/06/21 Pct Recovery = 83% Analysis Date = 10/01/21 Pct Recovery = 83% Analysis Date = 10/01/21 Pct Recovery = 83% Analysis Date = 09/27/21 Pct Recovery = 83% Analysis Date = 09/27/21 Pct Recovery = 83% Analysis Date = 09/23/21 Pct Recovery = 84% Analysis Date = 09/23/21 Pct Recovery = 84% Analysis Date = 09/18/21 Pct Recovery = 84% Analysis Date = 09/18/21 Pct Recovery = 84% Analysis Date = 09/14/21 Pct Recovery = 84% Analysis Date = 09/14/21 Pct Recovery = 84% Analysis Date = 09/10/21 Pct Recovery = 85% Analysis Date = 09/10/21 Pct Recovery = 85% Analysis Date = 09/05/21 Pct Recovery = 85% Analysis Date = 09/05/21 Pct Recovery = 85% Analysis Date = 09/01/21 Pct Recovery = 85% Analysis Date = 09/01/21 Pct Recovery = 85% Analysis Date = 08/28/21 Pct Recovery = 85% Analysis Date = 08/28/21 Pct Recovery = 85% Analysis Date = 08/23/21 Pct Recovery = 86% Analysis Date = 08/23/21 Pct Recovery = 86% Analysis Date = 08/19/21 Pct Recovery = 86% Analysis Date = 08/19/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/10/21 Pct Recovery = 86% Analysis Date = 08/10/21 Pct Recovery = 86% Analysis Date = 08/06/21 Pct Recovery = 87% Analysis Date = 08/06/21 Pct Recovery = 87% Analysis Date = 08/02/21 Pct Recovery = 87% Analysis Date = 08/02/21 Pct Recovery = 87% Analysis Date = 07/28/21 Pct Recovery = 87% Analysis Date = 07/28/21 Pct Recovery = 87% Analysis Date = 07/24/21 Pct Recovery = 88% Analysis Date = 07/24/21 Pct Recovery = 88% Analysis Date = 07/20/21 Pct Recovery = 88% Analysis Date = 07/20/21 Pct Recovery = 88% Analysis Date = 07/15/21 Pct Recovery = 88% Analysis Date = 07/15/21 Pct Recovery = 88% Analysis Date = 07/11/21 Pct Recovery = 88% Analysis Date = 07/11/21 Pct Recovery = 88% Analysis Date = 07/07/21 Pct Recovery = 89% Analysis Date = 07/07/21 Pct Recovery = 89% Analysis Date = 07/02/21 Pct Recovery = 89% Analysis Date = 07/02/21 Pct Recovery = 89% Analysis Date = 06/28/21 Pct Recovery = 89% Analysis Date = 06/28/21 Pct Recovery = 89% Analysis Date = 06/24/21 Pct Recovery = 89% Analysis Date = 06/24/21 Pct Recovery = 89% Analysis Date = 06/19/21 Pct Recovery = 90% Analysis Date = 06/19/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/06/21 Pct Recovery = 91% Analysis Date = 06/06/21 Pct Recovery = 91% Analysis Date = 06/02/21 Pct Recovery = 91% Analysis Date = 06/02/21 Pct Recovery = 91% Analysis Date = 05/29/21 Pct Recovery = 91% Analysis Date = 05/29/21 Pct Recovery = 91% Analysis Date = 05/24/21 Pct Recovery = 91% Analysis Date = 05/24/21 Pct Recovery = 91% Analysis Date = 05/20/21 Pct Recovery = 92% Analysis Date = 05/20/21 Pct Recovery = 92% Analysis Date = 05/16/21 Pct Recovery = 92% Analysis Date = 05/16/21 Pct Recovery = 92% Analysis Date = 05/11/21 Pct Recovery = 92% Analysis Date = 05/11/21 Pct Recovery = 92% Analysis Date = 05/07/21 Pct Recovery = 93% Analysis Date = 05/07/21 Pct Recovery = 93% Analysis Date = 05/03/21 Pct Recovery = 93% Analysis Date = 05/03/21 Pct Recovery = 93% Analysis Date = 04/28/21 Pct Recovery = 93% Analysis Date = 04/28/21 Pct Recovery = 93% Analysis Date = 04/24/21 Pct Recovery = 93% Analysis Date = 04/24/21 Pct Recovery = 93% Analysis Date = 04/20/21 Pct Recovery = 94% Analysis Date = 04/20/21 Pct Recovery = 94% Analysis Date = 04/15/21 Pct Recovery = 94% Analysis Date = 04/15/21 Pct Recovery = 94% Analysis Date = 04/11/21 Pct Recovery = 94% Analysis Date = 04/11/21 Pct Recovery = 94% Analysis Date = 04/07/21 Pct Recovery = 94% Analysis Date = 04/07/21 Pct Recovery = 94% Analysis Date = 04/02/21 Pct Recovery = 94% Analysis Date = 04/02/21 Pct Recovery = 94% Analysis Date = 03/29/21 Pct Recovery = 94% Analysis Date = 03/29/21 Pct Recovery = 94% Analysis Date = 03/25/21 Pct Recovery = 94% Analysis Date = 03/25/21 Pct Recovery = 94% Analysis Date = 03/20/21 Pct Recovery = 93% Analysis Date = 03/20/21 Pct Recovery = 93% Analysis Date = 03/16/21 Pct Recovery = 93% Analysis Date = 03/16/21 Pct Recovery = 93% Analysis Date = 03/12/21 Pct Recovery = 92% Analysis Date = 03/12/21 Pct Recovery = 92% Analysis Date = 03/07/21 Pct Recovery = 92% Analysis Date = 03/07/21 Pct Recovery = 92% Analysis Date = 03/03/21 Pct Recovery = 92% Analysis Date = 03/03/21 Pct Recovery = 92% Analysis Date = 02/27/21 Pct Recovery = 91% Analysis Date = 02/27/21 Pct Recovery = 91% Analysis Date = 02/22/21 Pct Recovery = 91% Analysis Date = 02/22/21 Pct Recovery = 91% Analysis Date = 02/18/21 Pct Recovery = 90% Analysis Date = 02/18/21 Pct Recovery = 90% Analysis Date = 02/14/21 Pct Recovery = 90% Analysis Date = 02/14/21 Pct Recovery = 90% Analysis Date = 02/09/21 Pct Recovery = 89% Analysis Date = 02/09/21 Pct Recovery = 89% Analysis Date = 02/05/21 Pct Recovery = 89% Analysis Date = 02/05/21 Pct Recovery = 89% Analysis Date = 02/01/21 Pct Recovery = 88% Analysis Date = 02/01/21 Pct Recovery = 88% Analysis Date = 01/27/21 Pct Recovery = 88% Analysis Date = 01/27/21 Pct Recovery = 88% Analysis Date = 01/23/21 Pct Recovery = 88% Analysis Date = 01/23/21 Pct Recovery = 88% Analysis Date = 01/19/21 Pct Recovery = 87% Analysis Date = 01/19/21 Pct Recovery = 87% Analysis Date = 01/14/21 Pct Recovery = 87% Analysis Date = 01/14/21 Pct Recovery = 87% Analysis Date = 01/10/21 Pct Recovery = 86% Analysis Date = 01/10/21 Pct Recovery = 86% Analysis Date = 01/06/21 Pct Recovery = 86% Analysis Date = 01/06/21 Pct Recovery = 86% Analysis Date = 01/01/21 Pct Recovery = 85% Analysis Date = 01/01/21 Pct Recovery = 85% Analysis Date = 12/28/20 Pct Recovery = 85% Analysis Date = 12/28/20 Pct Recovery = 85% Analysis Date = 12/24/20 Pct Recovery = 85% Analysis Date = 12/24/20 Pct Recovery = 85% Analysis Date = 12/19/20 Pct Recovery = 84% Analysis Date = 12/19/20 Pct Recovery = 84% Analysis Date = 12/15/20 Pct Recovery = 84% Analysis Date = 12/15/20 Pct Recovery = 84% Analysis Date = 12/11/20 Pct Recovery = 83% Analysis Date = 12/11/20 Pct Recovery = 83% Analysis Date = 12/06/20 Pct Recovery = 83% Analysis Date = 12/06/20 Pct Recovery = 83% Analysis Date = 12/02/20 Pct Recovery = 83% Analysis Date = 12/02/20 Pct Recovery = 83% Analysis Date = 11/28/20 Pct Recovery = 83% Analysis Date = 11/28/20 Pct Recovery = 83% Analysis Date = 11/23/20 Pct Recovery = 83% Analysis Date = 11/23/20 Pct Recovery = 83% Analysis Date = 11/19/20 Pct Recovery = 83% Analysis Date = 11/19/20 Pct Recovery = 83% Analysis Date = 11/15/20 Pct Recovery = 83% Analysis Date = 11/15/20 Pct Recovery = 83% Analysis Date = 11/10/20 Pct Recovery = 82% Analysis Date = 11/10/20 Pct Recovery = 82% Analysis Date = 11/06/20 Pct Recovery = 82% Analysis Date = 11/06/20 Pct Recovery = 82% Analysis Date = 11/02/20 Pct Recovery = 82% Analysis Date = 11/02/20 Pct Recovery = 82% Analysis Date = 10/28/20 Pct Recovery = 82% Analysis Date = 10/28/20 Pct Recovery = 82% Analysis Date = 10/24/20 Pct Recovery = 82% Analysis Date = 10/24/20 Pct Recovery = 82% Analysis Date = 10/20/20 Pct Recovery = 82% Analysis Date = 10/20/20 Pct Recovery = 82% Analysis Date = 10/15/20 Pct Recovery = 82% Analysis Date = 10/15/20 Pct Recovery = 82% Analysis Date = 10/11/20 Pct Recovery = 81% Analysis Date = 10/11/20 Pct Recovery = 81% Analysis Date = 10/07/20 Pct Recovery = 81% Analysis Date = 10/07/20 Pct Recovery = 81% Analysis Date = 10/02/20 Pct Recovery = 81% Analysis Date = 10/02/20 Pct Recovery = 81% Analysis Date = 09/28/20 Pct Recovery = 81% Analysis Date = 09/28/20 Pct Recovery = 81% Analysis Date = 09/24/20 Pct Recovery = 80% Analysis Date = 09/24/20 Pct Recovery = 80% Analysis Date = 09/19/20 Pct Recovery = 80% Analysis Date = 09/19/20 Pct Recovery = 80% Analysis Date = 09/15/20 Pct Recovery = 80% Analysis Date = 09/15/20 Pct Recovery = 80% Analysis Date = 09/11/20 Pct Recovery = 79% Analysis Date = 09/11/20 Pct Recovery = 79% Analysis Date = 09/06/20 Pct Recovery = 79% Analysis Date = 09/06/20 Pct Recovery = 79% Analysis Date = 09/02/20 Pct Recovery = 78% Analysis Date = 09/02/20 Pct Recovery = 78% Analysis Date = 08/29/20 Pct Recovery = 78% Analysis Date = 08/29/20 Pct Recovery = 78% Analysis Date = 08/24/20 Pct Recovery = 78% Analysis Date = 08/24/20 Pct Recovery = 78% Analysis Date = 08/20/20 Pct Recovery = 77% Analysis Date = 08/20/20 Pct Recovery = 77% Analysis Date = 08/16/20 Pct Recovery = 77% Analysis Date = 08/16/20 Pct Recovery = 77% Analysis Date = 08/11/20 Pct Recovery = 76% Analysis Date = 08/11/20 Pct Recovery = 76% Analysis Date = 08/07/20 Pct Recovery = 76% Analysis Date = 08/07/20 Pct Recovery = 76% Analysis Date = 08/03/20 Pct Recovery = 76% Analysis Date = 08/03/20 Pct Recovery = 76% Analysis Date = 07/29/20 Pct Recovery = 75% Analysis Date = 07/29/20 Pct Recovery = 75% Analysis Date = 07/25/20 Pct Recovery = 75% Analysis Date = 07/25/20 Pct Recovery = 75% Analysis Date = 07/21/20 Pct Recovery = 75% Analysis Date = 07/21/20 Pct Recovery = 75% Analysis Date = 07/16/20 Pct Recovery = 74% Analysis Date = 07/16/20 Pct Recovery = 74% Analysis Date = 07/12/20 Pct Recovery = 74% Analysis Date = 07/12/20 Pct Recovery = 74% Analysis Date = 07/08/20 Pct Recovery = 73% Analysis Date = 07/08/20 Pct Recovery = 73% Analysis Date = 07/03/20 Pct Recovery = 73% Analysis Date = 07/03/20 Pct Recovery = 73% Analysis Date = 06/29/20 Pct Recovery = 72% Analysis Date = 06/29/20 Pct Recovery = 72% Analysis Date = 06/25/20 Pct Recovery = 72% Analysis Date = 06/25/20 Pct Recovery = 72% Analysis Date = 06/20/20 Pct Recovery = 72% Analysis Date = 06/20/20 Pct Recovery = 72% Analysis Date = 06/16/20 Pct Recovery = 71% Analysis Date = 06/16/20 Pct Recovery = 71% Analysis Date = 06/12/20 Pct Recovery = 71% Analysis Date = 06/12/20 Pct Recovery = 71% Analysis Date = 06/07/20 Pct Recovery = 70% Analysis Date = 06/07/20 Pct Recovery = 70% Analysis Date = 06/03/20 Pct Recovery = 70% Analysis Date = 06/03/20 Pct Recovery = 70% Analysis Date = 05/30/20 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOXYNIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 80% 26% 72% 15%
Total 44 80% 26% 72% 15%

Sample Statistics
BROMOXYNIL

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 11 25% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 72 .  
False Positives 0 0% 0 out of 72

OBSP Determination:
CARBARYL
METHOD: 2447 , TESTIDCODE: 65069LCM60

Laboratory ID = 20213200091 Lab Value = 77.601 Expected Conc. = 35.6 Report level label = 5.6 Pct Recovery = 218% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20203230021 Lab Value = 59.583 Expected Conc. = 70.23 Report level label = 5.6 Pct Recovery = 85% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 60.518 Expected Conc. = 70.23 Report level label = 5.6 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 63.213 Expected Conc. = 70.2 Report level label = 5.6 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 64.537 Expected Conc. = 70.2 Report level label = 5.6 Pct Recovery = 92% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220190116 Lab Value = 39.556 Expected Conc. = 57.28 Report level label = 5.6 Pct Recovery = 69% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 39.186 Expected Conc. = 57.28 Report level label = 5.6 Pct Recovery = 68% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20212990174 Lab Value = 31.516 Expected Conc. = 56.96 Report level label = 5.6 Pct Recovery = 55% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220810134 Lab Value = 47.721 Expected Conc. = 56.8 Report level label = 5.6 Pct Recovery = 84% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222150193 Lab Value = 41.350 Expected Conc. = 56.4 Report level label = 5.6 Pct Recovery = 73% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20222010132 Lab Value = 34.357 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 61% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20221730293 Lab Value = 40.066 Expected Conc. = 35.8 Report level label = 5.6 Pct Recovery = 112% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 16.898 Expected Conc. = 35.8 Report level label = 5.6 Pct Recovery = 47% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20213340027 Lab Value = 32.497 Expected Conc. = 35.6 Report level label = 5.6 Pct Recovery = 91% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 27.733 Expected Conc. = 35.6 Report level label = 5.6 Pct Recovery = 78% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20220810133 Lab Value = 30.597 Expected Conc. = 35.5 Report level label = 5.6 Pct Recovery = 86% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20203230018 Lab Value = 26.741 Expected Conc. = 35.1 Report level label = 5.6 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 26.038 Expected Conc. = 35.1 Report level label = 5.6 Pct Recovery = 74% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 30.396 Expected Conc. = 35.1 Report level label = 5.6 Pct Recovery = 87% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 48.286 Expected Conc. = 35 Report level label = 5.6 Pct Recovery = 138% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 39.329 Expected Conc. = 35 Report level label = 5.6 Pct Recovery = 112% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201550031 Lab Value = 30.168 Expected Conc. = 34.9 Report level label = 5.6 Pct Recovery = 86% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20201960104 Lab Value = 29.949 Expected Conc. = 28 Report level label = 5.6 Pct Recovery = 107% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 37.626 Expected Conc. = 28 Report level label = 5.6 Pct Recovery = 134% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20222500483 Lab Value = 5.622 Expected Conc. = 14.32 Report level label = 5.6 Pct Recovery = 39% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 6.579 Expected Conc. = 14.32 Report level label = 5.6 Pct Recovery = 46% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213060210 Lab Value = 8.802 Expected Conc. = 14.24 Report level label = 5.6 Pct Recovery = 62% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222630205 Lab Value = 10.766 Expected Conc. = 14.2 Report level label = 5.6 Pct Recovery = 76% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210830019 Lab Value = 18.423 Expected Conc. = 14.046 Report level label = 5.6 Pct Recovery = 131% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 10.510 Expected Conc. = 14.046 Report level label = 5.6 Pct Recovery = 75% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 16.741 Expected Conc. = 14.04 Report level label = 5.6 Pct Recovery = 119% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 16.300 Expected Conc. = 14.04 Report level label = 5.6 Pct Recovery = 116% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 15.850 Expected Conc. = 14.04 Report level label = 5.6 Pct Recovery = 113% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 12.401 Expected Conc. = 14.04 Report level label = 5.6 Pct Recovery = 88% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 15.577 Expected Conc. = 14.04 Report level label = 5.6 Pct Recovery = 111% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 11.392 Expected Conc. = 14.04 Report level label = 5.6 Pct Recovery = 81% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 9.878 Expected Conc. = 13.96 Report level label = 5.6 Pct Recovery = 71% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 9.167 Expected Conc. = 13.96 Report level label = 5.6 Pct Recovery = 66% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 18.667 Expected Conc. = 13.96 Report level label = 5.6 Pct Recovery = 134% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 17.233 Expected Conc. = 13.96 Report level label = 5.6 Pct Recovery = 123% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 16.701 Expected Conc. = 13.96 Report level label = 5.6 Pct Recovery = 120% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Analysis Date = 09/28/22 Pct Recovery = 66% Analysis Date = 09/24/22 Pct Recovery = 66% Analysis Date = 09/24/22 Pct Recovery = 66% Analysis Date = 09/20/22 Pct Recovery = 67% Analysis Date = 09/20/22 Pct Recovery = 67% Analysis Date = 09/16/22 Pct Recovery = 67% Analysis Date = 09/16/22 Pct Recovery = 67% Analysis Date = 09/11/22 Pct Recovery = 67% Analysis Date = 09/11/22 Pct Recovery = 67% Analysis Date = 09/07/22 Pct Recovery = 67% Analysis Date = 09/07/22 Pct Recovery = 67% Analysis Date = 09/03/22 Pct Recovery = 68% Analysis Date = 09/03/22 Pct Recovery = 68% Analysis Date = 08/30/22 Pct Recovery = 68% Analysis Date = 08/30/22 Pct Recovery = 68% Analysis Date = 08/25/22 Pct Recovery = 68% Analysis Date = 08/25/22 Pct Recovery = 68% Analysis Date = 08/21/22 Pct Recovery = 69% Analysis Date = 08/21/22 Pct Recovery = 69% Analysis Date = 08/17/22 Pct Recovery = 69% Analysis Date = 08/17/22 Pct Recovery = 69% Analysis Date = 08/13/22 Pct Recovery = 69% Analysis Date = 08/13/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/04/22 Pct Recovery = 70% Analysis Date = 08/04/22 Pct Recovery = 70% Analysis Date = 07/31/22 Pct Recovery = 70% Analysis Date = 07/31/22 Pct Recovery = 70% Analysis Date = 07/27/22 Pct Recovery = 70% Analysis Date = 07/27/22 Pct Recovery = 70% Analysis Date = 07/22/22 Pct Recovery = 71% Analysis Date = 07/22/22 Pct Recovery = 71% Analysis Date = 07/18/22 Pct Recovery = 71% Analysis Date = 07/18/22 Pct Recovery = 71% Analysis Date = 07/14/22 Pct Recovery = 71% Analysis Date = 07/14/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 07/01/22 Pct Recovery = 72% Analysis Date = 07/01/22 Pct Recovery = 72% Analysis Date = 06/27/22 Pct Recovery = 72% Analysis Date = 06/27/22 Pct Recovery = 72% Analysis Date = 06/22/22 Pct Recovery = 73% Analysis Date = 06/22/22 Pct Recovery = 73% Analysis Date = 06/18/22 Pct Recovery = 73% Analysis Date = 06/18/22 Pct Recovery = 73% Analysis Date = 06/14/22 Pct Recovery = 73% Analysis Date = 06/14/22 Pct Recovery = 73% Analysis Date = 06/10/22 Pct Recovery = 73% Analysis Date = 06/10/22 Pct Recovery = 73% Analysis Date = 06/05/22 Pct Recovery = 74% Analysis Date = 06/05/22 Pct Recovery = 74% Analysis Date = 06/01/22 Pct Recovery = 74% Analysis Date = 06/01/22 Pct Recovery = 74% Analysis Date = 05/28/22 Pct Recovery = 74% Analysis Date = 05/28/22 Pct Recovery = 74% Analysis Date = 05/24/22 Pct Recovery = 75% Analysis Date = 05/24/22 Pct Recovery = 75% Analysis Date = 05/19/22 Pct Recovery = 75% Analysis Date = 05/19/22 Pct Recovery = 75% Analysis Date = 05/15/22 Pct Recovery = 75% Analysis Date = 05/15/22 Pct Recovery = 75% Analysis Date = 05/11/22 Pct Recovery = 76% Analysis Date = 05/11/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 04/28/22 Pct Recovery = 76% Analysis Date = 04/28/22 Pct Recovery = 76% Analysis Date = 04/24/22 Pct Recovery = 77% Analysis Date = 04/24/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/15/22 Pct Recovery = 77% Analysis Date = 04/15/22 Pct Recovery = 77% Analysis Date = 04/11/22 Pct Recovery = 78% Analysis Date = 04/11/22 Pct Recovery = 78% Analysis Date = 04/07/22 Pct Recovery = 78% Analysis Date = 04/07/22 Pct Recovery = 78% Analysis Date = 04/02/22 Pct Recovery = 78% Analysis Date = 04/02/22 Pct Recovery = 78% Analysis Date = 03/29/22 Pct Recovery = 78% Analysis Date = 03/29/22 Pct Recovery = 78% Analysis Date = 03/25/22 Pct Recovery = 79% Analysis Date = 03/25/22 Pct Recovery = 79% Analysis Date = 03/21/22 Pct Recovery = 79% Analysis Date = 03/21/22 Pct Recovery = 79% Analysis Date = 03/16/22 Pct Recovery = 79% Analysis Date = 03/16/22 Pct Recovery = 79% Analysis Date = 03/12/22 Pct Recovery = 80% Analysis Date = 03/12/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 80% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/23/22 Pct Recovery = 81% Analysis Date = 02/23/22 Pct Recovery = 81% Analysis Date = 02/19/22 Pct Recovery = 81% Analysis Date = 02/19/22 Pct Recovery = 81% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 01/28/22 Pct Recovery = 83% Analysis Date = 01/28/22 Pct Recovery = 83% Analysis Date = 01/24/22 Pct Recovery = 83% Analysis Date = 01/24/22 Pct Recovery = 83% Analysis Date = 01/20/22 Pct Recovery = 83% Analysis Date = 01/20/22 Pct Recovery = 83% Analysis Date = 01/16/22 Pct Recovery = 84% Analysis Date = 01/16/22 Pct Recovery = 84% Analysis Date = 01/11/22 Pct Recovery = 84% Analysis Date = 01/11/22 Pct Recovery = 84% Analysis Date = 01/07/22 Pct Recovery = 84% Analysis Date = 01/07/22 Pct Recovery = 84% Analysis Date = 01/03/22 Pct Recovery = 85% Analysis Date = 01/03/22 Pct Recovery = 85% Analysis Date = 12/30/21 Pct Recovery = 85% Analysis Date = 12/30/21 Pct Recovery = 85% Analysis Date = 12/25/21 Pct Recovery = 85% Analysis Date = 12/25/21 Pct Recovery = 85% Analysis Date = 12/21/21 Pct Recovery = 85% Analysis Date = 12/21/21 Pct Recovery = 85% Analysis Date = 12/17/21 Pct Recovery = 86% Analysis Date = 12/17/21 Pct Recovery = 86% Analysis Date = 12/12/21 Pct Recovery = 86% Analysis Date = 12/12/21 Pct Recovery = 86% Analysis Date = 12/08/21 Pct Recovery = 86% Analysis Date = 12/08/21 Pct Recovery = 86% Analysis Date = 12/04/21 Pct Recovery = 87% Analysis Date = 12/04/21 Pct Recovery = 87% Analysis Date = 11/30/21 Pct Recovery = 87% Analysis Date = 11/30/21 Pct Recovery = 87% Analysis Date = 11/25/21 Pct Recovery = 87% Analysis Date = 11/25/21 Pct Recovery = 87% Analysis Date = 11/21/21 Pct Recovery = 87% Analysis Date = 11/21/21 Pct Recovery = 87% Analysis Date = 11/17/21 Pct Recovery = 88% Analysis Date = 11/17/21 Pct Recovery = 88% Analysis Date = 11/13/21 Pct Recovery = 88% Analysis Date = 11/13/21 Pct Recovery = 88% Analysis Date = 11/08/21 Pct Recovery = 88% Analysis Date = 11/08/21 Pct Recovery = 88% Analysis Date = 11/04/21 Pct Recovery = 89% Analysis Date = 11/04/21 Pct Recovery = 89% Analysis Date = 10/31/21 Pct Recovery = 89% Analysis Date = 10/31/21 Pct Recovery = 89% Analysis Date = 10/27/21 Pct Recovery = 89% Analysis Date = 10/27/21 Pct Recovery = 89% Analysis Date = 10/22/21 Pct Recovery = 90% Analysis Date = 10/22/21 Pct Recovery = 90% Analysis Date = 10/18/21 Pct Recovery = 90% Analysis Date = 10/18/21 Pct Recovery = 90% Analysis Date = 10/14/21 Pct Recovery = 90% Analysis Date = 10/14/21 Pct Recovery = 90% Analysis Date = 10/10/21 Pct Recovery = 90% Analysis Date = 10/10/21 Pct Recovery = 90% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/01/21 Pct Recovery = 91% Analysis Date = 10/01/21 Pct Recovery = 91% Analysis Date = 09/27/21 Pct Recovery = 91% Analysis Date = 09/27/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 92% Analysis Date = 09/22/21 Pct Recovery = 92% Analysis Date = 09/18/21 Pct Recovery = 92% Analysis Date = 09/18/21 Pct Recovery = 92% Analysis Date = 09/14/21 Pct Recovery = 92% Analysis Date = 09/14/21 Pct Recovery = 92% Analysis Date = 09/10/21 Pct Recovery = 93% Analysis Date = 09/10/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 93% Analysis Date = 08/24/21 Pct Recovery = 94% Analysis Date = 08/24/21 Pct Recovery = 94% Analysis Date = 08/19/21 Pct Recovery = 94% Analysis Date = 08/19/21 Pct Recovery = 94% Analysis Date = 08/15/21 Pct Recovery = 94% Analysis Date = 08/15/21 Pct Recovery = 94% Analysis Date = 08/11/21 Pct Recovery = 95% Analysis Date = 08/11/21 Pct Recovery = 95% Analysis Date = 08/07/21 Pct Recovery = 95% Analysis Date = 08/07/21 Pct Recovery = 95% Analysis Date = 08/02/21 Pct Recovery = 95% Analysis Date = 08/02/21 Pct Recovery = 95% Analysis Date = 07/29/21 Pct Recovery = 95% Analysis Date = 07/29/21 Pct Recovery = 95% Analysis Date = 07/25/21 Pct Recovery = 96% Analysis Date = 07/25/21 Pct Recovery = 96% Analysis Date = 07/20/21 Pct Recovery = 96% Analysis Date = 07/20/21 Pct Recovery = 96% Analysis Date = 07/16/21 Pct Recovery = 96% Analysis Date = 07/16/21 Pct Recovery = 96% Analysis Date = 07/12/21 Pct Recovery = 97% Analysis Date = 07/12/21 Pct Recovery = 97% Analysis Date = 07/08/21 Pct Recovery = 97% Analysis Date = 07/08/21 Pct Recovery = 97% Analysis Date = 07/03/21 Pct Recovery = 97% Analysis Date = 07/03/21 Pct Recovery = 97% Analysis Date = 06/29/21 Pct Recovery = 98% Analysis Date = 06/29/21 Pct Recovery = 98% Analysis Date = 06/25/21 Pct Recovery = 98% Analysis Date = 06/25/21 Pct Recovery = 98% Analysis Date = 06/21/21 Pct Recovery = 98% Analysis Date = 06/21/21 Pct Recovery = 98% Analysis Date = 06/16/21 Pct Recovery = 98% Analysis Date = 06/16/21 Pct Recovery = 98% Analysis Date = 06/12/21 Pct Recovery = 99% Analysis Date = 06/12/21 Pct Recovery = 99% Analysis Date = 06/08/21 Pct Recovery = 99% Analysis Date = 06/08/21 Pct Recovery = 99% Analysis Date = 06/04/21 Pct Recovery = 99% Analysis Date = 06/04/21 Pct Recovery = 99% Analysis Date = 05/30/21 Pct Recovery = 100% Analysis Date = 05/30/21 Pct Recovery = 100% Analysis Date = 05/26/21 Pct Recovery = 100% Analysis Date = 05/26/21 Pct Recovery = 100% Analysis Date = 05/22/21 Pct Recovery = 100% Analysis Date = 05/22/21 Pct Recovery = 100% Analysis Date = 05/17/21 Pct Recovery = 101% Analysis Date = 05/17/21 Pct Recovery = 101% Analysis Date = 05/13/21 Pct Recovery = 101% Analysis Date = 05/13/21 Pct Recovery = 101% Analysis Date = 05/09/21 Pct Recovery = 101% Analysis Date = 05/09/21 Pct Recovery = 101% Analysis Date = 05/05/21 Pct Recovery = 101% Analysis Date = 05/05/21 Pct Recovery = 101% Analysis Date = 04/30/21 Pct Recovery = 102% Analysis Date = 04/30/21 Pct Recovery = 102% Analysis Date = 04/26/21 Pct Recovery = 102% Analysis Date = 04/26/21 Pct Recovery = 102% Analysis Date = 04/22/21 Pct Recovery = 102% Analysis Date = 04/22/21 Pct Recovery = 102% Analysis Date = 04/18/21 Pct Recovery = 103% Analysis Date = 04/18/21 Pct Recovery = 103% Analysis Date = 04/13/21 Pct Recovery = 103% Analysis Date = 04/13/21 Pct Recovery = 103% Analysis Date = 04/09/21 Pct Recovery = 103% Analysis Date = 04/09/21 Pct Recovery = 103% Analysis Date = 04/05/21 Pct Recovery = 103% Analysis Date = 04/05/21 Pct Recovery = 103% Analysis Date = 04/01/21 Pct Recovery = 104% Analysis Date = 04/01/21 Pct Recovery = 104% Analysis Date = 03/27/21 Pct Recovery = 104% Analysis Date = 03/27/21 Pct Recovery = 104% Analysis Date = 03/23/21 Pct Recovery = 103% Analysis Date = 03/23/21 Pct Recovery = 103% Analysis Date = 03/19/21 Pct Recovery = 103% Analysis Date = 03/19/21 Pct Recovery = 103% Analysis Date = 03/15/21 Pct Recovery = 102% Analysis Date = 03/15/21 Pct Recovery = 102% Analysis Date = 03/10/21 Pct Recovery = 102% Analysis Date = 03/10/21 Pct Recovery = 102% Analysis Date = 03/06/21 Pct Recovery = 102% Analysis Date = 03/06/21 Pct Recovery = 102% Analysis Date = 03/02/21 Pct Recovery = 101% Analysis Date = 03/02/21 Pct Recovery = 101% Analysis Date = 02/25/21 Pct Recovery = 101% Analysis Date = 02/25/21 Pct Recovery = 101% Analysis Date = 02/21/21 Pct Recovery = 100% Analysis Date = 02/21/21 Pct Recovery = 100% Analysis Date = 02/17/21 Pct Recovery = 100% Analysis Date = 02/17/21 Pct Recovery = 100% Analysis Date = 02/13/21 Pct Recovery = 100% Analysis Date = 02/13/21 Pct Recovery = 100% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/04/21 Pct Recovery = 99% Analysis Date = 02/04/21 Pct Recovery = 99% Analysis Date = 01/31/21 Pct Recovery = 99% Analysis Date = 01/31/21 Pct Recovery = 99% Analysis Date = 01/27/21 Pct Recovery = 98% Analysis Date = 01/27/21 Pct Recovery = 98% Analysis Date = 01/22/21 Pct Recovery = 98% Analysis Date = 01/22/21 Pct Recovery = 98% Analysis Date = 01/18/21 Pct Recovery = 98% Analysis Date = 01/18/21 Pct Recovery = 98% Analysis Date = 01/14/21 Pct Recovery = 97% Analysis Date = 01/14/21 Pct Recovery = 97% Analysis Date = 01/10/21 Pct Recovery = 97% Analysis Date = 01/10/21 Pct Recovery = 97% Analysis Date = 01/05/21 Pct Recovery = 97% Analysis Date = 01/05/21 Pct Recovery = 97% Analysis Date = 01/01/21 Pct Recovery = 96% Analysis Date = 01/01/21 Pct Recovery = 96% Analysis Date = 12/28/20 Pct Recovery = 96% Analysis Date = 12/28/20 Pct Recovery = 96% Analysis Date = 12/23/20 Pct Recovery = 96% Analysis Date = 12/23/20 Pct Recovery = 96% Analysis Date = 12/19/20 Pct Recovery = 95% Analysis Date = 12/19/20 Pct Recovery = 95% Analysis Date = 12/15/20 Pct Recovery = 95% Analysis Date = 12/15/20 Pct Recovery = 95% Analysis Date = 12/11/20 Pct Recovery = 95% Analysis Date = 12/11/20 Pct Recovery = 95% Analysis Date = 12/06/20 Pct Recovery = 94% Analysis Date = 12/06/20 Pct Recovery = 94% Analysis Date = 12/02/20 Pct Recovery = 94% Analysis Date = 12/02/20 Pct Recovery = 94% Analysis Date = 11/28/20 Pct Recovery = 94% Analysis Date = 11/28/20 Pct Recovery = 94% Analysis Date = 11/24/20 Pct Recovery = 93% Analysis Date = 11/24/20 Pct Recovery = 93% Analysis Date = 11/19/20 Pct Recovery = 93% Analysis Date = 11/19/20 Pct Recovery = 93% Analysis Date = 11/15/20 Pct Recovery = 93% Analysis Date = 11/15/20 Pct Recovery = 93% Analysis Date = 11/11/20 Pct Recovery = 93% Analysis Date = 11/11/20 Pct Recovery = 93% Analysis Date = 11/07/20 Pct Recovery = 93% Analysis Date = 11/07/20 Pct Recovery = 93% Analysis Date = 11/02/20 Pct Recovery = 94% Analysis Date = 11/02/20 Pct Recovery = 94% Analysis Date = 10/29/20 Pct Recovery = 94% Analysis Date = 10/29/20 Pct Recovery = 94% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 95% Analysis Date = 10/16/20 Pct Recovery = 96% Analysis Date = 10/16/20 Pct Recovery = 96% Analysis Date = 10/12/20 Pct Recovery = 96% Analysis Date = 10/12/20 Pct Recovery = 96% Analysis Date = 10/08/20 Pct Recovery = 97% Analysis Date = 10/08/20 Pct Recovery = 97% Analysis Date = 10/03/20 Pct Recovery = 98% Analysis Date = 10/03/20 Pct Recovery = 98% Analysis Date = 09/29/20 Pct Recovery = 98% Analysis Date = 09/29/20 Pct Recovery = 98% Analysis Date = 09/25/20 Pct Recovery = 99% Analysis Date = 09/25/20 Pct Recovery = 99% Analysis Date = 09/21/20 Pct Recovery = 99% Analysis Date = 09/21/20 Pct Recovery = 99% Analysis Date = 09/16/20 Pct Recovery = 100% Analysis Date = 09/16/20 Pct Recovery = 100% Analysis Date = 09/12/20 Pct Recovery = 100% Analysis Date = 09/12/20 Pct Recovery = 100% Analysis Date = 09/08/20 Pct Recovery = 101% Analysis Date = 09/08/20 Pct Recovery = 101% Analysis Date = 09/04/20 Pct Recovery = 102% Analysis Date = 09/04/20 Pct Recovery = 102% Analysis Date = 08/30/20 Pct Recovery = 102% Analysis Date = 08/30/20 Pct Recovery = 102% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/18/20 Pct Recovery = 104% Analysis Date = 08/18/20 Pct Recovery = 104% Analysis Date = 08/13/20 Pct Recovery = 105% Analysis Date = 08/13/20 Pct Recovery = 105% Analysis Date = 08/09/20 Pct Recovery = 105% Analysis Date = 08/09/20 Pct Recovery = 105% Analysis Date = 08/05/20 Pct Recovery = 106% Analysis Date = 08/05/20 Pct Recovery = 106% Analysis Date = 07/31/20 Pct Recovery = 106% Analysis Date = 07/31/20 Pct Recovery = 106% Analysis Date = 07/27/20 Pct Recovery = 107% Analysis Date = 07/27/20 Pct Recovery = 107% Analysis Date = 07/23/20 Pct Recovery = 107% Analysis Date = 07/23/20 Pct Recovery = 107% Analysis Date = 07/19/20 Pct Recovery = 108% Analysis Date = 07/19/20 Pct Recovery = 108% Analysis Date = 07/14/20 Pct Recovery = 109% Analysis Date = 07/14/20 Pct Recovery = 109% Analysis Date = 07/10/20 Pct Recovery = 109% Analysis Date = 07/10/20 Pct Recovery = 109% Analysis Date = 07/06/20 Pct Recovery = 110% Analysis Date = 07/06/20 Pct Recovery = 110% Analysis Date = 07/02/20 Pct Recovery = 111% Analysis Date = 07/02/20 Pct Recovery = 111% Analysis Date = 06/27/20 Pct Recovery = 111% Analysis Date = 06/27/20 Pct Recovery = 111% Analysis Date = 06/23/20 Pct Recovery = 112% Analysis Date = 06/23/20 Pct Recovery = 112% Analysis Date = 06/19/20 Pct Recovery = 113% Analysis Date = 06/19/20 Pct Recovery = 113% Analysis Date = 06/15/20 Pct Recovery = 113% Analysis Date = 06/15/20 Pct Recovery = 113% Analysis Date = 06/10/20 Pct Recovery = 114% Analysis Date = 06/10/20 Pct Recovery = 114% Analysis Date = 06/06/20 Pct Recovery = 115% Analysis Date = 06/06/20 Pct Recovery = 115% Analysis Date = 06/02/20 Pct Recovery = 115% Analysis Date = 06/02/20 Pct Recovery = 115% Analysis Date = 05/29/20 Pct Recovery = 116% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBARYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 92% 33% 86% 29%
Total 41 92% 33% 86% 29%

Sample Statistics
CARBARYL

Characteristic N % % Basis
Plotted 41 100% Spiked
Estimated Values 4 10% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 75 .  
False Positives 1 1% 1 out of 75

OBSP Determination:
CARBENDAZIM
METHOD: 2447 , TESTIDCODE: 68548LCM60

Laboratory ID = 20201820155 Lab Value = 109.729 Expected Conc. = 127.3 Report level label = 10 Pct Recovery = 86% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20202590106 Lab Value = 104.706 Expected Conc. = 125.7 Report level label = 10 Pct Recovery = 83% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 115.233 Expected Conc. = 125.7 Report level label = 10 Pct Recovery = 92% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 105.769 Expected Conc. = 125.1 Report level label = 10 Pct Recovery = 85% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 106.984 Expected Conc. = 125.1 Report level label = 10 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202110006 Lab Value = 107.228 Expected Conc. = 123.9 Report level label = 10 Pct Recovery = 87% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20212990174 Lab Value = 96.415 Expected Conc. = 100.8 Report level label = 10 Pct Recovery = 96% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12377000 Laboratory ID = 20222010132 Lab Value = 56.480 Expected Conc. = 100 Report level label = 10 Pct Recovery = 56% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20202530029 Lab Value = 54.392 Expected Conc. = 63.65 Report level label = 10 Pct Recovery = 85% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 56.486 Expected Conc. = 63.65 Report level label = 10 Pct Recovery = 89% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 64.744 Expected Conc. = 63.65 Report level label = 10 Pct Recovery = 102% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20213340027 Lab Value = 49.573 Expected Conc. = 63 Report level label = 10 Pct Recovery = 79% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12377000 Laboratory ID = 20213200091 Lab Value = 53.960 Expected Conc. = 63 Report level label = 10 Pct Recovery = 86% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12377000 Laboratory ID = 20213130215 Lab Value = 56.986 Expected Conc. = 63 Report level label = 10 Pct Recovery = 90% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12377000 Laboratory ID = 20203230018 Lab Value = 47.089 Expected Conc. = 62.85 Report level label = 10 Pct Recovery = 75% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 52.035 Expected Conc. = 62.85 Report level label = 10 Pct Recovery = 83% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 54.289 Expected Conc. = 62.85 Report level label = 10 Pct Recovery = 86% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201680155 Lab Value = 63.985 Expected Conc. = 61.95 Report level label = 10 Pct Recovery = 103% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 23.161 Expected Conc. = 25.46 Report level label = 10 Pct Recovery = 91% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 21.318 Expected Conc. = 25.46 Report level label = 10 Pct Recovery = 84% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 27.402 Expected Conc. = 25.46 Report level label = 10 Pct Recovery = 108% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 27.644 Expected Conc. = 25.46 Report level label = 10 Pct Recovery = 109% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20213060210 Lab Value = 20.903 Expected Conc. = 25.2 Report level label = 10 Pct Recovery = 83% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12377000 Laboratory ID = 20210340007 Lab Value = 22.470 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 89% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 21.945 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 87% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 26.109 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 104% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 24.845 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 99% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 23.798 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 95% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210830019 Lab Value = 24.926 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 100% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 25.231 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 101% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20201610160 Lab Value = 24.966 Expected Conc. = 24.78 Report level label = 10 Pct Recovery = 101% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Analysis Date = 07/23/22 Pct Recovery = 65% Analysis Date = 07/20/22 Pct Recovery = 65% Analysis Date = 07/20/22 Pct Recovery = 65% Analysis Date = 07/16/22 Pct Recovery = 65% Analysis Date = 07/16/22 Pct Recovery = 65% Analysis Date = 07/12/22 Pct Recovery = 66% Analysis Date = 07/12/22 Pct Recovery = 66% Analysis Date = 07/08/22 Pct Recovery = 66% Analysis Date = 07/08/22 Pct Recovery = 66% Analysis Date = 07/04/22 Pct Recovery = 66% Analysis Date = 07/04/22 Pct Recovery = 66% Analysis Date = 06/30/22 Pct Recovery = 67% Analysis Date = 06/30/22 Pct Recovery = 67% Analysis Date = 06/26/22 Pct Recovery = 67% Analysis Date = 06/26/22 Pct Recovery = 67% Analysis Date = 06/22/22 Pct Recovery = 67% Analysis Date = 06/22/22 Pct Recovery = 67% Analysis Date = 06/18/22 Pct Recovery = 68% Analysis Date = 06/18/22 Pct Recovery = 68% Analysis Date = 06/14/22 Pct Recovery = 68% Analysis Date = 06/14/22 Pct Recovery = 68% Analysis Date = 06/10/22 Pct Recovery = 68% Analysis Date = 06/10/22 Pct Recovery = 68% Analysis Date = 06/06/22 Pct Recovery = 68% Analysis Date = 06/06/22 Pct Recovery = 68% Analysis Date = 06/02/22 Pct Recovery = 69% Analysis Date = 06/02/22 Pct Recovery = 69% Analysis Date = 05/29/22 Pct Recovery = 69% Analysis Date = 05/29/22 Pct Recovery = 69% Analysis Date = 05/25/22 Pct Recovery = 69% Analysis Date = 05/25/22 Pct Recovery = 69% Analysis Date = 05/21/22 Pct Recovery = 70% Analysis Date = 05/21/22 Pct Recovery = 70% Analysis Date = 05/17/22 Pct Recovery = 70% Analysis Date = 05/17/22 Pct Recovery = 70% Analysis Date = 05/13/22 Pct Recovery = 70% Analysis Date = 05/13/22 Pct Recovery = 70% Analysis Date = 05/09/22 Pct Recovery = 71% Analysis Date = 05/09/22 Pct Recovery = 71% Analysis Date = 05/05/22 Pct Recovery = 71% Analysis Date = 05/05/22 Pct Recovery = 71% Analysis Date = 05/01/22 Pct Recovery = 71% Analysis Date = 05/01/22 Pct Recovery = 71% Analysis Date = 04/27/22 Pct Recovery = 71% Analysis Date = 04/27/22 Pct Recovery = 71% Analysis Date = 04/23/22 Pct Recovery = 72% Analysis Date = 04/23/22 Pct Recovery = 72% Analysis Date = 04/19/22 Pct Recovery = 72% Analysis Date = 04/19/22 Pct Recovery = 72% Analysis Date = 04/15/22 Pct Recovery = 72% Analysis Date = 04/15/22 Pct Recovery = 72% Analysis Date = 04/11/22 Pct Recovery = 73% Analysis Date = 04/11/22 Pct Recovery = 73% Analysis Date = 04/07/22 Pct Recovery = 73% Analysis Date = 04/07/22 Pct Recovery = 73% Analysis Date = 04/03/22 Pct Recovery = 73% Analysis Date = 04/03/22 Pct Recovery = 73% Analysis Date = 03/30/22 Pct Recovery = 74% Analysis Date = 03/30/22 Pct Recovery = 74% Analysis Date = 03/26/22 Pct Recovery = 74% Analysis Date = 03/26/22 Pct Recovery = 74% Analysis Date = 03/22/22 Pct Recovery = 74% Analysis Date = 03/22/22 Pct Recovery = 74% Analysis Date = 03/18/22 Pct Recovery = 75% Analysis Date = 03/18/22 Pct Recovery = 75% Analysis Date = 03/14/22 Pct Recovery = 75% Analysis Date = 03/14/22 Pct Recovery = 75% Analysis Date = 03/10/22 Pct Recovery = 75% Analysis Date = 03/10/22 Pct Recovery = 75% Analysis Date = 03/06/22 Pct Recovery = 75% Analysis Date = 03/06/22 Pct Recovery = 75% Analysis Date = 03/02/22 Pct Recovery = 76% Analysis Date = 03/02/22 Pct Recovery = 76% Analysis Date = 02/26/22 Pct Recovery = 76% Analysis Date = 02/26/22 Pct Recovery = 76% Analysis Date = 02/22/22 Pct Recovery = 76% Analysis Date = 02/22/22 Pct Recovery = 76% Analysis Date = 02/18/22 Pct Recovery = 77% Analysis Date = 02/18/22 Pct Recovery = 77% Analysis Date = 02/14/22 Pct Recovery = 77% Analysis Date = 02/14/22 Pct Recovery = 77% Analysis Date = 02/10/22 Pct Recovery = 77% Analysis Date = 02/10/22 Pct Recovery = 77% Analysis Date = 02/06/22 Pct Recovery = 78% Analysis Date = 02/06/22 Pct Recovery = 78% Analysis Date = 02/02/22 Pct Recovery = 78% Analysis Date = 02/02/22 Pct Recovery = 78% Analysis Date = 01/29/22 Pct Recovery = 78% Analysis Date = 01/29/22 Pct Recovery = 78% Analysis Date = 01/25/22 Pct Recovery = 79% Analysis Date = 01/25/22 Pct Recovery = 79% Analysis Date = 01/21/22 Pct Recovery = 79% Analysis Date = 01/21/22 Pct Recovery = 79% Analysis Date = 01/17/22 Pct Recovery = 79% Analysis Date = 01/17/22 Pct Recovery = 79% Analysis Date = 01/13/22 Pct Recovery = 79% Analysis Date = 01/13/22 Pct Recovery = 79% Analysis Date = 01/09/22 Pct Recovery = 80% Analysis Date = 01/09/22 Pct Recovery = 80% Analysis Date = 01/05/22 Pct Recovery = 80% Analysis Date = 01/05/22 Pct Recovery = 80% Analysis Date = 01/02/22 Pct Recovery = 80% Analysis Date = 01/02/22 Pct Recovery = 80% Analysis Date = 12/29/21 Pct Recovery = 81% Analysis Date = 12/29/21 Pct Recovery = 81% Analysis Date = 12/25/21 Pct Recovery = 81% Analysis Date = 12/25/21 Pct Recovery = 81% Analysis Date = 12/21/21 Pct Recovery = 81% Analysis Date = 12/21/21 Pct Recovery = 81% Analysis Date = 12/17/21 Pct Recovery = 82% Analysis Date = 12/17/21 Pct Recovery = 82% Analysis Date = 12/13/21 Pct Recovery = 82% Analysis Date = 12/13/21 Pct Recovery = 82% Analysis Date = 12/09/21 Pct Recovery = 82% Analysis Date = 12/09/21 Pct Recovery = 82% Analysis Date = 12/05/21 Pct Recovery = 82% Analysis Date = 12/05/21 Pct Recovery = 82% Analysis Date = 12/01/21 Pct Recovery = 83% Analysis Date = 12/01/21 Pct Recovery = 83% Analysis Date = 11/27/21 Pct Recovery = 83% Analysis Date = 11/27/21 Pct Recovery = 83% Analysis Date = 11/23/21 Pct Recovery = 83% Analysis Date = 11/23/21 Pct Recovery = 83% Analysis Date = 11/19/21 Pct Recovery = 84% Analysis Date = 11/19/21 Pct Recovery = 84% Analysis Date = 11/15/21 Pct Recovery = 84% Analysis Date = 11/15/21 Pct Recovery = 84% Analysis Date = 11/11/21 Pct Recovery = 84% Analysis Date = 11/11/21 Pct Recovery = 84% Analysis Date = 11/07/21 Pct Recovery = 85% Analysis Date = 11/07/21 Pct Recovery = 85% Analysis Date = 11/03/21 Pct Recovery = 85% Analysis Date = 11/03/21 Pct Recovery = 85% Analysis Date = 10/30/21 Pct Recovery = 85% Analysis Date = 10/30/21 Pct Recovery = 85% Analysis Date = 10/26/21 Pct Recovery = 85% Analysis Date = 10/26/21 Pct Recovery = 85% Analysis Date = 10/22/21 Pct Recovery = 85% Analysis Date = 10/22/21 Pct Recovery = 85% Analysis Date = 10/18/21 Pct Recovery = 85% Analysis Date = 10/18/21 Pct Recovery = 85% Analysis Date = 10/14/21 Pct Recovery = 85% Analysis Date = 10/14/21 Pct Recovery = 85% Analysis Date = 10/10/21 Pct Recovery = 85% Analysis Date = 10/10/21 Pct Recovery = 85% Analysis Date = 10/06/21 Pct Recovery = 85% Analysis Date = 10/06/21 Pct Recovery = 85% Analysis Date = 10/02/21 Pct Recovery = 85% Analysis Date = 10/02/21 Pct Recovery = 85% Analysis Date = 09/28/21 Pct Recovery = 86% Analysis Date = 09/28/21 Pct Recovery = 86% Analysis Date = 09/24/21 Pct Recovery = 86% Analysis Date = 09/24/21 Pct Recovery = 86% Analysis Date = 09/20/21 Pct Recovery = 86% Analysis Date = 09/20/21 Pct Recovery = 86% Analysis Date = 09/16/21 Pct Recovery = 86% Analysis Date = 09/16/21 Pct Recovery = 86% Analysis Date = 09/12/21 Pct Recovery = 86% Analysis Date = 09/12/21 Pct Recovery = 86% Analysis Date = 09/08/21 Pct Recovery = 86% Analysis Date = 09/08/21 Pct Recovery = 86% Analysis Date = 09/04/21 Pct Recovery = 86% Analysis Date = 09/04/21 Pct Recovery = 86% Analysis Date = 08/31/21 Pct Recovery = 86% Analysis Date = 08/31/21 Pct Recovery = 86% Analysis Date = 08/27/21 Pct Recovery = 86% Analysis Date = 08/27/21 Pct Recovery = 86% Analysis Date = 08/23/21 Pct Recovery = 86% Analysis Date = 08/23/21 Pct Recovery = 86% Analysis Date = 08/19/21 Pct Recovery = 86% Analysis Date = 08/19/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/11/21 Pct Recovery = 86% Analysis Date = 08/11/21 Pct Recovery = 86% Analysis Date = 08/07/21 Pct Recovery = 87% Analysis Date = 08/07/21 Pct Recovery = 87% Analysis Date = 08/03/21 Pct Recovery = 87% Analysis Date = 08/03/21 Pct Recovery = 87% Analysis Date = 07/30/21 Pct Recovery = 87% Analysis Date = 07/30/21 Pct Recovery = 87% Analysis Date = 07/26/21 Pct Recovery = 87% Analysis Date = 07/26/21 Pct Recovery = 87% Analysis Date = 07/22/21 Pct Recovery = 87% Analysis Date = 07/22/21 Pct Recovery = 87% Analysis Date = 07/18/21 Pct Recovery = 87% Analysis Date = 07/18/21 Pct Recovery = 87% Analysis Date = 07/14/21 Pct Recovery = 87% Analysis Date = 07/14/21 Pct Recovery = 87% Analysis Date = 07/10/21 Pct Recovery = 87% Analysis Date = 07/10/21 Pct Recovery = 87% Analysis Date = 07/06/21 Pct Recovery = 87% Analysis Date = 07/06/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/17/21 Pct Recovery = 88% Analysis Date = 06/17/21 Pct Recovery = 88% Analysis Date = 06/13/21 Pct Recovery = 88% Analysis Date = 06/13/21 Pct Recovery = 88% Analysis Date = 06/09/21 Pct Recovery = 88% Analysis Date = 06/09/21 Pct Recovery = 88% Analysis Date = 06/05/21 Pct Recovery = 88% Analysis Date = 06/05/21 Pct Recovery = 88% Analysis Date = 06/01/21 Pct Recovery = 88% Analysis Date = 06/01/21 Pct Recovery = 88% Analysis Date = 05/28/21 Pct Recovery = 88% Analysis Date = 05/28/21 Pct Recovery = 88% Analysis Date = 05/24/21 Pct Recovery = 88% Analysis Date = 05/24/21 Pct Recovery = 88% Analysis Date = 05/20/21 Pct Recovery = 88% Analysis Date = 05/20/21 Pct Recovery = 88% Analysis Date = 05/16/21 Pct Recovery = 88% Analysis Date = 05/16/21 Pct Recovery = 88% Analysis Date = 05/12/21 Pct Recovery = 88% Analysis Date = 05/12/21 Pct Recovery = 88% Analysis Date = 05/08/21 Pct Recovery = 88% Analysis Date = 05/08/21 Pct Recovery = 88% Analysis Date = 05/04/21 Pct Recovery = 88% Analysis Date = 05/04/21 Pct Recovery = 88% Analysis Date = 04/30/21 Pct Recovery = 88% Analysis Date = 04/30/21 Pct Recovery = 88% Analysis Date = 04/26/21 Pct Recovery = 88% Analysis Date = 04/26/21 Pct Recovery = 88% Analysis Date = 04/22/21 Pct Recovery = 89% Analysis Date = 04/22/21 Pct Recovery = 89% Analysis Date = 04/18/21 Pct Recovery = 89% Analysis Date = 04/18/21 Pct Recovery = 89% Analysis Date = 04/14/21 Pct Recovery = 89% Analysis Date = 04/14/21 Pct Recovery = 89% Analysis Date = 04/10/21 Pct Recovery = 89% Analysis Date = 04/10/21 Pct Recovery = 89% Analysis Date = 04/06/21 Pct Recovery = 89% Analysis Date = 04/06/21 Pct Recovery = 89% Analysis Date = 04/02/21 Pct Recovery = 89% Analysis Date = 04/02/21 Pct Recovery = 89% Analysis Date = 03/29/21 Pct Recovery = 89% Analysis Date = 03/29/21 Pct Recovery = 89% Analysis Date = 03/25/21 Pct Recovery = 89% Analysis Date = 03/25/21 Pct Recovery = 89% Analysis Date = 03/21/21 Pct Recovery = 89% Analysis Date = 03/21/21 Pct Recovery = 89% Analysis Date = 03/17/21 Pct Recovery = 89% Analysis Date = 03/17/21 Pct Recovery = 89% Analysis Date = 03/13/21 Pct Recovery = 89% Analysis Date = 03/13/21 Pct Recovery = 89% Analysis Date = 03/09/21 Pct Recovery = 89% Analysis Date = 03/09/21 Pct Recovery = 89% Analysis Date = 03/05/21 Pct Recovery = 89% Analysis Date = 03/05/21 Pct Recovery = 89% Analysis Date = 03/01/21 Pct Recovery = 90% Analysis Date = 03/01/21 Pct Recovery = 90% Analysis Date = 02/25/21 Pct Recovery = 90% Analysis Date = 02/25/21 Pct Recovery = 90% Analysis Date = 02/21/21 Pct Recovery = 90% Analysis Date = 02/21/21 Pct Recovery = 90% Analysis Date = 02/17/21 Pct Recovery = 90% Analysis Date = 02/17/21 Pct Recovery = 90% Analysis Date = 02/13/21 Pct Recovery = 90% Analysis Date = 02/13/21 Pct Recovery = 90% Analysis Date = 02/09/21 Pct Recovery = 90% Analysis Date = 02/09/21 Pct Recovery = 90% Analysis Date = 02/05/21 Pct Recovery = 90% Analysis Date = 02/05/21 Pct Recovery = 90% Analysis Date = 02/01/21 Pct Recovery = 90% Analysis Date = 02/01/21 Pct Recovery = 90% Analysis Date = 01/28/21 Pct Recovery = 90% Analysis Date = 01/28/21 Pct Recovery = 90% Analysis Date = 01/24/21 Pct Recovery = 90% Analysis Date = 01/24/21 Pct Recovery = 90% Analysis Date = 01/20/21 Pct Recovery = 90% Analysis Date = 01/20/21 Pct Recovery = 90% Analysis Date = 01/16/21 Pct Recovery = 90% Analysis Date = 01/16/21 Pct Recovery = 90% Analysis Date = 01/12/21 Pct Recovery = 90% Analysis Date = 01/12/21 Pct Recovery = 90% Analysis Date = 01/08/21 Pct Recovery = 90% Analysis Date = 01/08/21 Pct Recovery = 90% Analysis Date = 01/04/21 Pct Recovery = 90% Analysis Date = 01/04/21 Pct Recovery = 90% Analysis Date = 12/31/20 Pct Recovery = 90% Analysis Date = 12/31/20 Pct Recovery = 90% Analysis Date = 12/27/20 Pct Recovery = 90% Analysis Date = 12/27/20 Pct Recovery = 90% Analysis Date = 12/23/20 Pct Recovery = 90% Analysis Date = 12/23/20 Pct Recovery = 90% Analysis Date = 12/19/20 Pct Recovery = 89% Analysis Date = 12/19/20 Pct Recovery = 89% Analysis Date = 12/15/20 Pct Recovery = 89% Analysis Date = 12/15/20 Pct Recovery = 89% Analysis Date = 12/11/20 Pct Recovery = 90% Analysis Date = 12/11/20 Pct Recovery = 90% Analysis Date = 12/07/20 Pct Recovery = 90% Analysis Date = 12/07/20 Pct Recovery = 90% Analysis Date = 12/03/20 Pct Recovery = 90% Analysis Date = 12/03/20 Pct Recovery = 90% Analysis Date = 11/30/20 Pct Recovery = 90% Analysis Date = 11/30/20 Pct Recovery = 90% Analysis Date = 11/26/20 Pct Recovery = 90% Analysis Date = 11/26/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 90% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/10/20 Pct Recovery = 91% Analysis Date = 11/10/20 Pct Recovery = 91% Analysis Date = 11/06/20 Pct Recovery = 91% Analysis Date = 11/06/20 Pct Recovery = 91% Analysis Date = 11/02/20 Pct Recovery = 91% Analysis Date = 11/02/20 Pct Recovery = 91% Analysis Date = 10/29/20 Pct Recovery = 91% Analysis Date = 10/29/20 Pct Recovery = 91% Analysis Date = 10/25/20 Pct Recovery = 91% Analysis Date = 10/25/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 91% Analysis Date = 10/13/20 Pct Recovery = 91% Analysis Date = 10/13/20 Pct Recovery = 91% Analysis Date = 10/09/20 Pct Recovery = 91% Analysis Date = 10/09/20 Pct Recovery = 91% Analysis Date = 10/05/20 Pct Recovery = 91% Analysis Date = 10/05/20 Pct Recovery = 91% Analysis Date = 10/01/20 Pct Recovery = 91% Analysis Date = 10/01/20 Pct Recovery = 91% Analysis Date = 09/27/20 Pct Recovery = 91% Analysis Date = 09/27/20 Pct Recovery = 91% Analysis Date = 09/23/20 Pct Recovery = 91% Analysis Date = 09/23/20 Pct Recovery = 91% Analysis Date = 09/19/20 Pct Recovery = 91% Analysis Date = 09/19/20 Pct Recovery = 91% Analysis Date = 09/15/20 Pct Recovery = 91% Analysis Date = 09/15/20 Pct Recovery = 91% Analysis Date = 09/11/20 Pct Recovery = 91% Analysis Date = 09/11/20 Pct Recovery = 91% Analysis Date = 09/07/20 Pct Recovery = 91% Analysis Date = 09/07/20 Pct Recovery = 91% Analysis Date = 09/03/20 Pct Recovery = 91% Analysis Date = 09/03/20 Pct Recovery = 91% Analysis Date = 08/30/20 Pct Recovery = 91% Analysis Date = 08/30/20 Pct Recovery = 91% Analysis Date = 08/26/20 Pct Recovery = 92% Analysis Date = 08/26/20 Pct Recovery = 92% Analysis Date = 08/22/20 Pct Recovery = 92% Analysis Date = 08/22/20 Pct Recovery = 92% Analysis Date = 08/18/20 Pct Recovery = 92% Analysis Date = 08/18/20 Pct Recovery = 92% Analysis Date = 08/14/20 Pct Recovery = 93% Analysis Date = 08/14/20 Pct Recovery = 93% Analysis Date = 08/10/20 Pct Recovery = 93% Analysis Date = 08/10/20 Pct Recovery = 93% Analysis Date = 08/06/20 Pct Recovery = 94% Analysis Date = 08/06/20 Pct Recovery = 94% Analysis Date = 08/02/20 Pct Recovery = 94% Analysis Date = 08/02/20 Pct Recovery = 94% Analysis Date = 07/29/20 Pct Recovery = 94% Analysis Date = 07/29/20 Pct Recovery = 94% Analysis Date = 07/25/20 Pct Recovery = 95% Analysis Date = 07/25/20 Pct Recovery = 95% Analysis Date = 07/21/20 Pct Recovery = 95% Analysis Date = 07/21/20 Pct Recovery = 95% Analysis Date = 07/17/20 Pct Recovery = 96% Analysis Date = 07/17/20 Pct Recovery = 96% Analysis Date = 07/13/20 Pct Recovery = 96% Analysis Date = 07/13/20 Pct Recovery = 96% Analysis Date = 07/09/20 Pct Recovery = 97% Analysis Date = 07/09/20 Pct Recovery = 97% Analysis Date = 07/05/20 Pct Recovery = 97% Analysis Date = 07/05/20 Pct Recovery = 97% Analysis Date = 07/01/20 Pct Recovery = 98% Analysis Date = 07/01/20 Pct Recovery = 98% Analysis Date = 06/27/20 Pct Recovery = 98% Analysis Date = 06/27/20 Pct Recovery = 98% Analysis Date = 06/23/20 Pct Recovery = 99% Analysis Date = 06/23/20 Pct Recovery = 99% Analysis Date = 06/19/20 Pct Recovery = 99% Analysis Date = 06/19/20 Pct Recovery = 99% Analysis Date = 06/15/20 Pct Recovery = 100% Analysis Date = 06/15/20 Pct Recovery = 100% Analysis Date = 06/11/20 Pct Recovery = 100% Analysis Date = 06/11/20 Pct Recovery = 100% Analysis Date = 06/07/20 Pct Recovery = 101% Analysis Date = 06/07/20 Pct Recovery = 101% Analysis Date = 06/03/20 Pct Recovery = 101% Analysis Date = 06/03/20 Pct Recovery = 101% Analysis Date = 05/30/20 Pct Recovery = 102% Analysis Date = 05/30/20 Pct Recovery = 102% Analysis Date = 05/26/20 Pct Recovery = 102% Analysis Date = 05/26/20 Pct Recovery = 102% Analysis Date = 05/22/20 Pct Recovery = 103% Analysis Date = 05/22/20 Pct Recovery = 103% Analysis Date = 05/19/20 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBENDAZIM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 90% 11% 89% 11%
Total 31 90% 11% 89% 11%

Sample Statistics
CARBENDAZIM

Characteristic N % % Basis
Plotted 31 97% Spiked
Estimated Values 31 97% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 84 .  
False Positives 0 0% 0 out of 83

OBSP Determination:
CHLORIMURON-ETHYL
METHOD: 2447 , TESTIDCODE: 68872LCM60

Laboratory ID = 20201820155 Lab Value = 61.653 Expected Conc. = 111.6 Report level label = 8.8 Pct Recovery = 55% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 64.356 Expected Conc. = 111.6 Report level label = 8.8 Pct Recovery = 58% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20210760015 Lab Value = 84.855 Expected Conc. = 111.1 Report level label = 8.8 Pct Recovery = 76% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 111.322 Expected Conc. = 111.1 Report level label = 8.8 Pct Recovery = 100% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 121.366 Expected Conc. = 111.1 Report level label = 8.8 Pct Recovery = 109% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 99.705 Expected Conc. = 111.1 Report level label = 8.8 Pct Recovery = 90% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202390020 Lab Value = 44.103 Expected Conc. = 110.4 Report level label = 8.8 Pct Recovery = 40% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20222150193 Lab Value = 9.840 Expected Conc. = 89.6 Report level label = 8.8 Pct Recovery = 11% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220190116 Lab Value = 69.528 Expected Conc. = 88.64 Report level label = 8.8 Pct Recovery = 78% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 89.894 Expected Conc. = 88.64 Report level label = 8.8 Pct Recovery = 101% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20212990174 Lab Value = 31.012 Expected Conc. = 88.24 Report level label = 8.8 Pct Recovery = 35% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 37.533 Expected Conc. = 88 Report level label = 8.8 Pct Recovery = 43% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20202530029 Lab Value = 30.751 Expected Conc. = 55.8 Report level label = 8.8 Pct Recovery = 55% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 26.397 Expected Conc. = 55.8 Report level label = 8.8 Pct Recovery = 47% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 29.586 Expected Conc. = 55.8 Report level label = 8.8 Pct Recovery = 53% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20210480001 Lab Value = 53.222 Expected Conc. = 55.55 Report level label = 8.8 Pct Recovery = 96% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221730293 Lab Value = 31.695 Expected Conc. = 55.4 Report level label = 8.8 Pct Recovery = 57% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 44.280 Expected Conc. = 55.4 Report level label = 8.8 Pct Recovery = 80% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20201960104 Lab Value = 15.381 Expected Conc. = 55.2 Report level label = 8.8 Pct Recovery = 28% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20213340027 Lab Value = 18.425 Expected Conc. = 55.15 Report level label = 8.8 Pct Recovery = 33% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 68.513 Expected Conc. = 55.15 Report level label = 8.8 Pct Recovery = 124% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 26.445 Expected Conc. = 55.15 Report level label = 8.8 Pct Recovery = 48% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20210900005 Lab Value = 43.830 Expected Conc. = 44.44 Report level label = 8.8 Pct Recovery = 99% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202180001 Lab Value = 9.267 Expected Conc. = 22.32 Report level label = 8.8 Pct Recovery = 42% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 21.649 Expected Conc. = 22.32 Report level label = 8.8 Pct Recovery = 97% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20222630205 Lab Value = 13.117 Expected Conc. = 22.3 Report level label = 8.8 Pct Recovery = 59% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20222500483 Lab Value = 22.168 Expected Conc. = 22.16 Report level label = 8.8 Pct Recovery = 100% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 18.857 Expected Conc. = 22.16 Report level label = 8.8 Pct Recovery = 85% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20201610160 Lab Value = 7.065 Expected Conc. = 22.08 Report level label = 8.8 Pct Recovery = 32% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Analysis Date = 09/28/22 Pct Recovery = 55% Analysis Date = 09/24/22 Pct Recovery = 55% Analysis Date = 09/24/22 Pct Recovery = 55% Analysis Date = 09/20/22 Pct Recovery = 55% Analysis Date = 09/20/22 Pct Recovery = 55% Analysis Date = 09/16/22 Pct Recovery = 56% Analysis Date = 09/16/22 Pct Recovery = 56% Analysis Date = 09/11/22 Pct Recovery = 56% Analysis Date = 09/11/22 Pct Recovery = 56% Analysis Date = 09/07/22 Pct Recovery = 56% Analysis Date = 09/07/22 Pct Recovery = 56% Analysis Date = 09/03/22 Pct Recovery = 56% Analysis Date = 09/03/22 Pct Recovery = 56% Analysis Date = 08/29/22 Pct Recovery = 57% Analysis Date = 08/29/22 Pct Recovery = 57% Analysis Date = 08/25/22 Pct Recovery = 57% Analysis Date = 08/25/22 Pct Recovery = 57% Analysis Date = 08/21/22 Pct Recovery = 57% Analysis Date = 08/21/22 Pct Recovery = 57% Analysis Date = 08/16/22 Pct Recovery = 57% Analysis Date = 08/16/22 Pct Recovery = 57% Analysis Date = 08/12/22 Pct Recovery = 58% Analysis Date = 08/12/22 Pct Recovery = 58% Analysis Date = 08/08/22 Pct Recovery = 58% Analysis Date = 08/08/22 Pct Recovery = 58% Analysis Date = 08/03/22 Pct Recovery = 58% Analysis Date = 08/03/22 Pct Recovery = 58% Analysis Date = 07/30/22 Pct Recovery = 58% Analysis Date = 07/30/22 Pct Recovery = 58% Analysis Date = 07/26/22 Pct Recovery = 59% Analysis Date = 07/26/22 Pct Recovery = 59% Analysis Date = 07/21/22 Pct Recovery = 59% Analysis Date = 07/21/22 Pct Recovery = 59% Analysis Date = 07/17/22 Pct Recovery = 59% Analysis Date = 07/17/22 Pct Recovery = 59% Analysis Date = 07/13/22 Pct Recovery = 59% Analysis Date = 07/13/22 Pct Recovery = 59% Analysis Date = 07/09/22 Pct Recovery = 60% Analysis Date = 07/09/22 Pct Recovery = 60% Analysis Date = 07/04/22 Pct Recovery = 60% Analysis Date = 07/04/22 Pct Recovery = 60% Analysis Date = 06/30/22 Pct Recovery = 60% Analysis Date = 06/30/22 Pct Recovery = 60% Analysis Date = 06/26/22 Pct Recovery = 60% Analysis Date = 06/26/22 Pct Recovery = 60% Analysis Date = 06/21/22 Pct Recovery = 61% Analysis Date = 06/21/22 Pct Recovery = 61% Analysis Date = 06/17/22 Pct Recovery = 61% Analysis Date = 06/17/22 Pct Recovery = 61% Analysis Date = 06/13/22 Pct Recovery = 61% Analysis Date = 06/13/22 Pct Recovery = 61% Analysis Date = 06/08/22 Pct Recovery = 61% Analysis Date = 06/08/22 Pct Recovery = 61% Analysis Date = 06/04/22 Pct Recovery = 62% Analysis Date = 06/04/22 Pct Recovery = 62% Analysis Date = 05/31/22 Pct Recovery = 62% Analysis Date = 05/31/22 Pct Recovery = 62% Analysis Date = 05/26/22 Pct Recovery = 62% Analysis Date = 05/26/22 Pct Recovery = 62% Analysis Date = 05/22/22 Pct Recovery = 62% Analysis Date = 05/22/22 Pct Recovery = 62% Analysis Date = 05/18/22 Pct Recovery = 62% Analysis Date = 05/18/22 Pct Recovery = 62% Analysis Date = 05/13/22 Pct Recovery = 63% Analysis Date = 05/13/22 Pct Recovery = 63% Analysis Date = 05/09/22 Pct Recovery = 63% Analysis Date = 05/09/22 Pct Recovery = 63% Analysis Date = 05/05/22 Pct Recovery = 63% Analysis Date = 05/05/22 Pct Recovery = 63% Analysis Date = 04/30/22 Pct Recovery = 63% Analysis Date = 04/30/22 Pct Recovery = 63% Analysis Date = 04/26/22 Pct Recovery = 64% Analysis Date = 04/26/22 Pct Recovery = 64% Analysis Date = 04/22/22 Pct Recovery = 64% Analysis Date = 04/22/22 Pct Recovery = 64% Analysis Date = 04/18/22 Pct Recovery = 64% Analysis Date = 04/18/22 Pct Recovery = 64% Analysis Date = 04/13/22 Pct Recovery = 64% Analysis Date = 04/13/22 Pct Recovery = 64% Analysis Date = 04/09/22 Pct Recovery = 65% Analysis Date = 04/09/22 Pct Recovery = 65% Analysis Date = 04/05/22 Pct Recovery = 65% Analysis Date = 04/05/22 Pct Recovery = 65% Analysis Date = 03/31/22 Pct Recovery = 65% Analysis Date = 03/31/22 Pct Recovery = 65% Analysis Date = 03/27/22 Pct Recovery = 65% Analysis Date = 03/27/22 Pct Recovery = 65% Analysis Date = 03/23/22 Pct Recovery = 66% Analysis Date = 03/23/22 Pct Recovery = 66% Analysis Date = 03/18/22 Pct Recovery = 66% Analysis Date = 03/18/22 Pct Recovery = 66% Analysis Date = 03/14/22 Pct Recovery = 66% Analysis Date = 03/14/22 Pct Recovery = 66% Analysis Date = 03/10/22 Pct Recovery = 66% Analysis Date = 03/10/22 Pct Recovery = 66% Analysis Date = 03/05/22 Pct Recovery = 66% Analysis Date = 03/05/22 Pct Recovery = 66% Analysis Date = 03/01/22 Pct Recovery = 67% Analysis Date = 03/01/22 Pct Recovery = 67% Analysis Date = 02/25/22 Pct Recovery = 67% Analysis Date = 02/25/22 Pct Recovery = 67% Analysis Date = 02/20/22 Pct Recovery = 67% Analysis Date = 02/20/22 Pct Recovery = 67% Analysis Date = 02/16/22 Pct Recovery = 67% Analysis Date = 02/16/22 Pct Recovery = 67% Analysis Date = 02/12/22 Pct Recovery = 68% Analysis Date = 02/12/22 Pct Recovery = 68% Analysis Date = 02/07/22 Pct Recovery = 68% Analysis Date = 02/07/22 Pct Recovery = 68% Analysis Date = 02/03/22 Pct Recovery = 68% Analysis Date = 02/03/22 Pct Recovery = 68% Analysis Date = 01/30/22 Pct Recovery = 68% Analysis Date = 01/30/22 Pct Recovery = 68% Analysis Date = 01/26/22 Pct Recovery = 69% Analysis Date = 01/26/22 Pct Recovery = 69% Analysis Date = 01/21/22 Pct Recovery = 69% Analysis Date = 01/21/22 Pct Recovery = 69% Analysis Date = 01/17/22 Pct Recovery = 69% Analysis Date = 01/17/22 Pct Recovery = 69% Analysis Date = 01/13/22 Pct Recovery = 70% Analysis Date = 01/13/22 Pct Recovery = 70% Analysis Date = 01/08/22 Pct Recovery = 70% Analysis Date = 01/08/22 Pct Recovery = 70% Analysis Date = 01/04/22 Pct Recovery = 70% Analysis Date = 01/04/22 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 71% Analysis Date = 12/31/21 Pct Recovery = 71% Analysis Date = 12/26/21 Pct Recovery = 71% Analysis Date = 12/26/21 Pct Recovery = 71% Analysis Date = 12/22/21 Pct Recovery = 71% Analysis Date = 12/22/21 Pct Recovery = 71% Analysis Date = 12/18/21 Pct Recovery = 72% Analysis Date = 12/18/21 Pct Recovery = 72% Analysis Date = 12/13/21 Pct Recovery = 72% Analysis Date = 12/13/21 Pct Recovery = 72% Analysis Date = 12/09/21 Pct Recovery = 72% Analysis Date = 12/09/21 Pct Recovery = 72% Analysis Date = 12/05/21 Pct Recovery = 72% Analysis Date = 12/05/21 Pct Recovery = 72% Analysis Date = 11/30/21 Pct Recovery = 73% Analysis Date = 11/30/21 Pct Recovery = 73% Analysis Date = 11/26/21 Pct Recovery = 73% Analysis Date = 11/26/21 Pct Recovery = 73% Analysis Date = 11/22/21 Pct Recovery = 73% Analysis Date = 11/22/21 Pct Recovery = 73% Analysis Date = 11/18/21 Pct Recovery = 73% Analysis Date = 11/18/21 Pct Recovery = 73% Analysis Date = 11/13/21 Pct Recovery = 73% Analysis Date = 11/13/21 Pct Recovery = 73% Analysis Date = 11/09/21 Pct Recovery = 74% Analysis Date = 11/09/21 Pct Recovery = 74% Analysis Date = 11/05/21 Pct Recovery = 74% Analysis Date = 11/05/21 Pct Recovery = 74% Analysis Date = 10/31/21 Pct Recovery = 74% Analysis Date = 10/31/21 Pct Recovery = 74% Analysis Date = 10/27/21 Pct Recovery = 74% Analysis Date = 10/27/21 Pct Recovery = 74% Analysis Date = 10/23/21 Pct Recovery = 75% Analysis Date = 10/23/21 Pct Recovery = 75% Analysis Date = 10/18/21 Pct Recovery = 75% Analysis Date = 10/18/21 Pct Recovery = 75% Analysis Date = 10/14/21 Pct Recovery = 75% Analysis Date = 10/14/21 Pct Recovery = 75% Analysis Date = 10/10/21 Pct Recovery = 76% Analysis Date = 10/10/21 Pct Recovery = 76% Analysis Date = 10/05/21 Pct Recovery = 76% Analysis Date = 10/05/21 Pct Recovery = 76% Analysis Date = 10/01/21 Pct Recovery = 77% Analysis Date = 10/01/21 Pct Recovery = 77% Analysis Date = 09/27/21 Pct Recovery = 77% Analysis Date = 09/27/21 Pct Recovery = 77% Analysis Date = 09/22/21 Pct Recovery = 77% Analysis Date = 09/22/21 Pct Recovery = 77% Analysis Date = 09/18/21 Pct Recovery = 78% Analysis Date = 09/18/21 Pct Recovery = 78% Analysis Date = 09/14/21 Pct Recovery = 78% Analysis Date = 09/14/21 Pct Recovery = 78% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 80% Analysis Date = 08/28/21 Pct Recovery = 80% Analysis Date = 08/23/21 Pct Recovery = 80% Analysis Date = 08/23/21 Pct Recovery = 80% Analysis Date = 08/19/21 Pct Recovery = 80% Analysis Date = 08/19/21 Pct Recovery = 80% Analysis Date = 08/15/21 Pct Recovery = 81% Analysis Date = 08/15/21 Pct Recovery = 81% Analysis Date = 08/10/21 Pct Recovery = 81% Analysis Date = 08/10/21 Pct Recovery = 81% Analysis Date = 08/06/21 Pct Recovery = 82% Analysis Date = 08/06/21 Pct Recovery = 82% Analysis Date = 08/02/21 Pct Recovery = 82% Analysis Date = 08/02/21 Pct Recovery = 82% Analysis Date = 07/28/21 Pct Recovery = 82% Analysis Date = 07/28/21 Pct Recovery = 82% Analysis Date = 07/24/21 Pct Recovery = 83% Analysis Date = 07/24/21 Pct Recovery = 83% Analysis Date = 07/20/21 Pct Recovery = 83% Analysis Date = 07/20/21 Pct Recovery = 83% Analysis Date = 07/15/21 Pct Recovery = 84% Analysis Date = 07/15/21 Pct Recovery = 84% Analysis Date = 07/11/21 Pct Recovery = 84% Analysis Date = 07/11/21 Pct Recovery = 84% Analysis Date = 07/07/21 Pct Recovery = 84% Analysis Date = 07/07/21 Pct Recovery = 84% Analysis Date = 07/02/21 Pct Recovery = 85% Analysis Date = 07/02/21 Pct Recovery = 85% Analysis Date = 06/28/21 Pct Recovery = 85% Analysis Date = 06/28/21 Pct Recovery = 85% Analysis Date = 06/24/21 Pct Recovery = 86% Analysis Date = 06/24/21 Pct Recovery = 86% Analysis Date = 06/19/21 Pct Recovery = 86% Analysis Date = 06/19/21 Pct Recovery = 86% Analysis Date = 06/15/21 Pct Recovery = 86% Analysis Date = 06/15/21 Pct Recovery = 86% Analysis Date = 06/11/21 Pct Recovery = 87% Analysis Date = 06/11/21 Pct Recovery = 87% Analysis Date = 06/07/21 Pct Recovery = 87% Analysis Date = 06/07/21 Pct Recovery = 87% Analysis Date = 06/02/21 Pct Recovery = 88% Analysis Date = 06/02/21 Pct Recovery = 88% Analysis Date = 05/29/21 Pct Recovery = 88% Analysis Date = 05/29/21 Pct Recovery = 88% Analysis Date = 05/25/21 Pct Recovery = 88% Analysis Date = 05/25/21 Pct Recovery = 88% Analysis Date = 05/20/21 Pct Recovery = 89% Analysis Date = 05/20/21 Pct Recovery = 89% Analysis Date = 05/16/21 Pct Recovery = 89% Analysis Date = 05/16/21 Pct Recovery = 89% Analysis Date = 05/12/21 Pct Recovery = 89% Analysis Date = 05/12/21 Pct Recovery = 89% Analysis Date = 05/07/21 Pct Recovery = 90% Analysis Date = 05/07/21 Pct Recovery = 90% Analysis Date = 05/03/21 Pct Recovery = 90% Analysis Date = 05/03/21 Pct Recovery = 90% Analysis Date = 04/29/21 Pct Recovery = 91% Analysis Date = 04/29/21 Pct Recovery = 91% Analysis Date = 04/24/21 Pct Recovery = 91% Analysis Date = 04/24/21 Pct Recovery = 91% Analysis Date = 04/20/21 Pct Recovery = 91% Analysis Date = 04/20/21 Pct Recovery = 91% Analysis Date = 04/16/21 Pct Recovery = 92% Analysis Date = 04/16/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 93% Analysis Date = 04/07/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/25/21 Pct Recovery = 94% Analysis Date = 03/25/21 Pct Recovery = 94% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/12/21 Pct Recovery = 92% Analysis Date = 03/12/21 Pct Recovery = 92% Analysis Date = 03/08/21 Pct Recovery = 92% Analysis Date = 03/08/21 Pct Recovery = 92% Analysis Date = 03/04/21 Pct Recovery = 91% Analysis Date = 03/04/21 Pct Recovery = 91% Analysis Date = 02/27/21 Pct Recovery = 91% Analysis Date = 02/27/21 Pct Recovery = 91% Analysis Date = 02/23/21 Pct Recovery = 90% Analysis Date = 02/23/21 Pct Recovery = 90% Analysis Date = 02/19/21 Pct Recovery = 90% Analysis Date = 02/19/21 Pct Recovery = 90% Analysis Date = 02/14/21 Pct Recovery = 89% Analysis Date = 02/14/21 Pct Recovery = 89% Analysis Date = 02/10/21 Pct Recovery = 89% Analysis Date = 02/10/21 Pct Recovery = 89% Analysis Date = 02/06/21 Pct Recovery = 88% Analysis Date = 02/06/21 Pct Recovery = 88% Analysis Date = 02/01/21 Pct Recovery = 88% Analysis Date = 02/01/21 Pct Recovery = 88% Analysis Date = 01/28/21 Pct Recovery = 87% Analysis Date = 01/28/21 Pct Recovery = 87% Analysis Date = 01/24/21 Pct Recovery = 87% Analysis Date = 01/24/21 Pct Recovery = 87% Analysis Date = 01/19/21 Pct Recovery = 86% Analysis Date = 01/19/21 Pct Recovery = 86% Analysis Date = 01/15/21 Pct Recovery = 85% Analysis Date = 01/15/21 Pct Recovery = 85% Analysis Date = 01/11/21 Pct Recovery = 84% Analysis Date = 01/11/21 Pct Recovery = 84% Analysis Date = 01/07/21 Pct Recovery = 83% Analysis Date = 01/07/21 Pct Recovery = 83% Analysis Date = 01/02/21 Pct Recovery = 83% Analysis Date = 01/02/21 Pct Recovery = 83% Analysis Date = 12/29/20 Pct Recovery = 82% Analysis Date = 12/29/20 Pct Recovery = 82% Analysis Date = 12/25/20 Pct Recovery = 81% Analysis Date = 12/25/20 Pct Recovery = 81% Analysis Date = 12/20/20 Pct Recovery = 80% Analysis Date = 12/20/20 Pct Recovery = 80% Analysis Date = 12/16/20 Pct Recovery = 79% Analysis Date = 12/16/20 Pct Recovery = 79% Analysis Date = 12/12/20 Pct Recovery = 79% Analysis Date = 12/12/20 Pct Recovery = 79% Analysis Date = 12/07/20 Pct Recovery = 78% Analysis Date = 12/07/20 Pct Recovery = 78% Analysis Date = 12/03/20 Pct Recovery = 77% Analysis Date = 12/03/20 Pct Recovery = 77% Analysis Date = 11/29/20 Pct Recovery = 76% Analysis Date = 11/29/20 Pct Recovery = 76% Analysis Date = 11/24/20 Pct Recovery = 76% Analysis Date = 11/24/20 Pct Recovery = 76% Analysis Date = 11/20/20 Pct Recovery = 75% Analysis Date = 11/20/20 Pct Recovery = 75% Analysis Date = 11/16/20 Pct Recovery = 74% Analysis Date = 11/16/20 Pct Recovery = 74% Analysis Date = 11/11/20 Pct Recovery = 73% Analysis Date = 11/11/20 Pct Recovery = 73% Analysis Date = 11/07/20 Pct Recovery = 72% Analysis Date = 11/07/20 Pct Recovery = 72% Analysis Date = 11/03/20 Pct Recovery = 72% Analysis Date = 11/03/20 Pct Recovery = 72% Analysis Date = 10/29/20 Pct Recovery = 71% Analysis Date = 10/29/20 Pct Recovery = 71% Analysis Date = 10/25/20 Pct Recovery = 70% Analysis Date = 10/25/20 Pct Recovery = 70% Analysis Date = 10/21/20 Pct Recovery = 69% Analysis Date = 10/21/20 Pct Recovery = 69% Analysis Date = 10/17/20 Pct Recovery = 69% Analysis Date = 10/17/20 Pct Recovery = 69% Analysis Date = 10/12/20 Pct Recovery = 68% Analysis Date = 10/12/20 Pct Recovery = 68% Analysis Date = 10/08/20 Pct Recovery = 67% Analysis Date = 10/08/20 Pct Recovery = 67% Analysis Date = 10/04/20 Pct Recovery = 66% Analysis Date = 10/04/20 Pct Recovery = 66% Analysis Date = 09/29/20 Pct Recovery = 65% Analysis Date = 09/29/20 Pct Recovery = 65% Analysis Date = 09/25/20 Pct Recovery = 65% Analysis Date = 09/25/20 Pct Recovery = 65% Analysis Date = 09/21/20 Pct Recovery = 64% Analysis Date = 09/21/20 Pct Recovery = 64% Analysis Date = 09/16/20 Pct Recovery = 63% Analysis Date = 09/16/20 Pct Recovery = 63% Analysis Date = 09/12/20 Pct Recovery = 62% Analysis Date = 09/12/20 Pct Recovery = 62% Analysis Date = 09/08/20 Pct Recovery = 62% Analysis Date = 09/08/20 Pct Recovery = 62% Analysis Date = 09/03/20 Pct Recovery = 61% Analysis Date = 09/03/20 Pct Recovery = 61% Analysis Date = 08/30/20 Pct Recovery = 60% Analysis Date = 08/30/20 Pct Recovery = 60% Analysis Date = 08/26/20 Pct Recovery = 59% Analysis Date = 08/26/20 Pct Recovery = 59% Analysis Date = 08/21/20 Pct Recovery = 59% Analysis Date = 08/21/20 Pct Recovery = 59% Analysis Date = 08/17/20 Pct Recovery = 58% Analysis Date = 08/17/20 Pct Recovery = 58% Analysis Date = 08/13/20 Pct Recovery = 57% Analysis Date = 08/13/20 Pct Recovery = 57% Analysis Date = 08/08/20 Pct Recovery = 56% Analysis Date = 08/08/20 Pct Recovery = 56% Analysis Date = 08/04/20 Pct Recovery = 56% Analysis Date = 08/04/20 Pct Recovery = 56% Analysis Date = 07/31/20 Pct Recovery = 55% Analysis Date = 07/31/20 Pct Recovery = 55% Analysis Date = 07/27/20 Pct Recovery = 54% Analysis Date = 07/27/20 Pct Recovery = 54% Analysis Date = 07/22/20 Pct Recovery = 54% Analysis Date = 07/22/20 Pct Recovery = 54% Analysis Date = 07/18/20 Pct Recovery = 53% Analysis Date = 07/18/20 Pct Recovery = 53% Analysis Date = 07/14/20 Pct Recovery = 52% Analysis Date = 07/14/20 Pct Recovery = 52% Analysis Date = 07/09/20 Pct Recovery = 51% Analysis Date = 07/09/20 Pct Recovery = 51% Analysis Date = 07/05/20 Pct Recovery = 51% Analysis Date = 07/05/20 Pct Recovery = 51% Analysis Date = 07/01/20 Pct Recovery = 50% Analysis Date = 07/01/20 Pct Recovery = 50% Analysis Date = 06/26/20 Pct Recovery = 49% Analysis Date = 06/26/20 Pct Recovery = 49% Analysis Date = 06/22/20 Pct Recovery = 48% Analysis Date = 06/22/20 Pct Recovery = 48% Analysis Date = 06/18/20 Pct Recovery = 48% Analysis Date = 06/18/20 Pct Recovery = 48% Analysis Date = 06/13/20 Pct Recovery = 47% Analysis Date = 06/13/20 Pct Recovery = 47% Analysis Date = 06/09/20 Pct Recovery = 46% Analysis Date = 06/09/20 Pct Recovery = 46% Analysis Date = 06/05/20 Pct Recovery = 45% Analysis Date = 06/05/20 Pct Recovery = 45% Analysis Date = 05/31/20 Pct Recovery = 45% Analysis Date = 05/31/20 Pct Recovery = 45% Analysis Date = 05/27/20 Pct Recovery = 44% Analysis Date = 05/27/20 Pct Recovery = 44% Analysis Date = 05/23/20 Pct Recovery = 43% Analysis Date = 05/23/20 Pct Recovery = 43% Analysis Date = 05/19/20 Pct Recovery = 43% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORIMURON-ETHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 29 67% 29% 58% 39%
Total 29 67% 29% 58% 39%

Sample Statistics
CHLORIMURON-ETHYL

Characteristic N % % Basis
Plotted 29 91% Spiked
Estimated Values 5 16% Spiked
Deleted Values 7 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 3 9% 3 out of 32
Not Spiked 71 .  
False Positives 0 0% 0 out of 66

OBSP Determination:
CHLORPYRIFOS
METHOD: 2447 , TESTIDCODE: 65072LCM60

Laboratory ID = 20201820155 Lab Value = 37.027 Expected Conc. = 37.8 Report level label = 3 Pct Recovery = 98% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 42.266 Expected Conc. = 37.8 Report level label = 3 Pct Recovery = 112% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 45.280 Expected Conc. = 37.7 Report level label = 3 Pct Recovery = 120% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203230021 Lab Value = 23.844 Expected Conc. = 37.35 Report level label = 3 Pct Recovery = 64% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 20.288 Expected Conc. = 37.35 Report level label = 3 Pct Recovery = 54% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 33.876 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 91% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 41.755 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 113% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220190116 Lab Value = 17.421 Expected Conc. = 30.56 Report level label = 3 Pct Recovery = 57% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 22.058 Expected Conc. = 30.56 Report level label = 3 Pct Recovery = 72% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 15.764 Expected Conc. = 30 Report level label = 3 Pct Recovery = 53% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 22.709 Expected Conc. = 30 Report level label = 3 Pct Recovery = 76% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20212990174 Lab Value = 21.305 Expected Conc. = 29.92 Report level label = 3 Pct Recovery = 71% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 11.158 Expected Conc. = 19.1 Report level label = 3 Pct Recovery = 58% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 10.543 Expected Conc. = 19.1 Report level label = 3 Pct Recovery = 55% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202530029 Lab Value = 17.700 Expected Conc. = 18.9 Report level label = 3 Pct Recovery = 94% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 16.499 Expected Conc. = 18.9 Report level label = 3 Pct Recovery = 87% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 16.445 Expected Conc. = 18.9 Report level label = 3 Pct Recovery = 87% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201960104 Lab Value = 20.991 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 111% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20220810133 Lab Value = 13.899 Expected Conc. = 18.75 Report level label = 3 Pct Recovery = 74% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20213340027 Lab Value = 11.841 Expected Conc. = 18.7 Report level label = 3 Pct Recovery = 63% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 35.447 Expected Conc. = 18.7 Report level label = 3 Pct Recovery = 190% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 13.059 Expected Conc. = 18.7 Report level label = 3 Pct Recovery = 70% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20203230018 Lab Value = 13.078 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 71% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 18.297 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 99% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 21.715 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 117% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222500483 Lab Value = 6.903 Expected Conc. = 7.64 Report level label = 3 Pct Recovery = 90% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 6.493 Expected Conc. = 7.64 Report level label = 3 Pct Recovery = 85% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20201750122 Lab Value = 6.998 Expected Conc. = 7.56 Report level label = 3 Pct Recovery = 93% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201610160 Lab Value = 7.117 Expected Conc. = 7.54 Report level label = 3 Pct Recovery = 94% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20222630205 Lab Value = 4.753 Expected Conc. = 7.5 Report level label = 3 Pct Recovery = 63% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210830019 Lab Value = 10.612 Expected Conc. = 7.47 Report level label = 3 Pct Recovery = 142% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 5.407 Expected Conc. = 7.47 Report level label = 3 Pct Recovery = 72% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 5.374 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 72% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 5.932 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 80% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 7.797 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 105% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 9.089 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 122% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 7.982 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 108% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 7.094 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 96% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 09/28/22 Pct Recovery = 62% Analysis Date = 09/24/22 Pct Recovery = 63% Analysis Date = 09/24/22 Pct Recovery = 63% Analysis Date = 09/20/22 Pct Recovery = 63% Analysis Date = 09/20/22 Pct Recovery = 63% Analysis Date = 09/16/22 Pct Recovery = 63% Analysis Date = 09/16/22 Pct Recovery = 63% Analysis Date = 09/11/22 Pct Recovery = 64% Analysis Date = 09/11/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 08/29/22 Pct Recovery = 65% Analysis Date = 08/29/22 Pct Recovery = 65% Analysis Date = 08/25/22 Pct Recovery = 65% Analysis Date = 08/25/22 Pct Recovery = 65% Analysis Date = 08/21/22 Pct Recovery = 65% Analysis Date = 08/21/22 Pct Recovery = 65% Analysis Date = 08/16/22 Pct Recovery = 65% Analysis Date = 08/16/22 Pct Recovery = 65% Analysis Date = 08/12/22 Pct Recovery = 66% Analysis Date = 08/12/22 Pct Recovery = 66% Analysis Date = 08/08/22 Pct Recovery = 66% Analysis Date = 08/08/22 Pct Recovery = 66% Analysis Date = 08/03/22 Pct Recovery = 66% Analysis Date = 08/03/22 Pct Recovery = 66% Analysis Date = 07/30/22 Pct Recovery = 67% Analysis Date = 07/30/22 Pct Recovery = 67% Analysis Date = 07/26/22 Pct Recovery = 67% Analysis Date = 07/26/22 Pct Recovery = 67% Analysis Date = 07/21/22 Pct Recovery = 67% Analysis Date = 07/21/22 Pct Recovery = 67% Analysis Date = 07/17/22 Pct Recovery = 67% Analysis Date = 07/17/22 Pct Recovery = 67% Analysis Date = 07/13/22 Pct Recovery = 68% Analysis Date = 07/13/22 Pct Recovery = 68% Analysis Date = 07/09/22 Pct Recovery = 68% Analysis Date = 07/09/22 Pct Recovery = 68% Analysis Date = 07/04/22 Pct Recovery = 68% Analysis Date = 07/04/22 Pct Recovery = 68% Analysis Date = 06/30/22 Pct Recovery = 69% Analysis Date = 06/30/22 Pct Recovery = 69% Analysis Date = 06/26/22 Pct Recovery = 69% Analysis Date = 06/26/22 Pct Recovery = 69% Analysis Date = 06/21/22 Pct Recovery = 69% Analysis Date = 06/21/22 Pct Recovery = 69% Analysis Date = 06/17/22 Pct Recovery = 69% Analysis Date = 06/17/22 Pct Recovery = 69% Analysis Date = 06/13/22 Pct Recovery = 70% Analysis Date = 06/13/22 Pct Recovery = 70% Analysis Date = 06/08/22 Pct Recovery = 70% Analysis Date = 06/08/22 Pct Recovery = 70% Analysis Date = 06/04/22 Pct Recovery = 70% Analysis Date = 06/04/22 Pct Recovery = 70% Analysis Date = 05/31/22 Pct Recovery = 71% Analysis Date = 05/31/22 Pct Recovery = 71% Analysis Date = 05/26/22 Pct Recovery = 71% Analysis Date = 05/26/22 Pct Recovery = 71% Analysis Date = 05/22/22 Pct Recovery = 71% Analysis Date = 05/22/22 Pct Recovery = 71% Analysis Date = 05/18/22 Pct Recovery = 72% Analysis Date = 05/18/22 Pct Recovery = 72% Analysis Date = 05/13/22 Pct Recovery = 72% Analysis Date = 05/13/22 Pct Recovery = 72% Analysis Date = 05/09/22 Pct Recovery = 72% Analysis Date = 05/09/22 Pct Recovery = 72% Analysis Date = 05/05/22 Pct Recovery = 72% Analysis Date = 05/05/22 Pct Recovery = 72% Analysis Date = 04/30/22 Pct Recovery = 73% Analysis Date = 04/30/22 Pct Recovery = 73% Analysis Date = 04/26/22 Pct Recovery = 73% Analysis Date = 04/26/22 Pct Recovery = 73% Analysis Date = 04/22/22 Pct Recovery = 73% Analysis Date = 04/22/22 Pct Recovery = 73% Analysis Date = 04/18/22 Pct Recovery = 74% Analysis Date = 04/18/22 Pct Recovery = 74% Analysis Date = 04/13/22 Pct Recovery = 74% Analysis Date = 04/13/22 Pct Recovery = 74% Analysis Date = 04/09/22 Pct Recovery = 74% Analysis Date = 04/09/22 Pct Recovery = 74% Analysis Date = 04/05/22 Pct Recovery = 74% Analysis Date = 04/05/22 Pct Recovery = 74% Analysis Date = 03/31/22 Pct Recovery = 75% Analysis Date = 03/31/22 Pct Recovery = 75% Analysis Date = 03/27/22 Pct Recovery = 75% Analysis Date = 03/27/22 Pct Recovery = 75% Analysis Date = 03/23/22 Pct Recovery = 75% Analysis Date = 03/23/22 Pct Recovery = 75% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/05/22 Pct Recovery = 77% Analysis Date = 03/05/22 Pct Recovery = 77% Analysis Date = 03/01/22 Pct Recovery = 77% Analysis Date = 03/01/22 Pct Recovery = 77% Analysis Date = 02/25/22 Pct Recovery = 77% Analysis Date = 02/25/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 78% Analysis Date = 02/16/22 Pct Recovery = 78% Analysis Date = 02/12/22 Pct Recovery = 78% Analysis Date = 02/12/22 Pct Recovery = 78% Analysis Date = 02/07/22 Pct Recovery = 78% Analysis Date = 02/07/22 Pct Recovery = 78% Analysis Date = 02/03/22 Pct Recovery = 79% Analysis Date = 02/03/22 Pct Recovery = 79% Analysis Date = 01/30/22 Pct Recovery = 79% Analysis Date = 01/30/22 Pct Recovery = 79% Analysis Date = 01/26/22 Pct Recovery = 79% Analysis Date = 01/26/22 Pct Recovery = 79% Analysis Date = 01/21/22 Pct Recovery = 80% Analysis Date = 01/21/22 Pct Recovery = 80% Analysis Date = 01/17/22 Pct Recovery = 80% Analysis Date = 01/17/22 Pct Recovery = 80% Analysis Date = 01/13/22 Pct Recovery = 80% Analysis Date = 01/13/22 Pct Recovery = 80% Analysis Date = 01/08/22 Pct Recovery = 81% Analysis Date = 01/08/22 Pct Recovery = 81% Analysis Date = 01/04/22 Pct Recovery = 81% Analysis Date = 01/04/22 Pct Recovery = 81% Analysis Date = 12/31/21 Pct Recovery = 81% Analysis Date = 12/31/21 Pct Recovery = 81% Analysis Date = 12/26/21 Pct Recovery = 81% Analysis Date = 12/26/21 Pct Recovery = 81% Analysis Date = 12/22/21 Pct Recovery = 82% Analysis Date = 12/22/21 Pct Recovery = 82% Analysis Date = 12/18/21 Pct Recovery = 82% Analysis Date = 12/18/21 Pct Recovery = 82% Analysis Date = 12/13/21 Pct Recovery = 82% Analysis Date = 12/13/21 Pct Recovery = 82% Analysis Date = 12/09/21 Pct Recovery = 83% Analysis Date = 12/09/21 Pct Recovery = 83% Analysis Date = 12/05/21 Pct Recovery = 83% Analysis Date = 12/05/21 Pct Recovery = 83% Analysis Date = 11/30/21 Pct Recovery = 84% Analysis Date = 11/30/21 Pct Recovery = 84% Analysis Date = 11/26/21 Pct Recovery = 84% Analysis Date = 11/26/21 Pct Recovery = 84% Analysis Date = 11/22/21 Pct Recovery = 84% Analysis Date = 11/22/21 Pct Recovery = 84% Analysis Date = 11/18/21 Pct Recovery = 84% Analysis Date = 11/18/21 Pct Recovery = 84% Analysis Date = 11/13/21 Pct Recovery = 84% Analysis Date = 11/13/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 10/31/21 Pct Recovery = 84% Analysis Date = 10/31/21 Pct Recovery = 84% Analysis Date = 10/27/21 Pct Recovery = 84% Analysis Date = 10/27/21 Pct Recovery = 84% Analysis Date = 10/23/21 Pct Recovery = 84% Analysis Date = 10/23/21 Pct Recovery = 84% Analysis Date = 10/18/21 Pct Recovery = 84% Analysis Date = 10/18/21 Pct Recovery = 84% Analysis Date = 10/14/21 Pct Recovery = 84% Analysis Date = 10/14/21 Pct Recovery = 84% Analysis Date = 10/10/21 Pct Recovery = 84% Analysis Date = 10/10/21 Pct Recovery = 84% Analysis Date = 10/05/21 Pct Recovery = 84% Analysis Date = 10/05/21 Pct Recovery = 84% Analysis Date = 10/01/21 Pct Recovery = 84% Analysis Date = 10/01/21 Pct Recovery = 84% Analysis Date = 09/27/21 Pct Recovery = 84% Analysis Date = 09/27/21 Pct Recovery = 84% Analysis Date = 09/22/21 Pct Recovery = 84% Analysis Date = 09/22/21 Pct Recovery = 84% Analysis Date = 09/18/21 Pct Recovery = 84% Analysis Date = 09/18/21 Pct Recovery = 84% Analysis Date = 09/14/21 Pct Recovery = 84% Analysis Date = 09/14/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/05/21 Pct Recovery = 84% Analysis Date = 09/05/21 Pct Recovery = 84% Analysis Date = 09/01/21 Pct Recovery = 84% Analysis Date = 09/01/21 Pct Recovery = 84% Analysis Date = 08/28/21 Pct Recovery = 84% Analysis Date = 08/28/21 Pct Recovery = 84% Analysis Date = 08/23/21 Pct Recovery = 84% Analysis Date = 08/23/21 Pct Recovery = 84% Analysis Date = 08/19/21 Pct Recovery = 84% Analysis Date = 08/19/21 Pct Recovery = 84% Analysis Date = 08/15/21 Pct Recovery = 84% Analysis Date = 08/15/21 Pct Recovery = 84% Analysis Date = 08/10/21 Pct Recovery = 84% Analysis Date = 08/10/21 Pct Recovery = 84% Analysis Date = 08/06/21 Pct Recovery = 84% Analysis Date = 08/06/21 Pct Recovery = 84% Analysis Date = 08/02/21 Pct Recovery = 84% Analysis Date = 08/02/21 Pct Recovery = 84% Analysis Date = 07/28/21 Pct Recovery = 84% Analysis Date = 07/28/21 Pct Recovery = 84% Analysis Date = 07/24/21 Pct Recovery = 84% Analysis Date = 07/24/21 Pct Recovery = 84% Analysis Date = 07/20/21 Pct Recovery = 83% Analysis Date = 07/20/21 Pct Recovery = 83% Analysis Date = 07/15/21 Pct Recovery = 83% Analysis Date = 07/15/21 Pct Recovery = 83% Analysis Date = 07/11/21 Pct Recovery = 83% Analysis Date = 07/11/21 Pct Recovery = 83% Analysis Date = 07/07/21 Pct Recovery = 83% Analysis Date = 07/07/21 Pct Recovery = 83% Analysis Date = 07/02/21 Pct Recovery = 83% Analysis Date = 07/02/21 Pct Recovery = 83% Analysis Date = 06/28/21 Pct Recovery = 83% Analysis Date = 06/28/21 Pct Recovery = 83% Analysis Date = 06/24/21 Pct Recovery = 83% Analysis Date = 06/24/21 Pct Recovery = 83% Analysis Date = 06/19/21 Pct Recovery = 83% Analysis Date = 06/19/21 Pct Recovery = 83% Analysis Date = 06/15/21 Pct Recovery = 83% Analysis Date = 06/15/21 Pct Recovery = 83% Analysis Date = 06/11/21 Pct Recovery = 83% Analysis Date = 06/11/21 Pct Recovery = 83% Analysis Date = 06/07/21 Pct Recovery = 83% Analysis Date = 06/07/21 Pct Recovery = 83% Analysis Date = 06/02/21 Pct Recovery = 83% Analysis Date = 06/02/21 Pct Recovery = 83% Analysis Date = 05/29/21 Pct Recovery = 83% Analysis Date = 05/29/21 Pct Recovery = 83% Analysis Date = 05/25/21 Pct Recovery = 83% Analysis Date = 05/25/21 Pct Recovery = 83% Analysis Date = 05/20/21 Pct Recovery = 83% Analysis Date = 05/20/21 Pct Recovery = 83% Analysis Date = 05/16/21 Pct Recovery = 83% Analysis Date = 05/16/21 Pct Recovery = 83% Analysis Date = 05/12/21 Pct Recovery = 83% Analysis Date = 05/12/21 Pct Recovery = 83% Analysis Date = 05/07/21 Pct Recovery = 83% Analysis Date = 05/07/21 Pct Recovery = 83% Analysis Date = 05/03/21 Pct Recovery = 83% Analysis Date = 05/03/21 Pct Recovery = 83% Analysis Date = 04/29/21 Pct Recovery = 83% Analysis Date = 04/29/21 Pct Recovery = 83% Analysis Date = 04/24/21 Pct Recovery = 83% Analysis Date = 04/24/21 Pct Recovery = 83% Analysis Date = 04/20/21 Pct Recovery = 83% Analysis Date = 04/20/21 Pct Recovery = 83% Analysis Date = 04/16/21 Pct Recovery = 83% Analysis Date = 04/16/21 Pct Recovery = 83% Analysis Date = 04/11/21 Pct Recovery = 83% Analysis Date = 04/11/21 Pct Recovery = 83% Analysis Date = 04/07/21 Pct Recovery = 83% Analysis Date = 04/07/21 Pct Recovery = 83% Analysis Date = 04/03/21 Pct Recovery = 84% Analysis Date = 04/03/21 Pct Recovery = 84% Analysis Date = 03/29/21 Pct Recovery = 84% Analysis Date = 03/29/21 Pct Recovery = 84% Analysis Date = 03/25/21 Pct Recovery = 84% Analysis Date = 03/25/21 Pct Recovery = 84% Analysis Date = 03/21/21 Pct Recovery = 85% Analysis Date = 03/21/21 Pct Recovery = 85% Analysis Date = 03/17/21 Pct Recovery = 85% Analysis Date = 03/17/21 Pct Recovery = 85% Analysis Date = 03/12/21 Pct Recovery = 85% Analysis Date = 03/12/21 Pct Recovery = 85% Analysis Date = 03/08/21 Pct Recovery = 86% Analysis Date = 03/08/21 Pct Recovery = 86% Analysis Date = 03/04/21 Pct Recovery = 86% Analysis Date = 03/04/21 Pct Recovery = 86% Analysis Date = 02/27/21 Pct Recovery = 86% Analysis Date = 02/27/21 Pct Recovery = 86% Analysis Date = 02/23/21 Pct Recovery = 86% Analysis Date = 02/23/21 Pct Recovery = 86% Analysis Date = 02/19/21 Pct Recovery = 87% Analysis Date = 02/19/21 Pct Recovery = 87% Analysis Date = 02/14/21 Pct Recovery = 87% Analysis Date = 02/14/21 Pct Recovery = 87% Analysis Date = 02/10/21 Pct Recovery = 87% Analysis Date = 02/10/21 Pct Recovery = 87% Analysis Date = 02/06/21 Pct Recovery = 88% Analysis Date = 02/06/21 Pct Recovery = 88% Analysis Date = 02/01/21 Pct Recovery = 88% Analysis Date = 02/01/21 Pct Recovery = 88% Analysis Date = 01/28/21 Pct Recovery = 89% Analysis Date = 01/28/21 Pct Recovery = 89% Analysis Date = 01/24/21 Pct Recovery = 89% Analysis Date = 01/24/21 Pct Recovery = 89% Analysis Date = 01/19/21 Pct Recovery = 90% Analysis Date = 01/19/21 Pct Recovery = 90% Analysis Date = 01/15/21 Pct Recovery = 90% Analysis Date = 01/15/21 Pct Recovery = 90% Analysis Date = 01/11/21 Pct Recovery = 90% Analysis Date = 01/11/21 Pct Recovery = 90% Analysis Date = 01/07/21 Pct Recovery = 91% Analysis Date = 01/07/21 Pct Recovery = 91% Analysis Date = 01/02/21 Pct Recovery = 91% Analysis Date = 01/02/21 Pct Recovery = 91% Analysis Date = 12/29/20 Pct Recovery = 92% Analysis Date = 12/29/20 Pct Recovery = 92% Analysis Date = 12/25/20 Pct Recovery = 92% Analysis Date = 12/25/20 Pct Recovery = 92% Analysis Date = 12/20/20 Pct Recovery = 93% Analysis Date = 12/20/20 Pct Recovery = 93% Analysis Date = 12/16/20 Pct Recovery = 93% Analysis Date = 12/16/20 Pct Recovery = 93% Analysis Date = 12/12/20 Pct Recovery = 93% Analysis Date = 12/12/20 Pct Recovery = 93% Analysis Date = 12/07/20 Pct Recovery = 94% Analysis Date = 12/07/20 Pct Recovery = 94% Analysis Date = 12/03/20 Pct Recovery = 94% Analysis Date = 12/03/20 Pct Recovery = 94% Analysis Date = 11/29/20 Pct Recovery = 95% Analysis Date = 11/29/20 Pct Recovery = 95% Analysis Date = 11/24/20 Pct Recovery = 95% Analysis Date = 11/24/20 Pct Recovery = 95% Analysis Date = 11/20/20 Pct Recovery = 95% Analysis Date = 11/20/20 Pct Recovery = 95% Analysis Date = 11/16/20 Pct Recovery = 96% Analysis Date = 11/16/20 Pct Recovery = 96% Analysis Date = 11/11/20 Pct Recovery = 97% Analysis Date = 11/11/20 Pct Recovery = 97% Analysis Date = 11/07/20 Pct Recovery = 98% Analysis Date = 11/07/20 Pct Recovery = 98% Analysis Date = 11/03/20 Pct Recovery = 98% Analysis Date = 11/03/20 Pct Recovery = 98% Analysis Date = 10/29/20 Pct Recovery = 99% Analysis Date = 10/29/20 Pct Recovery = 99% Analysis Date = 10/25/20 Pct Recovery = 100% Analysis Date = 10/25/20 Pct Recovery = 100% Analysis Date = 10/21/20 Pct Recovery = 100% Analysis Date = 10/21/20 Pct Recovery = 100% Analysis Date = 10/17/20 Pct Recovery = 101% Analysis Date = 10/17/20 Pct Recovery = 101% Analysis Date = 10/12/20 Pct Recovery = 101% Analysis Date = 10/12/20 Pct Recovery = 101% Analysis Date = 10/08/20 Pct Recovery = 102% Analysis Date = 10/08/20 Pct Recovery = 102% Analysis Date = 10/04/20 Pct Recovery = 102% Analysis Date = 10/04/20 Pct Recovery = 102% Analysis Date = 09/29/20 Pct Recovery = 103% Analysis Date = 09/29/20 Pct Recovery = 103% Analysis Date = 09/25/20 Pct Recovery = 104% Analysis Date = 09/25/20 Pct Recovery = 104% Analysis Date = 09/21/20 Pct Recovery = 104% Analysis Date = 09/21/20 Pct Recovery = 104% Analysis Date = 09/16/20 Pct Recovery = 103% Analysis Date = 09/16/20 Pct Recovery = 103% Analysis Date = 09/12/20 Pct Recovery = 103% Analysis Date = 09/12/20 Pct Recovery = 103% Analysis Date = 09/08/20 Pct Recovery = 103% Analysis Date = 09/08/20 Pct Recovery = 103% Analysis Date = 09/03/20 Pct Recovery = 103% Analysis Date = 09/03/20 Pct Recovery = 103% Analysis Date = 08/30/20 Pct Recovery = 103% Analysis Date = 08/30/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 102% Analysis Date = 08/26/20 Pct Recovery = 102% Analysis Date = 08/21/20 Pct Recovery = 102% Analysis Date = 08/21/20 Pct Recovery = 102% Analysis Date = 08/17/20 Pct Recovery = 102% Analysis Date = 08/17/20 Pct Recovery = 102% Analysis Date = 08/13/20 Pct Recovery = 101% Analysis Date = 08/13/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/27/20 Pct Recovery = 100% Analysis Date = 07/27/20 Pct Recovery = 100% Analysis Date = 07/22/20 Pct Recovery = 100% Analysis Date = 07/22/20 Pct Recovery = 100% Analysis Date = 07/18/20 Pct Recovery = 100% Analysis Date = 07/18/20 Pct Recovery = 100% Analysis Date = 07/14/20 Pct Recovery = 100% Analysis Date = 07/14/20 Pct Recovery = 100% Analysis Date = 07/09/20 Pct Recovery = 99% Analysis Date = 07/09/20 Pct Recovery = 99% Analysis Date = 07/05/20 Pct Recovery = 99% Analysis Date = 07/05/20 Pct Recovery = 99% Analysis Date = 07/01/20 Pct Recovery = 99% Analysis Date = 07/01/20 Pct Recovery = 99% Analysis Date = 06/26/20 Pct Recovery = 98% Analysis Date = 06/26/20 Pct Recovery = 98% Analysis Date = 06/22/20 Pct Recovery = 98% Analysis Date = 06/22/20 Pct Recovery = 98% Analysis Date = 06/18/20 Pct Recovery = 98% Analysis Date = 06/18/20 Pct Recovery = 98% Analysis Date = 06/13/20 Pct Recovery = 98% Analysis Date = 06/13/20 Pct Recovery = 98% Analysis Date = 06/09/20 Pct Recovery = 97% Analysis Date = 06/09/20 Pct Recovery = 97% Analysis Date = 06/05/20 Pct Recovery = 97% Analysis Date = 06/05/20 Pct Recovery = 97% Analysis Date = 05/31/20 Pct Recovery = 97% Analysis Date = 05/31/20 Pct Recovery = 97% Analysis Date = 05/27/20 Pct Recovery = 97% Analysis Date = 05/27/20 Pct Recovery = 97% Analysis Date = 05/23/20 Pct Recovery = 96% Analysis Date = 05/23/20 Pct Recovery = 96% Analysis Date = 05/19/20 Pct Recovery = 96% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 89% 28% 87% 26%
Total 38 89% 28% 87% 26%

Sample Statistics
CHLORPYRIFOS

Characteristic N % % Basis
Plotted 38 90% Spiked
Estimated Values 2 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 5% Spiked
Spiked 42 .  
False Negatives 2 5% 2 out of 42
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

OBSP Determination:
CIS-CYHALOTHRIC ACID
METHOD: 2447 , TESTIDCODE: 68553LCM60

Laboratory ID = 20222010133 Lab Value = 698.453 Expected Conc. = 1050 Report level label = 105 Pct Recovery = 67% Analysis Date = 07/22/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20222640086 Lab Value = 827.436 Expected Conc. = 1045.6 Report level label = 105 Pct Recovery = 79% Analysis Date = 09/30/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20221870197 Lab Value = 456.336 Expected Conc. = 656.25 Report level label = 105 Pct Recovery = 70% Analysis Date = 07/14/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20201610160 Lab Value = 273.684 Expected Conc. = 261.2 Report level label = 105 Pct Recovery = 105% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Analysis Date = 09/30/22 Pct Recovery = 79% Analysis Date = 09/25/22 Pct Recovery = 78% Analysis Date = 09/25/22 Pct Recovery = 78% Analysis Date = 09/21/22 Pct Recovery = 78% Analysis Date = 09/21/22 Pct Recovery = 78% Analysis Date = 09/17/22 Pct Recovery = 77% Analysis Date = 09/17/22 Pct Recovery = 77% Analysis Date = 09/13/22 Pct Recovery = 76% Analysis Date = 09/13/22 Pct Recovery = 76% Analysis Date = 09/08/22 Pct Recovery = 75% Analysis Date = 09/08/22 Pct Recovery = 75% Analysis Date = 09/04/22 Pct Recovery = 75% Analysis Date = 09/04/22 Pct Recovery = 75% Analysis Date = 08/31/22 Pct Recovery = 74% Analysis Date = 08/31/22 Pct Recovery = 74% Analysis Date = 08/27/22 Pct Recovery = 73% Analysis Date = 08/27/22 Pct Recovery = 73% Analysis Date = 08/23/22 Pct Recovery = 72% Analysis Date = 08/23/22 Pct Recovery = 72% Analysis Date = 08/18/22 Pct Recovery = 72% Analysis Date = 08/18/22 Pct Recovery = 72% Analysis Date = 08/14/22 Pct Recovery = 71% Analysis Date = 08/14/22 Pct Recovery = 71% Analysis Date = 08/10/22 Pct Recovery = 70% Analysis Date = 08/10/22 Pct Recovery = 70% Analysis Date = 08/06/22 Pct Recovery = 69% Analysis Date = 08/06/22 Pct Recovery = 69% Analysis Date = 08/02/22 Pct Recovery = 69% Analysis Date = 08/02/22 Pct Recovery = 69% Analysis Date = 07/28/22 Pct Recovery = 68% Analysis Date = 07/28/22 Pct Recovery = 68% Analysis Date = 07/24/22 Pct Recovery = 67% Analysis Date = 07/24/22 Pct Recovery = 67% Analysis Date = 07/20/22 Pct Recovery = 67% Analysis Date = 07/20/22 Pct Recovery = 67% Analysis Date = 07/16/22 Pct Recovery = 69% Analysis Date = 07/16/22 Pct Recovery = 69% Analysis Date = 07/12/22 Pct Recovery = 70% Analysis Date = 07/12/22 Pct Recovery = 70% Analysis Date = 07/07/22 Pct Recovery = 70% Analysis Date = 07/07/22 Pct Recovery = 70% Analysis Date = 07/03/22 Pct Recovery = 70% Analysis Date = 07/03/22 Pct Recovery = 70% Analysis Date = 06/29/22 Pct Recovery = 70% Analysis Date = 06/29/22 Pct Recovery = 70% Analysis Date = 06/25/22 Pct Recovery = 70% Analysis Date = 06/25/22 Pct Recovery = 70% Analysis Date = 06/21/22 Pct Recovery = 71% Analysis Date = 06/21/22 Pct Recovery = 71% Analysis Date = 06/16/22 Pct Recovery = 71% Analysis Date = 06/16/22 Pct Recovery = 71% Analysis Date = 06/12/22 Pct Recovery = 71% Analysis Date = 06/12/22 Pct Recovery = 71% Analysis Date = 06/08/22 Pct Recovery = 71% Analysis Date = 06/08/22 Pct Recovery = 71% Analysis Date = 06/04/22 Pct Recovery = 71% Analysis Date = 06/04/22 Pct Recovery = 71% Analysis Date = 05/31/22 Pct Recovery = 72% Analysis Date = 05/31/22 Pct Recovery = 72% Analysis Date = 05/26/22 Pct Recovery = 72% Analysis Date = 05/26/22 Pct Recovery = 72% Analysis Date = 05/22/22 Pct Recovery = 72% Analysis Date = 05/22/22 Pct Recovery = 72% Analysis Date = 05/18/22 Pct Recovery = 72% Analysis Date = 05/18/22 Pct Recovery = 72% Analysis Date = 05/14/22 Pct Recovery = 72% Analysis Date = 05/14/22 Pct Recovery = 72% Analysis Date = 05/10/22 Pct Recovery = 73% Analysis Date = 05/10/22 Pct Recovery = 73% Analysis Date = 05/05/22 Pct Recovery = 73% Analysis Date = 05/05/22 Pct Recovery = 73% Analysis Date = 05/01/22 Pct Recovery = 73% Analysis Date = 05/01/22 Pct Recovery = 73% Analysis Date = 04/27/22 Pct Recovery = 73% Analysis Date = 04/27/22 Pct Recovery = 73% Analysis Date = 04/23/22 Pct Recovery = 73% Analysis Date = 04/23/22 Pct Recovery = 73% Analysis Date = 04/19/22 Pct Recovery = 74% Analysis Date = 04/19/22 Pct Recovery = 74% Analysis Date = 04/14/22 Pct Recovery = 74% Analysis Date = 04/14/22 Pct Recovery = 74% Analysis Date = 04/10/22 Pct Recovery = 74% Analysis Date = 04/10/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 03/28/22 Pct Recovery = 74% Analysis Date = 03/28/22 Pct Recovery = 74% Analysis Date = 03/24/22 Pct Recovery = 75% Analysis Date = 03/24/22 Pct Recovery = 75% Analysis Date = 03/20/22 Pct Recovery = 75% Analysis Date = 03/20/22 Pct Recovery = 75% Analysis Date = 03/16/22 Pct Recovery = 75% Analysis Date = 03/16/22 Pct Recovery = 75% Analysis Date = 03/12/22 Pct Recovery = 75% Analysis Date = 03/12/22 Pct Recovery = 75% Analysis Date = 03/07/22 Pct Recovery = 75% Analysis Date = 03/07/22 Pct Recovery = 75% Analysis Date = 03/03/22 Pct Recovery = 76% Analysis Date = 03/03/22 Pct Recovery = 76% Analysis Date = 02/27/22 Pct Recovery = 76% Analysis Date = 02/27/22 Pct Recovery = 76% Analysis Date = 02/23/22 Pct Recovery = 76% Analysis Date = 02/23/22 Pct Recovery = 76% Analysis Date = 02/19/22 Pct Recovery = 76% Analysis Date = 02/19/22 Pct Recovery = 76% Analysis Date = 02/14/22 Pct Recovery = 76% Analysis Date = 02/14/22 Pct Recovery = 76% Analysis Date = 02/10/22 Pct Recovery = 77% Analysis Date = 02/10/22 Pct Recovery = 77% Analysis Date = 02/06/22 Pct Recovery = 77% Analysis Date = 02/06/22 Pct Recovery = 77% Analysis Date = 02/02/22 Pct Recovery = 77% Analysis Date = 02/02/22 Pct Recovery = 77% Analysis Date = 01/29/22 Pct Recovery = 77% Analysis Date = 01/29/22 Pct Recovery = 77% Analysis Date = 01/24/22 Pct Recovery = 77% Analysis Date = 01/24/22 Pct Recovery = 77% Analysis Date = 01/20/22 Pct Recovery = 78% Analysis Date = 01/20/22 Pct Recovery = 78% Analysis Date = 01/16/22 Pct Recovery = 78% Analysis Date = 01/16/22 Pct Recovery = 78% Analysis Date = 01/12/22 Pct Recovery = 78% Analysis Date = 01/12/22 Pct Recovery = 78% Analysis Date = 01/08/22 Pct Recovery = 78% Analysis Date = 01/08/22 Pct Recovery = 78% Analysis Date = 01/03/22 Pct Recovery = 78% Analysis Date = 01/03/22 Pct Recovery = 78% Analysis Date = 12/30/21 Pct Recovery = 79% Analysis Date = 12/30/21 Pct Recovery = 79% Analysis Date = 12/26/21 Pct Recovery = 79% Analysis Date = 12/26/21 Pct Recovery = 79% Analysis Date = 12/22/21 Pct Recovery = 79% Analysis Date = 12/22/21 Pct Recovery = 79% Analysis Date = 12/18/21 Pct Recovery = 79% Analysis Date = 12/18/21 Pct Recovery = 79% Analysis Date = 12/13/21 Pct Recovery = 79% Analysis Date = 12/13/21 Pct Recovery = 79% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/05/21 Pct Recovery = 80% Analysis Date = 12/05/21 Pct Recovery = 80% Analysis Date = 12/01/21 Pct Recovery = 80% Analysis Date = 12/01/21 Pct Recovery = 80% Analysis Date = 11/27/21 Pct Recovery = 80% Analysis Date = 11/27/21 Pct Recovery = 80% Analysis Date = 11/22/21 Pct Recovery = 80% Analysis Date = 11/22/21 Pct Recovery = 80% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/14/21 Pct Recovery = 81% Analysis Date = 11/14/21 Pct Recovery = 81% Analysis Date = 11/10/21 Pct Recovery = 81% Analysis Date = 11/10/21 Pct Recovery = 81% Analysis Date = 11/06/21 Pct Recovery = 81% Analysis Date = 11/06/21 Pct Recovery = 81% Analysis Date = 11/01/21 Pct Recovery = 81% Analysis Date = 11/01/21 Pct Recovery = 81% Analysis Date = 10/28/21 Pct Recovery = 81% Analysis Date = 10/28/21 Pct Recovery = 81% Analysis Date = 10/24/21 Pct Recovery = 82% Analysis Date = 10/24/21 Pct Recovery = 82% Analysis Date = 10/20/21 Pct Recovery = 82% Analysis Date = 10/20/21 Pct Recovery = 82% Analysis Date = 10/15/21 Pct Recovery = 82% Analysis Date = 10/15/21 Pct Recovery = 82% Analysis Date = 10/11/21 Pct Recovery = 82% Analysis Date = 10/11/21 Pct Recovery = 82% Analysis Date = 10/07/21 Pct Recovery = 82% Analysis Date = 10/07/21 Pct Recovery = 82% Analysis Date = 10/03/21 Pct Recovery = 83% Analysis Date = 10/03/21 Pct Recovery = 83% Analysis Date = 09/29/21 Pct Recovery = 83% Analysis Date = 09/29/21 Pct Recovery = 83% Analysis Date = 09/24/21 Pct Recovery = 83% Analysis Date = 09/24/21 Pct Recovery = 83% Analysis Date = 09/20/21 Pct Recovery = 83% Analysis Date = 09/20/21 Pct Recovery = 83% Analysis Date = 09/16/21 Pct Recovery = 83% Analysis Date = 09/16/21 Pct Recovery = 83% Analysis Date = 09/12/21 Pct Recovery = 84% Analysis Date = 09/12/21 Pct Recovery = 84% Analysis Date = 09/08/21 Pct Recovery = 84% Analysis Date = 09/08/21 Pct Recovery = 84% Analysis Date = 09/03/21 Pct Recovery = 84% Analysis Date = 09/03/21 Pct Recovery = 84% Analysis Date = 08/30/21 Pct Recovery = 84% Analysis Date = 08/30/21 Pct Recovery = 84% Analysis Date = 08/26/21 Pct Recovery = 84% Analysis Date = 08/26/21 Pct Recovery = 84% Analysis Date = 08/22/21 Pct Recovery = 85% Analysis Date = 08/22/21 Pct Recovery = 85% Analysis Date = 08/18/21 Pct Recovery = 85% Analysis Date = 08/18/21 Pct Recovery = 85% Analysis Date = 08/13/21 Pct Recovery = 85% Analysis Date = 08/13/21 Pct Recovery = 85% Analysis Date = 08/09/21 Pct Recovery = 85% Analysis Date = 08/09/21 Pct Recovery = 85% Analysis Date = 08/05/21 Pct Recovery = 85% Analysis Date = 08/05/21 Pct Recovery = 85% Analysis Date = 08/01/21 Pct Recovery = 86% Analysis Date = 08/01/21 Pct Recovery = 86% Analysis Date = 07/28/21 Pct Recovery = 86% Analysis Date = 07/28/21 Pct Recovery = 86% Analysis Date = 07/23/21 Pct Recovery = 86% Analysis Date = 07/23/21 Pct Recovery = 86% Analysis Date = 07/19/21 Pct Recovery = 86% Analysis Date = 07/19/21 Pct Recovery = 86% Analysis Date = 07/15/21 Pct Recovery = 86% Analysis Date = 07/15/21 Pct Recovery = 86% Analysis Date = 07/11/21 Pct Recovery = 87% Analysis Date = 07/11/21 Pct Recovery = 87% Analysis Date = 07/07/21 Pct Recovery = 87% Analysis Date = 07/07/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/16/21 Pct Recovery = 88% Analysis Date = 06/16/21 Pct Recovery = 88% Analysis Date = 06/11/21 Pct Recovery = 88% Analysis Date = 06/11/21 Pct Recovery = 88% Analysis Date = 06/07/21 Pct Recovery = 88% Analysis Date = 06/07/21 Pct Recovery = 88% Analysis Date = 06/03/21 Pct Recovery = 88% Analysis Date = 06/03/21 Pct Recovery = 88% Analysis Date = 05/30/21 Pct Recovery = 88% Analysis Date = 05/30/21 Pct Recovery = 88% Analysis Date = 05/26/21 Pct Recovery = 89% Analysis Date = 05/26/21 Pct Recovery = 89% Analysis Date = 05/21/21 Pct Recovery = 89% Analysis Date = 05/21/21 Pct Recovery = 89% Analysis Date = 05/17/21 Pct Recovery = 89% Analysis Date = 05/17/21 Pct Recovery = 89% Analysis Date = 05/13/21 Pct Recovery = 89% Analysis Date = 05/13/21 Pct Recovery = 89% Analysis Date = 05/09/21 Pct Recovery = 89% Analysis Date = 05/09/21 Pct Recovery = 89% Analysis Date = 05/04/21 Pct Recovery = 90% Analysis Date = 05/04/21 Pct Recovery = 90% Analysis Date = 04/30/21 Pct Recovery = 90% Analysis Date = 04/30/21 Pct Recovery = 90% Analysis Date = 04/26/21 Pct Recovery = 90% Analysis Date = 04/26/21 Pct Recovery = 90% Analysis Date = 04/22/21 Pct Recovery = 90% Analysis Date = 04/22/21 Pct Recovery = 90% Analysis Date = 04/18/21 Pct Recovery = 90% Analysis Date = 04/18/21 Pct Recovery = 90% Analysis Date = 04/13/21 Pct Recovery = 91% Analysis Date = 04/13/21 Pct Recovery = 91% Analysis Date = 04/09/21 Pct Recovery = 91% Analysis Date = 04/09/21 Pct Recovery = 91% Analysis Date = 04/05/21 Pct Recovery = 91% Analysis Date = 04/05/21 Pct Recovery = 91% Analysis Date = 04/01/21 Pct Recovery = 91% Analysis Date = 04/01/21 Pct Recovery = 91% Analysis Date = 03/28/21 Pct Recovery = 91% Analysis Date = 03/28/21 Pct Recovery = 91% Analysis Date = 03/23/21 Pct Recovery = 92% Analysis Date = 03/23/21 Pct Recovery = 92% Analysis Date = 03/19/21 Pct Recovery = 92% Analysis Date = 03/19/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/11/21 Pct Recovery = 92% Analysis Date = 03/11/21 Pct Recovery = 92% Analysis Date = 03/07/21 Pct Recovery = 92% Analysis Date = 03/07/21 Pct Recovery = 92% Analysis Date = 03/02/21 Pct Recovery = 93% Analysis Date = 03/02/21 Pct Recovery = 93% Analysis Date = 02/26/21 Pct Recovery = 93% Analysis Date = 02/26/21 Pct Recovery = 93% Analysis Date = 02/22/21 Pct Recovery = 93% Analysis Date = 02/22/21 Pct Recovery = 93% Analysis Date = 02/18/21 Pct Recovery = 93% Analysis Date = 02/18/21 Pct Recovery = 93% Analysis Date = 02/14/21 Pct Recovery = 93% Analysis Date = 02/14/21 Pct Recovery = 93% Analysis Date = 02/09/21 Pct Recovery = 94% Analysis Date = 02/09/21 Pct Recovery = 94% Analysis Date = 02/05/21 Pct Recovery = 94% Analysis Date = 02/05/21 Pct Recovery = 94% Analysis Date = 02/01/21 Pct Recovery = 94% Analysis Date = 02/01/21 Pct Recovery = 94% Analysis Date = 01/28/21 Pct Recovery = 94% Analysis Date = 01/28/21 Pct Recovery = 94% Analysis Date = 01/24/21 Pct Recovery = 94% Analysis Date = 01/24/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/15/21 Pct Recovery = 95% Analysis Date = 01/15/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 95% Analysis Date = 01/07/21 Pct Recovery = 95% Analysis Date = 01/07/21 Pct Recovery = 95% Analysis Date = 01/03/21 Pct Recovery = 95% Analysis Date = 01/03/21 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/13/20 Pct Recovery = 96% Analysis Date = 12/13/20 Pct Recovery = 96% Analysis Date = 12/08/20 Pct Recovery = 96% Analysis Date = 12/08/20 Pct Recovery = 96% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 97% Analysis Date = 11/26/20 Pct Recovery = 97% Analysis Date = 11/26/20 Pct Recovery = 97% Analysis Date = 11/21/20 Pct Recovery = 97% Analysis Date = 11/21/20 Pct Recovery = 97% Analysis Date = 11/17/20 Pct Recovery = 97% Analysis Date = 11/17/20 Pct Recovery = 97% Analysis Date = 11/13/20 Pct Recovery = 98% Analysis Date = 11/13/20 Pct Recovery = 98% Analysis Date = 11/09/20 Pct Recovery = 98% Analysis Date = 11/09/20 Pct Recovery = 98% Analysis Date = 11/05/20 Pct Recovery = 98% Analysis Date = 11/05/20 Pct Recovery = 98% Analysis Date = 10/31/20 Pct Recovery = 98% Analysis Date = 10/31/20 Pct Recovery = 98% Analysis Date = 10/27/20 Pct Recovery = 98% Analysis Date = 10/27/20 Pct Recovery = 98% Analysis Date = 10/23/20 Pct Recovery = 99% Analysis Date = 10/23/20 Pct Recovery = 99% Analysis Date = 10/19/20 Pct Recovery = 99% Analysis Date = 10/19/20 Pct Recovery = 99% Analysis Date = 10/15/20 Pct Recovery = 99% Analysis Date = 10/15/20 Pct Recovery = 99% Analysis Date = 10/10/20 Pct Recovery = 99% Analysis Date = 10/10/20 Pct Recovery = 99% Analysis Date = 10/06/20 Pct Recovery = 99% Analysis Date = 10/06/20 Pct Recovery = 99% Analysis Date = 10/02/20 Pct Recovery = 100% Analysis Date = 10/02/20 Pct Recovery = 100% Analysis Date = 09/28/20 Pct Recovery = 100% Analysis Date = 09/28/20 Pct Recovery = 100% Analysis Date = 09/24/20 Pct Recovery = 100% Analysis Date = 09/24/20 Pct Recovery = 100% Analysis Date = 09/19/20 Pct Recovery = 100% Analysis Date = 09/19/20 Pct Recovery = 100% Analysis Date = 09/15/20 Pct Recovery = 100% Analysis Date = 09/15/20 Pct Recovery = 100% Analysis Date = 09/11/20 Pct Recovery = 101% Analysis Date = 09/11/20 Pct Recovery = 101% Analysis Date = 09/07/20 Pct Recovery = 101% Analysis Date = 09/07/20 Pct Recovery = 101% Analysis Date = 09/03/20 Pct Recovery = 101% Analysis Date = 09/03/20 Pct Recovery = 101% Analysis Date = 08/29/20 Pct Recovery = 101% Analysis Date = 08/29/20 Pct Recovery = 101% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/17/20 Pct Recovery = 102% Analysis Date = 08/17/20 Pct Recovery = 102% Analysis Date = 08/13/20 Pct Recovery = 102% Analysis Date = 08/13/20 Pct Recovery = 102% Analysis Date = 08/08/20 Pct Recovery = 102% Analysis Date = 08/08/20 Pct Recovery = 102% Analysis Date = 08/04/20 Pct Recovery = 102% Analysis Date = 08/04/20 Pct Recovery = 102% Analysis Date = 07/31/20 Pct Recovery = 102% Analysis Date = 07/31/20 Pct Recovery = 102% Analysis Date = 07/27/20 Pct Recovery = 103% Analysis Date = 07/27/20 Pct Recovery = 103% Analysis Date = 07/23/20 Pct Recovery = 103% Analysis Date = 07/23/20 Pct Recovery = 103% Analysis Date = 07/18/20 Pct Recovery = 103% Analysis Date = 07/18/20 Pct Recovery = 103% Analysis Date = 07/14/20 Pct Recovery = 103% Analysis Date = 07/14/20 Pct Recovery = 103% Analysis Date = 07/10/20 Pct Recovery = 103% Analysis Date = 07/10/20 Pct Recovery = 103% Analysis Date = 07/06/20 Pct Recovery = 104% Analysis Date = 07/06/20 Pct Recovery = 104% Analysis Date = 07/02/20 Pct Recovery = 104% Analysis Date = 07/02/20 Pct Recovery = 104% Analysis Date = 06/27/20 Pct Recovery = 104% Analysis Date = 06/27/20 Pct Recovery = 104% Analysis Date = 06/23/20 Pct Recovery = 104% Analysis Date = 06/23/20 Pct Recovery = 104% Analysis Date = 06/19/20 Pct Recovery = 104% Analysis Date = 06/19/20 Pct Recovery = 104% Analysis Date = 06/15/20 Pct Recovery = 105% Analysis Date = 06/15/20 Pct Recovery = 105% Analysis Date = 06/11/20 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-CYHALOTHRIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 4 80% 17% 74% 18%
Total 4 80% 17% 74% 18%

Sample Statistics
CIS-CYHALOTHRIC ACID

Characteristic N % % Basis
Plotted 4 44% Spiked
Estimated Values 1 11% Spiked
Deleted Values 10 9% Spiked + Not Spiked
Spiked, Censored 2 22% Spiked
Spiked 10 .  
False Negatives 3 33% 3 out of 9
Not Spiked 106 .  
False Positives 0 0% 0 out of 97

OBSP Determination:
CIS-PERMETHRIN
METHOD: 2447 , TESTIDCODE: 68769LCM60

Laboratory ID = 20203230020 Lab Value = 28.522 Expected Conc. = 53.44 Report level label = 4.2 Pct Recovery = 53% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20203230023 Lab Value = 29.827 Expected Conc. = 53.44 Report level label = 4.2 Pct Recovery = 56% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20202110006 Lab Value = 25.893 Expected Conc. = 53.2 Report level label = 4.2 Pct Recovery = 49% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 26.957 Expected Conc. = 53 Report level label = 4.2 Pct Recovery = 51% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 14.260 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 27% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202880004 Lab Value = 15.351 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 29% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590108 Lab Value = 56.391 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 108% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590109 Lab Value = 45.741 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 88% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20220190116 Lab Value = 10.234 Expected Conc. = 42.4 Report level label = 4.2 Pct Recovery = 24% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 14.301 Expected Conc. = 42.4 Report level label = 4.2 Pct Recovery = 34% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 22.638 Expected Conc. = 42 Report level label = 4.2 Pct Recovery = 54% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20212990174 Lab Value = 20.806 Expected Conc. = 41.84 Report level label = 4.2 Pct Recovery = 50% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220810134 Lab Value = 15.153 Expected Conc. = 41.6 Report level label = 4.2 Pct Recovery = 36% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20210400070 Lab Value = 9.459 Expected Conc. = 26.72 Report level label = 4.2 Pct Recovery = 35% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20201680155 Lab Value = 15.572 Expected Conc. = 26.6 Report level label = 4.2 Pct Recovery = 59% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20221730293 Lab Value = 17.093 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 65% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 8.268 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 31% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202530029 Lab Value = 12.130 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 46% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 13.801 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 52% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 20.726 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 78% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20213340027 Lab Value = 14.351 Expected Conc. = 26.15 Report level label = 4.2 Pct Recovery = 55% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 26.249 Expected Conc. = 26.15 Report level label = 4.2 Pct Recovery = 100% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 8.122 Expected Conc. = 26.15 Report level label = 4.2 Pct Recovery = 31% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202950016 Lab Value = 14.114 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 54% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20220810133 Lab Value = 16.555 Expected Conc. = 26 Report level label = 4.2 Pct Recovery = 64% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201610160 Lab Value = 6.249 Expected Conc. = 10.64 Report level label = 4.2 Pct Recovery = 59% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20222500483 Lab Value = 5.320 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 50% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20202330309 Lab Value = 6.568 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 62% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 7.223 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 68% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 6.433 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 61% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 8.242 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 78% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20213060210 Lab Value = 4.151 Expected Conc. = 10.46 Report level label = 4.2 Pct Recovery = 40% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20203170006 Lab Value = 5.275 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 51% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20222630205 Lab Value = 4.978 Expected Conc. = 10.4 Report level label = 4.2 Pct Recovery = 48% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Analysis Date = 09/28/22 Pct Recovery = 51% Analysis Date = 09/24/22 Pct Recovery = 51% Analysis Date = 09/24/22 Pct Recovery = 51% Analysis Date = 09/20/22 Pct Recovery = 51% Analysis Date = 09/20/22 Pct Recovery = 51% Analysis Date = 09/16/22 Pct Recovery = 51% Analysis Date = 09/16/22 Pct Recovery = 51% Analysis Date = 09/11/22 Pct Recovery = 51% Analysis Date = 09/11/22 Pct Recovery = 51% Analysis Date = 09/07/22 Pct Recovery = 51% Analysis Date = 09/07/22 Pct Recovery = 51% Analysis Date = 09/03/22 Pct Recovery = 51% Analysis Date = 09/03/22 Pct Recovery = 51% Analysis Date = 08/29/22 Pct Recovery = 51% Analysis Date = 08/29/22 Pct Recovery = 51% Analysis Date = 08/25/22 Pct Recovery = 51% Analysis Date = 08/25/22 Pct Recovery = 51% Analysis Date = 08/21/22 Pct Recovery = 51% Analysis Date = 08/21/22 Pct Recovery = 51% Analysis Date = 08/16/22 Pct Recovery = 51% Analysis Date = 08/16/22 Pct Recovery = 51% Analysis Date = 08/12/22 Pct Recovery = 51% Analysis Date = 08/12/22 Pct Recovery = 51% Analysis Date = 08/08/22 Pct Recovery = 51% Analysis Date = 08/08/22 Pct Recovery = 51% Analysis Date = 08/03/22 Pct Recovery = 51% Analysis Date = 08/03/22 Pct Recovery = 51% Analysis Date = 07/30/22 Pct Recovery = 51% Analysis Date = 07/30/22 Pct Recovery = 51% Analysis Date = 07/26/22 Pct Recovery = 50% Analysis Date = 07/26/22 Pct Recovery = 50% Analysis Date = 07/21/22 Pct Recovery = 50% Analysis Date = 07/21/22 Pct Recovery = 50% Analysis Date = 07/17/22 Pct Recovery = 50% Analysis Date = 07/17/22 Pct Recovery = 50% Analysis Date = 07/13/22 Pct Recovery = 50% Analysis Date = 07/13/22 Pct Recovery = 50% Analysis Date = 07/09/22 Pct Recovery = 50% Analysis Date = 07/09/22 Pct Recovery = 50% Analysis Date = 07/04/22 Pct Recovery = 50% Analysis Date = 07/04/22 Pct Recovery = 50% Analysis Date = 06/30/22 Pct Recovery = 50% Analysis Date = 06/30/22 Pct Recovery = 50% Analysis Date = 06/26/22 Pct Recovery = 50% Analysis Date = 06/26/22 Pct Recovery = 50% Analysis Date = 06/21/22 Pct Recovery = 50% Analysis Date = 06/21/22 Pct Recovery = 50% Analysis Date = 06/17/22 Pct Recovery = 50% Analysis Date = 06/17/22 Pct Recovery = 50% Analysis Date = 06/13/22 Pct Recovery = 50% Analysis Date = 06/13/22 Pct Recovery = 50% Analysis Date = 06/08/22 Pct Recovery = 50% Analysis Date = 06/08/22 Pct Recovery = 50% Analysis Date = 06/04/22 Pct Recovery = 50% Analysis Date = 06/04/22 Pct Recovery = 50% Analysis Date = 05/31/22 Pct Recovery = 50% Analysis Date = 05/31/22 Pct Recovery = 50% Analysis Date = 05/26/22 Pct Recovery = 50% Analysis Date = 05/26/22 Pct Recovery = 50% Analysis Date = 05/22/22 Pct Recovery = 50% Analysis Date = 05/22/22 Pct Recovery = 50% Analysis Date = 05/18/22 Pct Recovery = 50% Analysis Date = 05/18/22 Pct Recovery = 50% Analysis Date = 05/13/22 Pct Recovery = 49% Analysis Date = 05/13/22 Pct Recovery = 49% Analysis Date = 05/09/22 Pct Recovery = 49% Analysis Date = 05/09/22 Pct Recovery = 49% Analysis Date = 05/05/22 Pct Recovery = 49% Analysis Date = 05/05/22 Pct Recovery = 49% Analysis Date = 04/30/22 Pct Recovery = 49% Analysis Date = 04/30/22 Pct Recovery = 49% Analysis Date = 04/26/22 Pct Recovery = 49% Analysis Date = 04/26/22 Pct Recovery = 49% Analysis Date = 04/22/22 Pct Recovery = 49% Analysis Date = 04/22/22 Pct Recovery = 49% Analysis Date = 04/18/22 Pct Recovery = 49% Analysis Date = 04/18/22 Pct Recovery = 49% Analysis Date = 04/13/22 Pct Recovery = 49% Analysis Date = 04/13/22 Pct Recovery = 49% Analysis Date = 04/09/22 Pct Recovery = 49% Analysis Date = 04/09/22 Pct Recovery = 49% Analysis Date = 04/05/22 Pct Recovery = 49% Analysis Date = 04/05/22 Pct Recovery = 49% Analysis Date = 03/31/22 Pct Recovery = 49% Analysis Date = 03/31/22 Pct Recovery = 49% Analysis Date = 03/27/22 Pct Recovery = 49% Analysis Date = 03/27/22 Pct Recovery = 49% Analysis Date = 03/23/22 Pct Recovery = 49% Analysis Date = 03/23/22 Pct Recovery = 49% Analysis Date = 03/18/22 Pct Recovery = 49% Analysis Date = 03/18/22 Pct Recovery = 49% Analysis Date = 03/14/22 Pct Recovery = 49% Analysis Date = 03/14/22 Pct Recovery = 49% Analysis Date = 03/10/22 Pct Recovery = 49% Analysis Date = 03/10/22 Pct Recovery = 49% Analysis Date = 03/05/22 Pct Recovery = 49% Analysis Date = 03/05/22 Pct Recovery = 49% Analysis Date = 03/01/22 Pct Recovery = 49% Analysis Date = 03/01/22 Pct Recovery = 49% Analysis Date = 02/25/22 Pct Recovery = 48% Analysis Date = 02/25/22 Pct Recovery = 48% Analysis Date = 02/20/22 Pct Recovery = 48% Analysis Date = 02/20/22 Pct Recovery = 48% Analysis Date = 02/16/22 Pct Recovery = 48% Analysis Date = 02/16/22 Pct Recovery = 48% Analysis Date = 02/12/22 Pct Recovery = 48% Analysis Date = 02/12/22 Pct Recovery = 48% Analysis Date = 02/07/22 Pct Recovery = 48% Analysis Date = 02/07/22 Pct Recovery = 48% Analysis Date = 02/03/22 Pct Recovery = 48% Analysis Date = 02/03/22 Pct Recovery = 48% Analysis Date = 01/30/22 Pct Recovery = 48% Analysis Date = 01/30/22 Pct Recovery = 48% Analysis Date = 01/26/22 Pct Recovery = 48% Analysis Date = 01/26/22 Pct Recovery = 48% Analysis Date = 01/21/22 Pct Recovery = 48% Analysis Date = 01/21/22 Pct Recovery = 48% Analysis Date = 01/17/22 Pct Recovery = 48% Analysis Date = 01/17/22 Pct Recovery = 48% Analysis Date = 01/13/22 Pct Recovery = 48% Analysis Date = 01/13/22 Pct Recovery = 48% Analysis Date = 01/08/22 Pct Recovery = 48% Analysis Date = 01/08/22 Pct Recovery = 48% Analysis Date = 01/04/22 Pct Recovery = 48% Analysis Date = 01/04/22 Pct Recovery = 48% Analysis Date = 12/31/21 Pct Recovery = 48% Analysis Date = 12/31/21 Pct Recovery = 48% Analysis Date = 12/26/21 Pct Recovery = 48% Analysis Date = 12/26/21 Pct Recovery = 48% Analysis Date = 12/22/21 Pct Recovery = 48% Analysis Date = 12/22/21 Pct Recovery = 48% Analysis Date = 12/18/21 Pct Recovery = 48% Analysis Date = 12/18/21 Pct Recovery = 48% Analysis Date = 12/13/21 Pct Recovery = 48% Analysis Date = 12/13/21 Pct Recovery = 48% Analysis Date = 12/09/21 Pct Recovery = 48% Analysis Date = 12/09/21 Pct Recovery = 48% Analysis Date = 12/05/21 Pct Recovery = 48% Analysis Date = 12/05/21 Pct Recovery = 48% Analysis Date = 11/30/21 Pct Recovery = 48% Analysis Date = 11/30/21 Pct Recovery = 48% Analysis Date = 11/26/21 Pct Recovery = 48% Analysis Date = 11/26/21 Pct Recovery = 48% Analysis Date = 11/22/21 Pct Recovery = 48% Analysis Date = 11/22/21 Pct Recovery = 48% Analysis Date = 11/18/21 Pct Recovery = 47% Analysis Date = 11/18/21 Pct Recovery = 47% Analysis Date = 11/13/21 Pct Recovery = 47% Analysis Date = 11/13/21 Pct Recovery = 47% Analysis Date = 11/09/21 Pct Recovery = 47% Analysis Date = 11/09/21 Pct Recovery = 47% Analysis Date = 11/05/21 Pct Recovery = 47% Analysis Date = 11/05/21 Pct Recovery = 47% Analysis Date = 10/31/21 Pct Recovery = 47% Analysis Date = 10/31/21 Pct Recovery = 47% Analysis Date = 10/27/21 Pct Recovery = 47% Analysis Date = 10/27/21 Pct Recovery = 47% Analysis Date = 10/23/21 Pct Recovery = 47% Analysis Date = 10/23/21 Pct Recovery = 47% Analysis Date = 10/18/21 Pct Recovery = 47% Analysis Date = 10/18/21 Pct Recovery = 47% Analysis Date = 10/14/21 Pct Recovery = 47% Analysis Date = 10/14/21 Pct Recovery = 47% Analysis Date = 10/10/21 Pct Recovery = 47% Analysis Date = 10/10/21 Pct Recovery = 47% Analysis Date = 10/05/21 Pct Recovery = 47% Analysis Date = 10/05/21 Pct Recovery = 47% Analysis Date = 10/01/21 Pct Recovery = 47% Analysis Date = 10/01/21 Pct Recovery = 47% Analysis Date = 09/27/21 Pct Recovery = 47% Analysis Date = 09/27/21 Pct Recovery = 47% Analysis Date = 09/22/21 Pct Recovery = 47% Analysis Date = 09/22/21 Pct Recovery = 47% Analysis Date = 09/18/21 Pct Recovery = 47% Analysis Date = 09/18/21 Pct Recovery = 47% Analysis Date = 09/14/21 Pct Recovery = 46% Analysis Date = 09/14/21 Pct Recovery = 46% Analysis Date = 09/09/21 Pct Recovery = 46% Analysis Date = 09/09/21 Pct Recovery = 46% Analysis Date = 09/05/21 Pct Recovery = 46% Analysis Date = 09/05/21 Pct Recovery = 46% Analysis Date = 09/01/21 Pct Recovery = 46% Analysis Date = 09/01/21 Pct Recovery = 46% Analysis Date = 08/28/21 Pct Recovery = 46% Analysis Date = 08/28/21 Pct Recovery = 46% Analysis Date = 08/23/21 Pct Recovery = 46% Analysis Date = 08/23/21 Pct Recovery = 46% Analysis Date = 08/19/21 Pct Recovery = 46% Analysis Date = 08/19/21 Pct Recovery = 46% Analysis Date = 08/15/21 Pct Recovery = 46% Analysis Date = 08/15/21 Pct Recovery = 46% Analysis Date = 08/10/21 Pct Recovery = 46% Analysis Date = 08/10/21 Pct Recovery = 46% Analysis Date = 08/06/21 Pct Recovery = 46% Analysis Date = 08/06/21 Pct Recovery = 46% Analysis Date = 08/02/21 Pct Recovery = 46% Analysis Date = 08/02/21 Pct Recovery = 46% Analysis Date = 07/28/21 Pct Recovery = 46% Analysis Date = 07/28/21 Pct Recovery = 46% Analysis Date = 07/24/21 Pct Recovery = 46% Analysis Date = 07/24/21 Pct Recovery = 46% Analysis Date = 07/20/21 Pct Recovery = 46% Analysis Date = 07/20/21 Pct Recovery = 46% Analysis Date = 07/15/21 Pct Recovery = 45% Analysis Date = 07/15/21 Pct Recovery = 45% Analysis Date = 07/11/21 Pct Recovery = 45% Analysis Date = 07/11/21 Pct Recovery = 45% Analysis Date = 07/07/21 Pct Recovery = 45% Analysis Date = 07/07/21 Pct Recovery = 45% Analysis Date = 07/02/21 Pct Recovery = 45% Analysis Date = 07/02/21 Pct Recovery = 45% Analysis Date = 06/28/21 Pct Recovery = 45% Analysis Date = 06/28/21 Pct Recovery = 45% Analysis Date = 06/24/21 Pct Recovery = 45% Analysis Date = 06/24/21 Pct Recovery = 45% Analysis Date = 06/19/21 Pct Recovery = 45% Analysis Date = 06/19/21 Pct Recovery = 45% Analysis Date = 06/15/21 Pct Recovery = 45% Analysis Date = 06/15/21 Pct Recovery = 45% Analysis Date = 06/11/21 Pct Recovery = 45% Analysis Date = 06/11/21 Pct Recovery = 45% Analysis Date = 06/07/21 Pct Recovery = 45% Analysis Date = 06/07/21 Pct Recovery = 45% Analysis Date = 06/02/21 Pct Recovery = 45% Analysis Date = 06/02/21 Pct Recovery = 45% Analysis Date = 05/29/21 Pct Recovery = 45% Analysis Date = 05/29/21 Pct Recovery = 45% Analysis Date = 05/25/21 Pct Recovery = 45% Analysis Date = 05/25/21 Pct Recovery = 45% Analysis Date = 05/20/21 Pct Recovery = 45% Analysis Date = 05/20/21 Pct Recovery = 45% Analysis Date = 05/16/21 Pct Recovery = 44% Analysis Date = 05/16/21 Pct Recovery = 44% Analysis Date = 05/12/21 Pct Recovery = 44% Analysis Date = 05/12/21 Pct Recovery = 44% Analysis Date = 05/07/21 Pct Recovery = 44% Analysis Date = 05/07/21 Pct Recovery = 44% Analysis Date = 05/03/21 Pct Recovery = 44% Analysis Date = 05/03/21 Pct Recovery = 44% Analysis Date = 04/29/21 Pct Recovery = 44% Analysis Date = 04/29/21 Pct Recovery = 44% Analysis Date = 04/24/21 Pct Recovery = 44% Analysis Date = 04/24/21 Pct Recovery = 44% Analysis Date = 04/20/21 Pct Recovery = 44% Analysis Date = 04/20/21 Pct Recovery = 44% Analysis Date = 04/16/21 Pct Recovery = 44% Analysis Date = 04/16/21 Pct Recovery = 44% Analysis Date = 04/11/21 Pct Recovery = 44% Analysis Date = 04/11/21 Pct Recovery = 44% Analysis Date = 04/07/21 Pct Recovery = 44% Analysis Date = 04/07/21 Pct Recovery = 44% Analysis Date = 04/03/21 Pct Recovery = 44% Analysis Date = 04/03/21 Pct Recovery = 44% Analysis Date = 03/29/21 Pct Recovery = 44% Analysis Date = 03/29/21 Pct Recovery = 44% Analysis Date = 03/25/21 Pct Recovery = 44% Analysis Date = 03/25/21 Pct Recovery = 44% Analysis Date = 03/21/21 Pct Recovery = 44% Analysis Date = 03/21/21 Pct Recovery = 44% Analysis Date = 03/17/21 Pct Recovery = 43% Analysis Date = 03/17/21 Pct Recovery = 43% Analysis Date = 03/12/21 Pct Recovery = 43% Analysis Date = 03/12/21 Pct Recovery = 43% Analysis Date = 03/08/21 Pct Recovery = 43% Analysis Date = 03/08/21 Pct Recovery = 43% Analysis Date = 03/04/21 Pct Recovery = 43% Analysis Date = 03/04/21 Pct Recovery = 43% Analysis Date = 02/27/21 Pct Recovery = 43% Analysis Date = 02/27/21 Pct Recovery = 43% Analysis Date = 02/23/21 Pct Recovery = 43% Analysis Date = 02/23/21 Pct Recovery = 43% Analysis Date = 02/19/21 Pct Recovery = 43% Analysis Date = 02/19/21 Pct Recovery = 43% Analysis Date = 02/14/21 Pct Recovery = 43% Analysis Date = 02/14/21 Pct Recovery = 43% Analysis Date = 02/10/21 Pct Recovery = 44% Analysis Date = 02/10/21 Pct Recovery = 44% Analysis Date = 02/06/21 Pct Recovery = 44% Analysis Date = 02/06/21 Pct Recovery = 44% Analysis Date = 02/01/21 Pct Recovery = 45% Analysis Date = 02/01/21 Pct Recovery = 45% Analysis Date = 01/28/21 Pct Recovery = 45% Analysis Date = 01/28/21 Pct Recovery = 45% Analysis Date = 01/24/21 Pct Recovery = 46% Analysis Date = 01/24/21 Pct Recovery = 46% Analysis Date = 01/19/21 Pct Recovery = 46% Analysis Date = 01/19/21 Pct Recovery = 46% Analysis Date = 01/15/21 Pct Recovery = 47% Analysis Date = 01/15/21 Pct Recovery = 47% Analysis Date = 01/11/21 Pct Recovery = 47% Analysis Date = 01/11/21 Pct Recovery = 47% Analysis Date = 01/07/21 Pct Recovery = 47% Analysis Date = 01/07/21 Pct Recovery = 47% Analysis Date = 01/02/21 Pct Recovery = 48% Analysis Date = 01/02/21 Pct Recovery = 48% Analysis Date = 12/29/20 Pct Recovery = 48% Analysis Date = 12/29/20 Pct Recovery = 48% Analysis Date = 12/25/20 Pct Recovery = 49% Analysis Date = 12/25/20 Pct Recovery = 49% Analysis Date = 12/20/20 Pct Recovery = 49% Analysis Date = 12/20/20 Pct Recovery = 49% Analysis Date = 12/16/20 Pct Recovery = 50% Analysis Date = 12/16/20 Pct Recovery = 50% Analysis Date = 12/12/20 Pct Recovery = 50% Analysis Date = 12/12/20 Pct Recovery = 50% Analysis Date = 12/07/20 Pct Recovery = 51% Analysis Date = 12/07/20 Pct Recovery = 51% Analysis Date = 12/03/20 Pct Recovery = 51% Analysis Date = 12/03/20 Pct Recovery = 51% Analysis Date = 11/29/20 Pct Recovery = 52% Analysis Date = 11/29/20 Pct Recovery = 52% Analysis Date = 11/24/20 Pct Recovery = 52% Analysis Date = 11/24/20 Pct Recovery = 52% Analysis Date = 11/20/20 Pct Recovery = 52% Analysis Date = 11/20/20 Pct Recovery = 52% Analysis Date = 11/16/20 Pct Recovery = 53% Analysis Date = 11/16/20 Pct Recovery = 53% Analysis Date = 11/11/20 Pct Recovery = 53% Analysis Date = 11/11/20 Pct Recovery = 53% Analysis Date = 11/07/20 Pct Recovery = 53% Analysis Date = 11/07/20 Pct Recovery = 53% Analysis Date = 11/03/20 Pct Recovery = 54% Analysis Date = 11/03/20 Pct Recovery = 54% Analysis Date = 10/29/20 Pct Recovery = 54% Analysis Date = 10/29/20 Pct Recovery = 54% Analysis Date = 10/25/20 Pct Recovery = 54% Analysis Date = 10/25/20 Pct Recovery = 54% Analysis Date = 10/21/20 Pct Recovery = 55% Analysis Date = 10/21/20 Pct Recovery = 55% Analysis Date = 10/17/20 Pct Recovery = 55% Analysis Date = 10/17/20 Pct Recovery = 55% Analysis Date = 10/12/20 Pct Recovery = 55% Analysis Date = 10/12/20 Pct Recovery = 55% Analysis Date = 10/08/20 Pct Recovery = 56% Analysis Date = 10/08/20 Pct Recovery = 56% Analysis Date = 10/04/20 Pct Recovery = 56% Analysis Date = 10/04/20 Pct Recovery = 56% Analysis Date = 09/29/20 Pct Recovery = 56% Analysis Date = 09/29/20 Pct Recovery = 56% Analysis Date = 09/25/20 Pct Recovery = 57% Analysis Date = 09/25/20 Pct Recovery = 57% Analysis Date = 09/21/20 Pct Recovery = 57% Analysis Date = 09/21/20 Pct Recovery = 57% Analysis Date = 09/16/20 Pct Recovery = 58% Analysis Date = 09/16/20 Pct Recovery = 58% Analysis Date = 09/12/20 Pct Recovery = 58% Analysis Date = 09/12/20 Pct Recovery = 58% Analysis Date = 09/08/20 Pct Recovery = 58% Analysis Date = 09/08/20 Pct Recovery = 58% Analysis Date = 09/03/20 Pct Recovery = 59% Analysis Date = 09/03/20 Pct Recovery = 59% Analysis Date = 08/30/20 Pct Recovery = 59% Analysis Date = 08/30/20 Pct Recovery = 59% Analysis Date = 08/26/20 Pct Recovery = 60% Analysis Date = 08/26/20 Pct Recovery = 60% Analysis Date = 08/21/20 Pct Recovery = 60% Analysis Date = 08/21/20 Pct Recovery = 60% Analysis Date = 08/17/20 Pct Recovery = 61% Analysis Date = 08/17/20 Pct Recovery = 61% Analysis Date = 08/13/20 Pct Recovery = 61% Analysis Date = 08/13/20 Pct Recovery = 61% Analysis Date = 08/08/20 Pct Recovery = 61% Analysis Date = 08/08/20 Pct Recovery = 61% Analysis Date = 08/04/20 Pct Recovery = 62% Analysis Date = 08/04/20 Pct Recovery = 62% Analysis Date = 07/31/20 Pct Recovery = 62% Analysis Date = 07/31/20 Pct Recovery = 62% Analysis Date = 07/27/20 Pct Recovery = 63% Analysis Date = 07/27/20 Pct Recovery = 63% Analysis Date = 07/22/20 Pct Recovery = 63% Analysis Date = 07/22/20 Pct Recovery = 63% Analysis Date = 07/18/20 Pct Recovery = 64% Analysis Date = 07/18/20 Pct Recovery = 64% Analysis Date = 07/14/20 Pct Recovery = 64% Analysis Date = 07/14/20 Pct Recovery = 64% Analysis Date = 07/09/20 Pct Recovery = 65% Analysis Date = 07/09/20 Pct Recovery = 65% Analysis Date = 07/05/20 Pct Recovery = 65% Analysis Date = 07/05/20 Pct Recovery = 65% Analysis Date = 07/01/20 Pct Recovery = 65% Analysis Date = 07/01/20 Pct Recovery = 65% Analysis Date = 06/26/20 Pct Recovery = 66% Analysis Date = 06/26/20 Pct Recovery = 66% Analysis Date = 06/22/20 Pct Recovery = 66% Analysis Date = 06/22/20 Pct Recovery = 66% Analysis Date = 06/18/20 Pct Recovery = 67% Analysis Date = 06/18/20 Pct Recovery = 67% Analysis Date = 06/13/20 Pct Recovery = 67% Analysis Date = 06/13/20 Pct Recovery = 67% Analysis Date = 06/09/20 Pct Recovery = 67% Analysis Date = 06/09/20 Pct Recovery = 67% Analysis Date = 06/05/20 Pct Recovery = 68% Analysis Date = 06/05/20 Pct Recovery = 68% Analysis Date = 05/31/20 Pct Recovery = 68% Analysis Date = 05/31/20 Pct Recovery = 68% Analysis Date = 05/27/20 Pct Recovery = 68% Analysis Date = 05/27/20 Pct Recovery = 68% Analysis Date = 05/23/20 Pct Recovery = 69% Analysis Date = 05/23/20 Pct Recovery = 69% Analysis Date = 05/19/20 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-PERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 54% 20% 53% 17%
Total 34 54% 20% 53% 17%

Sample Statistics
CIS-PERMETHRIN

Characteristic N % % Basis
Plotted 34 89% Spiked
Estimated Values 7 18% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 5% Spiked
Spiked 38 .  
False Negatives 2 5% 2 out of 38
Not Spiked 78 .  
False Positives 0 0% 0 out of 78

OBSP Determination:
DECHLOROMETOLACHLOR
METHOD: 2447 , TESTIDCODE: 68562LCM60

Laboratory ID = 20202110006 Lab Value = 22.695 Expected Conc. = 25.4 Report level label = 2 Pct Recovery = 89% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20202590106 Lab Value = 21.358 Expected Conc. = 25 Report level label = 2 Pct Recovery = 85% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 21.978 Expected Conc. = 25 Report level label = 2 Pct Recovery = 88% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201820155 Lab Value = 15.024 Expected Conc. = 24.6 Report level label = 2 Pct Recovery = 61% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20201680155 Lab Value = 13.084 Expected Conc. = 12.7 Report level label = 2 Pct Recovery = 103% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20203230018 Lab Value = 12.844 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 103% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 9.529 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 76% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 9.994 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 80% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 7.202 Expected Conc. = 12.3 Report level label = 2 Pct Recovery = 59% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 8.465 Expected Conc. = 12.3 Report level label = 2 Pct Recovery = 69% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 9.587 Expected Conc. = 12.3 Report level label = 2 Pct Recovery = 78% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201610160 Lab Value = 5.124 Expected Conc. = 5.08 Report level label = 2 Pct Recovery = 101% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210970035 Lab Value = 4.421 Expected Conc. = 5 Report level label = 2 Pct Recovery = 88% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 4.598 Expected Conc. = 5 Report level label = 2 Pct Recovery = 92% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 6.257 Expected Conc. = 5 Report level label = 2 Pct Recovery = 125% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 4.769 Expected Conc. = 5 Report level label = 2 Pct Recovery = 95% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 4.008 Expected Conc. = 5 Report level label = 2 Pct Recovery = 80% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202040027 Lab Value = 3.717 Expected Conc. = 4.92 Report level label = 2 Pct Recovery = 76% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 3.706 Expected Conc. = 4.92 Report level label = 2 Pct Recovery = 75% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 4.342 Expected Conc. = 4.92 Report level label = 2 Pct Recovery = 88% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Analysis Date = 04/14/21 Pct Recovery = 91% Analysis Date = 04/12/21 Pct Recovery = 92% Analysis Date = 04/12/21 Pct Recovery = 92% Analysis Date = 04/10/21 Pct Recovery = 92% Analysis Date = 04/10/21 Pct Recovery = 92% Analysis Date = 04/09/21 Pct Recovery = 92% Analysis Date = 04/09/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 92% Analysis Date = 04/05/21 Pct Recovery = 92% Analysis Date = 04/05/21 Pct Recovery = 92% Analysis Date = 04/04/21 Pct Recovery = 92% Analysis Date = 04/04/21 Pct Recovery = 92% Analysis Date = 04/02/21 Pct Recovery = 92% Analysis Date = 04/02/21 Pct Recovery = 92% Analysis Date = 03/31/21 Pct Recovery = 92% Analysis Date = 03/31/21 Pct Recovery = 92% Analysis Date = 03/30/21 Pct Recovery = 92% Analysis Date = 03/30/21 Pct Recovery = 92% Analysis Date = 03/28/21 Pct Recovery = 92% Analysis Date = 03/28/21 Pct Recovery = 92% Analysis Date = 03/26/21 Pct Recovery = 92% Analysis Date = 03/26/21 Pct Recovery = 92% Analysis Date = 03/25/21 Pct Recovery = 92% Analysis Date = 03/25/21 Pct Recovery = 92% Analysis Date = 03/23/21 Pct Recovery = 92% Analysis Date = 03/23/21 Pct Recovery = 92% Analysis Date = 03/21/21 Pct Recovery = 92% Analysis Date = 03/21/21 Pct Recovery = 92% Analysis Date = 03/20/21 Pct Recovery = 92% Analysis Date = 03/20/21 Pct Recovery = 92% Analysis Date = 03/18/21 Pct Recovery = 92% Analysis Date = 03/18/21 Pct Recovery = 92% Analysis Date = 03/16/21 Pct Recovery = 92% Analysis Date = 03/16/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/12/21 Pct Recovery = 93% Analysis Date = 03/12/21 Pct Recovery = 93% Analysis Date = 03/10/21 Pct Recovery = 93% Analysis Date = 03/10/21 Pct Recovery = 93% Analysis Date = 03/08/21 Pct Recovery = 93% Analysis Date = 03/08/21 Pct Recovery = 93% Analysis Date = 03/07/21 Pct Recovery = 93% Analysis Date = 03/07/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 93% Analysis Date = 03/02/21 Pct Recovery = 93% Analysis Date = 03/02/21 Pct Recovery = 93% Analysis Date = 02/28/21 Pct Recovery = 93% Analysis Date = 02/28/21 Pct Recovery = 93% Analysis Date = 02/26/21 Pct Recovery = 93% Analysis Date = 02/26/21 Pct Recovery = 93% Analysis Date = 02/25/21 Pct Recovery = 93% Analysis Date = 02/25/21 Pct Recovery = 93% Analysis Date = 02/23/21 Pct Recovery = 93% Analysis Date = 02/23/21 Pct Recovery = 93% Analysis Date = 02/21/21 Pct Recovery = 93% Analysis Date = 02/21/21 Pct Recovery = 93% Analysis Date = 02/20/21 Pct Recovery = 93% Analysis Date = 02/20/21 Pct Recovery = 93% Analysis Date = 02/18/21 Pct Recovery = 93% Analysis Date = 02/18/21 Pct Recovery = 93% Analysis Date = 02/16/21 Pct Recovery = 93% Analysis Date = 02/16/21 Pct Recovery = 93% Analysis Date = 02/15/21 Pct Recovery = 93% Analysis Date = 02/15/21 Pct Recovery = 93% Analysis Date = 02/13/21 Pct Recovery = 93% Analysis Date = 02/13/21 Pct Recovery = 93% Analysis Date = 02/11/21 Pct Recovery = 94% Analysis Date = 02/11/21 Pct Recovery = 94% Analysis Date = 02/10/21 Pct Recovery = 94% Analysis Date = 02/10/21 Pct Recovery = 94% Analysis Date = 02/08/21 Pct Recovery = 94% Analysis Date = 02/08/21 Pct Recovery = 94% Analysis Date = 02/07/21 Pct Recovery = 94% Analysis Date = 02/07/21 Pct Recovery = 94% Analysis Date = 02/05/21 Pct Recovery = 94% Analysis Date = 02/05/21 Pct Recovery = 94% Analysis Date = 02/03/21 Pct Recovery = 94% Analysis Date = 02/03/21 Pct Recovery = 94% Analysis Date = 02/02/21 Pct Recovery = 94% Analysis Date = 02/02/21 Pct Recovery = 94% Analysis Date = 01/31/21 Pct Recovery = 94% Analysis Date = 01/31/21 Pct Recovery = 94% Analysis Date = 01/29/21 Pct Recovery = 94% Analysis Date = 01/29/21 Pct Recovery = 94% Analysis Date = 01/28/21 Pct Recovery = 94% Analysis Date = 01/28/21 Pct Recovery = 94% Analysis Date = 01/26/21 Pct Recovery = 94% Analysis Date = 01/26/21 Pct Recovery = 94% Analysis Date = 01/24/21 Pct Recovery = 94% Analysis Date = 01/24/21 Pct Recovery = 94% Analysis Date = 01/23/21 Pct Recovery = 94% Analysis Date = 01/23/21 Pct Recovery = 94% Analysis Date = 01/21/21 Pct Recovery = 94% Analysis Date = 01/21/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/18/21 Pct Recovery = 94% Analysis Date = 01/18/21 Pct Recovery = 94% Analysis Date = 01/16/21 Pct Recovery = 94% Analysis Date = 01/16/21 Pct Recovery = 94% Analysis Date = 01/14/21 Pct Recovery = 94% Analysis Date = 01/14/21 Pct Recovery = 94% Analysis Date = 01/13/21 Pct Recovery = 95% Analysis Date = 01/13/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 95% Analysis Date = 01/09/21 Pct Recovery = 95% Analysis Date = 01/09/21 Pct Recovery = 95% Analysis Date = 01/08/21 Pct Recovery = 95% Analysis Date = 01/08/21 Pct Recovery = 95% Analysis Date = 01/06/21 Pct Recovery = 95% Analysis Date = 01/06/21 Pct Recovery = 95% Analysis Date = 01/05/21 Pct Recovery = 95% Analysis Date = 01/05/21 Pct Recovery = 95% Analysis Date = 01/03/21 Pct Recovery = 95% Analysis Date = 01/03/21 Pct Recovery = 95% Analysis Date = 01/01/21 Pct Recovery = 95% Analysis Date = 01/01/21 Pct Recovery = 95% Analysis Date = 12/31/20 Pct Recovery = 95% Analysis Date = 12/31/20 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/27/20 Pct Recovery = 95% Analysis Date = 12/27/20 Pct Recovery = 95% Analysis Date = 12/26/20 Pct Recovery = 95% Analysis Date = 12/26/20 Pct Recovery = 95% Analysis Date = 12/24/20 Pct Recovery = 95% Analysis Date = 12/24/20 Pct Recovery = 95% Analysis Date = 12/22/20 Pct Recovery = 95% Analysis Date = 12/22/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/19/20 Pct Recovery = 95% Analysis Date = 12/19/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/16/20 Pct Recovery = 95% Analysis Date = 12/16/20 Pct Recovery = 95% Analysis Date = 12/14/20 Pct Recovery = 95% Analysis Date = 12/14/20 Pct Recovery = 95% Analysis Date = 12/12/20 Pct Recovery = 94% Analysis Date = 12/12/20 Pct Recovery = 94% Analysis Date = 12/11/20 Pct Recovery = 94% Analysis Date = 12/11/20 Pct Recovery = 94% Analysis Date = 12/09/20 Pct Recovery = 94% Analysis Date = 12/09/20 Pct Recovery = 94% Analysis Date = 12/07/20 Pct Recovery = 94% Analysis Date = 12/07/20 Pct Recovery = 94% Analysis Date = 12/06/20 Pct Recovery = 94% Analysis Date = 12/06/20 Pct Recovery = 94% Analysis Date = 12/04/20 Pct Recovery = 93% Analysis Date = 12/04/20 Pct Recovery = 93% Analysis Date = 12/03/20 Pct Recovery = 93% Analysis Date = 12/03/20 Pct Recovery = 93% Analysis Date = 12/01/20 Pct Recovery = 93% Analysis Date = 12/01/20 Pct Recovery = 93% Analysis Date = 11/29/20 Pct Recovery = 93% Analysis Date = 11/29/20 Pct Recovery = 93% Analysis Date = 11/28/20 Pct Recovery = 92% Analysis Date = 11/28/20 Pct Recovery = 92% Analysis Date = 11/26/20 Pct Recovery = 92% Analysis Date = 11/26/20 Pct Recovery = 92% Analysis Date = 11/24/20 Pct Recovery = 92% Analysis Date = 11/24/20 Pct Recovery = 92% Analysis Date = 11/23/20 Pct Recovery = 92% Analysis Date = 11/23/20 Pct Recovery = 92% Analysis Date = 11/21/20 Pct Recovery = 91% Analysis Date = 11/21/20 Pct Recovery = 91% Analysis Date = 11/19/20 Pct Recovery = 91% Analysis Date = 11/19/20 Pct Recovery = 91% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/16/20 Pct Recovery = 91% Analysis Date = 11/16/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/13/20 Pct Recovery = 90% Analysis Date = 11/13/20 Pct Recovery = 90% Analysis Date = 11/11/20 Pct Recovery = 90% Analysis Date = 11/11/20 Pct Recovery = 90% Analysis Date = 11/09/20 Pct Recovery = 90% Analysis Date = 11/09/20 Pct Recovery = 90% Analysis Date = 11/08/20 Pct Recovery = 90% Analysis Date = 11/08/20 Pct Recovery = 90% Analysis Date = 11/06/20 Pct Recovery = 89% Analysis Date = 11/06/20 Pct Recovery = 89% Analysis Date = 11/04/20 Pct Recovery = 89% Analysis Date = 11/04/20 Pct Recovery = 89% Analysis Date = 11/03/20 Pct Recovery = 89% Analysis Date = 11/03/20 Pct Recovery = 89% Analysis Date = 11/01/20 Pct Recovery = 89% Analysis Date = 11/01/20 Pct Recovery = 89% Analysis Date = 10/31/20 Pct Recovery = 88% Analysis Date = 10/31/20 Pct Recovery = 88% Analysis Date = 10/29/20 Pct Recovery = 88% Analysis Date = 10/29/20 Pct Recovery = 88% Analysis Date = 10/27/20 Pct Recovery = 88% Analysis Date = 10/27/20 Pct Recovery = 88% Analysis Date = 10/26/20 Pct Recovery = 88% Analysis Date = 10/26/20 Pct Recovery = 88% Analysis Date = 10/24/20 Pct Recovery = 88% Analysis Date = 10/24/20 Pct Recovery = 88% Analysis Date = 10/22/20 Pct Recovery = 87% Analysis Date = 10/22/20 Pct Recovery = 87% Analysis Date = 10/21/20 Pct Recovery = 87% Analysis Date = 10/21/20 Pct Recovery = 87% Analysis Date = 10/19/20 Pct Recovery = 87% Analysis Date = 10/19/20 Pct Recovery = 87% Analysis Date = 10/17/20 Pct Recovery = 87% Analysis Date = 10/17/20 Pct Recovery = 87% Analysis Date = 10/16/20 Pct Recovery = 86% Analysis Date = 10/16/20 Pct Recovery = 86% Analysis Date = 10/14/20 Pct Recovery = 86% Analysis Date = 10/14/20 Pct Recovery = 86% Analysis Date = 10/12/20 Pct Recovery = 86% Analysis Date = 10/12/20 Pct Recovery = 86% Analysis Date = 10/11/20 Pct Recovery = 85% Analysis Date = 10/11/20 Pct Recovery = 85% Analysis Date = 10/09/20 Pct Recovery = 85% Analysis Date = 10/09/20 Pct Recovery = 85% Analysis Date = 10/07/20 Pct Recovery = 84% Analysis Date = 10/07/20 Pct Recovery = 84% Analysis Date = 10/06/20 Pct Recovery = 84% Analysis Date = 10/06/20 Pct Recovery = 84% Analysis Date = 10/04/20 Pct Recovery = 83% Analysis Date = 10/04/20 Pct Recovery = 83% Analysis Date = 10/02/20 Pct Recovery = 83% Analysis Date = 10/02/20 Pct Recovery = 83% Analysis Date = 10/01/20 Pct Recovery = 82% Analysis Date = 10/01/20 Pct Recovery = 82% Analysis Date = 09/29/20 Pct Recovery = 82% Analysis Date = 09/29/20 Pct Recovery = 82% Analysis Date = 09/28/20 Pct Recovery = 82% Analysis Date = 09/28/20 Pct Recovery = 82% Analysis Date = 09/26/20 Pct Recovery = 81% Analysis Date = 09/26/20 Pct Recovery = 81% Analysis Date = 09/24/20 Pct Recovery = 81% Analysis Date = 09/24/20 Pct Recovery = 81% Analysis Date = 09/23/20 Pct Recovery = 80% Analysis Date = 09/23/20 Pct Recovery = 80% Analysis Date = 09/21/20 Pct Recovery = 80% Analysis Date = 09/21/20 Pct Recovery = 80% Analysis Date = 09/19/20 Pct Recovery = 79% Analysis Date = 09/19/20 Pct Recovery = 79% Analysis Date = 09/18/20 Pct Recovery = 79% Analysis Date = 09/18/20 Pct Recovery = 79% Analysis Date = 09/16/20 Pct Recovery = 78% Analysis Date = 09/16/20 Pct Recovery = 78% Analysis Date = 09/14/20 Pct Recovery = 78% Analysis Date = 09/14/20 Pct Recovery = 78% Analysis Date = 09/13/20 Pct Recovery = 78% Analysis Date = 09/13/20 Pct Recovery = 78% Analysis Date = 09/11/20 Pct Recovery = 78% Analysis Date = 09/11/20 Pct Recovery = 78% Analysis Date = 09/09/20 Pct Recovery = 78% Analysis Date = 09/09/20 Pct Recovery = 78% Analysis Date = 09/08/20 Pct Recovery = 78% Analysis Date = 09/08/20 Pct Recovery = 78% Analysis Date = 09/06/20 Pct Recovery = 78% Analysis Date = 09/06/20 Pct Recovery = 78% Analysis Date = 09/04/20 Pct Recovery = 78% Analysis Date = 09/04/20 Pct Recovery = 78% Analysis Date = 09/03/20 Pct Recovery = 78% Analysis Date = 09/03/20 Pct Recovery = 78% Analysis Date = 09/01/20 Pct Recovery = 78% Analysis Date = 09/01/20 Pct Recovery = 78% Analysis Date = 08/30/20 Pct Recovery = 78% Analysis Date = 08/30/20 Pct Recovery = 78% Analysis Date = 08/29/20 Pct Recovery = 78% Analysis Date = 08/29/20 Pct Recovery = 78% Analysis Date = 08/27/20 Pct Recovery = 78% Analysis Date = 08/27/20 Pct Recovery = 78% Analysis Date = 08/26/20 Pct Recovery = 78% Analysis Date = 08/26/20 Pct Recovery = 78% Analysis Date = 08/24/20 Pct Recovery = 78% Analysis Date = 08/24/20 Pct Recovery = 78% Analysis Date = 08/22/20 Pct Recovery = 78% Analysis Date = 08/22/20 Pct Recovery = 78% Analysis Date = 08/21/20 Pct Recovery = 78% Analysis Date = 08/21/20 Pct Recovery = 78% Analysis Date = 08/19/20 Pct Recovery = 78% Analysis Date = 08/19/20 Pct Recovery = 78% Analysis Date = 08/17/20 Pct Recovery = 78% Analysis Date = 08/17/20 Pct Recovery = 78% Analysis Date = 08/16/20 Pct Recovery = 78% Analysis Date = 08/16/20 Pct Recovery = 78% Analysis Date = 08/14/20 Pct Recovery = 78% Analysis Date = 08/14/20 Pct Recovery = 78% Analysis Date = 08/12/20 Pct Recovery = 78% Analysis Date = 08/12/20 Pct Recovery = 78% Analysis Date = 08/11/20 Pct Recovery = 78% Analysis Date = 08/11/20 Pct Recovery = 78% Analysis Date = 08/09/20 Pct Recovery = 78% Analysis Date = 08/09/20 Pct Recovery = 78% Analysis Date = 08/07/20 Pct Recovery = 78% Analysis Date = 08/07/20 Pct Recovery = 78% Analysis Date = 08/06/20 Pct Recovery = 78% Analysis Date = 08/06/20 Pct Recovery = 78% Analysis Date = 08/04/20 Pct Recovery = 78% Analysis Date = 08/04/20 Pct Recovery = 78% Analysis Date = 08/02/20 Pct Recovery = 78% Analysis Date = 08/02/20 Pct Recovery = 78% Analysis Date = 08/01/20 Pct Recovery = 79% Analysis Date = 08/01/20 Pct Recovery = 79% Analysis Date = 07/30/20 Pct Recovery = 79% Analysis Date = 07/30/20 Pct Recovery = 79% Analysis Date = 07/28/20 Pct Recovery = 79% Analysis Date = 07/28/20 Pct Recovery = 79% Analysis Date = 07/27/20 Pct Recovery = 80% Analysis Date = 07/27/20 Pct Recovery = 80% Analysis Date = 07/25/20 Pct Recovery = 80% Analysis Date = 07/25/20 Pct Recovery = 80% Analysis Date = 07/24/20 Pct Recovery = 80% Analysis Date = 07/24/20 Pct Recovery = 80% Analysis Date = 07/22/20 Pct Recovery = 81% Analysis Date = 07/22/20 Pct Recovery = 81% Analysis Date = 07/20/20 Pct Recovery = 81% Analysis Date = 07/20/20 Pct Recovery = 81% Analysis Date = 07/19/20 Pct Recovery = 81% Analysis Date = 07/19/20 Pct Recovery = 81% Analysis Date = 07/17/20 Pct Recovery = 81% Analysis Date = 07/17/20 Pct Recovery = 81% Analysis Date = 07/15/20 Pct Recovery = 82% Analysis Date = 07/15/20 Pct Recovery = 82% Analysis Date = 07/14/20 Pct Recovery = 82% Analysis Date = 07/14/20 Pct Recovery = 82% Analysis Date = 07/12/20 Pct Recovery = 82% Analysis Date = 07/12/20 Pct Recovery = 82% Analysis Date = 07/10/20 Pct Recovery = 83% Analysis Date = 07/10/20 Pct Recovery = 83% Analysis Date = 07/09/20 Pct Recovery = 83% Analysis Date = 07/09/20 Pct Recovery = 83% Analysis Date = 07/07/20 Pct Recovery = 83% Analysis Date = 07/07/20 Pct Recovery = 83% Analysis Date = 07/05/20 Pct Recovery = 83% Analysis Date = 07/05/20 Pct Recovery = 83% Analysis Date = 07/04/20 Pct Recovery = 84% Analysis Date = 07/04/20 Pct Recovery = 84% Analysis Date = 07/02/20 Pct Recovery = 84% Analysis Date = 07/02/20 Pct Recovery = 84% Analysis Date = 06/30/20 Pct Recovery = 84% Analysis Date = 06/30/20 Pct Recovery = 84% Analysis Date = 06/29/20 Pct Recovery = 84% Analysis Date = 06/29/20 Pct Recovery = 84% Analysis Date = 06/27/20 Pct Recovery = 84% Analysis Date = 06/27/20 Pct Recovery = 84% Analysis Date = 06/25/20 Pct Recovery = 84% Analysis Date = 06/25/20 Pct Recovery = 84% Analysis Date = 06/24/20 Pct Recovery = 85% Analysis Date = 06/24/20 Pct Recovery = 85% Analysis Date = 06/22/20 Pct Recovery = 85% Analysis Date = 06/22/20 Pct Recovery = 85% Analysis Date = 06/21/20 Pct Recovery = 85% Analysis Date = 06/21/20 Pct Recovery = 85% Analysis Date = 06/19/20 Pct Recovery = 85% Analysis Date = 06/19/20 Pct Recovery = 85% Analysis Date = 06/17/20 Pct Recovery = 85% Analysis Date = 06/17/20 Pct Recovery = 85% Analysis Date = 06/16/20 Pct Recovery = 86% Analysis Date = 06/16/20 Pct Recovery = 86% Analysis Date = 06/14/20 Pct Recovery = 86% Analysis Date = 06/14/20 Pct Recovery = 86% Analysis Date = 06/12/20 Pct Recovery = 86% Analysis Date = 06/12/20 Pct Recovery = 86% Analysis Date = 06/11/20 Pct Recovery = 86% Analysis Date = 06/11/20 Pct Recovery = 86% Analysis Date = 06/09/20 Pct Recovery = 86% Analysis Date = 06/09/20 Pct Recovery = 86% Analysis Date = 06/07/20 Pct Recovery = 86% Analysis Date = 06/07/20 Pct Recovery = 86% Analysis Date = 06/06/20 Pct Recovery = 87% Analysis Date = 06/06/20 Pct Recovery = 87% Analysis Date = 06/04/20 Pct Recovery = 87% Analysis Date = 06/04/20 Pct Recovery = 87% Analysis Date = 06/02/20 Pct Recovery = 87% Analysis Date = 06/02/20 Pct Recovery = 87% Analysis Date = 06/01/20 Pct Recovery = 87% Analysis Date = 06/01/20 Pct Recovery = 87% Analysis Date = 05/30/20 Pct Recovery = 87% Analysis Date = 05/30/20 Pct Recovery = 87% Analysis Date = 05/28/20 Pct Recovery = 88% Analysis Date = 05/28/20 Pct Recovery = 88% Analysis Date = 05/27/20 Pct Recovery = 88% Analysis Date = 05/27/20 Pct Recovery = 88% Analysis Date = 05/25/20 Pct Recovery = 88% Analysis Date = 05/25/20 Pct Recovery = 88% Analysis Date = 05/23/20 Pct Recovery = 88% Analysis Date = 05/23/20 Pct Recovery = 88% Analysis Date = 05/22/20 Pct Recovery = 88% Analysis Date = 05/22/20 Pct Recovery = 88% Analysis Date = 05/20/20 Pct Recovery = 89% Analysis Date = 05/20/20 Pct Recovery = 89% Analysis Date = 05/19/20 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DECHLOROMETOLACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 86% 16% 87% 13%
Total 20 86% 16% 87% 13%

Sample Statistics
DECHLOROMETOLACHLOR

Characteristic N % % Basis
Plotted 20 91% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 22 .  
False Negatives 2 9% 2 out of 22
Not Spiked 94 .  
False Positives 0 0% 0 out of 94

OBSP Determination:
DEETHYLATRAZINE
METHOD: 2447 , TESTIDCODE: 68552LCM60

Laboratory ID = 20210620007 Lab Value = 30.737 Expected Conc. = 137.8 Report level label = 11 Pct Recovery = 22% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20210620008 Lab Value = 24.920 Expected Conc. = 137.8 Report level label = 11 Pct Recovery = 18% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810053 Lab Value = 85.120 Expected Conc. = 137.8 Report level label = 11 Pct Recovery = 62% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810052 Lab Value = 88.124 Expected Conc. = 137.8 Report level label = 11 Pct Recovery = 64% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20201820155 Lab Value = 123.144 Expected Conc. = 137.3 Report level label = 11 Pct Recovery = 90% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 127.605 Expected Conc. = 137.3 Report level label = 11 Pct Recovery = 93% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202590106 Lab Value = 88.409 Expected Conc. = 135.5 Report level label = 11 Pct Recovery = 65% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 101.384 Expected Conc. = 135.5 Report level label = 11 Pct Recovery = 75% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 138.622 Expected Conc. = 135.2 Report level label = 11 Pct Recovery = 103% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20221370164 Lab Value = 87.397 Expected Conc. = 110.32 Report level label = 11 Pct Recovery = 79% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20222210250 Lab Value = 82.558 Expected Conc. = 110 Report level label = 11 Pct Recovery = 75% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 105.939 Expected Conc. = 110 Report level label = 11 Pct Recovery = 96% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 82.387 Expected Conc. = 110 Report level label = 11 Pct Recovery = 75% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20210400070 Lab Value = 20.540 Expected Conc. = 68.9 Report level label = 11 Pct Recovery = 30% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081395PEST3 Laboratory ID = 20222070177 Lab Value = 51.605 Expected Conc. = 68.75 Report level label = 11 Pct Recovery = 75% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20202530029 Lab Value = 44.554 Expected Conc. = 68.65 Report level label = 11 Pct Recovery = 65% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 53.951 Expected Conc. = 68.65 Report level label = 11 Pct Recovery = 79% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 63.240 Expected Conc. = 68.65 Report level label = 11 Pct Recovery = 92% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20203230018 Lab Value = 59.378 Expected Conc. = 67.75 Report level label = 11 Pct Recovery = 88% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 50.489 Expected Conc. = 67.75 Report level label = 11 Pct Recovery = 75% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 56.372 Expected Conc. = 67.75 Report level label = 11 Pct Recovery = 83% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201960104 Lab Value = 73.784 Expected Conc. = 67.6 Report level label = 11 Pct Recovery = 109% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20221160208 Lab Value = 21.779 Expected Conc. = 27.58 Report level label = 11 Pct Recovery = 79% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20222000207 Lab Value = 17.778 Expected Conc. = 27.5 Report level label = 11 Pct Recovery = 65% Analysis Date = 07/27/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20202180001 Lab Value = 23.835 Expected Conc. = 27.46 Report level label = 11 Pct Recovery = 87% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 28.118 Expected Conc. = 27.46 Report level label = 11 Pct Recovery = 102% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 19.759 Expected Conc. = 27.46 Report level label = 11 Pct Recovery = 72% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210970035 Lab Value = 23.747 Expected Conc. = 27.1 Report level label = 11 Pct Recovery = 88% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 22.720 Expected Conc. = 27.1 Report level label = 11 Pct Recovery = 84% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 25.341 Expected Conc. = 27.1 Report level label = 11 Pct Recovery = 94% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 35.055 Expected Conc. = 27.1 Report level label = 11 Pct Recovery = 129% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 32.922 Expected Conc. = 27.1 Report level label = 11 Pct Recovery = 121% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201610160 Lab Value = 33.395 Expected Conc. = 27.04 Report level label = 11 Pct Recovery = 124% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Analysis Date = 08/16/22 Pct Recovery = 79% Analysis Date = 08/11/22 Pct Recovery = 79% Analysis Date = 08/11/22 Pct Recovery = 79% Analysis Date = 08/07/22 Pct Recovery = 79% Analysis Date = 08/07/22 Pct Recovery = 79% Analysis Date = 08/03/22 Pct Recovery = 79% Analysis Date = 08/03/22 Pct Recovery = 79% Analysis Date = 07/30/22 Pct Recovery = 79% Analysis Date = 07/30/22 Pct Recovery = 79% Analysis Date = 07/26/22 Pct Recovery = 78% Analysis Date = 07/26/22 Pct Recovery = 78% Analysis Date = 07/22/22 Pct Recovery = 78% Analysis Date = 07/22/22 Pct Recovery = 78% Analysis Date = 07/18/22 Pct Recovery = 78% Analysis Date = 07/18/22 Pct Recovery = 78% Analysis Date = 07/14/22 Pct Recovery = 78% Analysis Date = 07/14/22 Pct Recovery = 78% Analysis Date = 07/10/22 Pct Recovery = 78% Analysis Date = 07/10/22 Pct Recovery = 78% Analysis Date = 07/06/22 Pct Recovery = 78% Analysis Date = 07/06/22 Pct Recovery = 78% Analysis Date = 07/01/22 Pct Recovery = 77% Analysis Date = 07/01/22 Pct Recovery = 77% Analysis Date = 06/27/22 Pct Recovery = 77% Analysis Date = 06/27/22 Pct Recovery = 77% Analysis Date = 06/23/22 Pct Recovery = 77% Analysis Date = 06/23/22 Pct Recovery = 77% Analysis Date = 06/19/22 Pct Recovery = 77% Analysis Date = 06/19/22 Pct Recovery = 77% Analysis Date = 06/15/22 Pct Recovery = 77% Analysis Date = 06/15/22 Pct Recovery = 77% Analysis Date = 06/11/22 Pct Recovery = 77% Analysis Date = 06/11/22 Pct Recovery = 77% Analysis Date = 06/07/22 Pct Recovery = 76% Analysis Date = 06/07/22 Pct Recovery = 76% Analysis Date = 06/03/22 Pct Recovery = 76% Analysis Date = 06/03/22 Pct Recovery = 76% Analysis Date = 05/30/22 Pct Recovery = 76% Analysis Date = 05/30/22 Pct Recovery = 76% Analysis Date = 05/26/22 Pct Recovery = 76% Analysis Date = 05/26/22 Pct Recovery = 76% Analysis Date = 05/22/22 Pct Recovery = 76% Analysis Date = 05/22/22 Pct Recovery = 76% Analysis Date = 05/17/22 Pct Recovery = 76% Analysis Date = 05/17/22 Pct Recovery = 76% Analysis Date = 05/13/22 Pct Recovery = 75% Analysis Date = 05/13/22 Pct Recovery = 75% Analysis Date = 05/09/22 Pct Recovery = 75% Analysis Date = 05/09/22 Pct Recovery = 75% Analysis Date = 05/05/22 Pct Recovery = 75% Analysis Date = 05/05/22 Pct Recovery = 75% Analysis Date = 05/01/22 Pct Recovery = 75% Analysis Date = 05/01/22 Pct Recovery = 75% Analysis Date = 04/27/22 Pct Recovery = 75% Analysis Date = 04/27/22 Pct Recovery = 75% Analysis Date = 04/23/22 Pct Recovery = 75% Analysis Date = 04/23/22 Pct Recovery = 75% Analysis Date = 04/19/22 Pct Recovery = 74% Analysis Date = 04/19/22 Pct Recovery = 74% Analysis Date = 04/15/22 Pct Recovery = 74% Analysis Date = 04/15/22 Pct Recovery = 74% Analysis Date = 04/11/22 Pct Recovery = 74% Analysis Date = 04/11/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 03/29/22 Pct Recovery = 73% Analysis Date = 03/29/22 Pct Recovery = 73% Analysis Date = 03/25/22 Pct Recovery = 73% Analysis Date = 03/25/22 Pct Recovery = 73% Analysis Date = 03/21/22 Pct Recovery = 73% Analysis Date = 03/21/22 Pct Recovery = 73% Analysis Date = 03/17/22 Pct Recovery = 73% Analysis Date = 03/17/22 Pct Recovery = 73% Analysis Date = 03/13/22 Pct Recovery = 73% Analysis Date = 03/13/22 Pct Recovery = 73% Analysis Date = 03/09/22 Pct Recovery = 73% Analysis Date = 03/09/22 Pct Recovery = 73% Analysis Date = 03/05/22 Pct Recovery = 72% Analysis Date = 03/05/22 Pct Recovery = 72% Analysis Date = 03/01/22 Pct Recovery = 72% Analysis Date = 03/01/22 Pct Recovery = 72% Analysis Date = 02/25/22 Pct Recovery = 72% Analysis Date = 02/25/22 Pct Recovery = 72% Analysis Date = 02/20/22 Pct Recovery = 72% Analysis Date = 02/20/22 Pct Recovery = 72% Analysis Date = 02/16/22 Pct Recovery = 72% Analysis Date = 02/16/22 Pct Recovery = 72% Analysis Date = 02/12/22 Pct Recovery = 71% Analysis Date = 02/12/22 Pct Recovery = 71% Analysis Date = 02/08/22 Pct Recovery = 71% Analysis Date = 02/08/22 Pct Recovery = 71% Analysis Date = 02/04/22 Pct Recovery = 71% Analysis Date = 02/04/22 Pct Recovery = 71% Analysis Date = 01/31/22 Pct Recovery = 71% Analysis Date = 01/31/22 Pct Recovery = 71% Analysis Date = 01/27/22 Pct Recovery = 71% Analysis Date = 01/27/22 Pct Recovery = 71% Analysis Date = 01/23/22 Pct Recovery = 70% Analysis Date = 01/23/22 Pct Recovery = 70% Analysis Date = 01/19/22 Pct Recovery = 70% Analysis Date = 01/19/22 Pct Recovery = 70% Analysis Date = 01/15/22 Pct Recovery = 70% Analysis Date = 01/15/22 Pct Recovery = 70% Analysis Date = 01/10/22 Pct Recovery = 70% Analysis Date = 01/10/22 Pct Recovery = 70% Analysis Date = 01/06/22 Pct Recovery = 70% Analysis Date = 01/06/22 Pct Recovery = 70% Analysis Date = 01/02/22 Pct Recovery = 69% Analysis Date = 01/02/22 Pct Recovery = 69% Analysis Date = 12/29/21 Pct Recovery = 69% Analysis Date = 12/29/21 Pct Recovery = 69% Analysis Date = 12/25/21 Pct Recovery = 69% Analysis Date = 12/25/21 Pct Recovery = 69% Analysis Date = 12/21/21 Pct Recovery = 69% Analysis Date = 12/21/21 Pct Recovery = 69% Analysis Date = 12/17/21 Pct Recovery = 69% Analysis Date = 12/17/21 Pct Recovery = 69% Analysis Date = 12/13/21 Pct Recovery = 69% Analysis Date = 12/13/21 Pct Recovery = 69% Analysis Date = 12/09/21 Pct Recovery = 68% Analysis Date = 12/09/21 Pct Recovery = 68% Analysis Date = 12/05/21 Pct Recovery = 68% Analysis Date = 12/05/21 Pct Recovery = 68% Analysis Date = 12/01/21 Pct Recovery = 68% Analysis Date = 12/01/21 Pct Recovery = 68% Analysis Date = 11/26/21 Pct Recovery = 68% Analysis Date = 11/26/21 Pct Recovery = 68% Analysis Date = 11/22/21 Pct Recovery = 68% Analysis Date = 11/22/21 Pct Recovery = 68% Analysis Date = 11/18/21 Pct Recovery = 67% Analysis Date = 11/18/21 Pct Recovery = 67% Analysis Date = 11/14/21 Pct Recovery = 67% Analysis Date = 11/14/21 Pct Recovery = 67% Analysis Date = 11/10/21 Pct Recovery = 67% Analysis Date = 11/10/21 Pct Recovery = 67% Analysis Date = 11/06/21 Pct Recovery = 67% Analysis Date = 11/06/21 Pct Recovery = 67% Analysis Date = 11/02/21 Pct Recovery = 67% Analysis Date = 11/02/21 Pct Recovery = 67% Analysis Date = 10/29/21 Pct Recovery = 66% Analysis Date = 10/29/21 Pct Recovery = 66% Analysis Date = 10/25/21 Pct Recovery = 66% Analysis Date = 10/25/21 Pct Recovery = 66% Analysis Date = 10/21/21 Pct Recovery = 66% Analysis Date = 10/21/21 Pct Recovery = 66% Analysis Date = 10/16/21 Pct Recovery = 66% Analysis Date = 10/16/21 Pct Recovery = 66% Analysis Date = 10/12/21 Pct Recovery = 66% Analysis Date = 10/12/21 Pct Recovery = 66% Analysis Date = 10/08/21 Pct Recovery = 66% Analysis Date = 10/08/21 Pct Recovery = 66% Analysis Date = 10/04/21 Pct Recovery = 65% Analysis Date = 10/04/21 Pct Recovery = 65% Analysis Date = 09/30/21 Pct Recovery = 65% Analysis Date = 09/30/21 Pct Recovery = 65% Analysis Date = 09/26/21 Pct Recovery = 65% Analysis Date = 09/26/21 Pct Recovery = 65% Analysis Date = 09/22/21 Pct Recovery = 65% Analysis Date = 09/22/21 Pct Recovery = 65% Analysis Date = 09/18/21 Pct Recovery = 65% Analysis Date = 09/18/21 Pct Recovery = 65% Analysis Date = 09/14/21 Pct Recovery = 64% Analysis Date = 09/14/21 Pct Recovery = 64% Analysis Date = 09/10/21 Pct Recovery = 64% Analysis Date = 09/10/21 Pct Recovery = 64% Analysis Date = 09/06/21 Pct Recovery = 64% Analysis Date = 09/06/21 Pct Recovery = 64% Analysis Date = 09/01/21 Pct Recovery = 64% Analysis Date = 09/01/21 Pct Recovery = 64% Analysis Date = 08/28/21 Pct Recovery = 64% Analysis Date = 08/28/21 Pct Recovery = 64% Analysis Date = 08/24/21 Pct Recovery = 63% Analysis Date = 08/24/21 Pct Recovery = 63% Analysis Date = 08/20/21 Pct Recovery = 63% Analysis Date = 08/20/21 Pct Recovery = 63% Analysis Date = 08/16/21 Pct Recovery = 63% Analysis Date = 08/16/21 Pct Recovery = 63% Analysis Date = 08/12/21 Pct Recovery = 63% Analysis Date = 08/12/21 Pct Recovery = 63% Analysis Date = 08/08/21 Pct Recovery = 63% Analysis Date = 08/08/21 Pct Recovery = 63% Analysis Date = 08/04/21 Pct Recovery = 62% Analysis Date = 08/04/21 Pct Recovery = 62% Analysis Date = 07/31/21 Pct Recovery = 62% Analysis Date = 07/31/21 Pct Recovery = 62% Analysis Date = 07/27/21 Pct Recovery = 62% Analysis Date = 07/27/21 Pct Recovery = 62% Analysis Date = 07/22/21 Pct Recovery = 62% Analysis Date = 07/22/21 Pct Recovery = 62% Analysis Date = 07/18/21 Pct Recovery = 62% Analysis Date = 07/18/21 Pct Recovery = 62% Analysis Date = 07/14/21 Pct Recovery = 62% Analysis Date = 07/14/21 Pct Recovery = 62% Analysis Date = 07/10/21 Pct Recovery = 61% Analysis Date = 07/10/21 Pct Recovery = 61% Analysis Date = 07/06/21 Pct Recovery = 61% Analysis Date = 07/06/21 Pct Recovery = 61% Analysis Date = 07/02/21 Pct Recovery = 61% Analysis Date = 07/02/21 Pct Recovery = 61% Analysis Date = 06/28/21 Pct Recovery = 61% Analysis Date = 06/28/21 Pct Recovery = 61% Analysis Date = 06/24/21 Pct Recovery = 61% Analysis Date = 06/24/21 Pct Recovery = 61% Analysis Date = 06/20/21 Pct Recovery = 60% Analysis Date = 06/20/21 Pct Recovery = 60% Analysis Date = 06/16/21 Pct Recovery = 60% Analysis Date = 06/16/21 Pct Recovery = 60% Analysis Date = 06/12/21 Pct Recovery = 60% Analysis Date = 06/12/21 Pct Recovery = 60% Analysis Date = 06/07/21 Pct Recovery = 60% Analysis Date = 06/07/21 Pct Recovery = 60% Analysis Date = 06/03/21 Pct Recovery = 60% Analysis Date = 06/03/21 Pct Recovery = 60% Analysis Date = 05/30/21 Pct Recovery = 59% Analysis Date = 05/30/21 Pct Recovery = 59% Analysis Date = 05/26/21 Pct Recovery = 59% Analysis Date = 05/26/21 Pct Recovery = 59% Analysis Date = 05/22/21 Pct Recovery = 59% Analysis Date = 05/22/21 Pct Recovery = 59% Analysis Date = 05/18/21 Pct Recovery = 59% Analysis Date = 05/18/21 Pct Recovery = 59% Analysis Date = 05/14/21 Pct Recovery = 59% Analysis Date = 05/14/21 Pct Recovery = 59% Analysis Date = 05/10/21 Pct Recovery = 59% Analysis Date = 05/10/21 Pct Recovery = 59% Analysis Date = 05/06/21 Pct Recovery = 58% Analysis Date = 05/06/21 Pct Recovery = 58% Analysis Date = 05/02/21 Pct Recovery = 58% Analysis Date = 05/02/21 Pct Recovery = 58% Analysis Date = 04/27/21 Pct Recovery = 58% Analysis Date = 04/27/21 Pct Recovery = 58% Analysis Date = 04/23/21 Pct Recovery = 58% Analysis Date = 04/23/21 Pct Recovery = 58% Analysis Date = 04/19/21 Pct Recovery = 58% Analysis Date = 04/19/21 Pct Recovery = 58% Analysis Date = 04/15/21 Pct Recovery = 57% Analysis Date = 04/15/21 Pct Recovery = 57% Analysis Date = 04/11/21 Pct Recovery = 57% Analysis Date = 04/11/21 Pct Recovery = 57% Analysis Date = 04/07/21 Pct Recovery = 57% Analysis Date = 04/07/21 Pct Recovery = 57% Analysis Date = 04/03/21 Pct Recovery = 57% Analysis Date = 04/03/21 Pct Recovery = 57% Analysis Date = 03/30/21 Pct Recovery = 57% Analysis Date = 03/30/21 Pct Recovery = 57% Analysis Date = 03/26/21 Pct Recovery = 56% Analysis Date = 03/26/21 Pct Recovery = 56% Analysis Date = 03/22/21 Pct Recovery = 56% Analysis Date = 03/22/21 Pct Recovery = 56% Analysis Date = 03/18/21 Pct Recovery = 56% Analysis Date = 03/18/21 Pct Recovery = 56% Analysis Date = 03/13/21 Pct Recovery = 56% Analysis Date = 03/13/21 Pct Recovery = 56% Analysis Date = 03/09/21 Pct Recovery = 56% Analysis Date = 03/09/21 Pct Recovery = 56% Analysis Date = 03/05/21 Pct Recovery = 57% Analysis Date = 03/05/21 Pct Recovery = 57% Analysis Date = 03/01/21 Pct Recovery = 58% Analysis Date = 03/01/21 Pct Recovery = 58% Analysis Date = 02/25/21 Pct Recovery = 59% Analysis Date = 02/25/21 Pct Recovery = 59% Analysis Date = 02/21/21 Pct Recovery = 60% Analysis Date = 02/21/21 Pct Recovery = 60% Analysis Date = 02/17/21 Pct Recovery = 61% Analysis Date = 02/17/21 Pct Recovery = 61% Analysis Date = 02/13/21 Pct Recovery = 62% Analysis Date = 02/13/21 Pct Recovery = 62% Analysis Date = 02/09/21 Pct Recovery = 63% Analysis Date = 02/09/21 Pct Recovery = 63% Analysis Date = 02/05/21 Pct Recovery = 64% Analysis Date = 02/05/21 Pct Recovery = 64% Analysis Date = 01/31/21 Pct Recovery = 65% Analysis Date = 01/31/21 Pct Recovery = 65% Analysis Date = 01/27/21 Pct Recovery = 66% Analysis Date = 01/27/21 Pct Recovery = 66% Analysis Date = 01/23/21 Pct Recovery = 67% Analysis Date = 01/23/21 Pct Recovery = 67% Analysis Date = 01/19/21 Pct Recovery = 68% Analysis Date = 01/19/21 Pct Recovery = 68% Analysis Date = 01/15/21 Pct Recovery = 70% Analysis Date = 01/15/21 Pct Recovery = 70% Analysis Date = 01/11/21 Pct Recovery = 71% Analysis Date = 01/11/21 Pct Recovery = 71% Analysis Date = 01/07/21 Pct Recovery = 72% Analysis Date = 01/07/21 Pct Recovery = 72% Analysis Date = 01/03/21 Pct Recovery = 73% Analysis Date = 01/03/21 Pct Recovery = 73% Analysis Date = 12/30/20 Pct Recovery = 74% Analysis Date = 12/30/20 Pct Recovery = 74% Analysis Date = 12/26/20 Pct Recovery = 76% Analysis Date = 12/26/20 Pct Recovery = 76% Analysis Date = 12/22/20 Pct Recovery = 77% Analysis Date = 12/22/20 Pct Recovery = 77% Analysis Date = 12/17/20 Pct Recovery = 78% Analysis Date = 12/17/20 Pct Recovery = 78% Analysis Date = 12/13/20 Pct Recovery = 79% Analysis Date = 12/13/20 Pct Recovery = 79% Analysis Date = 12/09/20 Pct Recovery = 80% Analysis Date = 12/09/20 Pct Recovery = 80% Analysis Date = 12/05/20 Pct Recovery = 81% Analysis Date = 12/05/20 Pct Recovery = 81% Analysis Date = 12/01/20 Pct Recovery = 81% Analysis Date = 12/01/20 Pct Recovery = 81% Analysis Date = 11/27/20 Pct Recovery = 82% Analysis Date = 11/27/20 Pct Recovery = 82% Analysis Date = 11/23/20 Pct Recovery = 83% Analysis Date = 11/23/20 Pct Recovery = 83% Analysis Date = 11/19/20 Pct Recovery = 84% Analysis Date = 11/19/20 Pct Recovery = 84% Analysis Date = 11/15/20 Pct Recovery = 85% Analysis Date = 11/15/20 Pct Recovery = 85% Analysis Date = 11/11/20 Pct Recovery = 85% Analysis Date = 11/11/20 Pct Recovery = 85% Analysis Date = 11/06/20 Pct Recovery = 86% Analysis Date = 11/06/20 Pct Recovery = 86% Analysis Date = 11/02/20 Pct Recovery = 87% Analysis Date = 11/02/20 Pct Recovery = 87% Analysis Date = 10/29/20 Pct Recovery = 86% Analysis Date = 10/29/20 Pct Recovery = 86% Analysis Date = 10/25/20 Pct Recovery = 86% Analysis Date = 10/25/20 Pct Recovery = 86% Analysis Date = 10/21/20 Pct Recovery = 86% Analysis Date = 10/21/20 Pct Recovery = 86% Analysis Date = 10/17/20 Pct Recovery = 86% Analysis Date = 10/17/20 Pct Recovery = 86% Analysis Date = 10/13/20 Pct Recovery = 86% Analysis Date = 10/13/20 Pct Recovery = 86% Analysis Date = 10/09/20 Pct Recovery = 86% Analysis Date = 10/09/20 Pct Recovery = 86% Analysis Date = 10/05/20 Pct Recovery = 86% Analysis Date = 10/05/20 Pct Recovery = 86% Analysis Date = 10/01/20 Pct Recovery = 85% Analysis Date = 10/01/20 Pct Recovery = 85% Analysis Date = 09/27/20 Pct Recovery = 85% Analysis Date = 09/27/20 Pct Recovery = 85% Analysis Date = 09/22/20 Pct Recovery = 85% Analysis Date = 09/22/20 Pct Recovery = 85% Analysis Date = 09/18/20 Pct Recovery = 85% Analysis Date = 09/18/20 Pct Recovery = 85% Analysis Date = 09/14/20 Pct Recovery = 85% Analysis Date = 09/14/20 Pct Recovery = 85% Analysis Date = 09/10/20 Pct Recovery = 85% Analysis Date = 09/10/20 Pct Recovery = 85% Analysis Date = 09/06/20 Pct Recovery = 85% Analysis Date = 09/06/20 Pct Recovery = 85% Analysis Date = 09/02/20 Pct Recovery = 85% Analysis Date = 09/02/20 Pct Recovery = 85% Analysis Date = 08/29/20 Pct Recovery = 86% Analysis Date = 08/29/20 Pct Recovery = 86% Analysis Date = 08/25/20 Pct Recovery = 86% Analysis Date = 08/25/20 Pct Recovery = 86% Analysis Date = 08/21/20 Pct Recovery = 87% Analysis Date = 08/21/20 Pct Recovery = 87% Analysis Date = 08/17/20 Pct Recovery = 87% Analysis Date = 08/17/20 Pct Recovery = 87% Analysis Date = 08/12/20 Pct Recovery = 88% Analysis Date = 08/12/20 Pct Recovery = 88% Analysis Date = 08/08/20 Pct Recovery = 89% Analysis Date = 08/08/20 Pct Recovery = 89% Analysis Date = 08/04/20 Pct Recovery = 89% Analysis Date = 08/04/20 Pct Recovery = 89% Analysis Date = 07/31/20 Pct Recovery = 90% Analysis Date = 07/31/20 Pct Recovery = 90% Analysis Date = 07/27/20 Pct Recovery = 90% Analysis Date = 07/27/20 Pct Recovery = 90% Analysis Date = 07/23/20 Pct Recovery = 91% Analysis Date = 07/23/20 Pct Recovery = 91% Analysis Date = 07/19/20 Pct Recovery = 92% Analysis Date = 07/19/20 Pct Recovery = 92% Analysis Date = 07/15/20 Pct Recovery = 92% Analysis Date = 07/15/20 Pct Recovery = 92% Analysis Date = 07/11/20 Pct Recovery = 93% Analysis Date = 07/11/20 Pct Recovery = 93% Analysis Date = 07/07/20 Pct Recovery = 94% Analysis Date = 07/07/20 Pct Recovery = 94% Analysis Date = 07/03/20 Pct Recovery = 94% Analysis Date = 07/03/20 Pct Recovery = 94% Analysis Date = 06/28/20 Pct Recovery = 95% Analysis Date = 06/28/20 Pct Recovery = 95% Analysis Date = 06/24/20 Pct Recovery = 96% Analysis Date = 06/24/20 Pct Recovery = 96% Analysis Date = 06/20/20 Pct Recovery = 96% Analysis Date = 06/20/20 Pct Recovery = 96% Analysis Date = 06/16/20 Pct Recovery = 97% Analysis Date = 06/16/20 Pct Recovery = 97% Analysis Date = 06/12/20 Pct Recovery = 98% Analysis Date = 06/12/20 Pct Recovery = 98% Analysis Date = 06/08/20 Pct Recovery = 98% Analysis Date = 06/08/20 Pct Recovery = 98% Analysis Date = 06/04/20 Pct Recovery = 99% Analysis Date = 06/04/20 Pct Recovery = 99% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 100% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/19/20 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEETHYLATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 80% 25% 79% 16%
Total 33 80% 25% 79% 16%

Sample Statistics
DEETHYLATRAZINE

Characteristic N % % Basis
Plotted 33 97% Spiked
Estimated Values 8 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 1 3% 1 out of 34
Not Spiked 82 .  
False Positives 1 1% 1 out of 82

OBSP Determination:
DEETHYLDEISOPROPYLATRAZINE
METHOD: 2447 , TESTIDCODE: 68547LCM60

Laboratory ID = 20202810053 Lab Value = 950.678 Expected Conc. = 300.2 Report level label = 24 Pct Recovery = 317% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810052 Lab Value = 1055.748 Expected Conc. = 300.2 Report level label = 24 Pct Recovery = 352% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202390020 Lab Value = 330.785 Expected Conc. = 305.7 Report level label = 24 Pct Recovery = 108% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203080100 Lab Value = 215.854 Expected Conc. = 301.7 Report level label = 24 Pct Recovery = 72% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 192.687 Expected Conc. = 301.7 Report level label = 24 Pct Recovery = 64% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 168.164 Expected Conc. = 301.7 Report level label = 24 Pct Recovery = 56% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201820155 Lab Value = 272.296 Expected Conc. = 301.3 Report level label = 24 Pct Recovery = 90% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 330.753 Expected Conc. = 301.3 Report level label = 24 Pct Recovery = 110% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20210620007 Lab Value = 62.502 Expected Conc. = 300.2 Report level label = 24 Pct Recovery = 21% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20210620008 Lab Value = 82.246 Expected Conc. = 300.2 Report level label = 24 Pct Recovery = 27% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20221940194 Lab Value = 84.241 Expected Conc. = 240 Report level label = 24 Pct Recovery = 35% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221370164 Lab Value = 161.587 Expected Conc. = 240 Report level label = 24 Pct Recovery = 67% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20201960104 Lab Value = 141.714 Expected Conc. = 152.85 Report level label = 24 Pct Recovery = 93% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202880004 Lab Value = 116.252 Expected Conc. = 150.85 Report level label = 24 Pct Recovery = 77% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202530029 Lab Value = 107.591 Expected Conc. = 150.65 Report level label = 24 Pct Recovery = 71% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 145.203 Expected Conc. = 150.65 Report level label = 24 Pct Recovery = 96% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 148.440 Expected Conc. = 150.65 Report level label = 24 Pct Recovery = 99% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20210400070 Lab Value = 99.940 Expected Conc. = 150.1 Report level label = 24 Pct Recovery = 67% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081395PEST3 Laboratory ID = 20222070177 Lab Value = 52.363 Expected Conc. = 150 Report level label = 24 Pct Recovery = 35% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20210620006 Lab Value = 75.528 Expected Conc. = 120.68 Report level label = 24 Pct Recovery = 63% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 90.974 Expected Conc. = 120.68 Report level label = 24 Pct Recovery = 75% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 45.278 Expected Conc. = 61.14 Report level label = 24 Pct Recovery = 74% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20203530076 Lab Value = 63.324 Expected Conc. = 60.34 Report level label = 24 Pct Recovery = 105% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 45.515 Expected Conc. = 60.34 Report level label = 24 Pct Recovery = 75% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 47.716 Expected Conc. = 60.34 Report level label = 24 Pct Recovery = 79% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 49.213 Expected Conc. = 60.34 Report level label = 24 Pct Recovery = 82% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202180001 Lab Value = 45.910 Expected Conc. = 60.26 Report level label = 24 Pct Recovery = 76% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 69.243 Expected Conc. = 60.26 Report level label = 24 Pct Recovery = 115% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 47.062 Expected Conc. = 60.26 Report level label = 24 Pct Recovery = 78% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Analysis Date = 08/02/22 Pct Recovery = 44% Analysis Date = 07/29/22 Pct Recovery = 44% Analysis Date = 07/29/22 Pct Recovery = 44% Analysis Date = 07/25/22 Pct Recovery = 44% Analysis Date = 07/25/22 Pct Recovery = 44% Analysis Date = 07/21/22 Pct Recovery = 44% Analysis Date = 07/21/22 Pct Recovery = 44% Analysis Date = 07/17/22 Pct Recovery = 44% Analysis Date = 07/17/22 Pct Recovery = 44% Analysis Date = 07/13/22 Pct Recovery = 44% Analysis Date = 07/13/22 Pct Recovery = 44% Analysis Date = 07/09/22 Pct Recovery = 44% Analysis Date = 07/09/22 Pct Recovery = 44% Analysis Date = 07/05/22 Pct Recovery = 44% Analysis Date = 07/05/22 Pct Recovery = 44% Analysis Date = 07/01/22 Pct Recovery = 44% Analysis Date = 07/01/22 Pct Recovery = 44% Analysis Date = 06/27/22 Pct Recovery = 44% Analysis Date = 06/27/22 Pct Recovery = 44% Analysis Date = 06/23/22 Pct Recovery = 44% Analysis Date = 06/23/22 Pct Recovery = 44% Analysis Date = 06/19/22 Pct Recovery = 44% Analysis Date = 06/19/22 Pct Recovery = 44% Analysis Date = 06/15/22 Pct Recovery = 44% Analysis Date = 06/15/22 Pct Recovery = 44% Analysis Date = 06/11/22 Pct Recovery = 44% Analysis Date = 06/11/22 Pct Recovery = 44% Analysis Date = 06/07/22 Pct Recovery = 44% Analysis Date = 06/07/22 Pct Recovery = 44% Analysis Date = 06/03/22 Pct Recovery = 44% Analysis Date = 06/03/22 Pct Recovery = 44% Analysis Date = 05/30/22 Pct Recovery = 43% Analysis Date = 05/30/22 Pct Recovery = 43% Analysis Date = 05/26/22 Pct Recovery = 43% Analysis Date = 05/26/22 Pct Recovery = 43% Analysis Date = 05/22/22 Pct Recovery = 43% Analysis Date = 05/22/22 Pct Recovery = 43% Analysis Date = 05/18/22 Pct Recovery = 43% Analysis Date = 05/18/22 Pct Recovery = 43% Analysis Date = 05/14/22 Pct Recovery = 43% Analysis Date = 05/14/22 Pct Recovery = 43% Analysis Date = 05/10/22 Pct Recovery = 43% Analysis Date = 05/10/22 Pct Recovery = 43% Analysis Date = 05/06/22 Pct Recovery = 43% Analysis Date = 05/06/22 Pct Recovery = 43% Analysis Date = 05/02/22 Pct Recovery = 43% Analysis Date = 05/02/22 Pct Recovery = 43% Analysis Date = 04/28/22 Pct Recovery = 43% Analysis Date = 04/28/22 Pct Recovery = 43% Analysis Date = 04/24/22 Pct Recovery = 43% Analysis Date = 04/24/22 Pct Recovery = 43% Analysis Date = 04/20/22 Pct Recovery = 43% Analysis Date = 04/20/22 Pct Recovery = 43% Analysis Date = 04/16/22 Pct Recovery = 43% Analysis Date = 04/16/22 Pct Recovery = 43% Analysis Date = 04/12/22 Pct Recovery = 43% Analysis Date = 04/12/22 Pct Recovery = 43% Analysis Date = 04/08/22 Pct Recovery = 43% Analysis Date = 04/08/22 Pct Recovery = 43% Analysis Date = 04/04/22 Pct Recovery = 43% Analysis Date = 04/04/22 Pct Recovery = 43% Analysis Date = 03/31/22 Pct Recovery = 43% Analysis Date = 03/31/22 Pct Recovery = 43% Analysis Date = 03/27/22 Pct Recovery = 43% Analysis Date = 03/27/22 Pct Recovery = 43% Analysis Date = 03/23/22 Pct Recovery = 43% Analysis Date = 03/23/22 Pct Recovery = 43% Analysis Date = 03/18/22 Pct Recovery = 43% Analysis Date = 03/18/22 Pct Recovery = 43% Analysis Date = 03/14/22 Pct Recovery = 43% Analysis Date = 03/14/22 Pct Recovery = 43% Analysis Date = 03/10/22 Pct Recovery = 43% Analysis Date = 03/10/22 Pct Recovery = 43% Analysis Date = 03/06/22 Pct Recovery = 43% Analysis Date = 03/06/22 Pct Recovery = 43% Analysis Date = 03/02/22 Pct Recovery = 43% Analysis Date = 03/02/22 Pct Recovery = 43% Analysis Date = 02/26/22 Pct Recovery = 43% Analysis Date = 02/26/22 Pct Recovery = 43% Analysis Date = 02/22/22 Pct Recovery = 43% Analysis Date = 02/22/22 Pct Recovery = 43% Analysis Date = 02/18/22 Pct Recovery = 43% Analysis Date = 02/18/22 Pct Recovery = 43% Analysis Date = 02/14/22 Pct Recovery = 43% Analysis Date = 02/14/22 Pct Recovery = 43% Analysis Date = 02/10/22 Pct Recovery = 43% Analysis Date = 02/10/22 Pct Recovery = 43% Analysis Date = 02/06/22 Pct Recovery = 43% Analysis Date = 02/06/22 Pct Recovery = 43% Analysis Date = 02/02/22 Pct Recovery = 43% Analysis Date = 02/02/22 Pct Recovery = 43% Analysis Date = 01/29/22 Pct Recovery = 43% Analysis Date = 01/29/22 Pct Recovery = 43% Analysis Date = 01/25/22 Pct Recovery = 43% Analysis Date = 01/25/22 Pct Recovery = 43% Analysis Date = 01/21/22 Pct Recovery = 43% Analysis Date = 01/21/22 Pct Recovery = 43% Analysis Date = 01/17/22 Pct Recovery = 43% Analysis Date = 01/17/22 Pct Recovery = 43% Analysis Date = 01/13/22 Pct Recovery = 43% Analysis Date = 01/13/22 Pct Recovery = 43% Analysis Date = 01/09/22 Pct Recovery = 42% Analysis Date = 01/09/22 Pct Recovery = 42% Analysis Date = 01/05/22 Pct Recovery = 42% Analysis Date = 01/05/22 Pct Recovery = 42% Analysis Date = 01/01/22 Pct Recovery = 42% Analysis Date = 01/01/22 Pct Recovery = 42% Analysis Date = 12/28/21 Pct Recovery = 42% Analysis Date = 12/28/21 Pct Recovery = 42% Analysis Date = 12/24/21 Pct Recovery = 42% Analysis Date = 12/24/21 Pct Recovery = 42% Analysis Date = 12/20/21 Pct Recovery = 42% Analysis Date = 12/20/21 Pct Recovery = 42% Analysis Date = 12/16/21 Pct Recovery = 42% Analysis Date = 12/16/21 Pct Recovery = 42% Analysis Date = 12/12/21 Pct Recovery = 42% Analysis Date = 12/12/21 Pct Recovery = 42% Analysis Date = 12/08/21 Pct Recovery = 42% Analysis Date = 12/08/21 Pct Recovery = 42% Analysis Date = 12/04/21 Pct Recovery = 42% Analysis Date = 12/04/21 Pct Recovery = 42% Analysis Date = 11/30/21 Pct Recovery = 42% Analysis Date = 11/30/21 Pct Recovery = 42% Analysis Date = 11/26/21 Pct Recovery = 42% Analysis Date = 11/26/21 Pct Recovery = 42% Analysis Date = 11/22/21 Pct Recovery = 42% Analysis Date = 11/22/21 Pct Recovery = 42% Analysis Date = 11/18/21 Pct Recovery = 42% Analysis Date = 11/18/21 Pct Recovery = 42% Analysis Date = 11/14/21 Pct Recovery = 42% Analysis Date = 11/14/21 Pct Recovery = 42% Analysis Date = 11/10/21 Pct Recovery = 42% Analysis Date = 11/10/21 Pct Recovery = 42% Analysis Date = 11/05/21 Pct Recovery = 42% Analysis Date = 11/05/21 Pct Recovery = 42% Analysis Date = 11/01/21 Pct Recovery = 42% Analysis Date = 11/01/21 Pct Recovery = 42% Analysis Date = 10/28/21 Pct Recovery = 42% Analysis Date = 10/28/21 Pct Recovery = 42% Analysis Date = 10/24/21 Pct Recovery = 42% Analysis Date = 10/24/21 Pct Recovery = 42% Analysis Date = 10/20/21 Pct Recovery = 42% Analysis Date = 10/20/21 Pct Recovery = 42% Analysis Date = 10/16/21 Pct Recovery = 42% Analysis Date = 10/16/21 Pct Recovery = 42% Analysis Date = 10/12/21 Pct Recovery = 42% Analysis Date = 10/12/21 Pct Recovery = 42% Analysis Date = 10/08/21 Pct Recovery = 42% Analysis Date = 10/08/21 Pct Recovery = 42% Analysis Date = 10/04/21 Pct Recovery = 42% Analysis Date = 10/04/21 Pct Recovery = 42% Analysis Date = 09/30/21 Pct Recovery = 42% Analysis Date = 09/30/21 Pct Recovery = 42% Analysis Date = 09/26/21 Pct Recovery = 42% Analysis Date = 09/26/21 Pct Recovery = 42% Analysis Date = 09/22/21 Pct Recovery = 42% Analysis Date = 09/22/21 Pct Recovery = 42% Analysis Date = 09/18/21 Pct Recovery = 42% Analysis Date = 09/18/21 Pct Recovery = 42% Analysis Date = 09/14/21 Pct Recovery = 42% Analysis Date = 09/14/21 Pct Recovery = 42% Analysis Date = 09/10/21 Pct Recovery = 42% Analysis Date = 09/10/21 Pct Recovery = 42% Analysis Date = 09/06/21 Pct Recovery = 42% Analysis Date = 09/06/21 Pct Recovery = 42% Analysis Date = 09/02/21 Pct Recovery = 42% Analysis Date = 09/02/21 Pct Recovery = 42% Analysis Date = 08/29/21 Pct Recovery = 42% Analysis Date = 08/29/21 Pct Recovery = 42% Analysis Date = 08/25/21 Pct Recovery = 42% Analysis Date = 08/25/21 Pct Recovery = 42% Analysis Date = 08/21/21 Pct Recovery = 41% Analysis Date = 08/21/21 Pct Recovery = 41% Analysis Date = 08/17/21 Pct Recovery = 41% Analysis Date = 08/17/21 Pct Recovery = 41% Analysis Date = 08/13/21 Pct Recovery = 41% Analysis Date = 08/13/21 Pct Recovery = 41% Analysis Date = 08/09/21 Pct Recovery = 41% Analysis Date = 08/09/21 Pct Recovery = 41% Analysis Date = 08/05/21 Pct Recovery = 41% Analysis Date = 08/05/21 Pct Recovery = 41% Analysis Date = 08/01/21 Pct Recovery = 41% Analysis Date = 08/01/21 Pct Recovery = 41% Analysis Date = 07/28/21 Pct Recovery = 41% Analysis Date = 07/28/21 Pct Recovery = 41% Analysis Date = 07/24/21 Pct Recovery = 41% Analysis Date = 07/24/21 Pct Recovery = 41% Analysis Date = 07/20/21 Pct Recovery = 41% Analysis Date = 07/20/21 Pct Recovery = 41% Analysis Date = 07/16/21 Pct Recovery = 41% Analysis Date = 07/16/21 Pct Recovery = 41% Analysis Date = 07/12/21 Pct Recovery = 41% Analysis Date = 07/12/21 Pct Recovery = 41% Analysis Date = 07/08/21 Pct Recovery = 41% Analysis Date = 07/08/21 Pct Recovery = 41% Analysis Date = 07/04/21 Pct Recovery = 41% Analysis Date = 07/04/21 Pct Recovery = 41% Analysis Date = 06/30/21 Pct Recovery = 41% Analysis Date = 06/30/21 Pct Recovery = 41% Analysis Date = 06/25/21 Pct Recovery = 41% Analysis Date = 06/25/21 Pct Recovery = 41% Analysis Date = 06/21/21 Pct Recovery = 41% Analysis Date = 06/21/21 Pct Recovery = 41% Analysis Date = 06/17/21 Pct Recovery = 41% Analysis Date = 06/17/21 Pct Recovery = 41% Analysis Date = 06/13/21 Pct Recovery = 41% Analysis Date = 06/13/21 Pct Recovery = 41% Analysis Date = 06/09/21 Pct Recovery = 41% Analysis Date = 06/09/21 Pct Recovery = 41% Analysis Date = 06/05/21 Pct Recovery = 41% Analysis Date = 06/05/21 Pct Recovery = 41% Analysis Date = 06/01/21 Pct Recovery = 41% Analysis Date = 06/01/21 Pct Recovery = 41% Analysis Date = 05/28/21 Pct Recovery = 41% Analysis Date = 05/28/21 Pct Recovery = 41% Analysis Date = 05/24/21 Pct Recovery = 41% Analysis Date = 05/24/21 Pct Recovery = 41% Analysis Date = 05/20/21 Pct Recovery = 41% Analysis Date = 05/20/21 Pct Recovery = 41% Analysis Date = 05/16/21 Pct Recovery = 41% Analysis Date = 05/16/21 Pct Recovery = 41% Analysis Date = 05/12/21 Pct Recovery = 41% Analysis Date = 05/12/21 Pct Recovery = 41% Analysis Date = 05/08/21 Pct Recovery = 41% Analysis Date = 05/08/21 Pct Recovery = 41% Analysis Date = 05/04/21 Pct Recovery = 41% Analysis Date = 05/04/21 Pct Recovery = 41% Analysis Date = 04/30/21 Pct Recovery = 41% Analysis Date = 04/30/21 Pct Recovery = 41% Analysis Date = 04/26/21 Pct Recovery = 41% Analysis Date = 04/26/21 Pct Recovery = 41% Analysis Date = 04/22/21 Pct Recovery = 41% Analysis Date = 04/22/21 Pct Recovery = 41% Analysis Date = 04/18/21 Pct Recovery = 41% Analysis Date = 04/18/21 Pct Recovery = 41% Analysis Date = 04/14/21 Pct Recovery = 41% Analysis Date = 04/14/21 Pct Recovery = 41% Analysis Date = 04/10/21 Pct Recovery = 41% Analysis Date = 04/10/21 Pct Recovery = 41% Analysis Date = 04/06/21 Pct Recovery = 41% Analysis Date = 04/06/21 Pct Recovery = 41% Analysis Date = 04/02/21 Pct Recovery = 40% Analysis Date = 04/02/21 Pct Recovery = 40% Analysis Date = 03/29/21 Pct Recovery = 40% Analysis Date = 03/29/21 Pct Recovery = 40% Analysis Date = 03/25/21 Pct Recovery = 40% Analysis Date = 03/25/21 Pct Recovery = 40% Analysis Date = 03/21/21 Pct Recovery = 40% Analysis Date = 03/21/21 Pct Recovery = 40% Analysis Date = 03/17/21 Pct Recovery = 40% Analysis Date = 03/17/21 Pct Recovery = 40% Analysis Date = 03/13/21 Pct Recovery = 40% Analysis Date = 03/13/21 Pct Recovery = 40% Analysis Date = 03/09/21 Pct Recovery = 40% Analysis Date = 03/09/21 Pct Recovery = 40% Analysis Date = 03/05/21 Pct Recovery = 43% Analysis Date = 03/05/21 Pct Recovery = 43% Analysis Date = 03/01/21 Pct Recovery = 46% Analysis Date = 03/01/21 Pct Recovery = 46% Analysis Date = 02/25/21 Pct Recovery = 48% Analysis Date = 02/25/21 Pct Recovery = 48% Analysis Date = 02/21/21 Pct Recovery = 51% Analysis Date = 02/21/21 Pct Recovery = 51% Analysis Date = 02/17/21 Pct Recovery = 54% Analysis Date = 02/17/21 Pct Recovery = 54% Analysis Date = 02/13/21 Pct Recovery = 57% Analysis Date = 02/13/21 Pct Recovery = 57% Analysis Date = 02/08/21 Pct Recovery = 59% Analysis Date = 02/08/21 Pct Recovery = 59% Analysis Date = 02/04/21 Pct Recovery = 62% Analysis Date = 02/04/21 Pct Recovery = 62% Analysis Date = 01/31/21 Pct Recovery = 65% Analysis Date = 01/31/21 Pct Recovery = 65% Analysis Date = 01/27/21 Pct Recovery = 67% Analysis Date = 01/27/21 Pct Recovery = 67% Analysis Date = 01/23/21 Pct Recovery = 70% Analysis Date = 01/23/21 Pct Recovery = 70% Analysis Date = 01/19/21 Pct Recovery = 73% Analysis Date = 01/19/21 Pct Recovery = 73% Analysis Date = 01/15/21 Pct Recovery = 75% Analysis Date = 01/15/21 Pct Recovery = 75% Analysis Date = 01/11/21 Pct Recovery = 78% Analysis Date = 01/11/21 Pct Recovery = 78% Analysis Date = 01/07/21 Pct Recovery = 81% Analysis Date = 01/07/21 Pct Recovery = 81% Analysis Date = 01/03/21 Pct Recovery = 83% Analysis Date = 01/03/21 Pct Recovery = 83% Analysis Date = 12/30/20 Pct Recovery = 86% Analysis Date = 12/30/20 Pct Recovery = 86% Analysis Date = 12/26/20 Pct Recovery = 89% Analysis Date = 12/26/20 Pct Recovery = 89% Analysis Date = 12/22/20 Pct Recovery = 91% Analysis Date = 12/22/20 Pct Recovery = 91% Analysis Date = 12/18/20 Pct Recovery = 94% Analysis Date = 12/18/20 Pct Recovery = 94% Analysis Date = 12/14/20 Pct Recovery = 97% Analysis Date = 12/14/20 Pct Recovery = 97% Analysis Date = 12/10/20 Pct Recovery = 99% Analysis Date = 12/10/20 Pct Recovery = 99% Analysis Date = 12/06/20 Pct Recovery = 102% Analysis Date = 12/06/20 Pct Recovery = 102% Analysis Date = 12/02/20 Pct Recovery = 105% Analysis Date = 12/02/20 Pct Recovery = 105% Analysis Date = 11/28/20 Pct Recovery = 107% Analysis Date = 11/28/20 Pct Recovery = 107% Analysis Date = 11/24/20 Pct Recovery = 110% Analysis Date = 11/24/20 Pct Recovery = 110% Analysis Date = 11/20/20 Pct Recovery = 113% Analysis Date = 11/20/20 Pct Recovery = 113% Analysis Date = 11/16/20 Pct Recovery = 115% Analysis Date = 11/16/20 Pct Recovery = 115% Analysis Date = 11/12/20 Pct Recovery = 118% Analysis Date = 11/12/20 Pct Recovery = 118% Analysis Date = 11/08/20 Pct Recovery = 119% Analysis Date = 11/08/20 Pct Recovery = 119% Analysis Date = 11/04/20 Pct Recovery = 120% Analysis Date = 11/04/20 Pct Recovery = 120% Analysis Date = 10/31/20 Pct Recovery = 121% Analysis Date = 10/31/20 Pct Recovery = 121% Analysis Date = 10/27/20 Pct Recovery = 122% Analysis Date = 10/27/20 Pct Recovery = 122% Analysis Date = 10/23/20 Pct Recovery = 123% Analysis Date = 10/23/20 Pct Recovery = 123% Analysis Date = 10/19/20 Pct Recovery = 123% Analysis Date = 10/19/20 Pct Recovery = 123% Analysis Date = 10/15/20 Pct Recovery = 124% Analysis Date = 10/15/20 Pct Recovery = 124% Analysis Date = 10/11/20 Pct Recovery = 123% Analysis Date = 10/11/20 Pct Recovery = 123% Analysis Date = 10/07/20 Pct Recovery = 123% Analysis Date = 10/07/20 Pct Recovery = 123% Analysis Date = 10/03/20 Pct Recovery = 122% Analysis Date = 10/03/20 Pct Recovery = 122% Analysis Date = 09/28/20 Pct Recovery = 122% Analysis Date = 09/28/20 Pct Recovery = 122% Analysis Date = 09/24/20 Pct Recovery = 121% Analysis Date = 09/24/20 Pct Recovery = 121% Analysis Date = 09/20/20 Pct Recovery = 120% Analysis Date = 09/20/20 Pct Recovery = 120% Analysis Date = 09/16/20 Pct Recovery = 117% Analysis Date = 09/16/20 Pct Recovery = 117% Analysis Date = 09/12/20 Pct Recovery = 114% Analysis Date = 09/12/20 Pct Recovery = 114% Analysis Date = 09/08/20 Pct Recovery = 112% Analysis Date = 09/08/20 Pct Recovery = 112% Analysis Date = 09/04/20 Pct Recovery = 109% Analysis Date = 09/04/20 Pct Recovery = 109% Analysis Date = 08/31/20 Pct Recovery = 106% Analysis Date = 08/31/20 Pct Recovery = 106% Analysis Date = 08/27/20 Pct Recovery = 104% Analysis Date = 08/27/20 Pct Recovery = 104% Analysis Date = 08/23/20 Pct Recovery = 101% Analysis Date = 08/23/20 Pct Recovery = 101% Analysis Date = 08/19/20 Pct Recovery = 98% Analysis Date = 08/19/20 Pct Recovery = 98% Analysis Date = 08/15/20 Pct Recovery = 95% Analysis Date = 08/15/20 Pct Recovery = 95% Analysis Date = 08/11/20 Pct Recovery = 94% Analysis Date = 08/11/20 Pct Recovery = 94% Analysis Date = 08/07/20 Pct Recovery = 93% Analysis Date = 08/07/20 Pct Recovery = 93% Analysis Date = 08/03/20 Pct Recovery = 93% Analysis Date = 08/03/20 Pct Recovery = 93% Analysis Date = 07/30/20 Pct Recovery = 92% Analysis Date = 07/30/20 Pct Recovery = 92% Analysis Date = 07/26/20 Pct Recovery = 91% Analysis Date = 07/26/20 Pct Recovery = 91% Analysis Date = 07/22/20 Pct Recovery = 91% Analysis Date = 07/22/20 Pct Recovery = 91% Analysis Date = 07/18/20 Pct Recovery = 91% Analysis Date = 07/18/20 Pct Recovery = 91% Analysis Date = 07/14/20 Pct Recovery = 91% Analysis Date = 07/14/20 Pct Recovery = 91% Analysis Date = 07/10/20 Pct Recovery = 91% Analysis Date = 07/10/20 Pct Recovery = 91% Analysis Date = 07/06/20 Pct Recovery = 92% Analysis Date = 07/06/20 Pct Recovery = 92% Analysis Date = 07/02/20 Pct Recovery = 92% Analysis Date = 07/02/20 Pct Recovery = 92% Analysis Date = 06/28/20 Pct Recovery = 92% Analysis Date = 06/28/20 Pct Recovery = 92% Analysis Date = 06/24/20 Pct Recovery = 93% Analysis Date = 06/24/20 Pct Recovery = 93% Analysis Date = 06/20/20 Pct Recovery = 93% Analysis Date = 06/20/20 Pct Recovery = 93% Analysis Date = 06/16/20 Pct Recovery = 93% Analysis Date = 06/16/20 Pct Recovery = 93% Analysis Date = 06/12/20 Pct Recovery = 94% Analysis Date = 06/12/20 Pct Recovery = 94% Analysis Date = 06/08/20 Pct Recovery = 94% Analysis Date = 06/08/20 Pct Recovery = 94% Analysis Date = 06/04/20 Pct Recovery = 94% Analysis Date = 06/04/20 Pct Recovery = 94% Analysis Date = 05/31/20 Pct Recovery = 94% Analysis Date = 05/31/20 Pct Recovery = 94% Analysis Date = 05/27/20 Pct Recovery = 95% Analysis Date = 05/27/20 Pct Recovery = 95% Analysis Date = 05/23/20 Pct Recovery = 95% Analysis Date = 05/23/20 Pct Recovery = 95% Analysis Date = 05/19/20 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEETHYLDEISOPROPYLATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 29 92% 71% 76% 22%
Total 29 92% 71% 76% 22%

Sample Statistics
DEETHYLDEISOPROPYLATRAZINE

Characteristic N % % Basis
Plotted 29 85% Spiked
Estimated Values 17 50% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 34 .  
False Negatives 4 12% 4 out of 34
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

OBSP Determination:
DEISOPROPYLATRAZINE
METHOD: 2447 , TESTIDCODE: 68550LCM60

Laboratory ID = 20202590106 Lab Value = 243.037 Expected Conc. = 250.5 Report level label = 20 Pct Recovery = 97% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 203.814 Expected Conc. = 250.5 Report level label = 20 Pct Recovery = 81% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210620007 Lab Value = 38.043 Expected Conc. = 250.4 Report level label = 20 Pct Recovery = 15% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20210620008 Lab Value = 40.337 Expected Conc. = 250.4 Report level label = 20 Pct Recovery = 16% Analysis Date = 03/09/21 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810053 Lab Value = 162.520 Expected Conc. = 250.4 Report level label = 20 Pct Recovery = 65% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20202810052 Lab Value = 186.533 Expected Conc. = 250.4 Report level label = 20 Pct Recovery = 74% Analysis Date = 10/14/20 SpikeMix = Accu 220081395PEST3: 100 µl SpecificMix = 220081395PEST3 Laboratory ID = 20221370164 Lab Value = 192.290 Expected Conc. = 200.8 Report level label = 20 Pct Recovery = 96% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4b Laboratory ID = 20222210250 Lab Value = 154.225 Expected Conc. = 200 Report level label = 20 Pct Recovery = 77% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 195.257 Expected Conc. = 200 Report level label = 20 Pct Recovery = 98% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 163.323 Expected Conc. = 200 Report level label = 20 Pct Recovery = 82% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20203230018 Lab Value = 95.221 Expected Conc. = 125.25 Report level label = 20 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 119.594 Expected Conc. = 125.25 Report level label = 20 Pct Recovery = 95% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 137.610 Expected Conc. = 125.25 Report level label = 20 Pct Recovery = 110% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210400070 Lab Value = 43.939 Expected Conc. = 125.2 Report level label = 20 Pct Recovery = 35% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081395PEST3 Laboratory ID = 20222070177 Lab Value = 82.731 Expected Conc. = 125 Report level label = 20 Pct Recovery = 66% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20201550031 Lab Value = 151.184 Expected Conc. = 124.8 Report level label = 20 Pct Recovery = 121% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20202390020 Lab Value = 172.758 Expected Conc. = 124.1 Report level label = 20 Pct Recovery = 139% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 108.639 Expected Conc. = 124.1 Report level label = 20 Pct Recovery = 88% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 157.081 Expected Conc. = 99.28 Report level label = 20 Pct Recovery = 158% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 100.368 Expected Conc. = 99.28 Report level label = 20 Pct Recovery = 101% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210970035 Lab Value = 38.479 Expected Conc. = 50.1 Report level label = 20 Pct Recovery = 77% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 48.927 Expected Conc. = 50.1 Report level label = 20 Pct Recovery = 98% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 42.354 Expected Conc. = 50.1 Report level label = 20 Pct Recovery = 85% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 52.276 Expected Conc. = 50.1 Report level label = 20 Pct Recovery = 104% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 42.335 Expected Conc. = 50.1 Report level label = 20 Pct Recovery = 85% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 54.784 Expected Conc. = 50.1 Report level label = 20 Pct Recovery = 109% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222000207 Lab Value = 42.791 Expected Conc. = 50 Report level label = 20 Pct Recovery = 86% Analysis Date = 07/27/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20202330309 Lab Value = 51.361 Expected Conc. = 49.92 Report level label = 20 Pct Recovery = 103% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 35.461 Expected Conc. = 49.92 Report level label = 20 Pct Recovery = 71% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 52.576 Expected Conc. = 49.92 Report level label = 20 Pct Recovery = 105% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 50.373 Expected Conc. = 49.92 Report level label = 20 Pct Recovery = 101% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 55.966 Expected Conc. = 49.92 Report level label = 20 Pct Recovery = 112% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Analysis Date = 08/15/22 Pct Recovery = 85% Analysis Date = 08/11/22 Pct Recovery = 85% Analysis Date = 08/11/22 Pct Recovery = 85% Analysis Date = 08/07/22 Pct Recovery = 85% Analysis Date = 08/07/22 Pct Recovery = 85% Analysis Date = 08/03/22 Pct Recovery = 85% Analysis Date = 08/03/22 Pct Recovery = 85% Analysis Date = 07/30/22 Pct Recovery = 84% Analysis Date = 07/30/22 Pct Recovery = 84% Analysis Date = 07/26/22 Pct Recovery = 84% Analysis Date = 07/26/22 Pct Recovery = 84% Analysis Date = 07/22/22 Pct Recovery = 84% Analysis Date = 07/22/22 Pct Recovery = 84% Analysis Date = 07/18/22 Pct Recovery = 84% Analysis Date = 07/18/22 Pct Recovery = 84% Analysis Date = 07/14/22 Pct Recovery = 84% Analysis Date = 07/14/22 Pct Recovery = 84% Analysis Date = 07/10/22 Pct Recovery = 83% Analysis Date = 07/10/22 Pct Recovery = 83% Analysis Date = 07/06/22 Pct Recovery = 83% Analysis Date = 07/06/22 Pct Recovery = 83% Analysis Date = 07/02/22 Pct Recovery = 83% Analysis Date = 07/02/22 Pct Recovery = 83% Analysis Date = 06/28/22 Pct Recovery = 83% Analysis Date = 06/28/22 Pct Recovery = 83% Analysis Date = 06/24/22 Pct Recovery = 82% Analysis Date = 06/24/22 Pct Recovery = 82% Analysis Date = 06/20/22 Pct Recovery = 82% Analysis Date = 06/20/22 Pct Recovery = 82% Analysis Date = 06/16/22 Pct Recovery = 82% Analysis Date = 06/16/22 Pct Recovery = 82% Analysis Date = 06/12/22 Pct Recovery = 81% Analysis Date = 06/12/22 Pct Recovery = 81% Analysis Date = 06/08/22 Pct Recovery = 81% Analysis Date = 06/08/22 Pct Recovery = 81% Analysis Date = 06/04/22 Pct Recovery = 81% Analysis Date = 06/04/22 Pct Recovery = 81% Analysis Date = 05/31/22 Pct Recovery = 80% Analysis Date = 05/31/22 Pct Recovery = 80% Analysis Date = 05/27/22 Pct Recovery = 80% Analysis Date = 05/27/22 Pct Recovery = 80% Analysis Date = 05/23/22 Pct Recovery = 79% Analysis Date = 05/23/22 Pct Recovery = 79% Analysis Date = 05/19/22 Pct Recovery = 79% Analysis Date = 05/19/22 Pct Recovery = 79% Analysis Date = 05/14/22 Pct Recovery = 79% Analysis Date = 05/14/22 Pct Recovery = 79% Analysis Date = 05/10/22 Pct Recovery = 78% Analysis Date = 05/10/22 Pct Recovery = 78% Analysis Date = 05/06/22 Pct Recovery = 78% Analysis Date = 05/06/22 Pct Recovery = 78% Analysis Date = 05/02/22 Pct Recovery = 77% Analysis Date = 05/02/22 Pct Recovery = 77% Analysis Date = 04/28/22 Pct Recovery = 77% Analysis Date = 04/28/22 Pct Recovery = 77% Analysis Date = 04/24/22 Pct Recovery = 77% Analysis Date = 04/24/22 Pct Recovery = 77% Analysis Date = 04/20/22 Pct Recovery = 76% Analysis Date = 04/20/22 Pct Recovery = 76% Analysis Date = 04/16/22 Pct Recovery = 76% Analysis Date = 04/16/22 Pct Recovery = 76% Analysis Date = 04/12/22 Pct Recovery = 75% Analysis Date = 04/12/22 Pct Recovery = 75% Analysis Date = 04/08/22 Pct Recovery = 75% Analysis Date = 04/08/22 Pct Recovery = 75% Analysis Date = 04/04/22 Pct Recovery = 75% Analysis Date = 04/04/22 Pct Recovery = 75% Analysis Date = 03/31/22 Pct Recovery = 74% Analysis Date = 03/31/22 Pct Recovery = 74% Analysis Date = 03/27/22 Pct Recovery = 74% Analysis Date = 03/27/22 Pct Recovery = 74% Analysis Date = 03/23/22 Pct Recovery = 73% Analysis Date = 03/23/22 Pct Recovery = 73% Analysis Date = 03/19/22 Pct Recovery = 73% Analysis Date = 03/19/22 Pct Recovery = 73% Analysis Date = 03/15/22 Pct Recovery = 73% Analysis Date = 03/15/22 Pct Recovery = 73% Analysis Date = 03/11/22 Pct Recovery = 72% Analysis Date = 03/11/22 Pct Recovery = 72% Analysis Date = 03/07/22 Pct Recovery = 72% Analysis Date = 03/07/22 Pct Recovery = 72% Analysis Date = 03/03/22 Pct Recovery = 71% Analysis Date = 03/03/22 Pct Recovery = 71% Analysis Date = 02/27/22 Pct Recovery = 71% Analysis Date = 02/27/22 Pct Recovery = 71% Analysis Date = 02/23/22 Pct Recovery = 71% Analysis Date = 02/23/22 Pct Recovery = 71% Analysis Date = 02/19/22 Pct Recovery = 70% Analysis Date = 02/19/22 Pct Recovery = 70% Analysis Date = 02/14/22 Pct Recovery = 70% Analysis Date = 02/14/22 Pct Recovery = 70% Analysis Date = 02/10/22 Pct Recovery = 69% Analysis Date = 02/10/22 Pct Recovery = 69% Analysis Date = 02/06/22 Pct Recovery = 69% Analysis Date = 02/06/22 Pct Recovery = 69% Analysis Date = 02/02/22 Pct Recovery = 69% Analysis Date = 02/02/22 Pct Recovery = 69% Analysis Date = 01/29/22 Pct Recovery = 68% Analysis Date = 01/29/22 Pct Recovery = 68% Analysis Date = 01/25/22 Pct Recovery = 68% Analysis Date = 01/25/22 Pct Recovery = 68% Analysis Date = 01/21/22 Pct Recovery = 67% Analysis Date = 01/21/22 Pct Recovery = 67% Analysis Date = 01/17/22 Pct Recovery = 67% Analysis Date = 01/17/22 Pct Recovery = 67% Analysis Date = 01/13/22 Pct Recovery = 67% Analysis Date = 01/13/22 Pct Recovery = 67% Analysis Date = 01/09/22 Pct Recovery = 66% Analysis Date = 01/09/22 Pct Recovery = 66% Analysis Date = 01/05/22 Pct Recovery = 66% Analysis Date = 01/05/22 Pct Recovery = 66% Analysis Date = 01/01/22 Pct Recovery = 65% Analysis Date = 01/01/22 Pct Recovery = 65% Analysis Date = 12/28/21 Pct Recovery = 65% Analysis Date = 12/28/21 Pct Recovery = 65% Analysis Date = 12/24/21 Pct Recovery = 65% Analysis Date = 12/24/21 Pct Recovery = 65% Analysis Date = 12/20/21 Pct Recovery = 64% Analysis Date = 12/20/21 Pct Recovery = 64% Analysis Date = 12/16/21 Pct Recovery = 64% Analysis Date = 12/16/21 Pct Recovery = 64% Analysis Date = 12/12/21 Pct Recovery = 64% Analysis Date = 12/12/21 Pct Recovery = 64% Analysis Date = 12/08/21 Pct Recovery = 63% Analysis Date = 12/08/21 Pct Recovery = 63% Analysis Date = 12/04/21 Pct Recovery = 63% Analysis Date = 12/04/21 Pct Recovery = 63% Analysis Date = 11/30/21 Pct Recovery = 62% Analysis Date = 11/30/21 Pct Recovery = 62% Analysis Date = 11/26/21 Pct Recovery = 62% Analysis Date = 11/26/21 Pct Recovery = 62% Analysis Date = 11/22/21 Pct Recovery = 62% Analysis Date = 11/22/21 Pct Recovery = 62% Analysis Date = 11/17/21 Pct Recovery = 61% Analysis Date = 11/17/21 Pct Recovery = 61% Analysis Date = 11/13/21 Pct Recovery = 61% Analysis Date = 11/13/21 Pct Recovery = 61% Analysis Date = 11/09/21 Pct Recovery = 60% Analysis Date = 11/09/21 Pct Recovery = 60% Analysis Date = 11/05/21 Pct Recovery = 60% Analysis Date = 11/05/21 Pct Recovery = 60% Analysis Date = 11/01/21 Pct Recovery = 60% Analysis Date = 11/01/21 Pct Recovery = 60% Analysis Date = 10/28/21 Pct Recovery = 59% Analysis Date = 10/28/21 Pct Recovery = 59% Analysis Date = 10/24/21 Pct Recovery = 59% Analysis Date = 10/24/21 Pct Recovery = 59% Analysis Date = 10/20/21 Pct Recovery = 58% Analysis Date = 10/20/21 Pct Recovery = 58% Analysis Date = 10/16/21 Pct Recovery = 58% Analysis Date = 10/16/21 Pct Recovery = 58% Analysis Date = 10/12/21 Pct Recovery = 58% Analysis Date = 10/12/21 Pct Recovery = 58% Analysis Date = 10/08/21 Pct Recovery = 57% Analysis Date = 10/08/21 Pct Recovery = 57% Analysis Date = 10/04/21 Pct Recovery = 57% Analysis Date = 10/04/21 Pct Recovery = 57% Analysis Date = 09/30/21 Pct Recovery = 56% Analysis Date = 09/30/21 Pct Recovery = 56% Analysis Date = 09/26/21 Pct Recovery = 56% Analysis Date = 09/26/21 Pct Recovery = 56% Analysis Date = 09/22/21 Pct Recovery = 56% Analysis Date = 09/22/21 Pct Recovery = 56% Analysis Date = 09/18/21 Pct Recovery = 55% Analysis Date = 09/18/21 Pct Recovery = 55% Analysis Date = 09/14/21 Pct Recovery = 55% Analysis Date = 09/14/21 Pct Recovery = 55% Analysis Date = 09/10/21 Pct Recovery = 54% Analysis Date = 09/10/21 Pct Recovery = 54% Analysis Date = 09/06/21 Pct Recovery = 54% Analysis Date = 09/06/21 Pct Recovery = 54% Analysis Date = 09/02/21 Pct Recovery = 54% Analysis Date = 09/02/21 Pct Recovery = 54% Analysis Date = 08/29/21 Pct Recovery = 53% Analysis Date = 08/29/21 Pct Recovery = 53% Analysis Date = 08/25/21 Pct Recovery = 53% Analysis Date = 08/25/21 Pct Recovery = 53% Analysis Date = 08/20/21 Pct Recovery = 52% Analysis Date = 08/20/21 Pct Recovery = 52% Analysis Date = 08/16/21 Pct Recovery = 52% Analysis Date = 08/16/21 Pct Recovery = 52% Analysis Date = 08/12/21 Pct Recovery = 52% Analysis Date = 08/12/21 Pct Recovery = 52% Analysis Date = 08/08/21 Pct Recovery = 51% Analysis Date = 08/08/21 Pct Recovery = 51% Analysis Date = 08/04/21 Pct Recovery = 51% Analysis Date = 08/04/21 Pct Recovery = 51% Analysis Date = 07/31/21 Pct Recovery = 50% Analysis Date = 07/31/21 Pct Recovery = 50% Analysis Date = 07/27/21 Pct Recovery = 50% Analysis Date = 07/27/21 Pct Recovery = 50% Analysis Date = 07/23/21 Pct Recovery = 50% Analysis Date = 07/23/21 Pct Recovery = 50% Analysis Date = 07/19/21 Pct Recovery = 49% Analysis Date = 07/19/21 Pct Recovery = 49% Analysis Date = 07/15/21 Pct Recovery = 49% Analysis Date = 07/15/21 Pct Recovery = 49% Analysis Date = 07/11/21 Pct Recovery = 48% Analysis Date = 07/11/21 Pct Recovery = 48% Analysis Date = 07/07/21 Pct Recovery = 48% Analysis Date = 07/07/21 Pct Recovery = 48% Analysis Date = 07/03/21 Pct Recovery = 48% Analysis Date = 07/03/21 Pct Recovery = 48% Analysis Date = 06/29/21 Pct Recovery = 47% Analysis Date = 06/29/21 Pct Recovery = 47% Analysis Date = 06/25/21 Pct Recovery = 47% Analysis Date = 06/25/21 Pct Recovery = 47% Analysis Date = 06/21/21 Pct Recovery = 46% Analysis Date = 06/21/21 Pct Recovery = 46% Analysis Date = 06/17/21 Pct Recovery = 46% Analysis Date = 06/17/21 Pct Recovery = 46% Analysis Date = 06/13/21 Pct Recovery = 46% Analysis Date = 06/13/21 Pct Recovery = 46% Analysis Date = 06/09/21 Pct Recovery = 45% Analysis Date = 06/09/21 Pct Recovery = 45% Analysis Date = 06/05/21 Pct Recovery = 45% Analysis Date = 06/05/21 Pct Recovery = 45% Analysis Date = 06/01/21 Pct Recovery = 45% Analysis Date = 06/01/21 Pct Recovery = 45% Analysis Date = 05/28/21 Pct Recovery = 44% Analysis Date = 05/28/21 Pct Recovery = 44% Analysis Date = 05/24/21 Pct Recovery = 44% Analysis Date = 05/24/21 Pct Recovery = 44% Analysis Date = 05/19/21 Pct Recovery = 43% Analysis Date = 05/19/21 Pct Recovery = 43% Analysis Date = 05/15/21 Pct Recovery = 43% Analysis Date = 05/15/21 Pct Recovery = 43% Analysis Date = 05/11/21 Pct Recovery = 43% Analysis Date = 05/11/21 Pct Recovery = 43% Analysis Date = 05/07/21 Pct Recovery = 42% Analysis Date = 05/07/21 Pct Recovery = 42% Analysis Date = 05/03/21 Pct Recovery = 42% Analysis Date = 05/03/21 Pct Recovery = 42% Analysis Date = 04/29/21 Pct Recovery = 41% Analysis Date = 04/29/21 Pct Recovery = 41% Analysis Date = 04/25/21 Pct Recovery = 41% Analysis Date = 04/25/21 Pct Recovery = 41% Analysis Date = 04/21/21 Pct Recovery = 41% Analysis Date = 04/21/21 Pct Recovery = 41% Analysis Date = 04/17/21 Pct Recovery = 40% Analysis Date = 04/17/21 Pct Recovery = 40% Analysis Date = 04/13/21 Pct Recovery = 40% Analysis Date = 04/13/21 Pct Recovery = 40% Analysis Date = 04/09/21 Pct Recovery = 41% Analysis Date = 04/09/21 Pct Recovery = 41% Analysis Date = 04/05/21 Pct Recovery = 43% Analysis Date = 04/05/21 Pct Recovery = 43% Analysis Date = 04/01/21 Pct Recovery = 44% Analysis Date = 04/01/21 Pct Recovery = 44% Analysis Date = 03/28/21 Pct Recovery = 46% Analysis Date = 03/28/21 Pct Recovery = 46% Analysis Date = 03/24/21 Pct Recovery = 47% Analysis Date = 03/24/21 Pct Recovery = 47% Analysis Date = 03/20/21 Pct Recovery = 48% Analysis Date = 03/20/21 Pct Recovery = 48% Analysis Date = 03/16/21 Pct Recovery = 50% Analysis Date = 03/16/21 Pct Recovery = 50% Analysis Date = 03/12/21 Pct Recovery = 51% Analysis Date = 03/12/21 Pct Recovery = 51% Analysis Date = 03/08/21 Pct Recovery = 53% Analysis Date = 03/08/21 Pct Recovery = 53% Analysis Date = 03/04/21 Pct Recovery = 54% Analysis Date = 03/04/21 Pct Recovery = 54% Analysis Date = 02/28/21 Pct Recovery = 55% Analysis Date = 02/28/21 Pct Recovery = 55% Analysis Date = 02/24/21 Pct Recovery = 56% Analysis Date = 02/24/21 Pct Recovery = 56% Analysis Date = 02/19/21 Pct Recovery = 58% Analysis Date = 02/19/21 Pct Recovery = 58% Analysis Date = 02/15/21 Pct Recovery = 59% Analysis Date = 02/15/21 Pct Recovery = 59% Analysis Date = 02/11/21 Pct Recovery = 60% Analysis Date = 02/11/21 Pct Recovery = 60% Analysis Date = 02/07/21 Pct Recovery = 62% Analysis Date = 02/07/21 Pct Recovery = 62% Analysis Date = 02/03/21 Pct Recovery = 63% Analysis Date = 02/03/21 Pct Recovery = 63% Analysis Date = 01/30/21 Pct Recovery = 64% Analysis Date = 01/30/21 Pct Recovery = 64% Analysis Date = 01/26/21 Pct Recovery = 65% Analysis Date = 01/26/21 Pct Recovery = 65% Analysis Date = 01/22/21 Pct Recovery = 67% Analysis Date = 01/22/21 Pct Recovery = 67% Analysis Date = 01/18/21 Pct Recovery = 68% Analysis Date = 01/18/21 Pct Recovery = 68% Analysis Date = 01/14/21 Pct Recovery = 69% Analysis Date = 01/14/21 Pct Recovery = 69% Analysis Date = 01/10/21 Pct Recovery = 71% Analysis Date = 01/10/21 Pct Recovery = 71% Analysis Date = 01/06/21 Pct Recovery = 72% Analysis Date = 01/06/21 Pct Recovery = 72% Analysis Date = 01/02/21 Pct Recovery = 73% Analysis Date = 01/02/21 Pct Recovery = 73% Analysis Date = 12/29/20 Pct Recovery = 75% Analysis Date = 12/29/20 Pct Recovery = 75% Analysis Date = 12/25/20 Pct Recovery = 76% Analysis Date = 12/25/20 Pct Recovery = 76% Analysis Date = 12/21/20 Pct Recovery = 77% Analysis Date = 12/21/20 Pct Recovery = 77% Analysis Date = 12/17/20 Pct Recovery = 79% Analysis Date = 12/17/20 Pct Recovery = 79% Analysis Date = 12/13/20 Pct Recovery = 81% Analysis Date = 12/13/20 Pct Recovery = 81% Analysis Date = 12/09/20 Pct Recovery = 82% Analysis Date = 12/09/20 Pct Recovery = 82% Analysis Date = 12/05/20 Pct Recovery = 84% Analysis Date = 12/05/20 Pct Recovery = 84% Analysis Date = 12/01/20 Pct Recovery = 85% Analysis Date = 12/01/20 Pct Recovery = 85% Analysis Date = 11/27/20 Pct Recovery = 87% Analysis Date = 11/27/20 Pct Recovery = 87% Analysis Date = 11/22/20 Pct Recovery = 89% Analysis Date = 11/22/20 Pct Recovery = 89% Analysis Date = 11/18/20 Pct Recovery = 90% Analysis Date = 11/18/20 Pct Recovery = 90% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/10/20 Pct Recovery = 92% Analysis Date = 11/10/20 Pct Recovery = 92% Analysis Date = 11/06/20 Pct Recovery = 92% Analysis Date = 11/06/20 Pct Recovery = 92% Analysis Date = 11/02/20 Pct Recovery = 93% Analysis Date = 11/02/20 Pct Recovery = 93% Analysis Date = 10/29/20 Pct Recovery = 93% Analysis Date = 10/29/20 Pct Recovery = 93% Analysis Date = 10/25/20 Pct Recovery = 93% Analysis Date = 10/25/20 Pct Recovery = 93% Analysis Date = 10/21/20 Pct Recovery = 94% Analysis Date = 10/21/20 Pct Recovery = 94% Analysis Date = 10/17/20 Pct Recovery = 94% Analysis Date = 10/17/20 Pct Recovery = 94% Analysis Date = 10/13/20 Pct Recovery = 95% Analysis Date = 10/13/20 Pct Recovery = 95% Analysis Date = 10/09/20 Pct Recovery = 95% Analysis Date = 10/09/20 Pct Recovery = 95% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/01/20 Pct Recovery = 96% Analysis Date = 10/01/20 Pct Recovery = 96% Analysis Date = 09/27/20 Pct Recovery = 96% Analysis Date = 09/27/20 Pct Recovery = 96% Analysis Date = 09/23/20 Pct Recovery = 97% Analysis Date = 09/23/20 Pct Recovery = 97% Analysis Date = 09/19/20 Pct Recovery = 97% Analysis Date = 09/19/20 Pct Recovery = 97% Analysis Date = 09/15/20 Pct Recovery = 98% Analysis Date = 09/15/20 Pct Recovery = 98% Analysis Date = 09/11/20 Pct Recovery = 99% Analysis Date = 09/11/20 Pct Recovery = 99% Analysis Date = 09/07/20 Pct Recovery = 99% Analysis Date = 09/07/20 Pct Recovery = 99% Analysis Date = 09/03/20 Pct Recovery = 100% Analysis Date = 09/03/20 Pct Recovery = 100% Analysis Date = 08/30/20 Pct Recovery = 100% Analysis Date = 08/30/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 102% Analysis Date = 08/21/20 Pct Recovery = 102% Analysis Date = 08/17/20 Pct Recovery = 103% Analysis Date = 08/17/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 104% Analysis Date = 08/09/20 Pct Recovery = 104% Analysis Date = 08/05/20 Pct Recovery = 105% Analysis Date = 08/05/20 Pct Recovery = 105% Analysis Date = 08/01/20 Pct Recovery = 105% Analysis Date = 08/01/20 Pct Recovery = 105% Analysis Date = 07/28/20 Pct Recovery = 106% Analysis Date = 07/28/20 Pct Recovery = 106% Analysis Date = 07/24/20 Pct Recovery = 107% Analysis Date = 07/24/20 Pct Recovery = 107% Analysis Date = 07/20/20 Pct Recovery = 107% Analysis Date = 07/20/20 Pct Recovery = 107% Analysis Date = 07/16/20 Pct Recovery = 108% Analysis Date = 07/16/20 Pct Recovery = 108% Analysis Date = 07/12/20 Pct Recovery = 109% Analysis Date = 07/12/20 Pct Recovery = 109% Analysis Date = 07/08/20 Pct Recovery = 110% Analysis Date = 07/08/20 Pct Recovery = 110% Analysis Date = 07/04/20 Pct Recovery = 110% Analysis Date = 07/04/20 Pct Recovery = 110% Analysis Date = 06/30/20 Pct Recovery = 111% Analysis Date = 06/30/20 Pct Recovery = 111% Analysis Date = 06/26/20 Pct Recovery = 112% Analysis Date = 06/26/20 Pct Recovery = 112% Analysis Date = 06/22/20 Pct Recovery = 112% Analysis Date = 06/22/20 Pct Recovery = 112% Analysis Date = 06/18/20 Pct Recovery = 113% Analysis Date = 06/18/20 Pct Recovery = 113% Analysis Date = 06/14/20 Pct Recovery = 114% Analysis Date = 06/14/20 Pct Recovery = 114% Analysis Date = 06/10/20 Pct Recovery = 115% Analysis Date = 06/10/20 Pct Recovery = 115% Analysis Date = 06/06/20 Pct Recovery = 115% Analysis Date = 06/06/20 Pct Recovery = 115% Analysis Date = 06/02/20 Pct Recovery = 116% Analysis Date = 06/02/20 Pct Recovery = 116% Analysis Date = 05/29/20 Pct Recovery = 117% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEISOPROPYLATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 88% 29% 92% 20%
Total 32 88% 29% 92% 20%

Sample Statistics
DEISOPROPYLATRAZINE

Characteristic N % % Basis
Plotted 32 97% Spiked
Estimated Values 5 15% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 33 .  
False Negatives 1 3% 1 out of 33
Not Spiked 83 .  
False Positives 1 1% 1 out of 83

OBSP Determination:
DESULFINYLFIPRONIL
METHOD: 2447 , TESTIDCODE: 66607LCM60

Laboratory ID = 20221940194 Lab Value = 452.378 Expected Conc. = 38 Report level label = 3.8 Pct Recovery = 1190% Analysis Date = 07/21/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20222000207 Lab Value = 82.313 Expected Conc. = 9.5 Report level label = 3.8 Pct Recovery = 866% Analysis Date = 07/26/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20203230021 Lab Value = 55.004 Expected Conc. = 47.92 Report level label = 3.8 Pct Recovery = 115% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 54.019 Expected Conc. = 47.92 Report level label = 3.8 Pct Recovery = 113% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590107 Lab Value = 50.121 Expected Conc. = 47 Report level label = 3.8 Pct Recovery = 107% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 54.898 Expected Conc. = 47 Report level label = 3.8 Pct Recovery = 117% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221370164 Lab Value = 28.012 Expected Conc. = 38.28 Report level label = 3.8 Pct Recovery = 73% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 38.040 Expected Conc. = 38 Report level label = 3.8 Pct Recovery = 100% Analysis Date = 08/17/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221580147 Lab Value = 26.706 Expected Conc. = 38 Report level label = 3.8 Pct Recovery = 70% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20201550031 Lab Value = 26.270 Expected Conc. = 23.8 Report level label = 3.8 Pct Recovery = 110% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20222070177 Lab Value = 18.241 Expected Conc. = 23.75 Report level label = 3.8 Pct Recovery = 77% Analysis Date = 08/02/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20203360042 Lab Value = 19.079 Expected Conc. = 23.5 Report level label = 3.8 Pct Recovery = 81% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 22.740 Expected Conc. = 23.5 Report level label = 3.8 Pct Recovery = 97% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 23.628 Expected Conc. = 23.5 Report level label = 3.8 Pct Recovery = 101% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 28.469 Expected Conc. = 23.45 Report level label = 3.8 Pct Recovery = 121% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 24.524 Expected Conc. = 23.45 Report level label = 3.8 Pct Recovery = 105% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 21.388 Expected Conc. = 18.76 Report level label = 3.8 Pct Recovery = 114% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 20.033 Expected Conc. = 18.76 Report level label = 3.8 Pct Recovery = 107% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210830019 Lab Value = 8.206 Expected Conc. = 9.584 Report level label = 3.8 Pct Recovery = 86% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 9.489 Expected Conc. = 9.584 Report level label = 3.8 Pct Recovery = 99% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20221160208 Lab Value = 5.911 Expected Conc. = 9.57 Report level label = 3.8 Pct Recovery = 62% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20202330309 Lab Value = 8.706 Expected Conc. = 9.52 Report level label = 3.8 Pct Recovery = 91% Analysis Date = 09/01/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 9.093 Expected Conc. = 9.52 Report level label = 3.8 Pct Recovery = 96% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 9.560 Expected Conc. = 9.52 Report level label = 3.8 Pct Recovery = 100% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 8.228 Expected Conc. = 9.52 Report level label = 3.8 Pct Recovery = 86% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 8.975 Expected Conc. = 9.52 Report level label = 3.8 Pct Recovery = 94% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210970035 Lab Value = 9.731 Expected Conc. = 9.4 Report level label = 3.8 Pct Recovery = 104% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 8.965 Expected Conc. = 9.4 Report level label = 3.8 Pct Recovery = 95% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 9.056 Expected Conc. = 9.4 Report level label = 3.8 Pct Recovery = 96% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 9.767 Expected Conc. = 9.4 Report level label = 3.8 Pct Recovery = 104% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 8.166 Expected Conc. = 9.4 Report level label = 3.8 Pct Recovery = 87% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 9.247 Expected Conc. = 9.4 Report level label = 3.8 Pct Recovery = 98% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 10/17/21 Pct Recovery = 205% Analysis Date = 10/17/21 Pct Recovery = 205% Analysis Date = 10/13/21 Pct Recovery = 202% Analysis Date = 10/13/21 Pct Recovery = 202% Analysis Date = 10/09/21 Pct Recovery = 200% Analysis Date = 10/09/21 Pct Recovery = 200% Analysis Date = 10/05/21 Pct Recovery = 198% Analysis Date = 10/05/21 Pct Recovery = 198% Analysis Date = 10/01/21 Pct Recovery = 196% Analysis Date = 10/01/21 Pct Recovery = 196% Analysis Date = 09/27/21 Pct Recovery = 194% Analysis Date = 09/27/21 Pct Recovery = 194% Analysis Date = 09/23/21 Pct Recovery = 191% Analysis Date = 09/23/21 Pct Recovery = 191% Analysis Date = 09/19/21 Pct Recovery = 189% Analysis Date = 09/19/21 Pct Recovery = 189% Analysis Date = 09/15/21 Pct Recovery = 187% Analysis Date = 09/15/21 Pct Recovery = 187% Analysis Date = 09/11/21 Pct Recovery = 185% Analysis Date = 09/11/21 Pct Recovery = 185% Analysis Date = 09/07/21 Pct Recovery = 183% Analysis Date = 09/07/21 Pct Recovery = 183% Analysis Date = 09/03/21 Pct Recovery = 180% Analysis Date = 09/03/21 Pct Recovery = 180% Analysis Date = 08/30/21 Pct Recovery = 178% Analysis Date = 08/30/21 Pct Recovery = 178% Analysis Date = 08/26/21 Pct Recovery = 176% Analysis Date = 08/26/21 Pct Recovery = 176% Analysis Date = 08/21/21 Pct Recovery = 174% Analysis Date = 08/21/21 Pct Recovery = 174% Analysis Date = 08/17/21 Pct Recovery = 171% Analysis Date = 08/17/21 Pct Recovery = 171% Analysis Date = 08/13/21 Pct Recovery = 169% Analysis Date = 08/13/21 Pct Recovery = 169% Analysis Date = 08/09/21 Pct Recovery = 167% Analysis Date = 08/09/21 Pct Recovery = 167% Analysis Date = 08/05/21 Pct Recovery = 165% Analysis Date = 08/05/21 Pct Recovery = 165% Analysis Date = 08/01/21 Pct Recovery = 163% Analysis Date = 08/01/21 Pct Recovery = 163% Analysis Date = 07/28/21 Pct Recovery = 160% Analysis Date = 07/28/21 Pct Recovery = 160% Analysis Date = 07/24/21 Pct Recovery = 158% Analysis Date = 07/24/21 Pct Recovery = 158% Analysis Date = 07/20/21 Pct Recovery = 156% Analysis Date = 07/20/21 Pct Recovery = 156% Analysis Date = 07/16/21 Pct Recovery = 154% Analysis Date = 07/16/21 Pct Recovery = 154% Analysis Date = 07/12/21 Pct Recovery = 152% Analysis Date = 07/12/21 Pct Recovery = 152% Analysis Date = 07/08/21 Pct Recovery = 149% Analysis Date = 07/08/21 Pct Recovery = 149% Analysis Date = 07/04/21 Pct Recovery = 147% Analysis Date = 07/04/21 Pct Recovery = 147% Analysis Date = 06/30/21 Pct Recovery = 145% Analysis Date = 06/30/21 Pct Recovery = 145% Analysis Date = 06/26/21 Pct Recovery = 143% Analysis Date = 06/26/21 Pct Recovery = 143% Analysis Date = 06/22/21 Pct Recovery = 140% Analysis Date = 06/22/21 Pct Recovery = 140% Analysis Date = 06/18/21 Pct Recovery = 138% Analysis Date = 06/18/21 Pct Recovery = 138% Analysis Date = 06/14/21 Pct Recovery = 136% Analysis Date = 06/14/21 Pct Recovery = 136% Analysis Date = 06/10/21 Pct Recovery = 134% Analysis Date = 06/10/21 Pct Recovery = 134% Analysis Date = 06/06/21 Pct Recovery = 132% Analysis Date = 06/06/21 Pct Recovery = 132% Analysis Date = 06/02/21 Pct Recovery = 129% Analysis Date = 06/02/21 Pct Recovery = 129% Analysis Date = 05/29/21 Pct Recovery = 127% Analysis Date = 05/29/21 Pct Recovery = 127% Analysis Date = 05/25/21 Pct Recovery = 125% Analysis Date = 05/25/21 Pct Recovery = 125% Analysis Date = 05/20/21 Pct Recovery = 123% Analysis Date = 05/20/21 Pct Recovery = 123% Analysis Date = 05/16/21 Pct Recovery = 121% Analysis Date = 05/16/21 Pct Recovery = 121% Analysis Date = 05/12/21 Pct Recovery = 118% Analysis Date = 05/12/21 Pct Recovery = 118% Analysis Date = 05/08/21 Pct Recovery = 116% Analysis Date = 05/08/21 Pct Recovery = 116% Analysis Date = 05/04/21 Pct Recovery = 114% Analysis Date = 05/04/21 Pct Recovery = 114% Analysis Date = 04/30/21 Pct Recovery = 112% Analysis Date = 04/30/21 Pct Recovery = 112% Analysis Date = 04/26/21 Pct Recovery = 109% Analysis Date = 04/26/21 Pct Recovery = 109% Analysis Date = 04/22/21 Pct Recovery = 107% Analysis Date = 04/22/21 Pct Recovery = 107% Analysis Date = 04/18/21 Pct Recovery = 105% Analysis Date = 04/18/21 Pct Recovery = 105% Analysis Date = 04/14/21 Pct Recovery = 103% Analysis Date = 04/14/21 Pct Recovery = 103% Analysis Date = 04/10/21 Pct Recovery = 101% Analysis Date = 04/10/21 Pct Recovery = 101% Analysis Date = 04/06/21 Pct Recovery = 98% Analysis Date = 04/06/21 Pct Recovery = 98% Analysis Date = 04/02/21 Pct Recovery = 96% Analysis Date = 04/02/21 Pct Recovery = 96% Analysis Date = 03/29/21 Pct Recovery = 95% Analysis Date = 03/29/21 Pct Recovery = 95% Analysis Date = 03/25/21 Pct Recovery = 95% Analysis Date = 03/25/21 Pct Recovery = 95% Analysis Date = 03/21/21 Pct Recovery = 95% Analysis Date = 03/21/21 Pct Recovery = 95% Analysis Date = 03/17/21 Pct Recovery = 95% Analysis Date = 03/17/21 Pct Recovery = 95% Analysis Date = 03/13/21 Pct Recovery = 96% Analysis Date = 03/13/21 Pct Recovery = 96% Analysis Date = 03/09/21 Pct Recovery = 96% Analysis Date = 03/09/21 Pct Recovery = 96% Analysis Date = 03/05/21 Pct Recovery = 96% Analysis Date = 03/05/21 Pct Recovery = 96% Analysis Date = 03/01/21 Pct Recovery = 96% Analysis Date = 03/01/21 Pct Recovery = 96% Analysis Date = 02/25/21 Pct Recovery = 96% Analysis Date = 02/25/21 Pct Recovery = 96% Analysis Date = 02/20/21 Pct Recovery = 96% Analysis Date = 02/20/21 Pct Recovery = 96% Analysis Date = 02/16/21 Pct Recovery = 96% Analysis Date = 02/16/21 Pct Recovery = 96% Analysis Date = 02/12/21 Pct Recovery = 97% Analysis Date = 02/12/21 Pct Recovery = 97% Analysis Date = 02/08/21 Pct Recovery = 97% Analysis Date = 02/08/21 Pct Recovery = 97% Analysis Date = 02/04/21 Pct Recovery = 97% Analysis Date = 02/04/21 Pct Recovery = 97% Analysis Date = 01/31/21 Pct Recovery = 97% Analysis Date = 01/31/21 Pct Recovery = 97% Analysis Date = 01/27/21 Pct Recovery = 97% Analysis Date = 01/27/21 Pct Recovery = 97% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/19/21 Pct Recovery = 98% Analysis Date = 01/19/21 Pct Recovery = 98% Analysis Date = 01/15/21 Pct Recovery = 98% Analysis Date = 01/15/21 Pct Recovery = 98% Analysis Date = 01/11/21 Pct Recovery = 98% Analysis Date = 01/11/21 Pct Recovery = 98% Analysis Date = 01/07/21 Pct Recovery = 98% Analysis Date = 01/07/21 Pct Recovery = 98% Analysis Date = 01/03/21 Pct Recovery = 98% Analysis Date = 01/03/21 Pct Recovery = 98% Analysis Date = 12/30/20 Pct Recovery = 98% Analysis Date = 12/30/20 Pct Recovery = 98% Analysis Date = 12/26/20 Pct Recovery = 99% Analysis Date = 12/26/20 Pct Recovery = 99% Analysis Date = 12/22/20 Pct Recovery = 99% Analysis Date = 12/22/20 Pct Recovery = 99% Analysis Date = 12/18/20 Pct Recovery = 99% Analysis Date = 12/18/20 Pct Recovery = 99% Analysis Date = 12/14/20 Pct Recovery = 99% Analysis Date = 12/14/20 Pct Recovery = 99% Analysis Date = 12/10/20 Pct Recovery = 99% Analysis Date = 12/10/20 Pct Recovery = 99% Analysis Date = 12/06/20 Pct Recovery = 100% Analysis Date = 12/06/20 Pct Recovery = 100% Analysis Date = 12/02/20 Pct Recovery = 100% Analysis Date = 12/02/20 Pct Recovery = 100% Analysis Date = 11/28/20 Pct Recovery = 100% Analysis Date = 11/28/20 Pct Recovery = 100% Analysis Date = 11/23/20 Pct Recovery = 101% Analysis Date = 11/23/20 Pct Recovery = 101% Analysis Date = 11/19/20 Pct Recovery = 101% Analysis Date = 11/19/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 101% Analysis Date = 11/11/20 Pct Recovery = 102% Analysis Date = 11/11/20 Pct Recovery = 102% Analysis Date = 11/07/20 Pct Recovery = 102% Analysis Date = 11/07/20 Pct Recovery = 102% Analysis Date = 11/03/20 Pct Recovery = 102% Analysis Date = 11/03/20 Pct Recovery = 102% Analysis Date = 10/30/20 Pct Recovery = 102% Analysis Date = 10/30/20 Pct Recovery = 102% Analysis Date = 10/26/20 Pct Recovery = 103% Analysis Date = 10/26/20 Pct Recovery = 103% Analysis Date = 10/22/20 Pct Recovery = 103% Analysis Date = 10/22/20 Pct Recovery = 103% Analysis Date = 10/18/20 Pct Recovery = 103% Analysis Date = 10/18/20 Pct Recovery = 103% Analysis Date = 10/14/20 Pct Recovery = 103% Analysis Date = 10/14/20 Pct Recovery = 103% Analysis Date = 10/10/20 Pct Recovery = 103% Analysis Date = 10/10/20 Pct Recovery = 103% Analysis Date = 10/06/20 Pct Recovery = 103% Analysis Date = 10/06/20 Pct Recovery = 103% Analysis Date = 10/02/20 Pct Recovery = 103% Analysis Date = 10/02/20 Pct Recovery = 103% Analysis Date = 09/28/20 Pct Recovery = 104% Analysis Date = 09/28/20 Pct Recovery = 104% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/20/20 Pct Recovery = 104% Analysis Date = 09/20/20 Pct Recovery = 104% Analysis Date = 09/16/20 Pct Recovery = 104% Analysis Date = 09/16/20 Pct Recovery = 104% Analysis Date = 09/12/20 Pct Recovery = 104% Analysis Date = 09/12/20 Pct Recovery = 104% Analysis Date = 09/08/20 Pct Recovery = 104% Analysis Date = 09/08/20 Pct Recovery = 104% Analysis Date = 09/04/20 Pct Recovery = 104% Analysis Date = 09/04/20 Pct Recovery = 104% Analysis Date = 08/31/20 Pct Recovery = 104% Analysis Date = 08/31/20 Pct Recovery = 104% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/18/20 Pct Recovery = 103% Analysis Date = 08/18/20 Pct Recovery = 103% Analysis Date = 08/14/20 Pct Recovery = 103% Analysis Date = 08/14/20 Pct Recovery = 103% Analysis Date = 08/10/20 Pct Recovery = 103% Analysis Date = 08/10/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/06/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 103% Analysis Date = 08/02/20 Pct Recovery = 103% Analysis Date = 07/29/20 Pct Recovery = 103% Analysis Date = 07/29/20 Pct Recovery = 103% Analysis Date = 07/25/20 Pct Recovery = 103% Analysis Date = 07/25/20 Pct Recovery = 103% Analysis Date = 07/21/20 Pct Recovery = 103% Analysis Date = 07/21/20 Pct Recovery = 103% Analysis Date = 07/17/20 Pct Recovery = 102% Analysis Date = 07/17/20 Pct Recovery = 102% Analysis Date = 07/13/20 Pct Recovery = 102% Analysis Date = 07/13/20 Pct Recovery = 102% Analysis Date = 07/09/20 Pct Recovery = 102% Analysis Date = 07/09/20 Pct Recovery = 102% Analysis Date = 07/05/20 Pct Recovery = 102% Analysis Date = 07/05/20 Pct Recovery = 102% Analysis Date = 07/01/20 Pct Recovery = 102% Analysis Date = 07/01/20 Pct Recovery = 102% Analysis Date = 06/27/20 Pct Recovery = 102% Analysis Date = 06/27/20 Pct Recovery = 102% Analysis Date = 06/23/20 Pct Recovery = 101% Analysis Date = 06/23/20 Pct Recovery = 101% Analysis Date = 06/19/20 Pct Recovery = 101% Analysis Date = 06/19/20 Pct Recovery = 101% Analysis Date = 06/15/20 Pct Recovery = 101% Analysis Date = 06/15/20 Pct Recovery = 101% Analysis Date = 06/11/20 Pct Recovery = 101% Analysis Date = 06/11/20 Pct Recovery = 101% Analysis Date = 06/07/20 Pct Recovery = 101% Analysis Date = 06/07/20 Pct Recovery = 101% Analysis Date = 06/03/20 Pct Recovery = 101% Analysis Date = 06/03/20 Pct Recovery = 101% Analysis Date = 05/30/20 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 155% 233% 100% 14%
Total 32 155% 233% 100% 14%

Sample Statistics
DESULFINYLFIPRONIL

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 84 .  
False Positives 2 2% 2 out of 84

OBSP Determination:
DIAZINON
METHOD: 2447 , TESTIDCODE: 65078LCM60

Laboratory ID = 20202590106 Lab Value = 75.466 Expected Conc. = 80.3 Report level label = 6.4 Pct Recovery = 94% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 78.697 Expected Conc. = 80.3 Report level label = 6.4 Pct Recovery = 98% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 53.948 Expected Conc. = 80 Report level label = 6.4 Pct Recovery = 67% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 55.760 Expected Conc. = 80 Report level label = 6.4 Pct Recovery = 70% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20212990174 Lab Value = 35.741 Expected Conc. = 65.44 Report level label = 6.4 Pct Recovery = 55% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 36.486 Expected Conc. = 64.48 Report level label = 6.4 Pct Recovery = 57% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 39.589 Expected Conc. = 64.48 Report level label = 6.4 Pct Recovery = 61% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 27.685 Expected Conc. = 64 Report level label = 6.4 Pct Recovery = 43% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20222150193 Lab Value = 10.422 Expected Conc. = 63.2 Report level label = 6.4 Pct Recovery = 16% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220810134 Lab Value = 23.893 Expected Conc. = 63.2 Report level label = 6.4 Pct Recovery = 38% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20213340027 Lab Value = 23.191 Expected Conc. = 40.9 Report level label = 6.4 Pct Recovery = 57% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 68.155 Expected Conc. = 40.9 Report level label = 6.4 Pct Recovery = 167% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 19.220 Expected Conc. = 40.9 Report level label = 6.4 Pct Recovery = 47% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 26.501 Expected Conc. = 40.3 Report level label = 6.4 Pct Recovery = 66% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 23.777 Expected Conc. = 40.3 Report level label = 6.4 Pct Recovery = 59% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20203230018 Lab Value = 30.407 Expected Conc. = 40.15 Report level label = 6.4 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 33.759 Expected Conc. = 40.15 Report level label = 6.4 Pct Recovery = 84% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 40.014 Expected Conc. = 40.15 Report level label = 6.4 Pct Recovery = 100% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220810133 Lab Value = 15.018 Expected Conc. = 39.5 Report level label = 6.4 Pct Recovery = 38% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20202390020 Lab Value = 27.148 Expected Conc. = 17.5 Report level label = 6.4 Pct Recovery = 155% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 19.364 Expected Conc. = 17.5 Report level label = 6.4 Pct Recovery = 111% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201550031 Lab Value = 23.693 Expected Conc. = 17.2 Report level label = 6.4 Pct Recovery = 138% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20213060210 Lab Value = 6.054 Expected Conc. = 16.36 Report level label = 6.4 Pct Recovery = 37% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222500483 Lab Value = 13.817 Expected Conc. = 16.12 Report level label = 6.4 Pct Recovery = 86% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 9.019 Expected Conc. = 16.12 Report level label = 6.4 Pct Recovery = 56% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210970035 Lab Value = 12.653 Expected Conc. = 16.06 Report level label = 6.4 Pct Recovery = 79% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 16.332 Expected Conc. = 16.06 Report level label = 6.4 Pct Recovery = 102% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 15.998 Expected Conc. = 16.06 Report level label = 6.4 Pct Recovery = 100% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 18.916 Expected Conc. = 16.06 Report level label = 6.4 Pct Recovery = 118% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 17.346 Expected Conc. = 16.06 Report level label = 6.4 Pct Recovery = 108% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 13.984 Expected Conc. = 16.06 Report level label = 6.4 Pct Recovery = 87% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210830019 Lab Value = 14.630 Expected Conc. = 16 Report level label = 6.4 Pct Recovery = 91% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 14.629 Expected Conc. = 16 Report level label = 6.4 Pct Recovery = 91% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222630205 Lab Value = 4.735 Expected Conc. = 15.8 Report level label = 6.4 Pct Recovery = 30% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20201960104 Lab Value = 24.217 Expected Conc. = 14 Report level label = 6.4 Pct Recovery = 173% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 16.350 Expected Conc. = 14 Report level label = 6.4 Pct Recovery = 117% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20202330309 Lab Value = 6.613 Expected Conc. = 6.88 Report level label = 6.4 Pct Recovery = 96% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 7.192 Expected Conc. = 6.88 Report level label = 6.4 Pct Recovery = 105% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 9.803 Expected Conc. = 6.88 Report level label = 6.4 Pct Recovery = 142% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 9.692 Expected Conc. = 6.88 Report level label = 6.4 Pct Recovery = 141% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 7.757 Expected Conc. = 6.88 Report level label = 6.4 Pct Recovery = 113% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Analysis Date = 09/28/22 Pct Recovery = 42% Analysis Date = 09/24/22 Pct Recovery = 42% Analysis Date = 09/24/22 Pct Recovery = 42% Analysis Date = 09/20/22 Pct Recovery = 43% Analysis Date = 09/20/22 Pct Recovery = 43% Analysis Date = 09/16/22 Pct Recovery = 43% Analysis Date = 09/16/22 Pct Recovery = 43% Analysis Date = 09/11/22 Pct Recovery = 43% Analysis Date = 09/11/22 Pct Recovery = 43% Analysis Date = 09/07/22 Pct Recovery = 44% Analysis Date = 09/07/22 Pct Recovery = 44% Analysis Date = 09/03/22 Pct Recovery = 44% Analysis Date = 09/03/22 Pct Recovery = 44% Analysis Date = 08/30/22 Pct Recovery = 44% Analysis Date = 08/30/22 Pct Recovery = 44% Analysis Date = 08/25/22 Pct Recovery = 45% Analysis Date = 08/25/22 Pct Recovery = 45% Analysis Date = 08/21/22 Pct Recovery = 45% Analysis Date = 08/21/22 Pct Recovery = 45% Analysis Date = 08/17/22 Pct Recovery = 45% Analysis Date = 08/17/22 Pct Recovery = 45% Analysis Date = 08/13/22 Pct Recovery = 45% Analysis Date = 08/13/22 Pct Recovery = 45% Analysis Date = 08/08/22 Pct Recovery = 46% Analysis Date = 08/08/22 Pct Recovery = 46% Analysis Date = 08/04/22 Pct Recovery = 46% Analysis Date = 08/04/22 Pct Recovery = 46% Analysis Date = 07/31/22 Pct Recovery = 46% Analysis Date = 07/31/22 Pct Recovery = 46% Analysis Date = 07/27/22 Pct Recovery = 47% Analysis Date = 07/27/22 Pct Recovery = 47% Analysis Date = 07/22/22 Pct Recovery = 47% Analysis Date = 07/22/22 Pct Recovery = 47% Analysis Date = 07/18/22 Pct Recovery = 47% Analysis Date = 07/18/22 Pct Recovery = 47% Analysis Date = 07/14/22 Pct Recovery = 48% Analysis Date = 07/14/22 Pct Recovery = 48% Analysis Date = 07/09/22 Pct Recovery = 48% Analysis Date = 07/09/22 Pct Recovery = 48% Analysis Date = 07/05/22 Pct Recovery = 48% Analysis Date = 07/05/22 Pct Recovery = 48% Analysis Date = 07/01/22 Pct Recovery = 49% Analysis Date = 07/01/22 Pct Recovery = 49% Analysis Date = 06/27/22 Pct Recovery = 49% Analysis Date = 06/27/22 Pct Recovery = 49% Analysis Date = 06/22/22 Pct Recovery = 49% Analysis Date = 06/22/22 Pct Recovery = 49% Analysis Date = 06/18/22 Pct Recovery = 50% Analysis Date = 06/18/22 Pct Recovery = 50% Analysis Date = 06/14/22 Pct Recovery = 50% Analysis Date = 06/14/22 Pct Recovery = 50% Analysis Date = 06/10/22 Pct Recovery = 50% Analysis Date = 06/10/22 Pct Recovery = 50% Analysis Date = 06/05/22 Pct Recovery = 50% Analysis Date = 06/05/22 Pct Recovery = 50% Analysis Date = 06/01/22 Pct Recovery = 51% Analysis Date = 06/01/22 Pct Recovery = 51% Analysis Date = 05/28/22 Pct Recovery = 51% Analysis Date = 05/28/22 Pct Recovery = 51% Analysis Date = 05/24/22 Pct Recovery = 51% Analysis Date = 05/24/22 Pct Recovery = 51% Analysis Date = 05/19/22 Pct Recovery = 52% Analysis Date = 05/19/22 Pct Recovery = 52% Analysis Date = 05/15/22 Pct Recovery = 52% Analysis Date = 05/15/22 Pct Recovery = 52% Analysis Date = 05/11/22 Pct Recovery = 52% Analysis Date = 05/11/22 Pct Recovery = 52% Analysis Date = 05/06/22 Pct Recovery = 53% Analysis Date = 05/06/22 Pct Recovery = 53% Analysis Date = 05/02/22 Pct Recovery = 53% Analysis Date = 05/02/22 Pct Recovery = 53% Analysis Date = 04/28/22 Pct Recovery = 53% Analysis Date = 04/28/22 Pct Recovery = 53% Analysis Date = 04/24/22 Pct Recovery = 54% Analysis Date = 04/24/22 Pct Recovery = 54% Analysis Date = 04/19/22 Pct Recovery = 54% Analysis Date = 04/19/22 Pct Recovery = 54% Analysis Date = 04/15/22 Pct Recovery = 54% Analysis Date = 04/15/22 Pct Recovery = 54% Analysis Date = 04/11/22 Pct Recovery = 55% Analysis Date = 04/11/22 Pct Recovery = 55% Analysis Date = 04/07/22 Pct Recovery = 55% Analysis Date = 04/07/22 Pct Recovery = 55% Analysis Date = 04/02/22 Pct Recovery = 55% Analysis Date = 04/02/22 Pct Recovery = 55% Analysis Date = 03/29/22 Pct Recovery = 55% Analysis Date = 03/29/22 Pct Recovery = 55% Analysis Date = 03/25/22 Pct Recovery = 56% Analysis Date = 03/25/22 Pct Recovery = 56% Analysis Date = 03/21/22 Pct Recovery = 56% Analysis Date = 03/21/22 Pct Recovery = 56% Analysis Date = 03/16/22 Pct Recovery = 56% Analysis Date = 03/16/22 Pct Recovery = 56% Analysis Date = 03/12/22 Pct Recovery = 57% Analysis Date = 03/12/22 Pct Recovery = 57% Analysis Date = 03/08/22 Pct Recovery = 57% Analysis Date = 03/08/22 Pct Recovery = 57% Analysis Date = 03/04/22 Pct Recovery = 57% Analysis Date = 03/04/22 Pct Recovery = 57% Analysis Date = 02/27/22 Pct Recovery = 58% Analysis Date = 02/27/22 Pct Recovery = 58% Analysis Date = 02/23/22 Pct Recovery = 58% Analysis Date = 02/23/22 Pct Recovery = 58% Analysis Date = 02/19/22 Pct Recovery = 58% Analysis Date = 02/19/22 Pct Recovery = 58% Analysis Date = 02/14/22 Pct Recovery = 59% Analysis Date = 02/14/22 Pct Recovery = 59% Analysis Date = 02/10/22 Pct Recovery = 59% Analysis Date = 02/10/22 Pct Recovery = 59% Analysis Date = 02/06/22 Pct Recovery = 59% Analysis Date = 02/06/22 Pct Recovery = 59% Analysis Date = 02/02/22 Pct Recovery = 60% Analysis Date = 02/02/22 Pct Recovery = 60% Analysis Date = 01/28/22 Pct Recovery = 60% Analysis Date = 01/28/22 Pct Recovery = 60% Analysis Date = 01/24/22 Pct Recovery = 60% Analysis Date = 01/24/22 Pct Recovery = 60% Analysis Date = 01/20/22 Pct Recovery = 61% Analysis Date = 01/20/22 Pct Recovery = 61% Analysis Date = 01/16/22 Pct Recovery = 61% Analysis Date = 01/16/22 Pct Recovery = 61% Analysis Date = 01/11/22 Pct Recovery = 61% Analysis Date = 01/11/22 Pct Recovery = 61% Analysis Date = 01/07/22 Pct Recovery = 62% Analysis Date = 01/07/22 Pct Recovery = 62% Analysis Date = 01/03/22 Pct Recovery = 62% Analysis Date = 01/03/22 Pct Recovery = 62% Analysis Date = 12/30/21 Pct Recovery = 62% Analysis Date = 12/30/21 Pct Recovery = 62% Analysis Date = 12/25/21 Pct Recovery = 63% Analysis Date = 12/25/21 Pct Recovery = 63% Analysis Date = 12/21/21 Pct Recovery = 63% Analysis Date = 12/21/21 Pct Recovery = 63% Analysis Date = 12/17/21 Pct Recovery = 63% Analysis Date = 12/17/21 Pct Recovery = 63% Analysis Date = 12/12/21 Pct Recovery = 64% Analysis Date = 12/12/21 Pct Recovery = 64% Analysis Date = 12/08/21 Pct Recovery = 64% Analysis Date = 12/08/21 Pct Recovery = 64% Analysis Date = 12/04/21 Pct Recovery = 65% Analysis Date = 12/04/21 Pct Recovery = 65% Analysis Date = 11/30/21 Pct Recovery = 65% Analysis Date = 11/30/21 Pct Recovery = 65% Analysis Date = 11/25/21 Pct Recovery = 65% Analysis Date = 11/25/21 Pct Recovery = 65% Analysis Date = 11/21/21 Pct Recovery = 66% Analysis Date = 11/21/21 Pct Recovery = 66% Analysis Date = 11/17/21 Pct Recovery = 66% Analysis Date = 11/17/21 Pct Recovery = 66% Analysis Date = 11/13/21 Pct Recovery = 66% Analysis Date = 11/13/21 Pct Recovery = 66% Analysis Date = 11/08/21 Pct Recovery = 67% Analysis Date = 11/08/21 Pct Recovery = 67% Analysis Date = 11/04/21 Pct Recovery = 67% Analysis Date = 11/04/21 Pct Recovery = 67% Analysis Date = 10/31/21 Pct Recovery = 68% Analysis Date = 10/31/21 Pct Recovery = 68% Analysis Date = 10/27/21 Pct Recovery = 68% Analysis Date = 10/27/21 Pct Recovery = 68% Analysis Date = 10/22/21 Pct Recovery = 68% Analysis Date = 10/22/21 Pct Recovery = 68% Analysis Date = 10/18/21 Pct Recovery = 68% Analysis Date = 10/18/21 Pct Recovery = 68% Analysis Date = 10/14/21 Pct Recovery = 69% Analysis Date = 10/14/21 Pct Recovery = 69% Analysis Date = 10/10/21 Pct Recovery = 69% Analysis Date = 10/10/21 Pct Recovery = 69% Analysis Date = 10/05/21 Pct Recovery = 69% Analysis Date = 10/05/21 Pct Recovery = 69% Analysis Date = 10/01/21 Pct Recovery = 69% Analysis Date = 10/01/21 Pct Recovery = 69% Analysis Date = 09/27/21 Pct Recovery = 69% Analysis Date = 09/27/21 Pct Recovery = 69% Analysis Date = 09/22/21 Pct Recovery = 70% Analysis Date = 09/22/21 Pct Recovery = 70% Analysis Date = 09/18/21 Pct Recovery = 70% Analysis Date = 09/18/21 Pct Recovery = 70% Analysis Date = 09/14/21 Pct Recovery = 70% Analysis Date = 09/14/21 Pct Recovery = 70% Analysis Date = 09/10/21 Pct Recovery = 70% Analysis Date = 09/10/21 Pct Recovery = 70% Analysis Date = 09/05/21 Pct Recovery = 71% Analysis Date = 09/05/21 Pct Recovery = 71% Analysis Date = 09/01/21 Pct Recovery = 71% Analysis Date = 09/01/21 Pct Recovery = 71% Analysis Date = 08/28/21 Pct Recovery = 71% Analysis Date = 08/28/21 Pct Recovery = 71% Analysis Date = 08/24/21 Pct Recovery = 71% Analysis Date = 08/24/21 Pct Recovery = 71% Analysis Date = 08/19/21 Pct Recovery = 72% Analysis Date = 08/19/21 Pct Recovery = 72% Analysis Date = 08/15/21 Pct Recovery = 72% Analysis Date = 08/15/21 Pct Recovery = 72% Analysis Date = 08/11/21 Pct Recovery = 72% Analysis Date = 08/11/21 Pct Recovery = 72% Analysis Date = 08/07/21 Pct Recovery = 72% Analysis Date = 08/07/21 Pct Recovery = 72% Analysis Date = 08/02/21 Pct Recovery = 73% Analysis Date = 08/02/21 Pct Recovery = 73% Analysis Date = 07/29/21 Pct Recovery = 73% Analysis Date = 07/29/21 Pct Recovery = 73% Analysis Date = 07/25/21 Pct Recovery = 73% Analysis Date = 07/25/21 Pct Recovery = 73% Analysis Date = 07/20/21 Pct Recovery = 73% Analysis Date = 07/20/21 Pct Recovery = 73% Analysis Date = 07/16/21 Pct Recovery = 74% Analysis Date = 07/16/21 Pct Recovery = 74% Analysis Date = 07/12/21 Pct Recovery = 74% Analysis Date = 07/12/21 Pct Recovery = 74% Analysis Date = 07/08/21 Pct Recovery = 74% Analysis Date = 07/08/21 Pct Recovery = 74% Analysis Date = 07/03/21 Pct Recovery = 74% Analysis Date = 07/03/21 Pct Recovery = 74% Analysis Date = 06/29/21 Pct Recovery = 75% Analysis Date = 06/29/21 Pct Recovery = 75% Analysis Date = 06/25/21 Pct Recovery = 75% Analysis Date = 06/25/21 Pct Recovery = 75% Analysis Date = 06/21/21 Pct Recovery = 75% Analysis Date = 06/21/21 Pct Recovery = 75% Analysis Date = 06/16/21 Pct Recovery = 75% Analysis Date = 06/16/21 Pct Recovery = 75% Analysis Date = 06/12/21 Pct Recovery = 76% Analysis Date = 06/12/21 Pct Recovery = 76% Analysis Date = 06/08/21 Pct Recovery = 76% Analysis Date = 06/08/21 Pct Recovery = 76% Analysis Date = 06/04/21 Pct Recovery = 76% Analysis Date = 06/04/21 Pct Recovery = 76% Analysis Date = 05/30/21 Pct Recovery = 76% Analysis Date = 05/30/21 Pct Recovery = 76% Analysis Date = 05/26/21 Pct Recovery = 77% Analysis Date = 05/26/21 Pct Recovery = 77% Analysis Date = 05/22/21 Pct Recovery = 77% Analysis Date = 05/22/21 Pct Recovery = 77% Analysis Date = 05/17/21 Pct Recovery = 77% Analysis Date = 05/17/21 Pct Recovery = 77% Analysis Date = 05/13/21 Pct Recovery = 77% Analysis Date = 05/13/21 Pct Recovery = 77% Analysis Date = 05/09/21 Pct Recovery = 78% Analysis Date = 05/09/21 Pct Recovery = 78% Analysis Date = 05/05/21 Pct Recovery = 78% Analysis Date = 05/05/21 Pct Recovery = 78% Analysis Date = 04/30/21 Pct Recovery = 78% Analysis Date = 04/30/21 Pct Recovery = 78% Analysis Date = 04/26/21 Pct Recovery = 78% Analysis Date = 04/26/21 Pct Recovery = 78% Analysis Date = 04/22/21 Pct Recovery = 79% Analysis Date = 04/22/21 Pct Recovery = 79% Analysis Date = 04/18/21 Pct Recovery = 79% Analysis Date = 04/18/21 Pct Recovery = 79% Analysis Date = 04/13/21 Pct Recovery = 79% Analysis Date = 04/13/21 Pct Recovery = 79% Analysis Date = 04/09/21 Pct Recovery = 79% Analysis Date = 04/09/21 Pct Recovery = 79% Analysis Date = 04/05/21 Pct Recovery = 80% Analysis Date = 04/05/21 Pct Recovery = 80% Analysis Date = 04/01/21 Pct Recovery = 80% Analysis Date = 04/01/21 Pct Recovery = 80% Analysis Date = 03/27/21 Pct Recovery = 80% Analysis Date = 03/27/21 Pct Recovery = 80% Analysis Date = 03/23/21 Pct Recovery = 81% Analysis Date = 03/23/21 Pct Recovery = 81% Analysis Date = 03/19/21 Pct Recovery = 81% Analysis Date = 03/19/21 Pct Recovery = 81% Analysis Date = 03/15/21 Pct Recovery = 82% Analysis Date = 03/15/21 Pct Recovery = 82% Analysis Date = 03/10/21 Pct Recovery = 82% Analysis Date = 03/10/21 Pct Recovery = 82% Analysis Date = 03/06/21 Pct Recovery = 83% Analysis Date = 03/06/21 Pct Recovery = 83% Analysis Date = 03/02/21 Pct Recovery = 83% Analysis Date = 03/02/21 Pct Recovery = 83% Analysis Date = 02/25/21 Pct Recovery = 84% Analysis Date = 02/25/21 Pct Recovery = 84% Analysis Date = 02/21/21 Pct Recovery = 84% Analysis Date = 02/21/21 Pct Recovery = 84% Analysis Date = 02/17/21 Pct Recovery = 85% Analysis Date = 02/17/21 Pct Recovery = 85% Analysis Date = 02/13/21 Pct Recovery = 85% Analysis Date = 02/13/21 Pct Recovery = 85% Analysis Date = 02/08/21 Pct Recovery = 86% Analysis Date = 02/08/21 Pct Recovery = 86% Analysis Date = 02/04/21 Pct Recovery = 86% Analysis Date = 02/04/21 Pct Recovery = 86% Analysis Date = 01/31/21 Pct Recovery = 87% Analysis Date = 01/31/21 Pct Recovery = 87% Analysis Date = 01/27/21 Pct Recovery = 88% Analysis Date = 01/27/21 Pct Recovery = 88% Analysis Date = 01/22/21 Pct Recovery = 88% Analysis Date = 01/22/21 Pct Recovery = 88% Analysis Date = 01/18/21 Pct Recovery = 89% Analysis Date = 01/18/21 Pct Recovery = 89% Analysis Date = 01/14/21 Pct Recovery = 90% Analysis Date = 01/14/21 Pct Recovery = 90% Analysis Date = 01/10/21 Pct Recovery = 90% Analysis Date = 01/10/21 Pct Recovery = 90% Analysis Date = 01/05/21 Pct Recovery = 91% Analysis Date = 01/05/21 Pct Recovery = 91% Analysis Date = 01/01/21 Pct Recovery = 91% Analysis Date = 01/01/21 Pct Recovery = 91% Analysis Date = 12/28/20 Pct Recovery = 92% Analysis Date = 12/28/20 Pct Recovery = 92% Analysis Date = 12/23/20 Pct Recovery = 93% Analysis Date = 12/23/20 Pct Recovery = 93% Analysis Date = 12/19/20 Pct Recovery = 93% Analysis Date = 12/19/20 Pct Recovery = 93% Analysis Date = 12/15/20 Pct Recovery = 94% Analysis Date = 12/15/20 Pct Recovery = 94% Analysis Date = 12/11/20 Pct Recovery = 95% Analysis Date = 12/11/20 Pct Recovery = 95% Analysis Date = 12/06/20 Pct Recovery = 95% Analysis Date = 12/06/20 Pct Recovery = 95% Analysis Date = 12/02/20 Pct Recovery = 96% Analysis Date = 12/02/20 Pct Recovery = 96% Analysis Date = 11/28/20 Pct Recovery = 97% Analysis Date = 11/28/20 Pct Recovery = 97% Analysis Date = 11/24/20 Pct Recovery = 97% Analysis Date = 11/24/20 Pct Recovery = 97% Analysis Date = 11/19/20 Pct Recovery = 98% Analysis Date = 11/19/20 Pct Recovery = 98% Analysis Date = 11/15/20 Pct Recovery = 99% Analysis Date = 11/15/20 Pct Recovery = 99% Analysis Date = 11/11/20 Pct Recovery = 100% Analysis Date = 11/11/20 Pct Recovery = 100% Analysis Date = 11/07/20 Pct Recovery = 101% Analysis Date = 11/07/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 104% Analysis Date = 10/25/20 Pct Recovery = 104% Analysis Date = 10/21/20 Pct Recovery = 105% Analysis Date = 10/21/20 Pct Recovery = 105% Analysis Date = 10/16/20 Pct Recovery = 106% Analysis Date = 10/16/20 Pct Recovery = 106% Analysis Date = 10/12/20 Pct Recovery = 107% Analysis Date = 10/12/20 Pct Recovery = 107% Analysis Date = 10/08/20 Pct Recovery = 108% Analysis Date = 10/08/20 Pct Recovery = 108% Analysis Date = 10/03/20 Pct Recovery = 109% Analysis Date = 10/03/20 Pct Recovery = 109% Analysis Date = 09/29/20 Pct Recovery = 110% Analysis Date = 09/29/20 Pct Recovery = 110% Analysis Date = 09/25/20 Pct Recovery = 111% Analysis Date = 09/25/20 Pct Recovery = 111% Analysis Date = 09/21/20 Pct Recovery = 112% Analysis Date = 09/21/20 Pct Recovery = 112% Analysis Date = 09/16/20 Pct Recovery = 113% Analysis Date = 09/16/20 Pct Recovery = 113% Analysis Date = 09/12/20 Pct Recovery = 114% Analysis Date = 09/12/20 Pct Recovery = 114% Analysis Date = 09/08/20 Pct Recovery = 115% Analysis Date = 09/08/20 Pct Recovery = 115% Analysis Date = 09/04/20 Pct Recovery = 116% Analysis Date = 09/04/20 Pct Recovery = 116% Analysis Date = 08/30/20 Pct Recovery = 117% Analysis Date = 08/30/20 Pct Recovery = 117% Analysis Date = 08/26/20 Pct Recovery = 117% Analysis Date = 08/26/20 Pct Recovery = 117% Analysis Date = 08/22/20 Pct Recovery = 118% Analysis Date = 08/22/20 Pct Recovery = 118% Analysis Date = 08/18/20 Pct Recovery = 119% Analysis Date = 08/18/20 Pct Recovery = 119% Analysis Date = 08/13/20 Pct Recovery = 120% Analysis Date = 08/13/20 Pct Recovery = 120% Analysis Date = 08/09/20 Pct Recovery = 121% Analysis Date = 08/09/20 Pct Recovery = 121% Analysis Date = 08/05/20 Pct Recovery = 122% Analysis Date = 08/05/20 Pct Recovery = 122% Analysis Date = 07/31/20 Pct Recovery = 123% Analysis Date = 07/31/20 Pct Recovery = 123% Analysis Date = 07/27/20 Pct Recovery = 124% Analysis Date = 07/27/20 Pct Recovery = 124% Analysis Date = 07/23/20 Pct Recovery = 125% Analysis Date = 07/23/20 Pct Recovery = 125% Analysis Date = 07/19/20 Pct Recovery = 126% Analysis Date = 07/19/20 Pct Recovery = 126% Analysis Date = 07/14/20 Pct Recovery = 127% Analysis Date = 07/14/20 Pct Recovery = 127% Analysis Date = 07/10/20 Pct Recovery = 128% Analysis Date = 07/10/20 Pct Recovery = 128% Analysis Date = 07/06/20 Pct Recovery = 129% Analysis Date = 07/06/20 Pct Recovery = 129% Analysis Date = 07/02/20 Pct Recovery = 130% Analysis Date = 07/02/20 Pct Recovery = 130% Analysis Date = 06/27/20 Pct Recovery = 131% Analysis Date = 06/27/20 Pct Recovery = 131% Analysis Date = 06/23/20 Pct Recovery = 132% Analysis Date = 06/23/20 Pct Recovery = 132% Analysis Date = 06/19/20 Pct Recovery = 133% Analysis Date = 06/19/20 Pct Recovery = 133% Analysis Date = 06/15/20 Pct Recovery = 134% Analysis Date = 06/15/20 Pct Recovery = 134% Analysis Date = 06/10/20 Pct Recovery = 134% Analysis Date = 06/10/20 Pct Recovery = 134% Analysis Date = 06/06/20 Pct Recovery = 135% Analysis Date = 06/06/20 Pct Recovery = 135% Analysis Date = 06/02/20 Pct Recovery = 136% Analysis Date = 06/02/20 Pct Recovery = 136% Analysis Date = 05/29/20 Pct Recovery = 137% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 87% 38% 87% 38%
Total 41 87% 38% 87% 38%

Sample Statistics
DIAZINON

Characteristic N % % Basis
Plotted 41 100% Spiked
Estimated Values 3 7% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 72 .  
False Positives 3 4% 3 out of 72

OBSP Determination:
DICAMBA
METHOD: 2447 , TESTIDCODE: 68571LCM60

Laboratory ID = 20202590107 Lab Value = 10940.33 Expected Conc. = 10047 Report level label = 800 Pct Recovery = 109% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 12463.08 Expected Conc. = 10047 Report level label = 800 Pct Recovery = 124% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 9933.937 Expected Conc. = 9880 Report level label = 800 Pct Recovery = 101% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 9432.667 Expected Conc. = 9880 Report level label = 800 Pct Recovery = 95% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203360042 Lab Value = 4654.707 Expected Conc. = 5023.3 Report level label = 800 Pct Recovery = 93% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 5420.023 Expected Conc. = 5023.3 Report level label = 800 Pct Recovery = 108% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 5180.797 Expected Conc. = 5023.3 Report level label = 800 Pct Recovery = 103% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201550031 Lab Value = 4811.872 Expected Conc. = 5010.8 Report level label = 800 Pct Recovery = 96% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20202390020 Lab Value = 6622.253 Expected Conc. = 5010 Report level label = 800 Pct Recovery = 132% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 6261.050 Expected Conc. = 5010 Report level label = 800 Pct Recovery = 125% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 5051.786 Expected Conc. = 4008 Report level label = 800 Pct Recovery = 126% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 4154.003 Expected Conc. = 4008 Report level label = 800 Pct Recovery = 104% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210970035 Lab Value = 2456.668 Expected Conc. = 2009.3 Report level label = 800 Pct Recovery = 122% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 2244.135 Expected Conc. = 2009.3 Report level label = 800 Pct Recovery = 112% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 1670.691 Expected Conc. = 2009.3 Report level label = 800 Pct Recovery = 83% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 2159.705 Expected Conc. = 2009.3 Report level label = 800 Pct Recovery = 107% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 2097.448 Expected Conc. = 2009.3 Report level label = 800 Pct Recovery = 104% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 1910.644 Expected Conc. = 2009.3 Report level label = 800 Pct Recovery = 95% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 1892.839 Expected Conc. = 2004.3 Report level label = 800 Pct Recovery = 94% Analysis Date = 09/01/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 1828.737 Expected Conc. = 2004.3 Report level label = 800 Pct Recovery = 91% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 1996.831 Expected Conc. = 2004.3 Report level label = 800 Pct Recovery = 100% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 2005.556 Expected Conc. = 2004.3 Report level label = 800 Pct Recovery = 100% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 1734.530 Expected Conc. = 2004.3 Report level label = 800 Pct Recovery = 87% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210830019 Lab Value = 1569.739 Expected Conc. = 1976 Report level label = 800 Pct Recovery = 79% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 1601.435 Expected Conc. = 1976 Report level label = 800 Pct Recovery = 81% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 04/14/21 Pct Recovery = 101% Analysis Date = 04/13/21 Pct Recovery = 101% Analysis Date = 04/13/21 Pct Recovery = 101% Analysis Date = 04/11/21 Pct Recovery = 101% Analysis Date = 04/11/21 Pct Recovery = 101% Analysis Date = 04/10/21 Pct Recovery = 101% Analysis Date = 04/10/21 Pct Recovery = 101% Analysis Date = 04/08/21 Pct Recovery = 101% Analysis Date = 04/08/21 Pct Recovery = 101% Analysis Date = 04/06/21 Pct Recovery = 101% Analysis Date = 04/06/21 Pct Recovery = 101% Analysis Date = 04/05/21 Pct Recovery = 101% Analysis Date = 04/05/21 Pct Recovery = 101% Analysis Date = 04/03/21 Pct Recovery = 101% Analysis Date = 04/03/21 Pct Recovery = 101% Analysis Date = 04/02/21 Pct Recovery = 101% Analysis Date = 04/02/21 Pct Recovery = 101% Analysis Date = 03/31/21 Pct Recovery = 100% Analysis Date = 03/31/21 Pct Recovery = 100% Analysis Date = 03/29/21 Pct Recovery = 100% Analysis Date = 03/29/21 Pct Recovery = 100% Analysis Date = 03/28/21 Pct Recovery = 100% Analysis Date = 03/28/21 Pct Recovery = 100% Analysis Date = 03/26/21 Pct Recovery = 100% Analysis Date = 03/26/21 Pct Recovery = 100% Analysis Date = 03/25/21 Pct Recovery = 100% Analysis Date = 03/25/21 Pct Recovery = 100% Analysis Date = 03/23/21 Pct Recovery = 100% Analysis Date = 03/23/21 Pct Recovery = 100% Analysis Date = 03/21/21 Pct Recovery = 100% Analysis Date = 03/21/21 Pct Recovery = 100% Analysis Date = 03/20/21 Pct Recovery = 100% Analysis Date = 03/20/21 Pct Recovery = 100% Analysis Date = 03/18/21 Pct Recovery = 100% Analysis Date = 03/18/21 Pct Recovery = 100% Analysis Date = 03/17/21 Pct Recovery = 100% Analysis Date = 03/17/21 Pct Recovery = 100% Analysis Date = 03/15/21 Pct Recovery = 100% Analysis Date = 03/15/21 Pct Recovery = 100% Analysis Date = 03/13/21 Pct Recovery = 99% Analysis Date = 03/13/21 Pct Recovery = 99% Analysis Date = 03/12/21 Pct Recovery = 99% Analysis Date = 03/12/21 Pct Recovery = 99% Analysis Date = 03/10/21 Pct Recovery = 99% Analysis Date = 03/10/21 Pct Recovery = 99% Analysis Date = 03/09/21 Pct Recovery = 99% Analysis Date = 03/09/21 Pct Recovery = 99% Analysis Date = 03/07/21 Pct Recovery = 99% Analysis Date = 03/07/21 Pct Recovery = 99% Analysis Date = 03/05/21 Pct Recovery = 99% Analysis Date = 03/05/21 Pct Recovery = 99% Analysis Date = 03/04/21 Pct Recovery = 99% Analysis Date = 03/04/21 Pct Recovery = 99% Analysis Date = 03/02/21 Pct Recovery = 99% Analysis Date = 03/02/21 Pct Recovery = 99% Analysis Date = 03/01/21 Pct Recovery = 99% Analysis Date = 03/01/21 Pct Recovery = 99% Analysis Date = 02/27/21 Pct Recovery = 99% Analysis Date = 02/27/21 Pct Recovery = 99% Analysis Date = 02/25/21 Pct Recovery = 99% Analysis Date = 02/25/21 Pct Recovery = 99% Analysis Date = 02/24/21 Pct Recovery = 98% Analysis Date = 02/24/21 Pct Recovery = 98% Analysis Date = 02/22/21 Pct Recovery = 98% Analysis Date = 02/22/21 Pct Recovery = 98% Analysis Date = 02/21/21 Pct Recovery = 98% Analysis Date = 02/21/21 Pct Recovery = 98% Analysis Date = 02/19/21 Pct Recovery = 98% Analysis Date = 02/19/21 Pct Recovery = 98% Analysis Date = 02/17/21 Pct Recovery = 98% Analysis Date = 02/17/21 Pct Recovery = 98% Analysis Date = 02/16/21 Pct Recovery = 98% Analysis Date = 02/16/21 Pct Recovery = 98% Analysis Date = 02/14/21 Pct Recovery = 98% Analysis Date = 02/14/21 Pct Recovery = 98% Analysis Date = 02/13/21 Pct Recovery = 98% Analysis Date = 02/13/21 Pct Recovery = 98% Analysis Date = 02/11/21 Pct Recovery = 98% Analysis Date = 02/11/21 Pct Recovery = 98% Analysis Date = 02/09/21 Pct Recovery = 98% Analysis Date = 02/09/21 Pct Recovery = 98% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/06/21 Pct Recovery = 97% Analysis Date = 02/06/21 Pct Recovery = 97% Analysis Date = 02/05/21 Pct Recovery = 97% Analysis Date = 02/05/21 Pct Recovery = 97% Analysis Date = 02/03/21 Pct Recovery = 97% Analysis Date = 02/03/21 Pct Recovery = 97% Analysis Date = 02/01/21 Pct Recovery = 97% Analysis Date = 02/01/21 Pct Recovery = 97% Analysis Date = 01/31/21 Pct Recovery = 97% Analysis Date = 01/31/21 Pct Recovery = 97% Analysis Date = 01/29/21 Pct Recovery = 97% Analysis Date = 01/29/21 Pct Recovery = 97% Analysis Date = 01/28/21 Pct Recovery = 97% Analysis Date = 01/28/21 Pct Recovery = 97% Analysis Date = 01/26/21 Pct Recovery = 97% Analysis Date = 01/26/21 Pct Recovery = 97% Analysis Date = 01/24/21 Pct Recovery = 97% Analysis Date = 01/24/21 Pct Recovery = 97% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/21/21 Pct Recovery = 97% Analysis Date = 01/21/21 Pct Recovery = 97% Analysis Date = 01/20/21 Pct Recovery = 97% Analysis Date = 01/20/21 Pct Recovery = 97% Analysis Date = 01/18/21 Pct Recovery = 97% Analysis Date = 01/18/21 Pct Recovery = 97% Analysis Date = 01/16/21 Pct Recovery = 97% Analysis Date = 01/16/21 Pct Recovery = 97% Analysis Date = 01/15/21 Pct Recovery = 97% Analysis Date = 01/15/21 Pct Recovery = 97% Analysis Date = 01/13/21 Pct Recovery = 97% Analysis Date = 01/13/21 Pct Recovery = 97% Analysis Date = 01/12/21 Pct Recovery = 98% Analysis Date = 01/12/21 Pct Recovery = 98% Analysis Date = 01/10/21 Pct Recovery = 98% Analysis Date = 01/10/21 Pct Recovery = 98% Analysis Date = 01/08/21 Pct Recovery = 98% Analysis Date = 01/08/21 Pct Recovery = 98% Analysis Date = 01/07/21 Pct Recovery = 98% Analysis Date = 01/07/21 Pct Recovery = 98% Analysis Date = 01/05/21 Pct Recovery = 98% Analysis Date = 01/05/21 Pct Recovery = 98% Analysis Date = 01/04/21 Pct Recovery = 98% Analysis Date = 01/04/21 Pct Recovery = 98% Analysis Date = 01/02/21 Pct Recovery = 98% Analysis Date = 01/02/21 Pct Recovery = 98% Analysis Date = 12/31/20 Pct Recovery = 98% Analysis Date = 12/31/20 Pct Recovery = 98% Analysis Date = 12/30/20 Pct Recovery = 98% Analysis Date = 12/30/20 Pct Recovery = 98% Analysis Date = 12/28/20 Pct Recovery = 98% Analysis Date = 12/28/20 Pct Recovery = 98% Analysis Date = 12/27/20 Pct Recovery = 98% Analysis Date = 12/27/20 Pct Recovery = 98% Analysis Date = 12/25/20 Pct Recovery = 98% Analysis Date = 12/25/20 Pct Recovery = 98% Analysis Date = 12/23/20 Pct Recovery = 98% Analysis Date = 12/23/20 Pct Recovery = 98% Analysis Date = 12/22/20 Pct Recovery = 98% Analysis Date = 12/22/20 Pct Recovery = 98% Analysis Date = 12/20/20 Pct Recovery = 98% Analysis Date = 12/20/20 Pct Recovery = 98% Analysis Date = 12/19/20 Pct Recovery = 98% Analysis Date = 12/19/20 Pct Recovery = 98% Analysis Date = 12/17/20 Pct Recovery = 98% Analysis Date = 12/17/20 Pct Recovery = 98% Analysis Date = 12/15/20 Pct Recovery = 98% Analysis Date = 12/15/20 Pct Recovery = 98% Analysis Date = 12/14/20 Pct Recovery = 98% Analysis Date = 12/14/20 Pct Recovery = 98% Analysis Date = 12/12/20 Pct Recovery = 98% Analysis Date = 12/12/20 Pct Recovery = 98% Analysis Date = 12/11/20 Pct Recovery = 98% Analysis Date = 12/11/20 Pct Recovery = 98% Analysis Date = 12/09/20 Pct Recovery = 98% Analysis Date = 12/09/20 Pct Recovery = 98% Analysis Date = 12/07/20 Pct Recovery = 98% Analysis Date = 12/07/20 Pct Recovery = 98% Analysis Date = 12/06/20 Pct Recovery = 98% Analysis Date = 12/06/20 Pct Recovery = 98% Analysis Date = 12/04/20 Pct Recovery = 99% Analysis Date = 12/04/20 Pct Recovery = 99% Analysis Date = 12/03/20 Pct Recovery = 99% Analysis Date = 12/03/20 Pct Recovery = 99% Analysis Date = 12/01/20 Pct Recovery = 99% Analysis Date = 12/01/20 Pct Recovery = 99% Analysis Date = 11/29/20 Pct Recovery = 99% Analysis Date = 11/29/20 Pct Recovery = 99% Analysis Date = 11/28/20 Pct Recovery = 100% Analysis Date = 11/28/20 Pct Recovery = 100% Analysis Date = 11/26/20 Pct Recovery = 100% Analysis Date = 11/26/20 Pct Recovery = 100% Analysis Date = 11/25/20 Pct Recovery = 100% Analysis Date = 11/25/20 Pct Recovery = 100% Analysis Date = 11/23/20 Pct Recovery = 100% Analysis Date = 11/23/20 Pct Recovery = 100% Analysis Date = 11/21/20 Pct Recovery = 101% Analysis Date = 11/21/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/18/20 Pct Recovery = 101% Analysis Date = 11/18/20 Pct Recovery = 101% Analysis Date = 11/17/20 Pct Recovery = 102% Analysis Date = 11/17/20 Pct Recovery = 102% Analysis Date = 11/15/20 Pct Recovery = 102% Analysis Date = 11/15/20 Pct Recovery = 102% Analysis Date = 11/13/20 Pct Recovery = 102% Analysis Date = 11/13/20 Pct Recovery = 102% Analysis Date = 11/12/20 Pct Recovery = 103% Analysis Date = 11/12/20 Pct Recovery = 103% Analysis Date = 11/10/20 Pct Recovery = 103% Analysis Date = 11/10/20 Pct Recovery = 103% Analysis Date = 11/09/20 Pct Recovery = 103% Analysis Date = 11/09/20 Pct Recovery = 103% Analysis Date = 11/07/20 Pct Recovery = 104% Analysis Date = 11/07/20 Pct Recovery = 104% Analysis Date = 11/05/20 Pct Recovery = 104% Analysis Date = 11/05/20 Pct Recovery = 104% Analysis Date = 11/04/20 Pct Recovery = 104% Analysis Date = 11/04/20 Pct Recovery = 104% Analysis Date = 11/02/20 Pct Recovery = 105% Analysis Date = 11/02/20 Pct Recovery = 105% Analysis Date = 11/01/20 Pct Recovery = 105% Analysis Date = 11/01/20 Pct Recovery = 105% Analysis Date = 10/30/20 Pct Recovery = 105% Analysis Date = 10/30/20 Pct Recovery = 105% Analysis Date = 10/28/20 Pct Recovery = 106% Analysis Date = 10/28/20 Pct Recovery = 106% Analysis Date = 10/27/20 Pct Recovery = 106% Analysis Date = 10/27/20 Pct Recovery = 106% Analysis Date = 10/25/20 Pct Recovery = 106% Analysis Date = 10/25/20 Pct Recovery = 106% Analysis Date = 10/24/20 Pct Recovery = 107% Analysis Date = 10/24/20 Pct Recovery = 107% Analysis Date = 10/22/20 Pct Recovery = 107% Analysis Date = 10/22/20 Pct Recovery = 107% Analysis Date = 10/20/20 Pct Recovery = 108% Analysis Date = 10/20/20 Pct Recovery = 108% Analysis Date = 10/19/20 Pct Recovery = 108% Analysis Date = 10/19/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 108% Analysis Date = 10/16/20 Pct Recovery = 108% Analysis Date = 10/16/20 Pct Recovery = 108% Analysis Date = 10/14/20 Pct Recovery = 109% Analysis Date = 10/14/20 Pct Recovery = 109% Analysis Date = 10/12/20 Pct Recovery = 109% Analysis Date = 10/12/20 Pct Recovery = 109% Analysis Date = 10/11/20 Pct Recovery = 109% Analysis Date = 10/11/20 Pct Recovery = 109% Analysis Date = 10/09/20 Pct Recovery = 109% Analysis Date = 10/09/20 Pct Recovery = 109% Analysis Date = 10/08/20 Pct Recovery = 109% Analysis Date = 10/08/20 Pct Recovery = 109% Analysis Date = 10/06/20 Pct Recovery = 109% Analysis Date = 10/06/20 Pct Recovery = 109% Analysis Date = 10/04/20 Pct Recovery = 109% Analysis Date = 10/04/20 Pct Recovery = 109% Analysis Date = 10/03/20 Pct Recovery = 109% Analysis Date = 10/03/20 Pct Recovery = 109% Analysis Date = 10/01/20 Pct Recovery = 109% Analysis Date = 10/01/20 Pct Recovery = 109% Analysis Date = 09/30/20 Pct Recovery = 109% Analysis Date = 09/30/20 Pct Recovery = 109% Analysis Date = 09/28/20 Pct Recovery = 109% Analysis Date = 09/28/20 Pct Recovery = 109% Analysis Date = 09/26/20 Pct Recovery = 109% Analysis Date = 09/26/20 Pct Recovery = 109% Analysis Date = 09/25/20 Pct Recovery = 109% Analysis Date = 09/25/20 Pct Recovery = 109% Analysis Date = 09/23/20 Pct Recovery = 109% Analysis Date = 09/23/20 Pct Recovery = 109% Analysis Date = 09/22/20 Pct Recovery = 110% Analysis Date = 09/22/20 Pct Recovery = 110% Analysis Date = 09/20/20 Pct Recovery = 110% Analysis Date = 09/20/20 Pct Recovery = 110% Analysis Date = 09/18/20 Pct Recovery = 110% Analysis Date = 09/18/20 Pct Recovery = 110% Analysis Date = 09/17/20 Pct Recovery = 110% Analysis Date = 09/17/20 Pct Recovery = 110% Analysis Date = 09/15/20 Pct Recovery = 110% Analysis Date = 09/15/20 Pct Recovery = 110% Analysis Date = 09/14/20 Pct Recovery = 110% Analysis Date = 09/14/20 Pct Recovery = 110% Analysis Date = 09/12/20 Pct Recovery = 110% Analysis Date = 09/12/20 Pct Recovery = 110% Analysis Date = 09/10/20 Pct Recovery = 110% Analysis Date = 09/10/20 Pct Recovery = 110% Analysis Date = 09/09/20 Pct Recovery = 110% Analysis Date = 09/09/20 Pct Recovery = 110% Analysis Date = 09/07/20 Pct Recovery = 110% Analysis Date = 09/07/20 Pct Recovery = 110% Analysis Date = 09/06/20 Pct Recovery = 110% Analysis Date = 09/06/20 Pct Recovery = 110% Analysis Date = 09/04/20 Pct Recovery = 110% Analysis Date = 09/04/20 Pct Recovery = 110% Analysis Date = 09/02/20 Pct Recovery = 110% Analysis Date = 09/02/20 Pct Recovery = 110% Analysis Date = 09/01/20 Pct Recovery = 110% Analysis Date = 09/01/20 Pct Recovery = 110% Analysis Date = 08/30/20 Pct Recovery = 109% Analysis Date = 08/30/20 Pct Recovery = 109% Analysis Date = 08/29/20 Pct Recovery = 109% Analysis Date = 08/29/20 Pct Recovery = 109% Analysis Date = 08/27/20 Pct Recovery = 109% Analysis Date = 08/27/20 Pct Recovery = 109% Analysis Date = 08/25/20 Pct Recovery = 109% Analysis Date = 08/25/20 Pct Recovery = 109% Analysis Date = 08/24/20 Pct Recovery = 109% Analysis Date = 08/24/20 Pct Recovery = 109% Analysis Date = 08/22/20 Pct Recovery = 109% Analysis Date = 08/22/20 Pct Recovery = 109% Analysis Date = 08/21/20 Pct Recovery = 109% Analysis Date = 08/21/20 Pct Recovery = 109% Analysis Date = 08/19/20 Pct Recovery = 109% Analysis Date = 08/19/20 Pct Recovery = 109% Analysis Date = 08/17/20 Pct Recovery = 109% Analysis Date = 08/17/20 Pct Recovery = 109% Analysis Date = 08/16/20 Pct Recovery = 109% Analysis Date = 08/16/20 Pct Recovery = 109% Analysis Date = 08/14/20 Pct Recovery = 109% Analysis Date = 08/14/20 Pct Recovery = 109% Analysis Date = 08/13/20 Pct Recovery = 109% Analysis Date = 08/13/20 Pct Recovery = 109% Analysis Date = 08/11/20 Pct Recovery = 109% Analysis Date = 08/11/20 Pct Recovery = 109% Analysis Date = 08/09/20 Pct Recovery = 109% Analysis Date = 08/09/20 Pct Recovery = 109% Analysis Date = 08/08/20 Pct Recovery = 109% Analysis Date = 08/08/20 Pct Recovery = 109% Analysis Date = 08/06/20 Pct Recovery = 109% Analysis Date = 08/06/20 Pct Recovery = 109% Analysis Date = 08/05/20 Pct Recovery = 109% Analysis Date = 08/05/20 Pct Recovery = 109% Analysis Date = 08/03/20 Pct Recovery = 108% Analysis Date = 08/03/20 Pct Recovery = 108% Analysis Date = 08/01/20 Pct Recovery = 108% Analysis Date = 08/01/20 Pct Recovery = 108% Analysis Date = 07/31/20 Pct Recovery = 108% Analysis Date = 07/31/20 Pct Recovery = 108% Analysis Date = 07/29/20 Pct Recovery = 107% Analysis Date = 07/29/20 Pct Recovery = 107% Analysis Date = 07/28/20 Pct Recovery = 107% Analysis Date = 07/28/20 Pct Recovery = 107% Analysis Date = 07/26/20 Pct Recovery = 107% Analysis Date = 07/26/20 Pct Recovery = 107% Analysis Date = 07/24/20 Pct Recovery = 106% Analysis Date = 07/24/20 Pct Recovery = 106% Analysis Date = 07/23/20 Pct Recovery = 106% Analysis Date = 07/23/20 Pct Recovery = 106% Analysis Date = 07/21/20 Pct Recovery = 106% Analysis Date = 07/21/20 Pct Recovery = 106% Analysis Date = 07/20/20 Pct Recovery = 105% Analysis Date = 07/20/20 Pct Recovery = 105% Analysis Date = 07/18/20 Pct Recovery = 105% Analysis Date = 07/18/20 Pct Recovery = 105% Analysis Date = 07/16/20 Pct Recovery = 105% Analysis Date = 07/16/20 Pct Recovery = 105% Analysis Date = 07/15/20 Pct Recovery = 105% Analysis Date = 07/15/20 Pct Recovery = 105% Analysis Date = 07/13/20 Pct Recovery = 104% Analysis Date = 07/13/20 Pct Recovery = 104% Analysis Date = 07/12/20 Pct Recovery = 104% Analysis Date = 07/12/20 Pct Recovery = 104% Analysis Date = 07/10/20 Pct Recovery = 104% Analysis Date = 07/10/20 Pct Recovery = 104% Analysis Date = 07/08/20 Pct Recovery = 103% Analysis Date = 07/08/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/05/20 Pct Recovery = 103% Analysis Date = 07/05/20 Pct Recovery = 103% Analysis Date = 07/04/20 Pct Recovery = 102% Analysis Date = 07/04/20 Pct Recovery = 102% Analysis Date = 07/02/20 Pct Recovery = 102% Analysis Date = 07/02/20 Pct Recovery = 102% Analysis Date = 06/30/20 Pct Recovery = 102% Analysis Date = 06/30/20 Pct Recovery = 102% Analysis Date = 06/29/20 Pct Recovery = 101% Analysis Date = 06/29/20 Pct Recovery = 101% Analysis Date = 06/27/20 Pct Recovery = 101% Analysis Date = 06/27/20 Pct Recovery = 101% Analysis Date = 06/26/20 Pct Recovery = 101% Analysis Date = 06/26/20 Pct Recovery = 101% Analysis Date = 06/24/20 Pct Recovery = 100% Analysis Date = 06/24/20 Pct Recovery = 100% Analysis Date = 06/22/20 Pct Recovery = 100% Analysis Date = 06/22/20 Pct Recovery = 100% Analysis Date = 06/21/20 Pct Recovery = 100% Analysis Date = 06/21/20 Pct Recovery = 100% Analysis Date = 06/19/20 Pct Recovery = 99% Analysis Date = 06/19/20 Pct Recovery = 99% Analysis Date = 06/18/20 Pct Recovery = 99% Analysis Date = 06/18/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/14/20 Pct Recovery = 98% Analysis Date = 06/14/20 Pct Recovery = 98% Analysis Date = 06/13/20 Pct Recovery = 98% Analysis Date = 06/13/20 Pct Recovery = 98% Analysis Date = 06/11/20 Pct Recovery = 98% Analysis Date = 06/11/20 Pct Recovery = 98% Analysis Date = 06/10/20 Pct Recovery = 97% Analysis Date = 06/10/20 Pct Recovery = 97% Analysis Date = 06/08/20 Pct Recovery = 97% Analysis Date = 06/08/20 Pct Recovery = 97% Analysis Date = 06/06/20 Pct Recovery = 97% Analysis Date = 06/06/20 Pct Recovery = 97% Analysis Date = 06/05/20 Pct Recovery = 97% Analysis Date = 06/05/20 Pct Recovery = 97% Analysis Date = 06/03/20 Pct Recovery = 96% Analysis Date = 06/03/20 Pct Recovery = 96% Analysis Date = 06/02/20 Pct Recovery = 96% Analysis Date = 06/02/20 Pct Recovery = 96% Analysis Date = 05/31/20 Pct Recovery = 96% Analysis Date = 05/31/20 Pct Recovery = 96% Analysis Date = 05/30/20 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICAMBA

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 25 103% 15% 101% 11%
Total 25 103% 15% 101% 11%

Sample Statistics
DICAMBA

Characteristic N % % Basis
Plotted 25 100% Spiked
Estimated Values 25 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 25 .  
False Negatives 0 0% 0 out of 25
Not Spiked 91 .  
False Positives 0 0% 0 out of 91

OBSP Determination:
DICHLOROVOS (DICHLORVOS)
METHOD: 2447 , TESTIDCODE: 68572LCM60

Laboratory ID = 20210760015 Lab Value = 519.227 Expected Conc. = 651.5 Report level label = 52 Pct Recovery = 80% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 229.863 Expected Conc. = 651.5 Report level label = 52 Pct Recovery = 35% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 259.088 Expected Conc. = 651.5 Report level label = 52 Pct Recovery = 40% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 535.497 Expected Conc. = 651.5 Report level label = 52 Pct Recovery = 82% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 334.928 Expected Conc. = 640.9 Report level label = 52 Pct Recovery = 52% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 312.759 Expected Conc. = 640.9 Report level label = 52 Pct Recovery = 49% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 319.987 Expected Conc. = 640.9 Report level label = 52 Pct Recovery = 50% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20212990174 Lab Value = 347.307 Expected Conc. = 523.52 Report level label = 52 Pct Recovery = 66% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 283.159 Expected Conc. = 523.2 Report level label = 52 Pct Recovery = 54% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 268.222 Expected Conc. = 523.2 Report level label = 52 Pct Recovery = 51% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20220810134 Lab Value = 376.752 Expected Conc. = 520.8 Report level label = 52 Pct Recovery = 72% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222010132 Lab Value = 292.103 Expected Conc. = 520 Report level label = 52 Pct Recovery = 56% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20222150193 Lab Value = 298.431 Expected Conc. = 516 Report level label = 52 Pct Recovery = 58% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20213340027 Lab Value = 242.478 Expected Conc. = 327.2 Report level label = 52 Pct Recovery = 74% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 453.915 Expected Conc. = 327.2 Report level label = 52 Pct Recovery = 139% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 196.034 Expected Conc. = 327.2 Report level label = 52 Pct Recovery = 60% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 185.043 Expected Conc. = 327 Report level label = 52 Pct Recovery = 57% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 139.992 Expected Conc. = 327 Report level label = 52 Pct Recovery = 43% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20210480001 Lab Value = 206.438 Expected Conc. = 325.75 Report level label = 52 Pct Recovery = 63% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202390020 Lab Value = 280.464 Expected Conc. = 325.7 Report level label = 52 Pct Recovery = 86% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 262.687 Expected Conc. = 325.7 Report level label = 52 Pct Recovery = 81% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20220810133 Lab Value = 225.593 Expected Conc. = 325.5 Report level label = 52 Pct Recovery = 69% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201550031 Lab Value = 349.601 Expected Conc. = 325.05 Report level label = 52 Pct Recovery = 108% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20202880004 Lab Value = 215.186 Expected Conc. = 320.45 Report level label = 52 Pct Recovery = 67% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 203.257 Expected Conc. = 260.6 Report level label = 52 Pct Recovery = 78% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201960104 Lab Value = 192.964 Expected Conc. = 260.56 Report level label = 52 Pct Recovery = 74% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 214.059 Expected Conc. = 260.56 Report level label = 52 Pct Recovery = 82% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210620006 Lab Value = 146.916 Expected Conc. = 256.36 Report level label = 52 Pct Recovery = 57% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 127.949 Expected Conc. = 256.36 Report level label = 52 Pct Recovery = 50% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20213060210 Lab Value = 70.944 Expected Conc. = 130.88 Report level label = 52 Pct Recovery = 54% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222500483 Lab Value = 99.736 Expected Conc. = 130.8 Report level label = 52 Pct Recovery = 76% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 58.554 Expected Conc. = 130.8 Report level label = 52 Pct Recovery = 45% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210690067 Lab Value = 108.587 Expected Conc. = 130.3 Report level label = 52 Pct Recovery = 83% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20222630205 Lab Value = 94.143 Expected Conc. = 130.2 Report level label = 52 Pct Recovery = 72% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20202330309 Lab Value = 84.038 Expected Conc. = 130.02 Report level label = 52 Pct Recovery = 65% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 110.963 Expected Conc. = 130.02 Report level label = 52 Pct Recovery = 85% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 107.529 Expected Conc. = 130.02 Report level label = 52 Pct Recovery = 83% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 87.742 Expected Conc. = 130.02 Report level label = 52 Pct Recovery = 67% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 132.709 Expected Conc. = 130.02 Report level label = 52 Pct Recovery = 102% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210120050 Lab Value = 70.502 Expected Conc. = 128.18 Report level label = 52 Pct Recovery = 55% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 79.086 Expected Conc. = 128.18 Report level label = 52 Pct Recovery = 62% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 83.977 Expected Conc. = 128.18 Report level label = 52 Pct Recovery = 66% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 65.397 Expected Conc. = 128.18 Report level label = 52 Pct Recovery = 51% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 72.292 Expected Conc. = 128.18 Report level label = 52 Pct Recovery = 56% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 09/28/22 Pct Recovery = 64% Analysis Date = 09/24/22 Pct Recovery = 64% Analysis Date = 09/24/22 Pct Recovery = 64% Analysis Date = 09/20/22 Pct Recovery = 64% Analysis Date = 09/20/22 Pct Recovery = 64% Analysis Date = 09/16/22 Pct Recovery = 64% Analysis Date = 09/16/22 Pct Recovery = 64% Analysis Date = 09/11/22 Pct Recovery = 64% Analysis Date = 09/11/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 08/30/22 Pct Recovery = 64% Analysis Date = 08/30/22 Pct Recovery = 64% Analysis Date = 08/25/22 Pct Recovery = 64% Analysis Date = 08/25/22 Pct Recovery = 64% Analysis Date = 08/21/22 Pct Recovery = 64% Analysis Date = 08/21/22 Pct Recovery = 64% Analysis Date = 08/17/22 Pct Recovery = 64% Analysis Date = 08/17/22 Pct Recovery = 64% Analysis Date = 08/13/22 Pct Recovery = 64% Analysis Date = 08/13/22 Pct Recovery = 64% Analysis Date = 08/08/22 Pct Recovery = 64% Analysis Date = 08/08/22 Pct Recovery = 64% Analysis Date = 08/04/22 Pct Recovery = 64% Analysis Date = 08/04/22 Pct Recovery = 64% Analysis Date = 07/31/22 Pct Recovery = 64% Analysis Date = 07/31/22 Pct Recovery = 64% Analysis Date = 07/27/22 Pct Recovery = 64% Analysis Date = 07/27/22 Pct Recovery = 64% Analysis Date = 07/22/22 Pct Recovery = 64% Analysis Date = 07/22/22 Pct Recovery = 64% Analysis Date = 07/18/22 Pct Recovery = 64% Analysis Date = 07/18/22 Pct Recovery = 64% Analysis Date = 07/14/22 Pct Recovery = 64% Analysis Date = 07/14/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/05/22 Pct Recovery = 64% Analysis Date = 07/05/22 Pct Recovery = 64% Analysis Date = 07/01/22 Pct Recovery = 64% Analysis Date = 07/01/22 Pct Recovery = 64% Analysis Date = 06/27/22 Pct Recovery = 64% Analysis Date = 06/27/22 Pct Recovery = 64% Analysis Date = 06/22/22 Pct Recovery = 64% Analysis Date = 06/22/22 Pct Recovery = 64% Analysis Date = 06/18/22 Pct Recovery = 64% Analysis Date = 06/18/22 Pct Recovery = 64% Analysis Date = 06/14/22 Pct Recovery = 64% Analysis Date = 06/14/22 Pct Recovery = 64% Analysis Date = 06/10/22 Pct Recovery = 64% Analysis Date = 06/10/22 Pct Recovery = 64% Analysis Date = 06/05/22 Pct Recovery = 64% Analysis Date = 06/05/22 Pct Recovery = 64% Analysis Date = 06/01/22 Pct Recovery = 64% Analysis Date = 06/01/22 Pct Recovery = 64% Analysis Date = 05/28/22 Pct Recovery = 64% Analysis Date = 05/28/22 Pct Recovery = 64% Analysis Date = 05/24/22 Pct Recovery = 64% Analysis Date = 05/24/22 Pct Recovery = 64% Analysis Date = 05/19/22 Pct Recovery = 65% Analysis Date = 05/19/22 Pct Recovery = 65% Analysis Date = 05/15/22 Pct Recovery = 65% Analysis Date = 05/15/22 Pct Recovery = 65% Analysis Date = 05/11/22 Pct Recovery = 65% Analysis Date = 05/11/22 Pct Recovery = 65% Analysis Date = 05/06/22 Pct Recovery = 65% Analysis Date = 05/06/22 Pct Recovery = 65% Analysis Date = 05/02/22 Pct Recovery = 65% Analysis Date = 05/02/22 Pct Recovery = 65% Analysis Date = 04/28/22 Pct Recovery = 65% Analysis Date = 04/28/22 Pct Recovery = 65% Analysis Date = 04/24/22 Pct Recovery = 65% Analysis Date = 04/24/22 Pct Recovery = 65% Analysis Date = 04/19/22 Pct Recovery = 65% Analysis Date = 04/19/22 Pct Recovery = 65% Analysis Date = 04/15/22 Pct Recovery = 65% Analysis Date = 04/15/22 Pct Recovery = 65% Analysis Date = 04/11/22 Pct Recovery = 65% Analysis Date = 04/11/22 Pct Recovery = 65% Analysis Date = 04/07/22 Pct Recovery = 65% Analysis Date = 04/07/22 Pct Recovery = 65% Analysis Date = 04/02/22 Pct Recovery = 65% Analysis Date = 04/02/22 Pct Recovery = 65% Analysis Date = 03/29/22 Pct Recovery = 65% Analysis Date = 03/29/22 Pct Recovery = 65% Analysis Date = 03/25/22 Pct Recovery = 65% Analysis Date = 03/25/22 Pct Recovery = 65% Analysis Date = 03/21/22 Pct Recovery = 65% Analysis Date = 03/21/22 Pct Recovery = 65% Analysis Date = 03/16/22 Pct Recovery = 65% Analysis Date = 03/16/22 Pct Recovery = 65% Analysis Date = 03/12/22 Pct Recovery = 65% Analysis Date = 03/12/22 Pct Recovery = 65% Analysis Date = 03/08/22 Pct Recovery = 65% Analysis Date = 03/08/22 Pct Recovery = 65% Analysis Date = 03/04/22 Pct Recovery = 65% Analysis Date = 03/04/22 Pct Recovery = 65% Analysis Date = 02/27/22 Pct Recovery = 65% Analysis Date = 02/27/22 Pct Recovery = 65% Analysis Date = 02/23/22 Pct Recovery = 65% Analysis Date = 02/23/22 Pct Recovery = 65% Analysis Date = 02/19/22 Pct Recovery = 65% Analysis Date = 02/19/22 Pct Recovery = 65% Analysis Date = 02/14/22 Pct Recovery = 65% Analysis Date = 02/14/22 Pct Recovery = 65% Analysis Date = 02/10/22 Pct Recovery = 65% Analysis Date = 02/10/22 Pct Recovery = 65% Analysis Date = 02/06/22 Pct Recovery = 66% Analysis Date = 02/06/22 Pct Recovery = 66% Analysis Date = 02/02/22 Pct Recovery = 66% Analysis Date = 02/02/22 Pct Recovery = 66% Analysis Date = 01/28/22 Pct Recovery = 66% Analysis Date = 01/28/22 Pct Recovery = 66% Analysis Date = 01/24/22 Pct Recovery = 66% Analysis Date = 01/24/22 Pct Recovery = 66% Analysis Date = 01/20/22 Pct Recovery = 66% Analysis Date = 01/20/22 Pct Recovery = 66% Analysis Date = 01/16/22 Pct Recovery = 66% Analysis Date = 01/16/22 Pct Recovery = 66% Analysis Date = 01/11/22 Pct Recovery = 66% Analysis Date = 01/11/22 Pct Recovery = 66% Analysis Date = 01/07/22 Pct Recovery = 66% Analysis Date = 01/07/22 Pct Recovery = 66% Analysis Date = 01/03/22 Pct Recovery = 66% Analysis Date = 01/03/22 Pct Recovery = 66% Analysis Date = 12/30/21 Pct Recovery = 67% Analysis Date = 12/30/21 Pct Recovery = 67% Analysis Date = 12/25/21 Pct Recovery = 67% Analysis Date = 12/25/21 Pct Recovery = 67% Analysis Date = 12/21/21 Pct Recovery = 67% Analysis Date = 12/21/21 Pct Recovery = 67% Analysis Date = 12/17/21 Pct Recovery = 67% Analysis Date = 12/17/21 Pct Recovery = 67% Analysis Date = 12/12/21 Pct Recovery = 67% Analysis Date = 12/12/21 Pct Recovery = 67% Analysis Date = 12/08/21 Pct Recovery = 67% Analysis Date = 12/08/21 Pct Recovery = 67% Analysis Date = 12/04/21 Pct Recovery = 67% Analysis Date = 12/04/21 Pct Recovery = 67% Analysis Date = 11/30/21 Pct Recovery = 67% Analysis Date = 11/30/21 Pct Recovery = 67% Analysis Date = 11/25/21 Pct Recovery = 67% Analysis Date = 11/25/21 Pct Recovery = 67% Analysis Date = 11/21/21 Pct Recovery = 67% Analysis Date = 11/21/21 Pct Recovery = 67% Analysis Date = 11/17/21 Pct Recovery = 67% Analysis Date = 11/17/21 Pct Recovery = 67% Analysis Date = 11/13/21 Pct Recovery = 67% Analysis Date = 11/13/21 Pct Recovery = 67% Analysis Date = 11/08/21 Pct Recovery = 67% Analysis Date = 11/08/21 Pct Recovery = 67% Analysis Date = 11/04/21 Pct Recovery = 67% Analysis Date = 11/04/21 Pct Recovery = 67% Analysis Date = 10/31/21 Pct Recovery = 68% Analysis Date = 10/31/21 Pct Recovery = 68% Analysis Date = 10/27/21 Pct Recovery = 68% Analysis Date = 10/27/21 Pct Recovery = 68% Analysis Date = 10/22/21 Pct Recovery = 68% Analysis Date = 10/22/21 Pct Recovery = 68% Analysis Date = 10/18/21 Pct Recovery = 68% Analysis Date = 10/18/21 Pct Recovery = 68% Analysis Date = 10/14/21 Pct Recovery = 68% Analysis Date = 10/14/21 Pct Recovery = 68% Analysis Date = 10/10/21 Pct Recovery = 68% Analysis Date = 10/10/21 Pct Recovery = 68% Analysis Date = 10/05/21 Pct Recovery = 68% Analysis Date = 10/05/21 Pct Recovery = 68% Analysis Date = 10/01/21 Pct Recovery = 68% Analysis Date = 10/01/21 Pct Recovery = 68% Analysis Date = 09/27/21 Pct Recovery = 68% Analysis Date = 09/27/21 Pct Recovery = 68% Analysis Date = 09/22/21 Pct Recovery = 68% Analysis Date = 09/22/21 Pct Recovery = 68% Analysis Date = 09/18/21 Pct Recovery = 68% Analysis Date = 09/18/21 Pct Recovery = 68% Analysis Date = 09/14/21 Pct Recovery = 68% Analysis Date = 09/14/21 Pct Recovery = 68% Analysis Date = 09/10/21 Pct Recovery = 68% Analysis Date = 09/10/21 Pct Recovery = 68% Analysis Date = 09/05/21 Pct Recovery = 68% Analysis Date = 09/05/21 Pct Recovery = 68% Analysis Date = 09/01/21 Pct Recovery = 68% Analysis Date = 09/01/21 Pct Recovery = 68% Analysis Date = 08/28/21 Pct Recovery = 68% Analysis Date = 08/28/21 Pct Recovery = 68% Analysis Date = 08/24/21 Pct Recovery = 68% Analysis Date = 08/24/21 Pct Recovery = 68% Analysis Date = 08/19/21 Pct Recovery = 68% Analysis Date = 08/19/21 Pct Recovery = 68% Analysis Date = 08/15/21 Pct Recovery = 68% Analysis Date = 08/15/21 Pct Recovery = 68% Analysis Date = 08/11/21 Pct Recovery = 68% Analysis Date = 08/11/21 Pct Recovery = 68% Analysis Date = 08/07/21 Pct Recovery = 68% Analysis Date = 08/07/21 Pct Recovery = 68% Analysis Date = 08/02/21 Pct Recovery = 68% Analysis Date = 08/02/21 Pct Recovery = 68% Analysis Date = 07/29/21 Pct Recovery = 68% Analysis Date = 07/29/21 Pct Recovery = 68% Analysis Date = 07/25/21 Pct Recovery = 68% Analysis Date = 07/25/21 Pct Recovery = 68% Analysis Date = 07/20/21 Pct Recovery = 68% Analysis Date = 07/20/21 Pct Recovery = 68% Analysis Date = 07/16/21 Pct Recovery = 68% Analysis Date = 07/16/21 Pct Recovery = 68% Analysis Date = 07/12/21 Pct Recovery = 68% Analysis Date = 07/12/21 Pct Recovery = 68% Analysis Date = 07/08/21 Pct Recovery = 68% Analysis Date = 07/08/21 Pct Recovery = 68% Analysis Date = 07/03/21 Pct Recovery = 68% Analysis Date = 07/03/21 Pct Recovery = 68% Analysis Date = 06/29/21 Pct Recovery = 68% Analysis Date = 06/29/21 Pct Recovery = 68% Analysis Date = 06/25/21 Pct Recovery = 68% Analysis Date = 06/25/21 Pct Recovery = 68% Analysis Date = 06/21/21 Pct Recovery = 68% Analysis Date = 06/21/21 Pct Recovery = 68% Analysis Date = 06/16/21 Pct Recovery = 68% Analysis Date = 06/16/21 Pct Recovery = 68% Analysis Date = 06/12/21 Pct Recovery = 69% Analysis Date = 06/12/21 Pct Recovery = 69% Analysis Date = 06/08/21 Pct Recovery = 69% Analysis Date = 06/08/21 Pct Recovery = 69% Analysis Date = 06/04/21 Pct Recovery = 69% Analysis Date = 06/04/21 Pct Recovery = 69% Analysis Date = 05/30/21 Pct Recovery = 69% Analysis Date = 05/30/21 Pct Recovery = 69% Analysis Date = 05/26/21 Pct Recovery = 69% Analysis Date = 05/26/21 Pct Recovery = 69% Analysis Date = 05/22/21 Pct Recovery = 69% Analysis Date = 05/22/21 Pct Recovery = 69% Analysis Date = 05/17/21 Pct Recovery = 69% Analysis Date = 05/17/21 Pct Recovery = 69% Analysis Date = 05/13/21 Pct Recovery = 69% Analysis Date = 05/13/21 Pct Recovery = 69% Analysis Date = 05/09/21 Pct Recovery = 69% Analysis Date = 05/09/21 Pct Recovery = 69% Analysis Date = 05/05/21 Pct Recovery = 69% Analysis Date = 05/05/21 Pct Recovery = 69% Analysis Date = 04/30/21 Pct Recovery = 69% Analysis Date = 04/30/21 Pct Recovery = 69% Analysis Date = 04/26/21 Pct Recovery = 69% Analysis Date = 04/26/21 Pct Recovery = 69% Analysis Date = 04/22/21 Pct Recovery = 69% Analysis Date = 04/22/21 Pct Recovery = 69% Analysis Date = 04/18/21 Pct Recovery = 69% Analysis Date = 04/18/21 Pct Recovery = 69% Analysis Date = 04/13/21 Pct Recovery = 69% Analysis Date = 04/13/21 Pct Recovery = 69% Analysis Date = 04/09/21 Pct Recovery = 69% Analysis Date = 04/09/21 Pct Recovery = 69% Analysis Date = 04/05/21 Pct Recovery = 69% Analysis Date = 04/05/21 Pct Recovery = 69% Analysis Date = 04/01/21 Pct Recovery = 68% Analysis Date = 04/01/21 Pct Recovery = 68% Analysis Date = 03/27/21 Pct Recovery = 67% Analysis Date = 03/27/21 Pct Recovery = 67% Analysis Date = 03/23/21 Pct Recovery = 67% Analysis Date = 03/23/21 Pct Recovery = 67% Analysis Date = 03/19/21 Pct Recovery = 66% Analysis Date = 03/19/21 Pct Recovery = 66% Analysis Date = 03/15/21 Pct Recovery = 66% Analysis Date = 03/15/21 Pct Recovery = 66% Analysis Date = 03/10/21 Pct Recovery = 65% Analysis Date = 03/10/21 Pct Recovery = 65% Analysis Date = 03/06/21 Pct Recovery = 65% Analysis Date = 03/06/21 Pct Recovery = 65% Analysis Date = 03/02/21 Pct Recovery = 65% Analysis Date = 03/02/21 Pct Recovery = 65% Analysis Date = 02/25/21 Pct Recovery = 64% Analysis Date = 02/25/21 Pct Recovery = 64% Analysis Date = 02/21/21 Pct Recovery = 64% Analysis Date = 02/21/21 Pct Recovery = 64% Analysis Date = 02/17/21 Pct Recovery = 64% Analysis Date = 02/17/21 Pct Recovery = 64% Analysis Date = 02/13/21 Pct Recovery = 63% Analysis Date = 02/13/21 Pct Recovery = 63% Analysis Date = 02/08/21 Pct Recovery = 63% Analysis Date = 02/08/21 Pct Recovery = 63% Analysis Date = 02/04/21 Pct Recovery = 63% Analysis Date = 02/04/21 Pct Recovery = 63% Analysis Date = 01/31/21 Pct Recovery = 63% Analysis Date = 01/31/21 Pct Recovery = 63% Analysis Date = 01/27/21 Pct Recovery = 62% Analysis Date = 01/27/21 Pct Recovery = 62% Analysis Date = 01/22/21 Pct Recovery = 62% Analysis Date = 01/22/21 Pct Recovery = 62% Analysis Date = 01/18/21 Pct Recovery = 62% Analysis Date = 01/18/21 Pct Recovery = 62% Analysis Date = 01/14/21 Pct Recovery = 62% Analysis Date = 01/14/21 Pct Recovery = 62% Analysis Date = 01/10/21 Pct Recovery = 61% Analysis Date = 01/10/21 Pct Recovery = 61% Analysis Date = 01/05/21 Pct Recovery = 61% Analysis Date = 01/05/21 Pct Recovery = 61% Analysis Date = 01/01/21 Pct Recovery = 61% Analysis Date = 01/01/21 Pct Recovery = 61% Analysis Date = 12/28/20 Pct Recovery = 61% Analysis Date = 12/28/20 Pct Recovery = 61% Analysis Date = 12/23/20 Pct Recovery = 61% Analysis Date = 12/23/20 Pct Recovery = 61% Analysis Date = 12/19/20 Pct Recovery = 60% Analysis Date = 12/19/20 Pct Recovery = 60% Analysis Date = 12/15/20 Pct Recovery = 60% Analysis Date = 12/15/20 Pct Recovery = 60% Analysis Date = 12/11/20 Pct Recovery = 60% Analysis Date = 12/11/20 Pct Recovery = 60% Analysis Date = 12/06/20 Pct Recovery = 60% Analysis Date = 12/06/20 Pct Recovery = 60% Analysis Date = 12/02/20 Pct Recovery = 61% Analysis Date = 12/02/20 Pct Recovery = 61% Analysis Date = 11/28/20 Pct Recovery = 61% Analysis Date = 11/28/20 Pct Recovery = 61% Analysis Date = 11/24/20 Pct Recovery = 61% Analysis Date = 11/24/20 Pct Recovery = 61% Analysis Date = 11/19/20 Pct Recovery = 61% Analysis Date = 11/19/20 Pct Recovery = 61% Analysis Date = 11/15/20 Pct Recovery = 61% Analysis Date = 11/15/20 Pct Recovery = 61% Analysis Date = 11/11/20 Pct Recovery = 62% Analysis Date = 11/11/20 Pct Recovery = 62% Analysis Date = 11/07/20 Pct Recovery = 62% Analysis Date = 11/07/20 Pct Recovery = 62% Analysis Date = 11/02/20 Pct Recovery = 62% Analysis Date = 11/02/20 Pct Recovery = 62% Analysis Date = 10/29/20 Pct Recovery = 62% Analysis Date = 10/29/20 Pct Recovery = 62% Analysis Date = 10/25/20 Pct Recovery = 62% Analysis Date = 10/25/20 Pct Recovery = 62% Analysis Date = 10/21/20 Pct Recovery = 63% Analysis Date = 10/21/20 Pct Recovery = 63% Analysis Date = 10/16/20 Pct Recovery = 63% Analysis Date = 10/16/20 Pct Recovery = 63% Analysis Date = 10/12/20 Pct Recovery = 64% Analysis Date = 10/12/20 Pct Recovery = 64% Analysis Date = 10/08/20 Pct Recovery = 65% Analysis Date = 10/08/20 Pct Recovery = 65% Analysis Date = 10/03/20 Pct Recovery = 65% Analysis Date = 10/03/20 Pct Recovery = 65% Analysis Date = 09/29/20 Pct Recovery = 66% Analysis Date = 09/29/20 Pct Recovery = 66% Analysis Date = 09/25/20 Pct Recovery = 67% Analysis Date = 09/25/20 Pct Recovery = 67% Analysis Date = 09/21/20 Pct Recovery = 68% Analysis Date = 09/21/20 Pct Recovery = 68% Analysis Date = 09/16/20 Pct Recovery = 69% Analysis Date = 09/16/20 Pct Recovery = 69% Analysis Date = 09/12/20 Pct Recovery = 69% Analysis Date = 09/12/20 Pct Recovery = 69% Analysis Date = 09/08/20 Pct Recovery = 70% Analysis Date = 09/08/20 Pct Recovery = 70% Analysis Date = 09/04/20 Pct Recovery = 71% Analysis Date = 09/04/20 Pct Recovery = 71% Analysis Date = 08/30/20 Pct Recovery = 72% Analysis Date = 08/30/20 Pct Recovery = 72% Analysis Date = 08/26/20 Pct Recovery = 73% Analysis Date = 08/26/20 Pct Recovery = 73% Analysis Date = 08/22/20 Pct Recovery = 74% Analysis Date = 08/22/20 Pct Recovery = 74% Analysis Date = 08/18/20 Pct Recovery = 75% Analysis Date = 08/18/20 Pct Recovery = 75% Analysis Date = 08/13/20 Pct Recovery = 76% Analysis Date = 08/13/20 Pct Recovery = 76% Analysis Date = 08/09/20 Pct Recovery = 76% Analysis Date = 08/09/20 Pct Recovery = 76% Analysis Date = 08/05/20 Pct Recovery = 77% Analysis Date = 08/05/20 Pct Recovery = 77% Analysis Date = 07/31/20 Pct Recovery = 78% Analysis Date = 07/31/20 Pct Recovery = 78% Analysis Date = 07/27/20 Pct Recovery = 79% Analysis Date = 07/27/20 Pct Recovery = 79% Analysis Date = 07/23/20 Pct Recovery = 80% Analysis Date = 07/23/20 Pct Recovery = 80% Analysis Date = 07/19/20 Pct Recovery = 81% Analysis Date = 07/19/20 Pct Recovery = 81% Analysis Date = 07/14/20 Pct Recovery = 82% Analysis Date = 07/14/20 Pct Recovery = 82% Analysis Date = 07/10/20 Pct Recovery = 83% Analysis Date = 07/10/20 Pct Recovery = 83% Analysis Date = 07/06/20 Pct Recovery = 84% Analysis Date = 07/06/20 Pct Recovery = 84% Analysis Date = 07/02/20 Pct Recovery = 85% Analysis Date = 07/02/20 Pct Recovery = 85% Analysis Date = 06/27/20 Pct Recovery = 86% Analysis Date = 06/27/20 Pct Recovery = 86% Analysis Date = 06/23/20 Pct Recovery = 87% Analysis Date = 06/23/20 Pct Recovery = 87% Analysis Date = 06/19/20 Pct Recovery = 87% Analysis Date = 06/19/20 Pct Recovery = 87% Analysis Date = 06/15/20 Pct Recovery = 88% Analysis Date = 06/15/20 Pct Recovery = 88% Analysis Date = 06/10/20 Pct Recovery = 89% Analysis Date = 06/10/20 Pct Recovery = 89% Analysis Date = 06/06/20 Pct Recovery = 90% Analysis Date = 06/06/20 Pct Recovery = 90% Analysis Date = 06/02/20 Pct Recovery = 91% Analysis Date = 06/02/20 Pct Recovery = 91% Analysis Date = 05/29/20 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLOROVOS (DICHLORVOS)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 67% 19% 65% 18%
Total 44 67% 19% 65% 18%

Sample Statistics
DICHLOROVOS (DICHLORVOS)

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 7 16% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 69 .  
False Positives 0 0% 0 out of 69

OBSP Determination:
DICROTOPHOS
METHOD: 2447 , TESTIDCODE: 68573LCM60

Laboratory ID = 20213200091 Lab Value = 52.736 Expected Conc. = 25.25 Report level label = 4 Pct Recovery = 209% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202180001 Lab Value = 101.006 Expected Conc. = 10.18 Report level label = 4 Pct Recovery = 992% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201820155 Lab Value = 48.099 Expected Conc. = 50.9 Report level label = 4 Pct Recovery = 94% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 50.350 Expected Conc. = 50.9 Report level label = 4 Pct Recovery = 99% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203080100 Lab Value = 49.760 Expected Conc. = 50.2 Report level label = 4 Pct Recovery = 99% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 47.065 Expected Conc. = 50.2 Report level label = 4 Pct Recovery = 94% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 40.205 Expected Conc. = 50.2 Report level label = 4 Pct Recovery = 80% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202390020 Lab Value = 64.484 Expected Conc. = 50.2 Report level label = 4 Pct Recovery = 128% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20210760015 Lab Value = 43.851 Expected Conc. = 50.17 Report level label = 4 Pct Recovery = 87% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 44.025 Expected Conc. = 50.17 Report level label = 4 Pct Recovery = 88% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 35.284 Expected Conc. = 50.17 Report level label = 4 Pct Recovery = 70% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 43.224 Expected Conc. = 50.17 Report level label = 4 Pct Recovery = 86% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20212990174 Lab Value = 26.145 Expected Conc. = 40.4 Report level label = 4 Pct Recovery = 65% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 24.463 Expected Conc. = 40.16 Report level label = 4 Pct Recovery = 61% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 40.744 Expected Conc. = 40.16 Report level label = 4 Pct Recovery = 101% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 18.424 Expected Conc. = 40 Report level label = 4 Pct Recovery = 46% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20222150193 Lab Value = 21.363 Expected Conc. = 39.84 Report level label = 4 Pct Recovery = 54% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20202530029 Lab Value = 26.194 Expected Conc. = 25.45 Report level label = 4 Pct Recovery = 103% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 22.696 Expected Conc. = 25.45 Report level label = 4 Pct Recovery = 89% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 19.986 Expected Conc. = 25.45 Report level label = 4 Pct Recovery = 79% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20213340027 Lab Value = 19.614 Expected Conc. = 25.25 Report level label = 4 Pct Recovery = 78% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 17.809 Expected Conc. = 25.25 Report level label = 4 Pct Recovery = 71% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 14.944 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 60% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 15.550 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 62% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202880004 Lab Value = 24.964 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 99% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 27.378 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 109% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20210480001 Lab Value = 21.495 Expected Conc. = 25.085 Report level label = 4 Pct Recovery = 86% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 19.810 Expected Conc. = 20.08 Report level label = 4 Pct Recovery = 99% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 16.590 Expected Conc. = 20.08 Report level label = 4 Pct Recovery = 83% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 19.183 Expected Conc. = 20.068 Report level label = 4 Pct Recovery = 96% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202040027 Lab Value = 12.345 Expected Conc. = 10.18 Report level label = 4 Pct Recovery = 121% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 9.085 Expected Conc. = 10.18 Report level label = 4 Pct Recovery = 89% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20213060210 Lab Value = 5.795 Expected Conc. = 10.1 Report level label = 4 Pct Recovery = 57% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222500483 Lab Value = 9.804 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 98% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 18.835 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 188% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210120050 Lab Value = 9.403 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 94% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 8.311 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 83% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 9.378 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 93% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 9.292 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 93% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 8.765 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 87% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210690067 Lab Value = 8.691 Expected Conc. = 10.034 Report level label = 4 Pct Recovery = 87% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 09/20/22 Pct Recovery = 62% Analysis Date = 09/15/22 Pct Recovery = 63% Analysis Date = 09/15/22 Pct Recovery = 63% Analysis Date = 09/11/22 Pct Recovery = 63% Analysis Date = 09/11/22 Pct Recovery = 63% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/02/22 Pct Recovery = 64% Analysis Date = 09/02/22 Pct Recovery = 64% Analysis Date = 08/29/22 Pct Recovery = 65% Analysis Date = 08/29/22 Pct Recovery = 65% Analysis Date = 08/25/22 Pct Recovery = 66% Analysis Date = 08/25/22 Pct Recovery = 66% Analysis Date = 08/21/22 Pct Recovery = 66% Analysis Date = 08/21/22 Pct Recovery = 66% Analysis Date = 08/16/22 Pct Recovery = 67% Analysis Date = 08/16/22 Pct Recovery = 67% Analysis Date = 08/12/22 Pct Recovery = 67% Analysis Date = 08/12/22 Pct Recovery = 67% Analysis Date = 08/08/22 Pct Recovery = 68% Analysis Date = 08/08/22 Pct Recovery = 68% Analysis Date = 08/04/22 Pct Recovery = 68% Analysis Date = 08/04/22 Pct Recovery = 68% Analysis Date = 07/30/22 Pct Recovery = 69% Analysis Date = 07/30/22 Pct Recovery = 69% Analysis Date = 07/26/22 Pct Recovery = 69% Analysis Date = 07/26/22 Pct Recovery = 69% Analysis Date = 07/22/22 Pct Recovery = 70% Analysis Date = 07/22/22 Pct Recovery = 70% Analysis Date = 07/17/22 Pct Recovery = 70% Analysis Date = 07/17/22 Pct Recovery = 70% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 73% Analysis Date = 06/26/22 Pct Recovery = 73% Analysis Date = 06/22/22 Pct Recovery = 73% Analysis Date = 06/22/22 Pct Recovery = 73% Analysis Date = 06/18/22 Pct Recovery = 74% Analysis Date = 06/18/22 Pct Recovery = 74% Analysis Date = 06/13/22 Pct Recovery = 74% Analysis Date = 06/13/22 Pct Recovery = 74% Analysis Date = 06/09/22 Pct Recovery = 74% Analysis Date = 06/09/22 Pct Recovery = 74% Analysis Date = 06/05/22 Pct Recovery = 75% Analysis Date = 06/05/22 Pct Recovery = 75% Analysis Date = 05/31/22 Pct Recovery = 75% Analysis Date = 05/31/22 Pct Recovery = 75% Analysis Date = 05/27/22 Pct Recovery = 76% Analysis Date = 05/27/22 Pct Recovery = 76% Analysis Date = 05/23/22 Pct Recovery = 76% Analysis Date = 05/23/22 Pct Recovery = 76% Analysis Date = 05/19/22 Pct Recovery = 77% Analysis Date = 05/19/22 Pct Recovery = 77% Analysis Date = 05/14/22 Pct Recovery = 77% Analysis Date = 05/14/22 Pct Recovery = 77% Analysis Date = 05/10/22 Pct Recovery = 78% Analysis Date = 05/10/22 Pct Recovery = 78% Analysis Date = 05/06/22 Pct Recovery = 78% Analysis Date = 05/06/22 Pct Recovery = 78% Analysis Date = 05/02/22 Pct Recovery = 79% Analysis Date = 05/02/22 Pct Recovery = 79% Analysis Date = 04/27/22 Pct Recovery = 79% Analysis Date = 04/27/22 Pct Recovery = 79% Analysis Date = 04/23/22 Pct Recovery = 80% Analysis Date = 04/23/22 Pct Recovery = 80% Analysis Date = 04/19/22 Pct Recovery = 80% Analysis Date = 04/19/22 Pct Recovery = 80% Analysis Date = 04/15/22 Pct Recovery = 81% Analysis Date = 04/15/22 Pct Recovery = 81% Analysis Date = 04/10/22 Pct Recovery = 81% Analysis Date = 04/10/22 Pct Recovery = 81% Analysis Date = 04/06/22 Pct Recovery = 82% Analysis Date = 04/06/22 Pct Recovery = 82% Analysis Date = 04/02/22 Pct Recovery = 82% Analysis Date = 04/02/22 Pct Recovery = 82% Analysis Date = 03/28/22 Pct Recovery = 82% Analysis Date = 03/28/22 Pct Recovery = 82% Analysis Date = 03/24/22 Pct Recovery = 83% Analysis Date = 03/24/22 Pct Recovery = 83% Analysis Date = 03/20/22 Pct Recovery = 83% Analysis Date = 03/20/22 Pct Recovery = 83% Analysis Date = 03/16/22 Pct Recovery = 84% Analysis Date = 03/16/22 Pct Recovery = 84% Analysis Date = 03/11/22 Pct Recovery = 84% Analysis Date = 03/11/22 Pct Recovery = 84% Analysis Date = 03/07/22 Pct Recovery = 85% Analysis Date = 03/07/22 Pct Recovery = 85% Analysis Date = 03/03/22 Pct Recovery = 85% Analysis Date = 03/03/22 Pct Recovery = 85% Analysis Date = 02/27/22 Pct Recovery = 86% Analysis Date = 02/27/22 Pct Recovery = 86% Analysis Date = 02/22/22 Pct Recovery = 86% Analysis Date = 02/22/22 Pct Recovery = 86% Analysis Date = 02/18/22 Pct Recovery = 87% Analysis Date = 02/18/22 Pct Recovery = 87% Analysis Date = 02/14/22 Pct Recovery = 87% Analysis Date = 02/14/22 Pct Recovery = 87% Analysis Date = 02/09/22 Pct Recovery = 88% Analysis Date = 02/09/22 Pct Recovery = 88% Analysis Date = 02/05/22 Pct Recovery = 88% Analysis Date = 02/05/22 Pct Recovery = 88% Analysis Date = 02/01/22 Pct Recovery = 89% Analysis Date = 02/01/22 Pct Recovery = 89% Analysis Date = 01/28/22 Pct Recovery = 89% Analysis Date = 01/28/22 Pct Recovery = 89% Analysis Date = 01/23/22 Pct Recovery = 89% Analysis Date = 01/23/22 Pct Recovery = 89% Analysis Date = 01/19/22 Pct Recovery = 90% Analysis Date = 01/19/22 Pct Recovery = 90% Analysis Date = 01/15/22 Pct Recovery = 90% Analysis Date = 01/15/22 Pct Recovery = 90% Analysis Date = 01/11/22 Pct Recovery = 91% Analysis Date = 01/11/22 Pct Recovery = 91% Analysis Date = 01/06/22 Pct Recovery = 91% Analysis Date = 01/06/22 Pct Recovery = 91% Analysis Date = 01/02/22 Pct Recovery = 91% Analysis Date = 01/02/22 Pct Recovery = 91% Analysis Date = 12/29/21 Pct Recovery = 92% Analysis Date = 12/29/21 Pct Recovery = 92% Analysis Date = 12/24/21 Pct Recovery = 92% Analysis Date = 12/24/21 Pct Recovery = 92% Analysis Date = 12/20/21 Pct Recovery = 93% Analysis Date = 12/20/21 Pct Recovery = 93% Analysis Date = 12/16/21 Pct Recovery = 93% Analysis Date = 12/16/21 Pct Recovery = 93% Analysis Date = 12/12/21 Pct Recovery = 93% Analysis Date = 12/12/21 Pct Recovery = 93% Analysis Date = 12/07/21 Pct Recovery = 94% Analysis Date = 12/07/21 Pct Recovery = 94% Analysis Date = 12/03/21 Pct Recovery = 94% Analysis Date = 12/03/21 Pct Recovery = 94% Analysis Date = 11/29/21 Pct Recovery = 95% Analysis Date = 11/29/21 Pct Recovery = 95% Analysis Date = 11/25/21 Pct Recovery = 95% Analysis Date = 11/25/21 Pct Recovery = 95% Analysis Date = 11/20/21 Pct Recovery = 96% Analysis Date = 11/20/21 Pct Recovery = 96% Analysis Date = 11/16/21 Pct Recovery = 96% Analysis Date = 11/16/21 Pct Recovery = 96% Analysis Date = 11/12/21 Pct Recovery = 96% Analysis Date = 11/12/21 Pct Recovery = 96% Analysis Date = 11/08/21 Pct Recovery = 97% Analysis Date = 11/08/21 Pct Recovery = 97% Analysis Date = 11/03/21 Pct Recovery = 97% Analysis Date = 11/03/21 Pct Recovery = 97% Analysis Date = 10/30/21 Pct Recovery = 97% Analysis Date = 10/30/21 Pct Recovery = 97% Analysis Date = 10/26/21 Pct Recovery = 97% Analysis Date = 10/26/21 Pct Recovery = 97% Analysis Date = 10/21/21 Pct Recovery = 96% Analysis Date = 10/21/21 Pct Recovery = 96% Analysis Date = 10/17/21 Pct Recovery = 96% Analysis Date = 10/17/21 Pct Recovery = 96% Analysis Date = 10/13/21 Pct Recovery = 96% Analysis Date = 10/13/21 Pct Recovery = 96% Analysis Date = 10/09/21 Pct Recovery = 96% Analysis Date = 10/09/21 Pct Recovery = 96% Analysis Date = 10/04/21 Pct Recovery = 96% Analysis Date = 10/04/21 Pct Recovery = 96% Analysis Date = 09/30/21 Pct Recovery = 95% Analysis Date = 09/30/21 Pct Recovery = 95% Analysis Date = 09/26/21 Pct Recovery = 95% Analysis Date = 09/26/21 Pct Recovery = 95% Analysis Date = 09/22/21 Pct Recovery = 95% Analysis Date = 09/22/21 Pct Recovery = 95% Analysis Date = 09/17/21 Pct Recovery = 95% Analysis Date = 09/17/21 Pct Recovery = 95% Analysis Date = 09/13/21 Pct Recovery = 94% Analysis Date = 09/13/21 Pct Recovery = 94% Analysis Date = 09/09/21 Pct Recovery = 94% Analysis Date = 09/09/21 Pct Recovery = 94% Analysis Date = 09/04/21 Pct Recovery = 94% Analysis Date = 09/04/21 Pct Recovery = 94% Analysis Date = 08/31/21 Pct Recovery = 94% Analysis Date = 08/31/21 Pct Recovery = 94% Analysis Date = 08/27/21 Pct Recovery = 94% Analysis Date = 08/27/21 Pct Recovery = 94% Analysis Date = 08/23/21 Pct Recovery = 93% Analysis Date = 08/23/21 Pct Recovery = 93% Analysis Date = 08/18/21 Pct Recovery = 93% Analysis Date = 08/18/21 Pct Recovery = 93% Analysis Date = 08/14/21 Pct Recovery = 93% Analysis Date = 08/14/21 Pct Recovery = 93% Analysis Date = 08/10/21 Pct Recovery = 93% Analysis Date = 08/10/21 Pct Recovery = 93% Analysis Date = 08/06/21 Pct Recovery = 92% Analysis Date = 08/06/21 Pct Recovery = 92% Analysis Date = 08/01/21 Pct Recovery = 92% Analysis Date = 08/01/21 Pct Recovery = 92% Analysis Date = 07/28/21 Pct Recovery = 92% Analysis Date = 07/28/21 Pct Recovery = 92% Analysis Date = 07/24/21 Pct Recovery = 92% Analysis Date = 07/24/21 Pct Recovery = 92% Analysis Date = 07/20/21 Pct Recovery = 92% Analysis Date = 07/20/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 91% Analysis Date = 07/15/21 Pct Recovery = 91% Analysis Date = 07/11/21 Pct Recovery = 91% Analysis Date = 07/11/21 Pct Recovery = 91% Analysis Date = 07/07/21 Pct Recovery = 91% Analysis Date = 07/07/21 Pct Recovery = 91% Analysis Date = 07/02/21 Pct Recovery = 91% Analysis Date = 07/02/21 Pct Recovery = 91% Analysis Date = 06/28/21 Pct Recovery = 90% Analysis Date = 06/28/21 Pct Recovery = 90% Analysis Date = 06/24/21 Pct Recovery = 90% Analysis Date = 06/24/21 Pct Recovery = 90% Analysis Date = 06/20/21 Pct Recovery = 90% Analysis Date = 06/20/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/07/21 Pct Recovery = 89% Analysis Date = 06/07/21 Pct Recovery = 89% Analysis Date = 06/03/21 Pct Recovery = 89% Analysis Date = 06/03/21 Pct Recovery = 89% Analysis Date = 05/29/21 Pct Recovery = 89% Analysis Date = 05/29/21 Pct Recovery = 89% Analysis Date = 05/25/21 Pct Recovery = 89% Analysis Date = 05/25/21 Pct Recovery = 89% Analysis Date = 05/21/21 Pct Recovery = 89% Analysis Date = 05/21/21 Pct Recovery = 89% Analysis Date = 05/16/21 Pct Recovery = 88% Analysis Date = 05/16/21 Pct Recovery = 88% Analysis Date = 05/12/21 Pct Recovery = 88% Analysis Date = 05/12/21 Pct Recovery = 88% Analysis Date = 05/08/21 Pct Recovery = 88% Analysis Date = 05/08/21 Pct Recovery = 88% Analysis Date = 05/04/21 Pct Recovery = 88% Analysis Date = 05/04/21 Pct Recovery = 88% Analysis Date = 04/29/21 Pct Recovery = 87% Analysis Date = 04/29/21 Pct Recovery = 87% Analysis Date = 04/25/21 Pct Recovery = 87% Analysis Date = 04/25/21 Pct Recovery = 87% Analysis Date = 04/21/21 Pct Recovery = 87% Analysis Date = 04/21/21 Pct Recovery = 87% Analysis Date = 04/17/21 Pct Recovery = 87% Analysis Date = 04/17/21 Pct Recovery = 87% Analysis Date = 04/12/21 Pct Recovery = 87% Analysis Date = 04/12/21 Pct Recovery = 87% Analysis Date = 04/08/21 Pct Recovery = 86% Analysis Date = 04/08/21 Pct Recovery = 86% Analysis Date = 04/04/21 Pct Recovery = 86% Analysis Date = 04/04/21 Pct Recovery = 86% Analysis Date = 03/30/21 Pct Recovery = 86% Analysis Date = 03/30/21 Pct Recovery = 86% Analysis Date = 03/26/21 Pct Recovery = 86% Analysis Date = 03/26/21 Pct Recovery = 86% Analysis Date = 03/22/21 Pct Recovery = 85% Analysis Date = 03/22/21 Pct Recovery = 85% Analysis Date = 03/18/21 Pct Recovery = 85% Analysis Date = 03/18/21 Pct Recovery = 85% Analysis Date = 03/13/21 Pct Recovery = 85% Analysis Date = 03/13/21 Pct Recovery = 85% Analysis Date = 03/09/21 Pct Recovery = 85% Analysis Date = 03/09/21 Pct Recovery = 85% Analysis Date = 03/05/21 Pct Recovery = 85% Analysis Date = 03/05/21 Pct Recovery = 85% Analysis Date = 03/01/21 Pct Recovery = 85% Analysis Date = 03/01/21 Pct Recovery = 85% Analysis Date = 02/24/21 Pct Recovery = 85% Analysis Date = 02/24/21 Pct Recovery = 85% Analysis Date = 02/20/21 Pct Recovery = 86% Analysis Date = 02/20/21 Pct Recovery = 86% Analysis Date = 02/16/21 Pct Recovery = 87% Analysis Date = 02/16/21 Pct Recovery = 87% Analysis Date = 02/12/21 Pct Recovery = 88% Analysis Date = 02/12/21 Pct Recovery = 88% Analysis Date = 02/07/21 Pct Recovery = 88% Analysis Date = 02/07/21 Pct Recovery = 88% Analysis Date = 02/03/21 Pct Recovery = 89% Analysis Date = 02/03/21 Pct Recovery = 89% Analysis Date = 01/30/21 Pct Recovery = 90% Analysis Date = 01/30/21 Pct Recovery = 90% Analysis Date = 01/25/21 Pct Recovery = 91% Analysis Date = 01/25/21 Pct Recovery = 91% Analysis Date = 01/21/21 Pct Recovery = 93% Analysis Date = 01/21/21 Pct Recovery = 93% Analysis Date = 01/17/21 Pct Recovery = 95% Analysis Date = 01/17/21 Pct Recovery = 95% Analysis Date = 01/13/21 Pct Recovery = 96% Analysis Date = 01/13/21 Pct Recovery = 96% Analysis Date = 01/08/21 Pct Recovery = 98% Analysis Date = 01/08/21 Pct Recovery = 98% Analysis Date = 01/04/21 Pct Recovery = 100% Analysis Date = 01/04/21 Pct Recovery = 100% Analysis Date = 12/31/20 Pct Recovery = 101% Analysis Date = 12/31/20 Pct Recovery = 101% Analysis Date = 12/27/20 Pct Recovery = 103% Analysis Date = 12/27/20 Pct Recovery = 103% Analysis Date = 12/22/20 Pct Recovery = 105% Analysis Date = 12/22/20 Pct Recovery = 105% Analysis Date = 12/18/20 Pct Recovery = 107% Analysis Date = 12/18/20 Pct Recovery = 107% Analysis Date = 12/14/20 Pct Recovery = 108% Analysis Date = 12/14/20 Pct Recovery = 108% Analysis Date = 12/09/20 Pct Recovery = 110% Analysis Date = 12/09/20 Pct Recovery = 110% Analysis Date = 12/05/20 Pct Recovery = 112% Analysis Date = 12/05/20 Pct Recovery = 112% Analysis Date = 12/01/20 Pct Recovery = 114% Analysis Date = 12/01/20 Pct Recovery = 114% Analysis Date = 11/27/20 Pct Recovery = 115% Analysis Date = 11/27/20 Pct Recovery = 115% Analysis Date = 11/22/20 Pct Recovery = 117% Analysis Date = 11/22/20 Pct Recovery = 117% Analysis Date = 11/18/20 Pct Recovery = 119% Analysis Date = 11/18/20 Pct Recovery = 119% Analysis Date = 11/14/20 Pct Recovery = 121% Analysis Date = 11/14/20 Pct Recovery = 121% Analysis Date = 11/10/20 Pct Recovery = 122% Analysis Date = 11/10/20 Pct Recovery = 122% Analysis Date = 11/05/20 Pct Recovery = 124% Analysis Date = 11/05/20 Pct Recovery = 124% Analysis Date = 11/01/20 Pct Recovery = 126% Analysis Date = 11/01/20 Pct Recovery = 126% Analysis Date = 10/28/20 Pct Recovery = 130% Analysis Date = 10/28/20 Pct Recovery = 130% Analysis Date = 10/23/20 Pct Recovery = 133% Analysis Date = 10/23/20 Pct Recovery = 133% Analysis Date = 10/19/20 Pct Recovery = 136% Analysis Date = 10/19/20 Pct Recovery = 136% Analysis Date = 10/15/20 Pct Recovery = 140% Analysis Date = 10/15/20 Pct Recovery = 140% Analysis Date = 10/11/20 Pct Recovery = 142% Analysis Date = 10/11/20 Pct Recovery = 142% Analysis Date = 10/06/20 Pct Recovery = 144% Analysis Date = 10/06/20 Pct Recovery = 144% Analysis Date = 10/02/20 Pct Recovery = 146% Analysis Date = 10/02/20 Pct Recovery = 146% Analysis Date = 09/28/20 Pct Recovery = 147% Analysis Date = 09/28/20 Pct Recovery = 147% Analysis Date = 09/24/20 Pct Recovery = 149% Analysis Date = 09/24/20 Pct Recovery = 149% Analysis Date = 09/19/20 Pct Recovery = 151% Analysis Date = 09/19/20 Pct Recovery = 151% Analysis Date = 09/15/20 Pct Recovery = 152% Analysis Date = 09/15/20 Pct Recovery = 152% Analysis Date = 09/11/20 Pct Recovery = 153% Analysis Date = 09/11/20 Pct Recovery = 153% Analysis Date = 09/07/20 Pct Recovery = 153% Analysis Date = 09/07/20 Pct Recovery = 153% Analysis Date = 09/02/20 Pct Recovery = 153% Analysis Date = 09/02/20 Pct Recovery = 153% Analysis Date = 08/29/20 Pct Recovery = 154% Analysis Date = 08/29/20 Pct Recovery = 154% Analysis Date = 08/25/20 Pct Recovery = 154% Analysis Date = 08/25/20 Pct Recovery = 154% Analysis Date = 08/20/20 Pct Recovery = 154% Analysis Date = 08/20/20 Pct Recovery = 154% Analysis Date = 08/16/20 Pct Recovery = 154% Analysis Date = 08/16/20 Pct Recovery = 154% Analysis Date = 08/12/20 Pct Recovery = 154% Analysis Date = 08/12/20 Pct Recovery = 154% Analysis Date = 08/08/20 Pct Recovery = 154% Analysis Date = 08/08/20 Pct Recovery = 154% Analysis Date = 08/03/20 Pct Recovery = 155% Analysis Date = 08/03/20 Pct Recovery = 155% Analysis Date = 07/30/20 Pct Recovery = 155% Analysis Date = 07/30/20 Pct Recovery = 155% Analysis Date = 07/26/20 Pct Recovery = 155% Analysis Date = 07/26/20 Pct Recovery = 155% Analysis Date = 07/22/20 Pct Recovery = 155% Analysis Date = 07/22/20 Pct Recovery = 155% Analysis Date = 07/17/20 Pct Recovery = 155% Analysis Date = 07/17/20 Pct Recovery = 155% Analysis Date = 07/13/20 Pct Recovery = 155% Analysis Date = 07/13/20 Pct Recovery = 155% Analysis Date = 07/09/20 Pct Recovery = 155% Analysis Date = 07/09/20 Pct Recovery = 155% Analysis Date = 07/04/20 Pct Recovery = 154% Analysis Date = 07/04/20 Pct Recovery = 154% Analysis Date = 06/30/20 Pct Recovery = 154% Analysis Date = 06/30/20 Pct Recovery = 154% Analysis Date = 06/26/20 Pct Recovery = 154% Analysis Date = 06/26/20 Pct Recovery = 154% Analysis Date = 06/22/20 Pct Recovery = 154% Analysis Date = 06/22/20 Pct Recovery = 154% Analysis Date = 06/17/20 Pct Recovery = 154% Analysis Date = 06/17/20 Pct Recovery = 154% Analysis Date = 06/13/20 Pct Recovery = 153% Analysis Date = 06/13/20 Pct Recovery = 153% Analysis Date = 06/09/20 Pct Recovery = 152% Analysis Date = 06/09/20 Pct Recovery = 152% Analysis Date = 06/05/20 Pct Recovery = 151% Analysis Date = 06/05/20 Pct Recovery = 151% Analysis Date = 05/31/20 Pct Recovery = 150% Analysis Date = 05/31/20 Pct Recovery = 150% Analysis Date = 05/27/20 Pct Recovery = 149% Analysis Date = 05/27/20 Pct Recovery = 149% Analysis Date = 05/23/20 Pct Recovery = 149% Analysis Date = 05/23/20 Pct Recovery = 149% Analysis Date = 05/19/20 Pct Recovery = 148% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICROTOPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 114% 144% 89% 15%
Total 41 114% 144% 89% 15%

Sample Statistics
DICROTOPHOS

Characteristic N % % Basis
Plotted 41 93% Spiked
Estimated Values 10 23% Spiked
Deleted Values 4 3% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 3 7% 3 out of 44
Not Spiked 71 .  
False Positives 1 1% 1 out of 68

OBSP Determination:
DIFLUBENZURON
METHOD: 2447 , TESTIDCODE: 68576LCM60

Laboratory ID = 20202390020 Lab Value = 95.581 Expected Conc. = 75.5 Report level label = 6 Pct Recovery = 127% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20201820155 Lab Value = 76.611 Expected Conc. = 75.4 Report level label = 6 Pct Recovery = 102% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 82.809 Expected Conc. = 75.4 Report level label = 6 Pct Recovery = 110% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203230021 Lab Value = 59.006 Expected Conc. = 75.39 Report level label = 6 Pct Recovery = 78% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 68.575 Expected Conc. = 75.39 Report level label = 6 Pct Recovery = 91% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 72.681 Expected Conc. = 75.3 Report level label = 6 Pct Recovery = 97% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 65.319 Expected Conc. = 75.3 Report level label = 6 Pct Recovery = 87% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221520237 Lab Value = 52.451 Expected Conc. = 60.88 Report level label = 6 Pct Recovery = 86% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20222150192 Lab Value = 45.058 Expected Conc. = 60 Report level label = 6 Pct Recovery = 75% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 36.294 Expected Conc. = 60 Report level label = 6 Pct Recovery = 60% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221870197 Lab Value = 23.134 Expected Conc. = 38.05 Report level label = 6 Pct Recovery = 61% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20201960104 Lab Value = 44.956 Expected Conc. = 37.75 Report level label = 6 Pct Recovery = 119% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202530029 Lab Value = 34.827 Expected Conc. = 37.7 Report level label = 6 Pct Recovery = 92% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 33.421 Expected Conc. = 37.7 Report level label = 6 Pct Recovery = 89% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 33.203 Expected Conc. = 37.7 Report level label = 6 Pct Recovery = 88% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20203230018 Lab Value = 33.996 Expected Conc. = 37.65 Report level label = 6 Pct Recovery = 90% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 32.512 Expected Conc. = 37.65 Report level label = 6 Pct Recovery = 86% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 33.484 Expected Conc. = 37.65 Report level label = 6 Pct Recovery = 89% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220740064 Lab Value = 23.805 Expected Conc. = 37.25 Report level label = 6 Pct Recovery = 64% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20221660151 Lab Value = 11.684 Expected Conc. = 15.22 Report level label = 6 Pct Recovery = 77% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20201610160 Lab Value = 14.710 Expected Conc. = 15.1 Report level label = 6 Pct Recovery = 97% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20202180001 Lab Value = 10.617 Expected Conc. = 15.08 Report level label = 6 Pct Recovery = 70% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 15.797 Expected Conc. = 15.08 Report level label = 6 Pct Recovery = 105% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 14.780 Expected Conc. = 15.08 Report level label = 6 Pct Recovery = 98% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210270007 Lab Value = 14.027 Expected Conc. = 15.078 Report level label = 6 Pct Recovery = 93% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 16.430 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 109% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 13.813 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 92% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 14.353 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 95% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 21.604 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 143% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 14.395 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 96% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 11.936 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 79% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 08/15/22 Pct Recovery = 68% Analysis Date = 08/10/22 Pct Recovery = 69% Analysis Date = 08/10/22 Pct Recovery = 69% Analysis Date = 08/06/22 Pct Recovery = 69% Analysis Date = 08/06/22 Pct Recovery = 69% Analysis Date = 08/02/22 Pct Recovery = 69% Analysis Date = 08/02/22 Pct Recovery = 69% Analysis Date = 07/29/22 Pct Recovery = 69% Analysis Date = 07/29/22 Pct Recovery = 69% Analysis Date = 07/25/22 Pct Recovery = 69% Analysis Date = 07/25/22 Pct Recovery = 69% Analysis Date = 07/21/22 Pct Recovery = 70% Analysis Date = 07/21/22 Pct Recovery = 70% Analysis Date = 07/17/22 Pct Recovery = 70% Analysis Date = 07/17/22 Pct Recovery = 70% Analysis Date = 07/13/22 Pct Recovery = 70% Analysis Date = 07/13/22 Pct Recovery = 70% Analysis Date = 07/09/22 Pct Recovery = 70% Analysis Date = 07/09/22 Pct Recovery = 70% Analysis Date = 07/05/22 Pct Recovery = 70% Analysis Date = 07/05/22 Pct Recovery = 70% Analysis Date = 07/01/22 Pct Recovery = 70% Analysis Date = 07/01/22 Pct Recovery = 70% Analysis Date = 06/26/22 Pct Recovery = 71% Analysis Date = 06/26/22 Pct Recovery = 71% Analysis Date = 06/22/22 Pct Recovery = 71% Analysis Date = 06/22/22 Pct Recovery = 71% Analysis Date = 06/18/22 Pct Recovery = 71% Analysis Date = 06/18/22 Pct Recovery = 71% Analysis Date = 06/14/22 Pct Recovery = 71% Analysis Date = 06/14/22 Pct Recovery = 71% Analysis Date = 06/10/22 Pct Recovery = 71% Analysis Date = 06/10/22 Pct Recovery = 71% Analysis Date = 06/06/22 Pct Recovery = 72% Analysis Date = 06/06/22 Pct Recovery = 72% Analysis Date = 06/02/22 Pct Recovery = 72% Analysis Date = 06/02/22 Pct Recovery = 72% Analysis Date = 05/29/22 Pct Recovery = 72% Analysis Date = 05/29/22 Pct Recovery = 72% Analysis Date = 05/25/22 Pct Recovery = 72% Analysis Date = 05/25/22 Pct Recovery = 72% Analysis Date = 05/21/22 Pct Recovery = 72% Analysis Date = 05/21/22 Pct Recovery = 72% Analysis Date = 05/17/22 Pct Recovery = 73% Analysis Date = 05/17/22 Pct Recovery = 73% Analysis Date = 05/12/22 Pct Recovery = 73% Analysis Date = 05/12/22 Pct Recovery = 73% Analysis Date = 05/08/22 Pct Recovery = 73% Analysis Date = 05/08/22 Pct Recovery = 73% Analysis Date = 05/04/22 Pct Recovery = 73% Analysis Date = 05/04/22 Pct Recovery = 73% Analysis Date = 04/30/22 Pct Recovery = 73% Analysis Date = 04/30/22 Pct Recovery = 73% Analysis Date = 04/26/22 Pct Recovery = 74% Analysis Date = 04/26/22 Pct Recovery = 74% Analysis Date = 04/22/22 Pct Recovery = 74% Analysis Date = 04/22/22 Pct Recovery = 74% Analysis Date = 04/18/22 Pct Recovery = 74% Analysis Date = 04/18/22 Pct Recovery = 74% Analysis Date = 04/14/22 Pct Recovery = 74% Analysis Date = 04/14/22 Pct Recovery = 74% Analysis Date = 04/10/22 Pct Recovery = 74% Analysis Date = 04/10/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 75% Analysis Date = 04/06/22 Pct Recovery = 75% Analysis Date = 04/02/22 Pct Recovery = 75% Analysis Date = 04/02/22 Pct Recovery = 75% Analysis Date = 03/28/22 Pct Recovery = 75% Analysis Date = 03/28/22 Pct Recovery = 75% Analysis Date = 03/24/22 Pct Recovery = 75% Analysis Date = 03/24/22 Pct Recovery = 75% Analysis Date = 03/20/22 Pct Recovery = 75% Analysis Date = 03/20/22 Pct Recovery = 75% Analysis Date = 03/16/22 Pct Recovery = 76% Analysis Date = 03/16/22 Pct Recovery = 76% Analysis Date = 03/12/22 Pct Recovery = 76% Analysis Date = 03/12/22 Pct Recovery = 76% Analysis Date = 03/08/22 Pct Recovery = 76% Analysis Date = 03/08/22 Pct Recovery = 76% Analysis Date = 03/04/22 Pct Recovery = 76% Analysis Date = 03/04/22 Pct Recovery = 76% Analysis Date = 02/28/22 Pct Recovery = 76% Analysis Date = 02/28/22 Pct Recovery = 76% Analysis Date = 02/24/22 Pct Recovery = 77% Analysis Date = 02/24/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 77% Analysis Date = 02/11/22 Pct Recovery = 77% Analysis Date = 02/11/22 Pct Recovery = 77% Analysis Date = 02/07/22 Pct Recovery = 77% Analysis Date = 02/07/22 Pct Recovery = 77% Analysis Date = 02/03/22 Pct Recovery = 78% Analysis Date = 02/03/22 Pct Recovery = 78% Analysis Date = 01/30/22 Pct Recovery = 78% Analysis Date = 01/30/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/22/22 Pct Recovery = 78% Analysis Date = 01/22/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/14/22 Pct Recovery = 78% Analysis Date = 01/14/22 Pct Recovery = 78% Analysis Date = 01/10/22 Pct Recovery = 79% Analysis Date = 01/10/22 Pct Recovery = 79% Analysis Date = 01/06/22 Pct Recovery = 79% Analysis Date = 01/06/22 Pct Recovery = 79% Analysis Date = 01/02/22 Pct Recovery = 79% Analysis Date = 01/02/22 Pct Recovery = 79% Analysis Date = 12/28/21 Pct Recovery = 79% Analysis Date = 12/28/21 Pct Recovery = 79% Analysis Date = 12/24/21 Pct Recovery = 79% Analysis Date = 12/24/21 Pct Recovery = 79% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/16/21 Pct Recovery = 80% Analysis Date = 12/16/21 Pct Recovery = 80% Analysis Date = 12/12/21 Pct Recovery = 80% Analysis Date = 12/12/21 Pct Recovery = 80% Analysis Date = 12/08/21 Pct Recovery = 80% Analysis Date = 12/08/21 Pct Recovery = 80% Analysis Date = 12/04/21 Pct Recovery = 80% Analysis Date = 12/04/21 Pct Recovery = 80% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/26/21 Pct Recovery = 81% Analysis Date = 11/26/21 Pct Recovery = 81% Analysis Date = 11/22/21 Pct Recovery = 81% Analysis Date = 11/22/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/13/21 Pct Recovery = 81% Analysis Date = 11/13/21 Pct Recovery = 81% Analysis Date = 11/09/21 Pct Recovery = 82% Analysis Date = 11/09/21 Pct Recovery = 82% Analysis Date = 11/05/21 Pct Recovery = 82% Analysis Date = 11/05/21 Pct Recovery = 82% Analysis Date = 11/01/21 Pct Recovery = 82% Analysis Date = 11/01/21 Pct Recovery = 82% Analysis Date = 10/28/21 Pct Recovery = 82% Analysis Date = 10/28/21 Pct Recovery = 82% Analysis Date = 10/24/21 Pct Recovery = 82% Analysis Date = 10/24/21 Pct Recovery = 82% Analysis Date = 10/20/21 Pct Recovery = 83% Analysis Date = 10/20/21 Pct Recovery = 83% Analysis Date = 10/16/21 Pct Recovery = 83% Analysis Date = 10/16/21 Pct Recovery = 83% Analysis Date = 10/12/21 Pct Recovery = 83% Analysis Date = 10/12/21 Pct Recovery = 83% Analysis Date = 10/08/21 Pct Recovery = 83% Analysis Date = 10/08/21 Pct Recovery = 83% Analysis Date = 10/04/21 Pct Recovery = 83% Analysis Date = 10/04/21 Pct Recovery = 83% Analysis Date = 09/29/21 Pct Recovery = 83% Analysis Date = 09/29/21 Pct Recovery = 83% Analysis Date = 09/25/21 Pct Recovery = 84% Analysis Date = 09/25/21 Pct Recovery = 84% Analysis Date = 09/21/21 Pct Recovery = 84% Analysis Date = 09/21/21 Pct Recovery = 84% Analysis Date = 09/17/21 Pct Recovery = 84% Analysis Date = 09/17/21 Pct Recovery = 84% Analysis Date = 09/13/21 Pct Recovery = 84% Analysis Date = 09/13/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/05/21 Pct Recovery = 85% Analysis Date = 09/05/21 Pct Recovery = 85% Analysis Date = 09/01/21 Pct Recovery = 85% Analysis Date = 09/01/21 Pct Recovery = 85% Analysis Date = 08/28/21 Pct Recovery = 85% Analysis Date = 08/28/21 Pct Recovery = 85% Analysis Date = 08/24/21 Pct Recovery = 85% Analysis Date = 08/24/21 Pct Recovery = 85% Analysis Date = 08/20/21 Pct Recovery = 85% Analysis Date = 08/20/21 Pct Recovery = 85% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/11/21 Pct Recovery = 86% Analysis Date = 08/11/21 Pct Recovery = 86% Analysis Date = 08/07/21 Pct Recovery = 86% Analysis Date = 08/07/21 Pct Recovery = 86% Analysis Date = 08/03/21 Pct Recovery = 86% Analysis Date = 08/03/21 Pct Recovery = 86% Analysis Date = 07/30/21 Pct Recovery = 86% Analysis Date = 07/30/21 Pct Recovery = 86% Analysis Date = 07/26/21 Pct Recovery = 87% Analysis Date = 07/26/21 Pct Recovery = 87% Analysis Date = 07/22/21 Pct Recovery = 87% Analysis Date = 07/22/21 Pct Recovery = 87% Analysis Date = 07/18/21 Pct Recovery = 87% Analysis Date = 07/18/21 Pct Recovery = 87% Analysis Date = 07/14/21 Pct Recovery = 87% Analysis Date = 07/14/21 Pct Recovery = 87% Analysis Date = 07/10/21 Pct Recovery = 87% Analysis Date = 07/10/21 Pct Recovery = 87% Analysis Date = 07/06/21 Pct Recovery = 88% Analysis Date = 07/06/21 Pct Recovery = 88% Analysis Date = 07/02/21 Pct Recovery = 88% Analysis Date = 07/02/21 Pct Recovery = 88% Analysis Date = 06/27/21 Pct Recovery = 88% Analysis Date = 06/27/21 Pct Recovery = 88% Analysis Date = 06/23/21 Pct Recovery = 88% Analysis Date = 06/23/21 Pct Recovery = 88% Analysis Date = 06/19/21 Pct Recovery = 88% Analysis Date = 06/19/21 Pct Recovery = 88% Analysis Date = 06/15/21 Pct Recovery = 89% Analysis Date = 06/15/21 Pct Recovery = 89% Analysis Date = 06/11/21 Pct Recovery = 89% Analysis Date = 06/11/21 Pct Recovery = 89% Analysis Date = 06/07/21 Pct Recovery = 89% Analysis Date = 06/07/21 Pct Recovery = 89% Analysis Date = 06/03/21 Pct Recovery = 89% Analysis Date = 06/03/21 Pct Recovery = 89% Analysis Date = 05/30/21 Pct Recovery = 89% Analysis Date = 05/30/21 Pct Recovery = 89% Analysis Date = 05/26/21 Pct Recovery = 89% Analysis Date = 05/26/21 Pct Recovery = 89% Analysis Date = 05/22/21 Pct Recovery = 90% Analysis Date = 05/22/21 Pct Recovery = 90% Analysis Date = 05/18/21 Pct Recovery = 90% Analysis Date = 05/18/21 Pct Recovery = 90% Analysis Date = 05/13/21 Pct Recovery = 90% Analysis Date = 05/13/21 Pct Recovery = 90% Analysis Date = 05/09/21 Pct Recovery = 90% Analysis Date = 05/09/21 Pct Recovery = 90% Analysis Date = 05/05/21 Pct Recovery = 90% Analysis Date = 05/05/21 Pct Recovery = 90% Analysis Date = 05/01/21 Pct Recovery = 91% Analysis Date = 05/01/21 Pct Recovery = 91% Analysis Date = 04/27/21 Pct Recovery = 91% Analysis Date = 04/27/21 Pct Recovery = 91% Analysis Date = 04/23/21 Pct Recovery = 91% Analysis Date = 04/23/21 Pct Recovery = 91% Analysis Date = 04/19/21 Pct Recovery = 91% Analysis Date = 04/19/21 Pct Recovery = 91% Analysis Date = 04/15/21 Pct Recovery = 91% Analysis Date = 04/15/21 Pct Recovery = 91% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 92% Analysis Date = 04/03/21 Pct Recovery = 92% Analysis Date = 04/03/21 Pct Recovery = 92% Analysis Date = 03/29/21 Pct Recovery = 92% Analysis Date = 03/29/21 Pct Recovery = 92% Analysis Date = 03/25/21 Pct Recovery = 92% Analysis Date = 03/25/21 Pct Recovery = 92% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/01/21 Pct Recovery = 94% Analysis Date = 03/01/21 Pct Recovery = 94% Analysis Date = 02/25/21 Pct Recovery = 94% Analysis Date = 02/25/21 Pct Recovery = 94% Analysis Date = 02/21/21 Pct Recovery = 94% Analysis Date = 02/21/21 Pct Recovery = 94% Analysis Date = 02/17/21 Pct Recovery = 94% Analysis Date = 02/17/21 Pct Recovery = 94% Analysis Date = 02/12/21 Pct Recovery = 94% Analysis Date = 02/12/21 Pct Recovery = 94% Analysis Date = 02/08/21 Pct Recovery = 94% Analysis Date = 02/08/21 Pct Recovery = 94% Analysis Date = 02/04/21 Pct Recovery = 94% Analysis Date = 02/04/21 Pct Recovery = 94% Analysis Date = 01/31/21 Pct Recovery = 94% Analysis Date = 01/31/21 Pct Recovery = 94% Analysis Date = 01/27/21 Pct Recovery = 94% Analysis Date = 01/27/21 Pct Recovery = 94% Analysis Date = 01/23/21 Pct Recovery = 94% Analysis Date = 01/23/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/15/21 Pct Recovery = 94% Analysis Date = 01/15/21 Pct Recovery = 94% Analysis Date = 01/11/21 Pct Recovery = 94% Analysis Date = 01/11/21 Pct Recovery = 94% Analysis Date = 01/07/21 Pct Recovery = 94% Analysis Date = 01/07/21 Pct Recovery = 94% Analysis Date = 01/03/21 Pct Recovery = 94% Analysis Date = 01/03/21 Pct Recovery = 94% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/25/20 Pct Recovery = 95% Analysis Date = 12/25/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 95% Analysis Date = 12/09/20 Pct Recovery = 95% Analysis Date = 12/09/20 Pct Recovery = 95% Analysis Date = 12/05/20 Pct Recovery = 95% Analysis Date = 12/05/20 Pct Recovery = 95% Analysis Date = 12/01/20 Pct Recovery = 96% Analysis Date = 12/01/20 Pct Recovery = 96% Analysis Date = 11/27/20 Pct Recovery = 96% Analysis Date = 11/27/20 Pct Recovery = 96% Analysis Date = 11/23/20 Pct Recovery = 97% Analysis Date = 11/23/20 Pct Recovery = 97% Analysis Date = 11/19/20 Pct Recovery = 97% Analysis Date = 11/19/20 Pct Recovery = 97% Analysis Date = 11/14/20 Pct Recovery = 97% Analysis Date = 11/14/20 Pct Recovery = 97% Analysis Date = 11/10/20 Pct Recovery = 98% Analysis Date = 11/10/20 Pct Recovery = 98% Analysis Date = 11/06/20 Pct Recovery = 98% Analysis Date = 11/06/20 Pct Recovery = 98% Analysis Date = 11/02/20 Pct Recovery = 98% Analysis Date = 11/02/20 Pct Recovery = 98% Analysis Date = 10/29/20 Pct Recovery = 98% Analysis Date = 10/29/20 Pct Recovery = 98% Analysis Date = 10/25/20 Pct Recovery = 98% Analysis Date = 10/25/20 Pct Recovery = 98% Analysis Date = 10/21/20 Pct Recovery = 98% Analysis Date = 10/21/20 Pct Recovery = 98% Analysis Date = 10/17/20 Pct Recovery = 98% Analysis Date = 10/17/20 Pct Recovery = 98% Analysis Date = 10/13/20 Pct Recovery = 98% Analysis Date = 10/13/20 Pct Recovery = 98% Analysis Date = 10/09/20 Pct Recovery = 98% Analysis Date = 10/09/20 Pct Recovery = 98% Analysis Date = 10/05/20 Pct Recovery = 98% Analysis Date = 10/05/20 Pct Recovery = 98% Analysis Date = 09/30/20 Pct Recovery = 97% Analysis Date = 09/30/20 Pct Recovery = 97% Analysis Date = 09/26/20 Pct Recovery = 97% Analysis Date = 09/26/20 Pct Recovery = 97% Analysis Date = 09/22/20 Pct Recovery = 97% Analysis Date = 09/22/20 Pct Recovery = 97% Analysis Date = 09/18/20 Pct Recovery = 97% Analysis Date = 09/18/20 Pct Recovery = 97% Analysis Date = 09/14/20 Pct Recovery = 97% Analysis Date = 09/14/20 Pct Recovery = 97% Analysis Date = 09/10/20 Pct Recovery = 97% Analysis Date = 09/10/20 Pct Recovery = 97% Analysis Date = 09/06/20 Pct Recovery = 97% Analysis Date = 09/06/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 97% Analysis Date = 08/29/20 Pct Recovery = 97% Analysis Date = 08/29/20 Pct Recovery = 97% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/21/20 Pct Recovery = 98% Analysis Date = 08/21/20 Pct Recovery = 98% Analysis Date = 08/16/20 Pct Recovery = 98% Analysis Date = 08/16/20 Pct Recovery = 98% Analysis Date = 08/12/20 Pct Recovery = 98% Analysis Date = 08/12/20 Pct Recovery = 98% Analysis Date = 08/08/20 Pct Recovery = 98% Analysis Date = 08/08/20 Pct Recovery = 98% Analysis Date = 08/04/20 Pct Recovery = 98% Analysis Date = 08/04/20 Pct Recovery = 98% Analysis Date = 07/31/20 Pct Recovery = 99% Analysis Date = 07/31/20 Pct Recovery = 99% Analysis Date = 07/27/20 Pct Recovery = 99% Analysis Date = 07/27/20 Pct Recovery = 99% Analysis Date = 07/23/20 Pct Recovery = 99% Analysis Date = 07/23/20 Pct Recovery = 99% Analysis Date = 07/19/20 Pct Recovery = 99% Analysis Date = 07/19/20 Pct Recovery = 99% Analysis Date = 07/15/20 Pct Recovery = 99% Analysis Date = 07/15/20 Pct Recovery = 99% Analysis Date = 07/11/20 Pct Recovery = 99% Analysis Date = 07/11/20 Pct Recovery = 99% Analysis Date = 07/07/20 Pct Recovery = 99% Analysis Date = 07/07/20 Pct Recovery = 99% Analysis Date = 07/02/20 Pct Recovery = 100% Analysis Date = 07/02/20 Pct Recovery = 100% Analysis Date = 06/28/20 Pct Recovery = 100% Analysis Date = 06/28/20 Pct Recovery = 100% Analysis Date = 06/24/20 Pct Recovery = 100% Analysis Date = 06/24/20 Pct Recovery = 100% Analysis Date = 06/20/20 Pct Recovery = 100% Analysis Date = 06/20/20 Pct Recovery = 100% Analysis Date = 06/16/20 Pct Recovery = 100% Analysis Date = 06/16/20 Pct Recovery = 100% Analysis Date = 06/12/20 Pct Recovery = 100% Analysis Date = 06/12/20 Pct Recovery = 100% Analysis Date = 06/08/20 Pct Recovery = 101% Analysis Date = 06/08/20 Pct Recovery = 101% Analysis Date = 06/04/20 Pct Recovery = 101% Analysis Date = 06/04/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/19/20 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIFLUBENZURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 92% 18% 91% 14%
Total 31 92% 18% 91% 14%

Sample Statistics
DIFLUBENZURON

Characteristic N % % Basis
Plotted 31 97% Spiked
Estimated Values 3 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 1 3% 1 out of 32
Not Spiked 84 .  
False Positives 0 0% 0 out of 84

OBSP Determination:
DIKETONITRILE-ISOXAFLUTOLE
METHOD: 2447 , TESTIDCODE: 68578LCM60

Laboratory ID = 20202390020 Lab Value = 401.109 Expected Conc. = 305.1 Report level label = 10 Pct Recovery = 131% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20201820155 Lab Value = 295.608 Expected Conc. = 300.6 Report level label = 10 Pct Recovery = 98% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 339.128 Expected Conc. = 300.6 Report level label = 10 Pct Recovery = 113% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201960104 Lab Value = 161.787 Expected Conc. = 152.55 Report level label = 10 Pct Recovery = 106% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202530029 Lab Value = 161.004 Expected Conc. = 150.3 Report level label = 10 Pct Recovery = 107% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 118.523 Expected Conc. = 150.3 Report level label = 10 Pct Recovery = 79% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 125.676 Expected Conc. = 150.3 Report level label = 10 Pct Recovery = 84% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202590107 Lab Value = 129.670 Expected Conc. = 125.5 Report level label = 10 Pct Recovery = 103% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 141.462 Expected Conc. = 125.5 Report level label = 10 Pct Recovery = 113% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221370164 Lab Value = 90.715 Expected Conc. = 100.12 Report level label = 10 Pct Recovery = 91% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 104.775 Expected Conc. = 100 Report level label = 10 Pct Recovery = 105% Analysis Date = 08/17/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 86.318 Expected Conc. = 100 Report level label = 10 Pct Recovery = 86% Analysis Date = 07/21/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 78.787 Expected Conc. = 100 Report level label = 10 Pct Recovery = 79% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20203360042 Lab Value = 75.918 Expected Conc. = 62.75 Report level label = 10 Pct Recovery = 121% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 68.323 Expected Conc. = 62.75 Report level label = 10 Pct Recovery = 109% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 72.049 Expected Conc. = 62.75 Report level label = 10 Pct Recovery = 115% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222070177 Lab Value = 56.485 Expected Conc. = 62.5 Report level label = 10 Pct Recovery = 90% Analysis Date = 08/02/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20201610160 Lab Value = 67.481 Expected Conc. = 61.02 Report level label = 10 Pct Recovery = 111% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20202180001 Lab Value = 63.550 Expected Conc. = 60.12 Report level label = 10 Pct Recovery = 106% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 55.453 Expected Conc. = 60.12 Report level label = 10 Pct Recovery = 92% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 56.594 Expected Conc. = 60.12 Report level label = 10 Pct Recovery = 94% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210970035 Lab Value = 22.073 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 88% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 20.092 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 80% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 25.220 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 100% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 26.975 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 107% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 20.721 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 83% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 24.746 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 99% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222000207 Lab Value = 18.680 Expected Conc. = 25 Report level label = 10 Pct Recovery = 75% Analysis Date = 07/26/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Analysis Date = 08/17/22 Pct Recovery = 88% Analysis Date = 08/12/22 Pct Recovery = 88% Analysis Date = 08/12/22 Pct Recovery = 88% Analysis Date = 08/08/22 Pct Recovery = 88% Analysis Date = 08/08/22 Pct Recovery = 88% Analysis Date = 08/04/22 Pct Recovery = 88% Analysis Date = 08/04/22 Pct Recovery = 88% Analysis Date = 07/31/22 Pct Recovery = 88% Analysis Date = 07/31/22 Pct Recovery = 88% Analysis Date = 07/27/22 Pct Recovery = 88% Analysis Date = 07/27/22 Pct Recovery = 88% Analysis Date = 07/23/22 Pct Recovery = 88% Analysis Date = 07/23/22 Pct Recovery = 88% Analysis Date = 07/19/22 Pct Recovery = 88% Analysis Date = 07/19/22 Pct Recovery = 88% Analysis Date = 07/15/22 Pct Recovery = 88% Analysis Date = 07/15/22 Pct Recovery = 88% Analysis Date = 07/11/22 Pct Recovery = 88% Analysis Date = 07/11/22 Pct Recovery = 88% Analysis Date = 07/07/22 Pct Recovery = 88% Analysis Date = 07/07/22 Pct Recovery = 88% Analysis Date = 07/02/22 Pct Recovery = 88% Analysis Date = 07/02/22 Pct Recovery = 88% Analysis Date = 06/28/22 Pct Recovery = 88% Analysis Date = 06/28/22 Pct Recovery = 88% Analysis Date = 06/24/22 Pct Recovery = 88% Analysis Date = 06/24/22 Pct Recovery = 88% Analysis Date = 06/20/22 Pct Recovery = 88% Analysis Date = 06/20/22 Pct Recovery = 88% Analysis Date = 06/16/22 Pct Recovery = 88% Analysis Date = 06/16/22 Pct Recovery = 88% Analysis Date = 06/12/22 Pct Recovery = 88% Analysis Date = 06/12/22 Pct Recovery = 88% Analysis Date = 06/08/22 Pct Recovery = 88% Analysis Date = 06/08/22 Pct Recovery = 88% Analysis Date = 06/04/22 Pct Recovery = 88% Analysis Date = 06/04/22 Pct Recovery = 88% Analysis Date = 05/31/22 Pct Recovery = 88% Analysis Date = 05/31/22 Pct Recovery = 88% Analysis Date = 05/27/22 Pct Recovery = 88% Analysis Date = 05/27/22 Pct Recovery = 88% Analysis Date = 05/23/22 Pct Recovery = 88% Analysis Date = 05/23/22 Pct Recovery = 88% Analysis Date = 05/18/22 Pct Recovery = 88% Analysis Date = 05/18/22 Pct Recovery = 88% Analysis Date = 05/14/22 Pct Recovery = 88% Analysis Date = 05/14/22 Pct Recovery = 88% Analysis Date = 05/10/22 Pct Recovery = 88% Analysis Date = 05/10/22 Pct Recovery = 88% Analysis Date = 05/06/22 Pct Recovery = 88% Analysis Date = 05/06/22 Pct Recovery = 88% Analysis Date = 05/02/22 Pct Recovery = 88% Analysis Date = 05/02/22 Pct Recovery = 88% Analysis Date = 04/28/22 Pct Recovery = 88% Analysis Date = 04/28/22 Pct Recovery = 88% Analysis Date = 04/24/22 Pct Recovery = 88% Analysis Date = 04/24/22 Pct Recovery = 88% Analysis Date = 04/20/22 Pct Recovery = 88% Analysis Date = 04/20/22 Pct Recovery = 88% Analysis Date = 04/16/22 Pct Recovery = 88% Analysis Date = 04/16/22 Pct Recovery = 88% Analysis Date = 04/12/22 Pct Recovery = 88% Analysis Date = 04/12/22 Pct Recovery = 88% Analysis Date = 04/07/22 Pct Recovery = 89% Analysis Date = 04/07/22 Pct Recovery = 89% Analysis Date = 04/03/22 Pct Recovery = 89% Analysis Date = 04/03/22 Pct Recovery = 89% Analysis Date = 03/30/22 Pct Recovery = 89% Analysis Date = 03/30/22 Pct Recovery = 89% Analysis Date = 03/26/22 Pct Recovery = 89% Analysis Date = 03/26/22 Pct Recovery = 89% Analysis Date = 03/22/22 Pct Recovery = 89% Analysis Date = 03/22/22 Pct Recovery = 89% Analysis Date = 03/18/22 Pct Recovery = 89% Analysis Date = 03/18/22 Pct Recovery = 89% Analysis Date = 03/14/22 Pct Recovery = 89% Analysis Date = 03/14/22 Pct Recovery = 89% Analysis Date = 03/10/22 Pct Recovery = 89% Analysis Date = 03/10/22 Pct Recovery = 89% Analysis Date = 03/06/22 Pct Recovery = 89% Analysis Date = 03/06/22 Pct Recovery = 89% Analysis Date = 03/02/22 Pct Recovery = 89% Analysis Date = 03/02/22 Pct Recovery = 89% Analysis Date = 02/26/22 Pct Recovery = 89% Analysis Date = 02/26/22 Pct Recovery = 89% Analysis Date = 02/21/22 Pct Recovery = 89% Analysis Date = 02/21/22 Pct Recovery = 89% Analysis Date = 02/17/22 Pct Recovery = 89% Analysis Date = 02/17/22 Pct Recovery = 89% Analysis Date = 02/13/22 Pct Recovery = 89% Analysis Date = 02/13/22 Pct Recovery = 89% Analysis Date = 02/09/22 Pct Recovery = 89% Analysis Date = 02/09/22 Pct Recovery = 89% Analysis Date = 02/05/22 Pct Recovery = 89% Analysis Date = 02/05/22 Pct Recovery = 89% Analysis Date = 02/01/22 Pct Recovery = 89% Analysis Date = 02/01/22 Pct Recovery = 89% Analysis Date = 01/28/22 Pct Recovery = 89% Analysis Date = 01/28/22 Pct Recovery = 89% Analysis Date = 01/24/22 Pct Recovery = 89% Analysis Date = 01/24/22 Pct Recovery = 89% Analysis Date = 01/20/22 Pct Recovery = 90% Analysis Date = 01/20/22 Pct Recovery = 90% Analysis Date = 01/16/22 Pct Recovery = 90% Analysis Date = 01/16/22 Pct Recovery = 90% Analysis Date = 01/11/22 Pct Recovery = 90% Analysis Date = 01/11/22 Pct Recovery = 90% Analysis Date = 01/07/22 Pct Recovery = 90% Analysis Date = 01/07/22 Pct Recovery = 90% Analysis Date = 01/03/22 Pct Recovery = 90% Analysis Date = 01/03/22 Pct Recovery = 90% Analysis Date = 12/30/21 Pct Recovery = 90% Analysis Date = 12/30/21 Pct Recovery = 90% Analysis Date = 12/26/21 Pct Recovery = 90% Analysis Date = 12/26/21 Pct Recovery = 90% Analysis Date = 12/22/21 Pct Recovery = 90% Analysis Date = 12/22/21 Pct Recovery = 90% Analysis Date = 12/18/21 Pct Recovery = 90% Analysis Date = 12/18/21 Pct Recovery = 90% Analysis Date = 12/14/21 Pct Recovery = 90% Analysis Date = 12/14/21 Pct Recovery = 90% Analysis Date = 12/10/21 Pct Recovery = 90% Analysis Date = 12/10/21 Pct Recovery = 90% Analysis Date = 12/06/21 Pct Recovery = 90% Analysis Date = 12/06/21 Pct Recovery = 90% Analysis Date = 12/02/21 Pct Recovery = 90% Analysis Date = 12/02/21 Pct Recovery = 90% Analysis Date = 11/27/21 Pct Recovery = 90% Analysis Date = 11/27/21 Pct Recovery = 90% Analysis Date = 11/23/21 Pct Recovery = 90% Analysis Date = 11/23/21 Pct Recovery = 90% Analysis Date = 11/19/21 Pct Recovery = 90% Analysis Date = 11/19/21 Pct Recovery = 90% Analysis Date = 11/15/21 Pct Recovery = 90% Analysis Date = 11/15/21 Pct Recovery = 90% Analysis Date = 11/11/21 Pct Recovery = 90% Analysis Date = 11/11/21 Pct Recovery = 90% Analysis Date = 11/07/21 Pct Recovery = 90% Analysis Date = 11/07/21 Pct Recovery = 90% Analysis Date = 11/03/21 Pct Recovery = 91% Analysis Date = 11/03/21 Pct Recovery = 91% Analysis Date = 10/30/21 Pct Recovery = 91% Analysis Date = 10/30/21 Pct Recovery = 91% Analysis Date = 10/26/21 Pct Recovery = 91% Analysis Date = 10/26/21 Pct Recovery = 91% Analysis Date = 10/22/21 Pct Recovery = 91% Analysis Date = 10/22/21 Pct Recovery = 91% Analysis Date = 10/17/21 Pct Recovery = 91% Analysis Date = 10/17/21 Pct Recovery = 91% Analysis Date = 10/13/21 Pct Recovery = 91% Analysis Date = 10/13/21 Pct Recovery = 91% Analysis Date = 10/09/21 Pct Recovery = 91% Analysis Date = 10/09/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/01/21 Pct Recovery = 91% Analysis Date = 10/01/21 Pct Recovery = 91% Analysis Date = 09/27/21 Pct Recovery = 91% Analysis Date = 09/27/21 Pct Recovery = 91% Analysis Date = 09/23/21 Pct Recovery = 91% Analysis Date = 09/23/21 Pct Recovery = 91% Analysis Date = 09/19/21 Pct Recovery = 91% Analysis Date = 09/19/21 Pct Recovery = 91% Analysis Date = 09/15/21 Pct Recovery = 91% Analysis Date = 09/15/21 Pct Recovery = 91% Analysis Date = 09/11/21 Pct Recovery = 91% Analysis Date = 09/11/21 Pct Recovery = 91% Analysis Date = 09/07/21 Pct Recovery = 91% Analysis Date = 09/07/21 Pct Recovery = 91% Analysis Date = 09/02/21 Pct Recovery = 91% Analysis Date = 09/02/21 Pct Recovery = 91% Analysis Date = 08/29/21 Pct Recovery = 91% Analysis Date = 08/29/21 Pct Recovery = 91% Analysis Date = 08/25/21 Pct Recovery = 91% Analysis Date = 08/25/21 Pct Recovery = 91% Analysis Date = 08/21/21 Pct Recovery = 91% Analysis Date = 08/21/21 Pct Recovery = 91% Analysis Date = 08/17/21 Pct Recovery = 91% Analysis Date = 08/17/21 Pct Recovery = 91% Analysis Date = 08/13/21 Pct Recovery = 92% Analysis Date = 08/13/21 Pct Recovery = 92% Analysis Date = 08/09/21 Pct Recovery = 92% Analysis Date = 08/09/21 Pct Recovery = 92% Analysis Date = 08/05/21 Pct Recovery = 92% Analysis Date = 08/05/21 Pct Recovery = 92% Analysis Date = 08/01/21 Pct Recovery = 92% Analysis Date = 08/01/21 Pct Recovery = 92% Analysis Date = 07/28/21 Pct Recovery = 92% Analysis Date = 07/28/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/03/21 Pct Recovery = 92% Analysis Date = 07/03/21 Pct Recovery = 92% Analysis Date = 06/29/21 Pct Recovery = 92% Analysis Date = 06/29/21 Pct Recovery = 92% Analysis Date = 06/25/21 Pct Recovery = 92% Analysis Date = 06/25/21 Pct Recovery = 92% Analysis Date = 06/21/21 Pct Recovery = 92% Analysis Date = 06/21/21 Pct Recovery = 92% Analysis Date = 06/17/21 Pct Recovery = 92% Analysis Date = 06/17/21 Pct Recovery = 92% Analysis Date = 06/13/21 Pct Recovery = 92% Analysis Date = 06/13/21 Pct Recovery = 92% Analysis Date = 06/08/21 Pct Recovery = 92% Analysis Date = 06/08/21 Pct Recovery = 92% Analysis Date = 06/04/21 Pct Recovery = 92% Analysis Date = 06/04/21 Pct Recovery = 92% Analysis Date = 05/31/21 Pct Recovery = 92% Analysis Date = 05/31/21 Pct Recovery = 92% Analysis Date = 05/27/21 Pct Recovery = 93% Analysis Date = 05/27/21 Pct Recovery = 93% Analysis Date = 05/23/21 Pct Recovery = 93% Analysis Date = 05/23/21 Pct Recovery = 93% Analysis Date = 05/19/21 Pct Recovery = 93% Analysis Date = 05/19/21 Pct Recovery = 93% Analysis Date = 05/15/21 Pct Recovery = 93% Analysis Date = 05/15/21 Pct Recovery = 93% Analysis Date = 05/11/21 Pct Recovery = 93% Analysis Date = 05/11/21 Pct Recovery = 93% Analysis Date = 05/07/21 Pct Recovery = 93% Analysis Date = 05/07/21 Pct Recovery = 93% Analysis Date = 05/03/21 Pct Recovery = 93% Analysis Date = 05/03/21 Pct Recovery = 93% Analysis Date = 04/28/21 Pct Recovery = 93% Analysis Date = 04/28/21 Pct Recovery = 93% Analysis Date = 04/24/21 Pct Recovery = 93% Analysis Date = 04/24/21 Pct Recovery = 93% Analysis Date = 04/20/21 Pct Recovery = 93% Analysis Date = 04/20/21 Pct Recovery = 93% Analysis Date = 04/16/21 Pct Recovery = 93% Analysis Date = 04/16/21 Pct Recovery = 93% Analysis Date = 04/12/21 Pct Recovery = 93% Analysis Date = 04/12/21 Pct Recovery = 93% Analysis Date = 04/08/21 Pct Recovery = 93% Analysis Date = 04/08/21 Pct Recovery = 93% Analysis Date = 04/04/21 Pct Recovery = 93% Analysis Date = 04/04/21 Pct Recovery = 93% Analysis Date = 03/31/21 Pct Recovery = 93% Analysis Date = 03/31/21 Pct Recovery = 93% Analysis Date = 03/27/21 Pct Recovery = 93% Analysis Date = 03/27/21 Pct Recovery = 93% Analysis Date = 03/23/21 Pct Recovery = 93% Analysis Date = 03/23/21 Pct Recovery = 93% Analysis Date = 03/19/21 Pct Recovery = 93% Analysis Date = 03/19/21 Pct Recovery = 93% Analysis Date = 03/14/21 Pct Recovery = 93% Analysis Date = 03/14/21 Pct Recovery = 93% Analysis Date = 03/10/21 Pct Recovery = 94% Analysis Date = 03/10/21 Pct Recovery = 94% Analysis Date = 03/06/21 Pct Recovery = 94% Analysis Date = 03/06/21 Pct Recovery = 94% Analysis Date = 03/02/21 Pct Recovery = 94% Analysis Date = 03/02/21 Pct Recovery = 94% Analysis Date = 02/26/21 Pct Recovery = 94% Analysis Date = 02/26/21 Pct Recovery = 94% Analysis Date = 02/22/21 Pct Recovery = 94% Analysis Date = 02/22/21 Pct Recovery = 94% Analysis Date = 02/18/21 Pct Recovery = 94% Analysis Date = 02/18/21 Pct Recovery = 94% Analysis Date = 02/14/21 Pct Recovery = 94% Analysis Date = 02/14/21 Pct Recovery = 94% Analysis Date = 02/10/21 Pct Recovery = 94% Analysis Date = 02/10/21 Pct Recovery = 94% Analysis Date = 02/06/21 Pct Recovery = 95% Analysis Date = 02/06/21 Pct Recovery = 95% Analysis Date = 02/01/21 Pct Recovery = 95% Analysis Date = 02/01/21 Pct Recovery = 95% Analysis Date = 01/28/21 Pct Recovery = 96% Analysis Date = 01/28/21 Pct Recovery = 96% Analysis Date = 01/24/21 Pct Recovery = 96% Analysis Date = 01/24/21 Pct Recovery = 96% Analysis Date = 01/20/21 Pct Recovery = 97% Analysis Date = 01/20/21 Pct Recovery = 97% Analysis Date = 01/16/21 Pct Recovery = 97% Analysis Date = 01/16/21 Pct Recovery = 97% Analysis Date = 01/12/21 Pct Recovery = 98% Analysis Date = 01/12/21 Pct Recovery = 98% Analysis Date = 01/08/21 Pct Recovery = 98% Analysis Date = 01/08/21 Pct Recovery = 98% Analysis Date = 01/04/21 Pct Recovery = 99% Analysis Date = 01/04/21 Pct Recovery = 99% Analysis Date = 12/31/20 Pct Recovery = 99% Analysis Date = 12/31/20 Pct Recovery = 99% Analysis Date = 12/27/20 Pct Recovery = 100% Analysis Date = 12/27/20 Pct Recovery = 100% Analysis Date = 12/23/20 Pct Recovery = 100% Analysis Date = 12/23/20 Pct Recovery = 100% Analysis Date = 12/18/20 Pct Recovery = 101% Analysis Date = 12/18/20 Pct Recovery = 101% Analysis Date = 12/14/20 Pct Recovery = 101% Analysis Date = 12/14/20 Pct Recovery = 101% Analysis Date = 12/10/20 Pct Recovery = 102% Analysis Date = 12/10/20 Pct Recovery = 102% Analysis Date = 12/06/20 Pct Recovery = 102% Analysis Date = 12/06/20 Pct Recovery = 102% Analysis Date = 12/02/20 Pct Recovery = 103% Analysis Date = 12/02/20 Pct Recovery = 103% Analysis Date = 11/28/20 Pct Recovery = 103% Analysis Date = 11/28/20 Pct Recovery = 103% Analysis Date = 11/24/20 Pct Recovery = 104% Analysis Date = 11/24/20 Pct Recovery = 104% Analysis Date = 11/20/20 Pct Recovery = 105% Analysis Date = 11/20/20 Pct Recovery = 105% Analysis Date = 11/16/20 Pct Recovery = 105% Analysis Date = 11/16/20 Pct Recovery = 105% Analysis Date = 11/12/20 Pct Recovery = 106% Analysis Date = 11/12/20 Pct Recovery = 106% Analysis Date = 11/07/20 Pct Recovery = 106% Analysis Date = 11/07/20 Pct Recovery = 106% Analysis Date = 11/03/20 Pct Recovery = 106% Analysis Date = 11/03/20 Pct Recovery = 106% Analysis Date = 10/30/20 Pct Recovery = 106% Analysis Date = 10/30/20 Pct Recovery = 106% Analysis Date = 10/26/20 Pct Recovery = 106% Analysis Date = 10/26/20 Pct Recovery = 106% Analysis Date = 10/22/20 Pct Recovery = 106% Analysis Date = 10/22/20 Pct Recovery = 106% Analysis Date = 10/18/20 Pct Recovery = 106% Analysis Date = 10/18/20 Pct Recovery = 106% Analysis Date = 10/14/20 Pct Recovery = 106% Analysis Date = 10/14/20 Pct Recovery = 106% Analysis Date = 10/10/20 Pct Recovery = 106% Analysis Date = 10/10/20 Pct Recovery = 106% Analysis Date = 10/06/20 Pct Recovery = 105% Analysis Date = 10/06/20 Pct Recovery = 105% Analysis Date = 10/02/20 Pct Recovery = 105% Analysis Date = 10/02/20 Pct Recovery = 105% Analysis Date = 09/28/20 Pct Recovery = 105% Analysis Date = 09/28/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 104% Analysis Date = 09/19/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/07/20 Pct Recovery = 104% Analysis Date = 09/07/20 Pct Recovery = 104% Analysis Date = 09/03/20 Pct Recovery = 104% Analysis Date = 09/03/20 Pct Recovery = 104% Analysis Date = 08/30/20 Pct Recovery = 103% Analysis Date = 08/30/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/18/20 Pct Recovery = 103% Analysis Date = 08/18/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/05/20 Pct Recovery = 102% Analysis Date = 08/05/20 Pct Recovery = 102% Analysis Date = 08/01/20 Pct Recovery = 102% Analysis Date = 08/01/20 Pct Recovery = 102% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 102% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/12/20 Pct Recovery = 101% Analysis Date = 07/12/20 Pct Recovery = 101% Analysis Date = 07/08/20 Pct Recovery = 100% Analysis Date = 07/08/20 Pct Recovery = 100% Analysis Date = 07/04/20 Pct Recovery = 100% Analysis Date = 07/04/20 Pct Recovery = 100% Analysis Date = 06/29/20 Pct Recovery = 100% Analysis Date = 06/29/20 Pct Recovery = 100% Analysis Date = 06/25/20 Pct Recovery = 100% Analysis Date = 06/25/20 Pct Recovery = 100% Analysis Date = 06/21/20 Pct Recovery = 99% Analysis Date = 06/21/20 Pct Recovery = 99% Analysis Date = 06/17/20 Pct Recovery = 99% Analysis Date = 06/17/20 Pct Recovery = 99% Analysis Date = 06/13/20 Pct Recovery = 99% Analysis Date = 06/13/20 Pct Recovery = 99% Analysis Date = 06/09/20 Pct Recovery = 99% Analysis Date = 06/09/20 Pct Recovery = 99% Analysis Date = 06/05/20 Pct Recovery = 98% Analysis Date = 06/05/20 Pct Recovery = 98% Analysis Date = 06/01/20 Pct Recovery = 98% Analysis Date = 06/01/20 Pct Recovery = 98% Analysis Date = 05/28/20 Pct Recovery = 98% Analysis Date = 05/28/20 Pct Recovery = 98% Analysis Date = 05/24/20 Pct Recovery = 98% Analysis Date = 05/24/20 Pct Recovery = 98% Analysis Date = 05/20/20 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIKETONITRILE-ISOXAFLUTOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 28 99% 14% 100% 16%
Total 28 99% 14% 100% 16%

Sample Statistics
DIKETONITRILE-ISOXAFLUTOLE

Characteristic N % % Basis
Plotted 28 97% Spiked
Estimated Values 7 24% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 29 .  
False Negatives 1 3% 1 out of 29
Not Spiked 77 .  
False Positives 1 1% 1 out of 77

OBSP Determination:
DIMETHENAMID
METHOD: 2447 , TESTIDCODE: 68580LCM60

Laboratory ID = 20202390020 Lab Value = 49.625 Expected Conc. = 37.7 Report level label = 3 Pct Recovery = 132% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20210760015 Lab Value = 40.453 Expected Conc. = 37.57 Report level label = 3 Pct Recovery = 108% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 31.933 Expected Conc. = 37.57 Report level label = 3 Pct Recovery = 85% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 30.159 Expected Conc. = 37.57 Report level label = 3 Pct Recovery = 80% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 34.507 Expected Conc. = 37.57 Report level label = 3 Pct Recovery = 92% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201820155 Lab Value = 38.941 Expected Conc. = 37.5 Report level label = 3 Pct Recovery = 104% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 48.034 Expected Conc. = 37.5 Report level label = 3 Pct Recovery = 128% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203080100 Lab Value = 32.243 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 87% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 32.654 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 88% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 36.149 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 97% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150192 Lab Value = 21.749 Expected Conc. = 30.56 Report level label = 3 Pct Recovery = 71% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 27.519 Expected Conc. = 30.064 Report level label = 3 Pct Recovery = 92% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 24.365 Expected Conc. = 30 Report level label = 3 Pct Recovery = 81% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20201960104 Lab Value = 22.950 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 122% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20221870197 Lab Value = 15.252 Expected Conc. = 18.79 Report level label = 3 Pct Recovery = 81% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 15.922 Expected Conc. = 18.785 Report level label = 3 Pct Recovery = 85% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202530029 Lab Value = 20.610 Expected Conc. = 18.75 Report level label = 3 Pct Recovery = 110% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 20.401 Expected Conc. = 18.75 Report level label = 3 Pct Recovery = 109% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 20.876 Expected Conc. = 18.75 Report level label = 3 Pct Recovery = 111% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202880004 Lab Value = 17.574 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 95% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 12.305 Expected Conc. = 15.028 Report level label = 3 Pct Recovery = 82% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 13.750 Expected Conc. = 14.84 Report level label = 3 Pct Recovery = 93% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 13.828 Expected Conc. = 14.84 Report level label = 3 Pct Recovery = 93% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 8.315 Expected Conc. = 7.54 Report level label = 3 Pct Recovery = 110% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20221660151 Lab Value = 8.920 Expected Conc. = 7.516 Report level label = 3 Pct Recovery = 119% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210690067 Lab Value = 5.891 Expected Conc. = 7.514 Report level label = 3 Pct Recovery = 78% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202180001 Lab Value = 7.409 Expected Conc. = 7.5 Report level label = 3 Pct Recovery = 99% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 8.617 Expected Conc. = 7.5 Report level label = 3 Pct Recovery = 115% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 8.057 Expected Conc. = 7.5 Report level label = 3 Pct Recovery = 107% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210120050 Lab Value = 7.030 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 95% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 6.374 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 86% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 4.739 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 64% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 11.263 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 152% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 8.542 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 115% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 88% Analysis Date = 08/10/22 Pct Recovery = 88% Analysis Date = 08/10/22 Pct Recovery = 88% Analysis Date = 08/06/22 Pct Recovery = 88% Analysis Date = 08/06/22 Pct Recovery = 88% Analysis Date = 08/02/22 Pct Recovery = 88% Analysis Date = 08/02/22 Pct Recovery = 88% Analysis Date = 07/29/22 Pct Recovery = 88% Analysis Date = 07/29/22 Pct Recovery = 88% Analysis Date = 07/25/22 Pct Recovery = 88% Analysis Date = 07/25/22 Pct Recovery = 88% Analysis Date = 07/21/22 Pct Recovery = 88% Analysis Date = 07/21/22 Pct Recovery = 88% Analysis Date = 07/17/22 Pct Recovery = 88% Analysis Date = 07/17/22 Pct Recovery = 88% Analysis Date = 07/13/22 Pct Recovery = 88% Analysis Date = 07/13/22 Pct Recovery = 88% Analysis Date = 07/09/22 Pct Recovery = 88% Analysis Date = 07/09/22 Pct Recovery = 88% Analysis Date = 07/05/22 Pct Recovery = 88% Analysis Date = 07/05/22 Pct Recovery = 88% Analysis Date = 07/01/22 Pct Recovery = 88% Analysis Date = 07/01/22 Pct Recovery = 88% Analysis Date = 06/26/22 Pct Recovery = 88% Analysis Date = 06/26/22 Pct Recovery = 88% Analysis Date = 06/22/22 Pct Recovery = 88% Analysis Date = 06/22/22 Pct Recovery = 88% Analysis Date = 06/18/22 Pct Recovery = 88% Analysis Date = 06/18/22 Pct Recovery = 88% Analysis Date = 06/14/22 Pct Recovery = 88% Analysis Date = 06/14/22 Pct Recovery = 88% Analysis Date = 06/10/22 Pct Recovery = 88% Analysis Date = 06/10/22 Pct Recovery = 88% Analysis Date = 06/06/22 Pct Recovery = 88% Analysis Date = 06/06/22 Pct Recovery = 88% Analysis Date = 06/02/22 Pct Recovery = 88% Analysis Date = 06/02/22 Pct Recovery = 88% Analysis Date = 05/29/22 Pct Recovery = 88% Analysis Date = 05/29/22 Pct Recovery = 88% Analysis Date = 05/25/22 Pct Recovery = 88% Analysis Date = 05/25/22 Pct Recovery = 88% Analysis Date = 05/21/22 Pct Recovery = 88% Analysis Date = 05/21/22 Pct Recovery = 88% Analysis Date = 05/17/22 Pct Recovery = 88% Analysis Date = 05/17/22 Pct Recovery = 88% Analysis Date = 05/12/22 Pct Recovery = 88% Analysis Date = 05/12/22 Pct Recovery = 88% Analysis Date = 05/08/22 Pct Recovery = 88% Analysis Date = 05/08/22 Pct Recovery = 88% Analysis Date = 05/04/22 Pct Recovery = 88% Analysis Date = 05/04/22 Pct Recovery = 88% Analysis Date = 04/30/22 Pct Recovery = 88% Analysis Date = 04/30/22 Pct Recovery = 88% Analysis Date = 04/26/22 Pct Recovery = 88% Analysis Date = 04/26/22 Pct Recovery = 88% Analysis Date = 04/22/22 Pct Recovery = 88% Analysis Date = 04/22/22 Pct Recovery = 88% Analysis Date = 04/18/22 Pct Recovery = 88% Analysis Date = 04/18/22 Pct Recovery = 88% Analysis Date = 04/14/22 Pct Recovery = 88% Analysis Date = 04/14/22 Pct Recovery = 88% Analysis Date = 04/10/22 Pct Recovery = 88% Analysis Date = 04/10/22 Pct Recovery = 88% Analysis Date = 04/06/22 Pct Recovery = 88% Analysis Date = 04/06/22 Pct Recovery = 88% Analysis Date = 04/02/22 Pct Recovery = 88% Analysis Date = 04/02/22 Pct Recovery = 88% Analysis Date = 03/28/22 Pct Recovery = 88% Analysis Date = 03/28/22 Pct Recovery = 88% Analysis Date = 03/24/22 Pct Recovery = 88% Analysis Date = 03/24/22 Pct Recovery = 88% Analysis Date = 03/20/22 Pct Recovery = 88% Analysis Date = 03/20/22 Pct Recovery = 88% Analysis Date = 03/16/22 Pct Recovery = 88% Analysis Date = 03/16/22 Pct Recovery = 88% Analysis Date = 03/12/22 Pct Recovery = 88% Analysis Date = 03/12/22 Pct Recovery = 88% Analysis Date = 03/08/22 Pct Recovery = 88% Analysis Date = 03/08/22 Pct Recovery = 88% Analysis Date = 03/04/22 Pct Recovery = 88% Analysis Date = 03/04/22 Pct Recovery = 88% Analysis Date = 02/28/22 Pct Recovery = 88% Analysis Date = 02/28/22 Pct Recovery = 88% Analysis Date = 02/24/22 Pct Recovery = 88% Analysis Date = 02/24/22 Pct Recovery = 88% Analysis Date = 02/20/22 Pct Recovery = 88% Analysis Date = 02/20/22 Pct Recovery = 88% Analysis Date = 02/16/22 Pct Recovery = 88% Analysis Date = 02/16/22 Pct Recovery = 88% Analysis Date = 02/11/22 Pct Recovery = 88% Analysis Date = 02/11/22 Pct Recovery = 88% Analysis Date = 02/07/22 Pct Recovery = 88% Analysis Date = 02/07/22 Pct Recovery = 88% Analysis Date = 02/03/22 Pct Recovery = 88% Analysis Date = 02/03/22 Pct Recovery = 88% Analysis Date = 01/30/22 Pct Recovery = 88% Analysis Date = 01/30/22 Pct Recovery = 88% Analysis Date = 01/26/22 Pct Recovery = 88% Analysis Date = 01/26/22 Pct Recovery = 88% Analysis Date = 01/22/22 Pct Recovery = 88% Analysis Date = 01/22/22 Pct Recovery = 88% Analysis Date = 01/18/22 Pct Recovery = 88% Analysis Date = 01/18/22 Pct Recovery = 88% Analysis Date = 01/14/22 Pct Recovery = 88% Analysis Date = 01/14/22 Pct Recovery = 88% Analysis Date = 01/10/22 Pct Recovery = 88% Analysis Date = 01/10/22 Pct Recovery = 88% Analysis Date = 01/06/22 Pct Recovery = 88% Analysis Date = 01/06/22 Pct Recovery = 88% Analysis Date = 01/02/22 Pct Recovery = 88% Analysis Date = 01/02/22 Pct Recovery = 88% Analysis Date = 12/28/21 Pct Recovery = 88% Analysis Date = 12/28/21 Pct Recovery = 88% Analysis Date = 12/24/21 Pct Recovery = 88% Analysis Date = 12/24/21 Pct Recovery = 88% Analysis Date = 12/20/21 Pct Recovery = 88% Analysis Date = 12/20/21 Pct Recovery = 88% Analysis Date = 12/16/21 Pct Recovery = 88% Analysis Date = 12/16/21 Pct Recovery = 88% Analysis Date = 12/12/21 Pct Recovery = 88% Analysis Date = 12/12/21 Pct Recovery = 88% Analysis Date = 12/08/21 Pct Recovery = 88% Analysis Date = 12/08/21 Pct Recovery = 88% Analysis Date = 12/04/21 Pct Recovery = 88% Analysis Date = 12/04/21 Pct Recovery = 88% Analysis Date = 11/30/21 Pct Recovery = 88% Analysis Date = 11/30/21 Pct Recovery = 88% Analysis Date = 11/26/21 Pct Recovery = 88% Analysis Date = 11/26/21 Pct Recovery = 88% Analysis Date = 11/22/21 Pct Recovery = 88% Analysis Date = 11/22/21 Pct Recovery = 88% Analysis Date = 11/18/21 Pct Recovery = 88% Analysis Date = 11/18/21 Pct Recovery = 88% Analysis Date = 11/13/21 Pct Recovery = 88% Analysis Date = 11/13/21 Pct Recovery = 88% Analysis Date = 11/09/21 Pct Recovery = 88% Analysis Date = 11/09/21 Pct Recovery = 88% Analysis Date = 11/05/21 Pct Recovery = 88% Analysis Date = 11/05/21 Pct Recovery = 88% Analysis Date = 11/01/21 Pct Recovery = 88% Analysis Date = 11/01/21 Pct Recovery = 88% Analysis Date = 10/28/21 Pct Recovery = 88% Analysis Date = 10/28/21 Pct Recovery = 88% Analysis Date = 10/24/21 Pct Recovery = 88% Analysis Date = 10/24/21 Pct Recovery = 88% Analysis Date = 10/20/21 Pct Recovery = 88% Analysis Date = 10/20/21 Pct Recovery = 88% Analysis Date = 10/16/21 Pct Recovery = 88% Analysis Date = 10/16/21 Pct Recovery = 88% Analysis Date = 10/12/21 Pct Recovery = 88% Analysis Date = 10/12/21 Pct Recovery = 88% Analysis Date = 10/08/21 Pct Recovery = 88% Analysis Date = 10/08/21 Pct Recovery = 88% Analysis Date = 10/04/21 Pct Recovery = 88% Analysis Date = 10/04/21 Pct Recovery = 88% Analysis Date = 09/29/21 Pct Recovery = 88% Analysis Date = 09/29/21 Pct Recovery = 88% Analysis Date = 09/25/21 Pct Recovery = 88% Analysis Date = 09/25/21 Pct Recovery = 88% Analysis Date = 09/21/21 Pct Recovery = 88% Analysis Date = 09/21/21 Pct Recovery = 88% Analysis Date = 09/17/21 Pct Recovery = 88% Analysis Date = 09/17/21 Pct Recovery = 88% Analysis Date = 09/13/21 Pct Recovery = 88% Analysis Date = 09/13/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 88% Analysis Date = 09/01/21 Pct Recovery = 88% Analysis Date = 09/01/21 Pct Recovery = 88% Analysis Date = 08/28/21 Pct Recovery = 88% Analysis Date = 08/28/21 Pct Recovery = 88% Analysis Date = 08/24/21 Pct Recovery = 88% Analysis Date = 08/24/21 Pct Recovery = 88% Analysis Date = 08/20/21 Pct Recovery = 88% Analysis Date = 08/20/21 Pct Recovery = 88% Analysis Date = 08/15/21 Pct Recovery = 88% Analysis Date = 08/15/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 88% Analysis Date = 08/03/21 Pct Recovery = 88% Analysis Date = 08/03/21 Pct Recovery = 88% Analysis Date = 07/30/21 Pct Recovery = 88% Analysis Date = 07/30/21 Pct Recovery = 88% Analysis Date = 07/26/21 Pct Recovery = 88% Analysis Date = 07/26/21 Pct Recovery = 88% Analysis Date = 07/22/21 Pct Recovery = 88% Analysis Date = 07/22/21 Pct Recovery = 88% Analysis Date = 07/18/21 Pct Recovery = 88% Analysis Date = 07/18/21 Pct Recovery = 88% Analysis Date = 07/14/21 Pct Recovery = 88% Analysis Date = 07/14/21 Pct Recovery = 88% Analysis Date = 07/10/21 Pct Recovery = 88% Analysis Date = 07/10/21 Pct Recovery = 88% Analysis Date = 07/06/21 Pct Recovery = 88% Analysis Date = 07/06/21 Pct Recovery = 88% Analysis Date = 07/02/21 Pct Recovery = 88% Analysis Date = 07/02/21 Pct Recovery = 88% Analysis Date = 06/27/21 Pct Recovery = 88% Analysis Date = 06/27/21 Pct Recovery = 88% Analysis Date = 06/23/21 Pct Recovery = 88% Analysis Date = 06/23/21 Pct Recovery = 88% Analysis Date = 06/19/21 Pct Recovery = 88% Analysis Date = 06/19/21 Pct Recovery = 88% Analysis Date = 06/15/21 Pct Recovery = 88% Analysis Date = 06/15/21 Pct Recovery = 88% Analysis Date = 06/11/21 Pct Recovery = 88% Analysis Date = 06/11/21 Pct Recovery = 88% Analysis Date = 06/07/21 Pct Recovery = 88% Analysis Date = 06/07/21 Pct Recovery = 88% Analysis Date = 06/03/21 Pct Recovery = 88% Analysis Date = 06/03/21 Pct Recovery = 88% Analysis Date = 05/30/21 Pct Recovery = 88% Analysis Date = 05/30/21 Pct Recovery = 88% Analysis Date = 05/26/21 Pct Recovery = 88% Analysis Date = 05/26/21 Pct Recovery = 88% Analysis Date = 05/22/21 Pct Recovery = 88% Analysis Date = 05/22/21 Pct Recovery = 88% Analysis Date = 05/18/21 Pct Recovery = 88% Analysis Date = 05/18/21 Pct Recovery = 88% Analysis Date = 05/13/21 Pct Recovery = 88% Analysis Date = 05/13/21 Pct Recovery = 88% Analysis Date = 05/09/21 Pct Recovery = 88% Analysis Date = 05/09/21 Pct Recovery = 88% Analysis Date = 05/05/21 Pct Recovery = 88% Analysis Date = 05/05/21 Pct Recovery = 88% Analysis Date = 05/01/21 Pct Recovery = 88% Analysis Date = 05/01/21 Pct Recovery = 88% Analysis Date = 04/27/21 Pct Recovery = 88% Analysis Date = 04/27/21 Pct Recovery = 88% Analysis Date = 04/23/21 Pct Recovery = 88% Analysis Date = 04/23/21 Pct Recovery = 88% Analysis Date = 04/19/21 Pct Recovery = 88% Analysis Date = 04/19/21 Pct Recovery = 88% Analysis Date = 04/15/21 Pct Recovery = 88% Analysis Date = 04/15/21 Pct Recovery = 88% Analysis Date = 04/11/21 Pct Recovery = 88% Analysis Date = 04/11/21 Pct Recovery = 88% Analysis Date = 04/07/21 Pct Recovery = 88% Analysis Date = 04/07/21 Pct Recovery = 88% Analysis Date = 04/03/21 Pct Recovery = 88% Analysis Date = 04/03/21 Pct Recovery = 88% Analysis Date = 03/29/21 Pct Recovery = 88% Analysis Date = 03/29/21 Pct Recovery = 88% Analysis Date = 03/25/21 Pct Recovery = 88% Analysis Date = 03/25/21 Pct Recovery = 88% Analysis Date = 03/21/21 Pct Recovery = 88% Analysis Date = 03/21/21 Pct Recovery = 88% Analysis Date = 03/17/21 Pct Recovery = 88% Analysis Date = 03/17/21 Pct Recovery = 88% Analysis Date = 03/13/21 Pct Recovery = 88% Analysis Date = 03/13/21 Pct Recovery = 88% Analysis Date = 03/09/21 Pct Recovery = 88% Analysis Date = 03/09/21 Pct Recovery = 88% Analysis Date = 03/05/21 Pct Recovery = 88% Analysis Date = 03/05/21 Pct Recovery = 88% Analysis Date = 03/01/21 Pct Recovery = 88% Analysis Date = 03/01/21 Pct Recovery = 88% Analysis Date = 02/25/21 Pct Recovery = 88% Analysis Date = 02/25/21 Pct Recovery = 88% Analysis Date = 02/21/21 Pct Recovery = 88% Analysis Date = 02/21/21 Pct Recovery = 88% Analysis Date = 02/17/21 Pct Recovery = 89% Analysis Date = 02/17/21 Pct Recovery = 89% Analysis Date = 02/12/21 Pct Recovery = 89% Analysis Date = 02/12/21 Pct Recovery = 89% Analysis Date = 02/08/21 Pct Recovery = 89% Analysis Date = 02/08/21 Pct Recovery = 89% Analysis Date = 02/04/21 Pct Recovery = 89% Analysis Date = 02/04/21 Pct Recovery = 89% Analysis Date = 01/31/21 Pct Recovery = 90% Analysis Date = 01/31/21 Pct Recovery = 90% Analysis Date = 01/27/21 Pct Recovery = 90% Analysis Date = 01/27/21 Pct Recovery = 90% Analysis Date = 01/23/21 Pct Recovery = 90% Analysis Date = 01/23/21 Pct Recovery = 90% Analysis Date = 01/19/21 Pct Recovery = 91% Analysis Date = 01/19/21 Pct Recovery = 91% Analysis Date = 01/15/21 Pct Recovery = 91% Analysis Date = 01/15/21 Pct Recovery = 91% Analysis Date = 01/11/21 Pct Recovery = 92% Analysis Date = 01/11/21 Pct Recovery = 92% Analysis Date = 01/07/21 Pct Recovery = 92% Analysis Date = 01/07/21 Pct Recovery = 92% Analysis Date = 01/03/21 Pct Recovery = 93% Analysis Date = 01/03/21 Pct Recovery = 93% Analysis Date = 12/29/20 Pct Recovery = 93% Analysis Date = 12/29/20 Pct Recovery = 93% Analysis Date = 12/25/20 Pct Recovery = 94% Analysis Date = 12/25/20 Pct Recovery = 94% Analysis Date = 12/21/20 Pct Recovery = 94% Analysis Date = 12/21/20 Pct Recovery = 94% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 95% Analysis Date = 12/09/20 Pct Recovery = 96% Analysis Date = 12/09/20 Pct Recovery = 96% Analysis Date = 12/05/20 Pct Recovery = 96% Analysis Date = 12/05/20 Pct Recovery = 96% Analysis Date = 12/01/20 Pct Recovery = 97% Analysis Date = 12/01/20 Pct Recovery = 97% Analysis Date = 11/27/20 Pct Recovery = 97% Analysis Date = 11/27/20 Pct Recovery = 97% Analysis Date = 11/23/20 Pct Recovery = 97% Analysis Date = 11/23/20 Pct Recovery = 97% Analysis Date = 11/19/20 Pct Recovery = 98% Analysis Date = 11/19/20 Pct Recovery = 98% Analysis Date = 11/14/20 Pct Recovery = 98% Analysis Date = 11/14/20 Pct Recovery = 98% Analysis Date = 11/10/20 Pct Recovery = 99% Analysis Date = 11/10/20 Pct Recovery = 99% Analysis Date = 11/06/20 Pct Recovery = 100% Analysis Date = 11/06/20 Pct Recovery = 100% Analysis Date = 11/02/20 Pct Recovery = 100% Analysis Date = 11/02/20 Pct Recovery = 100% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 101% Analysis Date = 10/25/20 Pct Recovery = 102% Analysis Date = 10/25/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 103% Analysis Date = 10/17/20 Pct Recovery = 103% Analysis Date = 10/13/20 Pct Recovery = 104% Analysis Date = 10/13/20 Pct Recovery = 104% Analysis Date = 10/09/20 Pct Recovery = 104% Analysis Date = 10/09/20 Pct Recovery = 104% Analysis Date = 10/05/20 Pct Recovery = 105% Analysis Date = 10/05/20 Pct Recovery = 105% Analysis Date = 09/30/20 Pct Recovery = 106% Analysis Date = 09/30/20 Pct Recovery = 106% Analysis Date = 09/26/20 Pct Recovery = 106% Analysis Date = 09/26/20 Pct Recovery = 106% Analysis Date = 09/22/20 Pct Recovery = 107% Analysis Date = 09/22/20 Pct Recovery = 107% Analysis Date = 09/18/20 Pct Recovery = 107% Analysis Date = 09/18/20 Pct Recovery = 107% Analysis Date = 09/14/20 Pct Recovery = 108% Analysis Date = 09/14/20 Pct Recovery = 108% Analysis Date = 09/10/20 Pct Recovery = 108% Analysis Date = 09/10/20 Pct Recovery = 108% Analysis Date = 09/06/20 Pct Recovery = 108% Analysis Date = 09/06/20 Pct Recovery = 108% Analysis Date = 09/02/20 Pct Recovery = 109% Analysis Date = 09/02/20 Pct Recovery = 109% Analysis Date = 08/29/20 Pct Recovery = 109% Analysis Date = 08/29/20 Pct Recovery = 109% Analysis Date = 08/25/20 Pct Recovery = 109% Analysis Date = 08/25/20 Pct Recovery = 109% Analysis Date = 08/21/20 Pct Recovery = 110% Analysis Date = 08/21/20 Pct Recovery = 110% Analysis Date = 08/16/20 Pct Recovery = 110% Analysis Date = 08/16/20 Pct Recovery = 110% Analysis Date = 08/12/20 Pct Recovery = 110% Analysis Date = 08/12/20 Pct Recovery = 110% Analysis Date = 08/08/20 Pct Recovery = 111% Analysis Date = 08/08/20 Pct Recovery = 111% Analysis Date = 08/04/20 Pct Recovery = 111% Analysis Date = 08/04/20 Pct Recovery = 111% Analysis Date = 07/31/20 Pct Recovery = 111% Analysis Date = 07/31/20 Pct Recovery = 111% Analysis Date = 07/27/20 Pct Recovery = 111% Analysis Date = 07/27/20 Pct Recovery = 111% Analysis Date = 07/23/20 Pct Recovery = 112% Analysis Date = 07/23/20 Pct Recovery = 112% Analysis Date = 07/19/20 Pct Recovery = 112% Analysis Date = 07/19/20 Pct Recovery = 112% Analysis Date = 07/15/20 Pct Recovery = 112% Analysis Date = 07/15/20 Pct Recovery = 112% Analysis Date = 07/11/20 Pct Recovery = 113% Analysis Date = 07/11/20 Pct Recovery = 113% Analysis Date = 07/07/20 Pct Recovery = 113% Analysis Date = 07/07/20 Pct Recovery = 113% Analysis Date = 07/02/20 Pct Recovery = 113% Analysis Date = 07/02/20 Pct Recovery = 113% Analysis Date = 06/28/20 Pct Recovery = 113% Analysis Date = 06/28/20 Pct Recovery = 113% Analysis Date = 06/24/20 Pct Recovery = 114% Analysis Date = 06/24/20 Pct Recovery = 114% Analysis Date = 06/20/20 Pct Recovery = 114% Analysis Date = 06/20/20 Pct Recovery = 114% Analysis Date = 06/16/20 Pct Recovery = 114% Analysis Date = 06/16/20 Pct Recovery = 114% Analysis Date = 06/12/20 Pct Recovery = 114% Analysis Date = 06/12/20 Pct Recovery = 114% Analysis Date = 06/08/20 Pct Recovery = 115% Analysis Date = 06/08/20 Pct Recovery = 115% Analysis Date = 06/04/20 Pct Recovery = 115% Analysis Date = 06/04/20 Pct Recovery = 115% Analysis Date = 05/31/20 Pct Recovery = 115% Analysis Date = 05/31/20 Pct Recovery = 115% Analysis Date = 05/27/20 Pct Recovery = 115% Analysis Date = 05/27/20 Pct Recovery = 115% Analysis Date = 05/23/20 Pct Recovery = 116% Analysis Date = 05/23/20 Pct Recovery = 116% Analysis Date = 05/19/20 Pct Recovery = 116% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHENAMID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 99% 19% 95% 19%
Total 34 99% 19% 95% 19%

Sample Statistics
DIMETHENAMID

Characteristic N % % Basis
Plotted 34 97% Spiked
Estimated Values 4 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
DIMETHOATE
METHOD: 2447 , TESTIDCODE: 66596LCM60

Laboratory ID = 20213200091 Lab Value = 59.723 Expected Conc. = 28.95 Report level label = 4.6 Pct Recovery = 206% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202110006 Lab Value = 54.668 Expected Conc. = 58.3 Report level label = 4.6 Pct Recovery = 94% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 52.563 Expected Conc. = 58 Report level label = 4.6 Pct Recovery = 91% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20210760015 Lab Value = 53.929 Expected Conc. = 57.32 Report level label = 4.6 Pct Recovery = 94% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 49.961 Expected Conc. = 57.32 Report level label = 4.6 Pct Recovery = 87% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 43.718 Expected Conc. = 57.32 Report level label = 4.6 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 48.103 Expected Conc. = 57.32 Report level label = 4.6 Pct Recovery = 84% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 55.438 Expected Conc. = 57.1 Report level label = 4.6 Pct Recovery = 97% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 51.853 Expected Conc. = 57.1 Report level label = 4.6 Pct Recovery = 91% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 46.451 Expected Conc. = 57.1 Report level label = 4.6 Pct Recovery = 81% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20212990174 Lab Value = 27.454 Expected Conc. = 46.32 Report level label = 4.6 Pct Recovery = 59% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222150193 Lab Value = 30.787 Expected Conc. = 46 Report level label = 4.6 Pct Recovery = 67% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20222010132 Lab Value = 22.800 Expected Conc. = 46 Report level label = 4.6 Pct Recovery = 50% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220190116 Lab Value = 22.994 Expected Conc. = 45.68 Report level label = 4.6 Pct Recovery = 50% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 29.771 Expected Conc. = 45.68 Report level label = 4.6 Pct Recovery = 65% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20220810134 Lab Value = 40.833 Expected Conc. = 45.6 Report level label = 4.6 Pct Recovery = 90% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20201680155 Lab Value = 27.958 Expected Conc. = 29.15 Report level label = 4.6 Pct Recovery = 96% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 23.478 Expected Conc. = 29 Report level label = 4.6 Pct Recovery = 81% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 23.204 Expected Conc. = 29 Report level label = 4.6 Pct Recovery = 80% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 24.488 Expected Conc. = 29 Report level label = 4.6 Pct Recovery = 84% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20213340027 Lab Value = 23.169 Expected Conc. = 28.95 Report level label = 4.6 Pct Recovery = 80% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 59.723 Expected Conc. = 28.95 Report level label = 4.6 Pct Recovery = 206% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 17.994 Expected Conc. = 28.95 Report level label = 4.6 Pct Recovery = 62% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20210480001 Lab Value = 20.535 Expected Conc. = 28.66 Report level label = 4.6 Pct Recovery = 72% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221730293 Lab Value = 16.152 Expected Conc. = 28.55 Report level label = 4.6 Pct Recovery = 57% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 14.128 Expected Conc. = 28.55 Report level label = 4.6 Pct Recovery = 49% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202880004 Lab Value = 27.885 Expected Conc. = 28.55 Report level label = 4.6 Pct Recovery = 98% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20220810133 Lab Value = 27.337 Expected Conc. = 28.5 Report level label = 4.6 Pct Recovery = 96% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20210900005 Lab Value = 20.496 Expected Conc. = 22.928 Report level label = 4.6 Pct Recovery = 89% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 24.505 Expected Conc. = 22.84 Report level label = 4.6 Pct Recovery = 107% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 22.602 Expected Conc. = 22.84 Report level label = 4.6 Pct Recovery = 99% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 12.036 Expected Conc. = 11.66 Report level label = 4.6 Pct Recovery = 103% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 7.769 Expected Conc. = 11.6 Report level label = 4.6 Pct Recovery = 67% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 12.924 Expected Conc. = 11.6 Report level label = 4.6 Pct Recovery = 111% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 16.188 Expected Conc. = 11.6 Report level label = 4.6 Pct Recovery = 140% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 12.954 Expected Conc. = 11.6 Report level label = 4.6 Pct Recovery = 112% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20213060210 Lab Value = 6.044 Expected Conc. = 11.58 Report level label = 4.6 Pct Recovery = 52% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210690067 Lab Value = 9.423 Expected Conc. = 11.464 Report level label = 4.6 Pct Recovery = 82% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20222500483 Lab Value = 7.701 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 67% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 9.621 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 84% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210120050 Lab Value = 10.386 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 91% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 11.448 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 100% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 12.230 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 107% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 10.957 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 96% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 12.950 Expected Conc. = 11.42 Report level label = 4.6 Pct Recovery = 113% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 09/20/22 Pct Recovery = 60% Analysis Date = 09/15/22 Pct Recovery = 60% Analysis Date = 09/15/22 Pct Recovery = 60% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/02/22 Pct Recovery = 61% Analysis Date = 09/02/22 Pct Recovery = 61% Analysis Date = 08/29/22 Pct Recovery = 62% Analysis Date = 08/29/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/16/22 Pct Recovery = 63% Analysis Date = 08/16/22 Pct Recovery = 63% Analysis Date = 08/12/22 Pct Recovery = 63% Analysis Date = 08/12/22 Pct Recovery = 63% Analysis Date = 08/08/22 Pct Recovery = 63% Analysis Date = 08/08/22 Pct Recovery = 63% Analysis Date = 08/04/22 Pct Recovery = 64% Analysis Date = 08/04/22 Pct Recovery = 64% Analysis Date = 07/30/22 Pct Recovery = 64% Analysis Date = 07/30/22 Pct Recovery = 64% Analysis Date = 07/26/22 Pct Recovery = 64% Analysis Date = 07/26/22 Pct Recovery = 64% Analysis Date = 07/22/22 Pct Recovery = 65% Analysis Date = 07/22/22 Pct Recovery = 65% Analysis Date = 07/17/22 Pct Recovery = 65% Analysis Date = 07/17/22 Pct Recovery = 65% Analysis Date = 07/13/22 Pct Recovery = 65% Analysis Date = 07/13/22 Pct Recovery = 65% Analysis Date = 07/09/22 Pct Recovery = 66% Analysis Date = 07/09/22 Pct Recovery = 66% Analysis Date = 07/05/22 Pct Recovery = 66% Analysis Date = 07/05/22 Pct Recovery = 66% Analysis Date = 06/30/22 Pct Recovery = 66% Analysis Date = 06/30/22 Pct Recovery = 66% Analysis Date = 06/26/22 Pct Recovery = 66% Analysis Date = 06/26/22 Pct Recovery = 66% Analysis Date = 06/22/22 Pct Recovery = 67% Analysis Date = 06/22/22 Pct Recovery = 67% Analysis Date = 06/18/22 Pct Recovery = 67% Analysis Date = 06/18/22 Pct Recovery = 67% Analysis Date = 06/13/22 Pct Recovery = 67% Analysis Date = 06/13/22 Pct Recovery = 67% Analysis Date = 06/09/22 Pct Recovery = 68% Analysis Date = 06/09/22 Pct Recovery = 68% Analysis Date = 06/05/22 Pct Recovery = 68% Analysis Date = 06/05/22 Pct Recovery = 68% Analysis Date = 05/31/22 Pct Recovery = 68% Analysis Date = 05/31/22 Pct Recovery = 68% Analysis Date = 05/27/22 Pct Recovery = 69% Analysis Date = 05/27/22 Pct Recovery = 69% Analysis Date = 05/23/22 Pct Recovery = 69% Analysis Date = 05/23/22 Pct Recovery = 69% Analysis Date = 05/19/22 Pct Recovery = 69% Analysis Date = 05/19/22 Pct Recovery = 69% Analysis Date = 05/14/22 Pct Recovery = 70% Analysis Date = 05/14/22 Pct Recovery = 70% Analysis Date = 05/10/22 Pct Recovery = 70% Analysis Date = 05/10/22 Pct Recovery = 70% Analysis Date = 05/06/22 Pct Recovery = 70% Analysis Date = 05/06/22 Pct Recovery = 70% Analysis Date = 05/02/22 Pct Recovery = 71% Analysis Date = 05/02/22 Pct Recovery = 71% Analysis Date = 04/27/22 Pct Recovery = 71% Analysis Date = 04/27/22 Pct Recovery = 71% Analysis Date = 04/23/22 Pct Recovery = 71% Analysis Date = 04/23/22 Pct Recovery = 71% Analysis Date = 04/19/22 Pct Recovery = 72% Analysis Date = 04/19/22 Pct Recovery = 72% Analysis Date = 04/15/22 Pct Recovery = 72% Analysis Date = 04/15/22 Pct Recovery = 72% Analysis Date = 04/10/22 Pct Recovery = 72% Analysis Date = 04/10/22 Pct Recovery = 72% Analysis Date = 04/06/22 Pct Recovery = 73% Analysis Date = 04/06/22 Pct Recovery = 73% Analysis Date = 04/02/22 Pct Recovery = 73% Analysis Date = 04/02/22 Pct Recovery = 73% Analysis Date = 03/28/22 Pct Recovery = 73% Analysis Date = 03/28/22 Pct Recovery = 73% Analysis Date = 03/24/22 Pct Recovery = 73% Analysis Date = 03/24/22 Pct Recovery = 73% Analysis Date = 03/20/22 Pct Recovery = 74% Analysis Date = 03/20/22 Pct Recovery = 74% Analysis Date = 03/16/22 Pct Recovery = 74% Analysis Date = 03/16/22 Pct Recovery = 74% Analysis Date = 03/11/22 Pct Recovery = 74% Analysis Date = 03/11/22 Pct Recovery = 74% Analysis Date = 03/07/22 Pct Recovery = 75% Analysis Date = 03/07/22 Pct Recovery = 75% Analysis Date = 03/03/22 Pct Recovery = 75% Analysis Date = 03/03/22 Pct Recovery = 75% Analysis Date = 02/27/22 Pct Recovery = 75% Analysis Date = 02/27/22 Pct Recovery = 75% Analysis Date = 02/22/22 Pct Recovery = 75% Analysis Date = 02/22/22 Pct Recovery = 75% Analysis Date = 02/18/22 Pct Recovery = 76% Analysis Date = 02/18/22 Pct Recovery = 76% Analysis Date = 02/14/22 Pct Recovery = 76% Analysis Date = 02/14/22 Pct Recovery = 76% Analysis Date = 02/09/22 Pct Recovery = 76% Analysis Date = 02/09/22 Pct Recovery = 76% Analysis Date = 02/05/22 Pct Recovery = 77% Analysis Date = 02/05/22 Pct Recovery = 77% Analysis Date = 02/01/22 Pct Recovery = 77% Analysis Date = 02/01/22 Pct Recovery = 77% Analysis Date = 01/28/22 Pct Recovery = 77% Analysis Date = 01/28/22 Pct Recovery = 77% Analysis Date = 01/23/22 Pct Recovery = 78% Analysis Date = 01/23/22 Pct Recovery = 78% Analysis Date = 01/19/22 Pct Recovery = 78% Analysis Date = 01/19/22 Pct Recovery = 78% Analysis Date = 01/15/22 Pct Recovery = 78% Analysis Date = 01/15/22 Pct Recovery = 78% Analysis Date = 01/11/22 Pct Recovery = 78% Analysis Date = 01/11/22 Pct Recovery = 78% Analysis Date = 01/06/22 Pct Recovery = 79% Analysis Date = 01/06/22 Pct Recovery = 79% Analysis Date = 01/02/22 Pct Recovery = 79% Analysis Date = 01/02/22 Pct Recovery = 79% Analysis Date = 12/29/21 Pct Recovery = 79% Analysis Date = 12/29/21 Pct Recovery = 79% Analysis Date = 12/24/21 Pct Recovery = 80% Analysis Date = 12/24/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/16/21 Pct Recovery = 80% Analysis Date = 12/16/21 Pct Recovery = 80% Analysis Date = 12/12/21 Pct Recovery = 80% Analysis Date = 12/12/21 Pct Recovery = 80% Analysis Date = 12/07/21 Pct Recovery = 81% Analysis Date = 12/07/21 Pct Recovery = 81% Analysis Date = 12/03/21 Pct Recovery = 81% Analysis Date = 12/03/21 Pct Recovery = 81% Analysis Date = 11/29/21 Pct Recovery = 81% Analysis Date = 11/29/21 Pct Recovery = 81% Analysis Date = 11/25/21 Pct Recovery = 81% Analysis Date = 11/25/21 Pct Recovery = 81% Analysis Date = 11/20/21 Pct Recovery = 82% Analysis Date = 11/20/21 Pct Recovery = 82% Analysis Date = 11/16/21 Pct Recovery = 82% Analysis Date = 11/16/21 Pct Recovery = 82% Analysis Date = 11/12/21 Pct Recovery = 82% Analysis Date = 11/12/21 Pct Recovery = 82% Analysis Date = 11/08/21 Pct Recovery = 82% Analysis Date = 11/08/21 Pct Recovery = 82% Analysis Date = 11/03/21 Pct Recovery = 82% Analysis Date = 11/03/21 Pct Recovery = 82% Analysis Date = 10/30/21 Pct Recovery = 82% Analysis Date = 10/30/21 Pct Recovery = 82% Analysis Date = 10/26/21 Pct Recovery = 82% Analysis Date = 10/26/21 Pct Recovery = 82% Analysis Date = 10/21/21 Pct Recovery = 82% Analysis Date = 10/21/21 Pct Recovery = 82% Analysis Date = 10/17/21 Pct Recovery = 83% Analysis Date = 10/17/21 Pct Recovery = 83% Analysis Date = 10/13/21 Pct Recovery = 83% Analysis Date = 10/13/21 Pct Recovery = 83% Analysis Date = 10/09/21 Pct Recovery = 83% Analysis Date = 10/09/21 Pct Recovery = 83% Analysis Date = 10/04/21 Pct Recovery = 83% Analysis Date = 10/04/21 Pct Recovery = 83% Analysis Date = 09/30/21 Pct Recovery = 83% Analysis Date = 09/30/21 Pct Recovery = 83% Analysis Date = 09/26/21 Pct Recovery = 83% Analysis Date = 09/26/21 Pct Recovery = 83% Analysis Date = 09/22/21 Pct Recovery = 83% Analysis Date = 09/22/21 Pct Recovery = 83% Analysis Date = 09/17/21 Pct Recovery = 83% Analysis Date = 09/17/21 Pct Recovery = 83% Analysis Date = 09/13/21 Pct Recovery = 84% Analysis Date = 09/13/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/04/21 Pct Recovery = 84% Analysis Date = 09/04/21 Pct Recovery = 84% Analysis Date = 08/31/21 Pct Recovery = 84% Analysis Date = 08/31/21 Pct Recovery = 84% Analysis Date = 08/27/21 Pct Recovery = 84% Analysis Date = 08/27/21 Pct Recovery = 84% Analysis Date = 08/23/21 Pct Recovery = 84% Analysis Date = 08/23/21 Pct Recovery = 84% Analysis Date = 08/18/21 Pct Recovery = 84% Analysis Date = 08/18/21 Pct Recovery = 84% Analysis Date = 08/14/21 Pct Recovery = 84% Analysis Date = 08/14/21 Pct Recovery = 84% Analysis Date = 08/10/21 Pct Recovery = 84% Analysis Date = 08/10/21 Pct Recovery = 84% Analysis Date = 08/06/21 Pct Recovery = 85% Analysis Date = 08/06/21 Pct Recovery = 85% Analysis Date = 08/01/21 Pct Recovery = 85% Analysis Date = 08/01/21 Pct Recovery = 85% Analysis Date = 07/28/21 Pct Recovery = 85% Analysis Date = 07/28/21 Pct Recovery = 85% Analysis Date = 07/24/21 Pct Recovery = 85% Analysis Date = 07/24/21 Pct Recovery = 85% Analysis Date = 07/20/21 Pct Recovery = 85% Analysis Date = 07/20/21 Pct Recovery = 85% Analysis Date = 07/15/21 Pct Recovery = 85% Analysis Date = 07/15/21 Pct Recovery = 85% Analysis Date = 07/11/21 Pct Recovery = 85% Analysis Date = 07/11/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/02/21 Pct Recovery = 86% Analysis Date = 07/02/21 Pct Recovery = 86% Analysis Date = 06/28/21 Pct Recovery = 86% Analysis Date = 06/28/21 Pct Recovery = 86% Analysis Date = 06/24/21 Pct Recovery = 86% Analysis Date = 06/24/21 Pct Recovery = 86% Analysis Date = 06/20/21 Pct Recovery = 86% Analysis Date = 06/20/21 Pct Recovery = 86% Analysis Date = 06/15/21 Pct Recovery = 86% Analysis Date = 06/15/21 Pct Recovery = 86% Analysis Date = 06/11/21 Pct Recovery = 86% Analysis Date = 06/11/21 Pct Recovery = 86% Analysis Date = 06/07/21 Pct Recovery = 86% Analysis Date = 06/07/21 Pct Recovery = 86% Analysis Date = 06/03/21 Pct Recovery = 86% Analysis Date = 06/03/21 Pct Recovery = 86% Analysis Date = 05/29/21 Pct Recovery = 86% Analysis Date = 05/29/21 Pct Recovery = 86% Analysis Date = 05/25/21 Pct Recovery = 87% Analysis Date = 05/25/21 Pct Recovery = 87% Analysis Date = 05/21/21 Pct Recovery = 87% Analysis Date = 05/21/21 Pct Recovery = 87% Analysis Date = 05/16/21 Pct Recovery = 87% Analysis Date = 05/16/21 Pct Recovery = 87% Analysis Date = 05/12/21 Pct Recovery = 87% Analysis Date = 05/12/21 Pct Recovery = 87% Analysis Date = 05/08/21 Pct Recovery = 87% Analysis Date = 05/08/21 Pct Recovery = 87% Analysis Date = 05/04/21 Pct Recovery = 87% Analysis Date = 05/04/21 Pct Recovery = 87% Analysis Date = 04/29/21 Pct Recovery = 87% Analysis Date = 04/29/21 Pct Recovery = 87% Analysis Date = 04/25/21 Pct Recovery = 87% Analysis Date = 04/25/21 Pct Recovery = 87% Analysis Date = 04/21/21 Pct Recovery = 87% Analysis Date = 04/21/21 Pct Recovery = 87% Analysis Date = 04/17/21 Pct Recovery = 88% Analysis Date = 04/17/21 Pct Recovery = 88% Analysis Date = 04/12/21 Pct Recovery = 88% Analysis Date = 04/12/21 Pct Recovery = 88% Analysis Date = 04/08/21 Pct Recovery = 88% Analysis Date = 04/08/21 Pct Recovery = 88% Analysis Date = 04/04/21 Pct Recovery = 88% Analysis Date = 04/04/21 Pct Recovery = 88% Analysis Date = 03/30/21 Pct Recovery = 88% Analysis Date = 03/30/21 Pct Recovery = 88% Analysis Date = 03/26/21 Pct Recovery = 88% Analysis Date = 03/26/21 Pct Recovery = 88% Analysis Date = 03/22/21 Pct Recovery = 88% Analysis Date = 03/22/21 Pct Recovery = 88% Analysis Date = 03/18/21 Pct Recovery = 89% Analysis Date = 03/18/21 Pct Recovery = 89% Analysis Date = 03/13/21 Pct Recovery = 89% Analysis Date = 03/13/21 Pct Recovery = 89% Analysis Date = 03/09/21 Pct Recovery = 89% Analysis Date = 03/09/21 Pct Recovery = 89% Analysis Date = 03/05/21 Pct Recovery = 90% Analysis Date = 03/05/21 Pct Recovery = 90% Analysis Date = 03/01/21 Pct Recovery = 90% Analysis Date = 03/01/21 Pct Recovery = 90% Analysis Date = 02/24/21 Pct Recovery = 90% Analysis Date = 02/24/21 Pct Recovery = 90% Analysis Date = 02/20/21 Pct Recovery = 90% Analysis Date = 02/20/21 Pct Recovery = 90% Analysis Date = 02/16/21 Pct Recovery = 90% Analysis Date = 02/16/21 Pct Recovery = 90% Analysis Date = 02/12/21 Pct Recovery = 91% Analysis Date = 02/12/21 Pct Recovery = 91% Analysis Date = 02/07/21 Pct Recovery = 91% Analysis Date = 02/07/21 Pct Recovery = 91% Analysis Date = 02/03/21 Pct Recovery = 91% Analysis Date = 02/03/21 Pct Recovery = 91% Analysis Date = 01/30/21 Pct Recovery = 91% Analysis Date = 01/30/21 Pct Recovery = 91% Analysis Date = 01/25/21 Pct Recovery = 91% Analysis Date = 01/25/21 Pct Recovery = 91% Analysis Date = 01/21/21 Pct Recovery = 91% Analysis Date = 01/21/21 Pct Recovery = 91% Analysis Date = 01/17/21 Pct Recovery = 91% Analysis Date = 01/17/21 Pct Recovery = 91% Analysis Date = 01/13/21 Pct Recovery = 91% Analysis Date = 01/13/21 Pct Recovery = 91% Analysis Date = 01/08/21 Pct Recovery = 91% Analysis Date = 01/08/21 Pct Recovery = 91% Analysis Date = 01/04/21 Pct Recovery = 91% Analysis Date = 01/04/21 Pct Recovery = 91% Analysis Date = 12/31/20 Pct Recovery = 91% Analysis Date = 12/31/20 Pct Recovery = 91% Analysis Date = 12/27/20 Pct Recovery = 92% Analysis Date = 12/27/20 Pct Recovery = 92% Analysis Date = 12/22/20 Pct Recovery = 92% Analysis Date = 12/22/20 Pct Recovery = 92% Analysis Date = 12/18/20 Pct Recovery = 92% Analysis Date = 12/18/20 Pct Recovery = 92% Analysis Date = 12/14/20 Pct Recovery = 92% Analysis Date = 12/14/20 Pct Recovery = 92% Analysis Date = 12/09/20 Pct Recovery = 92% Analysis Date = 12/09/20 Pct Recovery = 92% Analysis Date = 12/05/20 Pct Recovery = 92% Analysis Date = 12/05/20 Pct Recovery = 92% Analysis Date = 12/01/20 Pct Recovery = 92% Analysis Date = 12/01/20 Pct Recovery = 92% Analysis Date = 11/27/20 Pct Recovery = 92% Analysis Date = 11/27/20 Pct Recovery = 92% Analysis Date = 11/22/20 Pct Recovery = 92% Analysis Date = 11/22/20 Pct Recovery = 92% Analysis Date = 11/18/20 Pct Recovery = 92% Analysis Date = 11/18/20 Pct Recovery = 92% Analysis Date = 11/14/20 Pct Recovery = 92% Analysis Date = 11/14/20 Pct Recovery = 92% Analysis Date = 11/10/20 Pct Recovery = 92% Analysis Date = 11/10/20 Pct Recovery = 92% Analysis Date = 11/05/20 Pct Recovery = 93% Analysis Date = 11/05/20 Pct Recovery = 93% Analysis Date = 11/01/20 Pct Recovery = 93% Analysis Date = 11/01/20 Pct Recovery = 93% Analysis Date = 10/28/20 Pct Recovery = 93% Analysis Date = 10/28/20 Pct Recovery = 93% Analysis Date = 10/23/20 Pct Recovery = 93% Analysis Date = 10/23/20 Pct Recovery = 93% Analysis Date = 10/19/20 Pct Recovery = 94% Analysis Date = 10/19/20 Pct Recovery = 94% Analysis Date = 10/15/20 Pct Recovery = 94% Analysis Date = 10/15/20 Pct Recovery = 94% Analysis Date = 10/11/20 Pct Recovery = 94% Analysis Date = 10/11/20 Pct Recovery = 94% Analysis Date = 10/06/20 Pct Recovery = 94% Analysis Date = 10/06/20 Pct Recovery = 94% Analysis Date = 10/02/20 Pct Recovery = 95% Analysis Date = 10/02/20 Pct Recovery = 95% Analysis Date = 09/28/20 Pct Recovery = 95% Analysis Date = 09/28/20 Pct Recovery = 95% Analysis Date = 09/24/20 Pct Recovery = 95% Analysis Date = 09/24/20 Pct Recovery = 95% Analysis Date = 09/19/20 Pct Recovery = 95% Analysis Date = 09/19/20 Pct Recovery = 95% Analysis Date = 09/15/20 Pct Recovery = 96% Analysis Date = 09/15/20 Pct Recovery = 96% Analysis Date = 09/11/20 Pct Recovery = 96% Analysis Date = 09/11/20 Pct Recovery = 96% Analysis Date = 09/07/20 Pct Recovery = 96% Analysis Date = 09/07/20 Pct Recovery = 96% Analysis Date = 09/02/20 Pct Recovery = 96% Analysis Date = 09/02/20 Pct Recovery = 96% Analysis Date = 08/29/20 Pct Recovery = 96% Analysis Date = 08/29/20 Pct Recovery = 96% Analysis Date = 08/25/20 Pct Recovery = 97% Analysis Date = 08/25/20 Pct Recovery = 97% Analysis Date = 08/20/20 Pct Recovery = 97% Analysis Date = 08/20/20 Pct Recovery = 97% Analysis Date = 08/16/20 Pct Recovery = 97% Analysis Date = 08/16/20 Pct Recovery = 97% Analysis Date = 08/12/20 Pct Recovery = 97% Analysis Date = 08/12/20 Pct Recovery = 97% Analysis Date = 08/08/20 Pct Recovery = 97% Analysis Date = 08/08/20 Pct Recovery = 97% Analysis Date = 08/03/20 Pct Recovery = 97% Analysis Date = 08/03/20 Pct Recovery = 97% Analysis Date = 07/30/20 Pct Recovery = 97% Analysis Date = 07/30/20 Pct Recovery = 97% Analysis Date = 07/26/20 Pct Recovery = 98% Analysis Date = 07/26/20 Pct Recovery = 98% Analysis Date = 07/22/20 Pct Recovery = 98% Analysis Date = 07/22/20 Pct Recovery = 98% Analysis Date = 07/17/20 Pct Recovery = 98% Analysis Date = 07/17/20 Pct Recovery = 98% Analysis Date = 07/13/20 Pct Recovery = 98% Analysis Date = 07/13/20 Pct Recovery = 98% Analysis Date = 07/09/20 Pct Recovery = 98% Analysis Date = 07/09/20 Pct Recovery = 98% Analysis Date = 07/04/20 Pct Recovery = 99% Analysis Date = 07/04/20 Pct Recovery = 99% Analysis Date = 06/30/20 Pct Recovery = 99% Analysis Date = 06/30/20 Pct Recovery = 99% Analysis Date = 06/26/20 Pct Recovery = 99% Analysis Date = 06/26/20 Pct Recovery = 99% Analysis Date = 06/22/20 Pct Recovery = 99% Analysis Date = 06/22/20 Pct Recovery = 99% Analysis Date = 06/17/20 Pct Recovery = 99% Analysis Date = 06/17/20 Pct Recovery = 99% Analysis Date = 06/13/20 Pct Recovery = 100% Analysis Date = 06/13/20 Pct Recovery = 100% Analysis Date = 06/09/20 Pct Recovery = 100% Analysis Date = 06/09/20 Pct Recovery = 100% Analysis Date = 06/05/20 Pct Recovery = 100% Analysis Date = 06/05/20 Pct Recovery = 100% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/19/20 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHOATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 88% 27% 88% 21%
Total 44 88% 27% 88% 21%

Sample Statistics
DIMETHOATE

Characteristic N % % Basis
Plotted 44 98% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 1 2% 1 out of 45
Not Spiked 71 .  
False Positives 0 0% 0 out of 71

OBSP Determination:
DIURON
METHOD: 2447 , TESTIDCODE: 66598LCM60

Laboratory ID = 20203230021 Lab Value = 60.228 Expected Conc. = 63 Report level label = 5 Pct Recovery = 96% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 41.619 Expected Conc. = 63 Report level label = 5 Pct Recovery = 66% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 122.621 Expected Conc. = 62.1 Report level label = 5 Pct Recovery = 197% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 120.237 Expected Conc. = 62.1 Report level label = 5 Pct Recovery = 194% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221520237 Lab Value = 47.820 Expected Conc. = 50.56 Report level label = 5 Pct Recovery = 95% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20222150192 Lab Value = 31.899 Expected Conc. = 50 Report level label = 5 Pct Recovery = 64% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 29.625 Expected Conc. = 50 Report level label = 5 Pct Recovery = 59% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20220740064 Lab Value = 23.930 Expected Conc. = 31.5 Report level label = 5 Pct Recovery = 76% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20201550031 Lab Value = 33.740 Expected Conc. = 31.3 Report level label = 5 Pct Recovery = 108% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20203360042 Lab Value = 26.914 Expected Conc. = 31.05 Report level label = 5 Pct Recovery = 87% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 34.285 Expected Conc. = 31.05 Report level label = 5 Pct Recovery = 110% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 38.805 Expected Conc. = 31.05 Report level label = 5 Pct Recovery = 125% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 41.328 Expected Conc. = 31.05 Report level label = 5 Pct Recovery = 133% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 28.367 Expected Conc. = 24.84 Report level label = 5 Pct Recovery = 114% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 26.532 Expected Conc. = 24.84 Report level label = 5 Pct Recovery = 107% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20221660151 Lab Value = 13.345 Expected Conc. = 12.64 Report level label = 5 Pct Recovery = 106% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210270007 Lab Value = 12.286 Expected Conc. = 12.6 Report level label = 5 Pct Recovery = 98% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202330309 Lab Value = 10.992 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 88% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 8.501 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 68% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 11.485 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 92% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 12.768 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 102% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 12.690 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 101% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210970035 Lab Value = 11.078 Expected Conc. = 12.42 Report level label = 5 Pct Recovery = 89% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 12.193 Expected Conc. = 12.42 Report level label = 5 Pct Recovery = 98% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 12.588 Expected Conc. = 12.42 Report level label = 5 Pct Recovery = 101% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 13.096 Expected Conc. = 12.42 Report level label = 5 Pct Recovery = 105% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 08/15/22 Pct Recovery = 78% Analysis Date = 08/10/22 Pct Recovery = 78% Analysis Date = 08/10/22 Pct Recovery = 78% Analysis Date = 08/06/22 Pct Recovery = 78% Analysis Date = 08/06/22 Pct Recovery = 78% Analysis Date = 08/02/22 Pct Recovery = 78% Analysis Date = 08/02/22 Pct Recovery = 78% Analysis Date = 07/29/22 Pct Recovery = 78% Analysis Date = 07/29/22 Pct Recovery = 78% Analysis Date = 07/25/22 Pct Recovery = 78% Analysis Date = 07/25/22 Pct Recovery = 78% Analysis Date = 07/21/22 Pct Recovery = 78% Analysis Date = 07/21/22 Pct Recovery = 78% Analysis Date = 07/17/22 Pct Recovery = 79% Analysis Date = 07/17/22 Pct Recovery = 79% Analysis Date = 07/13/22 Pct Recovery = 79% Analysis Date = 07/13/22 Pct Recovery = 79% Analysis Date = 07/09/22 Pct Recovery = 79% Analysis Date = 07/09/22 Pct Recovery = 79% Analysis Date = 07/05/22 Pct Recovery = 79% Analysis Date = 07/05/22 Pct Recovery = 79% Analysis Date = 07/01/22 Pct Recovery = 79% Analysis Date = 07/01/22 Pct Recovery = 79% Analysis Date = 06/27/22 Pct Recovery = 79% Analysis Date = 06/27/22 Pct Recovery = 79% Analysis Date = 06/23/22 Pct Recovery = 79% Analysis Date = 06/23/22 Pct Recovery = 79% Analysis Date = 06/19/22 Pct Recovery = 79% Analysis Date = 06/19/22 Pct Recovery = 79% Analysis Date = 06/15/22 Pct Recovery = 79% Analysis Date = 06/15/22 Pct Recovery = 79% Analysis Date = 06/11/22 Pct Recovery = 80% Analysis Date = 06/11/22 Pct Recovery = 80% Analysis Date = 06/07/22 Pct Recovery = 80% Analysis Date = 06/07/22 Pct Recovery = 80% Analysis Date = 06/03/22 Pct Recovery = 80% Analysis Date = 06/03/22 Pct Recovery = 80% Analysis Date = 05/30/22 Pct Recovery = 80% Analysis Date = 05/30/22 Pct Recovery = 80% Analysis Date = 05/26/22 Pct Recovery = 80% Analysis Date = 05/26/22 Pct Recovery = 80% Analysis Date = 05/22/22 Pct Recovery = 80% Analysis Date = 05/22/22 Pct Recovery = 80% Analysis Date = 05/18/22 Pct Recovery = 80% Analysis Date = 05/18/22 Pct Recovery = 80% Analysis Date = 05/14/22 Pct Recovery = 80% Analysis Date = 05/14/22 Pct Recovery = 80% Analysis Date = 05/10/22 Pct Recovery = 80% Analysis Date = 05/10/22 Pct Recovery = 80% Analysis Date = 05/06/22 Pct Recovery = 80% Analysis Date = 05/06/22 Pct Recovery = 80% Analysis Date = 05/01/22 Pct Recovery = 80% Analysis Date = 05/01/22 Pct Recovery = 80% Analysis Date = 04/27/22 Pct Recovery = 81% Analysis Date = 04/27/22 Pct Recovery = 81% Analysis Date = 04/23/22 Pct Recovery = 81% Analysis Date = 04/23/22 Pct Recovery = 81% Analysis Date = 04/19/22 Pct Recovery = 81% Analysis Date = 04/19/22 Pct Recovery = 81% Analysis Date = 04/15/22 Pct Recovery = 81% Analysis Date = 04/15/22 Pct Recovery = 81% Analysis Date = 04/11/22 Pct Recovery = 81% Analysis Date = 04/11/22 Pct Recovery = 81% Analysis Date = 04/07/22 Pct Recovery = 81% Analysis Date = 04/07/22 Pct Recovery = 81% Analysis Date = 04/03/22 Pct Recovery = 81% Analysis Date = 04/03/22 Pct Recovery = 81% Analysis Date = 03/30/22 Pct Recovery = 81% Analysis Date = 03/30/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/22/22 Pct Recovery = 81% Analysis Date = 03/22/22 Pct Recovery = 81% Analysis Date = 03/18/22 Pct Recovery = 81% Analysis Date = 03/18/22 Pct Recovery = 81% Analysis Date = 03/14/22 Pct Recovery = 82% Analysis Date = 03/14/22 Pct Recovery = 82% Analysis Date = 03/10/22 Pct Recovery = 82% Analysis Date = 03/10/22 Pct Recovery = 82% Analysis Date = 03/06/22 Pct Recovery = 82% Analysis Date = 03/06/22 Pct Recovery = 82% Analysis Date = 03/02/22 Pct Recovery = 82% Analysis Date = 03/02/22 Pct Recovery = 82% Analysis Date = 02/26/22 Pct Recovery = 82% Analysis Date = 02/26/22 Pct Recovery = 82% Analysis Date = 02/22/22 Pct Recovery = 82% Analysis Date = 02/22/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 01/29/22 Pct Recovery = 82% Analysis Date = 01/29/22 Pct Recovery = 82% Analysis Date = 01/25/22 Pct Recovery = 83% Analysis Date = 01/25/22 Pct Recovery = 83% Analysis Date = 01/20/22 Pct Recovery = 83% Analysis Date = 01/20/22 Pct Recovery = 83% Analysis Date = 01/16/22 Pct Recovery = 83% Analysis Date = 01/16/22 Pct Recovery = 83% Analysis Date = 01/12/22 Pct Recovery = 83% Analysis Date = 01/12/22 Pct Recovery = 83% Analysis Date = 01/08/22 Pct Recovery = 83% Analysis Date = 01/08/22 Pct Recovery = 83% Analysis Date = 01/04/22 Pct Recovery = 83% Analysis Date = 01/04/22 Pct Recovery = 83% Analysis Date = 12/31/21 Pct Recovery = 83% Analysis Date = 12/31/21 Pct Recovery = 83% Analysis Date = 12/27/21 Pct Recovery = 83% Analysis Date = 12/27/21 Pct Recovery = 83% Analysis Date = 12/23/21 Pct Recovery = 83% Analysis Date = 12/23/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 83% Analysis Date = 12/15/21 Pct Recovery = 83% Analysis Date = 12/15/21 Pct Recovery = 83% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/07/21 Pct Recovery = 84% Analysis Date = 12/07/21 Pct Recovery = 84% Analysis Date = 12/03/21 Pct Recovery = 84% Analysis Date = 12/03/21 Pct Recovery = 84% Analysis Date = 11/29/21 Pct Recovery = 84% Analysis Date = 11/29/21 Pct Recovery = 84% Analysis Date = 11/25/21 Pct Recovery = 84% Analysis Date = 11/25/21 Pct Recovery = 84% Analysis Date = 11/21/21 Pct Recovery = 84% Analysis Date = 11/21/21 Pct Recovery = 84% Analysis Date = 11/17/21 Pct Recovery = 84% Analysis Date = 11/17/21 Pct Recovery = 84% Analysis Date = 11/13/21 Pct Recovery = 84% Analysis Date = 11/13/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 84% Analysis Date = 10/28/21 Pct Recovery = 84% Analysis Date = 10/28/21 Pct Recovery = 84% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 85% Analysis Date = 10/11/21 Pct Recovery = 85% Analysis Date = 10/11/21 Pct Recovery = 85% Analysis Date = 10/07/21 Pct Recovery = 85% Analysis Date = 10/07/21 Pct Recovery = 85% Analysis Date = 10/03/21 Pct Recovery = 85% Analysis Date = 10/03/21 Pct Recovery = 85% Analysis Date = 09/29/21 Pct Recovery = 85% Analysis Date = 09/29/21 Pct Recovery = 85% Analysis Date = 09/25/21 Pct Recovery = 85% Analysis Date = 09/25/21 Pct Recovery = 85% Analysis Date = 09/21/21 Pct Recovery = 85% Analysis Date = 09/21/21 Pct Recovery = 85% Analysis Date = 09/17/21 Pct Recovery = 85% Analysis Date = 09/17/21 Pct Recovery = 85% Analysis Date = 09/13/21 Pct Recovery = 85% Analysis Date = 09/13/21 Pct Recovery = 85% Analysis Date = 09/09/21 Pct Recovery = 85% Analysis Date = 09/09/21 Pct Recovery = 85% Analysis Date = 09/05/21 Pct Recovery = 86% Analysis Date = 09/05/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/16/21 Pct Recovery = 86% Analysis Date = 08/16/21 Pct Recovery = 86% Analysis Date = 08/12/21 Pct Recovery = 86% Analysis Date = 08/12/21 Pct Recovery = 86% Analysis Date = 08/08/21 Pct Recovery = 86% Analysis Date = 08/08/21 Pct Recovery = 86% Analysis Date = 08/04/21 Pct Recovery = 86% Analysis Date = 08/04/21 Pct Recovery = 86% Analysis Date = 07/31/21 Pct Recovery = 86% Analysis Date = 07/31/21 Pct Recovery = 86% Analysis Date = 07/27/21 Pct Recovery = 86% Analysis Date = 07/27/21 Pct Recovery = 86% Analysis Date = 07/23/21 Pct Recovery = 87% Analysis Date = 07/23/21 Pct Recovery = 87% Analysis Date = 07/19/21 Pct Recovery = 87% Analysis Date = 07/19/21 Pct Recovery = 87% Analysis Date = 07/15/21 Pct Recovery = 87% Analysis Date = 07/15/21 Pct Recovery = 87% Analysis Date = 07/11/21 Pct Recovery = 87% Analysis Date = 07/11/21 Pct Recovery = 87% Analysis Date = 07/07/21 Pct Recovery = 87% Analysis Date = 07/07/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/16/21 Pct Recovery = 87% Analysis Date = 06/16/21 Pct Recovery = 87% Analysis Date = 06/12/21 Pct Recovery = 87% Analysis Date = 06/12/21 Pct Recovery = 87% Analysis Date = 06/08/21 Pct Recovery = 87% Analysis Date = 06/08/21 Pct Recovery = 87% Analysis Date = 06/04/21 Pct Recovery = 88% Analysis Date = 06/04/21 Pct Recovery = 88% Analysis Date = 05/31/21 Pct Recovery = 88% Analysis Date = 05/31/21 Pct Recovery = 88% Analysis Date = 05/27/21 Pct Recovery = 88% Analysis Date = 05/27/21 Pct Recovery = 88% Analysis Date = 05/23/21 Pct Recovery = 88% Analysis Date = 05/23/21 Pct Recovery = 88% Analysis Date = 05/19/21 Pct Recovery = 88% Analysis Date = 05/19/21 Pct Recovery = 88% Analysis Date = 05/15/21 Pct Recovery = 88% Analysis Date = 05/15/21 Pct Recovery = 88% Analysis Date = 05/11/21 Pct Recovery = 88% Analysis Date = 05/11/21 Pct Recovery = 88% Analysis Date = 05/07/21 Pct Recovery = 88% Analysis Date = 05/07/21 Pct Recovery = 88% Analysis Date = 05/03/21 Pct Recovery = 88% Analysis Date = 05/03/21 Pct Recovery = 88% Analysis Date = 04/29/21 Pct Recovery = 88% Analysis Date = 04/29/21 Pct Recovery = 88% Analysis Date = 04/25/21 Pct Recovery = 88% Analysis Date = 04/25/21 Pct Recovery = 88% Analysis Date = 04/21/21 Pct Recovery = 89% Analysis Date = 04/21/21 Pct Recovery = 89% Analysis Date = 04/17/21 Pct Recovery = 89% Analysis Date = 04/17/21 Pct Recovery = 89% Analysis Date = 04/13/21 Pct Recovery = 89% Analysis Date = 04/13/21 Pct Recovery = 89% Analysis Date = 04/09/21 Pct Recovery = 89% Analysis Date = 04/09/21 Pct Recovery = 89% Analysis Date = 04/05/21 Pct Recovery = 89% Analysis Date = 04/05/21 Pct Recovery = 89% Analysis Date = 04/01/21 Pct Recovery = 89% Analysis Date = 04/01/21 Pct Recovery = 89% Analysis Date = 03/28/21 Pct Recovery = 89% Analysis Date = 03/28/21 Pct Recovery = 89% Analysis Date = 03/23/21 Pct Recovery = 89% Analysis Date = 03/23/21 Pct Recovery = 89% Analysis Date = 03/19/21 Pct Recovery = 89% Analysis Date = 03/19/21 Pct Recovery = 89% Analysis Date = 03/15/21 Pct Recovery = 89% Analysis Date = 03/15/21 Pct Recovery = 89% Analysis Date = 03/11/21 Pct Recovery = 89% Analysis Date = 03/11/21 Pct Recovery = 89% Analysis Date = 03/07/21 Pct Recovery = 89% Analysis Date = 03/07/21 Pct Recovery = 89% Analysis Date = 03/03/21 Pct Recovery = 90% Analysis Date = 03/03/21 Pct Recovery = 90% Analysis Date = 02/27/21 Pct Recovery = 90% Analysis Date = 02/27/21 Pct Recovery = 90% Analysis Date = 02/23/21 Pct Recovery = 90% Analysis Date = 02/23/21 Pct Recovery = 90% Analysis Date = 02/19/21 Pct Recovery = 90% Analysis Date = 02/19/21 Pct Recovery = 90% Analysis Date = 02/15/21 Pct Recovery = 90% Analysis Date = 02/15/21 Pct Recovery = 90% Analysis Date = 02/11/21 Pct Recovery = 90% Analysis Date = 02/11/21 Pct Recovery = 90% Analysis Date = 02/07/21 Pct Recovery = 91% Analysis Date = 02/07/21 Pct Recovery = 91% Analysis Date = 02/03/21 Pct Recovery = 92% Analysis Date = 02/03/21 Pct Recovery = 92% Analysis Date = 01/30/21 Pct Recovery = 93% Analysis Date = 01/30/21 Pct Recovery = 93% Analysis Date = 01/26/21 Pct Recovery = 94% Analysis Date = 01/26/21 Pct Recovery = 94% Analysis Date = 01/22/21 Pct Recovery = 95% Analysis Date = 01/22/21 Pct Recovery = 95% Analysis Date = 01/18/21 Pct Recovery = 96% Analysis Date = 01/18/21 Pct Recovery = 96% Analysis Date = 01/14/21 Pct Recovery = 97% Analysis Date = 01/14/21 Pct Recovery = 97% Analysis Date = 01/10/21 Pct Recovery = 98% Analysis Date = 01/10/21 Pct Recovery = 98% Analysis Date = 01/06/21 Pct Recovery = 99% Analysis Date = 01/06/21 Pct Recovery = 99% Analysis Date = 01/02/21 Pct Recovery = 101% Analysis Date = 01/02/21 Pct Recovery = 101% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 102% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/21/20 Pct Recovery = 104% Analysis Date = 12/21/20 Pct Recovery = 104% Analysis Date = 12/17/20 Pct Recovery = 105% Analysis Date = 12/17/20 Pct Recovery = 105% Analysis Date = 12/12/20 Pct Recovery = 107% Analysis Date = 12/12/20 Pct Recovery = 107% Analysis Date = 12/08/20 Pct Recovery = 108% Analysis Date = 12/08/20 Pct Recovery = 108% Analysis Date = 12/04/20 Pct Recovery = 109% Analysis Date = 12/04/20 Pct Recovery = 109% Analysis Date = 11/30/20 Pct Recovery = 111% Analysis Date = 11/30/20 Pct Recovery = 111% Analysis Date = 11/26/20 Pct Recovery = 112% Analysis Date = 11/26/20 Pct Recovery = 112% Analysis Date = 11/22/20 Pct Recovery = 114% Analysis Date = 11/22/20 Pct Recovery = 114% Analysis Date = 11/18/20 Pct Recovery = 115% Analysis Date = 11/18/20 Pct Recovery = 115% Analysis Date = 11/14/20 Pct Recovery = 116% Analysis Date = 11/14/20 Pct Recovery = 116% Analysis Date = 11/10/20 Pct Recovery = 118% Analysis Date = 11/10/20 Pct Recovery = 118% Analysis Date = 11/06/20 Pct Recovery = 119% Analysis Date = 11/06/20 Pct Recovery = 119% Analysis Date = 11/02/20 Pct Recovery = 120% Analysis Date = 11/02/20 Pct Recovery = 120% Analysis Date = 10/29/20 Pct Recovery = 121% Analysis Date = 10/29/20 Pct Recovery = 121% Analysis Date = 10/25/20 Pct Recovery = 121% Analysis Date = 10/25/20 Pct Recovery = 121% Analysis Date = 10/21/20 Pct Recovery = 122% Analysis Date = 10/21/20 Pct Recovery = 122% Analysis Date = 10/17/20 Pct Recovery = 122% Analysis Date = 10/17/20 Pct Recovery = 122% Analysis Date = 10/13/20 Pct Recovery = 123% Analysis Date = 10/13/20 Pct Recovery = 123% Analysis Date = 10/09/20 Pct Recovery = 123% Analysis Date = 10/09/20 Pct Recovery = 123% Analysis Date = 10/05/20 Pct Recovery = 124% Analysis Date = 10/05/20 Pct Recovery = 124% Analysis Date = 10/01/20 Pct Recovery = 124% Analysis Date = 10/01/20 Pct Recovery = 124% Analysis Date = 09/27/20 Pct Recovery = 125% Analysis Date = 09/27/20 Pct Recovery = 125% Analysis Date = 09/23/20 Pct Recovery = 125% Analysis Date = 09/23/20 Pct Recovery = 125% Analysis Date = 09/19/20 Pct Recovery = 126% Analysis Date = 09/19/20 Pct Recovery = 126% Analysis Date = 09/15/20 Pct Recovery = 126% Analysis Date = 09/15/20 Pct Recovery = 126% Analysis Date = 09/11/20 Pct Recovery = 127% Analysis Date = 09/11/20 Pct Recovery = 127% Analysis Date = 09/07/20 Pct Recovery = 127% Analysis Date = 09/07/20 Pct Recovery = 127% Analysis Date = 09/02/20 Pct Recovery = 127% Analysis Date = 09/02/20 Pct Recovery = 127% Analysis Date = 08/29/20 Pct Recovery = 126% Analysis Date = 08/29/20 Pct Recovery = 126% Analysis Date = 08/25/20 Pct Recovery = 124% Analysis Date = 08/25/20 Pct Recovery = 124% Analysis Date = 08/21/20 Pct Recovery = 123% Analysis Date = 08/21/20 Pct Recovery = 123% Analysis Date = 08/17/20 Pct Recovery = 122% Analysis Date = 08/17/20 Pct Recovery = 122% Analysis Date = 08/13/20 Pct Recovery = 120% Analysis Date = 08/13/20 Pct Recovery = 120% Analysis Date = 08/09/20 Pct Recovery = 119% Analysis Date = 08/09/20 Pct Recovery = 119% Analysis Date = 08/05/20 Pct Recovery = 117% Analysis Date = 08/05/20 Pct Recovery = 117% Analysis Date = 08/01/20 Pct Recovery = 116% Analysis Date = 08/01/20 Pct Recovery = 116% Analysis Date = 07/28/20 Pct Recovery = 115% Analysis Date = 07/28/20 Pct Recovery = 115% Analysis Date = 07/24/20 Pct Recovery = 113% Analysis Date = 07/24/20 Pct Recovery = 113% Analysis Date = 07/20/20 Pct Recovery = 112% Analysis Date = 07/20/20 Pct Recovery = 112% Analysis Date = 07/16/20 Pct Recovery = 110% Analysis Date = 07/16/20 Pct Recovery = 110% Analysis Date = 07/12/20 Pct Recovery = 109% Analysis Date = 07/12/20 Pct Recovery = 109% Analysis Date = 07/08/20 Pct Recovery = 107% Analysis Date = 07/08/20 Pct Recovery = 107% Analysis Date = 07/04/20 Pct Recovery = 106% Analysis Date = 07/04/20 Pct Recovery = 106% Analysis Date = 06/30/20 Pct Recovery = 105% Analysis Date = 06/30/20 Pct Recovery = 105% Analysis Date = 06/26/20 Pct Recovery = 103% Analysis Date = 06/26/20 Pct Recovery = 103% Analysis Date = 06/22/20 Pct Recovery = 102% Analysis Date = 06/22/20 Pct Recovery = 102% Analysis Date = 06/18/20 Pct Recovery = 100% Analysis Date = 06/18/20 Pct Recovery = 100% Analysis Date = 06/14/20 Pct Recovery = 99% Analysis Date = 06/14/20 Pct Recovery = 99% Analysis Date = 06/10/20 Pct Recovery = 98% Analysis Date = 06/10/20 Pct Recovery = 98% Analysis Date = 06/06/20 Pct Recovery = 96% Analysis Date = 06/06/20 Pct Recovery = 96% Analysis Date = 06/02/20 Pct Recovery = 95% Analysis Date = 06/02/20 Pct Recovery = 95% Analysis Date = 05/29/20 Pct Recovery = 94% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 26 103% 33% 100% 15%
Total 26 103% 33% 100% 15%

Sample Statistics
DIURON

Characteristic N % % Basis
Plotted 26 84% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 3 10% Spiked
Spiked 31 .  
False Negatives 2 6% 2 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
ETHOPROPHOS
METHOD: 2447 , TESTIDCODE: 68596LCM60

Laboratory ID = 20213200091 Lab Value = 65.770 Expected Conc. = 31.45 Report level label = 5 Pct Recovery = 209% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202110006 Lab Value = 65.395 Expected Conc. = 63.4 Report level label = 5 Pct Recovery = 103% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20210760015 Lab Value = 66.818 Expected Conc. = 63.15 Report level label = 5 Pct Recovery = 106% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 52.193 Expected Conc. = 63.15 Report level label = 5 Pct Recovery = 83% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 43.989 Expected Conc. = 63.15 Report level label = 5 Pct Recovery = 70% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 64.874 Expected Conc. = 63.15 Report level label = 5 Pct Recovery = 103% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201820155 Lab Value = 64.659 Expected Conc. = 63.1 Report level label = 5 Pct Recovery = 102% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 49.656 Expected Conc. = 62.3 Report level label = 5 Pct Recovery = 80% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 63.538 Expected Conc. = 62.3 Report level label = 5 Pct Recovery = 102% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 61.930 Expected Conc. = 62.3 Report level label = 5 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20212990174 Lab Value = 34.194 Expected Conc. = 50.32 Report level label = 5 Pct Recovery = 68% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 37.029 Expected Conc. = 50.08 Report level label = 5 Pct Recovery = 74% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 32.180 Expected Conc. = 50.08 Report level label = 5 Pct Recovery = 64% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 26.832 Expected Conc. = 50 Report level label = 5 Pct Recovery = 54% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20222150193 Lab Value = 33.761 Expected Conc. = 49.6 Report level label = 5 Pct Recovery = 68% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220810134 Lab Value = 42.609 Expected Conc. = 49.2 Report level label = 5 Pct Recovery = 87% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20201680155 Lab Value = 35.112 Expected Conc. = 31.7 Report level label = 5 Pct Recovery = 111% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20210480001 Lab Value = 25.036 Expected Conc. = 31.575 Report level label = 5 Pct Recovery = 79% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202530029 Lab Value = 27.905 Expected Conc. = 31.55 Report level label = 5 Pct Recovery = 88% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 29.390 Expected Conc. = 31.55 Report level label = 5 Pct Recovery = 93% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 32.810 Expected Conc. = 31.55 Report level label = 5 Pct Recovery = 104% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20213340027 Lab Value = 22.688 Expected Conc. = 31.45 Report level label = 5 Pct Recovery = 72% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 23.301 Expected Conc. = 31.45 Report level label = 5 Pct Recovery = 74% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 21.116 Expected Conc. = 31.3 Report level label = 5 Pct Recovery = 67% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 24.676 Expected Conc. = 31.3 Report level label = 5 Pct Recovery = 79% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202880004 Lab Value = 33.332 Expected Conc. = 31.15 Report level label = 5 Pct Recovery = 107% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20220810133 Lab Value = 29.147 Expected Conc. = 30.75 Report level label = 5 Pct Recovery = 95% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20210900005 Lab Value = 30.526 Expected Conc. = 25.26 Report level label = 5 Pct Recovery = 121% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 26.836 Expected Conc. = 24.92 Report level label = 5 Pct Recovery = 108% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 27.927 Expected Conc. = 24.92 Report level label = 5 Pct Recovery = 112% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 13.330 Expected Conc. = 12.68 Report level label = 5 Pct Recovery = 105% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210690067 Lab Value = 14.835 Expected Conc. = 12.63 Report level label = 5 Pct Recovery = 117% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202330309 Lab Value = 16.402 Expected Conc. = 12.62 Report level label = 5 Pct Recovery = 130% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 16.004 Expected Conc. = 12.62 Report level label = 5 Pct Recovery = 127% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 14.366 Expected Conc. = 12.62 Report level label = 5 Pct Recovery = 114% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 13.422 Expected Conc. = 12.62 Report level label = 5 Pct Recovery = 106% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20213060210 Lab Value = 9.180 Expected Conc. = 12.58 Report level label = 5 Pct Recovery = 73% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222500483 Lab Value = 8.466 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 68% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 9.948 Expected Conc. = 12.52 Report level label = 5 Pct Recovery = 79% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210120050 Lab Value = 11.000 Expected Conc. = 12.46 Report level label = 5 Pct Recovery = 88% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 14.803 Expected Conc. = 12.46 Report level label = 5 Pct Recovery = 119% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 12.122 Expected Conc. = 12.46 Report level label = 5 Pct Recovery = 97% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 11.596 Expected Conc. = 12.46 Report level label = 5 Pct Recovery = 93% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222630205 Lab Value = 9.153 Expected Conc. = 12.3 Report level label = 5 Pct Recovery = 74% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Analysis Date = 09/28/22 Pct Recovery = 64% Analysis Date = 09/24/22 Pct Recovery = 65% Analysis Date = 09/24/22 Pct Recovery = 65% Analysis Date = 09/20/22 Pct Recovery = 65% Analysis Date = 09/20/22 Pct Recovery = 65% Analysis Date = 09/16/22 Pct Recovery = 65% Analysis Date = 09/16/22 Pct Recovery = 65% Analysis Date = 09/11/22 Pct Recovery = 66% Analysis Date = 09/11/22 Pct Recovery = 66% Analysis Date = 09/07/22 Pct Recovery = 66% Analysis Date = 09/07/22 Pct Recovery = 66% Analysis Date = 09/03/22 Pct Recovery = 67% Analysis Date = 09/03/22 Pct Recovery = 67% Analysis Date = 08/29/22 Pct Recovery = 67% Analysis Date = 08/29/22 Pct Recovery = 67% Analysis Date = 08/25/22 Pct Recovery = 67% Analysis Date = 08/25/22 Pct Recovery = 67% Analysis Date = 08/21/22 Pct Recovery = 68% Analysis Date = 08/21/22 Pct Recovery = 68% Analysis Date = 08/16/22 Pct Recovery = 68% Analysis Date = 08/16/22 Pct Recovery = 68% Analysis Date = 08/12/22 Pct Recovery = 68% Analysis Date = 08/12/22 Pct Recovery = 68% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/03/22 Pct Recovery = 69% Analysis Date = 08/03/22 Pct Recovery = 69% Analysis Date = 07/30/22 Pct Recovery = 70% Analysis Date = 07/30/22 Pct Recovery = 70% Analysis Date = 07/26/22 Pct Recovery = 70% Analysis Date = 07/26/22 Pct Recovery = 70% Analysis Date = 07/21/22 Pct Recovery = 70% Analysis Date = 07/21/22 Pct Recovery = 70% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/04/22 Pct Recovery = 72% Analysis Date = 07/04/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/21/22 Pct Recovery = 73% Analysis Date = 06/21/22 Pct Recovery = 73% Analysis Date = 06/17/22 Pct Recovery = 73% Analysis Date = 06/17/22 Pct Recovery = 73% Analysis Date = 06/13/22 Pct Recovery = 74% Analysis Date = 06/13/22 Pct Recovery = 74% Analysis Date = 06/08/22 Pct Recovery = 74% Analysis Date = 06/08/22 Pct Recovery = 74% Analysis Date = 06/04/22 Pct Recovery = 74% Analysis Date = 06/04/22 Pct Recovery = 74% Analysis Date = 05/31/22 Pct Recovery = 75% Analysis Date = 05/31/22 Pct Recovery = 75% Analysis Date = 05/26/22 Pct Recovery = 75% Analysis Date = 05/26/22 Pct Recovery = 75% Analysis Date = 05/22/22 Pct Recovery = 75% Analysis Date = 05/22/22 Pct Recovery = 75% Analysis Date = 05/18/22 Pct Recovery = 76% Analysis Date = 05/18/22 Pct Recovery = 76% Analysis Date = 05/13/22 Pct Recovery = 76% Analysis Date = 05/13/22 Pct Recovery = 76% Analysis Date = 05/09/22 Pct Recovery = 77% Analysis Date = 05/09/22 Pct Recovery = 77% Analysis Date = 05/05/22 Pct Recovery = 77% Analysis Date = 05/05/22 Pct Recovery = 77% Analysis Date = 04/30/22 Pct Recovery = 77% Analysis Date = 04/30/22 Pct Recovery = 77% Analysis Date = 04/26/22 Pct Recovery = 78% Analysis Date = 04/26/22 Pct Recovery = 78% Analysis Date = 04/22/22 Pct Recovery = 78% Analysis Date = 04/22/22 Pct Recovery = 78% Analysis Date = 04/18/22 Pct Recovery = 78% Analysis Date = 04/18/22 Pct Recovery = 78% Analysis Date = 04/13/22 Pct Recovery = 79% Analysis Date = 04/13/22 Pct Recovery = 79% Analysis Date = 04/09/22 Pct Recovery = 79% Analysis Date = 04/09/22 Pct Recovery = 79% Analysis Date = 04/05/22 Pct Recovery = 79% Analysis Date = 04/05/22 Pct Recovery = 79% Analysis Date = 03/31/22 Pct Recovery = 80% Analysis Date = 03/31/22 Pct Recovery = 80% Analysis Date = 03/27/22 Pct Recovery = 80% Analysis Date = 03/27/22 Pct Recovery = 80% Analysis Date = 03/23/22 Pct Recovery = 81% Analysis Date = 03/23/22 Pct Recovery = 81% Analysis Date = 03/18/22 Pct Recovery = 81% Analysis Date = 03/18/22 Pct Recovery = 81% Analysis Date = 03/14/22 Pct Recovery = 81% Analysis Date = 03/14/22 Pct Recovery = 81% Analysis Date = 03/10/22 Pct Recovery = 82% Analysis Date = 03/10/22 Pct Recovery = 82% Analysis Date = 03/05/22 Pct Recovery = 82% Analysis Date = 03/05/22 Pct Recovery = 82% Analysis Date = 03/01/22 Pct Recovery = 82% Analysis Date = 03/01/22 Pct Recovery = 82% Analysis Date = 02/25/22 Pct Recovery = 83% Analysis Date = 02/25/22 Pct Recovery = 83% Analysis Date = 02/20/22 Pct Recovery = 83% Analysis Date = 02/20/22 Pct Recovery = 83% Analysis Date = 02/16/22 Pct Recovery = 84% Analysis Date = 02/16/22 Pct Recovery = 84% Analysis Date = 02/12/22 Pct Recovery = 84% Analysis Date = 02/12/22 Pct Recovery = 84% Analysis Date = 02/07/22 Pct Recovery = 84% Analysis Date = 02/07/22 Pct Recovery = 84% Analysis Date = 02/03/22 Pct Recovery = 85% Analysis Date = 02/03/22 Pct Recovery = 85% Analysis Date = 01/30/22 Pct Recovery = 85% Analysis Date = 01/30/22 Pct Recovery = 85% Analysis Date = 01/26/22 Pct Recovery = 86% Analysis Date = 01/26/22 Pct Recovery = 86% Analysis Date = 01/21/22 Pct Recovery = 86% Analysis Date = 01/21/22 Pct Recovery = 86% Analysis Date = 01/17/22 Pct Recovery = 86% Analysis Date = 01/17/22 Pct Recovery = 86% Analysis Date = 01/13/22 Pct Recovery = 87% Analysis Date = 01/13/22 Pct Recovery = 87% Analysis Date = 01/08/22 Pct Recovery = 87% Analysis Date = 01/08/22 Pct Recovery = 87% Analysis Date = 01/04/22 Pct Recovery = 88% Analysis Date = 01/04/22 Pct Recovery = 88% Analysis Date = 12/31/21 Pct Recovery = 88% Analysis Date = 12/31/21 Pct Recovery = 88% Analysis Date = 12/26/21 Pct Recovery = 88% Analysis Date = 12/26/21 Pct Recovery = 88% Analysis Date = 12/22/21 Pct Recovery = 89% Analysis Date = 12/22/21 Pct Recovery = 89% Analysis Date = 12/18/21 Pct Recovery = 89% Analysis Date = 12/18/21 Pct Recovery = 89% Analysis Date = 12/13/21 Pct Recovery = 90% Analysis Date = 12/13/21 Pct Recovery = 90% Analysis Date = 12/09/21 Pct Recovery = 90% Analysis Date = 12/09/21 Pct Recovery = 90% Analysis Date = 12/05/21 Pct Recovery = 90% Analysis Date = 12/05/21 Pct Recovery = 90% Analysis Date = 11/30/21 Pct Recovery = 90% Analysis Date = 11/30/21 Pct Recovery = 90% Analysis Date = 11/26/21 Pct Recovery = 91% Analysis Date = 11/26/21 Pct Recovery = 91% Analysis Date = 11/22/21 Pct Recovery = 91% Analysis Date = 11/22/21 Pct Recovery = 91% Analysis Date = 11/18/21 Pct Recovery = 91% Analysis Date = 11/18/21 Pct Recovery = 91% Analysis Date = 11/13/21 Pct Recovery = 91% Analysis Date = 11/13/21 Pct Recovery = 91% Analysis Date = 11/09/21 Pct Recovery = 92% Analysis Date = 11/09/21 Pct Recovery = 92% Analysis Date = 11/05/21 Pct Recovery = 92% Analysis Date = 11/05/21 Pct Recovery = 92% Analysis Date = 10/31/21 Pct Recovery = 92% Analysis Date = 10/31/21 Pct Recovery = 92% Analysis Date = 10/27/21 Pct Recovery = 92% Analysis Date = 10/27/21 Pct Recovery = 92% Analysis Date = 10/23/21 Pct Recovery = 92% Analysis Date = 10/23/21 Pct Recovery = 92% Analysis Date = 10/18/21 Pct Recovery = 93% Analysis Date = 10/18/21 Pct Recovery = 93% Analysis Date = 10/14/21 Pct Recovery = 93% Analysis Date = 10/14/21 Pct Recovery = 93% Analysis Date = 10/10/21 Pct Recovery = 93% Analysis Date = 10/10/21 Pct Recovery = 93% Analysis Date = 10/05/21 Pct Recovery = 93% Analysis Date = 10/05/21 Pct Recovery = 93% Analysis Date = 10/01/21 Pct Recovery = 94% Analysis Date = 10/01/21 Pct Recovery = 94% Analysis Date = 09/27/21 Pct Recovery = 94% Analysis Date = 09/27/21 Pct Recovery = 94% Analysis Date = 09/22/21 Pct Recovery = 94% Analysis Date = 09/22/21 Pct Recovery = 94% Analysis Date = 09/18/21 Pct Recovery = 94% Analysis Date = 09/18/21 Pct Recovery = 94% Analysis Date = 09/14/21 Pct Recovery = 94% Analysis Date = 09/14/21 Pct Recovery = 94% Analysis Date = 09/09/21 Pct Recovery = 95% Analysis Date = 09/09/21 Pct Recovery = 95% Analysis Date = 09/05/21 Pct Recovery = 95% Analysis Date = 09/05/21 Pct Recovery = 95% Analysis Date = 09/01/21 Pct Recovery = 95% Analysis Date = 09/01/21 Pct Recovery = 95% Analysis Date = 08/28/21 Pct Recovery = 95% Analysis Date = 08/28/21 Pct Recovery = 95% Analysis Date = 08/23/21 Pct Recovery = 96% Analysis Date = 08/23/21 Pct Recovery = 96% Analysis Date = 08/19/21 Pct Recovery = 96% Analysis Date = 08/19/21 Pct Recovery = 96% Analysis Date = 08/15/21 Pct Recovery = 96% Analysis Date = 08/15/21 Pct Recovery = 96% Analysis Date = 08/10/21 Pct Recovery = 96% Analysis Date = 08/10/21 Pct Recovery = 96% Analysis Date = 08/06/21 Pct Recovery = 96% Analysis Date = 08/06/21 Pct Recovery = 96% Analysis Date = 08/02/21 Pct Recovery = 97% Analysis Date = 08/02/21 Pct Recovery = 97% Analysis Date = 07/28/21 Pct Recovery = 97% Analysis Date = 07/28/21 Pct Recovery = 97% Analysis Date = 07/24/21 Pct Recovery = 97% Analysis Date = 07/24/21 Pct Recovery = 97% Analysis Date = 07/20/21 Pct Recovery = 97% Analysis Date = 07/20/21 Pct Recovery = 97% Analysis Date = 07/15/21 Pct Recovery = 98% Analysis Date = 07/15/21 Pct Recovery = 98% Analysis Date = 07/11/21 Pct Recovery = 98% Analysis Date = 07/11/21 Pct Recovery = 98% Analysis Date = 07/07/21 Pct Recovery = 98% Analysis Date = 07/07/21 Pct Recovery = 98% Analysis Date = 07/02/21 Pct Recovery = 98% Analysis Date = 07/02/21 Pct Recovery = 98% Analysis Date = 06/28/21 Pct Recovery = 98% Analysis Date = 06/28/21 Pct Recovery = 98% Analysis Date = 06/24/21 Pct Recovery = 99% Analysis Date = 06/24/21 Pct Recovery = 99% Analysis Date = 06/19/21 Pct Recovery = 99% Analysis Date = 06/19/21 Pct Recovery = 99% Analysis Date = 06/15/21 Pct Recovery = 99% Analysis Date = 06/15/21 Pct Recovery = 99% Analysis Date = 06/11/21 Pct Recovery = 99% Analysis Date = 06/11/21 Pct Recovery = 99% Analysis Date = 06/07/21 Pct Recovery = 100% Analysis Date = 06/07/21 Pct Recovery = 100% Analysis Date = 06/02/21 Pct Recovery = 100% Analysis Date = 06/02/21 Pct Recovery = 100% Analysis Date = 05/29/21 Pct Recovery = 100% Analysis Date = 05/29/21 Pct Recovery = 100% Analysis Date = 05/25/21 Pct Recovery = 100% Analysis Date = 05/25/21 Pct Recovery = 100% Analysis Date = 05/20/21 Pct Recovery = 100% Analysis Date = 05/20/21 Pct Recovery = 100% Analysis Date = 05/16/21 Pct Recovery = 101% Analysis Date = 05/16/21 Pct Recovery = 101% Analysis Date = 05/12/21 Pct Recovery = 101% Analysis Date = 05/12/21 Pct Recovery = 101% Analysis Date = 05/07/21 Pct Recovery = 101% Analysis Date = 05/07/21 Pct Recovery = 101% Analysis Date = 05/03/21 Pct Recovery = 101% Analysis Date = 05/03/21 Pct Recovery = 101% Analysis Date = 04/29/21 Pct Recovery = 102% Analysis Date = 04/29/21 Pct Recovery = 102% Analysis Date = 04/24/21 Pct Recovery = 102% Analysis Date = 04/24/21 Pct Recovery = 102% Analysis Date = 04/20/21 Pct Recovery = 102% Analysis Date = 04/20/21 Pct Recovery = 102% Analysis Date = 04/16/21 Pct Recovery = 102% Analysis Date = 04/16/21 Pct Recovery = 102% Analysis Date = 04/11/21 Pct Recovery = 102% Analysis Date = 04/11/21 Pct Recovery = 102% Analysis Date = 04/07/21 Pct Recovery = 103% Analysis Date = 04/07/21 Pct Recovery = 103% Analysis Date = 04/03/21 Pct Recovery = 102% Analysis Date = 04/03/21 Pct Recovery = 102% Analysis Date = 03/29/21 Pct Recovery = 102% Analysis Date = 03/29/21 Pct Recovery = 102% Analysis Date = 03/25/21 Pct Recovery = 102% Analysis Date = 03/25/21 Pct Recovery = 102% Analysis Date = 03/21/21 Pct Recovery = 102% Analysis Date = 03/21/21 Pct Recovery = 102% Analysis Date = 03/17/21 Pct Recovery = 102% Analysis Date = 03/17/21 Pct Recovery = 102% Analysis Date = 03/12/21 Pct Recovery = 102% Analysis Date = 03/12/21 Pct Recovery = 102% Analysis Date = 03/08/21 Pct Recovery = 102% Analysis Date = 03/08/21 Pct Recovery = 102% Analysis Date = 03/04/21 Pct Recovery = 101% Analysis Date = 03/04/21 Pct Recovery = 101% Analysis Date = 02/27/21 Pct Recovery = 101% Analysis Date = 02/27/21 Pct Recovery = 101% Analysis Date = 02/23/21 Pct Recovery = 101% Analysis Date = 02/23/21 Pct Recovery = 101% Analysis Date = 02/19/21 Pct Recovery = 101% Analysis Date = 02/19/21 Pct Recovery = 101% Analysis Date = 02/14/21 Pct Recovery = 101% Analysis Date = 02/14/21 Pct Recovery = 101% Analysis Date = 02/10/21 Pct Recovery = 100% Analysis Date = 02/10/21 Pct Recovery = 100% Analysis Date = 02/06/21 Pct Recovery = 100% Analysis Date = 02/06/21 Pct Recovery = 100% Analysis Date = 02/01/21 Pct Recovery = 100% Analysis Date = 02/01/21 Pct Recovery = 100% Analysis Date = 01/28/21 Pct Recovery = 100% Analysis Date = 01/28/21 Pct Recovery = 100% Analysis Date = 01/24/21 Pct Recovery = 100% Analysis Date = 01/24/21 Pct Recovery = 100% Analysis Date = 01/19/21 Pct Recovery = 100% Analysis Date = 01/19/21 Pct Recovery = 100% Analysis Date = 01/15/21 Pct Recovery = 100% Analysis Date = 01/15/21 Pct Recovery = 100% Analysis Date = 01/11/21 Pct Recovery = 100% Analysis Date = 01/11/21 Pct Recovery = 100% Analysis Date = 01/07/21 Pct Recovery = 100% Analysis Date = 01/07/21 Pct Recovery = 100% Analysis Date = 01/02/21 Pct Recovery = 99% Analysis Date = 01/02/21 Pct Recovery = 99% Analysis Date = 12/29/20 Pct Recovery = 99% Analysis Date = 12/29/20 Pct Recovery = 99% Analysis Date = 12/25/20 Pct Recovery = 99% Analysis Date = 12/25/20 Pct Recovery = 99% Analysis Date = 12/20/20 Pct Recovery = 99% Analysis Date = 12/20/20 Pct Recovery = 99% Analysis Date = 12/16/20 Pct Recovery = 99% Analysis Date = 12/16/20 Pct Recovery = 99% Analysis Date = 12/12/20 Pct Recovery = 99% Analysis Date = 12/12/20 Pct Recovery = 99% Analysis Date = 12/07/20 Pct Recovery = 99% Analysis Date = 12/07/20 Pct Recovery = 99% Analysis Date = 12/03/20 Pct Recovery = 99% Analysis Date = 12/03/20 Pct Recovery = 99% Analysis Date = 11/29/20 Pct Recovery = 99% Analysis Date = 11/29/20 Pct Recovery = 99% Analysis Date = 11/24/20 Pct Recovery = 99% Analysis Date = 11/24/20 Pct Recovery = 99% Analysis Date = 11/20/20 Pct Recovery = 99% Analysis Date = 11/20/20 Pct Recovery = 99% Analysis Date = 11/16/20 Pct Recovery = 99% Analysis Date = 11/16/20 Pct Recovery = 99% Analysis Date = 11/11/20 Pct Recovery = 98% Analysis Date = 11/11/20 Pct Recovery = 98% Analysis Date = 11/07/20 Pct Recovery = 99% Analysis Date = 11/07/20 Pct Recovery = 99% Analysis Date = 11/03/20 Pct Recovery = 99% Analysis Date = 11/03/20 Pct Recovery = 99% Analysis Date = 10/29/20 Pct Recovery = 99% Analysis Date = 10/29/20 Pct Recovery = 99% Analysis Date = 10/25/20 Pct Recovery = 100% Analysis Date = 10/25/20 Pct Recovery = 100% Analysis Date = 10/21/20 Pct Recovery = 100% Analysis Date = 10/21/20 Pct Recovery = 100% Analysis Date = 10/17/20 Pct Recovery = 101% Analysis Date = 10/17/20 Pct Recovery = 101% Analysis Date = 10/12/20 Pct Recovery = 101% Analysis Date = 10/12/20 Pct Recovery = 101% Analysis Date = 10/08/20 Pct Recovery = 101% Analysis Date = 10/08/20 Pct Recovery = 101% Analysis Date = 10/04/20 Pct Recovery = 102% Analysis Date = 10/04/20 Pct Recovery = 102% Analysis Date = 09/29/20 Pct Recovery = 102% Analysis Date = 09/29/20 Pct Recovery = 102% Analysis Date = 09/25/20 Pct Recovery = 102% Analysis Date = 09/25/20 Pct Recovery = 102% Analysis Date = 09/21/20 Pct Recovery = 102% Analysis Date = 09/21/20 Pct Recovery = 102% Analysis Date = 09/16/20 Pct Recovery = 103% Analysis Date = 09/16/20 Pct Recovery = 103% Analysis Date = 09/12/20 Pct Recovery = 103% Analysis Date = 09/12/20 Pct Recovery = 103% Analysis Date = 09/08/20 Pct Recovery = 103% Analysis Date = 09/08/20 Pct Recovery = 103% Analysis Date = 09/03/20 Pct Recovery = 104% Analysis Date = 09/03/20 Pct Recovery = 104% Analysis Date = 08/30/20 Pct Recovery = 104% Analysis Date = 08/30/20 Pct Recovery = 104% Analysis Date = 08/26/20 Pct Recovery = 104% Analysis Date = 08/26/20 Pct Recovery = 104% Analysis Date = 08/21/20 Pct Recovery = 104% Analysis Date = 08/21/20 Pct Recovery = 104% Analysis Date = 08/17/20 Pct Recovery = 105% Analysis Date = 08/17/20 Pct Recovery = 105% Analysis Date = 08/13/20 Pct Recovery = 105% Analysis Date = 08/13/20 Pct Recovery = 105% Analysis Date = 08/08/20 Pct Recovery = 105% Analysis Date = 08/08/20 Pct Recovery = 105% Analysis Date = 08/04/20 Pct Recovery = 106% Analysis Date = 08/04/20 Pct Recovery = 106% Analysis Date = 07/31/20 Pct Recovery = 106% Analysis Date = 07/31/20 Pct Recovery = 106% Analysis Date = 07/27/20 Pct Recovery = 106% Analysis Date = 07/27/20 Pct Recovery = 106% Analysis Date = 07/22/20 Pct Recovery = 106% Analysis Date = 07/22/20 Pct Recovery = 106% Analysis Date = 07/18/20 Pct Recovery = 107% Analysis Date = 07/18/20 Pct Recovery = 107% Analysis Date = 07/14/20 Pct Recovery = 107% Analysis Date = 07/14/20 Pct Recovery = 107% Analysis Date = 07/09/20 Pct Recovery = 107% Analysis Date = 07/09/20 Pct Recovery = 107% Analysis Date = 07/05/20 Pct Recovery = 108% Analysis Date = 07/05/20 Pct Recovery = 108% Analysis Date = 07/01/20 Pct Recovery = 108% Analysis Date = 07/01/20 Pct Recovery = 108% Analysis Date = 06/26/20 Pct Recovery = 108% Analysis Date = 06/26/20 Pct Recovery = 108% Analysis Date = 06/22/20 Pct Recovery = 108% Analysis Date = 06/22/20 Pct Recovery = 108% Analysis Date = 06/18/20 Pct Recovery = 109% Analysis Date = 06/18/20 Pct Recovery = 109% Analysis Date = 06/13/20 Pct Recovery = 109% Analysis Date = 06/13/20 Pct Recovery = 109% Analysis Date = 06/09/20 Pct Recovery = 109% Analysis Date = 06/09/20 Pct Recovery = 109% Analysis Date = 06/05/20 Pct Recovery = 110% Analysis Date = 06/05/20 Pct Recovery = 110% Analysis Date = 05/31/20 Pct Recovery = 110% Analysis Date = 05/31/20 Pct Recovery = 110% Analysis Date = 05/27/20 Pct Recovery = 110% Analysis Date = 05/27/20 Pct Recovery = 110% Analysis Date = 05/23/20 Pct Recovery = 110% Analysis Date = 05/23/20 Pct Recovery = 110% Analysis Date = 05/19/20 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHOPROPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 95% 26% 94% 24%
Total 44 95% 26% 94% 24%

Sample Statistics
ETHOPROPHOS

Characteristic N % % Basis
Plotted 44 98% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 1 2% 1 out of 45
Not Spiked 69 .  
False Positives 3 4% 3 out of 69

OBSP Determination:
ETOXAZOLE
METHOD: 2447 , TESTIDCODE: 68598LCM60

Laboratory ID = 20210760015 Lab Value = 29.474 Expected Conc. = 52.55 Report level label = 4.2 Pct Recovery = 56% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 27.753 Expected Conc. = 52.55 Report level label = 4.2 Pct Recovery = 53% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 27.522 Expected Conc. = 52.55 Report level label = 4.2 Pct Recovery = 52% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 40.599 Expected Conc. = 52.55 Report level label = 4.2 Pct Recovery = 77% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 33.016 Expected Conc. = 52.2 Report level label = 4.2 Pct Recovery = 63% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 41.013 Expected Conc. = 52.2 Report level label = 4.2 Pct Recovery = 79% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 39.839 Expected Conc. = 52.2 Report level label = 4.2 Pct Recovery = 76% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150192 Lab Value = 27.183 Expected Conc. = 42.4 Report level label = 4.2 Pct Recovery = 64% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 31.761 Expected Conc. = 42.4 Report level label = 4.2 Pct Recovery = 75% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 24.398 Expected Conc. = 42 Report level label = 4.2 Pct Recovery = 58% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221870197 Lab Value = 10.206 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 39% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20201550031 Lab Value = 19.939 Expected Conc. = 26.45 Report level label = 4.2 Pct Recovery = 75% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20210480001 Lab Value = 18.056 Expected Conc. = 26.275 Report level label = 4.2 Pct Recovery = 69% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20220740064 Lab Value = 16.368 Expected Conc. = 26.25 Report level label = 4.2 Pct Recovery = 62% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202880004 Lab Value = 16.480 Expected Conc. = 26.1 Report level label = 4.2 Pct Recovery = 63% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202390020 Lab Value = 24.830 Expected Conc. = 26.1 Report level label = 4.2 Pct Recovery = 95% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 21.747 Expected Conc. = 26.1 Report level label = 4.2 Pct Recovery = 83% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20210900005 Lab Value = 16.579 Expected Conc. = 21.02 Report level label = 4.2 Pct Recovery = 79% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 14.370 Expected Conc. = 20.88 Report level label = 4.2 Pct Recovery = 69% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 11.512 Expected Conc. = 20.88 Report level label = 4.2 Pct Recovery = 55% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 20.349 Expected Conc. = 20.88 Report level label = 4.2 Pct Recovery = 97% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 14.989 Expected Conc. = 20.88 Report level label = 4.2 Pct Recovery = 72% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20221660151 Lab Value = 6.143 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 58% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20202330309 Lab Value = 6.861 Expected Conc. = 10.58 Report level label = 4.2 Pct Recovery = 65% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 7.046 Expected Conc. = 10.58 Report level label = 4.2 Pct Recovery = 67% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 9.206 Expected Conc. = 10.58 Report level label = 4.2 Pct Recovery = 87% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 7.041 Expected Conc. = 10.58 Report level label = 4.2 Pct Recovery = 67% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 8.817 Expected Conc. = 10.58 Report level label = 4.2 Pct Recovery = 83% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210690067 Lab Value = 7.594 Expected Conc. = 10.51 Report level label = 4.2 Pct Recovery = 72% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210120050 Lab Value = 7.479 Expected Conc. = 10.44 Report level label = 4.2 Pct Recovery = 72% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 8.216 Expected Conc. = 10.44 Report level label = 4.2 Pct Recovery = 79% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.799 Expected Conc. = 10.44 Report level label = 4.2 Pct Recovery = 75% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 8.760 Expected Conc. = 10.44 Report level label = 4.2 Pct Recovery = 84% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 6.156 Expected Conc. = 10.44 Report level label = 4.2 Pct Recovery = 59% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 58% Analysis Date = 08/10/22 Pct Recovery = 58% Analysis Date = 08/10/22 Pct Recovery = 58% Analysis Date = 08/06/22 Pct Recovery = 58% Analysis Date = 08/06/22 Pct Recovery = 58% Analysis Date = 08/02/22 Pct Recovery = 58% Analysis Date = 08/02/22 Pct Recovery = 58% Analysis Date = 07/29/22 Pct Recovery = 58% Analysis Date = 07/29/22 Pct Recovery = 58% Analysis Date = 07/25/22 Pct Recovery = 59% Analysis Date = 07/25/22 Pct Recovery = 59% Analysis Date = 07/21/22 Pct Recovery = 59% Analysis Date = 07/21/22 Pct Recovery = 59% Analysis Date = 07/17/22 Pct Recovery = 59% Analysis Date = 07/17/22 Pct Recovery = 59% Analysis Date = 07/13/22 Pct Recovery = 59% Analysis Date = 07/13/22 Pct Recovery = 59% Analysis Date = 07/09/22 Pct Recovery = 59% Analysis Date = 07/09/22 Pct Recovery = 59% Analysis Date = 07/05/22 Pct Recovery = 59% Analysis Date = 07/05/22 Pct Recovery = 59% Analysis Date = 07/01/22 Pct Recovery = 59% Analysis Date = 07/01/22 Pct Recovery = 59% Analysis Date = 06/27/22 Pct Recovery = 59% Analysis Date = 06/27/22 Pct Recovery = 59% Analysis Date = 06/23/22 Pct Recovery = 59% Analysis Date = 06/23/22 Pct Recovery = 59% Analysis Date = 06/19/22 Pct Recovery = 59% Analysis Date = 06/19/22 Pct Recovery = 59% Analysis Date = 06/15/22 Pct Recovery = 59% Analysis Date = 06/15/22 Pct Recovery = 59% Analysis Date = 06/11/22 Pct Recovery = 59% Analysis Date = 06/11/22 Pct Recovery = 59% Analysis Date = 06/07/22 Pct Recovery = 59% Analysis Date = 06/07/22 Pct Recovery = 59% Analysis Date = 06/03/22 Pct Recovery = 60% Analysis Date = 06/03/22 Pct Recovery = 60% Analysis Date = 05/30/22 Pct Recovery = 60% Analysis Date = 05/30/22 Pct Recovery = 60% Analysis Date = 05/26/22 Pct Recovery = 60% Analysis Date = 05/26/22 Pct Recovery = 60% Analysis Date = 05/22/22 Pct Recovery = 60% Analysis Date = 05/22/22 Pct Recovery = 60% Analysis Date = 05/18/22 Pct Recovery = 60% Analysis Date = 05/18/22 Pct Recovery = 60% Analysis Date = 05/14/22 Pct Recovery = 60% Analysis Date = 05/14/22 Pct Recovery = 60% Analysis Date = 05/10/22 Pct Recovery = 60% Analysis Date = 05/10/22 Pct Recovery = 60% Analysis Date = 05/06/22 Pct Recovery = 60% Analysis Date = 05/06/22 Pct Recovery = 60% Analysis Date = 05/01/22 Pct Recovery = 60% Analysis Date = 05/01/22 Pct Recovery = 60% Analysis Date = 04/27/22 Pct Recovery = 60% Analysis Date = 04/27/22 Pct Recovery = 60% Analysis Date = 04/23/22 Pct Recovery = 60% Analysis Date = 04/23/22 Pct Recovery = 60% Analysis Date = 04/19/22 Pct Recovery = 60% Analysis Date = 04/19/22 Pct Recovery = 60% Analysis Date = 04/15/22 Pct Recovery = 60% Analysis Date = 04/15/22 Pct Recovery = 60% Analysis Date = 04/11/22 Pct Recovery = 60% Analysis Date = 04/11/22 Pct Recovery = 60% Analysis Date = 04/07/22 Pct Recovery = 60% Analysis Date = 04/07/22 Pct Recovery = 60% Analysis Date = 04/03/22 Pct Recovery = 61% Analysis Date = 04/03/22 Pct Recovery = 61% Analysis Date = 03/30/22 Pct Recovery = 61% Analysis Date = 03/30/22 Pct Recovery = 61% Analysis Date = 03/26/22 Pct Recovery = 61% Analysis Date = 03/26/22 Pct Recovery = 61% Analysis Date = 03/22/22 Pct Recovery = 61% Analysis Date = 03/22/22 Pct Recovery = 61% Analysis Date = 03/18/22 Pct Recovery = 61% Analysis Date = 03/18/22 Pct Recovery = 61% Analysis Date = 03/14/22 Pct Recovery = 61% Analysis Date = 03/14/22 Pct Recovery = 61% Analysis Date = 03/10/22 Pct Recovery = 61% Analysis Date = 03/10/22 Pct Recovery = 61% Analysis Date = 03/06/22 Pct Recovery = 61% Analysis Date = 03/06/22 Pct Recovery = 61% Analysis Date = 03/02/22 Pct Recovery = 61% Analysis Date = 03/02/22 Pct Recovery = 61% Analysis Date = 02/26/22 Pct Recovery = 61% Analysis Date = 02/26/22 Pct Recovery = 61% Analysis Date = 02/22/22 Pct Recovery = 61% Analysis Date = 02/22/22 Pct Recovery = 61% Analysis Date = 02/18/22 Pct Recovery = 61% Analysis Date = 02/18/22 Pct Recovery = 61% Analysis Date = 02/14/22 Pct Recovery = 61% Analysis Date = 02/14/22 Pct Recovery = 61% Analysis Date = 02/10/22 Pct Recovery = 61% Analysis Date = 02/10/22 Pct Recovery = 61% Analysis Date = 02/06/22 Pct Recovery = 61% Analysis Date = 02/06/22 Pct Recovery = 61% Analysis Date = 02/02/22 Pct Recovery = 61% Analysis Date = 02/02/22 Pct Recovery = 61% Analysis Date = 01/29/22 Pct Recovery = 62% Analysis Date = 01/29/22 Pct Recovery = 62% Analysis Date = 01/25/22 Pct Recovery = 62% Analysis Date = 01/25/22 Pct Recovery = 62% Analysis Date = 01/20/22 Pct Recovery = 62% Analysis Date = 01/20/22 Pct Recovery = 62% Analysis Date = 01/16/22 Pct Recovery = 62% Analysis Date = 01/16/22 Pct Recovery = 62% Analysis Date = 01/12/22 Pct Recovery = 62% Analysis Date = 01/12/22 Pct Recovery = 62% Analysis Date = 01/08/22 Pct Recovery = 62% Analysis Date = 01/08/22 Pct Recovery = 62% Analysis Date = 01/04/22 Pct Recovery = 62% Analysis Date = 01/04/22 Pct Recovery = 62% Analysis Date = 12/31/21 Pct Recovery = 62% Analysis Date = 12/31/21 Pct Recovery = 62% Analysis Date = 12/27/21 Pct Recovery = 62% Analysis Date = 12/27/21 Pct Recovery = 62% Analysis Date = 12/23/21 Pct Recovery = 62% Analysis Date = 12/23/21 Pct Recovery = 62% Analysis Date = 12/19/21 Pct Recovery = 62% Analysis Date = 12/19/21 Pct Recovery = 62% Analysis Date = 12/15/21 Pct Recovery = 62% Analysis Date = 12/15/21 Pct Recovery = 62% Analysis Date = 12/11/21 Pct Recovery = 62% Analysis Date = 12/11/21 Pct Recovery = 62% Analysis Date = 12/07/21 Pct Recovery = 62% Analysis Date = 12/07/21 Pct Recovery = 62% Analysis Date = 12/03/21 Pct Recovery = 62% Analysis Date = 12/03/21 Pct Recovery = 62% Analysis Date = 11/29/21 Pct Recovery = 63% Analysis Date = 11/29/21 Pct Recovery = 63% Analysis Date = 11/25/21 Pct Recovery = 63% Analysis Date = 11/25/21 Pct Recovery = 63% Analysis Date = 11/21/21 Pct Recovery = 63% Analysis Date = 11/21/21 Pct Recovery = 63% Analysis Date = 11/17/21 Pct Recovery = 63% Analysis Date = 11/17/21 Pct Recovery = 63% Analysis Date = 11/13/21 Pct Recovery = 63% Analysis Date = 11/13/21 Pct Recovery = 63% Analysis Date = 11/09/21 Pct Recovery = 63% Analysis Date = 11/09/21 Pct Recovery = 63% Analysis Date = 11/05/21 Pct Recovery = 63% Analysis Date = 11/05/21 Pct Recovery = 63% Analysis Date = 11/01/21 Pct Recovery = 63% Analysis Date = 11/01/21 Pct Recovery = 63% Analysis Date = 10/28/21 Pct Recovery = 63% Analysis Date = 10/28/21 Pct Recovery = 63% Analysis Date = 10/24/21 Pct Recovery = 63% Analysis Date = 10/24/21 Pct Recovery = 63% Analysis Date = 10/20/21 Pct Recovery = 63% Analysis Date = 10/20/21 Pct Recovery = 63% Analysis Date = 10/16/21 Pct Recovery = 63% Analysis Date = 10/16/21 Pct Recovery = 63% Analysis Date = 10/11/21 Pct Recovery = 63% Analysis Date = 10/11/21 Pct Recovery = 63% Analysis Date = 10/07/21 Pct Recovery = 63% Analysis Date = 10/07/21 Pct Recovery = 63% Analysis Date = 10/03/21 Pct Recovery = 63% Analysis Date = 10/03/21 Pct Recovery = 63% Analysis Date = 09/29/21 Pct Recovery = 64% Analysis Date = 09/29/21 Pct Recovery = 64% Analysis Date = 09/25/21 Pct Recovery = 64% Analysis Date = 09/25/21 Pct Recovery = 64% Analysis Date = 09/21/21 Pct Recovery = 64% Analysis Date = 09/21/21 Pct Recovery = 64% Analysis Date = 09/17/21 Pct Recovery = 64% Analysis Date = 09/17/21 Pct Recovery = 64% Analysis Date = 09/13/21 Pct Recovery = 64% Analysis Date = 09/13/21 Pct Recovery = 64% Analysis Date = 09/09/21 Pct Recovery = 64% Analysis Date = 09/09/21 Pct Recovery = 64% Analysis Date = 09/05/21 Pct Recovery = 64% Analysis Date = 09/05/21 Pct Recovery = 64% Analysis Date = 09/01/21 Pct Recovery = 64% Analysis Date = 09/01/21 Pct Recovery = 64% Analysis Date = 08/28/21 Pct Recovery = 64% Analysis Date = 08/28/21 Pct Recovery = 64% Analysis Date = 08/24/21 Pct Recovery = 64% Analysis Date = 08/24/21 Pct Recovery = 64% Analysis Date = 08/20/21 Pct Recovery = 64% Analysis Date = 08/20/21 Pct Recovery = 64% Analysis Date = 08/16/21 Pct Recovery = 64% Analysis Date = 08/16/21 Pct Recovery = 64% Analysis Date = 08/12/21 Pct Recovery = 64% Analysis Date = 08/12/21 Pct Recovery = 64% Analysis Date = 08/08/21 Pct Recovery = 64% Analysis Date = 08/08/21 Pct Recovery = 64% Analysis Date = 08/04/21 Pct Recovery = 64% Analysis Date = 08/04/21 Pct Recovery = 64% Analysis Date = 07/31/21 Pct Recovery = 64% Analysis Date = 07/31/21 Pct Recovery = 64% Analysis Date = 07/27/21 Pct Recovery = 65% Analysis Date = 07/27/21 Pct Recovery = 65% Analysis Date = 07/23/21 Pct Recovery = 65% Analysis Date = 07/23/21 Pct Recovery = 65% Analysis Date = 07/19/21 Pct Recovery = 65% Analysis Date = 07/19/21 Pct Recovery = 65% Analysis Date = 07/15/21 Pct Recovery = 65% Analysis Date = 07/15/21 Pct Recovery = 65% Analysis Date = 07/11/21 Pct Recovery = 65% Analysis Date = 07/11/21 Pct Recovery = 65% Analysis Date = 07/07/21 Pct Recovery = 65% Analysis Date = 07/07/21 Pct Recovery = 65% Analysis Date = 07/02/21 Pct Recovery = 65% Analysis Date = 07/02/21 Pct Recovery = 65% Analysis Date = 06/28/21 Pct Recovery = 65% Analysis Date = 06/28/21 Pct Recovery = 65% Analysis Date = 06/24/21 Pct Recovery = 65% Analysis Date = 06/24/21 Pct Recovery = 65% Analysis Date = 06/20/21 Pct Recovery = 65% Analysis Date = 06/20/21 Pct Recovery = 65% Analysis Date = 06/16/21 Pct Recovery = 65% Analysis Date = 06/16/21 Pct Recovery = 65% Analysis Date = 06/12/21 Pct Recovery = 65% Analysis Date = 06/12/21 Pct Recovery = 65% Analysis Date = 06/08/21 Pct Recovery = 65% Analysis Date = 06/08/21 Pct Recovery = 65% Analysis Date = 06/04/21 Pct Recovery = 65% Analysis Date = 06/04/21 Pct Recovery = 65% Analysis Date = 05/31/21 Pct Recovery = 65% Analysis Date = 05/31/21 Pct Recovery = 65% Analysis Date = 05/27/21 Pct Recovery = 66% Analysis Date = 05/27/21 Pct Recovery = 66% Analysis Date = 05/23/21 Pct Recovery = 66% Analysis Date = 05/23/21 Pct Recovery = 66% Analysis Date = 05/19/21 Pct Recovery = 66% Analysis Date = 05/19/21 Pct Recovery = 66% Analysis Date = 05/15/21 Pct Recovery = 66% Analysis Date = 05/15/21 Pct Recovery = 66% Analysis Date = 05/11/21 Pct Recovery = 66% Analysis Date = 05/11/21 Pct Recovery = 66% Analysis Date = 05/07/21 Pct Recovery = 66% Analysis Date = 05/07/21 Pct Recovery = 66% Analysis Date = 05/03/21 Pct Recovery = 66% Analysis Date = 05/03/21 Pct Recovery = 66% Analysis Date = 04/29/21 Pct Recovery = 66% Analysis Date = 04/29/21 Pct Recovery = 66% Analysis Date = 04/25/21 Pct Recovery = 66% Analysis Date = 04/25/21 Pct Recovery = 66% Analysis Date = 04/21/21 Pct Recovery = 66% Analysis Date = 04/21/21 Pct Recovery = 66% Analysis Date = 04/17/21 Pct Recovery = 66% Analysis Date = 04/17/21 Pct Recovery = 66% Analysis Date = 04/13/21 Pct Recovery = 66% Analysis Date = 04/13/21 Pct Recovery = 66% Analysis Date = 04/09/21 Pct Recovery = 66% Analysis Date = 04/09/21 Pct Recovery = 66% Analysis Date = 04/05/21 Pct Recovery = 66% Analysis Date = 04/05/21 Pct Recovery = 66% Analysis Date = 04/01/21 Pct Recovery = 66% Analysis Date = 04/01/21 Pct Recovery = 66% Analysis Date = 03/28/21 Pct Recovery = 67% Analysis Date = 03/28/21 Pct Recovery = 67% Analysis Date = 03/23/21 Pct Recovery = 67% Analysis Date = 03/23/21 Pct Recovery = 67% Analysis Date = 03/19/21 Pct Recovery = 67% Analysis Date = 03/19/21 Pct Recovery = 67% Analysis Date = 03/15/21 Pct Recovery = 67% Analysis Date = 03/15/21 Pct Recovery = 67% Analysis Date = 03/11/21 Pct Recovery = 67% Analysis Date = 03/11/21 Pct Recovery = 67% Analysis Date = 03/07/21 Pct Recovery = 67% Analysis Date = 03/07/21 Pct Recovery = 67% Analysis Date = 03/03/21 Pct Recovery = 67% Analysis Date = 03/03/21 Pct Recovery = 67% Analysis Date = 02/27/21 Pct Recovery = 67% Analysis Date = 02/27/21 Pct Recovery = 67% Analysis Date = 02/23/21 Pct Recovery = 67% Analysis Date = 02/23/21 Pct Recovery = 67% Analysis Date = 02/19/21 Pct Recovery = 67% Analysis Date = 02/19/21 Pct Recovery = 67% Analysis Date = 02/15/21 Pct Recovery = 67% Analysis Date = 02/15/21 Pct Recovery = 67% Analysis Date = 02/11/21 Pct Recovery = 67% Analysis Date = 02/11/21 Pct Recovery = 67% Analysis Date = 02/07/21 Pct Recovery = 67% Analysis Date = 02/07/21 Pct Recovery = 67% Analysis Date = 02/03/21 Pct Recovery = 67% Analysis Date = 02/03/21 Pct Recovery = 67% Analysis Date = 01/30/21 Pct Recovery = 67% Analysis Date = 01/30/21 Pct Recovery = 67% Analysis Date = 01/26/21 Pct Recovery = 67% Analysis Date = 01/26/21 Pct Recovery = 67% Analysis Date = 01/22/21 Pct Recovery = 67% Analysis Date = 01/22/21 Pct Recovery = 67% Analysis Date = 01/18/21 Pct Recovery = 67% Analysis Date = 01/18/21 Pct Recovery = 67% Analysis Date = 01/14/21 Pct Recovery = 68% Analysis Date = 01/14/21 Pct Recovery = 68% Analysis Date = 01/10/21 Pct Recovery = 68% Analysis Date = 01/10/21 Pct Recovery = 68% Analysis Date = 01/06/21 Pct Recovery = 68% Analysis Date = 01/06/21 Pct Recovery = 68% Analysis Date = 01/02/21 Pct Recovery = 68% Analysis Date = 01/02/21 Pct Recovery = 68% Analysis Date = 12/29/20 Pct Recovery = 68% Analysis Date = 12/29/20 Pct Recovery = 68% Analysis Date = 12/25/20 Pct Recovery = 68% Analysis Date = 12/25/20 Pct Recovery = 68% Analysis Date = 12/21/20 Pct Recovery = 68% Analysis Date = 12/21/20 Pct Recovery = 68% Analysis Date = 12/17/20 Pct Recovery = 68% Analysis Date = 12/17/20 Pct Recovery = 68% Analysis Date = 12/12/20 Pct Recovery = 68% Analysis Date = 12/12/20 Pct Recovery = 68% Analysis Date = 12/08/20 Pct Recovery = 69% Analysis Date = 12/08/20 Pct Recovery = 69% Analysis Date = 12/04/20 Pct Recovery = 69% Analysis Date = 12/04/20 Pct Recovery = 69% Analysis Date = 11/30/20 Pct Recovery = 69% Analysis Date = 11/30/20 Pct Recovery = 69% Analysis Date = 11/26/20 Pct Recovery = 70% Analysis Date = 11/26/20 Pct Recovery = 70% Analysis Date = 11/22/20 Pct Recovery = 70% Analysis Date = 11/22/20 Pct Recovery = 70% Analysis Date = 11/18/20 Pct Recovery = 70% Analysis Date = 11/18/20 Pct Recovery = 70% Analysis Date = 11/14/20 Pct Recovery = 71% Analysis Date = 11/14/20 Pct Recovery = 71% Analysis Date = 11/10/20 Pct Recovery = 71% Analysis Date = 11/10/20 Pct Recovery = 71% Analysis Date = 11/06/20 Pct Recovery = 71% Analysis Date = 11/06/20 Pct Recovery = 71% Analysis Date = 11/02/20 Pct Recovery = 72% Analysis Date = 11/02/20 Pct Recovery = 72% Analysis Date = 10/29/20 Pct Recovery = 72% Analysis Date = 10/29/20 Pct Recovery = 72% Analysis Date = 10/25/20 Pct Recovery = 72% Analysis Date = 10/25/20 Pct Recovery = 72% Analysis Date = 10/21/20 Pct Recovery = 73% Analysis Date = 10/21/20 Pct Recovery = 73% Analysis Date = 10/17/20 Pct Recovery = 73% Analysis Date = 10/17/20 Pct Recovery = 73% Analysis Date = 10/13/20 Pct Recovery = 73% Analysis Date = 10/13/20 Pct Recovery = 73% Analysis Date = 10/09/20 Pct Recovery = 73% Analysis Date = 10/09/20 Pct Recovery = 73% Analysis Date = 10/05/20 Pct Recovery = 74% Analysis Date = 10/05/20 Pct Recovery = 74% Analysis Date = 10/01/20 Pct Recovery = 74% Analysis Date = 10/01/20 Pct Recovery = 74% Analysis Date = 09/27/20 Pct Recovery = 74% Analysis Date = 09/27/20 Pct Recovery = 74% Analysis Date = 09/23/20 Pct Recovery = 74% Analysis Date = 09/23/20 Pct Recovery = 74% Analysis Date = 09/19/20 Pct Recovery = 75% Analysis Date = 09/19/20 Pct Recovery = 75% Analysis Date = 09/15/20 Pct Recovery = 75% Analysis Date = 09/15/20 Pct Recovery = 75% Analysis Date = 09/11/20 Pct Recovery = 75% Analysis Date = 09/11/20 Pct Recovery = 75% Analysis Date = 09/07/20 Pct Recovery = 76% Analysis Date = 09/07/20 Pct Recovery = 76% Analysis Date = 09/02/20 Pct Recovery = 76% Analysis Date = 09/02/20 Pct Recovery = 76% Analysis Date = 08/29/20 Pct Recovery = 76% Analysis Date = 08/29/20 Pct Recovery = 76% Analysis Date = 08/25/20 Pct Recovery = 76% Analysis Date = 08/25/20 Pct Recovery = 76% Analysis Date = 08/21/20 Pct Recovery = 76% Analysis Date = 08/21/20 Pct Recovery = 76% Analysis Date = 08/17/20 Pct Recovery = 77% Analysis Date = 08/17/20 Pct Recovery = 77% Analysis Date = 08/13/20 Pct Recovery = 77% Analysis Date = 08/13/20 Pct Recovery = 77% Analysis Date = 08/09/20 Pct Recovery = 77% Analysis Date = 08/09/20 Pct Recovery = 77% Analysis Date = 08/05/20 Pct Recovery = 77% Analysis Date = 08/05/20 Pct Recovery = 77% Analysis Date = 08/01/20 Pct Recovery = 78% Analysis Date = 08/01/20 Pct Recovery = 78% Analysis Date = 07/28/20 Pct Recovery = 78% Analysis Date = 07/28/20 Pct Recovery = 78% Analysis Date = 07/24/20 Pct Recovery = 78% Analysis Date = 07/24/20 Pct Recovery = 78% Analysis Date = 07/20/20 Pct Recovery = 78% Analysis Date = 07/20/20 Pct Recovery = 78% Analysis Date = 07/16/20 Pct Recovery = 78% Analysis Date = 07/16/20 Pct Recovery = 78% Analysis Date = 07/12/20 Pct Recovery = 79% Analysis Date = 07/12/20 Pct Recovery = 79% Analysis Date = 07/08/20 Pct Recovery = 79% Analysis Date = 07/08/20 Pct Recovery = 79% Analysis Date = 07/04/20 Pct Recovery = 79% Analysis Date = 07/04/20 Pct Recovery = 79% Analysis Date = 06/30/20 Pct Recovery = 79% Analysis Date = 06/30/20 Pct Recovery = 79% Analysis Date = 06/26/20 Pct Recovery = 79% Analysis Date = 06/26/20 Pct Recovery = 79% Analysis Date = 06/22/20 Pct Recovery = 80% Analysis Date = 06/22/20 Pct Recovery = 80% Analysis Date = 06/18/20 Pct Recovery = 80% Analysis Date = 06/18/20 Pct Recovery = 80% Analysis Date = 06/14/20 Pct Recovery = 80% Analysis Date = 06/14/20 Pct Recovery = 80% Analysis Date = 06/10/20 Pct Recovery = 80% Analysis Date = 06/10/20 Pct Recovery = 80% Analysis Date = 06/06/20 Pct Recovery = 80% Analysis Date = 06/06/20 Pct Recovery = 80% Analysis Date = 06/02/20 Pct Recovery = 81% Analysis Date = 06/02/20 Pct Recovery = 81% Analysis Date = 05/29/20 Pct Recovery = 81% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETOXAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 70% 13% 70% 12%
Total 34 70% 13% 70% 12%

Sample Statistics
ETOXAZOLE

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

OBSP Determination:
FIPRONIL
METHOD: 2447 , TESTIDCODE: 66604LCM60

Laboratory ID = 20203080100 Lab Value = 37.835 Expected Conc. = 50.1 Report level label = 4 Pct Recovery = 76% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 34.680 Expected Conc. = 50.1 Report level label = 4 Pct Recovery = 69% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 40.918 Expected Conc. = 50.1 Report level label = 4 Pct Recovery = 82% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 32.652 Expected Conc. = 49.15 Report level label = 4 Pct Recovery = 66% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 40.527 Expected Conc. = 49.15 Report level label = 4 Pct Recovery = 82% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 45.116 Expected Conc. = 49.15 Report level label = 4 Pct Recovery = 92% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 39.078 Expected Conc. = 49.15 Report level label = 4 Pct Recovery = 80% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20222150193 Lab Value = 27.273 Expected Conc. = 40.4 Report level label = 4 Pct Recovery = 68% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220190116 Lab Value = 27.616 Expected Conc. = 40.08 Report level label = 4 Pct Recovery = 69% Analysis Date = 02/01/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 28.506 Expected Conc. = 40.08 Report level label = 4 Pct Recovery = 71% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 23.282 Expected Conc. = 40 Report level label = 4 Pct Recovery = 58% Analysis Date = 07/22/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 28.655 Expected Conc. = 40 Report level label = 4 Pct Recovery = 72% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20212990174 Lab Value = 23.494 Expected Conc. = 40 Report level label = 4 Pct Recovery = 59% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20201550031 Lab Value = 30.626 Expected Conc. = 25.35 Report level label = 4 Pct Recovery = 121% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20221730293 Lab Value = 17.776 Expected Conc. = 25.05 Report level label = 4 Pct Recovery = 71% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 14.283 Expected Conc. = 25.05 Report level label = 4 Pct Recovery = 57% Analysis Date = 02/02/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202880004 Lab Value = 17.688 Expected Conc. = 25.05 Report level label = 4 Pct Recovery = 71% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20220810133 Lab Value = 19.378 Expected Conc. = 25 Report level label = 4 Pct Recovery = 78% Analysis Date = 03/30/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20213340027 Lab Value = 16.228 Expected Conc. = 25 Report level label = 4 Pct Recovery = 65% Analysis Date = 12/04/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 48.219 Expected Conc. = 25 Report level label = 4 Pct Recovery = 193% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 12.156 Expected Conc. = 25 Report level label = 4 Pct Recovery = 49% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202390020 Lab Value = 21.493 Expected Conc. = 25 Report level label = 4 Pct Recovery = 86% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 21.515 Expected Conc. = 25 Report level label = 4 Pct Recovery = 86% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20210480001 Lab Value = 19.385 Expected Conc. = 24.575 Report level label = 4 Pct Recovery = 79% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 12.630 Expected Conc. = 20.04 Report level label = 4 Pct Recovery = 63% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 14.830 Expected Conc. = 20.04 Report level label = 4 Pct Recovery = 74% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 18.563 Expected Conc. = 20 Report level label = 4 Pct Recovery = 93% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 18.554 Expected Conc. = 20 Report level label = 4 Pct Recovery = 93% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210900005 Lab Value = 20.684 Expected Conc. = 19.66 Report level label = 4 Pct Recovery = 105% Analysis Date = 04/06/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202330309 Lab Value = 8.002 Expected Conc. = 10.14 Report level label = 4 Pct Recovery = 79% Analysis Date = 09/01/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 8.708 Expected Conc. = 10.14 Report level label = 4 Pct Recovery = 86% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 9.651 Expected Conc. = 10.14 Report level label = 4 Pct Recovery = 95% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 8.026 Expected Conc. = 10.14 Report level label = 4 Pct Recovery = 79% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 9.654 Expected Conc. = 10.14 Report level label = 4 Pct Recovery = 95% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20222500483 Lab Value = 6.470 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 65% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 7.263 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 72% Analysis Date = 12/14/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210120050 Lab Value = 6.826 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 68% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 7.390 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 74% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.119 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 71% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 7.447 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 74% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 8.313 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 83% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222630205 Lab Value = 8.191 Expected Conc. = 10 Report level label = 4 Pct Recovery = 82% Analysis Date = 09/30/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20213060210 Lab Value = 6.444 Expected Conc. = 10 Report level label = 4 Pct Recovery = 64% Analysis Date = 11/09/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210690067 Lab Value = 8.267 Expected Conc. = 9.83 Report level label = 4 Pct Recovery = 84% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 10/13/22 Pct Recovery = 67% Analysis Date = 10/09/22 Pct Recovery = 67% Analysis Date = 10/09/22 Pct Recovery = 67% Analysis Date = 10/05/22 Pct Recovery = 67% Analysis Date = 10/05/22 Pct Recovery = 67% Analysis Date = 09/30/22 Pct Recovery = 67% Analysis Date = 09/30/22 Pct Recovery = 67% Analysis Date = 09/26/22 Pct Recovery = 68% Analysis Date = 09/26/22 Pct Recovery = 68% Analysis Date = 09/22/22 Pct Recovery = 68% Analysis Date = 09/22/22 Pct Recovery = 68% Analysis Date = 09/17/22 Pct Recovery = 68% Analysis Date = 09/17/22 Pct Recovery = 68% Analysis Date = 09/13/22 Pct Recovery = 68% Analysis Date = 09/13/22 Pct Recovery = 68% Analysis Date = 09/09/22 Pct Recovery = 68% Analysis Date = 09/09/22 Pct Recovery = 68% Analysis Date = 09/04/22 Pct Recovery = 68% Analysis Date = 09/04/22 Pct Recovery = 68% Analysis Date = 08/31/22 Pct Recovery = 68% Analysis Date = 08/31/22 Pct Recovery = 68% Analysis Date = 08/27/22 Pct Recovery = 69% Analysis Date = 08/27/22 Pct Recovery = 69% Analysis Date = 08/22/22 Pct Recovery = 69% Analysis Date = 08/22/22 Pct Recovery = 69% Analysis Date = 08/18/22 Pct Recovery = 69% Analysis Date = 08/18/22 Pct Recovery = 69% Analysis Date = 08/14/22 Pct Recovery = 69% Analysis Date = 08/14/22 Pct Recovery = 69% Analysis Date = 08/09/22 Pct Recovery = 69% Analysis Date = 08/09/22 Pct Recovery = 69% Analysis Date = 08/05/22 Pct Recovery = 69% Analysis Date = 08/05/22 Pct Recovery = 69% Analysis Date = 08/01/22 Pct Recovery = 69% Analysis Date = 08/01/22 Pct Recovery = 69% Analysis Date = 07/27/22 Pct Recovery = 70% Analysis Date = 07/27/22 Pct Recovery = 70% Analysis Date = 07/23/22 Pct Recovery = 70% Analysis Date = 07/23/22 Pct Recovery = 70% Analysis Date = 07/19/22 Pct Recovery = 70% Analysis Date = 07/19/22 Pct Recovery = 70% Analysis Date = 07/14/22 Pct Recovery = 70% Analysis Date = 07/14/22 Pct Recovery = 70% Analysis Date = 07/10/22 Pct Recovery = 70% Analysis Date = 07/10/22 Pct Recovery = 70% Analysis Date = 07/06/22 Pct Recovery = 70% Analysis Date = 07/06/22 Pct Recovery = 70% Analysis Date = 07/01/22 Pct Recovery = 70% Analysis Date = 07/01/22 Pct Recovery = 70% Analysis Date = 06/27/22 Pct Recovery = 71% Analysis Date = 06/27/22 Pct Recovery = 71% Analysis Date = 06/23/22 Pct Recovery = 71% Analysis Date = 06/23/22 Pct Recovery = 71% Analysis Date = 06/18/22 Pct Recovery = 71% Analysis Date = 06/18/22 Pct Recovery = 71% Analysis Date = 06/14/22 Pct Recovery = 71% Analysis Date = 06/14/22 Pct Recovery = 71% Analysis Date = 06/10/22 Pct Recovery = 71% Analysis Date = 06/10/22 Pct Recovery = 71% Analysis Date = 06/05/22 Pct Recovery = 71% Analysis Date = 06/05/22 Pct Recovery = 71% Analysis Date = 06/01/22 Pct Recovery = 71% Analysis Date = 06/01/22 Pct Recovery = 71% Analysis Date = 05/28/22 Pct Recovery = 72% Analysis Date = 05/28/22 Pct Recovery = 72% Analysis Date = 05/23/22 Pct Recovery = 72% Analysis Date = 05/23/22 Pct Recovery = 72% Analysis Date = 05/19/22 Pct Recovery = 72% Analysis Date = 05/19/22 Pct Recovery = 72% Analysis Date = 05/15/22 Pct Recovery = 72% Analysis Date = 05/15/22 Pct Recovery = 72% Analysis Date = 05/10/22 Pct Recovery = 72% Analysis Date = 05/10/22 Pct Recovery = 72% Analysis Date = 05/06/22 Pct Recovery = 72% Analysis Date = 05/06/22 Pct Recovery = 72% Analysis Date = 05/02/22 Pct Recovery = 72% Analysis Date = 05/02/22 Pct Recovery = 72% Analysis Date = 04/27/22 Pct Recovery = 73% Analysis Date = 04/27/22 Pct Recovery = 73% Analysis Date = 04/23/22 Pct Recovery = 73% Analysis Date = 04/23/22 Pct Recovery = 73% Analysis Date = 04/19/22 Pct Recovery = 73% Analysis Date = 04/19/22 Pct Recovery = 73% Analysis Date = 04/14/22 Pct Recovery = 73% Analysis Date = 04/14/22 Pct Recovery = 73% Analysis Date = 04/10/22 Pct Recovery = 73% Analysis Date = 04/10/22 Pct Recovery = 73% Analysis Date = 04/06/22 Pct Recovery = 73% Analysis Date = 04/06/22 Pct Recovery = 73% Analysis Date = 04/01/22 Pct Recovery = 73% Analysis Date = 04/01/22 Pct Recovery = 73% Analysis Date = 03/28/22 Pct Recovery = 74% Analysis Date = 03/28/22 Pct Recovery = 74% Analysis Date = 03/24/22 Pct Recovery = 74% Analysis Date = 03/24/22 Pct Recovery = 74% Analysis Date = 03/19/22 Pct Recovery = 74% Analysis Date = 03/19/22 Pct Recovery = 74% Analysis Date = 03/15/22 Pct Recovery = 74% Analysis Date = 03/15/22 Pct Recovery = 74% Analysis Date = 03/11/22 Pct Recovery = 74% Analysis Date = 03/11/22 Pct Recovery = 74% Analysis Date = 03/06/22 Pct Recovery = 74% Analysis Date = 03/06/22 Pct Recovery = 74% Analysis Date = 03/02/22 Pct Recovery = 74% Analysis Date = 03/02/22 Pct Recovery = 74% Analysis Date = 02/26/22 Pct Recovery = 75% Analysis Date = 02/26/22 Pct Recovery = 75% Analysis Date = 02/21/22 Pct Recovery = 75% Analysis Date = 02/21/22 Pct Recovery = 75% Analysis Date = 02/17/22 Pct Recovery = 75% Analysis Date = 02/17/22 Pct Recovery = 75% Analysis Date = 02/13/22 Pct Recovery = 75% Analysis Date = 02/13/22 Pct Recovery = 75% Analysis Date = 02/08/22 Pct Recovery = 75% Analysis Date = 02/08/22 Pct Recovery = 75% Analysis Date = 02/04/22 Pct Recovery = 75% Analysis Date = 02/04/22 Pct Recovery = 75% Analysis Date = 01/31/22 Pct Recovery = 75% Analysis Date = 01/31/22 Pct Recovery = 75% Analysis Date = 01/26/22 Pct Recovery = 76% Analysis Date = 01/26/22 Pct Recovery = 76% Analysis Date = 01/22/22 Pct Recovery = 76% Analysis Date = 01/22/22 Pct Recovery = 76% Analysis Date = 01/18/22 Pct Recovery = 76% Analysis Date = 01/18/22 Pct Recovery = 76% Analysis Date = 01/13/22 Pct Recovery = 76% Analysis Date = 01/13/22 Pct Recovery = 76% Analysis Date = 01/09/22 Pct Recovery = 76% Analysis Date = 01/09/22 Pct Recovery = 76% Analysis Date = 01/05/22 Pct Recovery = 76% Analysis Date = 01/05/22 Pct Recovery = 76% Analysis Date = 12/31/21 Pct Recovery = 76% Analysis Date = 12/31/21 Pct Recovery = 76% Analysis Date = 12/27/21 Pct Recovery = 76% Analysis Date = 12/27/21 Pct Recovery = 76% Analysis Date = 12/23/21 Pct Recovery = 77% Analysis Date = 12/23/21 Pct Recovery = 77% Analysis Date = 12/18/21 Pct Recovery = 77% Analysis Date = 12/18/21 Pct Recovery = 77% Analysis Date = 12/14/21 Pct Recovery = 77% Analysis Date = 12/14/21 Pct Recovery = 77% Analysis Date = 12/10/21 Pct Recovery = 77% Analysis Date = 12/10/21 Pct Recovery = 77% Analysis Date = 12/05/21 Pct Recovery = 77% Analysis Date = 12/05/21 Pct Recovery = 77% Analysis Date = 12/01/21 Pct Recovery = 77% Analysis Date = 12/01/21 Pct Recovery = 77% Analysis Date = 11/27/21 Pct Recovery = 77% Analysis Date = 11/27/21 Pct Recovery = 77% Analysis Date = 11/22/21 Pct Recovery = 77% Analysis Date = 11/22/21 Pct Recovery = 77% Analysis Date = 11/18/21 Pct Recovery = 77% Analysis Date = 11/18/21 Pct Recovery = 77% Analysis Date = 11/14/21 Pct Recovery = 77% Analysis Date = 11/14/21 Pct Recovery = 77% Analysis Date = 11/09/21 Pct Recovery = 77% Analysis Date = 11/09/21 Pct Recovery = 77% Analysis Date = 11/05/21 Pct Recovery = 77% Analysis Date = 11/05/21 Pct Recovery = 77% Analysis Date = 11/01/21 Pct Recovery = 78% Analysis Date = 11/01/21 Pct Recovery = 78% Analysis Date = 10/27/21 Pct Recovery = 78% Analysis Date = 10/27/21 Pct Recovery = 78% Analysis Date = 10/23/21 Pct Recovery = 78% Analysis Date = 10/23/21 Pct Recovery = 78% Analysis Date = 10/19/21 Pct Recovery = 78% Analysis Date = 10/19/21 Pct Recovery = 78% Analysis Date = 10/14/21 Pct Recovery = 78% Analysis Date = 10/14/21 Pct Recovery = 78% Analysis Date = 10/10/21 Pct Recovery = 78% Analysis Date = 10/10/21 Pct Recovery = 78% Analysis Date = 10/06/21 Pct Recovery = 78% Analysis Date = 10/06/21 Pct Recovery = 78% Analysis Date = 10/01/21 Pct Recovery = 78% Analysis Date = 10/01/21 Pct Recovery = 78% Analysis Date = 09/27/21 Pct Recovery = 78% Analysis Date = 09/27/21 Pct Recovery = 78% Analysis Date = 09/23/21 Pct Recovery = 78% Analysis Date = 09/23/21 Pct Recovery = 78% Analysis Date = 09/18/21 Pct Recovery = 78% Analysis Date = 09/18/21 Pct Recovery = 78% Analysis Date = 09/14/21 Pct Recovery = 78% Analysis Date = 09/14/21 Pct Recovery = 78% Analysis Date = 09/10/21 Pct Recovery = 78% Analysis Date = 09/10/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 78% Analysis Date = 09/01/21 Pct Recovery = 78% Analysis Date = 09/01/21 Pct Recovery = 78% Analysis Date = 08/28/21 Pct Recovery = 78% Analysis Date = 08/28/21 Pct Recovery = 78% Analysis Date = 08/23/21 Pct Recovery = 78% Analysis Date = 08/23/21 Pct Recovery = 78% Analysis Date = 08/19/21 Pct Recovery = 78% Analysis Date = 08/19/21 Pct Recovery = 78% Analysis Date = 08/15/21 Pct Recovery = 78% Analysis Date = 08/15/21 Pct Recovery = 78% Analysis Date = 08/10/21 Pct Recovery = 78% Analysis Date = 08/10/21 Pct Recovery = 78% Analysis Date = 08/06/21 Pct Recovery = 78% Analysis Date = 08/06/21 Pct Recovery = 78% Analysis Date = 08/02/21 Pct Recovery = 78% Analysis Date = 08/02/21 Pct Recovery = 78% Analysis Date = 07/28/21 Pct Recovery = 78% Analysis Date = 07/28/21 Pct Recovery = 78% Analysis Date = 07/24/21 Pct Recovery = 78% Analysis Date = 07/24/21 Pct Recovery = 78% Analysis Date = 07/20/21 Pct Recovery = 79% Analysis Date = 07/20/21 Pct Recovery = 79% Analysis Date = 07/15/21 Pct Recovery = 79% Analysis Date = 07/15/21 Pct Recovery = 79% Analysis Date = 07/11/21 Pct Recovery = 79% Analysis Date = 07/11/21 Pct Recovery = 79% Analysis Date = 07/07/21 Pct Recovery = 79% Analysis Date = 07/07/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 06/28/21 Pct Recovery = 79% Analysis Date = 06/28/21 Pct Recovery = 79% Analysis Date = 06/24/21 Pct Recovery = 79% Analysis Date = 06/24/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/06/21 Pct Recovery = 79% Analysis Date = 06/06/21 Pct Recovery = 79% Analysis Date = 06/02/21 Pct Recovery = 79% Analysis Date = 06/02/21 Pct Recovery = 79% Analysis Date = 05/29/21 Pct Recovery = 79% Analysis Date = 05/29/21 Pct Recovery = 79% Analysis Date = 05/24/21 Pct Recovery = 79% Analysis Date = 05/24/21 Pct Recovery = 79% Analysis Date = 05/20/21 Pct Recovery = 79% Analysis Date = 05/20/21 Pct Recovery = 79% Analysis Date = 05/16/21 Pct Recovery = 79% Analysis Date = 05/16/21 Pct Recovery = 79% Analysis Date = 05/11/21 Pct Recovery = 79% Analysis Date = 05/11/21 Pct Recovery = 79% Analysis Date = 05/07/21 Pct Recovery = 79% Analysis Date = 05/07/21 Pct Recovery = 79% Analysis Date = 05/03/21 Pct Recovery = 79% Analysis Date = 05/03/21 Pct Recovery = 79% Analysis Date = 04/28/21 Pct Recovery = 79% Analysis Date = 04/28/21 Pct Recovery = 79% Analysis Date = 04/24/21 Pct Recovery = 79% Analysis Date = 04/24/21 Pct Recovery = 79% Analysis Date = 04/20/21 Pct Recovery = 79% Analysis Date = 04/20/21 Pct Recovery = 79% Analysis Date = 04/15/21 Pct Recovery = 79% Analysis Date = 04/15/21 Pct Recovery = 79% Analysis Date = 04/11/21 Pct Recovery = 79% Analysis Date = 04/11/21 Pct Recovery = 79% Analysis Date = 04/07/21 Pct Recovery = 79% Analysis Date = 04/07/21 Pct Recovery = 79% Analysis Date = 04/02/21 Pct Recovery = 79% Analysis Date = 04/02/21 Pct Recovery = 79% Analysis Date = 03/29/21 Pct Recovery = 79% Analysis Date = 03/29/21 Pct Recovery = 79% Analysis Date = 03/25/21 Pct Recovery = 79% Analysis Date = 03/25/21 Pct Recovery = 79% Analysis Date = 03/20/21 Pct Recovery = 79% Analysis Date = 03/20/21 Pct Recovery = 79% Analysis Date = 03/16/21 Pct Recovery = 79% Analysis Date = 03/16/21 Pct Recovery = 79% Analysis Date = 03/12/21 Pct Recovery = 79% Analysis Date = 03/12/21 Pct Recovery = 79% Analysis Date = 03/07/21 Pct Recovery = 79% Analysis Date = 03/07/21 Pct Recovery = 79% Analysis Date = 03/03/21 Pct Recovery = 79% Analysis Date = 03/03/21 Pct Recovery = 79% Analysis Date = 02/27/21 Pct Recovery = 79% Analysis Date = 02/27/21 Pct Recovery = 79% Analysis Date = 02/22/21 Pct Recovery = 79% Analysis Date = 02/22/21 Pct Recovery = 79% Analysis Date = 02/18/21 Pct Recovery = 79% Analysis Date = 02/18/21 Pct Recovery = 79% Analysis Date = 02/14/21 Pct Recovery = 79% Analysis Date = 02/14/21 Pct Recovery = 79% Analysis Date = 02/09/21 Pct Recovery = 78% Analysis Date = 02/09/21 Pct Recovery = 78% Analysis Date = 02/05/21 Pct Recovery = 78% Analysis Date = 02/05/21 Pct Recovery = 78% Analysis Date = 02/01/21 Pct Recovery = 78% Analysis Date = 02/01/21 Pct Recovery = 78% Analysis Date = 01/27/21 Pct Recovery = 78% Analysis Date = 01/27/21 Pct Recovery = 78% Analysis Date = 01/23/21 Pct Recovery = 78% Analysis Date = 01/23/21 Pct Recovery = 78% Analysis Date = 01/19/21 Pct Recovery = 78% Analysis Date = 01/19/21 Pct Recovery = 78% Analysis Date = 01/14/21 Pct Recovery = 78% Analysis Date = 01/14/21 Pct Recovery = 78% Analysis Date = 01/10/21 Pct Recovery = 78% Analysis Date = 01/10/21 Pct Recovery = 78% Analysis Date = 01/06/21 Pct Recovery = 78% Analysis Date = 01/06/21 Pct Recovery = 78% Analysis Date = 01/01/21 Pct Recovery = 78% Analysis Date = 01/01/21 Pct Recovery = 78% Analysis Date = 12/28/20 Pct Recovery = 78% Analysis Date = 12/28/20 Pct Recovery = 78% Analysis Date = 12/24/20 Pct Recovery = 78% Analysis Date = 12/24/20 Pct Recovery = 78% Analysis Date = 12/19/20 Pct Recovery = 78% Analysis Date = 12/19/20 Pct Recovery = 78% Analysis Date = 12/15/20 Pct Recovery = 78% Analysis Date = 12/15/20 Pct Recovery = 78% Analysis Date = 12/11/20 Pct Recovery = 77% Analysis Date = 12/11/20 Pct Recovery = 77% Analysis Date = 12/06/20 Pct Recovery = 78% Analysis Date = 12/06/20 Pct Recovery = 78% Analysis Date = 12/02/20 Pct Recovery = 78% Analysis Date = 12/02/20 Pct Recovery = 78% Analysis Date = 11/28/20 Pct Recovery = 78% Analysis Date = 11/28/20 Pct Recovery = 78% Analysis Date = 11/23/20 Pct Recovery = 78% Analysis Date = 11/23/20 Pct Recovery = 78% Analysis Date = 11/19/20 Pct Recovery = 78% Analysis Date = 11/19/20 Pct Recovery = 78% Analysis Date = 11/15/20 Pct Recovery = 78% Analysis Date = 11/15/20 Pct Recovery = 78% Analysis Date = 11/10/20 Pct Recovery = 78% Analysis Date = 11/10/20 Pct Recovery = 78% Analysis Date = 11/06/20 Pct Recovery = 79% Analysis Date = 11/06/20 Pct Recovery = 79% Analysis Date = 11/02/20 Pct Recovery = 79% Analysis Date = 11/02/20 Pct Recovery = 79% Analysis Date = 10/28/20 Pct Recovery = 79% Analysis Date = 10/28/20 Pct Recovery = 79% Analysis Date = 10/24/20 Pct Recovery = 79% Analysis Date = 10/24/20 Pct Recovery = 79% Analysis Date = 10/20/20 Pct Recovery = 79% Analysis Date = 10/20/20 Pct Recovery = 79% Analysis Date = 10/15/20 Pct Recovery = 80% Analysis Date = 10/15/20 Pct Recovery = 80% Analysis Date = 10/11/20 Pct Recovery = 80% Analysis Date = 10/11/20 Pct Recovery = 80% Analysis Date = 10/07/20 Pct Recovery = 81% Analysis Date = 10/07/20 Pct Recovery = 81% Analysis Date = 10/02/20 Pct Recovery = 81% Analysis Date = 10/02/20 Pct Recovery = 81% Analysis Date = 09/28/20 Pct Recovery = 82% Analysis Date = 09/28/20 Pct Recovery = 82% Analysis Date = 09/24/20 Pct Recovery = 82% Analysis Date = 09/24/20 Pct Recovery = 82% Analysis Date = 09/19/20 Pct Recovery = 83% Analysis Date = 09/19/20 Pct Recovery = 83% Analysis Date = 09/15/20 Pct Recovery = 83% Analysis Date = 09/15/20 Pct Recovery = 83% Analysis Date = 09/11/20 Pct Recovery = 84% Analysis Date = 09/11/20 Pct Recovery = 84% Analysis Date = 09/06/20 Pct Recovery = 85% Analysis Date = 09/06/20 Pct Recovery = 85% Analysis Date = 09/02/20 Pct Recovery = 85% Analysis Date = 09/02/20 Pct Recovery = 85% Analysis Date = 08/29/20 Pct Recovery = 86% Analysis Date = 08/29/20 Pct Recovery = 86% Analysis Date = 08/24/20 Pct Recovery = 86% Analysis Date = 08/24/20 Pct Recovery = 86% Analysis Date = 08/20/20 Pct Recovery = 87% Analysis Date = 08/20/20 Pct Recovery = 87% Analysis Date = 08/16/20 Pct Recovery = 87% Analysis Date = 08/16/20 Pct Recovery = 87% Analysis Date = 08/11/20 Pct Recovery = 88% Analysis Date = 08/11/20 Pct Recovery = 88% Analysis Date = 08/07/20 Pct Recovery = 88% Analysis Date = 08/07/20 Pct Recovery = 88% Analysis Date = 08/03/20 Pct Recovery = 89% Analysis Date = 08/03/20 Pct Recovery = 89% Analysis Date = 07/29/20 Pct Recovery = 90% Analysis Date = 07/29/20 Pct Recovery = 90% Analysis Date = 07/25/20 Pct Recovery = 90% Analysis Date = 07/25/20 Pct Recovery = 90% Analysis Date = 07/21/20 Pct Recovery = 91% Analysis Date = 07/21/20 Pct Recovery = 91% Analysis Date = 07/16/20 Pct Recovery = 91% Analysis Date = 07/16/20 Pct Recovery = 91% Analysis Date = 07/12/20 Pct Recovery = 92% Analysis Date = 07/12/20 Pct Recovery = 92% Analysis Date = 07/08/20 Pct Recovery = 92% Analysis Date = 07/08/20 Pct Recovery = 92% Analysis Date = 07/03/20 Pct Recovery = 93% Analysis Date = 07/03/20 Pct Recovery = 93% Analysis Date = 06/29/20 Pct Recovery = 94% Analysis Date = 06/29/20 Pct Recovery = 94% Analysis Date = 06/25/20 Pct Recovery = 94% Analysis Date = 06/25/20 Pct Recovery = 94% Analysis Date = 06/20/20 Pct Recovery = 95% Analysis Date = 06/20/20 Pct Recovery = 95% Analysis Date = 06/16/20 Pct Recovery = 95% Analysis Date = 06/16/20 Pct Recovery = 95% Analysis Date = 06/12/20 Pct Recovery = 96% Analysis Date = 06/12/20 Pct Recovery = 96% Analysis Date = 06/07/20 Pct Recovery = 97% Analysis Date = 06/07/20 Pct Recovery = 97% Analysis Date = 06/03/20 Pct Recovery = 97% Analysis Date = 06/03/20 Pct Recovery = 97% Analysis Date = 05/30/20 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 79% 22% 75% 12%
Total 44 79% 22% 75% 12%

Sample Statistics
FIPRONIL

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 66 .  
False Positives 2 3% 2 out of 66

OBSP Determination:
FIPRONIL AMIDE
METHOD: 2447 , TESTIDCODE: 68604LCM60

Laboratory ID = 20202110006 Lab Value = 120.234 Expected Conc. = 116.5 Report level label = 9.2 Pct Recovery = 103% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20202590107 Lab Value = 135.298 Expected Conc. = 114.9 Report level label = 9.2 Pct Recovery = 118% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 151.420 Expected Conc. = 114.9 Report level label = 9.2 Pct Recovery = 132% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222010133 Lab Value = 51.136 Expected Conc. = 92 Report level label = 9.2 Pct Recovery = 56% Analysis Date = 07/22/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20222640086 Lab Value = 82.407 Expected Conc. = 91.6 Report level label = 9.2 Pct Recovery = 90% Analysis Date = 09/30/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20201680155 Lab Value = 65.349 Expected Conc. = 58.25 Report level label = 9.2 Pct Recovery = 112% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20221730293 Lab Value = 43.625 Expected Conc. = 57.5 Report level label = 9.2 Pct Recovery = 76% Analysis Date = 07/01/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20203360042 Lab Value = 49.109 Expected Conc. = 57.45 Report level label = 9.2 Pct Recovery = 85% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 74.594 Expected Conc. = 57.45 Report level label = 9.2 Pct Recovery = 130% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 49.430 Expected Conc. = 57.45 Report level label = 9.2 Pct Recovery = 86% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201610160 Lab Value = 24.522 Expected Conc. = 23.3 Report level label = 9.2 Pct Recovery = 105% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20222500483 Lab Value = 28.119 Expected Conc. = 23 Report level label = 9.2 Pct Recovery = 122% Analysis Date = 10/14/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Laboratory ID = 20210970035 Lab Value = 25.654 Expected Conc. = 22.98 Report level label = 9.2 Pct Recovery = 112% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 26.748 Expected Conc. = 22.98 Report level label = 9.2 Pct Recovery = 116% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 29.160 Expected Conc. = 22.98 Report level label = 9.2 Pct Recovery = 127% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 23.109 Expected Conc. = 22.98 Report level label = 9.2 Pct Recovery = 101% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 20.688 Expected Conc. = 22.98 Report level label = 9.2 Pct Recovery = 90% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 10/14/22 Pct Recovery = 88% Analysis Date = 10/09/22 Pct Recovery = 88% Analysis Date = 10/09/22 Pct Recovery = 88% Analysis Date = 10/05/22 Pct Recovery = 88% Analysis Date = 10/05/22 Pct Recovery = 88% Analysis Date = 10/01/22 Pct Recovery = 88% Analysis Date = 10/01/22 Pct Recovery = 88% Analysis Date = 09/26/22 Pct Recovery = 88% Analysis Date = 09/26/22 Pct Recovery = 88% Analysis Date = 09/22/22 Pct Recovery = 88% Analysis Date = 09/22/22 Pct Recovery = 88% Analysis Date = 09/18/22 Pct Recovery = 88% Analysis Date = 09/18/22 Pct Recovery = 88% Analysis Date = 09/14/22 Pct Recovery = 88% Analysis Date = 09/14/22 Pct Recovery = 88% Analysis Date = 09/09/22 Pct Recovery = 88% Analysis Date = 09/09/22 Pct Recovery = 88% Analysis Date = 09/05/22 Pct Recovery = 88% Analysis Date = 09/05/22 Pct Recovery = 88% Analysis Date = 09/01/22 Pct Recovery = 88% Analysis Date = 09/01/22 Pct Recovery = 88% Analysis Date = 08/27/22 Pct Recovery = 88% Analysis Date = 08/27/22 Pct Recovery = 88% Analysis Date = 08/23/22 Pct Recovery = 88% Analysis Date = 08/23/22 Pct Recovery = 88% Analysis Date = 08/19/22 Pct Recovery = 88% Analysis Date = 08/19/22 Pct Recovery = 88% Analysis Date = 08/15/22 Pct Recovery = 88% Analysis Date = 08/15/22 Pct Recovery = 88% Analysis Date = 08/10/22 Pct Recovery = 88% Analysis Date = 08/10/22 Pct Recovery = 88% Analysis Date = 08/06/22 Pct Recovery = 88% Analysis Date = 08/06/22 Pct Recovery = 88% Analysis Date = 08/02/22 Pct Recovery = 88% Analysis Date = 08/02/22 Pct Recovery = 88% Analysis Date = 07/29/22 Pct Recovery = 88% Analysis Date = 07/29/22 Pct Recovery = 88% Analysis Date = 07/24/22 Pct Recovery = 88% Analysis Date = 07/24/22 Pct Recovery = 88% Analysis Date = 07/20/22 Pct Recovery = 88% Analysis Date = 07/20/22 Pct Recovery = 88% Analysis Date = 07/16/22 Pct Recovery = 88% Analysis Date = 07/16/22 Pct Recovery = 88% Analysis Date = 07/11/22 Pct Recovery = 88% Analysis Date = 07/11/22 Pct Recovery = 88% Analysis Date = 07/07/22 Pct Recovery = 88% Analysis Date = 07/07/22 Pct Recovery = 88% Analysis Date = 07/03/22 Pct Recovery = 89% Analysis Date = 07/03/22 Pct Recovery = 89% Analysis Date = 06/29/22 Pct Recovery = 89% Analysis Date = 06/29/22 Pct Recovery = 89% Analysis Date = 06/24/22 Pct Recovery = 89% Analysis Date = 06/24/22 Pct Recovery = 89% Analysis Date = 06/20/22 Pct Recovery = 89% Analysis Date = 06/20/22 Pct Recovery = 89% Analysis Date = 06/16/22 Pct Recovery = 90% Analysis Date = 06/16/22 Pct Recovery = 90% Analysis Date = 06/12/22 Pct Recovery = 90% Analysis Date = 06/12/22 Pct Recovery = 90% Analysis Date = 06/07/22 Pct Recovery = 90% Analysis Date = 06/07/22 Pct Recovery = 90% Analysis Date = 06/03/22 Pct Recovery = 90% Analysis Date = 06/03/22 Pct Recovery = 90% Analysis Date = 05/30/22 Pct Recovery = 91% Analysis Date = 05/30/22 Pct Recovery = 91% Analysis Date = 05/25/22 Pct Recovery = 91% Analysis Date = 05/25/22 Pct Recovery = 91% Analysis Date = 05/21/22 Pct Recovery = 91% Analysis Date = 05/21/22 Pct Recovery = 91% Analysis Date = 05/17/22 Pct Recovery = 91% Analysis Date = 05/17/22 Pct Recovery = 91% Analysis Date = 05/13/22 Pct Recovery = 92% Analysis Date = 05/13/22 Pct Recovery = 92% Analysis Date = 05/08/22 Pct Recovery = 92% Analysis Date = 05/08/22 Pct Recovery = 92% Analysis Date = 05/04/22 Pct Recovery = 92% Analysis Date = 05/04/22 Pct Recovery = 92% Analysis Date = 04/30/22 Pct Recovery = 92% Analysis Date = 04/30/22 Pct Recovery = 92% Analysis Date = 04/26/22 Pct Recovery = 93% Analysis Date = 04/26/22 Pct Recovery = 93% Analysis Date = 04/21/22 Pct Recovery = 93% Analysis Date = 04/21/22 Pct Recovery = 93% Analysis Date = 04/17/22 Pct Recovery = 93% Analysis Date = 04/17/22 Pct Recovery = 93% Analysis Date = 04/13/22 Pct Recovery = 93% Analysis Date = 04/13/22 Pct Recovery = 93% Analysis Date = 04/08/22 Pct Recovery = 94% Analysis Date = 04/08/22 Pct Recovery = 94% Analysis Date = 04/04/22 Pct Recovery = 94% Analysis Date = 04/04/22 Pct Recovery = 94% Analysis Date = 03/31/22 Pct Recovery = 94% Analysis Date = 03/31/22 Pct Recovery = 94% Analysis Date = 03/27/22 Pct Recovery = 94% Analysis Date = 03/27/22 Pct Recovery = 94% Analysis Date = 03/22/22 Pct Recovery = 95% Analysis Date = 03/22/22 Pct Recovery = 95% Analysis Date = 03/18/22 Pct Recovery = 95% Analysis Date = 03/18/22 Pct Recovery = 95% Analysis Date = 03/14/22 Pct Recovery = 95% Analysis Date = 03/14/22 Pct Recovery = 95% Analysis Date = 03/09/22 Pct Recovery = 95% Analysis Date = 03/09/22 Pct Recovery = 95% Analysis Date = 03/05/22 Pct Recovery = 96% Analysis Date = 03/05/22 Pct Recovery = 96% Analysis Date = 03/01/22 Pct Recovery = 96% Analysis Date = 03/01/22 Pct Recovery = 96% Analysis Date = 02/25/22 Pct Recovery = 96% Analysis Date = 02/25/22 Pct Recovery = 96% Analysis Date = 02/20/22 Pct Recovery = 96% Analysis Date = 02/20/22 Pct Recovery = 96% Analysis Date = 02/16/22 Pct Recovery = 97% Analysis Date = 02/16/22 Pct Recovery = 97% Analysis Date = 02/12/22 Pct Recovery = 97% Analysis Date = 02/12/22 Pct Recovery = 97% Analysis Date = 02/08/22 Pct Recovery = 97% Analysis Date = 02/08/22 Pct Recovery = 97% Analysis Date = 02/03/22 Pct Recovery = 97% Analysis Date = 02/03/22 Pct Recovery = 97% Analysis Date = 01/30/22 Pct Recovery = 98% Analysis Date = 01/30/22 Pct Recovery = 98% Analysis Date = 01/26/22 Pct Recovery = 98% Analysis Date = 01/26/22 Pct Recovery = 98% Analysis Date = 01/21/22 Pct Recovery = 98% Analysis Date = 01/21/22 Pct Recovery = 98% Analysis Date = 01/17/22 Pct Recovery = 98% Analysis Date = 01/17/22 Pct Recovery = 98% Analysis Date = 01/13/22 Pct Recovery = 99% Analysis Date = 01/13/22 Pct Recovery = 99% Analysis Date = 01/09/22 Pct Recovery = 99% Analysis Date = 01/09/22 Pct Recovery = 99% Analysis Date = 01/04/22 Pct Recovery = 99% Analysis Date = 01/04/22 Pct Recovery = 99% Analysis Date = 12/31/21 Pct Recovery = 99% Analysis Date = 12/31/21 Pct Recovery = 99% Analysis Date = 12/27/21 Pct Recovery = 100% Analysis Date = 12/27/21 Pct Recovery = 100% Analysis Date = 12/23/21 Pct Recovery = 100% Analysis Date = 12/23/21 Pct Recovery = 100% Analysis Date = 12/18/21 Pct Recovery = 100% Analysis Date = 12/18/21 Pct Recovery = 100% Analysis Date = 12/14/21 Pct Recovery = 100% Analysis Date = 12/14/21 Pct Recovery = 100% Analysis Date = 12/10/21 Pct Recovery = 101% Analysis Date = 12/10/21 Pct Recovery = 101% Analysis Date = 12/05/21 Pct Recovery = 101% Analysis Date = 12/05/21 Pct Recovery = 101% Analysis Date = 12/01/21 Pct Recovery = 101% Analysis Date = 12/01/21 Pct Recovery = 101% Analysis Date = 11/27/21 Pct Recovery = 101% Analysis Date = 11/27/21 Pct Recovery = 101% Analysis Date = 11/23/21 Pct Recovery = 102% Analysis Date = 11/23/21 Pct Recovery = 102% Analysis Date = 11/18/21 Pct Recovery = 102% Analysis Date = 11/18/21 Pct Recovery = 102% Analysis Date = 11/14/21 Pct Recovery = 102% Analysis Date = 11/14/21 Pct Recovery = 102% Analysis Date = 11/10/21 Pct Recovery = 102% Analysis Date = 11/10/21 Pct Recovery = 102% Analysis Date = 11/06/21 Pct Recovery = 103% Analysis Date = 11/06/21 Pct Recovery = 103% Analysis Date = 11/01/21 Pct Recovery = 103% Analysis Date = 11/01/21 Pct Recovery = 103% Analysis Date = 10/28/21 Pct Recovery = 103% Analysis Date = 10/28/21 Pct Recovery = 103% Analysis Date = 10/24/21 Pct Recovery = 103% Analysis Date = 10/24/21 Pct Recovery = 103% Analysis Date = 10/19/21 Pct Recovery = 104% Analysis Date = 10/19/21 Pct Recovery = 104% Analysis Date = 10/15/21 Pct Recovery = 104% Analysis Date = 10/15/21 Pct Recovery = 104% Analysis Date = 10/11/21 Pct Recovery = 104% Analysis Date = 10/11/21 Pct Recovery = 104% Analysis Date = 10/07/21 Pct Recovery = 104% Analysis Date = 10/07/21 Pct Recovery = 104% Analysis Date = 10/02/21 Pct Recovery = 105% Analysis Date = 10/02/21 Pct Recovery = 105% Analysis Date = 09/28/21 Pct Recovery = 105% Analysis Date = 09/28/21 Pct Recovery = 105% Analysis Date = 09/24/21 Pct Recovery = 105% Analysis Date = 09/24/21 Pct Recovery = 105% Analysis Date = 09/19/21 Pct Recovery = 105% Analysis Date = 09/19/21 Pct Recovery = 105% Analysis Date = 09/15/21 Pct Recovery = 106% Analysis Date = 09/15/21 Pct Recovery = 106% Analysis Date = 09/11/21 Pct Recovery = 106% Analysis Date = 09/11/21 Pct Recovery = 106% Analysis Date = 09/07/21 Pct Recovery = 106% Analysis Date = 09/07/21 Pct Recovery = 106% Analysis Date = 09/02/21 Pct Recovery = 106% Analysis Date = 09/02/21 Pct Recovery = 106% Analysis Date = 08/29/21 Pct Recovery = 107% Analysis Date = 08/29/21 Pct Recovery = 107% Analysis Date = 08/25/21 Pct Recovery = 107% Analysis Date = 08/25/21 Pct Recovery = 107% Analysis Date = 08/21/21 Pct Recovery = 107% Analysis Date = 08/21/21 Pct Recovery = 107% Analysis Date = 08/16/21 Pct Recovery = 107% Analysis Date = 08/16/21 Pct Recovery = 107% Analysis Date = 08/12/21 Pct Recovery = 108% Analysis Date = 08/12/21 Pct Recovery = 108% Analysis Date = 08/08/21 Pct Recovery = 108% Analysis Date = 08/08/21 Pct Recovery = 108% Analysis Date = 08/03/21 Pct Recovery = 108% Analysis Date = 08/03/21 Pct Recovery = 108% Analysis Date = 07/30/21 Pct Recovery = 108% Analysis Date = 07/30/21 Pct Recovery = 108% Analysis Date = 07/26/21 Pct Recovery = 109% Analysis Date = 07/26/21 Pct Recovery = 109% Analysis Date = 07/22/21 Pct Recovery = 109% Analysis Date = 07/22/21 Pct Recovery = 109% Analysis Date = 07/17/21 Pct Recovery = 109% Analysis Date = 07/17/21 Pct Recovery = 109% Analysis Date = 07/13/21 Pct Recovery = 109% Analysis Date = 07/13/21 Pct Recovery = 109% Analysis Date = 07/09/21 Pct Recovery = 110% Analysis Date = 07/09/21 Pct Recovery = 110% Analysis Date = 07/05/21 Pct Recovery = 110% Analysis Date = 07/05/21 Pct Recovery = 110% Analysis Date = 06/30/21 Pct Recovery = 110% Analysis Date = 06/30/21 Pct Recovery = 110% Analysis Date = 06/26/21 Pct Recovery = 110% Analysis Date = 06/26/21 Pct Recovery = 110% Analysis Date = 06/22/21 Pct Recovery = 111% Analysis Date = 06/22/21 Pct Recovery = 111% Analysis Date = 06/17/21 Pct Recovery = 111% Analysis Date = 06/17/21 Pct Recovery = 111% Analysis Date = 06/13/21 Pct Recovery = 111% Analysis Date = 06/13/21 Pct Recovery = 111% Analysis Date = 06/09/21 Pct Recovery = 111% Analysis Date = 06/09/21 Pct Recovery = 111% Analysis Date = 06/05/21 Pct Recovery = 112% Analysis Date = 06/05/21 Pct Recovery = 112% Analysis Date = 05/31/21 Pct Recovery = 112% Analysis Date = 05/31/21 Pct Recovery = 112% Analysis Date = 05/27/21 Pct Recovery = 112% Analysis Date = 05/27/21 Pct Recovery = 112% Analysis Date = 05/23/21 Pct Recovery = 112% Analysis Date = 05/23/21 Pct Recovery = 112% Analysis Date = 05/19/21 Pct Recovery = 113% Analysis Date = 05/19/21 Pct Recovery = 113% Analysis Date = 05/14/21 Pct Recovery = 113% Analysis Date = 05/14/21 Pct Recovery = 113% Analysis Date = 05/10/21 Pct Recovery = 113% Analysis Date = 05/10/21 Pct Recovery = 113% Analysis Date = 05/06/21 Pct Recovery = 113% Analysis Date = 05/06/21 Pct Recovery = 113% Analysis Date = 05/01/21 Pct Recovery = 114% Analysis Date = 05/01/21 Pct Recovery = 114% Analysis Date = 04/27/21 Pct Recovery = 114% Analysis Date = 04/27/21 Pct Recovery = 114% Analysis Date = 04/23/21 Pct Recovery = 114% Analysis Date = 04/23/21 Pct Recovery = 114% Analysis Date = 04/19/21 Pct Recovery = 114% Analysis Date = 04/19/21 Pct Recovery = 114% Analysis Date = 04/14/21 Pct Recovery = 115% Analysis Date = 04/14/21 Pct Recovery = 115% Analysis Date = 04/10/21 Pct Recovery = 114% Analysis Date = 04/10/21 Pct Recovery = 114% Analysis Date = 04/06/21 Pct Recovery = 114% Analysis Date = 04/06/21 Pct Recovery = 114% Analysis Date = 04/01/21 Pct Recovery = 114% Analysis Date = 04/01/21 Pct Recovery = 114% Analysis Date = 03/28/21 Pct Recovery = 114% Analysis Date = 03/28/21 Pct Recovery = 114% Analysis Date = 03/24/21 Pct Recovery = 114% Analysis Date = 03/24/21 Pct Recovery = 114% Analysis Date = 03/20/21 Pct Recovery = 114% Analysis Date = 03/20/21 Pct Recovery = 114% Analysis Date = 03/15/21 Pct Recovery = 114% Analysis Date = 03/15/21 Pct Recovery = 114% Analysis Date = 03/11/21 Pct Recovery = 113% Analysis Date = 03/11/21 Pct Recovery = 113% Analysis Date = 03/07/21 Pct Recovery = 113% Analysis Date = 03/07/21 Pct Recovery = 113% Analysis Date = 03/03/21 Pct Recovery = 113% Analysis Date = 03/03/21 Pct Recovery = 113% Analysis Date = 02/26/21 Pct Recovery = 113% Analysis Date = 02/26/21 Pct Recovery = 113% Analysis Date = 02/22/21 Pct Recovery = 113% Analysis Date = 02/22/21 Pct Recovery = 113% Analysis Date = 02/18/21 Pct Recovery = 113% Analysis Date = 02/18/21 Pct Recovery = 113% Analysis Date = 02/13/21 Pct Recovery = 113% Analysis Date = 02/13/21 Pct Recovery = 113% Analysis Date = 02/09/21 Pct Recovery = 113% Analysis Date = 02/09/21 Pct Recovery = 113% Analysis Date = 02/05/21 Pct Recovery = 112% Analysis Date = 02/05/21 Pct Recovery = 112% Analysis Date = 02/01/21 Pct Recovery = 112% Analysis Date = 02/01/21 Pct Recovery = 112% Analysis Date = 01/27/21 Pct Recovery = 112% Analysis Date = 01/27/21 Pct Recovery = 112% Analysis Date = 01/23/21 Pct Recovery = 112% Analysis Date = 01/23/21 Pct Recovery = 112% Analysis Date = 01/19/21 Pct Recovery = 112% Analysis Date = 01/19/21 Pct Recovery = 112% Analysis Date = 01/15/21 Pct Recovery = 112% Analysis Date = 01/15/21 Pct Recovery = 112% Analysis Date = 01/10/21 Pct Recovery = 112% Analysis Date = 01/10/21 Pct Recovery = 112% Analysis Date = 01/06/21 Pct Recovery = 111% Analysis Date = 01/06/21 Pct Recovery = 111% Analysis Date = 01/02/21 Pct Recovery = 111% Analysis Date = 01/02/21 Pct Recovery = 111% Analysis Date = 12/28/20 Pct Recovery = 111% Analysis Date = 12/28/20 Pct Recovery = 111% Analysis Date = 12/24/20 Pct Recovery = 111% Analysis Date = 12/24/20 Pct Recovery = 111% Analysis Date = 12/20/20 Pct Recovery = 111% Analysis Date = 12/20/20 Pct Recovery = 111% Analysis Date = 12/16/20 Pct Recovery = 110% Analysis Date = 12/16/20 Pct Recovery = 110% Analysis Date = 12/11/20 Pct Recovery = 110% Analysis Date = 12/11/20 Pct Recovery = 110% Analysis Date = 12/07/20 Pct Recovery = 109% Analysis Date = 12/07/20 Pct Recovery = 109% Analysis Date = 12/03/20 Pct Recovery = 109% Analysis Date = 12/03/20 Pct Recovery = 109% Analysis Date = 11/29/20 Pct Recovery = 109% Analysis Date = 11/29/20 Pct Recovery = 109% Analysis Date = 11/24/20 Pct Recovery = 109% Analysis Date = 11/24/20 Pct Recovery = 109% Analysis Date = 11/20/20 Pct Recovery = 108% Analysis Date = 11/20/20 Pct Recovery = 108% Analysis Date = 11/16/20 Pct Recovery = 108% Analysis Date = 11/16/20 Pct Recovery = 108% Analysis Date = 11/11/20 Pct Recovery = 108% Analysis Date = 11/11/20 Pct Recovery = 108% Analysis Date = 11/07/20 Pct Recovery = 108% Analysis Date = 11/07/20 Pct Recovery = 108% Analysis Date = 11/03/20 Pct Recovery = 108% Analysis Date = 11/03/20 Pct Recovery = 108% Analysis Date = 10/30/20 Pct Recovery = 108% Analysis Date = 10/30/20 Pct Recovery = 108% Analysis Date = 10/25/20 Pct Recovery = 108% Analysis Date = 10/25/20 Pct Recovery = 108% Analysis Date = 10/21/20 Pct Recovery = 108% Analysis Date = 10/21/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 108% Analysis Date = 10/12/20 Pct Recovery = 108% Analysis Date = 10/12/20 Pct Recovery = 108% Analysis Date = 10/08/20 Pct Recovery = 108% Analysis Date = 10/08/20 Pct Recovery = 108% Analysis Date = 10/04/20 Pct Recovery = 108% Analysis Date = 10/04/20 Pct Recovery = 108% Analysis Date = 09/30/20 Pct Recovery = 108% Analysis Date = 09/30/20 Pct Recovery = 108% Analysis Date = 09/25/20 Pct Recovery = 108% Analysis Date = 09/25/20 Pct Recovery = 108% Analysis Date = 09/21/20 Pct Recovery = 108% Analysis Date = 09/21/20 Pct Recovery = 108% Analysis Date = 09/17/20 Pct Recovery = 108% Analysis Date = 09/17/20 Pct Recovery = 108% Analysis Date = 09/13/20 Pct Recovery = 109% Analysis Date = 09/13/20 Pct Recovery = 109% Analysis Date = 09/08/20 Pct Recovery = 109% Analysis Date = 09/08/20 Pct Recovery = 109% Analysis Date = 09/04/20 Pct Recovery = 109% Analysis Date = 09/04/20 Pct Recovery = 109% Analysis Date = 08/31/20 Pct Recovery = 109% Analysis Date = 08/31/20 Pct Recovery = 109% Analysis Date = 08/26/20 Pct Recovery = 109% Analysis Date = 08/26/20 Pct Recovery = 109% Analysis Date = 08/22/20 Pct Recovery = 109% Analysis Date = 08/22/20 Pct Recovery = 109% Analysis Date = 08/18/20 Pct Recovery = 109% Analysis Date = 08/18/20 Pct Recovery = 109% Analysis Date = 08/14/20 Pct Recovery = 109% Analysis Date = 08/14/20 Pct Recovery = 109% Analysis Date = 08/09/20 Pct Recovery = 109% Analysis Date = 08/09/20 Pct Recovery = 109% Analysis Date = 08/05/20 Pct Recovery = 109% Analysis Date = 08/05/20 Pct Recovery = 109% Analysis Date = 08/01/20 Pct Recovery = 109% Analysis Date = 08/01/20 Pct Recovery = 109% Analysis Date = 07/28/20 Pct Recovery = 109% Analysis Date = 07/28/20 Pct Recovery = 109% Analysis Date = 07/23/20 Pct Recovery = 109% Analysis Date = 07/23/20 Pct Recovery = 109% Analysis Date = 07/19/20 Pct Recovery = 109% Analysis Date = 07/19/20 Pct Recovery = 109% Analysis Date = 07/15/20 Pct Recovery = 109% Analysis Date = 07/15/20 Pct Recovery = 109% Analysis Date = 07/10/20 Pct Recovery = 109% Analysis Date = 07/10/20 Pct Recovery = 109% Analysis Date = 07/06/20 Pct Recovery = 109% Analysis Date = 07/06/20 Pct Recovery = 109% Analysis Date = 07/02/20 Pct Recovery = 109% Analysis Date = 07/02/20 Pct Recovery = 109% Analysis Date = 06/28/20 Pct Recovery = 109% Analysis Date = 06/28/20 Pct Recovery = 109% Analysis Date = 06/23/20 Pct Recovery = 109% Analysis Date = 06/23/20 Pct Recovery = 109% Analysis Date = 06/19/20 Pct Recovery = 109% Analysis Date = 06/19/20 Pct Recovery = 109% Analysis Date = 06/15/20 Pct Recovery = 109% Analysis Date = 06/15/20 Pct Recovery = 109% Analysis Date = 06/11/20 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL AMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 17 104% 21% 105% 21%
Total 17 104% 21% 105% 21%

Sample Statistics
FIPRONIL AMIDE

Characteristic N % % Basis
Plotted 17 81% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 21 .  
False Negatives 4 19% 4 out of 21
Not Spiked 95 .  
False Positives 0 0% 0 out of 95

OBSP Determination:
FIPRONIL SULFIDE
METHOD: 2447 , TESTIDCODE: 66610LCM60

Laboratory ID = 20202390020 Lab Value = 51.935 Expected Conc. = 52.6 Report level label = 4.2 Pct Recovery = 99% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20201820155 Lab Value = 47.307 Expected Conc. = 52.4 Report level label = 4.2 Pct Recovery = 90% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 50.491 Expected Conc. = 52.4 Report level label = 4.2 Pct Recovery = 96% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20210760015 Lab Value = 41.439 Expected Conc. = 52.14 Report level label = 4.2 Pct Recovery = 79% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 45.133 Expected Conc. = 52.14 Report level label = 4.2 Pct Recovery = 87% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 51.798 Expected Conc. = 52.14 Report level label = 4.2 Pct Recovery = 99% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 43.874 Expected Conc. = 52.14 Report level label = 4.2 Pct Recovery = 84% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 53.736 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 103% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 54.907 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 105% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 54.622 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 105% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221370164 Lab Value = 26.569 Expected Conc. = 42.32 Report level label = 4.2 Pct Recovery = 63% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 33.167 Expected Conc. = 42 Report level label = 4.2 Pct Recovery = 79% Analysis Date = 08/17/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 40.363 Expected Conc. = 42 Report level label = 4.2 Pct Recovery = 96% Analysis Date = 07/21/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 29.171 Expected Conc. = 42 Report level label = 4.2 Pct Recovery = 69% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20201960104 Lab Value = 24.992 Expected Conc. = 26.3 Report level label = 4.2 Pct Recovery = 95% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20222070177 Lab Value = 17.148 Expected Conc. = 26.25 Report level label = 4.2 Pct Recovery = 65% Analysis Date = 08/02/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20202530029 Lab Value = 19.354 Expected Conc. = 26.2 Report level label = 4.2 Pct Recovery = 74% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 20.135 Expected Conc. = 26.2 Report level label = 4.2 Pct Recovery = 77% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 24.563 Expected Conc. = 26.2 Report level label = 4.2 Pct Recovery = 94% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20210480001 Lab Value = 21.435 Expected Conc. = 26.07 Report level label = 4.2 Pct Recovery = 82% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202880004 Lab Value = 23.215 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 89% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 21.449 Expected Conc. = 20.856 Report level label = 4.2 Pct Recovery = 103% Analysis Date = 04/06/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 18.332 Expected Conc. = 20.84 Report level label = 4.2 Pct Recovery = 88% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 20.323 Expected Conc. = 20.84 Report level label = 4.2 Pct Recovery = 98% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221160208 Lab Value = 6.603 Expected Conc. = 10.58 Report level label = 4.2 Pct Recovery = 62% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20201610160 Lab Value = 10.873 Expected Conc. = 10.52 Report level label = 4.2 Pct Recovery = 103% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20222000207 Lab Value = 7.487 Expected Conc. = 10.5 Report level label = 4.2 Pct Recovery = 71% Analysis Date = 07/26/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20202180001 Lab Value = 9.146 Expected Conc. = 10.48 Report level label = 4.2 Pct Recovery = 87% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 9.532 Expected Conc. = 10.48 Report level label = 4.2 Pct Recovery = 91% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 8.046 Expected Conc. = 10.48 Report level label = 4.2 Pct Recovery = 77% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210690067 Lab Value = 8.864 Expected Conc. = 10.428 Report level label = 4.2 Pct Recovery = 85% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210120050 Lab Value = 9.795 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 94% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 11.559 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 111% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 10.346 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 99% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 9.355 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 90% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 10.934 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 105% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/17/22 Pct Recovery = 72% Analysis Date = 08/12/22 Pct Recovery = 72% Analysis Date = 08/12/22 Pct Recovery = 72% Analysis Date = 08/08/22 Pct Recovery = 72% Analysis Date = 08/08/22 Pct Recovery = 72% Analysis Date = 08/04/22 Pct Recovery = 72% Analysis Date = 08/04/22 Pct Recovery = 72% Analysis Date = 07/31/22 Pct Recovery = 72% Analysis Date = 07/31/22 Pct Recovery = 72% Analysis Date = 07/27/22 Pct Recovery = 72% Analysis Date = 07/27/22 Pct Recovery = 72% Analysis Date = 07/23/22 Pct Recovery = 72% Analysis Date = 07/23/22 Pct Recovery = 72% Analysis Date = 07/19/22 Pct Recovery = 73% Analysis Date = 07/19/22 Pct Recovery = 73% Analysis Date = 07/15/22 Pct Recovery = 73% Analysis Date = 07/15/22 Pct Recovery = 73% Analysis Date = 07/11/22 Pct Recovery = 73% Analysis Date = 07/11/22 Pct Recovery = 73% Analysis Date = 07/07/22 Pct Recovery = 73% Analysis Date = 07/07/22 Pct Recovery = 73% Analysis Date = 07/02/22 Pct Recovery = 73% Analysis Date = 07/02/22 Pct Recovery = 73% Analysis Date = 06/28/22 Pct Recovery = 73% Analysis Date = 06/28/22 Pct Recovery = 73% Analysis Date = 06/24/22 Pct Recovery = 73% Analysis Date = 06/24/22 Pct Recovery = 73% Analysis Date = 06/20/22 Pct Recovery = 73% Analysis Date = 06/20/22 Pct Recovery = 73% Analysis Date = 06/16/22 Pct Recovery = 73% Analysis Date = 06/16/22 Pct Recovery = 73% Analysis Date = 06/12/22 Pct Recovery = 73% Analysis Date = 06/12/22 Pct Recovery = 73% Analysis Date = 06/08/22 Pct Recovery = 74% Analysis Date = 06/08/22 Pct Recovery = 74% Analysis Date = 06/04/22 Pct Recovery = 74% Analysis Date = 06/04/22 Pct Recovery = 74% Analysis Date = 05/31/22 Pct Recovery = 74% Analysis Date = 05/31/22 Pct Recovery = 74% Analysis Date = 05/27/22 Pct Recovery = 74% Analysis Date = 05/27/22 Pct Recovery = 74% Analysis Date = 05/23/22 Pct Recovery = 74% Analysis Date = 05/23/22 Pct Recovery = 74% Analysis Date = 05/18/22 Pct Recovery = 74% Analysis Date = 05/18/22 Pct Recovery = 74% Analysis Date = 05/14/22 Pct Recovery = 74% Analysis Date = 05/14/22 Pct Recovery = 74% Analysis Date = 05/10/22 Pct Recovery = 74% Analysis Date = 05/10/22 Pct Recovery = 74% Analysis Date = 05/06/22 Pct Recovery = 74% Analysis Date = 05/06/22 Pct Recovery = 74% Analysis Date = 05/02/22 Pct Recovery = 75% Analysis Date = 05/02/22 Pct Recovery = 75% Analysis Date = 04/28/22 Pct Recovery = 75% Analysis Date = 04/28/22 Pct Recovery = 75% Analysis Date = 04/24/22 Pct Recovery = 75% Analysis Date = 04/24/22 Pct Recovery = 75% Analysis Date = 04/20/22 Pct Recovery = 75% Analysis Date = 04/20/22 Pct Recovery = 75% Analysis Date = 04/16/22 Pct Recovery = 75% Analysis Date = 04/16/22 Pct Recovery = 75% Analysis Date = 04/12/22 Pct Recovery = 75% Analysis Date = 04/12/22 Pct Recovery = 75% Analysis Date = 04/07/22 Pct Recovery = 75% Analysis Date = 04/07/22 Pct Recovery = 75% Analysis Date = 04/03/22 Pct Recovery = 75% Analysis Date = 04/03/22 Pct Recovery = 75% Analysis Date = 03/30/22 Pct Recovery = 76% Analysis Date = 03/30/22 Pct Recovery = 76% Analysis Date = 03/26/22 Pct Recovery = 76% Analysis Date = 03/26/22 Pct Recovery = 76% Analysis Date = 03/22/22 Pct Recovery = 76% Analysis Date = 03/22/22 Pct Recovery = 76% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/06/22 Pct Recovery = 76% Analysis Date = 03/06/22 Pct Recovery = 76% Analysis Date = 03/02/22 Pct Recovery = 77% Analysis Date = 03/02/22 Pct Recovery = 77% Analysis Date = 02/26/22 Pct Recovery = 77% Analysis Date = 02/26/22 Pct Recovery = 77% Analysis Date = 02/21/22 Pct Recovery = 77% Analysis Date = 02/21/22 Pct Recovery = 77% Analysis Date = 02/17/22 Pct Recovery = 77% Analysis Date = 02/17/22 Pct Recovery = 77% Analysis Date = 02/13/22 Pct Recovery = 77% Analysis Date = 02/13/22 Pct Recovery = 77% Analysis Date = 02/09/22 Pct Recovery = 77% Analysis Date = 02/09/22 Pct Recovery = 77% Analysis Date = 02/05/22 Pct Recovery = 77% Analysis Date = 02/05/22 Pct Recovery = 77% Analysis Date = 02/01/22 Pct Recovery = 78% Analysis Date = 02/01/22 Pct Recovery = 78% Analysis Date = 01/28/22 Pct Recovery = 78% Analysis Date = 01/28/22 Pct Recovery = 78% Analysis Date = 01/24/22 Pct Recovery = 78% Analysis Date = 01/24/22 Pct Recovery = 78% Analysis Date = 01/20/22 Pct Recovery = 78% Analysis Date = 01/20/22 Pct Recovery = 78% Analysis Date = 01/16/22 Pct Recovery = 78% Analysis Date = 01/16/22 Pct Recovery = 78% Analysis Date = 01/11/22 Pct Recovery = 78% Analysis Date = 01/11/22 Pct Recovery = 78% Analysis Date = 01/07/22 Pct Recovery = 78% Analysis Date = 01/07/22 Pct Recovery = 78% Analysis Date = 01/03/22 Pct Recovery = 79% Analysis Date = 01/03/22 Pct Recovery = 79% Analysis Date = 12/30/21 Pct Recovery = 79% Analysis Date = 12/30/21 Pct Recovery = 79% Analysis Date = 12/26/21 Pct Recovery = 79% Analysis Date = 12/26/21 Pct Recovery = 79% Analysis Date = 12/22/21 Pct Recovery = 79% Analysis Date = 12/22/21 Pct Recovery = 79% Analysis Date = 12/18/21 Pct Recovery = 79% Analysis Date = 12/18/21 Pct Recovery = 79% Analysis Date = 12/14/21 Pct Recovery = 79% Analysis Date = 12/14/21 Pct Recovery = 79% Analysis Date = 12/10/21 Pct Recovery = 79% Analysis Date = 12/10/21 Pct Recovery = 79% Analysis Date = 12/06/21 Pct Recovery = 80% Analysis Date = 12/06/21 Pct Recovery = 80% Analysis Date = 12/02/21 Pct Recovery = 80% Analysis Date = 12/02/21 Pct Recovery = 80% Analysis Date = 11/27/21 Pct Recovery = 80% Analysis Date = 11/27/21 Pct Recovery = 80% Analysis Date = 11/23/21 Pct Recovery = 80% Analysis Date = 11/23/21 Pct Recovery = 80% Analysis Date = 11/19/21 Pct Recovery = 80% Analysis Date = 11/19/21 Pct Recovery = 80% Analysis Date = 11/15/21 Pct Recovery = 80% Analysis Date = 11/15/21 Pct Recovery = 80% Analysis Date = 11/11/21 Pct Recovery = 80% Analysis Date = 11/11/21 Pct Recovery = 80% Analysis Date = 11/07/21 Pct Recovery = 81% Analysis Date = 11/07/21 Pct Recovery = 81% Analysis Date = 11/03/21 Pct Recovery = 81% Analysis Date = 11/03/21 Pct Recovery = 81% Analysis Date = 10/30/21 Pct Recovery = 81% Analysis Date = 10/30/21 Pct Recovery = 81% Analysis Date = 10/26/21 Pct Recovery = 81% Analysis Date = 10/26/21 Pct Recovery = 81% Analysis Date = 10/22/21 Pct Recovery = 81% Analysis Date = 10/22/21 Pct Recovery = 81% Analysis Date = 10/17/21 Pct Recovery = 81% Analysis Date = 10/17/21 Pct Recovery = 81% Analysis Date = 10/13/21 Pct Recovery = 81% Analysis Date = 10/13/21 Pct Recovery = 81% Analysis Date = 10/09/21 Pct Recovery = 82% Analysis Date = 10/09/21 Pct Recovery = 82% Analysis Date = 10/05/21 Pct Recovery = 82% Analysis Date = 10/05/21 Pct Recovery = 82% Analysis Date = 10/01/21 Pct Recovery = 82% Analysis Date = 10/01/21 Pct Recovery = 82% Analysis Date = 09/27/21 Pct Recovery = 82% Analysis Date = 09/27/21 Pct Recovery = 82% Analysis Date = 09/23/21 Pct Recovery = 82% Analysis Date = 09/23/21 Pct Recovery = 82% Analysis Date = 09/19/21 Pct Recovery = 82% Analysis Date = 09/19/21 Pct Recovery = 82% Analysis Date = 09/15/21 Pct Recovery = 82% Analysis Date = 09/15/21 Pct Recovery = 82% Analysis Date = 09/11/21 Pct Recovery = 83% Analysis Date = 09/11/21 Pct Recovery = 83% Analysis Date = 09/07/21 Pct Recovery = 83% Analysis Date = 09/07/21 Pct Recovery = 83% Analysis Date = 09/02/21 Pct Recovery = 83% Analysis Date = 09/02/21 Pct Recovery = 83% Analysis Date = 08/29/21 Pct Recovery = 83% Analysis Date = 08/29/21 Pct Recovery = 83% Analysis Date = 08/25/21 Pct Recovery = 83% Analysis Date = 08/25/21 Pct Recovery = 83% Analysis Date = 08/21/21 Pct Recovery = 83% Analysis Date = 08/21/21 Pct Recovery = 83% Analysis Date = 08/17/21 Pct Recovery = 83% Analysis Date = 08/17/21 Pct Recovery = 83% Analysis Date = 08/13/21 Pct Recovery = 84% Analysis Date = 08/13/21 Pct Recovery = 84% Analysis Date = 08/09/21 Pct Recovery = 84% Analysis Date = 08/09/21 Pct Recovery = 84% Analysis Date = 08/05/21 Pct Recovery = 84% Analysis Date = 08/05/21 Pct Recovery = 84% Analysis Date = 08/01/21 Pct Recovery = 84% Analysis Date = 08/01/21 Pct Recovery = 84% Analysis Date = 07/28/21 Pct Recovery = 84% Analysis Date = 07/28/21 Pct Recovery = 84% Analysis Date = 07/23/21 Pct Recovery = 84% Analysis Date = 07/23/21 Pct Recovery = 84% Analysis Date = 07/19/21 Pct Recovery = 84% Analysis Date = 07/19/21 Pct Recovery = 84% Analysis Date = 07/15/21 Pct Recovery = 85% Analysis Date = 07/15/21 Pct Recovery = 85% Analysis Date = 07/11/21 Pct Recovery = 85% Analysis Date = 07/11/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/03/21 Pct Recovery = 85% Analysis Date = 07/03/21 Pct Recovery = 85% Analysis Date = 06/29/21 Pct Recovery = 85% Analysis Date = 06/29/21 Pct Recovery = 85% Analysis Date = 06/25/21 Pct Recovery = 85% Analysis Date = 06/25/21 Pct Recovery = 85% Analysis Date = 06/21/21 Pct Recovery = 85% Analysis Date = 06/21/21 Pct Recovery = 85% Analysis Date = 06/17/21 Pct Recovery = 85% Analysis Date = 06/17/21 Pct Recovery = 85% Analysis Date = 06/13/21 Pct Recovery = 86% Analysis Date = 06/13/21 Pct Recovery = 86% Analysis Date = 06/08/21 Pct Recovery = 86% Analysis Date = 06/08/21 Pct Recovery = 86% Analysis Date = 06/04/21 Pct Recovery = 86% Analysis Date = 06/04/21 Pct Recovery = 86% Analysis Date = 05/31/21 Pct Recovery = 86% Analysis Date = 05/31/21 Pct Recovery = 86% Analysis Date = 05/27/21 Pct Recovery = 86% Analysis Date = 05/27/21 Pct Recovery = 86% Analysis Date = 05/23/21 Pct Recovery = 86% Analysis Date = 05/23/21 Pct Recovery = 86% Analysis Date = 05/19/21 Pct Recovery = 86% Analysis Date = 05/19/21 Pct Recovery = 86% Analysis Date = 05/15/21 Pct Recovery = 87% Analysis Date = 05/15/21 Pct Recovery = 87% Analysis Date = 05/11/21 Pct Recovery = 87% Analysis Date = 05/11/21 Pct Recovery = 87% Analysis Date = 05/07/21 Pct Recovery = 87% Analysis Date = 05/07/21 Pct Recovery = 87% Analysis Date = 05/03/21 Pct Recovery = 87% Analysis Date = 05/03/21 Pct Recovery = 87% Analysis Date = 04/28/21 Pct Recovery = 87% Analysis Date = 04/28/21 Pct Recovery = 87% Analysis Date = 04/24/21 Pct Recovery = 87% Analysis Date = 04/24/21 Pct Recovery = 87% Analysis Date = 04/20/21 Pct Recovery = 87% Analysis Date = 04/20/21 Pct Recovery = 87% Analysis Date = 04/16/21 Pct Recovery = 88% Analysis Date = 04/16/21 Pct Recovery = 88% Analysis Date = 04/12/21 Pct Recovery = 88% Analysis Date = 04/12/21 Pct Recovery = 88% Analysis Date = 04/08/21 Pct Recovery = 88% Analysis Date = 04/08/21 Pct Recovery = 88% Analysis Date = 04/04/21 Pct Recovery = 88% Analysis Date = 04/04/21 Pct Recovery = 88% Analysis Date = 03/31/21 Pct Recovery = 88% Analysis Date = 03/31/21 Pct Recovery = 88% Analysis Date = 03/27/21 Pct Recovery = 88% Analysis Date = 03/27/21 Pct Recovery = 88% Analysis Date = 03/23/21 Pct Recovery = 88% Analysis Date = 03/23/21 Pct Recovery = 88% Analysis Date = 03/19/21 Pct Recovery = 89% Analysis Date = 03/19/21 Pct Recovery = 89% Analysis Date = 03/14/21 Pct Recovery = 89% Analysis Date = 03/14/21 Pct Recovery = 89% Analysis Date = 03/10/21 Pct Recovery = 89% Analysis Date = 03/10/21 Pct Recovery = 89% Analysis Date = 03/06/21 Pct Recovery = 89% Analysis Date = 03/06/21 Pct Recovery = 89% Analysis Date = 03/02/21 Pct Recovery = 90% Analysis Date = 03/02/21 Pct Recovery = 90% Analysis Date = 02/26/21 Pct Recovery = 90% Analysis Date = 02/26/21 Pct Recovery = 90% Analysis Date = 02/22/21 Pct Recovery = 90% Analysis Date = 02/22/21 Pct Recovery = 90% Analysis Date = 02/18/21 Pct Recovery = 90% Analysis Date = 02/18/21 Pct Recovery = 90% Analysis Date = 02/14/21 Pct Recovery = 91% Analysis Date = 02/14/21 Pct Recovery = 91% Analysis Date = 02/10/21 Pct Recovery = 91% Analysis Date = 02/10/21 Pct Recovery = 91% Analysis Date = 02/06/21 Pct Recovery = 91% Analysis Date = 02/06/21 Pct Recovery = 91% Analysis Date = 02/01/21 Pct Recovery = 92% Analysis Date = 02/01/21 Pct Recovery = 92% Analysis Date = 01/28/21 Pct Recovery = 92% Analysis Date = 01/28/21 Pct Recovery = 92% Analysis Date = 01/24/21 Pct Recovery = 92% Analysis Date = 01/24/21 Pct Recovery = 92% Analysis Date = 01/20/21 Pct Recovery = 92% Analysis Date = 01/20/21 Pct Recovery = 92% Analysis Date = 01/16/21 Pct Recovery = 93% Analysis Date = 01/16/21 Pct Recovery = 93% Analysis Date = 01/12/21 Pct Recovery = 93% Analysis Date = 01/12/21 Pct Recovery = 93% Analysis Date = 01/08/21 Pct Recovery = 93% Analysis Date = 01/08/21 Pct Recovery = 93% Analysis Date = 01/04/21 Pct Recovery = 93% Analysis Date = 01/04/21 Pct Recovery = 93% Analysis Date = 12/31/20 Pct Recovery = 94% Analysis Date = 12/31/20 Pct Recovery = 94% Analysis Date = 12/27/20 Pct Recovery = 94% Analysis Date = 12/27/20 Pct Recovery = 94% Analysis Date = 12/23/20 Pct Recovery = 94% Analysis Date = 12/23/20 Pct Recovery = 94% Analysis Date = 12/18/20 Pct Recovery = 95% Analysis Date = 12/18/20 Pct Recovery = 95% Analysis Date = 12/14/20 Pct Recovery = 95% Analysis Date = 12/14/20 Pct Recovery = 95% Analysis Date = 12/10/20 Pct Recovery = 95% Analysis Date = 12/10/20 Pct Recovery = 95% Analysis Date = 12/06/20 Pct Recovery = 95% Analysis Date = 12/06/20 Pct Recovery = 95% Analysis Date = 12/02/20 Pct Recovery = 95% Analysis Date = 12/02/20 Pct Recovery = 95% Analysis Date = 11/28/20 Pct Recovery = 95% Analysis Date = 11/28/20 Pct Recovery = 95% Analysis Date = 11/24/20 Pct Recovery = 95% Analysis Date = 11/24/20 Pct Recovery = 95% Analysis Date = 11/20/20 Pct Recovery = 95% Analysis Date = 11/20/20 Pct Recovery = 95% Analysis Date = 11/16/20 Pct Recovery = 95% Analysis Date = 11/16/20 Pct Recovery = 95% Analysis Date = 11/12/20 Pct Recovery = 95% Analysis Date = 11/12/20 Pct Recovery = 95% Analysis Date = 11/07/20 Pct Recovery = 95% Analysis Date = 11/07/20 Pct Recovery = 95% Analysis Date = 11/03/20 Pct Recovery = 95% Analysis Date = 11/03/20 Pct Recovery = 95% Analysis Date = 10/30/20 Pct Recovery = 95% Analysis Date = 10/30/20 Pct Recovery = 95% Analysis Date = 10/26/20 Pct Recovery = 95% Analysis Date = 10/26/20 Pct Recovery = 95% Analysis Date = 10/22/20 Pct Recovery = 95% Analysis Date = 10/22/20 Pct Recovery = 95% Analysis Date = 10/18/20 Pct Recovery = 95% Analysis Date = 10/18/20 Pct Recovery = 95% Analysis Date = 10/14/20 Pct Recovery = 95% Analysis Date = 10/14/20 Pct Recovery = 95% Analysis Date = 10/10/20 Pct Recovery = 94% Analysis Date = 10/10/20 Pct Recovery = 94% Analysis Date = 10/06/20 Pct Recovery = 94% Analysis Date = 10/06/20 Pct Recovery = 94% Analysis Date = 10/02/20 Pct Recovery = 94% Analysis Date = 10/02/20 Pct Recovery = 94% Analysis Date = 09/28/20 Pct Recovery = 93% Analysis Date = 09/28/20 Pct Recovery = 93% Analysis Date = 09/23/20 Pct Recovery = 93% Analysis Date = 09/23/20 Pct Recovery = 93% Analysis Date = 09/19/20 Pct Recovery = 93% Analysis Date = 09/19/20 Pct Recovery = 93% Analysis Date = 09/15/20 Pct Recovery = 93% Analysis Date = 09/15/20 Pct Recovery = 93% Analysis Date = 09/11/20 Pct Recovery = 93% Analysis Date = 09/11/20 Pct Recovery = 93% Analysis Date = 09/07/20 Pct Recovery = 93% Analysis Date = 09/07/20 Pct Recovery = 93% Analysis Date = 09/03/20 Pct Recovery = 92% Analysis Date = 09/03/20 Pct Recovery = 92% Analysis Date = 08/30/20 Pct Recovery = 92% Analysis Date = 08/30/20 Pct Recovery = 92% Analysis Date = 08/26/20 Pct Recovery = 92% Analysis Date = 08/26/20 Pct Recovery = 92% Analysis Date = 08/22/20 Pct Recovery = 92% Analysis Date = 08/22/20 Pct Recovery = 92% Analysis Date = 08/18/20 Pct Recovery = 92% Analysis Date = 08/18/20 Pct Recovery = 92% Analysis Date = 08/13/20 Pct Recovery = 92% Analysis Date = 08/13/20 Pct Recovery = 92% Analysis Date = 08/09/20 Pct Recovery = 92% Analysis Date = 08/09/20 Pct Recovery = 92% Analysis Date = 08/05/20 Pct Recovery = 92% Analysis Date = 08/05/20 Pct Recovery = 92% Analysis Date = 08/01/20 Pct Recovery = 92% Analysis Date = 08/01/20 Pct Recovery = 92% Analysis Date = 07/28/20 Pct Recovery = 92% Analysis Date = 07/28/20 Pct Recovery = 92% Analysis Date = 07/24/20 Pct Recovery = 92% Analysis Date = 07/24/20 Pct Recovery = 92% Analysis Date = 07/20/20 Pct Recovery = 92% Analysis Date = 07/20/20 Pct Recovery = 92% Analysis Date = 07/16/20 Pct Recovery = 92% Analysis Date = 07/16/20 Pct Recovery = 92% Analysis Date = 07/12/20 Pct Recovery = 92% Analysis Date = 07/12/20 Pct Recovery = 92% Analysis Date = 07/08/20 Pct Recovery = 92% Analysis Date = 07/08/20 Pct Recovery = 92% Analysis Date = 07/04/20 Pct Recovery = 92% Analysis Date = 07/04/20 Pct Recovery = 92% Analysis Date = 06/29/20 Pct Recovery = 92% Analysis Date = 06/29/20 Pct Recovery = 92% Analysis Date = 06/25/20 Pct Recovery = 92% Analysis Date = 06/25/20 Pct Recovery = 92% Analysis Date = 06/21/20 Pct Recovery = 92% Analysis Date = 06/21/20 Pct Recovery = 92% Analysis Date = 06/17/20 Pct Recovery = 92% Analysis Date = 06/17/20 Pct Recovery = 92% Analysis Date = 06/13/20 Pct Recovery = 92% Analysis Date = 06/13/20 Pct Recovery = 92% Analysis Date = 06/09/20 Pct Recovery = 92% Analysis Date = 06/09/20 Pct Recovery = 92% Analysis Date = 06/05/20 Pct Recovery = 92% Analysis Date = 06/05/20 Pct Recovery = 92% Analysis Date = 06/01/20 Pct Recovery = 92% Analysis Date = 06/01/20 Pct Recovery = 92% Analysis Date = 05/28/20 Pct Recovery = 92% Analysis Date = 05/28/20 Pct Recovery = 92% Analysis Date = 05/24/20 Pct Recovery = 92% Analysis Date = 05/24/20 Pct Recovery = 92% Analysis Date = 05/20/20 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 89% 13% 90% 15%
Total 36 89% 13% 90% 15%

Sample Statistics
FIPRONIL SULFIDE

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 80 .  
False Positives 2 3% 2 out of 80

OBSP Determination:
FIPRONIL SULFONE
METHOD: 2447 , TESTIDCODE: 66613LCM60

Laboratory ID = 20202110006 Lab Value = 60.904 Expected Conc. = 71.1 Report level label = 5.6 Pct Recovery = 86% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203230021 Lab Value = 69.497 Expected Conc. = 70.73 Report level label = 5.6 Pct Recovery = 98% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 71.311 Expected Conc. = 70.73 Report level label = 5.6 Pct Recovery = 101% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590107 Lab Value = 68.814 Expected Conc. = 70.4 Report level label = 5.6 Pct Recovery = 98% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 69.854 Expected Conc. = 70.4 Report level label = 5.6 Pct Recovery = 99% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221370164 Lab Value = 32.773 Expected Conc. = 56.08 Report level label = 5.6 Pct Recovery = 58% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 48.703 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 87% Analysis Date = 08/17/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 46.415 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 83% Analysis Date = 07/21/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 39.830 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 71% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20201680155 Lab Value = 34.428 Expected Conc. = 35.55 Report level label = 5.6 Pct Recovery = 97% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20203360042 Lab Value = 29.540 Expected Conc. = 35.2 Report level label = 5.6 Pct Recovery = 84% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 33.358 Expected Conc. = 35.2 Report level label = 5.6 Pct Recovery = 95% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 28.526 Expected Conc. = 35.2 Report level label = 5.6 Pct Recovery = 81% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222070177 Lab Value = 19.154 Expected Conc. = 35 Report level label = 5.6 Pct Recovery = 55% Analysis Date = 08/02/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20201610160 Lab Value = 12.776 Expected Conc. = 14.22 Report level label = 5.6 Pct Recovery = 90% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210830019 Lab Value = 11.490 Expected Conc. = 14.146 Report level label = 5.6 Pct Recovery = 81% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 12.897 Expected Conc. = 14.146 Report level label = 5.6 Pct Recovery = 91% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 13.249 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 94% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 12.809 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 91% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 13.182 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 94% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 12.308 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 87% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 12.126 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 86% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 13.229 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 94% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221160208 Lab Value = 7.896 Expected Conc. = 14.02 Report level label = 5.6 Pct Recovery = 56% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222000207 Lab Value = 10.393 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 74% Analysis Date = 07/26/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Analysis Date = 08/17/22 Pct Recovery = 70% Analysis Date = 08/13/22 Pct Recovery = 70% Analysis Date = 08/13/22 Pct Recovery = 70% Analysis Date = 08/09/22 Pct Recovery = 70% Analysis Date = 08/09/22 Pct Recovery = 70% Analysis Date = 08/05/22 Pct Recovery = 70% Analysis Date = 08/05/22 Pct Recovery = 70% Analysis Date = 08/01/22 Pct Recovery = 70% Analysis Date = 08/01/22 Pct Recovery = 70% Analysis Date = 07/28/22 Pct Recovery = 70% Analysis Date = 07/28/22 Pct Recovery = 70% Analysis Date = 07/24/22 Pct Recovery = 70% Analysis Date = 07/24/22 Pct Recovery = 70% Analysis Date = 07/20/22 Pct Recovery = 70% Analysis Date = 07/20/22 Pct Recovery = 70% Analysis Date = 07/16/22 Pct Recovery = 70% Analysis Date = 07/16/22 Pct Recovery = 70% Analysis Date = 07/12/22 Pct Recovery = 70% Analysis Date = 07/12/22 Pct Recovery = 70% Analysis Date = 07/08/22 Pct Recovery = 70% Analysis Date = 07/08/22 Pct Recovery = 70% Analysis Date = 07/04/22 Pct Recovery = 70% Analysis Date = 07/04/22 Pct Recovery = 70% Analysis Date = 06/30/22 Pct Recovery = 70% Analysis Date = 06/30/22 Pct Recovery = 70% Analysis Date = 06/26/22 Pct Recovery = 70% Analysis Date = 06/26/22 Pct Recovery = 70% Analysis Date = 06/22/22 Pct Recovery = 70% Analysis Date = 06/22/22 Pct Recovery = 70% Analysis Date = 06/18/22 Pct Recovery = 70% Analysis Date = 06/18/22 Pct Recovery = 70% Analysis Date = 06/14/22 Pct Recovery = 70% Analysis Date = 06/14/22 Pct Recovery = 70% Analysis Date = 06/10/22 Pct Recovery = 70% Analysis Date = 06/10/22 Pct Recovery = 70% Analysis Date = 06/06/22 Pct Recovery = 70% Analysis Date = 06/06/22 Pct Recovery = 70% Analysis Date = 06/02/22 Pct Recovery = 70% Analysis Date = 06/02/22 Pct Recovery = 70% Analysis Date = 05/29/22 Pct Recovery = 70% Analysis Date = 05/29/22 Pct Recovery = 70% Analysis Date = 05/25/22 Pct Recovery = 71% Analysis Date = 05/25/22 Pct Recovery = 71% Analysis Date = 05/21/22 Pct Recovery = 71% Analysis Date = 05/21/22 Pct Recovery = 71% Analysis Date = 05/17/22 Pct Recovery = 71% Analysis Date = 05/17/22 Pct Recovery = 71% Analysis Date = 05/13/22 Pct Recovery = 71% Analysis Date = 05/13/22 Pct Recovery = 71% Analysis Date = 05/09/22 Pct Recovery = 71% Analysis Date = 05/09/22 Pct Recovery = 71% Analysis Date = 05/05/22 Pct Recovery = 71% Analysis Date = 05/05/22 Pct Recovery = 71% Analysis Date = 05/01/22 Pct Recovery = 71% Analysis Date = 05/01/22 Pct Recovery = 71% Analysis Date = 04/27/22 Pct Recovery = 71% Analysis Date = 04/27/22 Pct Recovery = 71% Analysis Date = 04/23/22 Pct Recovery = 71% Analysis Date = 04/23/22 Pct Recovery = 71% Analysis Date = 04/19/22 Pct Recovery = 71% Analysis Date = 04/19/22 Pct Recovery = 71% Analysis Date = 04/15/22 Pct Recovery = 72% Analysis Date = 04/15/22 Pct Recovery = 72% Analysis Date = 04/11/22 Pct Recovery = 72% Analysis Date = 04/11/22 Pct Recovery = 72% Analysis Date = 04/07/22 Pct Recovery = 72% Analysis Date = 04/07/22 Pct Recovery = 72% Analysis Date = 04/03/22 Pct Recovery = 72% Analysis Date = 04/03/22 Pct Recovery = 72% Analysis Date = 03/30/22 Pct Recovery = 72% Analysis Date = 03/30/22 Pct Recovery = 72% Analysis Date = 03/26/22 Pct Recovery = 72% Analysis Date = 03/26/22 Pct Recovery = 72% Analysis Date = 03/22/22 Pct Recovery = 73% Analysis Date = 03/22/22 Pct Recovery = 73% Analysis Date = 03/18/22 Pct Recovery = 73% Analysis Date = 03/18/22 Pct Recovery = 73% Analysis Date = 03/14/22 Pct Recovery = 73% Analysis Date = 03/14/22 Pct Recovery = 73% Analysis Date = 03/10/22 Pct Recovery = 73% Analysis Date = 03/10/22 Pct Recovery = 73% Analysis Date = 03/06/22 Pct Recovery = 73% Analysis Date = 03/06/22 Pct Recovery = 73% Analysis Date = 03/02/22 Pct Recovery = 74% Analysis Date = 03/02/22 Pct Recovery = 74% Analysis Date = 02/26/22 Pct Recovery = 74% Analysis Date = 02/26/22 Pct Recovery = 74% Analysis Date = 02/22/22 Pct Recovery = 74% Analysis Date = 02/22/22 Pct Recovery = 74% Analysis Date = 02/18/22 Pct Recovery = 74% Analysis Date = 02/18/22 Pct Recovery = 74% Analysis Date = 02/14/22 Pct Recovery = 74% Analysis Date = 02/14/22 Pct Recovery = 74% Analysis Date = 02/10/22 Pct Recovery = 74% Analysis Date = 02/10/22 Pct Recovery = 74% Analysis Date = 02/06/22 Pct Recovery = 75% Analysis Date = 02/06/22 Pct Recovery = 75% Analysis Date = 02/02/22 Pct Recovery = 75% Analysis Date = 02/02/22 Pct Recovery = 75% Analysis Date = 01/29/22 Pct Recovery = 75% Analysis Date = 01/29/22 Pct Recovery = 75% Analysis Date = 01/25/22 Pct Recovery = 75% Analysis Date = 01/25/22 Pct Recovery = 75% Analysis Date = 01/21/22 Pct Recovery = 75% Analysis Date = 01/21/22 Pct Recovery = 75% Analysis Date = 01/17/22 Pct Recovery = 75% Analysis Date = 01/17/22 Pct Recovery = 75% Analysis Date = 01/13/22 Pct Recovery = 76% Analysis Date = 01/13/22 Pct Recovery = 76% Analysis Date = 01/09/22 Pct Recovery = 76% Analysis Date = 01/09/22 Pct Recovery = 76% Analysis Date = 01/05/22 Pct Recovery = 76% Analysis Date = 01/05/22 Pct Recovery = 76% Analysis Date = 01/01/22 Pct Recovery = 76% Analysis Date = 01/01/22 Pct Recovery = 76% Analysis Date = 12/28/21 Pct Recovery = 76% Analysis Date = 12/28/21 Pct Recovery = 76% Analysis Date = 12/24/21 Pct Recovery = 76% Analysis Date = 12/24/21 Pct Recovery = 76% Analysis Date = 12/20/21 Pct Recovery = 77% Analysis Date = 12/20/21 Pct Recovery = 77% Analysis Date = 12/16/21 Pct Recovery = 77% Analysis Date = 12/16/21 Pct Recovery = 77% Analysis Date = 12/12/21 Pct Recovery = 77% Analysis Date = 12/12/21 Pct Recovery = 77% Analysis Date = 12/08/21 Pct Recovery = 77% Analysis Date = 12/08/21 Pct Recovery = 77% Analysis Date = 12/04/21 Pct Recovery = 77% Analysis Date = 12/04/21 Pct Recovery = 77% Analysis Date = 11/30/21 Pct Recovery = 78% Analysis Date = 11/30/21 Pct Recovery = 78% Analysis Date = 11/26/21 Pct Recovery = 78% Analysis Date = 11/26/21 Pct Recovery = 78% Analysis Date = 11/23/21 Pct Recovery = 78% Analysis Date = 11/23/21 Pct Recovery = 78% Analysis Date = 11/19/21 Pct Recovery = 78% Analysis Date = 11/19/21 Pct Recovery = 78% Analysis Date = 11/15/21 Pct Recovery = 78% Analysis Date = 11/15/21 Pct Recovery = 78% Analysis Date = 11/11/21 Pct Recovery = 78% Analysis Date = 11/11/21 Pct Recovery = 78% Analysis Date = 11/07/21 Pct Recovery = 79% Analysis Date = 11/07/21 Pct Recovery = 79% Analysis Date = 11/03/21 Pct Recovery = 79% Analysis Date = 11/03/21 Pct Recovery = 79% Analysis Date = 10/30/21 Pct Recovery = 79% Analysis Date = 10/30/21 Pct Recovery = 79% Analysis Date = 10/26/21 Pct Recovery = 79% Analysis Date = 10/26/21 Pct Recovery = 79% Analysis Date = 10/22/21 Pct Recovery = 79% Analysis Date = 10/22/21 Pct Recovery = 79% Analysis Date = 10/18/21 Pct Recovery = 79% Analysis Date = 10/18/21 Pct Recovery = 79% Analysis Date = 10/14/21 Pct Recovery = 80% Analysis Date = 10/14/21 Pct Recovery = 80% Analysis Date = 10/10/21 Pct Recovery = 80% Analysis Date = 10/10/21 Pct Recovery = 80% Analysis Date = 10/06/21 Pct Recovery = 80% Analysis Date = 10/06/21 Pct Recovery = 80% Analysis Date = 10/02/21 Pct Recovery = 80% Analysis Date = 10/02/21 Pct Recovery = 80% Analysis Date = 09/28/21 Pct Recovery = 80% Analysis Date = 09/28/21 Pct Recovery = 80% Analysis Date = 09/24/21 Pct Recovery = 80% Analysis Date = 09/24/21 Pct Recovery = 80% Analysis Date = 09/20/21 Pct Recovery = 81% Analysis Date = 09/20/21 Pct Recovery = 81% Analysis Date = 09/16/21 Pct Recovery = 81% Analysis Date = 09/16/21 Pct Recovery = 81% Analysis Date = 09/12/21 Pct Recovery = 81% Analysis Date = 09/12/21 Pct Recovery = 81% Analysis Date = 09/08/21 Pct Recovery = 81% Analysis Date = 09/08/21 Pct Recovery = 81% Analysis Date = 09/04/21 Pct Recovery = 81% Analysis Date = 09/04/21 Pct Recovery = 81% Analysis Date = 08/31/21 Pct Recovery = 82% Analysis Date = 08/31/21 Pct Recovery = 82% Analysis Date = 08/27/21 Pct Recovery = 82% Analysis Date = 08/27/21 Pct Recovery = 82% Analysis Date = 08/23/21 Pct Recovery = 82% Analysis Date = 08/23/21 Pct Recovery = 82% Analysis Date = 08/19/21 Pct Recovery = 82% Analysis Date = 08/19/21 Pct Recovery = 82% Analysis Date = 08/15/21 Pct Recovery = 82% Analysis Date = 08/15/21 Pct Recovery = 82% Analysis Date = 08/11/21 Pct Recovery = 82% Analysis Date = 08/11/21 Pct Recovery = 82% Analysis Date = 08/07/21 Pct Recovery = 83% Analysis Date = 08/07/21 Pct Recovery = 83% Analysis Date = 08/03/21 Pct Recovery = 83% Analysis Date = 08/03/21 Pct Recovery = 83% Analysis Date = 07/30/21 Pct Recovery = 83% Analysis Date = 07/30/21 Pct Recovery = 83% Analysis Date = 07/26/21 Pct Recovery = 83% Analysis Date = 07/26/21 Pct Recovery = 83% Analysis Date = 07/22/21 Pct Recovery = 83% Analysis Date = 07/22/21 Pct Recovery = 83% Analysis Date = 07/18/21 Pct Recovery = 83% Analysis Date = 07/18/21 Pct Recovery = 83% Analysis Date = 07/14/21 Pct Recovery = 84% Analysis Date = 07/14/21 Pct Recovery = 84% Analysis Date = 07/10/21 Pct Recovery = 84% Analysis Date = 07/10/21 Pct Recovery = 84% Analysis Date = 07/06/21 Pct Recovery = 84% Analysis Date = 07/06/21 Pct Recovery = 84% Analysis Date = 07/02/21 Pct Recovery = 84% Analysis Date = 07/02/21 Pct Recovery = 84% Analysis Date = 06/28/21 Pct Recovery = 84% Analysis Date = 06/28/21 Pct Recovery = 84% Analysis Date = 06/24/21 Pct Recovery = 84% Analysis Date = 06/24/21 Pct Recovery = 84% Analysis Date = 06/20/21 Pct Recovery = 85% Analysis Date = 06/20/21 Pct Recovery = 85% Analysis Date = 06/16/21 Pct Recovery = 85% Analysis Date = 06/16/21 Pct Recovery = 85% Analysis Date = 06/12/21 Pct Recovery = 85% Analysis Date = 06/12/21 Pct Recovery = 85% Analysis Date = 06/08/21 Pct Recovery = 85% Analysis Date = 06/08/21 Pct Recovery = 85% Analysis Date = 06/04/21 Pct Recovery = 85% Analysis Date = 06/04/21 Pct Recovery = 85% Analysis Date = 05/31/21 Pct Recovery = 86% Analysis Date = 05/31/21 Pct Recovery = 86% Analysis Date = 05/27/21 Pct Recovery = 86% Analysis Date = 05/27/21 Pct Recovery = 86% Analysis Date = 05/23/21 Pct Recovery = 86% Analysis Date = 05/23/21 Pct Recovery = 86% Analysis Date = 05/19/21 Pct Recovery = 86% Analysis Date = 05/19/21 Pct Recovery = 86% Analysis Date = 05/15/21 Pct Recovery = 86% Analysis Date = 05/15/21 Pct Recovery = 86% Analysis Date = 05/11/21 Pct Recovery = 86% Analysis Date = 05/11/21 Pct Recovery = 86% Analysis Date = 05/07/21 Pct Recovery = 87% Analysis Date = 05/07/21 Pct Recovery = 87% Analysis Date = 05/03/21 Pct Recovery = 87% Analysis Date = 05/03/21 Pct Recovery = 87% Analysis Date = 04/29/21 Pct Recovery = 87% Analysis Date = 04/29/21 Pct Recovery = 87% Analysis Date = 04/25/21 Pct Recovery = 87% Analysis Date = 04/25/21 Pct Recovery = 87% Analysis Date = 04/21/21 Pct Recovery = 87% Analysis Date = 04/21/21 Pct Recovery = 87% Analysis Date = 04/17/21 Pct Recovery = 87% Analysis Date = 04/17/21 Pct Recovery = 87% Analysis Date = 04/13/21 Pct Recovery = 88% Analysis Date = 04/13/21 Pct Recovery = 88% Analysis Date = 04/09/21 Pct Recovery = 88% Analysis Date = 04/09/21 Pct Recovery = 88% Analysis Date = 04/05/21 Pct Recovery = 88% Analysis Date = 04/05/21 Pct Recovery = 88% Analysis Date = 04/01/21 Pct Recovery = 88% Analysis Date = 04/01/21 Pct Recovery = 88% Analysis Date = 03/28/21 Pct Recovery = 88% Analysis Date = 03/28/21 Pct Recovery = 88% Analysis Date = 03/24/21 Pct Recovery = 88% Analysis Date = 03/24/21 Pct Recovery = 88% Analysis Date = 03/20/21 Pct Recovery = 89% Analysis Date = 03/20/21 Pct Recovery = 89% Analysis Date = 03/16/21 Pct Recovery = 89% Analysis Date = 03/16/21 Pct Recovery = 89% Analysis Date = 03/12/21 Pct Recovery = 89% Analysis Date = 03/12/21 Pct Recovery = 89% Analysis Date = 03/08/21 Pct Recovery = 89% Analysis Date = 03/08/21 Pct Recovery = 89% Analysis Date = 03/04/21 Pct Recovery = 89% Analysis Date = 03/04/21 Pct Recovery = 89% Analysis Date = 03/01/21 Pct Recovery = 90% Analysis Date = 03/01/21 Pct Recovery = 90% Analysis Date = 02/25/21 Pct Recovery = 90% Analysis Date = 02/25/21 Pct Recovery = 90% Analysis Date = 02/21/21 Pct Recovery = 90% Analysis Date = 02/21/21 Pct Recovery = 90% Analysis Date = 02/17/21 Pct Recovery = 90% Analysis Date = 02/17/21 Pct Recovery = 90% Analysis Date = 02/13/21 Pct Recovery = 90% Analysis Date = 02/13/21 Pct Recovery = 90% Analysis Date = 02/09/21 Pct Recovery = 90% Analysis Date = 02/09/21 Pct Recovery = 90% Analysis Date = 02/05/21 Pct Recovery = 90% Analysis Date = 02/05/21 Pct Recovery = 90% Analysis Date = 02/01/21 Pct Recovery = 91% Analysis Date = 02/01/21 Pct Recovery = 91% Analysis Date = 01/28/21 Pct Recovery = 91% Analysis Date = 01/28/21 Pct Recovery = 91% Analysis Date = 01/24/21 Pct Recovery = 91% Analysis Date = 01/24/21 Pct Recovery = 91% Analysis Date = 01/20/21 Pct Recovery = 91% Analysis Date = 01/20/21 Pct Recovery = 91% Analysis Date = 01/16/21 Pct Recovery = 91% Analysis Date = 01/16/21 Pct Recovery = 91% Analysis Date = 01/12/21 Pct Recovery = 91% Analysis Date = 01/12/21 Pct Recovery = 91% Analysis Date = 01/08/21 Pct Recovery = 91% Analysis Date = 01/08/21 Pct Recovery = 91% Analysis Date = 01/04/21 Pct Recovery = 91% Analysis Date = 01/04/21 Pct Recovery = 91% Analysis Date = 12/31/20 Pct Recovery = 91% Analysis Date = 12/31/20 Pct Recovery = 91% Analysis Date = 12/27/20 Pct Recovery = 91% Analysis Date = 12/27/20 Pct Recovery = 91% Analysis Date = 12/23/20 Pct Recovery = 92% Analysis Date = 12/23/20 Pct Recovery = 92% Analysis Date = 12/19/20 Pct Recovery = 92% Analysis Date = 12/19/20 Pct Recovery = 92% Analysis Date = 12/15/20 Pct Recovery = 92% Analysis Date = 12/15/20 Pct Recovery = 92% Analysis Date = 12/11/20 Pct Recovery = 92% Analysis Date = 12/11/20 Pct Recovery = 92% Analysis Date = 12/07/20 Pct Recovery = 92% Analysis Date = 12/07/20 Pct Recovery = 92% Analysis Date = 12/03/20 Pct Recovery = 92% Analysis Date = 12/03/20 Pct Recovery = 92% Analysis Date = 11/29/20 Pct Recovery = 92% Analysis Date = 11/29/20 Pct Recovery = 92% Analysis Date = 11/25/20 Pct Recovery = 92% Analysis Date = 11/25/20 Pct Recovery = 92% Analysis Date = 11/21/20 Pct Recovery = 92% Analysis Date = 11/21/20 Pct Recovery = 92% Analysis Date = 11/17/20 Pct Recovery = 92% Analysis Date = 11/17/20 Pct Recovery = 92% Analysis Date = 11/13/20 Pct Recovery = 92% Analysis Date = 11/13/20 Pct Recovery = 92% Analysis Date = 11/09/20 Pct Recovery = 92% Analysis Date = 11/09/20 Pct Recovery = 92% Analysis Date = 11/05/20 Pct Recovery = 92% Analysis Date = 11/05/20 Pct Recovery = 92% Analysis Date = 11/01/20 Pct Recovery = 92% Analysis Date = 11/01/20 Pct Recovery = 92% Analysis Date = 10/28/20 Pct Recovery = 92% Analysis Date = 10/28/20 Pct Recovery = 92% Analysis Date = 10/24/20 Pct Recovery = 92% Analysis Date = 10/24/20 Pct Recovery = 92% Analysis Date = 10/20/20 Pct Recovery = 92% Analysis Date = 10/20/20 Pct Recovery = 92% Analysis Date = 10/16/20 Pct Recovery = 92% Analysis Date = 10/16/20 Pct Recovery = 92% Analysis Date = 10/12/20 Pct Recovery = 92% Analysis Date = 10/12/20 Pct Recovery = 92% Analysis Date = 10/08/20 Pct Recovery = 92% Analysis Date = 10/08/20 Pct Recovery = 92% Analysis Date = 10/04/20 Pct Recovery = 92% Analysis Date = 10/04/20 Pct Recovery = 92% Analysis Date = 09/30/20 Pct Recovery = 92% Analysis Date = 09/30/20 Pct Recovery = 92% Analysis Date = 09/26/20 Pct Recovery = 92% Analysis Date = 09/26/20 Pct Recovery = 92% Analysis Date = 09/22/20 Pct Recovery = 92% Analysis Date = 09/22/20 Pct Recovery = 92% Analysis Date = 09/18/20 Pct Recovery = 92% Analysis Date = 09/18/20 Pct Recovery = 92% Analysis Date = 09/14/20 Pct Recovery = 92% Analysis Date = 09/14/20 Pct Recovery = 92% Analysis Date = 09/10/20 Pct Recovery = 92% Analysis Date = 09/10/20 Pct Recovery = 92% Analysis Date = 09/06/20 Pct Recovery = 92% Analysis Date = 09/06/20 Pct Recovery = 92% Analysis Date = 09/02/20 Pct Recovery = 92% Analysis Date = 09/02/20 Pct Recovery = 92% Analysis Date = 08/29/20 Pct Recovery = 92% Analysis Date = 08/29/20 Pct Recovery = 92% Analysis Date = 08/25/20 Pct Recovery = 92% Analysis Date = 08/25/20 Pct Recovery = 92% Analysis Date = 08/21/20 Pct Recovery = 92% Analysis Date = 08/21/20 Pct Recovery = 92% Analysis Date = 08/17/20 Pct Recovery = 92% Analysis Date = 08/17/20 Pct Recovery = 92% Analysis Date = 08/13/20 Pct Recovery = 92% Analysis Date = 08/13/20 Pct Recovery = 92% Analysis Date = 08/09/20 Pct Recovery = 92% Analysis Date = 08/09/20 Pct Recovery = 92% Analysis Date = 08/05/20 Pct Recovery = 92% Analysis Date = 08/05/20 Pct Recovery = 92% Analysis Date = 08/01/20 Pct Recovery = 92% Analysis Date = 08/01/20 Pct Recovery = 92% Analysis Date = 07/28/20 Pct Recovery = 92% Analysis Date = 07/28/20 Pct Recovery = 92% Analysis Date = 07/24/20 Pct Recovery = 92% Analysis Date = 07/24/20 Pct Recovery = 92% Analysis Date = 07/20/20 Pct Recovery = 92% Analysis Date = 07/20/20 Pct Recovery = 92% Analysis Date = 07/16/20 Pct Recovery = 92% Analysis Date = 07/16/20 Pct Recovery = 92% Analysis Date = 07/12/20 Pct Recovery = 92% Analysis Date = 07/12/20 Pct Recovery = 92% Analysis Date = 07/08/20 Pct Recovery = 92% Analysis Date = 07/08/20 Pct Recovery = 92% Analysis Date = 07/04/20 Pct Recovery = 92% Analysis Date = 07/04/20 Pct Recovery = 92% Analysis Date = 06/30/20 Pct Recovery = 92% Analysis Date = 06/30/20 Pct Recovery = 92% Analysis Date = 06/26/20 Pct Recovery = 92% Analysis Date = 06/26/20 Pct Recovery = 92% Analysis Date = 06/22/20 Pct Recovery = 92% Analysis Date = 06/22/20 Pct Recovery = 92% Analysis Date = 06/18/20 Pct Recovery = 92% Analysis Date = 06/18/20 Pct Recovery = 92% Analysis Date = 06/14/20 Pct Recovery = 92% Analysis Date = 06/14/20 Pct Recovery = 92% Analysis Date = 06/11/20 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 25 85% 13% 87% 10%
Total 25 85% 13% 87% 10%

Sample Statistics
FIPRONIL SULFONE

Characteristic N % % Basis
Plotted 25 100% Spiked
Estimated Values 3 12% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 25 .  
False Negatives 0 0% 0 out of 25
Not Spiked 83 .  
False Positives 5 6% 5 out of 83

OBSP Determination:
FLUOMETURON
METHOD: 2447 , TESTIDCODE: 68608LCM60

Laboratory ID = 20202590106 Lab Value = 267.744 Expected Conc. = 125.1 Report level label = 10 Pct Recovery = 214% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 267.142 Expected Conc. = 125.1 Report level label = 10 Pct Recovery = 214% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 120.459 Expected Conc. = 125.7 Report level label = 10 Pct Recovery = 96% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 106.802 Expected Conc. = 125.7 Report level label = 10 Pct Recovery = 85% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222150192 Lab Value = 80.323 Expected Conc. = 101.2 Report level label = 10 Pct Recovery = 79% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 102.098 Expected Conc. = 101.2 Report level label = 10 Pct Recovery = 101% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 71.506 Expected Conc. = 100 Report level label = 10 Pct Recovery = 72% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221870197 Lab Value = 45.913 Expected Conc. = 63.25 Report level label = 10 Pct Recovery = 73% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20201550031 Lab Value = 68.746 Expected Conc. = 62.75 Report level label = 10 Pct Recovery = 110% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20203230018 Lab Value = 53.265 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 85% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 52.733 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 84% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 79.228 Expected Conc. = 62.55 Report level label = 10 Pct Recovery = 127% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220740064 Lab Value = 43.408 Expected Conc. = 62.25 Report level label = 10 Pct Recovery = 70% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202390020 Lab Value = 87.209 Expected Conc. = 61.95 Report level label = 10 Pct Recovery = 141% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 74.258 Expected Conc. = 61.95 Report level label = 10 Pct Recovery = 120% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 68.820 Expected Conc. = 49.56 Report level label = 10 Pct Recovery = 139% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 58.704 Expected Conc. = 49.56 Report level label = 10 Pct Recovery = 118% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20221660151 Lab Value = 29.988 Expected Conc. = 25.3 Report level label = 10 Pct Recovery = 119% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210270007 Lab Value = 24.414 Expected Conc. = 25.14 Report level label = 10 Pct Recovery = 97% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202330309 Lab Value = 23.251 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 93% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 19.981 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 80% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 28.688 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 114% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 26.758 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 107% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 30.525 Expected Conc. = 25.1 Report level label = 10 Pct Recovery = 122% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210970035 Lab Value = 25.070 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 100% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 28.875 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 115% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 27.025 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 108% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 27.132 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 108% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 27.131 Expected Conc. = 25.02 Report level label = 10 Pct Recovery = 108% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 08/15/22 Pct Recovery = 84% Analysis Date = 08/10/22 Pct Recovery = 85% Analysis Date = 08/10/22 Pct Recovery = 85% Analysis Date = 08/06/22 Pct Recovery = 85% Analysis Date = 08/06/22 Pct Recovery = 85% Analysis Date = 08/02/22 Pct Recovery = 85% Analysis Date = 08/02/22 Pct Recovery = 85% Analysis Date = 07/29/22 Pct Recovery = 85% Analysis Date = 07/29/22 Pct Recovery = 85% Analysis Date = 07/25/22 Pct Recovery = 85% Analysis Date = 07/25/22 Pct Recovery = 85% Analysis Date = 07/21/22 Pct Recovery = 85% Analysis Date = 07/21/22 Pct Recovery = 85% Analysis Date = 07/17/22 Pct Recovery = 85% Analysis Date = 07/17/22 Pct Recovery = 85% Analysis Date = 07/13/22 Pct Recovery = 85% Analysis Date = 07/13/22 Pct Recovery = 85% Analysis Date = 07/09/22 Pct Recovery = 85% Analysis Date = 07/09/22 Pct Recovery = 85% Analysis Date = 07/05/22 Pct Recovery = 85% Analysis Date = 07/05/22 Pct Recovery = 85% Analysis Date = 07/01/22 Pct Recovery = 85% Analysis Date = 07/01/22 Pct Recovery = 85% Analysis Date = 06/27/22 Pct Recovery = 86% Analysis Date = 06/27/22 Pct Recovery = 86% Analysis Date = 06/23/22 Pct Recovery = 86% Analysis Date = 06/23/22 Pct Recovery = 86% Analysis Date = 06/19/22 Pct Recovery = 86% Analysis Date = 06/19/22 Pct Recovery = 86% Analysis Date = 06/15/22 Pct Recovery = 86% Analysis Date = 06/15/22 Pct Recovery = 86% Analysis Date = 06/11/22 Pct Recovery = 86% Analysis Date = 06/11/22 Pct Recovery = 86% Analysis Date = 06/07/22 Pct Recovery = 86% Analysis Date = 06/07/22 Pct Recovery = 86% Analysis Date = 06/03/22 Pct Recovery = 86% Analysis Date = 06/03/22 Pct Recovery = 86% Analysis Date = 05/30/22 Pct Recovery = 86% Analysis Date = 05/30/22 Pct Recovery = 86% Analysis Date = 05/26/22 Pct Recovery = 86% Analysis Date = 05/26/22 Pct Recovery = 86% Analysis Date = 05/22/22 Pct Recovery = 86% Analysis Date = 05/22/22 Pct Recovery = 86% Analysis Date = 05/18/22 Pct Recovery = 86% Analysis Date = 05/18/22 Pct Recovery = 86% Analysis Date = 05/14/22 Pct Recovery = 87% Analysis Date = 05/14/22 Pct Recovery = 87% Analysis Date = 05/10/22 Pct Recovery = 87% Analysis Date = 05/10/22 Pct Recovery = 87% Analysis Date = 05/06/22 Pct Recovery = 87% Analysis Date = 05/06/22 Pct Recovery = 87% Analysis Date = 05/01/22 Pct Recovery = 87% Analysis Date = 05/01/22 Pct Recovery = 87% Analysis Date = 04/27/22 Pct Recovery = 87% Analysis Date = 04/27/22 Pct Recovery = 87% Analysis Date = 04/23/22 Pct Recovery = 87% Analysis Date = 04/23/22 Pct Recovery = 87% Analysis Date = 04/19/22 Pct Recovery = 87% Analysis Date = 04/19/22 Pct Recovery = 87% Analysis Date = 04/15/22 Pct Recovery = 87% Analysis Date = 04/15/22 Pct Recovery = 87% Analysis Date = 04/11/22 Pct Recovery = 87% Analysis Date = 04/11/22 Pct Recovery = 87% Analysis Date = 04/07/22 Pct Recovery = 87% Analysis Date = 04/07/22 Pct Recovery = 87% Analysis Date = 04/03/22 Pct Recovery = 88% Analysis Date = 04/03/22 Pct Recovery = 88% Analysis Date = 03/30/22 Pct Recovery = 88% Analysis Date = 03/30/22 Pct Recovery = 88% Analysis Date = 03/26/22 Pct Recovery = 88% Analysis Date = 03/26/22 Pct Recovery = 88% Analysis Date = 03/22/22 Pct Recovery = 88% Analysis Date = 03/22/22 Pct Recovery = 88% Analysis Date = 03/18/22 Pct Recovery = 88% Analysis Date = 03/18/22 Pct Recovery = 88% Analysis Date = 03/14/22 Pct Recovery = 88% Analysis Date = 03/14/22 Pct Recovery = 88% Analysis Date = 03/10/22 Pct Recovery = 88% Analysis Date = 03/10/22 Pct Recovery = 88% Analysis Date = 03/06/22 Pct Recovery = 88% Analysis Date = 03/06/22 Pct Recovery = 88% Analysis Date = 03/02/22 Pct Recovery = 88% Analysis Date = 03/02/22 Pct Recovery = 88% Analysis Date = 02/26/22 Pct Recovery = 88% Analysis Date = 02/26/22 Pct Recovery = 88% Analysis Date = 02/22/22 Pct Recovery = 88% Analysis Date = 02/22/22 Pct Recovery = 88% Analysis Date = 02/18/22 Pct Recovery = 89% Analysis Date = 02/18/22 Pct Recovery = 89% Analysis Date = 02/14/22 Pct Recovery = 89% Analysis Date = 02/14/22 Pct Recovery = 89% Analysis Date = 02/10/22 Pct Recovery = 89% Analysis Date = 02/10/22 Pct Recovery = 89% Analysis Date = 02/06/22 Pct Recovery = 89% Analysis Date = 02/06/22 Pct Recovery = 89% Analysis Date = 02/02/22 Pct Recovery = 89% Analysis Date = 02/02/22 Pct Recovery = 89% Analysis Date = 01/29/22 Pct Recovery = 89% Analysis Date = 01/29/22 Pct Recovery = 89% Analysis Date = 01/25/22 Pct Recovery = 89% Analysis Date = 01/25/22 Pct Recovery = 89% Analysis Date = 01/20/22 Pct Recovery = 89% Analysis Date = 01/20/22 Pct Recovery = 89% Analysis Date = 01/16/22 Pct Recovery = 89% Analysis Date = 01/16/22 Pct Recovery = 89% Analysis Date = 01/12/22 Pct Recovery = 89% Analysis Date = 01/12/22 Pct Recovery = 89% Analysis Date = 01/08/22 Pct Recovery = 89% Analysis Date = 01/08/22 Pct Recovery = 89% Analysis Date = 01/04/22 Pct Recovery = 89% Analysis Date = 01/04/22 Pct Recovery = 89% Analysis Date = 12/31/21 Pct Recovery = 90% Analysis Date = 12/31/21 Pct Recovery = 90% Analysis Date = 12/27/21 Pct Recovery = 90% Analysis Date = 12/27/21 Pct Recovery = 90% Analysis Date = 12/23/21 Pct Recovery = 90% Analysis Date = 12/23/21 Pct Recovery = 90% Analysis Date = 12/19/21 Pct Recovery = 90% Analysis Date = 12/19/21 Pct Recovery = 90% Analysis Date = 12/15/21 Pct Recovery = 90% Analysis Date = 12/15/21 Pct Recovery = 90% Analysis Date = 12/11/21 Pct Recovery = 90% Analysis Date = 12/11/21 Pct Recovery = 90% Analysis Date = 12/07/21 Pct Recovery = 90% Analysis Date = 12/07/21 Pct Recovery = 90% Analysis Date = 12/03/21 Pct Recovery = 90% Analysis Date = 12/03/21 Pct Recovery = 90% Analysis Date = 11/29/21 Pct Recovery = 90% Analysis Date = 11/29/21 Pct Recovery = 90% Analysis Date = 11/25/21 Pct Recovery = 90% Analysis Date = 11/25/21 Pct Recovery = 90% Analysis Date = 11/21/21 Pct Recovery = 90% Analysis Date = 11/21/21 Pct Recovery = 90% Analysis Date = 11/17/21 Pct Recovery = 90% Analysis Date = 11/17/21 Pct Recovery = 90% Analysis Date = 11/13/21 Pct Recovery = 91% Analysis Date = 11/13/21 Pct Recovery = 91% Analysis Date = 11/09/21 Pct Recovery = 91% Analysis Date = 11/09/21 Pct Recovery = 91% Analysis Date = 11/05/21 Pct Recovery = 91% Analysis Date = 11/05/21 Pct Recovery = 91% Analysis Date = 11/01/21 Pct Recovery = 91% Analysis Date = 11/01/21 Pct Recovery = 91% Analysis Date = 10/28/21 Pct Recovery = 91% Analysis Date = 10/28/21 Pct Recovery = 91% Analysis Date = 10/24/21 Pct Recovery = 91% Analysis Date = 10/24/21 Pct Recovery = 91% Analysis Date = 10/20/21 Pct Recovery = 91% Analysis Date = 10/20/21 Pct Recovery = 91% Analysis Date = 10/16/21 Pct Recovery = 91% Analysis Date = 10/16/21 Pct Recovery = 91% Analysis Date = 10/11/21 Pct Recovery = 91% Analysis Date = 10/11/21 Pct Recovery = 91% Analysis Date = 10/07/21 Pct Recovery = 91% Analysis Date = 10/07/21 Pct Recovery = 91% Analysis Date = 10/03/21 Pct Recovery = 91% Analysis Date = 10/03/21 Pct Recovery = 91% Analysis Date = 09/29/21 Pct Recovery = 91% Analysis Date = 09/29/21 Pct Recovery = 91% Analysis Date = 09/25/21 Pct Recovery = 92% Analysis Date = 09/25/21 Pct Recovery = 92% Analysis Date = 09/21/21 Pct Recovery = 92% Analysis Date = 09/21/21 Pct Recovery = 92% Analysis Date = 09/17/21 Pct Recovery = 92% Analysis Date = 09/17/21 Pct Recovery = 92% Analysis Date = 09/13/21 Pct Recovery = 92% Analysis Date = 09/13/21 Pct Recovery = 92% Analysis Date = 09/09/21 Pct Recovery = 92% Analysis Date = 09/09/21 Pct Recovery = 92% Analysis Date = 09/05/21 Pct Recovery = 92% Analysis Date = 09/05/21 Pct Recovery = 92% Analysis Date = 09/01/21 Pct Recovery = 92% Analysis Date = 09/01/21 Pct Recovery = 92% Analysis Date = 08/28/21 Pct Recovery = 92% Analysis Date = 08/28/21 Pct Recovery = 92% Analysis Date = 08/24/21 Pct Recovery = 92% Analysis Date = 08/24/21 Pct Recovery = 92% Analysis Date = 08/20/21 Pct Recovery = 92% Analysis Date = 08/20/21 Pct Recovery = 92% Analysis Date = 08/16/21 Pct Recovery = 92% Analysis Date = 08/16/21 Pct Recovery = 92% Analysis Date = 08/12/21 Pct Recovery = 92% Analysis Date = 08/12/21 Pct Recovery = 92% Analysis Date = 08/08/21 Pct Recovery = 93% Analysis Date = 08/08/21 Pct Recovery = 93% Analysis Date = 08/04/21 Pct Recovery = 93% Analysis Date = 08/04/21 Pct Recovery = 93% Analysis Date = 07/31/21 Pct Recovery = 93% Analysis Date = 07/31/21 Pct Recovery = 93% Analysis Date = 07/27/21 Pct Recovery = 93% Analysis Date = 07/27/21 Pct Recovery = 93% Analysis Date = 07/23/21 Pct Recovery = 93% Analysis Date = 07/23/21 Pct Recovery = 93% Analysis Date = 07/19/21 Pct Recovery = 93% Analysis Date = 07/19/21 Pct Recovery = 93% Analysis Date = 07/15/21 Pct Recovery = 93% Analysis Date = 07/15/21 Pct Recovery = 93% Analysis Date = 07/11/21 Pct Recovery = 93% Analysis Date = 07/11/21 Pct Recovery = 93% Analysis Date = 07/07/21 Pct Recovery = 93% Analysis Date = 07/07/21 Pct Recovery = 93% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 06/28/21 Pct Recovery = 93% Analysis Date = 06/28/21 Pct Recovery = 93% Analysis Date = 06/24/21 Pct Recovery = 93% Analysis Date = 06/24/21 Pct Recovery = 93% Analysis Date = 06/20/21 Pct Recovery = 94% Analysis Date = 06/20/21 Pct Recovery = 94% Analysis Date = 06/16/21 Pct Recovery = 94% Analysis Date = 06/16/21 Pct Recovery = 94% Analysis Date = 06/12/21 Pct Recovery = 94% Analysis Date = 06/12/21 Pct Recovery = 94% Analysis Date = 06/08/21 Pct Recovery = 94% Analysis Date = 06/08/21 Pct Recovery = 94% Analysis Date = 06/04/21 Pct Recovery = 94% Analysis Date = 06/04/21 Pct Recovery = 94% Analysis Date = 05/31/21 Pct Recovery = 94% Analysis Date = 05/31/21 Pct Recovery = 94% Analysis Date = 05/27/21 Pct Recovery = 94% Analysis Date = 05/27/21 Pct Recovery = 94% Analysis Date = 05/23/21 Pct Recovery = 94% Analysis Date = 05/23/21 Pct Recovery = 94% Analysis Date = 05/19/21 Pct Recovery = 94% Analysis Date = 05/19/21 Pct Recovery = 94% Analysis Date = 05/15/21 Pct Recovery = 94% Analysis Date = 05/15/21 Pct Recovery = 94% Analysis Date = 05/11/21 Pct Recovery = 94% Analysis Date = 05/11/21 Pct Recovery = 94% Analysis Date = 05/07/21 Pct Recovery = 94% Analysis Date = 05/07/21 Pct Recovery = 94% Analysis Date = 05/03/21 Pct Recovery = 95% Analysis Date = 05/03/21 Pct Recovery = 95% Analysis Date = 04/29/21 Pct Recovery = 95% Analysis Date = 04/29/21 Pct Recovery = 95% Analysis Date = 04/25/21 Pct Recovery = 95% Analysis Date = 04/25/21 Pct Recovery = 95% Analysis Date = 04/21/21 Pct Recovery = 95% Analysis Date = 04/21/21 Pct Recovery = 95% Analysis Date = 04/17/21 Pct Recovery = 95% Analysis Date = 04/17/21 Pct Recovery = 95% Analysis Date = 04/13/21 Pct Recovery = 95% Analysis Date = 04/13/21 Pct Recovery = 95% Analysis Date = 04/09/21 Pct Recovery = 95% Analysis Date = 04/09/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/01/21 Pct Recovery = 95% Analysis Date = 04/01/21 Pct Recovery = 95% Analysis Date = 03/28/21 Pct Recovery = 95% Analysis Date = 03/28/21 Pct Recovery = 95% Analysis Date = 03/23/21 Pct Recovery = 95% Analysis Date = 03/23/21 Pct Recovery = 95% Analysis Date = 03/19/21 Pct Recovery = 95% Analysis Date = 03/19/21 Pct Recovery = 95% Analysis Date = 03/15/21 Pct Recovery = 96% Analysis Date = 03/15/21 Pct Recovery = 96% Analysis Date = 03/11/21 Pct Recovery = 96% Analysis Date = 03/11/21 Pct Recovery = 96% Analysis Date = 03/07/21 Pct Recovery = 96% Analysis Date = 03/07/21 Pct Recovery = 96% Analysis Date = 03/03/21 Pct Recovery = 96% Analysis Date = 03/03/21 Pct Recovery = 96% Analysis Date = 02/27/21 Pct Recovery = 96% Analysis Date = 02/27/21 Pct Recovery = 96% Analysis Date = 02/23/21 Pct Recovery = 96% Analysis Date = 02/23/21 Pct Recovery = 96% Analysis Date = 02/19/21 Pct Recovery = 96% Analysis Date = 02/19/21 Pct Recovery = 96% Analysis Date = 02/15/21 Pct Recovery = 96% Analysis Date = 02/15/21 Pct Recovery = 96% Analysis Date = 02/11/21 Pct Recovery = 96% Analysis Date = 02/11/21 Pct Recovery = 96% Analysis Date = 02/07/21 Pct Recovery = 97% Analysis Date = 02/07/21 Pct Recovery = 97% Analysis Date = 02/03/21 Pct Recovery = 98% Analysis Date = 02/03/21 Pct Recovery = 98% Analysis Date = 01/30/21 Pct Recovery = 99% Analysis Date = 01/30/21 Pct Recovery = 99% Analysis Date = 01/26/21 Pct Recovery = 100% Analysis Date = 01/26/21 Pct Recovery = 100% Analysis Date = 01/22/21 Pct Recovery = 101% Analysis Date = 01/22/21 Pct Recovery = 101% Analysis Date = 01/18/21 Pct Recovery = 102% Analysis Date = 01/18/21 Pct Recovery = 102% Analysis Date = 01/14/21 Pct Recovery = 103% Analysis Date = 01/14/21 Pct Recovery = 103% Analysis Date = 01/10/21 Pct Recovery = 104% Analysis Date = 01/10/21 Pct Recovery = 104% Analysis Date = 01/06/21 Pct Recovery = 105% Analysis Date = 01/06/21 Pct Recovery = 105% Analysis Date = 01/02/21 Pct Recovery = 106% Analysis Date = 01/02/21 Pct Recovery = 106% Analysis Date = 12/29/20 Pct Recovery = 107% Analysis Date = 12/29/20 Pct Recovery = 107% Analysis Date = 12/25/20 Pct Recovery = 108% Analysis Date = 12/25/20 Pct Recovery = 108% Analysis Date = 12/21/20 Pct Recovery = 109% Analysis Date = 12/21/20 Pct Recovery = 109% Analysis Date = 12/17/20 Pct Recovery = 110% Analysis Date = 12/17/20 Pct Recovery = 110% Analysis Date = 12/12/20 Pct Recovery = 112% Analysis Date = 12/12/20 Pct Recovery = 112% Analysis Date = 12/08/20 Pct Recovery = 113% Analysis Date = 12/08/20 Pct Recovery = 113% Analysis Date = 12/04/20 Pct Recovery = 115% Analysis Date = 12/04/20 Pct Recovery = 115% Analysis Date = 11/30/20 Pct Recovery = 116% Analysis Date = 11/30/20 Pct Recovery = 116% Analysis Date = 11/26/20 Pct Recovery = 117% Analysis Date = 11/26/20 Pct Recovery = 117% Analysis Date = 11/22/20 Pct Recovery = 119% Analysis Date = 11/22/20 Pct Recovery = 119% Analysis Date = 11/18/20 Pct Recovery = 120% Analysis Date = 11/18/20 Pct Recovery = 120% Analysis Date = 11/14/20 Pct Recovery = 122% Analysis Date = 11/14/20 Pct Recovery = 122% Analysis Date = 11/10/20 Pct Recovery = 123% Analysis Date = 11/10/20 Pct Recovery = 123% Analysis Date = 11/06/20 Pct Recovery = 124% Analysis Date = 11/06/20 Pct Recovery = 124% Analysis Date = 11/02/20 Pct Recovery = 125% Analysis Date = 11/02/20 Pct Recovery = 125% Analysis Date = 10/29/20 Pct Recovery = 126% Analysis Date = 10/29/20 Pct Recovery = 126% Analysis Date = 10/25/20 Pct Recovery = 127% Analysis Date = 10/25/20 Pct Recovery = 127% Analysis Date = 10/21/20 Pct Recovery = 127% Analysis Date = 10/21/20 Pct Recovery = 127% Analysis Date = 10/17/20 Pct Recovery = 128% Analysis Date = 10/17/20 Pct Recovery = 128% Analysis Date = 10/13/20 Pct Recovery = 129% Analysis Date = 10/13/20 Pct Recovery = 129% Analysis Date = 10/09/20 Pct Recovery = 130% Analysis Date = 10/09/20 Pct Recovery = 130% Analysis Date = 10/05/20 Pct Recovery = 130% Analysis Date = 10/05/20 Pct Recovery = 130% Analysis Date = 10/01/20 Pct Recovery = 131% Analysis Date = 10/01/20 Pct Recovery = 131% Analysis Date = 09/27/20 Pct Recovery = 132% Analysis Date = 09/27/20 Pct Recovery = 132% Analysis Date = 09/23/20 Pct Recovery = 132% Analysis Date = 09/23/20 Pct Recovery = 132% Analysis Date = 09/19/20 Pct Recovery = 133% Analysis Date = 09/19/20 Pct Recovery = 133% Analysis Date = 09/15/20 Pct Recovery = 133% Analysis Date = 09/15/20 Pct Recovery = 133% Analysis Date = 09/11/20 Pct Recovery = 133% Analysis Date = 09/11/20 Pct Recovery = 133% Analysis Date = 09/07/20 Pct Recovery = 134% Analysis Date = 09/07/20 Pct Recovery = 134% Analysis Date = 09/02/20 Pct Recovery = 133% Analysis Date = 09/02/20 Pct Recovery = 133% Analysis Date = 08/29/20 Pct Recovery = 133% Analysis Date = 08/29/20 Pct Recovery = 133% Analysis Date = 08/25/20 Pct Recovery = 132% Analysis Date = 08/25/20 Pct Recovery = 132% Analysis Date = 08/21/20 Pct Recovery = 131% Analysis Date = 08/21/20 Pct Recovery = 131% Analysis Date = 08/17/20 Pct Recovery = 130% Analysis Date = 08/17/20 Pct Recovery = 130% Analysis Date = 08/13/20 Pct Recovery = 129% Analysis Date = 08/13/20 Pct Recovery = 129% Analysis Date = 08/09/20 Pct Recovery = 128% Analysis Date = 08/09/20 Pct Recovery = 128% Analysis Date = 08/05/20 Pct Recovery = 127% Analysis Date = 08/05/20 Pct Recovery = 127% Analysis Date = 08/01/20 Pct Recovery = 125% Analysis Date = 08/01/20 Pct Recovery = 125% Analysis Date = 07/28/20 Pct Recovery = 124% Analysis Date = 07/28/20 Pct Recovery = 124% Analysis Date = 07/24/20 Pct Recovery = 123% Analysis Date = 07/24/20 Pct Recovery = 123% Analysis Date = 07/20/20 Pct Recovery = 122% Analysis Date = 07/20/20 Pct Recovery = 122% Analysis Date = 07/16/20 Pct Recovery = 121% Analysis Date = 07/16/20 Pct Recovery = 121% Analysis Date = 07/12/20 Pct Recovery = 120% Analysis Date = 07/12/20 Pct Recovery = 120% Analysis Date = 07/08/20 Pct Recovery = 119% Analysis Date = 07/08/20 Pct Recovery = 119% Analysis Date = 07/04/20 Pct Recovery = 118% Analysis Date = 07/04/20 Pct Recovery = 118% Analysis Date = 06/30/20 Pct Recovery = 116% Analysis Date = 06/30/20 Pct Recovery = 116% Analysis Date = 06/26/20 Pct Recovery = 115% Analysis Date = 06/26/20 Pct Recovery = 115% Analysis Date = 06/22/20 Pct Recovery = 114% Analysis Date = 06/22/20 Pct Recovery = 114% Analysis Date = 06/18/20 Pct Recovery = 113% Analysis Date = 06/18/20 Pct Recovery = 113% Analysis Date = 06/14/20 Pct Recovery = 112% Analysis Date = 06/14/20 Pct Recovery = 112% Analysis Date = 06/10/20 Pct Recovery = 111% Analysis Date = 06/10/20 Pct Recovery = 111% Analysis Date = 06/06/20 Pct Recovery = 110% Analysis Date = 06/06/20 Pct Recovery = 110% Analysis Date = 06/02/20 Pct Recovery = 109% Analysis Date = 06/02/20 Pct Recovery = 109% Analysis Date = 05/29/20 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FLUOMETURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 29 110% 34% 108% 25%
Total 29 110% 34% 108% 25%

Sample Statistics
FLUOMETURON

Characteristic N % % Basis
Plotted 29 94% Spiked
Estimated Values 4 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 6% Spiked
Spiked 31 .  
False Negatives 0 0% 0 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
HALOSULFURON-METHYL
METHOD: 2447 , TESTIDCODE: 61680LCM60

Laboratory ID = 20202590106 Lab Value = 128.875 Expected Conc. = 150.6 Report level label = 12 Pct Recovery = 86% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 136.879 Expected Conc. = 150.6 Report level label = 12 Pct Recovery = 91% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201820155 Lab Value = 132.819 Expected Conc. = 150.6 Report level label = 12 Pct Recovery = 88% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203230021 Lab Value = 85.251 Expected Conc. = 150.1 Report level label = 12 Pct Recovery = 57% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 92.804 Expected Conc. = 150.1 Report level label = 12 Pct Recovery = 62% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202110006 Lab Value = 147.542 Expected Conc. = 147.6 Report level label = 12 Pct Recovery = 100% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20220190116 Lab Value = 79.389 Expected Conc. = 121.12 Report level label = 12 Pct Recovery = 66% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 79.700 Expected Conc. = 121.12 Report level label = 12 Pct Recovery = 66% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20212990174 Lab Value = 32.820 Expected Conc. = 120.64 Report level label = 12 Pct Recovery = 27% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 46.588 Expected Conc. = 120 Report level label = 12 Pct Recovery = 39% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 38.454 Expected Conc. = 119.2 Report level label = 12 Pct Recovery = 32% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222150193 Lab Value = 30.788 Expected Conc. = 118.4 Report level label = 12 Pct Recovery = 26% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20221730293 Lab Value = 68.478 Expected Conc. = 75.7 Report level label = 12 Pct Recovery = 90% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 46.407 Expected Conc. = 75.7 Report level label = 12 Pct Recovery = 61% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20213200091 Lab Value = 119.300 Expected Conc. = 75.4 Report level label = 12 Pct Recovery = 158% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20203230018 Lab Value = 47.762 Expected Conc. = 75.3 Report level label = 12 Pct Recovery = 63% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 63.445 Expected Conc. = 75.3 Report level label = 12 Pct Recovery = 84% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 80.190 Expected Conc. = 75.3 Report level label = 12 Pct Recovery = 106% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 61.316 Expected Conc. = 75.3 Report level label = 12 Pct Recovery = 81% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 63.403 Expected Conc. = 75.3 Report level label = 12 Pct Recovery = 84% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 66.826 Expected Conc. = 75.3 Report level label = 12 Pct Recovery = 89% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201680155 Lab Value = 73.316 Expected Conc. = 73.8 Report level label = 12 Pct Recovery = 99% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20222500483 Lab Value = 30.340 Expected Conc. = 30.28 Report level label = 12 Pct Recovery = 100% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 24.758 Expected Conc. = 30.28 Report level label = 12 Pct Recovery = 82% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210970035 Lab Value = 25.805 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 86% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 31.835 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 106% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 33.854 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 112% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 27.027 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 90% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 30.113 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 100% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 30.299 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 101% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 32.279 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 107% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 31.108 Expected Conc. = 30.12 Report level label = 12 Pct Recovery = 103% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210270007 Lab Value = 19.263 Expected Conc. = 30.02 Report level label = 12 Pct Recovery = 64% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222630205 Lab Value = 19.295 Expected Conc. = 29.8 Report level label = 12 Pct Recovery = 65% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20201610160 Lab Value = 29.532 Expected Conc. = 29.52 Report level label = 12 Pct Recovery = 100% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Analysis Date = 09/28/22 Pct Recovery = 60% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 61% Analysis Date = 09/16/22 Pct Recovery = 61% Analysis Date = 09/16/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 61% Analysis Date = 08/29/22 Pct Recovery = 62% Analysis Date = 08/29/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/16/22 Pct Recovery = 62% Analysis Date = 08/16/22 Pct Recovery = 62% Analysis Date = 08/12/22 Pct Recovery = 62% Analysis Date = 08/12/22 Pct Recovery = 62% Analysis Date = 08/08/22 Pct Recovery = 62% Analysis Date = 08/08/22 Pct Recovery = 62% Analysis Date = 08/03/22 Pct Recovery = 63% Analysis Date = 08/03/22 Pct Recovery = 63% Analysis Date = 07/30/22 Pct Recovery = 63% Analysis Date = 07/30/22 Pct Recovery = 63% Analysis Date = 07/26/22 Pct Recovery = 63% Analysis Date = 07/26/22 Pct Recovery = 63% Analysis Date = 07/21/22 Pct Recovery = 63% Analysis Date = 07/21/22 Pct Recovery = 63% Analysis Date = 07/17/22 Pct Recovery = 63% Analysis Date = 07/17/22 Pct Recovery = 63% Analysis Date = 07/13/22 Pct Recovery = 63% Analysis Date = 07/13/22 Pct Recovery = 63% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/04/22 Pct Recovery = 64% Analysis Date = 07/04/22 Pct Recovery = 64% Analysis Date = 06/30/22 Pct Recovery = 64% Analysis Date = 06/30/22 Pct Recovery = 64% Analysis Date = 06/26/22 Pct Recovery = 64% Analysis Date = 06/26/22 Pct Recovery = 64% Analysis Date = 06/21/22 Pct Recovery = 64% Analysis Date = 06/21/22 Pct Recovery = 64% Analysis Date = 06/17/22 Pct Recovery = 64% Analysis Date = 06/17/22 Pct Recovery = 64% Analysis Date = 06/13/22 Pct Recovery = 65% Analysis Date = 06/13/22 Pct Recovery = 65% Analysis Date = 06/08/22 Pct Recovery = 65% Analysis Date = 06/08/22 Pct Recovery = 65% Analysis Date = 06/04/22 Pct Recovery = 65% Analysis Date = 06/04/22 Pct Recovery = 65% Analysis Date = 05/31/22 Pct Recovery = 65% Analysis Date = 05/31/22 Pct Recovery = 65% Analysis Date = 05/26/22 Pct Recovery = 65% Analysis Date = 05/26/22 Pct Recovery = 65% Analysis Date = 05/22/22 Pct Recovery = 65% Analysis Date = 05/22/22 Pct Recovery = 65% Analysis Date = 05/18/22 Pct Recovery = 65% Analysis Date = 05/18/22 Pct Recovery = 65% Analysis Date = 05/13/22 Pct Recovery = 66% Analysis Date = 05/13/22 Pct Recovery = 66% Analysis Date = 05/09/22 Pct Recovery = 66% Analysis Date = 05/09/22 Pct Recovery = 66% Analysis Date = 05/05/22 Pct Recovery = 66% Analysis Date = 05/05/22 Pct Recovery = 66% Analysis Date = 04/30/22 Pct Recovery = 66% Analysis Date = 04/30/22 Pct Recovery = 66% Analysis Date = 04/26/22 Pct Recovery = 66% Analysis Date = 04/26/22 Pct Recovery = 66% Analysis Date = 04/22/22 Pct Recovery = 66% Analysis Date = 04/22/22 Pct Recovery = 66% Analysis Date = 04/18/22 Pct Recovery = 66% Analysis Date = 04/18/22 Pct Recovery = 66% Analysis Date = 04/13/22 Pct Recovery = 67% Analysis Date = 04/13/22 Pct Recovery = 67% Analysis Date = 04/09/22 Pct Recovery = 67% Analysis Date = 04/09/22 Pct Recovery = 67% Analysis Date = 04/05/22 Pct Recovery = 67% Analysis Date = 04/05/22 Pct Recovery = 67% Analysis Date = 03/31/22 Pct Recovery = 67% Analysis Date = 03/31/22 Pct Recovery = 67% Analysis Date = 03/27/22 Pct Recovery = 67% Analysis Date = 03/27/22 Pct Recovery = 67% Analysis Date = 03/23/22 Pct Recovery = 67% Analysis Date = 03/23/22 Pct Recovery = 67% Analysis Date = 03/18/22 Pct Recovery = 67% Analysis Date = 03/18/22 Pct Recovery = 67% Analysis Date = 03/14/22 Pct Recovery = 68% Analysis Date = 03/14/22 Pct Recovery = 68% Analysis Date = 03/10/22 Pct Recovery = 68% Analysis Date = 03/10/22 Pct Recovery = 68% Analysis Date = 03/05/22 Pct Recovery = 68% Analysis Date = 03/05/22 Pct Recovery = 68% Analysis Date = 03/01/22 Pct Recovery = 68% Analysis Date = 03/01/22 Pct Recovery = 68% Analysis Date = 02/25/22 Pct Recovery = 68% Analysis Date = 02/25/22 Pct Recovery = 68% Analysis Date = 02/20/22 Pct Recovery = 68% Analysis Date = 02/20/22 Pct Recovery = 68% Analysis Date = 02/16/22 Pct Recovery = 68% Analysis Date = 02/16/22 Pct Recovery = 68% Analysis Date = 02/12/22 Pct Recovery = 69% Analysis Date = 02/12/22 Pct Recovery = 69% Analysis Date = 02/07/22 Pct Recovery = 69% Analysis Date = 02/07/22 Pct Recovery = 69% Analysis Date = 02/03/22 Pct Recovery = 69% Analysis Date = 02/03/22 Pct Recovery = 69% Analysis Date = 01/30/22 Pct Recovery = 69% Analysis Date = 01/30/22 Pct Recovery = 69% Analysis Date = 01/26/22 Pct Recovery = 69% Analysis Date = 01/26/22 Pct Recovery = 69% Analysis Date = 01/21/22 Pct Recovery = 69% Analysis Date = 01/21/22 Pct Recovery = 69% Analysis Date = 01/17/22 Pct Recovery = 69% Analysis Date = 01/17/22 Pct Recovery = 69% Analysis Date = 01/13/22 Pct Recovery = 70% Analysis Date = 01/13/22 Pct Recovery = 70% Analysis Date = 01/08/22 Pct Recovery = 70% Analysis Date = 01/08/22 Pct Recovery = 70% Analysis Date = 01/04/22 Pct Recovery = 70% Analysis Date = 01/04/22 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 70% Analysis Date = 12/26/21 Pct Recovery = 70% Analysis Date = 12/26/21 Pct Recovery = 70% Analysis Date = 12/22/21 Pct Recovery = 70% Analysis Date = 12/22/21 Pct Recovery = 70% Analysis Date = 12/18/21 Pct Recovery = 70% Analysis Date = 12/18/21 Pct Recovery = 70% Analysis Date = 12/13/21 Pct Recovery = 71% Analysis Date = 12/13/21 Pct Recovery = 71% Analysis Date = 12/09/21 Pct Recovery = 70% Analysis Date = 12/09/21 Pct Recovery = 70% Analysis Date = 12/05/21 Pct Recovery = 70% Analysis Date = 12/05/21 Pct Recovery = 70% Analysis Date = 11/30/21 Pct Recovery = 70% Analysis Date = 11/30/21 Pct Recovery = 70% Analysis Date = 11/26/21 Pct Recovery = 70% Analysis Date = 11/26/21 Pct Recovery = 70% Analysis Date = 11/22/21 Pct Recovery = 70% Analysis Date = 11/22/21 Pct Recovery = 70% Analysis Date = 11/18/21 Pct Recovery = 70% Analysis Date = 11/18/21 Pct Recovery = 70% Analysis Date = 11/13/21 Pct Recovery = 70% Analysis Date = 11/13/21 Pct Recovery = 70% Analysis Date = 11/09/21 Pct Recovery = 70% Analysis Date = 11/09/21 Pct Recovery = 70% Analysis Date = 11/05/21 Pct Recovery = 70% Analysis Date = 11/05/21 Pct Recovery = 70% Analysis Date = 10/31/21 Pct Recovery = 70% Analysis Date = 10/31/21 Pct Recovery = 70% Analysis Date = 10/27/21 Pct Recovery = 70% Analysis Date = 10/27/21 Pct Recovery = 70% Analysis Date = 10/23/21 Pct Recovery = 70% Analysis Date = 10/23/21 Pct Recovery = 70% Analysis Date = 10/18/21 Pct Recovery = 70% Analysis Date = 10/18/21 Pct Recovery = 70% Analysis Date = 10/14/21 Pct Recovery = 70% Analysis Date = 10/14/21 Pct Recovery = 70% Analysis Date = 10/10/21 Pct Recovery = 70% Analysis Date = 10/10/21 Pct Recovery = 70% Analysis Date = 10/05/21 Pct Recovery = 69% Analysis Date = 10/05/21 Pct Recovery = 69% Analysis Date = 10/01/21 Pct Recovery = 69% Analysis Date = 10/01/21 Pct Recovery = 69% Analysis Date = 09/27/21 Pct Recovery = 69% Analysis Date = 09/27/21 Pct Recovery = 69% Analysis Date = 09/22/21 Pct Recovery = 69% Analysis Date = 09/22/21 Pct Recovery = 69% Analysis Date = 09/18/21 Pct Recovery = 69% Analysis Date = 09/18/21 Pct Recovery = 69% Analysis Date = 09/14/21 Pct Recovery = 69% Analysis Date = 09/14/21 Pct Recovery = 69% Analysis Date = 09/09/21 Pct Recovery = 69% Analysis Date = 09/09/21 Pct Recovery = 69% Analysis Date = 09/05/21 Pct Recovery = 69% Analysis Date = 09/05/21 Pct Recovery = 69% Analysis Date = 09/01/21 Pct Recovery = 69% Analysis Date = 09/01/21 Pct Recovery = 69% Analysis Date = 08/28/21 Pct Recovery = 69% Analysis Date = 08/28/21 Pct Recovery = 69% Analysis Date = 08/23/21 Pct Recovery = 69% Analysis Date = 08/23/21 Pct Recovery = 69% Analysis Date = 08/19/21 Pct Recovery = 69% Analysis Date = 08/19/21 Pct Recovery = 69% Analysis Date = 08/15/21 Pct Recovery = 69% Analysis Date = 08/15/21 Pct Recovery = 69% Analysis Date = 08/10/21 Pct Recovery = 69% Analysis Date = 08/10/21 Pct Recovery = 69% Analysis Date = 08/06/21 Pct Recovery = 68% Analysis Date = 08/06/21 Pct Recovery = 68% Analysis Date = 08/02/21 Pct Recovery = 68% Analysis Date = 08/02/21 Pct Recovery = 68% Analysis Date = 07/28/21 Pct Recovery = 68% Analysis Date = 07/28/21 Pct Recovery = 68% Analysis Date = 07/24/21 Pct Recovery = 68% Analysis Date = 07/24/21 Pct Recovery = 68% Analysis Date = 07/20/21 Pct Recovery = 68% Analysis Date = 07/20/21 Pct Recovery = 68% Analysis Date = 07/15/21 Pct Recovery = 68% Analysis Date = 07/15/21 Pct Recovery = 68% Analysis Date = 07/11/21 Pct Recovery = 68% Analysis Date = 07/11/21 Pct Recovery = 68% Analysis Date = 07/07/21 Pct Recovery = 68% Analysis Date = 07/07/21 Pct Recovery = 68% Analysis Date = 07/02/21 Pct Recovery = 68% Analysis Date = 07/02/21 Pct Recovery = 68% Analysis Date = 06/28/21 Pct Recovery = 68% Analysis Date = 06/28/21 Pct Recovery = 68% Analysis Date = 06/24/21 Pct Recovery = 68% Analysis Date = 06/24/21 Pct Recovery = 68% Analysis Date = 06/19/21 Pct Recovery = 68% Analysis Date = 06/19/21 Pct Recovery = 68% Analysis Date = 06/15/21 Pct Recovery = 68% Analysis Date = 06/15/21 Pct Recovery = 68% Analysis Date = 06/11/21 Pct Recovery = 68% Analysis Date = 06/11/21 Pct Recovery = 68% Analysis Date = 06/07/21 Pct Recovery = 68% Analysis Date = 06/07/21 Pct Recovery = 68% Analysis Date = 06/02/21 Pct Recovery = 67% Analysis Date = 06/02/21 Pct Recovery = 67% Analysis Date = 05/29/21 Pct Recovery = 67% Analysis Date = 05/29/21 Pct Recovery = 67% Analysis Date = 05/25/21 Pct Recovery = 67% Analysis Date = 05/25/21 Pct Recovery = 67% Analysis Date = 05/20/21 Pct Recovery = 67% Analysis Date = 05/20/21 Pct Recovery = 67% Analysis Date = 05/16/21 Pct Recovery = 67% Analysis Date = 05/16/21 Pct Recovery = 67% Analysis Date = 05/12/21 Pct Recovery = 67% Analysis Date = 05/12/21 Pct Recovery = 67% Analysis Date = 05/07/21 Pct Recovery = 67% Analysis Date = 05/07/21 Pct Recovery = 67% Analysis Date = 05/03/21 Pct Recovery = 67% Analysis Date = 05/03/21 Pct Recovery = 67% Analysis Date = 04/29/21 Pct Recovery = 67% Analysis Date = 04/29/21 Pct Recovery = 67% Analysis Date = 04/24/21 Pct Recovery = 67% Analysis Date = 04/24/21 Pct Recovery = 67% Analysis Date = 04/20/21 Pct Recovery = 67% Analysis Date = 04/20/21 Pct Recovery = 67% Analysis Date = 04/16/21 Pct Recovery = 67% Analysis Date = 04/16/21 Pct Recovery = 67% Analysis Date = 04/11/21 Pct Recovery = 67% Analysis Date = 04/11/21 Pct Recovery = 67% Analysis Date = 04/07/21 Pct Recovery = 68% Analysis Date = 04/07/21 Pct Recovery = 68% Analysis Date = 04/03/21 Pct Recovery = 68% Analysis Date = 04/03/21 Pct Recovery = 68% Analysis Date = 03/29/21 Pct Recovery = 69% Analysis Date = 03/29/21 Pct Recovery = 69% Analysis Date = 03/25/21 Pct Recovery = 69% Analysis Date = 03/25/21 Pct Recovery = 69% Analysis Date = 03/21/21 Pct Recovery = 70% Analysis Date = 03/21/21 Pct Recovery = 70% Analysis Date = 03/17/21 Pct Recovery = 71% Analysis Date = 03/17/21 Pct Recovery = 71% Analysis Date = 03/12/21 Pct Recovery = 71% Analysis Date = 03/12/21 Pct Recovery = 71% Analysis Date = 03/08/21 Pct Recovery = 72% Analysis Date = 03/08/21 Pct Recovery = 72% Analysis Date = 03/04/21 Pct Recovery = 72% Analysis Date = 03/04/21 Pct Recovery = 72% Analysis Date = 02/27/21 Pct Recovery = 73% Analysis Date = 02/27/21 Pct Recovery = 73% Analysis Date = 02/23/21 Pct Recovery = 74% Analysis Date = 02/23/21 Pct Recovery = 74% Analysis Date = 02/19/21 Pct Recovery = 74% Analysis Date = 02/19/21 Pct Recovery = 74% Analysis Date = 02/14/21 Pct Recovery = 75% Analysis Date = 02/14/21 Pct Recovery = 75% Analysis Date = 02/10/21 Pct Recovery = 75% Analysis Date = 02/10/21 Pct Recovery = 75% Analysis Date = 02/06/21 Pct Recovery = 76% Analysis Date = 02/06/21 Pct Recovery = 76% Analysis Date = 02/01/21 Pct Recovery = 77% Analysis Date = 02/01/21 Pct Recovery = 77% Analysis Date = 01/28/21 Pct Recovery = 77% Analysis Date = 01/28/21 Pct Recovery = 77% Analysis Date = 01/24/21 Pct Recovery = 78% Analysis Date = 01/24/21 Pct Recovery = 78% Analysis Date = 01/19/21 Pct Recovery = 78% Analysis Date = 01/19/21 Pct Recovery = 78% Analysis Date = 01/15/21 Pct Recovery = 79% Analysis Date = 01/15/21 Pct Recovery = 79% Analysis Date = 01/11/21 Pct Recovery = 79% Analysis Date = 01/11/21 Pct Recovery = 79% Analysis Date = 01/07/21 Pct Recovery = 80% Analysis Date = 01/07/21 Pct Recovery = 80% Analysis Date = 01/02/21 Pct Recovery = 80% Analysis Date = 01/02/21 Pct Recovery = 80% Analysis Date = 12/29/20 Pct Recovery = 81% Analysis Date = 12/29/20 Pct Recovery = 81% Analysis Date = 12/25/20 Pct Recovery = 81% Analysis Date = 12/25/20 Pct Recovery = 81% Analysis Date = 12/20/20 Pct Recovery = 82% Analysis Date = 12/20/20 Pct Recovery = 82% Analysis Date = 12/16/20 Pct Recovery = 83% Analysis Date = 12/16/20 Pct Recovery = 83% Analysis Date = 12/12/20 Pct Recovery = 83% Analysis Date = 12/12/20 Pct Recovery = 83% Analysis Date = 12/07/20 Pct Recovery = 84% Analysis Date = 12/07/20 Pct Recovery = 84% Analysis Date = 12/03/20 Pct Recovery = 85% Analysis Date = 12/03/20 Pct Recovery = 85% Analysis Date = 11/29/20 Pct Recovery = 85% Analysis Date = 11/29/20 Pct Recovery = 85% Analysis Date = 11/24/20 Pct Recovery = 86% Analysis Date = 11/24/20 Pct Recovery = 86% Analysis Date = 11/20/20 Pct Recovery = 87% Analysis Date = 11/20/20 Pct Recovery = 87% Analysis Date = 11/16/20 Pct Recovery = 87% Analysis Date = 11/16/20 Pct Recovery = 87% Analysis Date = 11/11/20 Pct Recovery = 88% Analysis Date = 11/11/20 Pct Recovery = 88% Analysis Date = 11/07/20 Pct Recovery = 89% Analysis Date = 11/07/20 Pct Recovery = 89% Analysis Date = 11/03/20 Pct Recovery = 89% Analysis Date = 11/03/20 Pct Recovery = 89% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/25/20 Pct Recovery = 91% Analysis Date = 10/25/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 92% Analysis Date = 10/17/20 Pct Recovery = 92% Analysis Date = 10/12/20 Pct Recovery = 92% Analysis Date = 10/12/20 Pct Recovery = 92% Analysis Date = 10/08/20 Pct Recovery = 93% Analysis Date = 10/08/20 Pct Recovery = 93% Analysis Date = 10/04/20 Pct Recovery = 94% Analysis Date = 10/04/20 Pct Recovery = 94% Analysis Date = 09/29/20 Pct Recovery = 94% Analysis Date = 09/29/20 Pct Recovery = 94% Analysis Date = 09/25/20 Pct Recovery = 95% Analysis Date = 09/25/20 Pct Recovery = 95% Analysis Date = 09/21/20 Pct Recovery = 95% Analysis Date = 09/21/20 Pct Recovery = 95% Analysis Date = 09/16/20 Pct Recovery = 95% Analysis Date = 09/16/20 Pct Recovery = 95% Analysis Date = 09/12/20 Pct Recovery = 95% Analysis Date = 09/12/20 Pct Recovery = 95% Analysis Date = 09/08/20 Pct Recovery = 95% Analysis Date = 09/08/20 Pct Recovery = 95% Analysis Date = 09/03/20 Pct Recovery = 95% Analysis Date = 09/03/20 Pct Recovery = 95% Analysis Date = 08/30/20 Pct Recovery = 95% Analysis Date = 08/30/20 Pct Recovery = 95% Analysis Date = 08/26/20 Pct Recovery = 96% Analysis Date = 08/26/20 Pct Recovery = 96% Analysis Date = 08/21/20 Pct Recovery = 96% Analysis Date = 08/21/20 Pct Recovery = 96% Analysis Date = 08/17/20 Pct Recovery = 96% Analysis Date = 08/17/20 Pct Recovery = 96% Analysis Date = 08/13/20 Pct Recovery = 96% Analysis Date = 08/13/20 Pct Recovery = 96% Analysis Date = 08/08/20 Pct Recovery = 96% Analysis Date = 08/08/20 Pct Recovery = 96% Analysis Date = 08/04/20 Pct Recovery = 96% Analysis Date = 08/04/20 Pct Recovery = 96% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 96% Analysis Date = 07/22/20 Pct Recovery = 96% Analysis Date = 07/22/20 Pct Recovery = 96% Analysis Date = 07/18/20 Pct Recovery = 96% Analysis Date = 07/18/20 Pct Recovery = 96% Analysis Date = 07/14/20 Pct Recovery = 96% Analysis Date = 07/14/20 Pct Recovery = 96% Analysis Date = 07/09/20 Pct Recovery = 96% Analysis Date = 07/09/20 Pct Recovery = 96% Analysis Date = 07/05/20 Pct Recovery = 96% Analysis Date = 07/05/20 Pct Recovery = 96% Analysis Date = 07/01/20 Pct Recovery = 96% Analysis Date = 07/01/20 Pct Recovery = 96% Analysis Date = 06/26/20 Pct Recovery = 96% Analysis Date = 06/26/20 Pct Recovery = 96% Analysis Date = 06/22/20 Pct Recovery = 96% Analysis Date = 06/22/20 Pct Recovery = 96% Analysis Date = 06/18/20 Pct Recovery = 96% Analysis Date = 06/18/20 Pct Recovery = 96% Analysis Date = 06/13/20 Pct Recovery = 96% Analysis Date = 06/13/20 Pct Recovery = 96% Analysis Date = 06/09/20 Pct Recovery = 97% Analysis Date = 06/09/20 Pct Recovery = 97% Analysis Date = 06/05/20 Pct Recovery = 97% Analysis Date = 06/05/20 Pct Recovery = 97% Analysis Date = 05/31/20 Pct Recovery = 97% Analysis Date = 05/31/20 Pct Recovery = 97% Analysis Date = 05/27/20 Pct Recovery = 97% Analysis Date = 05/27/20 Pct Recovery = 97% Analysis Date = 05/23/20 Pct Recovery = 97% Analysis Date = 05/23/20 Pct Recovery = 97% Analysis Date = 05/19/20 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HALOSULFURON-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 82% 27% 86% 27%
Total 35 82% 27% 86% 27%

Sample Statistics
HALOSULFURON-METHYL

Characteristic N % % Basis
Plotted 35 83% Spiked
Estimated Values 7 17% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 42 .  
False Negatives 6 14% 6 out of 42
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

OBSP Determination:
HEXAZINONE
METHOD: 2447 , TESTIDCODE: 65085LCM60

Laboratory ID = 20202110006 Lab Value = 50.258 Expected Conc. = 45.6 Report level label = 3.6 Pct Recovery = 110% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 47.521 Expected Conc. = 45.5 Report level label = 3.6 Pct Recovery = 104% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203230021 Lab Value = 47.483 Expected Conc. = 45.3 Report level label = 3.6 Pct Recovery = 105% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 40.900 Expected Conc. = 45.3 Report level label = 3.6 Pct Recovery = 90% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 48.116 Expected Conc. = 45.2 Report level label = 3.6 Pct Recovery = 106% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 46.928 Expected Conc. = 45.2 Report level label = 3.6 Pct Recovery = 104% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222150192 Lab Value = 23.497 Expected Conc. = 36.6 Report level label = 3.6 Pct Recovery = 64% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 23.217 Expected Conc. = 36 Report level label = 3.6 Pct Recovery = 64% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221520237 Lab Value = 40.664 Expected Conc. = 36 Report level label = 3.6 Pct Recovery = 113% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20220740064 Lab Value = 17.169 Expected Conc. = 22.875 Report level label = 3.6 Pct Recovery = 75% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20201680155 Lab Value = 25.593 Expected Conc. = 22.8 Report level label = 3.6 Pct Recovery = 112% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 17.701 Expected Conc. = 22.75 Report level label = 3.6 Pct Recovery = 78% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 20.474 Expected Conc. = 22.75 Report level label = 3.6 Pct Recovery = 90% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 23.819 Expected Conc. = 22.75 Report level label = 3.6 Pct Recovery = 105% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20203230018 Lab Value = 22.089 Expected Conc. = 22.6 Report level label = 3.6 Pct Recovery = 98% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 24.510 Expected Conc. = 22.6 Report level label = 3.6 Pct Recovery = 108% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 25.555 Expected Conc. = 22.6 Report level label = 3.6 Pct Recovery = 113% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221870197 Lab Value = 18.516 Expected Conc. = 22.5 Report level label = 3.6 Pct Recovery = 82% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20201610160 Lab Value = 10.007 Expected Conc. = 9.12 Report level label = 3.6 Pct Recovery = 110% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 7.812 Expected Conc. = 9.1 Report level label = 3.6 Pct Recovery = 86% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 8.388 Expected Conc. = 9.1 Report level label = 3.6 Pct Recovery = 92% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 9.740 Expected Conc. = 9.1 Report level label = 3.6 Pct Recovery = 107% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 11.645 Expected Conc. = 9.1 Report level label = 3.6 Pct Recovery = 128% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210830019 Lab Value = 11.464 Expected Conc. = 9.06 Report level label = 3.6 Pct Recovery = 127% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 8.629 Expected Conc. = 9.06 Report level label = 3.6 Pct Recovery = 95% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 8.630 Expected Conc. = 9.04 Report level label = 3.6 Pct Recovery = 95% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 6.768 Expected Conc. = 9.04 Report level label = 3.6 Pct Recovery = 75% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 8.934 Expected Conc. = 9.04 Report level label = 3.6 Pct Recovery = 99% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 10.103 Expected Conc. = 9.04 Report level label = 3.6 Pct Recovery = 112% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 9.783 Expected Conc. = 9.04 Report level label = 3.6 Pct Recovery = 108% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 9.898 Expected Conc. = 9.04 Report level label = 3.6 Pct Recovery = 109% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221660151 Lab Value = 7.732 Expected Conc. = 9 Report level label = 3.6 Pct Recovery = 86% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Analysis Date = 08/15/22 Pct Recovery = 78% Analysis Date = 08/10/22 Pct Recovery = 78% Analysis Date = 08/10/22 Pct Recovery = 78% Analysis Date = 08/06/22 Pct Recovery = 79% Analysis Date = 08/06/22 Pct Recovery = 79% Analysis Date = 08/02/22 Pct Recovery = 79% Analysis Date = 08/02/22 Pct Recovery = 79% Analysis Date = 07/29/22 Pct Recovery = 79% Analysis Date = 07/29/22 Pct Recovery = 79% Analysis Date = 07/25/22 Pct Recovery = 79% Analysis Date = 07/25/22 Pct Recovery = 79% Analysis Date = 07/21/22 Pct Recovery = 79% Analysis Date = 07/21/22 Pct Recovery = 79% Analysis Date = 07/17/22 Pct Recovery = 79% Analysis Date = 07/17/22 Pct Recovery = 79% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/01/22 Pct Recovery = 80% Analysis Date = 07/01/22 Pct Recovery = 80% Analysis Date = 06/26/22 Pct Recovery = 80% Analysis Date = 06/26/22 Pct Recovery = 80% Analysis Date = 06/22/22 Pct Recovery = 81% Analysis Date = 06/22/22 Pct Recovery = 81% Analysis Date = 06/18/22 Pct Recovery = 81% Analysis Date = 06/18/22 Pct Recovery = 81% Analysis Date = 06/14/22 Pct Recovery = 81% Analysis Date = 06/14/22 Pct Recovery = 81% Analysis Date = 06/10/22 Pct Recovery = 81% Analysis Date = 06/10/22 Pct Recovery = 81% Analysis Date = 06/06/22 Pct Recovery = 81% Analysis Date = 06/06/22 Pct Recovery = 81% Analysis Date = 06/02/22 Pct Recovery = 82% Analysis Date = 06/02/22 Pct Recovery = 82% Analysis Date = 05/29/22 Pct Recovery = 82% Analysis Date = 05/29/22 Pct Recovery = 82% Analysis Date = 05/25/22 Pct Recovery = 82% Analysis Date = 05/25/22 Pct Recovery = 82% Analysis Date = 05/21/22 Pct Recovery = 82% Analysis Date = 05/21/22 Pct Recovery = 82% Analysis Date = 05/17/22 Pct Recovery = 82% Analysis Date = 05/17/22 Pct Recovery = 82% Analysis Date = 05/12/22 Pct Recovery = 82% Analysis Date = 05/12/22 Pct Recovery = 82% Analysis Date = 05/08/22 Pct Recovery = 83% Analysis Date = 05/08/22 Pct Recovery = 83% Analysis Date = 05/04/22 Pct Recovery = 83% Analysis Date = 05/04/22 Pct Recovery = 83% Analysis Date = 04/30/22 Pct Recovery = 83% Analysis Date = 04/30/22 Pct Recovery = 83% Analysis Date = 04/26/22 Pct Recovery = 83% Analysis Date = 04/26/22 Pct Recovery = 83% Analysis Date = 04/22/22 Pct Recovery = 83% Analysis Date = 04/22/22 Pct Recovery = 83% Analysis Date = 04/18/22 Pct Recovery = 83% Analysis Date = 04/18/22 Pct Recovery = 83% Analysis Date = 04/14/22 Pct Recovery = 84% Analysis Date = 04/14/22 Pct Recovery = 84% Analysis Date = 04/10/22 Pct Recovery = 84% Analysis Date = 04/10/22 Pct Recovery = 84% Analysis Date = 04/06/22 Pct Recovery = 84% Analysis Date = 04/06/22 Pct Recovery = 84% Analysis Date = 04/02/22 Pct Recovery = 84% Analysis Date = 04/02/22 Pct Recovery = 84% Analysis Date = 03/28/22 Pct Recovery = 84% Analysis Date = 03/28/22 Pct Recovery = 84% Analysis Date = 03/24/22 Pct Recovery = 85% Analysis Date = 03/24/22 Pct Recovery = 85% Analysis Date = 03/20/22 Pct Recovery = 85% Analysis Date = 03/20/22 Pct Recovery = 85% Analysis Date = 03/16/22 Pct Recovery = 85% Analysis Date = 03/16/22 Pct Recovery = 85% Analysis Date = 03/12/22 Pct Recovery = 85% Analysis Date = 03/12/22 Pct Recovery = 85% Analysis Date = 03/08/22 Pct Recovery = 85% Analysis Date = 03/08/22 Pct Recovery = 85% Analysis Date = 03/04/22 Pct Recovery = 85% Analysis Date = 03/04/22 Pct Recovery = 85% Analysis Date = 02/28/22 Pct Recovery = 86% Analysis Date = 02/28/22 Pct Recovery = 86% Analysis Date = 02/24/22 Pct Recovery = 86% Analysis Date = 02/24/22 Pct Recovery = 86% Analysis Date = 02/20/22 Pct Recovery = 86% Analysis Date = 02/20/22 Pct Recovery = 86% Analysis Date = 02/16/22 Pct Recovery = 86% Analysis Date = 02/16/22 Pct Recovery = 86% Analysis Date = 02/11/22 Pct Recovery = 86% Analysis Date = 02/11/22 Pct Recovery = 86% Analysis Date = 02/07/22 Pct Recovery = 86% Analysis Date = 02/07/22 Pct Recovery = 86% Analysis Date = 02/03/22 Pct Recovery = 87% Analysis Date = 02/03/22 Pct Recovery = 87% Analysis Date = 01/30/22 Pct Recovery = 87% Analysis Date = 01/30/22 Pct Recovery = 87% Analysis Date = 01/26/22 Pct Recovery = 87% Analysis Date = 01/26/22 Pct Recovery = 87% Analysis Date = 01/22/22 Pct Recovery = 87% Analysis Date = 01/22/22 Pct Recovery = 87% Analysis Date = 01/18/22 Pct Recovery = 87% Analysis Date = 01/18/22 Pct Recovery = 87% Analysis Date = 01/14/22 Pct Recovery = 88% Analysis Date = 01/14/22 Pct Recovery = 88% Analysis Date = 01/10/22 Pct Recovery = 88% Analysis Date = 01/10/22 Pct Recovery = 88% Analysis Date = 01/06/22 Pct Recovery = 88% Analysis Date = 01/06/22 Pct Recovery = 88% Analysis Date = 01/02/22 Pct Recovery = 88% Analysis Date = 01/02/22 Pct Recovery = 88% Analysis Date = 12/28/21 Pct Recovery = 88% Analysis Date = 12/28/21 Pct Recovery = 88% Analysis Date = 12/24/21 Pct Recovery = 88% Analysis Date = 12/24/21 Pct Recovery = 88% Analysis Date = 12/20/21 Pct Recovery = 89% Analysis Date = 12/20/21 Pct Recovery = 89% Analysis Date = 12/16/21 Pct Recovery = 89% Analysis Date = 12/16/21 Pct Recovery = 89% Analysis Date = 12/12/21 Pct Recovery = 89% Analysis Date = 12/12/21 Pct Recovery = 89% Analysis Date = 12/08/21 Pct Recovery = 89% Analysis Date = 12/08/21 Pct Recovery = 89% Analysis Date = 12/04/21 Pct Recovery = 89% Analysis Date = 12/04/21 Pct Recovery = 89% Analysis Date = 11/30/21 Pct Recovery = 89% Analysis Date = 11/30/21 Pct Recovery = 89% Analysis Date = 11/26/21 Pct Recovery = 90% Analysis Date = 11/26/21 Pct Recovery = 90% Analysis Date = 11/22/21 Pct Recovery = 90% Analysis Date = 11/22/21 Pct Recovery = 90% Analysis Date = 11/18/21 Pct Recovery = 90% Analysis Date = 11/18/21 Pct Recovery = 90% Analysis Date = 11/13/21 Pct Recovery = 90% Analysis Date = 11/13/21 Pct Recovery = 90% Analysis Date = 11/09/21 Pct Recovery = 90% Analysis Date = 11/09/21 Pct Recovery = 90% Analysis Date = 11/05/21 Pct Recovery = 91% Analysis Date = 11/05/21 Pct Recovery = 91% Analysis Date = 11/01/21 Pct Recovery = 91% Analysis Date = 11/01/21 Pct Recovery = 91% Analysis Date = 10/28/21 Pct Recovery = 91% Analysis Date = 10/28/21 Pct Recovery = 91% Analysis Date = 10/24/21 Pct Recovery = 91% Analysis Date = 10/24/21 Pct Recovery = 91% Analysis Date = 10/20/21 Pct Recovery = 91% Analysis Date = 10/20/21 Pct Recovery = 91% Analysis Date = 10/16/21 Pct Recovery = 91% Analysis Date = 10/16/21 Pct Recovery = 91% Analysis Date = 10/12/21 Pct Recovery = 92% Analysis Date = 10/12/21 Pct Recovery = 92% Analysis Date = 10/08/21 Pct Recovery = 92% Analysis Date = 10/08/21 Pct Recovery = 92% Analysis Date = 10/04/21 Pct Recovery = 92% Analysis Date = 10/04/21 Pct Recovery = 92% Analysis Date = 09/29/21 Pct Recovery = 92% Analysis Date = 09/29/21 Pct Recovery = 92% Analysis Date = 09/25/21 Pct Recovery = 92% Analysis Date = 09/25/21 Pct Recovery = 92% Analysis Date = 09/21/21 Pct Recovery = 92% Analysis Date = 09/21/21 Pct Recovery = 92% Analysis Date = 09/17/21 Pct Recovery = 93% Analysis Date = 09/17/21 Pct Recovery = 93% Analysis Date = 09/13/21 Pct Recovery = 93% Analysis Date = 09/13/21 Pct Recovery = 93% Analysis Date = 09/09/21 Pct Recovery = 93% Analysis Date = 09/09/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 94% Analysis Date = 08/28/21 Pct Recovery = 94% Analysis Date = 08/24/21 Pct Recovery = 94% Analysis Date = 08/24/21 Pct Recovery = 94% Analysis Date = 08/20/21 Pct Recovery = 94% Analysis Date = 08/20/21 Pct Recovery = 94% Analysis Date = 08/15/21 Pct Recovery = 94% Analysis Date = 08/15/21 Pct Recovery = 94% Analysis Date = 08/11/21 Pct Recovery = 94% Analysis Date = 08/11/21 Pct Recovery = 94% Analysis Date = 08/07/21 Pct Recovery = 94% Analysis Date = 08/07/21 Pct Recovery = 94% Analysis Date = 08/03/21 Pct Recovery = 95% Analysis Date = 08/03/21 Pct Recovery = 95% Analysis Date = 07/30/21 Pct Recovery = 95% Analysis Date = 07/30/21 Pct Recovery = 95% Analysis Date = 07/26/21 Pct Recovery = 95% Analysis Date = 07/26/21 Pct Recovery = 95% Analysis Date = 07/22/21 Pct Recovery = 95% Analysis Date = 07/22/21 Pct Recovery = 95% Analysis Date = 07/18/21 Pct Recovery = 95% Analysis Date = 07/18/21 Pct Recovery = 95% Analysis Date = 07/14/21 Pct Recovery = 95% Analysis Date = 07/14/21 Pct Recovery = 95% Analysis Date = 07/10/21 Pct Recovery = 96% Analysis Date = 07/10/21 Pct Recovery = 96% Analysis Date = 07/06/21 Pct Recovery = 96% Analysis Date = 07/06/21 Pct Recovery = 96% Analysis Date = 07/02/21 Pct Recovery = 96% Analysis Date = 07/02/21 Pct Recovery = 96% Analysis Date = 06/27/21 Pct Recovery = 96% Analysis Date = 06/27/21 Pct Recovery = 96% Analysis Date = 06/23/21 Pct Recovery = 96% Analysis Date = 06/23/21 Pct Recovery = 96% Analysis Date = 06/19/21 Pct Recovery = 97% Analysis Date = 06/19/21 Pct Recovery = 97% Analysis Date = 06/15/21 Pct Recovery = 97% Analysis Date = 06/15/21 Pct Recovery = 97% Analysis Date = 06/11/21 Pct Recovery = 97% Analysis Date = 06/11/21 Pct Recovery = 97% Analysis Date = 06/07/21 Pct Recovery = 97% Analysis Date = 06/07/21 Pct Recovery = 97% Analysis Date = 06/03/21 Pct Recovery = 97% Analysis Date = 06/03/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 98% Analysis Date = 05/26/21 Pct Recovery = 98% Analysis Date = 05/22/21 Pct Recovery = 98% Analysis Date = 05/22/21 Pct Recovery = 98% Analysis Date = 05/18/21 Pct Recovery = 98% Analysis Date = 05/18/21 Pct Recovery = 98% Analysis Date = 05/13/21 Pct Recovery = 98% Analysis Date = 05/13/21 Pct Recovery = 98% Analysis Date = 05/09/21 Pct Recovery = 98% Analysis Date = 05/09/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/01/21 Pct Recovery = 99% Analysis Date = 05/01/21 Pct Recovery = 99% Analysis Date = 04/27/21 Pct Recovery = 99% Analysis Date = 04/27/21 Pct Recovery = 99% Analysis Date = 04/23/21 Pct Recovery = 99% Analysis Date = 04/23/21 Pct Recovery = 99% Analysis Date = 04/19/21 Pct Recovery = 99% Analysis Date = 04/19/21 Pct Recovery = 99% Analysis Date = 04/15/21 Pct Recovery = 99% Analysis Date = 04/15/21 Pct Recovery = 99% Analysis Date = 04/11/21 Pct Recovery = 99% Analysis Date = 04/11/21 Pct Recovery = 99% Analysis Date = 04/07/21 Pct Recovery = 99% Analysis Date = 04/07/21 Pct Recovery = 99% Analysis Date = 04/03/21 Pct Recovery = 100% Analysis Date = 04/03/21 Pct Recovery = 100% Analysis Date = 03/29/21 Pct Recovery = 100% Analysis Date = 03/29/21 Pct Recovery = 100% Analysis Date = 03/25/21 Pct Recovery = 100% Analysis Date = 03/25/21 Pct Recovery = 100% Analysis Date = 03/21/21 Pct Recovery = 100% Analysis Date = 03/21/21 Pct Recovery = 100% Analysis Date = 03/17/21 Pct Recovery = 100% Analysis Date = 03/17/21 Pct Recovery = 100% Analysis Date = 03/13/21 Pct Recovery = 100% Analysis Date = 03/13/21 Pct Recovery = 100% Analysis Date = 03/09/21 Pct Recovery = 100% Analysis Date = 03/09/21 Pct Recovery = 100% Analysis Date = 03/05/21 Pct Recovery = 100% Analysis Date = 03/05/21 Pct Recovery = 100% Analysis Date = 03/01/21 Pct Recovery = 100% Analysis Date = 03/01/21 Pct Recovery = 100% Analysis Date = 02/25/21 Pct Recovery = 100% Analysis Date = 02/25/21 Pct Recovery = 100% Analysis Date = 02/21/21 Pct Recovery = 100% Analysis Date = 02/21/21 Pct Recovery = 100% Analysis Date = 02/17/21 Pct Recovery = 100% Analysis Date = 02/17/21 Pct Recovery = 100% Analysis Date = 02/12/21 Pct Recovery = 100% Analysis Date = 02/12/21 Pct Recovery = 100% Analysis Date = 02/08/21 Pct Recovery = 100% Analysis Date = 02/08/21 Pct Recovery = 100% Analysis Date = 02/04/21 Pct Recovery = 100% Analysis Date = 02/04/21 Pct Recovery = 100% Analysis Date = 01/31/21 Pct Recovery = 101% Analysis Date = 01/31/21 Pct Recovery = 101% Analysis Date = 01/27/21 Pct Recovery = 101% Analysis Date = 01/27/21 Pct Recovery = 101% Analysis Date = 01/23/21 Pct Recovery = 101% Analysis Date = 01/23/21 Pct Recovery = 101% Analysis Date = 01/19/21 Pct Recovery = 101% Analysis Date = 01/19/21 Pct Recovery = 101% Analysis Date = 01/15/21 Pct Recovery = 101% Analysis Date = 01/15/21 Pct Recovery = 101% Analysis Date = 01/11/21 Pct Recovery = 101% Analysis Date = 01/11/21 Pct Recovery = 101% Analysis Date = 01/07/21 Pct Recovery = 101% Analysis Date = 01/07/21 Pct Recovery = 101% Analysis Date = 01/03/21 Pct Recovery = 101% Analysis Date = 01/03/21 Pct Recovery = 101% Analysis Date = 12/29/20 Pct Recovery = 101% Analysis Date = 12/29/20 Pct Recovery = 101% Analysis Date = 12/25/20 Pct Recovery = 101% Analysis Date = 12/25/20 Pct Recovery = 101% Analysis Date = 12/21/20 Pct Recovery = 101% Analysis Date = 12/21/20 Pct Recovery = 101% Analysis Date = 12/17/20 Pct Recovery = 101% Analysis Date = 12/17/20 Pct Recovery = 101% Analysis Date = 12/13/20 Pct Recovery = 101% Analysis Date = 12/13/20 Pct Recovery = 101% Analysis Date = 12/09/20 Pct Recovery = 101% Analysis Date = 12/09/20 Pct Recovery = 101% Analysis Date = 12/05/20 Pct Recovery = 101% Analysis Date = 12/05/20 Pct Recovery = 101% Analysis Date = 12/01/20 Pct Recovery = 102% Analysis Date = 12/01/20 Pct Recovery = 102% Analysis Date = 11/27/20 Pct Recovery = 102% Analysis Date = 11/27/20 Pct Recovery = 102% Analysis Date = 11/23/20 Pct Recovery = 102% Analysis Date = 11/23/20 Pct Recovery = 102% Analysis Date = 11/19/20 Pct Recovery = 102% Analysis Date = 11/19/20 Pct Recovery = 102% Analysis Date = 11/14/20 Pct Recovery = 103% Analysis Date = 11/14/20 Pct Recovery = 103% Analysis Date = 11/10/20 Pct Recovery = 103% Analysis Date = 11/10/20 Pct Recovery = 103% Analysis Date = 11/06/20 Pct Recovery = 103% Analysis Date = 11/06/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 103% Analysis Date = 10/17/20 Pct Recovery = 103% Analysis Date = 10/17/20 Pct Recovery = 103% Analysis Date = 10/13/20 Pct Recovery = 102% Analysis Date = 10/13/20 Pct Recovery = 102% Analysis Date = 10/09/20 Pct Recovery = 102% Analysis Date = 10/09/20 Pct Recovery = 102% Analysis Date = 10/05/20 Pct Recovery = 102% Analysis Date = 10/05/20 Pct Recovery = 102% Analysis Date = 09/30/20 Pct Recovery = 102% Analysis Date = 09/30/20 Pct Recovery = 102% Analysis Date = 09/26/20 Pct Recovery = 102% Analysis Date = 09/26/20 Pct Recovery = 102% Analysis Date = 09/22/20 Pct Recovery = 102% Analysis Date = 09/22/20 Pct Recovery = 102% Analysis Date = 09/18/20 Pct Recovery = 102% Analysis Date = 09/18/20 Pct Recovery = 102% Analysis Date = 09/14/20 Pct Recovery = 101% Analysis Date = 09/14/20 Pct Recovery = 101% Analysis Date = 09/10/20 Pct Recovery = 101% Analysis Date = 09/10/20 Pct Recovery = 101% Analysis Date = 09/06/20 Pct Recovery = 101% Analysis Date = 09/06/20 Pct Recovery = 101% Analysis Date = 09/02/20 Pct Recovery = 101% Analysis Date = 09/02/20 Pct Recovery = 101% Analysis Date = 08/29/20 Pct Recovery = 101% Analysis Date = 08/29/20 Pct Recovery = 101% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 102% Analysis Date = 08/21/20 Pct Recovery = 102% Analysis Date = 08/16/20 Pct Recovery = 102% Analysis Date = 08/16/20 Pct Recovery = 102% Analysis Date = 08/12/20 Pct Recovery = 103% Analysis Date = 08/12/20 Pct Recovery = 103% Analysis Date = 08/08/20 Pct Recovery = 103% Analysis Date = 08/08/20 Pct Recovery = 103% Analysis Date = 08/04/20 Pct Recovery = 103% Analysis Date = 08/04/20 Pct Recovery = 103% Analysis Date = 07/31/20 Pct Recovery = 104% Analysis Date = 07/31/20 Pct Recovery = 104% Analysis Date = 07/27/20 Pct Recovery = 104% Analysis Date = 07/27/20 Pct Recovery = 104% Analysis Date = 07/23/20 Pct Recovery = 105% Analysis Date = 07/23/20 Pct Recovery = 105% Analysis Date = 07/19/20 Pct Recovery = 105% Analysis Date = 07/19/20 Pct Recovery = 105% Analysis Date = 07/15/20 Pct Recovery = 106% Analysis Date = 07/15/20 Pct Recovery = 106% Analysis Date = 07/11/20 Pct Recovery = 106% Analysis Date = 07/11/20 Pct Recovery = 106% Analysis Date = 07/07/20 Pct Recovery = 107% Analysis Date = 07/07/20 Pct Recovery = 107% Analysis Date = 07/02/20 Pct Recovery = 107% Analysis Date = 07/02/20 Pct Recovery = 107% Analysis Date = 06/28/20 Pct Recovery = 108% Analysis Date = 06/28/20 Pct Recovery = 108% Analysis Date = 06/24/20 Pct Recovery = 108% Analysis Date = 06/24/20 Pct Recovery = 108% Analysis Date = 06/20/20 Pct Recovery = 109% Analysis Date = 06/20/20 Pct Recovery = 109% Analysis Date = 06/16/20 Pct Recovery = 109% Analysis Date = 06/16/20 Pct Recovery = 109% Analysis Date = 06/12/20 Pct Recovery = 110% Analysis Date = 06/12/20 Pct Recovery = 110% Analysis Date = 06/08/20 Pct Recovery = 110% Analysis Date = 06/08/20 Pct Recovery = 110% Analysis Date = 06/04/20 Pct Recovery = 111% Analysis Date = 06/04/20 Pct Recovery = 111% Analysis Date = 05/31/20 Pct Recovery = 111% Analysis Date = 05/31/20 Pct Recovery = 111% Analysis Date = 05/27/20 Pct Recovery = 112% Analysis Date = 05/27/20 Pct Recovery = 112% Analysis Date = 05/23/20 Pct Recovery = 113% Analysis Date = 05/23/20 Pct Recovery = 113% Analysis Date = 05/19/20 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXAZINONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 99% 16% 104% 16%
Total 32 99% 16% 104% 16%

Sample Statistics
HEXAZINONE

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 4 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 84 .  
False Positives 1 1% 1 out of 84

OBSP Determination:
HYDROXYMETOLACHLOR
METHOD: 2447 , TESTIDCODE: 68622LCM60

Laboratory ID = 20203080100 Lab Value = 29.328 Expected Conc. = 30 Report level label = 2.4 Pct Recovery = 98% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 28.237 Expected Conc. = 30 Report level label = 2.4 Pct Recovery = 94% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 25.939 Expected Conc. = 30 Report level label = 2.4 Pct Recovery = 86% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221940195 Lab Value = 20.166 Expected Conc. = 24 Report level label = 2.4 Pct Recovery = 84% Analysis Date = 07/23/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20202880004 Lab Value = 17.454 Expected Conc. = 15 Report level label = 2.4 Pct Recovery = 116% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202390020 Lab Value = 17.410 Expected Conc. = 14.95 Report level label = 2.4 Pct Recovery = 116% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 17.300 Expected Conc. = 14.95 Report level label = 2.4 Pct Recovery = 116% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201550031 Lab Value = 14.845 Expected Conc. = 14.85 Report level label = 2.4 Pct Recovery = 100% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20210620006 Lab Value = 16.763 Expected Conc. = 12 Report level label = 2.4 Pct Recovery = 140% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 16.551 Expected Conc. = 12 Report level label = 2.4 Pct Recovery = 138% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 13.783 Expected Conc. = 11.96 Report level label = 2.4 Pct Recovery = 115% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 11.632 Expected Conc. = 11.96 Report level label = 2.4 Pct Recovery = 97% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210120050 Lab Value = 6.590 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 110% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 4.965 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 83% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 10.251 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 171% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 8.248 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 137% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 5.645 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 94% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202330309 Lab Value = 3.542 Expected Conc. = 5.94 Report level label = 2.4 Pct Recovery = 60% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 6.820 Expected Conc. = 5.94 Report level label = 2.4 Pct Recovery = 115% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 6.771 Expected Conc. = 5.94 Report level label = 2.4 Pct Recovery = 114% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 7.256 Expected Conc. = 5.94 Report level label = 2.4 Pct Recovery = 122% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Analysis Date = 07/22/22 Pct Recovery = 84% Analysis Date = 07/19/22 Pct Recovery = 85% Analysis Date = 07/19/22 Pct Recovery = 85% Analysis Date = 07/15/22 Pct Recovery = 85% Analysis Date = 07/15/22 Pct Recovery = 85% Analysis Date = 07/11/22 Pct Recovery = 85% Analysis Date = 07/11/22 Pct Recovery = 85% Analysis Date = 07/07/22 Pct Recovery = 86% Analysis Date = 07/07/22 Pct Recovery = 86% Analysis Date = 07/03/22 Pct Recovery = 86% Analysis Date = 07/03/22 Pct Recovery = 86% Analysis Date = 06/29/22 Pct Recovery = 86% Analysis Date = 06/29/22 Pct Recovery = 86% Analysis Date = 06/25/22 Pct Recovery = 87% Analysis Date = 06/25/22 Pct Recovery = 87% Analysis Date = 06/21/22 Pct Recovery = 87% Analysis Date = 06/21/22 Pct Recovery = 87% Analysis Date = 06/17/22 Pct Recovery = 87% Analysis Date = 06/17/22 Pct Recovery = 87% Analysis Date = 06/13/22 Pct Recovery = 88% Analysis Date = 06/13/22 Pct Recovery = 88% Analysis Date = 06/09/22 Pct Recovery = 88% Analysis Date = 06/09/22 Pct Recovery = 88% Analysis Date = 06/05/22 Pct Recovery = 88% Analysis Date = 06/05/22 Pct Recovery = 88% Analysis Date = 06/01/22 Pct Recovery = 89% Analysis Date = 06/01/22 Pct Recovery = 89% Analysis Date = 05/29/22 Pct Recovery = 89% Analysis Date = 05/29/22 Pct Recovery = 89% Analysis Date = 05/25/22 Pct Recovery = 89% Analysis Date = 05/25/22 Pct Recovery = 89% Analysis Date = 05/21/22 Pct Recovery = 89% Analysis Date = 05/21/22 Pct Recovery = 89% Analysis Date = 05/17/22 Pct Recovery = 90% Analysis Date = 05/17/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/05/22 Pct Recovery = 91% Analysis Date = 05/05/22 Pct Recovery = 91% Analysis Date = 05/01/22 Pct Recovery = 91% Analysis Date = 05/01/22 Pct Recovery = 91% Analysis Date = 04/27/22 Pct Recovery = 91% Analysis Date = 04/27/22 Pct Recovery = 91% Analysis Date = 04/23/22 Pct Recovery = 92% Analysis Date = 04/23/22 Pct Recovery = 92% Analysis Date = 04/19/22 Pct Recovery = 92% Analysis Date = 04/19/22 Pct Recovery = 92% Analysis Date = 04/15/22 Pct Recovery = 92% Analysis Date = 04/15/22 Pct Recovery = 92% Analysis Date = 04/11/22 Pct Recovery = 93% Analysis Date = 04/11/22 Pct Recovery = 93% Analysis Date = 04/08/22 Pct Recovery = 93% Analysis Date = 04/08/22 Pct Recovery = 93% Analysis Date = 04/04/22 Pct Recovery = 93% Analysis Date = 04/04/22 Pct Recovery = 93% Analysis Date = 03/31/22 Pct Recovery = 94% Analysis Date = 03/31/22 Pct Recovery = 94% Analysis Date = 03/27/22 Pct Recovery = 94% Analysis Date = 03/27/22 Pct Recovery = 94% Analysis Date = 03/23/22 Pct Recovery = 94% Analysis Date = 03/23/22 Pct Recovery = 94% Analysis Date = 03/19/22 Pct Recovery = 95% Analysis Date = 03/19/22 Pct Recovery = 95% Analysis Date = 03/15/22 Pct Recovery = 95% Analysis Date = 03/15/22 Pct Recovery = 95% Analysis Date = 03/11/22 Pct Recovery = 95% Analysis Date = 03/11/22 Pct Recovery = 95% Analysis Date = 03/07/22 Pct Recovery = 96% Analysis Date = 03/07/22 Pct Recovery = 96% Analysis Date = 03/03/22 Pct Recovery = 96% Analysis Date = 03/03/22 Pct Recovery = 96% Analysis Date = 02/27/22 Pct Recovery = 96% Analysis Date = 02/27/22 Pct Recovery = 96% Analysis Date = 02/23/22 Pct Recovery = 97% Analysis Date = 02/23/22 Pct Recovery = 97% Analysis Date = 02/19/22 Pct Recovery = 97% Analysis Date = 02/19/22 Pct Recovery = 97% Analysis Date = 02/15/22 Pct Recovery = 97% Analysis Date = 02/15/22 Pct Recovery = 97% Analysis Date = 02/12/22 Pct Recovery = 98% Analysis Date = 02/12/22 Pct Recovery = 98% Analysis Date = 02/08/22 Pct Recovery = 98% Analysis Date = 02/08/22 Pct Recovery = 98% Analysis Date = 02/04/22 Pct Recovery = 98% Analysis Date = 02/04/22 Pct Recovery = 98% Analysis Date = 01/31/22 Pct Recovery = 99% Analysis Date = 01/31/22 Pct Recovery = 99% Analysis Date = 01/27/22 Pct Recovery = 99% Analysis Date = 01/27/22 Pct Recovery = 99% Analysis Date = 01/23/22 Pct Recovery = 99% Analysis Date = 01/23/22 Pct Recovery = 99% Analysis Date = 01/19/22 Pct Recovery = 99% Analysis Date = 01/19/22 Pct Recovery = 99% Analysis Date = 01/15/22 Pct Recovery = 100% Analysis Date = 01/15/22 Pct Recovery = 100% Analysis Date = 01/11/22 Pct Recovery = 100% Analysis Date = 01/11/22 Pct Recovery = 100% Analysis Date = 01/07/22 Pct Recovery = 100% Analysis Date = 01/07/22 Pct Recovery = 100% Analysis Date = 01/03/22 Pct Recovery = 101% Analysis Date = 01/03/22 Pct Recovery = 101% Analysis Date = 12/30/21 Pct Recovery = 101% Analysis Date = 12/30/21 Pct Recovery = 101% Analysis Date = 12/26/21 Pct Recovery = 101% Analysis Date = 12/26/21 Pct Recovery = 101% Analysis Date = 12/23/21 Pct Recovery = 102% Analysis Date = 12/23/21 Pct Recovery = 102% Analysis Date = 12/19/21 Pct Recovery = 102% Analysis Date = 12/19/21 Pct Recovery = 102% Analysis Date = 12/15/21 Pct Recovery = 102% Analysis Date = 12/15/21 Pct Recovery = 102% Analysis Date = 12/11/21 Pct Recovery = 103% Analysis Date = 12/11/21 Pct Recovery = 103% Analysis Date = 12/07/21 Pct Recovery = 103% Analysis Date = 12/07/21 Pct Recovery = 103% Analysis Date = 12/03/21 Pct Recovery = 103% Analysis Date = 12/03/21 Pct Recovery = 103% Analysis Date = 11/29/21 Pct Recovery = 104% Analysis Date = 11/29/21 Pct Recovery = 104% Analysis Date = 11/25/21 Pct Recovery = 104% Analysis Date = 11/25/21 Pct Recovery = 104% Analysis Date = 11/21/21 Pct Recovery = 104% Analysis Date = 11/21/21 Pct Recovery = 104% Analysis Date = 11/17/21 Pct Recovery = 105% Analysis Date = 11/17/21 Pct Recovery = 105% Analysis Date = 11/13/21 Pct Recovery = 105% Analysis Date = 11/13/21 Pct Recovery = 105% Analysis Date = 11/09/21 Pct Recovery = 105% Analysis Date = 11/09/21 Pct Recovery = 105% Analysis Date = 11/05/21 Pct Recovery = 106% Analysis Date = 11/05/21 Pct Recovery = 106% Analysis Date = 11/02/21 Pct Recovery = 106% Analysis Date = 11/02/21 Pct Recovery = 106% Analysis Date = 10/29/21 Pct Recovery = 106% Analysis Date = 10/29/21 Pct Recovery = 106% Analysis Date = 10/25/21 Pct Recovery = 107% Analysis Date = 10/25/21 Pct Recovery = 107% Analysis Date = 10/21/21 Pct Recovery = 107% Analysis Date = 10/21/21 Pct Recovery = 107% Analysis Date = 10/17/21 Pct Recovery = 107% Analysis Date = 10/17/21 Pct Recovery = 107% Analysis Date = 10/13/21 Pct Recovery = 108% Analysis Date = 10/13/21 Pct Recovery = 108% Analysis Date = 10/09/21 Pct Recovery = 108% Analysis Date = 10/09/21 Pct Recovery = 108% Analysis Date = 10/05/21 Pct Recovery = 108% Analysis Date = 10/05/21 Pct Recovery = 108% Analysis Date = 10/01/21 Pct Recovery = 109% Analysis Date = 10/01/21 Pct Recovery = 109% Analysis Date = 09/27/21 Pct Recovery = 109% Analysis Date = 09/27/21 Pct Recovery = 109% Analysis Date = 09/23/21 Pct Recovery = 109% Analysis Date = 09/23/21 Pct Recovery = 109% Analysis Date = 09/19/21 Pct Recovery = 109% Analysis Date = 09/19/21 Pct Recovery = 109% Analysis Date = 09/15/21 Pct Recovery = 110% Analysis Date = 09/15/21 Pct Recovery = 110% Analysis Date = 09/11/21 Pct Recovery = 110% Analysis Date = 09/11/21 Pct Recovery = 110% Analysis Date = 09/08/21 Pct Recovery = 110% Analysis Date = 09/08/21 Pct Recovery = 110% Analysis Date = 09/04/21 Pct Recovery = 111% Analysis Date = 09/04/21 Pct Recovery = 111% Analysis Date = 08/31/21 Pct Recovery = 111% Analysis Date = 08/31/21 Pct Recovery = 111% Analysis Date = 08/27/21 Pct Recovery = 111% Analysis Date = 08/27/21 Pct Recovery = 111% Analysis Date = 08/23/21 Pct Recovery = 112% Analysis Date = 08/23/21 Pct Recovery = 112% Analysis Date = 08/19/21 Pct Recovery = 112% Analysis Date = 08/19/21 Pct Recovery = 112% Analysis Date = 08/15/21 Pct Recovery = 112% Analysis Date = 08/15/21 Pct Recovery = 112% Analysis Date = 08/11/21 Pct Recovery = 113% Analysis Date = 08/11/21 Pct Recovery = 113% Analysis Date = 08/07/21 Pct Recovery = 113% Analysis Date = 08/07/21 Pct Recovery = 113% Analysis Date = 08/03/21 Pct Recovery = 113% Analysis Date = 08/03/21 Pct Recovery = 113% Analysis Date = 07/30/21 Pct Recovery = 114% Analysis Date = 07/30/21 Pct Recovery = 114% Analysis Date = 07/26/21 Pct Recovery = 114% Analysis Date = 07/26/21 Pct Recovery = 114% Analysis Date = 07/22/21 Pct Recovery = 114% Analysis Date = 07/22/21 Pct Recovery = 114% Analysis Date = 07/19/21 Pct Recovery = 115% Analysis Date = 07/19/21 Pct Recovery = 115% Analysis Date = 07/15/21 Pct Recovery = 115% Analysis Date = 07/15/21 Pct Recovery = 115% Analysis Date = 07/11/21 Pct Recovery = 115% Analysis Date = 07/11/21 Pct Recovery = 115% Analysis Date = 07/07/21 Pct Recovery = 116% Analysis Date = 07/07/21 Pct Recovery = 116% Analysis Date = 07/03/21 Pct Recovery = 116% Analysis Date = 07/03/21 Pct Recovery = 116% Analysis Date = 06/29/21 Pct Recovery = 116% Analysis Date = 06/29/21 Pct Recovery = 116% Analysis Date = 06/25/21 Pct Recovery = 117% Analysis Date = 06/25/21 Pct Recovery = 117% Analysis Date = 06/21/21 Pct Recovery = 117% Analysis Date = 06/21/21 Pct Recovery = 117% Analysis Date = 06/17/21 Pct Recovery = 117% Analysis Date = 06/17/21 Pct Recovery = 117% Analysis Date = 06/13/21 Pct Recovery = 118% Analysis Date = 06/13/21 Pct Recovery = 118% Analysis Date = 06/09/21 Pct Recovery = 118% Analysis Date = 06/09/21 Pct Recovery = 118% Analysis Date = 06/05/21 Pct Recovery = 118% Analysis Date = 06/05/21 Pct Recovery = 118% Analysis Date = 06/01/21 Pct Recovery = 118% Analysis Date = 06/01/21 Pct Recovery = 118% Analysis Date = 05/29/21 Pct Recovery = 119% Analysis Date = 05/29/21 Pct Recovery = 119% Analysis Date = 05/25/21 Pct Recovery = 119% Analysis Date = 05/25/21 Pct Recovery = 119% Analysis Date = 05/21/21 Pct Recovery = 119% Analysis Date = 05/21/21 Pct Recovery = 119% Analysis Date = 05/17/21 Pct Recovery = 120% Analysis Date = 05/17/21 Pct Recovery = 120% Analysis Date = 05/13/21 Pct Recovery = 120% Analysis Date = 05/13/21 Pct Recovery = 120% Analysis Date = 05/09/21 Pct Recovery = 120% Analysis Date = 05/09/21 Pct Recovery = 120% Analysis Date = 05/05/21 Pct Recovery = 121% Analysis Date = 05/05/21 Pct Recovery = 121% Analysis Date = 05/01/21 Pct Recovery = 121% Analysis Date = 05/01/21 Pct Recovery = 121% Analysis Date = 04/27/21 Pct Recovery = 121% Analysis Date = 04/27/21 Pct Recovery = 121% Analysis Date = 04/23/21 Pct Recovery = 122% Analysis Date = 04/23/21 Pct Recovery = 122% Analysis Date = 04/19/21 Pct Recovery = 122% Analysis Date = 04/19/21 Pct Recovery = 122% Analysis Date = 04/15/21 Pct Recovery = 122% Analysis Date = 04/15/21 Pct Recovery = 122% Analysis Date = 04/11/21 Pct Recovery = 123% Analysis Date = 04/11/21 Pct Recovery = 123% Analysis Date = 04/07/21 Pct Recovery = 123% Analysis Date = 04/07/21 Pct Recovery = 123% Analysis Date = 04/04/21 Pct Recovery = 123% Analysis Date = 04/04/21 Pct Recovery = 123% Analysis Date = 03/31/21 Pct Recovery = 124% Analysis Date = 03/31/21 Pct Recovery = 124% Analysis Date = 03/27/21 Pct Recovery = 124% Analysis Date = 03/27/21 Pct Recovery = 124% Analysis Date = 03/23/21 Pct Recovery = 124% Analysis Date = 03/23/21 Pct Recovery = 124% Analysis Date = 03/19/21 Pct Recovery = 125% Analysis Date = 03/19/21 Pct Recovery = 125% Analysis Date = 03/15/21 Pct Recovery = 125% Analysis Date = 03/15/21 Pct Recovery = 125% Analysis Date = 03/11/21 Pct Recovery = 125% Analysis Date = 03/11/21 Pct Recovery = 125% Analysis Date = 03/07/21 Pct Recovery = 126% Analysis Date = 03/07/21 Pct Recovery = 126% Analysis Date = 03/03/21 Pct Recovery = 126% Analysis Date = 03/03/21 Pct Recovery = 126% Analysis Date = 02/27/21 Pct Recovery = 126% Analysis Date = 02/27/21 Pct Recovery = 126% Analysis Date = 02/23/21 Pct Recovery = 127% Analysis Date = 02/23/21 Pct Recovery = 127% Analysis Date = 02/19/21 Pct Recovery = 127% Analysis Date = 02/19/21 Pct Recovery = 127% Analysis Date = 02/15/21 Pct Recovery = 127% Analysis Date = 02/15/21 Pct Recovery = 127% Analysis Date = 02/12/21 Pct Recovery = 128% Analysis Date = 02/12/21 Pct Recovery = 128% Analysis Date = 02/08/21 Pct Recovery = 128% Analysis Date = 02/08/21 Pct Recovery = 128% Analysis Date = 02/04/21 Pct Recovery = 128% Analysis Date = 02/04/21 Pct Recovery = 128% Analysis Date = 01/31/21 Pct Recovery = 128% Analysis Date = 01/31/21 Pct Recovery = 128% Analysis Date = 01/27/21 Pct Recovery = 128% Analysis Date = 01/27/21 Pct Recovery = 128% Analysis Date = 01/23/21 Pct Recovery = 127% Analysis Date = 01/23/21 Pct Recovery = 127% Analysis Date = 01/19/21 Pct Recovery = 127% Analysis Date = 01/19/21 Pct Recovery = 127% Analysis Date = 01/15/21 Pct Recovery = 126% Analysis Date = 01/15/21 Pct Recovery = 126% Analysis Date = 01/11/21 Pct Recovery = 125% Analysis Date = 01/11/21 Pct Recovery = 125% Analysis Date = 01/07/21 Pct Recovery = 125% Analysis Date = 01/07/21 Pct Recovery = 125% Analysis Date = 01/03/21 Pct Recovery = 124% Analysis Date = 01/03/21 Pct Recovery = 124% Analysis Date = 12/30/20 Pct Recovery = 123% Analysis Date = 12/30/20 Pct Recovery = 123% Analysis Date = 12/26/20 Pct Recovery = 123% Analysis Date = 12/26/20 Pct Recovery = 123% Analysis Date = 12/23/20 Pct Recovery = 122% Analysis Date = 12/23/20 Pct Recovery = 122% Analysis Date = 12/19/20 Pct Recovery = 121% Analysis Date = 12/19/20 Pct Recovery = 121% Analysis Date = 12/15/20 Pct Recovery = 121% Analysis Date = 12/15/20 Pct Recovery = 121% Analysis Date = 12/11/20 Pct Recovery = 120% Analysis Date = 12/11/20 Pct Recovery = 120% Analysis Date = 12/07/20 Pct Recovery = 119% Analysis Date = 12/07/20 Pct Recovery = 119% Analysis Date = 12/03/20 Pct Recovery = 118% Analysis Date = 12/03/20 Pct Recovery = 118% Analysis Date = 11/29/20 Pct Recovery = 118% Analysis Date = 11/29/20 Pct Recovery = 118% Analysis Date = 11/25/20 Pct Recovery = 117% Analysis Date = 11/25/20 Pct Recovery = 117% Analysis Date = 11/21/20 Pct Recovery = 116% Analysis Date = 11/21/20 Pct Recovery = 116% Analysis Date = 11/17/20 Pct Recovery = 115% Analysis Date = 11/17/20 Pct Recovery = 115% Analysis Date = 11/13/20 Pct Recovery = 115% Analysis Date = 11/13/20 Pct Recovery = 115% Analysis Date = 11/09/20 Pct Recovery = 114% Analysis Date = 11/09/20 Pct Recovery = 114% Analysis Date = 11/05/20 Pct Recovery = 113% Analysis Date = 11/05/20 Pct Recovery = 113% Analysis Date = 11/01/20 Pct Recovery = 112% Analysis Date = 11/01/20 Pct Recovery = 112% Analysis Date = 10/29/20 Pct Recovery = 111% Analysis Date = 10/29/20 Pct Recovery = 111% Analysis Date = 10/25/20 Pct Recovery = 109% Analysis Date = 10/25/20 Pct Recovery = 109% Analysis Date = 10/21/20 Pct Recovery = 108% Analysis Date = 10/21/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 107% Analysis Date = 10/17/20 Pct Recovery = 107% Analysis Date = 10/13/20 Pct Recovery = 106% Analysis Date = 10/13/20 Pct Recovery = 106% Analysis Date = 10/09/20 Pct Recovery = 105% Analysis Date = 10/09/20 Pct Recovery = 105% Analysis Date = 10/05/20 Pct Recovery = 103% Analysis Date = 10/05/20 Pct Recovery = 103% Analysis Date = 10/01/20 Pct Recovery = 102% Analysis Date = 10/01/20 Pct Recovery = 102% Analysis Date = 09/27/20 Pct Recovery = 101% Analysis Date = 09/27/20 Pct Recovery = 101% Analysis Date = 09/23/20 Pct Recovery = 100% Analysis Date = 09/23/20 Pct Recovery = 100% Analysis Date = 09/19/20 Pct Recovery = 100% Analysis Date = 09/19/20 Pct Recovery = 100% Analysis Date = 09/15/20 Pct Recovery = 99% Analysis Date = 09/15/20 Pct Recovery = 99% Analysis Date = 09/11/20 Pct Recovery = 99% Analysis Date = 09/11/20 Pct Recovery = 99% Analysis Date = 09/08/20 Pct Recovery = 98% Analysis Date = 09/08/20 Pct Recovery = 98% Analysis Date = 09/04/20 Pct Recovery = 98% Analysis Date = 09/04/20 Pct Recovery = 98% Analysis Date = 08/31/20 Pct Recovery = 99% Analysis Date = 08/31/20 Pct Recovery = 99% Analysis Date = 08/27/20 Pct Recovery = 99% Analysis Date = 08/27/20 Pct Recovery = 99% Analysis Date = 08/23/20 Pct Recovery = 100% Analysis Date = 08/23/20 Pct Recovery = 100% Analysis Date = 08/19/20 Pct Recovery = 101% Analysis Date = 08/19/20 Pct Recovery = 101% Analysis Date = 08/15/20 Pct Recovery = 101% Analysis Date = 08/15/20 Pct Recovery = 101% Analysis Date = 08/11/20 Pct Recovery = 102% Analysis Date = 08/11/20 Pct Recovery = 102% Analysis Date = 08/07/20 Pct Recovery = 103% Analysis Date = 08/07/20 Pct Recovery = 103% Analysis Date = 08/03/20 Pct Recovery = 104% Analysis Date = 08/03/20 Pct Recovery = 104% Analysis Date = 07/30/20 Pct Recovery = 104% Analysis Date = 07/30/20 Pct Recovery = 104% Analysis Date = 07/26/20 Pct Recovery = 105% Analysis Date = 07/26/20 Pct Recovery = 105% Analysis Date = 07/22/20 Pct Recovery = 106% Analysis Date = 07/22/20 Pct Recovery = 106% Analysis Date = 07/19/20 Pct Recovery = 106% Analysis Date = 07/19/20 Pct Recovery = 106% Analysis Date = 07/15/20 Pct Recovery = 107% Analysis Date = 07/15/20 Pct Recovery = 107% Analysis Date = 07/11/20 Pct Recovery = 108% Analysis Date = 07/11/20 Pct Recovery = 108% Analysis Date = 07/07/20 Pct Recovery = 108% Analysis Date = 07/07/20 Pct Recovery = 108% Analysis Date = 07/03/20 Pct Recovery = 109% Analysis Date = 07/03/20 Pct Recovery = 109% Analysis Date = 06/29/20 Pct Recovery = 109% Analysis Date = 06/29/20 Pct Recovery = 109% Analysis Date = 06/25/20 Pct Recovery = 110% Analysis Date = 06/25/20 Pct Recovery = 110% Analysis Date = 06/21/20 Pct Recovery = 111% Analysis Date = 06/21/20 Pct Recovery = 111% Analysis Date = 06/17/20 Pct Recovery = 111% Analysis Date = 06/17/20 Pct Recovery = 111% Analysis Date = 06/13/20 Pct Recovery = 112% Analysis Date = 06/13/20 Pct Recovery = 112% Analysis Date = 06/09/20 Pct Recovery = 112% Analysis Date = 06/09/20 Pct Recovery = 112% Analysis Date = 06/05/20 Pct Recovery = 113% Analysis Date = 06/05/20 Pct Recovery = 113% Analysis Date = 06/01/20 Pct Recovery = 113% Analysis Date = 06/01/20 Pct Recovery = 113% Analysis Date = 05/29/20 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROXYMETOLACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 21 110% 24% 114% 17%
Total 21 110% 24% 114% 17%

Sample Statistics
HYDROXYMETOLACHLOR

Characteristic N % % Basis
Plotted 21 95% Spiked
Estimated Values 2 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 22 .  
False Negatives 1 5% 1 out of 22
Not Spiked 94 .  
False Positives 0 0% 0 out of 94

OBSP Determination:
HYDROXYSIMAZINE
METHOD: 2447 , TESTIDCODE: 68624LCM60

Laboratory ID = 20202590106 Lab Value = 1394.456 Expected Conc. = 1527.4 Report level label = 120 Pct Recovery = 91% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 1382.154 Expected Conc. = 1527.4 Report level label = 120 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201820155 Lab Value = 1599.204 Expected Conc. = 1500.5 Report level label = 120 Pct Recovery = 107% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 1923.536 Expected Conc. = 1500.5 Report level label = 120 Pct Recovery = 128% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20222010133 Lab Value = 186.530 Expected Conc. = 1200 Report level label = 120 Pct Recovery = 16% Analysis Date = 07/24/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20203230018 Lab Value = 626.245 Expected Conc. = 763.7 Report level label = 120 Pct Recovery = 82% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 606.701 Expected Conc. = 763.7 Report level label = 120 Pct Recovery = 79% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 661.561 Expected Conc. = 763.7 Report level label = 120 Pct Recovery = 87% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 579.981 Expected Conc. = 750.25 Report level label = 120 Pct Recovery = 77% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 695.779 Expected Conc. = 750.25 Report level label = 120 Pct Recovery = 93% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 475.183 Expected Conc. = 750.25 Report level label = 120 Pct Recovery = 63% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20221870197 Lab Value = 264.625 Expected Conc. = 750 Report level label = 120 Pct Recovery = 35% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20221730293 Lab Value = 241.331 Expected Conc. = 750 Report level label = 120 Pct Recovery = 32% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20210970035 Lab Value = 216.266 Expected Conc. = 305.48 Report level label = 120 Pct Recovery = 71% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 236.643 Expected Conc. = 305.48 Report level label = 120 Pct Recovery = 77% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 273.459 Expected Conc. = 305.48 Report level label = 120 Pct Recovery = 90% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 340.484 Expected Conc. = 305.48 Report level label = 120 Pct Recovery = 111% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 301.489 Expected Conc. = 305.48 Report level label = 120 Pct Recovery = 99% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 256.302 Expected Conc. = 305.48 Report level label = 120 Pct Recovery = 84% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202180001 Lab Value = 286.385 Expected Conc. = 300.1 Report level label = 120 Pct Recovery = 95% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 377.372 Expected Conc. = 300.1 Report level label = 120 Pct Recovery = 126% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 325.179 Expected Conc. = 300.1 Report level label = 120 Pct Recovery = 108% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20222500483 Lab Value = 96.135 Expected Conc. = 300 Report level label = 120 Pct Recovery = 32% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Analysis Date = 09/20/22 Pct Recovery = 24% Analysis Date = 09/15/22 Pct Recovery = 25% Analysis Date = 09/15/22 Pct Recovery = 25% Analysis Date = 09/11/22 Pct Recovery = 25% Analysis Date = 09/11/22 Pct Recovery = 25% Analysis Date = 09/07/22 Pct Recovery = 25% Analysis Date = 09/07/22 Pct Recovery = 25% Analysis Date = 09/02/22 Pct Recovery = 26% Analysis Date = 09/02/22 Pct Recovery = 26% Analysis Date = 08/29/22 Pct Recovery = 26% Analysis Date = 08/29/22 Pct Recovery = 26% Analysis Date = 08/25/22 Pct Recovery = 27% Analysis Date = 08/25/22 Pct Recovery = 27% Analysis Date = 08/21/22 Pct Recovery = 27% Analysis Date = 08/21/22 Pct Recovery = 27% Analysis Date = 08/16/22 Pct Recovery = 27% Analysis Date = 08/16/22 Pct Recovery = 27% Analysis Date = 08/12/22 Pct Recovery = 28% Analysis Date = 08/12/22 Pct Recovery = 28% Analysis Date = 08/08/22 Pct Recovery = 28% Analysis Date = 08/08/22 Pct Recovery = 28% Analysis Date = 08/04/22 Pct Recovery = 28% Analysis Date = 08/04/22 Pct Recovery = 28% Analysis Date = 07/30/22 Pct Recovery = 29% Analysis Date = 07/30/22 Pct Recovery = 29% Analysis Date = 07/26/22 Pct Recovery = 29% Analysis Date = 07/26/22 Pct Recovery = 29% Analysis Date = 07/22/22 Pct Recovery = 30% Analysis Date = 07/22/22 Pct Recovery = 30% Analysis Date = 07/17/22 Pct Recovery = 30% Analysis Date = 07/17/22 Pct Recovery = 30% Analysis Date = 07/13/22 Pct Recovery = 30% Analysis Date = 07/13/22 Pct Recovery = 30% Analysis Date = 07/09/22 Pct Recovery = 31% Analysis Date = 07/09/22 Pct Recovery = 31% Analysis Date = 07/05/22 Pct Recovery = 31% Analysis Date = 07/05/22 Pct Recovery = 31% Analysis Date = 06/30/22 Pct Recovery = 31% Analysis Date = 06/30/22 Pct Recovery = 31% Analysis Date = 06/26/22 Pct Recovery = 32% Analysis Date = 06/26/22 Pct Recovery = 32% Analysis Date = 06/22/22 Pct Recovery = 32% Analysis Date = 06/22/22 Pct Recovery = 32% Analysis Date = 06/18/22 Pct Recovery = 33% Analysis Date = 06/18/22 Pct Recovery = 33% Analysis Date = 06/13/22 Pct Recovery = 33% Analysis Date = 06/13/22 Pct Recovery = 33% Analysis Date = 06/09/22 Pct Recovery = 33% Analysis Date = 06/09/22 Pct Recovery = 33% Analysis Date = 06/05/22 Pct Recovery = 34% Analysis Date = 06/05/22 Pct Recovery = 34% Analysis Date = 05/31/22 Pct Recovery = 34% Analysis Date = 05/31/22 Pct Recovery = 34% Analysis Date = 05/27/22 Pct Recovery = 35% Analysis Date = 05/27/22 Pct Recovery = 35% Analysis Date = 05/23/22 Pct Recovery = 35% Analysis Date = 05/23/22 Pct Recovery = 35% Analysis Date = 05/19/22 Pct Recovery = 36% Analysis Date = 05/19/22 Pct Recovery = 36% Analysis Date = 05/14/22 Pct Recovery = 36% Analysis Date = 05/14/22 Pct Recovery = 36% Analysis Date = 05/10/22 Pct Recovery = 36% Analysis Date = 05/10/22 Pct Recovery = 36% Analysis Date = 05/06/22 Pct Recovery = 37% Analysis Date = 05/06/22 Pct Recovery = 37% Analysis Date = 05/02/22 Pct Recovery = 37% Analysis Date = 05/02/22 Pct Recovery = 37% Analysis Date = 04/27/22 Pct Recovery = 38% Analysis Date = 04/27/22 Pct Recovery = 38% Analysis Date = 04/23/22 Pct Recovery = 38% Analysis Date = 04/23/22 Pct Recovery = 38% Analysis Date = 04/19/22 Pct Recovery = 38% Analysis Date = 04/19/22 Pct Recovery = 38% Analysis Date = 04/15/22 Pct Recovery = 39% Analysis Date = 04/15/22 Pct Recovery = 39% Analysis Date = 04/10/22 Pct Recovery = 39% Analysis Date = 04/10/22 Pct Recovery = 39% Analysis Date = 04/06/22 Pct Recovery = 40% Analysis Date = 04/06/22 Pct Recovery = 40% Analysis Date = 04/02/22 Pct Recovery = 40% Analysis Date = 04/02/22 Pct Recovery = 40% Analysis Date = 03/28/22 Pct Recovery = 40% Analysis Date = 03/28/22 Pct Recovery = 40% Analysis Date = 03/24/22 Pct Recovery = 41% Analysis Date = 03/24/22 Pct Recovery = 41% Analysis Date = 03/20/22 Pct Recovery = 41% Analysis Date = 03/20/22 Pct Recovery = 41% Analysis Date = 03/16/22 Pct Recovery = 42% Analysis Date = 03/16/22 Pct Recovery = 42% Analysis Date = 03/11/22 Pct Recovery = 42% Analysis Date = 03/11/22 Pct Recovery = 42% Analysis Date = 03/07/22 Pct Recovery = 42% Analysis Date = 03/07/22 Pct Recovery = 42% Analysis Date = 03/03/22 Pct Recovery = 43% Analysis Date = 03/03/22 Pct Recovery = 43% Analysis Date = 02/27/22 Pct Recovery = 43% Analysis Date = 02/27/22 Pct Recovery = 43% Analysis Date = 02/22/22 Pct Recovery = 44% Analysis Date = 02/22/22 Pct Recovery = 44% Analysis Date = 02/18/22 Pct Recovery = 44% Analysis Date = 02/18/22 Pct Recovery = 44% Analysis Date = 02/14/22 Pct Recovery = 44% Analysis Date = 02/14/22 Pct Recovery = 44% Analysis Date = 02/09/22 Pct Recovery = 45% Analysis Date = 02/09/22 Pct Recovery = 45% Analysis Date = 02/05/22 Pct Recovery = 45% Analysis Date = 02/05/22 Pct Recovery = 45% Analysis Date = 02/01/22 Pct Recovery = 46% Analysis Date = 02/01/22 Pct Recovery = 46% Analysis Date = 01/28/22 Pct Recovery = 46% Analysis Date = 01/28/22 Pct Recovery = 46% Analysis Date = 01/23/22 Pct Recovery = 46% Analysis Date = 01/23/22 Pct Recovery = 46% Analysis Date = 01/19/22 Pct Recovery = 47% Analysis Date = 01/19/22 Pct Recovery = 47% Analysis Date = 01/15/22 Pct Recovery = 47% Analysis Date = 01/15/22 Pct Recovery = 47% Analysis Date = 01/11/22 Pct Recovery = 48% Analysis Date = 01/11/22 Pct Recovery = 48% Analysis Date = 01/06/22 Pct Recovery = 48% Analysis Date = 01/06/22 Pct Recovery = 48% Analysis Date = 01/02/22 Pct Recovery = 49% Analysis Date = 01/02/22 Pct Recovery = 49% Analysis Date = 12/29/21 Pct Recovery = 49% Analysis Date = 12/29/21 Pct Recovery = 49% Analysis Date = 12/24/21 Pct Recovery = 49% Analysis Date = 12/24/21 Pct Recovery = 49% Analysis Date = 12/20/21 Pct Recovery = 50% Analysis Date = 12/20/21 Pct Recovery = 50% Analysis Date = 12/16/21 Pct Recovery = 50% Analysis Date = 12/16/21 Pct Recovery = 50% Analysis Date = 12/12/21 Pct Recovery = 51% Analysis Date = 12/12/21 Pct Recovery = 51% Analysis Date = 12/07/21 Pct Recovery = 51% Analysis Date = 12/07/21 Pct Recovery = 51% Analysis Date = 12/03/21 Pct Recovery = 51% Analysis Date = 12/03/21 Pct Recovery = 51% Analysis Date = 11/29/21 Pct Recovery = 52% Analysis Date = 11/29/21 Pct Recovery = 52% Analysis Date = 11/25/21 Pct Recovery = 52% Analysis Date = 11/25/21 Pct Recovery = 52% Analysis Date = 11/20/21 Pct Recovery = 53% Analysis Date = 11/20/21 Pct Recovery = 53% Analysis Date = 11/16/21 Pct Recovery = 53% Analysis Date = 11/16/21 Pct Recovery = 53% Analysis Date = 11/12/21 Pct Recovery = 53% Analysis Date = 11/12/21 Pct Recovery = 53% Analysis Date = 11/08/21 Pct Recovery = 54% Analysis Date = 11/08/21 Pct Recovery = 54% Analysis Date = 11/03/21 Pct Recovery = 54% Analysis Date = 11/03/21 Pct Recovery = 54% Analysis Date = 10/30/21 Pct Recovery = 55% Analysis Date = 10/30/21 Pct Recovery = 55% Analysis Date = 10/26/21 Pct Recovery = 55% Analysis Date = 10/26/21 Pct Recovery = 55% Analysis Date = 10/21/21 Pct Recovery = 55% Analysis Date = 10/21/21 Pct Recovery = 55% Analysis Date = 10/17/21 Pct Recovery = 56% Analysis Date = 10/17/21 Pct Recovery = 56% Analysis Date = 10/13/21 Pct Recovery = 56% Analysis Date = 10/13/21 Pct Recovery = 56% Analysis Date = 10/09/21 Pct Recovery = 57% Analysis Date = 10/09/21 Pct Recovery = 57% Analysis Date = 10/04/21 Pct Recovery = 57% Analysis Date = 10/04/21 Pct Recovery = 57% Analysis Date = 09/30/21 Pct Recovery = 57% Analysis Date = 09/30/21 Pct Recovery = 57% Analysis Date = 09/26/21 Pct Recovery = 58% Analysis Date = 09/26/21 Pct Recovery = 58% Analysis Date = 09/22/21 Pct Recovery = 58% Analysis Date = 09/22/21 Pct Recovery = 58% Analysis Date = 09/17/21 Pct Recovery = 59% Analysis Date = 09/17/21 Pct Recovery = 59% Analysis Date = 09/13/21 Pct Recovery = 59% Analysis Date = 09/13/21 Pct Recovery = 59% Analysis Date = 09/09/21 Pct Recovery = 60% Analysis Date = 09/09/21 Pct Recovery = 60% Analysis Date = 09/04/21 Pct Recovery = 60% Analysis Date = 09/04/21 Pct Recovery = 60% Analysis Date = 08/31/21 Pct Recovery = 60% Analysis Date = 08/31/21 Pct Recovery = 60% Analysis Date = 08/27/21 Pct Recovery = 61% Analysis Date = 08/27/21 Pct Recovery = 61% Analysis Date = 08/23/21 Pct Recovery = 61% Analysis Date = 08/23/21 Pct Recovery = 61% Analysis Date = 08/18/21 Pct Recovery = 62% Analysis Date = 08/18/21 Pct Recovery = 62% Analysis Date = 08/14/21 Pct Recovery = 62% Analysis Date = 08/14/21 Pct Recovery = 62% Analysis Date = 08/10/21 Pct Recovery = 62% Analysis Date = 08/10/21 Pct Recovery = 62% Analysis Date = 08/06/21 Pct Recovery = 63% Analysis Date = 08/06/21 Pct Recovery = 63% Analysis Date = 08/01/21 Pct Recovery = 63% Analysis Date = 08/01/21 Pct Recovery = 63% Analysis Date = 07/28/21 Pct Recovery = 64% Analysis Date = 07/28/21 Pct Recovery = 64% Analysis Date = 07/24/21 Pct Recovery = 64% Analysis Date = 07/24/21 Pct Recovery = 64% Analysis Date = 07/20/21 Pct Recovery = 64% Analysis Date = 07/20/21 Pct Recovery = 64% Analysis Date = 07/15/21 Pct Recovery = 65% Analysis Date = 07/15/21 Pct Recovery = 65% Analysis Date = 07/11/21 Pct Recovery = 65% Analysis Date = 07/11/21 Pct Recovery = 65% Analysis Date = 07/07/21 Pct Recovery = 66% Analysis Date = 07/07/21 Pct Recovery = 66% Analysis Date = 07/02/21 Pct Recovery = 66% Analysis Date = 07/02/21 Pct Recovery = 66% Analysis Date = 06/28/21 Pct Recovery = 66% Analysis Date = 06/28/21 Pct Recovery = 66% Analysis Date = 06/24/21 Pct Recovery = 67% Analysis Date = 06/24/21 Pct Recovery = 67% Analysis Date = 06/20/21 Pct Recovery = 67% Analysis Date = 06/20/21 Pct Recovery = 67% Analysis Date = 06/15/21 Pct Recovery = 68% Analysis Date = 06/15/21 Pct Recovery = 68% Analysis Date = 06/11/21 Pct Recovery = 68% Analysis Date = 06/11/21 Pct Recovery = 68% Analysis Date = 06/07/21 Pct Recovery = 68% Analysis Date = 06/07/21 Pct Recovery = 68% Analysis Date = 06/03/21 Pct Recovery = 69% Analysis Date = 06/03/21 Pct Recovery = 69% Analysis Date = 05/29/21 Pct Recovery = 69% Analysis Date = 05/29/21 Pct Recovery = 69% Analysis Date = 05/25/21 Pct Recovery = 70% Analysis Date = 05/25/21 Pct Recovery = 70% Analysis Date = 05/21/21 Pct Recovery = 70% Analysis Date = 05/21/21 Pct Recovery = 70% Analysis Date = 05/16/21 Pct Recovery = 70% Analysis Date = 05/16/21 Pct Recovery = 70% Analysis Date = 05/12/21 Pct Recovery = 71% Analysis Date = 05/12/21 Pct Recovery = 71% Analysis Date = 05/08/21 Pct Recovery = 71% Analysis Date = 05/08/21 Pct Recovery = 71% Analysis Date = 05/04/21 Pct Recovery = 72% Analysis Date = 05/04/21 Pct Recovery = 72% Analysis Date = 04/29/21 Pct Recovery = 72% Analysis Date = 04/29/21 Pct Recovery = 72% Analysis Date = 04/25/21 Pct Recovery = 73% Analysis Date = 04/25/21 Pct Recovery = 73% Analysis Date = 04/21/21 Pct Recovery = 73% Analysis Date = 04/21/21 Pct Recovery = 73% Analysis Date = 04/17/21 Pct Recovery = 73% Analysis Date = 04/17/21 Pct Recovery = 73% Analysis Date = 04/12/21 Pct Recovery = 74% Analysis Date = 04/12/21 Pct Recovery = 74% Analysis Date = 04/08/21 Pct Recovery = 74% Analysis Date = 04/08/21 Pct Recovery = 74% Analysis Date = 04/04/21 Pct Recovery = 75% Analysis Date = 04/04/21 Pct Recovery = 75% Analysis Date = 03/30/21 Pct Recovery = 75% Analysis Date = 03/30/21 Pct Recovery = 75% Analysis Date = 03/26/21 Pct Recovery = 75% Analysis Date = 03/26/21 Pct Recovery = 75% Analysis Date = 03/22/21 Pct Recovery = 76% Analysis Date = 03/22/21 Pct Recovery = 76% Analysis Date = 03/18/21 Pct Recovery = 76% Analysis Date = 03/18/21 Pct Recovery = 76% Analysis Date = 03/13/21 Pct Recovery = 77% Analysis Date = 03/13/21 Pct Recovery = 77% Analysis Date = 03/09/21 Pct Recovery = 77% Analysis Date = 03/09/21 Pct Recovery = 77% Analysis Date = 03/05/21 Pct Recovery = 77% Analysis Date = 03/05/21 Pct Recovery = 77% Analysis Date = 03/01/21 Pct Recovery = 78% Analysis Date = 03/01/21 Pct Recovery = 78% Analysis Date = 02/24/21 Pct Recovery = 78% Analysis Date = 02/24/21 Pct Recovery = 78% Analysis Date = 02/20/21 Pct Recovery = 79% Analysis Date = 02/20/21 Pct Recovery = 79% Analysis Date = 02/16/21 Pct Recovery = 79% Analysis Date = 02/16/21 Pct Recovery = 79% Analysis Date = 02/12/21 Pct Recovery = 79% Analysis Date = 02/12/21 Pct Recovery = 79% Analysis Date = 02/07/21 Pct Recovery = 80% Analysis Date = 02/07/21 Pct Recovery = 80% Analysis Date = 02/03/21 Pct Recovery = 81% Analysis Date = 02/03/21 Pct Recovery = 81% Analysis Date = 01/30/21 Pct Recovery = 81% Analysis Date = 01/30/21 Pct Recovery = 81% Analysis Date = 01/25/21 Pct Recovery = 82% Analysis Date = 01/25/21 Pct Recovery = 82% Analysis Date = 01/21/21 Pct Recovery = 82% Analysis Date = 01/21/21 Pct Recovery = 82% Analysis Date = 01/17/21 Pct Recovery = 83% Analysis Date = 01/17/21 Pct Recovery = 83% Analysis Date = 01/13/21 Pct Recovery = 84% Analysis Date = 01/13/21 Pct Recovery = 84% Analysis Date = 01/08/21 Pct Recovery = 84% Analysis Date = 01/08/21 Pct Recovery = 84% Analysis Date = 01/04/21 Pct Recovery = 85% Analysis Date = 01/04/21 Pct Recovery = 85% Analysis Date = 12/31/20 Pct Recovery = 85% Analysis Date = 12/31/20 Pct Recovery = 85% Analysis Date = 12/27/20 Pct Recovery = 86% Analysis Date = 12/27/20 Pct Recovery = 86% Analysis Date = 12/22/20 Pct Recovery = 87% Analysis Date = 12/22/20 Pct Recovery = 87% Analysis Date = 12/18/20 Pct Recovery = 87% Analysis Date = 12/18/20 Pct Recovery = 87% Analysis Date = 12/14/20 Pct Recovery = 88% Analysis Date = 12/14/20 Pct Recovery = 88% Analysis Date = 12/09/20 Pct Recovery = 88% Analysis Date = 12/09/20 Pct Recovery = 88% Analysis Date = 12/05/20 Pct Recovery = 89% Analysis Date = 12/05/20 Pct Recovery = 89% Analysis Date = 12/01/20 Pct Recovery = 89% Analysis Date = 12/01/20 Pct Recovery = 89% Analysis Date = 11/27/20 Pct Recovery = 90% Analysis Date = 11/27/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 90% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 91% Analysis Date = 11/10/20 Pct Recovery = 91% Analysis Date = 11/10/20 Pct Recovery = 91% Analysis Date = 11/05/20 Pct Recovery = 91% Analysis Date = 11/05/20 Pct Recovery = 91% Analysis Date = 11/01/20 Pct Recovery = 91% Analysis Date = 11/01/20 Pct Recovery = 91% Analysis Date = 10/28/20 Pct Recovery = 91% Analysis Date = 10/28/20 Pct Recovery = 91% Analysis Date = 10/23/20 Pct Recovery = 91% Analysis Date = 10/23/20 Pct Recovery = 91% Analysis Date = 10/19/20 Pct Recovery = 91% Analysis Date = 10/19/20 Pct Recovery = 91% Analysis Date = 10/15/20 Pct Recovery = 92% Analysis Date = 10/15/20 Pct Recovery = 92% Analysis Date = 10/11/20 Pct Recovery = 92% Analysis Date = 10/11/20 Pct Recovery = 92% Analysis Date = 10/06/20 Pct Recovery = 92% Analysis Date = 10/06/20 Pct Recovery = 92% Analysis Date = 10/02/20 Pct Recovery = 92% Analysis Date = 10/02/20 Pct Recovery = 92% Analysis Date = 09/28/20 Pct Recovery = 92% Analysis Date = 09/28/20 Pct Recovery = 92% Analysis Date = 09/24/20 Pct Recovery = 92% Analysis Date = 09/24/20 Pct Recovery = 92% Analysis Date = 09/19/20 Pct Recovery = 93% Analysis Date = 09/19/20 Pct Recovery = 93% Analysis Date = 09/15/20 Pct Recovery = 94% Analysis Date = 09/15/20 Pct Recovery = 94% Analysis Date = 09/11/20 Pct Recovery = 95% Analysis Date = 09/11/20 Pct Recovery = 95% Analysis Date = 09/07/20 Pct Recovery = 96% Analysis Date = 09/07/20 Pct Recovery = 96% Analysis Date = 09/02/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 97% Analysis Date = 08/29/20 Pct Recovery = 97% Analysis Date = 08/29/20 Pct Recovery = 97% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/20/20 Pct Recovery = 99% Analysis Date = 08/20/20 Pct Recovery = 99% Analysis Date = 08/16/20 Pct Recovery = 100% Analysis Date = 08/16/20 Pct Recovery = 100% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 102% Analysis Date = 08/08/20 Pct Recovery = 102% Analysis Date = 08/03/20 Pct Recovery = 102% Analysis Date = 08/03/20 Pct Recovery = 102% Analysis Date = 07/30/20 Pct Recovery = 103% Analysis Date = 07/30/20 Pct Recovery = 103% Analysis Date = 07/26/20 Pct Recovery = 103% Analysis Date = 07/26/20 Pct Recovery = 103% Analysis Date = 07/22/20 Pct Recovery = 103% Analysis Date = 07/22/20 Pct Recovery = 103% Analysis Date = 07/17/20 Pct Recovery = 103% Analysis Date = 07/17/20 Pct Recovery = 103% Analysis Date = 07/13/20 Pct Recovery = 102% Analysis Date = 07/13/20 Pct Recovery = 102% Analysis Date = 07/09/20 Pct Recovery = 102% Analysis Date = 07/09/20 Pct Recovery = 102% Analysis Date = 07/04/20 Pct Recovery = 102% Analysis Date = 07/04/20 Pct Recovery = 102% Analysis Date = 06/30/20 Pct Recovery = 102% Analysis Date = 06/30/20 Pct Recovery = 102% Analysis Date = 06/26/20 Pct Recovery = 102% Analysis Date = 06/26/20 Pct Recovery = 102% Analysis Date = 06/22/20 Pct Recovery = 102% Analysis Date = 06/22/20 Pct Recovery = 102% Analysis Date = 06/17/20 Pct Recovery = 102% Analysis Date = 06/17/20 Pct Recovery = 102% Analysis Date = 06/13/20 Pct Recovery = 102% Analysis Date = 06/13/20 Pct Recovery = 102% Analysis Date = 06/09/20 Pct Recovery = 101% Analysis Date = 06/09/20 Pct Recovery = 101% Analysis Date = 06/05/20 Pct Recovery = 101% Analysis Date = 06/05/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/19/20 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HYDROXYSIMAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 23 81% 29% 87% 21%
Total 23 81% 29% 87% 21%

Sample Statistics
HYDROXYSIMAZINE

Characteristic N % % Basis
Plotted 23 92% Spiked
Estimated Values 23 92% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 25 .  
False Negatives 2 8% 2 out of 25
Not Spiked 84 .  
False Positives 2 2% 2 out of 83

OBSP Determination:
IMAZETHAPYR
METHOD: 2447 , TESTIDCODE: 61683LCM60

Laboratory ID = 20201820155 Lab Value = 99.269 Expected Conc. = 101.8 Report level label = 8 Pct Recovery = 98% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 111.187 Expected Conc. = 101.8 Report level label = 8 Pct Recovery = 109% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203230021 Lab Value = 81.268 Expected Conc. = 100.9 Report level label = 8 Pct Recovery = 81% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 68.933 Expected Conc. = 100.9 Report level label = 8 Pct Recovery = 68% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 85.347 Expected Conc. = 100.3 Report level label = 8 Pct Recovery = 85% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 81.807 Expected Conc. = 100.3 Report level label = 8 Pct Recovery = 82% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 113.501 Expected Conc. = 100.3 Report level label = 8 Pct Recovery = 113% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20221520237 Lab Value = 73.656 Expected Conc. = 80.16 Report level label = 8 Pct Recovery = 92% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 55.098 Expected Conc. = 80 Report level label = 8 Pct Recovery = 69% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 63.298 Expected Conc. = 79.2 Report level label = 8 Pct Recovery = 80% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20202530029 Lab Value = 45.906 Expected Conc. = 50.9 Report level label = 8 Pct Recovery = 90% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 40.578 Expected Conc. = 50.9 Report level label = 8 Pct Recovery = 80% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 38.039 Expected Conc. = 50.9 Report level label = 8 Pct Recovery = 75% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20203230018 Lab Value = 38.769 Expected Conc. = 50.15 Report level label = 8 Pct Recovery = 77% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 52.520 Expected Conc. = 50.15 Report level label = 8 Pct Recovery = 105% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 53.093 Expected Conc. = 50.15 Report level label = 8 Pct Recovery = 106% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201960104 Lab Value = 56.994 Expected Conc. = 50.15 Report level label = 8 Pct Recovery = 114% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20221870197 Lab Value = 39.867 Expected Conc. = 50.1 Report level label = 8 Pct Recovery = 80% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20220740064 Lab Value = 40.870 Expected Conc. = 49.75 Report level label = 8 Pct Recovery = 82% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202180001 Lab Value = 15.465 Expected Conc. = 20.36 Report level label = 8 Pct Recovery = 76% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 31.759 Expected Conc. = 20.36 Report level label = 8 Pct Recovery = 156% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 22.808 Expected Conc. = 20.36 Report level label = 8 Pct Recovery = 112% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210270007 Lab Value = 22.449 Expected Conc. = 20.18 Report level label = 8 Pct Recovery = 111% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 15.133 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 75% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 19.657 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 98% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 25.857 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 129% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 22.500 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 112% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 23.273 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 116% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 17.562 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 88% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201610160 Lab Value = 20.888 Expected Conc. = 20.06 Report level label = 8 Pct Recovery = 104% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Analysis Date = 08/15/22 Pct Recovery = 79% Analysis Date = 08/10/22 Pct Recovery = 79% Analysis Date = 08/10/22 Pct Recovery = 79% Analysis Date = 08/06/22 Pct Recovery = 79% Analysis Date = 08/06/22 Pct Recovery = 79% Analysis Date = 08/02/22 Pct Recovery = 79% Analysis Date = 08/02/22 Pct Recovery = 79% Analysis Date = 07/29/22 Pct Recovery = 79% Analysis Date = 07/29/22 Pct Recovery = 79% Analysis Date = 07/25/22 Pct Recovery = 80% Analysis Date = 07/25/22 Pct Recovery = 80% Analysis Date = 07/21/22 Pct Recovery = 80% Analysis Date = 07/21/22 Pct Recovery = 80% Analysis Date = 07/17/22 Pct Recovery = 80% Analysis Date = 07/17/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/01/22 Pct Recovery = 80% Analysis Date = 07/01/22 Pct Recovery = 80% Analysis Date = 06/26/22 Pct Recovery = 80% Analysis Date = 06/26/22 Pct Recovery = 80% Analysis Date = 06/22/22 Pct Recovery = 80% Analysis Date = 06/22/22 Pct Recovery = 80% Analysis Date = 06/18/22 Pct Recovery = 80% Analysis Date = 06/18/22 Pct Recovery = 80% Analysis Date = 06/14/22 Pct Recovery = 80% Analysis Date = 06/14/22 Pct Recovery = 80% Analysis Date = 06/10/22 Pct Recovery = 80% Analysis Date = 06/10/22 Pct Recovery = 80% Analysis Date = 06/06/22 Pct Recovery = 80% Analysis Date = 06/06/22 Pct Recovery = 80% Analysis Date = 06/02/22 Pct Recovery = 80% Analysis Date = 06/02/22 Pct Recovery = 80% Analysis Date = 05/29/22 Pct Recovery = 80% Analysis Date = 05/29/22 Pct Recovery = 80% Analysis Date = 05/25/22 Pct Recovery = 80% Analysis Date = 05/25/22 Pct Recovery = 80% Analysis Date = 05/21/22 Pct Recovery = 80% Analysis Date = 05/21/22 Pct Recovery = 80% Analysis Date = 05/17/22 Pct Recovery = 80% Analysis Date = 05/17/22 Pct Recovery = 80% Analysis Date = 05/12/22 Pct Recovery = 80% Analysis Date = 05/12/22 Pct Recovery = 80% Analysis Date = 05/08/22 Pct Recovery = 80% Analysis Date = 05/08/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 05/04/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/26/22 Pct Recovery = 80% Analysis Date = 04/26/22 Pct Recovery = 80% Analysis Date = 04/22/22 Pct Recovery = 80% Analysis Date = 04/22/22 Pct Recovery = 80% Analysis Date = 04/18/22 Pct Recovery = 80% Analysis Date = 04/18/22 Pct Recovery = 80% Analysis Date = 04/14/22 Pct Recovery = 80% Analysis Date = 04/14/22 Pct Recovery = 80% Analysis Date = 04/10/22 Pct Recovery = 80% Analysis Date = 04/10/22 Pct Recovery = 80% Analysis Date = 04/06/22 Pct Recovery = 80% Analysis Date = 04/06/22 Pct Recovery = 80% Analysis Date = 04/02/22 Pct Recovery = 80% Analysis Date = 04/02/22 Pct Recovery = 80% Analysis Date = 03/28/22 Pct Recovery = 80% Analysis Date = 03/28/22 Pct Recovery = 80% Analysis Date = 03/24/22 Pct Recovery = 80% Analysis Date = 03/24/22 Pct Recovery = 80% Analysis Date = 03/20/22 Pct Recovery = 80% Analysis Date = 03/20/22 Pct Recovery = 80% Analysis Date = 03/16/22 Pct Recovery = 80% Analysis Date = 03/16/22 Pct Recovery = 80% Analysis Date = 03/12/22 Pct Recovery = 80% Analysis Date = 03/12/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 80% Analysis Date = 02/28/22 Pct Recovery = 80% Analysis Date = 02/28/22 Pct Recovery = 80% Analysis Date = 02/24/22 Pct Recovery = 80% Analysis Date = 02/24/22 Pct Recovery = 80% Analysis Date = 02/20/22 Pct Recovery = 80% Analysis Date = 02/20/22 Pct Recovery = 80% Analysis Date = 02/16/22 Pct Recovery = 80% Analysis Date = 02/16/22 Pct Recovery = 80% Analysis Date = 02/11/22 Pct Recovery = 80% Analysis Date = 02/11/22 Pct Recovery = 80% Analysis Date = 02/07/22 Pct Recovery = 80% Analysis Date = 02/07/22 Pct Recovery = 80% Analysis Date = 02/03/22 Pct Recovery = 80% Analysis Date = 02/03/22 Pct Recovery = 80% Analysis Date = 01/30/22 Pct Recovery = 80% Analysis Date = 01/30/22 Pct Recovery = 80% Analysis Date = 01/26/22 Pct Recovery = 80% Analysis Date = 01/26/22 Pct Recovery = 80% Analysis Date = 01/22/22 Pct Recovery = 80% Analysis Date = 01/22/22 Pct Recovery = 80% Analysis Date = 01/18/22 Pct Recovery = 80% Analysis Date = 01/18/22 Pct Recovery = 80% Analysis Date = 01/14/22 Pct Recovery = 80% Analysis Date = 01/14/22 Pct Recovery = 80% Analysis Date = 01/10/22 Pct Recovery = 80% Analysis Date = 01/10/22 Pct Recovery = 80% Analysis Date = 01/06/22 Pct Recovery = 80% Analysis Date = 01/06/22 Pct Recovery = 80% Analysis Date = 01/02/22 Pct Recovery = 80% Analysis Date = 01/02/22 Pct Recovery = 80% Analysis Date = 12/28/21 Pct Recovery = 80% Analysis Date = 12/28/21 Pct Recovery = 80% Analysis Date = 12/24/21 Pct Recovery = 79% Analysis Date = 12/24/21 Pct Recovery = 79% Analysis Date = 12/20/21 Pct Recovery = 79% Analysis Date = 12/20/21 Pct Recovery = 79% Analysis Date = 12/16/21 Pct Recovery = 79% Analysis Date = 12/16/21 Pct Recovery = 79% Analysis Date = 12/12/21 Pct Recovery = 79% Analysis Date = 12/12/21 Pct Recovery = 79% Analysis Date = 12/08/21 Pct Recovery = 79% Analysis Date = 12/08/21 Pct Recovery = 79% Analysis Date = 12/04/21 Pct Recovery = 79% Analysis Date = 12/04/21 Pct Recovery = 79% Analysis Date = 11/30/21 Pct Recovery = 79% Analysis Date = 11/30/21 Pct Recovery = 79% Analysis Date = 11/26/21 Pct Recovery = 79% Analysis Date = 11/26/21 Pct Recovery = 79% Analysis Date = 11/22/21 Pct Recovery = 79% Analysis Date = 11/22/21 Pct Recovery = 79% Analysis Date = 11/18/21 Pct Recovery = 79% Analysis Date = 11/18/21 Pct Recovery = 79% Analysis Date = 11/13/21 Pct Recovery = 79% Analysis Date = 11/13/21 Pct Recovery = 79% Analysis Date = 11/09/21 Pct Recovery = 79% Analysis Date = 11/09/21 Pct Recovery = 79% Analysis Date = 11/05/21 Pct Recovery = 79% Analysis Date = 11/05/21 Pct Recovery = 79% Analysis Date = 11/01/21 Pct Recovery = 79% Analysis Date = 11/01/21 Pct Recovery = 79% Analysis Date = 10/28/21 Pct Recovery = 79% Analysis Date = 10/28/21 Pct Recovery = 79% Analysis Date = 10/24/21 Pct Recovery = 79% Analysis Date = 10/24/21 Pct Recovery = 79% Analysis Date = 10/20/21 Pct Recovery = 79% Analysis Date = 10/20/21 Pct Recovery = 79% Analysis Date = 10/16/21 Pct Recovery = 79% Analysis Date = 10/16/21 Pct Recovery = 79% Analysis Date = 10/12/21 Pct Recovery = 79% Analysis Date = 10/12/21 Pct Recovery = 79% Analysis Date = 10/08/21 Pct Recovery = 79% Analysis Date = 10/08/21 Pct Recovery = 79% Analysis Date = 10/04/21 Pct Recovery = 79% Analysis Date = 10/04/21 Pct Recovery = 79% Analysis Date = 09/29/21 Pct Recovery = 79% Analysis Date = 09/29/21 Pct Recovery = 79% Analysis Date = 09/25/21 Pct Recovery = 79% Analysis Date = 09/25/21 Pct Recovery = 79% Analysis Date = 09/21/21 Pct Recovery = 79% Analysis Date = 09/21/21 Pct Recovery = 79% Analysis Date = 09/17/21 Pct Recovery = 79% Analysis Date = 09/17/21 Pct Recovery = 79% Analysis Date = 09/13/21 Pct Recovery = 79% Analysis Date = 09/13/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 79% Analysis Date = 08/24/21 Pct Recovery = 79% Analysis Date = 08/24/21 Pct Recovery = 79% Analysis Date = 08/20/21 Pct Recovery = 79% Analysis Date = 08/20/21 Pct Recovery = 79% Analysis Date = 08/15/21 Pct Recovery = 79% Analysis Date = 08/15/21 Pct Recovery = 79% Analysis Date = 08/11/21 Pct Recovery = 79% Analysis Date = 08/11/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/26/21 Pct Recovery = 79% Analysis Date = 07/26/21 Pct Recovery = 79% Analysis Date = 07/22/21 Pct Recovery = 79% Analysis Date = 07/22/21 Pct Recovery = 79% Analysis Date = 07/18/21 Pct Recovery = 79% Analysis Date = 07/18/21 Pct Recovery = 79% Analysis Date = 07/14/21 Pct Recovery = 79% Analysis Date = 07/14/21 Pct Recovery = 79% Analysis Date = 07/10/21 Pct Recovery = 79% Analysis Date = 07/10/21 Pct Recovery = 79% Analysis Date = 07/06/21 Pct Recovery = 79% Analysis Date = 07/06/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 06/27/21 Pct Recovery = 78% Analysis Date = 06/27/21 Pct Recovery = 78% Analysis Date = 06/23/21 Pct Recovery = 78% Analysis Date = 06/23/21 Pct Recovery = 78% Analysis Date = 06/19/21 Pct Recovery = 78% Analysis Date = 06/19/21 Pct Recovery = 78% Analysis Date = 06/15/21 Pct Recovery = 78% Analysis Date = 06/15/21 Pct Recovery = 78% Analysis Date = 06/11/21 Pct Recovery = 78% Analysis Date = 06/11/21 Pct Recovery = 78% Analysis Date = 06/07/21 Pct Recovery = 78% Analysis Date = 06/07/21 Pct Recovery = 78% Analysis Date = 06/03/21 Pct Recovery = 78% Analysis Date = 06/03/21 Pct Recovery = 78% Analysis Date = 05/30/21 Pct Recovery = 78% Analysis Date = 05/30/21 Pct Recovery = 78% Analysis Date = 05/26/21 Pct Recovery = 78% Analysis Date = 05/26/21 Pct Recovery = 78% Analysis Date = 05/22/21 Pct Recovery = 78% Analysis Date = 05/22/21 Pct Recovery = 78% Analysis Date = 05/18/21 Pct Recovery = 78% Analysis Date = 05/18/21 Pct Recovery = 78% Analysis Date = 05/13/21 Pct Recovery = 78% Analysis Date = 05/13/21 Pct Recovery = 78% Analysis Date = 05/09/21 Pct Recovery = 78% Analysis Date = 05/09/21 Pct Recovery = 78% Analysis Date = 05/05/21 Pct Recovery = 78% Analysis Date = 05/05/21 Pct Recovery = 78% Analysis Date = 05/01/21 Pct Recovery = 78% Analysis Date = 05/01/21 Pct Recovery = 78% Analysis Date = 04/27/21 Pct Recovery = 78% Analysis Date = 04/27/21 Pct Recovery = 78% Analysis Date = 04/23/21 Pct Recovery = 78% Analysis Date = 04/23/21 Pct Recovery = 78% Analysis Date = 04/19/21 Pct Recovery = 78% Analysis Date = 04/19/21 Pct Recovery = 78% Analysis Date = 04/15/21 Pct Recovery = 78% Analysis Date = 04/15/21 Pct Recovery = 78% Analysis Date = 04/11/21 Pct Recovery = 79% Analysis Date = 04/11/21 Pct Recovery = 79% Analysis Date = 04/07/21 Pct Recovery = 79% Analysis Date = 04/07/21 Pct Recovery = 79% Analysis Date = 04/03/21 Pct Recovery = 80% Analysis Date = 04/03/21 Pct Recovery = 80% Analysis Date = 03/29/21 Pct Recovery = 81% Analysis Date = 03/29/21 Pct Recovery = 81% Analysis Date = 03/25/21 Pct Recovery = 82% Analysis Date = 03/25/21 Pct Recovery = 82% Analysis Date = 03/21/21 Pct Recovery = 83% Analysis Date = 03/21/21 Pct Recovery = 83% Analysis Date = 03/17/21 Pct Recovery = 83% Analysis Date = 03/17/21 Pct Recovery = 83% Analysis Date = 03/13/21 Pct Recovery = 84% Analysis Date = 03/13/21 Pct Recovery = 84% Analysis Date = 03/09/21 Pct Recovery = 85% Analysis Date = 03/09/21 Pct Recovery = 85% Analysis Date = 03/05/21 Pct Recovery = 86% Analysis Date = 03/05/21 Pct Recovery = 86% Analysis Date = 03/01/21 Pct Recovery = 87% Analysis Date = 03/01/21 Pct Recovery = 87% Analysis Date = 02/25/21 Pct Recovery = 87% Analysis Date = 02/25/21 Pct Recovery = 87% Analysis Date = 02/21/21 Pct Recovery = 88% Analysis Date = 02/21/21 Pct Recovery = 88% Analysis Date = 02/17/21 Pct Recovery = 89% Analysis Date = 02/17/21 Pct Recovery = 89% Analysis Date = 02/12/21 Pct Recovery = 90% Analysis Date = 02/12/21 Pct Recovery = 90% Analysis Date = 02/08/21 Pct Recovery = 91% Analysis Date = 02/08/21 Pct Recovery = 91% Analysis Date = 02/04/21 Pct Recovery = 91% Analysis Date = 02/04/21 Pct Recovery = 91% Analysis Date = 01/31/21 Pct Recovery = 92% Analysis Date = 01/31/21 Pct Recovery = 92% Analysis Date = 01/27/21 Pct Recovery = 93% Analysis Date = 01/27/21 Pct Recovery = 93% Analysis Date = 01/23/21 Pct Recovery = 93% Analysis Date = 01/23/21 Pct Recovery = 93% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/19/21 Pct Recovery = 94% Analysis Date = 01/15/21 Pct Recovery = 95% Analysis Date = 01/15/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 95% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 97% Analysis Date = 12/29/20 Pct Recovery = 97% Analysis Date = 12/25/20 Pct Recovery = 97% Analysis Date = 12/25/20 Pct Recovery = 97% Analysis Date = 12/21/20 Pct Recovery = 98% Analysis Date = 12/21/20 Pct Recovery = 98% Analysis Date = 12/17/20 Pct Recovery = 98% Analysis Date = 12/17/20 Pct Recovery = 98% Analysis Date = 12/13/20 Pct Recovery = 99% Analysis Date = 12/13/20 Pct Recovery = 99% Analysis Date = 12/09/20 Pct Recovery = 99% Analysis Date = 12/09/20 Pct Recovery = 99% Analysis Date = 12/05/20 Pct Recovery = 99% Analysis Date = 12/05/20 Pct Recovery = 99% Analysis Date = 12/01/20 Pct Recovery = 99% Analysis Date = 12/01/20 Pct Recovery = 99% Analysis Date = 11/27/20 Pct Recovery = 100% Analysis Date = 11/27/20 Pct Recovery = 100% Analysis Date = 11/23/20 Pct Recovery = 100% Analysis Date = 11/23/20 Pct Recovery = 100% Analysis Date = 11/19/20 Pct Recovery = 100% Analysis Date = 11/19/20 Pct Recovery = 100% Analysis Date = 11/14/20 Pct Recovery = 101% Analysis Date = 11/14/20 Pct Recovery = 101% Analysis Date = 11/10/20 Pct Recovery = 102% Analysis Date = 11/10/20 Pct Recovery = 102% Analysis Date = 11/06/20 Pct Recovery = 103% Analysis Date = 11/06/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 102% Analysis Date = 10/13/20 Pct Recovery = 101% Analysis Date = 10/13/20 Pct Recovery = 101% Analysis Date = 10/09/20 Pct Recovery = 101% Analysis Date = 10/09/20 Pct Recovery = 101% Analysis Date = 10/05/20 Pct Recovery = 101% Analysis Date = 10/05/20 Pct Recovery = 101% Analysis Date = 09/30/20 Pct Recovery = 100% Analysis Date = 09/30/20 Pct Recovery = 100% Analysis Date = 09/26/20 Pct Recovery = 100% Analysis Date = 09/26/20 Pct Recovery = 100% Analysis Date = 09/22/20 Pct Recovery = 99% Analysis Date = 09/22/20 Pct Recovery = 99% Analysis Date = 09/18/20 Pct Recovery = 99% Analysis Date = 09/18/20 Pct Recovery = 99% Analysis Date = 09/14/20 Pct Recovery = 100% Analysis Date = 09/14/20 Pct Recovery = 100% Analysis Date = 09/10/20 Pct Recovery = 100% Analysis Date = 09/10/20 Pct Recovery = 100% Analysis Date = 09/06/20 Pct Recovery = 100% Analysis Date = 09/06/20 Pct Recovery = 100% Analysis Date = 09/02/20 Pct Recovery = 100% Analysis Date = 09/02/20 Pct Recovery = 100% Analysis Date = 08/29/20 Pct Recovery = 100% Analysis Date = 08/29/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 100% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/16/20 Pct Recovery = 101% Analysis Date = 08/16/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/27/20 Pct Recovery = 102% Analysis Date = 07/27/20 Pct Recovery = 102% Analysis Date = 07/23/20 Pct Recovery = 102% Analysis Date = 07/23/20 Pct Recovery = 102% Analysis Date = 07/19/20 Pct Recovery = 102% Analysis Date = 07/19/20 Pct Recovery = 102% Analysis Date = 07/15/20 Pct Recovery = 102% Analysis Date = 07/15/20 Pct Recovery = 102% Analysis Date = 07/11/20 Pct Recovery = 102% Analysis Date = 07/11/20 Pct Recovery = 102% Analysis Date = 07/07/20 Pct Recovery = 102% Analysis Date = 07/07/20 Pct Recovery = 102% Analysis Date = 07/02/20 Pct Recovery = 102% Analysis Date = 07/02/20 Pct Recovery = 102% Analysis Date = 06/28/20 Pct Recovery = 102% Analysis Date = 06/28/20 Pct Recovery = 102% Analysis Date = 06/24/20 Pct Recovery = 103% Analysis Date = 06/24/20 Pct Recovery = 103% Analysis Date = 06/20/20 Pct Recovery = 103% Analysis Date = 06/20/20 Pct Recovery = 103% Analysis Date = 06/16/20 Pct Recovery = 103% Analysis Date = 06/16/20 Pct Recovery = 103% Analysis Date = 06/12/20 Pct Recovery = 103% Analysis Date = 06/12/20 Pct Recovery = 103% Analysis Date = 06/08/20 Pct Recovery = 103% Analysis Date = 06/08/20 Pct Recovery = 103% Analysis Date = 06/04/20 Pct Recovery = 103% Analysis Date = 06/04/20 Pct Recovery = 103% Analysis Date = 05/31/20 Pct Recovery = 103% Analysis Date = 05/31/20 Pct Recovery = 103% Analysis Date = 05/27/20 Pct Recovery = 103% Analysis Date = 05/27/20 Pct Recovery = 103% Analysis Date = 05/23/20 Pct Recovery = 103% Analysis Date = 05/23/20 Pct Recovery = 103% Analysis Date = 05/19/20 Pct Recovery = 104% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
IMAZETHAPYR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 95% 20% 91% 23%
Total 30 95% 20% 91% 23%

Sample Statistics
IMAZETHAPYR

Characteristic N % % Basis
Plotted 30 94% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 2 6% 2 out of 32
Not Spiked 84 .  
False Positives 0 0% 0 out of 84

OBSP Determination:
IMIDACLOPRID
METHOD: 2447 , TESTIDCODE: 68426LCM60

Laboratory ID = 20210760015 Lab Value = 181.743 Expected Conc. = 202 Report level label = 16 Pct Recovery = 90% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 172.604 Expected Conc. = 202 Report level label = 16 Pct Recovery = 85% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 154.044 Expected Conc. = 202 Report level label = 16 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 173.037 Expected Conc. = 202 Report level label = 16 Pct Recovery = 86% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202110006 Lab Value = 189.936 Expected Conc. = 200.8 Report level label = 16 Pct Recovery = 95% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 199.999 Expected Conc. = 200.6 Report level label = 16 Pct Recovery = 100% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 211.247 Expected Conc. = 200.3 Report level label = 16 Pct Recovery = 105% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 179.788 Expected Conc. = 200.3 Report level label = 16 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 198.668 Expected Conc. = 200.3 Report level label = 16 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150192 Lab Value = 117.148 Expected Conc. = 162.8 Report level label = 16 Pct Recovery = 72% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 78.129 Expected Conc. = 160 Report level label = 16 Pct Recovery = 49% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221870197 Lab Value = 80.426 Expected Conc. = 101.1 Report level label = 16 Pct Recovery = 80% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 78.045 Expected Conc. = 101 Report level label = 16 Pct Recovery = 77% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201680155 Lab Value = 102.459 Expected Conc. = 100.4 Report level label = 16 Pct Recovery = 102% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 71.588 Expected Conc. = 100.3 Report level label = 16 Pct Recovery = 71% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 90.374 Expected Conc. = 100.3 Report level label = 16 Pct Recovery = 90% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 81.936 Expected Conc. = 100.3 Report level label = 16 Pct Recovery = 82% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202880004 Lab Value = 105.317 Expected Conc. = 100.15 Report level label = 16 Pct Recovery = 105% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20220740064 Lab Value = 97.892 Expected Conc. = 99 Report level label = 16 Pct Recovery = 99% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20210900005 Lab Value = 84.624 Expected Conc. = 80.8 Report level label = 16 Pct Recovery = 105% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 71.169 Expected Conc. = 80.12 Report level label = 16 Pct Recovery = 89% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 64.067 Expected Conc. = 80.12 Report level label = 16 Pct Recovery = 80% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221660151 Lab Value = 36.913 Expected Conc. = 40.44 Report level label = 16 Pct Recovery = 91% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210690067 Lab Value = 53.526 Expected Conc. = 40.4 Report level label = 16 Pct Recovery = 132% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 53.884 Expected Conc. = 40.16 Report level label = 16 Pct Recovery = 134% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 39.459 Expected Conc. = 40.12 Report level label = 16 Pct Recovery = 98% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 50.384 Expected Conc. = 40.12 Report level label = 16 Pct Recovery = 126% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 42.171 Expected Conc. = 40.12 Report level label = 16 Pct Recovery = 105% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 44.407 Expected Conc. = 40.12 Report level label = 16 Pct Recovery = 111% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210120050 Lab Value = 32.028 Expected Conc. = 40.06 Report level label = 16 Pct Recovery = 80% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 36.290 Expected Conc. = 40.06 Report level label = 16 Pct Recovery = 91% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 36.923 Expected Conc. = 40.06 Report level label = 16 Pct Recovery = 92% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 38.343 Expected Conc. = 40.06 Report level label = 16 Pct Recovery = 96% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 29.071 Expected Conc. = 40.06 Report level label = 16 Pct Recovery = 73% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 75% Analysis Date = 08/10/22 Pct Recovery = 75% Analysis Date = 08/10/22 Pct Recovery = 75% Analysis Date = 08/06/22 Pct Recovery = 75% Analysis Date = 08/06/22 Pct Recovery = 75% Analysis Date = 08/02/22 Pct Recovery = 75% Analysis Date = 08/02/22 Pct Recovery = 75% Analysis Date = 07/29/22 Pct Recovery = 75% Analysis Date = 07/29/22 Pct Recovery = 75% Analysis Date = 07/25/22 Pct Recovery = 76% Analysis Date = 07/25/22 Pct Recovery = 76% Analysis Date = 07/21/22 Pct Recovery = 76% Analysis Date = 07/21/22 Pct Recovery = 76% Analysis Date = 07/17/22 Pct Recovery = 76% Analysis Date = 07/17/22 Pct Recovery = 76% Analysis Date = 07/13/22 Pct Recovery = 76% Analysis Date = 07/13/22 Pct Recovery = 76% Analysis Date = 07/09/22 Pct Recovery = 76% Analysis Date = 07/09/22 Pct Recovery = 76% Analysis Date = 07/05/22 Pct Recovery = 77% Analysis Date = 07/05/22 Pct Recovery = 77% Analysis Date = 07/01/22 Pct Recovery = 77% Analysis Date = 07/01/22 Pct Recovery = 77% Analysis Date = 06/26/22 Pct Recovery = 77% Analysis Date = 06/26/22 Pct Recovery = 77% Analysis Date = 06/22/22 Pct Recovery = 77% Analysis Date = 06/22/22 Pct Recovery = 77% Analysis Date = 06/18/22 Pct Recovery = 77% Analysis Date = 06/18/22 Pct Recovery = 77% Analysis Date = 06/14/22 Pct Recovery = 78% Analysis Date = 06/14/22 Pct Recovery = 78% Analysis Date = 06/10/22 Pct Recovery = 78% Analysis Date = 06/10/22 Pct Recovery = 78% Analysis Date = 06/06/22 Pct Recovery = 78% Analysis Date = 06/06/22 Pct Recovery = 78% Analysis Date = 06/02/22 Pct Recovery = 78% Analysis Date = 06/02/22 Pct Recovery = 78% Analysis Date = 05/29/22 Pct Recovery = 78% Analysis Date = 05/29/22 Pct Recovery = 78% Analysis Date = 05/25/22 Pct Recovery = 78% Analysis Date = 05/25/22 Pct Recovery = 78% Analysis Date = 05/21/22 Pct Recovery = 79% Analysis Date = 05/21/22 Pct Recovery = 79% Analysis Date = 05/17/22 Pct Recovery = 79% Analysis Date = 05/17/22 Pct Recovery = 79% Analysis Date = 05/12/22 Pct Recovery = 79% Analysis Date = 05/12/22 Pct Recovery = 79% Analysis Date = 05/08/22 Pct Recovery = 79% Analysis Date = 05/08/22 Pct Recovery = 79% Analysis Date = 05/04/22 Pct Recovery = 79% Analysis Date = 05/04/22 Pct Recovery = 79% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/30/22 Pct Recovery = 80% Analysis Date = 04/26/22 Pct Recovery = 80% Analysis Date = 04/26/22 Pct Recovery = 80% Analysis Date = 04/22/22 Pct Recovery = 80% Analysis Date = 04/22/22 Pct Recovery = 80% Analysis Date = 04/18/22 Pct Recovery = 80% Analysis Date = 04/18/22 Pct Recovery = 80% Analysis Date = 04/14/22 Pct Recovery = 80% Analysis Date = 04/14/22 Pct Recovery = 80% Analysis Date = 04/10/22 Pct Recovery = 80% Analysis Date = 04/10/22 Pct Recovery = 80% Analysis Date = 04/06/22 Pct Recovery = 81% Analysis Date = 04/06/22 Pct Recovery = 81% Analysis Date = 04/02/22 Pct Recovery = 81% Analysis Date = 04/02/22 Pct Recovery = 81% Analysis Date = 03/28/22 Pct Recovery = 81% Analysis Date = 03/28/22 Pct Recovery = 81% Analysis Date = 03/24/22 Pct Recovery = 81% Analysis Date = 03/24/22 Pct Recovery = 81% Analysis Date = 03/20/22 Pct Recovery = 81% Analysis Date = 03/20/22 Pct Recovery = 81% Analysis Date = 03/16/22 Pct Recovery = 81% Analysis Date = 03/16/22 Pct Recovery = 81% Analysis Date = 03/12/22 Pct Recovery = 82% Analysis Date = 03/12/22 Pct Recovery = 82% Analysis Date = 03/08/22 Pct Recovery = 82% Analysis Date = 03/08/22 Pct Recovery = 82% Analysis Date = 03/04/22 Pct Recovery = 82% Analysis Date = 03/04/22 Pct Recovery = 82% Analysis Date = 02/28/22 Pct Recovery = 82% Analysis Date = 02/28/22 Pct Recovery = 82% Analysis Date = 02/24/22 Pct Recovery = 82% Analysis Date = 02/24/22 Pct Recovery = 82% Analysis Date = 02/20/22 Pct Recovery = 82% Analysis Date = 02/20/22 Pct Recovery = 82% Analysis Date = 02/16/22 Pct Recovery = 82% Analysis Date = 02/16/22 Pct Recovery = 82% Analysis Date = 02/11/22 Pct Recovery = 83% Analysis Date = 02/11/22 Pct Recovery = 83% Analysis Date = 02/07/22 Pct Recovery = 83% Analysis Date = 02/07/22 Pct Recovery = 83% Analysis Date = 02/03/22 Pct Recovery = 83% Analysis Date = 02/03/22 Pct Recovery = 83% Analysis Date = 01/30/22 Pct Recovery = 83% Analysis Date = 01/30/22 Pct Recovery = 83% Analysis Date = 01/26/22 Pct Recovery = 83% Analysis Date = 01/26/22 Pct Recovery = 83% Analysis Date = 01/22/22 Pct Recovery = 83% Analysis Date = 01/22/22 Pct Recovery = 83% Analysis Date = 01/18/22 Pct Recovery = 83% Analysis Date = 01/18/22 Pct Recovery = 83% Analysis Date = 01/14/22 Pct Recovery = 83% Analysis Date = 01/14/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 84% Analysis Date = 01/10/22 Pct Recovery = 84% Analysis Date = 01/06/22 Pct Recovery = 84% Analysis Date = 01/06/22 Pct Recovery = 84% Analysis Date = 01/02/22 Pct Recovery = 84% Analysis Date = 01/02/22 Pct Recovery = 84% Analysis Date = 12/28/21 Pct Recovery = 84% Analysis Date = 12/28/21 Pct Recovery = 84% Analysis Date = 12/24/21 Pct Recovery = 84% Analysis Date = 12/24/21 Pct Recovery = 84% Analysis Date = 12/20/21 Pct Recovery = 84% Analysis Date = 12/20/21 Pct Recovery = 84% Analysis Date = 12/16/21 Pct Recovery = 84% Analysis Date = 12/16/21 Pct Recovery = 84% Analysis Date = 12/12/21 Pct Recovery = 85% Analysis Date = 12/12/21 Pct Recovery = 85% Analysis Date = 12/08/21 Pct Recovery = 85% Analysis Date = 12/08/21 Pct Recovery = 85% Analysis Date = 12/04/21 Pct Recovery = 85% Analysis Date = 12/04/21 Pct Recovery = 85% Analysis Date = 11/30/21 Pct Recovery = 85% Analysis Date = 11/30/21 Pct Recovery = 85% Analysis Date = 11/26/21 Pct Recovery = 85% Analysis Date = 11/26/21 Pct Recovery = 85% Analysis Date = 11/22/21 Pct Recovery = 85% Analysis Date = 11/22/21 Pct Recovery = 85% Analysis Date = 11/18/21 Pct Recovery = 85% Analysis Date = 11/18/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 86% Analysis Date = 11/09/21 Pct Recovery = 86% Analysis Date = 11/05/21 Pct Recovery = 86% Analysis Date = 11/05/21 Pct Recovery = 86% Analysis Date = 11/01/21 Pct Recovery = 86% Analysis Date = 11/01/21 Pct Recovery = 86% Analysis Date = 10/28/21 Pct Recovery = 86% Analysis Date = 10/28/21 Pct Recovery = 86% Analysis Date = 10/24/21 Pct Recovery = 86% Analysis Date = 10/24/21 Pct Recovery = 86% Analysis Date = 10/20/21 Pct Recovery = 86% Analysis Date = 10/20/21 Pct Recovery = 86% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/12/21 Pct Recovery = 86% Analysis Date = 10/12/21 Pct Recovery = 86% Analysis Date = 10/08/21 Pct Recovery = 87% Analysis Date = 10/08/21 Pct Recovery = 87% Analysis Date = 10/04/21 Pct Recovery = 87% Analysis Date = 10/04/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 87% Analysis Date = 09/13/21 Pct Recovery = 87% Analysis Date = 09/13/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 88% Analysis Date = 09/01/21 Pct Recovery = 88% Analysis Date = 09/01/21 Pct Recovery = 88% Analysis Date = 08/28/21 Pct Recovery = 88% Analysis Date = 08/28/21 Pct Recovery = 88% Analysis Date = 08/24/21 Pct Recovery = 88% Analysis Date = 08/24/21 Pct Recovery = 88% Analysis Date = 08/20/21 Pct Recovery = 88% Analysis Date = 08/20/21 Pct Recovery = 88% Analysis Date = 08/15/21 Pct Recovery = 88% Analysis Date = 08/15/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 89% Analysis Date = 08/07/21 Pct Recovery = 89% Analysis Date = 08/03/21 Pct Recovery = 89% Analysis Date = 08/03/21 Pct Recovery = 89% Analysis Date = 07/30/21 Pct Recovery = 89% Analysis Date = 07/30/21 Pct Recovery = 89% Analysis Date = 07/26/21 Pct Recovery = 89% Analysis Date = 07/26/21 Pct Recovery = 89% Analysis Date = 07/22/21 Pct Recovery = 89% Analysis Date = 07/22/21 Pct Recovery = 89% Analysis Date = 07/18/21 Pct Recovery = 89% Analysis Date = 07/18/21 Pct Recovery = 89% Analysis Date = 07/14/21 Pct Recovery = 89% Analysis Date = 07/14/21 Pct Recovery = 89% Analysis Date = 07/10/21 Pct Recovery = 90% Analysis Date = 07/10/21 Pct Recovery = 90% Analysis Date = 07/06/21 Pct Recovery = 90% Analysis Date = 07/06/21 Pct Recovery = 90% Analysis Date = 07/02/21 Pct Recovery = 90% Analysis Date = 07/02/21 Pct Recovery = 90% Analysis Date = 06/27/21 Pct Recovery = 90% Analysis Date = 06/27/21 Pct Recovery = 90% Analysis Date = 06/23/21 Pct Recovery = 90% Analysis Date = 06/23/21 Pct Recovery = 90% Analysis Date = 06/19/21 Pct Recovery = 90% Analysis Date = 06/19/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/15/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/11/21 Pct Recovery = 90% Analysis Date = 06/07/21 Pct Recovery = 91% Analysis Date = 06/07/21 Pct Recovery = 91% Analysis Date = 06/03/21 Pct Recovery = 91% Analysis Date = 06/03/21 Pct Recovery = 91% Analysis Date = 05/30/21 Pct Recovery = 91% Analysis Date = 05/30/21 Pct Recovery = 91% Analysis Date = 05/26/21 Pct Recovery = 91% Analysis Date = 05/26/21 Pct Recovery = 91% Analysis Date = 05/22/21 Pct Recovery = 91% Analysis Date = 05/22/21 Pct Recovery = 91% Analysis Date = 05/18/21 Pct Recovery = 91% Analysis Date = 05/18/21 Pct Recovery = 91% Analysis Date = 05/13/21 Pct Recovery = 91% Analysis Date = 05/13/21 Pct Recovery = 91% Analysis Date = 05/09/21 Pct Recovery = 91% Analysis Date = 05/09/21 Pct Recovery = 91% Analysis Date = 05/05/21 Pct Recovery = 92% Analysis Date = 05/05/21 Pct Recovery = 92% Analysis Date = 05/01/21 Pct Recovery = 92% Analysis Date = 05/01/21 Pct Recovery = 92% Analysis Date = 04/27/21 Pct Recovery = 92% Analysis Date = 04/27/21 Pct Recovery = 92% Analysis Date = 04/23/21 Pct Recovery = 92% Analysis Date = 04/23/21 Pct Recovery = 92% Analysis Date = 04/19/21 Pct Recovery = 92% Analysis Date = 04/19/21 Pct Recovery = 92% Analysis Date = 04/15/21 Pct Recovery = 92% Analysis Date = 04/15/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/11/21 Pct Recovery = 92% Analysis Date = 04/07/21 Pct Recovery = 93% Analysis Date = 04/07/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/25/21 Pct Recovery = 93% Analysis Date = 03/25/21 Pct Recovery = 93% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/01/21 Pct Recovery = 93% Analysis Date = 03/01/21 Pct Recovery = 93% Analysis Date = 02/25/21 Pct Recovery = 93% Analysis Date = 02/25/21 Pct Recovery = 93% Analysis Date = 02/21/21 Pct Recovery = 92% Analysis Date = 02/21/21 Pct Recovery = 92% Analysis Date = 02/17/21 Pct Recovery = 92% Analysis Date = 02/17/21 Pct Recovery = 92% Analysis Date = 02/12/21 Pct Recovery = 92% Analysis Date = 02/12/21 Pct Recovery = 92% Analysis Date = 02/08/21 Pct Recovery = 91% Analysis Date = 02/08/21 Pct Recovery = 91% Analysis Date = 02/04/21 Pct Recovery = 91% Analysis Date = 02/04/21 Pct Recovery = 91% Analysis Date = 01/31/21 Pct Recovery = 91% Analysis Date = 01/31/21 Pct Recovery = 91% Analysis Date = 01/27/21 Pct Recovery = 91% Analysis Date = 01/27/21 Pct Recovery = 91% Analysis Date = 01/23/21 Pct Recovery = 91% Analysis Date = 01/23/21 Pct Recovery = 91% Analysis Date = 01/19/21 Pct Recovery = 91% Analysis Date = 01/19/21 Pct Recovery = 91% Analysis Date = 01/15/21 Pct Recovery = 91% Analysis Date = 01/15/21 Pct Recovery = 91% Analysis Date = 01/11/21 Pct Recovery = 91% Analysis Date = 01/11/21 Pct Recovery = 91% Analysis Date = 01/07/21 Pct Recovery = 91% Analysis Date = 01/07/21 Pct Recovery = 91% Analysis Date = 01/03/21 Pct Recovery = 91% Analysis Date = 01/03/21 Pct Recovery = 91% Analysis Date = 12/29/20 Pct Recovery = 91% Analysis Date = 12/29/20 Pct Recovery = 91% Analysis Date = 12/25/20 Pct Recovery = 90% Analysis Date = 12/25/20 Pct Recovery = 90% Analysis Date = 12/21/20 Pct Recovery = 90% Analysis Date = 12/21/20 Pct Recovery = 90% Analysis Date = 12/17/20 Pct Recovery = 90% Analysis Date = 12/17/20 Pct Recovery = 90% Analysis Date = 12/13/20 Pct Recovery = 90% Analysis Date = 12/13/20 Pct Recovery = 90% Analysis Date = 12/09/20 Pct Recovery = 90% Analysis Date = 12/09/20 Pct Recovery = 90% Analysis Date = 12/05/20 Pct Recovery = 90% Analysis Date = 12/05/20 Pct Recovery = 90% Analysis Date = 12/01/20 Pct Recovery = 90% Analysis Date = 12/01/20 Pct Recovery = 90% Analysis Date = 11/27/20 Pct Recovery = 90% Analysis Date = 11/27/20 Pct Recovery = 90% Analysis Date = 11/23/20 Pct Recovery = 90% Analysis Date = 11/23/20 Pct Recovery = 90% Analysis Date = 11/19/20 Pct Recovery = 90% Analysis Date = 11/19/20 Pct Recovery = 90% Analysis Date = 11/14/20 Pct Recovery = 90% Analysis Date = 11/14/20 Pct Recovery = 90% Analysis Date = 11/10/20 Pct Recovery = 90% Analysis Date = 11/10/20 Pct Recovery = 90% Analysis Date = 11/06/20 Pct Recovery = 91% Analysis Date = 11/06/20 Pct Recovery = 91% Analysis Date = 11/02/20 Pct Recovery = 91% Analysis Date = 11/02/20 Pct Recovery = 91% Analysis Date = 10/29/20 Pct Recovery = 92% Analysis Date = 10/29/20 Pct Recovery = 92% Analysis Date = 10/25/20 Pct Recovery = 92% Analysis Date = 10/25/20 Pct Recovery = 92% Analysis Date = 10/21/20 Pct Recovery = 92% Analysis Date = 10/21/20 Pct Recovery = 92% Analysis Date = 10/17/20 Pct Recovery = 93% Analysis Date = 10/17/20 Pct Recovery = 93% Analysis Date = 10/13/20 Pct Recovery = 93% Analysis Date = 10/13/20 Pct Recovery = 93% Analysis Date = 10/09/20 Pct Recovery = 94% Analysis Date = 10/09/20 Pct Recovery = 94% Analysis Date = 10/05/20 Pct Recovery = 94% Analysis Date = 10/05/20 Pct Recovery = 94% Analysis Date = 09/30/20 Pct Recovery = 94% Analysis Date = 09/30/20 Pct Recovery = 94% Analysis Date = 09/26/20 Pct Recovery = 95% Analysis Date = 09/26/20 Pct Recovery = 95% Analysis Date = 09/22/20 Pct Recovery = 95% Analysis Date = 09/22/20 Pct Recovery = 95% Analysis Date = 09/18/20 Pct Recovery = 96% Analysis Date = 09/18/20 Pct Recovery = 96% Analysis Date = 09/14/20 Pct Recovery = 96% Analysis Date = 09/14/20 Pct Recovery = 96% Analysis Date = 09/10/20 Pct Recovery = 97% Analysis Date = 09/10/20 Pct Recovery = 97% Analysis Date = 09/06/20 Pct Recovery = 97% Analysis Date = 09/06/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 98% Analysis Date = 09/02/20 Pct Recovery = 98% Analysis Date = 08/29/20 Pct Recovery = 98% Analysis Date = 08/29/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 99% Analysis Date = 08/25/20 Pct Recovery = 99% Analysis Date = 08/21/20 Pct Recovery = 99% Analysis Date = 08/21/20 Pct Recovery = 99% Analysis Date = 08/16/20 Pct Recovery = 99% Analysis Date = 08/16/20 Pct Recovery = 99% Analysis Date = 08/12/20 Pct Recovery = 100% Analysis Date = 08/12/20 Pct Recovery = 100% Analysis Date = 08/08/20 Pct Recovery = 100% Analysis Date = 08/08/20 Pct Recovery = 100% Analysis Date = 08/04/20 Pct Recovery = 100% Analysis Date = 08/04/20 Pct Recovery = 100% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/27/20 Pct Recovery = 101% Analysis Date = 07/27/20 Pct Recovery = 101% Analysis Date = 07/23/20 Pct Recovery = 102% Analysis Date = 07/23/20 Pct Recovery = 102% Analysis Date = 07/19/20 Pct Recovery = 102% Analysis Date = 07/19/20 Pct Recovery = 102% Analysis Date = 07/15/20 Pct Recovery = 102% Analysis Date = 07/15/20 Pct Recovery = 102% Analysis Date = 07/11/20 Pct Recovery = 103% Analysis Date = 07/11/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/02/20 Pct Recovery = 104% Analysis Date = 07/02/20 Pct Recovery = 104% Analysis Date = 06/28/20 Pct Recovery = 104% Analysis Date = 06/28/20 Pct Recovery = 104% Analysis Date = 06/24/20 Pct Recovery = 105% Analysis Date = 06/24/20 Pct Recovery = 105% Analysis Date = 06/20/20 Pct Recovery = 105% Analysis Date = 06/20/20 Pct Recovery = 105% Analysis Date = 06/16/20 Pct Recovery = 105% Analysis Date = 06/16/20 Pct Recovery = 105% Analysis Date = 06/12/20 Pct Recovery = 106% Analysis Date = 06/12/20 Pct Recovery = 106% Analysis Date = 06/08/20 Pct Recovery = 106% Analysis Date = 06/08/20 Pct Recovery = 106% Analysis Date = 06/04/20 Pct Recovery = 107% Analysis Date = 06/04/20 Pct Recovery = 107% Analysis Date = 05/31/20 Pct Recovery = 107% Analysis Date = 05/31/20 Pct Recovery = 107% Analysis Date = 05/27/20 Pct Recovery = 108% Analysis Date = 05/27/20 Pct Recovery = 108% Analysis Date = 05/23/20 Pct Recovery = 108% Analysis Date = 05/23/20 Pct Recovery = 108% Analysis Date = 05/19/20 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
IMIDACLOPRID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 93% 17% 91% 16%
Total 34 93% 17% 91% 16%

Sample Statistics
IMIDACLOPRID

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 3 9% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 34
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
LINURON
METHOD: 2447 , TESTIDCODE: 68639LCM60

Laboratory ID = 20210760015 Lab Value = 67.139 Expected Conc. = 70.4 Report level label = 5.6 Pct Recovery = 95% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 67.771 Expected Conc. = 70.4 Report level label = 5.6 Pct Recovery = 96% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 54.965 Expected Conc. = 70.4 Report level label = 5.6 Pct Recovery = 78% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 65.046 Expected Conc. = 70.4 Report level label = 5.6 Pct Recovery = 92% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 49.077 Expected Conc. = 70 Report level label = 5.6 Pct Recovery = 70% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 60.135 Expected Conc. = 70 Report level label = 5.6 Pct Recovery = 86% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 60.711 Expected Conc. = 70 Report level label = 5.6 Pct Recovery = 87% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221520237 Lab Value = 45.982 Expected Conc. = 56.64 Report level label = 5.6 Pct Recovery = 81% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20222150192 Lab Value = 38.281 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 68% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 39.281 Expected Conc. = 56 Report level label = 5.6 Pct Recovery = 70% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20201550031 Lab Value = 46.183 Expected Conc. = 35.7 Report level label = 5.6 Pct Recovery = 129% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20221870197 Lab Value = 32.040 Expected Conc. = 35.4 Report level label = 5.6 Pct Recovery = 91% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20220740064 Lab Value = 23.971 Expected Conc. = 35.25 Report level label = 5.6 Pct Recovery = 68% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20210480001 Lab Value = 26.031 Expected Conc. = 35.2 Report level label = 5.6 Pct Recovery = 74% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202390020 Lab Value = 44.131 Expected Conc. = 35.05 Report level label = 5.6 Pct Recovery = 126% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 35.455 Expected Conc. = 35.05 Report level label = 5.6 Pct Recovery = 101% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202880004 Lab Value = 40.909 Expected Conc. = 35 Report level label = 5.6 Pct Recovery = 117% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 25.434 Expected Conc. = 28.16 Report level label = 5.6 Pct Recovery = 90% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201960104 Lab Value = 31.928 Expected Conc. = 28.04 Report level label = 5.6 Pct Recovery = 114% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 30.661 Expected Conc. = 28.04 Report level label = 5.6 Pct Recovery = 109% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210620006 Lab Value = 22.634 Expected Conc. = 28 Report level label = 5.6 Pct Recovery = 81% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 20.344 Expected Conc. = 28 Report level label = 5.6 Pct Recovery = 73% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202330309 Lab Value = 9.193 Expected Conc. = 14.28 Report level label = 5.6 Pct Recovery = 64% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 9.622 Expected Conc. = 14.28 Report level label = 5.6 Pct Recovery = 67% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 17.419 Expected Conc. = 14.28 Report level label = 5.6 Pct Recovery = 122% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 13.458 Expected Conc. = 14.28 Report level label = 5.6 Pct Recovery = 94% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 15.009 Expected Conc. = 14.28 Report level label = 5.6 Pct Recovery = 105% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20221660151 Lab Value = 12.265 Expected Conc. = 14.16 Report level label = 5.6 Pct Recovery = 87% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210690067 Lab Value = 18.223 Expected Conc. = 14.08 Report level label = 5.6 Pct Recovery = 129% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210120050 Lab Value = 13.469 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 96% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 15.582 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 111% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 18.872 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 135% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 13.775 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 98% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 14.277 Expected Conc. = 14 Report level label = 5.6 Pct Recovery = 102% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/02/22 Pct Recovery = 77% Analysis Date = 08/02/22 Pct Recovery = 77% Analysis Date = 07/29/22 Pct Recovery = 77% Analysis Date = 07/29/22 Pct Recovery = 77% Analysis Date = 07/25/22 Pct Recovery = 77% Analysis Date = 07/25/22 Pct Recovery = 77% Analysis Date = 07/21/22 Pct Recovery = 77% Analysis Date = 07/21/22 Pct Recovery = 77% Analysis Date = 07/17/22 Pct Recovery = 77% Analysis Date = 07/17/22 Pct Recovery = 77% Analysis Date = 07/13/22 Pct Recovery = 77% Analysis Date = 07/13/22 Pct Recovery = 77% Analysis Date = 07/09/22 Pct Recovery = 77% Analysis Date = 07/09/22 Pct Recovery = 77% Analysis Date = 07/05/22 Pct Recovery = 77% Analysis Date = 07/05/22 Pct Recovery = 77% Analysis Date = 07/01/22 Pct Recovery = 78% Analysis Date = 07/01/22 Pct Recovery = 78% Analysis Date = 06/27/22 Pct Recovery = 78% Analysis Date = 06/27/22 Pct Recovery = 78% Analysis Date = 06/23/22 Pct Recovery = 78% Analysis Date = 06/23/22 Pct Recovery = 78% Analysis Date = 06/19/22 Pct Recovery = 78% Analysis Date = 06/19/22 Pct Recovery = 78% Analysis Date = 06/15/22 Pct Recovery = 78% Analysis Date = 06/15/22 Pct Recovery = 78% Analysis Date = 06/11/22 Pct Recovery = 78% Analysis Date = 06/11/22 Pct Recovery = 78% Analysis Date = 06/07/22 Pct Recovery = 78% Analysis Date = 06/07/22 Pct Recovery = 78% Analysis Date = 06/03/22 Pct Recovery = 78% Analysis Date = 06/03/22 Pct Recovery = 78% Analysis Date = 05/30/22 Pct Recovery = 78% Analysis Date = 05/30/22 Pct Recovery = 78% Analysis Date = 05/26/22 Pct Recovery = 79% Analysis Date = 05/26/22 Pct Recovery = 79% Analysis Date = 05/22/22 Pct Recovery = 79% Analysis Date = 05/22/22 Pct Recovery = 79% Analysis Date = 05/18/22 Pct Recovery = 79% Analysis Date = 05/18/22 Pct Recovery = 79% Analysis Date = 05/14/22 Pct Recovery = 79% Analysis Date = 05/14/22 Pct Recovery = 79% Analysis Date = 05/10/22 Pct Recovery = 79% Analysis Date = 05/10/22 Pct Recovery = 79% Analysis Date = 05/06/22 Pct Recovery = 79% Analysis Date = 05/06/22 Pct Recovery = 79% Analysis Date = 05/01/22 Pct Recovery = 79% Analysis Date = 05/01/22 Pct Recovery = 79% Analysis Date = 04/27/22 Pct Recovery = 80% Analysis Date = 04/27/22 Pct Recovery = 80% Analysis Date = 04/23/22 Pct Recovery = 80% Analysis Date = 04/23/22 Pct Recovery = 80% Analysis Date = 04/19/22 Pct Recovery = 80% Analysis Date = 04/19/22 Pct Recovery = 80% Analysis Date = 04/15/22 Pct Recovery = 80% Analysis Date = 04/15/22 Pct Recovery = 80% Analysis Date = 04/11/22 Pct Recovery = 80% Analysis Date = 04/11/22 Pct Recovery = 80% Analysis Date = 04/07/22 Pct Recovery = 80% Analysis Date = 04/07/22 Pct Recovery = 80% Analysis Date = 04/03/22 Pct Recovery = 80% Analysis Date = 04/03/22 Pct Recovery = 80% Analysis Date = 03/30/22 Pct Recovery = 80% Analysis Date = 03/30/22 Pct Recovery = 80% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/26/22 Pct Recovery = 81% Analysis Date = 03/22/22 Pct Recovery = 81% Analysis Date = 03/22/22 Pct Recovery = 81% Analysis Date = 03/18/22 Pct Recovery = 81% Analysis Date = 03/18/22 Pct Recovery = 81% Analysis Date = 03/14/22 Pct Recovery = 81% Analysis Date = 03/14/22 Pct Recovery = 81% Analysis Date = 03/10/22 Pct Recovery = 81% Analysis Date = 03/10/22 Pct Recovery = 81% Analysis Date = 03/06/22 Pct Recovery = 81% Analysis Date = 03/06/22 Pct Recovery = 81% Analysis Date = 03/02/22 Pct Recovery = 81% Analysis Date = 03/02/22 Pct Recovery = 81% Analysis Date = 02/26/22 Pct Recovery = 81% Analysis Date = 02/26/22 Pct Recovery = 81% Analysis Date = 02/22/22 Pct Recovery = 82% Analysis Date = 02/22/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 01/29/22 Pct Recovery = 82% Analysis Date = 01/29/22 Pct Recovery = 82% Analysis Date = 01/25/22 Pct Recovery = 82% Analysis Date = 01/25/22 Pct Recovery = 82% Analysis Date = 01/20/22 Pct Recovery = 83% Analysis Date = 01/20/22 Pct Recovery = 83% Analysis Date = 01/16/22 Pct Recovery = 83% Analysis Date = 01/16/22 Pct Recovery = 83% Analysis Date = 01/12/22 Pct Recovery = 83% Analysis Date = 01/12/22 Pct Recovery = 83% Analysis Date = 01/08/22 Pct Recovery = 83% Analysis Date = 01/08/22 Pct Recovery = 83% Analysis Date = 01/04/22 Pct Recovery = 83% Analysis Date = 01/04/22 Pct Recovery = 83% Analysis Date = 12/31/21 Pct Recovery = 83% Analysis Date = 12/31/21 Pct Recovery = 83% Analysis Date = 12/27/21 Pct Recovery = 83% Analysis Date = 12/27/21 Pct Recovery = 83% Analysis Date = 12/23/21 Pct Recovery = 83% Analysis Date = 12/23/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 84% Analysis Date = 12/19/21 Pct Recovery = 84% Analysis Date = 12/15/21 Pct Recovery = 84% Analysis Date = 12/15/21 Pct Recovery = 84% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/11/21 Pct Recovery = 84% Analysis Date = 12/07/21 Pct Recovery = 84% Analysis Date = 12/07/21 Pct Recovery = 84% Analysis Date = 12/03/21 Pct Recovery = 84% Analysis Date = 12/03/21 Pct Recovery = 84% Analysis Date = 11/29/21 Pct Recovery = 84% Analysis Date = 11/29/21 Pct Recovery = 84% Analysis Date = 11/25/21 Pct Recovery = 84% Analysis Date = 11/25/21 Pct Recovery = 84% Analysis Date = 11/21/21 Pct Recovery = 84% Analysis Date = 11/21/21 Pct Recovery = 84% Analysis Date = 11/17/21 Pct Recovery = 85% Analysis Date = 11/17/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/11/21 Pct Recovery = 86% Analysis Date = 10/11/21 Pct Recovery = 86% Analysis Date = 10/07/21 Pct Recovery = 86% Analysis Date = 10/07/21 Pct Recovery = 86% Analysis Date = 10/03/21 Pct Recovery = 86% Analysis Date = 10/03/21 Pct Recovery = 86% Analysis Date = 09/29/21 Pct Recovery = 86% Analysis Date = 09/29/21 Pct Recovery = 86% Analysis Date = 09/25/21 Pct Recovery = 86% Analysis Date = 09/25/21 Pct Recovery = 86% Analysis Date = 09/21/21 Pct Recovery = 86% Analysis Date = 09/21/21 Pct Recovery = 86% Analysis Date = 09/17/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 87% Analysis Date = 09/13/21 Pct Recovery = 87% Analysis Date = 09/13/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 87% Analysis Date = 09/09/21 Pct Recovery = 87% Analysis Date = 09/05/21 Pct Recovery = 87% Analysis Date = 09/05/21 Pct Recovery = 87% Analysis Date = 09/01/21 Pct Recovery = 87% Analysis Date = 09/01/21 Pct Recovery = 87% Analysis Date = 08/28/21 Pct Recovery = 87% Analysis Date = 08/28/21 Pct Recovery = 87% Analysis Date = 08/24/21 Pct Recovery = 87% Analysis Date = 08/24/21 Pct Recovery = 87% Analysis Date = 08/20/21 Pct Recovery = 87% Analysis Date = 08/20/21 Pct Recovery = 87% Analysis Date = 08/16/21 Pct Recovery = 88% Analysis Date = 08/16/21 Pct Recovery = 88% Analysis Date = 08/12/21 Pct Recovery = 88% Analysis Date = 08/12/21 Pct Recovery = 88% Analysis Date = 08/08/21 Pct Recovery = 88% Analysis Date = 08/08/21 Pct Recovery = 88% Analysis Date = 08/04/21 Pct Recovery = 88% Analysis Date = 08/04/21 Pct Recovery = 88% Analysis Date = 07/31/21 Pct Recovery = 88% Analysis Date = 07/31/21 Pct Recovery = 88% Analysis Date = 07/27/21 Pct Recovery = 88% Analysis Date = 07/27/21 Pct Recovery = 88% Analysis Date = 07/23/21 Pct Recovery = 88% Analysis Date = 07/23/21 Pct Recovery = 88% Analysis Date = 07/19/21 Pct Recovery = 88% Analysis Date = 07/19/21 Pct Recovery = 88% Analysis Date = 07/15/21 Pct Recovery = 89% Analysis Date = 07/15/21 Pct Recovery = 89% Analysis Date = 07/11/21 Pct Recovery = 89% Analysis Date = 07/11/21 Pct Recovery = 89% Analysis Date = 07/07/21 Pct Recovery = 89% Analysis Date = 07/07/21 Pct Recovery = 89% Analysis Date = 07/02/21 Pct Recovery = 89% Analysis Date = 07/02/21 Pct Recovery = 89% Analysis Date = 06/28/21 Pct Recovery = 89% Analysis Date = 06/28/21 Pct Recovery = 89% Analysis Date = 06/24/21 Pct Recovery = 89% Analysis Date = 06/24/21 Pct Recovery = 89% Analysis Date = 06/20/21 Pct Recovery = 89% Analysis Date = 06/20/21 Pct Recovery = 89% Analysis Date = 06/16/21 Pct Recovery = 89% Analysis Date = 06/16/21 Pct Recovery = 89% Analysis Date = 06/12/21 Pct Recovery = 90% Analysis Date = 06/12/21 Pct Recovery = 90% Analysis Date = 06/08/21 Pct Recovery = 90% Analysis Date = 06/08/21 Pct Recovery = 90% Analysis Date = 06/04/21 Pct Recovery = 90% Analysis Date = 06/04/21 Pct Recovery = 90% Analysis Date = 05/31/21 Pct Recovery = 90% Analysis Date = 05/31/21 Pct Recovery = 90% Analysis Date = 05/27/21 Pct Recovery = 90% Analysis Date = 05/27/21 Pct Recovery = 90% Analysis Date = 05/23/21 Pct Recovery = 90% Analysis Date = 05/23/21 Pct Recovery = 90% Analysis Date = 05/19/21 Pct Recovery = 90% Analysis Date = 05/19/21 Pct Recovery = 90% Analysis Date = 05/15/21 Pct Recovery = 90% Analysis Date = 05/15/21 Pct Recovery = 90% Analysis Date = 05/11/21 Pct Recovery = 91% Analysis Date = 05/11/21 Pct Recovery = 91% Analysis Date = 05/07/21 Pct Recovery = 91% Analysis Date = 05/07/21 Pct Recovery = 91% Analysis Date = 05/03/21 Pct Recovery = 91% Analysis Date = 05/03/21 Pct Recovery = 91% Analysis Date = 04/29/21 Pct Recovery = 91% Analysis Date = 04/29/21 Pct Recovery = 91% Analysis Date = 04/25/21 Pct Recovery = 91% Analysis Date = 04/25/21 Pct Recovery = 91% Analysis Date = 04/21/21 Pct Recovery = 91% Analysis Date = 04/21/21 Pct Recovery = 91% Analysis Date = 04/17/21 Pct Recovery = 91% Analysis Date = 04/17/21 Pct Recovery = 91% Analysis Date = 04/13/21 Pct Recovery = 91% Analysis Date = 04/13/21 Pct Recovery = 91% Analysis Date = 04/09/21 Pct Recovery = 92% Analysis Date = 04/09/21 Pct Recovery = 92% Analysis Date = 04/05/21 Pct Recovery = 92% Analysis Date = 04/05/21 Pct Recovery = 92% Analysis Date = 04/01/21 Pct Recovery = 92% Analysis Date = 04/01/21 Pct Recovery = 92% Analysis Date = 03/28/21 Pct Recovery = 92% Analysis Date = 03/28/21 Pct Recovery = 92% Analysis Date = 03/23/21 Pct Recovery = 92% Analysis Date = 03/23/21 Pct Recovery = 92% Analysis Date = 03/19/21 Pct Recovery = 92% Analysis Date = 03/19/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/11/21 Pct Recovery = 93% Analysis Date = 03/11/21 Pct Recovery = 93% Analysis Date = 03/07/21 Pct Recovery = 93% Analysis Date = 03/07/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 93% Analysis Date = 02/27/21 Pct Recovery = 93% Analysis Date = 02/27/21 Pct Recovery = 93% Analysis Date = 02/23/21 Pct Recovery = 94% Analysis Date = 02/23/21 Pct Recovery = 94% Analysis Date = 02/19/21 Pct Recovery = 94% Analysis Date = 02/19/21 Pct Recovery = 94% Analysis Date = 02/15/21 Pct Recovery = 94% Analysis Date = 02/15/21 Pct Recovery = 94% Analysis Date = 02/11/21 Pct Recovery = 94% Analysis Date = 02/11/21 Pct Recovery = 94% Analysis Date = 02/07/21 Pct Recovery = 94% Analysis Date = 02/07/21 Pct Recovery = 94% Analysis Date = 02/03/21 Pct Recovery = 95% Analysis Date = 02/03/21 Pct Recovery = 95% Analysis Date = 01/30/21 Pct Recovery = 95% Analysis Date = 01/30/21 Pct Recovery = 95% Analysis Date = 01/26/21 Pct Recovery = 95% Analysis Date = 01/26/21 Pct Recovery = 95% Analysis Date = 01/22/21 Pct Recovery = 95% Analysis Date = 01/22/21 Pct Recovery = 95% Analysis Date = 01/18/21 Pct Recovery = 95% Analysis Date = 01/18/21 Pct Recovery = 95% Analysis Date = 01/14/21 Pct Recovery = 95% Analysis Date = 01/14/21 Pct Recovery = 95% Analysis Date = 01/10/21 Pct Recovery = 96% Analysis Date = 01/10/21 Pct Recovery = 96% Analysis Date = 01/06/21 Pct Recovery = 96% Analysis Date = 01/06/21 Pct Recovery = 96% Analysis Date = 01/02/21 Pct Recovery = 96% Analysis Date = 01/02/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/12/20 Pct Recovery = 97% Analysis Date = 12/12/20 Pct Recovery = 97% Analysis Date = 12/08/20 Pct Recovery = 97% Analysis Date = 12/08/20 Pct Recovery = 97% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 97% Analysis Date = 11/26/20 Pct Recovery = 97% Analysis Date = 11/26/20 Pct Recovery = 97% Analysis Date = 11/22/20 Pct Recovery = 97% Analysis Date = 11/22/20 Pct Recovery = 97% Analysis Date = 11/18/20 Pct Recovery = 97% Analysis Date = 11/18/20 Pct Recovery = 97% Analysis Date = 11/14/20 Pct Recovery = 97% Analysis Date = 11/14/20 Pct Recovery = 97% Analysis Date = 11/10/20 Pct Recovery = 97% Analysis Date = 11/10/20 Pct Recovery = 97% Analysis Date = 11/06/20 Pct Recovery = 97% Analysis Date = 11/06/20 Pct Recovery = 97% Analysis Date = 11/02/20 Pct Recovery = 97% Analysis Date = 11/02/20 Pct Recovery = 97% Analysis Date = 10/29/20 Pct Recovery = 97% Analysis Date = 10/29/20 Pct Recovery = 97% Analysis Date = 10/25/20 Pct Recovery = 97% Analysis Date = 10/25/20 Pct Recovery = 97% Analysis Date = 10/21/20 Pct Recovery = 97% Analysis Date = 10/21/20 Pct Recovery = 97% Analysis Date = 10/17/20 Pct Recovery = 97% Analysis Date = 10/17/20 Pct Recovery = 97% Analysis Date = 10/13/20 Pct Recovery = 97% Analysis Date = 10/13/20 Pct Recovery = 97% Analysis Date = 10/09/20 Pct Recovery = 98% Analysis Date = 10/09/20 Pct Recovery = 98% Analysis Date = 10/05/20 Pct Recovery = 98% Analysis Date = 10/05/20 Pct Recovery = 98% Analysis Date = 10/01/20 Pct Recovery = 98% Analysis Date = 10/01/20 Pct Recovery = 98% Analysis Date = 09/27/20 Pct Recovery = 98% Analysis Date = 09/27/20 Pct Recovery = 98% Analysis Date = 09/23/20 Pct Recovery = 98% Analysis Date = 09/23/20 Pct Recovery = 98% Analysis Date = 09/19/20 Pct Recovery = 98% Analysis Date = 09/19/20 Pct Recovery = 98% Analysis Date = 09/15/20 Pct Recovery = 99% Analysis Date = 09/15/20 Pct Recovery = 99% Analysis Date = 09/11/20 Pct Recovery = 99% Analysis Date = 09/11/20 Pct Recovery = 99% Analysis Date = 09/07/20 Pct Recovery = 99% Analysis Date = 09/07/20 Pct Recovery = 99% Analysis Date = 09/02/20 Pct Recovery = 99% Analysis Date = 09/02/20 Pct Recovery = 99% Analysis Date = 08/29/20 Pct Recovery = 99% Analysis Date = 08/29/20 Pct Recovery = 99% Analysis Date = 08/25/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 100% Analysis Date = 08/21/20 Pct Recovery = 100% Analysis Date = 08/21/20 Pct Recovery = 100% Analysis Date = 08/17/20 Pct Recovery = 101% Analysis Date = 08/17/20 Pct Recovery = 101% Analysis Date = 08/13/20 Pct Recovery = 101% Analysis Date = 08/13/20 Pct Recovery = 101% Analysis Date = 08/09/20 Pct Recovery = 102% Analysis Date = 08/09/20 Pct Recovery = 102% Analysis Date = 08/05/20 Pct Recovery = 102% Analysis Date = 08/05/20 Pct Recovery = 102% Analysis Date = 08/01/20 Pct Recovery = 103% Analysis Date = 08/01/20 Pct Recovery = 103% Analysis Date = 07/28/20 Pct Recovery = 103% Analysis Date = 07/28/20 Pct Recovery = 103% Analysis Date = 07/24/20 Pct Recovery = 104% Analysis Date = 07/24/20 Pct Recovery = 104% Analysis Date = 07/20/20 Pct Recovery = 104% Analysis Date = 07/20/20 Pct Recovery = 104% Analysis Date = 07/16/20 Pct Recovery = 104% Analysis Date = 07/16/20 Pct Recovery = 104% Analysis Date = 07/12/20 Pct Recovery = 105% Analysis Date = 07/12/20 Pct Recovery = 105% Analysis Date = 07/08/20 Pct Recovery = 105% Analysis Date = 07/08/20 Pct Recovery = 105% Analysis Date = 07/04/20 Pct Recovery = 106% Analysis Date = 07/04/20 Pct Recovery = 106% Analysis Date = 06/30/20 Pct Recovery = 107% Analysis Date = 06/30/20 Pct Recovery = 107% Analysis Date = 06/26/20 Pct Recovery = 107% Analysis Date = 06/26/20 Pct Recovery = 107% Analysis Date = 06/22/20 Pct Recovery = 108% Analysis Date = 06/22/20 Pct Recovery = 108% Analysis Date = 06/18/20 Pct Recovery = 108% Analysis Date = 06/18/20 Pct Recovery = 108% Analysis Date = 06/14/20 Pct Recovery = 109% Analysis Date = 06/14/20 Pct Recovery = 109% Analysis Date = 06/10/20 Pct Recovery = 109% Analysis Date = 06/10/20 Pct Recovery = 109% Analysis Date = 06/06/20 Pct Recovery = 110% Analysis Date = 06/06/20 Pct Recovery = 110% Analysis Date = 06/02/20 Pct Recovery = 111% Analysis Date = 06/02/20 Pct Recovery = 111% Analysis Date = 05/29/20 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
LINURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 94% 20% 93% 23%
Total 34 94% 20% 93% 23%

Sample Statistics
LINURON

Characteristic N % % Basis
Plotted 34 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 82 .  
False Positives 1 1% 1 out of 82

OBSP Determination:
MALATHION
METHOD: 2447 , TESTIDCODE: 65087LCM60

Laboratory ID = 20213200091 Lab Value = 80.625 Expected Conc. = 34.1 Report level label = 5.4 Pct Recovery = 236% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20203230021 Lab Value = 58.525 Expected Conc. = 67.9 Report level label = 5.4 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 53.596 Expected Conc. = 67.9 Report level label = 5.4 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 58.666 Expected Conc. = 67 Report level label = 5.4 Pct Recovery = 88% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 73.500 Expected Conc. = 67 Report level label = 5.4 Pct Recovery = 110% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222150193 Lab Value = 32.367 Expected Conc. = 54.8 Report level label = 5.4 Pct Recovery = 59% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20212990174 Lab Value = 26.178 Expected Conc. = 54.56 Report level label = 5.4 Pct Recovery = 48% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 27.884 Expected Conc. = 54.24 Report level label = 5.4 Pct Recovery = 51% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 32.578 Expected Conc. = 54.24 Report level label = 5.4 Pct Recovery = 60% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222010132 Lab Value = 28.676 Expected Conc. = 54 Report level label = 5.4 Pct Recovery = 53% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 40.175 Expected Conc. = 53.2 Report level label = 5.4 Pct Recovery = 76% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20201550031 Lab Value = 33.222 Expected Conc. = 34.2 Report level label = 5.4 Pct Recovery = 97% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20213340027 Lab Value = 22.443 Expected Conc. = 34.1 Report level label = 5.4 Pct Recovery = 66% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 19.364 Expected Conc. = 34.1 Report level label = 5.4 Pct Recovery = 57% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 20.348 Expected Conc. = 33.9 Report level label = 5.4 Pct Recovery = 60% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 20.372 Expected Conc. = 33.9 Report level label = 5.4 Pct Recovery = 60% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202390020 Lab Value = 45.074 Expected Conc. = 33.65 Report level label = 5.4 Pct Recovery = 134% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 39.686 Expected Conc. = 33.65 Report level label = 5.4 Pct Recovery = 118% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20203230018 Lab Value = 25.558 Expected Conc. = 33.5 Report level label = 5.4 Pct Recovery = 76% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 27.331 Expected Conc. = 33.5 Report level label = 5.4 Pct Recovery = 82% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 36.141 Expected Conc. = 33.5 Report level label = 5.4 Pct Recovery = 108% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220810133 Lab Value = 21.706 Expected Conc. = 33.25 Report level label = 5.4 Pct Recovery = 65% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201960104 Lab Value = 33.184 Expected Conc. = 26.92 Report level label = 5.4 Pct Recovery = 123% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 22.777 Expected Conc. = 26.92 Report level label = 5.4 Pct Recovery = 85% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20202330309 Lab Value = 13.106 Expected Conc. = 13.68 Report level label = 5.4 Pct Recovery = 96% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 8.947 Expected Conc. = 13.68 Report level label = 5.4 Pct Recovery = 65% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 15.765 Expected Conc. = 13.68 Report level label = 5.4 Pct Recovery = 115% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 13.920 Expected Conc. = 13.68 Report level label = 5.4 Pct Recovery = 102% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 18.692 Expected Conc. = 13.68 Report level label = 5.4 Pct Recovery = 137% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210830019 Lab Value = 14.861 Expected Conc. = 13.58 Report level label = 5.4 Pct Recovery = 109% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 11.591 Expected Conc. = 13.58 Report level label = 5.4 Pct Recovery = 85% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222500483 Lab Value = 8.858 Expected Conc. = 13.56 Report level label = 5.4 Pct Recovery = 65% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 6.511 Expected Conc. = 13.56 Report level label = 5.4 Pct Recovery = 48% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210970035 Lab Value = 14.646 Expected Conc. = 13.4 Report level label = 5.4 Pct Recovery = 109% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 14.998 Expected Conc. = 13.4 Report level label = 5.4 Pct Recovery = 112% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 16.420 Expected Conc. = 13.4 Report level label = 5.4 Pct Recovery = 123% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 13.690 Expected Conc. = 13.4 Report level label = 5.4 Pct Recovery = 102% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 15.276 Expected Conc. = 13.4 Report level label = 5.4 Pct Recovery = 114% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 17.803 Expected Conc. = 13.4 Report level label = 5.4 Pct Recovery = 133% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222630205 Lab Value = 10.909 Expected Conc. = 13.3 Report level label = 5.4 Pct Recovery = 82% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Analysis Date = 09/28/22 Pct Recovery = 60% Analysis Date = 09/24/22 Pct Recovery = 60% Analysis Date = 09/24/22 Pct Recovery = 60% Analysis Date = 09/20/22 Pct Recovery = 60% Analysis Date = 09/20/22 Pct Recovery = 60% Analysis Date = 09/16/22 Pct Recovery = 60% Analysis Date = 09/16/22 Pct Recovery = 60% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 61% Analysis Date = 08/30/22 Pct Recovery = 62% Analysis Date = 08/30/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/17/22 Pct Recovery = 62% Analysis Date = 08/17/22 Pct Recovery = 62% Analysis Date = 08/13/22 Pct Recovery = 63% Analysis Date = 08/13/22 Pct Recovery = 63% Analysis Date = 08/08/22 Pct Recovery = 63% Analysis Date = 08/08/22 Pct Recovery = 63% Analysis Date = 08/04/22 Pct Recovery = 63% Analysis Date = 08/04/22 Pct Recovery = 63% Analysis Date = 07/31/22 Pct Recovery = 63% Analysis Date = 07/31/22 Pct Recovery = 63% Analysis Date = 07/27/22 Pct Recovery = 64% Analysis Date = 07/27/22 Pct Recovery = 64% Analysis Date = 07/22/22 Pct Recovery = 64% Analysis Date = 07/22/22 Pct Recovery = 64% Analysis Date = 07/18/22 Pct Recovery = 64% Analysis Date = 07/18/22 Pct Recovery = 64% Analysis Date = 07/14/22 Pct Recovery = 65% Analysis Date = 07/14/22 Pct Recovery = 65% Analysis Date = 07/09/22 Pct Recovery = 65% Analysis Date = 07/09/22 Pct Recovery = 65% Analysis Date = 07/05/22 Pct Recovery = 65% Analysis Date = 07/05/22 Pct Recovery = 65% Analysis Date = 07/01/22 Pct Recovery = 65% Analysis Date = 07/01/22 Pct Recovery = 65% Analysis Date = 06/27/22 Pct Recovery = 66% Analysis Date = 06/27/22 Pct Recovery = 66% Analysis Date = 06/22/22 Pct Recovery = 66% Analysis Date = 06/22/22 Pct Recovery = 66% Analysis Date = 06/18/22 Pct Recovery = 66% Analysis Date = 06/18/22 Pct Recovery = 66% Analysis Date = 06/14/22 Pct Recovery = 67% Analysis Date = 06/14/22 Pct Recovery = 67% Analysis Date = 06/10/22 Pct Recovery = 67% Analysis Date = 06/10/22 Pct Recovery = 67% Analysis Date = 06/05/22 Pct Recovery = 67% Analysis Date = 06/05/22 Pct Recovery = 67% Analysis Date = 06/01/22 Pct Recovery = 67% Analysis Date = 06/01/22 Pct Recovery = 67% Analysis Date = 05/28/22 Pct Recovery = 68% Analysis Date = 05/28/22 Pct Recovery = 68% Analysis Date = 05/24/22 Pct Recovery = 68% Analysis Date = 05/24/22 Pct Recovery = 68% Analysis Date = 05/19/22 Pct Recovery = 68% Analysis Date = 05/19/22 Pct Recovery = 68% Analysis Date = 05/15/22 Pct Recovery = 68% Analysis Date = 05/15/22 Pct Recovery = 68% Analysis Date = 05/11/22 Pct Recovery = 69% Analysis Date = 05/11/22 Pct Recovery = 69% Analysis Date = 05/06/22 Pct Recovery = 69% Analysis Date = 05/06/22 Pct Recovery = 69% Analysis Date = 05/02/22 Pct Recovery = 69% Analysis Date = 05/02/22 Pct Recovery = 69% Analysis Date = 04/28/22 Pct Recovery = 70% Analysis Date = 04/28/22 Pct Recovery = 70% Analysis Date = 04/24/22 Pct Recovery = 70% Analysis Date = 04/24/22 Pct Recovery = 70% Analysis Date = 04/19/22 Pct Recovery = 70% Analysis Date = 04/19/22 Pct Recovery = 70% Analysis Date = 04/15/22 Pct Recovery = 70% Analysis Date = 04/15/22 Pct Recovery = 70% Analysis Date = 04/11/22 Pct Recovery = 71% Analysis Date = 04/11/22 Pct Recovery = 71% Analysis Date = 04/07/22 Pct Recovery = 71% Analysis Date = 04/07/22 Pct Recovery = 71% Analysis Date = 04/02/22 Pct Recovery = 71% Analysis Date = 04/02/22 Pct Recovery = 71% Analysis Date = 03/29/22 Pct Recovery = 72% Analysis Date = 03/29/22 Pct Recovery = 72% Analysis Date = 03/25/22 Pct Recovery = 72% Analysis Date = 03/25/22 Pct Recovery = 72% Analysis Date = 03/21/22 Pct Recovery = 72% Analysis Date = 03/21/22 Pct Recovery = 72% Analysis Date = 03/16/22 Pct Recovery = 72% Analysis Date = 03/16/22 Pct Recovery = 72% Analysis Date = 03/12/22 Pct Recovery = 73% Analysis Date = 03/12/22 Pct Recovery = 73% Analysis Date = 03/08/22 Pct Recovery = 73% Analysis Date = 03/08/22 Pct Recovery = 73% Analysis Date = 03/04/22 Pct Recovery = 73% Analysis Date = 03/04/22 Pct Recovery = 73% Analysis Date = 02/27/22 Pct Recovery = 74% Analysis Date = 02/27/22 Pct Recovery = 74% Analysis Date = 02/23/22 Pct Recovery = 74% Analysis Date = 02/23/22 Pct Recovery = 74% Analysis Date = 02/19/22 Pct Recovery = 74% Analysis Date = 02/19/22 Pct Recovery = 74% Analysis Date = 02/14/22 Pct Recovery = 75% Analysis Date = 02/14/22 Pct Recovery = 75% Analysis Date = 02/10/22 Pct Recovery = 75% Analysis Date = 02/10/22 Pct Recovery = 75% Analysis Date = 02/06/22 Pct Recovery = 75% Analysis Date = 02/06/22 Pct Recovery = 75% Analysis Date = 02/02/22 Pct Recovery = 76% Analysis Date = 02/02/22 Pct Recovery = 76% Analysis Date = 01/28/22 Pct Recovery = 76% Analysis Date = 01/28/22 Pct Recovery = 76% Analysis Date = 01/24/22 Pct Recovery = 76% Analysis Date = 01/24/22 Pct Recovery = 76% Analysis Date = 01/20/22 Pct Recovery = 77% Analysis Date = 01/20/22 Pct Recovery = 77% Analysis Date = 01/16/22 Pct Recovery = 77% Analysis Date = 01/16/22 Pct Recovery = 77% Analysis Date = 01/11/22 Pct Recovery = 77% Analysis Date = 01/11/22 Pct Recovery = 77% Analysis Date = 01/07/22 Pct Recovery = 78% Analysis Date = 01/07/22 Pct Recovery = 78% Analysis Date = 01/03/22 Pct Recovery = 78% Analysis Date = 01/03/22 Pct Recovery = 78% Analysis Date = 12/30/21 Pct Recovery = 78% Analysis Date = 12/30/21 Pct Recovery = 78% Analysis Date = 12/25/21 Pct Recovery = 79% Analysis Date = 12/25/21 Pct Recovery = 79% Analysis Date = 12/21/21 Pct Recovery = 79% Analysis Date = 12/21/21 Pct Recovery = 79% Analysis Date = 12/17/21 Pct Recovery = 79% Analysis Date = 12/17/21 Pct Recovery = 79% Analysis Date = 12/12/21 Pct Recovery = 80% Analysis Date = 12/12/21 Pct Recovery = 80% Analysis Date = 12/08/21 Pct Recovery = 80% Analysis Date = 12/08/21 Pct Recovery = 80% Analysis Date = 12/04/21 Pct Recovery = 80% Analysis Date = 12/04/21 Pct Recovery = 80% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/25/21 Pct Recovery = 81% Analysis Date = 11/25/21 Pct Recovery = 81% Analysis Date = 11/21/21 Pct Recovery = 81% Analysis Date = 11/21/21 Pct Recovery = 81% Analysis Date = 11/17/21 Pct Recovery = 82% Analysis Date = 11/17/21 Pct Recovery = 82% Analysis Date = 11/13/21 Pct Recovery = 82% Analysis Date = 11/13/21 Pct Recovery = 82% Analysis Date = 11/08/21 Pct Recovery = 82% Analysis Date = 11/08/21 Pct Recovery = 82% Analysis Date = 11/04/21 Pct Recovery = 83% Analysis Date = 11/04/21 Pct Recovery = 83% Analysis Date = 10/31/21 Pct Recovery = 83% Analysis Date = 10/31/21 Pct Recovery = 83% Analysis Date = 10/27/21 Pct Recovery = 83% Analysis Date = 10/27/21 Pct Recovery = 83% Analysis Date = 10/22/21 Pct Recovery = 83% Analysis Date = 10/22/21 Pct Recovery = 83% Analysis Date = 10/18/21 Pct Recovery = 84% Analysis Date = 10/18/21 Pct Recovery = 84% Analysis Date = 10/14/21 Pct Recovery = 84% Analysis Date = 10/14/21 Pct Recovery = 84% Analysis Date = 10/10/21 Pct Recovery = 84% Analysis Date = 10/10/21 Pct Recovery = 84% Analysis Date = 10/05/21 Pct Recovery = 84% Analysis Date = 10/05/21 Pct Recovery = 84% Analysis Date = 10/01/21 Pct Recovery = 85% Analysis Date = 10/01/21 Pct Recovery = 85% Analysis Date = 09/27/21 Pct Recovery = 85% Analysis Date = 09/27/21 Pct Recovery = 85% Analysis Date = 09/22/21 Pct Recovery = 85% Analysis Date = 09/22/21 Pct Recovery = 85% Analysis Date = 09/18/21 Pct Recovery = 85% Analysis Date = 09/18/21 Pct Recovery = 85% Analysis Date = 09/14/21 Pct Recovery = 86% Analysis Date = 09/14/21 Pct Recovery = 86% Analysis Date = 09/10/21 Pct Recovery = 86% Analysis Date = 09/10/21 Pct Recovery = 86% Analysis Date = 09/05/21 Pct Recovery = 86% Analysis Date = 09/05/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 87% Analysis Date = 08/28/21 Pct Recovery = 87% Analysis Date = 08/24/21 Pct Recovery = 87% Analysis Date = 08/24/21 Pct Recovery = 87% Analysis Date = 08/19/21 Pct Recovery = 87% Analysis Date = 08/19/21 Pct Recovery = 87% Analysis Date = 08/15/21 Pct Recovery = 87% Analysis Date = 08/15/21 Pct Recovery = 87% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/11/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 88% Analysis Date = 08/07/21 Pct Recovery = 88% Analysis Date = 08/02/21 Pct Recovery = 88% Analysis Date = 08/02/21 Pct Recovery = 88% Analysis Date = 07/29/21 Pct Recovery = 89% Analysis Date = 07/29/21 Pct Recovery = 89% Analysis Date = 07/25/21 Pct Recovery = 89% Analysis Date = 07/25/21 Pct Recovery = 89% Analysis Date = 07/20/21 Pct Recovery = 89% Analysis Date = 07/20/21 Pct Recovery = 89% Analysis Date = 07/16/21 Pct Recovery = 89% Analysis Date = 07/16/21 Pct Recovery = 89% Analysis Date = 07/12/21 Pct Recovery = 90% Analysis Date = 07/12/21 Pct Recovery = 90% Analysis Date = 07/08/21 Pct Recovery = 90% Analysis Date = 07/08/21 Pct Recovery = 90% Analysis Date = 07/03/21 Pct Recovery = 90% Analysis Date = 07/03/21 Pct Recovery = 90% Analysis Date = 06/29/21 Pct Recovery = 90% Analysis Date = 06/29/21 Pct Recovery = 90% Analysis Date = 06/25/21 Pct Recovery = 91% Analysis Date = 06/25/21 Pct Recovery = 91% Analysis Date = 06/21/21 Pct Recovery = 91% Analysis Date = 06/21/21 Pct Recovery = 91% Analysis Date = 06/16/21 Pct Recovery = 91% Analysis Date = 06/16/21 Pct Recovery = 91% Analysis Date = 06/12/21 Pct Recovery = 91% Analysis Date = 06/12/21 Pct Recovery = 91% Analysis Date = 06/08/21 Pct Recovery = 92% Analysis Date = 06/08/21 Pct Recovery = 92% Analysis Date = 06/04/21 Pct Recovery = 92% Analysis Date = 06/04/21 Pct Recovery = 92% Analysis Date = 05/30/21 Pct Recovery = 92% Analysis Date = 05/30/21 Pct Recovery = 92% Analysis Date = 05/26/21 Pct Recovery = 92% Analysis Date = 05/26/21 Pct Recovery = 92% Analysis Date = 05/22/21 Pct Recovery = 93% Analysis Date = 05/22/21 Pct Recovery = 93% Analysis Date = 05/17/21 Pct Recovery = 93% Analysis Date = 05/17/21 Pct Recovery = 93% Analysis Date = 05/13/21 Pct Recovery = 93% Analysis Date = 05/13/21 Pct Recovery = 93% Analysis Date = 05/09/21 Pct Recovery = 93% Analysis Date = 05/09/21 Pct Recovery = 93% Analysis Date = 05/05/21 Pct Recovery = 94% Analysis Date = 05/05/21 Pct Recovery = 94% Analysis Date = 04/30/21 Pct Recovery = 94% Analysis Date = 04/30/21 Pct Recovery = 94% Analysis Date = 04/26/21 Pct Recovery = 94% Analysis Date = 04/26/21 Pct Recovery = 94% Analysis Date = 04/22/21 Pct Recovery = 94% Analysis Date = 04/22/21 Pct Recovery = 94% Analysis Date = 04/18/21 Pct Recovery = 95% Analysis Date = 04/18/21 Pct Recovery = 95% Analysis Date = 04/13/21 Pct Recovery = 95% Analysis Date = 04/13/21 Pct Recovery = 95% Analysis Date = 04/09/21 Pct Recovery = 95% Analysis Date = 04/09/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/01/21 Pct Recovery = 96% Analysis Date = 04/01/21 Pct Recovery = 96% Analysis Date = 03/27/21 Pct Recovery = 96% Analysis Date = 03/27/21 Pct Recovery = 96% Analysis Date = 03/23/21 Pct Recovery = 96% Analysis Date = 03/23/21 Pct Recovery = 96% Analysis Date = 03/19/21 Pct Recovery = 96% Analysis Date = 03/19/21 Pct Recovery = 96% Analysis Date = 03/15/21 Pct Recovery = 96% Analysis Date = 03/15/21 Pct Recovery = 96% Analysis Date = 03/10/21 Pct Recovery = 97% Analysis Date = 03/10/21 Pct Recovery = 97% Analysis Date = 03/06/21 Pct Recovery = 97% Analysis Date = 03/06/21 Pct Recovery = 97% Analysis Date = 03/02/21 Pct Recovery = 97% Analysis Date = 03/02/21 Pct Recovery = 97% Analysis Date = 02/25/21 Pct Recovery = 97% Analysis Date = 02/25/21 Pct Recovery = 97% Analysis Date = 02/21/21 Pct Recovery = 97% Analysis Date = 02/21/21 Pct Recovery = 97% Analysis Date = 02/17/21 Pct Recovery = 98% Analysis Date = 02/17/21 Pct Recovery = 98% Analysis Date = 02/13/21 Pct Recovery = 98% Analysis Date = 02/13/21 Pct Recovery = 98% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/04/21 Pct Recovery = 98% Analysis Date = 02/04/21 Pct Recovery = 98% Analysis Date = 01/31/21 Pct Recovery = 98% Analysis Date = 01/31/21 Pct Recovery = 98% Analysis Date = 01/27/21 Pct Recovery = 99% Analysis Date = 01/27/21 Pct Recovery = 99% Analysis Date = 01/22/21 Pct Recovery = 99% Analysis Date = 01/22/21 Pct Recovery = 99% Analysis Date = 01/18/21 Pct Recovery = 99% Analysis Date = 01/18/21 Pct Recovery = 99% Analysis Date = 01/14/21 Pct Recovery = 99% Analysis Date = 01/14/21 Pct Recovery = 99% Analysis Date = 01/10/21 Pct Recovery = 99% Analysis Date = 01/10/21 Pct Recovery = 99% Analysis Date = 01/05/21 Pct Recovery = 100% Analysis Date = 01/05/21 Pct Recovery = 100% Analysis Date = 01/01/21 Pct Recovery = 100% Analysis Date = 01/01/21 Pct Recovery = 100% Analysis Date = 12/28/20 Pct Recovery = 100% Analysis Date = 12/28/20 Pct Recovery = 100% Analysis Date = 12/23/20 Pct Recovery = 100% Analysis Date = 12/23/20 Pct Recovery = 100% Analysis Date = 12/19/20 Pct Recovery = 100% Analysis Date = 12/19/20 Pct Recovery = 100% Analysis Date = 12/15/20 Pct Recovery = 100% Analysis Date = 12/15/20 Pct Recovery = 100% Analysis Date = 12/11/20 Pct Recovery = 101% Analysis Date = 12/11/20 Pct Recovery = 101% Analysis Date = 12/06/20 Pct Recovery = 101% Analysis Date = 12/06/20 Pct Recovery = 101% Analysis Date = 12/02/20 Pct Recovery = 101% Analysis Date = 12/02/20 Pct Recovery = 101% Analysis Date = 11/28/20 Pct Recovery = 101% Analysis Date = 11/28/20 Pct Recovery = 101% Analysis Date = 11/24/20 Pct Recovery = 102% Analysis Date = 11/24/20 Pct Recovery = 102% Analysis Date = 11/19/20 Pct Recovery = 102% Analysis Date = 11/19/20 Pct Recovery = 102% Analysis Date = 11/15/20 Pct Recovery = 102% Analysis Date = 11/15/20 Pct Recovery = 102% Analysis Date = 11/11/20 Pct Recovery = 102% Analysis Date = 11/11/20 Pct Recovery = 102% Analysis Date = 11/07/20 Pct Recovery = 103% Analysis Date = 11/07/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 104% Analysis Date = 10/21/20 Pct Recovery = 104% Analysis Date = 10/16/20 Pct Recovery = 104% Analysis Date = 10/16/20 Pct Recovery = 104% Analysis Date = 10/12/20 Pct Recovery = 104% Analysis Date = 10/12/20 Pct Recovery = 104% Analysis Date = 10/08/20 Pct Recovery = 104% Analysis Date = 10/08/20 Pct Recovery = 104% Analysis Date = 10/03/20 Pct Recovery = 105% Analysis Date = 10/03/20 Pct Recovery = 105% Analysis Date = 09/29/20 Pct Recovery = 105% Analysis Date = 09/29/20 Pct Recovery = 105% Analysis Date = 09/25/20 Pct Recovery = 105% Analysis Date = 09/25/20 Pct Recovery = 105% Analysis Date = 09/21/20 Pct Recovery = 105% Analysis Date = 09/21/20 Pct Recovery = 105% Analysis Date = 09/16/20 Pct Recovery = 106% Analysis Date = 09/16/20 Pct Recovery = 106% Analysis Date = 09/12/20 Pct Recovery = 106% Analysis Date = 09/12/20 Pct Recovery = 106% Analysis Date = 09/08/20 Pct Recovery = 106% Analysis Date = 09/08/20 Pct Recovery = 106% Analysis Date = 09/04/20 Pct Recovery = 106% Analysis Date = 09/04/20 Pct Recovery = 106% Analysis Date = 08/30/20 Pct Recovery = 106% Analysis Date = 08/30/20 Pct Recovery = 106% Analysis Date = 08/26/20 Pct Recovery = 107% Analysis Date = 08/26/20 Pct Recovery = 107% Analysis Date = 08/22/20 Pct Recovery = 107% Analysis Date = 08/22/20 Pct Recovery = 107% Analysis Date = 08/18/20 Pct Recovery = 107% Analysis Date = 08/18/20 Pct Recovery = 107% Analysis Date = 08/13/20 Pct Recovery = 107% Analysis Date = 08/13/20 Pct Recovery = 107% Analysis Date = 08/09/20 Pct Recovery = 107% Analysis Date = 08/09/20 Pct Recovery = 107% Analysis Date = 08/05/20 Pct Recovery = 107% Analysis Date = 08/05/20 Pct Recovery = 107% Analysis Date = 07/31/20 Pct Recovery = 108% Analysis Date = 07/31/20 Pct Recovery = 108% Analysis Date = 07/27/20 Pct Recovery = 108% Analysis Date = 07/27/20 Pct Recovery = 108% Analysis Date = 07/23/20 Pct Recovery = 108% Analysis Date = 07/23/20 Pct Recovery = 108% Analysis Date = 07/19/20 Pct Recovery = 108% Analysis Date = 07/19/20 Pct Recovery = 108% Analysis Date = 07/14/20 Pct Recovery = 108% Analysis Date = 07/14/20 Pct Recovery = 108% Analysis Date = 07/10/20 Pct Recovery = 108% Analysis Date = 07/10/20 Pct Recovery = 108% Analysis Date = 07/06/20 Pct Recovery = 109% Analysis Date = 07/06/20 Pct Recovery = 109% Analysis Date = 07/02/20 Pct Recovery = 109% Analysis Date = 07/02/20 Pct Recovery = 109% Analysis Date = 06/27/20 Pct Recovery = 109% Analysis Date = 06/27/20 Pct Recovery = 109% Analysis Date = 06/23/20 Pct Recovery = 109% Analysis Date = 06/23/20 Pct Recovery = 109% Analysis Date = 06/19/20 Pct Recovery = 109% Analysis Date = 06/19/20 Pct Recovery = 109% Analysis Date = 06/15/20 Pct Recovery = 109% Analysis Date = 06/15/20 Pct Recovery = 109% Analysis Date = 06/10/20 Pct Recovery = 109% Analysis Date = 06/10/20 Pct Recovery = 109% Analysis Date = 06/06/20 Pct Recovery = 109% Analysis Date = 06/06/20 Pct Recovery = 109% Analysis Date = 06/02/20 Pct Recovery = 110% Analysis Date = 06/02/20 Pct Recovery = 110% Analysis Date = 05/29/20 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALATHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 92% 35% 86% 34%
Total 40 92% 35% 86% 34%

Sample Statistics
MALATHION

Characteristic N % % Basis
Plotted 40 98% Spiked
Estimated Values 5 12% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

OBSP Determination:
METALAXYL
METHOD: 2447 , TESTIDCODE: 68437LCM60

Laboratory ID = 20202590106 Lab Value = 87.586 Expected Conc. = 75.1 Report level label = 6 Pct Recovery = 117% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 90.429 Expected Conc. = 75.1 Report level label = 6 Pct Recovery = 120% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 70.853 Expected Conc. = 74.14 Report level label = 6 Pct Recovery = 96% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 72.257 Expected Conc. = 74.14 Report level label = 6 Pct Recovery = 97% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222150192 Lab Value = 48.902 Expected Conc. = 60 Report level label = 6 Pct Recovery = 82% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 41.951 Expected Conc. = 60 Report level label = 6 Pct Recovery = 70% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221520237 Lab Value = 64.132 Expected Conc. = 59.32 Report level label = 6 Pct Recovery = 108% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20201550031 Lab Value = 34.052 Expected Conc. = 37.85 Report level label = 6 Pct Recovery = 90% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20203230018 Lab Value = 29.285 Expected Conc. = 37.55 Report level label = 6 Pct Recovery = 78% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 28.351 Expected Conc. = 37.55 Report level label = 6 Pct Recovery = 76% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 36.843 Expected Conc. = 37.55 Report level label = 6 Pct Recovery = 98% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20220740064 Lab Value = 26.827 Expected Conc. = 37.5 Report level label = 6 Pct Recovery = 72% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202390020 Lab Value = 42.790 Expected Conc. = 37.5 Report level label = 6 Pct Recovery = 114% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 35.844 Expected Conc. = 37.5 Report level label = 6 Pct Recovery = 96% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20221870197 Lab Value = 27.914 Expected Conc. = 37.075 Report level label = 6 Pct Recovery = 75% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20201960104 Lab Value = 40.561 Expected Conc. = 30 Report level label = 6 Pct Recovery = 135% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 30.633 Expected Conc. = 30 Report level label = 6 Pct Recovery = 102% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20202330309 Lab Value = 14.277 Expected Conc. = 15.14 Report level label = 6 Pct Recovery = 94% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 11.211 Expected Conc. = 15.14 Report level label = 6 Pct Recovery = 74% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 15.589 Expected Conc. = 15.14 Report level label = 6 Pct Recovery = 103% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 13.559 Expected Conc. = 15.14 Report level label = 6 Pct Recovery = 90% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 15.470 Expected Conc. = 15.14 Report level label = 6 Pct Recovery = 102% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210970035 Lab Value = 12.583 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 84% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 13.457 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 90% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 15.721 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 105% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 16.447 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 110% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 15.617 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 104% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 14.549 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 97% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221660151 Lab Value = 12.432 Expected Conc. = 14.83 Report level label = 6 Pct Recovery = 84% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210830019 Lab Value = 9.579 Expected Conc. = 14.828 Report level label = 6 Pct Recovery = 65% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 11.933 Expected Conc. = 14.828 Report level label = 6 Pct Recovery = 80% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 08/15/22 Pct Recovery = 82% Analysis Date = 08/10/22 Pct Recovery = 82% Analysis Date = 08/10/22 Pct Recovery = 82% Analysis Date = 08/06/22 Pct Recovery = 82% Analysis Date = 08/06/22 Pct Recovery = 82% Analysis Date = 08/02/22 Pct Recovery = 82% Analysis Date = 08/02/22 Pct Recovery = 82% Analysis Date = 07/29/22 Pct Recovery = 82% Analysis Date = 07/29/22 Pct Recovery = 82% Analysis Date = 07/25/22 Pct Recovery = 82% Analysis Date = 07/25/22 Pct Recovery = 82% Analysis Date = 07/21/22 Pct Recovery = 82% Analysis Date = 07/21/22 Pct Recovery = 82% Analysis Date = 07/17/22 Pct Recovery = 82% Analysis Date = 07/17/22 Pct Recovery = 82% Analysis Date = 07/13/22 Pct Recovery = 82% Analysis Date = 07/13/22 Pct Recovery = 82% Analysis Date = 07/09/22 Pct Recovery = 82% Analysis Date = 07/09/22 Pct Recovery = 82% Analysis Date = 07/05/22 Pct Recovery = 82% Analysis Date = 07/05/22 Pct Recovery = 82% Analysis Date = 07/01/22 Pct Recovery = 82% Analysis Date = 07/01/22 Pct Recovery = 82% Analysis Date = 06/27/22 Pct Recovery = 82% Analysis Date = 06/27/22 Pct Recovery = 82% Analysis Date = 06/23/22 Pct Recovery = 82% Analysis Date = 06/23/22 Pct Recovery = 82% Analysis Date = 06/19/22 Pct Recovery = 82% Analysis Date = 06/19/22 Pct Recovery = 82% Analysis Date = 06/15/22 Pct Recovery = 82% Analysis Date = 06/15/22 Pct Recovery = 82% Analysis Date = 06/11/22 Pct Recovery = 82% Analysis Date = 06/11/22 Pct Recovery = 82% Analysis Date = 06/07/22 Pct Recovery = 82% Analysis Date = 06/07/22 Pct Recovery = 82% Analysis Date = 06/03/22 Pct Recovery = 82% Analysis Date = 06/03/22 Pct Recovery = 82% Analysis Date = 05/30/22 Pct Recovery = 82% Analysis Date = 05/30/22 Pct Recovery = 82% Analysis Date = 05/26/22 Pct Recovery = 82% Analysis Date = 05/26/22 Pct Recovery = 82% Analysis Date = 05/22/22 Pct Recovery = 82% Analysis Date = 05/22/22 Pct Recovery = 82% Analysis Date = 05/18/22 Pct Recovery = 82% Analysis Date = 05/18/22 Pct Recovery = 82% Analysis Date = 05/14/22 Pct Recovery = 82% Analysis Date = 05/14/22 Pct Recovery = 82% Analysis Date = 05/10/22 Pct Recovery = 82% Analysis Date = 05/10/22 Pct Recovery = 82% Analysis Date = 05/06/22 Pct Recovery = 82% Analysis Date = 05/06/22 Pct Recovery = 82% Analysis Date = 05/01/22 Pct Recovery = 82% Analysis Date = 05/01/22 Pct Recovery = 82% Analysis Date = 04/27/22 Pct Recovery = 82% Analysis Date = 04/27/22 Pct Recovery = 82% Analysis Date = 04/23/22 Pct Recovery = 82% Analysis Date = 04/23/22 Pct Recovery = 82% Analysis Date = 04/19/22 Pct Recovery = 82% Analysis Date = 04/19/22 Pct Recovery = 82% Analysis Date = 04/15/22 Pct Recovery = 82% Analysis Date = 04/15/22 Pct Recovery = 82% Analysis Date = 04/11/22 Pct Recovery = 82% Analysis Date = 04/11/22 Pct Recovery = 82% Analysis Date = 04/07/22 Pct Recovery = 82% Analysis Date = 04/07/22 Pct Recovery = 82% Analysis Date = 04/03/22 Pct Recovery = 82% Analysis Date = 04/03/22 Pct Recovery = 82% Analysis Date = 03/30/22 Pct Recovery = 82% Analysis Date = 03/30/22 Pct Recovery = 82% Analysis Date = 03/26/22 Pct Recovery = 82% Analysis Date = 03/26/22 Pct Recovery = 82% Analysis Date = 03/22/22 Pct Recovery = 82% Analysis Date = 03/22/22 Pct Recovery = 82% Analysis Date = 03/18/22 Pct Recovery = 82% Analysis Date = 03/18/22 Pct Recovery = 82% Analysis Date = 03/14/22 Pct Recovery = 82% Analysis Date = 03/14/22 Pct Recovery = 82% Analysis Date = 03/10/22 Pct Recovery = 81% Analysis Date = 03/10/22 Pct Recovery = 81% Analysis Date = 03/06/22 Pct Recovery = 81% Analysis Date = 03/06/22 Pct Recovery = 81% Analysis Date = 03/02/22 Pct Recovery = 81% Analysis Date = 03/02/22 Pct Recovery = 81% Analysis Date = 02/26/22 Pct Recovery = 81% Analysis Date = 02/26/22 Pct Recovery = 81% Analysis Date = 02/22/22 Pct Recovery = 81% Analysis Date = 02/22/22 Pct Recovery = 81% Analysis Date = 02/18/22 Pct Recovery = 81% Analysis Date = 02/18/22 Pct Recovery = 81% Analysis Date = 02/14/22 Pct Recovery = 81% Analysis Date = 02/14/22 Pct Recovery = 81% Analysis Date = 02/10/22 Pct Recovery = 81% Analysis Date = 02/10/22 Pct Recovery = 81% Analysis Date = 02/06/22 Pct Recovery = 81% Analysis Date = 02/06/22 Pct Recovery = 81% Analysis Date = 02/02/22 Pct Recovery = 81% Analysis Date = 02/02/22 Pct Recovery = 81% Analysis Date = 01/29/22 Pct Recovery = 81% Analysis Date = 01/29/22 Pct Recovery = 81% Analysis Date = 01/25/22 Pct Recovery = 81% Analysis Date = 01/25/22 Pct Recovery = 81% Analysis Date = 01/20/22 Pct Recovery = 81% Analysis Date = 01/20/22 Pct Recovery = 81% Analysis Date = 01/16/22 Pct Recovery = 81% Analysis Date = 01/16/22 Pct Recovery = 81% Analysis Date = 01/12/22 Pct Recovery = 81% Analysis Date = 01/12/22 Pct Recovery = 81% Analysis Date = 01/08/22 Pct Recovery = 81% Analysis Date = 01/08/22 Pct Recovery = 81% Analysis Date = 01/04/22 Pct Recovery = 81% Analysis Date = 01/04/22 Pct Recovery = 81% Analysis Date = 12/31/21 Pct Recovery = 81% Analysis Date = 12/31/21 Pct Recovery = 81% Analysis Date = 12/27/21 Pct Recovery = 81% Analysis Date = 12/27/21 Pct Recovery = 81% Analysis Date = 12/23/21 Pct Recovery = 81% Analysis Date = 12/23/21 Pct Recovery = 81% Analysis Date = 12/19/21 Pct Recovery = 80% Analysis Date = 12/19/21 Pct Recovery = 80% Analysis Date = 12/15/21 Pct Recovery = 80% Analysis Date = 12/15/21 Pct Recovery = 80% Analysis Date = 12/11/21 Pct Recovery = 80% Analysis Date = 12/11/21 Pct Recovery = 80% Analysis Date = 12/07/21 Pct Recovery = 80% Analysis Date = 12/07/21 Pct Recovery = 80% Analysis Date = 12/03/21 Pct Recovery = 80% Analysis Date = 12/03/21 Pct Recovery = 80% Analysis Date = 11/29/21 Pct Recovery = 80% Analysis Date = 11/29/21 Pct Recovery = 80% Analysis Date = 11/25/21 Pct Recovery = 80% Analysis Date = 11/25/21 Pct Recovery = 80% Analysis Date = 11/21/21 Pct Recovery = 80% Analysis Date = 11/21/21 Pct Recovery = 80% Analysis Date = 11/17/21 Pct Recovery = 80% Analysis Date = 11/17/21 Pct Recovery = 80% Analysis Date = 11/13/21 Pct Recovery = 80% Analysis Date = 11/13/21 Pct Recovery = 80% Analysis Date = 11/09/21 Pct Recovery = 80% Analysis Date = 11/09/21 Pct Recovery = 80% Analysis Date = 11/05/21 Pct Recovery = 80% Analysis Date = 11/05/21 Pct Recovery = 80% Analysis Date = 11/01/21 Pct Recovery = 80% Analysis Date = 11/01/21 Pct Recovery = 80% Analysis Date = 10/28/21 Pct Recovery = 80% Analysis Date = 10/28/21 Pct Recovery = 80% Analysis Date = 10/24/21 Pct Recovery = 80% Analysis Date = 10/24/21 Pct Recovery = 80% Analysis Date = 10/20/21 Pct Recovery = 80% Analysis Date = 10/20/21 Pct Recovery = 80% Analysis Date = 10/16/21 Pct Recovery = 80% Analysis Date = 10/16/21 Pct Recovery = 80% Analysis Date = 10/11/21 Pct Recovery = 80% Analysis Date = 10/11/21 Pct Recovery = 80% Analysis Date = 10/07/21 Pct Recovery = 80% Analysis Date = 10/07/21 Pct Recovery = 80% Analysis Date = 10/03/21 Pct Recovery = 80% Analysis Date = 10/03/21 Pct Recovery = 80% Analysis Date = 09/29/21 Pct Recovery = 80% Analysis Date = 09/29/21 Pct Recovery = 80% Analysis Date = 09/25/21 Pct Recovery = 79% Analysis Date = 09/25/21 Pct Recovery = 79% Analysis Date = 09/21/21 Pct Recovery = 79% Analysis Date = 09/21/21 Pct Recovery = 79% Analysis Date = 09/17/21 Pct Recovery = 79% Analysis Date = 09/17/21 Pct Recovery = 79% Analysis Date = 09/13/21 Pct Recovery = 79% Analysis Date = 09/13/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 79% Analysis Date = 08/24/21 Pct Recovery = 79% Analysis Date = 08/24/21 Pct Recovery = 79% Analysis Date = 08/20/21 Pct Recovery = 79% Analysis Date = 08/20/21 Pct Recovery = 79% Analysis Date = 08/16/21 Pct Recovery = 79% Analysis Date = 08/16/21 Pct Recovery = 79% Analysis Date = 08/12/21 Pct Recovery = 79% Analysis Date = 08/12/21 Pct Recovery = 79% Analysis Date = 08/08/21 Pct Recovery = 79% Analysis Date = 08/08/21 Pct Recovery = 79% Analysis Date = 08/04/21 Pct Recovery = 79% Analysis Date = 08/04/21 Pct Recovery = 79% Analysis Date = 07/31/21 Pct Recovery = 79% Analysis Date = 07/31/21 Pct Recovery = 79% Analysis Date = 07/27/21 Pct Recovery = 79% Analysis Date = 07/27/21 Pct Recovery = 79% Analysis Date = 07/23/21 Pct Recovery = 79% Analysis Date = 07/23/21 Pct Recovery = 79% Analysis Date = 07/19/21 Pct Recovery = 79% Analysis Date = 07/19/21 Pct Recovery = 79% Analysis Date = 07/15/21 Pct Recovery = 79% Analysis Date = 07/15/21 Pct Recovery = 79% Analysis Date = 07/11/21 Pct Recovery = 79% Analysis Date = 07/11/21 Pct Recovery = 79% Analysis Date = 07/07/21 Pct Recovery = 78% Analysis Date = 07/07/21 Pct Recovery = 78% Analysis Date = 07/02/21 Pct Recovery = 78% Analysis Date = 07/02/21 Pct Recovery = 78% Analysis Date = 06/28/21 Pct Recovery = 78% Analysis Date = 06/28/21 Pct Recovery = 78% Analysis Date = 06/24/21 Pct Recovery = 78% Analysis Date = 06/24/21 Pct Recovery = 78% Analysis Date = 06/20/21 Pct Recovery = 78% Analysis Date = 06/20/21 Pct Recovery = 78% Analysis Date = 06/16/21 Pct Recovery = 78% Analysis Date = 06/16/21 Pct Recovery = 78% Analysis Date = 06/12/21 Pct Recovery = 78% Analysis Date = 06/12/21 Pct Recovery = 78% Analysis Date = 06/08/21 Pct Recovery = 78% Analysis Date = 06/08/21 Pct Recovery = 78% Analysis Date = 06/04/21 Pct Recovery = 78% Analysis Date = 06/04/21 Pct Recovery = 78% Analysis Date = 05/31/21 Pct Recovery = 78% Analysis Date = 05/31/21 Pct Recovery = 78% Analysis Date = 05/27/21 Pct Recovery = 78% Analysis Date = 05/27/21 Pct Recovery = 78% Analysis Date = 05/23/21 Pct Recovery = 78% Analysis Date = 05/23/21 Pct Recovery = 78% Analysis Date = 05/19/21 Pct Recovery = 78% Analysis Date = 05/19/21 Pct Recovery = 78% Analysis Date = 05/15/21 Pct Recovery = 78% Analysis Date = 05/15/21 Pct Recovery = 78% Analysis Date = 05/11/21 Pct Recovery = 78% Analysis Date = 05/11/21 Pct Recovery = 78% Analysis Date = 05/07/21 Pct Recovery = 78% Analysis Date = 05/07/21 Pct Recovery = 78% Analysis Date = 05/03/21 Pct Recovery = 78% Analysis Date = 05/03/21 Pct Recovery = 78% Analysis Date = 04/29/21 Pct Recovery = 78% Analysis Date = 04/29/21 Pct Recovery = 78% Analysis Date = 04/25/21 Pct Recovery = 78% Analysis Date = 04/25/21 Pct Recovery = 78% Analysis Date = 04/21/21 Pct Recovery = 78% Analysis Date = 04/21/21 Pct Recovery = 78% Analysis Date = 04/17/21 Pct Recovery = 78% Analysis Date = 04/17/21 Pct Recovery = 78% Analysis Date = 04/13/21 Pct Recovery = 77% Analysis Date = 04/13/21 Pct Recovery = 77% Analysis Date = 04/09/21 Pct Recovery = 77% Analysis Date = 04/09/21 Pct Recovery = 77% Analysis Date = 04/05/21 Pct Recovery = 77% Analysis Date = 04/05/21 Pct Recovery = 77% Analysis Date = 04/01/21 Pct Recovery = 77% Analysis Date = 04/01/21 Pct Recovery = 77% Analysis Date = 03/28/21 Pct Recovery = 78% Analysis Date = 03/28/21 Pct Recovery = 78% Analysis Date = 03/23/21 Pct Recovery = 78% Analysis Date = 03/23/21 Pct Recovery = 78% Analysis Date = 03/19/21 Pct Recovery = 79% Analysis Date = 03/19/21 Pct Recovery = 79% Analysis Date = 03/15/21 Pct Recovery = 80% Analysis Date = 03/15/21 Pct Recovery = 80% Analysis Date = 03/11/21 Pct Recovery = 81% Analysis Date = 03/11/21 Pct Recovery = 81% Analysis Date = 03/07/21 Pct Recovery = 81% Analysis Date = 03/07/21 Pct Recovery = 81% Analysis Date = 03/03/21 Pct Recovery = 82% Analysis Date = 03/03/21 Pct Recovery = 82% Analysis Date = 02/27/21 Pct Recovery = 83% Analysis Date = 02/27/21 Pct Recovery = 83% Analysis Date = 02/23/21 Pct Recovery = 83% Analysis Date = 02/23/21 Pct Recovery = 83% Analysis Date = 02/19/21 Pct Recovery = 84% Analysis Date = 02/19/21 Pct Recovery = 84% Analysis Date = 02/15/21 Pct Recovery = 85% Analysis Date = 02/15/21 Pct Recovery = 85% Analysis Date = 02/11/21 Pct Recovery = 85% Analysis Date = 02/11/21 Pct Recovery = 85% Analysis Date = 02/07/21 Pct Recovery = 86% Analysis Date = 02/07/21 Pct Recovery = 86% Analysis Date = 02/03/21 Pct Recovery = 87% Analysis Date = 02/03/21 Pct Recovery = 87% Analysis Date = 01/30/21 Pct Recovery = 87% Analysis Date = 01/30/21 Pct Recovery = 87% Analysis Date = 01/26/21 Pct Recovery = 88% Analysis Date = 01/26/21 Pct Recovery = 88% Analysis Date = 01/22/21 Pct Recovery = 89% Analysis Date = 01/22/21 Pct Recovery = 89% Analysis Date = 01/18/21 Pct Recovery = 89% Analysis Date = 01/18/21 Pct Recovery = 89% Analysis Date = 01/14/21 Pct Recovery = 90% Analysis Date = 01/14/21 Pct Recovery = 90% Analysis Date = 01/10/21 Pct Recovery = 91% Analysis Date = 01/10/21 Pct Recovery = 91% Analysis Date = 01/06/21 Pct Recovery = 92% Analysis Date = 01/06/21 Pct Recovery = 92% Analysis Date = 01/02/21 Pct Recovery = 92% Analysis Date = 01/02/21 Pct Recovery = 92% Analysis Date = 12/29/20 Pct Recovery = 93% Analysis Date = 12/29/20 Pct Recovery = 93% Analysis Date = 12/25/20 Pct Recovery = 94% Analysis Date = 12/25/20 Pct Recovery = 94% Analysis Date = 12/21/20 Pct Recovery = 94% Analysis Date = 12/21/20 Pct Recovery = 94% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/12/20 Pct Recovery = 96% Analysis Date = 12/12/20 Pct Recovery = 96% Analysis Date = 12/08/20 Pct Recovery = 96% Analysis Date = 12/08/20 Pct Recovery = 96% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 97% Analysis Date = 11/26/20 Pct Recovery = 98% Analysis Date = 11/26/20 Pct Recovery = 98% Analysis Date = 11/22/20 Pct Recovery = 99% Analysis Date = 11/22/20 Pct Recovery = 99% Analysis Date = 11/18/20 Pct Recovery = 99% Analysis Date = 11/18/20 Pct Recovery = 99% Analysis Date = 11/14/20 Pct Recovery = 100% Analysis Date = 11/14/20 Pct Recovery = 100% Analysis Date = 11/10/20 Pct Recovery = 100% Analysis Date = 11/10/20 Pct Recovery = 100% Analysis Date = 11/06/20 Pct Recovery = 101% Analysis Date = 11/06/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 11/02/20 Pct Recovery = 101% Analysis Date = 10/29/20 Pct Recovery = 102% Analysis Date = 10/29/20 Pct Recovery = 102% Analysis Date = 10/25/20 Pct Recovery = 102% Analysis Date = 10/25/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/21/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 102% Analysis Date = 10/17/20 Pct Recovery = 102% Analysis Date = 10/13/20 Pct Recovery = 102% Analysis Date = 10/13/20 Pct Recovery = 102% Analysis Date = 10/09/20 Pct Recovery = 103% Analysis Date = 10/09/20 Pct Recovery = 103% Analysis Date = 10/05/20 Pct Recovery = 103% Analysis Date = 10/05/20 Pct Recovery = 103% Analysis Date = 10/01/20 Pct Recovery = 103% Analysis Date = 10/01/20 Pct Recovery = 103% Analysis Date = 09/27/20 Pct Recovery = 103% Analysis Date = 09/27/20 Pct Recovery = 103% Analysis Date = 09/23/20 Pct Recovery = 103% Analysis Date = 09/23/20 Pct Recovery = 103% Analysis Date = 09/19/20 Pct Recovery = 104% Analysis Date = 09/19/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/07/20 Pct Recovery = 104% Analysis Date = 09/07/20 Pct Recovery = 104% Analysis Date = 09/02/20 Pct Recovery = 104% Analysis Date = 09/02/20 Pct Recovery = 104% Analysis Date = 08/29/20 Pct Recovery = 104% Analysis Date = 08/29/20 Pct Recovery = 104% Analysis Date = 08/25/20 Pct Recovery = 104% Analysis Date = 08/25/20 Pct Recovery = 104% Analysis Date = 08/21/20 Pct Recovery = 103% Analysis Date = 08/21/20 Pct Recovery = 103% Analysis Date = 08/17/20 Pct Recovery = 103% Analysis Date = 08/17/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/05/20 Pct Recovery = 102% Analysis Date = 08/05/20 Pct Recovery = 102% Analysis Date = 08/01/20 Pct Recovery = 102% Analysis Date = 08/01/20 Pct Recovery = 102% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 102% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/12/20 Pct Recovery = 101% Analysis Date = 07/12/20 Pct Recovery = 101% Analysis Date = 07/08/20 Pct Recovery = 101% Analysis Date = 07/08/20 Pct Recovery = 101% Analysis Date = 07/04/20 Pct Recovery = 100% Analysis Date = 07/04/20 Pct Recovery = 100% Analysis Date = 06/30/20 Pct Recovery = 100% Analysis Date = 06/30/20 Pct Recovery = 100% Analysis Date = 06/26/20 Pct Recovery = 100% Analysis Date = 06/26/20 Pct Recovery = 100% Analysis Date = 06/22/20 Pct Recovery = 100% Analysis Date = 06/22/20 Pct Recovery = 100% Analysis Date = 06/18/20 Pct Recovery = 99% Analysis Date = 06/18/20 Pct Recovery = 99% Analysis Date = 06/14/20 Pct Recovery = 99% Analysis Date = 06/14/20 Pct Recovery = 99% Analysis Date = 06/10/20 Pct Recovery = 99% Analysis Date = 06/10/20 Pct Recovery = 99% Analysis Date = 06/06/20 Pct Recovery = 99% Analysis Date = 06/06/20 Pct Recovery = 99% Analysis Date = 06/02/20 Pct Recovery = 98% Analysis Date = 06/02/20 Pct Recovery = 98% Analysis Date = 05/29/20 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METALAXYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 94% 16% 96% 17%
Total 31 94% 16% 96% 17%

Sample Statistics
METALAXYL

Characteristic N % % Basis
Plotted 31 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 0 0% 0 out of 31
Not Spiked 85 .  
False Positives 5 6% 5 out of 85

OBSP Determination:
METCONAZOLE
METHOD: 2447 , TESTIDCODE: 66620LCM60

Laboratory ID = 20201820155 Lab Value = 54.204 Expected Conc. = 63.5 Report level label = 5 Pct Recovery = 85% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 67.799 Expected Conc. = 63.5 Report level label = 5 Pct Recovery = 107% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 74.263 Expected Conc. = 63 Report level label = 5 Pct Recovery = 118% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203080100 Lab Value = 52.236 Expected Conc. = 62.4 Report level label = 5 Pct Recovery = 84% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 63.648 Expected Conc. = 62.4 Report level label = 5 Pct Recovery = 102% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 59.198 Expected Conc. = 62.4 Report level label = 5 Pct Recovery = 95% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 37.106 Expected Conc. = 61.85 Report level label = 5 Pct Recovery = 60% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 42.036 Expected Conc. = 61.85 Report level label = 5 Pct Recovery = 68% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 50.153 Expected Conc. = 61.85 Report level label = 5 Pct Recovery = 81% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 55.698 Expected Conc. = 61.85 Report level label = 5 Pct Recovery = 90% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221940196 Lab Value = 37.909 Expected Conc. = 50 Report level label = 5 Pct Recovery = 76% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221520237 Lab Value = 48.496 Expected Conc. = 49.64 Report level label = 5 Pct Recovery = 98% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20222150192 Lab Value = 34.710 Expected Conc. = 49.6 Report level label = 5 Pct Recovery = 70% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20202530029 Lab Value = 25.634 Expected Conc. = 31.75 Report level label = 5 Pct Recovery = 81% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 26.509 Expected Conc. = 31.75 Report level label = 5 Pct Recovery = 83% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 28.008 Expected Conc. = 31.75 Report level label = 5 Pct Recovery = 88% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201960104 Lab Value = 36.410 Expected Conc. = 31.5 Report level label = 5 Pct Recovery = 116% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20220740064 Lab Value = 24.261 Expected Conc. = 31.25 Report level label = 5 Pct Recovery = 78% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202880004 Lab Value = 30.814 Expected Conc. = 31.2 Report level label = 5 Pct Recovery = 99% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221870197 Lab Value = 24.141 Expected Conc. = 31.025 Report level label = 5 Pct Recovery = 78% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 22.773 Expected Conc. = 30.925 Report level label = 5 Pct Recovery = 74% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 25.707 Expected Conc. = 24.96 Report level label = 5 Pct Recovery = 103% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 19.807 Expected Conc. = 24.96 Report level label = 5 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 19.467 Expected Conc. = 24.74 Report level label = 5 Pct Recovery = 79% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202180001 Lab Value = 9.256 Expected Conc. = 12.7 Report level label = 5 Pct Recovery = 73% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 14.099 Expected Conc. = 12.7 Report level label = 5 Pct Recovery = 111% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 11.822 Expected Conc. = 12.7 Report level label = 5 Pct Recovery = 93% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201610160 Lab Value = 13.513 Expected Conc. = 12.6 Report level label = 5 Pct Recovery = 107% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210120050 Lab Value = 10.754 Expected Conc. = 12.48 Report level label = 5 Pct Recovery = 86% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 11.802 Expected Conc. = 12.48 Report level label = 5 Pct Recovery = 95% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 8.506 Expected Conc. = 12.48 Report level label = 5 Pct Recovery = 68% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 12.047 Expected Conc. = 12.48 Report level label = 5 Pct Recovery = 97% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 11.268 Expected Conc. = 12.48 Report level label = 5 Pct Recovery = 90% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221660151 Lab Value = 12.665 Expected Conc. = 12.41 Report level label = 5 Pct Recovery = 102% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Analysis Date = 08/15/22 Pct Recovery = 83% Analysis Date = 08/10/22 Pct Recovery = 83% Analysis Date = 08/10/22 Pct Recovery = 83% Analysis Date = 08/06/22 Pct Recovery = 83% Analysis Date = 08/06/22 Pct Recovery = 83% Analysis Date = 08/02/22 Pct Recovery = 83% Analysis Date = 08/02/22 Pct Recovery = 83% Analysis Date = 07/29/22 Pct Recovery = 83% Analysis Date = 07/29/22 Pct Recovery = 83% Analysis Date = 07/25/22 Pct Recovery = 83% Analysis Date = 07/25/22 Pct Recovery = 83% Analysis Date = 07/21/22 Pct Recovery = 83% Analysis Date = 07/21/22 Pct Recovery = 83% Analysis Date = 07/17/22 Pct Recovery = 83% Analysis Date = 07/17/22 Pct Recovery = 83% Analysis Date = 07/13/22 Pct Recovery = 83% Analysis Date = 07/13/22 Pct Recovery = 83% Analysis Date = 07/09/22 Pct Recovery = 83% Analysis Date = 07/09/22 Pct Recovery = 83% Analysis Date = 07/05/22 Pct Recovery = 83% Analysis Date = 07/05/22 Pct Recovery = 83% Analysis Date = 07/01/22 Pct Recovery = 83% Analysis Date = 07/01/22 Pct Recovery = 83% Analysis Date = 06/26/22 Pct Recovery = 83% Analysis Date = 06/26/22 Pct Recovery = 83% Analysis Date = 06/22/22 Pct Recovery = 83% Analysis Date = 06/22/22 Pct Recovery = 83% Analysis Date = 06/18/22 Pct Recovery = 83% Analysis Date = 06/18/22 Pct Recovery = 83% Analysis Date = 06/14/22 Pct Recovery = 83% Analysis Date = 06/14/22 Pct Recovery = 83% Analysis Date = 06/10/22 Pct Recovery = 83% Analysis Date = 06/10/22 Pct Recovery = 83% Analysis Date = 06/06/22 Pct Recovery = 83% Analysis Date = 06/06/22 Pct Recovery = 83% Analysis Date = 06/02/22 Pct Recovery = 83% Analysis Date = 06/02/22 Pct Recovery = 83% Analysis Date = 05/29/22 Pct Recovery = 83% Analysis Date = 05/29/22 Pct Recovery = 83% Analysis Date = 05/25/22 Pct Recovery = 83% Analysis Date = 05/25/22 Pct Recovery = 83% Analysis Date = 05/21/22 Pct Recovery = 83% Analysis Date = 05/21/22 Pct Recovery = 83% Analysis Date = 05/17/22 Pct Recovery = 83% Analysis Date = 05/17/22 Pct Recovery = 83% Analysis Date = 05/12/22 Pct Recovery = 83% Analysis Date = 05/12/22 Pct Recovery = 83% Analysis Date = 05/08/22 Pct Recovery = 83% Analysis Date = 05/08/22 Pct Recovery = 83% Analysis Date = 05/04/22 Pct Recovery = 83% Analysis Date = 05/04/22 Pct Recovery = 83% Analysis Date = 04/30/22 Pct Recovery = 83% Analysis Date = 04/30/22 Pct Recovery = 83% Analysis Date = 04/26/22 Pct Recovery = 83% Analysis Date = 04/26/22 Pct Recovery = 83% Analysis Date = 04/22/22 Pct Recovery = 83% Analysis Date = 04/22/22 Pct Recovery = 83% Analysis Date = 04/18/22 Pct Recovery = 83% Analysis Date = 04/18/22 Pct Recovery = 83% Analysis Date = 04/14/22 Pct Recovery = 83% Analysis Date = 04/14/22 Pct Recovery = 83% Analysis Date = 04/10/22 Pct Recovery = 82% Analysis Date = 04/10/22 Pct Recovery = 82% Analysis Date = 04/06/22 Pct Recovery = 82% Analysis Date = 04/06/22 Pct Recovery = 82% Analysis Date = 04/02/22 Pct Recovery = 82% Analysis Date = 04/02/22 Pct Recovery = 82% Analysis Date = 03/28/22 Pct Recovery = 82% Analysis Date = 03/28/22 Pct Recovery = 82% Analysis Date = 03/24/22 Pct Recovery = 82% Analysis Date = 03/24/22 Pct Recovery = 82% Analysis Date = 03/20/22 Pct Recovery = 82% Analysis Date = 03/20/22 Pct Recovery = 82% Analysis Date = 03/16/22 Pct Recovery = 82% Analysis Date = 03/16/22 Pct Recovery = 82% Analysis Date = 03/12/22 Pct Recovery = 82% Analysis Date = 03/12/22 Pct Recovery = 82% Analysis Date = 03/08/22 Pct Recovery = 82% Analysis Date = 03/08/22 Pct Recovery = 82% Analysis Date = 03/04/22 Pct Recovery = 82% Analysis Date = 03/04/22 Pct Recovery = 82% Analysis Date = 02/28/22 Pct Recovery = 82% Analysis Date = 02/28/22 Pct Recovery = 82% Analysis Date = 02/24/22 Pct Recovery = 82% Analysis Date = 02/24/22 Pct Recovery = 82% Analysis Date = 02/20/22 Pct Recovery = 82% Analysis Date = 02/20/22 Pct Recovery = 82% Analysis Date = 02/16/22 Pct Recovery = 82% Analysis Date = 02/16/22 Pct Recovery = 82% Analysis Date = 02/11/22 Pct Recovery = 82% Analysis Date = 02/11/22 Pct Recovery = 82% Analysis Date = 02/07/22 Pct Recovery = 82% Analysis Date = 02/07/22 Pct Recovery = 82% Analysis Date = 02/03/22 Pct Recovery = 82% Analysis Date = 02/03/22 Pct Recovery = 82% Analysis Date = 01/30/22 Pct Recovery = 82% Analysis Date = 01/30/22 Pct Recovery = 82% Analysis Date = 01/26/22 Pct Recovery = 82% Analysis Date = 01/26/22 Pct Recovery = 82% Analysis Date = 01/22/22 Pct Recovery = 82% Analysis Date = 01/22/22 Pct Recovery = 82% Analysis Date = 01/18/22 Pct Recovery = 82% Analysis Date = 01/18/22 Pct Recovery = 82% Analysis Date = 01/14/22 Pct Recovery = 82% Analysis Date = 01/14/22 Pct Recovery = 82% Analysis Date = 01/10/22 Pct Recovery = 82% Analysis Date = 01/10/22 Pct Recovery = 82% Analysis Date = 01/06/22 Pct Recovery = 82% Analysis Date = 01/06/22 Pct Recovery = 82% Analysis Date = 01/02/22 Pct Recovery = 81% Analysis Date = 01/02/22 Pct Recovery = 81% Analysis Date = 12/28/21 Pct Recovery = 81% Analysis Date = 12/28/21 Pct Recovery = 81% Analysis Date = 12/24/21 Pct Recovery = 81% Analysis Date = 12/24/21 Pct Recovery = 81% Analysis Date = 12/20/21 Pct Recovery = 81% Analysis Date = 12/20/21 Pct Recovery = 81% Analysis Date = 12/16/21 Pct Recovery = 81% Analysis Date = 12/16/21 Pct Recovery = 81% Analysis Date = 12/12/21 Pct Recovery = 81% Analysis Date = 12/12/21 Pct Recovery = 81% Analysis Date = 12/08/21 Pct Recovery = 81% Analysis Date = 12/08/21 Pct Recovery = 81% Analysis Date = 12/04/21 Pct Recovery = 81% Analysis Date = 12/04/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 81% Analysis Date = 11/26/21 Pct Recovery = 81% Analysis Date = 11/26/21 Pct Recovery = 81% Analysis Date = 11/22/21 Pct Recovery = 81% Analysis Date = 11/22/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/18/21 Pct Recovery = 81% Analysis Date = 11/13/21 Pct Recovery = 81% Analysis Date = 11/13/21 Pct Recovery = 81% Analysis Date = 11/09/21 Pct Recovery = 81% Analysis Date = 11/09/21 Pct Recovery = 81% Analysis Date = 11/05/21 Pct Recovery = 81% Analysis Date = 11/05/21 Pct Recovery = 81% Analysis Date = 11/01/21 Pct Recovery = 81% Analysis Date = 11/01/21 Pct Recovery = 81% Analysis Date = 10/28/21 Pct Recovery = 81% Analysis Date = 10/28/21 Pct Recovery = 81% Analysis Date = 10/24/21 Pct Recovery = 81% Analysis Date = 10/24/21 Pct Recovery = 81% Analysis Date = 10/20/21 Pct Recovery = 81% Analysis Date = 10/20/21 Pct Recovery = 81% Analysis Date = 10/16/21 Pct Recovery = 81% Analysis Date = 10/16/21 Pct Recovery = 81% Analysis Date = 10/12/21 Pct Recovery = 81% Analysis Date = 10/12/21 Pct Recovery = 81% Analysis Date = 10/08/21 Pct Recovery = 81% Analysis Date = 10/08/21 Pct Recovery = 81% Analysis Date = 10/04/21 Pct Recovery = 81% Analysis Date = 10/04/21 Pct Recovery = 81% Analysis Date = 09/29/21 Pct Recovery = 80% Analysis Date = 09/29/21 Pct Recovery = 80% Analysis Date = 09/25/21 Pct Recovery = 80% Analysis Date = 09/25/21 Pct Recovery = 80% Analysis Date = 09/21/21 Pct Recovery = 80% Analysis Date = 09/21/21 Pct Recovery = 80% Analysis Date = 09/17/21 Pct Recovery = 80% Analysis Date = 09/17/21 Pct Recovery = 80% Analysis Date = 09/13/21 Pct Recovery = 80% Analysis Date = 09/13/21 Pct Recovery = 80% Analysis Date = 09/09/21 Pct Recovery = 80% Analysis Date = 09/09/21 Pct Recovery = 80% Analysis Date = 09/05/21 Pct Recovery = 80% Analysis Date = 09/05/21 Pct Recovery = 80% Analysis Date = 09/01/21 Pct Recovery = 80% Analysis Date = 09/01/21 Pct Recovery = 80% Analysis Date = 08/28/21 Pct Recovery = 80% Analysis Date = 08/28/21 Pct Recovery = 80% Analysis Date = 08/24/21 Pct Recovery = 80% Analysis Date = 08/24/21 Pct Recovery = 80% Analysis Date = 08/20/21 Pct Recovery = 80% Analysis Date = 08/20/21 Pct Recovery = 80% Analysis Date = 08/15/21 Pct Recovery = 80% Analysis Date = 08/15/21 Pct Recovery = 80% Analysis Date = 08/11/21 Pct Recovery = 80% Analysis Date = 08/11/21 Pct Recovery = 80% Analysis Date = 08/07/21 Pct Recovery = 80% Analysis Date = 08/07/21 Pct Recovery = 80% Analysis Date = 08/03/21 Pct Recovery = 80% Analysis Date = 08/03/21 Pct Recovery = 80% Analysis Date = 07/30/21 Pct Recovery = 80% Analysis Date = 07/30/21 Pct Recovery = 80% Analysis Date = 07/26/21 Pct Recovery = 80% Analysis Date = 07/26/21 Pct Recovery = 80% Analysis Date = 07/22/21 Pct Recovery = 80% Analysis Date = 07/22/21 Pct Recovery = 80% Analysis Date = 07/18/21 Pct Recovery = 80% Analysis Date = 07/18/21 Pct Recovery = 80% Analysis Date = 07/14/21 Pct Recovery = 80% Analysis Date = 07/14/21 Pct Recovery = 80% Analysis Date = 07/10/21 Pct Recovery = 80% Analysis Date = 07/10/21 Pct Recovery = 80% Analysis Date = 07/06/21 Pct Recovery = 80% Analysis Date = 07/06/21 Pct Recovery = 80% Analysis Date = 07/02/21 Pct Recovery = 80% Analysis Date = 07/02/21 Pct Recovery = 80% Analysis Date = 06/27/21 Pct Recovery = 80% Analysis Date = 06/27/21 Pct Recovery = 80% Analysis Date = 06/23/21 Pct Recovery = 79% Analysis Date = 06/23/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/07/21 Pct Recovery = 79% Analysis Date = 06/07/21 Pct Recovery = 79% Analysis Date = 06/03/21 Pct Recovery = 79% Analysis Date = 06/03/21 Pct Recovery = 79% Analysis Date = 05/30/21 Pct Recovery = 79% Analysis Date = 05/30/21 Pct Recovery = 79% Analysis Date = 05/26/21 Pct Recovery = 79% Analysis Date = 05/26/21 Pct Recovery = 79% Analysis Date = 05/22/21 Pct Recovery = 79% Analysis Date = 05/22/21 Pct Recovery = 79% Analysis Date = 05/18/21 Pct Recovery = 79% Analysis Date = 05/18/21 Pct Recovery = 79% Analysis Date = 05/13/21 Pct Recovery = 79% Analysis Date = 05/13/21 Pct Recovery = 79% Analysis Date = 05/09/21 Pct Recovery = 79% Analysis Date = 05/09/21 Pct Recovery = 79% Analysis Date = 05/05/21 Pct Recovery = 79% Analysis Date = 05/05/21 Pct Recovery = 79% Analysis Date = 05/01/21 Pct Recovery = 79% Analysis Date = 05/01/21 Pct Recovery = 79% Analysis Date = 04/27/21 Pct Recovery = 79% Analysis Date = 04/27/21 Pct Recovery = 79% Analysis Date = 04/23/21 Pct Recovery = 79% Analysis Date = 04/23/21 Pct Recovery = 79% Analysis Date = 04/19/21 Pct Recovery = 79% Analysis Date = 04/19/21 Pct Recovery = 79% Analysis Date = 04/15/21 Pct Recovery = 79% Analysis Date = 04/15/21 Pct Recovery = 79% Analysis Date = 04/11/21 Pct Recovery = 79% Analysis Date = 04/11/21 Pct Recovery = 79% Analysis Date = 04/07/21 Pct Recovery = 79% Analysis Date = 04/07/21 Pct Recovery = 79% Analysis Date = 04/03/21 Pct Recovery = 79% Analysis Date = 04/03/21 Pct Recovery = 79% Analysis Date = 03/29/21 Pct Recovery = 79% Analysis Date = 03/29/21 Pct Recovery = 79% Analysis Date = 03/25/21 Pct Recovery = 79% Analysis Date = 03/25/21 Pct Recovery = 79% Analysis Date = 03/21/21 Pct Recovery = 78% Analysis Date = 03/21/21 Pct Recovery = 78% Analysis Date = 03/17/21 Pct Recovery = 78% Analysis Date = 03/17/21 Pct Recovery = 78% Analysis Date = 03/13/21 Pct Recovery = 78% Analysis Date = 03/13/21 Pct Recovery = 78% Analysis Date = 03/09/21 Pct Recovery = 78% Analysis Date = 03/09/21 Pct Recovery = 78% Analysis Date = 03/05/21 Pct Recovery = 79% Analysis Date = 03/05/21 Pct Recovery = 79% Analysis Date = 03/01/21 Pct Recovery = 79% Analysis Date = 03/01/21 Pct Recovery = 79% Analysis Date = 02/25/21 Pct Recovery = 79% Analysis Date = 02/25/21 Pct Recovery = 79% Analysis Date = 02/21/21 Pct Recovery = 80% Analysis Date = 02/21/21 Pct Recovery = 80% Analysis Date = 02/17/21 Pct Recovery = 80% Analysis Date = 02/17/21 Pct Recovery = 80% Analysis Date = 02/12/21 Pct Recovery = 80% Analysis Date = 02/12/21 Pct Recovery = 80% Analysis Date = 02/08/21 Pct Recovery = 81% Analysis Date = 02/08/21 Pct Recovery = 81% Analysis Date = 02/04/21 Pct Recovery = 81% Analysis Date = 02/04/21 Pct Recovery = 81% Analysis Date = 01/31/21 Pct Recovery = 81% Analysis Date = 01/31/21 Pct Recovery = 81% Analysis Date = 01/27/21 Pct Recovery = 82% Analysis Date = 01/27/21 Pct Recovery = 82% Analysis Date = 01/23/21 Pct Recovery = 82% Analysis Date = 01/23/21 Pct Recovery = 82% Analysis Date = 01/19/21 Pct Recovery = 82% Analysis Date = 01/19/21 Pct Recovery = 82% Analysis Date = 01/15/21 Pct Recovery = 83% Analysis Date = 01/15/21 Pct Recovery = 83% Analysis Date = 01/11/21 Pct Recovery = 83% Analysis Date = 01/11/21 Pct Recovery = 83% Analysis Date = 01/07/21 Pct Recovery = 84% Analysis Date = 01/07/21 Pct Recovery = 84% Analysis Date = 01/03/21 Pct Recovery = 84% Analysis Date = 01/03/21 Pct Recovery = 84% Analysis Date = 12/29/20 Pct Recovery = 84% Analysis Date = 12/29/20 Pct Recovery = 84% Analysis Date = 12/25/20 Pct Recovery = 85% Analysis Date = 12/25/20 Pct Recovery = 85% Analysis Date = 12/21/20 Pct Recovery = 85% Analysis Date = 12/21/20 Pct Recovery = 85% Analysis Date = 12/17/20 Pct Recovery = 85% Analysis Date = 12/17/20 Pct Recovery = 85% Analysis Date = 12/13/20 Pct Recovery = 86% Analysis Date = 12/13/20 Pct Recovery = 86% Analysis Date = 12/09/20 Pct Recovery = 86% Analysis Date = 12/09/20 Pct Recovery = 86% Analysis Date = 12/05/20 Pct Recovery = 87% Analysis Date = 12/05/20 Pct Recovery = 87% Analysis Date = 12/01/20 Pct Recovery = 87% Analysis Date = 12/01/20 Pct Recovery = 87% Analysis Date = 11/27/20 Pct Recovery = 87% Analysis Date = 11/27/20 Pct Recovery = 87% Analysis Date = 11/23/20 Pct Recovery = 88% Analysis Date = 11/23/20 Pct Recovery = 88% Analysis Date = 11/19/20 Pct Recovery = 88% Analysis Date = 11/19/20 Pct Recovery = 88% Analysis Date = 11/14/20 Pct Recovery = 88% Analysis Date = 11/14/20 Pct Recovery = 88% Analysis Date = 11/10/20 Pct Recovery = 89% Analysis Date = 11/10/20 Pct Recovery = 89% Analysis Date = 11/06/20 Pct Recovery = 89% Analysis Date = 11/06/20 Pct Recovery = 89% Analysis Date = 11/02/20 Pct Recovery = 90% Analysis Date = 11/02/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/25/20 Pct Recovery = 90% Analysis Date = 10/25/20 Pct Recovery = 90% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 91% Analysis Date = 10/13/20 Pct Recovery = 92% Analysis Date = 10/13/20 Pct Recovery = 92% Analysis Date = 10/09/20 Pct Recovery = 92% Analysis Date = 10/09/20 Pct Recovery = 92% Analysis Date = 10/05/20 Pct Recovery = 92% Analysis Date = 10/05/20 Pct Recovery = 92% Analysis Date = 09/30/20 Pct Recovery = 93% Analysis Date = 09/30/20 Pct Recovery = 93% Analysis Date = 09/26/20 Pct Recovery = 93% Analysis Date = 09/26/20 Pct Recovery = 93% Analysis Date = 09/22/20 Pct Recovery = 94% Analysis Date = 09/22/20 Pct Recovery = 94% Analysis Date = 09/18/20 Pct Recovery = 94% Analysis Date = 09/18/20 Pct Recovery = 94% Analysis Date = 09/14/20 Pct Recovery = 94% Analysis Date = 09/14/20 Pct Recovery = 94% Analysis Date = 09/10/20 Pct Recovery = 95% Analysis Date = 09/10/20 Pct Recovery = 95% Analysis Date = 09/06/20 Pct Recovery = 95% Analysis Date = 09/06/20 Pct Recovery = 95% Analysis Date = 09/02/20 Pct Recovery = 95% Analysis Date = 09/02/20 Pct Recovery = 95% Analysis Date = 08/29/20 Pct Recovery = 95% Analysis Date = 08/29/20 Pct Recovery = 95% Analysis Date = 08/25/20 Pct Recovery = 96% Analysis Date = 08/25/20 Pct Recovery = 96% Analysis Date = 08/21/20 Pct Recovery = 96% Analysis Date = 08/21/20 Pct Recovery = 96% Analysis Date = 08/16/20 Pct Recovery = 96% Analysis Date = 08/16/20 Pct Recovery = 96% Analysis Date = 08/12/20 Pct Recovery = 96% Analysis Date = 08/12/20 Pct Recovery = 96% Analysis Date = 08/08/20 Pct Recovery = 96% Analysis Date = 08/08/20 Pct Recovery = 96% Analysis Date = 08/04/20 Pct Recovery = 97% Analysis Date = 08/04/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 97% Analysis Date = 07/19/20 Pct Recovery = 97% Analysis Date = 07/19/20 Pct Recovery = 97% Analysis Date = 07/15/20 Pct Recovery = 98% Analysis Date = 07/15/20 Pct Recovery = 98% Analysis Date = 07/11/20 Pct Recovery = 98% Analysis Date = 07/11/20 Pct Recovery = 98% Analysis Date = 07/07/20 Pct Recovery = 98% Analysis Date = 07/07/20 Pct Recovery = 98% Analysis Date = 07/02/20 Pct Recovery = 98% Analysis Date = 07/02/20 Pct Recovery = 98% Analysis Date = 06/28/20 Pct Recovery = 98% Analysis Date = 06/28/20 Pct Recovery = 98% Analysis Date = 06/24/20 Pct Recovery = 99% Analysis Date = 06/24/20 Pct Recovery = 99% Analysis Date = 06/20/20 Pct Recovery = 99% Analysis Date = 06/20/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/12/20 Pct Recovery = 99% Analysis Date = 06/12/20 Pct Recovery = 99% Analysis Date = 06/08/20 Pct Recovery = 99% Analysis Date = 06/08/20 Pct Recovery = 99% Analysis Date = 06/04/20 Pct Recovery = 99% Analysis Date = 06/04/20 Pct Recovery = 99% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 100% Analysis Date = 05/23/20 Pct Recovery = 100% Analysis Date = 05/23/20 Pct Recovery = 100% Analysis Date = 05/19/20 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 89% 14% 87% 16%
Total 34 89% 14% 87% 16%

Sample Statistics
METCONAZOLE

Characteristic N % % Basis
Plotted 34 97% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 1 3% 1 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
METHAMIDOPHOS
METHOD: 2447 , TESTIDCODE: 68644LCM60

Laboratory ID = 20202110006 Lab Value = 162.294 Expected Conc. = 126.5 Report level label = 10 Pct Recovery = 128% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 147.974 Expected Conc. = 126.3 Report level label = 10 Pct Recovery = 117% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 118.752 Expected Conc. = 125.3 Report level label = 10 Pct Recovery = 95% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 141.442 Expected Conc. = 125.3 Report level label = 10 Pct Recovery = 113% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 133.246 Expected Conc. = 125.3 Report level label = 10 Pct Recovery = 106% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 119.284 Expected Conc. = 123.3 Report level label = 10 Pct Recovery = 97% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 108.193 Expected Conc. = 123.3 Report level label = 10 Pct Recovery = 88% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 94.339 Expected Conc. = 123.3 Report level label = 10 Pct Recovery = 77% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 113.552 Expected Conc. = 123.3 Report level label = 10 Pct Recovery = 92% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221370164 Lab Value = 96.606 Expected Conc. = 100.28 Report level label = 10 Pct Recovery = 96% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 111.862 Expected Conc. = 100 Report level label = 10 Pct Recovery = 112% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 102.584 Expected Conc. = 100 Report level label = 10 Pct Recovery = 103% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 75.429 Expected Conc. = 100 Report level label = 10 Pct Recovery = 75% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20201680155 Lab Value = 73.193 Expected Conc. = 63.25 Report level label = 10 Pct Recovery = 116% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 74.524 Expected Conc. = 63.15 Report level label = 10 Pct Recovery = 118% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 71.649 Expected Conc. = 63.15 Report level label = 10 Pct Recovery = 113% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 63.702 Expected Conc. = 63.15 Report level label = 10 Pct Recovery = 101% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202880004 Lab Value = 78.442 Expected Conc. = 62.65 Report level label = 10 Pct Recovery = 125% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222070177 Lab Value = 54.694 Expected Conc. = 62.5 Report level label = 10 Pct Recovery = 88% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20210480001 Lab Value = 53.369 Expected Conc. = 61.65 Report level label = 10 Pct Recovery = 87% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 65.405 Expected Conc. = 50.12 Report level label = 10 Pct Recovery = 130% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 59.240 Expected Conc. = 50.12 Report level label = 10 Pct Recovery = 118% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 54.109 Expected Conc. = 49.32 Report level label = 10 Pct Recovery = 110% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 27.436 Expected Conc. = 25.3 Report level label = 10 Pct Recovery = 108% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 23.541 Expected Conc. = 25.26 Report level label = 10 Pct Recovery = 93% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 38.064 Expected Conc. = 25.26 Report level label = 10 Pct Recovery = 151% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 41.661 Expected Conc. = 25.26 Report level label = 10 Pct Recovery = 165% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 33.392 Expected Conc. = 25.26 Report level label = 10 Pct Recovery = 132% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20221160208 Lab Value = 16.244 Expected Conc. = 25.07 Report level label = 10 Pct Recovery = 65% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20210120050 Lab Value = 26.420 Expected Conc. = 25.06 Report level label = 10 Pct Recovery = 105% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 29.776 Expected Conc. = 25.06 Report level label = 10 Pct Recovery = 119% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 30.559 Expected Conc. = 25.06 Report level label = 10 Pct Recovery = 122% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 30.544 Expected Conc. = 25.06 Report level label = 10 Pct Recovery = 122% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 35.550 Expected Conc. = 25.06 Report level label = 10 Pct Recovery = 142% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222000207 Lab Value = 20.986 Expected Conc. = 25 Report level label = 10 Pct Recovery = 84% Analysis Date = 07/27/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20210690067 Lab Value = 20.882 Expected Conc. = 24.66 Report level label = 10 Pct Recovery = 85% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 08/16/22 Pct Recovery = 89% Analysis Date = 08/11/22 Pct Recovery = 89% Analysis Date = 08/11/22 Pct Recovery = 89% Analysis Date = 08/07/22 Pct Recovery = 89% Analysis Date = 08/07/22 Pct Recovery = 89% Analysis Date = 08/03/22 Pct Recovery = 89% Analysis Date = 08/03/22 Pct Recovery = 89% Analysis Date = 07/30/22 Pct Recovery = 89% Analysis Date = 07/30/22 Pct Recovery = 89% Analysis Date = 07/26/22 Pct Recovery = 89% Analysis Date = 07/26/22 Pct Recovery = 89% Analysis Date = 07/22/22 Pct Recovery = 90% Analysis Date = 07/22/22 Pct Recovery = 90% Analysis Date = 07/18/22 Pct Recovery = 90% Analysis Date = 07/18/22 Pct Recovery = 90% Analysis Date = 07/14/22 Pct Recovery = 90% Analysis Date = 07/14/22 Pct Recovery = 90% Analysis Date = 07/10/22 Pct Recovery = 90% Analysis Date = 07/10/22 Pct Recovery = 90% Analysis Date = 07/06/22 Pct Recovery = 90% Analysis Date = 07/06/22 Pct Recovery = 90% Analysis Date = 07/01/22 Pct Recovery = 90% Analysis Date = 07/01/22 Pct Recovery = 90% Analysis Date = 06/27/22 Pct Recovery = 90% Analysis Date = 06/27/22 Pct Recovery = 90% Analysis Date = 06/23/22 Pct Recovery = 90% Analysis Date = 06/23/22 Pct Recovery = 90% Analysis Date = 06/19/22 Pct Recovery = 90% Analysis Date = 06/19/22 Pct Recovery = 90% Analysis Date = 06/15/22 Pct Recovery = 90% Analysis Date = 06/15/22 Pct Recovery = 90% Analysis Date = 06/11/22 Pct Recovery = 90% Analysis Date = 06/11/22 Pct Recovery = 90% Analysis Date = 06/07/22 Pct Recovery = 90% Analysis Date = 06/07/22 Pct Recovery = 90% Analysis Date = 06/03/22 Pct Recovery = 90% Analysis Date = 06/03/22 Pct Recovery = 90% Analysis Date = 05/30/22 Pct Recovery = 90% Analysis Date = 05/30/22 Pct Recovery = 90% Analysis Date = 05/26/22 Pct Recovery = 90% Analysis Date = 05/26/22 Pct Recovery = 90% Analysis Date = 05/22/22 Pct Recovery = 90% Analysis Date = 05/22/22 Pct Recovery = 90% Analysis Date = 05/17/22 Pct Recovery = 90% Analysis Date = 05/17/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/05/22 Pct Recovery = 91% Analysis Date = 05/05/22 Pct Recovery = 91% Analysis Date = 05/01/22 Pct Recovery = 91% Analysis Date = 05/01/22 Pct Recovery = 91% Analysis Date = 04/27/22 Pct Recovery = 91% Analysis Date = 04/27/22 Pct Recovery = 91% Analysis Date = 04/23/22 Pct Recovery = 91% Analysis Date = 04/23/22 Pct Recovery = 91% Analysis Date = 04/19/22 Pct Recovery = 91% Analysis Date = 04/19/22 Pct Recovery = 91% Analysis Date = 04/15/22 Pct Recovery = 91% Analysis Date = 04/15/22 Pct Recovery = 91% Analysis Date = 04/11/22 Pct Recovery = 91% Analysis Date = 04/11/22 Pct Recovery = 91% Analysis Date = 04/06/22 Pct Recovery = 91% Analysis Date = 04/06/22 Pct Recovery = 91% Analysis Date = 04/02/22 Pct Recovery = 91% Analysis Date = 04/02/22 Pct Recovery = 91% Analysis Date = 03/29/22 Pct Recovery = 91% Analysis Date = 03/29/22 Pct Recovery = 91% Analysis Date = 03/25/22 Pct Recovery = 91% Analysis Date = 03/25/22 Pct Recovery = 91% Analysis Date = 03/21/22 Pct Recovery = 91% Analysis Date = 03/21/22 Pct Recovery = 91% Analysis Date = 03/17/22 Pct Recovery = 91% Analysis Date = 03/17/22 Pct Recovery = 91% Analysis Date = 03/13/22 Pct Recovery = 92% Analysis Date = 03/13/22 Pct Recovery = 92% Analysis Date = 03/09/22 Pct Recovery = 92% Analysis Date = 03/09/22 Pct Recovery = 92% Analysis Date = 03/05/22 Pct Recovery = 92% Analysis Date = 03/05/22 Pct Recovery = 92% Analysis Date = 03/01/22 Pct Recovery = 92% Analysis Date = 03/01/22 Pct Recovery = 92% Analysis Date = 02/25/22 Pct Recovery = 92% Analysis Date = 02/25/22 Pct Recovery = 92% Analysis Date = 02/20/22 Pct Recovery = 92% Analysis Date = 02/20/22 Pct Recovery = 92% Analysis Date = 02/16/22 Pct Recovery = 92% Analysis Date = 02/16/22 Pct Recovery = 92% Analysis Date = 02/12/22 Pct Recovery = 92% Analysis Date = 02/12/22 Pct Recovery = 92% Analysis Date = 02/08/22 Pct Recovery = 92% Analysis Date = 02/08/22 Pct Recovery = 92% Analysis Date = 02/04/22 Pct Recovery = 92% Analysis Date = 02/04/22 Pct Recovery = 92% Analysis Date = 01/31/22 Pct Recovery = 92% Analysis Date = 01/31/22 Pct Recovery = 92% Analysis Date = 01/27/22 Pct Recovery = 92% Analysis Date = 01/27/22 Pct Recovery = 92% Analysis Date = 01/23/22 Pct Recovery = 92% Analysis Date = 01/23/22 Pct Recovery = 92% Analysis Date = 01/19/22 Pct Recovery = 93% Analysis Date = 01/19/22 Pct Recovery = 93% Analysis Date = 01/15/22 Pct Recovery = 93% Analysis Date = 01/15/22 Pct Recovery = 93% Analysis Date = 01/10/22 Pct Recovery = 93% Analysis Date = 01/10/22 Pct Recovery = 93% Analysis Date = 01/06/22 Pct Recovery = 93% Analysis Date = 01/06/22 Pct Recovery = 93% Analysis Date = 01/02/22 Pct Recovery = 93% Analysis Date = 01/02/22 Pct Recovery = 93% Analysis Date = 12/29/21 Pct Recovery = 93% Analysis Date = 12/29/21 Pct Recovery = 93% Analysis Date = 12/25/21 Pct Recovery = 93% Analysis Date = 12/25/21 Pct Recovery = 93% Analysis Date = 12/21/21 Pct Recovery = 93% Analysis Date = 12/21/21 Pct Recovery = 93% Analysis Date = 12/17/21 Pct Recovery = 93% Analysis Date = 12/17/21 Pct Recovery = 93% Analysis Date = 12/13/21 Pct Recovery = 93% Analysis Date = 12/13/21 Pct Recovery = 93% Analysis Date = 12/09/21 Pct Recovery = 93% Analysis Date = 12/09/21 Pct Recovery = 93% Analysis Date = 12/05/21 Pct Recovery = 93% Analysis Date = 12/05/21 Pct Recovery = 93% Analysis Date = 12/01/21 Pct Recovery = 93% Analysis Date = 12/01/21 Pct Recovery = 93% Analysis Date = 11/26/21 Pct Recovery = 94% Analysis Date = 11/26/21 Pct Recovery = 94% Analysis Date = 11/22/21 Pct Recovery = 94% Analysis Date = 11/22/21 Pct Recovery = 94% Analysis Date = 11/18/21 Pct Recovery = 94% Analysis Date = 11/18/21 Pct Recovery = 94% Analysis Date = 11/14/21 Pct Recovery = 94% Analysis Date = 11/14/21 Pct Recovery = 94% Analysis Date = 11/10/21 Pct Recovery = 94% Analysis Date = 11/10/21 Pct Recovery = 94% Analysis Date = 11/06/21 Pct Recovery = 94% Analysis Date = 11/06/21 Pct Recovery = 94% Analysis Date = 11/02/21 Pct Recovery = 94% Analysis Date = 11/02/21 Pct Recovery = 94% Analysis Date = 10/29/21 Pct Recovery = 94% Analysis Date = 10/29/21 Pct Recovery = 94% Analysis Date = 10/25/21 Pct Recovery = 94% Analysis Date = 10/25/21 Pct Recovery = 94% Analysis Date = 10/21/21 Pct Recovery = 94% Analysis Date = 10/21/21 Pct Recovery = 94% Analysis Date = 10/16/21 Pct Recovery = 94% Analysis Date = 10/16/21 Pct Recovery = 94% Analysis Date = 10/12/21 Pct Recovery = 94% Analysis Date = 10/12/21 Pct Recovery = 94% Analysis Date = 10/08/21 Pct Recovery = 94% Analysis Date = 10/08/21 Pct Recovery = 94% Analysis Date = 10/04/21 Pct Recovery = 95% Analysis Date = 10/04/21 Pct Recovery = 95% Analysis Date = 09/30/21 Pct Recovery = 95% Analysis Date = 09/30/21 Pct Recovery = 95% Analysis Date = 09/26/21 Pct Recovery = 95% Analysis Date = 09/26/21 Pct Recovery = 95% Analysis Date = 09/22/21 Pct Recovery = 95% Analysis Date = 09/22/21 Pct Recovery = 95% Analysis Date = 09/18/21 Pct Recovery = 95% Analysis Date = 09/18/21 Pct Recovery = 95% Analysis Date = 09/14/21 Pct Recovery = 95% Analysis Date = 09/14/21 Pct Recovery = 95% Analysis Date = 09/10/21 Pct Recovery = 95% Analysis Date = 09/10/21 Pct Recovery = 95% Analysis Date = 09/06/21 Pct Recovery = 95% Analysis Date = 09/06/21 Pct Recovery = 95% Analysis Date = 09/01/21 Pct Recovery = 95% Analysis Date = 09/01/21 Pct Recovery = 95% Analysis Date = 08/28/21 Pct Recovery = 95% Analysis Date = 08/28/21 Pct Recovery = 95% Analysis Date = 08/24/21 Pct Recovery = 95% Analysis Date = 08/24/21 Pct Recovery = 95% Analysis Date = 08/20/21 Pct Recovery = 95% Analysis Date = 08/20/21 Pct Recovery = 95% Analysis Date = 08/16/21 Pct Recovery = 95% Analysis Date = 08/16/21 Pct Recovery = 95% Analysis Date = 08/12/21 Pct Recovery = 96% Analysis Date = 08/12/21 Pct Recovery = 96% Analysis Date = 08/08/21 Pct Recovery = 96% Analysis Date = 08/08/21 Pct Recovery = 96% Analysis Date = 08/04/21 Pct Recovery = 96% Analysis Date = 08/04/21 Pct Recovery = 96% Analysis Date = 07/31/21 Pct Recovery = 96% Analysis Date = 07/31/21 Pct Recovery = 96% Analysis Date = 07/27/21 Pct Recovery = 96% Analysis Date = 07/27/21 Pct Recovery = 96% Analysis Date = 07/22/21 Pct Recovery = 96% Analysis Date = 07/22/21 Pct Recovery = 96% Analysis Date = 07/18/21 Pct Recovery = 96% Analysis Date = 07/18/21 Pct Recovery = 96% Analysis Date = 07/14/21 Pct Recovery = 96% Analysis Date = 07/14/21 Pct Recovery = 96% Analysis Date = 07/10/21 Pct Recovery = 96% Analysis Date = 07/10/21 Pct Recovery = 96% Analysis Date = 07/06/21 Pct Recovery = 96% Analysis Date = 07/06/21 Pct Recovery = 96% Analysis Date = 07/02/21 Pct Recovery = 96% Analysis Date = 07/02/21 Pct Recovery = 96% Analysis Date = 06/28/21 Pct Recovery = 96% Analysis Date = 06/28/21 Pct Recovery = 96% Analysis Date = 06/24/21 Pct Recovery = 96% Analysis Date = 06/24/21 Pct Recovery = 96% Analysis Date = 06/20/21 Pct Recovery = 97% Analysis Date = 06/20/21 Pct Recovery = 97% Analysis Date = 06/16/21 Pct Recovery = 97% Analysis Date = 06/16/21 Pct Recovery = 97% Analysis Date = 06/12/21 Pct Recovery = 97% Analysis Date = 06/12/21 Pct Recovery = 97% Analysis Date = 06/07/21 Pct Recovery = 97% Analysis Date = 06/07/21 Pct Recovery = 97% Analysis Date = 06/03/21 Pct Recovery = 97% Analysis Date = 06/03/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 97% Analysis Date = 05/22/21 Pct Recovery = 97% Analysis Date = 05/22/21 Pct Recovery = 97% Analysis Date = 05/18/21 Pct Recovery = 97% Analysis Date = 05/18/21 Pct Recovery = 97% Analysis Date = 05/14/21 Pct Recovery = 97% Analysis Date = 05/14/21 Pct Recovery = 97% Analysis Date = 05/10/21 Pct Recovery = 97% Analysis Date = 05/10/21 Pct Recovery = 97% Analysis Date = 05/06/21 Pct Recovery = 97% Analysis Date = 05/06/21 Pct Recovery = 97% Analysis Date = 05/02/21 Pct Recovery = 98% Analysis Date = 05/02/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/23/21 Pct Recovery = 98% Analysis Date = 04/23/21 Pct Recovery = 98% Analysis Date = 04/19/21 Pct Recovery = 98% Analysis Date = 04/19/21 Pct Recovery = 98% Analysis Date = 04/15/21 Pct Recovery = 98% Analysis Date = 04/15/21 Pct Recovery = 98% Analysis Date = 04/11/21 Pct Recovery = 98% Analysis Date = 04/11/21 Pct Recovery = 98% Analysis Date = 04/07/21 Pct Recovery = 98% Analysis Date = 04/07/21 Pct Recovery = 98% Analysis Date = 04/03/21 Pct Recovery = 98% Analysis Date = 04/03/21 Pct Recovery = 98% Analysis Date = 03/30/21 Pct Recovery = 98% Analysis Date = 03/30/21 Pct Recovery = 98% Analysis Date = 03/26/21 Pct Recovery = 98% Analysis Date = 03/26/21 Pct Recovery = 98% Analysis Date = 03/22/21 Pct Recovery = 98% Analysis Date = 03/22/21 Pct Recovery = 98% Analysis Date = 03/18/21 Pct Recovery = 98% Analysis Date = 03/18/21 Pct Recovery = 98% Analysis Date = 03/13/21 Pct Recovery = 99% Analysis Date = 03/13/21 Pct Recovery = 99% Analysis Date = 03/09/21 Pct Recovery = 99% Analysis Date = 03/09/21 Pct Recovery = 99% Analysis Date = 03/05/21 Pct Recovery = 100% Analysis Date = 03/05/21 Pct Recovery = 100% Analysis Date = 03/01/21 Pct Recovery = 100% Analysis Date = 03/01/21 Pct Recovery = 100% Analysis Date = 02/25/21 Pct Recovery = 101% Analysis Date = 02/25/21 Pct Recovery = 101% Analysis Date = 02/21/21 Pct Recovery = 101% Analysis Date = 02/21/21 Pct Recovery = 101% Analysis Date = 02/17/21 Pct Recovery = 102% Analysis Date = 02/17/21 Pct Recovery = 102% Analysis Date = 02/13/21 Pct Recovery = 102% Analysis Date = 02/13/21 Pct Recovery = 102% Analysis Date = 02/09/21 Pct Recovery = 102% Analysis Date = 02/09/21 Pct Recovery = 102% Analysis Date = 02/05/21 Pct Recovery = 103% Analysis Date = 02/05/21 Pct Recovery = 103% Analysis Date = 01/31/21 Pct Recovery = 103% Analysis Date = 01/31/21 Pct Recovery = 103% Analysis Date = 01/27/21 Pct Recovery = 104% Analysis Date = 01/27/21 Pct Recovery = 104% Analysis Date = 01/23/21 Pct Recovery = 104% Analysis Date = 01/23/21 Pct Recovery = 104% Analysis Date = 01/19/21 Pct Recovery = 105% Analysis Date = 01/19/21 Pct Recovery = 105% Analysis Date = 01/15/21 Pct Recovery = 105% Analysis Date = 01/15/21 Pct Recovery = 105% Analysis Date = 01/11/21 Pct Recovery = 106% Analysis Date = 01/11/21 Pct Recovery = 106% Analysis Date = 01/07/21 Pct Recovery = 106% Analysis Date = 01/07/21 Pct Recovery = 106% Analysis Date = 01/03/21 Pct Recovery = 107% Analysis Date = 01/03/21 Pct Recovery = 107% Analysis Date = 12/30/20 Pct Recovery = 107% Analysis Date = 12/30/20 Pct Recovery = 107% Analysis Date = 12/26/20 Pct Recovery = 108% Analysis Date = 12/26/20 Pct Recovery = 108% Analysis Date = 12/22/20 Pct Recovery = 108% Analysis Date = 12/22/20 Pct Recovery = 108% Analysis Date = 12/17/20 Pct Recovery = 109% Analysis Date = 12/17/20 Pct Recovery = 109% Analysis Date = 12/13/20 Pct Recovery = 109% Analysis Date = 12/13/20 Pct Recovery = 109% Analysis Date = 12/09/20 Pct Recovery = 110% Analysis Date = 12/09/20 Pct Recovery = 110% Analysis Date = 12/05/20 Pct Recovery = 110% Analysis Date = 12/05/20 Pct Recovery = 110% Analysis Date = 12/01/20 Pct Recovery = 111% Analysis Date = 12/01/20 Pct Recovery = 111% Analysis Date = 11/27/20 Pct Recovery = 111% Analysis Date = 11/27/20 Pct Recovery = 111% Analysis Date = 11/23/20 Pct Recovery = 112% Analysis Date = 11/23/20 Pct Recovery = 112% Analysis Date = 11/19/20 Pct Recovery = 112% Analysis Date = 11/19/20 Pct Recovery = 112% Analysis Date = 11/15/20 Pct Recovery = 113% Analysis Date = 11/15/20 Pct Recovery = 113% Analysis Date = 11/11/20 Pct Recovery = 114% Analysis Date = 11/11/20 Pct Recovery = 114% Analysis Date = 11/06/20 Pct Recovery = 114% Analysis Date = 11/06/20 Pct Recovery = 114% Analysis Date = 11/02/20 Pct Recovery = 115% Analysis Date = 11/02/20 Pct Recovery = 115% Analysis Date = 10/29/20 Pct Recovery = 115% Analysis Date = 10/29/20 Pct Recovery = 115% Analysis Date = 10/25/20 Pct Recovery = 116% Analysis Date = 10/25/20 Pct Recovery = 116% Analysis Date = 10/21/20 Pct Recovery = 116% Analysis Date = 10/21/20 Pct Recovery = 116% Analysis Date = 10/17/20 Pct Recovery = 117% Analysis Date = 10/17/20 Pct Recovery = 117% Analysis Date = 10/13/20 Pct Recovery = 117% Analysis Date = 10/13/20 Pct Recovery = 117% Analysis Date = 10/09/20 Pct Recovery = 118% Analysis Date = 10/09/20 Pct Recovery = 118% Analysis Date = 10/05/20 Pct Recovery = 118% Analysis Date = 10/05/20 Pct Recovery = 118% Analysis Date = 10/01/20 Pct Recovery = 119% Analysis Date = 10/01/20 Pct Recovery = 119% Analysis Date = 09/27/20 Pct Recovery = 119% Analysis Date = 09/27/20 Pct Recovery = 119% Analysis Date = 09/22/20 Pct Recovery = 120% Analysis Date = 09/22/20 Pct Recovery = 120% Analysis Date = 09/18/20 Pct Recovery = 120% Analysis Date = 09/18/20 Pct Recovery = 120% Analysis Date = 09/14/20 Pct Recovery = 120% Analysis Date = 09/14/20 Pct Recovery = 120% Analysis Date = 09/10/20 Pct Recovery = 121% Analysis Date = 09/10/20 Pct Recovery = 121% Analysis Date = 09/06/20 Pct Recovery = 121% Analysis Date = 09/06/20 Pct Recovery = 121% Analysis Date = 09/02/20 Pct Recovery = 121% Analysis Date = 09/02/20 Pct Recovery = 121% Analysis Date = 08/29/20 Pct Recovery = 121% Analysis Date = 08/29/20 Pct Recovery = 121% Analysis Date = 08/25/20 Pct Recovery = 121% Analysis Date = 08/25/20 Pct Recovery = 121% Analysis Date = 08/21/20 Pct Recovery = 121% Analysis Date = 08/21/20 Pct Recovery = 121% Analysis Date = 08/17/20 Pct Recovery = 121% Analysis Date = 08/17/20 Pct Recovery = 121% Analysis Date = 08/12/20 Pct Recovery = 121% Analysis Date = 08/12/20 Pct Recovery = 121% Analysis Date = 08/08/20 Pct Recovery = 122% Analysis Date = 08/08/20 Pct Recovery = 122% Analysis Date = 08/04/20 Pct Recovery = 122% Analysis Date = 08/04/20 Pct Recovery = 122% Analysis Date = 07/31/20 Pct Recovery = 122% Analysis Date = 07/31/20 Pct Recovery = 122% Analysis Date = 07/27/20 Pct Recovery = 122% Analysis Date = 07/27/20 Pct Recovery = 122% Analysis Date = 07/23/20 Pct Recovery = 122% Analysis Date = 07/23/20 Pct Recovery = 122% Analysis Date = 07/19/20 Pct Recovery = 122% Analysis Date = 07/19/20 Pct Recovery = 122% Analysis Date = 07/15/20 Pct Recovery = 122% Analysis Date = 07/15/20 Pct Recovery = 122% Analysis Date = 07/11/20 Pct Recovery = 122% Analysis Date = 07/11/20 Pct Recovery = 122% Analysis Date = 07/07/20 Pct Recovery = 122% Analysis Date = 07/07/20 Pct Recovery = 122% Analysis Date = 07/03/20 Pct Recovery = 122% Analysis Date = 07/03/20 Pct Recovery = 122% Analysis Date = 06/28/20 Pct Recovery = 122% Analysis Date = 06/28/20 Pct Recovery = 122% Analysis Date = 06/24/20 Pct Recovery = 122% Analysis Date = 06/24/20 Pct Recovery = 122% Analysis Date = 06/20/20 Pct Recovery = 123% Analysis Date = 06/20/20 Pct Recovery = 123% Analysis Date = 06/16/20 Pct Recovery = 123% Analysis Date = 06/16/20 Pct Recovery = 123% Analysis Date = 06/12/20 Pct Recovery = 123% Analysis Date = 06/12/20 Pct Recovery = 123% Analysis Date = 06/08/20 Pct Recovery = 123% Analysis Date = 06/08/20 Pct Recovery = 123% Analysis Date = 06/04/20 Pct Recovery = 123% Analysis Date = 06/04/20 Pct Recovery = 123% Analysis Date = 05/31/20 Pct Recovery = 123% Analysis Date = 05/31/20 Pct Recovery = 123% Analysis Date = 05/27/20 Pct Recovery = 123% Analysis Date = 05/27/20 Pct Recovery = 123% Analysis Date = 05/23/20 Pct Recovery = 123% Analysis Date = 05/23/20 Pct Recovery = 123% Analysis Date = 05/19/20 Pct Recovery = 123% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHAMIDOPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 36 108% 22% 109% 21%
Total 36 108% 22% 109% 21%

Sample Statistics
METHAMIDOPHOS

Characteristic N % % Basis
Plotted 36 100% Spiked
Estimated Values 5 14% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 36 .  
False Negatives 0 0% 0 out of 36
Not Spiked 80 .  
False Positives 0 0% 0 out of 80

OBSP Determination:
METHOMYL
METHOD: 2447 , TESTIDCODE: 68645LCM60

Laboratory ID = 20213200091 Lab Value = 45.975 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 244% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202110006 Lab Value = 34.637 Expected Conc. = 37.9 Report level label = 3 Pct Recovery = 91% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203230021 Lab Value = 29.741 Expected Conc. = 37.51 Report level label = 3 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 32.169 Expected Conc. = 37.51 Report level label = 3 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 29.795 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 80% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 34.531 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 93% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201820155 Lab Value = 58.043 Expected Conc. = 36.5 Report level label = 3 Pct Recovery = 159% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20220190116 Lab Value = 21.335 Expected Conc. = 30.32 Report level label = 3 Pct Recovery = 70% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 19.918 Expected Conc. = 30.32 Report level label = 3 Pct Recovery = 66% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 14.726 Expected Conc. = 30.24 Report level label = 3 Pct Recovery = 49% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220810134 Lab Value = 26.583 Expected Conc. = 30.16 Report level label = 3 Pct Recovery = 88% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20212990174 Lab Value = 20.989 Expected Conc. = 30.16 Report level label = 3 Pct Recovery = 70% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 19.932 Expected Conc. = 30 Report level label = 3 Pct Recovery = 66% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20221730293 Lab Value = 11.320 Expected Conc. = 18.95 Report level label = 3 Pct Recovery = 60% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 13.866 Expected Conc. = 18.95 Report level label = 3 Pct Recovery = 73% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20201680155 Lab Value = 18.754 Expected Conc. = 18.95 Report level label = 3 Pct Recovery = 99% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20220810133 Lab Value = 15.086 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 80% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20213340027 Lab Value = 10.453 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 55% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 14.046 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 75% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20203230018 Lab Value = 18.373 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 99% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 14.700 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 79% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 12.078 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 65% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 22.453 Expected Conc. = 18.25 Report level label = 3 Pct Recovery = 123% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 28.673 Expected Conc. = 18.25 Report level label = 3 Pct Recovery = 157% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 24.835 Expected Conc. = 18.25 Report level label = 3 Pct Recovery = 136% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20222500483 Lab Value = 7.313 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 96% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 6.163 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 81% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20201610160 Lab Value = 9.309 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 123% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20213060210 Lab Value = 3.740 Expected Conc. = 7.54 Report level label = 3 Pct Recovery = 50% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210830019 Lab Value = 8.519 Expected Conc. = 7.502 Report level label = 3 Pct Recovery = 114% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 6.495 Expected Conc. = 7.502 Report level label = 3 Pct Recovery = 87% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 6.880 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 93% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 6.579 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 89% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 6.668 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 90% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 5.538 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 75% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 4.157 Expected Conc. = 7.3 Report level label = 3 Pct Recovery = 57% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 13.923 Expected Conc. = 7.3 Report level label = 3 Pct Recovery = 191% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 9.255 Expected Conc. = 7.3 Report level label = 3 Pct Recovery = 127% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 9.188 Expected Conc. = 7.3 Report level label = 3 Pct Recovery = 126% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Analysis Date = 09/20/22 Pct Recovery = 66% Analysis Date = 09/15/22 Pct Recovery = 67% Analysis Date = 09/15/22 Pct Recovery = 67% Analysis Date = 09/11/22 Pct Recovery = 67% Analysis Date = 09/11/22 Pct Recovery = 67% Analysis Date = 09/07/22 Pct Recovery = 67% Analysis Date = 09/07/22 Pct Recovery = 67% Analysis Date = 09/02/22 Pct Recovery = 68% Analysis Date = 09/02/22 Pct Recovery = 68% Analysis Date = 08/29/22 Pct Recovery = 68% Analysis Date = 08/29/22 Pct Recovery = 68% Analysis Date = 08/25/22 Pct Recovery = 68% Analysis Date = 08/25/22 Pct Recovery = 68% Analysis Date = 08/21/22 Pct Recovery = 68% Analysis Date = 08/21/22 Pct Recovery = 68% Analysis Date = 08/16/22 Pct Recovery = 69% Analysis Date = 08/16/22 Pct Recovery = 69% Analysis Date = 08/12/22 Pct Recovery = 69% Analysis Date = 08/12/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/04/22 Pct Recovery = 70% Analysis Date = 08/04/22 Pct Recovery = 70% Analysis Date = 07/30/22 Pct Recovery = 70% Analysis Date = 07/30/22 Pct Recovery = 70% Analysis Date = 07/26/22 Pct Recovery = 70% Analysis Date = 07/26/22 Pct Recovery = 70% Analysis Date = 07/22/22 Pct Recovery = 71% Analysis Date = 07/22/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 72% Analysis Date = 07/09/22 Pct Recovery = 72% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/30/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/22/22 Pct Recovery = 73% Analysis Date = 06/22/22 Pct Recovery = 73% Analysis Date = 06/18/22 Pct Recovery = 73% Analysis Date = 06/18/22 Pct Recovery = 73% Analysis Date = 06/13/22 Pct Recovery = 73% Analysis Date = 06/13/22 Pct Recovery = 73% Analysis Date = 06/09/22 Pct Recovery = 74% Analysis Date = 06/09/22 Pct Recovery = 74% Analysis Date = 06/05/22 Pct Recovery = 74% Analysis Date = 06/05/22 Pct Recovery = 74% Analysis Date = 05/31/22 Pct Recovery = 74% Analysis Date = 05/31/22 Pct Recovery = 74% Analysis Date = 05/27/22 Pct Recovery = 75% Analysis Date = 05/27/22 Pct Recovery = 75% Analysis Date = 05/23/22 Pct Recovery = 75% Analysis Date = 05/23/22 Pct Recovery = 75% Analysis Date = 05/19/22 Pct Recovery = 75% Analysis Date = 05/19/22 Pct Recovery = 75% Analysis Date = 05/14/22 Pct Recovery = 76% Analysis Date = 05/14/22 Pct Recovery = 76% Analysis Date = 05/10/22 Pct Recovery = 76% Analysis Date = 05/10/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 04/27/22 Pct Recovery = 77% Analysis Date = 04/27/22 Pct Recovery = 77% Analysis Date = 04/23/22 Pct Recovery = 77% Analysis Date = 04/23/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/15/22 Pct Recovery = 78% Analysis Date = 04/15/22 Pct Recovery = 78% Analysis Date = 04/10/22 Pct Recovery = 78% Analysis Date = 04/10/22 Pct Recovery = 78% Analysis Date = 04/06/22 Pct Recovery = 78% Analysis Date = 04/06/22 Pct Recovery = 78% Analysis Date = 04/02/22 Pct Recovery = 79% Analysis Date = 04/02/22 Pct Recovery = 79% Analysis Date = 03/28/22 Pct Recovery = 79% Analysis Date = 03/28/22 Pct Recovery = 79% Analysis Date = 03/24/22 Pct Recovery = 79% Analysis Date = 03/24/22 Pct Recovery = 79% Analysis Date = 03/20/22 Pct Recovery = 79% Analysis Date = 03/20/22 Pct Recovery = 79% Analysis Date = 03/16/22 Pct Recovery = 80% Analysis Date = 03/16/22 Pct Recovery = 80% Analysis Date = 03/11/22 Pct Recovery = 80% Analysis Date = 03/11/22 Pct Recovery = 80% Analysis Date = 03/07/22 Pct Recovery = 80% Analysis Date = 03/07/22 Pct Recovery = 80% Analysis Date = 03/03/22 Pct Recovery = 81% Analysis Date = 03/03/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/27/22 Pct Recovery = 81% Analysis Date = 02/22/22 Pct Recovery = 81% Analysis Date = 02/22/22 Pct Recovery = 81% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/09/22 Pct Recovery = 82% Analysis Date = 02/09/22 Pct Recovery = 82% Analysis Date = 02/05/22 Pct Recovery = 83% Analysis Date = 02/05/22 Pct Recovery = 83% Analysis Date = 02/01/22 Pct Recovery = 83% Analysis Date = 02/01/22 Pct Recovery = 83% Analysis Date = 01/28/22 Pct Recovery = 83% Analysis Date = 01/28/22 Pct Recovery = 83% Analysis Date = 01/23/22 Pct Recovery = 83% Analysis Date = 01/23/22 Pct Recovery = 83% Analysis Date = 01/19/22 Pct Recovery = 84% Analysis Date = 01/19/22 Pct Recovery = 84% Analysis Date = 01/15/22 Pct Recovery = 84% Analysis Date = 01/15/22 Pct Recovery = 84% Analysis Date = 01/11/22 Pct Recovery = 84% Analysis Date = 01/11/22 Pct Recovery = 84% Analysis Date = 01/06/22 Pct Recovery = 85% Analysis Date = 01/06/22 Pct Recovery = 85% Analysis Date = 01/02/22 Pct Recovery = 85% Analysis Date = 01/02/22 Pct Recovery = 85% Analysis Date = 12/29/21 Pct Recovery = 85% Analysis Date = 12/29/21 Pct Recovery = 85% Analysis Date = 12/24/21 Pct Recovery = 86% Analysis Date = 12/24/21 Pct Recovery = 86% Analysis Date = 12/20/21 Pct Recovery = 86% Analysis Date = 12/20/21 Pct Recovery = 86% Analysis Date = 12/16/21 Pct Recovery = 86% Analysis Date = 12/16/21 Pct Recovery = 86% Analysis Date = 12/12/21 Pct Recovery = 87% Analysis Date = 12/12/21 Pct Recovery = 87% Analysis Date = 12/07/21 Pct Recovery = 87% Analysis Date = 12/07/21 Pct Recovery = 87% Analysis Date = 12/03/21 Pct Recovery = 87% Analysis Date = 12/03/21 Pct Recovery = 87% Analysis Date = 11/29/21 Pct Recovery = 88% Analysis Date = 11/29/21 Pct Recovery = 88% Analysis Date = 11/25/21 Pct Recovery = 88% Analysis Date = 11/25/21 Pct Recovery = 88% Analysis Date = 11/20/21 Pct Recovery = 88% Analysis Date = 11/20/21 Pct Recovery = 88% Analysis Date = 11/16/21 Pct Recovery = 89% Analysis Date = 11/16/21 Pct Recovery = 89% Analysis Date = 11/12/21 Pct Recovery = 89% Analysis Date = 11/12/21 Pct Recovery = 89% Analysis Date = 11/08/21 Pct Recovery = 89% Analysis Date = 11/08/21 Pct Recovery = 89% Analysis Date = 11/03/21 Pct Recovery = 89% Analysis Date = 11/03/21 Pct Recovery = 89% Analysis Date = 10/30/21 Pct Recovery = 89% Analysis Date = 10/30/21 Pct Recovery = 89% Analysis Date = 10/26/21 Pct Recovery = 90% Analysis Date = 10/26/21 Pct Recovery = 90% Analysis Date = 10/21/21 Pct Recovery = 90% Analysis Date = 10/21/21 Pct Recovery = 90% Analysis Date = 10/17/21 Pct Recovery = 90% Analysis Date = 10/17/21 Pct Recovery = 90% Analysis Date = 10/13/21 Pct Recovery = 90% Analysis Date = 10/13/21 Pct Recovery = 90% Analysis Date = 10/09/21 Pct Recovery = 90% Analysis Date = 10/09/21 Pct Recovery = 90% Analysis Date = 10/04/21 Pct Recovery = 90% Analysis Date = 10/04/21 Pct Recovery = 90% Analysis Date = 09/30/21 Pct Recovery = 90% Analysis Date = 09/30/21 Pct Recovery = 90% Analysis Date = 09/26/21 Pct Recovery = 90% Analysis Date = 09/26/21 Pct Recovery = 90% Analysis Date = 09/22/21 Pct Recovery = 90% Analysis Date = 09/22/21 Pct Recovery = 90% Analysis Date = 09/17/21 Pct Recovery = 90% Analysis Date = 09/17/21 Pct Recovery = 90% Analysis Date = 09/13/21 Pct Recovery = 90% Analysis Date = 09/13/21 Pct Recovery = 90% Analysis Date = 09/09/21 Pct Recovery = 90% Analysis Date = 09/09/21 Pct Recovery = 90% Analysis Date = 09/04/21 Pct Recovery = 91% Analysis Date = 09/04/21 Pct Recovery = 91% Analysis Date = 08/31/21 Pct Recovery = 91% Analysis Date = 08/31/21 Pct Recovery = 91% Analysis Date = 08/27/21 Pct Recovery = 91% Analysis Date = 08/27/21 Pct Recovery = 91% Analysis Date = 08/23/21 Pct Recovery = 91% Analysis Date = 08/23/21 Pct Recovery = 91% Analysis Date = 08/18/21 Pct Recovery = 91% Analysis Date = 08/18/21 Pct Recovery = 91% Analysis Date = 08/14/21 Pct Recovery = 91% Analysis Date = 08/14/21 Pct Recovery = 91% Analysis Date = 08/10/21 Pct Recovery = 91% Analysis Date = 08/10/21 Pct Recovery = 91% Analysis Date = 08/06/21 Pct Recovery = 91% Analysis Date = 08/06/21 Pct Recovery = 91% Analysis Date = 08/01/21 Pct Recovery = 91% Analysis Date = 08/01/21 Pct Recovery = 91% Analysis Date = 07/28/21 Pct Recovery = 91% Analysis Date = 07/28/21 Pct Recovery = 91% Analysis Date = 07/24/21 Pct Recovery = 91% Analysis Date = 07/24/21 Pct Recovery = 91% Analysis Date = 07/20/21 Pct Recovery = 91% Analysis Date = 07/20/21 Pct Recovery = 91% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/02/21 Pct Recovery = 92% Analysis Date = 07/02/21 Pct Recovery = 92% Analysis Date = 06/28/21 Pct Recovery = 92% Analysis Date = 06/28/21 Pct Recovery = 92% Analysis Date = 06/24/21 Pct Recovery = 92% Analysis Date = 06/24/21 Pct Recovery = 92% Analysis Date = 06/20/21 Pct Recovery = 92% Analysis Date = 06/20/21 Pct Recovery = 92% Analysis Date = 06/15/21 Pct Recovery = 92% Analysis Date = 06/15/21 Pct Recovery = 92% Analysis Date = 06/11/21 Pct Recovery = 92% Analysis Date = 06/11/21 Pct Recovery = 92% Analysis Date = 06/07/21 Pct Recovery = 92% Analysis Date = 06/07/21 Pct Recovery = 92% Analysis Date = 06/03/21 Pct Recovery = 92% Analysis Date = 06/03/21 Pct Recovery = 92% Analysis Date = 05/29/21 Pct Recovery = 92% Analysis Date = 05/29/21 Pct Recovery = 92% Analysis Date = 05/25/21 Pct Recovery = 93% Analysis Date = 05/25/21 Pct Recovery = 93% Analysis Date = 05/21/21 Pct Recovery = 93% Analysis Date = 05/21/21 Pct Recovery = 93% Analysis Date = 05/16/21 Pct Recovery = 93% Analysis Date = 05/16/21 Pct Recovery = 93% Analysis Date = 05/12/21 Pct Recovery = 93% Analysis Date = 05/12/21 Pct Recovery = 93% Analysis Date = 05/08/21 Pct Recovery = 93% Analysis Date = 05/08/21 Pct Recovery = 93% Analysis Date = 05/04/21 Pct Recovery = 93% Analysis Date = 05/04/21 Pct Recovery = 93% Analysis Date = 04/29/21 Pct Recovery = 93% Analysis Date = 04/29/21 Pct Recovery = 93% Analysis Date = 04/25/21 Pct Recovery = 93% Analysis Date = 04/25/21 Pct Recovery = 93% Analysis Date = 04/21/21 Pct Recovery = 93% Analysis Date = 04/21/21 Pct Recovery = 93% Analysis Date = 04/17/21 Pct Recovery = 93% Analysis Date = 04/17/21 Pct Recovery = 93% Analysis Date = 04/12/21 Pct Recovery = 93% Analysis Date = 04/12/21 Pct Recovery = 93% Analysis Date = 04/08/21 Pct Recovery = 93% Analysis Date = 04/08/21 Pct Recovery = 93% Analysis Date = 04/04/21 Pct Recovery = 93% Analysis Date = 04/04/21 Pct Recovery = 93% Analysis Date = 03/30/21 Pct Recovery = 94% Analysis Date = 03/30/21 Pct Recovery = 94% Analysis Date = 03/26/21 Pct Recovery = 93% Analysis Date = 03/26/21 Pct Recovery = 93% Analysis Date = 03/22/21 Pct Recovery = 93% Analysis Date = 03/22/21 Pct Recovery = 93% Analysis Date = 03/18/21 Pct Recovery = 93% Analysis Date = 03/18/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 92% Analysis Date = 03/09/21 Pct Recovery = 92% Analysis Date = 03/05/21 Pct Recovery = 92% Analysis Date = 03/05/21 Pct Recovery = 92% Analysis Date = 03/01/21 Pct Recovery = 92% Analysis Date = 03/01/21 Pct Recovery = 92% Analysis Date = 02/24/21 Pct Recovery = 92% Analysis Date = 02/24/21 Pct Recovery = 92% Analysis Date = 02/20/21 Pct Recovery = 91% Analysis Date = 02/20/21 Pct Recovery = 91% Analysis Date = 02/16/21 Pct Recovery = 91% Analysis Date = 02/16/21 Pct Recovery = 91% Analysis Date = 02/12/21 Pct Recovery = 91% Analysis Date = 02/12/21 Pct Recovery = 91% Analysis Date = 02/07/21 Pct Recovery = 90% Analysis Date = 02/07/21 Pct Recovery = 90% Analysis Date = 02/03/21 Pct Recovery = 90% Analysis Date = 02/03/21 Pct Recovery = 90% Analysis Date = 01/30/21 Pct Recovery = 90% Analysis Date = 01/30/21 Pct Recovery = 90% Analysis Date = 01/25/21 Pct Recovery = 90% Analysis Date = 01/25/21 Pct Recovery = 90% Analysis Date = 01/21/21 Pct Recovery = 90% Analysis Date = 01/21/21 Pct Recovery = 90% Analysis Date = 01/17/21 Pct Recovery = 91% Analysis Date = 01/17/21 Pct Recovery = 91% Analysis Date = 01/13/21 Pct Recovery = 91% Analysis Date = 01/13/21 Pct Recovery = 91% Analysis Date = 01/08/21 Pct Recovery = 91% Analysis Date = 01/08/21 Pct Recovery = 91% Analysis Date = 01/04/21 Pct Recovery = 91% Analysis Date = 01/04/21 Pct Recovery = 91% Analysis Date = 12/31/20 Pct Recovery = 91% Analysis Date = 12/31/20 Pct Recovery = 91% Analysis Date = 12/27/20 Pct Recovery = 92% Analysis Date = 12/27/20 Pct Recovery = 92% Analysis Date = 12/22/20 Pct Recovery = 92% Analysis Date = 12/22/20 Pct Recovery = 92% Analysis Date = 12/18/20 Pct Recovery = 92% Analysis Date = 12/18/20 Pct Recovery = 92% Analysis Date = 12/14/20 Pct Recovery = 92% Analysis Date = 12/14/20 Pct Recovery = 92% Analysis Date = 12/09/20 Pct Recovery = 93% Analysis Date = 12/09/20 Pct Recovery = 93% Analysis Date = 12/05/20 Pct Recovery = 93% Analysis Date = 12/05/20 Pct Recovery = 93% Analysis Date = 12/01/20 Pct Recovery = 93% Analysis Date = 12/01/20 Pct Recovery = 93% Analysis Date = 11/27/20 Pct Recovery = 93% Analysis Date = 11/27/20 Pct Recovery = 93% Analysis Date = 11/22/20 Pct Recovery = 93% Analysis Date = 11/22/20 Pct Recovery = 93% Analysis Date = 11/18/20 Pct Recovery = 94% Analysis Date = 11/18/20 Pct Recovery = 94% Analysis Date = 11/14/20 Pct Recovery = 94% Analysis Date = 11/14/20 Pct Recovery = 94% Analysis Date = 11/10/20 Pct Recovery = 94% Analysis Date = 11/10/20 Pct Recovery = 94% Analysis Date = 11/05/20 Pct Recovery = 94% Analysis Date = 11/05/20 Pct Recovery = 94% Analysis Date = 11/01/20 Pct Recovery = 95% Analysis Date = 11/01/20 Pct Recovery = 95% Analysis Date = 10/28/20 Pct Recovery = 96% Analysis Date = 10/28/20 Pct Recovery = 96% Analysis Date = 10/23/20 Pct Recovery = 97% Analysis Date = 10/23/20 Pct Recovery = 97% Analysis Date = 10/19/20 Pct Recovery = 98% Analysis Date = 10/19/20 Pct Recovery = 98% Analysis Date = 10/15/20 Pct Recovery = 99% Analysis Date = 10/15/20 Pct Recovery = 99% Analysis Date = 10/11/20 Pct Recovery = 100% Analysis Date = 10/11/20 Pct Recovery = 100% Analysis Date = 10/06/20 Pct Recovery = 101% Analysis Date = 10/06/20 Pct Recovery = 101% Analysis Date = 10/02/20 Pct Recovery = 102% Analysis Date = 10/02/20 Pct Recovery = 102% Analysis Date = 09/28/20 Pct Recovery = 103% Analysis Date = 09/28/20 Pct Recovery = 103% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/24/20 Pct Recovery = 104% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/15/20 Pct Recovery = 106% Analysis Date = 09/15/20 Pct Recovery = 106% Analysis Date = 09/11/20 Pct Recovery = 107% Analysis Date = 09/11/20 Pct Recovery = 107% Analysis Date = 09/07/20 Pct Recovery = 109% Analysis Date = 09/07/20 Pct Recovery = 109% Analysis Date = 09/02/20 Pct Recovery = 110% Analysis Date = 09/02/20 Pct Recovery = 110% Analysis Date = 08/29/20 Pct Recovery = 111% Analysis Date = 08/29/20 Pct Recovery = 111% Analysis Date = 08/25/20 Pct Recovery = 112% Analysis Date = 08/25/20 Pct Recovery = 112% Analysis Date = 08/20/20 Pct Recovery = 113% Analysis Date = 08/20/20 Pct Recovery = 113% Analysis Date = 08/16/20 Pct Recovery = 114% Analysis Date = 08/16/20 Pct Recovery = 114% Analysis Date = 08/12/20 Pct Recovery = 115% Analysis Date = 08/12/20 Pct Recovery = 115% Analysis Date = 08/08/20 Pct Recovery = 116% Analysis Date = 08/08/20 Pct Recovery = 116% Analysis Date = 08/03/20 Pct Recovery = 117% Analysis Date = 08/03/20 Pct Recovery = 117% Analysis Date = 07/30/20 Pct Recovery = 119% Analysis Date = 07/30/20 Pct Recovery = 119% Analysis Date = 07/26/20 Pct Recovery = 120% Analysis Date = 07/26/20 Pct Recovery = 120% Analysis Date = 07/22/20 Pct Recovery = 121% Analysis Date = 07/22/20 Pct Recovery = 121% Analysis Date = 07/17/20 Pct Recovery = 122% Analysis Date = 07/17/20 Pct Recovery = 122% Analysis Date = 07/13/20 Pct Recovery = 123% Analysis Date = 07/13/20 Pct Recovery = 123% Analysis Date = 07/09/20 Pct Recovery = 124% Analysis Date = 07/09/20 Pct Recovery = 124% Analysis Date = 07/04/20 Pct Recovery = 126% Analysis Date = 07/04/20 Pct Recovery = 126% Analysis Date = 06/30/20 Pct Recovery = 127% Analysis Date = 06/30/20 Pct Recovery = 127% Analysis Date = 06/26/20 Pct Recovery = 128% Analysis Date = 06/26/20 Pct Recovery = 128% Analysis Date = 06/22/20 Pct Recovery = 129% Analysis Date = 06/22/20 Pct Recovery = 129% Analysis Date = 06/17/20 Pct Recovery = 131% Analysis Date = 06/17/20 Pct Recovery = 131% Analysis Date = 06/13/20 Pct Recovery = 132% Analysis Date = 06/13/20 Pct Recovery = 132% Analysis Date = 06/09/20 Pct Recovery = 133% Analysis Date = 06/09/20 Pct Recovery = 133% Analysis Date = 06/05/20 Pct Recovery = 134% Analysis Date = 06/05/20 Pct Recovery = 134% Analysis Date = 05/31/20 Pct Recovery = 135% Analysis Date = 05/31/20 Pct Recovery = 135% Analysis Date = 05/27/20 Pct Recovery = 137% Analysis Date = 05/27/20 Pct Recovery = 137% Analysis Date = 05/23/20 Pct Recovery = 138% Analysis Date = 05/23/20 Pct Recovery = 138% Analysis Date = 05/19/20 Pct Recovery = 139% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHOMYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 39 96% 40% 87% 32%
Total 39 96% 40% 87% 32%

Sample Statistics
METHOMYL

Characteristic N % % Basis
Plotted 39 93% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 42 .  
False Negatives 2 5% 2 out of 42
Not Spiked 69 .  
False Positives 1 1% 1 out of 69

OBSP Determination:
METHOXYFENOZIDE
METHOD: 2447 , TESTIDCODE: 68647LCM60

Laboratory ID = 20203230021 Lab Value = 20.357 Expected Conc. = 27.47 Report level label = 2.2 Pct Recovery = 74% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 20.156 Expected Conc. = 27.47 Report level label = 2.2 Pct Recovery = 73% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 28.987 Expected Conc. = 27.2 Report level label = 2.2 Pct Recovery = 107% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 27.038 Expected Conc. = 27.2 Report level label = 2.2 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222150192 Lab Value = 18.190 Expected Conc. = 22.28 Report level label = 2.2 Pct Recovery = 82% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 16.464 Expected Conc. = 22 Report level label = 2.2 Pct Recovery = 75% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221520237 Lab Value = 19.515 Expected Conc. = 21.972 Report level label = 2.2 Pct Recovery = 89% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20201550031 Lab Value = 15.110 Expected Conc. = 13.9 Report level label = 2.2 Pct Recovery = 109% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20221870197 Lab Value = 9.861 Expected Conc. = 13.733 Report level label = 2.2 Pct Recovery = 72% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20220740064 Lab Value = 10.205 Expected Conc. = 13.675 Report level label = 2.2 Pct Recovery = 75% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20203230018 Lab Value = 14.164 Expected Conc. = 13.6 Report level label = 2.2 Pct Recovery = 104% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 14.399 Expected Conc. = 13.6 Report level label = 2.2 Pct Recovery = 106% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 15.114 Expected Conc. = 13.6 Report level label = 2.2 Pct Recovery = 111% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 16.152 Expected Conc. = 13.55 Report level label = 2.2 Pct Recovery = 119% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 15.967 Expected Conc. = 13.55 Report level label = 2.2 Pct Recovery = 118% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 13.333 Expected Conc. = 10.84 Report level label = 2.2 Pct Recovery = 123% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 11.322 Expected Conc. = 10.84 Report level label = 2.2 Pct Recovery = 104% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20202330309 Lab Value = 6.073 Expected Conc. = 5.56 Report level label = 2.2 Pct Recovery = 109% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 4.431 Expected Conc. = 5.56 Report level label = 2.2 Pct Recovery = 80% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 7.019 Expected Conc. = 5.56 Report level label = 2.2 Pct Recovery = 126% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 5.107 Expected Conc. = 5.56 Report level label = 2.2 Pct Recovery = 92% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 6.217 Expected Conc. = 5.56 Report level label = 2.2 Pct Recovery = 112% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210830019 Lab Value = 6.493 Expected Conc. = 5.494 Report level label = 2.2 Pct Recovery = 118% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 4.054 Expected Conc. = 5.494 Report level label = 2.2 Pct Recovery = 74% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 5.503 Expected Conc. = 5.44 Report level label = 2.2 Pct Recovery = 101% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 5.181 Expected Conc. = 5.44 Report level label = 2.2 Pct Recovery = 95% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 5.731 Expected Conc. = 5.44 Report level label = 2.2 Pct Recovery = 105% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 5.049 Expected Conc. = 5.44 Report level label = 2.2 Pct Recovery = 93% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 5.446 Expected Conc. = 5.44 Report level label = 2.2 Pct Recovery = 100% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 5.517 Expected Conc. = 5.44 Report level label = 2.2 Pct Recovery = 101% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 08/15/22 Pct Recovery = 77% Analysis Date = 08/10/22 Pct Recovery = 77% Analysis Date = 08/10/22 Pct Recovery = 77% Analysis Date = 08/06/22 Pct Recovery = 77% Analysis Date = 08/06/22 Pct Recovery = 77% Analysis Date = 08/02/22 Pct Recovery = 77% Analysis Date = 08/02/22 Pct Recovery = 77% Analysis Date = 07/29/22 Pct Recovery = 77% Analysis Date = 07/29/22 Pct Recovery = 77% Analysis Date = 07/25/22 Pct Recovery = 78% Analysis Date = 07/25/22 Pct Recovery = 78% Analysis Date = 07/21/22 Pct Recovery = 78% Analysis Date = 07/21/22 Pct Recovery = 78% Analysis Date = 07/17/22 Pct Recovery = 78% Analysis Date = 07/17/22 Pct Recovery = 78% Analysis Date = 07/13/22 Pct Recovery = 78% Analysis Date = 07/13/22 Pct Recovery = 78% Analysis Date = 07/09/22 Pct Recovery = 78% Analysis Date = 07/09/22 Pct Recovery = 78% Analysis Date = 07/05/22 Pct Recovery = 78% Analysis Date = 07/05/22 Pct Recovery = 78% Analysis Date = 07/01/22 Pct Recovery = 78% Analysis Date = 07/01/22 Pct Recovery = 78% Analysis Date = 06/27/22 Pct Recovery = 79% Analysis Date = 06/27/22 Pct Recovery = 79% Analysis Date = 06/23/22 Pct Recovery = 79% Analysis Date = 06/23/22 Pct Recovery = 79% Analysis Date = 06/19/22 Pct Recovery = 79% Analysis Date = 06/19/22 Pct Recovery = 79% Analysis Date = 06/15/22 Pct Recovery = 79% Analysis Date = 06/15/22 Pct Recovery = 79% Analysis Date = 06/11/22 Pct Recovery = 79% Analysis Date = 06/11/22 Pct Recovery = 79% Analysis Date = 06/07/22 Pct Recovery = 79% Analysis Date = 06/07/22 Pct Recovery = 79% Analysis Date = 06/03/22 Pct Recovery = 79% Analysis Date = 06/03/22 Pct Recovery = 79% Analysis Date = 05/30/22 Pct Recovery = 80% Analysis Date = 05/30/22 Pct Recovery = 80% Analysis Date = 05/26/22 Pct Recovery = 80% Analysis Date = 05/26/22 Pct Recovery = 80% Analysis Date = 05/22/22 Pct Recovery = 80% Analysis Date = 05/22/22 Pct Recovery = 80% Analysis Date = 05/18/22 Pct Recovery = 80% Analysis Date = 05/18/22 Pct Recovery = 80% Analysis Date = 05/14/22 Pct Recovery = 80% Analysis Date = 05/14/22 Pct Recovery = 80% Analysis Date = 05/10/22 Pct Recovery = 80% Analysis Date = 05/10/22 Pct Recovery = 80% Analysis Date = 05/06/22 Pct Recovery = 81% Analysis Date = 05/06/22 Pct Recovery = 81% Analysis Date = 05/01/22 Pct Recovery = 81% Analysis Date = 05/01/22 Pct Recovery = 81% Analysis Date = 04/27/22 Pct Recovery = 81% Analysis Date = 04/27/22 Pct Recovery = 81% Analysis Date = 04/23/22 Pct Recovery = 81% Analysis Date = 04/23/22 Pct Recovery = 81% Analysis Date = 04/19/22 Pct Recovery = 81% Analysis Date = 04/19/22 Pct Recovery = 81% Analysis Date = 04/15/22 Pct Recovery = 81% Analysis Date = 04/15/22 Pct Recovery = 81% Analysis Date = 04/11/22 Pct Recovery = 81% Analysis Date = 04/11/22 Pct Recovery = 81% Analysis Date = 04/07/22 Pct Recovery = 82% Analysis Date = 04/07/22 Pct Recovery = 82% Analysis Date = 04/03/22 Pct Recovery = 82% Analysis Date = 04/03/22 Pct Recovery = 82% Analysis Date = 03/30/22 Pct Recovery = 82% Analysis Date = 03/30/22 Pct Recovery = 82% Analysis Date = 03/26/22 Pct Recovery = 82% Analysis Date = 03/26/22 Pct Recovery = 82% Analysis Date = 03/22/22 Pct Recovery = 82% Analysis Date = 03/22/22 Pct Recovery = 82% Analysis Date = 03/18/22 Pct Recovery = 82% Analysis Date = 03/18/22 Pct Recovery = 82% Analysis Date = 03/14/22 Pct Recovery = 83% Analysis Date = 03/14/22 Pct Recovery = 83% Analysis Date = 03/10/22 Pct Recovery = 83% Analysis Date = 03/10/22 Pct Recovery = 83% Analysis Date = 03/06/22 Pct Recovery = 83% Analysis Date = 03/06/22 Pct Recovery = 83% Analysis Date = 03/02/22 Pct Recovery = 83% Analysis Date = 03/02/22 Pct Recovery = 83% Analysis Date = 02/26/22 Pct Recovery = 83% Analysis Date = 02/26/22 Pct Recovery = 83% Analysis Date = 02/22/22 Pct Recovery = 83% Analysis Date = 02/22/22 Pct Recovery = 83% Analysis Date = 02/18/22 Pct Recovery = 84% Analysis Date = 02/18/22 Pct Recovery = 84% Analysis Date = 02/14/22 Pct Recovery = 84% Analysis Date = 02/14/22 Pct Recovery = 84% Analysis Date = 02/10/22 Pct Recovery = 84% Analysis Date = 02/10/22 Pct Recovery = 84% Analysis Date = 02/06/22 Pct Recovery = 84% Analysis Date = 02/06/22 Pct Recovery = 84% Analysis Date = 02/02/22 Pct Recovery = 84% Analysis Date = 02/02/22 Pct Recovery = 84% Analysis Date = 01/29/22 Pct Recovery = 84% Analysis Date = 01/29/22 Pct Recovery = 84% Analysis Date = 01/25/22 Pct Recovery = 84% Analysis Date = 01/25/22 Pct Recovery = 84% Analysis Date = 01/20/22 Pct Recovery = 85% Analysis Date = 01/20/22 Pct Recovery = 85% Analysis Date = 01/16/22 Pct Recovery = 85% Analysis Date = 01/16/22 Pct Recovery = 85% Analysis Date = 01/12/22 Pct Recovery = 85% Analysis Date = 01/12/22 Pct Recovery = 85% Analysis Date = 01/08/22 Pct Recovery = 85% Analysis Date = 01/08/22 Pct Recovery = 85% Analysis Date = 01/04/22 Pct Recovery = 85% Analysis Date = 01/04/22 Pct Recovery = 85% Analysis Date = 12/31/21 Pct Recovery = 85% Analysis Date = 12/31/21 Pct Recovery = 85% Analysis Date = 12/27/21 Pct Recovery = 86% Analysis Date = 12/27/21 Pct Recovery = 86% Analysis Date = 12/23/21 Pct Recovery = 86% Analysis Date = 12/23/21 Pct Recovery = 86% Analysis Date = 12/19/21 Pct Recovery = 86% Analysis Date = 12/19/21 Pct Recovery = 86% Analysis Date = 12/15/21 Pct Recovery = 86% Analysis Date = 12/15/21 Pct Recovery = 86% Analysis Date = 12/11/21 Pct Recovery = 86% Analysis Date = 12/11/21 Pct Recovery = 86% Analysis Date = 12/07/21 Pct Recovery = 86% Analysis Date = 12/07/21 Pct Recovery = 86% Analysis Date = 12/03/21 Pct Recovery = 87% Analysis Date = 12/03/21 Pct Recovery = 87% Analysis Date = 11/29/21 Pct Recovery = 87% Analysis Date = 11/29/21 Pct Recovery = 87% Analysis Date = 11/25/21 Pct Recovery = 87% Analysis Date = 11/25/21 Pct Recovery = 87% Analysis Date = 11/21/21 Pct Recovery = 87% Analysis Date = 11/21/21 Pct Recovery = 87% Analysis Date = 11/17/21 Pct Recovery = 87% Analysis Date = 11/17/21 Pct Recovery = 87% Analysis Date = 11/13/21 Pct Recovery = 87% Analysis Date = 11/13/21 Pct Recovery = 87% Analysis Date = 11/09/21 Pct Recovery = 87% Analysis Date = 11/09/21 Pct Recovery = 87% Analysis Date = 11/05/21 Pct Recovery = 88% Analysis Date = 11/05/21 Pct Recovery = 88% Analysis Date = 11/01/21 Pct Recovery = 88% Analysis Date = 11/01/21 Pct Recovery = 88% Analysis Date = 10/28/21 Pct Recovery = 88% Analysis Date = 10/28/21 Pct Recovery = 88% Analysis Date = 10/24/21 Pct Recovery = 88% Analysis Date = 10/24/21 Pct Recovery = 88% Analysis Date = 10/20/21 Pct Recovery = 88% Analysis Date = 10/20/21 Pct Recovery = 88% Analysis Date = 10/16/21 Pct Recovery = 88% Analysis Date = 10/16/21 Pct Recovery = 88% Analysis Date = 10/11/21 Pct Recovery = 89% Analysis Date = 10/11/21 Pct Recovery = 89% Analysis Date = 10/07/21 Pct Recovery = 89% Analysis Date = 10/07/21 Pct Recovery = 89% Analysis Date = 10/03/21 Pct Recovery = 89% Analysis Date = 10/03/21 Pct Recovery = 89% Analysis Date = 09/29/21 Pct Recovery = 89% Analysis Date = 09/29/21 Pct Recovery = 89% Analysis Date = 09/25/21 Pct Recovery = 89% Analysis Date = 09/25/21 Pct Recovery = 89% Analysis Date = 09/21/21 Pct Recovery = 89% Analysis Date = 09/21/21 Pct Recovery = 89% Analysis Date = 09/17/21 Pct Recovery = 90% Analysis Date = 09/17/21 Pct Recovery = 90% Analysis Date = 09/13/21 Pct Recovery = 90% Analysis Date = 09/13/21 Pct Recovery = 90% Analysis Date = 09/09/21 Pct Recovery = 90% Analysis Date = 09/09/21 Pct Recovery = 90% Analysis Date = 09/05/21 Pct Recovery = 90% Analysis Date = 09/05/21 Pct Recovery = 90% Analysis Date = 09/01/21 Pct Recovery = 90% Analysis Date = 09/01/21 Pct Recovery = 90% Analysis Date = 08/28/21 Pct Recovery = 90% Analysis Date = 08/28/21 Pct Recovery = 90% Analysis Date = 08/24/21 Pct Recovery = 90% Analysis Date = 08/24/21 Pct Recovery = 90% Analysis Date = 08/20/21 Pct Recovery = 91% Analysis Date = 08/20/21 Pct Recovery = 91% Analysis Date = 08/16/21 Pct Recovery = 91% Analysis Date = 08/16/21 Pct Recovery = 91% Analysis Date = 08/12/21 Pct Recovery = 91% Analysis Date = 08/12/21 Pct Recovery = 91% Analysis Date = 08/08/21 Pct Recovery = 91% Analysis Date = 08/08/21 Pct Recovery = 91% Analysis Date = 08/04/21 Pct Recovery = 91% Analysis Date = 08/04/21 Pct Recovery = 91% Analysis Date = 07/31/21 Pct Recovery = 91% Analysis Date = 07/31/21 Pct Recovery = 91% Analysis Date = 07/27/21 Pct Recovery = 92% Analysis Date = 07/27/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 06/28/21 Pct Recovery = 93% Analysis Date = 06/28/21 Pct Recovery = 93% Analysis Date = 06/24/21 Pct Recovery = 93% Analysis Date = 06/24/21 Pct Recovery = 93% Analysis Date = 06/20/21 Pct Recovery = 93% Analysis Date = 06/20/21 Pct Recovery = 93% Analysis Date = 06/16/21 Pct Recovery = 93% Analysis Date = 06/16/21 Pct Recovery = 93% Analysis Date = 06/12/21 Pct Recovery = 93% Analysis Date = 06/12/21 Pct Recovery = 93% Analysis Date = 06/08/21 Pct Recovery = 93% Analysis Date = 06/08/21 Pct Recovery = 93% Analysis Date = 06/04/21 Pct Recovery = 94% Analysis Date = 06/04/21 Pct Recovery = 94% Analysis Date = 05/31/21 Pct Recovery = 94% Analysis Date = 05/31/21 Pct Recovery = 94% Analysis Date = 05/27/21 Pct Recovery = 94% Analysis Date = 05/27/21 Pct Recovery = 94% Analysis Date = 05/23/21 Pct Recovery = 94% Analysis Date = 05/23/21 Pct Recovery = 94% Analysis Date = 05/19/21 Pct Recovery = 94% Analysis Date = 05/19/21 Pct Recovery = 94% Analysis Date = 05/15/21 Pct Recovery = 94% Analysis Date = 05/15/21 Pct Recovery = 94% Analysis Date = 05/11/21 Pct Recovery = 95% Analysis Date = 05/11/21 Pct Recovery = 95% Analysis Date = 05/07/21 Pct Recovery = 95% Analysis Date = 05/07/21 Pct Recovery = 95% Analysis Date = 05/03/21 Pct Recovery = 95% Analysis Date = 05/03/21 Pct Recovery = 95% Analysis Date = 04/29/21 Pct Recovery = 95% Analysis Date = 04/29/21 Pct Recovery = 95% Analysis Date = 04/25/21 Pct Recovery = 95% Analysis Date = 04/25/21 Pct Recovery = 95% Analysis Date = 04/21/21 Pct Recovery = 95% Analysis Date = 04/21/21 Pct Recovery = 95% Analysis Date = 04/17/21 Pct Recovery = 95% Analysis Date = 04/17/21 Pct Recovery = 95% Analysis Date = 04/13/21 Pct Recovery = 96% Analysis Date = 04/13/21 Pct Recovery = 96% Analysis Date = 04/09/21 Pct Recovery = 96% Analysis Date = 04/09/21 Pct Recovery = 96% Analysis Date = 04/05/21 Pct Recovery = 96% Analysis Date = 04/05/21 Pct Recovery = 96% Analysis Date = 04/01/21 Pct Recovery = 96% Analysis Date = 04/01/21 Pct Recovery = 96% Analysis Date = 03/28/21 Pct Recovery = 95% Analysis Date = 03/28/21 Pct Recovery = 95% Analysis Date = 03/23/21 Pct Recovery = 95% Analysis Date = 03/23/21 Pct Recovery = 95% Analysis Date = 03/19/21 Pct Recovery = 95% Analysis Date = 03/19/21 Pct Recovery = 95% Analysis Date = 03/15/21 Pct Recovery = 95% Analysis Date = 03/15/21 Pct Recovery = 95% Analysis Date = 03/11/21 Pct Recovery = 95% Analysis Date = 03/11/21 Pct Recovery = 95% Analysis Date = 03/07/21 Pct Recovery = 95% Analysis Date = 03/07/21 Pct Recovery = 95% Analysis Date = 03/03/21 Pct Recovery = 95% Analysis Date = 03/03/21 Pct Recovery = 95% Analysis Date = 02/27/21 Pct Recovery = 95% Analysis Date = 02/27/21 Pct Recovery = 95% Analysis Date = 02/23/21 Pct Recovery = 95% Analysis Date = 02/23/21 Pct Recovery = 95% Analysis Date = 02/19/21 Pct Recovery = 95% Analysis Date = 02/19/21 Pct Recovery = 95% Analysis Date = 02/15/21 Pct Recovery = 95% Analysis Date = 02/15/21 Pct Recovery = 95% Analysis Date = 02/11/21 Pct Recovery = 95% Analysis Date = 02/11/21 Pct Recovery = 95% Analysis Date = 02/07/21 Pct Recovery = 95% Analysis Date = 02/07/21 Pct Recovery = 95% Analysis Date = 02/03/21 Pct Recovery = 95% Analysis Date = 02/03/21 Pct Recovery = 95% Analysis Date = 01/30/21 Pct Recovery = 95% Analysis Date = 01/30/21 Pct Recovery = 95% Analysis Date = 01/26/21 Pct Recovery = 95% Analysis Date = 01/26/21 Pct Recovery = 95% Analysis Date = 01/22/21 Pct Recovery = 95% Analysis Date = 01/22/21 Pct Recovery = 95% Analysis Date = 01/18/21 Pct Recovery = 95% Analysis Date = 01/18/21 Pct Recovery = 95% Analysis Date = 01/14/21 Pct Recovery = 95% Analysis Date = 01/14/21 Pct Recovery = 95% Analysis Date = 01/10/21 Pct Recovery = 95% Analysis Date = 01/10/21 Pct Recovery = 95% Analysis Date = 01/06/21 Pct Recovery = 95% Analysis Date = 01/06/21 Pct Recovery = 95% Analysis Date = 01/02/21 Pct Recovery = 96% Analysis Date = 01/02/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/12/20 Pct Recovery = 96% Analysis Date = 12/12/20 Pct Recovery = 96% Analysis Date = 12/08/20 Pct Recovery = 97% Analysis Date = 12/08/20 Pct Recovery = 97% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 12/04/20 Pct Recovery = 97% Analysis Date = 11/30/20 Pct Recovery = 98% Analysis Date = 11/30/20 Pct Recovery = 98% Analysis Date = 11/26/20 Pct Recovery = 99% Analysis Date = 11/26/20 Pct Recovery = 99% Analysis Date = 11/22/20 Pct Recovery = 99% Analysis Date = 11/22/20 Pct Recovery = 99% Analysis Date = 11/18/20 Pct Recovery = 100% Analysis Date = 11/18/20 Pct Recovery = 100% Analysis Date = 11/14/20 Pct Recovery = 101% Analysis Date = 11/14/20 Pct Recovery = 101% Analysis Date = 11/10/20 Pct Recovery = 102% Analysis Date = 11/10/20 Pct Recovery = 102% Analysis Date = 11/06/20 Pct Recovery = 102% Analysis Date = 11/06/20 Pct Recovery = 102% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 11/02/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/29/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/25/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 103% Analysis Date = 10/21/20 Pct Recovery = 103% Analysis Date = 10/17/20 Pct Recovery = 104% Analysis Date = 10/17/20 Pct Recovery = 104% Analysis Date = 10/13/20 Pct Recovery = 104% Analysis Date = 10/13/20 Pct Recovery = 104% Analysis Date = 10/09/20 Pct Recovery = 104% Analysis Date = 10/09/20 Pct Recovery = 104% Analysis Date = 10/05/20 Pct Recovery = 105% Analysis Date = 10/05/20 Pct Recovery = 105% Analysis Date = 10/01/20 Pct Recovery = 105% Analysis Date = 10/01/20 Pct Recovery = 105% Analysis Date = 09/27/20 Pct Recovery = 105% Analysis Date = 09/27/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 106% Analysis Date = 09/19/20 Pct Recovery = 106% Analysis Date = 09/15/20 Pct Recovery = 106% Analysis Date = 09/15/20 Pct Recovery = 106% Analysis Date = 09/11/20 Pct Recovery = 106% Analysis Date = 09/11/20 Pct Recovery = 106% Analysis Date = 09/07/20 Pct Recovery = 106% Analysis Date = 09/07/20 Pct Recovery = 106% Analysis Date = 09/02/20 Pct Recovery = 107% Analysis Date = 09/02/20 Pct Recovery = 107% Analysis Date = 08/29/20 Pct Recovery = 107% Analysis Date = 08/29/20 Pct Recovery = 107% Analysis Date = 08/25/20 Pct Recovery = 107% Analysis Date = 08/25/20 Pct Recovery = 107% Analysis Date = 08/21/20 Pct Recovery = 107% Analysis Date = 08/21/20 Pct Recovery = 107% Analysis Date = 08/17/20 Pct Recovery = 107% Analysis Date = 08/17/20 Pct Recovery = 107% Analysis Date = 08/13/20 Pct Recovery = 107% Analysis Date = 08/13/20 Pct Recovery = 107% Analysis Date = 08/09/20 Pct Recovery = 108% Analysis Date = 08/09/20 Pct Recovery = 108% Analysis Date = 08/05/20 Pct Recovery = 108% Analysis Date = 08/05/20 Pct Recovery = 108% Analysis Date = 08/01/20 Pct Recovery = 108% Analysis Date = 08/01/20 Pct Recovery = 108% Analysis Date = 07/28/20 Pct Recovery = 108% Analysis Date = 07/28/20 Pct Recovery = 108% Analysis Date = 07/24/20 Pct Recovery = 108% Analysis Date = 07/24/20 Pct Recovery = 108% Analysis Date = 07/20/20 Pct Recovery = 108% Analysis Date = 07/20/20 Pct Recovery = 108% Analysis Date = 07/16/20 Pct Recovery = 109% Analysis Date = 07/16/20 Pct Recovery = 109% Analysis Date = 07/12/20 Pct Recovery = 109% Analysis Date = 07/12/20 Pct Recovery = 109% Analysis Date = 07/08/20 Pct Recovery = 109% Analysis Date = 07/08/20 Pct Recovery = 109% Analysis Date = 07/04/20 Pct Recovery = 109% Analysis Date = 07/04/20 Pct Recovery = 109% Analysis Date = 06/30/20 Pct Recovery = 109% Analysis Date = 06/30/20 Pct Recovery = 109% Analysis Date = 06/26/20 Pct Recovery = 109% Analysis Date = 06/26/20 Pct Recovery = 109% Analysis Date = 06/22/20 Pct Recovery = 109% Analysis Date = 06/22/20 Pct Recovery = 109% Analysis Date = 06/18/20 Pct Recovery = 110% Analysis Date = 06/18/20 Pct Recovery = 110% Analysis Date = 06/14/20 Pct Recovery = 110% Analysis Date = 06/14/20 Pct Recovery = 110% Analysis Date = 06/10/20 Pct Recovery = 110% Analysis Date = 06/10/20 Pct Recovery = 110% Analysis Date = 06/06/20 Pct Recovery = 110% Analysis Date = 06/06/20 Pct Recovery = 110% Analysis Date = 06/02/20 Pct Recovery = 110% Analysis Date = 06/02/20 Pct Recovery = 110% Analysis Date = 05/29/20 Pct Recovery = 110% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHOXYFENOZIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 98% 16% 101% 20%
Total 30 98% 16% 101% 20%

Sample Statistics
METHOXYFENOZIDE

Characteristic N % % Basis
Plotted 30 97% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 1 3% 1 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
METOLACHLOR
METHOD: 2447 , TESTIDCODE: 65090LCM60

Laboratory ID = 20201820155 Lab Value = 41.551 Expected Conc. = 40.9 Report level label = 3.2 Pct Recovery = 102% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20202110006 Lab Value = 41.211 Expected Conc. = 40.5 Report level label = 3.2 Pct Recovery = 102% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203080100 Lab Value = 37.631 Expected Conc. = 40.1 Report level label = 3.2 Pct Recovery = 94% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 38.688 Expected Conc. = 40.1 Report level label = 3.2 Pct Recovery = 96% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 40.214 Expected Conc. = 40.1 Report level label = 3.2 Pct Recovery = 100% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 34.978 Expected Conc. = 39.76 Report level label = 3.2 Pct Recovery = 88% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 33.383 Expected Conc. = 39.76 Report level label = 3.2 Pct Recovery = 84% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 36.611 Expected Conc. = 39.76 Report level label = 3.2 Pct Recovery = 92% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 39.038 Expected Conc. = 39.76 Report level label = 3.2 Pct Recovery = 98% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20222150192 Lab Value = 25.775 Expected Conc. = 32.52 Report level label = 3.2 Pct Recovery = 79% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 30.828 Expected Conc. = 32.156 Report level label = 3.2 Pct Recovery = 96% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 25.938 Expected Conc. = 32 Report level label = 3.2 Pct Recovery = 81% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20202530029 Lab Value = 20.941 Expected Conc. = 20.45 Report level label = 3.2 Pct Recovery = 102% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 19.936 Expected Conc. = 20.45 Report level label = 3.2 Pct Recovery = 97% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 17.618 Expected Conc. = 20.45 Report level label = 3.2 Pct Recovery = 86% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20220740064 Lab Value = 13.775 Expected Conc. = 20.325 Report level label = 3.2 Pct Recovery = 68% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20201680155 Lab Value = 20.106 Expected Conc. = 20.25 Report level label = 3.2 Pct Recovery = 99% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20221870197 Lab Value = 14.804 Expected Conc. = 20.098 Report level label = 3.2 Pct Recovery = 74% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20202880004 Lab Value = 21.070 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 105% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210480001 Lab Value = 17.186 Expected Conc. = 19.88 Report level label = 3.2 Pct Recovery = 86% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 16.324 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 102% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 16.360 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 102% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 17.324 Expected Conc. = 15.904 Report level label = 3.2 Pct Recovery = 109% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202330309 Lab Value = 8.234 Expected Conc. = 8.18 Report level label = 3.2 Pct Recovery = 101% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 10.211 Expected Conc. = 8.18 Report level label = 3.2 Pct Recovery = 125% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 6.908 Expected Conc. = 8.18 Report level label = 3.2 Pct Recovery = 84% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 10.725 Expected Conc. = 8.18 Report level label = 3.2 Pct Recovery = 131% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201610160 Lab Value = 8.436 Expected Conc. = 8.1 Report level label = 3.2 Pct Recovery = 104% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20221660151 Lab Value = 6.884 Expected Conc. = 8.039 Report level label = 3.2 Pct Recovery = 86% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20203530076 Lab Value = 8.076 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 101% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 6.339 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 79% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 8.523 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 106% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 6.564 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 82% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210690067 Lab Value = 9.246 Expected Conc. = 7.952 Report level label = 3.2 Pct Recovery = 116% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 08/15/22 Pct Recovery = 79% Analysis Date = 08/10/22 Pct Recovery = 79% Analysis Date = 08/10/22 Pct Recovery = 79% Analysis Date = 08/06/22 Pct Recovery = 80% Analysis Date = 08/06/22 Pct Recovery = 80% Analysis Date = 08/02/22 Pct Recovery = 80% Analysis Date = 08/02/22 Pct Recovery = 80% Analysis Date = 07/29/22 Pct Recovery = 80% Analysis Date = 07/29/22 Pct Recovery = 80% Analysis Date = 07/25/22 Pct Recovery = 80% Analysis Date = 07/25/22 Pct Recovery = 80% Analysis Date = 07/21/22 Pct Recovery = 80% Analysis Date = 07/21/22 Pct Recovery = 80% Analysis Date = 07/17/22 Pct Recovery = 80% Analysis Date = 07/17/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/13/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/09/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 81% Analysis Date = 07/05/22 Pct Recovery = 81% Analysis Date = 07/01/22 Pct Recovery = 81% Analysis Date = 07/01/22 Pct Recovery = 81% Analysis Date = 06/26/22 Pct Recovery = 81% Analysis Date = 06/26/22 Pct Recovery = 81% Analysis Date = 06/22/22 Pct Recovery = 81% Analysis Date = 06/22/22 Pct Recovery = 81% Analysis Date = 06/18/22 Pct Recovery = 81% Analysis Date = 06/18/22 Pct Recovery = 81% Analysis Date = 06/14/22 Pct Recovery = 81% Analysis Date = 06/14/22 Pct Recovery = 81% Analysis Date = 06/10/22 Pct Recovery = 81% Analysis Date = 06/10/22 Pct Recovery = 81% Analysis Date = 06/06/22 Pct Recovery = 82% Analysis Date = 06/06/22 Pct Recovery = 82% Analysis Date = 06/02/22 Pct Recovery = 82% Analysis Date = 06/02/22 Pct Recovery = 82% Analysis Date = 05/29/22 Pct Recovery = 82% Analysis Date = 05/29/22 Pct Recovery = 82% Analysis Date = 05/25/22 Pct Recovery = 82% Analysis Date = 05/25/22 Pct Recovery = 82% Analysis Date = 05/21/22 Pct Recovery = 82% Analysis Date = 05/21/22 Pct Recovery = 82% Analysis Date = 05/17/22 Pct Recovery = 82% Analysis Date = 05/17/22 Pct Recovery = 82% Analysis Date = 05/12/22 Pct Recovery = 83% Analysis Date = 05/12/22 Pct Recovery = 83% Analysis Date = 05/08/22 Pct Recovery = 83% Analysis Date = 05/08/22 Pct Recovery = 83% Analysis Date = 05/04/22 Pct Recovery = 83% Analysis Date = 05/04/22 Pct Recovery = 83% Analysis Date = 04/30/22 Pct Recovery = 83% Analysis Date = 04/30/22 Pct Recovery = 83% Analysis Date = 04/26/22 Pct Recovery = 83% Analysis Date = 04/26/22 Pct Recovery = 83% Analysis Date = 04/22/22 Pct Recovery = 83% Analysis Date = 04/22/22 Pct Recovery = 83% Analysis Date = 04/18/22 Pct Recovery = 84% Analysis Date = 04/18/22 Pct Recovery = 84% Analysis Date = 04/14/22 Pct Recovery = 84% Analysis Date = 04/14/22 Pct Recovery = 84% Analysis Date = 04/10/22 Pct Recovery = 84% Analysis Date = 04/10/22 Pct Recovery = 84% Analysis Date = 04/06/22 Pct Recovery = 84% Analysis Date = 04/06/22 Pct Recovery = 84% Analysis Date = 04/02/22 Pct Recovery = 84% Analysis Date = 04/02/22 Pct Recovery = 84% Analysis Date = 03/28/22 Pct Recovery = 84% Analysis Date = 03/28/22 Pct Recovery = 84% Analysis Date = 03/24/22 Pct Recovery = 85% Analysis Date = 03/24/22 Pct Recovery = 85% Analysis Date = 03/20/22 Pct Recovery = 85% Analysis Date = 03/20/22 Pct Recovery = 85% Analysis Date = 03/16/22 Pct Recovery = 85% Analysis Date = 03/16/22 Pct Recovery = 85% Analysis Date = 03/12/22 Pct Recovery = 85% Analysis Date = 03/12/22 Pct Recovery = 85% Analysis Date = 03/08/22 Pct Recovery = 85% Analysis Date = 03/08/22 Pct Recovery = 85% Analysis Date = 03/04/22 Pct Recovery = 85% Analysis Date = 03/04/22 Pct Recovery = 85% Analysis Date = 02/28/22 Pct Recovery = 86% Analysis Date = 02/28/22 Pct Recovery = 86% Analysis Date = 02/24/22 Pct Recovery = 86% Analysis Date = 02/24/22 Pct Recovery = 86% Analysis Date = 02/20/22 Pct Recovery = 86% Analysis Date = 02/20/22 Pct Recovery = 86% Analysis Date = 02/16/22 Pct Recovery = 86% Analysis Date = 02/16/22 Pct Recovery = 86% Analysis Date = 02/11/22 Pct Recovery = 86% Analysis Date = 02/11/22 Pct Recovery = 86% Analysis Date = 02/07/22 Pct Recovery = 86% Analysis Date = 02/07/22 Pct Recovery = 86% Analysis Date = 02/03/22 Pct Recovery = 87% Analysis Date = 02/03/22 Pct Recovery = 87% Analysis Date = 01/30/22 Pct Recovery = 87% Analysis Date = 01/30/22 Pct Recovery = 87% Analysis Date = 01/26/22 Pct Recovery = 87% Analysis Date = 01/26/22 Pct Recovery = 87% Analysis Date = 01/22/22 Pct Recovery = 87% Analysis Date = 01/22/22 Pct Recovery = 87% Analysis Date = 01/18/22 Pct Recovery = 87% Analysis Date = 01/18/22 Pct Recovery = 87% Analysis Date = 01/14/22 Pct Recovery = 87% Analysis Date = 01/14/22 Pct Recovery = 87% Analysis Date = 01/10/22 Pct Recovery = 87% Analysis Date = 01/10/22 Pct Recovery = 87% Analysis Date = 01/06/22 Pct Recovery = 88% Analysis Date = 01/06/22 Pct Recovery = 88% Analysis Date = 01/02/22 Pct Recovery = 88% Analysis Date = 01/02/22 Pct Recovery = 88% Analysis Date = 12/28/21 Pct Recovery = 88% Analysis Date = 12/28/21 Pct Recovery = 88% Analysis Date = 12/24/21 Pct Recovery = 88% Analysis Date = 12/24/21 Pct Recovery = 88% Analysis Date = 12/20/21 Pct Recovery = 88% Analysis Date = 12/20/21 Pct Recovery = 88% Analysis Date = 12/16/21 Pct Recovery = 88% Analysis Date = 12/16/21 Pct Recovery = 88% Analysis Date = 12/12/21 Pct Recovery = 89% Analysis Date = 12/12/21 Pct Recovery = 89% Analysis Date = 12/08/21 Pct Recovery = 89% Analysis Date = 12/08/21 Pct Recovery = 89% Analysis Date = 12/04/21 Pct Recovery = 89% Analysis Date = 12/04/21 Pct Recovery = 89% Analysis Date = 11/30/21 Pct Recovery = 89% Analysis Date = 11/30/21 Pct Recovery = 89% Analysis Date = 11/26/21 Pct Recovery = 89% Analysis Date = 11/26/21 Pct Recovery = 89% Analysis Date = 11/22/21 Pct Recovery = 89% Analysis Date = 11/22/21 Pct Recovery = 89% Analysis Date = 11/18/21 Pct Recovery = 90% Analysis Date = 11/18/21 Pct Recovery = 90% Analysis Date = 11/13/21 Pct Recovery = 90% Analysis Date = 11/13/21 Pct Recovery = 90% Analysis Date = 11/09/21 Pct Recovery = 90% Analysis Date = 11/09/21 Pct Recovery = 90% Analysis Date = 11/05/21 Pct Recovery = 90% Analysis Date = 11/05/21 Pct Recovery = 90% Analysis Date = 11/01/21 Pct Recovery = 90% Analysis Date = 11/01/21 Pct Recovery = 90% Analysis Date = 10/28/21 Pct Recovery = 90% Analysis Date = 10/28/21 Pct Recovery = 90% Analysis Date = 10/24/21 Pct Recovery = 91% Analysis Date = 10/24/21 Pct Recovery = 91% Analysis Date = 10/20/21 Pct Recovery = 91% Analysis Date = 10/20/21 Pct Recovery = 91% Analysis Date = 10/16/21 Pct Recovery = 91% Analysis Date = 10/16/21 Pct Recovery = 91% Analysis Date = 10/12/21 Pct Recovery = 91% Analysis Date = 10/12/21 Pct Recovery = 91% Analysis Date = 10/08/21 Pct Recovery = 91% Analysis Date = 10/08/21 Pct Recovery = 91% Analysis Date = 10/04/21 Pct Recovery = 91% Analysis Date = 10/04/21 Pct Recovery = 91% Analysis Date = 09/29/21 Pct Recovery = 92% Analysis Date = 09/29/21 Pct Recovery = 92% Analysis Date = 09/25/21 Pct Recovery = 92% Analysis Date = 09/25/21 Pct Recovery = 92% Analysis Date = 09/21/21 Pct Recovery = 92% Analysis Date = 09/21/21 Pct Recovery = 92% Analysis Date = 09/17/21 Pct Recovery = 92% Analysis Date = 09/17/21 Pct Recovery = 92% Analysis Date = 09/13/21 Pct Recovery = 92% Analysis Date = 09/13/21 Pct Recovery = 92% Analysis Date = 09/09/21 Pct Recovery = 92% Analysis Date = 09/09/21 Pct Recovery = 92% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 93% Analysis Date = 08/24/21 Pct Recovery = 93% Analysis Date = 08/24/21 Pct Recovery = 93% Analysis Date = 08/20/21 Pct Recovery = 93% Analysis Date = 08/20/21 Pct Recovery = 93% Analysis Date = 08/15/21 Pct Recovery = 93% Analysis Date = 08/15/21 Pct Recovery = 93% Analysis Date = 08/11/21 Pct Recovery = 94% Analysis Date = 08/11/21 Pct Recovery = 94% Analysis Date = 08/07/21 Pct Recovery = 94% Analysis Date = 08/07/21 Pct Recovery = 94% Analysis Date = 08/03/21 Pct Recovery = 94% Analysis Date = 08/03/21 Pct Recovery = 94% Analysis Date = 07/30/21 Pct Recovery = 94% Analysis Date = 07/30/21 Pct Recovery = 94% Analysis Date = 07/26/21 Pct Recovery = 94% Analysis Date = 07/26/21 Pct Recovery = 94% Analysis Date = 07/22/21 Pct Recovery = 94% Analysis Date = 07/22/21 Pct Recovery = 94% Analysis Date = 07/18/21 Pct Recovery = 95% Analysis Date = 07/18/21 Pct Recovery = 95% Analysis Date = 07/14/21 Pct Recovery = 95% Analysis Date = 07/14/21 Pct Recovery = 95% Analysis Date = 07/10/21 Pct Recovery = 95% Analysis Date = 07/10/21 Pct Recovery = 95% Analysis Date = 07/06/21 Pct Recovery = 95% Analysis Date = 07/06/21 Pct Recovery = 95% Analysis Date = 07/02/21 Pct Recovery = 95% Analysis Date = 07/02/21 Pct Recovery = 95% Analysis Date = 06/27/21 Pct Recovery = 95% Analysis Date = 06/27/21 Pct Recovery = 95% Analysis Date = 06/23/21 Pct Recovery = 96% Analysis Date = 06/23/21 Pct Recovery = 96% Analysis Date = 06/19/21 Pct Recovery = 96% Analysis Date = 06/19/21 Pct Recovery = 96% Analysis Date = 06/15/21 Pct Recovery = 96% Analysis Date = 06/15/21 Pct Recovery = 96% Analysis Date = 06/11/21 Pct Recovery = 96% Analysis Date = 06/11/21 Pct Recovery = 96% Analysis Date = 06/07/21 Pct Recovery = 96% Analysis Date = 06/07/21 Pct Recovery = 96% Analysis Date = 06/03/21 Pct Recovery = 96% Analysis Date = 06/03/21 Pct Recovery = 96% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 97% Analysis Date = 05/22/21 Pct Recovery = 97% Analysis Date = 05/22/21 Pct Recovery = 97% Analysis Date = 05/18/21 Pct Recovery = 97% Analysis Date = 05/18/21 Pct Recovery = 97% Analysis Date = 05/13/21 Pct Recovery = 97% Analysis Date = 05/13/21 Pct Recovery = 97% Analysis Date = 05/09/21 Pct Recovery = 97% Analysis Date = 05/09/21 Pct Recovery = 97% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/01/21 Pct Recovery = 98% Analysis Date = 05/01/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/23/21 Pct Recovery = 98% Analysis Date = 04/23/21 Pct Recovery = 98% Analysis Date = 04/19/21 Pct Recovery = 98% Analysis Date = 04/19/21 Pct Recovery = 98% Analysis Date = 04/15/21 Pct Recovery = 98% Analysis Date = 04/15/21 Pct Recovery = 98% Analysis Date = 04/11/21 Pct Recovery = 99% Analysis Date = 04/11/21 Pct Recovery = 99% Analysis Date = 04/07/21 Pct Recovery = 99% Analysis Date = 04/07/21 Pct Recovery = 99% Analysis Date = 04/03/21 Pct Recovery = 99% Analysis Date = 04/03/21 Pct Recovery = 99% Analysis Date = 03/29/21 Pct Recovery = 99% Analysis Date = 03/29/21 Pct Recovery = 99% Analysis Date = 03/25/21 Pct Recovery = 99% Analysis Date = 03/25/21 Pct Recovery = 99% Analysis Date = 03/21/21 Pct Recovery = 99% Analysis Date = 03/21/21 Pct Recovery = 99% Analysis Date = 03/17/21 Pct Recovery = 99% Analysis Date = 03/17/21 Pct Recovery = 99% Analysis Date = 03/13/21 Pct Recovery = 99% Analysis Date = 03/13/21 Pct Recovery = 99% Analysis Date = 03/09/21 Pct Recovery = 99% Analysis Date = 03/09/21 Pct Recovery = 99% Analysis Date = 03/05/21 Pct Recovery = 99% Analysis Date = 03/05/21 Pct Recovery = 99% Analysis Date = 03/01/21 Pct Recovery = 98% Analysis Date = 03/01/21 Pct Recovery = 98% Analysis Date = 02/25/21 Pct Recovery = 98% Analysis Date = 02/25/21 Pct Recovery = 98% Analysis Date = 02/21/21 Pct Recovery = 98% Analysis Date = 02/21/21 Pct Recovery = 98% Analysis Date = 02/17/21 Pct Recovery = 97% Analysis Date = 02/17/21 Pct Recovery = 97% Analysis Date = 02/12/21 Pct Recovery = 97% Analysis Date = 02/12/21 Pct Recovery = 97% Analysis Date = 02/08/21 Pct Recovery = 97% Analysis Date = 02/08/21 Pct Recovery = 97% Analysis Date = 02/04/21 Pct Recovery = 97% Analysis Date = 02/04/21 Pct Recovery = 97% Analysis Date = 01/31/21 Pct Recovery = 96% Analysis Date = 01/31/21 Pct Recovery = 96% Analysis Date = 01/27/21 Pct Recovery = 96% Analysis Date = 01/27/21 Pct Recovery = 96% Analysis Date = 01/23/21 Pct Recovery = 96% Analysis Date = 01/23/21 Pct Recovery = 96% Analysis Date = 01/19/21 Pct Recovery = 96% Analysis Date = 01/19/21 Pct Recovery = 96% Analysis Date = 01/15/21 Pct Recovery = 96% Analysis Date = 01/15/21 Pct Recovery = 96% Analysis Date = 01/11/21 Pct Recovery = 96% Analysis Date = 01/11/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/17/20 Pct Recovery = 96% Analysis Date = 12/13/20 Pct Recovery = 96% Analysis Date = 12/13/20 Pct Recovery = 96% Analysis Date = 12/09/20 Pct Recovery = 96% Analysis Date = 12/09/20 Pct Recovery = 96% Analysis Date = 12/05/20 Pct Recovery = 96% Analysis Date = 12/05/20 Pct Recovery = 96% Analysis Date = 12/01/20 Pct Recovery = 96% Analysis Date = 12/01/20 Pct Recovery = 96% Analysis Date = 11/27/20 Pct Recovery = 96% Analysis Date = 11/27/20 Pct Recovery = 96% Analysis Date = 11/23/20 Pct Recovery = 96% Analysis Date = 11/23/20 Pct Recovery = 96% Analysis Date = 11/19/20 Pct Recovery = 96% Analysis Date = 11/19/20 Pct Recovery = 96% Analysis Date = 11/14/20 Pct Recovery = 96% Analysis Date = 11/14/20 Pct Recovery = 96% Analysis Date = 11/10/20 Pct Recovery = 96% Analysis Date = 11/10/20 Pct Recovery = 96% Analysis Date = 11/06/20 Pct Recovery = 96% Analysis Date = 11/06/20 Pct Recovery = 96% Analysis Date = 11/02/20 Pct Recovery = 96% Analysis Date = 11/02/20 Pct Recovery = 96% Analysis Date = 10/29/20 Pct Recovery = 97% Analysis Date = 10/29/20 Pct Recovery = 97% Analysis Date = 10/25/20 Pct Recovery = 97% Analysis Date = 10/25/20 Pct Recovery = 97% Analysis Date = 10/21/20 Pct Recovery = 97% Analysis Date = 10/21/20 Pct Recovery = 97% Analysis Date = 10/17/20 Pct Recovery = 97% Analysis Date = 10/17/20 Pct Recovery = 97% Analysis Date = 10/13/20 Pct Recovery = 98% Analysis Date = 10/13/20 Pct Recovery = 98% Analysis Date = 10/09/20 Pct Recovery = 98% Analysis Date = 10/09/20 Pct Recovery = 98% Analysis Date = 10/05/20 Pct Recovery = 98% Analysis Date = 10/05/20 Pct Recovery = 98% Analysis Date = 09/30/20 Pct Recovery = 98% Analysis Date = 09/30/20 Pct Recovery = 98% Analysis Date = 09/26/20 Pct Recovery = 99% Analysis Date = 09/26/20 Pct Recovery = 99% Analysis Date = 09/22/20 Pct Recovery = 99% Analysis Date = 09/22/20 Pct Recovery = 99% Analysis Date = 09/18/20 Pct Recovery = 99% Analysis Date = 09/18/20 Pct Recovery = 99% Analysis Date = 09/14/20 Pct Recovery = 99% Analysis Date = 09/14/20 Pct Recovery = 99% Analysis Date = 09/10/20 Pct Recovery = 100% Analysis Date = 09/10/20 Pct Recovery = 100% Analysis Date = 09/06/20 Pct Recovery = 100% Analysis Date = 09/06/20 Pct Recovery = 100% Analysis Date = 09/02/20 Pct Recovery = 100% Analysis Date = 09/02/20 Pct Recovery = 100% Analysis Date = 08/29/20 Pct Recovery = 100% Analysis Date = 08/29/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/25/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/16/20 Pct Recovery = 101% Analysis Date = 08/16/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 102% Analysis Date = 08/04/20 Pct Recovery = 102% Analysis Date = 07/31/20 Pct Recovery = 102% Analysis Date = 07/31/20 Pct Recovery = 102% Analysis Date = 07/27/20 Pct Recovery = 102% Analysis Date = 07/27/20 Pct Recovery = 102% Analysis Date = 07/23/20 Pct Recovery = 102% Analysis Date = 07/23/20 Pct Recovery = 102% Analysis Date = 07/19/20 Pct Recovery = 103% Analysis Date = 07/19/20 Pct Recovery = 103% Analysis Date = 07/15/20 Pct Recovery = 103% Analysis Date = 07/15/20 Pct Recovery = 103% Analysis Date = 07/11/20 Pct Recovery = 103% Analysis Date = 07/11/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/07/20 Pct Recovery = 103% Analysis Date = 07/02/20 Pct Recovery = 103% Analysis Date = 07/02/20 Pct Recovery = 103% Analysis Date = 06/28/20 Pct Recovery = 104% Analysis Date = 06/28/20 Pct Recovery = 104% Analysis Date = 06/24/20 Pct Recovery = 104% Analysis Date = 06/24/20 Pct Recovery = 104% Analysis Date = 06/20/20 Pct Recovery = 104% Analysis Date = 06/20/20 Pct Recovery = 104% Analysis Date = 06/16/20 Pct Recovery = 104% Analysis Date = 06/16/20 Pct Recovery = 104% Analysis Date = 06/12/20 Pct Recovery = 104% Analysis Date = 06/12/20 Pct Recovery = 104% Analysis Date = 06/08/20 Pct Recovery = 105% Analysis Date = 06/08/20 Pct Recovery = 105% Analysis Date = 06/04/20 Pct Recovery = 105% Analysis Date = 06/04/20 Pct Recovery = 105% Analysis Date = 05/31/20 Pct Recovery = 105% Analysis Date = 05/31/20 Pct Recovery = 105% Analysis Date = 05/27/20 Pct Recovery = 105% Analysis Date = 05/27/20 Pct Recovery = 105% Analysis Date = 05/23/20 Pct Recovery = 105% Analysis Date = 05/23/20 Pct Recovery = 105% Analysis Date = 05/19/20 Pct Recovery = 106% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOLACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 96% 14% 98% 12%
Total 34 96% 14% 98% 12%

Sample Statistics
METOLACHLOR

Characteristic N % % Basis
Plotted 34 97% Spiked
Estimated Values 3 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 1 3% 1 out of 35
Not Spiked 79 .  
False Positives 0 0% 0 out of 79

OBSP Determination:
METOLACHLOR OXANILIC ACID
METHOD: 2447 , TESTIDCODE: 68650LCM60

Laboratory ID = 20202110006 Lab Value = 2492.557 Expected Conc. = 1873.3 Report level label = 149 Pct Recovery = 133% Analysis Date = 08/07/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203080100 Lab Value = 2906.449 Expected Conc. = 1869.1 Report level label = 149 Pct Recovery = 155% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 2337.372 Expected Conc. = 1869.1 Report level label = 149 Pct Recovery = 125% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 2243.573 Expected Conc. = 1869.1 Report level label = 149 Pct Recovery = 120% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201820155 Lab Value = 2440.996 Expected Conc. = 1860.7 Report level label = 149 Pct Recovery = 131% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20210760015 Lab Value = 1097.270 Expected Conc. = 1834 Report level label = 149 Pct Recovery = 60% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 1308.200 Expected Conc. = 1834 Report level label = 149 Pct Recovery = 71% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 2241.663 Expected Conc. = 1834 Report level label = 149 Pct Recovery = 122% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 1755.769 Expected Conc. = 1834 Report level label = 149 Pct Recovery = 96% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221940195 Lab Value = 1141.622 Expected Conc. = 1495.3 Report level label = 149 Pct Recovery = 76% Analysis Date = 07/21/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20222640086 Lab Value = 1331.721 Expected Conc. = 1468.4 Report level label = 149 Pct Recovery = 91% Analysis Date = 09/30/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20201680155 Lab Value = 935.498 Expected Conc. = 936.65 Report level label = 149 Pct Recovery = 100% Analysis Date = 06/20/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202880004 Lab Value = 974.097 Expected Conc. = 934.55 Report level label = 149 Pct Recovery = 104% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202530029 Lab Value = 1126.881 Expected Conc. = 930.35 Report level label = 149 Pct Recovery = 121% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 1045.847 Expected Conc. = 930.35 Report level label = 149 Pct Recovery = 112% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 1123.785 Expected Conc. = 930.35 Report level label = 149 Pct Recovery = 121% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20210480001 Lab Value = 862.773 Expected Conc. = 917 Report level label = 149 Pct Recovery = 94% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 908.552 Expected Conc. = 747.64 Report level label = 149 Pct Recovery = 122% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 988.598 Expected Conc. = 747.64 Report level label = 149 Pct Recovery = 132% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 410.963 Expected Conc. = 374.66 Report level label = 149 Pct Recovery = 110% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210120050 Lab Value = 453.575 Expected Conc. = 373.82 Report level label = 149 Pct Recovery = 121% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 318.501 Expected Conc. = 373.82 Report level label = 149 Pct Recovery = 85% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 438.705 Expected Conc. = 373.82 Report level label = 149 Pct Recovery = 117% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 409.819 Expected Conc. = 373.82 Report level label = 149 Pct Recovery = 110% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201890192 Lab Value = 536.841 Expected Conc. = 372.14 Report level label = 149 Pct Recovery = 144% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 321.687 Expected Conc. = 372.14 Report level label = 149 Pct Recovery = 86% Analysis Date = 05/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210690067 Lab Value = 291.077 Expected Conc. = 366.8 Report level label = 149 Pct Recovery = 79% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 09/29/22 Pct Recovery = 84% Analysis Date = 09/25/22 Pct Recovery = 84% Analysis Date = 09/25/22 Pct Recovery = 84% Analysis Date = 09/21/22 Pct Recovery = 84% Analysis Date = 09/21/22 Pct Recovery = 84% Analysis Date = 09/17/22 Pct Recovery = 84% Analysis Date = 09/17/22 Pct Recovery = 84% Analysis Date = 09/12/22 Pct Recovery = 84% Analysis Date = 09/12/22 Pct Recovery = 84% Analysis Date = 09/08/22 Pct Recovery = 84% Analysis Date = 09/08/22 Pct Recovery = 84% Analysis Date = 09/04/22 Pct Recovery = 84% Analysis Date = 09/04/22 Pct Recovery = 84% Analysis Date = 08/30/22 Pct Recovery = 84% Analysis Date = 08/30/22 Pct Recovery = 84% Analysis Date = 08/26/22 Pct Recovery = 84% Analysis Date = 08/26/22 Pct Recovery = 84% Analysis Date = 08/22/22 Pct Recovery = 84% Analysis Date = 08/22/22 Pct Recovery = 84% Analysis Date = 08/17/22 Pct Recovery = 83% Analysis Date = 08/17/22 Pct Recovery = 83% Analysis Date = 08/13/22 Pct Recovery = 83% Analysis Date = 08/13/22 Pct Recovery = 83% Analysis Date = 08/09/22 Pct Recovery = 83% Analysis Date = 08/09/22 Pct Recovery = 83% Analysis Date = 08/04/22 Pct Recovery = 83% Analysis Date = 08/04/22 Pct Recovery = 83% Analysis Date = 07/31/22 Pct Recovery = 83% Analysis Date = 07/31/22 Pct Recovery = 83% Analysis Date = 07/27/22 Pct Recovery = 83% Analysis Date = 07/27/22 Pct Recovery = 83% Analysis Date = 07/22/22 Pct Recovery = 83% Analysis Date = 07/22/22 Pct Recovery = 83% Analysis Date = 07/18/22 Pct Recovery = 83% Analysis Date = 07/18/22 Pct Recovery = 83% Analysis Date = 07/14/22 Pct Recovery = 83% Analysis Date = 07/14/22 Pct Recovery = 83% Analysis Date = 07/10/22 Pct Recovery = 83% Analysis Date = 07/10/22 Pct Recovery = 83% Analysis Date = 07/05/22 Pct Recovery = 83% Analysis Date = 07/05/22 Pct Recovery = 83% Analysis Date = 07/01/22 Pct Recovery = 83% Analysis Date = 07/01/22 Pct Recovery = 83% Analysis Date = 06/27/22 Pct Recovery = 83% Analysis Date = 06/27/22 Pct Recovery = 83% Analysis Date = 06/22/22 Pct Recovery = 83% Analysis Date = 06/22/22 Pct Recovery = 83% Analysis Date = 06/18/22 Pct Recovery = 83% Analysis Date = 06/18/22 Pct Recovery = 83% Analysis Date = 06/14/22 Pct Recovery = 83% Analysis Date = 06/14/22 Pct Recovery = 83% Analysis Date = 06/09/22 Pct Recovery = 83% Analysis Date = 06/09/22 Pct Recovery = 83% Analysis Date = 06/05/22 Pct Recovery = 83% Analysis Date = 06/05/22 Pct Recovery = 83% Analysis Date = 06/01/22 Pct Recovery = 83% Analysis Date = 06/01/22 Pct Recovery = 83% Analysis Date = 05/27/22 Pct Recovery = 83% Analysis Date = 05/27/22 Pct Recovery = 83% Analysis Date = 05/23/22 Pct Recovery = 83% Analysis Date = 05/23/22 Pct Recovery = 83% Analysis Date = 05/19/22 Pct Recovery = 83% Analysis Date = 05/19/22 Pct Recovery = 83% Analysis Date = 05/14/22 Pct Recovery = 83% Analysis Date = 05/14/22 Pct Recovery = 83% Analysis Date = 05/10/22 Pct Recovery = 83% Analysis Date = 05/10/22 Pct Recovery = 83% Analysis Date = 05/06/22 Pct Recovery = 83% Analysis Date = 05/06/22 Pct Recovery = 83% Analysis Date = 05/01/22 Pct Recovery = 83% Analysis Date = 05/01/22 Pct Recovery = 83% Analysis Date = 04/27/22 Pct Recovery = 83% Analysis Date = 04/27/22 Pct Recovery = 83% Analysis Date = 04/23/22 Pct Recovery = 83% Analysis Date = 04/23/22 Pct Recovery = 83% Analysis Date = 04/19/22 Pct Recovery = 83% Analysis Date = 04/19/22 Pct Recovery = 83% Analysis Date = 04/14/22 Pct Recovery = 83% Analysis Date = 04/14/22 Pct Recovery = 83% Analysis Date = 04/10/22 Pct Recovery = 83% Analysis Date = 04/10/22 Pct Recovery = 83% Analysis Date = 04/06/22 Pct Recovery = 83% Analysis Date = 04/06/22 Pct Recovery = 83% Analysis Date = 04/01/22 Pct Recovery = 83% Analysis Date = 04/01/22 Pct Recovery = 83% Analysis Date = 03/28/22 Pct Recovery = 83% Analysis Date = 03/28/22 Pct Recovery = 83% Analysis Date = 03/24/22 Pct Recovery = 83% Analysis Date = 03/24/22 Pct Recovery = 83% Analysis Date = 03/19/22 Pct Recovery = 83% Analysis Date = 03/19/22 Pct Recovery = 83% Analysis Date = 03/15/22 Pct Recovery = 83% Analysis Date = 03/15/22 Pct Recovery = 83% Analysis Date = 03/11/22 Pct Recovery = 83% Analysis Date = 03/11/22 Pct Recovery = 83% Analysis Date = 03/06/22 Pct Recovery = 83% Analysis Date = 03/06/22 Pct Recovery = 83% Analysis Date = 03/02/22 Pct Recovery = 83% Analysis Date = 03/02/22 Pct Recovery = 83% Analysis Date = 02/26/22 Pct Recovery = 83% Analysis Date = 02/26/22 Pct Recovery = 83% Analysis Date = 02/21/22 Pct Recovery = 83% Analysis Date = 02/21/22 Pct Recovery = 83% Analysis Date = 02/17/22 Pct Recovery = 83% Analysis Date = 02/17/22 Pct Recovery = 83% Analysis Date = 02/13/22 Pct Recovery = 83% Analysis Date = 02/13/22 Pct Recovery = 83% Analysis Date = 02/08/22 Pct Recovery = 83% Analysis Date = 02/08/22 Pct Recovery = 83% Analysis Date = 02/04/22 Pct Recovery = 83% Analysis Date = 02/04/22 Pct Recovery = 83% Analysis Date = 01/31/22 Pct Recovery = 83% Analysis Date = 01/31/22 Pct Recovery = 83% Analysis Date = 01/27/22 Pct Recovery = 83% Analysis Date = 01/27/22 Pct Recovery = 83% Analysis Date = 01/22/22 Pct Recovery = 83% Analysis Date = 01/22/22 Pct Recovery = 83% Analysis Date = 01/18/22 Pct Recovery = 83% Analysis Date = 01/18/22 Pct Recovery = 83% Analysis Date = 01/14/22 Pct Recovery = 83% Analysis Date = 01/14/22 Pct Recovery = 83% Analysis Date = 01/09/22 Pct Recovery = 83% Analysis Date = 01/09/22 Pct Recovery = 83% Analysis Date = 01/05/22 Pct Recovery = 83% Analysis Date = 01/05/22 Pct Recovery = 83% Analysis Date = 01/01/22 Pct Recovery = 83% Analysis Date = 01/01/22 Pct Recovery = 83% Analysis Date = 12/27/21 Pct Recovery = 83% Analysis Date = 12/27/21 Pct Recovery = 83% Analysis Date = 12/23/21 Pct Recovery = 83% Analysis Date = 12/23/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 83% Analysis Date = 12/19/21 Pct Recovery = 83% Analysis Date = 12/14/21 Pct Recovery = 83% Analysis Date = 12/14/21 Pct Recovery = 83% Analysis Date = 12/10/21 Pct Recovery = 83% Analysis Date = 12/10/21 Pct Recovery = 83% Analysis Date = 12/06/21 Pct Recovery = 83% Analysis Date = 12/06/21 Pct Recovery = 83% Analysis Date = 12/01/21 Pct Recovery = 83% Analysis Date = 12/01/21 Pct Recovery = 83% Analysis Date = 11/27/21 Pct Recovery = 83% Analysis Date = 11/27/21 Pct Recovery = 83% Analysis Date = 11/23/21 Pct Recovery = 83% Analysis Date = 11/23/21 Pct Recovery = 83% Analysis Date = 11/19/21 Pct Recovery = 83% Analysis Date = 11/19/21 Pct Recovery = 83% Analysis Date = 11/14/21 Pct Recovery = 83% Analysis Date = 11/14/21 Pct Recovery = 83% Analysis Date = 11/10/21 Pct Recovery = 83% Analysis Date = 11/10/21 Pct Recovery = 83% Analysis Date = 11/06/21 Pct Recovery = 83% Analysis Date = 11/06/21 Pct Recovery = 83% Analysis Date = 11/01/21 Pct Recovery = 83% Analysis Date = 11/01/21 Pct Recovery = 83% Analysis Date = 10/28/21 Pct Recovery = 83% Analysis Date = 10/28/21 Pct Recovery = 83% Analysis Date = 10/24/21 Pct Recovery = 83% Analysis Date = 10/24/21 Pct Recovery = 83% Analysis Date = 10/19/21 Pct Recovery = 83% Analysis Date = 10/19/21 Pct Recovery = 83% Analysis Date = 10/15/21 Pct Recovery = 83% Analysis Date = 10/15/21 Pct Recovery = 83% Analysis Date = 10/11/21 Pct Recovery = 83% Analysis Date = 10/11/21 Pct Recovery = 83% Analysis Date = 10/06/21 Pct Recovery = 83% Analysis Date = 10/06/21 Pct Recovery = 83% Analysis Date = 10/02/21 Pct Recovery = 83% Analysis Date = 10/02/21 Pct Recovery = 83% Analysis Date = 09/28/21 Pct Recovery = 83% Analysis Date = 09/28/21 Pct Recovery = 83% Analysis Date = 09/23/21 Pct Recovery = 83% Analysis Date = 09/23/21 Pct Recovery = 83% Analysis Date = 09/19/21 Pct Recovery = 83% Analysis Date = 09/19/21 Pct Recovery = 83% Analysis Date = 09/15/21 Pct Recovery = 83% Analysis Date = 09/15/21 Pct Recovery = 83% Analysis Date = 09/10/21 Pct Recovery = 83% Analysis Date = 09/10/21 Pct Recovery = 83% Analysis Date = 09/06/21 Pct Recovery = 83% Analysis Date = 09/06/21 Pct Recovery = 83% Analysis Date = 09/02/21 Pct Recovery = 83% Analysis Date = 09/02/21 Pct Recovery = 83% Analysis Date = 08/29/21 Pct Recovery = 83% Analysis Date = 08/29/21 Pct Recovery = 83% Analysis Date = 08/24/21 Pct Recovery = 83% Analysis Date = 08/24/21 Pct Recovery = 83% Analysis Date = 08/20/21 Pct Recovery = 83% Analysis Date = 08/20/21 Pct Recovery = 83% Analysis Date = 08/16/21 Pct Recovery = 83% Analysis Date = 08/16/21 Pct Recovery = 83% Analysis Date = 08/11/21 Pct Recovery = 83% Analysis Date = 08/11/21 Pct Recovery = 83% Analysis Date = 08/07/21 Pct Recovery = 83% Analysis Date = 08/07/21 Pct Recovery = 83% Analysis Date = 08/03/21 Pct Recovery = 83% Analysis Date = 08/03/21 Pct Recovery = 83% Analysis Date = 07/29/21 Pct Recovery = 83% Analysis Date = 07/29/21 Pct Recovery = 83% Analysis Date = 07/25/21 Pct Recovery = 83% Analysis Date = 07/25/21 Pct Recovery = 83% Analysis Date = 07/21/21 Pct Recovery = 83% Analysis Date = 07/21/21 Pct Recovery = 83% Analysis Date = 07/16/21 Pct Recovery = 83% Analysis Date = 07/16/21 Pct Recovery = 83% Analysis Date = 07/12/21 Pct Recovery = 83% Analysis Date = 07/12/21 Pct Recovery = 83% Analysis Date = 07/08/21 Pct Recovery = 83% Analysis Date = 07/08/21 Pct Recovery = 83% Analysis Date = 07/03/21 Pct Recovery = 83% Analysis Date = 07/03/21 Pct Recovery = 83% Analysis Date = 06/29/21 Pct Recovery = 83% Analysis Date = 06/29/21 Pct Recovery = 83% Analysis Date = 06/25/21 Pct Recovery = 83% Analysis Date = 06/25/21 Pct Recovery = 83% Analysis Date = 06/20/21 Pct Recovery = 83% Analysis Date = 06/20/21 Pct Recovery = 83% Analysis Date = 06/16/21 Pct Recovery = 83% Analysis Date = 06/16/21 Pct Recovery = 83% Analysis Date = 06/12/21 Pct Recovery = 83% Analysis Date = 06/12/21 Pct Recovery = 83% Analysis Date = 06/08/21 Pct Recovery = 83% Analysis Date = 06/08/21 Pct Recovery = 83% Analysis Date = 06/03/21 Pct Recovery = 83% Analysis Date = 06/03/21 Pct Recovery = 83% Analysis Date = 05/30/21 Pct Recovery = 83% Analysis Date = 05/30/21 Pct Recovery = 83% Analysis Date = 05/26/21 Pct Recovery = 83% Analysis Date = 05/26/21 Pct Recovery = 83% Analysis Date = 05/21/21 Pct Recovery = 83% Analysis Date = 05/21/21 Pct Recovery = 83% Analysis Date = 05/17/21 Pct Recovery = 83% Analysis Date = 05/17/21 Pct Recovery = 83% Analysis Date = 05/13/21 Pct Recovery = 83% Analysis Date = 05/13/21 Pct Recovery = 83% Analysis Date = 05/08/21 Pct Recovery = 83% Analysis Date = 05/08/21 Pct Recovery = 83% Analysis Date = 05/04/21 Pct Recovery = 83% Analysis Date = 05/04/21 Pct Recovery = 83% Analysis Date = 04/30/21 Pct Recovery = 83% Analysis Date = 04/30/21 Pct Recovery = 83% Analysis Date = 04/25/21 Pct Recovery = 83% Analysis Date = 04/25/21 Pct Recovery = 83% Analysis Date = 04/21/21 Pct Recovery = 83% Analysis Date = 04/21/21 Pct Recovery = 83% Analysis Date = 04/17/21 Pct Recovery = 83% Analysis Date = 04/17/21 Pct Recovery = 83% Analysis Date = 04/12/21 Pct Recovery = 83% Analysis Date = 04/12/21 Pct Recovery = 83% Analysis Date = 04/08/21 Pct Recovery = 83% Analysis Date = 04/08/21 Pct Recovery = 83% Analysis Date = 04/04/21 Pct Recovery = 83% Analysis Date = 04/04/21 Pct Recovery = 83% Analysis Date = 03/30/21 Pct Recovery = 83% Analysis Date = 03/30/21 Pct Recovery = 83% Analysis Date = 03/26/21 Pct Recovery = 83% Analysis Date = 03/26/21 Pct Recovery = 83% Analysis Date = 03/22/21 Pct Recovery = 83% Analysis Date = 03/22/21 Pct Recovery = 83% Analysis Date = 03/18/21 Pct Recovery = 83% Analysis Date = 03/18/21 Pct Recovery = 83% Analysis Date = 03/13/21 Pct Recovery = 85% Analysis Date = 03/13/21 Pct Recovery = 85% Analysis Date = 03/09/21 Pct Recovery = 86% Analysis Date = 03/09/21 Pct Recovery = 86% Analysis Date = 03/05/21 Pct Recovery = 87% Analysis Date = 03/05/21 Pct Recovery = 87% Analysis Date = 02/28/21 Pct Recovery = 89% Analysis Date = 02/28/21 Pct Recovery = 89% Analysis Date = 02/24/21 Pct Recovery = 90% Analysis Date = 02/24/21 Pct Recovery = 90% Analysis Date = 02/20/21 Pct Recovery = 92% Analysis Date = 02/20/21 Pct Recovery = 92% Analysis Date = 02/15/21 Pct Recovery = 93% Analysis Date = 02/15/21 Pct Recovery = 93% Analysis Date = 02/11/21 Pct Recovery = 95% Analysis Date = 02/11/21 Pct Recovery = 95% Analysis Date = 02/07/21 Pct Recovery = 96% Analysis Date = 02/07/21 Pct Recovery = 96% Analysis Date = 02/02/21 Pct Recovery = 97% Analysis Date = 02/02/21 Pct Recovery = 97% Analysis Date = 01/29/21 Pct Recovery = 99% Analysis Date = 01/29/21 Pct Recovery = 99% Analysis Date = 01/25/21 Pct Recovery = 100% Analysis Date = 01/25/21 Pct Recovery = 100% Analysis Date = 01/20/21 Pct Recovery = 101% Analysis Date = 01/20/21 Pct Recovery = 101% Analysis Date = 01/16/21 Pct Recovery = 103% Analysis Date = 01/16/21 Pct Recovery = 103% Analysis Date = 01/12/21 Pct Recovery = 104% Analysis Date = 01/12/21 Pct Recovery = 104% Analysis Date = 01/08/21 Pct Recovery = 105% Analysis Date = 01/08/21 Pct Recovery = 105% Analysis Date = 01/03/21 Pct Recovery = 106% Analysis Date = 01/03/21 Pct Recovery = 106% Analysis Date = 12/30/20 Pct Recovery = 108% Analysis Date = 12/30/20 Pct Recovery = 108% Analysis Date = 12/26/20 Pct Recovery = 109% Analysis Date = 12/26/20 Pct Recovery = 109% Analysis Date = 12/21/20 Pct Recovery = 110% Analysis Date = 12/21/20 Pct Recovery = 110% Analysis Date = 12/17/20 Pct Recovery = 111% Analysis Date = 12/17/20 Pct Recovery = 111% Analysis Date = 12/13/20 Pct Recovery = 112% Analysis Date = 12/13/20 Pct Recovery = 112% Analysis Date = 12/08/20 Pct Recovery = 113% Analysis Date = 12/08/20 Pct Recovery = 113% Analysis Date = 12/04/20 Pct Recovery = 113% Analysis Date = 12/04/20 Pct Recovery = 113% Analysis Date = 11/30/20 Pct Recovery = 114% Analysis Date = 11/30/20 Pct Recovery = 114% Analysis Date = 11/25/20 Pct Recovery = 115% Analysis Date = 11/25/20 Pct Recovery = 115% Analysis Date = 11/21/20 Pct Recovery = 115% Analysis Date = 11/21/20 Pct Recovery = 115% Analysis Date = 11/17/20 Pct Recovery = 116% Analysis Date = 11/17/20 Pct Recovery = 116% Analysis Date = 11/12/20 Pct Recovery = 117% Analysis Date = 11/12/20 Pct Recovery = 117% Analysis Date = 11/08/20 Pct Recovery = 117% Analysis Date = 11/08/20 Pct Recovery = 117% Analysis Date = 11/04/20 Pct Recovery = 118% Analysis Date = 11/04/20 Pct Recovery = 118% Analysis Date = 10/30/20 Pct Recovery = 118% Analysis Date = 10/30/20 Pct Recovery = 118% Analysis Date = 10/26/20 Pct Recovery = 118% Analysis Date = 10/26/20 Pct Recovery = 118% Analysis Date = 10/22/20 Pct Recovery = 119% Analysis Date = 10/22/20 Pct Recovery = 119% Analysis Date = 10/18/20 Pct Recovery = 119% Analysis Date = 10/18/20 Pct Recovery = 119% Analysis Date = 10/13/20 Pct Recovery = 120% Analysis Date = 10/13/20 Pct Recovery = 120% Analysis Date = 10/09/20 Pct Recovery = 120% Analysis Date = 10/09/20 Pct Recovery = 120% Analysis Date = 10/05/20 Pct Recovery = 120% Analysis Date = 10/05/20 Pct Recovery = 120% Analysis Date = 09/30/20 Pct Recovery = 121% Analysis Date = 09/30/20 Pct Recovery = 121% Analysis Date = 09/26/20 Pct Recovery = 121% Analysis Date = 09/26/20 Pct Recovery = 121% Analysis Date = 09/22/20 Pct Recovery = 122% Analysis Date = 09/22/20 Pct Recovery = 122% Analysis Date = 09/17/20 Pct Recovery = 122% Analysis Date = 09/17/20 Pct Recovery = 122% Analysis Date = 09/13/20 Pct Recovery = 121% Analysis Date = 09/13/20 Pct Recovery = 121% Analysis Date = 09/09/20 Pct Recovery = 121% Analysis Date = 09/09/20 Pct Recovery = 121% Analysis Date = 09/04/20 Pct Recovery = 121% Analysis Date = 09/04/20 Pct Recovery = 121% Analysis Date = 08/31/20 Pct Recovery = 121% Analysis Date = 08/31/20 Pct Recovery = 121% Analysis Date = 08/27/20 Pct Recovery = 120% Analysis Date = 08/27/20 Pct Recovery = 120% Analysis Date = 08/22/20 Pct Recovery = 120% Analysis Date = 08/22/20 Pct Recovery = 120% Analysis Date = 08/18/20 Pct Recovery = 120% Analysis Date = 08/18/20 Pct Recovery = 120% Analysis Date = 08/14/20 Pct Recovery = 120% Analysis Date = 08/14/20 Pct Recovery = 120% Analysis Date = 08/09/20 Pct Recovery = 119% Analysis Date = 08/09/20 Pct Recovery = 119% Analysis Date = 08/05/20 Pct Recovery = 119% Analysis Date = 08/05/20 Pct Recovery = 119% Analysis Date = 08/01/20 Pct Recovery = 119% Analysis Date = 08/01/20 Pct Recovery = 119% Analysis Date = 07/28/20 Pct Recovery = 118% Analysis Date = 07/28/20 Pct Recovery = 118% Analysis Date = 07/23/20 Pct Recovery = 118% Analysis Date = 07/23/20 Pct Recovery = 118% Analysis Date = 07/19/20 Pct Recovery = 117% Analysis Date = 07/19/20 Pct Recovery = 117% Analysis Date = 07/15/20 Pct Recovery = 117% Analysis Date = 07/15/20 Pct Recovery = 117% Analysis Date = 07/10/20 Pct Recovery = 117% Analysis Date = 07/10/20 Pct Recovery = 117% Analysis Date = 07/06/20 Pct Recovery = 116% Analysis Date = 07/06/20 Pct Recovery = 116% Analysis Date = 07/02/20 Pct Recovery = 116% Analysis Date = 07/02/20 Pct Recovery = 116% Analysis Date = 06/27/20 Pct Recovery = 115% Analysis Date = 06/27/20 Pct Recovery = 115% Analysis Date = 06/23/20 Pct Recovery = 115% Analysis Date = 06/23/20 Pct Recovery = 115% Analysis Date = 06/19/20 Pct Recovery = 114% Analysis Date = 06/19/20 Pct Recovery = 114% Analysis Date = 06/14/20 Pct Recovery = 114% Analysis Date = 06/14/20 Pct Recovery = 114% Analysis Date = 06/10/20 Pct Recovery = 113% Analysis Date = 06/10/20 Pct Recovery = 113% Analysis Date = 06/06/20 Pct Recovery = 113% Analysis Date = 06/06/20 Pct Recovery = 113% Analysis Date = 06/01/20 Pct Recovery = 112% Analysis Date = 06/01/20 Pct Recovery = 112% Analysis Date = 05/28/20 Pct Recovery = 112% Analysis Date = 05/28/20 Pct Recovery = 112% Analysis Date = 05/24/20 Pct Recovery = 111% Analysis Date = 05/24/20 Pct Recovery = 111% Analysis Date = 05/20/20 Pct Recovery = 111% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOLACHLOR OXANILIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 27 109% 23% 112% 23%
Total 27 109% 23% 112% 23%

Sample Statistics
METOLACHLOR OXANILIC ACID

Characteristic N % % Basis
Plotted 27 87% Spiked
Estimated Values 27 87% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 6% Spiked
Spiked 31 .  
False Negatives 2 6% 2 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
METOLACHLOR SULFONIC ACID
METHOD: 2447 , TESTIDCODE: 68651LCM60

Laboratory ID = 20202590107 Lab Value = 601.747 Expected Conc. = 856.2 Report level label = 68 Pct Recovery = 70% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 700.212 Expected Conc. = 856.2 Report level label = 68 Pct Recovery = 82% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 967.214 Expected Conc. = 854 Report level label = 68 Pct Recovery = 113% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20201820155 Lab Value = 661.097 Expected Conc. = 852.2 Report level label = 68 Pct Recovery = 78% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 985.754 Expected Conc. = 852.2 Report level label = 68 Pct Recovery = 116% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203230021 Lab Value = 670.725 Expected Conc. = 850.7 Report level label = 68 Pct Recovery = 79% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 652.045 Expected Conc. = 850.7 Report level label = 68 Pct Recovery = 77% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203360042 Lab Value = 353.364 Expected Conc. = 428.1 Report level label = 68 Pct Recovery = 83% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 302.571 Expected Conc. = 428.1 Report level label = 68 Pct Recovery = 71% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 270.020 Expected Conc. = 428.1 Report level label = 68 Pct Recovery = 63% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201960104 Lab Value = 412.127 Expected Conc. = 427 Report level label = 68 Pct Recovery = 97% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202530029 Lab Value = 245.708 Expected Conc. = 426.1 Report level label = 68 Pct Recovery = 58% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 279.466 Expected Conc. = 426.1 Report level label = 68 Pct Recovery = 66% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 562.955 Expected Conc. = 426.1 Report level label = 68 Pct Recovery = 132% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20210970035 Lab Value = 186.460 Expected Conc. = 171.24 Report level label = 68 Pct Recovery = 109% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 102.314 Expected Conc. = 171.24 Report level label = 68 Pct Recovery = 60% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 122.331 Expected Conc. = 171.24 Report level label = 68 Pct Recovery = 71% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 149.055 Expected Conc. = 171.24 Report level label = 68 Pct Recovery = 87% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 103.520 Expected Conc. = 171.24 Report level label = 68 Pct Recovery = 60% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 128.265 Expected Conc. = 171.24 Report level label = 68 Pct Recovery = 75% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201610160 Lab Value = 231.737 Expected Conc. = 170.8 Report level label = 68 Pct Recovery = 136% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20202180001 Lab Value = 241.709 Expected Conc. = 170.44 Report level label = 68 Pct Recovery = 142% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 178.545 Expected Conc. = 170.44 Report level label = 68 Pct Recovery = 105% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 118.701 Expected Conc. = 170.44 Report level label = 68 Pct Recovery = 70% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Analysis Date = 04/15/21 Pct Recovery = 97% Analysis Date = 04/13/21 Pct Recovery = 96% Analysis Date = 04/13/21 Pct Recovery = 96% Analysis Date = 04/11/21 Pct Recovery = 96% Analysis Date = 04/11/21 Pct Recovery = 96% Analysis Date = 04/10/21 Pct Recovery = 96% Analysis Date = 04/10/21 Pct Recovery = 96% Analysis Date = 04/08/21 Pct Recovery = 95% Analysis Date = 04/08/21 Pct Recovery = 95% Analysis Date = 04/06/21 Pct Recovery = 95% Analysis Date = 04/06/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/03/21 Pct Recovery = 94% Analysis Date = 04/03/21 Pct Recovery = 94% Analysis Date = 04/01/21 Pct Recovery = 94% Analysis Date = 04/01/21 Pct Recovery = 94% Analysis Date = 03/31/21 Pct Recovery = 94% Analysis Date = 03/31/21 Pct Recovery = 94% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/27/21 Pct Recovery = 93% Analysis Date = 03/27/21 Pct Recovery = 93% Analysis Date = 03/26/21 Pct Recovery = 92% Analysis Date = 03/26/21 Pct Recovery = 92% Analysis Date = 03/24/21 Pct Recovery = 92% Analysis Date = 03/24/21 Pct Recovery = 92% Analysis Date = 03/22/21 Pct Recovery = 92% Analysis Date = 03/22/21 Pct Recovery = 92% Analysis Date = 03/21/21 Pct Recovery = 91% Analysis Date = 03/21/21 Pct Recovery = 91% Analysis Date = 03/19/21 Pct Recovery = 91% Analysis Date = 03/19/21 Pct Recovery = 91% Analysis Date = 03/17/21 Pct Recovery = 91% Analysis Date = 03/17/21 Pct Recovery = 91% Analysis Date = 03/16/21 Pct Recovery = 90% Analysis Date = 03/16/21 Pct Recovery = 90% Analysis Date = 03/14/21 Pct Recovery = 90% Analysis Date = 03/14/21 Pct Recovery = 90% Analysis Date = 03/13/21 Pct Recovery = 90% Analysis Date = 03/13/21 Pct Recovery = 90% Analysis Date = 03/11/21 Pct Recovery = 89% Analysis Date = 03/11/21 Pct Recovery = 89% Analysis Date = 03/09/21 Pct Recovery = 89% Analysis Date = 03/09/21 Pct Recovery = 89% Analysis Date = 03/08/21 Pct Recovery = 89% Analysis Date = 03/08/21 Pct Recovery = 89% Analysis Date = 03/06/21 Pct Recovery = 88% Analysis Date = 03/06/21 Pct Recovery = 88% Analysis Date = 03/04/21 Pct Recovery = 88% Analysis Date = 03/04/21 Pct Recovery = 88% Analysis Date = 03/03/21 Pct Recovery = 88% Analysis Date = 03/03/21 Pct Recovery = 88% Analysis Date = 03/01/21 Pct Recovery = 87% Analysis Date = 03/01/21 Pct Recovery = 87% Analysis Date = 02/27/21 Pct Recovery = 87% Analysis Date = 02/27/21 Pct Recovery = 87% Analysis Date = 02/26/21 Pct Recovery = 87% Analysis Date = 02/26/21 Pct Recovery = 87% Analysis Date = 02/24/21 Pct Recovery = 86% Analysis Date = 02/24/21 Pct Recovery = 86% Analysis Date = 02/22/21 Pct Recovery = 86% Analysis Date = 02/22/21 Pct Recovery = 86% Analysis Date = 02/21/21 Pct Recovery = 86% Analysis Date = 02/21/21 Pct Recovery = 86% Analysis Date = 02/19/21 Pct Recovery = 85% Analysis Date = 02/19/21 Pct Recovery = 85% Analysis Date = 02/17/21 Pct Recovery = 85% Analysis Date = 02/17/21 Pct Recovery = 85% Analysis Date = 02/16/21 Pct Recovery = 84% Analysis Date = 02/16/21 Pct Recovery = 84% Analysis Date = 02/14/21 Pct Recovery = 84% Analysis Date = 02/14/21 Pct Recovery = 84% Analysis Date = 02/12/21 Pct Recovery = 84% Analysis Date = 02/12/21 Pct Recovery = 84% Analysis Date = 02/11/21 Pct Recovery = 83% Analysis Date = 02/11/21 Pct Recovery = 83% Analysis Date = 02/09/21 Pct Recovery = 83% Analysis Date = 02/09/21 Pct Recovery = 83% Analysis Date = 02/08/21 Pct Recovery = 83% Analysis Date = 02/08/21 Pct Recovery = 83% Analysis Date = 02/06/21 Pct Recovery = 83% Analysis Date = 02/06/21 Pct Recovery = 83% Analysis Date = 02/04/21 Pct Recovery = 82% Analysis Date = 02/04/21 Pct Recovery = 82% Analysis Date = 02/03/21 Pct Recovery = 82% Analysis Date = 02/03/21 Pct Recovery = 82% Analysis Date = 02/01/21 Pct Recovery = 82% Analysis Date = 02/01/21 Pct Recovery = 82% Analysis Date = 01/30/21 Pct Recovery = 81% Analysis Date = 01/30/21 Pct Recovery = 81% Analysis Date = 01/29/21 Pct Recovery = 81% Analysis Date = 01/29/21 Pct Recovery = 81% Analysis Date = 01/27/21 Pct Recovery = 81% Analysis Date = 01/27/21 Pct Recovery = 81% Analysis Date = 01/25/21 Pct Recovery = 81% Analysis Date = 01/25/21 Pct Recovery = 81% Analysis Date = 01/24/21 Pct Recovery = 80% Analysis Date = 01/24/21 Pct Recovery = 80% Analysis Date = 01/22/21 Pct Recovery = 80% Analysis Date = 01/22/21 Pct Recovery = 80% Analysis Date = 01/20/21 Pct Recovery = 80% Analysis Date = 01/20/21 Pct Recovery = 80% Analysis Date = 01/19/21 Pct Recovery = 79% Analysis Date = 01/19/21 Pct Recovery = 79% Analysis Date = 01/17/21 Pct Recovery = 79% Analysis Date = 01/17/21 Pct Recovery = 79% Analysis Date = 01/15/21 Pct Recovery = 79% Analysis Date = 01/15/21 Pct Recovery = 79% Analysis Date = 01/14/21 Pct Recovery = 79% Analysis Date = 01/14/21 Pct Recovery = 79% Analysis Date = 01/12/21 Pct Recovery = 78% Analysis Date = 01/12/21 Pct Recovery = 78% Analysis Date = 01/10/21 Pct Recovery = 78% Analysis Date = 01/10/21 Pct Recovery = 78% Analysis Date = 01/09/21 Pct Recovery = 78% Analysis Date = 01/09/21 Pct Recovery = 78% Analysis Date = 01/07/21 Pct Recovery = 77% Analysis Date = 01/07/21 Pct Recovery = 77% Analysis Date = 01/06/21 Pct Recovery = 77% Analysis Date = 01/06/21 Pct Recovery = 77% Analysis Date = 01/04/21 Pct Recovery = 77% Analysis Date = 01/04/21 Pct Recovery = 77% Analysis Date = 01/02/21 Pct Recovery = 77% Analysis Date = 01/02/21 Pct Recovery = 77% Analysis Date = 01/01/21 Pct Recovery = 76% Analysis Date = 01/01/21 Pct Recovery = 76% Analysis Date = 12/30/20 Pct Recovery = 76% Analysis Date = 12/30/20 Pct Recovery = 76% Analysis Date = 12/28/20 Pct Recovery = 76% Analysis Date = 12/28/20 Pct Recovery = 76% Analysis Date = 12/27/20 Pct Recovery = 75% Analysis Date = 12/27/20 Pct Recovery = 75% Analysis Date = 12/25/20 Pct Recovery = 75% Analysis Date = 12/25/20 Pct Recovery = 75% Analysis Date = 12/23/20 Pct Recovery = 75% Analysis Date = 12/23/20 Pct Recovery = 75% Analysis Date = 12/22/20 Pct Recovery = 75% Analysis Date = 12/22/20 Pct Recovery = 75% Analysis Date = 12/20/20 Pct Recovery = 74% Analysis Date = 12/20/20 Pct Recovery = 74% Analysis Date = 12/18/20 Pct Recovery = 74% Analysis Date = 12/18/20 Pct Recovery = 74% Analysis Date = 12/17/20 Pct Recovery = 74% Analysis Date = 12/17/20 Pct Recovery = 74% Analysis Date = 12/15/20 Pct Recovery = 74% Analysis Date = 12/15/20 Pct Recovery = 74% Analysis Date = 12/13/20 Pct Recovery = 74% Analysis Date = 12/13/20 Pct Recovery = 74% Analysis Date = 12/12/20 Pct Recovery = 74% Analysis Date = 12/12/20 Pct Recovery = 74% Analysis Date = 12/10/20 Pct Recovery = 75% Analysis Date = 12/10/20 Pct Recovery = 75% Analysis Date = 12/08/20 Pct Recovery = 75% Analysis Date = 12/08/20 Pct Recovery = 75% Analysis Date = 12/07/20 Pct Recovery = 75% Analysis Date = 12/07/20 Pct Recovery = 75% Analysis Date = 12/05/20 Pct Recovery = 75% Analysis Date = 12/05/20 Pct Recovery = 75% Analysis Date = 12/04/20 Pct Recovery = 75% Analysis Date = 12/04/20 Pct Recovery = 75% Analysis Date = 12/02/20 Pct Recovery = 75% Analysis Date = 12/02/20 Pct Recovery = 75% Analysis Date = 11/30/20 Pct Recovery = 75% Analysis Date = 11/30/20 Pct Recovery = 75% Analysis Date = 11/29/20 Pct Recovery = 75% Analysis Date = 11/29/20 Pct Recovery = 75% Analysis Date = 11/27/20 Pct Recovery = 75% Analysis Date = 11/27/20 Pct Recovery = 75% Analysis Date = 11/25/20 Pct Recovery = 75% Analysis Date = 11/25/20 Pct Recovery = 75% Analysis Date = 11/24/20 Pct Recovery = 75% Analysis Date = 11/24/20 Pct Recovery = 75% Analysis Date = 11/22/20 Pct Recovery = 75% Analysis Date = 11/22/20 Pct Recovery = 75% Analysis Date = 11/20/20 Pct Recovery = 74% Analysis Date = 11/20/20 Pct Recovery = 74% Analysis Date = 11/19/20 Pct Recovery = 74% Analysis Date = 11/19/20 Pct Recovery = 74% Analysis Date = 11/17/20 Pct Recovery = 74% Analysis Date = 11/17/20 Pct Recovery = 74% Analysis Date = 11/15/20 Pct Recovery = 74% Analysis Date = 11/15/20 Pct Recovery = 74% Analysis Date = 11/14/20 Pct Recovery = 74% Analysis Date = 11/14/20 Pct Recovery = 74% Analysis Date = 11/12/20 Pct Recovery = 74% Analysis Date = 11/12/20 Pct Recovery = 74% Analysis Date = 11/10/20 Pct Recovery = 74% Analysis Date = 11/10/20 Pct Recovery = 74% Analysis Date = 11/09/20 Pct Recovery = 74% Analysis Date = 11/09/20 Pct Recovery = 74% Analysis Date = 11/07/20 Pct Recovery = 74% Analysis Date = 11/07/20 Pct Recovery = 74% Analysis Date = 11/05/20 Pct Recovery = 74% Analysis Date = 11/05/20 Pct Recovery = 74% Analysis Date = 11/04/20 Pct Recovery = 74% Analysis Date = 11/04/20 Pct Recovery = 74% Analysis Date = 11/02/20 Pct Recovery = 75% Analysis Date = 11/02/20 Pct Recovery = 75% Analysis Date = 11/01/20 Pct Recovery = 75% Analysis Date = 11/01/20 Pct Recovery = 75% Analysis Date = 10/30/20 Pct Recovery = 75% Analysis Date = 10/30/20 Pct Recovery = 75% Analysis Date = 10/28/20 Pct Recovery = 75% Analysis Date = 10/28/20 Pct Recovery = 75% Analysis Date = 10/27/20 Pct Recovery = 75% Analysis Date = 10/27/20 Pct Recovery = 75% Analysis Date = 10/25/20 Pct Recovery = 74% Analysis Date = 10/25/20 Pct Recovery = 74% Analysis Date = 10/23/20 Pct Recovery = 74% Analysis Date = 10/23/20 Pct Recovery = 74% Analysis Date = 10/22/20 Pct Recovery = 74% Analysis Date = 10/22/20 Pct Recovery = 74% Analysis Date = 10/20/20 Pct Recovery = 74% Analysis Date = 10/20/20 Pct Recovery = 74% Analysis Date = 10/18/20 Pct Recovery = 74% Analysis Date = 10/18/20 Pct Recovery = 74% Analysis Date = 10/17/20 Pct Recovery = 74% Analysis Date = 10/17/20 Pct Recovery = 74% Analysis Date = 10/15/20 Pct Recovery = 75% Analysis Date = 10/15/20 Pct Recovery = 75% Analysis Date = 10/13/20 Pct Recovery = 75% Analysis Date = 10/13/20 Pct Recovery = 75% Analysis Date = 10/12/20 Pct Recovery = 76% Analysis Date = 10/12/20 Pct Recovery = 76% Analysis Date = 10/10/20 Pct Recovery = 76% Analysis Date = 10/10/20 Pct Recovery = 76% Analysis Date = 10/08/20 Pct Recovery = 77% Analysis Date = 10/08/20 Pct Recovery = 77% Analysis Date = 10/07/20 Pct Recovery = 77% Analysis Date = 10/07/20 Pct Recovery = 77% Analysis Date = 10/05/20 Pct Recovery = 78% Analysis Date = 10/05/20 Pct Recovery = 78% Analysis Date = 10/03/20 Pct Recovery = 78% Analysis Date = 10/03/20 Pct Recovery = 78% Analysis Date = 10/02/20 Pct Recovery = 79% Analysis Date = 10/02/20 Pct Recovery = 79% Analysis Date = 09/30/20 Pct Recovery = 79% Analysis Date = 09/30/20 Pct Recovery = 79% Analysis Date = 09/29/20 Pct Recovery = 80% Analysis Date = 09/29/20 Pct Recovery = 80% Analysis Date = 09/27/20 Pct Recovery = 80% Analysis Date = 09/27/20 Pct Recovery = 80% Analysis Date = 09/25/20 Pct Recovery = 81% Analysis Date = 09/25/20 Pct Recovery = 81% Analysis Date = 09/24/20 Pct Recovery = 81% Analysis Date = 09/24/20 Pct Recovery = 81% Analysis Date = 09/22/20 Pct Recovery = 82% Analysis Date = 09/22/20 Pct Recovery = 82% Analysis Date = 09/20/20 Pct Recovery = 83% Analysis Date = 09/20/20 Pct Recovery = 83% Analysis Date = 09/19/20 Pct Recovery = 83% Analysis Date = 09/19/20 Pct Recovery = 83% Analysis Date = 09/17/20 Pct Recovery = 84% Analysis Date = 09/17/20 Pct Recovery = 84% Analysis Date = 09/15/20 Pct Recovery = 84% Analysis Date = 09/15/20 Pct Recovery = 84% Analysis Date = 09/14/20 Pct Recovery = 85% Analysis Date = 09/14/20 Pct Recovery = 85% Analysis Date = 09/12/20 Pct Recovery = 85% Analysis Date = 09/12/20 Pct Recovery = 85% Analysis Date = 09/10/20 Pct Recovery = 85% Analysis Date = 09/10/20 Pct Recovery = 85% Analysis Date = 09/09/20 Pct Recovery = 86% Analysis Date = 09/09/20 Pct Recovery = 86% Analysis Date = 09/07/20 Pct Recovery = 86% Analysis Date = 09/07/20 Pct Recovery = 86% Analysis Date = 09/05/20 Pct Recovery = 87% Analysis Date = 09/05/20 Pct Recovery = 87% Analysis Date = 09/04/20 Pct Recovery = 87% Analysis Date = 09/04/20 Pct Recovery = 87% Analysis Date = 09/02/20 Pct Recovery = 87% Analysis Date = 09/02/20 Pct Recovery = 87% Analysis Date = 08/31/20 Pct Recovery = 88% Analysis Date = 08/31/20 Pct Recovery = 88% Analysis Date = 08/30/20 Pct Recovery = 88% Analysis Date = 08/30/20 Pct Recovery = 88% Analysis Date = 08/28/20 Pct Recovery = 89% Analysis Date = 08/28/20 Pct Recovery = 89% Analysis Date = 08/27/20 Pct Recovery = 89% Analysis Date = 08/27/20 Pct Recovery = 89% Analysis Date = 08/25/20 Pct Recovery = 89% Analysis Date = 08/25/20 Pct Recovery = 89% Analysis Date = 08/23/20 Pct Recovery = 90% Analysis Date = 08/23/20 Pct Recovery = 90% Analysis Date = 08/22/20 Pct Recovery = 90% Analysis Date = 08/22/20 Pct Recovery = 90% Analysis Date = 08/20/20 Pct Recovery = 91% Analysis Date = 08/20/20 Pct Recovery = 91% Analysis Date = 08/18/20 Pct Recovery = 91% Analysis Date = 08/18/20 Pct Recovery = 91% Analysis Date = 08/17/20 Pct Recovery = 91% Analysis Date = 08/17/20 Pct Recovery = 91% Analysis Date = 08/15/20 Pct Recovery = 91% Analysis Date = 08/15/20 Pct Recovery = 91% Analysis Date = 08/13/20 Pct Recovery = 92% Analysis Date = 08/13/20 Pct Recovery = 92% Analysis Date = 08/12/20 Pct Recovery = 92% Analysis Date = 08/12/20 Pct Recovery = 92% Analysis Date = 08/10/20 Pct Recovery = 92% Analysis Date = 08/10/20 Pct Recovery = 92% Analysis Date = 08/08/20 Pct Recovery = 93% Analysis Date = 08/08/20 Pct Recovery = 93% Analysis Date = 08/07/20 Pct Recovery = 93% Analysis Date = 08/07/20 Pct Recovery = 93% Analysis Date = 08/05/20 Pct Recovery = 94% Analysis Date = 08/05/20 Pct Recovery = 94% Analysis Date = 08/03/20 Pct Recovery = 94% Analysis Date = 08/03/20 Pct Recovery = 94% Analysis Date = 08/02/20 Pct Recovery = 95% Analysis Date = 08/02/20 Pct Recovery = 95% Analysis Date = 07/31/20 Pct Recovery = 95% Analysis Date = 07/31/20 Pct Recovery = 95% Analysis Date = 07/29/20 Pct Recovery = 96% Analysis Date = 07/29/20 Pct Recovery = 96% Analysis Date = 07/28/20 Pct Recovery = 97% Analysis Date = 07/28/20 Pct Recovery = 97% Analysis Date = 07/26/20 Pct Recovery = 97% Analysis Date = 07/26/20 Pct Recovery = 97% Analysis Date = 07/25/20 Pct Recovery = 98% Analysis Date = 07/25/20 Pct Recovery = 98% Analysis Date = 07/23/20 Pct Recovery = 98% Analysis Date = 07/23/20 Pct Recovery = 98% Analysis Date = 07/21/20 Pct Recovery = 99% Analysis Date = 07/21/20 Pct Recovery = 99% Analysis Date = 07/20/20 Pct Recovery = 99% Analysis Date = 07/20/20 Pct Recovery = 99% Analysis Date = 07/18/20 Pct Recovery = 100% Analysis Date = 07/18/20 Pct Recovery = 100% Analysis Date = 07/16/20 Pct Recovery = 100% Analysis Date = 07/16/20 Pct Recovery = 100% Analysis Date = 07/15/20 Pct Recovery = 101% Analysis Date = 07/15/20 Pct Recovery = 101% Analysis Date = 07/13/20 Pct Recovery = 102% Analysis Date = 07/13/20 Pct Recovery = 102% Analysis Date = 07/11/20 Pct Recovery = 102% Analysis Date = 07/11/20 Pct Recovery = 102% Analysis Date = 07/10/20 Pct Recovery = 103% Analysis Date = 07/10/20 Pct Recovery = 103% Analysis Date = 07/08/20 Pct Recovery = 103% Analysis Date = 07/08/20 Pct Recovery = 103% Analysis Date = 07/06/20 Pct Recovery = 104% Analysis Date = 07/06/20 Pct Recovery = 104% Analysis Date = 07/05/20 Pct Recovery = 105% Analysis Date = 07/05/20 Pct Recovery = 105% Analysis Date = 07/03/20 Pct Recovery = 105% Analysis Date = 07/03/20 Pct Recovery = 105% Analysis Date = 07/01/20 Pct Recovery = 106% Analysis Date = 07/01/20 Pct Recovery = 106% Analysis Date = 06/30/20 Pct Recovery = 106% Analysis Date = 06/30/20 Pct Recovery = 106% Analysis Date = 06/28/20 Pct Recovery = 107% Analysis Date = 06/28/20 Pct Recovery = 107% Analysis Date = 06/26/20 Pct Recovery = 107% Analysis Date = 06/26/20 Pct Recovery = 107% Analysis Date = 06/25/20 Pct Recovery = 108% Analysis Date = 06/25/20 Pct Recovery = 108% Analysis Date = 06/23/20 Pct Recovery = 109% Analysis Date = 06/23/20 Pct Recovery = 109% Analysis Date = 06/22/20 Pct Recovery = 109% Analysis Date = 06/22/20 Pct Recovery = 109% Analysis Date = 06/20/20 Pct Recovery = 110% Analysis Date = 06/20/20 Pct Recovery = 110% Analysis Date = 06/18/20 Pct Recovery = 110% Analysis Date = 06/18/20 Pct Recovery = 110% Analysis Date = 06/17/20 Pct Recovery = 111% Analysis Date = 06/17/20 Pct Recovery = 111% Analysis Date = 06/15/20 Pct Recovery = 111% Analysis Date = 06/15/20 Pct Recovery = 111% Analysis Date = 06/13/20 Pct Recovery = 112% Analysis Date = 06/13/20 Pct Recovery = 112% Analysis Date = 06/12/20 Pct Recovery = 112% Analysis Date = 06/12/20 Pct Recovery = 112% Analysis Date = 06/10/20 Pct Recovery = 113% Analysis Date = 06/10/20 Pct Recovery = 113% Analysis Date = 06/08/20 Pct Recovery = 114% Analysis Date = 06/08/20 Pct Recovery = 114% Analysis Date = 06/07/20 Pct Recovery = 114% Analysis Date = 06/07/20 Pct Recovery = 114% Analysis Date = 06/05/20 Pct Recovery = 115% Analysis Date = 06/05/20 Pct Recovery = 115% Analysis Date = 06/03/20 Pct Recovery = 115% Analysis Date = 06/03/20 Pct Recovery = 115% Analysis Date = 06/02/20 Pct Recovery = 116% Analysis Date = 06/02/20 Pct Recovery = 116% Analysis Date = 05/31/20 Pct Recovery = 117% Analysis Date = 05/31/20 Pct Recovery = 117% Analysis Date = 05/29/20 Pct Recovery = 117% Analysis Date = 05/29/20 Pct Recovery = 117% Analysis Date = 05/28/20 Pct Recovery = 118% Analysis Date = 05/28/20 Pct Recovery = 118% Analysis Date = 05/26/20 Pct Recovery = 119% Analysis Date = 05/26/20 Pct Recovery = 119% Analysis Date = 05/24/20 Pct Recovery = 119% Analysis Date = 05/24/20 Pct Recovery = 119% Analysis Date = 05/23/20 Pct Recovery = 120% Analysis Date = 05/23/20 Pct Recovery = 120% Analysis Date = 05/21/20 Pct Recovery = 120% Analysis Date = 05/21/20 Pct Recovery = 120% Analysis Date = 05/20/20 Pct Recovery = 121% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOLACHLOR SULFONIC ACID

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 24 87% 25% 78% 27%
Total 24 87% 25% 78% 27%

Sample Statistics
METOLACHLOR SULFONIC ACID

Characteristic N % % Basis
Plotted 24 92% Spiked
Estimated Values 7 27% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 26 .  
False Negatives 2 8% 2 out of 26
Not Spiked 90 .  
False Positives 0 0% 0 out of 90

OBSP Determination:
METRIBUZIN
METHOD: 2447 , TESTIDCODE: 68652LCM60

Laboratory ID = 20203230021 Lab Value = 220.860 Expected Conc. = 252 Report level label = 20 Pct Recovery = 88% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 251.909 Expected Conc. = 252 Report level label = 20 Pct Recovery = 100% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 255.671 Expected Conc. = 250.3 Report level label = 20 Pct Recovery = 102% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 261.162 Expected Conc. = 250.3 Report level label = 20 Pct Recovery = 104% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221940196 Lab Value = 163.294 Expected Conc. = 200 Report level label = 20 Pct Recovery = 82% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 183.629 Expected Conc. = 199.2 Report level label = 20 Pct Recovery = 92% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 227.435 Expected Conc. = 198.8 Report level label = 20 Pct Recovery = 114% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20203360042 Lab Value = 119.315 Expected Conc. = 125.15 Report level label = 20 Pct Recovery = 95% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 143.566 Expected Conc. = 125.15 Report level label = 20 Pct Recovery = 115% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201550031 Lab Value = 172.118 Expected Conc. = 124.9 Report level label = 20 Pct Recovery = 138% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20220740064 Lab Value = 88.738 Expected Conc. = 124.5 Report level label = 20 Pct Recovery = 71% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20221870197 Lab Value = 85.180 Expected Conc. = 124.25 Report level label = 20 Pct Recovery = 69% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20202390020 Lab Value = 137.652 Expected Conc. = 124.1 Report level label = 20 Pct Recovery = 111% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 136.638 Expected Conc. = 124.1 Report level label = 20 Pct Recovery = 110% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201960104 Lab Value = 119.890 Expected Conc. = 99.28 Report level label = 20 Pct Recovery = 121% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 141.506 Expected Conc. = 99.28 Report level label = 20 Pct Recovery = 143% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210830019 Lab Value = 53.021 Expected Conc. = 50.4 Report level label = 20 Pct Recovery = 105% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 47.630 Expected Conc. = 50.4 Report level label = 20 Pct Recovery = 95% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 47.108 Expected Conc. = 50.06 Report level label = 20 Pct Recovery = 94% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 50.640 Expected Conc. = 50.06 Report level label = 20 Pct Recovery = 101% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 58.682 Expected Conc. = 50.06 Report level label = 20 Pct Recovery = 117% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 40.700 Expected Conc. = 50.06 Report level label = 20 Pct Recovery = 81% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 42.208 Expected Conc. = 50.06 Report level label = 20 Pct Recovery = 84% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 51.812 Expected Conc. = 50.06 Report level label = 20 Pct Recovery = 103% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202330309 Lab Value = 55.951 Expected Conc. = 49.96 Report level label = 20 Pct Recovery = 112% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 31.390 Expected Conc. = 49.96 Report level label = 20 Pct Recovery = 63% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 52.367 Expected Conc. = 49.96 Report level label = 20 Pct Recovery = 105% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 41.015 Expected Conc. = 49.96 Report level label = 20 Pct Recovery = 82% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 72.618 Expected Conc. = 49.96 Report level label = 20 Pct Recovery = 145% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20221660151 Lab Value = 45.027 Expected Conc. = 49.7 Report level label = 20 Pct Recovery = 91% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Analysis Date = 08/15/22 Pct Recovery = 86% Analysis Date = 08/10/22 Pct Recovery = 86% Analysis Date = 08/10/22 Pct Recovery = 86% Analysis Date = 08/06/22 Pct Recovery = 86% Analysis Date = 08/06/22 Pct Recovery = 86% Analysis Date = 08/02/22 Pct Recovery = 86% Analysis Date = 08/02/22 Pct Recovery = 86% Analysis Date = 07/29/22 Pct Recovery = 86% Analysis Date = 07/29/22 Pct Recovery = 86% Analysis Date = 07/25/22 Pct Recovery = 86% Analysis Date = 07/25/22 Pct Recovery = 86% Analysis Date = 07/21/22 Pct Recovery = 86% Analysis Date = 07/21/22 Pct Recovery = 86% Analysis Date = 07/17/22 Pct Recovery = 86% Analysis Date = 07/17/22 Pct Recovery = 86% Analysis Date = 07/13/22 Pct Recovery = 86% Analysis Date = 07/13/22 Pct Recovery = 86% Analysis Date = 07/09/22 Pct Recovery = 86% Analysis Date = 07/09/22 Pct Recovery = 86% Analysis Date = 07/05/22 Pct Recovery = 87% Analysis Date = 07/05/22 Pct Recovery = 87% Analysis Date = 07/01/22 Pct Recovery = 87% Analysis Date = 07/01/22 Pct Recovery = 87% Analysis Date = 06/27/22 Pct Recovery = 87% Analysis Date = 06/27/22 Pct Recovery = 87% Analysis Date = 06/23/22 Pct Recovery = 87% Analysis Date = 06/23/22 Pct Recovery = 87% Analysis Date = 06/19/22 Pct Recovery = 87% Analysis Date = 06/19/22 Pct Recovery = 87% Analysis Date = 06/15/22 Pct Recovery = 87% Analysis Date = 06/15/22 Pct Recovery = 87% Analysis Date = 06/11/22 Pct Recovery = 87% Analysis Date = 06/11/22 Pct Recovery = 87% Analysis Date = 06/07/22 Pct Recovery = 87% Analysis Date = 06/07/22 Pct Recovery = 87% Analysis Date = 06/03/22 Pct Recovery = 87% Analysis Date = 06/03/22 Pct Recovery = 87% Analysis Date = 05/30/22 Pct Recovery = 87% Analysis Date = 05/30/22 Pct Recovery = 87% Analysis Date = 05/26/22 Pct Recovery = 87% Analysis Date = 05/26/22 Pct Recovery = 87% Analysis Date = 05/22/22 Pct Recovery = 87% Analysis Date = 05/22/22 Pct Recovery = 87% Analysis Date = 05/18/22 Pct Recovery = 88% Analysis Date = 05/18/22 Pct Recovery = 88% Analysis Date = 05/14/22 Pct Recovery = 88% Analysis Date = 05/14/22 Pct Recovery = 88% Analysis Date = 05/10/22 Pct Recovery = 88% Analysis Date = 05/10/22 Pct Recovery = 88% Analysis Date = 05/06/22 Pct Recovery = 88% Analysis Date = 05/06/22 Pct Recovery = 88% Analysis Date = 05/01/22 Pct Recovery = 88% Analysis Date = 05/01/22 Pct Recovery = 88% Analysis Date = 04/27/22 Pct Recovery = 88% Analysis Date = 04/27/22 Pct Recovery = 88% Analysis Date = 04/23/22 Pct Recovery = 88% Analysis Date = 04/23/22 Pct Recovery = 88% Analysis Date = 04/19/22 Pct Recovery = 88% Analysis Date = 04/19/22 Pct Recovery = 88% Analysis Date = 04/15/22 Pct Recovery = 88% Analysis Date = 04/15/22 Pct Recovery = 88% Analysis Date = 04/11/22 Pct Recovery = 88% Analysis Date = 04/11/22 Pct Recovery = 88% Analysis Date = 04/07/22 Pct Recovery = 88% Analysis Date = 04/07/22 Pct Recovery = 88% Analysis Date = 04/03/22 Pct Recovery = 88% Analysis Date = 04/03/22 Pct Recovery = 88% Analysis Date = 03/30/22 Pct Recovery = 89% Analysis Date = 03/30/22 Pct Recovery = 89% Analysis Date = 03/26/22 Pct Recovery = 89% Analysis Date = 03/26/22 Pct Recovery = 89% Analysis Date = 03/22/22 Pct Recovery = 89% Analysis Date = 03/22/22 Pct Recovery = 89% Analysis Date = 03/18/22 Pct Recovery = 89% Analysis Date = 03/18/22 Pct Recovery = 89% Analysis Date = 03/14/22 Pct Recovery = 89% Analysis Date = 03/14/22 Pct Recovery = 89% Analysis Date = 03/10/22 Pct Recovery = 89% Analysis Date = 03/10/22 Pct Recovery = 89% Analysis Date = 03/06/22 Pct Recovery = 89% Analysis Date = 03/06/22 Pct Recovery = 89% Analysis Date = 03/02/22 Pct Recovery = 89% Analysis Date = 03/02/22 Pct Recovery = 89% Analysis Date = 02/26/22 Pct Recovery = 89% Analysis Date = 02/26/22 Pct Recovery = 89% Analysis Date = 02/22/22 Pct Recovery = 89% Analysis Date = 02/22/22 Pct Recovery = 89% Analysis Date = 02/18/22 Pct Recovery = 90% Analysis Date = 02/18/22 Pct Recovery = 90% Analysis Date = 02/14/22 Pct Recovery = 90% Analysis Date = 02/14/22 Pct Recovery = 90% Analysis Date = 02/10/22 Pct Recovery = 90% Analysis Date = 02/10/22 Pct Recovery = 90% Analysis Date = 02/06/22 Pct Recovery = 90% Analysis Date = 02/06/22 Pct Recovery = 90% Analysis Date = 02/02/22 Pct Recovery = 90% Analysis Date = 02/02/22 Pct Recovery = 90% Analysis Date = 01/29/22 Pct Recovery = 90% Analysis Date = 01/29/22 Pct Recovery = 90% Analysis Date = 01/25/22 Pct Recovery = 90% Analysis Date = 01/25/22 Pct Recovery = 90% Analysis Date = 01/20/22 Pct Recovery = 90% Analysis Date = 01/20/22 Pct Recovery = 90% Analysis Date = 01/16/22 Pct Recovery = 90% Analysis Date = 01/16/22 Pct Recovery = 90% Analysis Date = 01/12/22 Pct Recovery = 90% Analysis Date = 01/12/22 Pct Recovery = 90% Analysis Date = 01/08/22 Pct Recovery = 91% Analysis Date = 01/08/22 Pct Recovery = 91% Analysis Date = 01/04/22 Pct Recovery = 91% Analysis Date = 01/04/22 Pct Recovery = 91% Analysis Date = 12/31/21 Pct Recovery = 91% Analysis Date = 12/31/21 Pct Recovery = 91% Analysis Date = 12/27/21 Pct Recovery = 91% Analysis Date = 12/27/21 Pct Recovery = 91% Analysis Date = 12/23/21 Pct Recovery = 91% Analysis Date = 12/23/21 Pct Recovery = 91% Analysis Date = 12/19/21 Pct Recovery = 91% Analysis Date = 12/19/21 Pct Recovery = 91% Analysis Date = 12/15/21 Pct Recovery = 91% Analysis Date = 12/15/21 Pct Recovery = 91% Analysis Date = 12/11/21 Pct Recovery = 91% Analysis Date = 12/11/21 Pct Recovery = 91% Analysis Date = 12/07/21 Pct Recovery = 91% Analysis Date = 12/07/21 Pct Recovery = 91% Analysis Date = 12/03/21 Pct Recovery = 92% Analysis Date = 12/03/21 Pct Recovery = 92% Analysis Date = 11/29/21 Pct Recovery = 92% Analysis Date = 11/29/21 Pct Recovery = 92% Analysis Date = 11/25/21 Pct Recovery = 92% Analysis Date = 11/25/21 Pct Recovery = 92% Analysis Date = 11/21/21 Pct Recovery = 92% Analysis Date = 11/21/21 Pct Recovery = 92% Analysis Date = 11/17/21 Pct Recovery = 92% Analysis Date = 11/17/21 Pct Recovery = 92% Analysis Date = 11/13/21 Pct Recovery = 92% Analysis Date = 11/13/21 Pct Recovery = 92% Analysis Date = 11/09/21 Pct Recovery = 92% Analysis Date = 11/09/21 Pct Recovery = 92% Analysis Date = 11/05/21 Pct Recovery = 92% Analysis Date = 11/05/21 Pct Recovery = 92% Analysis Date = 11/01/21 Pct Recovery = 92% Analysis Date = 11/01/21 Pct Recovery = 92% Analysis Date = 10/28/21 Pct Recovery = 92% Analysis Date = 10/28/21 Pct Recovery = 92% Analysis Date = 10/24/21 Pct Recovery = 93% Analysis Date = 10/24/21 Pct Recovery = 93% Analysis Date = 10/20/21 Pct Recovery = 93% Analysis Date = 10/20/21 Pct Recovery = 93% Analysis Date = 10/16/21 Pct Recovery = 93% Analysis Date = 10/16/21 Pct Recovery = 93% Analysis Date = 10/11/21 Pct Recovery = 93% Analysis Date = 10/11/21 Pct Recovery = 93% Analysis Date = 10/07/21 Pct Recovery = 93% Analysis Date = 10/07/21 Pct Recovery = 93% Analysis Date = 10/03/21 Pct Recovery = 93% Analysis Date = 10/03/21 Pct Recovery = 93% Analysis Date = 09/29/21 Pct Recovery = 93% Analysis Date = 09/29/21 Pct Recovery = 93% Analysis Date = 09/25/21 Pct Recovery = 93% Analysis Date = 09/25/21 Pct Recovery = 93% Analysis Date = 09/21/21 Pct Recovery = 93% Analysis Date = 09/21/21 Pct Recovery = 93% Analysis Date = 09/17/21 Pct Recovery = 94% Analysis Date = 09/17/21 Pct Recovery = 94% Analysis Date = 09/13/21 Pct Recovery = 94% Analysis Date = 09/13/21 Pct Recovery = 94% Analysis Date = 09/09/21 Pct Recovery = 94% Analysis Date = 09/09/21 Pct Recovery = 94% Analysis Date = 09/05/21 Pct Recovery = 94% Analysis Date = 09/05/21 Pct Recovery = 94% Analysis Date = 09/01/21 Pct Recovery = 94% Analysis Date = 09/01/21 Pct Recovery = 94% Analysis Date = 08/28/21 Pct Recovery = 94% Analysis Date = 08/28/21 Pct Recovery = 94% Analysis Date = 08/24/21 Pct Recovery = 94% Analysis Date = 08/24/21 Pct Recovery = 94% Analysis Date = 08/20/21 Pct Recovery = 94% Analysis Date = 08/20/21 Pct Recovery = 94% Analysis Date = 08/16/21 Pct Recovery = 94% Analysis Date = 08/16/21 Pct Recovery = 94% Analysis Date = 08/12/21 Pct Recovery = 94% Analysis Date = 08/12/21 Pct Recovery = 94% Analysis Date = 08/08/21 Pct Recovery = 95% Analysis Date = 08/08/21 Pct Recovery = 95% Analysis Date = 08/04/21 Pct Recovery = 95% Analysis Date = 08/04/21 Pct Recovery = 95% Analysis Date = 07/31/21 Pct Recovery = 95% Analysis Date = 07/31/21 Pct Recovery = 95% Analysis Date = 07/27/21 Pct Recovery = 95% Analysis Date = 07/27/21 Pct Recovery = 95% Analysis Date = 07/23/21 Pct Recovery = 95% Analysis Date = 07/23/21 Pct Recovery = 95% Analysis Date = 07/19/21 Pct Recovery = 95% Analysis Date = 07/19/21 Pct Recovery = 95% Analysis Date = 07/15/21 Pct Recovery = 95% Analysis Date = 07/15/21 Pct Recovery = 95% Analysis Date = 07/11/21 Pct Recovery = 95% Analysis Date = 07/11/21 Pct Recovery = 95% Analysis Date = 07/07/21 Pct Recovery = 95% Analysis Date = 07/07/21 Pct Recovery = 95% Analysis Date = 07/02/21 Pct Recovery = 96% Analysis Date = 07/02/21 Pct Recovery = 96% Analysis Date = 06/28/21 Pct Recovery = 96% Analysis Date = 06/28/21 Pct Recovery = 96% Analysis Date = 06/24/21 Pct Recovery = 96% Analysis Date = 06/24/21 Pct Recovery = 96% Analysis Date = 06/20/21 Pct Recovery = 96% Analysis Date = 06/20/21 Pct Recovery = 96% Analysis Date = 06/16/21 Pct Recovery = 96% Analysis Date = 06/16/21 Pct Recovery = 96% Analysis Date = 06/12/21 Pct Recovery = 96% Analysis Date = 06/12/21 Pct Recovery = 96% Analysis Date = 06/08/21 Pct Recovery = 96% Analysis Date = 06/08/21 Pct Recovery = 96% Analysis Date = 06/04/21 Pct Recovery = 96% Analysis Date = 06/04/21 Pct Recovery = 96% Analysis Date = 05/31/21 Pct Recovery = 96% Analysis Date = 05/31/21 Pct Recovery = 96% Analysis Date = 05/27/21 Pct Recovery = 96% Analysis Date = 05/27/21 Pct Recovery = 96% Analysis Date = 05/23/21 Pct Recovery = 97% Analysis Date = 05/23/21 Pct Recovery = 97% Analysis Date = 05/19/21 Pct Recovery = 97% Analysis Date = 05/19/21 Pct Recovery = 97% Analysis Date = 05/15/21 Pct Recovery = 97% Analysis Date = 05/15/21 Pct Recovery = 97% Analysis Date = 05/11/21 Pct Recovery = 97% Analysis Date = 05/11/21 Pct Recovery = 97% Analysis Date = 05/07/21 Pct Recovery = 97% Analysis Date = 05/07/21 Pct Recovery = 97% Analysis Date = 05/03/21 Pct Recovery = 97% Analysis Date = 05/03/21 Pct Recovery = 97% Analysis Date = 04/29/21 Pct Recovery = 97% Analysis Date = 04/29/21 Pct Recovery = 97% Analysis Date = 04/25/21 Pct Recovery = 97% Analysis Date = 04/25/21 Pct Recovery = 97% Analysis Date = 04/21/21 Pct Recovery = 97% Analysis Date = 04/21/21 Pct Recovery = 97% Analysis Date = 04/17/21 Pct Recovery = 97% Analysis Date = 04/17/21 Pct Recovery = 97% Analysis Date = 04/13/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 98% Analysis Date = 04/09/21 Pct Recovery = 98% Analysis Date = 04/09/21 Pct Recovery = 98% Analysis Date = 04/05/21 Pct Recovery = 98% Analysis Date = 04/05/21 Pct Recovery = 98% Analysis Date = 04/01/21 Pct Recovery = 98% Analysis Date = 04/01/21 Pct Recovery = 98% Analysis Date = 03/28/21 Pct Recovery = 98% Analysis Date = 03/28/21 Pct Recovery = 98% Analysis Date = 03/23/21 Pct Recovery = 98% Analysis Date = 03/23/21 Pct Recovery = 98% Analysis Date = 03/19/21 Pct Recovery = 98% Analysis Date = 03/19/21 Pct Recovery = 98% Analysis Date = 03/15/21 Pct Recovery = 98% Analysis Date = 03/15/21 Pct Recovery = 98% Analysis Date = 03/11/21 Pct Recovery = 98% Analysis Date = 03/11/21 Pct Recovery = 98% Analysis Date = 03/07/21 Pct Recovery = 98% Analysis Date = 03/07/21 Pct Recovery = 98% Analysis Date = 03/03/21 Pct Recovery = 98% Analysis Date = 03/03/21 Pct Recovery = 98% Analysis Date = 02/27/21 Pct Recovery = 98% Analysis Date = 02/27/21 Pct Recovery = 98% Analysis Date = 02/23/21 Pct Recovery = 98% Analysis Date = 02/23/21 Pct Recovery = 98% Analysis Date = 02/19/21 Pct Recovery = 98% Analysis Date = 02/19/21 Pct Recovery = 98% Analysis Date = 02/15/21 Pct Recovery = 98% Analysis Date = 02/15/21 Pct Recovery = 98% Analysis Date = 02/11/21 Pct Recovery = 98% Analysis Date = 02/11/21 Pct Recovery = 98% Analysis Date = 02/07/21 Pct Recovery = 98% Analysis Date = 02/07/21 Pct Recovery = 98% Analysis Date = 02/03/21 Pct Recovery = 98% Analysis Date = 02/03/21 Pct Recovery = 98% Analysis Date = 01/30/21 Pct Recovery = 98% Analysis Date = 01/30/21 Pct Recovery = 98% Analysis Date = 01/26/21 Pct Recovery = 98% Analysis Date = 01/26/21 Pct Recovery = 98% Analysis Date = 01/22/21 Pct Recovery = 98% Analysis Date = 01/22/21 Pct Recovery = 98% Analysis Date = 01/18/21 Pct Recovery = 98% Analysis Date = 01/18/21 Pct Recovery = 98% Analysis Date = 01/14/21 Pct Recovery = 98% Analysis Date = 01/14/21 Pct Recovery = 98% Analysis Date = 01/10/21 Pct Recovery = 98% Analysis Date = 01/10/21 Pct Recovery = 98% Analysis Date = 01/06/21 Pct Recovery = 98% Analysis Date = 01/06/21 Pct Recovery = 98% Analysis Date = 01/02/21 Pct Recovery = 99% Analysis Date = 01/02/21 Pct Recovery = 99% Analysis Date = 12/29/20 Pct Recovery = 99% Analysis Date = 12/29/20 Pct Recovery = 99% Analysis Date = 12/25/20 Pct Recovery = 99% Analysis Date = 12/25/20 Pct Recovery = 99% Analysis Date = 12/21/20 Pct Recovery = 99% Analysis Date = 12/21/20 Pct Recovery = 99% Analysis Date = 12/17/20 Pct Recovery = 99% Analysis Date = 12/17/20 Pct Recovery = 99% Analysis Date = 12/12/20 Pct Recovery = 99% Analysis Date = 12/12/20 Pct Recovery = 99% Analysis Date = 12/08/20 Pct Recovery = 99% Analysis Date = 12/08/20 Pct Recovery = 99% Analysis Date = 12/04/20 Pct Recovery = 99% Analysis Date = 12/04/20 Pct Recovery = 99% Analysis Date = 11/30/20 Pct Recovery = 99% Analysis Date = 11/30/20 Pct Recovery = 99% Analysis Date = 11/26/20 Pct Recovery = 99% Analysis Date = 11/26/20 Pct Recovery = 99% Analysis Date = 11/22/20 Pct Recovery = 99% Analysis Date = 11/22/20 Pct Recovery = 99% Analysis Date = 11/18/20 Pct Recovery = 100% Analysis Date = 11/18/20 Pct Recovery = 100% Analysis Date = 11/14/20 Pct Recovery = 100% Analysis Date = 11/14/20 Pct Recovery = 100% Analysis Date = 11/10/20 Pct Recovery = 100% Analysis Date = 11/10/20 Pct Recovery = 100% Analysis Date = 11/06/20 Pct Recovery = 100% Analysis Date = 11/06/20 Pct Recovery = 100% Analysis Date = 11/02/20 Pct Recovery = 100% Analysis Date = 11/02/20 Pct Recovery = 100% Analysis Date = 10/29/20 Pct Recovery = 100% Analysis Date = 10/29/20 Pct Recovery = 100% Analysis Date = 10/25/20 Pct Recovery = 100% Analysis Date = 10/25/20 Pct Recovery = 100% Analysis Date = 10/21/20 Pct Recovery = 100% Analysis Date = 10/21/20 Pct Recovery = 100% Analysis Date = 10/17/20 Pct Recovery = 100% Analysis Date = 10/17/20 Pct Recovery = 100% Analysis Date = 10/13/20 Pct Recovery = 100% Analysis Date = 10/13/20 Pct Recovery = 100% Analysis Date = 10/09/20 Pct Recovery = 101% Analysis Date = 10/09/20 Pct Recovery = 101% Analysis Date = 10/05/20 Pct Recovery = 101% Analysis Date = 10/05/20 Pct Recovery = 101% Analysis Date = 10/01/20 Pct Recovery = 101% Analysis Date = 10/01/20 Pct Recovery = 101% Analysis Date = 09/27/20 Pct Recovery = 101% Analysis Date = 09/27/20 Pct Recovery = 101% Analysis Date = 09/23/20 Pct Recovery = 101% Analysis Date = 09/23/20 Pct Recovery = 101% Analysis Date = 09/19/20 Pct Recovery = 101% Analysis Date = 09/19/20 Pct Recovery = 101% Analysis Date = 09/15/20 Pct Recovery = 102% Analysis Date = 09/15/20 Pct Recovery = 102% Analysis Date = 09/11/20 Pct Recovery = 102% Analysis Date = 09/11/20 Pct Recovery = 102% Analysis Date = 09/07/20 Pct Recovery = 102% Analysis Date = 09/07/20 Pct Recovery = 102% Analysis Date = 09/02/20 Pct Recovery = 103% Analysis Date = 09/02/20 Pct Recovery = 103% Analysis Date = 08/29/20 Pct Recovery = 104% Analysis Date = 08/29/20 Pct Recovery = 104% Analysis Date = 08/25/20 Pct Recovery = 105% Analysis Date = 08/25/20 Pct Recovery = 105% Analysis Date = 08/21/20 Pct Recovery = 106% Analysis Date = 08/21/20 Pct Recovery = 106% Analysis Date = 08/17/20 Pct Recovery = 107% Analysis Date = 08/17/20 Pct Recovery = 107% Analysis Date = 08/13/20 Pct Recovery = 108% Analysis Date = 08/13/20 Pct Recovery = 108% Analysis Date = 08/09/20 Pct Recovery = 109% Analysis Date = 08/09/20 Pct Recovery = 109% Analysis Date = 08/05/20 Pct Recovery = 110% Analysis Date = 08/05/20 Pct Recovery = 110% Analysis Date = 08/01/20 Pct Recovery = 111% Analysis Date = 08/01/20 Pct Recovery = 111% Analysis Date = 07/28/20 Pct Recovery = 112% Analysis Date = 07/28/20 Pct Recovery = 112% Analysis Date = 07/24/20 Pct Recovery = 113% Analysis Date = 07/24/20 Pct Recovery = 113% Analysis Date = 07/20/20 Pct Recovery = 114% Analysis Date = 07/20/20 Pct Recovery = 114% Analysis Date = 07/16/20 Pct Recovery = 115% Analysis Date = 07/16/20 Pct Recovery = 115% Analysis Date = 07/12/20 Pct Recovery = 116% Analysis Date = 07/12/20 Pct Recovery = 116% Analysis Date = 07/08/20 Pct Recovery = 117% Analysis Date = 07/08/20 Pct Recovery = 117% Analysis Date = 07/04/20 Pct Recovery = 118% Analysis Date = 07/04/20 Pct Recovery = 118% Analysis Date = 06/30/20 Pct Recovery = 120% Analysis Date = 06/30/20 Pct Recovery = 120% Analysis Date = 06/26/20 Pct Recovery = 121% Analysis Date = 06/26/20 Pct Recovery = 121% Analysis Date = 06/22/20 Pct Recovery = 122% Analysis Date = 06/22/20 Pct Recovery = 122% Analysis Date = 06/18/20 Pct Recovery = 123% Analysis Date = 06/18/20 Pct Recovery = 123% Analysis Date = 06/14/20 Pct Recovery = 124% Analysis Date = 06/14/20 Pct Recovery = 124% Analysis Date = 06/10/20 Pct Recovery = 125% Analysis Date = 06/10/20 Pct Recovery = 125% Analysis Date = 06/06/20 Pct Recovery = 126% Analysis Date = 06/06/20 Pct Recovery = 126% Analysis Date = 06/02/20 Pct Recovery = 128% Analysis Date = 06/02/20 Pct Recovery = 128% Analysis Date = 05/29/20 Pct Recovery = 129% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METRIBUZIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 30 101% 20% 102% 18%
Total 30 101% 20% 102% 18%

Sample Statistics
METRIBUZIN

Characteristic N % % Basis
Plotted 30 97% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 1 3% 1 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
MYCLOBUTANIL
METHOD: 2447 , TESTIDCODE: 66632LCM60

Laboratory ID = 20210760015 Lab Value = 67.100 Expected Conc. = 88 Report level label = 7 Pct Recovery = 76% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 73.860 Expected Conc. = 88 Report level label = 7 Pct Recovery = 84% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 70.544 Expected Conc. = 88 Report level label = 7 Pct Recovery = 80% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 84.680 Expected Conc. = 88 Report level label = 7 Pct Recovery = 96% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 59.467 Expected Conc. = 87.2 Report level label = 7 Pct Recovery = 68% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 86.141 Expected Conc. = 87.2 Report level label = 7 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 90.090 Expected Conc. = 87.2 Report level label = 7 Pct Recovery = 103% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221520237 Lab Value = 71.128 Expected Conc. = 70.64 Report level label = 7 Pct Recovery = 101% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 50.659 Expected Conc. = 70 Report level label = 7 Pct Recovery = 72% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 45.896 Expected Conc. = 69.2 Report level label = 7 Pct Recovery = 66% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20220740064 Lab Value = 30.905 Expected Conc. = 44.25 Report level label = 7 Pct Recovery = 70% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20221870197 Lab Value = 40.122 Expected Conc. = 44.15 Report level label = 7 Pct Recovery = 91% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 35.693 Expected Conc. = 44 Report level label = 7 Pct Recovery = 81% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202390020 Lab Value = 54.693 Expected Conc. = 43.85 Report level label = 7 Pct Recovery = 125% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 42.760 Expected Conc. = 43.85 Report level label = 7 Pct Recovery = 98% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201550031 Lab Value = 35.539 Expected Conc. = 43.8 Report level label = 7 Pct Recovery = 81% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20202880004 Lab Value = 45.986 Expected Conc. = 43.6 Report level label = 7 Pct Recovery = 105% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 31.475 Expected Conc. = 35.2 Report level label = 7 Pct Recovery = 89% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201960104 Lab Value = 45.030 Expected Conc. = 35.08 Report level label = 7 Pct Recovery = 128% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 29.468 Expected Conc. = 35.08 Report level label = 7 Pct Recovery = 84% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210620006 Lab Value = 32.276 Expected Conc. = 34.88 Report level label = 7 Pct Recovery = 93% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 30.303 Expected Conc. = 34.88 Report level label = 7 Pct Recovery = 87% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221660151 Lab Value = 15.480 Expected Conc. = 17.66 Report level label = 7 Pct Recovery = 88% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20202330309 Lab Value = 14.879 Expected Conc. = 17.52 Report level label = 7 Pct Recovery = 85% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 13.089 Expected Conc. = 17.52 Report level label = 7 Pct Recovery = 75% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 20.758 Expected Conc. = 17.52 Report level label = 7 Pct Recovery = 118% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 15.333 Expected Conc. = 17.52 Report level label = 7 Pct Recovery = 88% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 16.079 Expected Conc. = 17.52 Report level label = 7 Pct Recovery = 92% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210120050 Lab Value = 13.702 Expected Conc. = 17.44 Report level label = 7 Pct Recovery = 79% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 17.581 Expected Conc. = 17.44 Report level label = 7 Pct Recovery = 101% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 12.473 Expected Conc. = 17.44 Report level label = 7 Pct Recovery = 72% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 16.230 Expected Conc. = 17.44 Report level label = 7 Pct Recovery = 93% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 18.965 Expected Conc. = 17.44 Report level label = 7 Pct Recovery = 109% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 81% Analysis Date = 08/10/22 Pct Recovery = 81% Analysis Date = 08/10/22 Pct Recovery = 81% Analysis Date = 08/06/22 Pct Recovery = 81% Analysis Date = 08/06/22 Pct Recovery = 81% Analysis Date = 08/02/22 Pct Recovery = 81% Analysis Date = 08/02/22 Pct Recovery = 81% Analysis Date = 07/29/22 Pct Recovery = 81% Analysis Date = 07/29/22 Pct Recovery = 81% Analysis Date = 07/25/22 Pct Recovery = 81% Analysis Date = 07/25/22 Pct Recovery = 81% Analysis Date = 07/21/22 Pct Recovery = 81% Analysis Date = 07/21/22 Pct Recovery = 81% Analysis Date = 07/17/22 Pct Recovery = 81% Analysis Date = 07/17/22 Pct Recovery = 81% Analysis Date = 07/13/22 Pct Recovery = 81% Analysis Date = 07/13/22 Pct Recovery = 81% Analysis Date = 07/09/22 Pct Recovery = 81% Analysis Date = 07/09/22 Pct Recovery = 81% Analysis Date = 07/05/22 Pct Recovery = 81% Analysis Date = 07/05/22 Pct Recovery = 81% Analysis Date = 07/01/22 Pct Recovery = 81% Analysis Date = 07/01/22 Pct Recovery = 81% Analysis Date = 06/27/22 Pct Recovery = 81% Analysis Date = 06/27/22 Pct Recovery = 81% Analysis Date = 06/23/22 Pct Recovery = 81% Analysis Date = 06/23/22 Pct Recovery = 81% Analysis Date = 06/19/22 Pct Recovery = 81% Analysis Date = 06/19/22 Pct Recovery = 81% Analysis Date = 06/15/22 Pct Recovery = 81% Analysis Date = 06/15/22 Pct Recovery = 81% Analysis Date = 06/11/22 Pct Recovery = 81% Analysis Date = 06/11/22 Pct Recovery = 81% Analysis Date = 06/07/22 Pct Recovery = 81% Analysis Date = 06/07/22 Pct Recovery = 81% Analysis Date = 06/03/22 Pct Recovery = 81% Analysis Date = 06/03/22 Pct Recovery = 81% Analysis Date = 05/30/22 Pct Recovery = 81% Analysis Date = 05/30/22 Pct Recovery = 81% Analysis Date = 05/26/22 Pct Recovery = 82% Analysis Date = 05/26/22 Pct Recovery = 82% Analysis Date = 05/22/22 Pct Recovery = 82% Analysis Date = 05/22/22 Pct Recovery = 82% Analysis Date = 05/18/22 Pct Recovery = 82% Analysis Date = 05/18/22 Pct Recovery = 82% Analysis Date = 05/14/22 Pct Recovery = 82% Analysis Date = 05/14/22 Pct Recovery = 82% Analysis Date = 05/10/22 Pct Recovery = 82% Analysis Date = 05/10/22 Pct Recovery = 82% Analysis Date = 05/06/22 Pct Recovery = 82% Analysis Date = 05/06/22 Pct Recovery = 82% Analysis Date = 05/01/22 Pct Recovery = 82% Analysis Date = 05/01/22 Pct Recovery = 82% Analysis Date = 04/27/22 Pct Recovery = 82% Analysis Date = 04/27/22 Pct Recovery = 82% Analysis Date = 04/23/22 Pct Recovery = 82% Analysis Date = 04/23/22 Pct Recovery = 82% Analysis Date = 04/19/22 Pct Recovery = 82% Analysis Date = 04/19/22 Pct Recovery = 82% Analysis Date = 04/15/22 Pct Recovery = 82% Analysis Date = 04/15/22 Pct Recovery = 82% Analysis Date = 04/11/22 Pct Recovery = 82% Analysis Date = 04/11/22 Pct Recovery = 82% Analysis Date = 04/07/22 Pct Recovery = 82% Analysis Date = 04/07/22 Pct Recovery = 82% Analysis Date = 04/03/22 Pct Recovery = 82% Analysis Date = 04/03/22 Pct Recovery = 82% Analysis Date = 03/30/22 Pct Recovery = 82% Analysis Date = 03/30/22 Pct Recovery = 82% Analysis Date = 03/26/22 Pct Recovery = 82% Analysis Date = 03/26/22 Pct Recovery = 82% Analysis Date = 03/22/22 Pct Recovery = 82% Analysis Date = 03/22/22 Pct Recovery = 82% Analysis Date = 03/18/22 Pct Recovery = 82% Analysis Date = 03/18/22 Pct Recovery = 82% Analysis Date = 03/14/22 Pct Recovery = 82% Analysis Date = 03/14/22 Pct Recovery = 82% Analysis Date = 03/10/22 Pct Recovery = 82% Analysis Date = 03/10/22 Pct Recovery = 82% Analysis Date = 03/06/22 Pct Recovery = 82% Analysis Date = 03/06/22 Pct Recovery = 82% Analysis Date = 03/02/22 Pct Recovery = 82% Analysis Date = 03/02/22 Pct Recovery = 82% Analysis Date = 02/26/22 Pct Recovery = 82% Analysis Date = 02/26/22 Pct Recovery = 82% Analysis Date = 02/22/22 Pct Recovery = 82% Analysis Date = 02/22/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/18/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/14/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/10/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/06/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 02/02/22 Pct Recovery = 82% Analysis Date = 01/29/22 Pct Recovery = 82% Analysis Date = 01/29/22 Pct Recovery = 82% Analysis Date = 01/25/22 Pct Recovery = 82% Analysis Date = 01/25/22 Pct Recovery = 82% Analysis Date = 01/20/22 Pct Recovery = 82% Analysis Date = 01/20/22 Pct Recovery = 82% Analysis Date = 01/16/22 Pct Recovery = 82% Analysis Date = 01/16/22 Pct Recovery = 82% Analysis Date = 01/12/22 Pct Recovery = 82% Analysis Date = 01/12/22 Pct Recovery = 82% Analysis Date = 01/08/22 Pct Recovery = 82% Analysis Date = 01/08/22 Pct Recovery = 82% Analysis Date = 01/04/22 Pct Recovery = 82% Analysis Date = 01/04/22 Pct Recovery = 82% Analysis Date = 12/31/21 Pct Recovery = 82% Analysis Date = 12/31/21 Pct Recovery = 82% Analysis Date = 12/27/21 Pct Recovery = 82% Analysis Date = 12/27/21 Pct Recovery = 82% Analysis Date = 12/23/21 Pct Recovery = 82% Analysis Date = 12/23/21 Pct Recovery = 82% Analysis Date = 12/19/21 Pct Recovery = 82% Analysis Date = 12/19/21 Pct Recovery = 82% Analysis Date = 12/15/21 Pct Recovery = 83% Analysis Date = 12/15/21 Pct Recovery = 83% Analysis Date = 12/11/21 Pct Recovery = 83% Analysis Date = 12/11/21 Pct Recovery = 83% Analysis Date = 12/07/21 Pct Recovery = 83% Analysis Date = 12/07/21 Pct Recovery = 83% Analysis Date = 12/03/21 Pct Recovery = 83% Analysis Date = 12/03/21 Pct Recovery = 83% Analysis Date = 11/29/21 Pct Recovery = 83% Analysis Date = 11/29/21 Pct Recovery = 83% Analysis Date = 11/25/21 Pct Recovery = 83% Analysis Date = 11/25/21 Pct Recovery = 83% Analysis Date = 11/21/21 Pct Recovery = 83% Analysis Date = 11/21/21 Pct Recovery = 83% Analysis Date = 11/17/21 Pct Recovery = 83% Analysis Date = 11/17/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/09/21 Pct Recovery = 83% Analysis Date = 11/09/21 Pct Recovery = 83% Analysis Date = 11/05/21 Pct Recovery = 83% Analysis Date = 11/05/21 Pct Recovery = 83% Analysis Date = 11/01/21 Pct Recovery = 83% Analysis Date = 11/01/21 Pct Recovery = 83% Analysis Date = 10/28/21 Pct Recovery = 83% Analysis Date = 10/28/21 Pct Recovery = 83% Analysis Date = 10/24/21 Pct Recovery = 83% Analysis Date = 10/24/21 Pct Recovery = 83% Analysis Date = 10/20/21 Pct Recovery = 83% Analysis Date = 10/20/21 Pct Recovery = 83% Analysis Date = 10/16/21 Pct Recovery = 83% Analysis Date = 10/16/21 Pct Recovery = 83% Analysis Date = 10/11/21 Pct Recovery = 83% Analysis Date = 10/11/21 Pct Recovery = 83% Analysis Date = 10/07/21 Pct Recovery = 83% Analysis Date = 10/07/21 Pct Recovery = 83% Analysis Date = 10/03/21 Pct Recovery = 83% Analysis Date = 10/03/21 Pct Recovery = 83% Analysis Date = 09/29/21 Pct Recovery = 83% Analysis Date = 09/29/21 Pct Recovery = 83% Analysis Date = 09/25/21 Pct Recovery = 83% Analysis Date = 09/25/21 Pct Recovery = 83% Analysis Date = 09/21/21 Pct Recovery = 83% Analysis Date = 09/21/21 Pct Recovery = 83% Analysis Date = 09/17/21 Pct Recovery = 83% Analysis Date = 09/17/21 Pct Recovery = 83% Analysis Date = 09/13/21 Pct Recovery = 83% Analysis Date = 09/13/21 Pct Recovery = 83% Analysis Date = 09/09/21 Pct Recovery = 83% Analysis Date = 09/09/21 Pct Recovery = 83% Analysis Date = 09/05/21 Pct Recovery = 83% Analysis Date = 09/05/21 Pct Recovery = 83% Analysis Date = 09/01/21 Pct Recovery = 83% Analysis Date = 09/01/21 Pct Recovery = 83% Analysis Date = 08/28/21 Pct Recovery = 83% Analysis Date = 08/28/21 Pct Recovery = 83% Analysis Date = 08/24/21 Pct Recovery = 83% Analysis Date = 08/24/21 Pct Recovery = 83% Analysis Date = 08/20/21 Pct Recovery = 83% Analysis Date = 08/20/21 Pct Recovery = 83% Analysis Date = 08/16/21 Pct Recovery = 83% Analysis Date = 08/16/21 Pct Recovery = 83% Analysis Date = 08/12/21 Pct Recovery = 83% Analysis Date = 08/12/21 Pct Recovery = 83% Analysis Date = 08/08/21 Pct Recovery = 83% Analysis Date = 08/08/21 Pct Recovery = 83% Analysis Date = 08/04/21 Pct Recovery = 83% Analysis Date = 08/04/21 Pct Recovery = 83% Analysis Date = 07/31/21 Pct Recovery = 83% Analysis Date = 07/31/21 Pct Recovery = 83% Analysis Date = 07/27/21 Pct Recovery = 83% Analysis Date = 07/27/21 Pct Recovery = 83% Analysis Date = 07/23/21 Pct Recovery = 83% Analysis Date = 07/23/21 Pct Recovery = 83% Analysis Date = 07/19/21 Pct Recovery = 83% Analysis Date = 07/19/21 Pct Recovery = 83% Analysis Date = 07/15/21 Pct Recovery = 83% Analysis Date = 07/15/21 Pct Recovery = 83% Analysis Date = 07/11/21 Pct Recovery = 83% Analysis Date = 07/11/21 Pct Recovery = 83% Analysis Date = 07/07/21 Pct Recovery = 84% Analysis Date = 07/07/21 Pct Recovery = 84% Analysis Date = 07/02/21 Pct Recovery = 84% Analysis Date = 07/02/21 Pct Recovery = 84% Analysis Date = 06/28/21 Pct Recovery = 84% Analysis Date = 06/28/21 Pct Recovery = 84% Analysis Date = 06/24/21 Pct Recovery = 84% Analysis Date = 06/24/21 Pct Recovery = 84% Analysis Date = 06/20/21 Pct Recovery = 84% Analysis Date = 06/20/21 Pct Recovery = 84% Analysis Date = 06/16/21 Pct Recovery = 84% Analysis Date = 06/16/21 Pct Recovery = 84% Analysis Date = 06/12/21 Pct Recovery = 84% Analysis Date = 06/12/21 Pct Recovery = 84% Analysis Date = 06/08/21 Pct Recovery = 84% Analysis Date = 06/08/21 Pct Recovery = 84% Analysis Date = 06/04/21 Pct Recovery = 84% Analysis Date = 06/04/21 Pct Recovery = 84% Analysis Date = 05/31/21 Pct Recovery = 84% Analysis Date = 05/31/21 Pct Recovery = 84% Analysis Date = 05/27/21 Pct Recovery = 84% Analysis Date = 05/27/21 Pct Recovery = 84% Analysis Date = 05/23/21 Pct Recovery = 84% Analysis Date = 05/23/21 Pct Recovery = 84% Analysis Date = 05/19/21 Pct Recovery = 84% Analysis Date = 05/19/21 Pct Recovery = 84% Analysis Date = 05/15/21 Pct Recovery = 84% Analysis Date = 05/15/21 Pct Recovery = 84% Analysis Date = 05/11/21 Pct Recovery = 84% Analysis Date = 05/11/21 Pct Recovery = 84% Analysis Date = 05/07/21 Pct Recovery = 84% Analysis Date = 05/07/21 Pct Recovery = 84% Analysis Date = 05/03/21 Pct Recovery = 84% Analysis Date = 05/03/21 Pct Recovery = 84% Analysis Date = 04/29/21 Pct Recovery = 84% Analysis Date = 04/29/21 Pct Recovery = 84% Analysis Date = 04/25/21 Pct Recovery = 84% Analysis Date = 04/25/21 Pct Recovery = 84% Analysis Date = 04/21/21 Pct Recovery = 84% Analysis Date = 04/21/21 Pct Recovery = 84% Analysis Date = 04/17/21 Pct Recovery = 84% Analysis Date = 04/17/21 Pct Recovery = 84% Analysis Date = 04/13/21 Pct Recovery = 84% Analysis Date = 04/13/21 Pct Recovery = 84% Analysis Date = 04/09/21 Pct Recovery = 84% Analysis Date = 04/09/21 Pct Recovery = 84% Analysis Date = 04/05/21 Pct Recovery = 84% Analysis Date = 04/05/21 Pct Recovery = 84% Analysis Date = 04/01/21 Pct Recovery = 84% Analysis Date = 04/01/21 Pct Recovery = 84% Analysis Date = 03/28/21 Pct Recovery = 84% Analysis Date = 03/28/21 Pct Recovery = 84% Analysis Date = 03/23/21 Pct Recovery = 84% Analysis Date = 03/23/21 Pct Recovery = 84% Analysis Date = 03/19/21 Pct Recovery = 84% Analysis Date = 03/19/21 Pct Recovery = 84% Analysis Date = 03/15/21 Pct Recovery = 84% Analysis Date = 03/15/21 Pct Recovery = 84% Analysis Date = 03/11/21 Pct Recovery = 85% Analysis Date = 03/11/21 Pct Recovery = 85% Analysis Date = 03/07/21 Pct Recovery = 85% Analysis Date = 03/07/21 Pct Recovery = 85% Analysis Date = 03/03/21 Pct Recovery = 85% Analysis Date = 03/03/21 Pct Recovery = 85% Analysis Date = 02/27/21 Pct Recovery = 85% Analysis Date = 02/27/21 Pct Recovery = 85% Analysis Date = 02/23/21 Pct Recovery = 85% Analysis Date = 02/23/21 Pct Recovery = 85% Analysis Date = 02/19/21 Pct Recovery = 85% Analysis Date = 02/19/21 Pct Recovery = 85% Analysis Date = 02/15/21 Pct Recovery = 85% Analysis Date = 02/15/21 Pct Recovery = 85% Analysis Date = 02/11/21 Pct Recovery = 85% Analysis Date = 02/11/21 Pct Recovery = 85% Analysis Date = 02/07/21 Pct Recovery = 85% Analysis Date = 02/07/21 Pct Recovery = 85% Analysis Date = 02/03/21 Pct Recovery = 85% Analysis Date = 02/03/21 Pct Recovery = 85% Analysis Date = 01/30/21 Pct Recovery = 86% Analysis Date = 01/30/21 Pct Recovery = 86% Analysis Date = 01/26/21 Pct Recovery = 86% Analysis Date = 01/26/21 Pct Recovery = 86% Analysis Date = 01/22/21 Pct Recovery = 86% Analysis Date = 01/22/21 Pct Recovery = 86% Analysis Date = 01/18/21 Pct Recovery = 86% Analysis Date = 01/18/21 Pct Recovery = 86% Analysis Date = 01/14/21 Pct Recovery = 86% Analysis Date = 01/14/21 Pct Recovery = 86% Analysis Date = 01/10/21 Pct Recovery = 87% Analysis Date = 01/10/21 Pct Recovery = 87% Analysis Date = 01/06/21 Pct Recovery = 87% Analysis Date = 01/06/21 Pct Recovery = 87% Analysis Date = 01/02/21 Pct Recovery = 87% Analysis Date = 01/02/21 Pct Recovery = 87% Analysis Date = 12/29/20 Pct Recovery = 88% Analysis Date = 12/29/20 Pct Recovery = 88% Analysis Date = 12/25/20 Pct Recovery = 88% Analysis Date = 12/25/20 Pct Recovery = 88% Analysis Date = 12/21/20 Pct Recovery = 88% Analysis Date = 12/21/20 Pct Recovery = 88% Analysis Date = 12/17/20 Pct Recovery = 88% Analysis Date = 12/17/20 Pct Recovery = 88% Analysis Date = 12/12/20 Pct Recovery = 89% Analysis Date = 12/12/20 Pct Recovery = 89% Analysis Date = 12/08/20 Pct Recovery = 89% Analysis Date = 12/08/20 Pct Recovery = 89% Analysis Date = 12/04/20 Pct Recovery = 90% Analysis Date = 12/04/20 Pct Recovery = 90% Analysis Date = 11/30/20 Pct Recovery = 90% Analysis Date = 11/30/20 Pct Recovery = 90% Analysis Date = 11/26/20 Pct Recovery = 90% Analysis Date = 11/26/20 Pct Recovery = 90% Analysis Date = 11/22/20 Pct Recovery = 91% Analysis Date = 11/22/20 Pct Recovery = 91% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/18/20 Pct Recovery = 91% Analysis Date = 11/14/20 Pct Recovery = 92% Analysis Date = 11/14/20 Pct Recovery = 92% Analysis Date = 11/10/20 Pct Recovery = 92% Analysis Date = 11/10/20 Pct Recovery = 92% Analysis Date = 11/06/20 Pct Recovery = 93% Analysis Date = 11/06/20 Pct Recovery = 93% Analysis Date = 11/02/20 Pct Recovery = 93% Analysis Date = 11/02/20 Pct Recovery = 93% Analysis Date = 10/29/20 Pct Recovery = 93% Analysis Date = 10/29/20 Pct Recovery = 93% Analysis Date = 10/25/20 Pct Recovery = 94% Analysis Date = 10/25/20 Pct Recovery = 94% Analysis Date = 10/21/20 Pct Recovery = 94% Analysis Date = 10/21/20 Pct Recovery = 94% Analysis Date = 10/17/20 Pct Recovery = 95% Analysis Date = 10/17/20 Pct Recovery = 95% Analysis Date = 10/13/20 Pct Recovery = 95% Analysis Date = 10/13/20 Pct Recovery = 95% Analysis Date = 10/09/20 Pct Recovery = 96% Analysis Date = 10/09/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/01/20 Pct Recovery = 96% Analysis Date = 10/01/20 Pct Recovery = 96% Analysis Date = 09/27/20 Pct Recovery = 97% Analysis Date = 09/27/20 Pct Recovery = 97% Analysis Date = 09/23/20 Pct Recovery = 97% Analysis Date = 09/23/20 Pct Recovery = 97% Analysis Date = 09/19/20 Pct Recovery = 98% Analysis Date = 09/19/20 Pct Recovery = 98% Analysis Date = 09/15/20 Pct Recovery = 98% Analysis Date = 09/15/20 Pct Recovery = 98% Analysis Date = 09/11/20 Pct Recovery = 98% Analysis Date = 09/11/20 Pct Recovery = 98% Analysis Date = 09/07/20 Pct Recovery = 98% Analysis Date = 09/07/20 Pct Recovery = 98% Analysis Date = 09/02/20 Pct Recovery = 98% Analysis Date = 09/02/20 Pct Recovery = 98% Analysis Date = 08/29/20 Pct Recovery = 98% Analysis Date = 08/29/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/21/20 Pct Recovery = 98% Analysis Date = 08/21/20 Pct Recovery = 98% Analysis Date = 08/17/20 Pct Recovery = 98% Analysis Date = 08/17/20 Pct Recovery = 98% Analysis Date = 08/13/20 Pct Recovery = 98% Analysis Date = 08/13/20 Pct Recovery = 98% Analysis Date = 08/09/20 Pct Recovery = 97% Analysis Date = 08/09/20 Pct Recovery = 97% Analysis Date = 08/05/20 Pct Recovery = 97% Analysis Date = 08/05/20 Pct Recovery = 97% Analysis Date = 08/01/20 Pct Recovery = 97% Analysis Date = 08/01/20 Pct Recovery = 97% Analysis Date = 07/28/20 Pct Recovery = 97% Analysis Date = 07/28/20 Pct Recovery = 97% Analysis Date = 07/24/20 Pct Recovery = 97% Analysis Date = 07/24/20 Pct Recovery = 97% Analysis Date = 07/20/20 Pct Recovery = 97% Analysis Date = 07/20/20 Pct Recovery = 97% Analysis Date = 07/16/20 Pct Recovery = 97% Analysis Date = 07/16/20 Pct Recovery = 97% Analysis Date = 07/12/20 Pct Recovery = 97% Analysis Date = 07/12/20 Pct Recovery = 97% Analysis Date = 07/08/20 Pct Recovery = 96% Analysis Date = 07/08/20 Pct Recovery = 96% Analysis Date = 07/04/20 Pct Recovery = 96% Analysis Date = 07/04/20 Pct Recovery = 96% Analysis Date = 06/30/20 Pct Recovery = 96% Analysis Date = 06/30/20 Pct Recovery = 96% Analysis Date = 06/26/20 Pct Recovery = 96% Analysis Date = 06/26/20 Pct Recovery = 96% Analysis Date = 06/22/20 Pct Recovery = 96% Analysis Date = 06/22/20 Pct Recovery = 96% Analysis Date = 06/18/20 Pct Recovery = 96% Analysis Date = 06/18/20 Pct Recovery = 96% Analysis Date = 06/14/20 Pct Recovery = 95% Analysis Date = 06/14/20 Pct Recovery = 95% Analysis Date = 06/10/20 Pct Recovery = 95% Analysis Date = 06/10/20 Pct Recovery = 95% Analysis Date = 06/06/20 Pct Recovery = 95% Analysis Date = 06/06/20 Pct Recovery = 95% Analysis Date = 06/02/20 Pct Recovery = 95% Analysis Date = 06/02/20 Pct Recovery = 95% Analysis Date = 05/29/20 Pct Recovery = 94% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MYCLOBUTANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 90% 16% 88% 14%
Total 33 90% 16% 88% 14%

Sample Statistics
MYCLOBUTANIL

Characteristic N % % Basis
Plotted 33 97% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 34 .  
False Negatives 0 0% 0 out of 34
Not Spiked 82 .  
False Positives 0 0% 0 out of 82

OBSP Determination:
N-(3,4-DICHLOROPHENYL)-N'-METHYLUREA
METHOD: 2447 , TESTIDCODE: 68231LCM60

Laboratory ID = 20202590104 Lab Value = 132.300 Expected Conc. = 62.2 Report level label = 5 Pct Recovery = 213% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 136.860 Expected Conc. = 62.2 Report level label = 5 Pct Recovery = 220% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230021 Lab Value = 1316.407 Expected Conc. = 1354 Report level label = 5 Pct Recovery = 97% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 1285.403 Expected Conc. = 1354 Report level label = 5 Pct Recovery = 95% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210830019 Lab Value = 285.020 Expected Conc. = 270.8 Report level label = 5 Pct Recovery = 105% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 242.328 Expected Conc. = 270.8 Report level label = 5 Pct Recovery = 89% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20201820155 Lab Value = 62.163 Expected Conc. = 64.8 Report level label = 5 Pct Recovery = 96% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 63.374 Expected Conc. = 64.8 Report level label = 5 Pct Recovery = 98% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20210760015 Lab Value = 49.434 Expected Conc. = 62.8 Report level label = 5 Pct Recovery = 79% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 55.652 Expected Conc. = 62.8 Report level label = 5 Pct Recovery = 89% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 57.113 Expected Conc. = 62.8 Report level label = 5 Pct Recovery = 91% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 57.174 Expected Conc. = 62.8 Report level label = 5 Pct Recovery = 91% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202390020 Lab Value = 77.711 Expected Conc. = 62.8 Report level label = 5 Pct Recovery = 124% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203080100 Lab Value = 67.450 Expected Conc. = 62.2 Report level label = 5 Pct Recovery = 108% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221940195 Lab Value = 44.667 Expected Conc. = 50.32 Report level label = 5 Pct Recovery = 89% Analysis Date = 07/23/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20222010133 Lab Value = 46.595 Expected Conc. = 50 Report level label = 5 Pct Recovery = 93% Analysis Date = 07/24/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20222640086 Lab Value = 40.443 Expected Conc. = 49.6 Report level label = 5 Pct Recovery = 82% Analysis Date = 09/29/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20202530029 Lab Value = 30.134 Expected Conc. = 32.4 Report level label = 5 Pct Recovery = 93% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 31.994 Expected Conc. = 32.4 Report level label = 5 Pct Recovery = 99% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 33.547 Expected Conc. = 32.4 Report level label = 5 Pct Recovery = 104% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20210480001 Lab Value = 10.876 Expected Conc. = 31.4 Report level label = 5 Pct Recovery = 35% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201960104 Lab Value = 51.418 Expected Conc. = 31.4 Report level label = 5 Pct Recovery = 164% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20221870197 Lab Value = 17.186 Expected Conc. = 31.25 Report level label = 5 Pct Recovery = 55% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20221730293 Lab Value = 22.641 Expected Conc. = 31.25 Report level label = 5 Pct Recovery = 72% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20202880004 Lab Value = 40.789 Expected Conc. = 31.1 Report level label = 5 Pct Recovery = 131% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 32.699 Expected Conc. = 25.12 Report level label = 5 Pct Recovery = 130% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 28.942 Expected Conc. = 24.88 Report level label = 5 Pct Recovery = 116% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 27.193 Expected Conc. = 24.88 Report level label = 5 Pct Recovery = 109% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202180001 Lab Value = 11.905 Expected Conc. = 12.96 Report level label = 5 Pct Recovery = 92% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 11.304 Expected Conc. = 12.96 Report level label = 5 Pct Recovery = 87% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 14.173 Expected Conc. = 12.96 Report level label = 5 Pct Recovery = 109% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210690067 Lab Value = 19.702 Expected Conc. = 12.56 Report level label = 5 Pct Recovery = 157% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 13.321 Expected Conc. = 12.56 Report level label = 5 Pct Recovery = 106% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20222500483 Lab Value = 15.611 Expected Conc. = 12.5 Report level label = 5 Pct Recovery = 125% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Laboratory ID = 20210120050 Lab Value = 13.767 Expected Conc. = 12.44 Report level label = 5 Pct Recovery = 111% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 15.440 Expected Conc. = 12.44 Report level label = 5 Pct Recovery = 124% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 16.767 Expected Conc. = 12.44 Report level label = 5 Pct Recovery = 135% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 14.636 Expected Conc. = 12.44 Report level label = 5 Pct Recovery = 118% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 09/28/22 Pct Recovery = 86% Analysis Date = 09/24/22 Pct Recovery = 86% Analysis Date = 09/24/22 Pct Recovery = 86% Analysis Date = 09/20/22 Pct Recovery = 86% Analysis Date = 09/20/22 Pct Recovery = 86% Analysis Date = 09/16/22 Pct Recovery = 86% Analysis Date = 09/16/22 Pct Recovery = 86% Analysis Date = 09/11/22 Pct Recovery = 86% Analysis Date = 09/11/22 Pct Recovery = 86% Analysis Date = 09/07/22 Pct Recovery = 86% Analysis Date = 09/07/22 Pct Recovery = 86% Analysis Date = 09/03/22 Pct Recovery = 86% Analysis Date = 09/03/22 Pct Recovery = 86% Analysis Date = 08/29/22 Pct Recovery = 87% Analysis Date = 08/29/22 Pct Recovery = 87% Analysis Date = 08/25/22 Pct Recovery = 87% Analysis Date = 08/25/22 Pct Recovery = 87% Analysis Date = 08/21/22 Pct Recovery = 87% Analysis Date = 08/21/22 Pct Recovery = 87% Analysis Date = 08/16/22 Pct Recovery = 87% Analysis Date = 08/16/22 Pct Recovery = 87% Analysis Date = 08/12/22 Pct Recovery = 87% Analysis Date = 08/12/22 Pct Recovery = 87% Analysis Date = 08/08/22 Pct Recovery = 87% Analysis Date = 08/08/22 Pct Recovery = 87% Analysis Date = 08/03/22 Pct Recovery = 87% Analysis Date = 08/03/22 Pct Recovery = 87% Analysis Date = 07/30/22 Pct Recovery = 87% Analysis Date = 07/30/22 Pct Recovery = 87% Analysis Date = 07/26/22 Pct Recovery = 87% Analysis Date = 07/26/22 Pct Recovery = 87% Analysis Date = 07/21/22 Pct Recovery = 87% Analysis Date = 07/21/22 Pct Recovery = 87% Analysis Date = 07/17/22 Pct Recovery = 88% Analysis Date = 07/17/22 Pct Recovery = 88% Analysis Date = 07/13/22 Pct Recovery = 88% Analysis Date = 07/13/22 Pct Recovery = 88% Analysis Date = 07/09/22 Pct Recovery = 88% Analysis Date = 07/09/22 Pct Recovery = 88% Analysis Date = 07/04/22 Pct Recovery = 88% Analysis Date = 07/04/22 Pct Recovery = 88% Analysis Date = 06/30/22 Pct Recovery = 88% Analysis Date = 06/30/22 Pct Recovery = 88% Analysis Date = 06/26/22 Pct Recovery = 88% Analysis Date = 06/26/22 Pct Recovery = 88% Analysis Date = 06/21/22 Pct Recovery = 88% Analysis Date = 06/21/22 Pct Recovery = 88% Analysis Date = 06/17/22 Pct Recovery = 89% Analysis Date = 06/17/22 Pct Recovery = 89% Analysis Date = 06/13/22 Pct Recovery = 89% Analysis Date = 06/13/22 Pct Recovery = 89% Analysis Date = 06/08/22 Pct Recovery = 89% Analysis Date = 06/08/22 Pct Recovery = 89% Analysis Date = 06/04/22 Pct Recovery = 89% Analysis Date = 06/04/22 Pct Recovery = 89% Analysis Date = 05/31/22 Pct Recovery = 89% Analysis Date = 05/31/22 Pct Recovery = 89% Analysis Date = 05/26/22 Pct Recovery = 89% Analysis Date = 05/26/22 Pct Recovery = 89% Analysis Date = 05/22/22 Pct Recovery = 89% Analysis Date = 05/22/22 Pct Recovery = 89% Analysis Date = 05/18/22 Pct Recovery = 90% Analysis Date = 05/18/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/05/22 Pct Recovery = 90% Analysis Date = 05/05/22 Pct Recovery = 90% Analysis Date = 04/30/22 Pct Recovery = 90% Analysis Date = 04/30/22 Pct Recovery = 90% Analysis Date = 04/26/22 Pct Recovery = 90% Analysis Date = 04/26/22 Pct Recovery = 90% Analysis Date = 04/22/22 Pct Recovery = 91% Analysis Date = 04/22/22 Pct Recovery = 91% Analysis Date = 04/18/22 Pct Recovery = 91% Analysis Date = 04/18/22 Pct Recovery = 91% Analysis Date = 04/13/22 Pct Recovery = 91% Analysis Date = 04/13/22 Pct Recovery = 91% Analysis Date = 04/09/22 Pct Recovery = 91% Analysis Date = 04/09/22 Pct Recovery = 91% Analysis Date = 04/05/22 Pct Recovery = 91% Analysis Date = 04/05/22 Pct Recovery = 91% Analysis Date = 03/31/22 Pct Recovery = 91% Analysis Date = 03/31/22 Pct Recovery = 91% Analysis Date = 03/27/22 Pct Recovery = 92% Analysis Date = 03/27/22 Pct Recovery = 92% Analysis Date = 03/23/22 Pct Recovery = 92% Analysis Date = 03/23/22 Pct Recovery = 92% Analysis Date = 03/18/22 Pct Recovery = 92% Analysis Date = 03/18/22 Pct Recovery = 92% Analysis Date = 03/14/22 Pct Recovery = 92% Analysis Date = 03/14/22 Pct Recovery = 92% Analysis Date = 03/10/22 Pct Recovery = 92% Analysis Date = 03/10/22 Pct Recovery = 92% Analysis Date = 03/05/22 Pct Recovery = 92% Analysis Date = 03/05/22 Pct Recovery = 92% Analysis Date = 03/01/22 Pct Recovery = 92% Analysis Date = 03/01/22 Pct Recovery = 92% Analysis Date = 02/25/22 Pct Recovery = 93% Analysis Date = 02/25/22 Pct Recovery = 93% Analysis Date = 02/20/22 Pct Recovery = 93% Analysis Date = 02/20/22 Pct Recovery = 93% Analysis Date = 02/16/22 Pct Recovery = 93% Analysis Date = 02/16/22 Pct Recovery = 93% Analysis Date = 02/12/22 Pct Recovery = 93% Analysis Date = 02/12/22 Pct Recovery = 93% Analysis Date = 02/07/22 Pct Recovery = 93% Analysis Date = 02/07/22 Pct Recovery = 93% Analysis Date = 02/03/22 Pct Recovery = 93% Analysis Date = 02/03/22 Pct Recovery = 93% Analysis Date = 01/30/22 Pct Recovery = 94% Analysis Date = 01/30/22 Pct Recovery = 94% Analysis Date = 01/26/22 Pct Recovery = 94% Analysis Date = 01/26/22 Pct Recovery = 94% Analysis Date = 01/21/22 Pct Recovery = 94% Analysis Date = 01/21/22 Pct Recovery = 94% Analysis Date = 01/17/22 Pct Recovery = 94% Analysis Date = 01/17/22 Pct Recovery = 94% Analysis Date = 01/13/22 Pct Recovery = 94% Analysis Date = 01/13/22 Pct Recovery = 94% Analysis Date = 01/08/22 Pct Recovery = 94% Analysis Date = 01/08/22 Pct Recovery = 94% Analysis Date = 01/04/22 Pct Recovery = 95% Analysis Date = 01/04/22 Pct Recovery = 95% Analysis Date = 12/31/21 Pct Recovery = 95% Analysis Date = 12/31/21 Pct Recovery = 95% Analysis Date = 12/26/21 Pct Recovery = 95% Analysis Date = 12/26/21 Pct Recovery = 95% Analysis Date = 12/22/21 Pct Recovery = 95% Analysis Date = 12/22/21 Pct Recovery = 95% Analysis Date = 12/18/21 Pct Recovery = 95% Analysis Date = 12/18/21 Pct Recovery = 95% Analysis Date = 12/13/21 Pct Recovery = 95% Analysis Date = 12/13/21 Pct Recovery = 95% Analysis Date = 12/09/21 Pct Recovery = 96% Analysis Date = 12/09/21 Pct Recovery = 96% Analysis Date = 12/05/21 Pct Recovery = 96% Analysis Date = 12/05/21 Pct Recovery = 96% Analysis Date = 11/30/21 Pct Recovery = 96% Analysis Date = 11/30/21 Pct Recovery = 96% Analysis Date = 11/26/21 Pct Recovery = 96% Analysis Date = 11/26/21 Pct Recovery = 96% Analysis Date = 11/22/21 Pct Recovery = 96% Analysis Date = 11/22/21 Pct Recovery = 96% Analysis Date = 11/18/21 Pct Recovery = 96% Analysis Date = 11/18/21 Pct Recovery = 96% Analysis Date = 11/13/21 Pct Recovery = 96% Analysis Date = 11/13/21 Pct Recovery = 96% Analysis Date = 11/09/21 Pct Recovery = 97% Analysis Date = 11/09/21 Pct Recovery = 97% Analysis Date = 11/05/21 Pct Recovery = 97% Analysis Date = 11/05/21 Pct Recovery = 97% Analysis Date = 10/31/21 Pct Recovery = 97% Analysis Date = 10/31/21 Pct Recovery = 97% Analysis Date = 10/27/21 Pct Recovery = 97% Analysis Date = 10/27/21 Pct Recovery = 97% Analysis Date = 10/23/21 Pct Recovery = 97% Analysis Date = 10/23/21 Pct Recovery = 97% Analysis Date = 10/18/21 Pct Recovery = 97% Analysis Date = 10/18/21 Pct Recovery = 97% Analysis Date = 10/14/21 Pct Recovery = 98% Analysis Date = 10/14/21 Pct Recovery = 98% Analysis Date = 10/10/21 Pct Recovery = 98% Analysis Date = 10/10/21 Pct Recovery = 98% Analysis Date = 10/05/21 Pct Recovery = 98% Analysis Date = 10/05/21 Pct Recovery = 98% Analysis Date = 10/01/21 Pct Recovery = 98% Analysis Date = 10/01/21 Pct Recovery = 98% Analysis Date = 09/27/21 Pct Recovery = 98% Analysis Date = 09/27/21 Pct Recovery = 98% Analysis Date = 09/22/21 Pct Recovery = 98% Analysis Date = 09/22/21 Pct Recovery = 98% Analysis Date = 09/18/21 Pct Recovery = 99% Analysis Date = 09/18/21 Pct Recovery = 99% Analysis Date = 09/14/21 Pct Recovery = 99% Analysis Date = 09/14/21 Pct Recovery = 99% Analysis Date = 09/09/21 Pct Recovery = 99% Analysis Date = 09/09/21 Pct Recovery = 99% Analysis Date = 09/05/21 Pct Recovery = 99% Analysis Date = 09/05/21 Pct Recovery = 99% Analysis Date = 09/01/21 Pct Recovery = 99% Analysis Date = 09/01/21 Pct Recovery = 99% Analysis Date = 08/28/21 Pct Recovery = 99% Analysis Date = 08/28/21 Pct Recovery = 99% Analysis Date = 08/23/21 Pct Recovery = 99% Analysis Date = 08/23/21 Pct Recovery = 99% Analysis Date = 08/19/21 Pct Recovery = 100% Analysis Date = 08/19/21 Pct Recovery = 100% Analysis Date = 08/15/21 Pct Recovery = 100% Analysis Date = 08/15/21 Pct Recovery = 100% Analysis Date = 08/10/21 Pct Recovery = 100% Analysis Date = 08/10/21 Pct Recovery = 100% Analysis Date = 08/06/21 Pct Recovery = 100% Analysis Date = 08/06/21 Pct Recovery = 100% Analysis Date = 08/02/21 Pct Recovery = 100% Analysis Date = 08/02/21 Pct Recovery = 100% Analysis Date = 07/28/21 Pct Recovery = 100% Analysis Date = 07/28/21 Pct Recovery = 100% Analysis Date = 07/24/21 Pct Recovery = 101% Analysis Date = 07/24/21 Pct Recovery = 101% Analysis Date = 07/20/21 Pct Recovery = 101% Analysis Date = 07/20/21 Pct Recovery = 101% Analysis Date = 07/15/21 Pct Recovery = 101% Analysis Date = 07/15/21 Pct Recovery = 101% Analysis Date = 07/11/21 Pct Recovery = 101% Analysis Date = 07/11/21 Pct Recovery = 101% Analysis Date = 07/07/21 Pct Recovery = 101% Analysis Date = 07/07/21 Pct Recovery = 101% Analysis Date = 07/02/21 Pct Recovery = 101% Analysis Date = 07/02/21 Pct Recovery = 101% Analysis Date = 06/28/21 Pct Recovery = 102% Analysis Date = 06/28/21 Pct Recovery = 102% Analysis Date = 06/24/21 Pct Recovery = 102% Analysis Date = 06/24/21 Pct Recovery = 102% Analysis Date = 06/19/21 Pct Recovery = 102% Analysis Date = 06/19/21 Pct Recovery = 102% Analysis Date = 06/15/21 Pct Recovery = 102% Analysis Date = 06/15/21 Pct Recovery = 102% Analysis Date = 06/11/21 Pct Recovery = 102% Analysis Date = 06/11/21 Pct Recovery = 102% Analysis Date = 06/07/21 Pct Recovery = 102% Analysis Date = 06/07/21 Pct Recovery = 102% Analysis Date = 06/02/21 Pct Recovery = 102% Analysis Date = 06/02/21 Pct Recovery = 102% Analysis Date = 05/29/21 Pct Recovery = 103% Analysis Date = 05/29/21 Pct Recovery = 103% Analysis Date = 05/25/21 Pct Recovery = 103% Analysis Date = 05/25/21 Pct Recovery = 103% Analysis Date = 05/20/21 Pct Recovery = 103% Analysis Date = 05/20/21 Pct Recovery = 103% Analysis Date = 05/16/21 Pct Recovery = 103% Analysis Date = 05/16/21 Pct Recovery = 103% Analysis Date = 05/12/21 Pct Recovery = 103% Analysis Date = 05/12/21 Pct Recovery = 103% Analysis Date = 05/07/21 Pct Recovery = 103% Analysis Date = 05/07/21 Pct Recovery = 103% Analysis Date = 05/03/21 Pct Recovery = 104% Analysis Date = 05/03/21 Pct Recovery = 104% Analysis Date = 04/29/21 Pct Recovery = 104% Analysis Date = 04/29/21 Pct Recovery = 104% Analysis Date = 04/24/21 Pct Recovery = 104% Analysis Date = 04/24/21 Pct Recovery = 104% Analysis Date = 04/20/21 Pct Recovery = 104% Analysis Date = 04/20/21 Pct Recovery = 104% Analysis Date = 04/16/21 Pct Recovery = 104% Analysis Date = 04/16/21 Pct Recovery = 104% Analysis Date = 04/11/21 Pct Recovery = 104% Analysis Date = 04/11/21 Pct Recovery = 104% Analysis Date = 04/07/21 Pct Recovery = 104% Analysis Date = 04/07/21 Pct Recovery = 104% Analysis Date = 04/03/21 Pct Recovery = 104% Analysis Date = 04/03/21 Pct Recovery = 104% Analysis Date = 03/29/21 Pct Recovery = 104% Analysis Date = 03/29/21 Pct Recovery = 104% Analysis Date = 03/25/21 Pct Recovery = 103% Analysis Date = 03/25/21 Pct Recovery = 103% Analysis Date = 03/21/21 Pct Recovery = 103% Analysis Date = 03/21/21 Pct Recovery = 103% Analysis Date = 03/17/21 Pct Recovery = 103% Analysis Date = 03/17/21 Pct Recovery = 103% Analysis Date = 03/12/21 Pct Recovery = 102% Analysis Date = 03/12/21 Pct Recovery = 102% Analysis Date = 03/08/21 Pct Recovery = 102% Analysis Date = 03/08/21 Pct Recovery = 102% Analysis Date = 03/04/21 Pct Recovery = 102% Analysis Date = 03/04/21 Pct Recovery = 102% Analysis Date = 02/27/21 Pct Recovery = 102% Analysis Date = 02/27/21 Pct Recovery = 102% Analysis Date = 02/23/21 Pct Recovery = 102% Analysis Date = 02/23/21 Pct Recovery = 102% Analysis Date = 02/19/21 Pct Recovery = 102% Analysis Date = 02/19/21 Pct Recovery = 102% Analysis Date = 02/14/21 Pct Recovery = 102% Analysis Date = 02/14/21 Pct Recovery = 102% Analysis Date = 02/10/21 Pct Recovery = 102% Analysis Date = 02/10/21 Pct Recovery = 102% Analysis Date = 02/06/21 Pct Recovery = 102% Analysis Date = 02/06/21 Pct Recovery = 102% Analysis Date = 02/01/21 Pct Recovery = 102% Analysis Date = 02/01/21 Pct Recovery = 102% Analysis Date = 01/28/21 Pct Recovery = 102% Analysis Date = 01/28/21 Pct Recovery = 102% Analysis Date = 01/24/21 Pct Recovery = 103% Analysis Date = 01/24/21 Pct Recovery = 103% Analysis Date = 01/19/21 Pct Recovery = 104% Analysis Date = 01/19/21 Pct Recovery = 104% Analysis Date = 01/15/21 Pct Recovery = 106% Analysis Date = 01/15/21 Pct Recovery = 106% Analysis Date = 01/11/21 Pct Recovery = 107% Analysis Date = 01/11/21 Pct Recovery = 107% Analysis Date = 01/07/21 Pct Recovery = 109% Analysis Date = 01/07/21 Pct Recovery = 109% Analysis Date = 01/02/21 Pct Recovery = 110% Analysis Date = 01/02/21 Pct Recovery = 110% Analysis Date = 12/29/20 Pct Recovery = 111% Analysis Date = 12/29/20 Pct Recovery = 111% Analysis Date = 12/25/20 Pct Recovery = 113% Analysis Date = 12/25/20 Pct Recovery = 113% Analysis Date = 12/20/20 Pct Recovery = 114% Analysis Date = 12/20/20 Pct Recovery = 114% Analysis Date = 12/16/20 Pct Recovery = 115% Analysis Date = 12/16/20 Pct Recovery = 115% Analysis Date = 12/12/20 Pct Recovery = 117% Analysis Date = 12/12/20 Pct Recovery = 117% Analysis Date = 12/07/20 Pct Recovery = 118% Analysis Date = 12/07/20 Pct Recovery = 118% Analysis Date = 12/03/20 Pct Recovery = 119% Analysis Date = 12/03/20 Pct Recovery = 119% Analysis Date = 11/29/20 Pct Recovery = 121% Analysis Date = 11/29/20 Pct Recovery = 121% Analysis Date = 11/24/20 Pct Recovery = 122% Analysis Date = 11/24/20 Pct Recovery = 122% Analysis Date = 11/20/20 Pct Recovery = 124% Analysis Date = 11/20/20 Pct Recovery = 124% Analysis Date = 11/16/20 Pct Recovery = 125% Analysis Date = 11/16/20 Pct Recovery = 125% Analysis Date = 11/11/20 Pct Recovery = 126% Analysis Date = 11/11/20 Pct Recovery = 126% Analysis Date = 11/07/20 Pct Recovery = 128% Analysis Date = 11/07/20 Pct Recovery = 128% Analysis Date = 11/03/20 Pct Recovery = 129% Analysis Date = 11/03/20 Pct Recovery = 129% Analysis Date = 10/29/20 Pct Recovery = 130% Analysis Date = 10/29/20 Pct Recovery = 130% Analysis Date = 10/25/20 Pct Recovery = 132% Analysis Date = 10/25/20 Pct Recovery = 132% Analysis Date = 10/21/20 Pct Recovery = 133% Analysis Date = 10/21/20 Pct Recovery = 133% Analysis Date = 10/17/20 Pct Recovery = 133% Analysis Date = 10/17/20 Pct Recovery = 133% Analysis Date = 10/12/20 Pct Recovery = 133% Analysis Date = 10/12/20 Pct Recovery = 133% Analysis Date = 10/08/20 Pct Recovery = 133% Analysis Date = 10/08/20 Pct Recovery = 133% Analysis Date = 10/04/20 Pct Recovery = 132% Analysis Date = 10/04/20 Pct Recovery = 132% Analysis Date = 09/29/20 Pct Recovery = 132% Analysis Date = 09/29/20 Pct Recovery = 132% Analysis Date = 09/25/20 Pct Recovery = 132% Analysis Date = 09/25/20 Pct Recovery = 132% Analysis Date = 09/21/20 Pct Recovery = 131% Analysis Date = 09/21/20 Pct Recovery = 131% Analysis Date = 09/16/20 Pct Recovery = 130% Analysis Date = 09/16/20 Pct Recovery = 130% Analysis Date = 09/12/20 Pct Recovery = 129% Analysis Date = 09/12/20 Pct Recovery = 129% Analysis Date = 09/08/20 Pct Recovery = 128% Analysis Date = 09/08/20 Pct Recovery = 128% Analysis Date = 09/03/20 Pct Recovery = 127% Analysis Date = 09/03/20 Pct Recovery = 127% Analysis Date = 08/30/20 Pct Recovery = 126% Analysis Date = 08/30/20 Pct Recovery = 126% Analysis Date = 08/26/20 Pct Recovery = 125% Analysis Date = 08/26/20 Pct Recovery = 125% Analysis Date = 08/21/20 Pct Recovery = 124% Analysis Date = 08/21/20 Pct Recovery = 124% Analysis Date = 08/17/20 Pct Recovery = 123% Analysis Date = 08/17/20 Pct Recovery = 123% Analysis Date = 08/13/20 Pct Recovery = 122% Analysis Date = 08/13/20 Pct Recovery = 122% Analysis Date = 08/08/20 Pct Recovery = 121% Analysis Date = 08/08/20 Pct Recovery = 121% Analysis Date = 08/04/20 Pct Recovery = 120% Analysis Date = 08/04/20 Pct Recovery = 120% Analysis Date = 07/31/20 Pct Recovery = 118% Analysis Date = 07/31/20 Pct Recovery = 118% Analysis Date = 07/27/20 Pct Recovery = 117% Analysis Date = 07/27/20 Pct Recovery = 117% Analysis Date = 07/22/20 Pct Recovery = 116% Analysis Date = 07/22/20 Pct Recovery = 116% Analysis Date = 07/18/20 Pct Recovery = 115% Analysis Date = 07/18/20 Pct Recovery = 115% Analysis Date = 07/14/20 Pct Recovery = 114% Analysis Date = 07/14/20 Pct Recovery = 114% Analysis Date = 07/09/20 Pct Recovery = 113% Analysis Date = 07/09/20 Pct Recovery = 113% Analysis Date = 07/05/20 Pct Recovery = 111% Analysis Date = 07/05/20 Pct Recovery = 111% Analysis Date = 07/01/20 Pct Recovery = 110% Analysis Date = 07/01/20 Pct Recovery = 110% Analysis Date = 06/26/20 Pct Recovery = 109% Analysis Date = 06/26/20 Pct Recovery = 109% Analysis Date = 06/22/20 Pct Recovery = 108% Analysis Date = 06/22/20 Pct Recovery = 108% Analysis Date = 06/18/20 Pct Recovery = 106% Analysis Date = 06/18/20 Pct Recovery = 106% Analysis Date = 06/13/20 Pct Recovery = 105% Analysis Date = 06/13/20 Pct Recovery = 105% Analysis Date = 06/09/20 Pct Recovery = 104% Analysis Date = 06/09/20 Pct Recovery = 104% Analysis Date = 06/05/20 Pct Recovery = 103% Analysis Date = 06/05/20 Pct Recovery = 103% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 100% Analysis Date = 05/23/20 Pct Recovery = 99% Analysis Date = 05/23/20 Pct Recovery = 99% Analysis Date = 05/19/20 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
N-(3,4-DICHLOROPHENYL)-N'-METHYLUREA

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 38 109% 35% 101% 24%
Total 38 109% 35% 101% 24%

Sample Statistics
N-(3,4-DICHLOROPHENYL)-N'-METHYLUREA

Characteristic N % % Basis
Plotted 38 93% Spiked
Estimated Values 8 20% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 41 .  
False Negatives 3 7% 3 out of 41
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

OBSP Determination:
ORYZALIN
METHOD: 2447 , TESTIDCODE: 68663LCM60

Laboratory ID = 20202590107 Lab Value = 177.217 Expected Conc. = 150.5 Report level label = 12 Pct Recovery = 118% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 176.785 Expected Conc. = 150.5 Report level label = 12 Pct Recovery = 117% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 193.328 Expected Conc. = 150.3 Report level label = 12 Pct Recovery = 129% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 190.294 Expected Conc. = 150.3 Report level label = 12 Pct Recovery = 127% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20201820155 Lab Value = 153.147 Expected Conc. = 150.3 Report level label = 12 Pct Recovery = 102% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 180.751 Expected Conc. = 150.3 Report level label = 12 Pct Recovery = 120% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202390020 Lab Value = 142.502 Expected Conc. = 149.7 Report level label = 12 Pct Recovery = 95% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20221520237 Lab Value = 112.892 Expected Conc. = 121.16 Report level label = 12 Pct Recovery = 93% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20222150192 Lab Value = 121.934 Expected Conc. = 120 Report level label = 12 Pct Recovery = 102% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 89.117 Expected Conc. = 120 Report level label = 12 Pct Recovery = 74% Analysis Date = 07/21/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221870197 Lab Value = 66.432 Expected Conc. = 75.725 Report level label = 12 Pct Recovery = 88% Analysis Date = 07/14/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20203360042 Lab Value = 75.003 Expected Conc. = 75.25 Report level label = 12 Pct Recovery = 100% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 77.789 Expected Conc. = 75.25 Report level label = 12 Pct Recovery = 103% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 76.829 Expected Conc. = 75.25 Report level label = 12 Pct Recovery = 102% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 80.925 Expected Conc. = 75.15 Report level label = 12 Pct Recovery = 108% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 72.187 Expected Conc. = 75.15 Report level label = 12 Pct Recovery = 96% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 86.095 Expected Conc. = 75.15 Report level label = 12 Pct Recovery = 115% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201960104 Lab Value = 81.287 Expected Conc. = 74.85 Report level label = 12 Pct Recovery = 109% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20221660151 Lab Value = 33.843 Expected Conc. = 30.29 Report level label = 12 Pct Recovery = 112% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210970035 Lab Value = 27.031 Expected Conc. = 30.1 Report level label = 12 Pct Recovery = 90% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 43.694 Expected Conc. = 30.1 Report level label = 12 Pct Recovery = 145% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 26.643 Expected Conc. = 30.1 Report level label = 12 Pct Recovery = 89% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 48.609 Expected Conc. = 30.1 Report level label = 12 Pct Recovery = 161% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 28.461 Expected Conc. = 30.1 Report level label = 12 Pct Recovery = 95% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 27.720 Expected Conc. = 30.1 Report level label = 12 Pct Recovery = 92% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210270007 Lab Value = 44.762 Expected Conc. = 30.06 Report level label = 12 Pct Recovery = 149% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202040027 Lab Value = 26.529 Expected Conc. = 30.06 Report level label = 12 Pct Recovery = 88% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 27.358 Expected Conc. = 30.06 Report level label = 12 Pct Recovery = 91% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201610160 Lab Value = 30.423 Expected Conc. = 29.94 Report level label = 12 Pct Recovery = 102% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Analysis Date = 08/16/22 Pct Recovery = 92% Analysis Date = 08/11/22 Pct Recovery = 92% Analysis Date = 08/11/22 Pct Recovery = 92% Analysis Date = 08/07/22 Pct Recovery = 92% Analysis Date = 08/07/22 Pct Recovery = 92% Analysis Date = 08/03/22 Pct Recovery = 93% Analysis Date = 08/03/22 Pct Recovery = 93% Analysis Date = 07/30/22 Pct Recovery = 93% Analysis Date = 07/30/22 Pct Recovery = 93% Analysis Date = 07/26/22 Pct Recovery = 93% Analysis Date = 07/26/22 Pct Recovery = 93% Analysis Date = 07/22/22 Pct Recovery = 93% Analysis Date = 07/22/22 Pct Recovery = 93% Analysis Date = 07/18/22 Pct Recovery = 93% Analysis Date = 07/18/22 Pct Recovery = 93% Analysis Date = 07/14/22 Pct Recovery = 93% Analysis Date = 07/14/22 Pct Recovery = 93% Analysis Date = 07/10/22 Pct Recovery = 94% Analysis Date = 07/10/22 Pct Recovery = 94% Analysis Date = 07/06/22 Pct Recovery = 94% Analysis Date = 07/06/22 Pct Recovery = 94% Analysis Date = 07/02/22 Pct Recovery = 94% Analysis Date = 07/02/22 Pct Recovery = 94% Analysis Date = 06/27/22 Pct Recovery = 94% Analysis Date = 06/27/22 Pct Recovery = 94% Analysis Date = 06/23/22 Pct Recovery = 94% Analysis Date = 06/23/22 Pct Recovery = 94% Analysis Date = 06/19/22 Pct Recovery = 94% Analysis Date = 06/19/22 Pct Recovery = 94% Analysis Date = 06/15/22 Pct Recovery = 95% Analysis Date = 06/15/22 Pct Recovery = 95% Analysis Date = 06/11/22 Pct Recovery = 95% Analysis Date = 06/11/22 Pct Recovery = 95% Analysis Date = 06/07/22 Pct Recovery = 95% Analysis Date = 06/07/22 Pct Recovery = 95% Analysis Date = 06/03/22 Pct Recovery = 95% Analysis Date = 06/03/22 Pct Recovery = 95% Analysis Date = 05/30/22 Pct Recovery = 95% Analysis Date = 05/30/22 Pct Recovery = 95% Analysis Date = 05/26/22 Pct Recovery = 96% Analysis Date = 05/26/22 Pct Recovery = 96% Analysis Date = 05/22/22 Pct Recovery = 96% Analysis Date = 05/22/22 Pct Recovery = 96% Analysis Date = 05/18/22 Pct Recovery = 96% Analysis Date = 05/18/22 Pct Recovery = 96% Analysis Date = 05/13/22 Pct Recovery = 96% Analysis Date = 05/13/22 Pct Recovery = 96% Analysis Date = 05/09/22 Pct Recovery = 96% Analysis Date = 05/09/22 Pct Recovery = 96% Analysis Date = 05/05/22 Pct Recovery = 97% Analysis Date = 05/05/22 Pct Recovery = 97% Analysis Date = 05/01/22 Pct Recovery = 97% Analysis Date = 05/01/22 Pct Recovery = 97% Analysis Date = 04/27/22 Pct Recovery = 97% Analysis Date = 04/27/22 Pct Recovery = 97% Analysis Date = 04/23/22 Pct Recovery = 97% Analysis Date = 04/23/22 Pct Recovery = 97% Analysis Date = 04/19/22 Pct Recovery = 97% Analysis Date = 04/19/22 Pct Recovery = 97% Analysis Date = 04/15/22 Pct Recovery = 98% Analysis Date = 04/15/22 Pct Recovery = 98% Analysis Date = 04/11/22 Pct Recovery = 98% Analysis Date = 04/11/22 Pct Recovery = 98% Analysis Date = 04/07/22 Pct Recovery = 98% Analysis Date = 04/07/22 Pct Recovery = 98% Analysis Date = 04/03/22 Pct Recovery = 98% Analysis Date = 04/03/22 Pct Recovery = 98% Analysis Date = 03/29/22 Pct Recovery = 99% Analysis Date = 03/29/22 Pct Recovery = 99% Analysis Date = 03/25/22 Pct Recovery = 99% Analysis Date = 03/25/22 Pct Recovery = 99% Analysis Date = 03/21/22 Pct Recovery = 99% Analysis Date = 03/21/22 Pct Recovery = 99% Analysis Date = 03/17/22 Pct Recovery = 99% Analysis Date = 03/17/22 Pct Recovery = 99% Analysis Date = 03/13/22 Pct Recovery = 99% Analysis Date = 03/13/22 Pct Recovery = 99% Analysis Date = 03/09/22 Pct Recovery = 100% Analysis Date = 03/09/22 Pct Recovery = 100% Analysis Date = 03/05/22 Pct Recovery = 100% Analysis Date = 03/05/22 Pct Recovery = 100% Analysis Date = 03/01/22 Pct Recovery = 100% Analysis Date = 03/01/22 Pct Recovery = 100% Analysis Date = 02/25/22 Pct Recovery = 100% Analysis Date = 02/25/22 Pct Recovery = 100% Analysis Date = 02/21/22 Pct Recovery = 100% Analysis Date = 02/21/22 Pct Recovery = 100% Analysis Date = 02/17/22 Pct Recovery = 101% Analysis Date = 02/17/22 Pct Recovery = 101% Analysis Date = 02/12/22 Pct Recovery = 101% Analysis Date = 02/12/22 Pct Recovery = 101% Analysis Date = 02/08/22 Pct Recovery = 101% Analysis Date = 02/08/22 Pct Recovery = 101% Analysis Date = 02/04/22 Pct Recovery = 101% Analysis Date = 02/04/22 Pct Recovery = 101% Analysis Date = 01/31/22 Pct Recovery = 101% Analysis Date = 01/31/22 Pct Recovery = 101% Analysis Date = 01/27/22 Pct Recovery = 102% Analysis Date = 01/27/22 Pct Recovery = 102% Analysis Date = 01/23/22 Pct Recovery = 102% Analysis Date = 01/23/22 Pct Recovery = 102% Analysis Date = 01/19/22 Pct Recovery = 102% Analysis Date = 01/19/22 Pct Recovery = 102% Analysis Date = 01/15/22 Pct Recovery = 102% Analysis Date = 01/15/22 Pct Recovery = 102% Analysis Date = 01/11/22 Pct Recovery = 102% Analysis Date = 01/11/22 Pct Recovery = 102% Analysis Date = 01/07/22 Pct Recovery = 103% Analysis Date = 01/07/22 Pct Recovery = 103% Analysis Date = 01/03/22 Pct Recovery = 103% Analysis Date = 01/03/22 Pct Recovery = 103% Analysis Date = 12/29/21 Pct Recovery = 103% Analysis Date = 12/29/21 Pct Recovery = 103% Analysis Date = 12/25/21 Pct Recovery = 103% Analysis Date = 12/25/21 Pct Recovery = 103% Analysis Date = 12/21/21 Pct Recovery = 104% Analysis Date = 12/21/21 Pct Recovery = 104% Analysis Date = 12/17/21 Pct Recovery = 104% Analysis Date = 12/17/21 Pct Recovery = 104% Analysis Date = 12/13/21 Pct Recovery = 104% Analysis Date = 12/13/21 Pct Recovery = 104% Analysis Date = 12/09/21 Pct Recovery = 104% Analysis Date = 12/09/21 Pct Recovery = 104% Analysis Date = 12/05/21 Pct Recovery = 104% Analysis Date = 12/05/21 Pct Recovery = 104% Analysis Date = 12/01/21 Pct Recovery = 105% Analysis Date = 12/01/21 Pct Recovery = 105% Analysis Date = 11/27/21 Pct Recovery = 105% Analysis Date = 11/27/21 Pct Recovery = 105% Analysis Date = 11/23/21 Pct Recovery = 105% Analysis Date = 11/23/21 Pct Recovery = 105% Analysis Date = 11/19/21 Pct Recovery = 105% Analysis Date = 11/19/21 Pct Recovery = 105% Analysis Date = 11/14/21 Pct Recovery = 105% Analysis Date = 11/14/21 Pct Recovery = 105% Analysis Date = 11/10/21 Pct Recovery = 106% Analysis Date = 11/10/21 Pct Recovery = 106% Analysis Date = 11/06/21 Pct Recovery = 106% Analysis Date = 11/06/21 Pct Recovery = 106% Analysis Date = 11/02/21 Pct Recovery = 106% Analysis Date = 11/02/21 Pct Recovery = 106% Analysis Date = 10/29/21 Pct Recovery = 106% Analysis Date = 10/29/21 Pct Recovery = 106% Analysis Date = 10/25/21 Pct Recovery = 106% Analysis Date = 10/25/21 Pct Recovery = 106% Analysis Date = 10/21/21 Pct Recovery = 107% Analysis Date = 10/21/21 Pct Recovery = 107% Analysis Date = 10/17/21 Pct Recovery = 107% Analysis Date = 10/17/21 Pct Recovery = 107% Analysis Date = 10/13/21 Pct Recovery = 107% Analysis Date = 10/13/21 Pct Recovery = 107% Analysis Date = 10/09/21 Pct Recovery = 107% Analysis Date = 10/09/21 Pct Recovery = 107% Analysis Date = 10/05/21 Pct Recovery = 107% Analysis Date = 10/05/21 Pct Recovery = 107% Analysis Date = 09/30/21 Pct Recovery = 108% Analysis Date = 09/30/21 Pct Recovery = 108% Analysis Date = 09/26/21 Pct Recovery = 108% Analysis Date = 09/26/21 Pct Recovery = 108% Analysis Date = 09/22/21 Pct Recovery = 108% Analysis Date = 09/22/21 Pct Recovery = 108% Analysis Date = 09/18/21 Pct Recovery = 108% Analysis Date = 09/18/21 Pct Recovery = 108% Analysis Date = 09/14/21 Pct Recovery = 109% Analysis Date = 09/14/21 Pct Recovery = 109% Analysis Date = 09/10/21 Pct Recovery = 109% Analysis Date = 09/10/21 Pct Recovery = 109% Analysis Date = 09/06/21 Pct Recovery = 109% Analysis Date = 09/06/21 Pct Recovery = 109% Analysis Date = 09/02/21 Pct Recovery = 109% Analysis Date = 09/02/21 Pct Recovery = 109% Analysis Date = 08/29/21 Pct Recovery = 109% Analysis Date = 08/29/21 Pct Recovery = 109% Analysis Date = 08/25/21 Pct Recovery = 110% Analysis Date = 08/25/21 Pct Recovery = 110% Analysis Date = 08/21/21 Pct Recovery = 110% Analysis Date = 08/21/21 Pct Recovery = 110% Analysis Date = 08/16/21 Pct Recovery = 110% Analysis Date = 08/16/21 Pct Recovery = 110% Analysis Date = 08/12/21 Pct Recovery = 110% Analysis Date = 08/12/21 Pct Recovery = 110% Analysis Date = 08/08/21 Pct Recovery = 110% Analysis Date = 08/08/21 Pct Recovery = 110% Analysis Date = 08/04/21 Pct Recovery = 111% Analysis Date = 08/04/21 Pct Recovery = 111% Analysis Date = 07/31/21 Pct Recovery = 111% Analysis Date = 07/31/21 Pct Recovery = 111% Analysis Date = 07/27/21 Pct Recovery = 111% Analysis Date = 07/27/21 Pct Recovery = 111% Analysis Date = 07/23/21 Pct Recovery = 111% Analysis Date = 07/23/21 Pct Recovery = 111% Analysis Date = 07/19/21 Pct Recovery = 111% Analysis Date = 07/19/21 Pct Recovery = 111% Analysis Date = 07/15/21 Pct Recovery = 112% Analysis Date = 07/15/21 Pct Recovery = 112% Analysis Date = 07/11/21 Pct Recovery = 112% Analysis Date = 07/11/21 Pct Recovery = 112% Analysis Date = 07/07/21 Pct Recovery = 112% Analysis Date = 07/07/21 Pct Recovery = 112% Analysis Date = 07/03/21 Pct Recovery = 112% Analysis Date = 07/03/21 Pct Recovery = 112% Analysis Date = 06/28/21 Pct Recovery = 112% Analysis Date = 06/28/21 Pct Recovery = 112% Analysis Date = 06/24/21 Pct Recovery = 113% Analysis Date = 06/24/21 Pct Recovery = 113% Analysis Date = 06/20/21 Pct Recovery = 113% Analysis Date = 06/20/21 Pct Recovery = 113% Analysis Date = 06/16/21 Pct Recovery = 113% Analysis Date = 06/16/21 Pct Recovery = 113% Analysis Date = 06/12/21 Pct Recovery = 113% Analysis Date = 06/12/21 Pct Recovery = 113% Analysis Date = 06/08/21 Pct Recovery = 113% Analysis Date = 06/08/21 Pct Recovery = 113% Analysis Date = 06/04/21 Pct Recovery = 114% Analysis Date = 06/04/21 Pct Recovery = 114% Analysis Date = 05/31/21 Pct Recovery = 114% Analysis Date = 05/31/21 Pct Recovery = 114% Analysis Date = 05/27/21 Pct Recovery = 114% Analysis Date = 05/27/21 Pct Recovery = 114% Analysis Date = 05/23/21 Pct Recovery = 114% Analysis Date = 05/23/21 Pct Recovery = 114% Analysis Date = 05/19/21 Pct Recovery = 115% Analysis Date = 05/19/21 Pct Recovery = 115% Analysis Date = 05/14/21 Pct Recovery = 115% Analysis Date = 05/14/21 Pct Recovery = 115% Analysis Date = 05/10/21 Pct Recovery = 115% Analysis Date = 05/10/21 Pct Recovery = 115% Analysis Date = 05/06/21 Pct Recovery = 115% Analysis Date = 05/06/21 Pct Recovery = 115% Analysis Date = 05/02/21 Pct Recovery = 115% Analysis Date = 05/02/21 Pct Recovery = 115% Analysis Date = 04/28/21 Pct Recovery = 116% Analysis Date = 04/28/21 Pct Recovery = 116% Analysis Date = 04/24/21 Pct Recovery = 116% Analysis Date = 04/24/21 Pct Recovery = 116% Analysis Date = 04/20/21 Pct Recovery = 116% Analysis Date = 04/20/21 Pct Recovery = 116% Analysis Date = 04/16/21 Pct Recovery = 116% Analysis Date = 04/16/21 Pct Recovery = 116% Analysis Date = 04/12/21 Pct Recovery = 116% Analysis Date = 04/12/21 Pct Recovery = 116% Analysis Date = 04/08/21 Pct Recovery = 117% Analysis Date = 04/08/21 Pct Recovery = 117% Analysis Date = 04/04/21 Pct Recovery = 117% Analysis Date = 04/04/21 Pct Recovery = 117% Analysis Date = 03/30/21 Pct Recovery = 117% Analysis Date = 03/30/21 Pct Recovery = 117% Analysis Date = 03/26/21 Pct Recovery = 117% Analysis Date = 03/26/21 Pct Recovery = 117% Analysis Date = 03/22/21 Pct Recovery = 117% Analysis Date = 03/22/21 Pct Recovery = 117% Analysis Date = 03/18/21 Pct Recovery = 117% Analysis Date = 03/18/21 Pct Recovery = 117% Analysis Date = 03/14/21 Pct Recovery = 118% Analysis Date = 03/14/21 Pct Recovery = 118% Analysis Date = 03/10/21 Pct Recovery = 118% Analysis Date = 03/10/21 Pct Recovery = 118% Analysis Date = 03/06/21 Pct Recovery = 118% Analysis Date = 03/06/21 Pct Recovery = 118% Analysis Date = 03/02/21 Pct Recovery = 118% Analysis Date = 03/02/21 Pct Recovery = 118% Analysis Date = 02/26/21 Pct Recovery = 118% Analysis Date = 02/26/21 Pct Recovery = 118% Analysis Date = 02/22/21 Pct Recovery = 118% Analysis Date = 02/22/21 Pct Recovery = 118% Analysis Date = 02/18/21 Pct Recovery = 119% Analysis Date = 02/18/21 Pct Recovery = 119% Analysis Date = 02/13/21 Pct Recovery = 119% Analysis Date = 02/13/21 Pct Recovery = 119% Analysis Date = 02/09/21 Pct Recovery = 119% Analysis Date = 02/09/21 Pct Recovery = 119% Analysis Date = 02/05/21 Pct Recovery = 119% Analysis Date = 02/05/21 Pct Recovery = 119% Analysis Date = 02/01/21 Pct Recovery = 119% Analysis Date = 02/01/21 Pct Recovery = 119% Analysis Date = 01/28/21 Pct Recovery = 119% Analysis Date = 01/28/21 Pct Recovery = 119% Analysis Date = 01/24/21 Pct Recovery = 119% Analysis Date = 01/24/21 Pct Recovery = 119% Analysis Date = 01/20/21 Pct Recovery = 119% Analysis Date = 01/20/21 Pct Recovery = 119% Analysis Date = 01/16/21 Pct Recovery = 119% Analysis Date = 01/16/21 Pct Recovery = 119% Analysis Date = 01/12/21 Pct Recovery = 119% Analysis Date = 01/12/21 Pct Recovery = 119% Analysis Date = 01/08/21 Pct Recovery = 119% Analysis Date = 01/08/21 Pct Recovery = 119% Analysis Date = 01/04/21 Pct Recovery = 119% Analysis Date = 01/04/21 Pct Recovery = 119% Analysis Date = 12/30/20 Pct Recovery = 119% Analysis Date = 12/30/20 Pct Recovery = 119% Analysis Date = 12/26/20 Pct Recovery = 119% Analysis Date = 12/26/20 Pct Recovery = 119% Analysis Date = 12/22/20 Pct Recovery = 119% Analysis Date = 12/22/20 Pct Recovery = 119% Analysis Date = 12/18/20 Pct Recovery = 119% Analysis Date = 12/18/20 Pct Recovery = 119% Analysis Date = 12/14/20 Pct Recovery = 119% Analysis Date = 12/14/20 Pct Recovery = 119% Analysis Date = 12/10/20 Pct Recovery = 119% Analysis Date = 12/10/20 Pct Recovery = 119% Analysis Date = 12/06/20 Pct Recovery = 118% Analysis Date = 12/06/20 Pct Recovery = 118% Analysis Date = 12/02/20 Pct Recovery = 117% Analysis Date = 12/02/20 Pct Recovery = 117% Analysis Date = 11/28/20 Pct Recovery = 116% Analysis Date = 11/28/20 Pct Recovery = 116% Analysis Date = 11/24/20 Pct Recovery = 115% Analysis Date = 11/24/20 Pct Recovery = 115% Analysis Date = 11/20/20 Pct Recovery = 114% Analysis Date = 11/20/20 Pct Recovery = 114% Analysis Date = 11/15/20 Pct Recovery = 113% Analysis Date = 11/15/20 Pct Recovery = 113% Analysis Date = 11/11/20 Pct Recovery = 112% Analysis Date = 11/11/20 Pct Recovery = 112% Analysis Date = 11/07/20 Pct Recovery = 112% Analysis Date = 11/07/20 Pct Recovery = 112% Analysis Date = 11/03/20 Pct Recovery = 111% Analysis Date = 11/03/20 Pct Recovery = 111% Analysis Date = 10/30/20 Pct Recovery = 110% Analysis Date = 10/30/20 Pct Recovery = 110% Analysis Date = 10/26/20 Pct Recovery = 110% Analysis Date = 10/26/20 Pct Recovery = 110% Analysis Date = 10/22/20 Pct Recovery = 109% Analysis Date = 10/22/20 Pct Recovery = 109% Analysis Date = 10/18/20 Pct Recovery = 109% Analysis Date = 10/18/20 Pct Recovery = 109% Analysis Date = 10/14/20 Pct Recovery = 108% Analysis Date = 10/14/20 Pct Recovery = 108% Analysis Date = 10/10/20 Pct Recovery = 108% Analysis Date = 10/10/20 Pct Recovery = 108% Analysis Date = 10/06/20 Pct Recovery = 107% Analysis Date = 10/06/20 Pct Recovery = 107% Analysis Date = 10/01/20 Pct Recovery = 106% Analysis Date = 10/01/20 Pct Recovery = 106% Analysis Date = 09/27/20 Pct Recovery = 106% Analysis Date = 09/27/20 Pct Recovery = 106% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/15/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/11/20 Pct Recovery = 104% Analysis Date = 09/07/20 Pct Recovery = 104% Analysis Date = 09/07/20 Pct Recovery = 104% Analysis Date = 09/03/20 Pct Recovery = 104% Analysis Date = 09/03/20 Pct Recovery = 104% Analysis Date = 08/30/20 Pct Recovery = 103% Analysis Date = 08/30/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/26/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/22/20 Pct Recovery = 103% Analysis Date = 08/17/20 Pct Recovery = 103% Analysis Date = 08/17/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/13/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/09/20 Pct Recovery = 103% Analysis Date = 08/05/20 Pct Recovery = 103% Analysis Date = 08/05/20 Pct Recovery = 103% Analysis Date = 08/01/20 Pct Recovery = 104% Analysis Date = 08/01/20 Pct Recovery = 104% Analysis Date = 07/28/20 Pct Recovery = 104% Analysis Date = 07/28/20 Pct Recovery = 104% Analysis Date = 07/24/20 Pct Recovery = 104% Analysis Date = 07/24/20 Pct Recovery = 104% Analysis Date = 07/20/20 Pct Recovery = 104% Analysis Date = 07/20/20 Pct Recovery = 104% Analysis Date = 07/16/20 Pct Recovery = 104% Analysis Date = 07/16/20 Pct Recovery = 104% Analysis Date = 07/12/20 Pct Recovery = 104% Analysis Date = 07/12/20 Pct Recovery = 104% Analysis Date = 07/08/20 Pct Recovery = 104% Analysis Date = 07/08/20 Pct Recovery = 104% Analysis Date = 07/03/20 Pct Recovery = 105% Analysis Date = 07/03/20 Pct Recovery = 105% Analysis Date = 06/29/20 Pct Recovery = 105% Analysis Date = 06/29/20 Pct Recovery = 105% Analysis Date = 06/25/20 Pct Recovery = 105% Analysis Date = 06/25/20 Pct Recovery = 105% Analysis Date = 06/21/20 Pct Recovery = 105% Analysis Date = 06/21/20 Pct Recovery = 105% Analysis Date = 06/17/20 Pct Recovery = 105% Analysis Date = 06/17/20 Pct Recovery = 105% Analysis Date = 06/13/20 Pct Recovery = 106% Analysis Date = 06/13/20 Pct Recovery = 106% Analysis Date = 06/09/20 Pct Recovery = 106% Analysis Date = 06/09/20 Pct Recovery = 106% Analysis Date = 06/05/20 Pct Recovery = 106% Analysis Date = 06/05/20 Pct Recovery = 106% Analysis Date = 06/01/20 Pct Recovery = 106% Analysis Date = 06/01/20 Pct Recovery = 106% Analysis Date = 05/28/20 Pct Recovery = 106% Analysis Date = 05/28/20 Pct Recovery = 106% Analysis Date = 05/24/20 Pct Recovery = 107% Analysis Date = 05/24/20 Pct Recovery = 107% Analysis Date = 05/20/20 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ORYZALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 29 107% 20% 102% 18%
Total 29 107% 20% 102% 18%

Sample Statistics
ORYZALIN

Characteristic N % % Basis
Plotted 29 91% Spiked
Estimated Values 10 31% Spiked
Deleted Values 3 3% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 32 .  
False Negatives 2 6% 2 out of 32
Not Spiked 84 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
PIPERONYL BUTOXIDE
METHOD: 2447 , TESTIDCODE: 65102LCM60

Laboratory ID = 20201820155 Lab Value = 676.118 Expected Conc. = 754.1 Report level label = 25 Pct Recovery = 90% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20202110006 Lab Value = 692.249 Expected Conc. = 736.7 Report level label = 25 Pct Recovery = 94% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 352.247 Expected Conc. = 377.05 Report level label = 25 Pct Recovery = 93% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 308.350 Expected Conc. = 377.05 Report level label = 25 Pct Recovery = 82% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 362.768 Expected Conc. = 377.05 Report level label = 25 Pct Recovery = 96% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201680155 Lab Value = 360.278 Expected Conc. = 368.35 Report level label = 25 Pct Recovery = 98% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20203080100 Lab Value = 278.090 Expected Conc. = 310 Report level label = 25 Pct Recovery = 90% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 272.811 Expected Conc. = 310 Report level label = 25 Pct Recovery = 88% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 278.664 Expected Conc. = 310 Report level label = 25 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 250.369 Expected Conc. = 307.8 Report level label = 25 Pct Recovery = 81% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 224.618 Expected Conc. = 307.8 Report level label = 25 Pct Recovery = 73% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 227.328 Expected Conc. = 307.8 Report level label = 25 Pct Recovery = 74% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 288.785 Expected Conc. = 307.8 Report level label = 25 Pct Recovery = 94% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20212990174 Lab Value = 163.002 Expected Conc. = 251.28 Report level label = 25 Pct Recovery = 65% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 116.248 Expected Conc. = 250 Report level label = 25 Pct Recovery = 46% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 206.304 Expected Conc. = 249.2 Report level label = 25 Pct Recovery = 83% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20220190116 Lab Value = 139.416 Expected Conc. = 247.92 Report level label = 25 Pct Recovery = 56% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 153.675 Expected Conc. = 247.92 Report level label = 25 Pct Recovery = 62% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 142.314 Expected Conc. = 247.2 Report level label = 25 Pct Recovery = 58% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20213340027 Lab Value = 108.680 Expected Conc. = 157.05 Report level label = 25 Pct Recovery = 69% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 303.556 Expected Conc. = 157.05 Report level label = 25 Pct Recovery = 193% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 87.511 Expected Conc. = 157.05 Report level label = 25 Pct Recovery = 56% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20220810133 Lab Value = 129.395 Expected Conc. = 155.75 Report level label = 25 Pct Recovery = 83% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20202880004 Lab Value = 148.553 Expected Conc. = 155 Report level label = 25 Pct Recovery = 96% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221730293 Lab Value = 104.298 Expected Conc. = 154.95 Report level label = 25 Pct Recovery = 67% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 84.440 Expected Conc. = 154.95 Report level label = 25 Pct Recovery = 54% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20210480001 Lab Value = 104.838 Expected Conc. = 153.9 Report level label = 25 Pct Recovery = 68% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202330309 Lab Value = 137.747 Expected Conc. = 150.82 Report level label = 25 Pct Recovery = 91% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 164.972 Expected Conc. = 150.82 Report level label = 25 Pct Recovery = 109% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 169.764 Expected Conc. = 150.82 Report level label = 25 Pct Recovery = 113% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 169.620 Expected Conc. = 150.82 Report level label = 25 Pct Recovery = 112% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201610160 Lab Value = 123.831 Expected Conc. = 147.34 Report level label = 25 Pct Recovery = 84% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20210620006 Lab Value = 104.223 Expected Conc. = 124 Report level label = 25 Pct Recovery = 84% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 97.645 Expected Conc. = 124 Report level label = 25 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 109.098 Expected Conc. = 123.12 Report level label = 25 Pct Recovery = 89% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20213060210 Lab Value = 30.796 Expected Conc. = 62.82 Report level label = 25 Pct Recovery = 49% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222630205 Lab Value = 45.573 Expected Conc. = 62.3 Report level label = 25 Pct Recovery = 73% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210120050 Lab Value = 43.832 Expected Conc. = 62 Report level label = 25 Pct Recovery = 71% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 56.268 Expected Conc. = 62 Report level label = 25 Pct Recovery = 91% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 48.730 Expected Conc. = 62 Report level label = 25 Pct Recovery = 79% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 56.331 Expected Conc. = 62 Report level label = 25 Pct Recovery = 91% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 53.607 Expected Conc. = 62 Report level label = 25 Pct Recovery = 86% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222500483 Lab Value = 44.275 Expected Conc. = 61.98 Report level label = 25 Pct Recovery = 71% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 35.521 Expected Conc. = 61.98 Report level label = 25 Pct Recovery = 57% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210690067 Lab Value = 56.004 Expected Conc. = 61.56 Report level label = 25 Pct Recovery = 91% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 09/28/22 Pct Recovery = 63% Analysis Date = 09/24/22 Pct Recovery = 63% Analysis Date = 09/24/22 Pct Recovery = 63% Analysis Date = 09/20/22 Pct Recovery = 63% Analysis Date = 09/20/22 Pct Recovery = 63% Analysis Date = 09/16/22 Pct Recovery = 63% Analysis Date = 09/16/22 Pct Recovery = 63% Analysis Date = 09/11/22 Pct Recovery = 64% Analysis Date = 09/11/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/07/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 09/03/22 Pct Recovery = 64% Analysis Date = 08/29/22 Pct Recovery = 64% Analysis Date = 08/29/22 Pct Recovery = 64% Analysis Date = 08/25/22 Pct Recovery = 64% Analysis Date = 08/25/22 Pct Recovery = 64% Analysis Date = 08/21/22 Pct Recovery = 64% Analysis Date = 08/21/22 Pct Recovery = 64% Analysis Date = 08/16/22 Pct Recovery = 65% Analysis Date = 08/16/22 Pct Recovery = 65% Analysis Date = 08/12/22 Pct Recovery = 65% Analysis Date = 08/12/22 Pct Recovery = 65% Analysis Date = 08/08/22 Pct Recovery = 65% Analysis Date = 08/08/22 Pct Recovery = 65% Analysis Date = 08/03/22 Pct Recovery = 65% Analysis Date = 08/03/22 Pct Recovery = 65% Analysis Date = 07/30/22 Pct Recovery = 65% Analysis Date = 07/30/22 Pct Recovery = 65% Analysis Date = 07/26/22 Pct Recovery = 66% Analysis Date = 07/26/22 Pct Recovery = 66% Analysis Date = 07/21/22 Pct Recovery = 66% Analysis Date = 07/21/22 Pct Recovery = 66% Analysis Date = 07/17/22 Pct Recovery = 66% Analysis Date = 07/17/22 Pct Recovery = 66% Analysis Date = 07/13/22 Pct Recovery = 66% Analysis Date = 07/13/22 Pct Recovery = 66% Analysis Date = 07/09/22 Pct Recovery = 66% Analysis Date = 07/09/22 Pct Recovery = 66% Analysis Date = 07/04/22 Pct Recovery = 66% Analysis Date = 07/04/22 Pct Recovery = 66% Analysis Date = 06/30/22 Pct Recovery = 67% Analysis Date = 06/30/22 Pct Recovery = 67% Analysis Date = 06/26/22 Pct Recovery = 67% Analysis Date = 06/26/22 Pct Recovery = 67% Analysis Date = 06/21/22 Pct Recovery = 67% Analysis Date = 06/21/22 Pct Recovery = 67% Analysis Date = 06/17/22 Pct Recovery = 67% Analysis Date = 06/17/22 Pct Recovery = 67% Analysis Date = 06/13/22 Pct Recovery = 67% Analysis Date = 06/13/22 Pct Recovery = 67% Analysis Date = 06/08/22 Pct Recovery = 68% Analysis Date = 06/08/22 Pct Recovery = 68% Analysis Date = 06/04/22 Pct Recovery = 68% Analysis Date = 06/04/22 Pct Recovery = 68% Analysis Date = 05/31/22 Pct Recovery = 68% Analysis Date = 05/31/22 Pct Recovery = 68% Analysis Date = 05/26/22 Pct Recovery = 68% Analysis Date = 05/26/22 Pct Recovery = 68% Analysis Date = 05/22/22 Pct Recovery = 68% Analysis Date = 05/22/22 Pct Recovery = 68% Analysis Date = 05/18/22 Pct Recovery = 68% Analysis Date = 05/18/22 Pct Recovery = 68% Analysis Date = 05/13/22 Pct Recovery = 69% Analysis Date = 05/13/22 Pct Recovery = 69% Analysis Date = 05/09/22 Pct Recovery = 69% Analysis Date = 05/09/22 Pct Recovery = 69% Analysis Date = 05/05/22 Pct Recovery = 69% Analysis Date = 05/05/22 Pct Recovery = 69% Analysis Date = 04/30/22 Pct Recovery = 69% Analysis Date = 04/30/22 Pct Recovery = 69% Analysis Date = 04/26/22 Pct Recovery = 69% Analysis Date = 04/26/22 Pct Recovery = 69% Analysis Date = 04/22/22 Pct Recovery = 70% Analysis Date = 04/22/22 Pct Recovery = 70% Analysis Date = 04/18/22 Pct Recovery = 70% Analysis Date = 04/18/22 Pct Recovery = 70% Analysis Date = 04/13/22 Pct Recovery = 70% Analysis Date = 04/13/22 Pct Recovery = 70% Analysis Date = 04/09/22 Pct Recovery = 70% Analysis Date = 04/09/22 Pct Recovery = 70% Analysis Date = 04/05/22 Pct Recovery = 70% Analysis Date = 04/05/22 Pct Recovery = 70% Analysis Date = 03/31/22 Pct Recovery = 70% Analysis Date = 03/31/22 Pct Recovery = 70% Analysis Date = 03/27/22 Pct Recovery = 71% Analysis Date = 03/27/22 Pct Recovery = 71% Analysis Date = 03/23/22 Pct Recovery = 71% Analysis Date = 03/23/22 Pct Recovery = 71% Analysis Date = 03/18/22 Pct Recovery = 71% Analysis Date = 03/18/22 Pct Recovery = 71% Analysis Date = 03/14/22 Pct Recovery = 71% Analysis Date = 03/14/22 Pct Recovery = 71% Analysis Date = 03/10/22 Pct Recovery = 71% Analysis Date = 03/10/22 Pct Recovery = 71% Analysis Date = 03/05/22 Pct Recovery = 72% Analysis Date = 03/05/22 Pct Recovery = 72% Analysis Date = 03/01/22 Pct Recovery = 72% Analysis Date = 03/01/22 Pct Recovery = 72% Analysis Date = 02/25/22 Pct Recovery = 72% Analysis Date = 02/25/22 Pct Recovery = 72% Analysis Date = 02/20/22 Pct Recovery = 72% Analysis Date = 02/20/22 Pct Recovery = 72% Analysis Date = 02/16/22 Pct Recovery = 72% Analysis Date = 02/16/22 Pct Recovery = 72% Analysis Date = 02/12/22 Pct Recovery = 72% Analysis Date = 02/12/22 Pct Recovery = 72% Analysis Date = 02/07/22 Pct Recovery = 73% Analysis Date = 02/07/22 Pct Recovery = 73% Analysis Date = 02/03/22 Pct Recovery = 73% Analysis Date = 02/03/22 Pct Recovery = 73% Analysis Date = 01/30/22 Pct Recovery = 73% Analysis Date = 01/30/22 Pct Recovery = 73% Analysis Date = 01/26/22 Pct Recovery = 73% Analysis Date = 01/26/22 Pct Recovery = 73% Analysis Date = 01/21/22 Pct Recovery = 73% Analysis Date = 01/21/22 Pct Recovery = 73% Analysis Date = 01/17/22 Pct Recovery = 74% Analysis Date = 01/17/22 Pct Recovery = 74% Analysis Date = 01/13/22 Pct Recovery = 74% Analysis Date = 01/13/22 Pct Recovery = 74% Analysis Date = 01/08/22 Pct Recovery = 74% Analysis Date = 01/08/22 Pct Recovery = 74% Analysis Date = 01/04/22 Pct Recovery = 74% Analysis Date = 01/04/22 Pct Recovery = 74% Analysis Date = 12/31/21 Pct Recovery = 74% Analysis Date = 12/31/21 Pct Recovery = 74% Analysis Date = 12/26/21 Pct Recovery = 74% Analysis Date = 12/26/21 Pct Recovery = 74% Analysis Date = 12/22/21 Pct Recovery = 75% Analysis Date = 12/22/21 Pct Recovery = 75% Analysis Date = 12/18/21 Pct Recovery = 75% Analysis Date = 12/18/21 Pct Recovery = 75% Analysis Date = 12/13/21 Pct Recovery = 75% Analysis Date = 12/13/21 Pct Recovery = 75% Analysis Date = 12/09/21 Pct Recovery = 75% Analysis Date = 12/09/21 Pct Recovery = 75% Analysis Date = 12/05/21 Pct Recovery = 75% Analysis Date = 12/05/21 Pct Recovery = 75% Analysis Date = 11/30/21 Pct Recovery = 75% Analysis Date = 11/30/21 Pct Recovery = 75% Analysis Date = 11/26/21 Pct Recovery = 76% Analysis Date = 11/26/21 Pct Recovery = 76% Analysis Date = 11/22/21 Pct Recovery = 76% Analysis Date = 11/22/21 Pct Recovery = 76% Analysis Date = 11/18/21 Pct Recovery = 76% Analysis Date = 11/18/21 Pct Recovery = 76% Analysis Date = 11/13/21 Pct Recovery = 76% Analysis Date = 11/13/21 Pct Recovery = 76% Analysis Date = 11/09/21 Pct Recovery = 76% Analysis Date = 11/09/21 Pct Recovery = 76% Analysis Date = 11/05/21 Pct Recovery = 76% Analysis Date = 11/05/21 Pct Recovery = 76% Analysis Date = 10/31/21 Pct Recovery = 76% Analysis Date = 10/31/21 Pct Recovery = 76% Analysis Date = 10/27/21 Pct Recovery = 76% Analysis Date = 10/27/21 Pct Recovery = 76% Analysis Date = 10/23/21 Pct Recovery = 76% Analysis Date = 10/23/21 Pct Recovery = 76% Analysis Date = 10/18/21 Pct Recovery = 76% Analysis Date = 10/18/21 Pct Recovery = 76% Analysis Date = 10/14/21 Pct Recovery = 76% Analysis Date = 10/14/21 Pct Recovery = 76% Analysis Date = 10/10/21 Pct Recovery = 76% Analysis Date = 10/10/21 Pct Recovery = 76% Analysis Date = 10/05/21 Pct Recovery = 77% Analysis Date = 10/05/21 Pct Recovery = 77% Analysis Date = 10/01/21 Pct Recovery = 77% Analysis Date = 10/01/21 Pct Recovery = 77% Analysis Date = 09/27/21 Pct Recovery = 77% Analysis Date = 09/27/21 Pct Recovery = 77% Analysis Date = 09/22/21 Pct Recovery = 77% Analysis Date = 09/22/21 Pct Recovery = 77% Analysis Date = 09/18/21 Pct Recovery = 77% Analysis Date = 09/18/21 Pct Recovery = 77% Analysis Date = 09/14/21 Pct Recovery = 77% Analysis Date = 09/14/21 Pct Recovery = 77% Analysis Date = 09/09/21 Pct Recovery = 77% Analysis Date = 09/09/21 Pct Recovery = 77% Analysis Date = 09/05/21 Pct Recovery = 77% Analysis Date = 09/05/21 Pct Recovery = 77% Analysis Date = 09/01/21 Pct Recovery = 77% Analysis Date = 09/01/21 Pct Recovery = 77% Analysis Date = 08/28/21 Pct Recovery = 77% Analysis Date = 08/28/21 Pct Recovery = 77% Analysis Date = 08/23/21 Pct Recovery = 77% Analysis Date = 08/23/21 Pct Recovery = 77% Analysis Date = 08/19/21 Pct Recovery = 77% Analysis Date = 08/19/21 Pct Recovery = 77% Analysis Date = 08/15/21 Pct Recovery = 77% Analysis Date = 08/15/21 Pct Recovery = 77% Analysis Date = 08/10/21 Pct Recovery = 78% Analysis Date = 08/10/21 Pct Recovery = 78% Analysis Date = 08/06/21 Pct Recovery = 78% Analysis Date = 08/06/21 Pct Recovery = 78% Analysis Date = 08/02/21 Pct Recovery = 78% Analysis Date = 08/02/21 Pct Recovery = 78% Analysis Date = 07/28/21 Pct Recovery = 78% Analysis Date = 07/28/21 Pct Recovery = 78% Analysis Date = 07/24/21 Pct Recovery = 78% Analysis Date = 07/24/21 Pct Recovery = 78% Analysis Date = 07/20/21 Pct Recovery = 78% Analysis Date = 07/20/21 Pct Recovery = 78% Analysis Date = 07/15/21 Pct Recovery = 78% Analysis Date = 07/15/21 Pct Recovery = 78% Analysis Date = 07/11/21 Pct Recovery = 78% Analysis Date = 07/11/21 Pct Recovery = 78% Analysis Date = 07/07/21 Pct Recovery = 78% Analysis Date = 07/07/21 Pct Recovery = 78% Analysis Date = 07/02/21 Pct Recovery = 78% Analysis Date = 07/02/21 Pct Recovery = 78% Analysis Date = 06/28/21 Pct Recovery = 78% Analysis Date = 06/28/21 Pct Recovery = 78% Analysis Date = 06/24/21 Pct Recovery = 78% Analysis Date = 06/24/21 Pct Recovery = 78% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/07/21 Pct Recovery = 79% Analysis Date = 06/07/21 Pct Recovery = 79% Analysis Date = 06/02/21 Pct Recovery = 79% Analysis Date = 06/02/21 Pct Recovery = 79% Analysis Date = 05/29/21 Pct Recovery = 79% Analysis Date = 05/29/21 Pct Recovery = 79% Analysis Date = 05/25/21 Pct Recovery = 79% Analysis Date = 05/25/21 Pct Recovery = 79% Analysis Date = 05/20/21 Pct Recovery = 79% Analysis Date = 05/20/21 Pct Recovery = 79% Analysis Date = 05/16/21 Pct Recovery = 79% Analysis Date = 05/16/21 Pct Recovery = 79% Analysis Date = 05/12/21 Pct Recovery = 79% Analysis Date = 05/12/21 Pct Recovery = 79% Analysis Date = 05/07/21 Pct Recovery = 79% Analysis Date = 05/07/21 Pct Recovery = 79% Analysis Date = 05/03/21 Pct Recovery = 79% Analysis Date = 05/03/21 Pct Recovery = 79% Analysis Date = 04/29/21 Pct Recovery = 80% Analysis Date = 04/29/21 Pct Recovery = 80% Analysis Date = 04/24/21 Pct Recovery = 80% Analysis Date = 04/24/21 Pct Recovery = 80% Analysis Date = 04/20/21 Pct Recovery = 80% Analysis Date = 04/20/21 Pct Recovery = 80% Analysis Date = 04/16/21 Pct Recovery = 80% Analysis Date = 04/16/21 Pct Recovery = 80% Analysis Date = 04/11/21 Pct Recovery = 80% Analysis Date = 04/11/21 Pct Recovery = 80% Analysis Date = 04/07/21 Pct Recovery = 80% Analysis Date = 04/07/21 Pct Recovery = 80% Analysis Date = 04/03/21 Pct Recovery = 80% Analysis Date = 04/03/21 Pct Recovery = 80% Analysis Date = 03/29/21 Pct Recovery = 80% Analysis Date = 03/29/21 Pct Recovery = 80% Analysis Date = 03/25/21 Pct Recovery = 80% Analysis Date = 03/25/21 Pct Recovery = 80% Analysis Date = 03/21/21 Pct Recovery = 80% Analysis Date = 03/21/21 Pct Recovery = 80% Analysis Date = 03/17/21 Pct Recovery = 81% Analysis Date = 03/17/21 Pct Recovery = 81% Analysis Date = 03/12/21 Pct Recovery = 81% Analysis Date = 03/12/21 Pct Recovery = 81% Analysis Date = 03/08/21 Pct Recovery = 81% Analysis Date = 03/08/21 Pct Recovery = 81% Analysis Date = 03/04/21 Pct Recovery = 81% Analysis Date = 03/04/21 Pct Recovery = 81% Analysis Date = 02/27/21 Pct Recovery = 81% Analysis Date = 02/27/21 Pct Recovery = 81% Analysis Date = 02/23/21 Pct Recovery = 81% Analysis Date = 02/23/21 Pct Recovery = 81% Analysis Date = 02/19/21 Pct Recovery = 82% Analysis Date = 02/19/21 Pct Recovery = 82% Analysis Date = 02/14/21 Pct Recovery = 82% Analysis Date = 02/14/21 Pct Recovery = 82% Analysis Date = 02/10/21 Pct Recovery = 82% Analysis Date = 02/10/21 Pct Recovery = 82% Analysis Date = 02/06/21 Pct Recovery = 82% Analysis Date = 02/06/21 Pct Recovery = 82% Analysis Date = 02/01/21 Pct Recovery = 82% Analysis Date = 02/01/21 Pct Recovery = 82% Analysis Date = 01/28/21 Pct Recovery = 83% Analysis Date = 01/28/21 Pct Recovery = 83% Analysis Date = 01/24/21 Pct Recovery = 83% Analysis Date = 01/24/21 Pct Recovery = 83% Analysis Date = 01/19/21 Pct Recovery = 83% Analysis Date = 01/19/21 Pct Recovery = 83% Analysis Date = 01/15/21 Pct Recovery = 83% Analysis Date = 01/15/21 Pct Recovery = 83% Analysis Date = 01/11/21 Pct Recovery = 83% Analysis Date = 01/11/21 Pct Recovery = 83% Analysis Date = 01/07/21 Pct Recovery = 84% Analysis Date = 01/07/21 Pct Recovery = 84% Analysis Date = 01/02/21 Pct Recovery = 84% Analysis Date = 01/02/21 Pct Recovery = 84% Analysis Date = 12/29/20 Pct Recovery = 84% Analysis Date = 12/29/20 Pct Recovery = 84% Analysis Date = 12/25/20 Pct Recovery = 84% Analysis Date = 12/25/20 Pct Recovery = 84% Analysis Date = 12/20/20 Pct Recovery = 84% Analysis Date = 12/20/20 Pct Recovery = 84% Analysis Date = 12/16/20 Pct Recovery = 85% Analysis Date = 12/16/20 Pct Recovery = 85% Analysis Date = 12/12/20 Pct Recovery = 85% Analysis Date = 12/12/20 Pct Recovery = 85% Analysis Date = 12/07/20 Pct Recovery = 85% Analysis Date = 12/07/20 Pct Recovery = 85% Analysis Date = 12/03/20 Pct Recovery = 86% Analysis Date = 12/03/20 Pct Recovery = 86% Analysis Date = 11/29/20 Pct Recovery = 86% Analysis Date = 11/29/20 Pct Recovery = 86% Analysis Date = 11/24/20 Pct Recovery = 86% Analysis Date = 11/24/20 Pct Recovery = 86% Analysis Date = 11/20/20 Pct Recovery = 87% Analysis Date = 11/20/20 Pct Recovery = 87% Analysis Date = 11/16/20 Pct Recovery = 87% Analysis Date = 11/16/20 Pct Recovery = 87% Analysis Date = 11/11/20 Pct Recovery = 87% Analysis Date = 11/11/20 Pct Recovery = 87% Analysis Date = 11/07/20 Pct Recovery = 88% Analysis Date = 11/07/20 Pct Recovery = 88% Analysis Date = 11/03/20 Pct Recovery = 88% Analysis Date = 11/03/20 Pct Recovery = 88% Analysis Date = 10/29/20 Pct Recovery = 88% Analysis Date = 10/29/20 Pct Recovery = 88% Analysis Date = 10/25/20 Pct Recovery = 89% Analysis Date = 10/25/20 Pct Recovery = 89% Analysis Date = 10/21/20 Pct Recovery = 89% Analysis Date = 10/21/20 Pct Recovery = 89% Analysis Date = 10/17/20 Pct Recovery = 89% Analysis Date = 10/17/20 Pct Recovery = 89% Analysis Date = 10/12/20 Pct Recovery = 90% Analysis Date = 10/12/20 Pct Recovery = 90% Analysis Date = 10/08/20 Pct Recovery = 90% Analysis Date = 10/08/20 Pct Recovery = 90% Analysis Date = 10/04/20 Pct Recovery = 90% Analysis Date = 10/04/20 Pct Recovery = 90% Analysis Date = 09/29/20 Pct Recovery = 91% Analysis Date = 09/29/20 Pct Recovery = 91% Analysis Date = 09/25/20 Pct Recovery = 91% Analysis Date = 09/25/20 Pct Recovery = 91% Analysis Date = 09/21/20 Pct Recovery = 91% Analysis Date = 09/21/20 Pct Recovery = 91% Analysis Date = 09/16/20 Pct Recovery = 92% Analysis Date = 09/16/20 Pct Recovery = 92% Analysis Date = 09/12/20 Pct Recovery = 92% Analysis Date = 09/12/20 Pct Recovery = 92% Analysis Date = 09/08/20 Pct Recovery = 93% Analysis Date = 09/08/20 Pct Recovery = 93% Analysis Date = 09/03/20 Pct Recovery = 93% Analysis Date = 09/03/20 Pct Recovery = 93% Analysis Date = 08/30/20 Pct Recovery = 93% Analysis Date = 08/30/20 Pct Recovery = 93% Analysis Date = 08/26/20 Pct Recovery = 94% Analysis Date = 08/26/20 Pct Recovery = 94% Analysis Date = 08/21/20 Pct Recovery = 94% Analysis Date = 08/21/20 Pct Recovery = 94% Analysis Date = 08/17/20 Pct Recovery = 94% Analysis Date = 08/17/20 Pct Recovery = 94% Analysis Date = 08/13/20 Pct Recovery = 95% Analysis Date = 08/13/20 Pct Recovery = 95% Analysis Date = 08/08/20 Pct Recovery = 95% Analysis Date = 08/08/20 Pct Recovery = 95% Analysis Date = 08/04/20 Pct Recovery = 95% Analysis Date = 08/04/20 Pct Recovery = 95% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 96% Analysis Date = 07/22/20 Pct Recovery = 96% Analysis Date = 07/22/20 Pct Recovery = 96% Analysis Date = 07/18/20 Pct Recovery = 97% Analysis Date = 07/18/20 Pct Recovery = 97% Analysis Date = 07/14/20 Pct Recovery = 97% Analysis Date = 07/14/20 Pct Recovery = 97% Analysis Date = 07/09/20 Pct Recovery = 97% Analysis Date = 07/09/20 Pct Recovery = 97% Analysis Date = 07/05/20 Pct Recovery = 98% Analysis Date = 07/05/20 Pct Recovery = 98% Analysis Date = 07/01/20 Pct Recovery = 98% Analysis Date = 07/01/20 Pct Recovery = 98% Analysis Date = 06/26/20 Pct Recovery = 98% Analysis Date = 06/26/20 Pct Recovery = 98% Analysis Date = 06/22/20 Pct Recovery = 99% Analysis Date = 06/22/20 Pct Recovery = 99% Analysis Date = 06/18/20 Pct Recovery = 99% Analysis Date = 06/18/20 Pct Recovery = 99% Analysis Date = 06/13/20 Pct Recovery = 99% Analysis Date = 06/13/20 Pct Recovery = 99% Analysis Date = 06/09/20 Pct Recovery = 100% Analysis Date = 06/09/20 Pct Recovery = 100% Analysis Date = 06/05/20 Pct Recovery = 100% Analysis Date = 06/05/20 Pct Recovery = 100% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/31/20 Pct Recovery = 100% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 101% Analysis Date = 05/19/20 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PIPERONYL BUTOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 45 83% 23% 83% 16%
Total 45 83% 23% 83% 16%

Sample Statistics
PIPERONYL BUTOXIDE

Characteristic N % % Basis
Plotted 45 100% Spiked
Estimated Values 2 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 45 .  
False Negatives 0 0% 0 out of 45
Not Spiked 71 .  
False Positives 0 0% 0 out of 71

OBSP Determination:
PROMETON
METHOD: 2447 , TESTIDCODE: 67702LCM60

Laboratory ID = 20202110006 Lab Value = 49.903 Expected Conc. = 50.5 Report level label = 4 Pct Recovery = 99% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 48.365 Expected Conc. = 50.4 Report level label = 4 Pct Recovery = 96% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 44.807 Expected Conc. = 50.1 Report level label = 4 Pct Recovery = 89% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 41.389 Expected Conc. = 50.1 Report level label = 4 Pct Recovery = 83% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 47.312 Expected Conc. = 50.1 Report level label = 4 Pct Recovery = 94% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 33.889 Expected Conc. = 49.95 Report level label = 4 Pct Recovery = 68% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 35.072 Expected Conc. = 49.95 Report level label = 4 Pct Recovery = 70% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 43.061 Expected Conc. = 49.95 Report level label = 4 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 46.629 Expected Conc. = 49.95 Report level label = 4 Pct Recovery = 93% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20222150192 Lab Value = 28.538 Expected Conc. = 40.4 Report level label = 4 Pct Recovery = 71% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 31.699 Expected Conc. = 40 Report level label = 4 Pct Recovery = 79% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221520237 Lab Value = 48.669 Expected Conc. = 40 Report level label = 4 Pct Recovery = 122% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20220740064 Lab Value = 19.702 Expected Conc. = 25.25 Report level label = 4 Pct Recovery = 78% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20201680155 Lab Value = 23.784 Expected Conc. = 25.25 Report level label = 4 Pct Recovery = 94% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 24.054 Expected Conc. = 25.2 Report level label = 4 Pct Recovery = 95% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 22.635 Expected Conc. = 25.2 Report level label = 4 Pct Recovery = 90% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 20.251 Expected Conc. = 25.2 Report level label = 4 Pct Recovery = 80% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202880004 Lab Value = 24.463 Expected Conc. = 25.05 Report level label = 4 Pct Recovery = 98% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221870197 Lab Value = 21.942 Expected Conc. = 25 Report level label = 4 Pct Recovery = 88% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 21.383 Expected Conc. = 24.975 Report level label = 4 Pct Recovery = 86% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 19.347 Expected Conc. = 20.04 Report level label = 4 Pct Recovery = 97% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 14.732 Expected Conc. = 20.04 Report level label = 4 Pct Recovery = 74% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 21.580 Expected Conc. = 19.98 Report level label = 4 Pct Recovery = 108% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 9.656 Expected Conc. = 10.1 Report level label = 4 Pct Recovery = 96% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 11.541 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 114% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 10.066 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 100% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 10.664 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 106% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 10.434 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 104% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210120050 Lab Value = 10.793 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 108% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 10.314 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 103% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.918 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 79% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 9.932 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 99% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 10.985 Expected Conc. = 10.02 Report level label = 4 Pct Recovery = 110% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221660151 Lab Value = 12.173 Expected Conc. = 10 Report level label = 4 Pct Recovery = 122% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210690067 Lab Value = 12.186 Expected Conc. = 9.99 Report level label = 4 Pct Recovery = 122% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 08/15/22 Pct Recovery = 93% Analysis Date = 08/10/22 Pct Recovery = 93% Analysis Date = 08/10/22 Pct Recovery = 93% Analysis Date = 08/06/22 Pct Recovery = 93% Analysis Date = 08/06/22 Pct Recovery = 93% Analysis Date = 08/02/22 Pct Recovery = 93% Analysis Date = 08/02/22 Pct Recovery = 93% Analysis Date = 07/29/22 Pct Recovery = 93% Analysis Date = 07/29/22 Pct Recovery = 93% Analysis Date = 07/25/22 Pct Recovery = 93% Analysis Date = 07/25/22 Pct Recovery = 93% Analysis Date = 07/21/22 Pct Recovery = 93% Analysis Date = 07/21/22 Pct Recovery = 93% Analysis Date = 07/17/22 Pct Recovery = 93% Analysis Date = 07/17/22 Pct Recovery = 93% Analysis Date = 07/13/22 Pct Recovery = 93% Analysis Date = 07/13/22 Pct Recovery = 93% Analysis Date = 07/09/22 Pct Recovery = 93% Analysis Date = 07/09/22 Pct Recovery = 93% Analysis Date = 07/05/22 Pct Recovery = 93% Analysis Date = 07/05/22 Pct Recovery = 93% Analysis Date = 07/01/22 Pct Recovery = 93% Analysis Date = 07/01/22 Pct Recovery = 93% Analysis Date = 06/26/22 Pct Recovery = 93% Analysis Date = 06/26/22 Pct Recovery = 93% Analysis Date = 06/22/22 Pct Recovery = 93% Analysis Date = 06/22/22 Pct Recovery = 93% Analysis Date = 06/18/22 Pct Recovery = 93% Analysis Date = 06/18/22 Pct Recovery = 93% Analysis Date = 06/14/22 Pct Recovery = 93% Analysis Date = 06/14/22 Pct Recovery = 93% Analysis Date = 06/10/22 Pct Recovery = 93% Analysis Date = 06/10/22 Pct Recovery = 93% Analysis Date = 06/06/22 Pct Recovery = 93% Analysis Date = 06/06/22 Pct Recovery = 93% Analysis Date = 06/02/22 Pct Recovery = 93% Analysis Date = 06/02/22 Pct Recovery = 93% Analysis Date = 05/29/22 Pct Recovery = 93% Analysis Date = 05/29/22 Pct Recovery = 93% Analysis Date = 05/25/22 Pct Recovery = 93% Analysis Date = 05/25/22 Pct Recovery = 93% Analysis Date = 05/21/22 Pct Recovery = 93% Analysis Date = 05/21/22 Pct Recovery = 93% Analysis Date = 05/17/22 Pct Recovery = 93% Analysis Date = 05/17/22 Pct Recovery = 93% Analysis Date = 05/12/22 Pct Recovery = 93% Analysis Date = 05/12/22 Pct Recovery = 93% Analysis Date = 05/08/22 Pct Recovery = 93% Analysis Date = 05/08/22 Pct Recovery = 93% Analysis Date = 05/04/22 Pct Recovery = 93% Analysis Date = 05/04/22 Pct Recovery = 93% Analysis Date = 04/30/22 Pct Recovery = 93% Analysis Date = 04/30/22 Pct Recovery = 93% Analysis Date = 04/26/22 Pct Recovery = 93% Analysis Date = 04/26/22 Pct Recovery = 93% Analysis Date = 04/22/22 Pct Recovery = 93% Analysis Date = 04/22/22 Pct Recovery = 93% Analysis Date = 04/18/22 Pct Recovery = 93% Analysis Date = 04/18/22 Pct Recovery = 93% Analysis Date = 04/14/22 Pct Recovery = 93% Analysis Date = 04/14/22 Pct Recovery = 93% Analysis Date = 04/10/22 Pct Recovery = 93% Analysis Date = 04/10/22 Pct Recovery = 93% Analysis Date = 04/06/22 Pct Recovery = 93% Analysis Date = 04/06/22 Pct Recovery = 93% Analysis Date = 04/02/22 Pct Recovery = 93% Analysis Date = 04/02/22 Pct Recovery = 93% Analysis Date = 03/28/22 Pct Recovery = 93% Analysis Date = 03/28/22 Pct Recovery = 93% Analysis Date = 03/24/22 Pct Recovery = 93% Analysis Date = 03/24/22 Pct Recovery = 93% Analysis Date = 03/20/22 Pct Recovery = 93% Analysis Date = 03/20/22 Pct Recovery = 93% Analysis Date = 03/16/22 Pct Recovery = 93% Analysis Date = 03/16/22 Pct Recovery = 93% Analysis Date = 03/12/22 Pct Recovery = 93% Analysis Date = 03/12/22 Pct Recovery = 93% Analysis Date = 03/08/22 Pct Recovery = 93% Analysis Date = 03/08/22 Pct Recovery = 93% Analysis Date = 03/04/22 Pct Recovery = 93% Analysis Date = 03/04/22 Pct Recovery = 93% Analysis Date = 02/28/22 Pct Recovery = 93% Analysis Date = 02/28/22 Pct Recovery = 93% Analysis Date = 02/24/22 Pct Recovery = 93% Analysis Date = 02/24/22 Pct Recovery = 93% Analysis Date = 02/20/22 Pct Recovery = 93% Analysis Date = 02/20/22 Pct Recovery = 93% Analysis Date = 02/16/22 Pct Recovery = 93% Analysis Date = 02/16/22 Pct Recovery = 93% Analysis Date = 02/11/22 Pct Recovery = 93% Analysis Date = 02/11/22 Pct Recovery = 93% Analysis Date = 02/07/22 Pct Recovery = 93% Analysis Date = 02/07/22 Pct Recovery = 93% Analysis Date = 02/03/22 Pct Recovery = 93% Analysis Date = 02/03/22 Pct Recovery = 93% Analysis Date = 01/30/22 Pct Recovery = 93% Analysis Date = 01/30/22 Pct Recovery = 93% Analysis Date = 01/26/22 Pct Recovery = 93% Analysis Date = 01/26/22 Pct Recovery = 93% Analysis Date = 01/22/22 Pct Recovery = 93% Analysis Date = 01/22/22 Pct Recovery = 93% Analysis Date = 01/18/22 Pct Recovery = 93% Analysis Date = 01/18/22 Pct Recovery = 93% Analysis Date = 01/14/22 Pct Recovery = 93% Analysis Date = 01/14/22 Pct Recovery = 93% Analysis Date = 01/10/22 Pct Recovery = 93% Analysis Date = 01/10/22 Pct Recovery = 93% Analysis Date = 01/06/22 Pct Recovery = 93% Analysis Date = 01/06/22 Pct Recovery = 93% Analysis Date = 01/02/22 Pct Recovery = 93% Analysis Date = 01/02/22 Pct Recovery = 93% Analysis Date = 12/28/21 Pct Recovery = 93% Analysis Date = 12/28/21 Pct Recovery = 93% Analysis Date = 12/24/21 Pct Recovery = 93% Analysis Date = 12/24/21 Pct Recovery = 93% Analysis Date = 12/20/21 Pct Recovery = 93% Analysis Date = 12/20/21 Pct Recovery = 93% Analysis Date = 12/16/21 Pct Recovery = 93% Analysis Date = 12/16/21 Pct Recovery = 93% Analysis Date = 12/12/21 Pct Recovery = 93% Analysis Date = 12/12/21 Pct Recovery = 93% Analysis Date = 12/08/21 Pct Recovery = 93% Analysis Date = 12/08/21 Pct Recovery = 93% Analysis Date = 12/04/21 Pct Recovery = 93% Analysis Date = 12/04/21 Pct Recovery = 93% Analysis Date = 11/30/21 Pct Recovery = 93% Analysis Date = 11/30/21 Pct Recovery = 93% Analysis Date = 11/26/21 Pct Recovery = 93% Analysis Date = 11/26/21 Pct Recovery = 93% Analysis Date = 11/22/21 Pct Recovery = 93% Analysis Date = 11/22/21 Pct Recovery = 93% Analysis Date = 11/18/21 Pct Recovery = 93% Analysis Date = 11/18/21 Pct Recovery = 93% Analysis Date = 11/13/21 Pct Recovery = 93% Analysis Date = 11/13/21 Pct Recovery = 93% Analysis Date = 11/09/21 Pct Recovery = 93% Analysis Date = 11/09/21 Pct Recovery = 93% Analysis Date = 11/05/21 Pct Recovery = 93% Analysis Date = 11/05/21 Pct Recovery = 93% Analysis Date = 11/01/21 Pct Recovery = 93% Analysis Date = 11/01/21 Pct Recovery = 93% Analysis Date = 10/28/21 Pct Recovery = 93% Analysis Date = 10/28/21 Pct Recovery = 93% Analysis Date = 10/24/21 Pct Recovery = 93% Analysis Date = 10/24/21 Pct Recovery = 93% Analysis Date = 10/20/21 Pct Recovery = 93% Analysis Date = 10/20/21 Pct Recovery = 93% Analysis Date = 10/16/21 Pct Recovery = 93% Analysis Date = 10/16/21 Pct Recovery = 93% Analysis Date = 10/12/21 Pct Recovery = 93% Analysis Date = 10/12/21 Pct Recovery = 93% Analysis Date = 10/08/21 Pct Recovery = 93% Analysis Date = 10/08/21 Pct Recovery = 93% Analysis Date = 10/04/21 Pct Recovery = 93% Analysis Date = 10/04/21 Pct Recovery = 93% Analysis Date = 09/29/21 Pct Recovery = 93% Analysis Date = 09/29/21 Pct Recovery = 93% Analysis Date = 09/25/21 Pct Recovery = 93% Analysis Date = 09/25/21 Pct Recovery = 93% Analysis Date = 09/21/21 Pct Recovery = 93% Analysis Date = 09/21/21 Pct Recovery = 93% Analysis Date = 09/17/21 Pct Recovery = 93% Analysis Date = 09/17/21 Pct Recovery = 93% Analysis Date = 09/13/21 Pct Recovery = 93% Analysis Date = 09/13/21 Pct Recovery = 93% Analysis Date = 09/09/21 Pct Recovery = 93% Analysis Date = 09/09/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/05/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 09/01/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 93% Analysis Date = 08/28/21 Pct Recovery = 93% Analysis Date = 08/24/21 Pct Recovery = 93% Analysis Date = 08/24/21 Pct Recovery = 93% Analysis Date = 08/20/21 Pct Recovery = 93% Analysis Date = 08/20/21 Pct Recovery = 93% Analysis Date = 08/15/21 Pct Recovery = 93% Analysis Date = 08/15/21 Pct Recovery = 93% Analysis Date = 08/11/21 Pct Recovery = 93% Analysis Date = 08/11/21 Pct Recovery = 93% Analysis Date = 08/07/21 Pct Recovery = 93% Analysis Date = 08/07/21 Pct Recovery = 93% Analysis Date = 08/03/21 Pct Recovery = 93% Analysis Date = 08/03/21 Pct Recovery = 93% Analysis Date = 07/30/21 Pct Recovery = 93% Analysis Date = 07/30/21 Pct Recovery = 93% Analysis Date = 07/26/21 Pct Recovery = 93% Analysis Date = 07/26/21 Pct Recovery = 93% Analysis Date = 07/22/21 Pct Recovery = 93% Analysis Date = 07/22/21 Pct Recovery = 93% Analysis Date = 07/18/21 Pct Recovery = 93% Analysis Date = 07/18/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/10/21 Pct Recovery = 93% Analysis Date = 07/10/21 Pct Recovery = 93% Analysis Date = 07/06/21 Pct Recovery = 93% Analysis Date = 07/06/21 Pct Recovery = 93% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 06/27/21 Pct Recovery = 93% Analysis Date = 06/27/21 Pct Recovery = 93% Analysis Date = 06/23/21 Pct Recovery = 93% Analysis Date = 06/23/21 Pct Recovery = 93% Analysis Date = 06/19/21 Pct Recovery = 93% Analysis Date = 06/19/21 Pct Recovery = 93% Analysis Date = 06/15/21 Pct Recovery = 93% Analysis Date = 06/15/21 Pct Recovery = 93% Analysis Date = 06/11/21 Pct Recovery = 93% Analysis Date = 06/11/21 Pct Recovery = 93% Analysis Date = 06/07/21 Pct Recovery = 93% Analysis Date = 06/07/21 Pct Recovery = 93% Analysis Date = 06/03/21 Pct Recovery = 93% Analysis Date = 06/03/21 Pct Recovery = 93% Analysis Date = 05/30/21 Pct Recovery = 93% Analysis Date = 05/30/21 Pct Recovery = 93% Analysis Date = 05/26/21 Pct Recovery = 93% Analysis Date = 05/26/21 Pct Recovery = 93% Analysis Date = 05/22/21 Pct Recovery = 93% Analysis Date = 05/22/21 Pct Recovery = 93% Analysis Date = 05/18/21 Pct Recovery = 93% Analysis Date = 05/18/21 Pct Recovery = 93% Analysis Date = 05/13/21 Pct Recovery = 93% Analysis Date = 05/13/21 Pct Recovery = 93% Analysis Date = 05/09/21 Pct Recovery = 93% Analysis Date = 05/09/21 Pct Recovery = 93% Analysis Date = 05/05/21 Pct Recovery = 93% Analysis Date = 05/05/21 Pct Recovery = 93% Analysis Date = 05/01/21 Pct Recovery = 93% Analysis Date = 05/01/21 Pct Recovery = 93% Analysis Date = 04/27/21 Pct Recovery = 93% Analysis Date = 04/27/21 Pct Recovery = 93% Analysis Date = 04/23/21 Pct Recovery = 93% Analysis Date = 04/23/21 Pct Recovery = 93% Analysis Date = 04/19/21 Pct Recovery = 93% Analysis Date = 04/19/21 Pct Recovery = 93% Analysis Date = 04/15/21 Pct Recovery = 93% Analysis Date = 04/15/21 Pct Recovery = 93% Analysis Date = 04/11/21 Pct Recovery = 93% Analysis Date = 04/11/21 Pct Recovery = 93% Analysis Date = 04/07/21 Pct Recovery = 93% Analysis Date = 04/07/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 04/03/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/29/21 Pct Recovery = 93% Analysis Date = 03/25/21 Pct Recovery = 93% Analysis Date = 03/25/21 Pct Recovery = 93% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/21/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/17/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/13/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 93% Analysis Date = 03/09/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/05/21 Pct Recovery = 93% Analysis Date = 03/01/21 Pct Recovery = 93% Analysis Date = 03/01/21 Pct Recovery = 93% Analysis Date = 02/25/21 Pct Recovery = 92% Analysis Date = 02/25/21 Pct Recovery = 92% Analysis Date = 02/21/21 Pct Recovery = 92% Analysis Date = 02/21/21 Pct Recovery = 92% Analysis Date = 02/17/21 Pct Recovery = 92% Analysis Date = 02/17/21 Pct Recovery = 92% Analysis Date = 02/12/21 Pct Recovery = 92% Analysis Date = 02/12/21 Pct Recovery = 92% Analysis Date = 02/08/21 Pct Recovery = 92% Analysis Date = 02/08/21 Pct Recovery = 92% Analysis Date = 02/04/21 Pct Recovery = 92% Analysis Date = 02/04/21 Pct Recovery = 92% Analysis Date = 01/31/21 Pct Recovery = 92% Analysis Date = 01/31/21 Pct Recovery = 92% Analysis Date = 01/27/21 Pct Recovery = 92% Analysis Date = 01/27/21 Pct Recovery = 92% Analysis Date = 01/23/21 Pct Recovery = 92% Analysis Date = 01/23/21 Pct Recovery = 92% Analysis Date = 01/19/21 Pct Recovery = 92% Analysis Date = 01/19/21 Pct Recovery = 92% Analysis Date = 01/15/21 Pct Recovery = 92% Analysis Date = 01/15/21 Pct Recovery = 92% Analysis Date = 01/11/21 Pct Recovery = 92% Analysis Date = 01/11/21 Pct Recovery = 92% Analysis Date = 01/07/21 Pct Recovery = 92% Analysis Date = 01/07/21 Pct Recovery = 92% Analysis Date = 01/03/21 Pct Recovery = 92% Analysis Date = 01/03/21 Pct Recovery = 92% Analysis Date = 12/29/20 Pct Recovery = 92% Analysis Date = 12/29/20 Pct Recovery = 92% Analysis Date = 12/25/20 Pct Recovery = 92% Analysis Date = 12/25/20 Pct Recovery = 92% Analysis Date = 12/21/20 Pct Recovery = 92% Analysis Date = 12/21/20 Pct Recovery = 92% Analysis Date = 12/17/20 Pct Recovery = 92% Analysis Date = 12/17/20 Pct Recovery = 92% Analysis Date = 12/13/20 Pct Recovery = 92% Analysis Date = 12/13/20 Pct Recovery = 92% Analysis Date = 12/09/20 Pct Recovery = 92% Analysis Date = 12/09/20 Pct Recovery = 92% Analysis Date = 12/05/20 Pct Recovery = 92% Analysis Date = 12/05/20 Pct Recovery = 92% Analysis Date = 12/01/20 Pct Recovery = 93% Analysis Date = 12/01/20 Pct Recovery = 93% Analysis Date = 11/27/20 Pct Recovery = 93% Analysis Date = 11/27/20 Pct Recovery = 93% Analysis Date = 11/23/20 Pct Recovery = 93% Analysis Date = 11/23/20 Pct Recovery = 93% Analysis Date = 11/19/20 Pct Recovery = 93% Analysis Date = 11/19/20 Pct Recovery = 93% Analysis Date = 11/14/20 Pct Recovery = 94% Analysis Date = 11/14/20 Pct Recovery = 94% Analysis Date = 11/10/20 Pct Recovery = 94% Analysis Date = 11/10/20 Pct Recovery = 94% Analysis Date = 11/06/20 Pct Recovery = 94% Analysis Date = 11/06/20 Pct Recovery = 94% Analysis Date = 11/02/20 Pct Recovery = 95% Analysis Date = 11/02/20 Pct Recovery = 95% Analysis Date = 10/29/20 Pct Recovery = 95% Analysis Date = 10/29/20 Pct Recovery = 95% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 95% Analysis Date = 10/17/20 Pct Recovery = 96% Analysis Date = 10/17/20 Pct Recovery = 96% Analysis Date = 10/13/20 Pct Recovery = 96% Analysis Date = 10/13/20 Pct Recovery = 96% Analysis Date = 10/09/20 Pct Recovery = 96% Analysis Date = 10/09/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 09/30/20 Pct Recovery = 97% Analysis Date = 09/30/20 Pct Recovery = 97% Analysis Date = 09/26/20 Pct Recovery = 97% Analysis Date = 09/26/20 Pct Recovery = 97% Analysis Date = 09/22/20 Pct Recovery = 97% Analysis Date = 09/22/20 Pct Recovery = 97% Analysis Date = 09/18/20 Pct Recovery = 97% Analysis Date = 09/18/20 Pct Recovery = 97% Analysis Date = 09/14/20 Pct Recovery = 97% Analysis Date = 09/14/20 Pct Recovery = 97% Analysis Date = 09/10/20 Pct Recovery = 97% Analysis Date = 09/10/20 Pct Recovery = 97% Analysis Date = 09/06/20 Pct Recovery = 97% Analysis Date = 09/06/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 97% Analysis Date = 08/29/20 Pct Recovery = 97% Analysis Date = 08/29/20 Pct Recovery = 97% Analysis Date = 08/25/20 Pct Recovery = 97% Analysis Date = 08/25/20 Pct Recovery = 97% Analysis Date = 08/21/20 Pct Recovery = 97% Analysis Date = 08/21/20 Pct Recovery = 97% Analysis Date = 08/16/20 Pct Recovery = 97% Analysis Date = 08/16/20 Pct Recovery = 97% Analysis Date = 08/12/20 Pct Recovery = 97% Analysis Date = 08/12/20 Pct Recovery = 97% Analysis Date = 08/08/20 Pct Recovery = 97% Analysis Date = 08/08/20 Pct Recovery = 97% Analysis Date = 08/04/20 Pct Recovery = 97% Analysis Date = 08/04/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 97% Analysis Date = 07/19/20 Pct Recovery = 97% Analysis Date = 07/19/20 Pct Recovery = 97% Analysis Date = 07/15/20 Pct Recovery = 97% Analysis Date = 07/15/20 Pct Recovery = 97% Analysis Date = 07/11/20 Pct Recovery = 96% Analysis Date = 07/11/20 Pct Recovery = 96% Analysis Date = 07/07/20 Pct Recovery = 96% Analysis Date = 07/07/20 Pct Recovery = 96% Analysis Date = 07/02/20 Pct Recovery = 96% Analysis Date = 07/02/20 Pct Recovery = 96% Analysis Date = 06/28/20 Pct Recovery = 96% Analysis Date = 06/28/20 Pct Recovery = 96% Analysis Date = 06/24/20 Pct Recovery = 96% Analysis Date = 06/24/20 Pct Recovery = 96% Analysis Date = 06/20/20 Pct Recovery = 96% Analysis Date = 06/20/20 Pct Recovery = 96% Analysis Date = 06/16/20 Pct Recovery = 96% Analysis Date = 06/16/20 Pct Recovery = 96% Analysis Date = 06/12/20 Pct Recovery = 96% Analysis Date = 06/12/20 Pct Recovery = 96% Analysis Date = 06/08/20 Pct Recovery = 96% Analysis Date = 06/08/20 Pct Recovery = 96% Analysis Date = 06/04/20 Pct Recovery = 96% Analysis Date = 06/04/20 Pct Recovery = 96% Analysis Date = 05/31/20 Pct Recovery = 96% Analysis Date = 05/31/20 Pct Recovery = 96% Analysis Date = 05/27/20 Pct Recovery = 96% Analysis Date = 05/27/20 Pct Recovery = 96% Analysis Date = 05/23/20 Pct Recovery = 95% Analysis Date = 05/23/20 Pct Recovery = 95% Analysis Date = 05/19/20 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 94% 15% 95% 15%
Total 35 94% 15% 95% 15%

Sample Statistics
PROMETON

Characteristic N % % Basis
Plotted 35 100% Spiked
Estimated Values 1 3% Spiked
Deleted Values 1 1% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 80

OBSP Determination:
PROPAZINE
METHOD: 2447 , TESTIDCODE: 68678LCM60

Laboratory ID = 20210760015 Lab Value = 37.583 Expected Conc. = 40.35 Report level label = 3.2 Pct Recovery = 93% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 43.133 Expected Conc. = 40.35 Report level label = 3.2 Pct Recovery = 107% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 40.211 Expected Conc. = 40.35 Report level label = 3.2 Pct Recovery = 100% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 41.377 Expected Conc. = 40.35 Report level label = 3.2 Pct Recovery = 103% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 43.057 Expected Conc. = 40.1 Report level label = 3.2 Pct Recovery = 107% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 36.011 Expected Conc. = 40.1 Report level label = 3.2 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 41.295 Expected Conc. = 40.1 Report level label = 3.2 Pct Recovery = 103% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221520237 Lab Value = 33.314 Expected Conc. = 32.544 Report level label = 3.2 Pct Recovery = 102% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 22.295 Expected Conc. = 32 Report level label = 3.2 Pct Recovery = 70% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 26.207 Expected Conc. = 31.6 Report level label = 3.2 Pct Recovery = 83% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221870197 Lab Value = 16.472 Expected Conc. = 20.34 Report level label = 3.2 Pct Recovery = 81% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 16.939 Expected Conc. = 20.175 Report level label = 3.2 Pct Recovery = 84% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202880004 Lab Value = 21.027 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 105% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202390020 Lab Value = 28.055 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 140% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 21.776 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 109% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20201550031 Lab Value = 23.294 Expected Conc. = 20 Report level label = 3.2 Pct Recovery = 116% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20220740064 Lab Value = 14.550 Expected Conc. = 19.75 Report level label = 3.2 Pct Recovery = 74% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20210900005 Lab Value = 14.979 Expected Conc. = 16.14 Report level label = 3.2 Pct Recovery = 93% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 13.134 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 82% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 17.033 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 106% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 19.203 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 120% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 16.182 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 101% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20221660151 Lab Value = 6.444 Expected Conc. = 8.136 Report level label = 3.2 Pct Recovery = 79% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210120050 Lab Value = 7.882 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 98% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 7.967 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 99% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.861 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 98% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 8.359 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 104% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 12.667 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 158% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202330309 Lab Value = 6.472 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 81% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 6.222 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 78% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 11.128 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 139% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 8.236 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 103% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 10.013 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 125% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Analysis Date = 08/15/22 Pct Recovery = 80% Analysis Date = 08/10/22 Pct Recovery = 80% Analysis Date = 08/10/22 Pct Recovery = 80% Analysis Date = 08/06/22 Pct Recovery = 81% Analysis Date = 08/06/22 Pct Recovery = 81% Analysis Date = 08/02/22 Pct Recovery = 81% Analysis Date = 08/02/22 Pct Recovery = 81% Analysis Date = 07/29/22 Pct Recovery = 81% Analysis Date = 07/29/22 Pct Recovery = 81% Analysis Date = 07/25/22 Pct Recovery = 81% Analysis Date = 07/25/22 Pct Recovery = 81% Analysis Date = 07/21/22 Pct Recovery = 81% Analysis Date = 07/21/22 Pct Recovery = 81% Analysis Date = 07/17/22 Pct Recovery = 81% Analysis Date = 07/17/22 Pct Recovery = 81% Analysis Date = 07/13/22 Pct Recovery = 81% Analysis Date = 07/13/22 Pct Recovery = 81% Analysis Date = 07/09/22 Pct Recovery = 81% Analysis Date = 07/09/22 Pct Recovery = 81% Analysis Date = 07/05/22 Pct Recovery = 81% Analysis Date = 07/05/22 Pct Recovery = 81% Analysis Date = 07/01/22 Pct Recovery = 81% Analysis Date = 07/01/22 Pct Recovery = 81% Analysis Date = 06/27/22 Pct Recovery = 81% Analysis Date = 06/27/22 Pct Recovery = 81% Analysis Date = 06/23/22 Pct Recovery = 82% Analysis Date = 06/23/22 Pct Recovery = 82% Analysis Date = 06/19/22 Pct Recovery = 82% Analysis Date = 06/19/22 Pct Recovery = 82% Analysis Date = 06/15/22 Pct Recovery = 82% Analysis Date = 06/15/22 Pct Recovery = 82% Analysis Date = 06/11/22 Pct Recovery = 82% Analysis Date = 06/11/22 Pct Recovery = 82% Analysis Date = 06/07/22 Pct Recovery = 82% Analysis Date = 06/07/22 Pct Recovery = 82% Analysis Date = 06/03/22 Pct Recovery = 82% Analysis Date = 06/03/22 Pct Recovery = 82% Analysis Date = 05/30/22 Pct Recovery = 82% Analysis Date = 05/30/22 Pct Recovery = 82% Analysis Date = 05/26/22 Pct Recovery = 82% Analysis Date = 05/26/22 Pct Recovery = 82% Analysis Date = 05/22/22 Pct Recovery = 82% Analysis Date = 05/22/22 Pct Recovery = 82% Analysis Date = 05/18/22 Pct Recovery = 82% Analysis Date = 05/18/22 Pct Recovery = 82% Analysis Date = 05/14/22 Pct Recovery = 82% Analysis Date = 05/14/22 Pct Recovery = 82% Analysis Date = 05/10/22 Pct Recovery = 82% Analysis Date = 05/10/22 Pct Recovery = 82% Analysis Date = 05/06/22 Pct Recovery = 82% Analysis Date = 05/06/22 Pct Recovery = 82% Analysis Date = 05/01/22 Pct Recovery = 82% Analysis Date = 05/01/22 Pct Recovery = 82% Analysis Date = 04/27/22 Pct Recovery = 83% Analysis Date = 04/27/22 Pct Recovery = 83% Analysis Date = 04/23/22 Pct Recovery = 83% Analysis Date = 04/23/22 Pct Recovery = 83% Analysis Date = 04/19/22 Pct Recovery = 83% Analysis Date = 04/19/22 Pct Recovery = 83% Analysis Date = 04/15/22 Pct Recovery = 83% Analysis Date = 04/15/22 Pct Recovery = 83% Analysis Date = 04/11/22 Pct Recovery = 83% Analysis Date = 04/11/22 Pct Recovery = 83% Analysis Date = 04/07/22 Pct Recovery = 83% Analysis Date = 04/07/22 Pct Recovery = 83% Analysis Date = 04/03/22 Pct Recovery = 83% Analysis Date = 04/03/22 Pct Recovery = 83% Analysis Date = 03/30/22 Pct Recovery = 83% Analysis Date = 03/30/22 Pct Recovery = 83% Analysis Date = 03/26/22 Pct Recovery = 83% Analysis Date = 03/26/22 Pct Recovery = 83% Analysis Date = 03/22/22 Pct Recovery = 83% Analysis Date = 03/22/22 Pct Recovery = 83% Analysis Date = 03/18/22 Pct Recovery = 83% Analysis Date = 03/18/22 Pct Recovery = 83% Analysis Date = 03/14/22 Pct Recovery = 83% Analysis Date = 03/14/22 Pct Recovery = 83% Analysis Date = 03/10/22 Pct Recovery = 83% Analysis Date = 03/10/22 Pct Recovery = 83% Analysis Date = 03/06/22 Pct Recovery = 83% Analysis Date = 03/06/22 Pct Recovery = 83% Analysis Date = 03/02/22 Pct Recovery = 83% Analysis Date = 03/02/22 Pct Recovery = 83% Analysis Date = 02/26/22 Pct Recovery = 83% Analysis Date = 02/26/22 Pct Recovery = 83% Analysis Date = 02/22/22 Pct Recovery = 84% Analysis Date = 02/22/22 Pct Recovery = 84% Analysis Date = 02/18/22 Pct Recovery = 84% Analysis Date = 02/18/22 Pct Recovery = 84% Analysis Date = 02/14/22 Pct Recovery = 84% Analysis Date = 02/14/22 Pct Recovery = 84% Analysis Date = 02/10/22 Pct Recovery = 84% Analysis Date = 02/10/22 Pct Recovery = 84% Analysis Date = 02/06/22 Pct Recovery = 84% Analysis Date = 02/06/22 Pct Recovery = 84% Analysis Date = 02/02/22 Pct Recovery = 84% Analysis Date = 02/02/22 Pct Recovery = 84% Analysis Date = 01/29/22 Pct Recovery = 84% Analysis Date = 01/29/22 Pct Recovery = 84% Analysis Date = 01/25/22 Pct Recovery = 84% Analysis Date = 01/25/22 Pct Recovery = 84% Analysis Date = 01/20/22 Pct Recovery = 84% Analysis Date = 01/20/22 Pct Recovery = 84% Analysis Date = 01/16/22 Pct Recovery = 84% Analysis Date = 01/16/22 Pct Recovery = 84% Analysis Date = 01/12/22 Pct Recovery = 84% Analysis Date = 01/12/22 Pct Recovery = 84% Analysis Date = 01/08/22 Pct Recovery = 84% Analysis Date = 01/08/22 Pct Recovery = 84% Analysis Date = 01/04/22 Pct Recovery = 84% Analysis Date = 01/04/22 Pct Recovery = 84% Analysis Date = 12/31/21 Pct Recovery = 84% Analysis Date = 12/31/21 Pct Recovery = 84% Analysis Date = 12/27/21 Pct Recovery = 84% Analysis Date = 12/27/21 Pct Recovery = 84% Analysis Date = 12/23/21 Pct Recovery = 84% Analysis Date = 12/23/21 Pct Recovery = 84% Analysis Date = 12/19/21 Pct Recovery = 84% Analysis Date = 12/19/21 Pct Recovery = 84% Analysis Date = 12/15/21 Pct Recovery = 85% Analysis Date = 12/15/21 Pct Recovery = 85% Analysis Date = 12/11/21 Pct Recovery = 85% Analysis Date = 12/11/21 Pct Recovery = 85% Analysis Date = 12/07/21 Pct Recovery = 85% Analysis Date = 12/07/21 Pct Recovery = 85% Analysis Date = 12/03/21 Pct Recovery = 85% Analysis Date = 12/03/21 Pct Recovery = 85% Analysis Date = 11/29/21 Pct Recovery = 85% Analysis Date = 11/29/21 Pct Recovery = 85% Analysis Date = 11/25/21 Pct Recovery = 85% Analysis Date = 11/25/21 Pct Recovery = 85% Analysis Date = 11/21/21 Pct Recovery = 85% Analysis Date = 11/21/21 Pct Recovery = 85% Analysis Date = 11/17/21 Pct Recovery = 85% Analysis Date = 11/17/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 85% Analysis Date = 11/09/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/05/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 85% Analysis Date = 10/11/21 Pct Recovery = 86% Analysis Date = 10/11/21 Pct Recovery = 86% Analysis Date = 10/07/21 Pct Recovery = 86% Analysis Date = 10/07/21 Pct Recovery = 86% Analysis Date = 10/03/21 Pct Recovery = 86% Analysis Date = 10/03/21 Pct Recovery = 86% Analysis Date = 09/29/21 Pct Recovery = 86% Analysis Date = 09/29/21 Pct Recovery = 86% Analysis Date = 09/25/21 Pct Recovery = 86% Analysis Date = 09/25/21 Pct Recovery = 86% Analysis Date = 09/21/21 Pct Recovery = 86% Analysis Date = 09/21/21 Pct Recovery = 86% Analysis Date = 09/17/21 Pct Recovery = 86% Analysis Date = 09/17/21 Pct Recovery = 86% Analysis Date = 09/13/21 Pct Recovery = 86% Analysis Date = 09/13/21 Pct Recovery = 86% Analysis Date = 09/09/21 Pct Recovery = 86% Analysis Date = 09/09/21 Pct Recovery = 86% Analysis Date = 09/05/21 Pct Recovery = 86% Analysis Date = 09/05/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/16/21 Pct Recovery = 86% Analysis Date = 08/16/21 Pct Recovery = 86% Analysis Date = 08/12/21 Pct Recovery = 86% Analysis Date = 08/12/21 Pct Recovery = 86% Analysis Date = 08/08/21 Pct Recovery = 86% Analysis Date = 08/08/21 Pct Recovery = 86% Analysis Date = 08/04/21 Pct Recovery = 87% Analysis Date = 08/04/21 Pct Recovery = 87% Analysis Date = 07/31/21 Pct Recovery = 87% Analysis Date = 07/31/21 Pct Recovery = 87% Analysis Date = 07/27/21 Pct Recovery = 87% Analysis Date = 07/27/21 Pct Recovery = 87% Analysis Date = 07/23/21 Pct Recovery = 87% Analysis Date = 07/23/21 Pct Recovery = 87% Analysis Date = 07/19/21 Pct Recovery = 87% Analysis Date = 07/19/21 Pct Recovery = 87% Analysis Date = 07/15/21 Pct Recovery = 87% Analysis Date = 07/15/21 Pct Recovery = 87% Analysis Date = 07/11/21 Pct Recovery = 87% Analysis Date = 07/11/21 Pct Recovery = 87% Analysis Date = 07/07/21 Pct Recovery = 87% Analysis Date = 07/07/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/28/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/24/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/20/21 Pct Recovery = 87% Analysis Date = 06/16/21 Pct Recovery = 87% Analysis Date = 06/16/21 Pct Recovery = 87% Analysis Date = 06/12/21 Pct Recovery = 87% Analysis Date = 06/12/21 Pct Recovery = 87% Analysis Date = 06/08/21 Pct Recovery = 87% Analysis Date = 06/08/21 Pct Recovery = 87% Analysis Date = 06/04/21 Pct Recovery = 87% Analysis Date = 06/04/21 Pct Recovery = 87% Analysis Date = 05/31/21 Pct Recovery = 88% Analysis Date = 05/31/21 Pct Recovery = 88% Analysis Date = 05/27/21 Pct Recovery = 88% Analysis Date = 05/27/21 Pct Recovery = 88% Analysis Date = 05/23/21 Pct Recovery = 88% Analysis Date = 05/23/21 Pct Recovery = 88% Analysis Date = 05/19/21 Pct Recovery = 88% Analysis Date = 05/19/21 Pct Recovery = 88% Analysis Date = 05/15/21 Pct Recovery = 88% Analysis Date = 05/15/21 Pct Recovery = 88% Analysis Date = 05/11/21 Pct Recovery = 88% Analysis Date = 05/11/21 Pct Recovery = 88% Analysis Date = 05/07/21 Pct Recovery = 88% Analysis Date = 05/07/21 Pct Recovery = 88% Analysis Date = 05/03/21 Pct Recovery = 88% Analysis Date = 05/03/21 Pct Recovery = 88% Analysis Date = 04/29/21 Pct Recovery = 88% Analysis Date = 04/29/21 Pct Recovery = 88% Analysis Date = 04/25/21 Pct Recovery = 88% Analysis Date = 04/25/21 Pct Recovery = 88% Analysis Date = 04/21/21 Pct Recovery = 88% Analysis Date = 04/21/21 Pct Recovery = 88% Analysis Date = 04/17/21 Pct Recovery = 88% Analysis Date = 04/17/21 Pct Recovery = 88% Analysis Date = 04/13/21 Pct Recovery = 88% Analysis Date = 04/13/21 Pct Recovery = 88% Analysis Date = 04/09/21 Pct Recovery = 88% Analysis Date = 04/09/21 Pct Recovery = 88% Analysis Date = 04/05/21 Pct Recovery = 89% Analysis Date = 04/05/21 Pct Recovery = 89% Analysis Date = 04/01/21 Pct Recovery = 89% Analysis Date = 04/01/21 Pct Recovery = 89% Analysis Date = 03/28/21 Pct Recovery = 90% Analysis Date = 03/28/21 Pct Recovery = 90% Analysis Date = 03/23/21 Pct Recovery = 91% Analysis Date = 03/23/21 Pct Recovery = 91% Analysis Date = 03/19/21 Pct Recovery = 91% Analysis Date = 03/19/21 Pct Recovery = 91% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/15/21 Pct Recovery = 92% Analysis Date = 03/11/21 Pct Recovery = 92% Analysis Date = 03/11/21 Pct Recovery = 92% Analysis Date = 03/07/21 Pct Recovery = 93% Analysis Date = 03/07/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 93% Analysis Date = 02/27/21 Pct Recovery = 94% Analysis Date = 02/27/21 Pct Recovery = 94% Analysis Date = 02/23/21 Pct Recovery = 95% Analysis Date = 02/23/21 Pct Recovery = 95% Analysis Date = 02/19/21 Pct Recovery = 95% Analysis Date = 02/19/21 Pct Recovery = 95% Analysis Date = 02/15/21 Pct Recovery = 96% Analysis Date = 02/15/21 Pct Recovery = 96% Analysis Date = 02/11/21 Pct Recovery = 96% Analysis Date = 02/11/21 Pct Recovery = 96% Analysis Date = 02/07/21 Pct Recovery = 97% Analysis Date = 02/07/21 Pct Recovery = 97% Analysis Date = 02/03/21 Pct Recovery = 97% Analysis Date = 02/03/21 Pct Recovery = 97% Analysis Date = 01/30/21 Pct Recovery = 98% Analysis Date = 01/30/21 Pct Recovery = 98% Analysis Date = 01/26/21 Pct Recovery = 99% Analysis Date = 01/26/21 Pct Recovery = 99% Analysis Date = 01/22/21 Pct Recovery = 99% Analysis Date = 01/22/21 Pct Recovery = 99% Analysis Date = 01/18/21 Pct Recovery = 100% Analysis Date = 01/18/21 Pct Recovery = 100% Analysis Date = 01/14/21 Pct Recovery = 100% Analysis Date = 01/14/21 Pct Recovery = 100% Analysis Date = 01/10/21 Pct Recovery = 101% Analysis Date = 01/10/21 Pct Recovery = 101% Analysis Date = 01/06/21 Pct Recovery = 102% Analysis Date = 01/06/21 Pct Recovery = 102% Analysis Date = 01/02/21 Pct Recovery = 102% Analysis Date = 01/02/21 Pct Recovery = 102% Analysis Date = 12/29/20 Pct Recovery = 103% Analysis Date = 12/29/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/25/20 Pct Recovery = 103% Analysis Date = 12/21/20 Pct Recovery = 104% Analysis Date = 12/21/20 Pct Recovery = 104% Analysis Date = 12/17/20 Pct Recovery = 105% Analysis Date = 12/17/20 Pct Recovery = 105% Analysis Date = 12/12/20 Pct Recovery = 105% Analysis Date = 12/12/20 Pct Recovery = 105% Analysis Date = 12/08/20 Pct Recovery = 105% Analysis Date = 12/08/20 Pct Recovery = 105% Analysis Date = 12/04/20 Pct Recovery = 106% Analysis Date = 12/04/20 Pct Recovery = 106% Analysis Date = 11/30/20 Pct Recovery = 106% Analysis Date = 11/30/20 Pct Recovery = 106% Analysis Date = 11/26/20 Pct Recovery = 106% Analysis Date = 11/26/20 Pct Recovery = 106% Analysis Date = 11/22/20 Pct Recovery = 106% Analysis Date = 11/22/20 Pct Recovery = 106% Analysis Date = 11/18/20 Pct Recovery = 107% Analysis Date = 11/18/20 Pct Recovery = 107% Analysis Date = 11/14/20 Pct Recovery = 107% Analysis Date = 11/14/20 Pct Recovery = 107% Analysis Date = 11/10/20 Pct Recovery = 107% Analysis Date = 11/10/20 Pct Recovery = 107% Analysis Date = 11/06/20 Pct Recovery = 107% Analysis Date = 11/06/20 Pct Recovery = 107% Analysis Date = 11/02/20 Pct Recovery = 108% Analysis Date = 11/02/20 Pct Recovery = 108% Analysis Date = 10/29/20 Pct Recovery = 108% Analysis Date = 10/29/20 Pct Recovery = 108% Analysis Date = 10/25/20 Pct Recovery = 108% Analysis Date = 10/25/20 Pct Recovery = 108% Analysis Date = 10/21/20 Pct Recovery = 108% Analysis Date = 10/21/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 108% Analysis Date = 10/17/20 Pct Recovery = 108% Analysis Date = 10/13/20 Pct Recovery = 108% Analysis Date = 10/13/20 Pct Recovery = 108% Analysis Date = 10/09/20 Pct Recovery = 109% Analysis Date = 10/09/20 Pct Recovery = 109% Analysis Date = 10/05/20 Pct Recovery = 109% Analysis Date = 10/05/20 Pct Recovery = 109% Analysis Date = 10/01/20 Pct Recovery = 109% Analysis Date = 10/01/20 Pct Recovery = 109% Analysis Date = 09/27/20 Pct Recovery = 109% Analysis Date = 09/27/20 Pct Recovery = 109% Analysis Date = 09/23/20 Pct Recovery = 109% Analysis Date = 09/23/20 Pct Recovery = 109% Analysis Date = 09/19/20 Pct Recovery = 109% Analysis Date = 09/19/20 Pct Recovery = 109% Analysis Date = 09/15/20 Pct Recovery = 109% Analysis Date = 09/15/20 Pct Recovery = 109% Analysis Date = 09/11/20 Pct Recovery = 110% Analysis Date = 09/11/20 Pct Recovery = 110% Analysis Date = 09/07/20 Pct Recovery = 110% Analysis Date = 09/07/20 Pct Recovery = 110% Analysis Date = 09/02/20 Pct Recovery = 110% Analysis Date = 09/02/20 Pct Recovery = 110% Analysis Date = 08/29/20 Pct Recovery = 110% Analysis Date = 08/29/20 Pct Recovery = 110% Analysis Date = 08/25/20 Pct Recovery = 110% Analysis Date = 08/25/20 Pct Recovery = 110% Analysis Date = 08/21/20 Pct Recovery = 110% Analysis Date = 08/21/20 Pct Recovery = 110% Analysis Date = 08/17/20 Pct Recovery = 111% Analysis Date = 08/17/20 Pct Recovery = 111% Analysis Date = 08/13/20 Pct Recovery = 111% Analysis Date = 08/13/20 Pct Recovery = 111% Analysis Date = 08/09/20 Pct Recovery = 111% Analysis Date = 08/09/20 Pct Recovery = 111% Analysis Date = 08/05/20 Pct Recovery = 111% Analysis Date = 08/05/20 Pct Recovery = 111% Analysis Date = 08/01/20 Pct Recovery = 111% Analysis Date = 08/01/20 Pct Recovery = 111% Analysis Date = 07/28/20 Pct Recovery = 112% Analysis Date = 07/28/20 Pct Recovery = 112% Analysis Date = 07/24/20 Pct Recovery = 112% Analysis Date = 07/24/20 Pct Recovery = 112% Analysis Date = 07/20/20 Pct Recovery = 112% Analysis Date = 07/20/20 Pct Recovery = 112% Analysis Date = 07/16/20 Pct Recovery = 112% Analysis Date = 07/16/20 Pct Recovery = 112% Analysis Date = 07/12/20 Pct Recovery = 112% Analysis Date = 07/12/20 Pct Recovery = 112% Analysis Date = 07/08/20 Pct Recovery = 113% Analysis Date = 07/08/20 Pct Recovery = 113% Analysis Date = 07/04/20 Pct Recovery = 113% Analysis Date = 07/04/20 Pct Recovery = 113% Analysis Date = 06/30/20 Pct Recovery = 113% Analysis Date = 06/30/20 Pct Recovery = 113% Analysis Date = 06/26/20 Pct Recovery = 113% Analysis Date = 06/26/20 Pct Recovery = 113% Analysis Date = 06/22/20 Pct Recovery = 113% Analysis Date = 06/22/20 Pct Recovery = 113% Analysis Date = 06/18/20 Pct Recovery = 114% Analysis Date = 06/18/20 Pct Recovery = 114% Analysis Date = 06/14/20 Pct Recovery = 114% Analysis Date = 06/14/20 Pct Recovery = 114% Analysis Date = 06/10/20 Pct Recovery = 114% Analysis Date = 06/10/20 Pct Recovery = 114% Analysis Date = 06/06/20 Pct Recovery = 114% Analysis Date = 06/06/20 Pct Recovery = 114% Analysis Date = 06/02/20 Pct Recovery = 115% Analysis Date = 06/02/20 Pct Recovery = 115% Analysis Date = 05/29/20 Pct Recovery = 115% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 101% 20% 101% 17%
Total 33 101% 20% 101% 17%

Sample Statistics
PROPAZINE

Characteristic N % % Basis
Plotted 33 97% Spiked
Estimated Values 1 3% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 34 .  
False Negatives 1 3% 1 out of 34
Not Spiked 82 .  
False Positives 2 2% 2 out of 82

OBSP Determination:
PROPICONAZOLE (TILT)
METHOD: 2447 , TESTIDCODE: 66643LCM60

Laboratory ID = 20202590106 Lab Value = 65.654 Expected Conc. = 75.3 Report level label = 6 Pct Recovery = 87% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 72.966 Expected Conc. = 75.3 Report level label = 6 Pct Recovery = 97% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 64.269 Expected Conc. = 75.1 Report level label = 6 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 70.351 Expected Conc. = 75.1 Report level label = 6 Pct Recovery = 94% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20221940195 Lab Value = 50.123 Expected Conc. = 60.68 Report level label = 6 Pct Recovery = 83% Analysis Date = 07/23/22 SpikeMix = ChemService 13290400: 80 µl SpecificMix = 13290400 Laboratory ID = 20222010133 Lab Value = 40.974 Expected Conc. = 60 Report level label = 6 Pct Recovery = 68% Analysis Date = 07/24/22 SpikeMix = Crescent 04DD026: 80 µl SpecificMix = 04DD026 Laboratory ID = 20222640086 Lab Value = 51.695 Expected Conc. = 59.6 Report level label = 6 Pct Recovery = 87% Analysis Date = 09/29/22 SpikeMix = Spex Organics NA220729007: 80 µl SpecificMix = NA220729007 Laboratory ID = 20203230018 Lab Value = 28.927 Expected Conc. = 37.65 Report level label = 6 Pct Recovery = 77% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 26.824 Expected Conc. = 37.65 Report level label = 6 Pct Recovery = 71% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 39.352 Expected Conc. = 37.65 Report level label = 6 Pct Recovery = 105% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 58.882 Expected Conc. = 37.6 Report level label = 6 Pct Recovery = 157% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 39.113 Expected Conc. = 37.6 Report level label = 6 Pct Recovery = 104% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20221870197 Lab Value = 35.656 Expected Conc. = 37.5 Report level label = 6 Pct Recovery = 95% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 02AA022 Laboratory ID = 20221730293 Lab Value = 27.157 Expected Conc. = 37.5 Report level label = 6 Pct Recovery = 72% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 02AA022 Laboratory ID = 20201960104 Lab Value = 34.992 Expected Conc. = 30.08 Report level label = 6 Pct Recovery = 116% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 30.648 Expected Conc. = 30.08 Report level label = 6 Pct Recovery = 102% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210970035 Lab Value = 14.706 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 98% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 11.341 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 75% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 14.684 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 98% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 12.146 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 81% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 13.485 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 90% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 15.785 Expected Conc. = 15.06 Report level label = 6 Pct Recovery = 105% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210270007 Lab Value = 17.221 Expected Conc. = 15.02 Report level label = 6 Pct Recovery = 115% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222500483 Lab Value = 12.259 Expected Conc. = 15 Report level label = 6 Pct Recovery = 82% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 02AA022 Analysis Date = 09/29/22 Pct Recovery = 81% Analysis Date = 09/24/22 Pct Recovery = 81% Analysis Date = 09/24/22 Pct Recovery = 81% Analysis Date = 09/20/22 Pct Recovery = 81% Analysis Date = 09/20/22 Pct Recovery = 81% Analysis Date = 09/16/22 Pct Recovery = 81% Analysis Date = 09/16/22 Pct Recovery = 81% Analysis Date = 09/12/22 Pct Recovery = 81% Analysis Date = 09/12/22 Pct Recovery = 81% Analysis Date = 09/08/22 Pct Recovery = 81% Analysis Date = 09/08/22 Pct Recovery = 81% Analysis Date = 09/04/22 Pct Recovery = 81% Analysis Date = 09/04/22 Pct Recovery = 81% Analysis Date = 08/31/22 Pct Recovery = 81% Analysis Date = 08/31/22 Pct Recovery = 81% Analysis Date = 08/26/22 Pct Recovery = 81% Analysis Date = 08/26/22 Pct Recovery = 81% Analysis Date = 08/22/22 Pct Recovery = 81% Analysis Date = 08/22/22 Pct Recovery = 81% Analysis Date = 08/18/22 Pct Recovery = 81% Analysis Date = 08/18/22 Pct Recovery = 81% Analysis Date = 08/14/22 Pct Recovery = 81% Analysis Date = 08/14/22 Pct Recovery = 81% Analysis Date = 08/10/22 Pct Recovery = 81% Analysis Date = 08/10/22 Pct Recovery = 81% Analysis Date = 08/06/22 Pct Recovery = 81% Analysis Date = 08/06/22 Pct Recovery = 81% Analysis Date = 08/02/22 Pct Recovery = 81% Analysis Date = 08/02/22 Pct Recovery = 81% Analysis Date = 07/29/22 Pct Recovery = 81% Analysis Date = 07/29/22 Pct Recovery = 81% Analysis Date = 07/24/22 Pct Recovery = 82% Analysis Date = 07/24/22 Pct Recovery = 82% Analysis Date = 07/20/22 Pct Recovery = 82% Analysis Date = 07/20/22 Pct Recovery = 82% Analysis Date = 07/16/22 Pct Recovery = 82% Analysis Date = 07/16/22 Pct Recovery = 82% Analysis Date = 07/12/22 Pct Recovery = 82% Analysis Date = 07/12/22 Pct Recovery = 82% Analysis Date = 07/08/22 Pct Recovery = 82% Analysis Date = 07/08/22 Pct Recovery = 82% Analysis Date = 07/04/22 Pct Recovery = 82% Analysis Date = 07/04/22 Pct Recovery = 82% Analysis Date = 06/30/22 Pct Recovery = 82% Analysis Date = 06/30/22 Pct Recovery = 82% Analysis Date = 06/26/22 Pct Recovery = 82% Analysis Date = 06/26/22 Pct Recovery = 82% Analysis Date = 06/21/22 Pct Recovery = 82% Analysis Date = 06/21/22 Pct Recovery = 82% Analysis Date = 06/17/22 Pct Recovery = 83% Analysis Date = 06/17/22 Pct Recovery = 83% Analysis Date = 06/13/22 Pct Recovery = 83% Analysis Date = 06/13/22 Pct Recovery = 83% Analysis Date = 06/09/22 Pct Recovery = 83% Analysis Date = 06/09/22 Pct Recovery = 83% Analysis Date = 06/05/22 Pct Recovery = 83% Analysis Date = 06/05/22 Pct Recovery = 83% Analysis Date = 06/01/22 Pct Recovery = 83% Analysis Date = 06/01/22 Pct Recovery = 83% Analysis Date = 05/28/22 Pct Recovery = 83% Analysis Date = 05/28/22 Pct Recovery = 83% Analysis Date = 05/23/22 Pct Recovery = 83% Analysis Date = 05/23/22 Pct Recovery = 83% Analysis Date = 05/19/22 Pct Recovery = 83% Analysis Date = 05/19/22 Pct Recovery = 83% Analysis Date = 05/15/22 Pct Recovery = 84% Analysis Date = 05/15/22 Pct Recovery = 84% Analysis Date = 05/11/22 Pct Recovery = 84% Analysis Date = 05/11/22 Pct Recovery = 84% Analysis Date = 05/07/22 Pct Recovery = 84% Analysis Date = 05/07/22 Pct Recovery = 84% Analysis Date = 05/03/22 Pct Recovery = 84% Analysis Date = 05/03/22 Pct Recovery = 84% Analysis Date = 04/29/22 Pct Recovery = 84% Analysis Date = 04/29/22 Pct Recovery = 84% Analysis Date = 04/25/22 Pct Recovery = 84% Analysis Date = 04/25/22 Pct Recovery = 84% Analysis Date = 04/20/22 Pct Recovery = 84% Analysis Date = 04/20/22 Pct Recovery = 84% Analysis Date = 04/16/22 Pct Recovery = 84% Analysis Date = 04/16/22 Pct Recovery = 84% Analysis Date = 04/12/22 Pct Recovery = 85% Analysis Date = 04/12/22 Pct Recovery = 85% Analysis Date = 04/08/22 Pct Recovery = 85% Analysis Date = 04/08/22 Pct Recovery = 85% Analysis Date = 04/04/22 Pct Recovery = 85% Analysis Date = 04/04/22 Pct Recovery = 85% Analysis Date = 03/31/22 Pct Recovery = 85% Analysis Date = 03/31/22 Pct Recovery = 85% Analysis Date = 03/27/22 Pct Recovery = 85% Analysis Date = 03/27/22 Pct Recovery = 85% Analysis Date = 03/23/22 Pct Recovery = 85% Analysis Date = 03/23/22 Pct Recovery = 85% Analysis Date = 03/18/22 Pct Recovery = 85% Analysis Date = 03/18/22 Pct Recovery = 85% Analysis Date = 03/14/22 Pct Recovery = 85% Analysis Date = 03/14/22 Pct Recovery = 85% Analysis Date = 03/10/22 Pct Recovery = 86% Analysis Date = 03/10/22 Pct Recovery = 86% Analysis Date = 03/06/22 Pct Recovery = 86% Analysis Date = 03/06/22 Pct Recovery = 86% Analysis Date = 03/02/22 Pct Recovery = 86% Analysis Date = 03/02/22 Pct Recovery = 86% Analysis Date = 02/26/22 Pct Recovery = 86% Analysis Date = 02/26/22 Pct Recovery = 86% Analysis Date = 02/22/22 Pct Recovery = 86% Analysis Date = 02/22/22 Pct Recovery = 86% Analysis Date = 02/17/22 Pct Recovery = 86% Analysis Date = 02/17/22 Pct Recovery = 86% Analysis Date = 02/13/22 Pct Recovery = 86% Analysis Date = 02/13/22 Pct Recovery = 86% Analysis Date = 02/09/22 Pct Recovery = 86% Analysis Date = 02/09/22 Pct Recovery = 86% Analysis Date = 02/05/22 Pct Recovery = 87% Analysis Date = 02/05/22 Pct Recovery = 87% Analysis Date = 02/01/22 Pct Recovery = 87% Analysis Date = 02/01/22 Pct Recovery = 87% Analysis Date = 01/28/22 Pct Recovery = 87% Analysis Date = 01/28/22 Pct Recovery = 87% Analysis Date = 01/24/22 Pct Recovery = 87% Analysis Date = 01/24/22 Pct Recovery = 87% Analysis Date = 01/20/22 Pct Recovery = 87% Analysis Date = 01/20/22 Pct Recovery = 87% Analysis Date = 01/15/22 Pct Recovery = 87% Analysis Date = 01/15/22 Pct Recovery = 87% Analysis Date = 01/11/22 Pct Recovery = 87% Analysis Date = 01/11/22 Pct Recovery = 87% Analysis Date = 01/07/22 Pct Recovery = 88% Analysis Date = 01/07/22 Pct Recovery = 88% Analysis Date = 01/03/22 Pct Recovery = 88% Analysis Date = 01/03/22 Pct Recovery = 88% Analysis Date = 12/30/21 Pct Recovery = 88% Analysis Date = 12/30/21 Pct Recovery = 88% Analysis Date = 12/26/21 Pct Recovery = 88% Analysis Date = 12/26/21 Pct Recovery = 88% Analysis Date = 12/22/21 Pct Recovery = 88% Analysis Date = 12/22/21 Pct Recovery = 88% Analysis Date = 12/18/21 Pct Recovery = 88% Analysis Date = 12/18/21 Pct Recovery = 88% Analysis Date = 12/13/21 Pct Recovery = 88% Analysis Date = 12/13/21 Pct Recovery = 88% Analysis Date = 12/09/21 Pct Recovery = 88% Analysis Date = 12/09/21 Pct Recovery = 88% Analysis Date = 12/05/21 Pct Recovery = 89% Analysis Date = 12/05/21 Pct Recovery = 89% Analysis Date = 12/01/21 Pct Recovery = 89% Analysis Date = 12/01/21 Pct Recovery = 89% Analysis Date = 11/27/21 Pct Recovery = 89% Analysis Date = 11/27/21 Pct Recovery = 89% Analysis Date = 11/23/21 Pct Recovery = 89% Analysis Date = 11/23/21 Pct Recovery = 89% Analysis Date = 11/19/21 Pct Recovery = 89% Analysis Date = 11/19/21 Pct Recovery = 89% Analysis Date = 11/14/21 Pct Recovery = 89% Analysis Date = 11/14/21 Pct Recovery = 89% Analysis Date = 11/10/21 Pct Recovery = 89% Analysis Date = 11/10/21 Pct Recovery = 89% Analysis Date = 11/06/21 Pct Recovery = 89% Analysis Date = 11/06/21 Pct Recovery = 89% Analysis Date = 11/02/21 Pct Recovery = 90% Analysis Date = 11/02/21 Pct Recovery = 90% Analysis Date = 10/29/21 Pct Recovery = 90% Analysis Date = 10/29/21 Pct Recovery = 90% Analysis Date = 10/25/21 Pct Recovery = 90% Analysis Date = 10/25/21 Pct Recovery = 90% Analysis Date = 10/21/21 Pct Recovery = 90% Analysis Date = 10/21/21 Pct Recovery = 90% Analysis Date = 10/17/21 Pct Recovery = 90% Analysis Date = 10/17/21 Pct Recovery = 90% Analysis Date = 10/12/21 Pct Recovery = 90% Analysis Date = 10/12/21 Pct Recovery = 90% Analysis Date = 10/08/21 Pct Recovery = 90% Analysis Date = 10/08/21 Pct Recovery = 90% Analysis Date = 10/04/21 Pct Recovery = 90% Analysis Date = 10/04/21 Pct Recovery = 90% Analysis Date = 09/30/21 Pct Recovery = 91% Analysis Date = 09/30/21 Pct Recovery = 91% Analysis Date = 09/26/21 Pct Recovery = 91% Analysis Date = 09/26/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 91% Analysis Date = 09/18/21 Pct Recovery = 91% Analysis Date = 09/18/21 Pct Recovery = 91% Analysis Date = 09/14/21 Pct Recovery = 91% Analysis Date = 09/14/21 Pct Recovery = 91% Analysis Date = 09/09/21 Pct Recovery = 91% Analysis Date = 09/09/21 Pct Recovery = 91% Analysis Date = 09/05/21 Pct Recovery = 91% Analysis Date = 09/05/21 Pct Recovery = 91% Analysis Date = 09/01/21 Pct Recovery = 92% Analysis Date = 09/01/21 Pct Recovery = 92% Analysis Date = 08/28/21 Pct Recovery = 92% Analysis Date = 08/28/21 Pct Recovery = 92% Analysis Date = 08/24/21 Pct Recovery = 92% Analysis Date = 08/24/21 Pct Recovery = 92% Analysis Date = 08/20/21 Pct Recovery = 92% Analysis Date = 08/20/21 Pct Recovery = 92% Analysis Date = 08/16/21 Pct Recovery = 92% Analysis Date = 08/16/21 Pct Recovery = 92% Analysis Date = 08/12/21 Pct Recovery = 92% Analysis Date = 08/12/21 Pct Recovery = 92% Analysis Date = 08/07/21 Pct Recovery = 92% Analysis Date = 08/07/21 Pct Recovery = 92% Analysis Date = 08/03/21 Pct Recovery = 92% Analysis Date = 08/03/21 Pct Recovery = 92% Analysis Date = 07/30/21 Pct Recovery = 93% Analysis Date = 07/30/21 Pct Recovery = 93% Analysis Date = 07/26/21 Pct Recovery = 93% Analysis Date = 07/26/21 Pct Recovery = 93% Analysis Date = 07/22/21 Pct Recovery = 93% Analysis Date = 07/22/21 Pct Recovery = 93% Analysis Date = 07/18/21 Pct Recovery = 93% Analysis Date = 07/18/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/09/21 Pct Recovery = 93% Analysis Date = 07/09/21 Pct Recovery = 93% Analysis Date = 07/05/21 Pct Recovery = 93% Analysis Date = 07/05/21 Pct Recovery = 93% Analysis Date = 07/01/21 Pct Recovery = 93% Analysis Date = 07/01/21 Pct Recovery = 93% Analysis Date = 06/27/21 Pct Recovery = 94% Analysis Date = 06/27/21 Pct Recovery = 94% Analysis Date = 06/23/21 Pct Recovery = 94% Analysis Date = 06/23/21 Pct Recovery = 94% Analysis Date = 06/19/21 Pct Recovery = 94% Analysis Date = 06/19/21 Pct Recovery = 94% Analysis Date = 06/15/21 Pct Recovery = 94% Analysis Date = 06/15/21 Pct Recovery = 94% Analysis Date = 06/11/21 Pct Recovery = 94% Analysis Date = 06/11/21 Pct Recovery = 94% Analysis Date = 06/06/21 Pct Recovery = 94% Analysis Date = 06/06/21 Pct Recovery = 94% Analysis Date = 06/02/21 Pct Recovery = 94% Analysis Date = 06/02/21 Pct Recovery = 94% Analysis Date = 05/29/21 Pct Recovery = 94% Analysis Date = 05/29/21 Pct Recovery = 94% Analysis Date = 05/25/21 Pct Recovery = 95% Analysis Date = 05/25/21 Pct Recovery = 95% Analysis Date = 05/21/21 Pct Recovery = 95% Analysis Date = 05/21/21 Pct Recovery = 95% Analysis Date = 05/17/21 Pct Recovery = 95% Analysis Date = 05/17/21 Pct Recovery = 95% Analysis Date = 05/13/21 Pct Recovery = 95% Analysis Date = 05/13/21 Pct Recovery = 95% Analysis Date = 05/09/21 Pct Recovery = 95% Analysis Date = 05/09/21 Pct Recovery = 95% Analysis Date = 05/04/21 Pct Recovery = 95% Analysis Date = 05/04/21 Pct Recovery = 95% Analysis Date = 04/30/21 Pct Recovery = 95% Analysis Date = 04/30/21 Pct Recovery = 95% Analysis Date = 04/26/21 Pct Recovery = 95% Analysis Date = 04/26/21 Pct Recovery = 95% Analysis Date = 04/22/21 Pct Recovery = 96% Analysis Date = 04/22/21 Pct Recovery = 96% Analysis Date = 04/18/21 Pct Recovery = 96% Analysis Date = 04/18/21 Pct Recovery = 96% Analysis Date = 04/14/21 Pct Recovery = 96% Analysis Date = 04/14/21 Pct Recovery = 96% Analysis Date = 04/10/21 Pct Recovery = 96% Analysis Date = 04/10/21 Pct Recovery = 96% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/05/21 Pct Recovery = 95% Analysis Date = 04/01/21 Pct Recovery = 95% Analysis Date = 04/01/21 Pct Recovery = 95% Analysis Date = 03/28/21 Pct Recovery = 94% Analysis Date = 03/28/21 Pct Recovery = 94% Analysis Date = 03/24/21 Pct Recovery = 94% Analysis Date = 03/24/21 Pct Recovery = 94% Analysis Date = 03/20/21 Pct Recovery = 94% Analysis Date = 03/20/21 Pct Recovery = 94% Analysis Date = 03/16/21 Pct Recovery = 93% Analysis Date = 03/16/21 Pct Recovery = 93% Analysis Date = 03/12/21 Pct Recovery = 93% Analysis Date = 03/12/21 Pct Recovery = 93% Analysis Date = 03/08/21 Pct Recovery = 93% Analysis Date = 03/08/21 Pct Recovery = 93% Analysis Date = 03/03/21 Pct Recovery = 92% Analysis Date = 03/03/21 Pct Recovery = 92% Analysis Date = 02/27/21 Pct Recovery = 92% Analysis Date = 02/27/21 Pct Recovery = 92% Analysis Date = 02/23/21 Pct Recovery = 92% Analysis Date = 02/23/21 Pct Recovery = 92% Analysis Date = 02/19/21 Pct Recovery = 91% Analysis Date = 02/19/21 Pct Recovery = 91% Analysis Date = 02/15/21 Pct Recovery = 91% Analysis Date = 02/15/21 Pct Recovery = 91% Analysis Date = 02/11/21 Pct Recovery = 91% Analysis Date = 02/11/21 Pct Recovery = 91% Analysis Date = 02/07/21 Pct Recovery = 90% Analysis Date = 02/07/21 Pct Recovery = 90% Analysis Date = 02/03/21 Pct Recovery = 90% Analysis Date = 02/03/21 Pct Recovery = 90% Analysis Date = 01/29/21 Pct Recovery = 90% Analysis Date = 01/29/21 Pct Recovery = 90% Analysis Date = 01/25/21 Pct Recovery = 90% Analysis Date = 01/25/21 Pct Recovery = 90% Analysis Date = 01/21/21 Pct Recovery = 90% Analysis Date = 01/21/21 Pct Recovery = 90% Analysis Date = 01/17/21 Pct Recovery = 90% Analysis Date = 01/17/21 Pct Recovery = 90% Analysis Date = 01/13/21 Pct Recovery = 90% Analysis Date = 01/13/21 Pct Recovery = 90% Analysis Date = 01/09/21 Pct Recovery = 89% Analysis Date = 01/09/21 Pct Recovery = 89% Analysis Date = 01/05/21 Pct Recovery = 89% Analysis Date = 01/05/21 Pct Recovery = 89% Analysis Date = 12/31/20 Pct Recovery = 89% Analysis Date = 12/31/20 Pct Recovery = 89% Analysis Date = 12/27/20 Pct Recovery = 89% Analysis Date = 12/27/20 Pct Recovery = 89% Analysis Date = 12/23/20 Pct Recovery = 89% Analysis Date = 12/23/20 Pct Recovery = 89% Analysis Date = 12/19/20 Pct Recovery = 89% Analysis Date = 12/19/20 Pct Recovery = 89% Analysis Date = 12/15/20 Pct Recovery = 90% Analysis Date = 12/15/20 Pct Recovery = 90% Analysis Date = 12/11/20 Pct Recovery = 90% Analysis Date = 12/11/20 Pct Recovery = 90% Analysis Date = 12/07/20 Pct Recovery = 90% Analysis Date = 12/07/20 Pct Recovery = 90% Analysis Date = 12/03/20 Pct Recovery = 91% Analysis Date = 12/03/20 Pct Recovery = 91% Analysis Date = 11/28/20 Pct Recovery = 91% Analysis Date = 11/28/20 Pct Recovery = 91% Analysis Date = 11/24/20 Pct Recovery = 92% Analysis Date = 11/24/20 Pct Recovery = 92% Analysis Date = 11/20/20 Pct Recovery = 92% Analysis Date = 11/20/20 Pct Recovery = 92% Analysis Date = 11/16/20 Pct Recovery = 93% Analysis Date = 11/16/20 Pct Recovery = 93% Analysis Date = 11/12/20 Pct Recovery = 93% Analysis Date = 11/12/20 Pct Recovery = 93% Analysis Date = 11/08/20 Pct Recovery = 94% Analysis Date = 11/08/20 Pct Recovery = 94% Analysis Date = 11/04/20 Pct Recovery = 94% Analysis Date = 11/04/20 Pct Recovery = 94% Analysis Date = 10/31/20 Pct Recovery = 96% Analysis Date = 10/31/20 Pct Recovery = 96% Analysis Date = 10/26/20 Pct Recovery = 97% Analysis Date = 10/26/20 Pct Recovery = 97% Analysis Date = 10/22/20 Pct Recovery = 98% Analysis Date = 10/22/20 Pct Recovery = 98% Analysis Date = 10/18/20 Pct Recovery = 99% Analysis Date = 10/18/20 Pct Recovery = 99% Analysis Date = 10/14/20 Pct Recovery = 100% Analysis Date = 10/14/20 Pct Recovery = 100% Analysis Date = 10/10/20 Pct Recovery = 101% Analysis Date = 10/10/20 Pct Recovery = 101% Analysis Date = 10/06/20 Pct Recovery = 102% Analysis Date = 10/06/20 Pct Recovery = 102% Analysis Date = 10/02/20 Pct Recovery = 103% Analysis Date = 10/02/20 Pct Recovery = 103% Analysis Date = 09/27/20 Pct Recovery = 104% Analysis Date = 09/27/20 Pct Recovery = 104% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/15/20 Pct Recovery = 106% Analysis Date = 09/15/20 Pct Recovery = 106% Analysis Date = 09/11/20 Pct Recovery = 106% Analysis Date = 09/11/20 Pct Recovery = 106% Analysis Date = 09/07/20 Pct Recovery = 107% Analysis Date = 09/07/20 Pct Recovery = 107% Analysis Date = 09/03/20 Pct Recovery = 107% Analysis Date = 09/03/20 Pct Recovery = 107% Analysis Date = 08/30/20 Pct Recovery = 108% Analysis Date = 08/30/20 Pct Recovery = 108% Analysis Date = 08/25/20 Pct Recovery = 109% Analysis Date = 08/25/20 Pct Recovery = 109% Analysis Date = 08/21/20 Pct Recovery = 109% Analysis Date = 08/21/20 Pct Recovery = 109% Analysis Date = 08/17/20 Pct Recovery = 110% Analysis Date = 08/17/20 Pct Recovery = 110% Analysis Date = 08/13/20 Pct Recovery = 110% Analysis Date = 08/13/20 Pct Recovery = 110% Analysis Date = 08/09/20 Pct Recovery = 111% Analysis Date = 08/09/20 Pct Recovery = 111% Analysis Date = 08/05/20 Pct Recovery = 111% Analysis Date = 08/05/20 Pct Recovery = 111% Analysis Date = 08/01/20 Pct Recovery = 112% Analysis Date = 08/01/20 Pct Recovery = 112% Analysis Date = 07/28/20 Pct Recovery = 112% Analysis Date = 07/28/20 Pct Recovery = 112% Analysis Date = 07/23/20 Pct Recovery = 113% Analysis Date = 07/23/20 Pct Recovery = 113% Analysis Date = 07/19/20 Pct Recovery = 113% Analysis Date = 07/19/20 Pct Recovery = 113% Analysis Date = 07/15/20 Pct Recovery = 114% Analysis Date = 07/15/20 Pct Recovery = 114% Analysis Date = 07/11/20 Pct Recovery = 114% Analysis Date = 07/11/20 Pct Recovery = 114% Analysis Date = 07/07/20 Pct Recovery = 115% Analysis Date = 07/07/20 Pct Recovery = 115% Analysis Date = 07/03/20 Pct Recovery = 115% Analysis Date = 07/03/20 Pct Recovery = 115% Analysis Date = 06/29/20 Pct Recovery = 116% Analysis Date = 06/29/20 Pct Recovery = 116% Analysis Date = 06/25/20 Pct Recovery = 116% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPICONAZOLE (TILT)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 24 93% 19% 92% 16%
Total 24 93% 19% 92% 16%

Sample Statistics
PROPICONAZOLE (TILT)

Characteristic N % % Basis
Plotted 24 89% Spiked
Estimated Values 1 4% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 4% Spiked
Spiked 27 .  
False Negatives 2 7% 2 out of 27
Not Spiked 83 .  
False Positives 0 0% 0 out of 83

OBSP Determination:
PROPOXUR
METHOD: 2447 , TESTIDCODE: 68679LCM60

Laboratory ID = 20213200091 Lab Value = 46.842 Expected Conc. = 20.15 Report level label = 3.2 Pct Recovery = 232% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20210760015 Lab Value = 30.673 Expected Conc. = 40.11 Report level label = 3.2 Pct Recovery = 76% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 47.222 Expected Conc. = 40.11 Report level label = 3.2 Pct Recovery = 118% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 46.534 Expected Conc. = 40.11 Report level label = 3.2 Pct Recovery = 116% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 43.078 Expected Conc. = 40.11 Report level label = 3.2 Pct Recovery = 107% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 42.248 Expected Conc. = 40 Report level label = 3.2 Pct Recovery = 106% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 35.412 Expected Conc. = 40 Report level label = 3.2 Pct Recovery = 89% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 39.992 Expected Conc. = 40 Report level label = 3.2 Pct Recovery = 100% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150193 Lab Value = 20.169 Expected Conc. = 32.48 Report level label = 3.2 Pct Recovery = 62% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20220190116 Lab Value = 19.863 Expected Conc. = 32.24 Report level label = 3.2 Pct Recovery = 62% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 27.681 Expected Conc. = 32.24 Report level label = 3.2 Pct Recovery = 86% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20212990174 Lab Value = 23.298 Expected Conc. = 32.24 Report level label = 3.2 Pct Recovery = 72% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220810134 Lab Value = 31.102 Expected Conc. = 32.08 Report level label = 3.2 Pct Recovery = 97% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222010132 Lab Value = 26.094 Expected Conc. = 32 Report level label = 3.2 Pct Recovery = 82% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20201550031 Lab Value = 19.709 Expected Conc. = 20.2 Report level label = 3.2 Pct Recovery = 98% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20221730293 Lab Value = 15.202 Expected Conc. = 20.15 Report level label = 3.2 Pct Recovery = 75% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 10.418 Expected Conc. = 20.15 Report level label = 3.2 Pct Recovery = 52% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20213340027 Lab Value = 15.129 Expected Conc. = 20.15 Report level label = 3.2 Pct Recovery = 75% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 22.204 Expected Conc. = 20.15 Report level label = 3.2 Pct Recovery = 110% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20210480001 Lab Value = 21.628 Expected Conc. = 20.055 Report level label = 3.2 Pct Recovery = 108% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20220810133 Lab Value = 15.625 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 78% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20202390020 Lab Value = 27.408 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 137% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 27.594 Expected Conc. = 20.05 Report level label = 3.2 Pct Recovery = 138% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202880004 Lab Value = 26.147 Expected Conc. = 20 Report level label = 3.2 Pct Recovery = 131% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 14.029 Expected Conc. = 16.044 Report level label = 3.2 Pct Recovery = 87% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201960104 Lab Value = 20.750 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 129% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 18.655 Expected Conc. = 16.04 Report level label = 3.2 Pct Recovery = 116% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20210620006 Lab Value = 15.962 Expected Conc. = 16 Report level label = 3.2 Pct Recovery = 100% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 20.769 Expected Conc. = 16 Report level label = 3.2 Pct Recovery = 130% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202330309 Lab Value = 7.147 Expected Conc. = 8.08 Report level label = 3.2 Pct Recovery = 88% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 7.039 Expected Conc. = 8.08 Report level label = 3.2 Pct Recovery = 87% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 9.111 Expected Conc. = 8.08 Report level label = 3.2 Pct Recovery = 113% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 9.125 Expected Conc. = 8.08 Report level label = 3.2 Pct Recovery = 113% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 11.690 Expected Conc. = 8.08 Report level label = 3.2 Pct Recovery = 145% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20222500483 Lab Value = 8.133 Expected Conc. = 8.06 Report level label = 3.2 Pct Recovery = 101% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 6.698 Expected Conc. = 8.06 Report level label = 3.2 Pct Recovery = 83% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213060210 Lab Value = 5.094 Expected Conc. = 8.06 Report level label = 3.2 Pct Recovery = 63% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210690067 Lab Value = 9.227 Expected Conc. = 8.022 Report level label = 3.2 Pct Recovery = 115% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20222630205 Lab Value = 5.884 Expected Conc. = 8.02 Report level label = 3.2 Pct Recovery = 73% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210120050 Lab Value = 7.856 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 98% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 10.469 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 131% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 6.177 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 77% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 9.458 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 118% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 9.954 Expected Conc. = 8 Report level label = 3.2 Pct Recovery = 124% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 09/28/22 Pct Recovery = 74% Analysis Date = 09/24/22 Pct Recovery = 74% Analysis Date = 09/24/22 Pct Recovery = 74% Analysis Date = 09/20/22 Pct Recovery = 75% Analysis Date = 09/20/22 Pct Recovery = 75% Analysis Date = 09/16/22 Pct Recovery = 75% Analysis Date = 09/16/22 Pct Recovery = 75% Analysis Date = 09/11/22 Pct Recovery = 75% Analysis Date = 09/11/22 Pct Recovery = 75% Analysis Date = 09/07/22 Pct Recovery = 76% Analysis Date = 09/07/22 Pct Recovery = 76% Analysis Date = 09/03/22 Pct Recovery = 76% Analysis Date = 09/03/22 Pct Recovery = 76% Analysis Date = 08/30/22 Pct Recovery = 76% Analysis Date = 08/30/22 Pct Recovery = 76% Analysis Date = 08/25/22 Pct Recovery = 76% Analysis Date = 08/25/22 Pct Recovery = 76% Analysis Date = 08/21/22 Pct Recovery = 77% Analysis Date = 08/21/22 Pct Recovery = 77% Analysis Date = 08/17/22 Pct Recovery = 77% Analysis Date = 08/17/22 Pct Recovery = 77% Analysis Date = 08/13/22 Pct Recovery = 77% Analysis Date = 08/13/22 Pct Recovery = 77% Analysis Date = 08/08/22 Pct Recovery = 77% Analysis Date = 08/08/22 Pct Recovery = 77% Analysis Date = 08/04/22 Pct Recovery = 78% Analysis Date = 08/04/22 Pct Recovery = 78% Analysis Date = 07/31/22 Pct Recovery = 78% Analysis Date = 07/31/22 Pct Recovery = 78% Analysis Date = 07/27/22 Pct Recovery = 78% Analysis Date = 07/27/22 Pct Recovery = 78% Analysis Date = 07/22/22 Pct Recovery = 79% Analysis Date = 07/22/22 Pct Recovery = 79% Analysis Date = 07/18/22 Pct Recovery = 79% Analysis Date = 07/18/22 Pct Recovery = 79% Analysis Date = 07/14/22 Pct Recovery = 79% Analysis Date = 07/14/22 Pct Recovery = 79% Analysis Date = 07/09/22 Pct Recovery = 79% Analysis Date = 07/09/22 Pct Recovery = 79% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/05/22 Pct Recovery = 80% Analysis Date = 07/01/22 Pct Recovery = 80% Analysis Date = 07/01/22 Pct Recovery = 80% Analysis Date = 06/27/22 Pct Recovery = 80% Analysis Date = 06/27/22 Pct Recovery = 80% Analysis Date = 06/22/22 Pct Recovery = 80% Analysis Date = 06/22/22 Pct Recovery = 80% Analysis Date = 06/18/22 Pct Recovery = 81% Analysis Date = 06/18/22 Pct Recovery = 81% Analysis Date = 06/14/22 Pct Recovery = 81% Analysis Date = 06/14/22 Pct Recovery = 81% Analysis Date = 06/10/22 Pct Recovery = 81% Analysis Date = 06/10/22 Pct Recovery = 81% Analysis Date = 06/05/22 Pct Recovery = 82% Analysis Date = 06/05/22 Pct Recovery = 82% Analysis Date = 06/01/22 Pct Recovery = 82% Analysis Date = 06/01/22 Pct Recovery = 82% Analysis Date = 05/28/22 Pct Recovery = 82% Analysis Date = 05/28/22 Pct Recovery = 82% Analysis Date = 05/24/22 Pct Recovery = 82% Analysis Date = 05/24/22 Pct Recovery = 82% Analysis Date = 05/19/22 Pct Recovery = 83% Analysis Date = 05/19/22 Pct Recovery = 83% Analysis Date = 05/15/22 Pct Recovery = 83% Analysis Date = 05/15/22 Pct Recovery = 83% Analysis Date = 05/11/22 Pct Recovery = 83% Analysis Date = 05/11/22 Pct Recovery = 83% Analysis Date = 05/06/22 Pct Recovery = 83% Analysis Date = 05/06/22 Pct Recovery = 83% Analysis Date = 05/02/22 Pct Recovery = 84% Analysis Date = 05/02/22 Pct Recovery = 84% Analysis Date = 04/28/22 Pct Recovery = 84% Analysis Date = 04/28/22 Pct Recovery = 84% Analysis Date = 04/24/22 Pct Recovery = 84% Analysis Date = 04/24/22 Pct Recovery = 84% Analysis Date = 04/19/22 Pct Recovery = 84% Analysis Date = 04/19/22 Pct Recovery = 84% Analysis Date = 04/15/22 Pct Recovery = 85% Analysis Date = 04/15/22 Pct Recovery = 85% Analysis Date = 04/11/22 Pct Recovery = 85% Analysis Date = 04/11/22 Pct Recovery = 85% Analysis Date = 04/07/22 Pct Recovery = 85% Analysis Date = 04/07/22 Pct Recovery = 85% Analysis Date = 04/02/22 Pct Recovery = 86% Analysis Date = 04/02/22 Pct Recovery = 86% Analysis Date = 03/29/22 Pct Recovery = 86% Analysis Date = 03/29/22 Pct Recovery = 86% Analysis Date = 03/25/22 Pct Recovery = 86% Analysis Date = 03/25/22 Pct Recovery = 86% Analysis Date = 03/21/22 Pct Recovery = 86% Analysis Date = 03/21/22 Pct Recovery = 86% Analysis Date = 03/16/22 Pct Recovery = 87% Analysis Date = 03/16/22 Pct Recovery = 87% Analysis Date = 03/12/22 Pct Recovery = 87% Analysis Date = 03/12/22 Pct Recovery = 87% Analysis Date = 03/08/22 Pct Recovery = 87% Analysis Date = 03/08/22 Pct Recovery = 87% Analysis Date = 03/04/22 Pct Recovery = 88% Analysis Date = 03/04/22 Pct Recovery = 88% Analysis Date = 02/27/22 Pct Recovery = 88% Analysis Date = 02/27/22 Pct Recovery = 88% Analysis Date = 02/23/22 Pct Recovery = 88% Analysis Date = 02/23/22 Pct Recovery = 88% Analysis Date = 02/19/22 Pct Recovery = 88% Analysis Date = 02/19/22 Pct Recovery = 88% Analysis Date = 02/14/22 Pct Recovery = 89% Analysis Date = 02/14/22 Pct Recovery = 89% Analysis Date = 02/10/22 Pct Recovery = 89% Analysis Date = 02/10/22 Pct Recovery = 89% Analysis Date = 02/06/22 Pct Recovery = 89% Analysis Date = 02/06/22 Pct Recovery = 89% Analysis Date = 02/02/22 Pct Recovery = 89% Analysis Date = 02/02/22 Pct Recovery = 89% Analysis Date = 01/28/22 Pct Recovery = 90% Analysis Date = 01/28/22 Pct Recovery = 90% Analysis Date = 01/24/22 Pct Recovery = 90% Analysis Date = 01/24/22 Pct Recovery = 90% Analysis Date = 01/20/22 Pct Recovery = 90% Analysis Date = 01/20/22 Pct Recovery = 90% Analysis Date = 01/16/22 Pct Recovery = 91% Analysis Date = 01/16/22 Pct Recovery = 91% Analysis Date = 01/11/22 Pct Recovery = 91% Analysis Date = 01/11/22 Pct Recovery = 91% Analysis Date = 01/07/22 Pct Recovery = 91% Analysis Date = 01/07/22 Pct Recovery = 91% Analysis Date = 01/03/22 Pct Recovery = 92% Analysis Date = 01/03/22 Pct Recovery = 92% Analysis Date = 12/30/21 Pct Recovery = 92% Analysis Date = 12/30/21 Pct Recovery = 92% Analysis Date = 12/25/21 Pct Recovery = 92% Analysis Date = 12/25/21 Pct Recovery = 92% Analysis Date = 12/21/21 Pct Recovery = 93% Analysis Date = 12/21/21 Pct Recovery = 93% Analysis Date = 12/17/21 Pct Recovery = 93% Analysis Date = 12/17/21 Pct Recovery = 93% Analysis Date = 12/12/21 Pct Recovery = 93% Analysis Date = 12/12/21 Pct Recovery = 93% Analysis Date = 12/08/21 Pct Recovery = 94% Analysis Date = 12/08/21 Pct Recovery = 94% Analysis Date = 12/04/21 Pct Recovery = 94% Analysis Date = 12/04/21 Pct Recovery = 94% Analysis Date = 11/30/21 Pct Recovery = 94% Analysis Date = 11/30/21 Pct Recovery = 94% Analysis Date = 11/25/21 Pct Recovery = 94% Analysis Date = 11/25/21 Pct Recovery = 94% Analysis Date = 11/21/21 Pct Recovery = 94% Analysis Date = 11/21/21 Pct Recovery = 94% Analysis Date = 11/17/21 Pct Recovery = 94% Analysis Date = 11/17/21 Pct Recovery = 94% Analysis Date = 11/13/21 Pct Recovery = 94% Analysis Date = 11/13/21 Pct Recovery = 94% Analysis Date = 11/08/21 Pct Recovery = 94% Analysis Date = 11/08/21 Pct Recovery = 94% Analysis Date = 11/04/21 Pct Recovery = 94% Analysis Date = 11/04/21 Pct Recovery = 94% Analysis Date = 10/31/21 Pct Recovery = 94% Analysis Date = 10/31/21 Pct Recovery = 94% Analysis Date = 10/27/21 Pct Recovery = 94% Analysis Date = 10/27/21 Pct Recovery = 94% Analysis Date = 10/22/21 Pct Recovery = 95% Analysis Date = 10/22/21 Pct Recovery = 95% Analysis Date = 10/18/21 Pct Recovery = 95% Analysis Date = 10/18/21 Pct Recovery = 95% Analysis Date = 10/14/21 Pct Recovery = 95% Analysis Date = 10/14/21 Pct Recovery = 95% Analysis Date = 10/10/21 Pct Recovery = 95% Analysis Date = 10/10/21 Pct Recovery = 95% Analysis Date = 10/05/21 Pct Recovery = 95% Analysis Date = 10/05/21 Pct Recovery = 95% Analysis Date = 10/01/21 Pct Recovery = 95% Analysis Date = 10/01/21 Pct Recovery = 95% Analysis Date = 09/27/21 Pct Recovery = 95% Analysis Date = 09/27/21 Pct Recovery = 95% Analysis Date = 09/22/21 Pct Recovery = 95% Analysis Date = 09/22/21 Pct Recovery = 95% Analysis Date = 09/18/21 Pct Recovery = 95% Analysis Date = 09/18/21 Pct Recovery = 95% Analysis Date = 09/14/21 Pct Recovery = 95% Analysis Date = 09/14/21 Pct Recovery = 95% Analysis Date = 09/10/21 Pct Recovery = 95% Analysis Date = 09/10/21 Pct Recovery = 95% Analysis Date = 09/05/21 Pct Recovery = 96% Analysis Date = 09/05/21 Pct Recovery = 96% Analysis Date = 09/01/21 Pct Recovery = 96% Analysis Date = 09/01/21 Pct Recovery = 96% Analysis Date = 08/28/21 Pct Recovery = 96% Analysis Date = 08/28/21 Pct Recovery = 96% Analysis Date = 08/24/21 Pct Recovery = 96% Analysis Date = 08/24/21 Pct Recovery = 96% Analysis Date = 08/19/21 Pct Recovery = 96% Analysis Date = 08/19/21 Pct Recovery = 96% Analysis Date = 08/15/21 Pct Recovery = 96% Analysis Date = 08/15/21 Pct Recovery = 96% Analysis Date = 08/11/21 Pct Recovery = 96% Analysis Date = 08/11/21 Pct Recovery = 96% Analysis Date = 08/07/21 Pct Recovery = 96% Analysis Date = 08/07/21 Pct Recovery = 96% Analysis Date = 08/02/21 Pct Recovery = 96% Analysis Date = 08/02/21 Pct Recovery = 96% Analysis Date = 07/29/21 Pct Recovery = 96% Analysis Date = 07/29/21 Pct Recovery = 96% Analysis Date = 07/25/21 Pct Recovery = 96% Analysis Date = 07/25/21 Pct Recovery = 96% Analysis Date = 07/20/21 Pct Recovery = 96% Analysis Date = 07/20/21 Pct Recovery = 96% Analysis Date = 07/16/21 Pct Recovery = 97% Analysis Date = 07/16/21 Pct Recovery = 97% Analysis Date = 07/12/21 Pct Recovery = 97% Analysis Date = 07/12/21 Pct Recovery = 97% Analysis Date = 07/08/21 Pct Recovery = 97% Analysis Date = 07/08/21 Pct Recovery = 97% Analysis Date = 07/03/21 Pct Recovery = 97% Analysis Date = 07/03/21 Pct Recovery = 97% Analysis Date = 06/29/21 Pct Recovery = 97% Analysis Date = 06/29/21 Pct Recovery = 97% Analysis Date = 06/25/21 Pct Recovery = 97% Analysis Date = 06/25/21 Pct Recovery = 97% Analysis Date = 06/21/21 Pct Recovery = 97% Analysis Date = 06/21/21 Pct Recovery = 97% Analysis Date = 06/16/21 Pct Recovery = 97% Analysis Date = 06/16/21 Pct Recovery = 97% Analysis Date = 06/12/21 Pct Recovery = 97% Analysis Date = 06/12/21 Pct Recovery = 97% Analysis Date = 06/08/21 Pct Recovery = 97% Analysis Date = 06/08/21 Pct Recovery = 97% Analysis Date = 06/04/21 Pct Recovery = 97% Analysis Date = 06/04/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 98% Analysis Date = 05/30/21 Pct Recovery = 98% Analysis Date = 05/26/21 Pct Recovery = 98% Analysis Date = 05/26/21 Pct Recovery = 98% Analysis Date = 05/22/21 Pct Recovery = 98% Analysis Date = 05/22/21 Pct Recovery = 98% Analysis Date = 05/17/21 Pct Recovery = 98% Analysis Date = 05/17/21 Pct Recovery = 98% Analysis Date = 05/13/21 Pct Recovery = 98% Analysis Date = 05/13/21 Pct Recovery = 98% Analysis Date = 05/09/21 Pct Recovery = 98% Analysis Date = 05/09/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 98% Analysis Date = 04/30/21 Pct Recovery = 98% Analysis Date = 04/30/21 Pct Recovery = 98% Analysis Date = 04/26/21 Pct Recovery = 98% Analysis Date = 04/26/21 Pct Recovery = 98% Analysis Date = 04/22/21 Pct Recovery = 98% Analysis Date = 04/22/21 Pct Recovery = 98% Analysis Date = 04/18/21 Pct Recovery = 98% Analysis Date = 04/18/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 99% Analysis Date = 04/13/21 Pct Recovery = 99% Analysis Date = 04/09/21 Pct Recovery = 99% Analysis Date = 04/09/21 Pct Recovery = 99% Analysis Date = 04/05/21 Pct Recovery = 99% Analysis Date = 04/05/21 Pct Recovery = 99% Analysis Date = 04/01/21 Pct Recovery = 100% Analysis Date = 04/01/21 Pct Recovery = 100% Analysis Date = 03/27/21 Pct Recovery = 100% Analysis Date = 03/27/21 Pct Recovery = 100% Analysis Date = 03/23/21 Pct Recovery = 101% Analysis Date = 03/23/21 Pct Recovery = 101% Analysis Date = 03/19/21 Pct Recovery = 101% Analysis Date = 03/19/21 Pct Recovery = 101% Analysis Date = 03/15/21 Pct Recovery = 102% Analysis Date = 03/15/21 Pct Recovery = 102% Analysis Date = 03/10/21 Pct Recovery = 103% Analysis Date = 03/10/21 Pct Recovery = 103% Analysis Date = 03/06/21 Pct Recovery = 103% Analysis Date = 03/06/21 Pct Recovery = 103% Analysis Date = 03/02/21 Pct Recovery = 103% Analysis Date = 03/02/21 Pct Recovery = 103% Analysis Date = 02/25/21 Pct Recovery = 104% Analysis Date = 02/25/21 Pct Recovery = 104% Analysis Date = 02/21/21 Pct Recovery = 104% Analysis Date = 02/21/21 Pct Recovery = 104% Analysis Date = 02/17/21 Pct Recovery = 104% Analysis Date = 02/17/21 Pct Recovery = 104% Analysis Date = 02/13/21 Pct Recovery = 105% Analysis Date = 02/13/21 Pct Recovery = 105% Analysis Date = 02/08/21 Pct Recovery = 105% Analysis Date = 02/08/21 Pct Recovery = 105% Analysis Date = 02/04/21 Pct Recovery = 106% Analysis Date = 02/04/21 Pct Recovery = 106% Analysis Date = 01/31/21 Pct Recovery = 106% Analysis Date = 01/31/21 Pct Recovery = 106% Analysis Date = 01/27/21 Pct Recovery = 106% Analysis Date = 01/27/21 Pct Recovery = 106% Analysis Date = 01/22/21 Pct Recovery = 107% Analysis Date = 01/22/21 Pct Recovery = 107% Analysis Date = 01/18/21 Pct Recovery = 107% Analysis Date = 01/18/21 Pct Recovery = 107% Analysis Date = 01/14/21 Pct Recovery = 107% Analysis Date = 01/14/21 Pct Recovery = 107% Analysis Date = 01/10/21 Pct Recovery = 108% Analysis Date = 01/10/21 Pct Recovery = 108% Analysis Date = 01/05/21 Pct Recovery = 108% Analysis Date = 01/05/21 Pct Recovery = 108% Analysis Date = 01/01/21 Pct Recovery = 108% Analysis Date = 01/01/21 Pct Recovery = 108% Analysis Date = 12/28/20 Pct Recovery = 108% Analysis Date = 12/28/20 Pct Recovery = 108% Analysis Date = 12/23/20 Pct Recovery = 109% Analysis Date = 12/23/20 Pct Recovery = 109% Analysis Date = 12/19/20 Pct Recovery = 109% Analysis Date = 12/19/20 Pct Recovery = 109% Analysis Date = 12/15/20 Pct Recovery = 109% Analysis Date = 12/15/20 Pct Recovery = 109% Analysis Date = 12/11/20 Pct Recovery = 110% Analysis Date = 12/11/20 Pct Recovery = 110% Analysis Date = 12/06/20 Pct Recovery = 110% Analysis Date = 12/06/20 Pct Recovery = 110% Analysis Date = 12/02/20 Pct Recovery = 110% Analysis Date = 12/02/20 Pct Recovery = 110% Analysis Date = 11/28/20 Pct Recovery = 110% Analysis Date = 11/28/20 Pct Recovery = 110% Analysis Date = 11/24/20 Pct Recovery = 110% Analysis Date = 11/24/20 Pct Recovery = 110% Analysis Date = 11/19/20 Pct Recovery = 110% Analysis Date = 11/19/20 Pct Recovery = 110% Analysis Date = 11/15/20 Pct Recovery = 110% Analysis Date = 11/15/20 Pct Recovery = 110% Analysis Date = 11/11/20 Pct Recovery = 111% Analysis Date = 11/11/20 Pct Recovery = 111% Analysis Date = 11/07/20 Pct Recovery = 111% Analysis Date = 11/07/20 Pct Recovery = 111% Analysis Date = 11/02/20 Pct Recovery = 111% Analysis Date = 11/02/20 Pct Recovery = 111% Analysis Date = 10/29/20 Pct Recovery = 111% Analysis Date = 10/29/20 Pct Recovery = 111% Analysis Date = 10/25/20 Pct Recovery = 111% Analysis Date = 10/25/20 Pct Recovery = 111% Analysis Date = 10/21/20 Pct Recovery = 111% Analysis Date = 10/21/20 Pct Recovery = 111% Analysis Date = 10/16/20 Pct Recovery = 112% Analysis Date = 10/16/20 Pct Recovery = 112% Analysis Date = 10/12/20 Pct Recovery = 112% Analysis Date = 10/12/20 Pct Recovery = 112% Analysis Date = 10/08/20 Pct Recovery = 112% Analysis Date = 10/08/20 Pct Recovery = 112% Analysis Date = 10/03/20 Pct Recovery = 112% Analysis Date = 10/03/20 Pct Recovery = 112% Analysis Date = 09/29/20 Pct Recovery = 112% Analysis Date = 09/29/20 Pct Recovery = 112% Analysis Date = 09/25/20 Pct Recovery = 112% Analysis Date = 09/25/20 Pct Recovery = 112% Analysis Date = 09/21/20 Pct Recovery = 113% Analysis Date = 09/21/20 Pct Recovery = 113% Analysis Date = 09/16/20 Pct Recovery = 113% Analysis Date = 09/16/20 Pct Recovery = 113% Analysis Date = 09/12/20 Pct Recovery = 113% Analysis Date = 09/12/20 Pct Recovery = 113% Analysis Date = 09/08/20 Pct Recovery = 113% Analysis Date = 09/08/20 Pct Recovery = 113% Analysis Date = 09/04/20 Pct Recovery = 113% Analysis Date = 09/04/20 Pct Recovery = 113% Analysis Date = 08/30/20 Pct Recovery = 114% Analysis Date = 08/30/20 Pct Recovery = 114% Analysis Date = 08/26/20 Pct Recovery = 114% Analysis Date = 08/26/20 Pct Recovery = 114% Analysis Date = 08/22/20 Pct Recovery = 114% Analysis Date = 08/22/20 Pct Recovery = 114% Analysis Date = 08/18/20 Pct Recovery = 114% Analysis Date = 08/18/20 Pct Recovery = 114% Analysis Date = 08/13/20 Pct Recovery = 115% Analysis Date = 08/13/20 Pct Recovery = 115% Analysis Date = 08/09/20 Pct Recovery = 115% Analysis Date = 08/09/20 Pct Recovery = 115% Analysis Date = 08/05/20 Pct Recovery = 115% Analysis Date = 08/05/20 Pct Recovery = 115% Analysis Date = 07/31/20 Pct Recovery = 115% Analysis Date = 07/31/20 Pct Recovery = 115% Analysis Date = 07/27/20 Pct Recovery = 115% Analysis Date = 07/27/20 Pct Recovery = 115% Analysis Date = 07/23/20 Pct Recovery = 116% Analysis Date = 07/23/20 Pct Recovery = 116% Analysis Date = 07/19/20 Pct Recovery = 116% Analysis Date = 07/19/20 Pct Recovery = 116% Analysis Date = 07/14/20 Pct Recovery = 116% Analysis Date = 07/14/20 Pct Recovery = 116% Analysis Date = 07/10/20 Pct Recovery = 116% Analysis Date = 07/10/20 Pct Recovery = 116% Analysis Date = 07/06/20 Pct Recovery = 117% Analysis Date = 07/06/20 Pct Recovery = 117% Analysis Date = 07/02/20 Pct Recovery = 117% Analysis Date = 07/02/20 Pct Recovery = 117% Analysis Date = 06/27/20 Pct Recovery = 117% Analysis Date = 06/27/20 Pct Recovery = 117% Analysis Date = 06/23/20 Pct Recovery = 117% Analysis Date = 06/23/20 Pct Recovery = 117% Analysis Date = 06/19/20 Pct Recovery = 118% Analysis Date = 06/19/20 Pct Recovery = 118% Analysis Date = 06/15/20 Pct Recovery = 118% Analysis Date = 06/15/20 Pct Recovery = 118% Analysis Date = 06/10/20 Pct Recovery = 118% Analysis Date = 06/10/20 Pct Recovery = 118% Analysis Date = 06/06/20 Pct Recovery = 118% Analysis Date = 06/06/20 Pct Recovery = 118% Analysis Date = 06/02/20 Pct Recovery = 119% Analysis Date = 06/02/20 Pct Recovery = 119% Analysis Date = 05/29/20 Pct Recovery = 119% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPOXUR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 44 102% 31% 100% 28%
Total 44 102% 31% 100% 28%

Sample Statistics
PROPOXUR

Characteristic N % % Basis
Plotted 44 100% Spiked
Estimated Values 4 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 44 .  
False Negatives 0 0% 0 out of 44
Not Spiked 72 .  
False Positives 0 0% 0 out of 72

OBSP Determination:
PYRACLOSTROBIN
METHOD: 2447 , TESTIDCODE: 66646LCM60

Laboratory ID = 20201820155 Lab Value = 29.106 Expected Conc. = 30.6 Report level label = 2.4 Pct Recovery = 95% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 29.181 Expected Conc. = 30.6 Report level label = 2.4 Pct Recovery = 95% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203230021 Lab Value = 22.008 Expected Conc. = 30.05 Report level label = 2.4 Pct Recovery = 73% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 17.781 Expected Conc. = 30.05 Report level label = 2.4 Pct Recovery = 59% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 29.922 Expected Conc. = 30 Report level label = 2.4 Pct Recovery = 100% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 29.612 Expected Conc. = 30 Report level label = 2.4 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 35.309 Expected Conc. = 30 Report level label = 2.4 Pct Recovery = 118% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20221520237 Lab Value = 18.815 Expected Conc. = 24.32 Report level label = 2.4 Pct Recovery = 77% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 16.107 Expected Conc. = 24 Report level label = 2.4 Pct Recovery = 67% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 16.807 Expected Conc. = 23.96 Report level label = 2.4 Pct Recovery = 70% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20202530029 Lab Value = 12.218 Expected Conc. = 15.3 Report level label = 2.4 Pct Recovery = 80% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 11.383 Expected Conc. = 15.3 Report level label = 2.4 Pct Recovery = 74% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 16.719 Expected Conc. = 15.3 Report level label = 2.4 Pct Recovery = 109% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20221870197 Lab Value = 10.743 Expected Conc. = 15.2 Report level label = 2.4 Pct Recovery = 71% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20203230018 Lab Value = 9.145 Expected Conc. = 15 Report level label = 2.4 Pct Recovery = 61% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 11.028 Expected Conc. = 15 Report level label = 2.4 Pct Recovery = 74% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 13.320 Expected Conc. = 15 Report level label = 2.4 Pct Recovery = 89% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201960104 Lab Value = 14.961 Expected Conc. = 15 Report level label = 2.4 Pct Recovery = 100% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20220740064 Lab Value = 9.461 Expected Conc. = 14.975 Report level label = 2.4 Pct Recovery = 63% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202180001 Lab Value = 4.301 Expected Conc. = 6.12 Report level label = 2.4 Pct Recovery = 70% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 6.138 Expected Conc. = 6.12 Report level label = 2.4 Pct Recovery = 100% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20221660151 Lab Value = 4.949 Expected Conc. = 6.08 Report level label = 2.4 Pct Recovery = 81% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210830019 Lab Value = 7.004 Expected Conc. = 6.01 Report level label = 2.4 Pct Recovery = 117% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 4.160 Expected Conc. = 6.01 Report level label = 2.4 Pct Recovery = 69% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 4.699 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 78% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 4.719 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 79% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 5.173 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 86% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 5.878 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 98% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 5.217 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 87% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 6.199 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 103% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201610160 Lab Value = 6.228 Expected Conc. = 6 Report level label = 2.4 Pct Recovery = 104% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Analysis Date = 08/15/22 Pct Recovery = 71% Analysis Date = 08/10/22 Pct Recovery = 71% Analysis Date = 08/10/22 Pct Recovery = 71% Analysis Date = 08/06/22 Pct Recovery = 71% Analysis Date = 08/06/22 Pct Recovery = 71% Analysis Date = 08/02/22 Pct Recovery = 71% Analysis Date = 08/02/22 Pct Recovery = 71% Analysis Date = 07/29/22 Pct Recovery = 71% Analysis Date = 07/29/22 Pct Recovery = 71% Analysis Date = 07/25/22 Pct Recovery = 71% Analysis Date = 07/25/22 Pct Recovery = 71% Analysis Date = 07/21/22 Pct Recovery = 71% Analysis Date = 07/21/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 72% Analysis Date = 07/17/22 Pct Recovery = 72% Analysis Date = 07/13/22 Pct Recovery = 72% Analysis Date = 07/13/22 Pct Recovery = 72% Analysis Date = 07/09/22 Pct Recovery = 72% Analysis Date = 07/09/22 Pct Recovery = 72% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 07/05/22 Pct Recovery = 72% Analysis Date = 07/01/22 Pct Recovery = 72% Analysis Date = 07/01/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/26/22 Pct Recovery = 72% Analysis Date = 06/22/22 Pct Recovery = 72% Analysis Date = 06/22/22 Pct Recovery = 72% Analysis Date = 06/18/22 Pct Recovery = 72% Analysis Date = 06/18/22 Pct Recovery = 72% Analysis Date = 06/14/22 Pct Recovery = 72% Analysis Date = 06/14/22 Pct Recovery = 72% Analysis Date = 06/10/22 Pct Recovery = 72% Analysis Date = 06/10/22 Pct Recovery = 72% Analysis Date = 06/06/22 Pct Recovery = 72% Analysis Date = 06/06/22 Pct Recovery = 72% Analysis Date = 06/02/22 Pct Recovery = 72% Analysis Date = 06/02/22 Pct Recovery = 72% Analysis Date = 05/29/22 Pct Recovery = 72% Analysis Date = 05/29/22 Pct Recovery = 72% Analysis Date = 05/25/22 Pct Recovery = 73% Analysis Date = 05/25/22 Pct Recovery = 73% Analysis Date = 05/21/22 Pct Recovery = 73% Analysis Date = 05/21/22 Pct Recovery = 73% Analysis Date = 05/17/22 Pct Recovery = 73% Analysis Date = 05/17/22 Pct Recovery = 73% Analysis Date = 05/12/22 Pct Recovery = 73% Analysis Date = 05/12/22 Pct Recovery = 73% Analysis Date = 05/08/22 Pct Recovery = 73% Analysis Date = 05/08/22 Pct Recovery = 73% Analysis Date = 05/04/22 Pct Recovery = 73% Analysis Date = 05/04/22 Pct Recovery = 73% Analysis Date = 04/30/22 Pct Recovery = 73% Analysis Date = 04/30/22 Pct Recovery = 73% Analysis Date = 04/26/22 Pct Recovery = 73% Analysis Date = 04/26/22 Pct Recovery = 73% Analysis Date = 04/22/22 Pct Recovery = 73% Analysis Date = 04/22/22 Pct Recovery = 73% Analysis Date = 04/18/22 Pct Recovery = 73% Analysis Date = 04/18/22 Pct Recovery = 73% Analysis Date = 04/14/22 Pct Recovery = 73% Analysis Date = 04/14/22 Pct Recovery = 73% Analysis Date = 04/10/22 Pct Recovery = 74% Analysis Date = 04/10/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 74% Analysis Date = 04/06/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 03/28/22 Pct Recovery = 74% Analysis Date = 03/28/22 Pct Recovery = 74% Analysis Date = 03/24/22 Pct Recovery = 74% Analysis Date = 03/24/22 Pct Recovery = 74% Analysis Date = 03/20/22 Pct Recovery = 74% Analysis Date = 03/20/22 Pct Recovery = 74% Analysis Date = 03/16/22 Pct Recovery = 74% Analysis Date = 03/16/22 Pct Recovery = 74% Analysis Date = 03/12/22 Pct Recovery = 74% Analysis Date = 03/12/22 Pct Recovery = 74% Analysis Date = 03/08/22 Pct Recovery = 74% Analysis Date = 03/08/22 Pct Recovery = 74% Analysis Date = 03/04/22 Pct Recovery = 74% Analysis Date = 03/04/22 Pct Recovery = 74% Analysis Date = 02/28/22 Pct Recovery = 74% Analysis Date = 02/28/22 Pct Recovery = 74% Analysis Date = 02/24/22 Pct Recovery = 74% Analysis Date = 02/24/22 Pct Recovery = 74% Analysis Date = 02/20/22 Pct Recovery = 75% Analysis Date = 02/20/22 Pct Recovery = 75% Analysis Date = 02/16/22 Pct Recovery = 75% Analysis Date = 02/16/22 Pct Recovery = 75% Analysis Date = 02/11/22 Pct Recovery = 75% Analysis Date = 02/11/22 Pct Recovery = 75% Analysis Date = 02/07/22 Pct Recovery = 75% Analysis Date = 02/07/22 Pct Recovery = 75% Analysis Date = 02/03/22 Pct Recovery = 75% Analysis Date = 02/03/22 Pct Recovery = 75% Analysis Date = 01/30/22 Pct Recovery = 75% Analysis Date = 01/30/22 Pct Recovery = 75% Analysis Date = 01/26/22 Pct Recovery = 75% Analysis Date = 01/26/22 Pct Recovery = 75% Analysis Date = 01/22/22 Pct Recovery = 75% Analysis Date = 01/22/22 Pct Recovery = 75% Analysis Date = 01/18/22 Pct Recovery = 75% Analysis Date = 01/18/22 Pct Recovery = 75% Analysis Date = 01/14/22 Pct Recovery = 75% Analysis Date = 01/14/22 Pct Recovery = 75% Analysis Date = 01/10/22 Pct Recovery = 75% Analysis Date = 01/10/22 Pct Recovery = 75% Analysis Date = 01/06/22 Pct Recovery = 75% Analysis Date = 01/06/22 Pct Recovery = 75% Analysis Date = 01/02/22 Pct Recovery = 76% Analysis Date = 01/02/22 Pct Recovery = 76% Analysis Date = 12/28/21 Pct Recovery = 76% Analysis Date = 12/28/21 Pct Recovery = 76% Analysis Date = 12/24/21 Pct Recovery = 76% Analysis Date = 12/24/21 Pct Recovery = 76% Analysis Date = 12/20/21 Pct Recovery = 76% Analysis Date = 12/20/21 Pct Recovery = 76% Analysis Date = 12/16/21 Pct Recovery = 76% Analysis Date = 12/16/21 Pct Recovery = 76% Analysis Date = 12/12/21 Pct Recovery = 76% Analysis Date = 12/12/21 Pct Recovery = 76% Analysis Date = 12/08/21 Pct Recovery = 76% Analysis Date = 12/08/21 Pct Recovery = 76% Analysis Date = 12/04/21 Pct Recovery = 76% Analysis Date = 12/04/21 Pct Recovery = 76% Analysis Date = 11/30/21 Pct Recovery = 76% Analysis Date = 11/30/21 Pct Recovery = 76% Analysis Date = 11/26/21 Pct Recovery = 76% Analysis Date = 11/26/21 Pct Recovery = 76% Analysis Date = 11/22/21 Pct Recovery = 76% Analysis Date = 11/22/21 Pct Recovery = 76% Analysis Date = 11/18/21 Pct Recovery = 77% Analysis Date = 11/18/21 Pct Recovery = 77% Analysis Date = 11/13/21 Pct Recovery = 77% Analysis Date = 11/13/21 Pct Recovery = 77% Analysis Date = 11/09/21 Pct Recovery = 77% Analysis Date = 11/09/21 Pct Recovery = 77% Analysis Date = 11/05/21 Pct Recovery = 77% Analysis Date = 11/05/21 Pct Recovery = 77% Analysis Date = 11/01/21 Pct Recovery = 77% Analysis Date = 11/01/21 Pct Recovery = 77% Analysis Date = 10/28/21 Pct Recovery = 77% Analysis Date = 10/28/21 Pct Recovery = 77% Analysis Date = 10/24/21 Pct Recovery = 77% Analysis Date = 10/24/21 Pct Recovery = 77% Analysis Date = 10/20/21 Pct Recovery = 77% Analysis Date = 10/20/21 Pct Recovery = 77% Analysis Date = 10/16/21 Pct Recovery = 77% Analysis Date = 10/16/21 Pct Recovery = 77% Analysis Date = 10/12/21 Pct Recovery = 77% Analysis Date = 10/12/21 Pct Recovery = 77% Analysis Date = 10/08/21 Pct Recovery = 77% Analysis Date = 10/08/21 Pct Recovery = 77% Analysis Date = 10/04/21 Pct Recovery = 77% Analysis Date = 10/04/21 Pct Recovery = 77% Analysis Date = 09/29/21 Pct Recovery = 78% Analysis Date = 09/29/21 Pct Recovery = 78% Analysis Date = 09/25/21 Pct Recovery = 78% Analysis Date = 09/25/21 Pct Recovery = 78% Analysis Date = 09/21/21 Pct Recovery = 78% Analysis Date = 09/21/21 Pct Recovery = 78% Analysis Date = 09/17/21 Pct Recovery = 78% Analysis Date = 09/17/21 Pct Recovery = 78% Analysis Date = 09/13/21 Pct Recovery = 78% Analysis Date = 09/13/21 Pct Recovery = 78% Analysis Date = 09/09/21 Pct Recovery = 78% Analysis Date = 09/09/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 78% Analysis Date = 09/01/21 Pct Recovery = 78% Analysis Date = 09/01/21 Pct Recovery = 78% Analysis Date = 08/28/21 Pct Recovery = 78% Analysis Date = 08/28/21 Pct Recovery = 78% Analysis Date = 08/24/21 Pct Recovery = 78% Analysis Date = 08/24/21 Pct Recovery = 78% Analysis Date = 08/20/21 Pct Recovery = 78% Analysis Date = 08/20/21 Pct Recovery = 78% Analysis Date = 08/15/21 Pct Recovery = 78% Analysis Date = 08/15/21 Pct Recovery = 78% Analysis Date = 08/11/21 Pct Recovery = 79% Analysis Date = 08/11/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/26/21 Pct Recovery = 79% Analysis Date = 07/26/21 Pct Recovery = 79% Analysis Date = 07/22/21 Pct Recovery = 79% Analysis Date = 07/22/21 Pct Recovery = 79% Analysis Date = 07/18/21 Pct Recovery = 79% Analysis Date = 07/18/21 Pct Recovery = 79% Analysis Date = 07/14/21 Pct Recovery = 79% Analysis Date = 07/14/21 Pct Recovery = 79% Analysis Date = 07/10/21 Pct Recovery = 79% Analysis Date = 07/10/21 Pct Recovery = 79% Analysis Date = 07/06/21 Pct Recovery = 79% Analysis Date = 07/06/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 06/27/21 Pct Recovery = 80% Analysis Date = 06/27/21 Pct Recovery = 80% Analysis Date = 06/23/21 Pct Recovery = 80% Analysis Date = 06/23/21 Pct Recovery = 80% Analysis Date = 06/19/21 Pct Recovery = 80% Analysis Date = 06/19/21 Pct Recovery = 80% Analysis Date = 06/15/21 Pct Recovery = 80% Analysis Date = 06/15/21 Pct Recovery = 80% Analysis Date = 06/11/21 Pct Recovery = 80% Analysis Date = 06/11/21 Pct Recovery = 80% Analysis Date = 06/07/21 Pct Recovery = 80% Analysis Date = 06/07/21 Pct Recovery = 80% Analysis Date = 06/03/21 Pct Recovery = 80% Analysis Date = 06/03/21 Pct Recovery = 80% Analysis Date = 05/30/21 Pct Recovery = 80% Analysis Date = 05/30/21 Pct Recovery = 80% Analysis Date = 05/26/21 Pct Recovery = 80% Analysis Date = 05/26/21 Pct Recovery = 80% Analysis Date = 05/22/21 Pct Recovery = 80% Analysis Date = 05/22/21 Pct Recovery = 80% Analysis Date = 05/18/21 Pct Recovery = 80% Analysis Date = 05/18/21 Pct Recovery = 80% Analysis Date = 05/13/21 Pct Recovery = 80% Analysis Date = 05/13/21 Pct Recovery = 80% Analysis Date = 05/09/21 Pct Recovery = 81% Analysis Date = 05/09/21 Pct Recovery = 81% Analysis Date = 05/05/21 Pct Recovery = 81% Analysis Date = 05/05/21 Pct Recovery = 81% Analysis Date = 05/01/21 Pct Recovery = 81% Analysis Date = 05/01/21 Pct Recovery = 81% Analysis Date = 04/27/21 Pct Recovery = 81% Analysis Date = 04/27/21 Pct Recovery = 81% Analysis Date = 04/23/21 Pct Recovery = 81% Analysis Date = 04/23/21 Pct Recovery = 81% Analysis Date = 04/19/21 Pct Recovery = 81% Analysis Date = 04/19/21 Pct Recovery = 81% Analysis Date = 04/15/21 Pct Recovery = 81% Analysis Date = 04/15/21 Pct Recovery = 81% Analysis Date = 04/11/21 Pct Recovery = 81% Analysis Date = 04/11/21 Pct Recovery = 81% Analysis Date = 04/07/21 Pct Recovery = 81% Analysis Date = 04/07/21 Pct Recovery = 81% Analysis Date = 04/03/21 Pct Recovery = 81% Analysis Date = 04/03/21 Pct Recovery = 81% Analysis Date = 03/29/21 Pct Recovery = 81% Analysis Date = 03/29/21 Pct Recovery = 81% Analysis Date = 03/25/21 Pct Recovery = 81% Analysis Date = 03/25/21 Pct Recovery = 81% Analysis Date = 03/21/21 Pct Recovery = 81% Analysis Date = 03/21/21 Pct Recovery = 81% Analysis Date = 03/17/21 Pct Recovery = 81% Analysis Date = 03/17/21 Pct Recovery = 81% Analysis Date = 03/13/21 Pct Recovery = 81% Analysis Date = 03/13/21 Pct Recovery = 81% Analysis Date = 03/09/21 Pct Recovery = 81% Analysis Date = 03/09/21 Pct Recovery = 81% Analysis Date = 03/05/21 Pct Recovery = 80% Analysis Date = 03/05/21 Pct Recovery = 80% Analysis Date = 03/01/21 Pct Recovery = 80% Analysis Date = 03/01/21 Pct Recovery = 80% Analysis Date = 02/25/21 Pct Recovery = 80% Analysis Date = 02/25/21 Pct Recovery = 80% Analysis Date = 02/21/21 Pct Recovery = 80% Analysis Date = 02/21/21 Pct Recovery = 80% Analysis Date = 02/17/21 Pct Recovery = 80% Analysis Date = 02/17/21 Pct Recovery = 80% Analysis Date = 02/12/21 Pct Recovery = 80% Analysis Date = 02/12/21 Pct Recovery = 80% Analysis Date = 02/08/21 Pct Recovery = 80% Analysis Date = 02/08/21 Pct Recovery = 80% Analysis Date = 02/04/21 Pct Recovery = 79% Analysis Date = 02/04/21 Pct Recovery = 79% Analysis Date = 01/31/21 Pct Recovery = 79% Analysis Date = 01/31/21 Pct Recovery = 79% Analysis Date = 01/27/21 Pct Recovery = 79% Analysis Date = 01/27/21 Pct Recovery = 79% Analysis Date = 01/23/21 Pct Recovery = 79% Analysis Date = 01/23/21 Pct Recovery = 79% Analysis Date = 01/19/21 Pct Recovery = 79% Analysis Date = 01/19/21 Pct Recovery = 79% Analysis Date = 01/15/21 Pct Recovery = 79% Analysis Date = 01/15/21 Pct Recovery = 79% Analysis Date = 01/11/21 Pct Recovery = 80% Analysis Date = 01/11/21 Pct Recovery = 80% Analysis Date = 01/07/21 Pct Recovery = 80% Analysis Date = 01/07/21 Pct Recovery = 80% Analysis Date = 01/03/21 Pct Recovery = 80% Analysis Date = 01/03/21 Pct Recovery = 80% Analysis Date = 12/29/20 Pct Recovery = 80% Analysis Date = 12/29/20 Pct Recovery = 80% Analysis Date = 12/25/20 Pct Recovery = 80% Analysis Date = 12/25/20 Pct Recovery = 80% Analysis Date = 12/21/20 Pct Recovery = 80% Analysis Date = 12/21/20 Pct Recovery = 80% Analysis Date = 12/17/20 Pct Recovery = 81% Analysis Date = 12/17/20 Pct Recovery = 81% Analysis Date = 12/13/20 Pct Recovery = 81% Analysis Date = 12/13/20 Pct Recovery = 81% Analysis Date = 12/09/20 Pct Recovery = 82% Analysis Date = 12/09/20 Pct Recovery = 82% Analysis Date = 12/05/20 Pct Recovery = 83% Analysis Date = 12/05/20 Pct Recovery = 83% Analysis Date = 12/01/20 Pct Recovery = 84% Analysis Date = 12/01/20 Pct Recovery = 84% Analysis Date = 11/27/20 Pct Recovery = 84% Analysis Date = 11/27/20 Pct Recovery = 84% Analysis Date = 11/23/20 Pct Recovery = 85% Analysis Date = 11/23/20 Pct Recovery = 85% Analysis Date = 11/19/20 Pct Recovery = 86% Analysis Date = 11/19/20 Pct Recovery = 86% Analysis Date = 11/14/20 Pct Recovery = 87% Analysis Date = 11/14/20 Pct Recovery = 87% Analysis Date = 11/10/20 Pct Recovery = 88% Analysis Date = 11/10/20 Pct Recovery = 88% Analysis Date = 11/06/20 Pct Recovery = 89% Analysis Date = 11/06/20 Pct Recovery = 89% Analysis Date = 11/02/20 Pct Recovery = 90% Analysis Date = 11/02/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/29/20 Pct Recovery = 90% Analysis Date = 10/25/20 Pct Recovery = 91% Analysis Date = 10/25/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/21/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 91% Analysis Date = 10/17/20 Pct Recovery = 91% Analysis Date = 10/13/20 Pct Recovery = 91% Analysis Date = 10/13/20 Pct Recovery = 91% Analysis Date = 10/09/20 Pct Recovery = 91% Analysis Date = 10/09/20 Pct Recovery = 91% Analysis Date = 10/05/20 Pct Recovery = 92% Analysis Date = 10/05/20 Pct Recovery = 92% Analysis Date = 09/30/20 Pct Recovery = 92% Analysis Date = 09/30/20 Pct Recovery = 92% Analysis Date = 09/26/20 Pct Recovery = 92% Analysis Date = 09/26/20 Pct Recovery = 92% Analysis Date = 09/22/20 Pct Recovery = 92% Analysis Date = 09/22/20 Pct Recovery = 92% Analysis Date = 09/18/20 Pct Recovery = 93% Analysis Date = 09/18/20 Pct Recovery = 93% Analysis Date = 09/14/20 Pct Recovery = 93% Analysis Date = 09/14/20 Pct Recovery = 93% Analysis Date = 09/10/20 Pct Recovery = 93% Analysis Date = 09/10/20 Pct Recovery = 93% Analysis Date = 09/06/20 Pct Recovery = 93% Analysis Date = 09/06/20 Pct Recovery = 93% Analysis Date = 09/02/20 Pct Recovery = 93% Analysis Date = 09/02/20 Pct Recovery = 93% Analysis Date = 08/29/20 Pct Recovery = 94% Analysis Date = 08/29/20 Pct Recovery = 94% Analysis Date = 08/25/20 Pct Recovery = 94% Analysis Date = 08/25/20 Pct Recovery = 94% Analysis Date = 08/21/20 Pct Recovery = 94% Analysis Date = 08/21/20 Pct Recovery = 94% Analysis Date = 08/16/20 Pct Recovery = 95% Analysis Date = 08/16/20 Pct Recovery = 95% Analysis Date = 08/12/20 Pct Recovery = 95% Analysis Date = 08/12/20 Pct Recovery = 95% Analysis Date = 08/08/20 Pct Recovery = 95% Analysis Date = 08/08/20 Pct Recovery = 95% Analysis Date = 08/04/20 Pct Recovery = 95% Analysis Date = 08/04/20 Pct Recovery = 95% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 96% Analysis Date = 07/23/20 Pct Recovery = 96% Analysis Date = 07/23/20 Pct Recovery = 96% Analysis Date = 07/19/20 Pct Recovery = 97% Analysis Date = 07/19/20 Pct Recovery = 97% Analysis Date = 07/15/20 Pct Recovery = 97% Analysis Date = 07/15/20 Pct Recovery = 97% Analysis Date = 07/11/20 Pct Recovery = 97% Analysis Date = 07/11/20 Pct Recovery = 97% Analysis Date = 07/07/20 Pct Recovery = 98% Analysis Date = 07/07/20 Pct Recovery = 98% Analysis Date = 07/02/20 Pct Recovery = 98% Analysis Date = 07/02/20 Pct Recovery = 98% Analysis Date = 06/28/20 Pct Recovery = 98% Analysis Date = 06/28/20 Pct Recovery = 98% Analysis Date = 06/24/20 Pct Recovery = 99% Analysis Date = 06/24/20 Pct Recovery = 99% Analysis Date = 06/20/20 Pct Recovery = 99% Analysis Date = 06/20/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/12/20 Pct Recovery = 100% Analysis Date = 06/12/20 Pct Recovery = 100% Analysis Date = 06/08/20 Pct Recovery = 100% Analysis Date = 06/08/20 Pct Recovery = 100% Analysis Date = 06/04/20 Pct Recovery = 101% Analysis Date = 06/04/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/31/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/27/20 Pct Recovery = 101% Analysis Date = 05/23/20 Pct Recovery = 102% Analysis Date = 05/23/20 Pct Recovery = 102% Analysis Date = 05/19/20 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PYRACLOSTROBIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 85% 16% 81% 22%
Total 31 85% 16% 81% 22%

Sample Statistics
PYRACLOSTROBIN

Characteristic N % % Basis
Plotted 31 97% Spiked
Estimated Values 4 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 1 3% 1 out of 32
Not Spiked 84 .  
False Positives 0 0% 0 out of 84

OBSP Determination:
SIMAZINE
METHOD: 2447 , TESTIDCODE: 65105LCM60

Laboratory ID = 20201820155 Lab Value = 77.812 Expected Conc. = 90.3 Report level label = 7.2 Pct Recovery = 86% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 93.204 Expected Conc. = 90.3 Report level label = 7.2 Pct Recovery = 103% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203080100 Lab Value = 86.698 Expected Conc. = 90.1 Report level label = 7.2 Pct Recovery = 96% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 80.407 Expected Conc. = 90.1 Report level label = 7.2 Pct Recovery = 89% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 69.611 Expected Conc. = 90.1 Report level label = 7.2 Pct Recovery = 77% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202390020 Lab Value = 97.093 Expected Conc. = 90.1 Report level label = 7.2 Pct Recovery = 108% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20210760015 Lab Value = 82.030 Expected Conc. = 89.58 Report level label = 7.2 Pct Recovery = 92% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 71.123 Expected Conc. = 89.58 Report level label = 7.2 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 62.317 Expected Conc. = 89.58 Report level label = 7.2 Pct Recovery = 70% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 80.777 Expected Conc. = 89.58 Report level label = 7.2 Pct Recovery = 90% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221520237 Lab Value = 63.696 Expected Conc. = 72.28 Report level label = 7.2 Pct Recovery = 88% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 51.859 Expected Conc. = 72 Report level label = 7.2 Pct Recovery = 72% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 29.207 Expected Conc. = 70.8 Report level label = 7.2 Pct Recovery = 41% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20220740064 Lab Value = 16.327 Expected Conc. = 45.25 Report level label = 7.2 Pct Recovery = 36% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20221870197 Lab Value = 30.282 Expected Conc. = 45.175 Report level label = 7.2 Pct Recovery = 67% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20202530029 Lab Value = 45.585 Expected Conc. = 45.15 Report level label = 7.2 Pct Recovery = 101% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 37.533 Expected Conc. = 45.15 Report level label = 7.2 Pct Recovery = 83% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 39.904 Expected Conc. = 45.15 Report level label = 7.2 Pct Recovery = 88% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202880004 Lab Value = 48.033 Expected Conc. = 45.05 Report level label = 7.2 Pct Recovery = 107% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201960104 Lab Value = 56.488 Expected Conc. = 45.05 Report level label = 7.2 Pct Recovery = 125% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20210480001 Lab Value = 41.432 Expected Conc. = 44.79 Report level label = 7.2 Pct Recovery = 93% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 26.068 Expected Conc. = 36.04 Report level label = 7.2 Pct Recovery = 72% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 32.428 Expected Conc. = 36.04 Report level label = 7.2 Pct Recovery = 90% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 33.802 Expected Conc. = 35.832 Report level label = 7.2 Pct Recovery = 94% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221660151 Lab Value = 14.640 Expected Conc. = 18.07 Report level label = 7.2 Pct Recovery = 81% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20202180001 Lab Value = 14.438 Expected Conc. = 18.06 Report level label = 7.2 Pct Recovery = 80% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 27.118 Expected Conc. = 18.06 Report level label = 7.2 Pct Recovery = 150% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 19.534 Expected Conc. = 18.06 Report level label = 7.2 Pct Recovery = 108% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210120050 Lab Value = 21.466 Expected Conc. = 18.02 Report level label = 7.2 Pct Recovery = 119% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 23.520 Expected Conc. = 18.02 Report level label = 7.2 Pct Recovery = 131% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 9.876 Expected Conc. = 18.02 Report level label = 7.2 Pct Recovery = 55% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 21.261 Expected Conc. = 18.02 Report level label = 7.2 Pct Recovery = 118% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 14.601 Expected Conc. = 18.02 Report level label = 7.2 Pct Recovery = 81% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 13.513 Expected Conc. = 18.02 Report level label = 7.2 Pct Recovery = 75% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210690067 Lab Value = 32.742 Expected Conc. = 17.916 Report level label = 7.2 Pct Recovery = 183% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 08/15/22 Pct Recovery = 61% Analysis Date = 08/10/22 Pct Recovery = 62% Analysis Date = 08/10/22 Pct Recovery = 62% Analysis Date = 08/06/22 Pct Recovery = 62% Analysis Date = 08/06/22 Pct Recovery = 62% Analysis Date = 08/02/22 Pct Recovery = 62% Analysis Date = 08/02/22 Pct Recovery = 62% Analysis Date = 07/29/22 Pct Recovery = 63% Analysis Date = 07/29/22 Pct Recovery = 63% Analysis Date = 07/25/22 Pct Recovery = 63% Analysis Date = 07/25/22 Pct Recovery = 63% Analysis Date = 07/21/22 Pct Recovery = 63% Analysis Date = 07/21/22 Pct Recovery = 63% Analysis Date = 07/17/22 Pct Recovery = 63% Analysis Date = 07/17/22 Pct Recovery = 63% Analysis Date = 07/13/22 Pct Recovery = 64% Analysis Date = 07/13/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/09/22 Pct Recovery = 64% Analysis Date = 07/05/22 Pct Recovery = 64% Analysis Date = 07/05/22 Pct Recovery = 64% Analysis Date = 07/01/22 Pct Recovery = 65% Analysis Date = 07/01/22 Pct Recovery = 65% Analysis Date = 06/26/22 Pct Recovery = 65% Analysis Date = 06/26/22 Pct Recovery = 65% Analysis Date = 06/22/22 Pct Recovery = 65% Analysis Date = 06/22/22 Pct Recovery = 65% Analysis Date = 06/18/22 Pct Recovery = 65% Analysis Date = 06/18/22 Pct Recovery = 65% Analysis Date = 06/14/22 Pct Recovery = 66% Analysis Date = 06/14/22 Pct Recovery = 66% Analysis Date = 06/10/22 Pct Recovery = 66% Analysis Date = 06/10/22 Pct Recovery = 66% Analysis Date = 06/06/22 Pct Recovery = 66% Analysis Date = 06/06/22 Pct Recovery = 66% Analysis Date = 06/02/22 Pct Recovery = 67% Analysis Date = 06/02/22 Pct Recovery = 67% Analysis Date = 05/29/22 Pct Recovery = 67% Analysis Date = 05/29/22 Pct Recovery = 67% Analysis Date = 05/25/22 Pct Recovery = 67% Analysis Date = 05/25/22 Pct Recovery = 67% Analysis Date = 05/21/22 Pct Recovery = 68% Analysis Date = 05/21/22 Pct Recovery = 68% Analysis Date = 05/17/22 Pct Recovery = 68% Analysis Date = 05/17/22 Pct Recovery = 68% Analysis Date = 05/12/22 Pct Recovery = 68% Analysis Date = 05/12/22 Pct Recovery = 68% Analysis Date = 05/08/22 Pct Recovery = 69% Analysis Date = 05/08/22 Pct Recovery = 69% Analysis Date = 05/04/22 Pct Recovery = 69% Analysis Date = 05/04/22 Pct Recovery = 69% Analysis Date = 04/30/22 Pct Recovery = 69% Analysis Date = 04/30/22 Pct Recovery = 69% Analysis Date = 04/26/22 Pct Recovery = 70% Analysis Date = 04/26/22 Pct Recovery = 70% Analysis Date = 04/22/22 Pct Recovery = 70% Analysis Date = 04/22/22 Pct Recovery = 70% Analysis Date = 04/18/22 Pct Recovery = 70% Analysis Date = 04/18/22 Pct Recovery = 70% Analysis Date = 04/14/22 Pct Recovery = 71% Analysis Date = 04/14/22 Pct Recovery = 71% Analysis Date = 04/10/22 Pct Recovery = 71% Analysis Date = 04/10/22 Pct Recovery = 71% Analysis Date = 04/06/22 Pct Recovery = 71% Analysis Date = 04/06/22 Pct Recovery = 71% Analysis Date = 04/02/22 Pct Recovery = 72% Analysis Date = 04/02/22 Pct Recovery = 72% Analysis Date = 03/28/22 Pct Recovery = 72% Analysis Date = 03/28/22 Pct Recovery = 72% Analysis Date = 03/24/22 Pct Recovery = 72% Analysis Date = 03/24/22 Pct Recovery = 72% Analysis Date = 03/20/22 Pct Recovery = 73% Analysis Date = 03/20/22 Pct Recovery = 73% Analysis Date = 03/16/22 Pct Recovery = 73% Analysis Date = 03/16/22 Pct Recovery = 73% Analysis Date = 03/12/22 Pct Recovery = 73% Analysis Date = 03/12/22 Pct Recovery = 73% Analysis Date = 03/08/22 Pct Recovery = 74% Analysis Date = 03/08/22 Pct Recovery = 74% Analysis Date = 03/04/22 Pct Recovery = 74% Analysis Date = 03/04/22 Pct Recovery = 74% Analysis Date = 02/28/22 Pct Recovery = 74% Analysis Date = 02/28/22 Pct Recovery = 74% Analysis Date = 02/24/22 Pct Recovery = 75% Analysis Date = 02/24/22 Pct Recovery = 75% Analysis Date = 02/20/22 Pct Recovery = 75% Analysis Date = 02/20/22 Pct Recovery = 75% Analysis Date = 02/16/22 Pct Recovery = 75% Analysis Date = 02/16/22 Pct Recovery = 75% Analysis Date = 02/11/22 Pct Recovery = 76% Analysis Date = 02/11/22 Pct Recovery = 76% Analysis Date = 02/07/22 Pct Recovery = 76% Analysis Date = 02/07/22 Pct Recovery = 76% Analysis Date = 02/03/22 Pct Recovery = 76% Analysis Date = 02/03/22 Pct Recovery = 76% Analysis Date = 01/30/22 Pct Recovery = 77% Analysis Date = 01/30/22 Pct Recovery = 77% Analysis Date = 01/26/22 Pct Recovery = 77% Analysis Date = 01/26/22 Pct Recovery = 77% Analysis Date = 01/22/22 Pct Recovery = 77% Analysis Date = 01/22/22 Pct Recovery = 77% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/14/22 Pct Recovery = 78% Analysis Date = 01/14/22 Pct Recovery = 78% Analysis Date = 01/10/22 Pct Recovery = 78% Analysis Date = 01/10/22 Pct Recovery = 78% Analysis Date = 01/06/22 Pct Recovery = 79% Analysis Date = 01/06/22 Pct Recovery = 79% Analysis Date = 01/02/22 Pct Recovery = 79% Analysis Date = 01/02/22 Pct Recovery = 79% Analysis Date = 12/28/21 Pct Recovery = 79% Analysis Date = 12/28/21 Pct Recovery = 79% Analysis Date = 12/24/21 Pct Recovery = 80% Analysis Date = 12/24/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/20/21 Pct Recovery = 80% Analysis Date = 12/16/21 Pct Recovery = 80% Analysis Date = 12/16/21 Pct Recovery = 80% Analysis Date = 12/12/21 Pct Recovery = 81% Analysis Date = 12/12/21 Pct Recovery = 81% Analysis Date = 12/08/21 Pct Recovery = 81% Analysis Date = 12/08/21 Pct Recovery = 81% Analysis Date = 12/04/21 Pct Recovery = 81% Analysis Date = 12/04/21 Pct Recovery = 81% Analysis Date = 11/30/21 Pct Recovery = 82% Analysis Date = 11/30/21 Pct Recovery = 82% Analysis Date = 11/26/21 Pct Recovery = 82% Analysis Date = 11/26/21 Pct Recovery = 82% Analysis Date = 11/22/21 Pct Recovery = 82% Analysis Date = 11/22/21 Pct Recovery = 82% Analysis Date = 11/18/21 Pct Recovery = 83% Analysis Date = 11/18/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/09/21 Pct Recovery = 83% Analysis Date = 11/09/21 Pct Recovery = 83% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 84% Analysis Date = 10/28/21 Pct Recovery = 84% Analysis Date = 10/28/21 Pct Recovery = 84% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 85% Analysis Date = 10/12/21 Pct Recovery = 86% Analysis Date = 10/12/21 Pct Recovery = 86% Analysis Date = 10/08/21 Pct Recovery = 86% Analysis Date = 10/08/21 Pct Recovery = 86% Analysis Date = 10/04/21 Pct Recovery = 86% Analysis Date = 10/04/21 Pct Recovery = 86% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 88% Analysis Date = 09/17/21 Pct Recovery = 88% Analysis Date = 09/13/21 Pct Recovery = 88% Analysis Date = 09/13/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 89% Analysis Date = 09/05/21 Pct Recovery = 89% Analysis Date = 09/01/21 Pct Recovery = 89% Analysis Date = 09/01/21 Pct Recovery = 89% Analysis Date = 08/28/21 Pct Recovery = 89% Analysis Date = 08/28/21 Pct Recovery = 89% Analysis Date = 08/24/21 Pct Recovery = 90% Analysis Date = 08/24/21 Pct Recovery = 90% Analysis Date = 08/20/21 Pct Recovery = 90% Analysis Date = 08/20/21 Pct Recovery = 90% Analysis Date = 08/15/21 Pct Recovery = 90% Analysis Date = 08/15/21 Pct Recovery = 90% Analysis Date = 08/11/21 Pct Recovery = 91% Analysis Date = 08/11/21 Pct Recovery = 91% Analysis Date = 08/07/21 Pct Recovery = 91% Analysis Date = 08/07/21 Pct Recovery = 91% Analysis Date = 08/03/21 Pct Recovery = 91% Analysis Date = 08/03/21 Pct Recovery = 91% Analysis Date = 07/30/21 Pct Recovery = 92% Analysis Date = 07/30/21 Pct Recovery = 92% Analysis Date = 07/26/21 Pct Recovery = 92% Analysis Date = 07/26/21 Pct Recovery = 92% Analysis Date = 07/22/21 Pct Recovery = 92% Analysis Date = 07/22/21 Pct Recovery = 92% Analysis Date = 07/18/21 Pct Recovery = 93% Analysis Date = 07/18/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/14/21 Pct Recovery = 93% Analysis Date = 07/10/21 Pct Recovery = 93% Analysis Date = 07/10/21 Pct Recovery = 93% Analysis Date = 07/06/21 Pct Recovery = 94% Analysis Date = 07/06/21 Pct Recovery = 94% Analysis Date = 07/02/21 Pct Recovery = 94% Analysis Date = 07/02/21 Pct Recovery = 94% Analysis Date = 06/27/21 Pct Recovery = 94% Analysis Date = 06/27/21 Pct Recovery = 94% Analysis Date = 06/23/21 Pct Recovery = 95% Analysis Date = 06/23/21 Pct Recovery = 95% Analysis Date = 06/19/21 Pct Recovery = 95% Analysis Date = 06/19/21 Pct Recovery = 95% Analysis Date = 06/15/21 Pct Recovery = 95% Analysis Date = 06/15/21 Pct Recovery = 95% Analysis Date = 06/11/21 Pct Recovery = 96% Analysis Date = 06/11/21 Pct Recovery = 96% Analysis Date = 06/07/21 Pct Recovery = 96% Analysis Date = 06/07/21 Pct Recovery = 96% Analysis Date = 06/03/21 Pct Recovery = 96% Analysis Date = 06/03/21 Pct Recovery = 96% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/30/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 97% Analysis Date = 05/26/21 Pct Recovery = 97% Analysis Date = 05/22/21 Pct Recovery = 97% Analysis Date = 05/22/21 Pct Recovery = 97% Analysis Date = 05/18/21 Pct Recovery = 98% Analysis Date = 05/18/21 Pct Recovery = 98% Analysis Date = 05/13/21 Pct Recovery = 98% Analysis Date = 05/13/21 Pct Recovery = 98% Analysis Date = 05/09/21 Pct Recovery = 98% Analysis Date = 05/09/21 Pct Recovery = 98% Analysis Date = 05/05/21 Pct Recovery = 99% Analysis Date = 05/05/21 Pct Recovery = 99% Analysis Date = 05/01/21 Pct Recovery = 99% Analysis Date = 05/01/21 Pct Recovery = 99% Analysis Date = 04/27/21 Pct Recovery = 99% Analysis Date = 04/27/21 Pct Recovery = 99% Analysis Date = 04/23/21 Pct Recovery = 100% Analysis Date = 04/23/21 Pct Recovery = 100% Analysis Date = 04/19/21 Pct Recovery = 100% Analysis Date = 04/19/21 Pct Recovery = 100% Analysis Date = 04/15/21 Pct Recovery = 100% Analysis Date = 04/15/21 Pct Recovery = 100% Analysis Date = 04/11/21 Pct Recovery = 101% Analysis Date = 04/11/21 Pct Recovery = 101% Analysis Date = 04/07/21 Pct Recovery = 101% Analysis Date = 04/07/21 Pct Recovery = 101% Analysis Date = 04/03/21 Pct Recovery = 101% Analysis Date = 04/03/21 Pct Recovery = 101% Analysis Date = 03/29/21 Pct Recovery = 102% Analysis Date = 03/29/21 Pct Recovery = 102% Analysis Date = 03/25/21 Pct Recovery = 102% Analysis Date = 03/25/21 Pct Recovery = 102% Analysis Date = 03/21/21 Pct Recovery = 102% Analysis Date = 03/21/21 Pct Recovery = 102% Analysis Date = 03/17/21 Pct Recovery = 102% Analysis Date = 03/17/21 Pct Recovery = 102% Analysis Date = 03/13/21 Pct Recovery = 102% Analysis Date = 03/13/21 Pct Recovery = 102% Analysis Date = 03/09/21 Pct Recovery = 102% Analysis Date = 03/09/21 Pct Recovery = 102% Analysis Date = 03/05/21 Pct Recovery = 101% Analysis Date = 03/05/21 Pct Recovery = 101% Analysis Date = 03/01/21 Pct Recovery = 101% Analysis Date = 03/01/21 Pct Recovery = 101% Analysis Date = 02/25/21 Pct Recovery = 100% Analysis Date = 02/25/21 Pct Recovery = 100% Analysis Date = 02/21/21 Pct Recovery = 100% Analysis Date = 02/21/21 Pct Recovery = 100% Analysis Date = 02/17/21 Pct Recovery = 100% Analysis Date = 02/17/21 Pct Recovery = 100% Analysis Date = 02/12/21 Pct Recovery = 99% Analysis Date = 02/12/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/04/21 Pct Recovery = 98% Analysis Date = 02/04/21 Pct Recovery = 98% Analysis Date = 01/31/21 Pct Recovery = 98% Analysis Date = 01/31/21 Pct Recovery = 98% Analysis Date = 01/27/21 Pct Recovery = 98% Analysis Date = 01/27/21 Pct Recovery = 98% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/19/21 Pct Recovery = 97% Analysis Date = 01/19/21 Pct Recovery = 97% Analysis Date = 01/15/21 Pct Recovery = 97% Analysis Date = 01/15/21 Pct Recovery = 97% Analysis Date = 01/11/21 Pct Recovery = 96% Analysis Date = 01/11/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 95% Analysis Date = 12/25/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 94% Analysis Date = 12/13/20 Pct Recovery = 94% Analysis Date = 12/09/20 Pct Recovery = 95% Analysis Date = 12/09/20 Pct Recovery = 95% Analysis Date = 12/05/20 Pct Recovery = 95% Analysis Date = 12/05/20 Pct Recovery = 95% Analysis Date = 12/01/20 Pct Recovery = 95% Analysis Date = 12/01/20 Pct Recovery = 95% Analysis Date = 11/27/20 Pct Recovery = 95% Analysis Date = 11/27/20 Pct Recovery = 95% Analysis Date = 11/23/20 Pct Recovery = 95% Analysis Date = 11/23/20 Pct Recovery = 95% Analysis Date = 11/19/20 Pct Recovery = 95% Analysis Date = 11/19/20 Pct Recovery = 95% Analysis Date = 11/14/20 Pct Recovery = 95% Analysis Date = 11/14/20 Pct Recovery = 95% Analysis Date = 11/10/20 Pct Recovery = 95% Analysis Date = 11/10/20 Pct Recovery = 95% Analysis Date = 11/06/20 Pct Recovery = 95% Analysis Date = 11/06/20 Pct Recovery = 95% Analysis Date = 11/02/20 Pct Recovery = 95% Analysis Date = 11/02/20 Pct Recovery = 95% Analysis Date = 10/29/20 Pct Recovery = 95% Analysis Date = 10/29/20 Pct Recovery = 95% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 96% Analysis Date = 10/21/20 Pct Recovery = 96% Analysis Date = 10/17/20 Pct Recovery = 96% Analysis Date = 10/17/20 Pct Recovery = 96% Analysis Date = 10/13/20 Pct Recovery = 96% Analysis Date = 10/13/20 Pct Recovery = 96% Analysis Date = 10/09/20 Pct Recovery = 96% Analysis Date = 10/09/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 97% Analysis Date = 10/05/20 Pct Recovery = 97% Analysis Date = 09/30/20 Pct Recovery = 97% Analysis Date = 09/30/20 Pct Recovery = 97% Analysis Date = 09/26/20 Pct Recovery = 98% Analysis Date = 09/26/20 Pct Recovery = 98% Analysis Date = 09/22/20 Pct Recovery = 98% Analysis Date = 09/22/20 Pct Recovery = 98% Analysis Date = 09/18/20 Pct Recovery = 98% Analysis Date = 09/18/20 Pct Recovery = 98% Analysis Date = 09/14/20 Pct Recovery = 98% Analysis Date = 09/14/20 Pct Recovery = 98% Analysis Date = 09/10/20 Pct Recovery = 98% Analysis Date = 09/10/20 Pct Recovery = 98% Analysis Date = 09/06/20 Pct Recovery = 99% Analysis Date = 09/06/20 Pct Recovery = 99% Analysis Date = 09/02/20 Pct Recovery = 99% Analysis Date = 09/02/20 Pct Recovery = 99% Analysis Date = 08/29/20 Pct Recovery = 99% Analysis Date = 08/29/20 Pct Recovery = 99% Analysis Date = 08/25/20 Pct Recovery = 99% Analysis Date = 08/25/20 Pct Recovery = 99% Analysis Date = 08/21/20 Pct Recovery = 99% Analysis Date = 08/21/20 Pct Recovery = 99% Analysis Date = 08/16/20 Pct Recovery = 99% Analysis Date = 08/16/20 Pct Recovery = 99% Analysis Date = 08/12/20 Pct Recovery = 99% Analysis Date = 08/12/20 Pct Recovery = 99% Analysis Date = 08/08/20 Pct Recovery = 99% Analysis Date = 08/08/20 Pct Recovery = 99% Analysis Date = 08/04/20 Pct Recovery = 99% Analysis Date = 08/04/20 Pct Recovery = 99% Analysis Date = 07/31/20 Pct Recovery = 99% Analysis Date = 07/31/20 Pct Recovery = 99% Analysis Date = 07/27/20 Pct Recovery = 99% Analysis Date = 07/27/20 Pct Recovery = 99% Analysis Date = 07/23/20 Pct Recovery = 99% Analysis Date = 07/23/20 Pct Recovery = 99% Analysis Date = 07/19/20 Pct Recovery = 99% Analysis Date = 07/19/20 Pct Recovery = 99% Analysis Date = 07/15/20 Pct Recovery = 99% Analysis Date = 07/15/20 Pct Recovery = 99% Analysis Date = 07/11/20 Pct Recovery = 99% Analysis Date = 07/11/20 Pct Recovery = 99% Analysis Date = 07/07/20 Pct Recovery = 99% Analysis Date = 07/07/20 Pct Recovery = 99% Analysis Date = 07/02/20 Pct Recovery = 99% Analysis Date = 07/02/20 Pct Recovery = 99% Analysis Date = 06/28/20 Pct Recovery = 99% Analysis Date = 06/28/20 Pct Recovery = 99% Analysis Date = 06/24/20 Pct Recovery = 99% Analysis Date = 06/24/20 Pct Recovery = 99% Analysis Date = 06/20/20 Pct Recovery = 99% Analysis Date = 06/20/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/16/20 Pct Recovery = 99% Analysis Date = 06/12/20 Pct Recovery = 99% Analysis Date = 06/12/20 Pct Recovery = 99% Analysis Date = 06/08/20 Pct Recovery = 99% Analysis Date = 06/08/20 Pct Recovery = 99% Analysis Date = 06/04/20 Pct Recovery = 99% Analysis Date = 06/04/20 Pct Recovery = 99% Analysis Date = 05/31/20 Pct Recovery = 99% Analysis Date = 05/31/20 Pct Recovery = 99% Analysis Date = 05/27/20 Pct Recovery = 99% Analysis Date = 05/27/20 Pct Recovery = 99% Analysis Date = 05/23/20 Pct Recovery = 99% Analysis Date = 05/23/20 Pct Recovery = 99% Analysis Date = 05/19/20 Pct Recovery = 99% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SIMAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 92% 28% 89% 22%
Total 35 92% 28% 89% 22%

Sample Statistics
SIMAZINE

Characteristic N % % Basis
Plotted 35 100% Spiked
Estimated Values 3 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 78 .  
False Positives 1 1% 1 out of 78

OBSP Determination:
SULFENTRAZONE
METHOD: 2447 , TESTIDCODE: 68687LCM60

Laboratory ID = 20202390020 Lab Value = 237.826 Expected Conc. = 230.3 Report level label = 18 Pct Recovery = 103% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20202590107 Lab Value = 248.454 Expected Conc. = 226.8 Report level label = 18 Pct Recovery = 110% Analysis Date = 09/25/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590106 Lab Value = 242.972 Expected Conc. = 226.8 Report level label = 18 Pct Recovery = 107% Analysis Date = 09/24/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 226.506 Expected Conc. = 225.4 Report level label = 18 Pct Recovery = 100% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 180.482 Expected Conc. = 225.4 Report level label = 18 Pct Recovery = 80% Analysis Date = 12/09/20 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20201820155 Lab Value = 233.873 Expected Conc. = 224.5 Report level label = 18 Pct Recovery = 104% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 242.384 Expected Conc. = 224.5 Report level label = 18 Pct Recovery = 108% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20221520237 Lab Value = 181.251 Expected Conc. = 182.32 Report level label = 18 Pct Recovery = 99% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20222150192 Lab Value = 139.138 Expected Conc. = 181.2 Report level label = 18 Pct Recovery = 77% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221940196 Lab Value = 179.999 Expected Conc. = 180 Report level label = 18 Pct Recovery = 100% Analysis Date = 07/21/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20201960104 Lab Value = 115.289 Expected Conc. = 115.15 Report level label = 18 Pct Recovery = 100% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20221870197 Lab Value = 75.425 Expected Conc. = 113.95 Report level label = 18 Pct Recovery = 66% Analysis Date = 07/14/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20203360042 Lab Value = 91.424 Expected Conc. = 113.4 Report level label = 18 Pct Recovery = 81% Analysis Date = 12/17/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230018 Lab Value = 151.146 Expected Conc. = 113.4 Report level label = 18 Pct Recovery = 133% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 111.746 Expected Conc. = 113.4 Report level label = 18 Pct Recovery = 99% Analysis Date = 10/29/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202530029 Lab Value = 117.992 Expected Conc. = 112.25 Report level label = 18 Pct Recovery = 105% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 92.381 Expected Conc. = 112.25 Report level label = 18 Pct Recovery = 82% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 123.272 Expected Conc. = 112.25 Report level label = 18 Pct Recovery = 110% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20220740064 Lab Value = 105.615 Expected Conc. = 112 Report level label = 18 Pct Recovery = 94% Analysis Date = 03/24/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20201610160 Lab Value = 55.962 Expected Conc. = 46.06 Report level label = 18 Pct Recovery = 121% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20221660151 Lab Value = 37.843 Expected Conc. = 45.58 Report level label = 18 Pct Recovery = 83% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210970035 Lab Value = 37.587 Expected Conc. = 45.36 Report level label = 18 Pct Recovery = 83% Analysis Date = 04/15/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 37.515 Expected Conc. = 45.36 Report level label = 18 Pct Recovery = 83% Analysis Date = 02/11/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 41.144 Expected Conc. = 45.36 Report level label = 18 Pct Recovery = 91% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 61.589 Expected Conc. = 45.36 Report level label = 18 Pct Recovery = 136% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 46.559 Expected Conc. = 45.36 Report level label = 18 Pct Recovery = 103% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 47.742 Expected Conc. = 45.36 Report level label = 18 Pct Recovery = 105% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210830019 Lab Value = 46.494 Expected Conc. = 45.08 Report level label = 18 Pct Recovery = 103% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 35.445 Expected Conc. = 45.08 Report level label = 18 Pct Recovery = 79% Analysis Date = 02/02/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202180001 Lab Value = 43.947 Expected Conc. = 44.9 Report level label = 18 Pct Recovery = 98% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 61.519 Expected Conc. = 44.9 Report level label = 18 Pct Recovery = 137% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 39.501 Expected Conc. = 44.9 Report level label = 18 Pct Recovery = 88% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Analysis Date = 08/16/22 Pct Recovery = 85% Analysis Date = 08/11/22 Pct Recovery = 85% Analysis Date = 08/11/22 Pct Recovery = 85% Analysis Date = 08/07/22 Pct Recovery = 85% Analysis Date = 08/07/22 Pct Recovery = 85% Analysis Date = 08/03/22 Pct Recovery = 85% Analysis Date = 08/03/22 Pct Recovery = 85% Analysis Date = 07/30/22 Pct Recovery = 86% Analysis Date = 07/30/22 Pct Recovery = 86% Analysis Date = 07/26/22 Pct Recovery = 86% Analysis Date = 07/26/22 Pct Recovery = 86% Analysis Date = 07/22/22 Pct Recovery = 86% Analysis Date = 07/22/22 Pct Recovery = 86% Analysis Date = 07/18/22 Pct Recovery = 86% Analysis Date = 07/18/22 Pct Recovery = 86% Analysis Date = 07/14/22 Pct Recovery = 86% Analysis Date = 07/14/22 Pct Recovery = 86% Analysis Date = 07/10/22 Pct Recovery = 86% Analysis Date = 07/10/22 Pct Recovery = 86% Analysis Date = 07/06/22 Pct Recovery = 86% Analysis Date = 07/06/22 Pct Recovery = 86% Analysis Date = 07/02/22 Pct Recovery = 86% Analysis Date = 07/02/22 Pct Recovery = 86% Analysis Date = 06/27/22 Pct Recovery = 86% Analysis Date = 06/27/22 Pct Recovery = 86% Analysis Date = 06/23/22 Pct Recovery = 86% Analysis Date = 06/23/22 Pct Recovery = 86% Analysis Date = 06/19/22 Pct Recovery = 86% Analysis Date = 06/19/22 Pct Recovery = 86% Analysis Date = 06/15/22 Pct Recovery = 86% Analysis Date = 06/15/22 Pct Recovery = 86% Analysis Date = 06/11/22 Pct Recovery = 86% Analysis Date = 06/11/22 Pct Recovery = 86% Analysis Date = 06/07/22 Pct Recovery = 86% Analysis Date = 06/07/22 Pct Recovery = 86% Analysis Date = 06/03/22 Pct Recovery = 86% Analysis Date = 06/03/22 Pct Recovery = 86% Analysis Date = 05/30/22 Pct Recovery = 86% Analysis Date = 05/30/22 Pct Recovery = 86% Analysis Date = 05/26/22 Pct Recovery = 86% Analysis Date = 05/26/22 Pct Recovery = 86% Analysis Date = 05/22/22 Pct Recovery = 86% Analysis Date = 05/22/22 Pct Recovery = 86% Analysis Date = 05/18/22 Pct Recovery = 86% Analysis Date = 05/18/22 Pct Recovery = 86% Analysis Date = 05/13/22 Pct Recovery = 86% Analysis Date = 05/13/22 Pct Recovery = 86% Analysis Date = 05/09/22 Pct Recovery = 86% Analysis Date = 05/09/22 Pct Recovery = 86% Analysis Date = 05/05/22 Pct Recovery = 86% Analysis Date = 05/05/22 Pct Recovery = 86% Analysis Date = 05/01/22 Pct Recovery = 86% Analysis Date = 05/01/22 Pct Recovery = 86% Analysis Date = 04/27/22 Pct Recovery = 86% Analysis Date = 04/27/22 Pct Recovery = 86% Analysis Date = 04/23/22 Pct Recovery = 86% Analysis Date = 04/23/22 Pct Recovery = 86% Analysis Date = 04/19/22 Pct Recovery = 86% Analysis Date = 04/19/22 Pct Recovery = 86% Analysis Date = 04/15/22 Pct Recovery = 86% Analysis Date = 04/15/22 Pct Recovery = 86% Analysis Date = 04/11/22 Pct Recovery = 86% Analysis Date = 04/11/22 Pct Recovery = 86% Analysis Date = 04/07/22 Pct Recovery = 86% Analysis Date = 04/07/22 Pct Recovery = 86% Analysis Date = 04/03/22 Pct Recovery = 86% Analysis Date = 04/03/22 Pct Recovery = 86% Analysis Date = 03/29/22 Pct Recovery = 86% Analysis Date = 03/29/22 Pct Recovery = 86% Analysis Date = 03/25/22 Pct Recovery = 86% Analysis Date = 03/25/22 Pct Recovery = 86% Analysis Date = 03/21/22 Pct Recovery = 86% Analysis Date = 03/21/22 Pct Recovery = 86% Analysis Date = 03/17/22 Pct Recovery = 86% Analysis Date = 03/17/22 Pct Recovery = 86% Analysis Date = 03/13/22 Pct Recovery = 86% Analysis Date = 03/13/22 Pct Recovery = 86% Analysis Date = 03/09/22 Pct Recovery = 86% Analysis Date = 03/09/22 Pct Recovery = 86% Analysis Date = 03/05/22 Pct Recovery = 86% Analysis Date = 03/05/22 Pct Recovery = 86% Analysis Date = 03/01/22 Pct Recovery = 86% Analysis Date = 03/01/22 Pct Recovery = 86% Analysis Date = 02/25/22 Pct Recovery = 86% Analysis Date = 02/25/22 Pct Recovery = 86% Analysis Date = 02/21/22 Pct Recovery = 86% Analysis Date = 02/21/22 Pct Recovery = 86% Analysis Date = 02/17/22 Pct Recovery = 86% Analysis Date = 02/17/22 Pct Recovery = 86% Analysis Date = 02/12/22 Pct Recovery = 86% Analysis Date = 02/12/22 Pct Recovery = 86% Analysis Date = 02/08/22 Pct Recovery = 86% Analysis Date = 02/08/22 Pct Recovery = 86% Analysis Date = 02/04/22 Pct Recovery = 86% Analysis Date = 02/04/22 Pct Recovery = 86% Analysis Date = 01/31/22 Pct Recovery = 86% Analysis Date = 01/31/22 Pct Recovery = 86% Analysis Date = 01/27/22 Pct Recovery = 86% Analysis Date = 01/27/22 Pct Recovery = 86% Analysis Date = 01/23/22 Pct Recovery = 86% Analysis Date = 01/23/22 Pct Recovery = 86% Analysis Date = 01/19/22 Pct Recovery = 86% Analysis Date = 01/19/22 Pct Recovery = 86% Analysis Date = 01/15/22 Pct Recovery = 86% Analysis Date = 01/15/22 Pct Recovery = 86% Analysis Date = 01/11/22 Pct Recovery = 86% Analysis Date = 01/11/22 Pct Recovery = 86% Analysis Date = 01/07/22 Pct Recovery = 86% Analysis Date = 01/07/22 Pct Recovery = 86% Analysis Date = 01/03/22 Pct Recovery = 86% Analysis Date = 01/03/22 Pct Recovery = 86% Analysis Date = 12/29/21 Pct Recovery = 86% Analysis Date = 12/29/21 Pct Recovery = 86% Analysis Date = 12/25/21 Pct Recovery = 86% Analysis Date = 12/25/21 Pct Recovery = 86% Analysis Date = 12/21/21 Pct Recovery = 86% Analysis Date = 12/21/21 Pct Recovery = 86% Analysis Date = 12/17/21 Pct Recovery = 86% Analysis Date = 12/17/21 Pct Recovery = 86% Analysis Date = 12/13/21 Pct Recovery = 86% Analysis Date = 12/13/21 Pct Recovery = 86% Analysis Date = 12/09/21 Pct Recovery = 86% Analysis Date = 12/09/21 Pct Recovery = 86% Analysis Date = 12/05/21 Pct Recovery = 86% Analysis Date = 12/05/21 Pct Recovery = 86% Analysis Date = 12/01/21 Pct Recovery = 86% Analysis Date = 12/01/21 Pct Recovery = 86% Analysis Date = 11/27/21 Pct Recovery = 86% Analysis Date = 11/27/21 Pct Recovery = 86% Analysis Date = 11/23/21 Pct Recovery = 86% Analysis Date = 11/23/21 Pct Recovery = 86% Analysis Date = 11/19/21 Pct Recovery = 86% Analysis Date = 11/19/21 Pct Recovery = 86% Analysis Date = 11/14/21 Pct Recovery = 85% Analysis Date = 11/14/21 Pct Recovery = 85% Analysis Date = 11/10/21 Pct Recovery = 85% Analysis Date = 11/10/21 Pct Recovery = 85% Analysis Date = 11/06/21 Pct Recovery = 85% Analysis Date = 11/06/21 Pct Recovery = 85% Analysis Date = 11/02/21 Pct Recovery = 85% Analysis Date = 11/02/21 Pct Recovery = 85% Analysis Date = 10/29/21 Pct Recovery = 85% Analysis Date = 10/29/21 Pct Recovery = 85% Analysis Date = 10/25/21 Pct Recovery = 85% Analysis Date = 10/25/21 Pct Recovery = 85% Analysis Date = 10/21/21 Pct Recovery = 85% Analysis Date = 10/21/21 Pct Recovery = 85% Analysis Date = 10/17/21 Pct Recovery = 85% Analysis Date = 10/17/21 Pct Recovery = 85% Analysis Date = 10/13/21 Pct Recovery = 85% Analysis Date = 10/13/21 Pct Recovery = 85% Analysis Date = 10/09/21 Pct Recovery = 85% Analysis Date = 10/09/21 Pct Recovery = 85% Analysis Date = 10/05/21 Pct Recovery = 85% Analysis Date = 10/05/21 Pct Recovery = 85% Analysis Date = 09/30/21 Pct Recovery = 85% Analysis Date = 09/30/21 Pct Recovery = 85% Analysis Date = 09/26/21 Pct Recovery = 85% Analysis Date = 09/26/21 Pct Recovery = 85% Analysis Date = 09/22/21 Pct Recovery = 85% Analysis Date = 09/22/21 Pct Recovery = 85% Analysis Date = 09/18/21 Pct Recovery = 85% Analysis Date = 09/18/21 Pct Recovery = 85% Analysis Date = 09/14/21 Pct Recovery = 85% Analysis Date = 09/14/21 Pct Recovery = 85% Analysis Date = 09/10/21 Pct Recovery = 85% Analysis Date = 09/10/21 Pct Recovery = 85% Analysis Date = 09/06/21 Pct Recovery = 85% Analysis Date = 09/06/21 Pct Recovery = 85% Analysis Date = 09/02/21 Pct Recovery = 85% Analysis Date = 09/02/21 Pct Recovery = 85% Analysis Date = 08/29/21 Pct Recovery = 85% Analysis Date = 08/29/21 Pct Recovery = 85% Analysis Date = 08/25/21 Pct Recovery = 85% Analysis Date = 08/25/21 Pct Recovery = 85% Analysis Date = 08/21/21 Pct Recovery = 85% Analysis Date = 08/21/21 Pct Recovery = 85% Analysis Date = 08/16/21 Pct Recovery = 85% Analysis Date = 08/16/21 Pct Recovery = 85% Analysis Date = 08/12/21 Pct Recovery = 85% Analysis Date = 08/12/21 Pct Recovery = 85% Analysis Date = 08/08/21 Pct Recovery = 85% Analysis Date = 08/08/21 Pct Recovery = 85% Analysis Date = 08/04/21 Pct Recovery = 85% Analysis Date = 08/04/21 Pct Recovery = 85% Analysis Date = 07/31/21 Pct Recovery = 85% Analysis Date = 07/31/21 Pct Recovery = 85% Analysis Date = 07/27/21 Pct Recovery = 85% Analysis Date = 07/27/21 Pct Recovery = 85% Analysis Date = 07/23/21 Pct Recovery = 85% Analysis Date = 07/23/21 Pct Recovery = 85% Analysis Date = 07/19/21 Pct Recovery = 85% Analysis Date = 07/19/21 Pct Recovery = 85% Analysis Date = 07/15/21 Pct Recovery = 85% Analysis Date = 07/15/21 Pct Recovery = 85% Analysis Date = 07/11/21 Pct Recovery = 85% Analysis Date = 07/11/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/07/21 Pct Recovery = 85% Analysis Date = 07/03/21 Pct Recovery = 85% Analysis Date = 07/03/21 Pct Recovery = 85% Analysis Date = 06/28/21 Pct Recovery = 85% Analysis Date = 06/28/21 Pct Recovery = 85% Analysis Date = 06/24/21 Pct Recovery = 85% Analysis Date = 06/24/21 Pct Recovery = 85% Analysis Date = 06/20/21 Pct Recovery = 85% Analysis Date = 06/20/21 Pct Recovery = 85% Analysis Date = 06/16/21 Pct Recovery = 85% Analysis Date = 06/16/21 Pct Recovery = 85% Analysis Date = 06/12/21 Pct Recovery = 85% Analysis Date = 06/12/21 Pct Recovery = 85% Analysis Date = 06/08/21 Pct Recovery = 85% Analysis Date = 06/08/21 Pct Recovery = 85% Analysis Date = 06/04/21 Pct Recovery = 85% Analysis Date = 06/04/21 Pct Recovery = 85% Analysis Date = 05/31/21 Pct Recovery = 85% Analysis Date = 05/31/21 Pct Recovery = 85% Analysis Date = 05/27/21 Pct Recovery = 85% Analysis Date = 05/27/21 Pct Recovery = 85% Analysis Date = 05/23/21 Pct Recovery = 85% Analysis Date = 05/23/21 Pct Recovery = 85% Analysis Date = 05/19/21 Pct Recovery = 85% Analysis Date = 05/19/21 Pct Recovery = 85% Analysis Date = 05/14/21 Pct Recovery = 85% Analysis Date = 05/14/21 Pct Recovery = 85% Analysis Date = 05/10/21 Pct Recovery = 85% Analysis Date = 05/10/21 Pct Recovery = 85% Analysis Date = 05/06/21 Pct Recovery = 85% Analysis Date = 05/06/21 Pct Recovery = 85% Analysis Date = 05/02/21 Pct Recovery = 85% Analysis Date = 05/02/21 Pct Recovery = 85% Analysis Date = 04/28/21 Pct Recovery = 85% Analysis Date = 04/28/21 Pct Recovery = 85% Analysis Date = 04/24/21 Pct Recovery = 85% Analysis Date = 04/24/21 Pct Recovery = 85% Analysis Date = 04/20/21 Pct Recovery = 85% Analysis Date = 04/20/21 Pct Recovery = 85% Analysis Date = 04/16/21 Pct Recovery = 85% Analysis Date = 04/16/21 Pct Recovery = 85% Analysis Date = 04/12/21 Pct Recovery = 85% Analysis Date = 04/12/21 Pct Recovery = 85% Analysis Date = 04/08/21 Pct Recovery = 85% Analysis Date = 04/08/21 Pct Recovery = 85% Analysis Date = 04/04/21 Pct Recovery = 86% Analysis Date = 04/04/21 Pct Recovery = 86% Analysis Date = 03/30/21 Pct Recovery = 86% Analysis Date = 03/30/21 Pct Recovery = 86% Analysis Date = 03/26/21 Pct Recovery = 87% Analysis Date = 03/26/21 Pct Recovery = 87% Analysis Date = 03/22/21 Pct Recovery = 87% Analysis Date = 03/22/21 Pct Recovery = 87% Analysis Date = 03/18/21 Pct Recovery = 88% Analysis Date = 03/18/21 Pct Recovery = 88% Analysis Date = 03/14/21 Pct Recovery = 88% Analysis Date = 03/14/21 Pct Recovery = 88% Analysis Date = 03/10/21 Pct Recovery = 89% Analysis Date = 03/10/21 Pct Recovery = 89% Analysis Date = 03/06/21 Pct Recovery = 89% Analysis Date = 03/06/21 Pct Recovery = 89% Analysis Date = 03/02/21 Pct Recovery = 89% Analysis Date = 03/02/21 Pct Recovery = 89% Analysis Date = 02/26/21 Pct Recovery = 90% Analysis Date = 02/26/21 Pct Recovery = 90% Analysis Date = 02/22/21 Pct Recovery = 90% Analysis Date = 02/22/21 Pct Recovery = 90% Analysis Date = 02/18/21 Pct Recovery = 91% Analysis Date = 02/18/21 Pct Recovery = 91% Analysis Date = 02/13/21 Pct Recovery = 91% Analysis Date = 02/13/21 Pct Recovery = 91% Analysis Date = 02/09/21 Pct Recovery = 92% Analysis Date = 02/09/21 Pct Recovery = 92% Analysis Date = 02/05/21 Pct Recovery = 92% Analysis Date = 02/05/21 Pct Recovery = 92% Analysis Date = 02/01/21 Pct Recovery = 93% Analysis Date = 02/01/21 Pct Recovery = 93% Analysis Date = 01/28/21 Pct Recovery = 93% Analysis Date = 01/28/21 Pct Recovery = 93% Analysis Date = 01/24/21 Pct Recovery = 93% Analysis Date = 01/24/21 Pct Recovery = 93% Analysis Date = 01/20/21 Pct Recovery = 94% Analysis Date = 01/20/21 Pct Recovery = 94% Analysis Date = 01/16/21 Pct Recovery = 94% Analysis Date = 01/16/21 Pct Recovery = 94% Analysis Date = 01/12/21 Pct Recovery = 94% Analysis Date = 01/12/21 Pct Recovery = 94% Analysis Date = 01/08/21 Pct Recovery = 95% Analysis Date = 01/08/21 Pct Recovery = 95% Analysis Date = 01/04/21 Pct Recovery = 95% Analysis Date = 01/04/21 Pct Recovery = 95% Analysis Date = 12/30/20 Pct Recovery = 96% Analysis Date = 12/30/20 Pct Recovery = 96% Analysis Date = 12/26/20 Pct Recovery = 96% Analysis Date = 12/26/20 Pct Recovery = 96% Analysis Date = 12/22/20 Pct Recovery = 96% Analysis Date = 12/22/20 Pct Recovery = 96% Analysis Date = 12/18/20 Pct Recovery = 97% Analysis Date = 12/18/20 Pct Recovery = 97% Analysis Date = 12/14/20 Pct Recovery = 98% Analysis Date = 12/14/20 Pct Recovery = 98% Analysis Date = 12/10/20 Pct Recovery = 98% Analysis Date = 12/10/20 Pct Recovery = 98% Analysis Date = 12/06/20 Pct Recovery = 99% Analysis Date = 12/06/20 Pct Recovery = 99% Analysis Date = 12/02/20 Pct Recovery = 99% Analysis Date = 12/02/20 Pct Recovery = 99% Analysis Date = 11/28/20 Pct Recovery = 100% Analysis Date = 11/28/20 Pct Recovery = 100% Analysis Date = 11/24/20 Pct Recovery = 101% Analysis Date = 11/24/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/20/20 Pct Recovery = 101% Analysis Date = 11/15/20 Pct Recovery = 102% Analysis Date = 11/15/20 Pct Recovery = 102% Analysis Date = 11/11/20 Pct Recovery = 103% Analysis Date = 11/11/20 Pct Recovery = 103% Analysis Date = 11/07/20 Pct Recovery = 103% Analysis Date = 11/07/20 Pct Recovery = 103% Analysis Date = 11/03/20 Pct Recovery = 104% Analysis Date = 11/03/20 Pct Recovery = 104% Analysis Date = 10/30/20 Pct Recovery = 104% Analysis Date = 10/30/20 Pct Recovery = 104% Analysis Date = 10/26/20 Pct Recovery = 104% Analysis Date = 10/26/20 Pct Recovery = 104% Analysis Date = 10/22/20 Pct Recovery = 104% Analysis Date = 10/22/20 Pct Recovery = 104% Analysis Date = 10/18/20 Pct Recovery = 104% Analysis Date = 10/18/20 Pct Recovery = 104% Analysis Date = 10/14/20 Pct Recovery = 105% Analysis Date = 10/14/20 Pct Recovery = 105% Analysis Date = 10/10/20 Pct Recovery = 105% Analysis Date = 10/10/20 Pct Recovery = 105% Analysis Date = 10/06/20 Pct Recovery = 105% Analysis Date = 10/06/20 Pct Recovery = 105% Analysis Date = 10/01/20 Pct Recovery = 105% Analysis Date = 10/01/20 Pct Recovery = 105% Analysis Date = 09/27/20 Pct Recovery = 105% Analysis Date = 09/27/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/23/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/19/20 Pct Recovery = 105% Analysis Date = 09/15/20 Pct Recovery = 105% Analysis Date = 09/15/20 Pct Recovery = 105% Analysis Date = 09/11/20 Pct Recovery = 105% Analysis Date = 09/11/20 Pct Recovery = 105% Analysis Date = 09/07/20 Pct Recovery = 105% Analysis Date = 09/07/20 Pct Recovery = 105% Analysis Date = 09/03/20 Pct Recovery = 105% Analysis Date = 09/03/20 Pct Recovery = 105% Analysis Date = 08/30/20 Pct Recovery = 105% Analysis Date = 08/30/20 Pct Recovery = 105% Analysis Date = 08/26/20 Pct Recovery = 105% Analysis Date = 08/26/20 Pct Recovery = 105% Analysis Date = 08/22/20 Pct Recovery = 105% Analysis Date = 08/22/20 Pct Recovery = 105% Analysis Date = 08/17/20 Pct Recovery = 105% Analysis Date = 08/17/20 Pct Recovery = 105% Analysis Date = 08/13/20 Pct Recovery = 105% Analysis Date = 08/13/20 Pct Recovery = 105% Analysis Date = 08/09/20 Pct Recovery = 105% Analysis Date = 08/09/20 Pct Recovery = 105% Analysis Date = 08/05/20 Pct Recovery = 105% Analysis Date = 08/05/20 Pct Recovery = 105% Analysis Date = 08/01/20 Pct Recovery = 105% Analysis Date = 08/01/20 Pct Recovery = 105% Analysis Date = 07/28/20 Pct Recovery = 106% Analysis Date = 07/28/20 Pct Recovery = 106% Analysis Date = 07/24/20 Pct Recovery = 106% Analysis Date = 07/24/20 Pct Recovery = 106% Analysis Date = 07/20/20 Pct Recovery = 106% Analysis Date = 07/20/20 Pct Recovery = 106% Analysis Date = 07/16/20 Pct Recovery = 106% Analysis Date = 07/16/20 Pct Recovery = 106% Analysis Date = 07/12/20 Pct Recovery = 106% Analysis Date = 07/12/20 Pct Recovery = 106% Analysis Date = 07/08/20 Pct Recovery = 107% Analysis Date = 07/08/20 Pct Recovery = 107% Analysis Date = 07/03/20 Pct Recovery = 107% Analysis Date = 07/03/20 Pct Recovery = 107% Analysis Date = 06/29/20 Pct Recovery = 107% Analysis Date = 06/29/20 Pct Recovery = 107% Analysis Date = 06/25/20 Pct Recovery = 107% Analysis Date = 06/25/20 Pct Recovery = 107% Analysis Date = 06/21/20 Pct Recovery = 107% Analysis Date = 06/21/20 Pct Recovery = 107% Analysis Date = 06/17/20 Pct Recovery = 107% Analysis Date = 06/17/20 Pct Recovery = 107% Analysis Date = 06/13/20 Pct Recovery = 108% Analysis Date = 06/13/20 Pct Recovery = 108% Analysis Date = 06/09/20 Pct Recovery = 108% Analysis Date = 06/09/20 Pct Recovery = 108% Analysis Date = 06/05/20 Pct Recovery = 108% Analysis Date = 06/05/20 Pct Recovery = 108% Analysis Date = 06/01/20 Pct Recovery = 108% Analysis Date = 06/01/20 Pct Recovery = 108% Analysis Date = 05/28/20 Pct Recovery = 109% Analysis Date = 05/28/20 Pct Recovery = 109% Analysis Date = 05/24/20 Pct Recovery = 109% Analysis Date = 05/24/20 Pct Recovery = 109% Analysis Date = 05/20/20 Pct Recovery = 109% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFENTRAZONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 32 99% 17% 100% 17%
Total 32 99% 17% 100% 17%

Sample Statistics
SULFENTRAZONE

Characteristic N % % Basis
Plotted 32 100% Spiked
Estimated Values 5 16% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 32 .  
False Negatives 0 0% 0 out of 32
Not Spiked 84 .  
False Positives 0 0% 0 out of 84

OBSP Determination:
SULFOMETURON-METHYL
METHOD: 2447 , TESTIDCODE: 68688LCM60

Laboratory ID = 20202110006 Lab Value = 42.339 Expected Conc. = 50.5 Report level label = 4 Pct Recovery = 84% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 43.069 Expected Conc. = 50.4 Report level label = 4 Pct Recovery = 85% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 33.439 Expected Conc. = 50.3 Report level label = 4 Pct Recovery = 66% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 49.199 Expected Conc. = 50.3 Report level label = 4 Pct Recovery = 98% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 47.518 Expected Conc. = 50.3 Report level label = 4 Pct Recovery = 94% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210760015 Lab Value = 47.522 Expected Conc. = 49.49 Report level label = 4 Pct Recovery = 96% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 54.083 Expected Conc. = 49.49 Report level label = 4 Pct Recovery = 109% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 51.928 Expected Conc. = 49.49 Report level label = 4 Pct Recovery = 105% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 49.981 Expected Conc. = 49.49 Report level label = 4 Pct Recovery = 101% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20220190116 Lab Value = 24.779 Expected Conc. = 40.56 Report level label = 4 Pct Recovery = 61% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 30.935 Expected Conc. = 40.56 Report level label = 4 Pct Recovery = 76% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 10.591 Expected Conc. = 40.4 Report level label = 4 Pct Recovery = 26% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20212990174 Lab Value = 20.314 Expected Conc. = 40.16 Report level label = 4 Pct Recovery = 51% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 14.739 Expected Conc. = 40 Report level label = 4 Pct Recovery = 37% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 39.312 Expected Conc. = 39.84 Report level label = 4 Pct Recovery = 99% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20221730293 Lab Value = 19.922 Expected Conc. = 25.35 Report level label = 4 Pct Recovery = 79% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 13.366 Expected Conc. = 25.35 Report level label = 4 Pct Recovery = 53% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20201680155 Lab Value = 22.786 Expected Conc. = 25.25 Report level label = 4 Pct Recovery = 90% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 20.593 Expected Conc. = 25.2 Report level label = 4 Pct Recovery = 82% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 19.875 Expected Conc. = 25.2 Report level label = 4 Pct Recovery = 79% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 20.881 Expected Conc. = 25.2 Report level label = 4 Pct Recovery = 83% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202880004 Lab Value = 26.246 Expected Conc. = 25.15 Report level label = 4 Pct Recovery = 104% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20213340027 Lab Value = 11.830 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 47% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 41.854 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 167% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 13.825 Expected Conc. = 25.1 Report level label = 4 Pct Recovery = 55% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20220810133 Lab Value = 22.552 Expected Conc. = 24.9 Report level label = 4 Pct Recovery = 91% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20210480001 Lab Value = 23.573 Expected Conc. = 24.745 Report level label = 4 Pct Recovery = 95% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 22.791 Expected Conc. = 20.12 Report level label = 4 Pct Recovery = 113% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 17.319 Expected Conc. = 20.12 Report level label = 4 Pct Recovery = 86% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 22.683 Expected Conc. = 19.796 Report level label = 4 Pct Recovery = 115% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20213410072 Lab Value = 7.661 Expected Conc. = 10.14 Report level label = 4 Pct Recovery = 76% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20201610160 Lab Value = 8.532 Expected Conc. = 10.1 Report level label = 4 Pct Recovery = 84% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 9.712 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 96% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 10.106 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 100% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 9.212 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 91% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 9.604 Expected Conc. = 10.08 Report level label = 4 Pct Recovery = 95% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210120050 Lab Value = 10.834 Expected Conc. = 10.06 Report level label = 4 Pct Recovery = 108% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 9.931 Expected Conc. = 10.06 Report level label = 4 Pct Recovery = 99% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.758 Expected Conc. = 10.06 Report level label = 4 Pct Recovery = 77% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 10.098 Expected Conc. = 10.06 Report level label = 4 Pct Recovery = 100% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20213060210 Lab Value = 3.830 Expected Conc. = 10.04 Report level label = 4 Pct Recovery = 38% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210690067 Lab Value = 7.757 Expected Conc. = 9.898 Report level label = 4 Pct Recovery = 78% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Analysis Date = 08/15/22 Pct Recovery = 52% Analysis Date = 08/10/22 Pct Recovery = 52% Analysis Date = 08/10/22 Pct Recovery = 52% Analysis Date = 08/06/22 Pct Recovery = 53% Analysis Date = 08/06/22 Pct Recovery = 53% Analysis Date = 08/02/22 Pct Recovery = 53% Analysis Date = 08/02/22 Pct Recovery = 53% Analysis Date = 07/29/22 Pct Recovery = 53% Analysis Date = 07/29/22 Pct Recovery = 53% Analysis Date = 07/25/22 Pct Recovery = 54% Analysis Date = 07/25/22 Pct Recovery = 54% Analysis Date = 07/21/22 Pct Recovery = 54% Analysis Date = 07/21/22 Pct Recovery = 54% Analysis Date = 07/17/22 Pct Recovery = 55% Analysis Date = 07/17/22 Pct Recovery = 55% Analysis Date = 07/13/22 Pct Recovery = 55% Analysis Date = 07/13/22 Pct Recovery = 55% Analysis Date = 07/09/22 Pct Recovery = 55% Analysis Date = 07/09/22 Pct Recovery = 55% Analysis Date = 07/05/22 Pct Recovery = 56% Analysis Date = 07/05/22 Pct Recovery = 56% Analysis Date = 07/01/22 Pct Recovery = 56% Analysis Date = 07/01/22 Pct Recovery = 56% Analysis Date = 06/26/22 Pct Recovery = 57% Analysis Date = 06/26/22 Pct Recovery = 57% Analysis Date = 06/22/22 Pct Recovery = 57% Analysis Date = 06/22/22 Pct Recovery = 57% Analysis Date = 06/18/22 Pct Recovery = 57% Analysis Date = 06/18/22 Pct Recovery = 57% Analysis Date = 06/14/22 Pct Recovery = 58% Analysis Date = 06/14/22 Pct Recovery = 58% Analysis Date = 06/10/22 Pct Recovery = 58% Analysis Date = 06/10/22 Pct Recovery = 58% Analysis Date = 06/06/22 Pct Recovery = 58% Analysis Date = 06/06/22 Pct Recovery = 58% Analysis Date = 06/02/22 Pct Recovery = 59% Analysis Date = 06/02/22 Pct Recovery = 59% Analysis Date = 05/29/22 Pct Recovery = 59% Analysis Date = 05/29/22 Pct Recovery = 59% Analysis Date = 05/25/22 Pct Recovery = 60% Analysis Date = 05/25/22 Pct Recovery = 60% Analysis Date = 05/21/22 Pct Recovery = 60% Analysis Date = 05/21/22 Pct Recovery = 60% Analysis Date = 05/17/22 Pct Recovery = 60% Analysis Date = 05/17/22 Pct Recovery = 60% Analysis Date = 05/12/22 Pct Recovery = 61% Analysis Date = 05/12/22 Pct Recovery = 61% Analysis Date = 05/08/22 Pct Recovery = 61% Analysis Date = 05/08/22 Pct Recovery = 61% Analysis Date = 05/04/22 Pct Recovery = 62% Analysis Date = 05/04/22 Pct Recovery = 62% Analysis Date = 04/30/22 Pct Recovery = 62% Analysis Date = 04/30/22 Pct Recovery = 62% Analysis Date = 04/26/22 Pct Recovery = 62% Analysis Date = 04/26/22 Pct Recovery = 62% Analysis Date = 04/22/22 Pct Recovery = 63% Analysis Date = 04/22/22 Pct Recovery = 63% Analysis Date = 04/18/22 Pct Recovery = 63% Analysis Date = 04/18/22 Pct Recovery = 63% Analysis Date = 04/14/22 Pct Recovery = 63% Analysis Date = 04/14/22 Pct Recovery = 63% Analysis Date = 04/10/22 Pct Recovery = 64% Analysis Date = 04/10/22 Pct Recovery = 64% Analysis Date = 04/06/22 Pct Recovery = 64% Analysis Date = 04/06/22 Pct Recovery = 64% Analysis Date = 04/02/22 Pct Recovery = 65% Analysis Date = 04/02/22 Pct Recovery = 65% Analysis Date = 03/28/22 Pct Recovery = 65% Analysis Date = 03/28/22 Pct Recovery = 65% Analysis Date = 03/24/22 Pct Recovery = 65% Analysis Date = 03/24/22 Pct Recovery = 65% Analysis Date = 03/20/22 Pct Recovery = 66% Analysis Date = 03/20/22 Pct Recovery = 66% Analysis Date = 03/16/22 Pct Recovery = 66% Analysis Date = 03/16/22 Pct Recovery = 66% Analysis Date = 03/12/22 Pct Recovery = 66% Analysis Date = 03/12/22 Pct Recovery = 66% Analysis Date = 03/08/22 Pct Recovery = 67% Analysis Date = 03/08/22 Pct Recovery = 67% Analysis Date = 03/04/22 Pct Recovery = 67% Analysis Date = 03/04/22 Pct Recovery = 67% Analysis Date = 02/28/22 Pct Recovery = 68% Analysis Date = 02/28/22 Pct Recovery = 68% Analysis Date = 02/24/22 Pct Recovery = 68% Analysis Date = 02/24/22 Pct Recovery = 68% Analysis Date = 02/20/22 Pct Recovery = 68% Analysis Date = 02/20/22 Pct Recovery = 68% Analysis Date = 02/16/22 Pct Recovery = 69% Analysis Date = 02/16/22 Pct Recovery = 69% Analysis Date = 02/11/22 Pct Recovery = 69% Analysis Date = 02/11/22 Pct Recovery = 69% Analysis Date = 02/07/22 Pct Recovery = 70% Analysis Date = 02/07/22 Pct Recovery = 70% Analysis Date = 02/03/22 Pct Recovery = 70% Analysis Date = 02/03/22 Pct Recovery = 70% Analysis Date = 01/30/22 Pct Recovery = 70% Analysis Date = 01/30/22 Pct Recovery = 70% Analysis Date = 01/26/22 Pct Recovery = 71% Analysis Date = 01/26/22 Pct Recovery = 71% Analysis Date = 01/22/22 Pct Recovery = 71% Analysis Date = 01/22/22 Pct Recovery = 71% Analysis Date = 01/18/22 Pct Recovery = 71% Analysis Date = 01/18/22 Pct Recovery = 71% Analysis Date = 01/14/22 Pct Recovery = 72% Analysis Date = 01/14/22 Pct Recovery = 72% Analysis Date = 01/10/22 Pct Recovery = 72% Analysis Date = 01/10/22 Pct Recovery = 72% Analysis Date = 01/06/22 Pct Recovery = 72% Analysis Date = 01/06/22 Pct Recovery = 72% Analysis Date = 01/02/22 Pct Recovery = 73% Analysis Date = 01/02/22 Pct Recovery = 73% Analysis Date = 12/28/21 Pct Recovery = 73% Analysis Date = 12/28/21 Pct Recovery = 73% Analysis Date = 12/24/21 Pct Recovery = 73% Analysis Date = 12/24/21 Pct Recovery = 73% Analysis Date = 12/20/21 Pct Recovery = 74% Analysis Date = 12/20/21 Pct Recovery = 74% Analysis Date = 12/16/21 Pct Recovery = 74% Analysis Date = 12/16/21 Pct Recovery = 74% Analysis Date = 12/12/21 Pct Recovery = 74% Analysis Date = 12/12/21 Pct Recovery = 74% Analysis Date = 12/08/21 Pct Recovery = 75% Analysis Date = 12/08/21 Pct Recovery = 75% Analysis Date = 12/04/21 Pct Recovery = 75% Analysis Date = 12/04/21 Pct Recovery = 75% Analysis Date = 11/30/21 Pct Recovery = 76% Analysis Date = 11/30/21 Pct Recovery = 76% Analysis Date = 11/26/21 Pct Recovery = 76% Analysis Date = 11/26/21 Pct Recovery = 76% Analysis Date = 11/22/21 Pct Recovery = 76% Analysis Date = 11/22/21 Pct Recovery = 76% Analysis Date = 11/18/21 Pct Recovery = 77% Analysis Date = 11/18/21 Pct Recovery = 77% Analysis Date = 11/13/21 Pct Recovery = 77% Analysis Date = 11/13/21 Pct Recovery = 77% Analysis Date = 11/09/21 Pct Recovery = 78% Analysis Date = 11/09/21 Pct Recovery = 78% Analysis Date = 11/05/21 Pct Recovery = 78% Analysis Date = 11/05/21 Pct Recovery = 78% Analysis Date = 11/01/21 Pct Recovery = 78% Analysis Date = 11/01/21 Pct Recovery = 78% Analysis Date = 10/28/21 Pct Recovery = 79% Analysis Date = 10/28/21 Pct Recovery = 79% Analysis Date = 10/24/21 Pct Recovery = 79% Analysis Date = 10/24/21 Pct Recovery = 79% Analysis Date = 10/20/21 Pct Recovery = 80% Analysis Date = 10/20/21 Pct Recovery = 80% Analysis Date = 10/16/21 Pct Recovery = 80% Analysis Date = 10/16/21 Pct Recovery = 80% Analysis Date = 10/12/21 Pct Recovery = 81% Analysis Date = 10/12/21 Pct Recovery = 81% Analysis Date = 10/08/21 Pct Recovery = 81% Analysis Date = 10/08/21 Pct Recovery = 81% Analysis Date = 10/04/21 Pct Recovery = 81% Analysis Date = 10/04/21 Pct Recovery = 81% Analysis Date = 09/29/21 Pct Recovery = 82% Analysis Date = 09/29/21 Pct Recovery = 82% Analysis Date = 09/25/21 Pct Recovery = 82% Analysis Date = 09/25/21 Pct Recovery = 82% Analysis Date = 09/21/21 Pct Recovery = 83% Analysis Date = 09/21/21 Pct Recovery = 83% Analysis Date = 09/17/21 Pct Recovery = 83% Analysis Date = 09/17/21 Pct Recovery = 83% Analysis Date = 09/13/21 Pct Recovery = 84% Analysis Date = 09/13/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/09/21 Pct Recovery = 84% Analysis Date = 09/05/21 Pct Recovery = 84% Analysis Date = 09/05/21 Pct Recovery = 84% Analysis Date = 09/01/21 Pct Recovery = 85% Analysis Date = 09/01/21 Pct Recovery = 85% Analysis Date = 08/28/21 Pct Recovery = 85% Analysis Date = 08/28/21 Pct Recovery = 85% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 87% Analysis Date = 08/15/21 Pct Recovery = 87% Analysis Date = 08/11/21 Pct Recovery = 87% Analysis Date = 08/11/21 Pct Recovery = 87% Analysis Date = 08/07/21 Pct Recovery = 87% Analysis Date = 08/07/21 Pct Recovery = 87% Analysis Date = 08/03/21 Pct Recovery = 88% Analysis Date = 08/03/21 Pct Recovery = 88% Analysis Date = 07/30/21 Pct Recovery = 88% Analysis Date = 07/30/21 Pct Recovery = 88% Analysis Date = 07/26/21 Pct Recovery = 89% Analysis Date = 07/26/21 Pct Recovery = 89% Analysis Date = 07/22/21 Pct Recovery = 89% Analysis Date = 07/22/21 Pct Recovery = 89% Analysis Date = 07/18/21 Pct Recovery = 90% Analysis Date = 07/18/21 Pct Recovery = 90% Analysis Date = 07/14/21 Pct Recovery = 90% Analysis Date = 07/14/21 Pct Recovery = 90% Analysis Date = 07/10/21 Pct Recovery = 91% Analysis Date = 07/10/21 Pct Recovery = 91% Analysis Date = 07/06/21 Pct Recovery = 91% Analysis Date = 07/06/21 Pct Recovery = 91% Analysis Date = 07/02/21 Pct Recovery = 91% Analysis Date = 07/02/21 Pct Recovery = 91% Analysis Date = 06/27/21 Pct Recovery = 92% Analysis Date = 06/27/21 Pct Recovery = 92% Analysis Date = 06/23/21 Pct Recovery = 92% Analysis Date = 06/23/21 Pct Recovery = 92% Analysis Date = 06/19/21 Pct Recovery = 93% Analysis Date = 06/19/21 Pct Recovery = 93% Analysis Date = 06/15/21 Pct Recovery = 93% Analysis Date = 06/15/21 Pct Recovery = 93% Analysis Date = 06/11/21 Pct Recovery = 94% Analysis Date = 06/11/21 Pct Recovery = 94% Analysis Date = 06/07/21 Pct Recovery = 94% Analysis Date = 06/07/21 Pct Recovery = 94% Analysis Date = 06/03/21 Pct Recovery = 94% Analysis Date = 06/03/21 Pct Recovery = 94% Analysis Date = 05/30/21 Pct Recovery = 95% Analysis Date = 05/30/21 Pct Recovery = 95% Analysis Date = 05/26/21 Pct Recovery = 95% Analysis Date = 05/26/21 Pct Recovery = 95% Analysis Date = 05/22/21 Pct Recovery = 96% Analysis Date = 05/22/21 Pct Recovery = 96% Analysis Date = 05/18/21 Pct Recovery = 96% Analysis Date = 05/18/21 Pct Recovery = 96% Analysis Date = 05/13/21 Pct Recovery = 97% Analysis Date = 05/13/21 Pct Recovery = 97% Analysis Date = 05/09/21 Pct Recovery = 97% Analysis Date = 05/09/21 Pct Recovery = 97% Analysis Date = 05/05/21 Pct Recovery = 97% Analysis Date = 05/05/21 Pct Recovery = 97% Analysis Date = 05/01/21 Pct Recovery = 98% Analysis Date = 05/01/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/27/21 Pct Recovery = 98% Analysis Date = 04/23/21 Pct Recovery = 99% Analysis Date = 04/23/21 Pct Recovery = 99% Analysis Date = 04/19/21 Pct Recovery = 99% Analysis Date = 04/19/21 Pct Recovery = 99% Analysis Date = 04/15/21 Pct Recovery = 100% Analysis Date = 04/15/21 Pct Recovery = 100% Analysis Date = 04/11/21 Pct Recovery = 100% Analysis Date = 04/11/21 Pct Recovery = 100% Analysis Date = 04/07/21 Pct Recovery = 100% Analysis Date = 04/07/21 Pct Recovery = 100% Analysis Date = 04/03/21 Pct Recovery = 101% Analysis Date = 04/03/21 Pct Recovery = 101% Analysis Date = 03/29/21 Pct Recovery = 101% Analysis Date = 03/29/21 Pct Recovery = 101% Analysis Date = 03/25/21 Pct Recovery = 102% Analysis Date = 03/25/21 Pct Recovery = 102% Analysis Date = 03/21/21 Pct Recovery = 101% Analysis Date = 03/21/21 Pct Recovery = 101% Analysis Date = 03/17/21 Pct Recovery = 101% Analysis Date = 03/17/21 Pct Recovery = 101% Analysis Date = 03/13/21 Pct Recovery = 101% Analysis Date = 03/13/21 Pct Recovery = 101% Analysis Date = 03/09/21 Pct Recovery = 100% Analysis Date = 03/09/21 Pct Recovery = 100% Analysis Date = 03/05/21 Pct Recovery = 100% Analysis Date = 03/05/21 Pct Recovery = 100% Analysis Date = 03/01/21 Pct Recovery = 100% Analysis Date = 03/01/21 Pct Recovery = 100% Analysis Date = 02/25/21 Pct Recovery = 99% Analysis Date = 02/25/21 Pct Recovery = 99% Analysis Date = 02/21/21 Pct Recovery = 99% Analysis Date = 02/21/21 Pct Recovery = 99% Analysis Date = 02/17/21 Pct Recovery = 99% Analysis Date = 02/17/21 Pct Recovery = 99% Analysis Date = 02/12/21 Pct Recovery = 99% Analysis Date = 02/12/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/08/21 Pct Recovery = 98% Analysis Date = 02/04/21 Pct Recovery = 98% Analysis Date = 02/04/21 Pct Recovery = 98% Analysis Date = 01/31/21 Pct Recovery = 98% Analysis Date = 01/31/21 Pct Recovery = 98% Analysis Date = 01/27/21 Pct Recovery = 98% Analysis Date = 01/27/21 Pct Recovery = 98% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/23/21 Pct Recovery = 97% Analysis Date = 01/19/21 Pct Recovery = 97% Analysis Date = 01/19/21 Pct Recovery = 97% Analysis Date = 01/15/21 Pct Recovery = 97% Analysis Date = 01/15/21 Pct Recovery = 97% Analysis Date = 01/11/21 Pct Recovery = 97% Analysis Date = 01/11/21 Pct Recovery = 97% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/25/20 Pct Recovery = 96% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 95% Analysis Date = 12/13/20 Pct Recovery = 95% Analysis Date = 12/09/20 Pct Recovery = 95% Analysis Date = 12/09/20 Pct Recovery = 95% Analysis Date = 12/05/20 Pct Recovery = 94% Analysis Date = 12/05/20 Pct Recovery = 94% Analysis Date = 12/01/20 Pct Recovery = 94% Analysis Date = 12/01/20 Pct Recovery = 94% Analysis Date = 11/27/20 Pct Recovery = 94% Analysis Date = 11/27/20 Pct Recovery = 94% Analysis Date = 11/23/20 Pct Recovery = 94% Analysis Date = 11/23/20 Pct Recovery = 94% Analysis Date = 11/19/20 Pct Recovery = 93% Analysis Date = 11/19/20 Pct Recovery = 93% Analysis Date = 11/14/20 Pct Recovery = 93% Analysis Date = 11/14/20 Pct Recovery = 93% Analysis Date = 11/10/20 Pct Recovery = 93% Analysis Date = 11/10/20 Pct Recovery = 93% Analysis Date = 11/06/20 Pct Recovery = 93% Analysis Date = 11/06/20 Pct Recovery = 93% Analysis Date = 11/02/20 Pct Recovery = 92% Analysis Date = 11/02/20 Pct Recovery = 92% Analysis Date = 10/29/20 Pct Recovery = 92% Analysis Date = 10/29/20 Pct Recovery = 92% Analysis Date = 10/25/20 Pct Recovery = 92% Analysis Date = 10/25/20 Pct Recovery = 92% Analysis Date = 10/21/20 Pct Recovery = 92% Analysis Date = 10/21/20 Pct Recovery = 92% Analysis Date = 10/17/20 Pct Recovery = 92% Analysis Date = 10/17/20 Pct Recovery = 92% Analysis Date = 10/13/20 Pct Recovery = 92% Analysis Date = 10/13/20 Pct Recovery = 92% Analysis Date = 10/09/20 Pct Recovery = 91% Analysis Date = 10/09/20 Pct Recovery = 91% Analysis Date = 10/05/20 Pct Recovery = 91% Analysis Date = 10/05/20 Pct Recovery = 91% Analysis Date = 09/30/20 Pct Recovery = 91% Analysis Date = 09/30/20 Pct Recovery = 91% Analysis Date = 09/26/20 Pct Recovery = 91% Analysis Date = 09/26/20 Pct Recovery = 91% Analysis Date = 09/22/20 Pct Recovery = 91% Analysis Date = 09/22/20 Pct Recovery = 91% Analysis Date = 09/18/20 Pct Recovery = 91% Analysis Date = 09/18/20 Pct Recovery = 91% Analysis Date = 09/14/20 Pct Recovery = 90% Analysis Date = 09/14/20 Pct Recovery = 90% Analysis Date = 09/10/20 Pct Recovery = 90% Analysis Date = 09/10/20 Pct Recovery = 90% Analysis Date = 09/06/20 Pct Recovery = 90% Analysis Date = 09/06/20 Pct Recovery = 90% Analysis Date = 09/02/20 Pct Recovery = 90% Analysis Date = 09/02/20 Pct Recovery = 90% Analysis Date = 08/29/20 Pct Recovery = 90% Analysis Date = 08/29/20 Pct Recovery = 90% Analysis Date = 08/25/20 Pct Recovery = 90% Analysis Date = 08/25/20 Pct Recovery = 90% Analysis Date = 08/21/20 Pct Recovery = 90% Analysis Date = 08/21/20 Pct Recovery = 90% Analysis Date = 08/16/20 Pct Recovery = 90% Analysis Date = 08/16/20 Pct Recovery = 90% Analysis Date = 08/12/20 Pct Recovery = 90% Analysis Date = 08/12/20 Pct Recovery = 90% Analysis Date = 08/08/20 Pct Recovery = 90% Analysis Date = 08/08/20 Pct Recovery = 90% Analysis Date = 08/04/20 Pct Recovery = 90% Analysis Date = 08/04/20 Pct Recovery = 90% Analysis Date = 07/31/20 Pct Recovery = 90% Analysis Date = 07/31/20 Pct Recovery = 90% Analysis Date = 07/27/20 Pct Recovery = 89% Analysis Date = 07/27/20 Pct Recovery = 89% Analysis Date = 07/23/20 Pct Recovery = 89% Analysis Date = 07/23/20 Pct Recovery = 89% Analysis Date = 07/19/20 Pct Recovery = 89% Analysis Date = 07/19/20 Pct Recovery = 89% Analysis Date = 07/15/20 Pct Recovery = 89% Analysis Date = 07/15/20 Pct Recovery = 89% Analysis Date = 07/11/20 Pct Recovery = 89% Analysis Date = 07/11/20 Pct Recovery = 89% Analysis Date = 07/07/20 Pct Recovery = 89% Analysis Date = 07/07/20 Pct Recovery = 89% Analysis Date = 07/02/20 Pct Recovery = 89% Analysis Date = 07/02/20 Pct Recovery = 89% Analysis Date = 06/28/20 Pct Recovery = 89% Analysis Date = 06/28/20 Pct Recovery = 89% Analysis Date = 06/24/20 Pct Recovery = 89% Analysis Date = 06/24/20 Pct Recovery = 89% Analysis Date = 06/20/20 Pct Recovery = 89% Analysis Date = 06/20/20 Pct Recovery = 89% Analysis Date = 06/16/20 Pct Recovery = 89% Analysis Date = 06/16/20 Pct Recovery = 89% Analysis Date = 06/12/20 Pct Recovery = 89% Analysis Date = 06/12/20 Pct Recovery = 89% Analysis Date = 06/08/20 Pct Recovery = 89% Analysis Date = 06/08/20 Pct Recovery = 89% Analysis Date = 06/04/20 Pct Recovery = 88% Analysis Date = 06/04/20 Pct Recovery = 88% Analysis Date = 05/31/20 Pct Recovery = 88% Analysis Date = 05/31/20 Pct Recovery = 88% Analysis Date = 05/27/20 Pct Recovery = 88% Analysis Date = 05/27/20 Pct Recovery = 88% Analysis Date = 05/23/20 Pct Recovery = 88% Analysis Date = 05/23/20 Pct Recovery = 88% Analysis Date = 05/19/20 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SULFOMETURON-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 85% 25% 88% 17%
Total 42 85% 25% 88% 17%

Sample Statistics
SULFOMETURON-METHYL

Characteristic N % % Basis
Plotted 42 93% Spiked
Estimated Values 6 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 4% Spiked
Spiked 45 .  
False Negatives 1 2% 1 out of 45
Not Spiked 71 .  
False Positives 0 0% 0 out of 71

OBSP Determination:
TEBUCONAZOLE
METHOD: 2447 , TESTIDCODE: 66649LCM60

Laboratory ID = 20202390020 Lab Value = 233.510 Expected Conc. = 190 Report level label = 15 Pct Recovery = 123% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20210760015 Lab Value = 146.395 Expected Conc. = 188.8 Report level label = 15 Pct Recovery = 78% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 148.910 Expected Conc. = 188.8 Report level label = 15 Pct Recovery = 79% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 141.270 Expected Conc. = 188.8 Report level label = 15 Pct Recovery = 75% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 170.649 Expected Conc. = 188.8 Report level label = 15 Pct Recovery = 90% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201820155 Lab Value = 154.135 Expected Conc. = 187.6 Report level label = 15 Pct Recovery = 82% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 203.850 Expected Conc. = 187.6 Report level label = 15 Pct Recovery = 109% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203080100 Lab Value = 159.453 Expected Conc. = 185.8 Report level label = 15 Pct Recovery = 86% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 167.599 Expected Conc. = 185.8 Report level label = 15 Pct Recovery = 90% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 161.554 Expected Conc. = 185.8 Report level label = 15 Pct Recovery = 87% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221520237 Lab Value = 140.842 Expected Conc. = 150.16 Report level label = 15 Pct Recovery = 94% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 102.702 Expected Conc. = 150 Report level label = 15 Pct Recovery = 68% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 108.189 Expected Conc. = 149.2 Report level label = 15 Pct Recovery = 73% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20201960104 Lab Value = 101.051 Expected Conc. = 95 Report level label = 15 Pct Recovery = 106% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20210480001 Lab Value = 70.609 Expected Conc. = 94.4 Report level label = 15 Pct Recovery = 75% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221870197 Lab Value = 65.111 Expected Conc. = 93.85 Report level label = 15 Pct Recovery = 69% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20202530029 Lab Value = 77.927 Expected Conc. = 93.8 Report level label = 15 Pct Recovery = 83% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 73.010 Expected Conc. = 93.8 Report level label = 15 Pct Recovery = 78% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 96.745 Expected Conc. = 93.8 Report level label = 15 Pct Recovery = 103% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20220740064 Lab Value = 71.781 Expected Conc. = 93.5 Report level label = 15 Pct Recovery = 77% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202880004 Lab Value = 90.554 Expected Conc. = 92.9 Report level label = 15 Pct Recovery = 97% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 58.796 Expected Conc. = 75.52 Report level label = 15 Pct Recovery = 78% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 64.955 Expected Conc. = 74.32 Report level label = 15 Pct Recovery = 87% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 60.807 Expected Conc. = 74.32 Report level label = 15 Pct Recovery = 82% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 35.247 Expected Conc. = 38 Report level label = 15 Pct Recovery = 93% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210690067 Lab Value = 32.644 Expected Conc. = 37.76 Report level label = 15 Pct Recovery = 86% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221660151 Lab Value = 29.658 Expected Conc. = 37.54 Report level label = 15 Pct Recovery = 79% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20202180001 Lab Value = 24.796 Expected Conc. = 37.52 Report level label = 15 Pct Recovery = 66% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 33.751 Expected Conc. = 37.52 Report level label = 15 Pct Recovery = 90% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 32.168 Expected Conc. = 37.52 Report level label = 15 Pct Recovery = 86% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210120050 Lab Value = 31.783 Expected Conc. = 37.16 Report level label = 15 Pct Recovery = 86% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 29.434 Expected Conc. = 37.16 Report level label = 15 Pct Recovery = 79% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 29.153 Expected Conc. = 37.16 Report level label = 15 Pct Recovery = 78% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 38.304 Expected Conc. = 37.16 Report level label = 15 Pct Recovery = 103% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 29.533 Expected Conc. = 37.16 Report level label = 15 Pct Recovery = 79% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/02/22 Pct Recovery = 76% Analysis Date = 08/02/22 Pct Recovery = 76% Analysis Date = 07/29/22 Pct Recovery = 76% Analysis Date = 07/29/22 Pct Recovery = 76% Analysis Date = 07/25/22 Pct Recovery = 76% Analysis Date = 07/25/22 Pct Recovery = 76% Analysis Date = 07/21/22 Pct Recovery = 76% Analysis Date = 07/21/22 Pct Recovery = 76% Analysis Date = 07/17/22 Pct Recovery = 76% Analysis Date = 07/17/22 Pct Recovery = 76% Analysis Date = 07/13/22 Pct Recovery = 76% Analysis Date = 07/13/22 Pct Recovery = 76% Analysis Date = 07/09/22 Pct Recovery = 76% Analysis Date = 07/09/22 Pct Recovery = 76% Analysis Date = 07/05/22 Pct Recovery = 76% Analysis Date = 07/05/22 Pct Recovery = 76% Analysis Date = 07/01/22 Pct Recovery = 76% Analysis Date = 07/01/22 Pct Recovery = 76% Analysis Date = 06/26/22 Pct Recovery = 76% Analysis Date = 06/26/22 Pct Recovery = 76% Analysis Date = 06/22/22 Pct Recovery = 76% Analysis Date = 06/22/22 Pct Recovery = 76% Analysis Date = 06/18/22 Pct Recovery = 76% Analysis Date = 06/18/22 Pct Recovery = 76% Analysis Date = 06/14/22 Pct Recovery = 76% Analysis Date = 06/14/22 Pct Recovery = 76% Analysis Date = 06/10/22 Pct Recovery = 77% Analysis Date = 06/10/22 Pct Recovery = 77% Analysis Date = 06/06/22 Pct Recovery = 77% Analysis Date = 06/06/22 Pct Recovery = 77% Analysis Date = 06/02/22 Pct Recovery = 77% Analysis Date = 06/02/22 Pct Recovery = 77% Analysis Date = 05/29/22 Pct Recovery = 77% Analysis Date = 05/29/22 Pct Recovery = 77% Analysis Date = 05/25/22 Pct Recovery = 77% Analysis Date = 05/25/22 Pct Recovery = 77% Analysis Date = 05/21/22 Pct Recovery = 77% Analysis Date = 05/21/22 Pct Recovery = 77% Analysis Date = 05/17/22 Pct Recovery = 77% Analysis Date = 05/17/22 Pct Recovery = 77% Analysis Date = 05/12/22 Pct Recovery = 77% Analysis Date = 05/12/22 Pct Recovery = 77% Analysis Date = 05/08/22 Pct Recovery = 77% Analysis Date = 05/08/22 Pct Recovery = 77% Analysis Date = 05/04/22 Pct Recovery = 77% Analysis Date = 05/04/22 Pct Recovery = 77% Analysis Date = 04/30/22 Pct Recovery = 77% Analysis Date = 04/30/22 Pct Recovery = 77% Analysis Date = 04/26/22 Pct Recovery = 77% Analysis Date = 04/26/22 Pct Recovery = 77% Analysis Date = 04/22/22 Pct Recovery = 77% Analysis Date = 04/22/22 Pct Recovery = 77% Analysis Date = 04/18/22 Pct Recovery = 77% Analysis Date = 04/18/22 Pct Recovery = 77% Analysis Date = 04/14/22 Pct Recovery = 77% Analysis Date = 04/14/22 Pct Recovery = 77% Analysis Date = 04/10/22 Pct Recovery = 77% Analysis Date = 04/10/22 Pct Recovery = 77% Analysis Date = 04/06/22 Pct Recovery = 77% Analysis Date = 04/06/22 Pct Recovery = 77% Analysis Date = 04/02/22 Pct Recovery = 77% Analysis Date = 04/02/22 Pct Recovery = 77% Analysis Date = 03/28/22 Pct Recovery = 77% Analysis Date = 03/28/22 Pct Recovery = 77% Analysis Date = 03/24/22 Pct Recovery = 77% Analysis Date = 03/24/22 Pct Recovery = 77% Analysis Date = 03/20/22 Pct Recovery = 77% Analysis Date = 03/20/22 Pct Recovery = 77% Analysis Date = 03/16/22 Pct Recovery = 77% Analysis Date = 03/16/22 Pct Recovery = 77% Analysis Date = 03/12/22 Pct Recovery = 77% Analysis Date = 03/12/22 Pct Recovery = 77% Analysis Date = 03/08/22 Pct Recovery = 77% Analysis Date = 03/08/22 Pct Recovery = 77% Analysis Date = 03/04/22 Pct Recovery = 77% Analysis Date = 03/04/22 Pct Recovery = 77% Analysis Date = 02/28/22 Pct Recovery = 77% Analysis Date = 02/28/22 Pct Recovery = 77% Analysis Date = 02/24/22 Pct Recovery = 77% Analysis Date = 02/24/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/20/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 77% Analysis Date = 02/16/22 Pct Recovery = 77% Analysis Date = 02/11/22 Pct Recovery = 78% Analysis Date = 02/11/22 Pct Recovery = 78% Analysis Date = 02/07/22 Pct Recovery = 78% Analysis Date = 02/07/22 Pct Recovery = 78% Analysis Date = 02/03/22 Pct Recovery = 78% Analysis Date = 02/03/22 Pct Recovery = 78% Analysis Date = 01/30/22 Pct Recovery = 78% Analysis Date = 01/30/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/26/22 Pct Recovery = 78% Analysis Date = 01/22/22 Pct Recovery = 78% Analysis Date = 01/22/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/18/22 Pct Recovery = 78% Analysis Date = 01/14/22 Pct Recovery = 78% Analysis Date = 01/14/22 Pct Recovery = 78% Analysis Date = 01/10/22 Pct Recovery = 78% Analysis Date = 01/10/22 Pct Recovery = 78% Analysis Date = 01/06/22 Pct Recovery = 78% Analysis Date = 01/06/22 Pct Recovery = 78% Analysis Date = 01/02/22 Pct Recovery = 78% Analysis Date = 01/02/22 Pct Recovery = 78% Analysis Date = 12/28/21 Pct Recovery = 78% Analysis Date = 12/28/21 Pct Recovery = 78% Analysis Date = 12/24/21 Pct Recovery = 78% Analysis Date = 12/24/21 Pct Recovery = 78% Analysis Date = 12/20/21 Pct Recovery = 78% Analysis Date = 12/20/21 Pct Recovery = 78% Analysis Date = 12/16/21 Pct Recovery = 78% Analysis Date = 12/16/21 Pct Recovery = 78% Analysis Date = 12/12/21 Pct Recovery = 78% Analysis Date = 12/12/21 Pct Recovery = 78% Analysis Date = 12/08/21 Pct Recovery = 78% Analysis Date = 12/08/21 Pct Recovery = 78% Analysis Date = 12/04/21 Pct Recovery = 78% Analysis Date = 12/04/21 Pct Recovery = 78% Analysis Date = 11/30/21 Pct Recovery = 78% Analysis Date = 11/30/21 Pct Recovery = 78% Analysis Date = 11/26/21 Pct Recovery = 78% Analysis Date = 11/26/21 Pct Recovery = 78% Analysis Date = 11/22/21 Pct Recovery = 78% Analysis Date = 11/22/21 Pct Recovery = 78% Analysis Date = 11/18/21 Pct Recovery = 78% Analysis Date = 11/18/21 Pct Recovery = 78% Analysis Date = 11/13/21 Pct Recovery = 78% Analysis Date = 11/13/21 Pct Recovery = 78% Analysis Date = 11/09/21 Pct Recovery = 78% Analysis Date = 11/09/21 Pct Recovery = 78% Analysis Date = 11/05/21 Pct Recovery = 78% Analysis Date = 11/05/21 Pct Recovery = 78% Analysis Date = 11/01/21 Pct Recovery = 78% Analysis Date = 11/01/21 Pct Recovery = 78% Analysis Date = 10/28/21 Pct Recovery = 78% Analysis Date = 10/28/21 Pct Recovery = 78% Analysis Date = 10/24/21 Pct Recovery = 78% Analysis Date = 10/24/21 Pct Recovery = 78% Analysis Date = 10/20/21 Pct Recovery = 78% Analysis Date = 10/20/21 Pct Recovery = 78% Analysis Date = 10/16/21 Pct Recovery = 78% Analysis Date = 10/16/21 Pct Recovery = 78% Analysis Date = 10/12/21 Pct Recovery = 78% Analysis Date = 10/12/21 Pct Recovery = 78% Analysis Date = 10/08/21 Pct Recovery = 79% Analysis Date = 10/08/21 Pct Recovery = 79% Analysis Date = 10/04/21 Pct Recovery = 79% Analysis Date = 10/04/21 Pct Recovery = 79% Analysis Date = 09/29/21 Pct Recovery = 79% Analysis Date = 09/29/21 Pct Recovery = 79% Analysis Date = 09/25/21 Pct Recovery = 79% Analysis Date = 09/25/21 Pct Recovery = 79% Analysis Date = 09/21/21 Pct Recovery = 79% Analysis Date = 09/21/21 Pct Recovery = 79% Analysis Date = 09/17/21 Pct Recovery = 79% Analysis Date = 09/17/21 Pct Recovery = 79% Analysis Date = 09/13/21 Pct Recovery = 79% Analysis Date = 09/13/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/09/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/05/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 09/01/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 79% Analysis Date = 08/28/21 Pct Recovery = 79% Analysis Date = 08/24/21 Pct Recovery = 79% Analysis Date = 08/24/21 Pct Recovery = 79% Analysis Date = 08/20/21 Pct Recovery = 79% Analysis Date = 08/20/21 Pct Recovery = 79% Analysis Date = 08/15/21 Pct Recovery = 79% Analysis Date = 08/15/21 Pct Recovery = 79% Analysis Date = 08/11/21 Pct Recovery = 79% Analysis Date = 08/11/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/07/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 08/03/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/30/21 Pct Recovery = 79% Analysis Date = 07/26/21 Pct Recovery = 79% Analysis Date = 07/26/21 Pct Recovery = 79% Analysis Date = 07/22/21 Pct Recovery = 79% Analysis Date = 07/22/21 Pct Recovery = 79% Analysis Date = 07/18/21 Pct Recovery = 79% Analysis Date = 07/18/21 Pct Recovery = 79% Analysis Date = 07/14/21 Pct Recovery = 79% Analysis Date = 07/14/21 Pct Recovery = 79% Analysis Date = 07/10/21 Pct Recovery = 79% Analysis Date = 07/10/21 Pct Recovery = 79% Analysis Date = 07/06/21 Pct Recovery = 79% Analysis Date = 07/06/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 07/02/21 Pct Recovery = 79% Analysis Date = 06/27/21 Pct Recovery = 79% Analysis Date = 06/27/21 Pct Recovery = 79% Analysis Date = 06/23/21 Pct Recovery = 79% Analysis Date = 06/23/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/19/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/15/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/11/21 Pct Recovery = 79% Analysis Date = 06/07/21 Pct Recovery = 80% Analysis Date = 06/07/21 Pct Recovery = 80% Analysis Date = 06/03/21 Pct Recovery = 80% Analysis Date = 06/03/21 Pct Recovery = 80% Analysis Date = 05/30/21 Pct Recovery = 80% Analysis Date = 05/30/21 Pct Recovery = 80% Analysis Date = 05/26/21 Pct Recovery = 80% Analysis Date = 05/26/21 Pct Recovery = 80% Analysis Date = 05/22/21 Pct Recovery = 80% Analysis Date = 05/22/21 Pct Recovery = 80% Analysis Date = 05/18/21 Pct Recovery = 80% Analysis Date = 05/18/21 Pct Recovery = 80% Analysis Date = 05/13/21 Pct Recovery = 80% Analysis Date = 05/13/21 Pct Recovery = 80% Analysis Date = 05/09/21 Pct Recovery = 80% Analysis Date = 05/09/21 Pct Recovery = 80% Analysis Date = 05/05/21 Pct Recovery = 80% Analysis Date = 05/05/21 Pct Recovery = 80% Analysis Date = 05/01/21 Pct Recovery = 80% Analysis Date = 05/01/21 Pct Recovery = 80% Analysis Date = 04/27/21 Pct Recovery = 80% Analysis Date = 04/27/21 Pct Recovery = 80% Analysis Date = 04/23/21 Pct Recovery = 80% Analysis Date = 04/23/21 Pct Recovery = 80% Analysis Date = 04/19/21 Pct Recovery = 80% Analysis Date = 04/19/21 Pct Recovery = 80% Analysis Date = 04/15/21 Pct Recovery = 80% Analysis Date = 04/15/21 Pct Recovery = 80% Analysis Date = 04/11/21 Pct Recovery = 80% Analysis Date = 04/11/21 Pct Recovery = 80% Analysis Date = 04/07/21 Pct Recovery = 80% Analysis Date = 04/07/21 Pct Recovery = 80% Analysis Date = 04/03/21 Pct Recovery = 80% Analysis Date = 04/03/21 Pct Recovery = 80% Analysis Date = 03/29/21 Pct Recovery = 80% Analysis Date = 03/29/21 Pct Recovery = 80% Analysis Date = 03/25/21 Pct Recovery = 80% Analysis Date = 03/25/21 Pct Recovery = 80% Analysis Date = 03/21/21 Pct Recovery = 80% Analysis Date = 03/21/21 Pct Recovery = 80% Analysis Date = 03/17/21 Pct Recovery = 80% Analysis Date = 03/17/21 Pct Recovery = 80% Analysis Date = 03/13/21 Pct Recovery = 80% Analysis Date = 03/13/21 Pct Recovery = 80% Analysis Date = 03/09/21 Pct Recovery = 81% Analysis Date = 03/09/21 Pct Recovery = 81% Analysis Date = 03/05/21 Pct Recovery = 81% Analysis Date = 03/05/21 Pct Recovery = 81% Analysis Date = 03/01/21 Pct Recovery = 81% Analysis Date = 03/01/21 Pct Recovery = 81% Analysis Date = 02/25/21 Pct Recovery = 81% Analysis Date = 02/25/21 Pct Recovery = 81% Analysis Date = 02/21/21 Pct Recovery = 81% Analysis Date = 02/21/21 Pct Recovery = 81% Analysis Date = 02/17/21 Pct Recovery = 82% Analysis Date = 02/17/21 Pct Recovery = 82% Analysis Date = 02/12/21 Pct Recovery = 82% Analysis Date = 02/12/21 Pct Recovery = 82% Analysis Date = 02/08/21 Pct Recovery = 82% Analysis Date = 02/08/21 Pct Recovery = 82% Analysis Date = 02/04/21 Pct Recovery = 82% Analysis Date = 02/04/21 Pct Recovery = 82% Analysis Date = 01/31/21 Pct Recovery = 82% Analysis Date = 01/31/21 Pct Recovery = 82% Analysis Date = 01/27/21 Pct Recovery = 83% Analysis Date = 01/27/21 Pct Recovery = 83% Analysis Date = 01/23/21 Pct Recovery = 83% Analysis Date = 01/23/21 Pct Recovery = 83% Analysis Date = 01/19/21 Pct Recovery = 83% Analysis Date = 01/19/21 Pct Recovery = 83% Analysis Date = 01/15/21 Pct Recovery = 83% Analysis Date = 01/15/21 Pct Recovery = 83% Analysis Date = 01/11/21 Pct Recovery = 84% Analysis Date = 01/11/21 Pct Recovery = 84% Analysis Date = 01/07/21 Pct Recovery = 84% Analysis Date = 01/07/21 Pct Recovery = 84% Analysis Date = 01/03/21 Pct Recovery = 84% Analysis Date = 01/03/21 Pct Recovery = 84% Analysis Date = 12/29/20 Pct Recovery = 84% Analysis Date = 12/29/20 Pct Recovery = 84% Analysis Date = 12/25/20 Pct Recovery = 84% Analysis Date = 12/25/20 Pct Recovery = 84% Analysis Date = 12/21/20 Pct Recovery = 85% Analysis Date = 12/21/20 Pct Recovery = 85% Analysis Date = 12/17/20 Pct Recovery = 85% Analysis Date = 12/17/20 Pct Recovery = 85% Analysis Date = 12/13/20 Pct Recovery = 85% Analysis Date = 12/13/20 Pct Recovery = 85% Analysis Date = 12/09/20 Pct Recovery = 85% Analysis Date = 12/09/20 Pct Recovery = 85% Analysis Date = 12/05/20 Pct Recovery = 86% Analysis Date = 12/05/20 Pct Recovery = 86% Analysis Date = 12/01/20 Pct Recovery = 86% Analysis Date = 12/01/20 Pct Recovery = 86% Analysis Date = 11/27/20 Pct Recovery = 86% Analysis Date = 11/27/20 Pct Recovery = 86% Analysis Date = 11/23/20 Pct Recovery = 86% Analysis Date = 11/23/20 Pct Recovery = 86% Analysis Date = 11/19/20 Pct Recovery = 87% Analysis Date = 11/19/20 Pct Recovery = 87% Analysis Date = 11/14/20 Pct Recovery = 87% Analysis Date = 11/14/20 Pct Recovery = 87% Analysis Date = 11/10/20 Pct Recovery = 87% Analysis Date = 11/10/20 Pct Recovery = 87% Analysis Date = 11/06/20 Pct Recovery = 88% Analysis Date = 11/06/20 Pct Recovery = 88% Analysis Date = 11/02/20 Pct Recovery = 88% Analysis Date = 11/02/20 Pct Recovery = 88% Analysis Date = 10/29/20 Pct Recovery = 88% Analysis Date = 10/29/20 Pct Recovery = 88% Analysis Date = 10/25/20 Pct Recovery = 88% Analysis Date = 10/25/20 Pct Recovery = 88% Analysis Date = 10/21/20 Pct Recovery = 89% Analysis Date = 10/21/20 Pct Recovery = 89% Analysis Date = 10/17/20 Pct Recovery = 89% Analysis Date = 10/17/20 Pct Recovery = 89% Analysis Date = 10/13/20 Pct Recovery = 89% Analysis Date = 10/13/20 Pct Recovery = 89% Analysis Date = 10/09/20 Pct Recovery = 89% Analysis Date = 10/09/20 Pct Recovery = 89% Analysis Date = 10/05/20 Pct Recovery = 89% Analysis Date = 10/05/20 Pct Recovery = 89% Analysis Date = 09/30/20 Pct Recovery = 89% Analysis Date = 09/30/20 Pct Recovery = 89% Analysis Date = 09/26/20 Pct Recovery = 89% Analysis Date = 09/26/20 Pct Recovery = 89% Analysis Date = 09/22/20 Pct Recovery = 89% Analysis Date = 09/22/20 Pct Recovery = 89% Analysis Date = 09/18/20 Pct Recovery = 90% Analysis Date = 09/18/20 Pct Recovery = 90% Analysis Date = 09/14/20 Pct Recovery = 90% Analysis Date = 09/14/20 Pct Recovery = 90% Analysis Date = 09/10/20 Pct Recovery = 90% Analysis Date = 09/10/20 Pct Recovery = 90% Analysis Date = 09/06/20 Pct Recovery = 90% Analysis Date = 09/06/20 Pct Recovery = 90% Analysis Date = 09/02/20 Pct Recovery = 90% Analysis Date = 09/02/20 Pct Recovery = 90% Analysis Date = 08/29/20 Pct Recovery = 91% Analysis Date = 08/29/20 Pct Recovery = 91% Analysis Date = 08/25/20 Pct Recovery = 91% Analysis Date = 08/25/20 Pct Recovery = 91% Analysis Date = 08/21/20 Pct Recovery = 91% Analysis Date = 08/21/20 Pct Recovery = 91% Analysis Date = 08/16/20 Pct Recovery = 91% Analysis Date = 08/16/20 Pct Recovery = 91% Analysis Date = 08/12/20 Pct Recovery = 92% Analysis Date = 08/12/20 Pct Recovery = 92% Analysis Date = 08/08/20 Pct Recovery = 92% Analysis Date = 08/08/20 Pct Recovery = 92% Analysis Date = 08/04/20 Pct Recovery = 92% Analysis Date = 08/04/20 Pct Recovery = 92% Analysis Date = 07/31/20 Pct Recovery = 92% Analysis Date = 07/31/20 Pct Recovery = 92% Analysis Date = 07/27/20 Pct Recovery = 93% Analysis Date = 07/27/20 Pct Recovery = 93% Analysis Date = 07/23/20 Pct Recovery = 93% Analysis Date = 07/23/20 Pct Recovery = 93% Analysis Date = 07/19/20 Pct Recovery = 93% Analysis Date = 07/19/20 Pct Recovery = 93% Analysis Date = 07/15/20 Pct Recovery = 93% Analysis Date = 07/15/20 Pct Recovery = 93% Analysis Date = 07/11/20 Pct Recovery = 94% Analysis Date = 07/11/20 Pct Recovery = 94% Analysis Date = 07/07/20 Pct Recovery = 94% Analysis Date = 07/07/20 Pct Recovery = 94% Analysis Date = 07/02/20 Pct Recovery = 94% Analysis Date = 07/02/20 Pct Recovery = 94% Analysis Date = 06/28/20 Pct Recovery = 95% Analysis Date = 06/28/20 Pct Recovery = 95% Analysis Date = 06/24/20 Pct Recovery = 95% Analysis Date = 06/24/20 Pct Recovery = 95% Analysis Date = 06/20/20 Pct Recovery = 95% Analysis Date = 06/20/20 Pct Recovery = 95% Analysis Date = 06/16/20 Pct Recovery = 95% Analysis Date = 06/16/20 Pct Recovery = 95% Analysis Date = 06/12/20 Pct Recovery = 96% Analysis Date = 06/12/20 Pct Recovery = 96% Analysis Date = 06/08/20 Pct Recovery = 96% Analysis Date = 06/08/20 Pct Recovery = 96% Analysis Date = 06/04/20 Pct Recovery = 96% Analysis Date = 06/04/20 Pct Recovery = 96% Analysis Date = 05/31/20 Pct Recovery = 96% Analysis Date = 05/31/20 Pct Recovery = 96% Analysis Date = 05/27/20 Pct Recovery = 97% Analysis Date = 05/27/20 Pct Recovery = 97% Analysis Date = 05/23/20 Pct Recovery = 97% Analysis Date = 05/23/20 Pct Recovery = 97% Analysis Date = 05/19/20 Pct Recovery = 97% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 86% 12% 83% 9%
Total 35 86% 12% 83% 9%

Sample Statistics
TEBUCONAZOLE

Characteristic N % % Basis
Plotted 35 100% Spiked
Estimated Values 3 9% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
TEBUPIRIMPHOS (PHOSTEBUPIRIM)
METHOD: 2447 , TESTIDCODE: 68693LCM60

Laboratory ID = 20202590106 Lab Value = 22.261 Expected Conc. = 25.1 Report level label = 2 Pct Recovery = 89% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 23.595 Expected Conc. = 25.1 Report level label = 2 Pct Recovery = 94% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 13.222 Expected Conc. = 24.67 Report level label = 2 Pct Recovery = 54% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 13.607 Expected Conc. = 24.67 Report level label = 2 Pct Recovery = 55% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20220810134 Lab Value = 15.561 Expected Conc. = 20.08 Report level label = 2 Pct Recovery = 77% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222010132 Lab Value = 11.654 Expected Conc. = 20 Report level label = 2 Pct Recovery = 58% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220190116 Lab Value = 11.817 Expected Conc. = 20 Report level label = 2 Pct Recovery = 59% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 12.425 Expected Conc. = 20 Report level label = 2 Pct Recovery = 62% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20212990174 Lab Value = 11.390 Expected Conc. = 19.92 Report level label = 2 Pct Recovery = 57% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222150193 Lab Value = 12.571 Expected Conc. = 19.68 Report level label = 2 Pct Recovery = 64% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20201550031 Lab Value = 14.336 Expected Conc. = 13 Report level label = 2 Pct Recovery = 110% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20220810133 Lab Value = 10.488 Expected Conc. = 12.55 Report level label = 2 Pct Recovery = 84% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20203230018 Lab Value = 8.180 Expected Conc. = 12.55 Report level label = 2 Pct Recovery = 65% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 10.097 Expected Conc. = 12.55 Report level label = 2 Pct Recovery = 80% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 11.553 Expected Conc. = 12.55 Report level label = 2 Pct Recovery = 92% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221730293 Lab Value = 8.168 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 65% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 7.665 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 61% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202390020 Lab Value = 15.894 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 127% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 13.806 Expected Conc. = 12.5 Report level label = 2 Pct Recovery = 110% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20213340027 Lab Value = 9.747 Expected Conc. = 12.45 Report level label = 2 Pct Recovery = 78% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 24.532 Expected Conc. = 12.45 Report level label = 2 Pct Recovery = 197% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 7.692 Expected Conc. = 12.45 Report level label = 2 Pct Recovery = 62% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20201960104 Lab Value = 10.944 Expected Conc. = 10 Report level label = 2 Pct Recovery = 109% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 9.135 Expected Conc. = 10 Report level label = 2 Pct Recovery = 91% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20202330309 Lab Value = 3.998 Expected Conc. = 5.2 Report level label = 2 Pct Recovery = 77% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 4.598 Expected Conc. = 5.2 Report level label = 2 Pct Recovery = 88% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 5.660 Expected Conc. = 5.2 Report level label = 2 Pct Recovery = 109% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 3.805 Expected Conc. = 5.2 Report level label = 2 Pct Recovery = 73% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 4.783 Expected Conc. = 5.2 Report level label = 2 Pct Recovery = 92% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20222630205 Lab Value = 3.690 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 74% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210970035 Lab Value = 4.067 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 81% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 4.393 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 88% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 4.371 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 87% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 4.727 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 94% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 4.014 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 80% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 4.772 Expected Conc. = 5.02 Report level label = 2 Pct Recovery = 95% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222500483 Lab Value = 3.877 Expected Conc. = 5 Report level label = 2 Pct Recovery = 78% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 3.596 Expected Conc. = 5 Report level label = 2 Pct Recovery = 72% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213060210 Lab Value = 2.890 Expected Conc. = 4.98 Report level label = 2 Pct Recovery = 58% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20210270007 Lab Value = 3.240 Expected Conc. = 4.934 Report level label = 2 Pct Recovery = 66% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 09/28/22 Pct Recovery = 67% Analysis Date = 09/24/22 Pct Recovery = 67% Analysis Date = 09/24/22 Pct Recovery = 67% Analysis Date = 09/20/22 Pct Recovery = 67% Analysis Date = 09/20/22 Pct Recovery = 67% Analysis Date = 09/16/22 Pct Recovery = 67% Analysis Date = 09/16/22 Pct Recovery = 67% Analysis Date = 09/11/22 Pct Recovery = 68% Analysis Date = 09/11/22 Pct Recovery = 68% Analysis Date = 09/07/22 Pct Recovery = 68% Analysis Date = 09/07/22 Pct Recovery = 68% Analysis Date = 09/03/22 Pct Recovery = 68% Analysis Date = 09/03/22 Pct Recovery = 68% Analysis Date = 08/30/22 Pct Recovery = 68% Analysis Date = 08/30/22 Pct Recovery = 68% Analysis Date = 08/25/22 Pct Recovery = 68% Analysis Date = 08/25/22 Pct Recovery = 68% Analysis Date = 08/21/22 Pct Recovery = 68% Analysis Date = 08/21/22 Pct Recovery = 68% Analysis Date = 08/17/22 Pct Recovery = 69% Analysis Date = 08/17/22 Pct Recovery = 69% Analysis Date = 08/13/22 Pct Recovery = 69% Analysis Date = 08/13/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/08/22 Pct Recovery = 69% Analysis Date = 08/04/22 Pct Recovery = 69% Analysis Date = 08/04/22 Pct Recovery = 69% Analysis Date = 07/31/22 Pct Recovery = 69% Analysis Date = 07/31/22 Pct Recovery = 69% Analysis Date = 07/27/22 Pct Recovery = 70% Analysis Date = 07/27/22 Pct Recovery = 70% Analysis Date = 07/22/22 Pct Recovery = 70% Analysis Date = 07/22/22 Pct Recovery = 70% Analysis Date = 07/18/22 Pct Recovery = 70% Analysis Date = 07/18/22 Pct Recovery = 70% Analysis Date = 07/14/22 Pct Recovery = 70% Analysis Date = 07/14/22 Pct Recovery = 70% Analysis Date = 07/09/22 Pct Recovery = 70% Analysis Date = 07/09/22 Pct Recovery = 70% Analysis Date = 07/05/22 Pct Recovery = 70% Analysis Date = 07/05/22 Pct Recovery = 70% Analysis Date = 07/01/22 Pct Recovery = 71% Analysis Date = 07/01/22 Pct Recovery = 71% Analysis Date = 06/27/22 Pct Recovery = 71% Analysis Date = 06/27/22 Pct Recovery = 71% Analysis Date = 06/22/22 Pct Recovery = 71% Analysis Date = 06/22/22 Pct Recovery = 71% Analysis Date = 06/18/22 Pct Recovery = 71% Analysis Date = 06/18/22 Pct Recovery = 71% Analysis Date = 06/14/22 Pct Recovery = 71% Analysis Date = 06/14/22 Pct Recovery = 71% Analysis Date = 06/10/22 Pct Recovery = 71% Analysis Date = 06/10/22 Pct Recovery = 71% Analysis Date = 06/05/22 Pct Recovery = 72% Analysis Date = 06/05/22 Pct Recovery = 72% Analysis Date = 06/01/22 Pct Recovery = 72% Analysis Date = 06/01/22 Pct Recovery = 72% Analysis Date = 05/28/22 Pct Recovery = 72% Analysis Date = 05/28/22 Pct Recovery = 72% Analysis Date = 05/24/22 Pct Recovery = 72% Analysis Date = 05/24/22 Pct Recovery = 72% Analysis Date = 05/19/22 Pct Recovery = 72% Analysis Date = 05/19/22 Pct Recovery = 72% Analysis Date = 05/15/22 Pct Recovery = 72% Analysis Date = 05/15/22 Pct Recovery = 72% Analysis Date = 05/11/22 Pct Recovery = 73% Analysis Date = 05/11/22 Pct Recovery = 73% Analysis Date = 05/06/22 Pct Recovery = 73% Analysis Date = 05/06/22 Pct Recovery = 73% Analysis Date = 05/02/22 Pct Recovery = 73% Analysis Date = 05/02/22 Pct Recovery = 73% Analysis Date = 04/28/22 Pct Recovery = 73% Analysis Date = 04/28/22 Pct Recovery = 73% Analysis Date = 04/24/22 Pct Recovery = 73% Analysis Date = 04/24/22 Pct Recovery = 73% Analysis Date = 04/19/22 Pct Recovery = 73% Analysis Date = 04/19/22 Pct Recovery = 73% Analysis Date = 04/15/22 Pct Recovery = 74% Analysis Date = 04/15/22 Pct Recovery = 74% Analysis Date = 04/11/22 Pct Recovery = 74% Analysis Date = 04/11/22 Pct Recovery = 74% Analysis Date = 04/07/22 Pct Recovery = 74% Analysis Date = 04/07/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 04/02/22 Pct Recovery = 74% Analysis Date = 03/29/22 Pct Recovery = 74% Analysis Date = 03/29/22 Pct Recovery = 74% Analysis Date = 03/25/22 Pct Recovery = 74% Analysis Date = 03/25/22 Pct Recovery = 74% Analysis Date = 03/21/22 Pct Recovery = 75% Analysis Date = 03/21/22 Pct Recovery = 75% Analysis Date = 03/16/22 Pct Recovery = 75% Analysis Date = 03/16/22 Pct Recovery = 75% Analysis Date = 03/12/22 Pct Recovery = 75% Analysis Date = 03/12/22 Pct Recovery = 75% Analysis Date = 03/08/22 Pct Recovery = 75% Analysis Date = 03/08/22 Pct Recovery = 75% Analysis Date = 03/04/22 Pct Recovery = 75% Analysis Date = 03/04/22 Pct Recovery = 75% Analysis Date = 02/27/22 Pct Recovery = 75% Analysis Date = 02/27/22 Pct Recovery = 75% Analysis Date = 02/23/22 Pct Recovery = 76% Analysis Date = 02/23/22 Pct Recovery = 76% Analysis Date = 02/19/22 Pct Recovery = 76% Analysis Date = 02/19/22 Pct Recovery = 76% Analysis Date = 02/14/22 Pct Recovery = 76% Analysis Date = 02/14/22 Pct Recovery = 76% Analysis Date = 02/10/22 Pct Recovery = 76% Analysis Date = 02/10/22 Pct Recovery = 76% Analysis Date = 02/06/22 Pct Recovery = 76% Analysis Date = 02/06/22 Pct Recovery = 76% Analysis Date = 02/02/22 Pct Recovery = 76% Analysis Date = 02/02/22 Pct Recovery = 76% Analysis Date = 01/28/22 Pct Recovery = 77% Analysis Date = 01/28/22 Pct Recovery = 77% Analysis Date = 01/24/22 Pct Recovery = 77% Analysis Date = 01/24/22 Pct Recovery = 77% Analysis Date = 01/20/22 Pct Recovery = 77% Analysis Date = 01/20/22 Pct Recovery = 77% Analysis Date = 01/16/22 Pct Recovery = 77% Analysis Date = 01/16/22 Pct Recovery = 77% Analysis Date = 01/11/22 Pct Recovery = 77% Analysis Date = 01/11/22 Pct Recovery = 77% Analysis Date = 01/07/22 Pct Recovery = 77% Analysis Date = 01/07/22 Pct Recovery = 77% Analysis Date = 01/03/22 Pct Recovery = 77% Analysis Date = 01/03/22 Pct Recovery = 77% Analysis Date = 12/30/21 Pct Recovery = 78% Analysis Date = 12/30/21 Pct Recovery = 78% Analysis Date = 12/25/21 Pct Recovery = 78% Analysis Date = 12/25/21 Pct Recovery = 78% Analysis Date = 12/21/21 Pct Recovery = 78% Analysis Date = 12/21/21 Pct Recovery = 78% Analysis Date = 12/17/21 Pct Recovery = 78% Analysis Date = 12/17/21 Pct Recovery = 78% Analysis Date = 12/12/21 Pct Recovery = 78% Analysis Date = 12/12/21 Pct Recovery = 78% Analysis Date = 12/08/21 Pct Recovery = 78% Analysis Date = 12/08/21 Pct Recovery = 78% Analysis Date = 12/04/21 Pct Recovery = 78% Analysis Date = 12/04/21 Pct Recovery = 78% Analysis Date = 11/30/21 Pct Recovery = 79% Analysis Date = 11/30/21 Pct Recovery = 79% Analysis Date = 11/25/21 Pct Recovery = 79% Analysis Date = 11/25/21 Pct Recovery = 79% Analysis Date = 11/21/21 Pct Recovery = 79% Analysis Date = 11/21/21 Pct Recovery = 79% Analysis Date = 11/17/21 Pct Recovery = 79% Analysis Date = 11/17/21 Pct Recovery = 79% Analysis Date = 11/13/21 Pct Recovery = 79% Analysis Date = 11/13/21 Pct Recovery = 79% Analysis Date = 11/08/21 Pct Recovery = 79% Analysis Date = 11/08/21 Pct Recovery = 79% Analysis Date = 11/04/21 Pct Recovery = 79% Analysis Date = 11/04/21 Pct Recovery = 79% Analysis Date = 10/31/21 Pct Recovery = 79% Analysis Date = 10/31/21 Pct Recovery = 79% Analysis Date = 10/27/21 Pct Recovery = 79% Analysis Date = 10/27/21 Pct Recovery = 79% Analysis Date = 10/22/21 Pct Recovery = 79% Analysis Date = 10/22/21 Pct Recovery = 79% Analysis Date = 10/18/21 Pct Recovery = 79% Analysis Date = 10/18/21 Pct Recovery = 79% Analysis Date = 10/14/21 Pct Recovery = 78% Analysis Date = 10/14/21 Pct Recovery = 78% Analysis Date = 10/10/21 Pct Recovery = 78% Analysis Date = 10/10/21 Pct Recovery = 78% Analysis Date = 10/05/21 Pct Recovery = 78% Analysis Date = 10/05/21 Pct Recovery = 78% Analysis Date = 10/01/21 Pct Recovery = 78% Analysis Date = 10/01/21 Pct Recovery = 78% Analysis Date = 09/27/21 Pct Recovery = 78% Analysis Date = 09/27/21 Pct Recovery = 78% Analysis Date = 09/22/21 Pct Recovery = 78% Analysis Date = 09/22/21 Pct Recovery = 78% Analysis Date = 09/18/21 Pct Recovery = 78% Analysis Date = 09/18/21 Pct Recovery = 78% Analysis Date = 09/14/21 Pct Recovery = 78% Analysis Date = 09/14/21 Pct Recovery = 78% Analysis Date = 09/10/21 Pct Recovery = 78% Analysis Date = 09/10/21 Pct Recovery = 78% Analysis Date = 09/05/21 Pct Recovery = 77% Analysis Date = 09/05/21 Pct Recovery = 77% Analysis Date = 09/01/21 Pct Recovery = 77% Analysis Date = 09/01/21 Pct Recovery = 77% Analysis Date = 08/28/21 Pct Recovery = 77% Analysis Date = 08/28/21 Pct Recovery = 77% Analysis Date = 08/24/21 Pct Recovery = 77% Analysis Date = 08/24/21 Pct Recovery = 77% Analysis Date = 08/19/21 Pct Recovery = 77% Analysis Date = 08/19/21 Pct Recovery = 77% Analysis Date = 08/15/21 Pct Recovery = 77% Analysis Date = 08/15/21 Pct Recovery = 77% Analysis Date = 08/11/21 Pct Recovery = 77% Analysis Date = 08/11/21 Pct Recovery = 77% Analysis Date = 08/07/21 Pct Recovery = 77% Analysis Date = 08/07/21 Pct Recovery = 77% Analysis Date = 08/02/21 Pct Recovery = 77% Analysis Date = 08/02/21 Pct Recovery = 77% Analysis Date = 07/29/21 Pct Recovery = 76% Analysis Date = 07/29/21 Pct Recovery = 76% Analysis Date = 07/25/21 Pct Recovery = 76% Analysis Date = 07/25/21 Pct Recovery = 76% Analysis Date = 07/20/21 Pct Recovery = 76% Analysis Date = 07/20/21 Pct Recovery = 76% Analysis Date = 07/16/21 Pct Recovery = 76% Analysis Date = 07/16/21 Pct Recovery = 76% Analysis Date = 07/12/21 Pct Recovery = 76% Analysis Date = 07/12/21 Pct Recovery = 76% Analysis Date = 07/08/21 Pct Recovery = 76% Analysis Date = 07/08/21 Pct Recovery = 76% Analysis Date = 07/03/21 Pct Recovery = 76% Analysis Date = 07/03/21 Pct Recovery = 76% Analysis Date = 06/29/21 Pct Recovery = 76% Analysis Date = 06/29/21 Pct Recovery = 76% Analysis Date = 06/25/21 Pct Recovery = 76% Analysis Date = 06/25/21 Pct Recovery = 76% Analysis Date = 06/21/21 Pct Recovery = 75% Analysis Date = 06/21/21 Pct Recovery = 75% Analysis Date = 06/16/21 Pct Recovery = 75% Analysis Date = 06/16/21 Pct Recovery = 75% Analysis Date = 06/12/21 Pct Recovery = 75% Analysis Date = 06/12/21 Pct Recovery = 75% Analysis Date = 06/08/21 Pct Recovery = 75% Analysis Date = 06/08/21 Pct Recovery = 75% Analysis Date = 06/04/21 Pct Recovery = 75% Analysis Date = 06/04/21 Pct Recovery = 75% Analysis Date = 05/30/21 Pct Recovery = 75% Analysis Date = 05/30/21 Pct Recovery = 75% Analysis Date = 05/26/21 Pct Recovery = 75% Analysis Date = 05/26/21 Pct Recovery = 75% Analysis Date = 05/22/21 Pct Recovery = 75% Analysis Date = 05/22/21 Pct Recovery = 75% Analysis Date = 05/17/21 Pct Recovery = 74% Analysis Date = 05/17/21 Pct Recovery = 74% Analysis Date = 05/13/21 Pct Recovery = 74% Analysis Date = 05/13/21 Pct Recovery = 74% Analysis Date = 05/09/21 Pct Recovery = 74% Analysis Date = 05/09/21 Pct Recovery = 74% Analysis Date = 05/05/21 Pct Recovery = 74% Analysis Date = 05/05/21 Pct Recovery = 74% Analysis Date = 04/30/21 Pct Recovery = 74% Analysis Date = 04/30/21 Pct Recovery = 74% Analysis Date = 04/26/21 Pct Recovery = 74% Analysis Date = 04/26/21 Pct Recovery = 74% Analysis Date = 04/22/21 Pct Recovery = 74% Analysis Date = 04/22/21 Pct Recovery = 74% Analysis Date = 04/18/21 Pct Recovery = 74% Analysis Date = 04/18/21 Pct Recovery = 74% Analysis Date = 04/13/21 Pct Recovery = 74% Analysis Date = 04/13/21 Pct Recovery = 74% Analysis Date = 04/09/21 Pct Recovery = 73% Analysis Date = 04/09/21 Pct Recovery = 73% Analysis Date = 04/05/21 Pct Recovery = 73% Analysis Date = 04/05/21 Pct Recovery = 73% Analysis Date = 04/01/21 Pct Recovery = 73% Analysis Date = 04/01/21 Pct Recovery = 73% Analysis Date = 03/27/21 Pct Recovery = 73% Analysis Date = 03/27/21 Pct Recovery = 73% Analysis Date = 03/23/21 Pct Recovery = 73% Analysis Date = 03/23/21 Pct Recovery = 73% Analysis Date = 03/19/21 Pct Recovery = 73% Analysis Date = 03/19/21 Pct Recovery = 73% Analysis Date = 03/15/21 Pct Recovery = 73% Analysis Date = 03/15/21 Pct Recovery = 73% Analysis Date = 03/10/21 Pct Recovery = 73% Analysis Date = 03/10/21 Pct Recovery = 73% Analysis Date = 03/06/21 Pct Recovery = 73% Analysis Date = 03/06/21 Pct Recovery = 73% Analysis Date = 03/02/21 Pct Recovery = 72% Analysis Date = 03/02/21 Pct Recovery = 72% Analysis Date = 02/25/21 Pct Recovery = 72% Analysis Date = 02/25/21 Pct Recovery = 72% Analysis Date = 02/21/21 Pct Recovery = 72% Analysis Date = 02/21/21 Pct Recovery = 72% Analysis Date = 02/17/21 Pct Recovery = 72% Analysis Date = 02/17/21 Pct Recovery = 72% Analysis Date = 02/13/21 Pct Recovery = 72% Analysis Date = 02/13/21 Pct Recovery = 72% Analysis Date = 02/08/21 Pct Recovery = 72% Analysis Date = 02/08/21 Pct Recovery = 72% Analysis Date = 02/04/21 Pct Recovery = 73% Analysis Date = 02/04/21 Pct Recovery = 73% Analysis Date = 01/31/21 Pct Recovery = 73% Analysis Date = 01/31/21 Pct Recovery = 73% Analysis Date = 01/27/21 Pct Recovery = 74% Analysis Date = 01/27/21 Pct Recovery = 74% Analysis Date = 01/22/21 Pct Recovery = 75% Analysis Date = 01/22/21 Pct Recovery = 75% Analysis Date = 01/18/21 Pct Recovery = 75% Analysis Date = 01/18/21 Pct Recovery = 75% Analysis Date = 01/14/21 Pct Recovery = 76% Analysis Date = 01/14/21 Pct Recovery = 76% Analysis Date = 01/10/21 Pct Recovery = 76% Analysis Date = 01/10/21 Pct Recovery = 76% Analysis Date = 01/05/21 Pct Recovery = 77% Analysis Date = 01/05/21 Pct Recovery = 77% Analysis Date = 01/01/21 Pct Recovery = 77% Analysis Date = 01/01/21 Pct Recovery = 77% Analysis Date = 12/28/20 Pct Recovery = 78% Analysis Date = 12/28/20 Pct Recovery = 78% Analysis Date = 12/23/20 Pct Recovery = 79% Analysis Date = 12/23/20 Pct Recovery = 79% Analysis Date = 12/19/20 Pct Recovery = 79% Analysis Date = 12/19/20 Pct Recovery = 79% Analysis Date = 12/15/20 Pct Recovery = 80% Analysis Date = 12/15/20 Pct Recovery = 80% Analysis Date = 12/11/20 Pct Recovery = 81% Analysis Date = 12/11/20 Pct Recovery = 81% Analysis Date = 12/06/20 Pct Recovery = 81% Analysis Date = 12/06/20 Pct Recovery = 81% Analysis Date = 12/02/20 Pct Recovery = 82% Analysis Date = 12/02/20 Pct Recovery = 82% Analysis Date = 11/28/20 Pct Recovery = 83% Analysis Date = 11/28/20 Pct Recovery = 83% Analysis Date = 11/24/20 Pct Recovery = 83% Analysis Date = 11/24/20 Pct Recovery = 83% Analysis Date = 11/19/20 Pct Recovery = 84% Analysis Date = 11/19/20 Pct Recovery = 84% Analysis Date = 11/15/20 Pct Recovery = 85% Analysis Date = 11/15/20 Pct Recovery = 85% Analysis Date = 11/11/20 Pct Recovery = 85% Analysis Date = 11/11/20 Pct Recovery = 85% Analysis Date = 11/07/20 Pct Recovery = 86% Analysis Date = 11/07/20 Pct Recovery = 86% Analysis Date = 11/02/20 Pct Recovery = 87% Analysis Date = 11/02/20 Pct Recovery = 87% Analysis Date = 10/29/20 Pct Recovery = 87% Analysis Date = 10/29/20 Pct Recovery = 87% Analysis Date = 10/25/20 Pct Recovery = 88% Analysis Date = 10/25/20 Pct Recovery = 88% Analysis Date = 10/21/20 Pct Recovery = 88% Analysis Date = 10/21/20 Pct Recovery = 88% Analysis Date = 10/16/20 Pct Recovery = 89% Analysis Date = 10/16/20 Pct Recovery = 89% Analysis Date = 10/12/20 Pct Recovery = 89% Analysis Date = 10/12/20 Pct Recovery = 89% Analysis Date = 10/08/20 Pct Recovery = 90% Analysis Date = 10/08/20 Pct Recovery = 90% Analysis Date = 10/03/20 Pct Recovery = 90% Analysis Date = 10/03/20 Pct Recovery = 90% Analysis Date = 09/29/20 Pct Recovery = 91% Analysis Date = 09/29/20 Pct Recovery = 91% Analysis Date = 09/25/20 Pct Recovery = 91% Analysis Date = 09/25/20 Pct Recovery = 91% Analysis Date = 09/21/20 Pct Recovery = 92% Analysis Date = 09/21/20 Pct Recovery = 92% Analysis Date = 09/16/20 Pct Recovery = 92% Analysis Date = 09/16/20 Pct Recovery = 92% Analysis Date = 09/12/20 Pct Recovery = 93% Analysis Date = 09/12/20 Pct Recovery = 93% Analysis Date = 09/08/20 Pct Recovery = 93% Analysis Date = 09/08/20 Pct Recovery = 93% Analysis Date = 09/04/20 Pct Recovery = 94% Analysis Date = 09/04/20 Pct Recovery = 94% Analysis Date = 08/30/20 Pct Recovery = 94% Analysis Date = 08/30/20 Pct Recovery = 94% Analysis Date = 08/26/20 Pct Recovery = 94% Analysis Date = 08/26/20 Pct Recovery = 94% Analysis Date = 08/22/20 Pct Recovery = 95% Analysis Date = 08/22/20 Pct Recovery = 95% Analysis Date = 08/18/20 Pct Recovery = 95% Analysis Date = 08/18/20 Pct Recovery = 95% Analysis Date = 08/13/20 Pct Recovery = 96% Analysis Date = 08/13/20 Pct Recovery = 96% Analysis Date = 08/09/20 Pct Recovery = 96% Analysis Date = 08/09/20 Pct Recovery = 96% Analysis Date = 08/05/20 Pct Recovery = 97% Analysis Date = 08/05/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/31/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 98% Analysis Date = 07/23/20 Pct Recovery = 98% Analysis Date = 07/19/20 Pct Recovery = 98% Analysis Date = 07/19/20 Pct Recovery = 98% Analysis Date = 07/14/20 Pct Recovery = 99% Analysis Date = 07/14/20 Pct Recovery = 99% Analysis Date = 07/10/20 Pct Recovery = 99% Analysis Date = 07/10/20 Pct Recovery = 99% Analysis Date = 07/06/20 Pct Recovery = 99% Analysis Date = 07/06/20 Pct Recovery = 99% Analysis Date = 07/02/20 Pct Recovery = 100% Analysis Date = 07/02/20 Pct Recovery = 100% Analysis Date = 06/27/20 Pct Recovery = 100% Analysis Date = 06/27/20 Pct Recovery = 100% Analysis Date = 06/23/20 Pct Recovery = 101% Analysis Date = 06/23/20 Pct Recovery = 101% Analysis Date = 06/19/20 Pct Recovery = 101% Analysis Date = 06/19/20 Pct Recovery = 101% Analysis Date = 06/15/20 Pct Recovery = 101% Analysis Date = 06/15/20 Pct Recovery = 101% Analysis Date = 06/10/20 Pct Recovery = 102% Analysis Date = 06/10/20 Pct Recovery = 102% Analysis Date = 06/06/20 Pct Recovery = 102% Analysis Date = 06/06/20 Pct Recovery = 102% Analysis Date = 06/02/20 Pct Recovery = 102% Analysis Date = 06/02/20 Pct Recovery = 102% Analysis Date = 05/29/20 Pct Recovery = 103% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUPIRIMPHOS (PHOSTEBUPIRIM)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 40 83% 26% 79% 20%
Total 40 83% 26% 79% 20%

Sample Statistics
TEBUPIRIMPHOS (PHOSTEBUPIRIM)

Characteristic N % % Basis
Plotted 40 98% Spiked
Estimated Values 1 2% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 2% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 75 .  
False Positives 0 0% 0 out of 75

OBSP Determination:
TEBUTHIURON
METHOD: 2447 , TESTIDCODE: 68695LCM60

Laboratory ID = 20202110006 Lab Value = 40.774 Expected Conc. = 37.9 Report level label = 3 Pct Recovery = 108% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 35.133 Expected Conc. = 37.8 Report level label = 3 Pct Recovery = 93% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20210760015 Lab Value = 28.554 Expected Conc. = 37.6 Report level label = 3 Pct Recovery = 76% Analysis Date = 03/26/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 31.240 Expected Conc. = 37.6 Report level label = 3 Pct Recovery = 83% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 38.410 Expected Conc. = 37.6 Report level label = 3 Pct Recovery = 102% Analysis Date = 01/30/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 42.492 Expected Conc. = 37.6 Report level label = 3 Pct Recovery = 113% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203080100 Lab Value = 36.145 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 97% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 38.058 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 103% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 37.527 Expected Conc. = 37.1 Report level label = 3 Pct Recovery = 101% Analysis Date = 09/23/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20222150192 Lab Value = 21.954 Expected Conc. = 30.2 Report level label = 3 Pct Recovery = 73% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 22.825 Expected Conc. = 30.048 Report level label = 3 Pct Recovery = 76% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 20.405 Expected Conc. = 30 Report level label = 3 Pct Recovery = 68% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20201680155 Lab Value = 19.210 Expected Conc. = 18.95 Report level label = 3 Pct Recovery = 101% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 17.536 Expected Conc. = 18.9 Report level label = 3 Pct Recovery = 93% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 16.344 Expected Conc. = 18.9 Report level label = 3 Pct Recovery = 86% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 18.781 Expected Conc. = 18.9 Report level label = 3 Pct Recovery = 99% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20220740064 Lab Value = 14.226 Expected Conc. = 18.875 Report level label = 3 Pct Recovery = 75% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20210480001 Lab Value = 18.046 Expected Conc. = 18.8 Report level label = 3 Pct Recovery = 96% Analysis Date = 02/24/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221870197 Lab Value = 14.841 Expected Conc. = 18.78 Report level label = 3 Pct Recovery = 79% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20202880004 Lab Value = 20.300 Expected Conc. = 18.55 Report level label = 3 Pct Recovery = 109% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 15.703 Expected Conc. = 15.04 Report level label = 3 Pct Recovery = 104% Analysis Date = 04/09/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 12.910 Expected Conc. = 14.84 Report level label = 3 Pct Recovery = 87% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 14.719 Expected Conc. = 14.84 Report level label = 3 Pct Recovery = 99% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20201610160 Lab Value = 8.530 Expected Conc. = 7.58 Report level label = 3 Pct Recovery = 113% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 8.124 Expected Conc. = 7.56 Report level label = 3 Pct Recovery = 107% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 7.681 Expected Conc. = 7.56 Report level label = 3 Pct Recovery = 102% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 7.264 Expected Conc. = 7.56 Report level label = 3 Pct Recovery = 96% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 7.764 Expected Conc. = 7.56 Report level label = 3 Pct Recovery = 103% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20210690067 Lab Value = 5.543 Expected Conc. = 7.52 Report level label = 3 Pct Recovery = 74% Analysis Date = 03/19/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20221660151 Lab Value = 6.989 Expected Conc. = 7.512 Report level label = 3 Pct Recovery = 93% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20210120050 Lab Value = 7.343 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 99% Analysis Date = 01/26/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 6.838 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 92% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 7.034 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 95% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 6.441 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 87% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 8.418 Expected Conc. = 7.42 Report level label = 3 Pct Recovery = 113% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/15/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/10/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/06/22 Pct Recovery = 76% Analysis Date = 08/02/22 Pct Recovery = 76% Analysis Date = 08/02/22 Pct Recovery = 76% Analysis Date = 07/29/22 Pct Recovery = 76% Analysis Date = 07/29/22 Pct Recovery = 76% Analysis Date = 07/25/22 Pct Recovery = 76% Analysis Date = 07/25/22 Pct Recovery = 76% Analysis Date = 07/21/22 Pct Recovery = 77% Analysis Date = 07/21/22 Pct Recovery = 77% Analysis Date = 07/17/22 Pct Recovery = 77% Analysis Date = 07/17/22 Pct Recovery = 77% Analysis Date = 07/13/22 Pct Recovery = 77% Analysis Date = 07/13/22 Pct Recovery = 77% Analysis Date = 07/09/22 Pct Recovery = 77% Analysis Date = 07/09/22 Pct Recovery = 77% Analysis Date = 07/05/22 Pct Recovery = 77% Analysis Date = 07/05/22 Pct Recovery = 77% Analysis Date = 07/01/22 Pct Recovery = 77% Analysis Date = 07/01/22 Pct Recovery = 77% Analysis Date = 06/26/22 Pct Recovery = 77% Analysis Date = 06/26/22 Pct Recovery = 77% Analysis Date = 06/22/22 Pct Recovery = 77% Analysis Date = 06/22/22 Pct Recovery = 77% Analysis Date = 06/18/22 Pct Recovery = 77% Analysis Date = 06/18/22 Pct Recovery = 77% Analysis Date = 06/14/22 Pct Recovery = 78% Analysis Date = 06/14/22 Pct Recovery = 78% Analysis Date = 06/10/22 Pct Recovery = 78% Analysis Date = 06/10/22 Pct Recovery = 78% Analysis Date = 06/06/22 Pct Recovery = 78% Analysis Date = 06/06/22 Pct Recovery = 78% Analysis Date = 06/02/22 Pct Recovery = 78% Analysis Date = 06/02/22 Pct Recovery = 78% Analysis Date = 05/29/22 Pct Recovery = 78% Analysis Date = 05/29/22 Pct Recovery = 78% Analysis Date = 05/25/22 Pct Recovery = 78% Analysis Date = 05/25/22 Pct Recovery = 78% Analysis Date = 05/21/22 Pct Recovery = 78% Analysis Date = 05/21/22 Pct Recovery = 78% Analysis Date = 05/17/22 Pct Recovery = 78% Analysis Date = 05/17/22 Pct Recovery = 78% Analysis Date = 05/12/22 Pct Recovery = 78% Analysis Date = 05/12/22 Pct Recovery = 78% Analysis Date = 05/08/22 Pct Recovery = 79% Analysis Date = 05/08/22 Pct Recovery = 79% Analysis Date = 05/04/22 Pct Recovery = 79% Analysis Date = 05/04/22 Pct Recovery = 79% Analysis Date = 04/30/22 Pct Recovery = 79% Analysis Date = 04/30/22 Pct Recovery = 79% Analysis Date = 04/26/22 Pct Recovery = 79% Analysis Date = 04/26/22 Pct Recovery = 79% Analysis Date = 04/22/22 Pct Recovery = 79% Analysis Date = 04/22/22 Pct Recovery = 79% Analysis Date = 04/18/22 Pct Recovery = 79% Analysis Date = 04/18/22 Pct Recovery = 79% Analysis Date = 04/14/22 Pct Recovery = 79% Analysis Date = 04/14/22 Pct Recovery = 79% Analysis Date = 04/10/22 Pct Recovery = 79% Analysis Date = 04/10/22 Pct Recovery = 79% Analysis Date = 04/06/22 Pct Recovery = 80% Analysis Date = 04/06/22 Pct Recovery = 80% Analysis Date = 04/02/22 Pct Recovery = 80% Analysis Date = 04/02/22 Pct Recovery = 80% Analysis Date = 03/28/22 Pct Recovery = 80% Analysis Date = 03/28/22 Pct Recovery = 80% Analysis Date = 03/24/22 Pct Recovery = 80% Analysis Date = 03/24/22 Pct Recovery = 80% Analysis Date = 03/20/22 Pct Recovery = 80% Analysis Date = 03/20/22 Pct Recovery = 80% Analysis Date = 03/16/22 Pct Recovery = 80% Analysis Date = 03/16/22 Pct Recovery = 80% Analysis Date = 03/12/22 Pct Recovery = 80% Analysis Date = 03/12/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/08/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 80% Analysis Date = 03/04/22 Pct Recovery = 80% Analysis Date = 02/28/22 Pct Recovery = 81% Analysis Date = 02/28/22 Pct Recovery = 81% Analysis Date = 02/24/22 Pct Recovery = 81% Analysis Date = 02/24/22 Pct Recovery = 81% Analysis Date = 02/20/22 Pct Recovery = 81% Analysis Date = 02/20/22 Pct Recovery = 81% Analysis Date = 02/16/22 Pct Recovery = 81% Analysis Date = 02/16/22 Pct Recovery = 81% Analysis Date = 02/11/22 Pct Recovery = 81% Analysis Date = 02/11/22 Pct Recovery = 81% Analysis Date = 02/07/22 Pct Recovery = 81% Analysis Date = 02/07/22 Pct Recovery = 81% Analysis Date = 02/03/22 Pct Recovery = 81% Analysis Date = 02/03/22 Pct Recovery = 81% Analysis Date = 01/30/22 Pct Recovery = 81% Analysis Date = 01/30/22 Pct Recovery = 81% Analysis Date = 01/26/22 Pct Recovery = 81% Analysis Date = 01/26/22 Pct Recovery = 81% Analysis Date = 01/22/22 Pct Recovery = 82% Analysis Date = 01/22/22 Pct Recovery = 82% Analysis Date = 01/18/22 Pct Recovery = 82% Analysis Date = 01/18/22 Pct Recovery = 82% Analysis Date = 01/14/22 Pct Recovery = 82% Analysis Date = 01/14/22 Pct Recovery = 82% Analysis Date = 01/10/22 Pct Recovery = 82% Analysis Date = 01/10/22 Pct Recovery = 82% Analysis Date = 01/06/22 Pct Recovery = 82% Analysis Date = 01/06/22 Pct Recovery = 82% Analysis Date = 01/02/22 Pct Recovery = 82% Analysis Date = 01/02/22 Pct Recovery = 82% Analysis Date = 12/28/21 Pct Recovery = 82% Analysis Date = 12/28/21 Pct Recovery = 82% Analysis Date = 12/24/21 Pct Recovery = 82% Analysis Date = 12/24/21 Pct Recovery = 82% Analysis Date = 12/20/21 Pct Recovery = 82% Analysis Date = 12/20/21 Pct Recovery = 82% Analysis Date = 12/16/21 Pct Recovery = 83% Analysis Date = 12/16/21 Pct Recovery = 83% Analysis Date = 12/12/21 Pct Recovery = 83% Analysis Date = 12/12/21 Pct Recovery = 83% Analysis Date = 12/08/21 Pct Recovery = 83% Analysis Date = 12/08/21 Pct Recovery = 83% Analysis Date = 12/04/21 Pct Recovery = 83% Analysis Date = 12/04/21 Pct Recovery = 83% Analysis Date = 11/30/21 Pct Recovery = 83% Analysis Date = 11/30/21 Pct Recovery = 83% Analysis Date = 11/26/21 Pct Recovery = 83% Analysis Date = 11/26/21 Pct Recovery = 83% Analysis Date = 11/22/21 Pct Recovery = 83% Analysis Date = 11/22/21 Pct Recovery = 83% Analysis Date = 11/18/21 Pct Recovery = 83% Analysis Date = 11/18/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/13/21 Pct Recovery = 83% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 84% Analysis Date = 10/28/21 Pct Recovery = 84% Analysis Date = 10/28/21 Pct Recovery = 84% Analysis Date = 10/24/21 Pct Recovery = 84% Analysis Date = 10/24/21 Pct Recovery = 84% Analysis Date = 10/20/21 Pct Recovery = 84% Analysis Date = 10/20/21 Pct Recovery = 84% Analysis Date = 10/16/21 Pct Recovery = 84% Analysis Date = 10/16/21 Pct Recovery = 84% Analysis Date = 10/12/21 Pct Recovery = 84% Analysis Date = 10/12/21 Pct Recovery = 84% Analysis Date = 10/08/21 Pct Recovery = 85% Analysis Date = 10/08/21 Pct Recovery = 85% Analysis Date = 10/04/21 Pct Recovery = 85% Analysis Date = 10/04/21 Pct Recovery = 85% Analysis Date = 09/29/21 Pct Recovery = 85% Analysis Date = 09/29/21 Pct Recovery = 85% Analysis Date = 09/25/21 Pct Recovery = 85% Analysis Date = 09/25/21 Pct Recovery = 85% Analysis Date = 09/21/21 Pct Recovery = 85% Analysis Date = 09/21/21 Pct Recovery = 85% Analysis Date = 09/17/21 Pct Recovery = 85% Analysis Date = 09/17/21 Pct Recovery = 85% Analysis Date = 09/13/21 Pct Recovery = 85% Analysis Date = 09/13/21 Pct Recovery = 85% Analysis Date = 09/09/21 Pct Recovery = 85% Analysis Date = 09/09/21 Pct Recovery = 85% Analysis Date = 09/05/21 Pct Recovery = 85% Analysis Date = 09/05/21 Pct Recovery = 85% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 09/01/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 86% Analysis Date = 08/28/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/24/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/20/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/15/21 Pct Recovery = 86% Analysis Date = 08/11/21 Pct Recovery = 86% Analysis Date = 08/11/21 Pct Recovery = 86% Analysis Date = 08/07/21 Pct Recovery = 86% Analysis Date = 08/07/21 Pct Recovery = 86% Analysis Date = 08/03/21 Pct Recovery = 86% Analysis Date = 08/03/21 Pct Recovery = 86% Analysis Date = 07/30/21 Pct Recovery = 86% Analysis Date = 07/30/21 Pct Recovery = 86% Analysis Date = 07/26/21 Pct Recovery = 87% Analysis Date = 07/26/21 Pct Recovery = 87% Analysis Date = 07/22/21 Pct Recovery = 87% Analysis Date = 07/22/21 Pct Recovery = 87% Analysis Date = 07/18/21 Pct Recovery = 87% Analysis Date = 07/18/21 Pct Recovery = 87% Analysis Date = 07/14/21 Pct Recovery = 87% Analysis Date = 07/14/21 Pct Recovery = 87% Analysis Date = 07/10/21 Pct Recovery = 87% Analysis Date = 07/10/21 Pct Recovery = 87% Analysis Date = 07/06/21 Pct Recovery = 87% Analysis Date = 07/06/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 07/02/21 Pct Recovery = 87% Analysis Date = 06/27/21 Pct Recovery = 87% Analysis Date = 06/27/21 Pct Recovery = 87% Analysis Date = 06/23/21 Pct Recovery = 87% Analysis Date = 06/23/21 Pct Recovery = 87% Analysis Date = 06/19/21 Pct Recovery = 88% Analysis Date = 06/19/21 Pct Recovery = 88% Analysis Date = 06/15/21 Pct Recovery = 88% Analysis Date = 06/15/21 Pct Recovery = 88% Analysis Date = 06/11/21 Pct Recovery = 88% Analysis Date = 06/11/21 Pct Recovery = 88% Analysis Date = 06/07/21 Pct Recovery = 88% Analysis Date = 06/07/21 Pct Recovery = 88% Analysis Date = 06/03/21 Pct Recovery = 88% Analysis Date = 06/03/21 Pct Recovery = 88% Analysis Date = 05/30/21 Pct Recovery = 88% Analysis Date = 05/30/21 Pct Recovery = 88% Analysis Date = 05/26/21 Pct Recovery = 88% Analysis Date = 05/26/21 Pct Recovery = 88% Analysis Date = 05/22/21 Pct Recovery = 88% Analysis Date = 05/22/21 Pct Recovery = 88% Analysis Date = 05/18/21 Pct Recovery = 88% Analysis Date = 05/18/21 Pct Recovery = 88% Analysis Date = 05/13/21 Pct Recovery = 89% Analysis Date = 05/13/21 Pct Recovery = 89% Analysis Date = 05/09/21 Pct Recovery = 89% Analysis Date = 05/09/21 Pct Recovery = 89% Analysis Date = 05/05/21 Pct Recovery = 89% Analysis Date = 05/05/21 Pct Recovery = 89% Analysis Date = 05/01/21 Pct Recovery = 89% Analysis Date = 05/01/21 Pct Recovery = 89% Analysis Date = 04/27/21 Pct Recovery = 89% Analysis Date = 04/27/21 Pct Recovery = 89% Analysis Date = 04/23/21 Pct Recovery = 89% Analysis Date = 04/23/21 Pct Recovery = 89% Analysis Date = 04/19/21 Pct Recovery = 89% Analysis Date = 04/19/21 Pct Recovery = 89% Analysis Date = 04/15/21 Pct Recovery = 89% Analysis Date = 04/15/21 Pct Recovery = 89% Analysis Date = 04/11/21 Pct Recovery = 90% Analysis Date = 04/11/21 Pct Recovery = 90% Analysis Date = 04/07/21 Pct Recovery = 90% Analysis Date = 04/07/21 Pct Recovery = 90% Analysis Date = 04/03/21 Pct Recovery = 90% Analysis Date = 04/03/21 Pct Recovery = 90% Analysis Date = 03/29/21 Pct Recovery = 90% Analysis Date = 03/29/21 Pct Recovery = 90% Analysis Date = 03/25/21 Pct Recovery = 90% Analysis Date = 03/25/21 Pct Recovery = 90% Analysis Date = 03/21/21 Pct Recovery = 90% Analysis Date = 03/21/21 Pct Recovery = 90% Analysis Date = 03/17/21 Pct Recovery = 90% Analysis Date = 03/17/21 Pct Recovery = 90% Analysis Date = 03/13/21 Pct Recovery = 91% Analysis Date = 03/13/21 Pct Recovery = 91% Analysis Date = 03/09/21 Pct Recovery = 91% Analysis Date = 03/09/21 Pct Recovery = 91% Analysis Date = 03/05/21 Pct Recovery = 91% Analysis Date = 03/05/21 Pct Recovery = 91% Analysis Date = 03/01/21 Pct Recovery = 92% Analysis Date = 03/01/21 Pct Recovery = 92% Analysis Date = 02/25/21 Pct Recovery = 92% Analysis Date = 02/25/21 Pct Recovery = 92% Analysis Date = 02/21/21 Pct Recovery = 92% Analysis Date = 02/21/21 Pct Recovery = 92% Analysis Date = 02/17/21 Pct Recovery = 93% Analysis Date = 02/17/21 Pct Recovery = 93% Analysis Date = 02/12/21 Pct Recovery = 93% Analysis Date = 02/12/21 Pct Recovery = 93% Analysis Date = 02/08/21 Pct Recovery = 93% Analysis Date = 02/08/21 Pct Recovery = 93% Analysis Date = 02/04/21 Pct Recovery = 93% Analysis Date = 02/04/21 Pct Recovery = 93% Analysis Date = 01/31/21 Pct Recovery = 94% Analysis Date = 01/31/21 Pct Recovery = 94% Analysis Date = 01/27/21 Pct Recovery = 94% Analysis Date = 01/27/21 Pct Recovery = 94% Analysis Date = 01/23/21 Pct Recovery = 95% Analysis Date = 01/23/21 Pct Recovery = 95% Analysis Date = 01/19/21 Pct Recovery = 95% Analysis Date = 01/19/21 Pct Recovery = 95% Analysis Date = 01/15/21 Pct Recovery = 95% Analysis Date = 01/15/21 Pct Recovery = 95% Analysis Date = 01/11/21 Pct Recovery = 96% Analysis Date = 01/11/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/07/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 01/03/21 Pct Recovery = 96% Analysis Date = 12/29/20 Pct Recovery = 97% Analysis Date = 12/29/20 Pct Recovery = 97% Analysis Date = 12/25/20 Pct Recovery = 97% Analysis Date = 12/25/20 Pct Recovery = 97% Analysis Date = 12/21/20 Pct Recovery = 97% Analysis Date = 12/21/20 Pct Recovery = 97% Analysis Date = 12/17/20 Pct Recovery = 98% Analysis Date = 12/17/20 Pct Recovery = 98% Analysis Date = 12/13/20 Pct Recovery = 98% Analysis Date = 12/13/20 Pct Recovery = 98% Analysis Date = 12/09/20 Pct Recovery = 98% Analysis Date = 12/09/20 Pct Recovery = 98% Analysis Date = 12/05/20 Pct Recovery = 98% Analysis Date = 12/05/20 Pct Recovery = 98% Analysis Date = 12/01/20 Pct Recovery = 98% Analysis Date = 12/01/20 Pct Recovery = 98% Analysis Date = 11/27/20 Pct Recovery = 98% Analysis Date = 11/27/20 Pct Recovery = 98% Analysis Date = 11/23/20 Pct Recovery = 98% Analysis Date = 11/23/20 Pct Recovery = 98% Analysis Date = 11/19/20 Pct Recovery = 99% Analysis Date = 11/19/20 Pct Recovery = 99% Analysis Date = 11/14/20 Pct Recovery = 99% Analysis Date = 11/14/20 Pct Recovery = 99% Analysis Date = 11/10/20 Pct Recovery = 99% Analysis Date = 11/10/20 Pct Recovery = 99% Analysis Date = 11/06/20 Pct Recovery = 99% Analysis Date = 11/06/20 Pct Recovery = 99% Analysis Date = 11/02/20 Pct Recovery = 99% Analysis Date = 11/02/20 Pct Recovery = 99% Analysis Date = 10/29/20 Pct Recovery = 99% Analysis Date = 10/29/20 Pct Recovery = 99% Analysis Date = 10/25/20 Pct Recovery = 99% Analysis Date = 10/25/20 Pct Recovery = 99% Analysis Date = 10/21/20 Pct Recovery = 99% Analysis Date = 10/21/20 Pct Recovery = 99% Analysis Date = 10/17/20 Pct Recovery = 99% Analysis Date = 10/17/20 Pct Recovery = 99% Analysis Date = 10/13/20 Pct Recovery = 99% Analysis Date = 10/13/20 Pct Recovery = 99% Analysis Date = 10/09/20 Pct Recovery = 99% Analysis Date = 10/09/20 Pct Recovery = 99% Analysis Date = 10/05/20 Pct Recovery = 100% Analysis Date = 10/05/20 Pct Recovery = 100% Analysis Date = 09/30/20 Pct Recovery = 100% Analysis Date = 09/30/20 Pct Recovery = 100% Analysis Date = 09/26/20 Pct Recovery = 100% Analysis Date = 09/26/20 Pct Recovery = 100% Analysis Date = 09/22/20 Pct Recovery = 100% Analysis Date = 09/22/20 Pct Recovery = 100% Analysis Date = 09/18/20 Pct Recovery = 100% Analysis Date = 09/18/20 Pct Recovery = 100% Analysis Date = 09/14/20 Pct Recovery = 100% Analysis Date = 09/14/20 Pct Recovery = 100% Analysis Date = 09/10/20 Pct Recovery = 100% Analysis Date = 09/10/20 Pct Recovery = 100% Analysis Date = 09/06/20 Pct Recovery = 100% Analysis Date = 09/06/20 Pct Recovery = 100% Analysis Date = 09/02/20 Pct Recovery = 100% Analysis Date = 09/02/20 Pct Recovery = 100% Analysis Date = 08/29/20 Pct Recovery = 100% Analysis Date = 08/29/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 100% Analysis Date = 08/25/20 Pct Recovery = 100% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/21/20 Pct Recovery = 101% Analysis Date = 08/16/20 Pct Recovery = 101% Analysis Date = 08/16/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/12/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/08/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 101% Analysis Date = 08/04/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/31/20 Pct Recovery = 101% Analysis Date = 07/27/20 Pct Recovery = 101% Analysis Date = 07/27/20 Pct Recovery = 101% Analysis Date = 07/23/20 Pct Recovery = 101% Analysis Date = 07/23/20 Pct Recovery = 101% Analysis Date = 07/19/20 Pct Recovery = 101% Analysis Date = 07/19/20 Pct Recovery = 101% Analysis Date = 07/15/20 Pct Recovery = 101% Analysis Date = 07/15/20 Pct Recovery = 101% Analysis Date = 07/11/20 Pct Recovery = 101% Analysis Date = 07/11/20 Pct Recovery = 101% Analysis Date = 07/07/20 Pct Recovery = 101% Analysis Date = 07/07/20 Pct Recovery = 101% Analysis Date = 07/02/20 Pct Recovery = 101% Analysis Date = 07/02/20 Pct Recovery = 101% Analysis Date = 06/28/20 Pct Recovery = 101% Analysis Date = 06/28/20 Pct Recovery = 101% Analysis Date = 06/24/20 Pct Recovery = 102% Analysis Date = 06/24/20 Pct Recovery = 102% Analysis Date = 06/20/20 Pct Recovery = 102% Analysis Date = 06/20/20 Pct Recovery = 102% Analysis Date = 06/16/20 Pct Recovery = 102% Analysis Date = 06/16/20 Pct Recovery = 102% Analysis Date = 06/12/20 Pct Recovery = 102% Analysis Date = 06/12/20 Pct Recovery = 102% Analysis Date = 06/08/20 Pct Recovery = 102% Analysis Date = 06/08/20 Pct Recovery = 102% Analysis Date = 06/04/20 Pct Recovery = 102% Analysis Date = 06/04/20 Pct Recovery = 102% Analysis Date = 05/31/20 Pct Recovery = 102% Analysis Date = 05/31/20 Pct Recovery = 102% Analysis Date = 05/27/20 Pct Recovery = 102% Analysis Date = 05/27/20 Pct Recovery = 102% Analysis Date = 05/23/20 Pct Recovery = 102% Analysis Date = 05/23/20 Pct Recovery = 102% Analysis Date = 05/19/20 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUTHIURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 35 94% 13% 96% 12%
Total 35 94% 13% 96% 12%

Sample Statistics
TEBUTHIURON

Characteristic N % % Basis
Plotted 35 100% Spiked
Estimated Values 2 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 35 .  
False Negatives 0 0% 0 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
TERBUFOS
METHOD: 2447 , TESTIDCODE: 68699LCM60

Laboratory ID = 20203230020 Lab Value = 34.842 Expected Conc. = 86.16 Report level label = 6.8 Pct Recovery = 40% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20203230023 Lab Value = 35.096 Expected Conc. = 86.16 Report level label = 6.8 Pct Recovery = 41% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20202110006 Lab Value = 67.957 Expected Conc. = 85.9 Report level label = 6.8 Pct Recovery = 79% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20201820155 Lab Value = 54.819 Expected Conc. = 85.6 Report level label = 6.8 Pct Recovery = 64% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 66.100 Expected Conc. = 85.4 Report level label = 6.8 Pct Recovery = 77% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202880004 Lab Value = 75.391 Expected Conc. = 85.4 Report level label = 6.8 Pct Recovery = 88% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590108 Lab Value = 74.446 Expected Conc. = 85.4 Report level label = 6.8 Pct Recovery = 87% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590109 Lab Value = 65.153 Expected Conc. = 85.4 Report level label = 6.8 Pct Recovery = 76% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20212990174 Lab Value = 35.764 Expected Conc. = 68.88 Report level label = 6.8 Pct Recovery = 52% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220810134 Lab Value = 41.099 Expected Conc. = 68.4 Report level label = 6.8 Pct Recovery = 60% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222010132 Lab Value = 32.394 Expected Conc. = 68 Report level label = 6.8 Pct Recovery = 48% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220190116 Lab Value = 28.963 Expected Conc. = 67.92 Report level label = 6.8 Pct Recovery = 43% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 29.400 Expected Conc. = 67.92 Report level label = 6.8 Pct Recovery = 43% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20222150193 Lab Value = 30.726 Expected Conc. = 67.6 Report level label = 6.8 Pct Recovery = 45% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20210400070 Lab Value = 34.558 Expected Conc. = 43.08 Report level label = 6.8 Pct Recovery = 80% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20213340027 Lab Value = 25.888 Expected Conc. = 43.05 Report level label = 6.8 Pct Recovery = 60% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 58.234 Expected Conc. = 43.05 Report level label = 6.8 Pct Recovery = 135% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 23.451 Expected Conc. = 43.05 Report level label = 6.8 Pct Recovery = 54% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20201680155 Lab Value = 29.108 Expected Conc. = 42.95 Report level label = 6.8 Pct Recovery = 68% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20202530029 Lab Value = 25.276 Expected Conc. = 42.8 Report level label = 6.8 Pct Recovery = 59% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 23.850 Expected Conc. = 42.8 Report level label = 6.8 Pct Recovery = 56% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 25.692 Expected Conc. = 42.8 Report level label = 6.8 Pct Recovery = 60% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20220810133 Lab Value = 36.898 Expected Conc. = 42.75 Report level label = 6.8 Pct Recovery = 86% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20203360042 Lab Value = 27.306 Expected Conc. = 42.7 Report level label = 6.8 Pct Recovery = 64% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202950016 Lab Value = 32.817 Expected Conc. = 42.7 Report level label = 6.8 Pct Recovery = 77% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20221730293 Lab Value = 23.124 Expected Conc. = 42.45 Report level label = 6.8 Pct Recovery = 54% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 21.172 Expected Conc. = 42.45 Report level label = 6.8 Pct Recovery = 50% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20201610160 Lab Value = 12.139 Expected Conc. = 17.18 Report level label = 6.8 Pct Recovery = 71% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 8.274 Expected Conc. = 17.12 Report level label = 6.8 Pct Recovery = 48% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 13.105 Expected Conc. = 17.12 Report level label = 6.8 Pct Recovery = 77% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 10.676 Expected Conc. = 17.12 Report level label = 6.8 Pct Recovery = 62% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 11.403 Expected Conc. = 17.12 Report level label = 6.8 Pct Recovery = 67% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20222630205 Lab Value = 12.913 Expected Conc. = 17.1 Report level label = 6.8 Pct Recovery = 76% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20203440004 Lab Value = 12.499 Expected Conc. = 17.08 Report level label = 6.8 Pct Recovery = 73% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20203170006 Lab Value = 13.844 Expected Conc. = 17.08 Report level label = 6.8 Pct Recovery = 81% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20222500483 Lab Value = 9.997 Expected Conc. = 16.98 Report level label = 6.8 Pct Recovery = 59% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 9.557 Expected Conc. = 16.98 Report level label = 6.8 Pct Recovery = 56% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Analysis Date = 09/28/22 Pct Recovery = 57% Analysis Date = 09/24/22 Pct Recovery = 57% Analysis Date = 09/24/22 Pct Recovery = 57% Analysis Date = 09/20/22 Pct Recovery = 57% Analysis Date = 09/20/22 Pct Recovery = 57% Analysis Date = 09/16/22 Pct Recovery = 58% Analysis Date = 09/16/22 Pct Recovery = 58% Analysis Date = 09/11/22 Pct Recovery = 58% Analysis Date = 09/11/22 Pct Recovery = 58% Analysis Date = 09/07/22 Pct Recovery = 58% Analysis Date = 09/07/22 Pct Recovery = 58% Analysis Date = 09/03/22 Pct Recovery = 58% Analysis Date = 09/03/22 Pct Recovery = 58% Analysis Date = 08/29/22 Pct Recovery = 58% Analysis Date = 08/29/22 Pct Recovery = 58% Analysis Date = 08/25/22 Pct Recovery = 58% Analysis Date = 08/25/22 Pct Recovery = 58% Analysis Date = 08/21/22 Pct Recovery = 58% Analysis Date = 08/21/22 Pct Recovery = 58% Analysis Date = 08/16/22 Pct Recovery = 58% Analysis Date = 08/16/22 Pct Recovery = 58% Analysis Date = 08/12/22 Pct Recovery = 58% Analysis Date = 08/12/22 Pct Recovery = 58% Analysis Date = 08/08/22 Pct Recovery = 58% Analysis Date = 08/08/22 Pct Recovery = 58% Analysis Date = 08/03/22 Pct Recovery = 58% Analysis Date = 08/03/22 Pct Recovery = 58% Analysis Date = 07/30/22 Pct Recovery = 59% Analysis Date = 07/30/22 Pct Recovery = 59% Analysis Date = 07/26/22 Pct Recovery = 59% Analysis Date = 07/26/22 Pct Recovery = 59% Analysis Date = 07/21/22 Pct Recovery = 59% Analysis Date = 07/21/22 Pct Recovery = 59% Analysis Date = 07/17/22 Pct Recovery = 59% Analysis Date = 07/17/22 Pct Recovery = 59% Analysis Date = 07/13/22 Pct Recovery = 59% Analysis Date = 07/13/22 Pct Recovery = 59% Analysis Date = 07/09/22 Pct Recovery = 59% Analysis Date = 07/09/22 Pct Recovery = 59% Analysis Date = 07/04/22 Pct Recovery = 59% Analysis Date = 07/04/22 Pct Recovery = 59% Analysis Date = 06/30/22 Pct Recovery = 59% Analysis Date = 06/30/22 Pct Recovery = 59% Analysis Date = 06/26/22 Pct Recovery = 59% Analysis Date = 06/26/22 Pct Recovery = 59% Analysis Date = 06/21/22 Pct Recovery = 59% Analysis Date = 06/21/22 Pct Recovery = 59% Analysis Date = 06/17/22 Pct Recovery = 59% Analysis Date = 06/17/22 Pct Recovery = 59% Analysis Date = 06/13/22 Pct Recovery = 59% Analysis Date = 06/13/22 Pct Recovery = 59% Analysis Date = 06/08/22 Pct Recovery = 60% Analysis Date = 06/08/22 Pct Recovery = 60% Analysis Date = 06/04/22 Pct Recovery = 60% Analysis Date = 06/04/22 Pct Recovery = 60% Analysis Date = 05/31/22 Pct Recovery = 60% Analysis Date = 05/31/22 Pct Recovery = 60% Analysis Date = 05/26/22 Pct Recovery = 60% Analysis Date = 05/26/22 Pct Recovery = 60% Analysis Date = 05/22/22 Pct Recovery = 60% Analysis Date = 05/22/22 Pct Recovery = 60% Analysis Date = 05/18/22 Pct Recovery = 60% Analysis Date = 05/18/22 Pct Recovery = 60% Analysis Date = 05/13/22 Pct Recovery = 60% Analysis Date = 05/13/22 Pct Recovery = 60% Analysis Date = 05/09/22 Pct Recovery = 60% Analysis Date = 05/09/22 Pct Recovery = 60% Analysis Date = 05/05/22 Pct Recovery = 60% Analysis Date = 05/05/22 Pct Recovery = 60% Analysis Date = 04/30/22 Pct Recovery = 60% Analysis Date = 04/30/22 Pct Recovery = 60% Analysis Date = 04/26/22 Pct Recovery = 60% Analysis Date = 04/26/22 Pct Recovery = 60% Analysis Date = 04/22/22 Pct Recovery = 60% Analysis Date = 04/22/22 Pct Recovery = 60% Analysis Date = 04/18/22 Pct Recovery = 61% Analysis Date = 04/18/22 Pct Recovery = 61% Analysis Date = 04/13/22 Pct Recovery = 61% Analysis Date = 04/13/22 Pct Recovery = 61% Analysis Date = 04/09/22 Pct Recovery = 61% Analysis Date = 04/09/22 Pct Recovery = 61% Analysis Date = 04/05/22 Pct Recovery = 61% Analysis Date = 04/05/22 Pct Recovery = 61% Analysis Date = 03/31/22 Pct Recovery = 61% Analysis Date = 03/31/22 Pct Recovery = 61% Analysis Date = 03/27/22 Pct Recovery = 61% Analysis Date = 03/27/22 Pct Recovery = 61% Analysis Date = 03/23/22 Pct Recovery = 61% Analysis Date = 03/23/22 Pct Recovery = 61% Analysis Date = 03/18/22 Pct Recovery = 61% Analysis Date = 03/18/22 Pct Recovery = 61% Analysis Date = 03/14/22 Pct Recovery = 61% Analysis Date = 03/14/22 Pct Recovery = 61% Analysis Date = 03/10/22 Pct Recovery = 61% Analysis Date = 03/10/22 Pct Recovery = 61% Analysis Date = 03/05/22 Pct Recovery = 61% Analysis Date = 03/05/22 Pct Recovery = 61% Analysis Date = 03/01/22 Pct Recovery = 61% Analysis Date = 03/01/22 Pct Recovery = 61% Analysis Date = 02/25/22 Pct Recovery = 62% Analysis Date = 02/25/22 Pct Recovery = 62% Analysis Date = 02/20/22 Pct Recovery = 62% Analysis Date = 02/20/22 Pct Recovery = 62% Analysis Date = 02/16/22 Pct Recovery = 62% Analysis Date = 02/16/22 Pct Recovery = 62% Analysis Date = 02/12/22 Pct Recovery = 62% Analysis Date = 02/12/22 Pct Recovery = 62% Analysis Date = 02/07/22 Pct Recovery = 62% Analysis Date = 02/07/22 Pct Recovery = 62% Analysis Date = 02/03/22 Pct Recovery = 62% Analysis Date = 02/03/22 Pct Recovery = 62% Analysis Date = 01/30/22 Pct Recovery = 62% Analysis Date = 01/30/22 Pct Recovery = 62% Analysis Date = 01/26/22 Pct Recovery = 62% Analysis Date = 01/26/22 Pct Recovery = 62% Analysis Date = 01/21/22 Pct Recovery = 62% Analysis Date = 01/21/22 Pct Recovery = 62% Analysis Date = 01/17/22 Pct Recovery = 62% Analysis Date = 01/17/22 Pct Recovery = 62% Analysis Date = 01/13/22 Pct Recovery = 62% Analysis Date = 01/13/22 Pct Recovery = 62% Analysis Date = 01/08/22 Pct Recovery = 63% Analysis Date = 01/08/22 Pct Recovery = 63% Analysis Date = 01/04/22 Pct Recovery = 63% Analysis Date = 01/04/22 Pct Recovery = 63% Analysis Date = 12/31/21 Pct Recovery = 63% Analysis Date = 12/31/21 Pct Recovery = 63% Analysis Date = 12/26/21 Pct Recovery = 63% Analysis Date = 12/26/21 Pct Recovery = 63% Analysis Date = 12/22/21 Pct Recovery = 63% Analysis Date = 12/22/21 Pct Recovery = 63% Analysis Date = 12/18/21 Pct Recovery = 63% Analysis Date = 12/18/21 Pct Recovery = 63% Analysis Date = 12/13/21 Pct Recovery = 63% Analysis Date = 12/13/21 Pct Recovery = 63% Analysis Date = 12/09/21 Pct Recovery = 63% Analysis Date = 12/09/21 Pct Recovery = 63% Analysis Date = 12/05/21 Pct Recovery = 63% Analysis Date = 12/05/21 Pct Recovery = 63% Analysis Date = 11/30/21 Pct Recovery = 63% Analysis Date = 11/30/21 Pct Recovery = 63% Analysis Date = 11/26/21 Pct Recovery = 63% Analysis Date = 11/26/21 Pct Recovery = 63% Analysis Date = 11/22/21 Pct Recovery = 63% Analysis Date = 11/22/21 Pct Recovery = 63% Analysis Date = 11/18/21 Pct Recovery = 63% Analysis Date = 11/18/21 Pct Recovery = 63% Analysis Date = 11/13/21 Pct Recovery = 63% Analysis Date = 11/13/21 Pct Recovery = 63% Analysis Date = 11/09/21 Pct Recovery = 63% Analysis Date = 11/09/21 Pct Recovery = 63% Analysis Date = 11/05/21 Pct Recovery = 63% Analysis Date = 11/05/21 Pct Recovery = 63% Analysis Date = 10/31/21 Pct Recovery = 63% Analysis Date = 10/31/21 Pct Recovery = 63% Analysis Date = 10/27/21 Pct Recovery = 63% Analysis Date = 10/27/21 Pct Recovery = 63% Analysis Date = 10/23/21 Pct Recovery = 63% Analysis Date = 10/23/21 Pct Recovery = 63% Analysis Date = 10/18/21 Pct Recovery = 63% Analysis Date = 10/18/21 Pct Recovery = 63% Analysis Date = 10/14/21 Pct Recovery = 63% Analysis Date = 10/14/21 Pct Recovery = 63% Analysis Date = 10/10/21 Pct Recovery = 63% Analysis Date = 10/10/21 Pct Recovery = 63% Analysis Date = 10/05/21 Pct Recovery = 63% Analysis Date = 10/05/21 Pct Recovery = 63% Analysis Date = 10/01/21 Pct Recovery = 63% Analysis Date = 10/01/21 Pct Recovery = 63% Analysis Date = 09/27/21 Pct Recovery = 63% Analysis Date = 09/27/21 Pct Recovery = 63% Analysis Date = 09/22/21 Pct Recovery = 63% Analysis Date = 09/22/21 Pct Recovery = 63% Analysis Date = 09/18/21 Pct Recovery = 63% Analysis Date = 09/18/21 Pct Recovery = 63% Analysis Date = 09/14/21 Pct Recovery = 63% Analysis Date = 09/14/21 Pct Recovery = 63% Analysis Date = 09/09/21 Pct Recovery = 63% Analysis Date = 09/09/21 Pct Recovery = 63% Analysis Date = 09/05/21 Pct Recovery = 63% Analysis Date = 09/05/21 Pct Recovery = 63% Analysis Date = 09/01/21 Pct Recovery = 63% Analysis Date = 09/01/21 Pct Recovery = 63% Analysis Date = 08/28/21 Pct Recovery = 63% Analysis Date = 08/28/21 Pct Recovery = 63% Analysis Date = 08/23/21 Pct Recovery = 63% Analysis Date = 08/23/21 Pct Recovery = 63% Analysis Date = 08/19/21 Pct Recovery = 62% Analysis Date = 08/19/21 Pct Recovery = 62% Analysis Date = 08/15/21 Pct Recovery = 62% Analysis Date = 08/15/21 Pct Recovery = 62% Analysis Date = 08/10/21 Pct Recovery = 62% Analysis Date = 08/10/21 Pct Recovery = 62% Analysis Date = 08/06/21 Pct Recovery = 62% Analysis Date = 08/06/21 Pct Recovery = 62% Analysis Date = 08/02/21 Pct Recovery = 62% Analysis Date = 08/02/21 Pct Recovery = 62% Analysis Date = 07/28/21 Pct Recovery = 62% Analysis Date = 07/28/21 Pct Recovery = 62% Analysis Date = 07/24/21 Pct Recovery = 62% Analysis Date = 07/24/21 Pct Recovery = 62% Analysis Date = 07/20/21 Pct Recovery = 62% Analysis Date = 07/20/21 Pct Recovery = 62% Analysis Date = 07/15/21 Pct Recovery = 62% Analysis Date = 07/15/21 Pct Recovery = 62% Analysis Date = 07/11/21 Pct Recovery = 62% Analysis Date = 07/11/21 Pct Recovery = 62% Analysis Date = 07/07/21 Pct Recovery = 62% Analysis Date = 07/07/21 Pct Recovery = 62% Analysis Date = 07/02/21 Pct Recovery = 62% Analysis Date = 07/02/21 Pct Recovery = 62% Analysis Date = 06/28/21 Pct Recovery = 62% Analysis Date = 06/28/21 Pct Recovery = 62% Analysis Date = 06/24/21 Pct Recovery = 62% Analysis Date = 06/24/21 Pct Recovery = 62% Analysis Date = 06/19/21 Pct Recovery = 62% Analysis Date = 06/19/21 Pct Recovery = 62% Analysis Date = 06/15/21 Pct Recovery = 62% Analysis Date = 06/15/21 Pct Recovery = 62% Analysis Date = 06/11/21 Pct Recovery = 62% Analysis Date = 06/11/21 Pct Recovery = 62% Analysis Date = 06/07/21 Pct Recovery = 62% Analysis Date = 06/07/21 Pct Recovery = 62% Analysis Date = 06/02/21 Pct Recovery = 62% Analysis Date = 06/02/21 Pct Recovery = 62% Analysis Date = 05/29/21 Pct Recovery = 62% Analysis Date = 05/29/21 Pct Recovery = 62% Analysis Date = 05/25/21 Pct Recovery = 62% Analysis Date = 05/25/21 Pct Recovery = 62% Analysis Date = 05/20/21 Pct Recovery = 61% Analysis Date = 05/20/21 Pct Recovery = 61% Analysis Date = 05/16/21 Pct Recovery = 61% Analysis Date = 05/16/21 Pct Recovery = 61% Analysis Date = 05/12/21 Pct Recovery = 61% Analysis Date = 05/12/21 Pct Recovery = 61% Analysis Date = 05/07/21 Pct Recovery = 61% Analysis Date = 05/07/21 Pct Recovery = 61% Analysis Date = 05/03/21 Pct Recovery = 61% Analysis Date = 05/03/21 Pct Recovery = 61% Analysis Date = 04/29/21 Pct Recovery = 61% Analysis Date = 04/29/21 Pct Recovery = 61% Analysis Date = 04/24/21 Pct Recovery = 61% Analysis Date = 04/24/21 Pct Recovery = 61% Analysis Date = 04/20/21 Pct Recovery = 61% Analysis Date = 04/20/21 Pct Recovery = 61% Analysis Date = 04/16/21 Pct Recovery = 61% Analysis Date = 04/16/21 Pct Recovery = 61% Analysis Date = 04/11/21 Pct Recovery = 61% Analysis Date = 04/11/21 Pct Recovery = 61% Analysis Date = 04/07/21 Pct Recovery = 61% Analysis Date = 04/07/21 Pct Recovery = 61% Analysis Date = 04/03/21 Pct Recovery = 61% Analysis Date = 04/03/21 Pct Recovery = 61% Analysis Date = 03/29/21 Pct Recovery = 61% Analysis Date = 03/29/21 Pct Recovery = 61% Analysis Date = 03/25/21 Pct Recovery = 61% Analysis Date = 03/25/21 Pct Recovery = 61% Analysis Date = 03/21/21 Pct Recovery = 61% Analysis Date = 03/21/21 Pct Recovery = 61% Analysis Date = 03/17/21 Pct Recovery = 61% Analysis Date = 03/17/21 Pct Recovery = 61% Analysis Date = 03/12/21 Pct Recovery = 61% Analysis Date = 03/12/21 Pct Recovery = 61% Analysis Date = 03/08/21 Pct Recovery = 61% Analysis Date = 03/08/21 Pct Recovery = 61% Analysis Date = 03/04/21 Pct Recovery = 61% Analysis Date = 03/04/21 Pct Recovery = 61% Analysis Date = 02/27/21 Pct Recovery = 61% Analysis Date = 02/27/21 Pct Recovery = 61% Analysis Date = 02/23/21 Pct Recovery = 61% Analysis Date = 02/23/21 Pct Recovery = 61% Analysis Date = 02/19/21 Pct Recovery = 60% Analysis Date = 02/19/21 Pct Recovery = 60% Analysis Date = 02/14/21 Pct Recovery = 61% Analysis Date = 02/14/21 Pct Recovery = 61% Analysis Date = 02/10/21 Pct Recovery = 61% Analysis Date = 02/10/21 Pct Recovery = 61% Analysis Date = 02/06/21 Pct Recovery = 62% Analysis Date = 02/06/21 Pct Recovery = 62% Analysis Date = 02/01/21 Pct Recovery = 62% Analysis Date = 02/01/21 Pct Recovery = 62% Analysis Date = 01/28/21 Pct Recovery = 62% Analysis Date = 01/28/21 Pct Recovery = 62% Analysis Date = 01/24/21 Pct Recovery = 63% Analysis Date = 01/24/21 Pct Recovery = 63% Analysis Date = 01/19/21 Pct Recovery = 63% Analysis Date = 01/19/21 Pct Recovery = 63% Analysis Date = 01/15/21 Pct Recovery = 63% Analysis Date = 01/15/21 Pct Recovery = 63% Analysis Date = 01/11/21 Pct Recovery = 64% Analysis Date = 01/11/21 Pct Recovery = 64% Analysis Date = 01/07/21 Pct Recovery = 64% Analysis Date = 01/07/21 Pct Recovery = 64% Analysis Date = 01/02/21 Pct Recovery = 65% Analysis Date = 01/02/21 Pct Recovery = 65% Analysis Date = 12/29/20 Pct Recovery = 65% Analysis Date = 12/29/20 Pct Recovery = 65% Analysis Date = 12/25/20 Pct Recovery = 65% Analysis Date = 12/25/20 Pct Recovery = 65% Analysis Date = 12/20/20 Pct Recovery = 66% Analysis Date = 12/20/20 Pct Recovery = 66% Analysis Date = 12/16/20 Pct Recovery = 66% Analysis Date = 12/16/20 Pct Recovery = 66% Analysis Date = 12/12/20 Pct Recovery = 66% Analysis Date = 12/12/20 Pct Recovery = 66% Analysis Date = 12/07/20 Pct Recovery = 67% Analysis Date = 12/07/20 Pct Recovery = 67% Analysis Date = 12/03/20 Pct Recovery = 67% Analysis Date = 12/03/20 Pct Recovery = 67% Analysis Date = 11/29/20 Pct Recovery = 67% Analysis Date = 11/29/20 Pct Recovery = 67% Analysis Date = 11/24/20 Pct Recovery = 68% Analysis Date = 11/24/20 Pct Recovery = 68% Analysis Date = 11/20/20 Pct Recovery = 68% Analysis Date = 11/20/20 Pct Recovery = 68% Analysis Date = 11/16/20 Pct Recovery = 68% Analysis Date = 11/16/20 Pct Recovery = 68% Analysis Date = 11/11/20 Pct Recovery = 68% Analysis Date = 11/11/20 Pct Recovery = 68% Analysis Date = 11/07/20 Pct Recovery = 69% Analysis Date = 11/07/20 Pct Recovery = 69% Analysis Date = 11/03/20 Pct Recovery = 69% Analysis Date = 11/03/20 Pct Recovery = 69% Analysis Date = 10/29/20 Pct Recovery = 69% Analysis Date = 10/29/20 Pct Recovery = 69% Analysis Date = 10/25/20 Pct Recovery = 70% Analysis Date = 10/25/20 Pct Recovery = 70% Analysis Date = 10/21/20 Pct Recovery = 70% Analysis Date = 10/21/20 Pct Recovery = 70% Analysis Date = 10/17/20 Pct Recovery = 70% Analysis Date = 10/17/20 Pct Recovery = 70% Analysis Date = 10/12/20 Pct Recovery = 70% Analysis Date = 10/12/20 Pct Recovery = 70% Analysis Date = 10/08/20 Pct Recovery = 71% Analysis Date = 10/08/20 Pct Recovery = 71% Analysis Date = 10/04/20 Pct Recovery = 71% Analysis Date = 10/04/20 Pct Recovery = 71% Analysis Date = 09/29/20 Pct Recovery = 71% Analysis Date = 09/29/20 Pct Recovery = 71% Analysis Date = 09/25/20 Pct Recovery = 71% Analysis Date = 09/25/20 Pct Recovery = 71% Analysis Date = 09/21/20 Pct Recovery = 71% Analysis Date = 09/21/20 Pct Recovery = 71% Analysis Date = 09/16/20 Pct Recovery = 71% Analysis Date = 09/16/20 Pct Recovery = 71% Analysis Date = 09/12/20 Pct Recovery = 71% Analysis Date = 09/12/20 Pct Recovery = 71% Analysis Date = 09/08/20 Pct Recovery = 71% Analysis Date = 09/08/20 Pct Recovery = 71% Analysis Date = 09/03/20 Pct Recovery = 70% Analysis Date = 09/03/20 Pct Recovery = 70% Analysis Date = 08/30/20 Pct Recovery = 70% Analysis Date = 08/30/20 Pct Recovery = 70% Analysis Date = 08/26/20 Pct Recovery = 70% Analysis Date = 08/26/20 Pct Recovery = 70% Analysis Date = 08/21/20 Pct Recovery = 70% Analysis Date = 08/21/20 Pct Recovery = 70% Analysis Date = 08/17/20 Pct Recovery = 69% Analysis Date = 08/17/20 Pct Recovery = 69% Analysis Date = 08/13/20 Pct Recovery = 69% Analysis Date = 08/13/20 Pct Recovery = 69% Analysis Date = 08/08/20 Pct Recovery = 69% Analysis Date = 08/08/20 Pct Recovery = 69% Analysis Date = 08/04/20 Pct Recovery = 69% Analysis Date = 08/04/20 Pct Recovery = 69% Analysis Date = 07/31/20 Pct Recovery = 68% Analysis Date = 07/31/20 Pct Recovery = 68% Analysis Date = 07/27/20 Pct Recovery = 68% Analysis Date = 07/27/20 Pct Recovery = 68% Analysis Date = 07/22/20 Pct Recovery = 68% Analysis Date = 07/22/20 Pct Recovery = 68% Analysis Date = 07/18/20 Pct Recovery = 67% Analysis Date = 07/18/20 Pct Recovery = 67% Analysis Date = 07/14/20 Pct Recovery = 67% Analysis Date = 07/14/20 Pct Recovery = 67% Analysis Date = 07/09/20 Pct Recovery = 67% Analysis Date = 07/09/20 Pct Recovery = 67% Analysis Date = 07/05/20 Pct Recovery = 67% Analysis Date = 07/05/20 Pct Recovery = 67% Analysis Date = 07/01/20 Pct Recovery = 66% Analysis Date = 07/01/20 Pct Recovery = 66% Analysis Date = 06/26/20 Pct Recovery = 66% Analysis Date = 06/26/20 Pct Recovery = 66% Analysis Date = 06/22/20 Pct Recovery = 66% Analysis Date = 06/22/20 Pct Recovery = 66% Analysis Date = 06/18/20 Pct Recovery = 66% Analysis Date = 06/18/20 Pct Recovery = 66% Analysis Date = 06/13/20 Pct Recovery = 65% Analysis Date = 06/13/20 Pct Recovery = 65% Analysis Date = 06/09/20 Pct Recovery = 65% Analysis Date = 06/09/20 Pct Recovery = 65% Analysis Date = 06/05/20 Pct Recovery = 65% Analysis Date = 06/05/20 Pct Recovery = 65% Analysis Date = 05/31/20 Pct Recovery = 64% Analysis Date = 05/31/20 Pct Recovery = 64% Analysis Date = 05/27/20 Pct Recovery = 64% Analysis Date = 05/27/20 Pct Recovery = 64% Analysis Date = 05/23/20 Pct Recovery = 64% Analysis Date = 05/23/20 Pct Recovery = 64% Analysis Date = 05/19/20 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 37 65% 18% 62% 16%
Total 37 65% 18% 62% 16%

Sample Statistics
TERBUFOS

Characteristic N % % Basis
Plotted 37 97% Spiked
Estimated Values 4 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 38 .  
False Negatives 1 3% 1 out of 38
Not Spiked 78 .  
False Positives 1 1% 1 out of 78

OBSP Determination:
TERBUFOS SULFONE
METHOD: 2447 , TESTIDCODE: 68703LCM60

Laboratory ID = 20203170006 Lab Value = 63.407 Expected Conc. = 27.06 Report level label = 32 Pct Recovery = 234% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20221370164 Lab Value = 295.141 Expected Conc. = 321.64 Report level label = 32 Pct Recovery = 92% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 275.184 Expected Conc. = 320 Report level label = 32 Pct Recovery = 86% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 285.190 Expected Conc. = 320 Report level label = 32 Pct Recovery = 89% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 312.628 Expected Conc. = 320 Report level label = 32 Pct Recovery = 98% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20222070177 Lab Value = 237.528 Expected Conc. = 200 Report level label = 32 Pct Recovery = 119% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20202110006 Lab Value = 95.399 Expected Conc. = 140.5 Report level label = 11 Pct Recovery = 68% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 090519Pest3 Laboratory ID = 20203230020 Lab Value = 118.761 Expected Conc. = 136.4 Report level label = 32 Pct Recovery = 87% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20203230023 Lab Value = 114.870 Expected Conc. = 136.4 Report level label = 32 Pct Recovery = 84% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20201820155 Lab Value = 128.881 Expected Conc. = 136.4 Report level label = 11 Pct Recovery = 94% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 9089700 Laboratory ID = 20203080100 Lab Value = 118.004 Expected Conc. = 135.3 Report level label = 32 Pct Recovery = 87% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202880004 Lab Value = 157.333 Expected Conc. = 135.3 Report level label = 32 Pct Recovery = 116% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590108 Lab Value = 179.442 Expected Conc. = 135.3 Report level label = 11 Pct Recovery = 133% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590109 Lab Value = 133.317 Expected Conc. = 135.3 Report level label = 11 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20201680155 Lab Value = 89.136 Expected Conc. = 70.25 Report level label = 11 Pct Recovery = 127% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 090519Pest3 Laboratory ID = 20210400070 Lab Value = 99.717 Expected Conc. = 68.2 Report level label = 32 Pct Recovery = 146% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20202530029 Lab Value = 65.823 Expected Conc. = 68.2 Report level label = 11 Pct Recovery = 97% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20202240086 Lab Value = 71.285 Expected Conc. = 68.2 Report level label = 11 Pct Recovery = 105% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20201330113 Lab Value = 72.381 Expected Conc. = 68.2 Report level label = 11 Pct Recovery = 106% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 9089700 Laboratory ID = 20203360042 Lab Value = 67.871 Expected Conc. = 67.65 Report level label = 32 Pct Recovery = 100% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202950016 Lab Value = 54.844 Expected Conc. = 67.65 Report level label = 32 Pct Recovery = 81% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20201610160 Lab Value = 35.699 Expected Conc. = 28.1 Report level label = 11 Pct Recovery = 127% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090519Pest3 Laboratory ID = 20202330309 Lab Value = 17.115 Expected Conc. = 27.28 Report level label = 11 Pct Recovery = 63% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20202040027 Lab Value = 30.194 Expected Conc. = 27.28 Report level label = 11 Pct Recovery = 111% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9089700 Laboratory ID = 20201890192 Lab Value = 49.555 Expected Conc. = 27.28 Report level label = 11 Pct Recovery = 182% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20201470020 Lab Value = 36.870 Expected Conc. = 27.28 Report level label = 11 Pct Recovery = 135% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9089700 Laboratory ID = 20203440004 Lab Value = 25.630 Expected Conc. = 27.06 Report level label = 32 Pct Recovery = 95% Analysis Date = 12/15/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-3 Analysis Date = 08/16/22 Pct Recovery = 96% Analysis Date = 08/11/22 Pct Recovery = 96% Analysis Date = 08/11/22 Pct Recovery = 96% Analysis Date = 08/07/22 Pct Recovery = 96% Analysis Date = 08/07/22 Pct Recovery = 96% Analysis Date = 08/03/22 Pct Recovery = 96% Analysis Date = 08/03/22 Pct Recovery = 96% Analysis Date = 07/30/22 Pct Recovery = 96% Analysis Date = 07/30/22 Pct Recovery = 96% Analysis Date = 07/26/22 Pct Recovery = 96% Analysis Date = 07/26/22 Pct Recovery = 96% Analysis Date = 07/22/22 Pct Recovery = 97% Analysis Date = 07/22/22 Pct Recovery = 97% Analysis Date = 07/18/22 Pct Recovery = 97% Analysis Date = 07/18/22 Pct Recovery = 97% Analysis Date = 07/14/22 Pct Recovery = 97% Analysis Date = 07/14/22 Pct Recovery = 97% Analysis Date = 07/10/22 Pct Recovery = 97% Analysis Date = 07/10/22 Pct Recovery = 97% Analysis Date = 07/06/22 Pct Recovery = 97% Analysis Date = 07/06/22 Pct Recovery = 97% Analysis Date = 07/01/22 Pct Recovery = 97% Analysis Date = 07/01/22 Pct Recovery = 97% Analysis Date = 06/27/22 Pct Recovery = 97% Analysis Date = 06/27/22 Pct Recovery = 97% Analysis Date = 06/23/22 Pct Recovery = 97% Analysis Date = 06/23/22 Pct Recovery = 97% Analysis Date = 06/19/22 Pct Recovery = 97% Analysis Date = 06/19/22 Pct Recovery = 97% Analysis Date = 06/15/22 Pct Recovery = 97% Analysis Date = 06/15/22 Pct Recovery = 97% Analysis Date = 06/11/22 Pct Recovery = 98% Analysis Date = 06/11/22 Pct Recovery = 98% Analysis Date = 06/07/22 Pct Recovery = 98% Analysis Date = 06/07/22 Pct Recovery = 98% Analysis Date = 06/03/22 Pct Recovery = 98% Analysis Date = 06/03/22 Pct Recovery = 98% Analysis Date = 05/30/22 Pct Recovery = 98% Analysis Date = 05/30/22 Pct Recovery = 98% Analysis Date = 05/26/22 Pct Recovery = 98% Analysis Date = 05/26/22 Pct Recovery = 98% Analysis Date = 05/22/22 Pct Recovery = 98% Analysis Date = 05/22/22 Pct Recovery = 98% Analysis Date = 05/17/22 Pct Recovery = 98% Analysis Date = 05/17/22 Pct Recovery = 98% Analysis Date = 05/13/22 Pct Recovery = 98% Analysis Date = 05/13/22 Pct Recovery = 98% Analysis Date = 05/09/22 Pct Recovery = 98% Analysis Date = 05/09/22 Pct Recovery = 98% Analysis Date = 05/05/22 Pct Recovery = 99% Analysis Date = 05/05/22 Pct Recovery = 99% Analysis Date = 05/01/22 Pct Recovery = 99% Analysis Date = 05/01/22 Pct Recovery = 99% Analysis Date = 04/27/22 Pct Recovery = 99% Analysis Date = 04/27/22 Pct Recovery = 99% Analysis Date = 04/23/22 Pct Recovery = 99% Analysis Date = 04/23/22 Pct Recovery = 99% Analysis Date = 04/19/22 Pct Recovery = 99% Analysis Date = 04/19/22 Pct Recovery = 99% Analysis Date = 04/15/22 Pct Recovery = 99% Analysis Date = 04/15/22 Pct Recovery = 99% Analysis Date = 04/11/22 Pct Recovery = 99% Analysis Date = 04/11/22 Pct Recovery = 99% Analysis Date = 04/06/22 Pct Recovery = 99% Analysis Date = 04/06/22 Pct Recovery = 99% Analysis Date = 04/02/22 Pct Recovery = 99% Analysis Date = 04/02/22 Pct Recovery = 99% Analysis Date = 03/29/22 Pct Recovery = 100% Analysis Date = 03/29/22 Pct Recovery = 100% Analysis Date = 03/25/22 Pct Recovery = 100% Analysis Date = 03/25/22 Pct Recovery = 100% Analysis Date = 03/21/22 Pct Recovery = 100% Analysis Date = 03/21/22 Pct Recovery = 100% Analysis Date = 03/17/22 Pct Recovery = 100% Analysis Date = 03/17/22 Pct Recovery = 100% Analysis Date = 03/13/22 Pct Recovery = 100% Analysis Date = 03/13/22 Pct Recovery = 100% Analysis Date = 03/09/22 Pct Recovery = 100% Analysis Date = 03/09/22 Pct Recovery = 100% Analysis Date = 03/05/22 Pct Recovery = 100% Analysis Date = 03/05/22 Pct Recovery = 100% Analysis Date = 03/01/22 Pct Recovery = 100% Analysis Date = 03/01/22 Pct Recovery = 100% Analysis Date = 02/25/22 Pct Recovery = 100% Analysis Date = 02/25/22 Pct Recovery = 100% Analysis Date = 02/20/22 Pct Recovery = 101% Analysis Date = 02/20/22 Pct Recovery = 101% Analysis Date = 02/16/22 Pct Recovery = 101% Analysis Date = 02/16/22 Pct Recovery = 101% Analysis Date = 02/12/22 Pct Recovery = 101% Analysis Date = 02/12/22 Pct Recovery = 101% Analysis Date = 02/08/22 Pct Recovery = 101% Analysis Date = 02/08/22 Pct Recovery = 101% Analysis Date = 02/04/22 Pct Recovery = 101% Analysis Date = 02/04/22 Pct Recovery = 101% Analysis Date = 01/31/22 Pct Recovery = 101% Analysis Date = 01/31/22 Pct Recovery = 101% Analysis Date = 01/27/22 Pct Recovery = 101% Analysis Date = 01/27/22 Pct Recovery = 101% Analysis Date = 01/23/22 Pct Recovery = 101% Analysis Date = 01/23/22 Pct Recovery = 101% Analysis Date = 01/19/22 Pct Recovery = 101% Analysis Date = 01/19/22 Pct Recovery = 101% Analysis Date = 01/15/22 Pct Recovery = 102% Analysis Date = 01/15/22 Pct Recovery = 102% Analysis Date = 01/10/22 Pct Recovery = 102% Analysis Date = 01/10/22 Pct Recovery = 102% Analysis Date = 01/06/22 Pct Recovery = 102% Analysis Date = 01/06/22 Pct Recovery = 102% Analysis Date = 01/02/22 Pct Recovery = 102% Analysis Date = 01/02/22 Pct Recovery = 102% Analysis Date = 12/29/21 Pct Recovery = 102% Analysis Date = 12/29/21 Pct Recovery = 102% Analysis Date = 12/25/21 Pct Recovery = 102% Analysis Date = 12/25/21 Pct Recovery = 102% Analysis Date = 12/21/21 Pct Recovery = 102% Analysis Date = 12/21/21 Pct Recovery = 102% Analysis Date = 12/17/21 Pct Recovery = 102% Analysis Date = 12/17/21 Pct Recovery = 102% Analysis Date = 12/13/21 Pct Recovery = 102% Analysis Date = 12/13/21 Pct Recovery = 102% Analysis Date = 12/09/21 Pct Recovery = 103% Analysis Date = 12/09/21 Pct Recovery = 103% Analysis Date = 12/05/21 Pct Recovery = 103% Analysis Date = 12/05/21 Pct Recovery = 103% Analysis Date = 12/01/21 Pct Recovery = 103% Analysis Date = 12/01/21 Pct Recovery = 103% Analysis Date = 11/26/21 Pct Recovery = 103% Analysis Date = 11/26/21 Pct Recovery = 103% Analysis Date = 11/22/21 Pct Recovery = 103% Analysis Date = 11/22/21 Pct Recovery = 103% Analysis Date = 11/18/21 Pct Recovery = 103% Analysis Date = 11/18/21 Pct Recovery = 103% Analysis Date = 11/14/21 Pct Recovery = 103% Analysis Date = 11/14/21 Pct Recovery = 103% Analysis Date = 11/10/21 Pct Recovery = 103% Analysis Date = 11/10/21 Pct Recovery = 103% Analysis Date = 11/06/21 Pct Recovery = 103% Analysis Date = 11/06/21 Pct Recovery = 103% Analysis Date = 11/02/21 Pct Recovery = 104% Analysis Date = 11/02/21 Pct Recovery = 104% Analysis Date = 10/29/21 Pct Recovery = 104% Analysis Date = 10/29/21 Pct Recovery = 104% Analysis Date = 10/25/21 Pct Recovery = 104% Analysis Date = 10/25/21 Pct Recovery = 104% Analysis Date = 10/21/21 Pct Recovery = 104% Analysis Date = 10/21/21 Pct Recovery = 104% Analysis Date = 10/16/21 Pct Recovery = 104% Analysis Date = 10/16/21 Pct Recovery = 104% Analysis Date = 10/12/21 Pct Recovery = 104% Analysis Date = 10/12/21 Pct Recovery = 104% Analysis Date = 10/08/21 Pct Recovery = 104% Analysis Date = 10/08/21 Pct Recovery = 104% Analysis Date = 10/04/21 Pct Recovery = 104% Analysis Date = 10/04/21 Pct Recovery = 104% Analysis Date = 09/30/21 Pct Recovery = 104% Analysis Date = 09/30/21 Pct Recovery = 104% Analysis Date = 09/26/21 Pct Recovery = 105% Analysis Date = 09/26/21 Pct Recovery = 105% Analysis Date = 09/22/21 Pct Recovery = 105% Analysis Date = 09/22/21 Pct Recovery = 105% Analysis Date = 09/18/21 Pct Recovery = 105% Analysis Date = 09/18/21 Pct Recovery = 105% Analysis Date = 09/14/21 Pct Recovery = 105% Analysis Date = 09/14/21 Pct Recovery = 105% Analysis Date = 09/10/21 Pct Recovery = 105% Analysis Date = 09/10/21 Pct Recovery = 105% Analysis Date = 09/06/21 Pct Recovery = 105% Analysis Date = 09/06/21 Pct Recovery = 105% Analysis Date = 09/01/21 Pct Recovery = 105% Analysis Date = 09/01/21 Pct Recovery = 105% Analysis Date = 08/28/21 Pct Recovery = 105% Analysis Date = 08/28/21 Pct Recovery = 105% Analysis Date = 08/24/21 Pct Recovery = 105% Analysis Date = 08/24/21 Pct Recovery = 105% Analysis Date = 08/20/21 Pct Recovery = 106% Analysis Date = 08/20/21 Pct Recovery = 106% Analysis Date = 08/16/21 Pct Recovery = 106% Analysis Date = 08/16/21 Pct Recovery = 106% Analysis Date = 08/12/21 Pct Recovery = 106% Analysis Date = 08/12/21 Pct Recovery = 106% Analysis Date = 08/08/21 Pct Recovery = 106% Analysis Date = 08/08/21 Pct Recovery = 106% Analysis Date = 08/04/21 Pct Recovery = 106% Analysis Date = 08/04/21 Pct Recovery = 106% Analysis Date = 07/31/21 Pct Recovery = 106% Analysis Date = 07/31/21 Pct Recovery = 106% Analysis Date = 07/27/21 Pct Recovery = 106% Analysis Date = 07/27/21 Pct Recovery = 106% Analysis Date = 07/22/21 Pct Recovery = 106% Analysis Date = 07/22/21 Pct Recovery = 106% Analysis Date = 07/18/21 Pct Recovery = 106% Analysis Date = 07/18/21 Pct Recovery = 106% Analysis Date = 07/14/21 Pct Recovery = 107% Analysis Date = 07/14/21 Pct Recovery = 107% Analysis Date = 07/10/21 Pct Recovery = 107% Analysis Date = 07/10/21 Pct Recovery = 107% Analysis Date = 07/06/21 Pct Recovery = 107% Analysis Date = 07/06/21 Pct Recovery = 107% Analysis Date = 07/02/21 Pct Recovery = 107% Analysis Date = 07/02/21 Pct Recovery = 107% Analysis Date = 06/28/21 Pct Recovery = 107% Analysis Date = 06/28/21 Pct Recovery = 107% Analysis Date = 06/24/21 Pct Recovery = 107% Analysis Date = 06/24/21 Pct Recovery = 107% Analysis Date = 06/20/21 Pct Recovery = 107% Analysis Date = 06/20/21 Pct Recovery = 107% Analysis Date = 06/16/21 Pct Recovery = 107% Analysis Date = 06/16/21 Pct Recovery = 107% Analysis Date = 06/12/21 Pct Recovery = 107% Analysis Date = 06/12/21 Pct Recovery = 107% Analysis Date = 06/07/21 Pct Recovery = 108% Analysis Date = 06/07/21 Pct Recovery = 108% Analysis Date = 06/03/21 Pct Recovery = 108% Analysis Date = 06/03/21 Pct Recovery = 108% Analysis Date = 05/30/21 Pct Recovery = 108% Analysis Date = 05/30/21 Pct Recovery = 108% Analysis Date = 05/26/21 Pct Recovery = 108% Analysis Date = 05/26/21 Pct Recovery = 108% Analysis Date = 05/22/21 Pct Recovery = 108% Analysis Date = 05/22/21 Pct Recovery = 108% Analysis Date = 05/18/21 Pct Recovery = 108% Analysis Date = 05/18/21 Pct Recovery = 108% Analysis Date = 05/14/21 Pct Recovery = 108% Analysis Date = 05/14/21 Pct Recovery = 108% Analysis Date = 05/10/21 Pct Recovery = 108% Analysis Date = 05/10/21 Pct Recovery = 108% Analysis Date = 05/06/21 Pct Recovery = 108% Analysis Date = 05/06/21 Pct Recovery = 108% Analysis Date = 05/02/21 Pct Recovery = 109% Analysis Date = 05/02/21 Pct Recovery = 109% Analysis Date = 04/27/21 Pct Recovery = 109% Analysis Date = 04/27/21 Pct Recovery = 109% Analysis Date = 04/23/21 Pct Recovery = 109% Analysis Date = 04/23/21 Pct Recovery = 109% Analysis Date = 04/19/21 Pct Recovery = 109% Analysis Date = 04/19/21 Pct Recovery = 109% Analysis Date = 04/15/21 Pct Recovery = 109% Analysis Date = 04/15/21 Pct Recovery = 109% Analysis Date = 04/11/21 Pct Recovery = 109% Analysis Date = 04/11/21 Pct Recovery = 109% Analysis Date = 04/07/21 Pct Recovery = 109% Analysis Date = 04/07/21 Pct Recovery = 109% Analysis Date = 04/03/21 Pct Recovery = 109% Analysis Date = 04/03/21 Pct Recovery = 109% Analysis Date = 03/30/21 Pct Recovery = 109% Analysis Date = 03/30/21 Pct Recovery = 109% Analysis Date = 03/26/21 Pct Recovery = 110% Analysis Date = 03/26/21 Pct Recovery = 110% Analysis Date = 03/22/21 Pct Recovery = 110% Analysis Date = 03/22/21 Pct Recovery = 110% Analysis Date = 03/18/21 Pct Recovery = 110% Analysis Date = 03/18/21 Pct Recovery = 110% Analysis Date = 03/13/21 Pct Recovery = 110% Analysis Date = 03/13/21 Pct Recovery = 110% Analysis Date = 03/09/21 Pct Recovery = 110% Analysis Date = 03/09/21 Pct Recovery = 110% Analysis Date = 03/05/21 Pct Recovery = 110% Analysis Date = 03/05/21 Pct Recovery = 110% Analysis Date = 03/01/21 Pct Recovery = 110% Analysis Date = 03/01/21 Pct Recovery = 110% Analysis Date = 02/25/21 Pct Recovery = 110% Analysis Date = 02/25/21 Pct Recovery = 110% Analysis Date = 02/21/21 Pct Recovery = 110% Analysis Date = 02/21/21 Pct Recovery = 110% Analysis Date = 02/17/21 Pct Recovery = 111% Analysis Date = 02/17/21 Pct Recovery = 111% Analysis Date = 02/13/21 Pct Recovery = 111% Analysis Date = 02/13/21 Pct Recovery = 111% Analysis Date = 02/09/21 Pct Recovery = 111% Analysis Date = 02/09/21 Pct Recovery = 111% Analysis Date = 02/05/21 Pct Recovery = 111% Analysis Date = 02/05/21 Pct Recovery = 111% Analysis Date = 01/31/21 Pct Recovery = 111% Analysis Date = 01/31/21 Pct Recovery = 111% Analysis Date = 01/27/21 Pct Recovery = 111% Analysis Date = 01/27/21 Pct Recovery = 111% Analysis Date = 01/23/21 Pct Recovery = 111% Analysis Date = 01/23/21 Pct Recovery = 111% Analysis Date = 01/19/21 Pct Recovery = 111% Analysis Date = 01/19/21 Pct Recovery = 111% Analysis Date = 01/15/21 Pct Recovery = 111% Analysis Date = 01/15/21 Pct Recovery = 111% Analysis Date = 01/11/21 Pct Recovery = 111% Analysis Date = 01/11/21 Pct Recovery = 111% Analysis Date = 01/07/21 Pct Recovery = 112% Analysis Date = 01/07/21 Pct Recovery = 112% Analysis Date = 01/03/21 Pct Recovery = 112% Analysis Date = 01/03/21 Pct Recovery = 112% Analysis Date = 12/30/20 Pct Recovery = 112% Analysis Date = 12/30/20 Pct Recovery = 112% Analysis Date = 12/26/20 Pct Recovery = 112% Analysis Date = 12/26/20 Pct Recovery = 112% Analysis Date = 12/22/20 Pct Recovery = 112% Analysis Date = 12/22/20 Pct Recovery = 112% Analysis Date = 12/17/20 Pct Recovery = 112% Analysis Date = 12/17/20 Pct Recovery = 112% Analysis Date = 12/13/20 Pct Recovery = 112% Analysis Date = 12/13/20 Pct Recovery = 112% Analysis Date = 12/09/20 Pct Recovery = 113% Analysis Date = 12/09/20 Pct Recovery = 113% Analysis Date = 12/05/20 Pct Recovery = 113% Analysis Date = 12/05/20 Pct Recovery = 113% Analysis Date = 12/01/20 Pct Recovery = 113% Analysis Date = 12/01/20 Pct Recovery = 113% Analysis Date = 11/27/20 Pct Recovery = 113% Analysis Date = 11/27/20 Pct Recovery = 113% Analysis Date = 11/23/20 Pct Recovery = 114% Analysis Date = 11/23/20 Pct Recovery = 114% Analysis Date = 11/19/20 Pct Recovery = 114% Analysis Date = 11/19/20 Pct Recovery = 114% Analysis Date = 11/15/20 Pct Recovery = 114% Analysis Date = 11/15/20 Pct Recovery = 114% Analysis Date = 11/11/20 Pct Recovery = 114% Analysis Date = 11/11/20 Pct Recovery = 114% Analysis Date = 11/06/20 Pct Recovery = 114% Analysis Date = 11/06/20 Pct Recovery = 114% Analysis Date = 11/02/20 Pct Recovery = 114% Analysis Date = 11/02/20 Pct Recovery = 114% Analysis Date = 10/29/20 Pct Recovery = 113% Analysis Date = 10/29/20 Pct Recovery = 113% Analysis Date = 10/25/20 Pct Recovery = 113% Analysis Date = 10/25/20 Pct Recovery = 113% Analysis Date = 10/21/20 Pct Recovery = 113% Analysis Date = 10/21/20 Pct Recovery = 113% Analysis Date = 10/17/20 Pct Recovery = 112% Analysis Date = 10/17/20 Pct Recovery = 112% Analysis Date = 10/13/20 Pct Recovery = 111% Analysis Date = 10/13/20 Pct Recovery = 111% Analysis Date = 10/09/20 Pct Recovery = 110% Analysis Date = 10/09/20 Pct Recovery = 110% Analysis Date = 10/05/20 Pct Recovery = 109% Analysis Date = 10/05/20 Pct Recovery = 109% Analysis Date = 10/01/20 Pct Recovery = 108% Analysis Date = 10/01/20 Pct Recovery = 108% Analysis Date = 09/27/20 Pct Recovery = 107% Analysis Date = 09/27/20 Pct Recovery = 107% Analysis Date = 09/22/20 Pct Recovery = 106% Analysis Date = 09/22/20 Pct Recovery = 106% Analysis Date = 09/18/20 Pct Recovery = 104% Analysis Date = 09/18/20 Pct Recovery = 104% Analysis Date = 09/14/20 Pct Recovery = 104% Analysis Date = 09/14/20 Pct Recovery = 104% Analysis Date = 09/10/20 Pct Recovery = 104% Analysis Date = 09/10/20 Pct Recovery = 104% Analysis Date = 09/06/20 Pct Recovery = 105% Analysis Date = 09/06/20 Pct Recovery = 105% Analysis Date = 09/02/20 Pct Recovery = 105% Analysis Date = 09/02/20 Pct Recovery = 105% Analysis Date = 08/29/20 Pct Recovery = 106% Analysis Date = 08/29/20 Pct Recovery = 106% Analysis Date = 08/25/20 Pct Recovery = 107% Analysis Date = 08/25/20 Pct Recovery = 107% Analysis Date = 08/21/20 Pct Recovery = 107% Analysis Date = 08/21/20 Pct Recovery = 107% Analysis Date = 08/17/20 Pct Recovery = 108% Analysis Date = 08/17/20 Pct Recovery = 108% Analysis Date = 08/12/20 Pct Recovery = 109% Analysis Date = 08/12/20 Pct Recovery = 109% Analysis Date = 08/08/20 Pct Recovery = 109% Analysis Date = 08/08/20 Pct Recovery = 109% Analysis Date = 08/04/20 Pct Recovery = 110% Analysis Date = 08/04/20 Pct Recovery = 110% Analysis Date = 07/31/20 Pct Recovery = 111% Analysis Date = 07/31/20 Pct Recovery = 111% Analysis Date = 07/27/20 Pct Recovery = 112% Analysis Date = 07/27/20 Pct Recovery = 112% Analysis Date = 07/23/20 Pct Recovery = 113% Analysis Date = 07/23/20 Pct Recovery = 113% Analysis Date = 07/19/20 Pct Recovery = 114% Analysis Date = 07/19/20 Pct Recovery = 114% Analysis Date = 07/15/20 Pct Recovery = 115% Analysis Date = 07/15/20 Pct Recovery = 115% Analysis Date = 07/11/20 Pct Recovery = 116% Analysis Date = 07/11/20 Pct Recovery = 116% Analysis Date = 07/07/20 Pct Recovery = 117% Analysis Date = 07/07/20 Pct Recovery = 117% Analysis Date = 07/03/20 Pct Recovery = 118% Analysis Date = 07/03/20 Pct Recovery = 118% Analysis Date = 06/28/20 Pct Recovery = 119% Analysis Date = 06/28/20 Pct Recovery = 119% Analysis Date = 06/24/20 Pct Recovery = 120% Analysis Date = 06/24/20 Pct Recovery = 120% Analysis Date = 06/20/20 Pct Recovery = 121% Analysis Date = 06/20/20 Pct Recovery = 121% Analysis Date = 06/16/20 Pct Recovery = 122% Analysis Date = 06/16/20 Pct Recovery = 122% Analysis Date = 06/12/20 Pct Recovery = 123% Analysis Date = 06/12/20 Pct Recovery = 123% Analysis Date = 06/08/20 Pct Recovery = 124% Analysis Date = 06/08/20 Pct Recovery = 124% Analysis Date = 06/04/20 Pct Recovery = 125% Analysis Date = 06/04/20 Pct Recovery = 125% Analysis Date = 05/31/20 Pct Recovery = 126% Analysis Date = 05/31/20 Pct Recovery = 126% Analysis Date = 05/27/20 Pct Recovery = 127% Analysis Date = 05/27/20 Pct Recovery = 127% Analysis Date = 05/23/20 Pct Recovery = 128% Analysis Date = 05/23/20 Pct Recovery = 128% Analysis Date = 05/19/20 Pct Recovery = 129% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 2 165% 99% 165% 103%
>= Reporting Level 25 105% 26% 99% 23%
Total 27 110% 35% 99% 29%

Sample Statistics
TERBUFOS SULFONE

Characteristic N % % Basis
Plotted 27 96% Spiked
Estimated Values 7 25% Spiked
Deleted Values 2 2% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 29 .  
False Negatives 1 4% 1 out of 28
Not Spiked 87 .  
False Positives 1 1% 1 out of 86

OBSP Determination:
TERBUFOS SULFOXIDE
METHOD: 2447 , TESTIDCODE: 68704LCM60

Laboratory ID = 20202390020 Lab Value = 34.540 Expected Conc. = 37.7 Report level label = 3 Pct Recovery = 92% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20201820155 Lab Value = 44.292 Expected Conc. = 37.4 Report level label = 3 Pct Recovery = 118% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 40.188 Expected Conc. = 37.4 Report level label = 3 Pct Recovery = 107% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202590106 Lab Value = 27.601 Expected Conc. = 37.3 Report level label = 3 Pct Recovery = 74% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 24.349 Expected Conc. = 37.3 Report level label = 3 Pct Recovery = 65% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203230021 Lab Value = 22.989 Expected Conc. = 36.75 Report level label = 3 Pct Recovery = 63% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 22.469 Expected Conc. = 36.75 Report level label = 3 Pct Recovery = 61% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20221370164 Lab Value = 21.601 Expected Conc. = 30.2 Report level label = 3 Pct Recovery = 72% Analysis Date = 05/24/22 SpikeMix = Abs 100521Pest3_4a: 80 µl & Abs 100521Pest3_4b: 80 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20222210250 Lab Value = 41.251 Expected Conc. = 30 Report level label = 3 Pct Recovery = 138% Analysis Date = 08/16/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20221940194 Lab Value = 29.704 Expected Conc. = 30 Report level label = 3 Pct Recovery = 99% Analysis Date = 07/23/22 SpikeMix = Crescent 04EE026: 80 µl SpecificMix = 04EE026 Laboratory ID = 20221580147 Lab Value = 33.406 Expected Conc. = 30 Report level label = 3 Pct Recovery = 111% Analysis Date = 06/22/22 SpikeMix = Crescent 02BB022: 80 µl SpecificMix = 02BB022 Laboratory ID = 20201960104 Lab Value = 16.035 Expected Conc. = 18.85 Report level label = 3 Pct Recovery = 85% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20222070177 Lab Value = 18.620 Expected Conc. = 18.75 Report level label = 3 Pct Recovery = 99% Analysis Date = 08/03/22 SpikeMix = Crescent 02BB022: 50 µl SpecificMix = 02BB022 Laboratory ID = 20202530029 Lab Value = 20.221 Expected Conc. = 18.7 Report level label = 3 Pct Recovery = 108% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 19.451 Expected Conc. = 18.7 Report level label = 3 Pct Recovery = 104% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 21.517 Expected Conc. = 18.7 Report level label = 3 Pct Recovery = 115% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20203230018 Lab Value = 12.317 Expected Conc. = 18.65 Report level label = 3 Pct Recovery = 66% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 10.636 Expected Conc. = 18.65 Report level label = 3 Pct Recovery = 57% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 17.052 Expected Conc. = 18.65 Report level label = 3 Pct Recovery = 91% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20221160208 Lab Value = 4.035 Expected Conc. = 7.55 Report level label = 3 Pct Recovery = 53% Analysis Date = 05/03/22 SpikeMix = Abs 100521Pest3_4a: 20 µl & Abs 100521Pest3_4b: 20 µl SpecificMix = 100521Pest3_4a Laboratory ID = 20201610160 Lab Value = 7.351 Expected Conc. = 7.54 Report level label = 3 Pct Recovery = 97% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20222000207 Lab Value = 7.782 Expected Conc. = 7.5 Report level label = 3 Pct Recovery = 104% Analysis Date = 07/27/22 SpikeMix = Crescent 02BB022: 20 µl SpecificMix = 02BB022 Laboratory ID = 20202180001 Lab Value = 5.832 Expected Conc. = 7.48 Report level label = 3 Pct Recovery = 78% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 10.584 Expected Conc. = 7.48 Report level label = 3 Pct Recovery = 141% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 4.845 Expected Conc. = 7.48 Report level label = 3 Pct Recovery = 65% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210970035 Lab Value = 4.266 Expected Conc. = 7.46 Report level label = 3 Pct Recovery = 57% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 5.277 Expected Conc. = 7.46 Report level label = 3 Pct Recovery = 71% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 6.436 Expected Conc. = 7.46 Report level label = 3 Pct Recovery = 86% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 7.230 Expected Conc. = 7.46 Report level label = 3 Pct Recovery = 97% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 4.924 Expected Conc. = 7.46 Report level label = 3 Pct Recovery = 66% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 5.635 Expected Conc. = 7.46 Report level label = 3 Pct Recovery = 76% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210830019 Lab Value = 4.607 Expected Conc. = 7.35 Report level label = 3 Pct Recovery = 63% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 4.712 Expected Conc. = 7.35 Report level label = 3 Pct Recovery = 64% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 08/16/22 Pct Recovery = 102% Analysis Date = 08/11/22 Pct Recovery = 102% Analysis Date = 08/11/22 Pct Recovery = 102% Analysis Date = 08/07/22 Pct Recovery = 102% Analysis Date = 08/07/22 Pct Recovery = 102% Analysis Date = 08/03/22 Pct Recovery = 101% Analysis Date = 08/03/22 Pct Recovery = 101% Analysis Date = 07/30/22 Pct Recovery = 101% Analysis Date = 07/30/22 Pct Recovery = 101% Analysis Date = 07/26/22 Pct Recovery = 100% Analysis Date = 07/26/22 Pct Recovery = 100% Analysis Date = 07/22/22 Pct Recovery = 100% Analysis Date = 07/22/22 Pct Recovery = 100% Analysis Date = 07/18/22 Pct Recovery = 99% Analysis Date = 07/18/22 Pct Recovery = 99% Analysis Date = 07/14/22 Pct Recovery = 99% Analysis Date = 07/14/22 Pct Recovery = 99% Analysis Date = 07/10/22 Pct Recovery = 99% Analysis Date = 07/10/22 Pct Recovery = 99% Analysis Date = 07/06/22 Pct Recovery = 98% Analysis Date = 07/06/22 Pct Recovery = 98% Analysis Date = 07/01/22 Pct Recovery = 98% Analysis Date = 07/01/22 Pct Recovery = 98% Analysis Date = 06/27/22 Pct Recovery = 97% Analysis Date = 06/27/22 Pct Recovery = 97% Analysis Date = 06/23/22 Pct Recovery = 97% Analysis Date = 06/23/22 Pct Recovery = 97% Analysis Date = 06/19/22 Pct Recovery = 96% Analysis Date = 06/19/22 Pct Recovery = 96% Analysis Date = 06/15/22 Pct Recovery = 96% Analysis Date = 06/15/22 Pct Recovery = 96% Analysis Date = 06/11/22 Pct Recovery = 96% Analysis Date = 06/11/22 Pct Recovery = 96% Analysis Date = 06/07/22 Pct Recovery = 95% Analysis Date = 06/07/22 Pct Recovery = 95% Analysis Date = 06/03/22 Pct Recovery = 95% Analysis Date = 06/03/22 Pct Recovery = 95% Analysis Date = 05/30/22 Pct Recovery = 95% Analysis Date = 05/30/22 Pct Recovery = 95% Analysis Date = 05/26/22 Pct Recovery = 94% Analysis Date = 05/26/22 Pct Recovery = 94% Analysis Date = 05/22/22 Pct Recovery = 94% Analysis Date = 05/22/22 Pct Recovery = 94% Analysis Date = 05/17/22 Pct Recovery = 93% Analysis Date = 05/17/22 Pct Recovery = 93% Analysis Date = 05/13/22 Pct Recovery = 93% Analysis Date = 05/13/22 Pct Recovery = 93% Analysis Date = 05/09/22 Pct Recovery = 93% Analysis Date = 05/09/22 Pct Recovery = 93% Analysis Date = 05/05/22 Pct Recovery = 92% Analysis Date = 05/05/22 Pct Recovery = 92% Analysis Date = 05/01/22 Pct Recovery = 92% Analysis Date = 05/01/22 Pct Recovery = 92% Analysis Date = 04/27/22 Pct Recovery = 91% Analysis Date = 04/27/22 Pct Recovery = 91% Analysis Date = 04/23/22 Pct Recovery = 91% Analysis Date = 04/23/22 Pct Recovery = 91% Analysis Date = 04/19/22 Pct Recovery = 91% Analysis Date = 04/19/22 Pct Recovery = 91% Analysis Date = 04/15/22 Pct Recovery = 90% Analysis Date = 04/15/22 Pct Recovery = 90% Analysis Date = 04/11/22 Pct Recovery = 90% Analysis Date = 04/11/22 Pct Recovery = 90% Analysis Date = 04/06/22 Pct Recovery = 90% Analysis Date = 04/06/22 Pct Recovery = 90% Analysis Date = 04/02/22 Pct Recovery = 89% Analysis Date = 04/02/22 Pct Recovery = 89% Analysis Date = 03/29/22 Pct Recovery = 89% Analysis Date = 03/29/22 Pct Recovery = 89% Analysis Date = 03/25/22 Pct Recovery = 89% Analysis Date = 03/25/22 Pct Recovery = 89% Analysis Date = 03/21/22 Pct Recovery = 88% Analysis Date = 03/21/22 Pct Recovery = 88% Analysis Date = 03/17/22 Pct Recovery = 88% Analysis Date = 03/17/22 Pct Recovery = 88% Analysis Date = 03/13/22 Pct Recovery = 88% Analysis Date = 03/13/22 Pct Recovery = 88% Analysis Date = 03/09/22 Pct Recovery = 87% Analysis Date = 03/09/22 Pct Recovery = 87% Analysis Date = 03/05/22 Pct Recovery = 87% Analysis Date = 03/05/22 Pct Recovery = 87% Analysis Date = 03/01/22 Pct Recovery = 87% Analysis Date = 03/01/22 Pct Recovery = 87% Analysis Date = 02/25/22 Pct Recovery = 86% Analysis Date = 02/25/22 Pct Recovery = 86% Analysis Date = 02/20/22 Pct Recovery = 86% Analysis Date = 02/20/22 Pct Recovery = 86% Analysis Date = 02/16/22 Pct Recovery = 86% Analysis Date = 02/16/22 Pct Recovery = 86% Analysis Date = 02/12/22 Pct Recovery = 85% Analysis Date = 02/12/22 Pct Recovery = 85% Analysis Date = 02/08/22 Pct Recovery = 85% Analysis Date = 02/08/22 Pct Recovery = 85% Analysis Date = 02/04/22 Pct Recovery = 85% Analysis Date = 02/04/22 Pct Recovery = 85% Analysis Date = 01/31/22 Pct Recovery = 84% Analysis Date = 01/31/22 Pct Recovery = 84% Analysis Date = 01/27/22 Pct Recovery = 84% Analysis Date = 01/27/22 Pct Recovery = 84% Analysis Date = 01/23/22 Pct Recovery = 84% Analysis Date = 01/23/22 Pct Recovery = 84% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/19/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/15/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/10/22 Pct Recovery = 83% Analysis Date = 01/06/22 Pct Recovery = 82% Analysis Date = 01/06/22 Pct Recovery = 82% Analysis Date = 01/02/22 Pct Recovery = 82% Analysis Date = 01/02/22 Pct Recovery = 82% Analysis Date = 12/29/21 Pct Recovery = 82% Analysis Date = 12/29/21 Pct Recovery = 82% Analysis Date = 12/25/21 Pct Recovery = 81% Analysis Date = 12/25/21 Pct Recovery = 81% Analysis Date = 12/21/21 Pct Recovery = 81% Analysis Date = 12/21/21 Pct Recovery = 81% Analysis Date = 12/17/21 Pct Recovery = 81% Analysis Date = 12/17/21 Pct Recovery = 81% Analysis Date = 12/13/21 Pct Recovery = 80% Analysis Date = 12/13/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/09/21 Pct Recovery = 80% Analysis Date = 12/05/21 Pct Recovery = 80% Analysis Date = 12/05/21 Pct Recovery = 80% Analysis Date = 12/01/21 Pct Recovery = 79% Analysis Date = 12/01/21 Pct Recovery = 79% Analysis Date = 11/26/21 Pct Recovery = 79% Analysis Date = 11/26/21 Pct Recovery = 79% Analysis Date = 11/22/21 Pct Recovery = 79% Analysis Date = 11/22/21 Pct Recovery = 79% Analysis Date = 11/18/21 Pct Recovery = 78% Analysis Date = 11/18/21 Pct Recovery = 78% Analysis Date = 11/14/21 Pct Recovery = 78% Analysis Date = 11/14/21 Pct Recovery = 78% Analysis Date = 11/10/21 Pct Recovery = 78% Analysis Date = 11/10/21 Pct Recovery = 78% Analysis Date = 11/06/21 Pct Recovery = 77% Analysis Date = 11/06/21 Pct Recovery = 77% Analysis Date = 11/02/21 Pct Recovery = 77% Analysis Date = 11/02/21 Pct Recovery = 77% Analysis Date = 10/29/21 Pct Recovery = 77% Analysis Date = 10/29/21 Pct Recovery = 77% Analysis Date = 10/25/21 Pct Recovery = 76% Analysis Date = 10/25/21 Pct Recovery = 76% Analysis Date = 10/21/21 Pct Recovery = 76% Analysis Date = 10/21/21 Pct Recovery = 76% Analysis Date = 10/16/21 Pct Recovery = 76% Analysis Date = 10/16/21 Pct Recovery = 76% Analysis Date = 10/12/21 Pct Recovery = 75% Analysis Date = 10/12/21 Pct Recovery = 75% Analysis Date = 10/08/21 Pct Recovery = 75% Analysis Date = 10/08/21 Pct Recovery = 75% Analysis Date = 10/04/21 Pct Recovery = 75% Analysis Date = 10/04/21 Pct Recovery = 75% Analysis Date = 09/30/21 Pct Recovery = 74% Analysis Date = 09/30/21 Pct Recovery = 74% Analysis Date = 09/26/21 Pct Recovery = 74% Analysis Date = 09/26/21 Pct Recovery = 74% Analysis Date = 09/22/21 Pct Recovery = 74% Analysis Date = 09/22/21 Pct Recovery = 74% Analysis Date = 09/18/21 Pct Recovery = 73% Analysis Date = 09/18/21 Pct Recovery = 73% Analysis Date = 09/14/21 Pct Recovery = 73% Analysis Date = 09/14/21 Pct Recovery = 73% Analysis Date = 09/10/21 Pct Recovery = 73% Analysis Date = 09/10/21 Pct Recovery = 73% Analysis Date = 09/06/21 Pct Recovery = 72% Analysis Date = 09/06/21 Pct Recovery = 72% Analysis Date = 09/01/21 Pct Recovery = 72% Analysis Date = 09/01/21 Pct Recovery = 72% Analysis Date = 08/28/21 Pct Recovery = 72% Analysis Date = 08/28/21 Pct Recovery = 72% Analysis Date = 08/24/21 Pct Recovery = 71% Analysis Date = 08/24/21 Pct Recovery = 71% Analysis Date = 08/20/21 Pct Recovery = 71% Analysis Date = 08/20/21 Pct Recovery = 71% Analysis Date = 08/16/21 Pct Recovery = 71% Analysis Date = 08/16/21 Pct Recovery = 71% Analysis Date = 08/12/21 Pct Recovery = 70% Analysis Date = 08/12/21 Pct Recovery = 70% Analysis Date = 08/08/21 Pct Recovery = 70% Analysis Date = 08/08/21 Pct Recovery = 70% Analysis Date = 08/04/21 Pct Recovery = 70% Analysis Date = 08/04/21 Pct Recovery = 70% Analysis Date = 07/31/21 Pct Recovery = 69% Analysis Date = 07/31/21 Pct Recovery = 69% Analysis Date = 07/27/21 Pct Recovery = 69% Analysis Date = 07/27/21 Pct Recovery = 69% Analysis Date = 07/22/21 Pct Recovery = 69% Analysis Date = 07/22/21 Pct Recovery = 69% Analysis Date = 07/18/21 Pct Recovery = 68% Analysis Date = 07/18/21 Pct Recovery = 68% Analysis Date = 07/14/21 Pct Recovery = 68% Analysis Date = 07/14/21 Pct Recovery = 68% Analysis Date = 07/10/21 Pct Recovery = 68% Analysis Date = 07/10/21 Pct Recovery = 68% Analysis Date = 07/06/21 Pct Recovery = 67% Analysis Date = 07/06/21 Pct Recovery = 67% Analysis Date = 07/02/21 Pct Recovery = 67% Analysis Date = 07/02/21 Pct Recovery = 67% Analysis Date = 06/28/21 Pct Recovery = 66% Analysis Date = 06/28/21 Pct Recovery = 66% Analysis Date = 06/24/21 Pct Recovery = 66% Analysis Date = 06/24/21 Pct Recovery = 66% Analysis Date = 06/20/21 Pct Recovery = 66% Analysis Date = 06/20/21 Pct Recovery = 66% Analysis Date = 06/16/21 Pct Recovery = 65% Analysis Date = 06/16/21 Pct Recovery = 65% Analysis Date = 06/12/21 Pct Recovery = 65% Analysis Date = 06/12/21 Pct Recovery = 65% Analysis Date = 06/07/21 Pct Recovery = 65% Analysis Date = 06/07/21 Pct Recovery = 65% Analysis Date = 06/03/21 Pct Recovery = 64% Analysis Date = 06/03/21 Pct Recovery = 64% Analysis Date = 05/30/21 Pct Recovery = 64% Analysis Date = 05/30/21 Pct Recovery = 64% Analysis Date = 05/26/21 Pct Recovery = 64% Analysis Date = 05/26/21 Pct Recovery = 64% Analysis Date = 05/22/21 Pct Recovery = 63% Analysis Date = 05/22/21 Pct Recovery = 63% Analysis Date = 05/18/21 Pct Recovery = 63% Analysis Date = 05/18/21 Pct Recovery = 63% Analysis Date = 05/14/21 Pct Recovery = 63% Analysis Date = 05/14/21 Pct Recovery = 63% Analysis Date = 05/10/21 Pct Recovery = 62% Analysis Date = 05/10/21 Pct Recovery = 62% Analysis Date = 05/06/21 Pct Recovery = 62% Analysis Date = 05/06/21 Pct Recovery = 62% Analysis Date = 05/02/21 Pct Recovery = 62% Analysis Date = 05/02/21 Pct Recovery = 62% Analysis Date = 04/27/21 Pct Recovery = 61% Analysis Date = 04/27/21 Pct Recovery = 61% Analysis Date = 04/23/21 Pct Recovery = 61% Analysis Date = 04/23/21 Pct Recovery = 61% Analysis Date = 04/19/21 Pct Recovery = 61% Analysis Date = 04/19/21 Pct Recovery = 61% Analysis Date = 04/15/21 Pct Recovery = 60% Analysis Date = 04/15/21 Pct Recovery = 60% Analysis Date = 04/11/21 Pct Recovery = 60% Analysis Date = 04/11/21 Pct Recovery = 60% Analysis Date = 04/07/21 Pct Recovery = 60% Analysis Date = 04/07/21 Pct Recovery = 60% Analysis Date = 04/03/21 Pct Recovery = 59% Analysis Date = 04/03/21 Pct Recovery = 59% Analysis Date = 03/30/21 Pct Recovery = 59% Analysis Date = 03/30/21 Pct Recovery = 59% Analysis Date = 03/26/21 Pct Recovery = 60% Analysis Date = 03/26/21 Pct Recovery = 60% Analysis Date = 03/22/21 Pct Recovery = 60% Analysis Date = 03/22/21 Pct Recovery = 60% Analysis Date = 03/18/21 Pct Recovery = 61% Analysis Date = 03/18/21 Pct Recovery = 61% Analysis Date = 03/13/21 Pct Recovery = 61% Analysis Date = 03/13/21 Pct Recovery = 61% Analysis Date = 03/09/21 Pct Recovery = 62% Analysis Date = 03/09/21 Pct Recovery = 62% Analysis Date = 03/05/21 Pct Recovery = 63% Analysis Date = 03/05/21 Pct Recovery = 63% Analysis Date = 03/01/21 Pct Recovery = 63% Analysis Date = 03/01/21 Pct Recovery = 63% Analysis Date = 02/25/21 Pct Recovery = 64% Analysis Date = 02/25/21 Pct Recovery = 64% Analysis Date = 02/21/21 Pct Recovery = 64% Analysis Date = 02/21/21 Pct Recovery = 64% Analysis Date = 02/17/21 Pct Recovery = 65% Analysis Date = 02/17/21 Pct Recovery = 65% Analysis Date = 02/13/21 Pct Recovery = 65% Analysis Date = 02/13/21 Pct Recovery = 65% Analysis Date = 02/09/21 Pct Recovery = 66% Analysis Date = 02/09/21 Pct Recovery = 66% Analysis Date = 02/05/21 Pct Recovery = 67% Analysis Date = 02/05/21 Pct Recovery = 67% Analysis Date = 01/31/21 Pct Recovery = 67% Analysis Date = 01/31/21 Pct Recovery = 67% Analysis Date = 01/27/21 Pct Recovery = 68% Analysis Date = 01/27/21 Pct Recovery = 68% Analysis Date = 01/23/21 Pct Recovery = 68% Analysis Date = 01/23/21 Pct Recovery = 68% Analysis Date = 01/19/21 Pct Recovery = 69% Analysis Date = 01/19/21 Pct Recovery = 69% Analysis Date = 01/15/21 Pct Recovery = 69% Analysis Date = 01/15/21 Pct Recovery = 69% Analysis Date = 01/11/21 Pct Recovery = 70% Analysis Date = 01/11/21 Pct Recovery = 70% Analysis Date = 01/07/21 Pct Recovery = 70% Analysis Date = 01/07/21 Pct Recovery = 70% Analysis Date = 01/03/21 Pct Recovery = 71% Analysis Date = 01/03/21 Pct Recovery = 71% Analysis Date = 12/30/20 Pct Recovery = 72% Analysis Date = 12/30/20 Pct Recovery = 72% Analysis Date = 12/26/20 Pct Recovery = 72% Analysis Date = 12/26/20 Pct Recovery = 72% Analysis Date = 12/22/20 Pct Recovery = 73% Analysis Date = 12/22/20 Pct Recovery = 73% Analysis Date = 12/17/20 Pct Recovery = 73% Analysis Date = 12/17/20 Pct Recovery = 73% Analysis Date = 12/13/20 Pct Recovery = 74% Analysis Date = 12/13/20 Pct Recovery = 74% Analysis Date = 12/09/20 Pct Recovery = 74% Analysis Date = 12/09/20 Pct Recovery = 74% Analysis Date = 12/05/20 Pct Recovery = 75% Analysis Date = 12/05/20 Pct Recovery = 75% Analysis Date = 12/01/20 Pct Recovery = 76% Analysis Date = 12/01/20 Pct Recovery = 76% Analysis Date = 11/27/20 Pct Recovery = 76% Analysis Date = 11/27/20 Pct Recovery = 76% Analysis Date = 11/23/20 Pct Recovery = 77% Analysis Date = 11/23/20 Pct Recovery = 77% Analysis Date = 11/19/20 Pct Recovery = 77% Analysis Date = 11/19/20 Pct Recovery = 77% Analysis Date = 11/15/20 Pct Recovery = 78% Analysis Date = 11/15/20 Pct Recovery = 78% Analysis Date = 11/11/20 Pct Recovery = 79% Analysis Date = 11/11/20 Pct Recovery = 79% Analysis Date = 11/06/20 Pct Recovery = 80% Analysis Date = 11/06/20 Pct Recovery = 80% Analysis Date = 11/02/20 Pct Recovery = 80% Analysis Date = 11/02/20 Pct Recovery = 80% Analysis Date = 10/29/20 Pct Recovery = 81% Analysis Date = 10/29/20 Pct Recovery = 81% Analysis Date = 10/25/20 Pct Recovery = 82% Analysis Date = 10/25/20 Pct Recovery = 82% Analysis Date = 10/21/20 Pct Recovery = 83% Analysis Date = 10/21/20 Pct Recovery = 83% Analysis Date = 10/17/20 Pct Recovery = 83% Analysis Date = 10/17/20 Pct Recovery = 83% Analysis Date = 10/13/20 Pct Recovery = 84% Analysis Date = 10/13/20 Pct Recovery = 84% Analysis Date = 10/09/20 Pct Recovery = 85% Analysis Date = 10/09/20 Pct Recovery = 85% Analysis Date = 10/05/20 Pct Recovery = 86% Analysis Date = 10/05/20 Pct Recovery = 86% Analysis Date = 10/01/20 Pct Recovery = 86% Analysis Date = 10/01/20 Pct Recovery = 86% Analysis Date = 09/27/20 Pct Recovery = 87% Analysis Date = 09/27/20 Pct Recovery = 87% Analysis Date = 09/22/20 Pct Recovery = 88% Analysis Date = 09/22/20 Pct Recovery = 88% Analysis Date = 09/18/20 Pct Recovery = 88% Analysis Date = 09/18/20 Pct Recovery = 88% Analysis Date = 09/14/20 Pct Recovery = 89% Analysis Date = 09/14/20 Pct Recovery = 89% Analysis Date = 09/10/20 Pct Recovery = 90% Analysis Date = 09/10/20 Pct Recovery = 90% Analysis Date = 09/06/20 Pct Recovery = 90% Analysis Date = 09/06/20 Pct Recovery = 90% Analysis Date = 09/02/20 Pct Recovery = 91% Analysis Date = 09/02/20 Pct Recovery = 91% Analysis Date = 08/29/20 Pct Recovery = 92% Analysis Date = 08/29/20 Pct Recovery = 92% Analysis Date = 08/25/20 Pct Recovery = 92% Analysis Date = 08/25/20 Pct Recovery = 92% Analysis Date = 08/21/20 Pct Recovery = 93% Analysis Date = 08/21/20 Pct Recovery = 93% Analysis Date = 08/17/20 Pct Recovery = 93% Analysis Date = 08/17/20 Pct Recovery = 93% Analysis Date = 08/12/20 Pct Recovery = 94% Analysis Date = 08/12/20 Pct Recovery = 94% Analysis Date = 08/08/20 Pct Recovery = 95% Analysis Date = 08/08/20 Pct Recovery = 95% Analysis Date = 08/04/20 Pct Recovery = 95% Analysis Date = 08/04/20 Pct Recovery = 95% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/31/20 Pct Recovery = 96% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/27/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 97% Analysis Date = 07/23/20 Pct Recovery = 97% Analysis Date = 07/19/20 Pct Recovery = 98% Analysis Date = 07/19/20 Pct Recovery = 98% Analysis Date = 07/15/20 Pct Recovery = 99% Analysis Date = 07/15/20 Pct Recovery = 99% Analysis Date = 07/11/20 Pct Recovery = 100% Analysis Date = 07/11/20 Pct Recovery = 100% Analysis Date = 07/07/20 Pct Recovery = 100% Analysis Date = 07/07/20 Pct Recovery = 100% Analysis Date = 07/03/20 Pct Recovery = 101% Analysis Date = 07/03/20 Pct Recovery = 101% Analysis Date = 06/28/20 Pct Recovery = 102% Analysis Date = 06/28/20 Pct Recovery = 102% Analysis Date = 06/24/20 Pct Recovery = 102% Analysis Date = 06/24/20 Pct Recovery = 102% Analysis Date = 06/20/20 Pct Recovery = 103% Analysis Date = 06/20/20 Pct Recovery = 103% Analysis Date = 06/16/20 Pct Recovery = 104% Analysis Date = 06/16/20 Pct Recovery = 104% Analysis Date = 06/12/20 Pct Recovery = 104% Analysis Date = 06/12/20 Pct Recovery = 104% Analysis Date = 06/08/20 Pct Recovery = 105% Analysis Date = 06/08/20 Pct Recovery = 105% Analysis Date = 06/04/20 Pct Recovery = 106% Analysis Date = 06/04/20 Pct Recovery = 106% Analysis Date = 05/31/20 Pct Recovery = 106% Analysis Date = 05/31/20 Pct Recovery = 106% Analysis Date = 05/27/20 Pct Recovery = 107% Analysis Date = 05/27/20 Pct Recovery = 107% Analysis Date = 05/23/20 Pct Recovery = 108% Analysis Date = 05/23/20 Pct Recovery = 108% Analysis Date = 05/19/20 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 86% 24% 85% 29%
Total 33 86% 24% 85% 29%

Sample Statistics
TERBUFOS SULFOXIDE

Characteristic N % % Basis
Plotted 33 100% Spiked
Estimated Values 10 30% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 33 .  
False Negatives 0 0% 0 out of 33
Not Spiked 74 .  
False Positives 12 16% 12 out of 74

OBSP Determination:
TETRACONAZOLE
METHOD: 2447 , TESTIDCODE: 66654LCM60

Laboratory ID = 20203230021 Lab Value = 90.156 Expected Conc. = 87.7 Report level label = 7 Pct Recovery = 103% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 70.424 Expected Conc. = 87.7 Report level label = 7 Pct Recovery = 80% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20202590106 Lab Value = 75.322 Expected Conc. = 87.4 Report level label = 7 Pct Recovery = 86% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 80.739 Expected Conc. = 87.4 Report level label = 7 Pct Recovery = 92% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222150192 Lab Value = 57.070 Expected Conc. = 71.2 Report level label = 7 Pct Recovery = 80% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20221520237 Lab Value = 57.954 Expected Conc. = 70.36 Report level label = 7 Pct Recovery = 82% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 45.821 Expected Conc. = 70 Report level label = 7 Pct Recovery = 65% Analysis Date = 07/23/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20221870197 Lab Value = 30.055 Expected Conc. = 43.975 Report level label = 7 Pct Recovery = 68% Analysis Date = 07/12/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20201550031 Lab Value = 43.854 Expected Conc. = 43.95 Report level label = 7 Pct Recovery = 100% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20220740064 Lab Value = 14.270 Expected Conc. = 43.75 Report level label = 7 Pct Recovery = 33% Analysis Date = 03/25/22 SpikeMix = Spex Organics MP211228015: 50 µl SpecificMix = MP211228015 Laboratory ID = 20202390020 Lab Value = 53.042 Expected Conc. = 43.75 Report level label = 7 Pct Recovery = 121% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 42.579 Expected Conc. = 43.75 Report level label = 7 Pct Recovery = 97% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20203230018 Lab Value = 39.885 Expected Conc. = 43.7 Report level label = 7 Pct Recovery = 91% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 33.653 Expected Conc. = 43.7 Report level label = 7 Pct Recovery = 77% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 43.060 Expected Conc. = 43.7 Report level label = 7 Pct Recovery = 99% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20201960104 Lab Value = 43.750 Expected Conc. = 35 Report level label = 7 Pct Recovery = 125% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 33.432 Expected Conc. = 35 Report level label = 7 Pct Recovery = 96% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20221660151 Lab Value = 16.225 Expected Conc. = 17.59 Report level label = 7 Pct Recovery = 92% Analysis Date = 06/22/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101208: 20 µl SpecificMix = 221101208 Laboratory ID = 20202330309 Lab Value = 16.975 Expected Conc. = 17.58 Report level label = 7 Pct Recovery = 97% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 13.665 Expected Conc. = 17.58 Report level label = 7 Pct Recovery = 78% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 16.048 Expected Conc. = 17.58 Report level label = 7 Pct Recovery = 91% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 16.430 Expected Conc. = 17.58 Report level label = 7 Pct Recovery = 93% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 21.306 Expected Conc. = 17.58 Report level label = 7 Pct Recovery = 121% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20210830019 Lab Value = 17.569 Expected Conc. = 17.54 Report level label = 7 Pct Recovery = 100% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 14.095 Expected Conc. = 17.54 Report level label = 7 Pct Recovery = 80% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210970035 Lab Value = 17.430 Expected Conc. = 17.48 Report level label = 7 Pct Recovery = 100% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 21.431 Expected Conc. = 17.48 Report level label = 7 Pct Recovery = 123% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 20.659 Expected Conc. = 17.48 Report level label = 7 Pct Recovery = 118% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 11.100 Expected Conc. = 17.48 Report level label = 7 Pct Recovery = 64% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 18.922 Expected Conc. = 17.48 Report level label = 7 Pct Recovery = 108% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 17.959 Expected Conc. = 17.48 Report level label = 7 Pct Recovery = 103% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Analysis Date = 08/15/22 Pct Recovery = 70% Analysis Date = 08/10/22 Pct Recovery = 70% Analysis Date = 08/10/22 Pct Recovery = 70% Analysis Date = 08/06/22 Pct Recovery = 70% Analysis Date = 08/06/22 Pct Recovery = 70% Analysis Date = 08/02/22 Pct Recovery = 71% Analysis Date = 08/02/22 Pct Recovery = 71% Analysis Date = 07/29/22 Pct Recovery = 71% Analysis Date = 07/29/22 Pct Recovery = 71% Analysis Date = 07/25/22 Pct Recovery = 71% Analysis Date = 07/25/22 Pct Recovery = 71% Analysis Date = 07/21/22 Pct Recovery = 71% Analysis Date = 07/21/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/17/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/13/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/09/22 Pct Recovery = 71% Analysis Date = 07/05/22 Pct Recovery = 71% Analysis Date = 07/05/22 Pct Recovery = 71% Analysis Date = 07/01/22 Pct Recovery = 71% Analysis Date = 07/01/22 Pct Recovery = 71% Analysis Date = 06/27/22 Pct Recovery = 72% Analysis Date = 06/27/22 Pct Recovery = 72% Analysis Date = 06/23/22 Pct Recovery = 72% Analysis Date = 06/23/22 Pct Recovery = 72% Analysis Date = 06/19/22 Pct Recovery = 72% Analysis Date = 06/19/22 Pct Recovery = 72% Analysis Date = 06/15/22 Pct Recovery = 72% Analysis Date = 06/15/22 Pct Recovery = 72% Analysis Date = 06/11/22 Pct Recovery = 72% Analysis Date = 06/11/22 Pct Recovery = 72% Analysis Date = 06/07/22 Pct Recovery = 72% Analysis Date = 06/07/22 Pct Recovery = 72% Analysis Date = 06/03/22 Pct Recovery = 72% Analysis Date = 06/03/22 Pct Recovery = 72% Analysis Date = 05/30/22 Pct Recovery = 73% Analysis Date = 05/30/22 Pct Recovery = 73% Analysis Date = 05/26/22 Pct Recovery = 73% Analysis Date = 05/26/22 Pct Recovery = 73% Analysis Date = 05/22/22 Pct Recovery = 73% Analysis Date = 05/22/22 Pct Recovery = 73% Analysis Date = 05/18/22 Pct Recovery = 73% Analysis Date = 05/18/22 Pct Recovery = 73% Analysis Date = 05/14/22 Pct Recovery = 73% Analysis Date = 05/14/22 Pct Recovery = 73% Analysis Date = 05/10/22 Pct Recovery = 73% Analysis Date = 05/10/22 Pct Recovery = 73% Analysis Date = 05/06/22 Pct Recovery = 73% Analysis Date = 05/06/22 Pct Recovery = 73% Analysis Date = 05/01/22 Pct Recovery = 74% Analysis Date = 05/01/22 Pct Recovery = 74% Analysis Date = 04/27/22 Pct Recovery = 74% Analysis Date = 04/27/22 Pct Recovery = 74% Analysis Date = 04/23/22 Pct Recovery = 74% Analysis Date = 04/23/22 Pct Recovery = 74% Analysis Date = 04/19/22 Pct Recovery = 74% Analysis Date = 04/19/22 Pct Recovery = 74% Analysis Date = 04/15/22 Pct Recovery = 74% Analysis Date = 04/15/22 Pct Recovery = 74% Analysis Date = 04/11/22 Pct Recovery = 74% Analysis Date = 04/11/22 Pct Recovery = 74% Analysis Date = 04/07/22 Pct Recovery = 75% Analysis Date = 04/07/22 Pct Recovery = 75% Analysis Date = 04/03/22 Pct Recovery = 75% Analysis Date = 04/03/22 Pct Recovery = 75% Analysis Date = 03/30/22 Pct Recovery = 75% Analysis Date = 03/30/22 Pct Recovery = 75% Analysis Date = 03/26/22 Pct Recovery = 75% Analysis Date = 03/26/22 Pct Recovery = 75% Analysis Date = 03/22/22 Pct Recovery = 75% Analysis Date = 03/22/22 Pct Recovery = 75% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/18/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/14/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/10/22 Pct Recovery = 76% Analysis Date = 03/06/22 Pct Recovery = 76% Analysis Date = 03/06/22 Pct Recovery = 76% Analysis Date = 03/02/22 Pct Recovery = 77% Analysis Date = 03/02/22 Pct Recovery = 77% Analysis Date = 02/26/22 Pct Recovery = 77% Analysis Date = 02/26/22 Pct Recovery = 77% Analysis Date = 02/22/22 Pct Recovery = 77% Analysis Date = 02/22/22 Pct Recovery = 77% Analysis Date = 02/18/22 Pct Recovery = 77% Analysis Date = 02/18/22 Pct Recovery = 77% Analysis Date = 02/14/22 Pct Recovery = 78% Analysis Date = 02/14/22 Pct Recovery = 78% Analysis Date = 02/10/22 Pct Recovery = 78% Analysis Date = 02/10/22 Pct Recovery = 78% Analysis Date = 02/06/22 Pct Recovery = 78% Analysis Date = 02/06/22 Pct Recovery = 78% Analysis Date = 02/02/22 Pct Recovery = 78% Analysis Date = 02/02/22 Pct Recovery = 78% Analysis Date = 01/29/22 Pct Recovery = 79% Analysis Date = 01/29/22 Pct Recovery = 79% Analysis Date = 01/25/22 Pct Recovery = 79% Analysis Date = 01/25/22 Pct Recovery = 79% Analysis Date = 01/20/22 Pct Recovery = 79% Analysis Date = 01/20/22 Pct Recovery = 79% Analysis Date = 01/16/22 Pct Recovery = 80% Analysis Date = 01/16/22 Pct Recovery = 80% Analysis Date = 01/12/22 Pct Recovery = 80% Analysis Date = 01/12/22 Pct Recovery = 80% Analysis Date = 01/08/22 Pct Recovery = 80% Analysis Date = 01/08/22 Pct Recovery = 80% Analysis Date = 01/04/22 Pct Recovery = 80% Analysis Date = 01/04/22 Pct Recovery = 80% Analysis Date = 12/31/21 Pct Recovery = 81% Analysis Date = 12/31/21 Pct Recovery = 81% Analysis Date = 12/27/21 Pct Recovery = 81% Analysis Date = 12/27/21 Pct Recovery = 81% Analysis Date = 12/23/21 Pct Recovery = 81% Analysis Date = 12/23/21 Pct Recovery = 81% Analysis Date = 12/19/21 Pct Recovery = 81% Analysis Date = 12/19/21 Pct Recovery = 81% Analysis Date = 12/15/21 Pct Recovery = 82% Analysis Date = 12/15/21 Pct Recovery = 82% Analysis Date = 12/11/21 Pct Recovery = 82% Analysis Date = 12/11/21 Pct Recovery = 82% Analysis Date = 12/07/21 Pct Recovery = 82% Analysis Date = 12/07/21 Pct Recovery = 82% Analysis Date = 12/03/21 Pct Recovery = 83% Analysis Date = 12/03/21 Pct Recovery = 83% Analysis Date = 11/29/21 Pct Recovery = 83% Analysis Date = 11/29/21 Pct Recovery = 83% Analysis Date = 11/25/21 Pct Recovery = 83% Analysis Date = 11/25/21 Pct Recovery = 83% Analysis Date = 11/21/21 Pct Recovery = 83% Analysis Date = 11/21/21 Pct Recovery = 83% Analysis Date = 11/17/21 Pct Recovery = 84% Analysis Date = 11/17/21 Pct Recovery = 84% Analysis Date = 11/13/21 Pct Recovery = 84% Analysis Date = 11/13/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/09/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/05/21 Pct Recovery = 84% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 11/01/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/28/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/24/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/20/21 Pct Recovery = 85% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/16/21 Pct Recovery = 86% Analysis Date = 10/11/21 Pct Recovery = 86% Analysis Date = 10/11/21 Pct Recovery = 86% Analysis Date = 10/07/21 Pct Recovery = 86% Analysis Date = 10/07/21 Pct Recovery = 86% Analysis Date = 10/03/21 Pct Recovery = 87% Analysis Date = 10/03/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/29/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/25/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/21/21 Pct Recovery = 87% Analysis Date = 09/17/21 Pct Recovery = 88% Analysis Date = 09/17/21 Pct Recovery = 88% Analysis Date = 09/13/21 Pct Recovery = 88% Analysis Date = 09/13/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/09/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 88% Analysis Date = 09/05/21 Pct Recovery = 88% Analysis Date = 09/01/21 Pct Recovery = 89% Analysis Date = 09/01/21 Pct Recovery = 89% Analysis Date = 08/28/21 Pct Recovery = 89% Analysis Date = 08/28/21 Pct Recovery = 89% Analysis Date = 08/24/21 Pct Recovery = 89% Analysis Date = 08/24/21 Pct Recovery = 89% Analysis Date = 08/20/21 Pct Recovery = 90% Analysis Date = 08/20/21 Pct Recovery = 90% Analysis Date = 08/16/21 Pct Recovery = 90% Analysis Date = 08/16/21 Pct Recovery = 90% Analysis Date = 08/12/21 Pct Recovery = 90% Analysis Date = 08/12/21 Pct Recovery = 90% Analysis Date = 08/08/21 Pct Recovery = 90% Analysis Date = 08/08/21 Pct Recovery = 90% Analysis Date = 08/04/21 Pct Recovery = 91% Analysis Date = 08/04/21 Pct Recovery = 91% Analysis Date = 07/31/21 Pct Recovery = 91% Analysis Date = 07/31/21 Pct Recovery = 91% Analysis Date = 07/27/21 Pct Recovery = 91% Analysis Date = 07/27/21 Pct Recovery = 91% Analysis Date = 07/23/21 Pct Recovery = 91% Analysis Date = 07/23/21 Pct Recovery = 91% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 07/02/21 Pct Recovery = 93% Analysis Date = 06/28/21 Pct Recovery = 93% Analysis Date = 06/28/21 Pct Recovery = 93% Analysis Date = 06/24/21 Pct Recovery = 93% Analysis Date = 06/24/21 Pct Recovery = 93% Analysis Date = 06/20/21 Pct Recovery = 94% Analysis Date = 06/20/21 Pct Recovery = 94% Analysis Date = 06/16/21 Pct Recovery = 94% Analysis Date = 06/16/21 Pct Recovery = 94% Analysis Date = 06/12/21 Pct Recovery = 94% Analysis Date = 06/12/21 Pct Recovery = 94% Analysis Date = 06/08/21 Pct Recovery = 94% Analysis Date = 06/08/21 Pct Recovery = 94% Analysis Date = 06/04/21 Pct Recovery = 95% Analysis Date = 06/04/21 Pct Recovery = 95% Analysis Date = 05/31/21 Pct Recovery = 95% Analysis Date = 05/31/21 Pct Recovery = 95% Analysis Date = 05/27/21 Pct Recovery = 95% Analysis Date = 05/27/21 Pct Recovery = 95% Analysis Date = 05/23/21 Pct Recovery = 95% Analysis Date = 05/23/21 Pct Recovery = 95% Analysis Date = 05/19/21 Pct Recovery = 96% Analysis Date = 05/19/21 Pct Recovery = 96% Analysis Date = 05/15/21 Pct Recovery = 96% Analysis Date = 05/15/21 Pct Recovery = 96% Analysis Date = 05/11/21 Pct Recovery = 96% Analysis Date = 05/11/21 Pct Recovery = 96% Analysis Date = 05/07/21 Pct Recovery = 97% Analysis Date = 05/07/21 Pct Recovery = 97% Analysis Date = 05/03/21 Pct Recovery = 97% Analysis Date = 05/03/21 Pct Recovery = 97% Analysis Date = 04/29/21 Pct Recovery = 97% Analysis Date = 04/29/21 Pct Recovery = 97% Analysis Date = 04/25/21 Pct Recovery = 97% Analysis Date = 04/25/21 Pct Recovery = 97% Analysis Date = 04/21/21 Pct Recovery = 98% Analysis Date = 04/21/21 Pct Recovery = 98% Analysis Date = 04/17/21 Pct Recovery = 98% Analysis Date = 04/17/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 98% Analysis Date = 04/09/21 Pct Recovery = 98% Analysis Date = 04/09/21 Pct Recovery = 98% Analysis Date = 04/05/21 Pct Recovery = 99% Analysis Date = 04/05/21 Pct Recovery = 99% Analysis Date = 04/01/21 Pct Recovery = 99% Analysis Date = 04/01/21 Pct Recovery = 99% Analysis Date = 03/28/21 Pct Recovery = 99% Analysis Date = 03/28/21 Pct Recovery = 99% Analysis Date = 03/23/21 Pct Recovery = 99% Analysis Date = 03/23/21 Pct Recovery = 99% Analysis Date = 03/19/21 Pct Recovery = 98% Analysis Date = 03/19/21 Pct Recovery = 98% Analysis Date = 03/15/21 Pct Recovery = 98% Analysis Date = 03/15/21 Pct Recovery = 98% Analysis Date = 03/11/21 Pct Recovery = 98% Analysis Date = 03/11/21 Pct Recovery = 98% Analysis Date = 03/07/21 Pct Recovery = 98% Analysis Date = 03/07/21 Pct Recovery = 98% Analysis Date = 03/03/21 Pct Recovery = 98% Analysis Date = 03/03/21 Pct Recovery = 98% Analysis Date = 02/27/21 Pct Recovery = 97% Analysis Date = 02/27/21 Pct Recovery = 97% Analysis Date = 02/23/21 Pct Recovery = 97% Analysis Date = 02/23/21 Pct Recovery = 97% Analysis Date = 02/19/21 Pct Recovery = 97% Analysis Date = 02/19/21 Pct Recovery = 97% Analysis Date = 02/15/21 Pct Recovery = 97% Analysis Date = 02/15/21 Pct Recovery = 97% Analysis Date = 02/11/21 Pct Recovery = 97% Analysis Date = 02/11/21 Pct Recovery = 97% Analysis Date = 02/07/21 Pct Recovery = 96% Analysis Date = 02/07/21 Pct Recovery = 96% Analysis Date = 02/03/21 Pct Recovery = 96% Analysis Date = 02/03/21 Pct Recovery = 96% Analysis Date = 01/30/21 Pct Recovery = 96% Analysis Date = 01/30/21 Pct Recovery = 96% Analysis Date = 01/26/21 Pct Recovery = 96% Analysis Date = 01/26/21 Pct Recovery = 96% Analysis Date = 01/22/21 Pct Recovery = 96% Analysis Date = 01/22/21 Pct Recovery = 96% Analysis Date = 01/18/21 Pct Recovery = 96% Analysis Date = 01/18/21 Pct Recovery = 96% Analysis Date = 01/14/21 Pct Recovery = 95% Analysis Date = 01/14/21 Pct Recovery = 95% Analysis Date = 01/10/21 Pct Recovery = 95% Analysis Date = 01/10/21 Pct Recovery = 95% Analysis Date = 01/06/21 Pct Recovery = 95% Analysis Date = 01/06/21 Pct Recovery = 95% Analysis Date = 01/02/21 Pct Recovery = 95% Analysis Date = 01/02/21 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/29/20 Pct Recovery = 95% Analysis Date = 12/25/20 Pct Recovery = 95% Analysis Date = 12/25/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/21/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/17/20 Pct Recovery = 95% Analysis Date = 12/12/20 Pct Recovery = 95% Analysis Date = 12/12/20 Pct Recovery = 95% Analysis Date = 12/08/20 Pct Recovery = 95% Analysis Date = 12/08/20 Pct Recovery = 95% Analysis Date = 12/04/20 Pct Recovery = 95% Analysis Date = 12/04/20 Pct Recovery = 95% Analysis Date = 11/30/20 Pct Recovery = 95% Analysis Date = 11/30/20 Pct Recovery = 95% Analysis Date = 11/26/20 Pct Recovery = 95% Analysis Date = 11/26/20 Pct Recovery = 95% Analysis Date = 11/22/20 Pct Recovery = 95% Analysis Date = 11/22/20 Pct Recovery = 95% Analysis Date = 11/18/20 Pct Recovery = 95% Analysis Date = 11/18/20 Pct Recovery = 95% Analysis Date = 11/14/20 Pct Recovery = 95% Analysis Date = 11/14/20 Pct Recovery = 95% Analysis Date = 11/10/20 Pct Recovery = 94% Analysis Date = 11/10/20 Pct Recovery = 94% Analysis Date = 11/06/20 Pct Recovery = 94% Analysis Date = 11/06/20 Pct Recovery = 94% Analysis Date = 11/02/20 Pct Recovery = 94% Analysis Date = 11/02/20 Pct Recovery = 94% Analysis Date = 10/29/20 Pct Recovery = 94% Analysis Date = 10/29/20 Pct Recovery = 94% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/25/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 95% Analysis Date = 10/21/20 Pct Recovery = 95% Analysis Date = 10/17/20 Pct Recovery = 95% Analysis Date = 10/17/20 Pct Recovery = 95% Analysis Date = 10/13/20 Pct Recovery = 95% Analysis Date = 10/13/20 Pct Recovery = 95% Analysis Date = 10/09/20 Pct Recovery = 95% Analysis Date = 10/09/20 Pct Recovery = 95% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/05/20 Pct Recovery = 96% Analysis Date = 10/01/20 Pct Recovery = 96% Analysis Date = 10/01/20 Pct Recovery = 96% Analysis Date = 09/27/20 Pct Recovery = 96% Analysis Date = 09/27/20 Pct Recovery = 96% Analysis Date = 09/23/20 Pct Recovery = 96% Analysis Date = 09/23/20 Pct Recovery = 96% Analysis Date = 09/19/20 Pct Recovery = 97% Analysis Date = 09/19/20 Pct Recovery = 97% Analysis Date = 09/15/20 Pct Recovery = 97% Analysis Date = 09/15/20 Pct Recovery = 97% Analysis Date = 09/11/20 Pct Recovery = 97% Analysis Date = 09/11/20 Pct Recovery = 97% Analysis Date = 09/07/20 Pct Recovery = 97% Analysis Date = 09/07/20 Pct Recovery = 97% Analysis Date = 09/02/20 Pct Recovery = 98% Analysis Date = 09/02/20 Pct Recovery = 98% Analysis Date = 08/29/20 Pct Recovery = 98% Analysis Date = 08/29/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/25/20 Pct Recovery = 98% Analysis Date = 08/21/20 Pct Recovery = 99% Analysis Date = 08/21/20 Pct Recovery = 99% Analysis Date = 08/17/20 Pct Recovery = 99% Analysis Date = 08/17/20 Pct Recovery = 99% Analysis Date = 08/13/20 Pct Recovery = 99% Analysis Date = 08/13/20 Pct Recovery = 99% Analysis Date = 08/09/20 Pct Recovery = 99% Analysis Date = 08/09/20 Pct Recovery = 99% Analysis Date = 08/05/20 Pct Recovery = 100% Analysis Date = 08/05/20 Pct Recovery = 100% Analysis Date = 08/01/20 Pct Recovery = 100% Analysis Date = 08/01/20 Pct Recovery = 100% Analysis Date = 07/28/20 Pct Recovery = 100% Analysis Date = 07/28/20 Pct Recovery = 100% Analysis Date = 07/24/20 Pct Recovery = 101% Analysis Date = 07/24/20 Pct Recovery = 101% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/20/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/16/20 Pct Recovery = 101% Analysis Date = 07/12/20 Pct Recovery = 102% Analysis Date = 07/12/20 Pct Recovery = 102% Analysis Date = 07/08/20 Pct Recovery = 102% Analysis Date = 07/08/20 Pct Recovery = 102% Analysis Date = 07/04/20 Pct Recovery = 102% Analysis Date = 07/04/20 Pct Recovery = 102% Analysis Date = 06/30/20 Pct Recovery = 103% Analysis Date = 06/30/20 Pct Recovery = 103% Analysis Date = 06/26/20 Pct Recovery = 103% Analysis Date = 06/26/20 Pct Recovery = 103% Analysis Date = 06/22/20 Pct Recovery = 103% Analysis Date = 06/22/20 Pct Recovery = 103% Analysis Date = 06/18/20 Pct Recovery = 104% Analysis Date = 06/18/20 Pct Recovery = 104% Analysis Date = 06/14/20 Pct Recovery = 104% Analysis Date = 06/14/20 Pct Recovery = 104% Analysis Date = 06/10/20 Pct Recovery = 104% Analysis Date = 06/10/20 Pct Recovery = 104% Analysis Date = 06/06/20 Pct Recovery = 105% Analysis Date = 06/06/20 Pct Recovery = 105% Analysis Date = 06/02/20 Pct Recovery = 105% Analysis Date = 06/02/20 Pct Recovery = 105% Analysis Date = 05/29/20 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TETRACONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 31 92% 20% 93% 17%
Total 31 92% 20% 93% 17%

Sample Statistics
TETRACONAZOLE

Characteristic N % % Basis
Plotted 31 100% Spiked
Estimated Values 4 13% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 31 .  
False Negatives 0 0% 0 out of 31
Not Spiked 85 .  
False Positives 0 0% 0 out of 85

OBSP Determination:
THIOBENCARB
METHOD: 2447 , TESTIDCODE: 65107LCM60

Laboratory ID = 20213200091 Lab Value = 55.022 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 208% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20202590106 Lab Value = 51.757 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 99% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 50.111 Expected Conc. = 52.1 Report level label = 4.2 Pct Recovery = 96% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222150193 Lab Value = 30.052 Expected Conc. = 42.4 Report level label = 4.2 Pct Recovery = 71% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20212990174 Lab Value = 30.354 Expected Conc. = 42.4 Report level label = 4.2 Pct Recovery = 72% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20220190116 Lab Value = 24.949 Expected Conc. = 42.08 Report level label = 4.2 Pct Recovery = 59% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 26.971 Expected Conc. = 42.08 Report level label = 4.2 Pct Recovery = 64% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20203230021 Lab Value = 42.326 Expected Conc. = 42.08 Report level label = 4.2 Pct Recovery = 101% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 38.408 Expected Conc. = 42.08 Report level label = 4.2 Pct Recovery = 91% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222010132 Lab Value = 25.337 Expected Conc. = 42 Report level label = 4.2 Pct Recovery = 60% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 33.861 Expected Conc. = 41.6 Report level label = 4.2 Pct Recovery = 81% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20201550031 Lab Value = 28.189 Expected Conc. = 26.65 Report level label = 4.2 Pct Recovery = 106% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 9042800 Laboratory ID = 20213340027 Lab Value = 17.285 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 65% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 18.404 Expected Conc. = 26.5 Report level label = 4.2 Pct Recovery = 69% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20221730293 Lab Value = 18.527 Expected Conc. = 26.3 Report level label = 4.2 Pct Recovery = 70% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 15.727 Expected Conc. = 26.3 Report level label = 4.2 Pct Recovery = 60% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20203230018 Lab Value = 27.271 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 105% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 23.230 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 89% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 27.104 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 104% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 34.135 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 131% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20202110006 Lab Value = 29.706 Expected Conc. = 26.05 Report level label = 4.2 Pct Recovery = 114% Analysis Date = 08/06/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090519Pest3: 100 µl SpecificMix = 082719Pest3 Laboratory ID = 20220810133 Lab Value = 25.339 Expected Conc. = 26 Report level label = 4.2 Pct Recovery = 97% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20201960104 Lab Value = 25.101 Expected Conc. = 20.84 Report level label = 4.2 Pct Recovery = 120% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20201680155 Lab Value = 19.441 Expected Conc. = 20.84 Report level label = 4.2 Pct Recovery = 93% Analysis Date = 06/25/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090519Pest3: 50 µl SpecificMix = 082719Pest3 Laboratory ID = 20202330309 Lab Value = 8.318 Expected Conc. = 10.66 Report level label = 4.2 Pct Recovery = 78% Analysis Date = 09/02/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20202180001 Lab Value = 7.832 Expected Conc. = 10.66 Report level label = 4.2 Pct Recovery = 73% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201890192 Lab Value = 10.849 Expected Conc. = 10.66 Report level label = 4.2 Pct Recovery = 102% Analysis Date = 07/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20201750122 Lab Value = 8.532 Expected Conc. = 10.66 Report level label = 4.2 Pct Recovery = 80% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 9042800 Laboratory ID = 20201470020 Lab Value = 11.029 Expected Conc. = 10.66 Report level label = 4.2 Pct Recovery = 103% Analysis Date = 05/29/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 9089700: 20 µl SpecificMix = 9042800 Laboratory ID = 20213060210 Lab Value = 6.304 Expected Conc. = 10.6 Report level label = 4.2 Pct Recovery = 59% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20222500483 Lab Value = 7.285 Expected Conc. = 10.52 Report level label = 4.2 Pct Recovery = 69% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 7.282 Expected Conc. = 10.52 Report level label = 4.2 Pct Recovery = 69% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20210970035 Lab Value = 10.822 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 104% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 10.063 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 97% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 9.437 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 91% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 10.636 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 102% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 10.566 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 101% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 9.667 Expected Conc. = 10.42 Report level label = 4.2 Pct Recovery = 93% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20222630205 Lab Value = 8.797 Expected Conc. = 10.4 Report level label = 4.2 Pct Recovery = 85% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20210830019 Lab Value = 8.236 Expected Conc. = 8.416 Report level label = 4.2 Pct Recovery = 98% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 8.858 Expected Conc. = 8.416 Report level label = 4.2 Pct Recovery = 105% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Analysis Date = 09/28/22 Pct Recovery = 70% Analysis Date = 09/24/22 Pct Recovery = 70% Analysis Date = 09/24/22 Pct Recovery = 70% Analysis Date = 09/20/22 Pct Recovery = 70% Analysis Date = 09/20/22 Pct Recovery = 70% Analysis Date = 09/16/22 Pct Recovery = 70% Analysis Date = 09/16/22 Pct Recovery = 70% Analysis Date = 09/11/22 Pct Recovery = 70% Analysis Date = 09/11/22 Pct Recovery = 70% Analysis Date = 09/07/22 Pct Recovery = 71% Analysis Date = 09/07/22 Pct Recovery = 71% Analysis Date = 09/03/22 Pct Recovery = 71% Analysis Date = 09/03/22 Pct Recovery = 71% Analysis Date = 08/30/22 Pct Recovery = 71% Analysis Date = 08/30/22 Pct Recovery = 71% Analysis Date = 08/25/22 Pct Recovery = 71% Analysis Date = 08/25/22 Pct Recovery = 71% Analysis Date = 08/21/22 Pct Recovery = 71% Analysis Date = 08/21/22 Pct Recovery = 71% Analysis Date = 08/17/22 Pct Recovery = 71% Analysis Date = 08/17/22 Pct Recovery = 71% Analysis Date = 08/13/22 Pct Recovery = 72% Analysis Date = 08/13/22 Pct Recovery = 72% Analysis Date = 08/08/22 Pct Recovery = 72% Analysis Date = 08/08/22 Pct Recovery = 72% Analysis Date = 08/04/22 Pct Recovery = 72% Analysis Date = 08/04/22 Pct Recovery = 72% Analysis Date = 07/31/22 Pct Recovery = 72% Analysis Date = 07/31/22 Pct Recovery = 72% Analysis Date = 07/27/22 Pct Recovery = 72% Analysis Date = 07/27/22 Pct Recovery = 72% Analysis Date = 07/22/22 Pct Recovery = 73% Analysis Date = 07/22/22 Pct Recovery = 73% Analysis Date = 07/18/22 Pct Recovery = 73% Analysis Date = 07/18/22 Pct Recovery = 73% Analysis Date = 07/14/22 Pct Recovery = 73% Analysis Date = 07/14/22 Pct Recovery = 73% Analysis Date = 07/09/22 Pct Recovery = 73% Analysis Date = 07/09/22 Pct Recovery = 73% Analysis Date = 07/05/22 Pct Recovery = 73% Analysis Date = 07/05/22 Pct Recovery = 73% Analysis Date = 07/01/22 Pct Recovery = 74% Analysis Date = 07/01/22 Pct Recovery = 74% Analysis Date = 06/27/22 Pct Recovery = 74% Analysis Date = 06/27/22 Pct Recovery = 74% Analysis Date = 06/22/22 Pct Recovery = 74% Analysis Date = 06/22/22 Pct Recovery = 74% Analysis Date = 06/18/22 Pct Recovery = 74% Analysis Date = 06/18/22 Pct Recovery = 74% Analysis Date = 06/14/22 Pct Recovery = 74% Analysis Date = 06/14/22 Pct Recovery = 74% Analysis Date = 06/10/22 Pct Recovery = 75% Analysis Date = 06/10/22 Pct Recovery = 75% Analysis Date = 06/05/22 Pct Recovery = 75% Analysis Date = 06/05/22 Pct Recovery = 75% Analysis Date = 06/01/22 Pct Recovery = 75% Analysis Date = 06/01/22 Pct Recovery = 75% Analysis Date = 05/28/22 Pct Recovery = 75% Analysis Date = 05/28/22 Pct Recovery = 75% Analysis Date = 05/24/22 Pct Recovery = 75% Analysis Date = 05/24/22 Pct Recovery = 75% Analysis Date = 05/19/22 Pct Recovery = 76% Analysis Date = 05/19/22 Pct Recovery = 76% Analysis Date = 05/15/22 Pct Recovery = 76% Analysis Date = 05/15/22 Pct Recovery = 76% Analysis Date = 05/11/22 Pct Recovery = 76% Analysis Date = 05/11/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/06/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 05/02/22 Pct Recovery = 76% Analysis Date = 04/28/22 Pct Recovery = 76% Analysis Date = 04/28/22 Pct Recovery = 76% Analysis Date = 04/24/22 Pct Recovery = 77% Analysis Date = 04/24/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/19/22 Pct Recovery = 77% Analysis Date = 04/15/22 Pct Recovery = 77% Analysis Date = 04/15/22 Pct Recovery = 77% Analysis Date = 04/11/22 Pct Recovery = 77% Analysis Date = 04/11/22 Pct Recovery = 77% Analysis Date = 04/07/22 Pct Recovery = 77% Analysis Date = 04/07/22 Pct Recovery = 77% Analysis Date = 04/02/22 Pct Recovery = 78% Analysis Date = 04/02/22 Pct Recovery = 78% Analysis Date = 03/29/22 Pct Recovery = 78% Analysis Date = 03/29/22 Pct Recovery = 78% Analysis Date = 03/25/22 Pct Recovery = 78% Analysis Date = 03/25/22 Pct Recovery = 78% Analysis Date = 03/21/22 Pct Recovery = 78% Analysis Date = 03/21/22 Pct Recovery = 78% Analysis Date = 03/16/22 Pct Recovery = 78% Analysis Date = 03/16/22 Pct Recovery = 78% Analysis Date = 03/12/22 Pct Recovery = 79% Analysis Date = 03/12/22 Pct Recovery = 79% Analysis Date = 03/08/22 Pct Recovery = 79% Analysis Date = 03/08/22 Pct Recovery = 79% Analysis Date = 03/04/22 Pct Recovery = 79% Analysis Date = 03/04/22 Pct Recovery = 79% Analysis Date = 02/27/22 Pct Recovery = 79% Analysis Date = 02/27/22 Pct Recovery = 79% Analysis Date = 02/23/22 Pct Recovery = 80% Analysis Date = 02/23/22 Pct Recovery = 80% Analysis Date = 02/19/22 Pct Recovery = 80% Analysis Date = 02/19/22 Pct Recovery = 80% Analysis Date = 02/14/22 Pct Recovery = 80% Analysis Date = 02/14/22 Pct Recovery = 80% Analysis Date = 02/10/22 Pct Recovery = 80% Analysis Date = 02/10/22 Pct Recovery = 80% Analysis Date = 02/06/22 Pct Recovery = 80% Analysis Date = 02/06/22 Pct Recovery = 80% Analysis Date = 02/02/22 Pct Recovery = 81% Analysis Date = 02/02/22 Pct Recovery = 81% Analysis Date = 01/28/22 Pct Recovery = 81% Analysis Date = 01/28/22 Pct Recovery = 81% Analysis Date = 01/24/22 Pct Recovery = 81% Analysis Date = 01/24/22 Pct Recovery = 81% Analysis Date = 01/20/22 Pct Recovery = 81% Analysis Date = 01/20/22 Pct Recovery = 81% Analysis Date = 01/16/22 Pct Recovery = 82% Analysis Date = 01/16/22 Pct Recovery = 82% Analysis Date = 01/11/22 Pct Recovery = 82% Analysis Date = 01/11/22 Pct Recovery = 82% Analysis Date = 01/07/22 Pct Recovery = 82% Analysis Date = 01/07/22 Pct Recovery = 82% Analysis Date = 01/03/22 Pct Recovery = 82% Analysis Date = 01/03/22 Pct Recovery = 82% Analysis Date = 12/30/21 Pct Recovery = 82% Analysis Date = 12/30/21 Pct Recovery = 82% Analysis Date = 12/25/21 Pct Recovery = 83% Analysis Date = 12/25/21 Pct Recovery = 83% Analysis Date = 12/21/21 Pct Recovery = 83% Analysis Date = 12/21/21 Pct Recovery = 83% Analysis Date = 12/17/21 Pct Recovery = 83% Analysis Date = 12/17/21 Pct Recovery = 83% Analysis Date = 12/12/21 Pct Recovery = 83% Analysis Date = 12/12/21 Pct Recovery = 83% Analysis Date = 12/08/21 Pct Recovery = 84% Analysis Date = 12/08/21 Pct Recovery = 84% Analysis Date = 12/04/21 Pct Recovery = 84% Analysis Date = 12/04/21 Pct Recovery = 84% Analysis Date = 11/30/21 Pct Recovery = 84% Analysis Date = 11/30/21 Pct Recovery = 84% Analysis Date = 11/25/21 Pct Recovery = 84% Analysis Date = 11/25/21 Pct Recovery = 84% Analysis Date = 11/21/21 Pct Recovery = 85% Analysis Date = 11/21/21 Pct Recovery = 85% Analysis Date = 11/17/21 Pct Recovery = 85% Analysis Date = 11/17/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/13/21 Pct Recovery = 85% Analysis Date = 11/08/21 Pct Recovery = 86% Analysis Date = 11/08/21 Pct Recovery = 86% Analysis Date = 11/04/21 Pct Recovery = 86% Analysis Date = 11/04/21 Pct Recovery = 86% Analysis Date = 10/31/21 Pct Recovery = 86% Analysis Date = 10/31/21 Pct Recovery = 86% Analysis Date = 10/27/21 Pct Recovery = 86% Analysis Date = 10/27/21 Pct Recovery = 86% Analysis Date = 10/22/21 Pct Recovery = 87% Analysis Date = 10/22/21 Pct Recovery = 87% Analysis Date = 10/18/21 Pct Recovery = 87% Analysis Date = 10/18/21 Pct Recovery = 87% Analysis Date = 10/14/21 Pct Recovery = 87% Analysis Date = 10/14/21 Pct Recovery = 87% Analysis Date = 10/10/21 Pct Recovery = 87% Analysis Date = 10/10/21 Pct Recovery = 87% Analysis Date = 10/05/21 Pct Recovery = 88% Analysis Date = 10/05/21 Pct Recovery = 88% Analysis Date = 10/01/21 Pct Recovery = 88% Analysis Date = 10/01/21 Pct Recovery = 88% Analysis Date = 09/27/21 Pct Recovery = 88% Analysis Date = 09/27/21 Pct Recovery = 88% Analysis Date = 09/22/21 Pct Recovery = 88% Analysis Date = 09/22/21 Pct Recovery = 88% Analysis Date = 09/18/21 Pct Recovery = 89% Analysis Date = 09/18/21 Pct Recovery = 89% Analysis Date = 09/14/21 Pct Recovery = 89% Analysis Date = 09/14/21 Pct Recovery = 89% Analysis Date = 09/10/21 Pct Recovery = 89% Analysis Date = 09/10/21 Pct Recovery = 89% Analysis Date = 09/05/21 Pct Recovery = 89% Analysis Date = 09/05/21 Pct Recovery = 89% Analysis Date = 09/01/21 Pct Recovery = 90% Analysis Date = 09/01/21 Pct Recovery = 90% Analysis Date = 08/28/21 Pct Recovery = 90% Analysis Date = 08/28/21 Pct Recovery = 90% Analysis Date = 08/24/21 Pct Recovery = 90% Analysis Date = 08/24/21 Pct Recovery = 90% Analysis Date = 08/19/21 Pct Recovery = 90% Analysis Date = 08/19/21 Pct Recovery = 90% Analysis Date = 08/15/21 Pct Recovery = 91% Analysis Date = 08/15/21 Pct Recovery = 91% Analysis Date = 08/11/21 Pct Recovery = 91% Analysis Date = 08/11/21 Pct Recovery = 91% Analysis Date = 08/07/21 Pct Recovery = 91% Analysis Date = 08/07/21 Pct Recovery = 91% Analysis Date = 08/02/21 Pct Recovery = 91% Analysis Date = 08/02/21 Pct Recovery = 91% Analysis Date = 07/29/21 Pct Recovery = 92% Analysis Date = 07/29/21 Pct Recovery = 92% Analysis Date = 07/25/21 Pct Recovery = 92% Analysis Date = 07/25/21 Pct Recovery = 92% Analysis Date = 07/20/21 Pct Recovery = 92% Analysis Date = 07/20/21 Pct Recovery = 92% Analysis Date = 07/16/21 Pct Recovery = 92% Analysis Date = 07/16/21 Pct Recovery = 92% Analysis Date = 07/12/21 Pct Recovery = 93% Analysis Date = 07/12/21 Pct Recovery = 93% Analysis Date = 07/08/21 Pct Recovery = 93% Analysis Date = 07/08/21 Pct Recovery = 93% Analysis Date = 07/03/21 Pct Recovery = 93% Analysis Date = 07/03/21 Pct Recovery = 93% Analysis Date = 06/29/21 Pct Recovery = 93% Analysis Date = 06/29/21 Pct Recovery = 93% Analysis Date = 06/25/21 Pct Recovery = 94% Analysis Date = 06/25/21 Pct Recovery = 94% Analysis Date = 06/21/21 Pct Recovery = 94% Analysis Date = 06/21/21 Pct Recovery = 94% Analysis Date = 06/16/21 Pct Recovery = 94% Analysis Date = 06/16/21 Pct Recovery = 94% Analysis Date = 06/12/21 Pct Recovery = 94% Analysis Date = 06/12/21 Pct Recovery = 94% Analysis Date = 06/08/21 Pct Recovery = 95% Analysis Date = 06/08/21 Pct Recovery = 95% Analysis Date = 06/04/21 Pct Recovery = 95% Analysis Date = 06/04/21 Pct Recovery = 95% Analysis Date = 05/30/21 Pct Recovery = 95% Analysis Date = 05/30/21 Pct Recovery = 95% Analysis Date = 05/26/21 Pct Recovery = 95% Analysis Date = 05/26/21 Pct Recovery = 95% Analysis Date = 05/22/21 Pct Recovery = 96% Analysis Date = 05/22/21 Pct Recovery = 96% Analysis Date = 05/17/21 Pct Recovery = 96% Analysis Date = 05/17/21 Pct Recovery = 96% Analysis Date = 05/13/21 Pct Recovery = 96% Analysis Date = 05/13/21 Pct Recovery = 96% Analysis Date = 05/09/21 Pct Recovery = 96% Analysis Date = 05/09/21 Pct Recovery = 96% Analysis Date = 05/05/21 Pct Recovery = 97% Analysis Date = 05/05/21 Pct Recovery = 97% Analysis Date = 04/30/21 Pct Recovery = 97% Analysis Date = 04/30/21 Pct Recovery = 97% Analysis Date = 04/26/21 Pct Recovery = 97% Analysis Date = 04/26/21 Pct Recovery = 97% Analysis Date = 04/22/21 Pct Recovery = 97% Analysis Date = 04/22/21 Pct Recovery = 97% Analysis Date = 04/18/21 Pct Recovery = 98% Analysis Date = 04/18/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 98% Analysis Date = 04/13/21 Pct Recovery = 98% Analysis Date = 04/09/21 Pct Recovery = 98% Analysis Date = 04/09/21 Pct Recovery = 98% Analysis Date = 04/05/21 Pct Recovery = 98% Analysis Date = 04/05/21 Pct Recovery = 98% Analysis Date = 04/01/21 Pct Recovery = 99% Analysis Date = 04/01/21 Pct Recovery = 99% Analysis Date = 03/27/21 Pct Recovery = 99% Analysis Date = 03/27/21 Pct Recovery = 99% Analysis Date = 03/23/21 Pct Recovery = 99% Analysis Date = 03/23/21 Pct Recovery = 99% Analysis Date = 03/19/21 Pct Recovery = 99% Analysis Date = 03/19/21 Pct Recovery = 99% Analysis Date = 03/15/21 Pct Recovery = 99% Analysis Date = 03/15/21 Pct Recovery = 99% Analysis Date = 03/10/21 Pct Recovery = 99% Analysis Date = 03/10/21 Pct Recovery = 99% Analysis Date = 03/06/21 Pct Recovery = 99% Analysis Date = 03/06/21 Pct Recovery = 99% Analysis Date = 03/02/21 Pct Recovery = 99% Analysis Date = 03/02/21 Pct Recovery = 99% Analysis Date = 02/25/21 Pct Recovery = 99% Analysis Date = 02/25/21 Pct Recovery = 99% Analysis Date = 02/21/21 Pct Recovery = 99% Analysis Date = 02/21/21 Pct Recovery = 99% Analysis Date = 02/17/21 Pct Recovery = 99% Analysis Date = 02/17/21 Pct Recovery = 99% Analysis Date = 02/13/21 Pct Recovery = 99% Analysis Date = 02/13/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/08/21 Pct Recovery = 99% Analysis Date = 02/04/21 Pct Recovery = 99% Analysis Date = 02/04/21 Pct Recovery = 99% Analysis Date = 01/31/21 Pct Recovery = 99% Analysis Date = 01/31/21 Pct Recovery = 99% Analysis Date = 01/27/21 Pct Recovery = 99% Analysis Date = 01/27/21 Pct Recovery = 99% Analysis Date = 01/22/21 Pct Recovery = 99% Analysis Date = 01/22/21 Pct Recovery = 99% Analysis Date = 01/18/21 Pct Recovery = 99% Analysis Date = 01/18/21 Pct Recovery = 99% Analysis Date = 01/14/21 Pct Recovery = 99% Analysis Date = 01/14/21 Pct Recovery = 99% Analysis Date = 01/10/21 Pct Recovery = 99% Analysis Date = 01/10/21 Pct Recovery = 99% Analysis Date = 01/05/21 Pct Recovery = 99% Analysis Date = 01/05/21 Pct Recovery = 99% Analysis Date = 01/01/21 Pct Recovery = 99% Analysis Date = 01/01/21 Pct Recovery = 99% Analysis Date = 12/28/20 Pct Recovery = 99% Analysis Date = 12/28/20 Pct Recovery = 99% Analysis Date = 12/23/20 Pct Recovery = 99% Analysis Date = 12/23/20 Pct Recovery = 99% Analysis Date = 12/19/20 Pct Recovery = 99% Analysis Date = 12/19/20 Pct Recovery = 99% Analysis Date = 12/15/20 Pct Recovery = 99% Analysis Date = 12/15/20 Pct Recovery = 99% Analysis Date = 12/11/20 Pct Recovery = 99% Analysis Date = 12/11/20 Pct Recovery = 99% Analysis Date = 12/06/20 Pct Recovery = 99% Analysis Date = 12/06/20 Pct Recovery = 99% Analysis Date = 12/02/20 Pct Recovery = 98% Analysis Date = 12/02/20 Pct Recovery = 98% Analysis Date = 11/28/20 Pct Recovery = 98% Analysis Date = 11/28/20 Pct Recovery = 98% Analysis Date = 11/24/20 Pct Recovery = 98% Analysis Date = 11/24/20 Pct Recovery = 98% Analysis Date = 11/19/20 Pct Recovery = 98% Analysis Date = 11/19/20 Pct Recovery = 98% Analysis Date = 11/15/20 Pct Recovery = 98% Analysis Date = 11/15/20 Pct Recovery = 98% Analysis Date = 11/11/20 Pct Recovery = 98% Analysis Date = 11/11/20 Pct Recovery = 98% Analysis Date = 11/07/20 Pct Recovery = 98% Analysis Date = 11/07/20 Pct Recovery = 98% Analysis Date = 11/02/20 Pct Recovery = 98% Analysis Date = 11/02/20 Pct Recovery = 98% Analysis Date = 10/29/20 Pct Recovery = 98% Analysis Date = 10/29/20 Pct Recovery = 98% Analysis Date = 10/25/20 Pct Recovery = 99% Analysis Date = 10/25/20 Pct Recovery = 99% Analysis Date = 10/21/20 Pct Recovery = 99% Analysis Date = 10/21/20 Pct Recovery = 99% Analysis Date = 10/16/20 Pct Recovery = 99% Analysis Date = 10/16/20 Pct Recovery = 99% Analysis Date = 10/12/20 Pct Recovery = 99% Analysis Date = 10/12/20 Pct Recovery = 99% Analysis Date = 10/08/20 Pct Recovery = 99% Analysis Date = 10/08/20 Pct Recovery = 99% Analysis Date = 10/03/20 Pct Recovery = 99% Analysis Date = 10/03/20 Pct Recovery = 99% Analysis Date = 09/29/20 Pct Recovery = 99% Analysis Date = 09/29/20 Pct Recovery = 99% Analysis Date = 09/25/20 Pct Recovery = 99% Analysis Date = 09/25/20 Pct Recovery = 99% Analysis Date = 09/21/20 Pct Recovery = 99% Analysis Date = 09/21/20 Pct Recovery = 99% Analysis Date = 09/16/20 Pct Recovery = 99% Analysis Date = 09/16/20 Pct Recovery = 99% Analysis Date = 09/12/20 Pct Recovery = 99% Analysis Date = 09/12/20 Pct Recovery = 99% Analysis Date = 09/08/20 Pct Recovery = 99% Analysis Date = 09/08/20 Pct Recovery = 99% Analysis Date = 09/04/20 Pct Recovery = 99% Analysis Date = 09/04/20 Pct Recovery = 99% Analysis Date = 08/30/20 Pct Recovery = 99% Analysis Date = 08/30/20 Pct Recovery = 99% Analysis Date = 08/26/20 Pct Recovery = 99% Analysis Date = 08/26/20 Pct Recovery = 99% Analysis Date = 08/22/20 Pct Recovery = 99% Analysis Date = 08/22/20 Pct Recovery = 99% Analysis Date = 08/18/20 Pct Recovery = 99% Analysis Date = 08/18/20 Pct Recovery = 99% Analysis Date = 08/13/20 Pct Recovery = 99% Analysis Date = 08/13/20 Pct Recovery = 99% Analysis Date = 08/09/20 Pct Recovery = 99% Analysis Date = 08/09/20 Pct Recovery = 99% Analysis Date = 08/05/20 Pct Recovery = 100% Analysis Date = 08/05/20 Pct Recovery = 100% Analysis Date = 07/31/20 Pct Recovery = 100% Analysis Date = 07/31/20 Pct Recovery = 100% Analysis Date = 07/27/20 Pct Recovery = 100% Analysis Date = 07/27/20 Pct Recovery = 100% Analysis Date = 07/23/20 Pct Recovery = 100% Analysis Date = 07/23/20 Pct Recovery = 100% Analysis Date = 07/19/20 Pct Recovery = 100% Analysis Date = 07/19/20 Pct Recovery = 100% Analysis Date = 07/14/20 Pct Recovery = 100% Analysis Date = 07/14/20 Pct Recovery = 100% Analysis Date = 07/10/20 Pct Recovery = 100% Analysis Date = 07/10/20 Pct Recovery = 100% Analysis Date = 07/06/20 Pct Recovery = 100% Analysis Date = 07/06/20 Pct Recovery = 100% Analysis Date = 07/02/20 Pct Recovery = 100% Analysis Date = 07/02/20 Pct Recovery = 100% Analysis Date = 06/27/20 Pct Recovery = 100% Analysis Date = 06/27/20 Pct Recovery = 100% Analysis Date = 06/23/20 Pct Recovery = 100% Analysis Date = 06/23/20 Pct Recovery = 100% Analysis Date = 06/19/20 Pct Recovery = 100% Analysis Date = 06/19/20 Pct Recovery = 100% Analysis Date = 06/15/20 Pct Recovery = 100% Analysis Date = 06/15/20 Pct Recovery = 100% Analysis Date = 06/10/20 Pct Recovery = 100% Analysis Date = 06/10/20 Pct Recovery = 100% Analysis Date = 06/06/20 Pct Recovery = 100% Analysis Date = 06/06/20 Pct Recovery = 100% Analysis Date = 06/02/20 Pct Recovery = 100% Analysis Date = 06/02/20 Pct Recovery = 100% Analysis Date = 05/29/20 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
THIOBENCARB

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 41 91% 26% 93% 23%
Total 41 91% 26% 93% 23%

Sample Statistics
THIOBENCARB

Characteristic N % % Basis
Plotted 41 100% Spiked
Estimated Values 2 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 41 .  
False Negatives 0 0% 0 out of 41
Not Spiked 74 .  
False Positives 0 0% 0 out of 74

OBSP Determination:
TRANS-PERMETHRIN
METHOD: 2447 , TESTIDCODE: 68708LCM60

Laboratory ID = 20201820155 Lab Value = 26.819 Expected Conc. = 48.4 Report level label = 3.8 Pct Recovery = 55% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 26.549 Expected Conc. = 48.4 Report level label = 3.8 Pct Recovery = 55% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20203230020 Lab Value = 17.078 Expected Conc. = 48.01 Report level label = 3.8 Pct Recovery = 36% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20203230023 Lab Value = 21.487 Expected Conc. = 48.01 Report level label = 3.8 Pct Recovery = 45% Analysis Date = 01/30/21 SpikeMix = Accu 220081475PEST3_3: 100 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20202390020 Lab Value = 26.962 Expected Conc. = 47.8 Report level label = 3.8 Pct Recovery = 56% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203080100 Lab Value = 15.349 Expected Conc. = 47.1 Report level label = 3.8 Pct Recovery = 33% Analysis Date = 11/11/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202880004 Lab Value = 16.633 Expected Conc. = 47.1 Report level label = 3.8 Pct Recovery = 35% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590108 Lab Value = 65.272 Expected Conc. = 47.1 Report level label = 3.8 Pct Recovery = 139% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20202590109 Lab Value = 49.604 Expected Conc. = 47.1 Report level label = 3.8 Pct Recovery = 105% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-3: 100 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20220810134 Lab Value = 18.355 Expected Conc. = 38.64 Report level label = 3.8 Pct Recovery = 48% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222150193 Lab Value = 16.667 Expected Conc. = 38.4 Report level label = 3.8 Pct Recovery = 43% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20212990174 Lab Value = 18.350 Expected Conc. = 38.24 Report level label = 3.8 Pct Recovery = 48% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 29.110 Expected Conc. = 38 Report level label = 3.8 Pct Recovery = 77% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220190116 Lab Value = 9.545 Expected Conc. = 36.88 Report level label = 3.8 Pct Recovery = 26% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 12.985 Expected Conc. = 36.88 Report level label = 3.8 Pct Recovery = 35% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20202530029 Lab Value = 14.629 Expected Conc. = 24.2 Report level label = 3.8 Pct Recovery = 60% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 15.100 Expected Conc. = 24.2 Report level label = 3.8 Pct Recovery = 62% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 23.067 Expected Conc. = 24.2 Report level label = 3.8 Pct Recovery = 95% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20220810133 Lab Value = 16.822 Expected Conc. = 24.15 Report level label = 3.8 Pct Recovery = 70% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20210400070 Lab Value = 8.091 Expected Conc. = 24.005 Report level label = 3.8 Pct Recovery = 34% Analysis Date = 02/18/21 SpikeMix = Accu 220081475PEST3_3: 50 µl & Accu 220081395PEST3: 50 µl SpecificMix = 220081475PEST3_3 Laboratory ID = 20213340027 Lab Value = 14.224 Expected Conc. = 23.9 Report level label = 3.8 Pct Recovery = 60% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 23.136 Expected Conc. = 23.9 Report level label = 3.8 Pct Recovery = 97% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 5.914 Expected Conc. = 23.9 Report level label = 3.8 Pct Recovery = 25% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20201960104 Lab Value = 23.310 Expected Conc. = 23.9 Report level label = 3.8 Pct Recovery = 98% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202950016 Lab Value = 15.039 Expected Conc. = 23.55 Report level label = 3.8 Pct Recovery = 64% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20221730293 Lab Value = 19.486 Expected Conc. = 23.05 Report level label = 3.8 Pct Recovery = 85% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202180001 Lab Value = 6.829 Expected Conc. = 9.68 Report level label = 3.8 Pct Recovery = 71% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 7.755 Expected Conc. = 9.68 Report level label = 3.8 Pct Recovery = 80% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 6.518 Expected Conc. = 9.68 Report level label = 3.8 Pct Recovery = 67% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20222630205 Lab Value = 2.845 Expected Conc. = 9.66 Report level label = 3.8 Pct Recovery = 29% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Laboratory ID = 20213060210 Lab Value = 5.437 Expected Conc. = 9.56 Report level label = 3.8 Pct Recovery = 57% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20201610160 Lab Value = 6.619 Expected Conc. = 9.56 Report level label = 3.8 Pct Recovery = 69% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20203170006 Lab Value = 6.608 Expected Conc. = 9.42 Report level label = 3.8 Pct Recovery = 70% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-3 Laboratory ID = 20213410072 Lab Value = 5.678 Expected Conc. = 9.22 Report level label = 3.8 Pct Recovery = 62% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Analysis Date = 09/28/22 Pct Recovery = 56% Analysis Date = 09/24/22 Pct Recovery = 56% Analysis Date = 09/24/22 Pct Recovery = 56% Analysis Date = 09/20/22 Pct Recovery = 56% Analysis Date = 09/20/22 Pct Recovery = 56% Analysis Date = 09/16/22 Pct Recovery = 56% Analysis Date = 09/16/22 Pct Recovery = 56% Analysis Date = 09/11/22 Pct Recovery = 56% Analysis Date = 09/11/22 Pct Recovery = 56% Analysis Date = 09/07/22 Pct Recovery = 56% Analysis Date = 09/07/22 Pct Recovery = 56% Analysis Date = 09/03/22 Pct Recovery = 56% Analysis Date = 09/03/22 Pct Recovery = 56% Analysis Date = 08/29/22 Pct Recovery = 56% Analysis Date = 08/29/22 Pct Recovery = 56% Analysis Date = 08/25/22 Pct Recovery = 56% Analysis Date = 08/25/22 Pct Recovery = 56% Analysis Date = 08/21/22 Pct Recovery = 55% Analysis Date = 08/21/22 Pct Recovery = 55% Analysis Date = 08/16/22 Pct Recovery = 55% Analysis Date = 08/16/22 Pct Recovery = 55% Analysis Date = 08/12/22 Pct Recovery = 55% Analysis Date = 08/12/22 Pct Recovery = 55% Analysis Date = 08/08/22 Pct Recovery = 55% Analysis Date = 08/08/22 Pct Recovery = 55% Analysis Date = 08/03/22 Pct Recovery = 55% Analysis Date = 08/03/22 Pct Recovery = 55% Analysis Date = 07/30/22 Pct Recovery = 55% Analysis Date = 07/30/22 Pct Recovery = 55% Analysis Date = 07/26/22 Pct Recovery = 55% Analysis Date = 07/26/22 Pct Recovery = 55% Analysis Date = 07/21/22 Pct Recovery = 55% Analysis Date = 07/21/22 Pct Recovery = 55% Analysis Date = 07/17/22 Pct Recovery = 55% Analysis Date = 07/17/22 Pct Recovery = 55% Analysis Date = 07/13/22 Pct Recovery = 55% Analysis Date = 07/13/22 Pct Recovery = 55% Analysis Date = 07/09/22 Pct Recovery = 55% Analysis Date = 07/09/22 Pct Recovery = 55% Analysis Date = 07/04/22 Pct Recovery = 55% Analysis Date = 07/04/22 Pct Recovery = 55% Analysis Date = 06/30/22 Pct Recovery = 55% Analysis Date = 06/30/22 Pct Recovery = 55% Analysis Date = 06/26/22 Pct Recovery = 55% Analysis Date = 06/26/22 Pct Recovery = 55% Analysis Date = 06/21/22 Pct Recovery = 55% Analysis Date = 06/21/22 Pct Recovery = 55% Analysis Date = 06/17/22 Pct Recovery = 55% Analysis Date = 06/17/22 Pct Recovery = 55% Analysis Date = 06/13/22 Pct Recovery = 55% Analysis Date = 06/13/22 Pct Recovery = 55% Analysis Date = 06/08/22 Pct Recovery = 55% Analysis Date = 06/08/22 Pct Recovery = 55% Analysis Date = 06/04/22 Pct Recovery = 55% Analysis Date = 06/04/22 Pct Recovery = 55% Analysis Date = 05/31/22 Pct Recovery = 55% Analysis Date = 05/31/22 Pct Recovery = 55% Analysis Date = 05/26/22 Pct Recovery = 55% Analysis Date = 05/26/22 Pct Recovery = 55% Analysis Date = 05/22/22 Pct Recovery = 55% Analysis Date = 05/22/22 Pct Recovery = 55% Analysis Date = 05/18/22 Pct Recovery = 55% Analysis Date = 05/18/22 Pct Recovery = 55% Analysis Date = 05/13/22 Pct Recovery = 55% Analysis Date = 05/13/22 Pct Recovery = 55% Analysis Date = 05/09/22 Pct Recovery = 55% Analysis Date = 05/09/22 Pct Recovery = 55% Analysis Date = 05/05/22 Pct Recovery = 55% Analysis Date = 05/05/22 Pct Recovery = 55% Analysis Date = 04/30/22 Pct Recovery = 55% Analysis Date = 04/30/22 Pct Recovery = 55% Analysis Date = 04/26/22 Pct Recovery = 55% Analysis Date = 04/26/22 Pct Recovery = 55% Analysis Date = 04/22/22 Pct Recovery = 55% Analysis Date = 04/22/22 Pct Recovery = 55% Analysis Date = 04/18/22 Pct Recovery = 55% Analysis Date = 04/18/22 Pct Recovery = 55% Analysis Date = 04/13/22 Pct Recovery = 55% Analysis Date = 04/13/22 Pct Recovery = 55% Analysis Date = 04/09/22 Pct Recovery = 55% Analysis Date = 04/09/22 Pct Recovery = 55% Analysis Date = 04/05/22 Pct Recovery = 55% Analysis Date = 04/05/22 Pct Recovery = 55% Analysis Date = 03/31/22 Pct Recovery = 55% Analysis Date = 03/31/22 Pct Recovery = 55% Analysis Date = 03/27/22 Pct Recovery = 55% Analysis Date = 03/27/22 Pct Recovery = 55% Analysis Date = 03/23/22 Pct Recovery = 55% Analysis Date = 03/23/22 Pct Recovery = 55% Analysis Date = 03/18/22 Pct Recovery = 54% Analysis Date = 03/18/22 Pct Recovery = 54% Analysis Date = 03/14/22 Pct Recovery = 54% Analysis Date = 03/14/22 Pct Recovery = 54% Analysis Date = 03/10/22 Pct Recovery = 54% Analysis Date = 03/10/22 Pct Recovery = 54% Analysis Date = 03/05/22 Pct Recovery = 54% Analysis Date = 03/05/22 Pct Recovery = 54% Analysis Date = 03/01/22 Pct Recovery = 54% Analysis Date = 03/01/22 Pct Recovery = 54% Analysis Date = 02/25/22 Pct Recovery = 54% Analysis Date = 02/25/22 Pct Recovery = 54% Analysis Date = 02/20/22 Pct Recovery = 54% Analysis Date = 02/20/22 Pct Recovery = 54% Analysis Date = 02/16/22 Pct Recovery = 54% Analysis Date = 02/16/22 Pct Recovery = 54% Analysis Date = 02/12/22 Pct Recovery = 54% Analysis Date = 02/12/22 Pct Recovery = 54% Analysis Date = 02/07/22 Pct Recovery = 54% Analysis Date = 02/07/22 Pct Recovery = 54% Analysis Date = 02/03/22 Pct Recovery = 54% Analysis Date = 02/03/22 Pct Recovery = 54% Analysis Date = 01/30/22 Pct Recovery = 54% Analysis Date = 01/30/22 Pct Recovery = 54% Analysis Date = 01/26/22 Pct Recovery = 54% Analysis Date = 01/26/22 Pct Recovery = 54% Analysis Date = 01/21/22 Pct Recovery = 53% Analysis Date = 01/21/22 Pct Recovery = 53% Analysis Date = 01/17/22 Pct Recovery = 53% Analysis Date = 01/17/22 Pct Recovery = 53% Analysis Date = 01/13/22 Pct Recovery = 53% Analysis Date = 01/13/22 Pct Recovery = 53% Analysis Date = 01/08/22 Pct Recovery = 53% Analysis Date = 01/08/22 Pct Recovery = 53% Analysis Date = 01/04/22 Pct Recovery = 53% Analysis Date = 01/04/22 Pct Recovery = 53% Analysis Date = 12/31/21 Pct Recovery = 53% Analysis Date = 12/31/21 Pct Recovery = 53% Analysis Date = 12/26/21 Pct Recovery = 53% Analysis Date = 12/26/21 Pct Recovery = 53% Analysis Date = 12/22/21 Pct Recovery = 53% Analysis Date = 12/22/21 Pct Recovery = 53% Analysis Date = 12/18/21 Pct Recovery = 53% Analysis Date = 12/18/21 Pct Recovery = 53% Analysis Date = 12/13/21 Pct Recovery = 53% Analysis Date = 12/13/21 Pct Recovery = 53% Analysis Date = 12/09/21 Pct Recovery = 53% Analysis Date = 12/09/21 Pct Recovery = 53% Analysis Date = 12/05/21 Pct Recovery = 52% Analysis Date = 12/05/21 Pct Recovery = 52% Analysis Date = 11/30/21 Pct Recovery = 52% Analysis Date = 11/30/21 Pct Recovery = 52% Analysis Date = 11/26/21 Pct Recovery = 52% Analysis Date = 11/26/21 Pct Recovery = 52% Analysis Date = 11/22/21 Pct Recovery = 52% Analysis Date = 11/22/21 Pct Recovery = 52% Analysis Date = 11/18/21 Pct Recovery = 52% Analysis Date = 11/18/21 Pct Recovery = 52% Analysis Date = 11/13/21 Pct Recovery = 51% Analysis Date = 11/13/21 Pct Recovery = 51% Analysis Date = 11/09/21 Pct Recovery = 51% Analysis Date = 11/09/21 Pct Recovery = 51% Analysis Date = 11/05/21 Pct Recovery = 51% Analysis Date = 11/05/21 Pct Recovery = 51% Analysis Date = 10/31/21 Pct Recovery = 51% Analysis Date = 10/31/21 Pct Recovery = 51% Analysis Date = 10/27/21 Pct Recovery = 50% Analysis Date = 10/27/21 Pct Recovery = 50% Analysis Date = 10/23/21 Pct Recovery = 50% Analysis Date = 10/23/21 Pct Recovery = 50% Analysis Date = 10/18/21 Pct Recovery = 50% Analysis Date = 10/18/21 Pct Recovery = 50% Analysis Date = 10/14/21 Pct Recovery = 49% Analysis Date = 10/14/21 Pct Recovery = 49% Analysis Date = 10/10/21 Pct Recovery = 49% Analysis Date = 10/10/21 Pct Recovery = 49% Analysis Date = 10/05/21 Pct Recovery = 49% Analysis Date = 10/05/21 Pct Recovery = 49% Analysis Date = 10/01/21 Pct Recovery = 49% Analysis Date = 10/01/21 Pct Recovery = 49% Analysis Date = 09/27/21 Pct Recovery = 48% Analysis Date = 09/27/21 Pct Recovery = 48% Analysis Date = 09/22/21 Pct Recovery = 48% Analysis Date = 09/22/21 Pct Recovery = 48% Analysis Date = 09/18/21 Pct Recovery = 48% Analysis Date = 09/18/21 Pct Recovery = 48% Analysis Date = 09/14/21 Pct Recovery = 47% Analysis Date = 09/14/21 Pct Recovery = 47% Analysis Date = 09/09/21 Pct Recovery = 47% Analysis Date = 09/09/21 Pct Recovery = 47% Analysis Date = 09/05/21 Pct Recovery = 47% Analysis Date = 09/05/21 Pct Recovery = 47% Analysis Date = 09/01/21 Pct Recovery = 47% Analysis Date = 09/01/21 Pct Recovery = 47% Analysis Date = 08/28/21 Pct Recovery = 46% Analysis Date = 08/28/21 Pct Recovery = 46% Analysis Date = 08/23/21 Pct Recovery = 46% Analysis Date = 08/23/21 Pct Recovery = 46% Analysis Date = 08/19/21 Pct Recovery = 46% Analysis Date = 08/19/21 Pct Recovery = 46% Analysis Date = 08/15/21 Pct Recovery = 45% Analysis Date = 08/15/21 Pct Recovery = 45% Analysis Date = 08/10/21 Pct Recovery = 45% Analysis Date = 08/10/21 Pct Recovery = 45% Analysis Date = 08/06/21 Pct Recovery = 45% Analysis Date = 08/06/21 Pct Recovery = 45% Analysis Date = 08/02/21 Pct Recovery = 45% Analysis Date = 08/02/21 Pct Recovery = 45% Analysis Date = 07/28/21 Pct Recovery = 44% Analysis Date = 07/28/21 Pct Recovery = 44% Analysis Date = 07/24/21 Pct Recovery = 44% Analysis Date = 07/24/21 Pct Recovery = 44% Analysis Date = 07/20/21 Pct Recovery = 44% Analysis Date = 07/20/21 Pct Recovery = 44% Analysis Date = 07/15/21 Pct Recovery = 43% Analysis Date = 07/15/21 Pct Recovery = 43% Analysis Date = 07/11/21 Pct Recovery = 43% Analysis Date = 07/11/21 Pct Recovery = 43% Analysis Date = 07/07/21 Pct Recovery = 43% Analysis Date = 07/07/21 Pct Recovery = 43% Analysis Date = 07/02/21 Pct Recovery = 43% Analysis Date = 07/02/21 Pct Recovery = 43% Analysis Date = 06/28/21 Pct Recovery = 42% Analysis Date = 06/28/21 Pct Recovery = 42% Analysis Date = 06/24/21 Pct Recovery = 42% Analysis Date = 06/24/21 Pct Recovery = 42% Analysis Date = 06/19/21 Pct Recovery = 42% Analysis Date = 06/19/21 Pct Recovery = 42% Analysis Date = 06/15/21 Pct Recovery = 41% Analysis Date = 06/15/21 Pct Recovery = 41% Analysis Date = 06/11/21 Pct Recovery = 41% Analysis Date = 06/11/21 Pct Recovery = 41% Analysis Date = 06/07/21 Pct Recovery = 41% Analysis Date = 06/07/21 Pct Recovery = 41% Analysis Date = 06/02/21 Pct Recovery = 41% Analysis Date = 06/02/21 Pct Recovery = 41% Analysis Date = 05/29/21 Pct Recovery = 40% Analysis Date = 05/29/21 Pct Recovery = 40% Analysis Date = 05/25/21 Pct Recovery = 40% Analysis Date = 05/25/21 Pct Recovery = 40% Analysis Date = 05/20/21 Pct Recovery = 40% Analysis Date = 05/20/21 Pct Recovery = 40% Analysis Date = 05/16/21 Pct Recovery = 39% Analysis Date = 05/16/21 Pct Recovery = 39% Analysis Date = 05/12/21 Pct Recovery = 39% Analysis Date = 05/12/21 Pct Recovery = 39% Analysis Date = 05/07/21 Pct Recovery = 39% Analysis Date = 05/07/21 Pct Recovery = 39% Analysis Date = 05/03/21 Pct Recovery = 39% Analysis Date = 05/03/21 Pct Recovery = 39% Analysis Date = 04/29/21 Pct Recovery = 38% Analysis Date = 04/29/21 Pct Recovery = 38% Analysis Date = 04/24/21 Pct Recovery = 38% Analysis Date = 04/24/21 Pct Recovery = 38% Analysis Date = 04/20/21 Pct Recovery = 38% Analysis Date = 04/20/21 Pct Recovery = 38% Analysis Date = 04/16/21 Pct Recovery = 37% Analysis Date = 04/16/21 Pct Recovery = 37% Analysis Date = 04/11/21 Pct Recovery = 37% Analysis Date = 04/11/21 Pct Recovery = 37% Analysis Date = 04/07/21 Pct Recovery = 37% Analysis Date = 04/07/21 Pct Recovery = 37% Analysis Date = 04/03/21 Pct Recovery = 37% Analysis Date = 04/03/21 Pct Recovery = 37% Analysis Date = 03/29/21 Pct Recovery = 36% Analysis Date = 03/29/21 Pct Recovery = 36% Analysis Date = 03/25/21 Pct Recovery = 36% Analysis Date = 03/25/21 Pct Recovery = 36% Analysis Date = 03/21/21 Pct Recovery = 36% Analysis Date = 03/21/21 Pct Recovery = 36% Analysis Date = 03/17/21 Pct Recovery = 35% Analysis Date = 03/17/21 Pct Recovery = 35% Analysis Date = 03/12/21 Pct Recovery = 35% Analysis Date = 03/12/21 Pct Recovery = 35% Analysis Date = 03/08/21 Pct Recovery = 35% Analysis Date = 03/08/21 Pct Recovery = 35% Analysis Date = 03/04/21 Pct Recovery = 35% Analysis Date = 03/04/21 Pct Recovery = 35% Analysis Date = 02/27/21 Pct Recovery = 34% Analysis Date = 02/27/21 Pct Recovery = 34% Analysis Date = 02/23/21 Pct Recovery = 34% Analysis Date = 02/23/21 Pct Recovery = 34% Analysis Date = 02/19/21 Pct Recovery = 34% Analysis Date = 02/19/21 Pct Recovery = 34% Analysis Date = 02/14/21 Pct Recovery = 34% Analysis Date = 02/14/21 Pct Recovery = 34% Analysis Date = 02/10/21 Pct Recovery = 36% Analysis Date = 02/10/21 Pct Recovery = 36% Analysis Date = 02/06/21 Pct Recovery = 37% Analysis Date = 02/06/21 Pct Recovery = 37% Analysis Date = 02/01/21 Pct Recovery = 38% Analysis Date = 02/01/21 Pct Recovery = 38% Analysis Date = 01/28/21 Pct Recovery = 39% Analysis Date = 01/28/21 Pct Recovery = 39% Analysis Date = 01/24/21 Pct Recovery = 40% Analysis Date = 01/24/21 Pct Recovery = 40% Analysis Date = 01/19/21 Pct Recovery = 41% Analysis Date = 01/19/21 Pct Recovery = 41% Analysis Date = 01/15/21 Pct Recovery = 42% Analysis Date = 01/15/21 Pct Recovery = 42% Analysis Date = 01/11/21 Pct Recovery = 43% Analysis Date = 01/11/21 Pct Recovery = 43% Analysis Date = 01/07/21 Pct Recovery = 45% Analysis Date = 01/07/21 Pct Recovery = 45% Analysis Date = 01/02/21 Pct Recovery = 46% Analysis Date = 01/02/21 Pct Recovery = 46% Analysis Date = 12/29/20 Pct Recovery = 47% Analysis Date = 12/29/20 Pct Recovery = 47% Analysis Date = 12/25/20 Pct Recovery = 48% Analysis Date = 12/25/20 Pct Recovery = 48% Analysis Date = 12/20/20 Pct Recovery = 49% Analysis Date = 12/20/20 Pct Recovery = 49% Analysis Date = 12/16/20 Pct Recovery = 50% Analysis Date = 12/16/20 Pct Recovery = 50% Analysis Date = 12/12/20 Pct Recovery = 51% Analysis Date = 12/12/20 Pct Recovery = 51% Analysis Date = 12/07/20 Pct Recovery = 53% Analysis Date = 12/07/20 Pct Recovery = 53% Analysis Date = 12/03/20 Pct Recovery = 54% Analysis Date = 12/03/20 Pct Recovery = 54% Analysis Date = 11/29/20 Pct Recovery = 55% Analysis Date = 11/29/20 Pct Recovery = 55% Analysis Date = 11/24/20 Pct Recovery = 56% Analysis Date = 11/24/20 Pct Recovery = 56% Analysis Date = 11/20/20 Pct Recovery = 57% Analysis Date = 11/20/20 Pct Recovery = 57% Analysis Date = 11/16/20 Pct Recovery = 58% Analysis Date = 11/16/20 Pct Recovery = 58% Analysis Date = 11/11/20 Pct Recovery = 59% Analysis Date = 11/11/20 Pct Recovery = 59% Analysis Date = 11/07/20 Pct Recovery = 60% Analysis Date = 11/07/20 Pct Recovery = 60% Analysis Date = 11/03/20 Pct Recovery = 61% Analysis Date = 11/03/20 Pct Recovery = 61% Analysis Date = 10/29/20 Pct Recovery = 62% Analysis Date = 10/29/20 Pct Recovery = 62% Analysis Date = 10/25/20 Pct Recovery = 63% Analysis Date = 10/25/20 Pct Recovery = 63% Analysis Date = 10/21/20 Pct Recovery = 64% Analysis Date = 10/21/20 Pct Recovery = 64% Analysis Date = 10/17/20 Pct Recovery = 65% Analysis Date = 10/17/20 Pct Recovery = 65% Analysis Date = 10/12/20 Pct Recovery = 66% Analysis Date = 10/12/20 Pct Recovery = 66% Analysis Date = 10/08/20 Pct Recovery = 66% Analysis Date = 10/08/20 Pct Recovery = 66% Analysis Date = 10/04/20 Pct Recovery = 67% Analysis Date = 10/04/20 Pct Recovery = 67% Analysis Date = 09/29/20 Pct Recovery = 68% Analysis Date = 09/29/20 Pct Recovery = 68% Analysis Date = 09/25/20 Pct Recovery = 69% Analysis Date = 09/25/20 Pct Recovery = 69% Analysis Date = 09/21/20 Pct Recovery = 70% Analysis Date = 09/21/20 Pct Recovery = 70% Analysis Date = 09/16/20 Pct Recovery = 70% Analysis Date = 09/16/20 Pct Recovery = 70% Analysis Date = 09/12/20 Pct Recovery = 71% Analysis Date = 09/12/20 Pct Recovery = 71% Analysis Date = 09/08/20 Pct Recovery = 71% Analysis Date = 09/08/20 Pct Recovery = 71% Analysis Date = 09/03/20 Pct Recovery = 71% Analysis Date = 09/03/20 Pct Recovery = 71% Analysis Date = 08/30/20 Pct Recovery = 72% Analysis Date = 08/30/20 Pct Recovery = 72% Analysis Date = 08/26/20 Pct Recovery = 72% Analysis Date = 08/26/20 Pct Recovery = 72% Analysis Date = 08/21/20 Pct Recovery = 72% Analysis Date = 08/21/20 Pct Recovery = 72% Analysis Date = 08/17/20 Pct Recovery = 72% Analysis Date = 08/17/20 Pct Recovery = 72% Analysis Date = 08/13/20 Pct Recovery = 73% Analysis Date = 08/13/20 Pct Recovery = 73% Analysis Date = 08/08/20 Pct Recovery = 73% Analysis Date = 08/08/20 Pct Recovery = 73% Analysis Date = 08/04/20 Pct Recovery = 73% Analysis Date = 08/04/20 Pct Recovery = 73% Analysis Date = 07/31/20 Pct Recovery = 73% Analysis Date = 07/31/20 Pct Recovery = 73% Analysis Date = 07/27/20 Pct Recovery = 74% Analysis Date = 07/27/20 Pct Recovery = 74% Analysis Date = 07/22/20 Pct Recovery = 74% Analysis Date = 07/22/20 Pct Recovery = 74% Analysis Date = 07/18/20 Pct Recovery = 74% Analysis Date = 07/18/20 Pct Recovery = 74% Analysis Date = 07/14/20 Pct Recovery = 74% Analysis Date = 07/14/20 Pct Recovery = 74% Analysis Date = 07/09/20 Pct Recovery = 75% Analysis Date = 07/09/20 Pct Recovery = 75% Analysis Date = 07/05/20 Pct Recovery = 75% Analysis Date = 07/05/20 Pct Recovery = 75% Analysis Date = 07/01/20 Pct Recovery = 75% Analysis Date = 07/01/20 Pct Recovery = 75% Analysis Date = 06/26/20 Pct Recovery = 75% Analysis Date = 06/26/20 Pct Recovery = 75% Analysis Date = 06/22/20 Pct Recovery = 75% Analysis Date = 06/22/20 Pct Recovery = 75% Analysis Date = 06/18/20 Pct Recovery = 76% Analysis Date = 06/18/20 Pct Recovery = 76% Analysis Date = 06/13/20 Pct Recovery = 76% Analysis Date = 06/13/20 Pct Recovery = 76% Analysis Date = 06/09/20 Pct Recovery = 76% Analysis Date = 06/09/20 Pct Recovery = 76% Analysis Date = 06/05/20 Pct Recovery = 76% Analysis Date = 06/05/20 Pct Recovery = 76% Analysis Date = 05/31/20 Pct Recovery = 76% Analysis Date = 05/31/20 Pct Recovery = 76% Analysis Date = 05/27/20 Pct Recovery = 76% Analysis Date = 05/27/20 Pct Recovery = 76% Analysis Date = 05/23/20 Pct Recovery = 76% Analysis Date = 05/23/20 Pct Recovery = 76% Analysis Date = 05/19/20 Pct Recovery = 77% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRANS-PERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 34 61% 25% 60% 20%
Total 34 61% 25% 60% 20%

Sample Statistics
TRANS-PERMETHRIN

Characteristic N % % Basis
Plotted 34 89% Spiked
Estimated Values 7 18% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 5% Spiked
Spiked 38 .  
False Negatives 2 5% 2 out of 38
Not Spiked 78 .  
False Positives 0 0% 0 out of 78

OBSP Determination:
TRICLOPYR
METHOD: 2447 , TESTIDCODE: 68712LCM60

Laboratory ID = 20201820155 Lab Value = 1316.948 Expected Conc. = 1113.6 Report level label = 88 Pct Recovery = 118% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 853.015 Expected Conc. = 1113.6 Report level label = 88 Pct Recovery = 77% Analysis Date = 06/04/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20210760015 Lab Value = 997.124 Expected Conc. = 1110 Report level label = 88 Pct Recovery = 90% Analysis Date = 03/24/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210220007 Lab Value = 1176.914 Expected Conc. = 1110 Report level label = 88 Pct Recovery = 106% Analysis Date = 01/29/21 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230022 Lab Value = 1427.248 Expected Conc. = 1110 Report level label = 88 Pct Recovery = 129% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20203230017 Lab Value = 1435.715 Expected Conc. = 1110 Report level label = 88 Pct Recovery = 129% Analysis Date = 12/09/20 SpikeMix = Accu 220111019PEST3_1: 100 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20202390020 Lab Value = 1535.748 Expected Conc. = 1102.1 Report level label = 88 Pct Recovery = 139% Analysis Date = 09/15/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203080100 Lab Value = 1457.242 Expected Conc. = 1096.1 Report level label = 88 Pct Recovery = 133% Analysis Date = 11/13/20 SpikeMix = Abs 081220PEST3-1: 100 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590104 Lab Value = 1298.808 Expected Conc. = 1096.1 Report level label = 88 Pct Recovery = 118% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202590105 Lab Value = 1229.238 Expected Conc. = 1096.1 Report level label = 88 Pct Recovery = 112% Analysis Date = 09/24/20 SpikeMix = Abs 081220PEST3-1: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20221520237 Lab Value = 752.337 Expected Conc. = 890.4 Report level label = 88 Pct Recovery = 84% Analysis Date = 06/07/22 SpikeMix = Accu 221101208: 80 µl SpecificMix = 221101208 Laboratory ID = 20221940196 Lab Value = 654.734 Expected Conc. = 880 Report level label = 88 Pct Recovery = 74% Analysis Date = 07/21/22 SpikeMix = Crescent 04JJ026: 80 µl SpecificMix = 04JJ026 Laboratory ID = 20222150192 Lab Value = 810.998 Expected Conc. = 872.8 Report level label = 88 Pct Recovery = 93% Analysis Date = 08/16/22 SpikeMix = Spex Organics NA220624009: 80 µl SpecificMix = NA220624009 Laboratory ID = 20202530029 Lab Value = 469.117 Expected Conc. = 556.8 Report level label = 88 Pct Recovery = 84% Analysis Date = 09/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 612.792 Expected Conc. = 556.8 Report level label = 88 Pct Recovery = 110% Analysis Date = 08/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 395.959 Expected Conc. = 556.8 Report level label = 88 Pct Recovery = 71% Analysis Date = 05/20/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20221870197 Lab Value = 585.378 Expected Conc. = 556.5 Report level label = 88 Pct Recovery = 105% Analysis Date = 07/14/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101208: 50 µl SpecificMix = 221101208 Laboratory ID = 20210480001 Lab Value = 490.852 Expected Conc. = 555 Report level label = 88 Pct Recovery = 88% Analysis Date = 02/23/21 SpikeMix = Accu 220111019PEST3_1: 50 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201960104 Lab Value = 526.254 Expected Conc. = 551.05 Report level label = 88 Pct Recovery = 96% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20202880004 Lab Value = 453.397 Expected Conc. = 548.05 Report level label = 88 Pct Recovery = 83% Analysis Date = 10/20/20 SpikeMix = Abs 081220PEST3-1: 50 µl & Abs 081120PEST3-3: 100 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20210900005 Lab Value = 385.025 Expected Conc. = 444 Report level label = 88 Pct Recovery = 87% Analysis Date = 04/06/21 SpikeMix = Accu 220111019PEST3_1: 40 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20210620006 Lab Value = 440.911 Expected Conc. = 438.44 Report level label = 88 Pct Recovery = 101% Analysis Date = 03/09/21 SpikeMix = Abs 081220PEST3-1: 40 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203230018 Lab Value = 458.204 Expected Conc. = 438.44 Report level label = 88 Pct Recovery = 105% Analysis Date = 12/09/20 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202180001 Lab Value = 270.998 Expected Conc. = 222.72 Report level label = 88 Pct Recovery = 122% Analysis Date = 08/12/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 248.952 Expected Conc. = 222.72 Report level label = 88 Pct Recovery = 112% Analysis Date = 07/30/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 252.977 Expected Conc. = 222.72 Report level label = 88 Pct Recovery = 114% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210690067 Lab Value = 252.410 Expected Conc. = 222 Report level label = 88 Pct Recovery = 114% Analysis Date = 03/18/21 SpikeMix = Accu 220111019PEST3_1: 20 µl SpecificMix = 220111019PEST3_1 Laboratory ID = 20201610160 Lab Value = 151.509 Expected Conc. = 220.42 Report level label = 88 Pct Recovery = 69% Analysis Date = 06/11/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210120050 Lab Value = 228.719 Expected Conc. = 219.22 Report level label = 88 Pct Recovery = 104% Analysis Date = 01/21/21 SpikeMix = Abs 081220PEST3-1: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203530076 Lab Value = 290.751 Expected Conc. = 219.22 Report level label = 88 Pct Recovery = 133% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203440004 Lab Value = 182.652 Expected Conc. = 219.22 Report level label = 88 Pct Recovery = 83% Analysis Date = 12/18/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20203020006 Lab Value = 245.729 Expected Conc. = 219.22 Report level label = 88 Pct Recovery = 112% Analysis Date = 11/06/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Laboratory ID = 20202810054 Lab Value = 207.209 Expected Conc. = 219.22 Report level label = 88 Pct Recovery = 95% Analysis Date = 10/17/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081220PEST3-1 Analysis Date = 08/16/22 Pct Recovery = 89% Analysis Date = 08/11/22 Pct Recovery = 89% Analysis Date = 08/11/22 Pct Recovery = 89% Analysis Date = 08/07/22 Pct Recovery = 89% Analysis Date = 08/07/22 Pct Recovery = 89% Analysis Date = 08/03/22 Pct Recovery = 89% Analysis Date = 08/03/22 Pct Recovery = 89% Analysis Date = 07/30/22 Pct Recovery = 89% Analysis Date = 07/30/22 Pct Recovery = 89% Analysis Date = 07/26/22 Pct Recovery = 89% Analysis Date = 07/26/22 Pct Recovery = 89% Analysis Date = 07/22/22 Pct Recovery = 89% Analysis Date = 07/22/22 Pct Recovery = 89% Analysis Date = 07/18/22 Pct Recovery = 89% Analysis Date = 07/18/22 Pct Recovery = 89% Analysis Date = 07/14/22 Pct Recovery = 89% Analysis Date = 07/14/22 Pct Recovery = 89% Analysis Date = 07/10/22 Pct Recovery = 89% Analysis Date = 07/10/22 Pct Recovery = 89% Analysis Date = 07/06/22 Pct Recovery = 89% Analysis Date = 07/06/22 Pct Recovery = 89% Analysis Date = 07/02/22 Pct Recovery = 89% Analysis Date = 07/02/22 Pct Recovery = 89% Analysis Date = 06/27/22 Pct Recovery = 89% Analysis Date = 06/27/22 Pct Recovery = 89% Analysis Date = 06/23/22 Pct Recovery = 89% Analysis Date = 06/23/22 Pct Recovery = 89% Analysis Date = 06/19/22 Pct Recovery = 89% Analysis Date = 06/19/22 Pct Recovery = 89% Analysis Date = 06/15/22 Pct Recovery = 90% Analysis Date = 06/15/22 Pct Recovery = 90% Analysis Date = 06/11/22 Pct Recovery = 90% Analysis Date = 06/11/22 Pct Recovery = 90% Analysis Date = 06/07/22 Pct Recovery = 90% Analysis Date = 06/07/22 Pct Recovery = 90% Analysis Date = 06/03/22 Pct Recovery = 90% Analysis Date = 06/03/22 Pct Recovery = 90% Analysis Date = 05/30/22 Pct Recovery = 90% Analysis Date = 05/30/22 Pct Recovery = 90% Analysis Date = 05/26/22 Pct Recovery = 90% Analysis Date = 05/26/22 Pct Recovery = 90% Analysis Date = 05/22/22 Pct Recovery = 90% Analysis Date = 05/22/22 Pct Recovery = 90% Analysis Date = 05/18/22 Pct Recovery = 90% Analysis Date = 05/18/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/13/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/09/22 Pct Recovery = 90% Analysis Date = 05/05/22 Pct Recovery = 90% Analysis Date = 05/05/22 Pct Recovery = 90% Analysis Date = 05/01/22 Pct Recovery = 90% Analysis Date = 05/01/22 Pct Recovery = 90% Analysis Date = 04/27/22 Pct Recovery = 90% Analysis Date = 04/27/22 Pct Recovery = 90% Analysis Date = 04/23/22 Pct Recovery = 90% Analysis Date = 04/23/22 Pct Recovery = 90% Analysis Date = 04/19/22 Pct Recovery = 90% Analysis Date = 04/19/22 Pct Recovery = 90% Analysis Date = 04/15/22 Pct Recovery = 90% Analysis Date = 04/15/22 Pct Recovery = 90% Analysis Date = 04/11/22 Pct Recovery = 90% Analysis Date = 04/11/22 Pct Recovery = 90% Analysis Date = 04/07/22 Pct Recovery = 90% Analysis Date = 04/07/22 Pct Recovery = 90% Analysis Date = 04/03/22 Pct Recovery = 90% Analysis Date = 04/03/22 Pct Recovery = 90% Analysis Date = 03/29/22 Pct Recovery = 90% Analysis Date = 03/29/22 Pct Recovery = 90% Analysis Date = 03/25/22 Pct Recovery = 90% Analysis Date = 03/25/22 Pct Recovery = 90% Analysis Date = 03/21/22 Pct Recovery = 90% Analysis Date = 03/21/22 Pct Recovery = 90% Analysis Date = 03/17/22 Pct Recovery = 90% Analysis Date = 03/17/22 Pct Recovery = 90% Analysis Date = 03/13/22 Pct Recovery = 90% Analysis Date = 03/13/22 Pct Recovery = 90% Analysis Date = 03/09/22 Pct Recovery = 90% Analysis Date = 03/09/22 Pct Recovery = 90% Analysis Date = 03/05/22 Pct Recovery = 90% Analysis Date = 03/05/22 Pct Recovery = 90% Analysis Date = 03/01/22 Pct Recovery = 90% Analysis Date = 03/01/22 Pct Recovery = 90% Analysis Date = 02/25/22 Pct Recovery = 90% Analysis Date = 02/25/22 Pct Recovery = 90% Analysis Date = 02/21/22 Pct Recovery = 90% Analysis Date = 02/21/22 Pct Recovery = 90% Analysis Date = 02/17/22 Pct Recovery = 90% Analysis Date = 02/17/22 Pct Recovery = 90% Analysis Date = 02/12/22 Pct Recovery = 90% Analysis Date = 02/12/22 Pct Recovery = 90% Analysis Date = 02/08/22 Pct Recovery = 90% Analysis Date = 02/08/22 Pct Recovery = 90% Analysis Date = 02/04/22 Pct Recovery = 90% Analysis Date = 02/04/22 Pct Recovery = 90% Analysis Date = 01/31/22 Pct Recovery = 90% Analysis Date = 01/31/22 Pct Recovery = 90% Analysis Date = 01/27/22 Pct Recovery = 91% Analysis Date = 01/27/22 Pct Recovery = 91% Analysis Date = 01/23/22 Pct Recovery = 91% Analysis Date = 01/23/22 Pct Recovery = 91% Analysis Date = 01/19/22 Pct Recovery = 91% Analysis Date = 01/19/22 Pct Recovery = 91% Analysis Date = 01/15/22 Pct Recovery = 91% Analysis Date = 01/15/22 Pct Recovery = 91% Analysis Date = 01/11/22 Pct Recovery = 91% Analysis Date = 01/11/22 Pct Recovery = 91% Analysis Date = 01/07/22 Pct Recovery = 91% Analysis Date = 01/07/22 Pct Recovery = 91% Analysis Date = 01/03/22 Pct Recovery = 91% Analysis Date = 01/03/22 Pct Recovery = 91% Analysis Date = 12/29/21 Pct Recovery = 91% Analysis Date = 12/29/21 Pct Recovery = 91% Analysis Date = 12/25/21 Pct Recovery = 91% Analysis Date = 12/25/21 Pct Recovery = 91% Analysis Date = 12/21/21 Pct Recovery = 91% Analysis Date = 12/21/21 Pct Recovery = 91% Analysis Date = 12/17/21 Pct Recovery = 91% Analysis Date = 12/17/21 Pct Recovery = 91% Analysis Date = 12/13/21 Pct Recovery = 91% Analysis Date = 12/13/21 Pct Recovery = 91% Analysis Date = 12/09/21 Pct Recovery = 91% Analysis Date = 12/09/21 Pct Recovery = 91% Analysis Date = 12/05/21 Pct Recovery = 91% Analysis Date = 12/05/21 Pct Recovery = 91% Analysis Date = 12/01/21 Pct Recovery = 91% Analysis Date = 12/01/21 Pct Recovery = 91% Analysis Date = 11/27/21 Pct Recovery = 91% Analysis Date = 11/27/21 Pct Recovery = 91% Analysis Date = 11/23/21 Pct Recovery = 91% Analysis Date = 11/23/21 Pct Recovery = 91% Analysis Date = 11/19/21 Pct Recovery = 91% Analysis Date = 11/19/21 Pct Recovery = 91% Analysis Date = 11/14/21 Pct Recovery = 91% Analysis Date = 11/14/21 Pct Recovery = 91% Analysis Date = 11/10/21 Pct Recovery = 91% Analysis Date = 11/10/21 Pct Recovery = 91% Analysis Date = 11/06/21 Pct Recovery = 91% Analysis Date = 11/06/21 Pct Recovery = 91% Analysis Date = 11/02/21 Pct Recovery = 91% Analysis Date = 11/02/21 Pct Recovery = 91% Analysis Date = 10/29/21 Pct Recovery = 91% Analysis Date = 10/29/21 Pct Recovery = 91% Analysis Date = 10/25/21 Pct Recovery = 91% Analysis Date = 10/25/21 Pct Recovery = 91% Analysis Date = 10/21/21 Pct Recovery = 91% Analysis Date = 10/21/21 Pct Recovery = 91% Analysis Date = 10/17/21 Pct Recovery = 91% Analysis Date = 10/17/21 Pct Recovery = 91% Analysis Date = 10/13/21 Pct Recovery = 91% Analysis Date = 10/13/21 Pct Recovery = 91% Analysis Date = 10/09/21 Pct Recovery = 91% Analysis Date = 10/09/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 10/05/21 Pct Recovery = 91% Analysis Date = 09/30/21 Pct Recovery = 91% Analysis Date = 09/30/21 Pct Recovery = 91% Analysis Date = 09/26/21 Pct Recovery = 91% Analysis Date = 09/26/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 91% Analysis Date = 09/22/21 Pct Recovery = 91% Analysis Date = 09/18/21 Pct Recovery = 91% Analysis Date = 09/18/21 Pct Recovery = 91% Analysis Date = 09/14/21 Pct Recovery = 92% Analysis Date = 09/14/21 Pct Recovery = 92% Analysis Date = 09/10/21 Pct Recovery = 92% Analysis Date = 09/10/21 Pct Recovery = 92% Analysis Date = 09/06/21 Pct Recovery = 92% Analysis Date = 09/06/21 Pct Recovery = 92% Analysis Date = 09/02/21 Pct Recovery = 92% Analysis Date = 09/02/21 Pct Recovery = 92% Analysis Date = 08/29/21 Pct Recovery = 92% Analysis Date = 08/29/21 Pct Recovery = 92% Analysis Date = 08/25/21 Pct Recovery = 92% Analysis Date = 08/25/21 Pct Recovery = 92% Analysis Date = 08/21/21 Pct Recovery = 92% Analysis Date = 08/21/21 Pct Recovery = 92% Analysis Date = 08/16/21 Pct Recovery = 92% Analysis Date = 08/16/21 Pct Recovery = 92% Analysis Date = 08/12/21 Pct Recovery = 92% Analysis Date = 08/12/21 Pct Recovery = 92% Analysis Date = 08/08/21 Pct Recovery = 92% Analysis Date = 08/08/21 Pct Recovery = 92% Analysis Date = 08/04/21 Pct Recovery = 92% Analysis Date = 08/04/21 Pct Recovery = 92% Analysis Date = 07/31/21 Pct Recovery = 92% Analysis Date = 07/31/21 Pct Recovery = 92% Analysis Date = 07/27/21 Pct Recovery = 92% Analysis Date = 07/27/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/23/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/19/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/15/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/11/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/07/21 Pct Recovery = 92% Analysis Date = 07/03/21 Pct Recovery = 92% Analysis Date = 07/03/21 Pct Recovery = 92% Analysis Date = 06/28/21 Pct Recovery = 92% Analysis Date = 06/28/21 Pct Recovery = 92% Analysis Date = 06/24/21 Pct Recovery = 92% Analysis Date = 06/24/21 Pct Recovery = 92% Analysis Date = 06/20/21 Pct Recovery = 92% Analysis Date = 06/20/21 Pct Recovery = 92% Analysis Date = 06/16/21 Pct Recovery = 92% Analysis Date = 06/16/21 Pct Recovery = 92% Analysis Date = 06/12/21 Pct Recovery = 92% Analysis Date = 06/12/21 Pct Recovery = 92% Analysis Date = 06/08/21 Pct Recovery = 92% Analysis Date = 06/08/21 Pct Recovery = 92% Analysis Date = 06/04/21 Pct Recovery = 92% Analysis Date = 06/04/21 Pct Recovery = 92% Analysis Date = 05/31/21 Pct Recovery = 92% Analysis Date = 05/31/21 Pct Recovery = 92% Analysis Date = 05/27/21 Pct Recovery = 92% Analysis Date = 05/27/21 Pct Recovery = 92% Analysis Date = 05/23/21 Pct Recovery = 92% Analysis Date = 05/23/21 Pct Recovery = 92% Analysis Date = 05/19/21 Pct Recovery = 92% Analysis Date = 05/19/21 Pct Recovery = 92% Analysis Date = 05/14/21 Pct Recovery = 92% Analysis Date = 05/14/21 Pct Recovery = 92% Analysis Date = 05/10/21 Pct Recovery = 92% Analysis Date = 05/10/21 Pct Recovery = 92% Analysis Date = 05/06/21 Pct Recovery = 92% Analysis Date = 05/06/21 Pct Recovery = 92% Analysis Date = 05/02/21 Pct Recovery = 92% Analysis Date = 05/02/21 Pct Recovery = 92% Analysis Date = 04/28/21 Pct Recovery = 93% Analysis Date = 04/28/21 Pct Recovery = 93% Analysis Date = 04/24/21 Pct Recovery = 93% Analysis Date = 04/24/21 Pct Recovery = 93% Analysis Date = 04/20/21 Pct Recovery = 93% Analysis Date = 04/20/21 Pct Recovery = 93% Analysis Date = 04/16/21 Pct Recovery = 93% Analysis Date = 04/16/21 Pct Recovery = 93% Analysis Date = 04/12/21 Pct Recovery = 93% Analysis Date = 04/12/21 Pct Recovery = 93% Analysis Date = 04/08/21 Pct Recovery = 93% Analysis Date = 04/08/21 Pct Recovery = 93% Analysis Date = 04/04/21 Pct Recovery = 93% Analysis Date = 04/04/21 Pct Recovery = 93% Analysis Date = 03/30/21 Pct Recovery = 94% Analysis Date = 03/30/21 Pct Recovery = 94% Analysis Date = 03/26/21 Pct Recovery = 95% Analysis Date = 03/26/21 Pct Recovery = 95% Analysis Date = 03/22/21 Pct Recovery = 95% Analysis Date = 03/22/21 Pct Recovery = 95% Analysis Date = 03/18/21 Pct Recovery = 96% Analysis Date = 03/18/21 Pct Recovery = 96% Analysis Date = 03/14/21 Pct Recovery = 97% Analysis Date = 03/14/21 Pct Recovery = 97% Analysis Date = 03/10/21 Pct Recovery = 98% Analysis Date = 03/10/21 Pct Recovery = 98% Analysis Date = 03/06/21 Pct Recovery = 98% Analysis Date = 03/06/21 Pct Recovery = 98% Analysis Date = 03/02/21 Pct Recovery = 99% Analysis Date = 03/02/21 Pct Recovery = 99% Analysis Date = 02/26/21 Pct Recovery = 100% Analysis Date = 02/26/21 Pct Recovery = 100% Analysis Date = 02/22/21 Pct Recovery = 101% Analysis Date = 02/22/21 Pct Recovery = 101% Analysis Date = 02/18/21 Pct Recovery = 101% Analysis Date = 02/18/21 Pct Recovery = 101% Analysis Date = 02/13/21 Pct Recovery = 102% Analysis Date = 02/13/21 Pct Recovery = 102% Analysis Date = 02/09/21 Pct Recovery = 103% Analysis Date = 02/09/21 Pct Recovery = 103% Analysis Date = 02/05/21 Pct Recovery = 104% Analysis Date = 02/05/21 Pct Recovery = 104% Analysis Date = 02/01/21 Pct Recovery = 104% Analysis Date = 02/01/21 Pct Recovery = 104% Analysis Date = 01/28/21 Pct Recovery = 105% Analysis Date = 01/28/21 Pct Recovery = 105% Analysis Date = 01/24/21 Pct Recovery = 106% Analysis Date = 01/24/21 Pct Recovery = 106% Analysis Date = 01/20/21 Pct Recovery = 106% Analysis Date = 01/20/21 Pct Recovery = 106% Analysis Date = 01/16/21 Pct Recovery = 107% Analysis Date = 01/16/21 Pct Recovery = 107% Analysis Date = 01/12/21 Pct Recovery = 108% Analysis Date = 01/12/21 Pct Recovery = 108% Analysis Date = 01/08/21 Pct Recovery = 108% Analysis Date = 01/08/21 Pct Recovery = 108% Analysis Date = 01/04/21 Pct Recovery = 109% Analysis Date = 01/04/21 Pct Recovery = 109% Analysis Date = 12/30/20 Pct Recovery = 110% Analysis Date = 12/30/20 Pct Recovery = 110% Analysis Date = 12/26/20 Pct Recovery = 110% Analysis Date = 12/26/20 Pct Recovery = 110% Analysis Date = 12/22/20 Pct Recovery = 111% Analysis Date = 12/22/20 Pct Recovery = 111% Analysis Date = 12/18/20 Pct Recovery = 111% Analysis Date = 12/18/20 Pct Recovery = 111% Analysis Date = 12/14/20 Pct Recovery = 111% Analysis Date = 12/14/20 Pct Recovery = 111% Analysis Date = 12/10/20 Pct Recovery = 111% Analysis Date = 12/10/20 Pct Recovery = 111% Analysis Date = 12/06/20 Pct Recovery = 111% Analysis Date = 12/06/20 Pct Recovery = 111% Analysis Date = 12/02/20 Pct Recovery = 111% Analysis Date = 12/02/20 Pct Recovery = 111% Analysis Date = 11/28/20 Pct Recovery = 111% Analysis Date = 11/28/20 Pct Recovery = 111% Analysis Date = 11/24/20 Pct Recovery = 111% Analysis Date = 11/24/20 Pct Recovery = 111% Analysis Date = 11/20/20 Pct Recovery = 111% Analysis Date = 11/20/20 Pct Recovery = 111% Analysis Date = 11/15/20 Pct Recovery = 111% Analysis Date = 11/15/20 Pct Recovery = 111% Analysis Date = 11/11/20 Pct Recovery = 111% Analysis Date = 11/11/20 Pct Recovery = 111% Analysis Date = 11/07/20 Pct Recovery = 111% Analysis Date = 11/07/20 Pct Recovery = 111% Analysis Date = 11/03/20 Pct Recovery = 111% Analysis Date = 11/03/20 Pct Recovery = 111% Analysis Date = 10/30/20 Pct Recovery = 111% Analysis Date = 10/30/20 Pct Recovery = 111% Analysis Date = 10/26/20 Pct Recovery = 111% Analysis Date = 10/26/20 Pct Recovery = 111% Analysis Date = 10/22/20 Pct Recovery = 111% Analysis Date = 10/22/20 Pct Recovery = 111% Analysis Date = 10/18/20 Pct Recovery = 111% Analysis Date = 10/18/20 Pct Recovery = 111% Analysis Date = 10/14/20 Pct Recovery = 111% Analysis Date = 10/14/20 Pct Recovery = 111% Analysis Date = 10/10/20 Pct Recovery = 111% Analysis Date = 10/10/20 Pct Recovery = 111% Analysis Date = 10/06/20 Pct Recovery = 110% Analysis Date = 10/06/20 Pct Recovery = 110% Analysis Date = 10/01/20 Pct Recovery = 110% Analysis Date = 10/01/20 Pct Recovery = 110% Analysis Date = 09/27/20 Pct Recovery = 110% Analysis Date = 09/27/20 Pct Recovery = 110% Analysis Date = 09/23/20 Pct Recovery = 110% Analysis Date = 09/23/20 Pct Recovery = 110% Analysis Date = 09/19/20 Pct Recovery = 110% Analysis Date = 09/19/20 Pct Recovery = 110% Analysis Date = 09/15/20 Pct Recovery = 109% Analysis Date = 09/15/20 Pct Recovery = 109% Analysis Date = 09/11/20 Pct Recovery = 109% Analysis Date = 09/11/20 Pct Recovery = 109% Analysis Date = 09/07/20 Pct Recovery = 109% Analysis Date = 09/07/20 Pct Recovery = 109% Analysis Date = 09/03/20 Pct Recovery = 108% Analysis Date = 09/03/20 Pct Recovery = 108% Analysis Date = 08/30/20 Pct Recovery = 108% Analysis Date = 08/30/20 Pct Recovery = 108% Analysis Date = 08/26/20 Pct Recovery = 108% Analysis Date = 08/26/20 Pct Recovery = 108% Analysis Date = 08/22/20 Pct Recovery = 107% Analysis Date = 08/22/20 Pct Recovery = 107% Analysis Date = 08/17/20 Pct Recovery = 107% Analysis Date = 08/17/20 Pct Recovery = 107% Analysis Date = 08/13/20 Pct Recovery = 106% Analysis Date = 08/13/20 Pct Recovery = 106% Analysis Date = 08/09/20 Pct Recovery = 105% Analysis Date = 08/09/20 Pct Recovery = 105% Analysis Date = 08/05/20 Pct Recovery = 104% Analysis Date = 08/05/20 Pct Recovery = 104% Analysis Date = 08/01/20 Pct Recovery = 103% Analysis Date = 08/01/20 Pct Recovery = 103% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/28/20 Pct Recovery = 102% Analysis Date = 07/24/20 Pct Recovery = 101% Analysis Date = 07/24/20 Pct Recovery = 101% Analysis Date = 07/20/20 Pct Recovery = 100% Analysis Date = 07/20/20 Pct Recovery = 100% Analysis Date = 07/16/20 Pct Recovery = 99% Analysis Date = 07/16/20 Pct Recovery = 99% Analysis Date = 07/12/20 Pct Recovery = 98% Analysis Date = 07/12/20 Pct Recovery = 98% Analysis Date = 07/08/20 Pct Recovery = 97% Analysis Date = 07/08/20 Pct Recovery = 97% Analysis Date = 07/03/20 Pct Recovery = 95% Analysis Date = 07/03/20 Pct Recovery = 95% Analysis Date = 06/29/20 Pct Recovery = 94% Analysis Date = 06/29/20 Pct Recovery = 94% Analysis Date = 06/25/20 Pct Recovery = 93% Analysis Date = 06/25/20 Pct Recovery = 93% Analysis Date = 06/21/20 Pct Recovery = 92% Analysis Date = 06/21/20 Pct Recovery = 92% Analysis Date = 06/17/20 Pct Recovery = 91% Analysis Date = 06/17/20 Pct Recovery = 91% Analysis Date = 06/13/20 Pct Recovery = 90% Analysis Date = 06/13/20 Pct Recovery = 90% Analysis Date = 06/09/20 Pct Recovery = 89% Analysis Date = 06/09/20 Pct Recovery = 89% Analysis Date = 06/05/20 Pct Recovery = 88% Analysis Date = 06/05/20 Pct Recovery = 88% Analysis Date = 06/01/20 Pct Recovery = 86% Analysis Date = 06/01/20 Pct Recovery = 86% Analysis Date = 05/28/20 Pct Recovery = 85% Analysis Date = 05/28/20 Pct Recovery = 85% Analysis Date = 05/24/20 Pct Recovery = 84% Analysis Date = 05/24/20 Pct Recovery = 84% Analysis Date = 05/20/20 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRICLOPYR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 33 103% 19% 105% 20%
Total 33 103% 19% 105% 20%

Sample Statistics
TRICLOPYR

Characteristic N % % Basis
Plotted 33 94% Spiked
Estimated Values 15 43% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 3% Spiked
Spiked 35 .  
False Negatives 1 3% 1 out of 35
Not Spiked 81 .  
False Positives 0 0% 0 out of 81

OBSP Determination:
TRIFLOXYSTROBIN
METHOD: 2447 , TESTIDCODE: 66660LCM60

Laboratory ID = 20201820155 Lab Value = 26.682 Expected Conc. = 35.5 Report level label = 2.8 Pct Recovery = 75% Analysis Date = 07/07/20 SpikeMix = ChemService 9089700: 100 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20201550031 Lab Value = 30.359 Expected Conc. = 35.5 Report level label = 2.8 Pct Recovery = 86% Analysis Date = 06/05/20 SpikeMix = ChemService 9042800: 50 µl & ChemService 8817300: 100 µl SpecificMix = 8817300 Laboratory ID = 20202590106 Lab Value = 27.733 Expected Conc. = 35.3 Report level label = 2.8 Pct Recovery = 79% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202590107 Lab Value = 29.542 Expected Conc. = 35.3 Report level label = 2.8 Pct Recovery = 84% Analysis Date = 09/23/20 SpikeMix = Abs 081120PEST3-2: 100 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202390020 Lab Value = 36.683 Expected Conc. = 35.1 Report level label = 2.8 Pct Recovery = 105% Analysis Date = 09/04/20 SpikeMix = Abs 082719Pest3: 50 µl & Abs 090419Pest3: 100 µl SpecificMix = 090419Pest3 Laboratory ID = 20203230021 Lab Value = 23.139 Expected Conc. = 35 Report level label = 2.8 Pct Recovery = 66% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20203230019 Lab Value = 22.276 Expected Conc. = 35 Report level label = 2.8 Pct Recovery = 64% Analysis Date = 01/30/21 SpikeMix = Accu 220091405PEST3_2: 100 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20220190116 Lab Value = 16.861 Expected Conc. = 28.48 Report level label = 2.8 Pct Recovery = 59% Analysis Date = 02/05/22 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20213410073 Lab Value = 15.930 Expected Conc. = 28.48 Report level label = 2.8 Pct Recovery = 56% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 80 µl SpecificMix = 221101324 Laboratory ID = 20212990174 Lab Value = 13.993 Expected Conc. = 28.16 Report level label = 2.8 Pct Recovery = 50% Analysis Date = 11/03/21 SpikeMix = ChemService 12377000: 80 µl & ChemService 12373100: 80 µl SpecificMix = 12373100 Laboratory ID = 20222010132 Lab Value = 12.467 Expected Conc. = 28 Report level label = 2.8 Pct Recovery = 45% Analysis Date = 07/24/22 SpikeMix = Crescent 04CC026: 80 µl SpecificMix = 04CC026 Laboratory ID = 20220810134 Lab Value = 18.243 Expected Conc. = 27.92 Report level label = 2.8 Pct Recovery = 65% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 80 µl SpecificMix = ND211027021B Laboratory ID = 20222150193 Lab Value = 15.366 Expected Conc. = 27.84 Report level label = 2.8 Pct Recovery = 55% Analysis Date = 08/15/22 SpikeMix = Spex Organics NA220629010: 80 µl SpecificMix = NA220629010 Laboratory ID = 20221730293 Lab Value = 12.976 Expected Conc. = 17.8 Report level label = 2.8 Pct Recovery = 73% Analysis Date = 06/29/22 SpikeMix = Crescent 02AA022: 50 µl & Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20220250055 Lab Value = 11.601 Expected Conc. = 17.8 Report level label = 2.8 Pct Recovery = 65% Analysis Date = 02/06/22 SpikeMix = Accu 221101324: 50 µl SpecificMix = 221101324 Laboratory ID = 20202530029 Lab Value = 13.216 Expected Conc. = 17.75 Report level label = 2.8 Pct Recovery = 74% Analysis Date = 09/17/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20202240086 Lab Value = 13.581 Expected Conc. = 17.75 Report level label = 2.8 Pct Recovery = 77% Analysis Date = 09/02/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20201330113 Lab Value = 13.337 Expected Conc. = 17.75 Report level label = 2.8 Pct Recovery = 75% Analysis Date = 05/19/20 SpikeMix = ChemService 9089700: 50 µl & ChemService 8817300: 50 µl SpecificMix = 8817300 Laboratory ID = 20203230018 Lab Value = 10.903 Expected Conc. = 17.65 Report level label = 2.8 Pct Recovery = 62% Analysis Date = 01/30/21 SpikeMix = Abs 081220PEST3-1: 40 µl & Abs 081120PEST3-2: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203360042 Lab Value = 12.828 Expected Conc. = 17.65 Report level label = 2.8 Pct Recovery = 73% Analysis Date = 12/15/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202950016 Lab Value = 14.302 Expected Conc. = 17.65 Report level label = 2.8 Pct Recovery = 81% Analysis Date = 11/05/20 SpikeMix = Abs 081120PEST3-2: 50 µl & Abs 081120PEST3-3: 50 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20213340027 Lab Value = 12.105 Expected Conc. = 17.6 Report level label = 2.8 Pct Recovery = 69% Analysis Date = 12/07/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213200091 Lab Value = 31.842 Expected Conc. = 17.6 Report level label = 2.8 Pct Recovery = 181% Analysis Date = 11/23/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20213130215 Lab Value = 9.722 Expected Conc. = 17.6 Report level label = 2.8 Pct Recovery = 55% Analysis Date = 11/17/21 SpikeMix = ChemService 12373100: 50 µl & ChemService 12377000: 50 µl SpecificMix = 12373100 Laboratory ID = 20201960104 Lab Value = 17.721 Expected Conc. = 17.55 Report level label = 2.8 Pct Recovery = 101% Analysis Date = 07/21/20 SpikeMix = Abs 082719Pest3: 40 µl & Abs 090419Pest3: 50 µl SpecificMix = 090419Pest3 Laboratory ID = 20220810133 Lab Value = 11.899 Expected Conc. = 17.45 Report level label = 2.8 Pct Recovery = 68% Analysis Date = 03/31/22 SpikeMix = Spex Organics ND211027021B: 50 µl SpecificMix = ND211027021B Laboratory ID = 20222500483 Lab Value = 4.782 Expected Conc. = 7.12 Report level label = 2.8 Pct Recovery = 67% Analysis Date = 09/20/22 SpikeMix = Crescent 02AA022: 20 µl & Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20213410072 Lab Value = 3.701 Expected Conc. = 7.12 Report level label = 2.8 Pct Recovery = 52% Analysis Date = 12/15/21 SpikeMix = Accu 221101324: 20 µl SpecificMix = 221101324 Laboratory ID = 20202180001 Lab Value = 4.846 Expected Conc. = 7.1 Report level label = 2.8 Pct Recovery = 68% Analysis Date = 08/15/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20202040027 Lab Value = 6.945 Expected Conc. = 7.1 Report level label = 2.8 Pct Recovery = 98% Analysis Date = 07/31/20 SpikeMix = ChemService 9089700: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20201750122 Lab Value = 5.837 Expected Conc. = 7.1 Report level label = 2.8 Pct Recovery = 82% Analysis Date = 06/30/20 SpikeMix = ChemService 9042800: 20 µl & ChemService 8817300: 20 µl SpecificMix = 8817300 Laboratory ID = 20210970035 Lab Value = 6.202 Expected Conc. = 7.06 Report level label = 2.8 Pct Recovery = 88% Analysis Date = 04/14/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20210340007 Lab Value = 6.056 Expected Conc. = 7.06 Report level label = 2.8 Pct Recovery = 86% Analysis Date = 02/10/21 SpikeMix = Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203530076 Lab Value = 5.777 Expected Conc. = 7.06 Report level label = 2.8 Pct Recovery = 82% Analysis Date = 12/22/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203170006 Lab Value = 7.847 Expected Conc. = 7.06 Report level label = 2.8 Pct Recovery = 111% Analysis Date = 11/18/20 SpikeMix = Abs 081120PEST3-2: 20 µl & Abs 081120PEST3-3: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20203020006 Lab Value = 6.577 Expected Conc. = 7.06 Report level label = 2.8 Pct Recovery = 93% Analysis Date = 11/03/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20202810054 Lab Value = 6.116 Expected Conc. = 7.06 Report level label = 2.8 Pct Recovery = 87% Analysis Date = 10/14/20 SpikeMix = Abs 081220PEST3-1: 20 µl & Abs 081120PEST3-2: 20 µl SpecificMix = 081120PEST3-2 Laboratory ID = 20213060210 Lab Value = 3.765 Expected Conc. = 7.04 Report level label = 2.8 Pct Recovery = 53% Analysis Date = 11/13/21 SpikeMix = ChemService 12373100: 20 µl & ChemService 12377000: 20 µl SpecificMix = 12373100 Laboratory ID = 20201610160 Lab Value = 6.420 Expected Conc. = 7.02 Report level label = 2.8 Pct Recovery = 91% Analysis Date = 06/17/20 SpikeMix = Abs 090519Pest3: 20 µl & Abs 090419Pest3: 20 µl SpecificMix = 090419Pest3 Laboratory ID = 20210830019 Lab Value = 4.475 Expected Conc. = 7 Report level label = 2.8 Pct Recovery = 64% Analysis Date = 03/31/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20210270007 Lab Value = 4.794 Expected Conc. = 7 Report level label = 2.8 Pct Recovery = 68% Analysis Date = 02/10/21 SpikeMix = Accu 220091405PEST3_2: 20 µl SpecificMix = 220091405PEST3_2 Laboratory ID = 20222630205 Lab Value = 4.943 Expected Conc. = 6.98 Report level label = 2.8 Pct Recovery = 71% Analysis Date = 09/29/22 SpikeMix = Spex Organics ND211027021B: 20 µl SpecificMix = ND211027021B Analysis Date = 09/28/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/24/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 61% Analysis Date = 09/20/22 Pct Recovery = 61% Analysis Date = 09/16/22 Pct Recovery = 61% Analysis Date = 09/16/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/11/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/07/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 61% Analysis Date = 09/03/22 Pct Recovery = 61% Analysis Date = 08/29/22 Pct Recovery = 62% Analysis Date = 08/29/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/25/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/21/22 Pct Recovery = 62% Analysis Date = 08/16/22 Pct Recovery = 62% Analysis Date = 08/16/22 Pct Recovery = 62% Analysis Date = 08/12/22 Pct Recovery = 62% Analysis Date = 08/12/22 Pct Recovery = 62% Analysis Date = 08/08/22 Pct Recovery = 62% Analysis Date = 08/08/22 Pct Recovery = 62% Analysis Date = 08/03/22 Pct Recovery = 63% Analysis Date = 08/03/22 Pct Recovery = 63% Analysis Date = 07/30/22 Pct Recovery = 63% Analysis Date = 07/30/22 Pct Recovery = 63% Analysis Date = 07/26/22 Pct Recovery = 63% Analysis Date = 07/26/22 Pct Recovery = 63% Analysis Date = 07/21/22 Pct Recovery = 63% Analysis Date = 07/21/22 Pct Recovery = 63% Analysis Date = 07/17/22 Pct Recovery = 63% Analysis Date = 07/17/22 Pct Recovery = 63% Analysis Date = 07/13/22 Pct Recovery = 63% Analysis Date = 07/13/22 Pct Recovery = 63% Analysis Date = 07/09/22 Pct Recovery = 63% Analysis Date = 07/09/22 Pct Recovery = 63% Analysis Date = 07/04/22 Pct Recovery = 64% Analysis Date = 07/04/22 Pct Recovery = 64% Analysis Date = 06/30/22 Pct Recovery = 64% Analysis Date = 06/30/22 Pct Recovery = 64% Analysis Date = 06/26/22 Pct Recovery = 64% Analysis Date = 06/26/22 Pct Recovery = 64% Analysis Date = 06/21/22 Pct Recovery = 64% Analysis Date = 06/21/22 Pct Recovery = 64% Analysis Date = 06/17/22 Pct Recovery = 64% Analysis Date = 06/17/22 Pct Recovery = 64% Analysis Date = 06/13/22 Pct Recovery = 64% Analysis Date = 06/13/22 Pct Recovery = 64% Analysis Date = 06/08/22 Pct Recovery = 64% Analysis Date = 06/08/22 Pct Recovery = 64% Analysis Date = 06/04/22 Pct Recovery = 65% Analysis Date = 06/04/22 Pct Recovery = 65% Analysis Date = 05/31/22 Pct Recovery = 65% Analysis Date = 05/31/22 Pct Recovery = 65% Analysis Date = 05/26/22 Pct Recovery = 65% Analysis Date = 05/26/22 Pct Recovery = 65% Analysis Date = 05/22/22 Pct Recovery = 65% Analysis Date = 05/22/22 Pct Recovery = 65% Analysis Date = 05/18/22 Pct Recovery = 65% Analysis Date = 05/18/22 Pct Recovery = 65% Analysis Date = 05/13/22 Pct Recovery = 65% Analysis Date = 05/13/22 Pct Recovery = 65% Analysis Date = 05/09/22 Pct Recovery = 66% Analysis Date = 05/09/22 Pct Recovery = 66% Analysis Date = 05/05/22 Pct Recovery = 66% Analysis Date = 05/05/22 Pct Recovery = 66% Analysis Date = 04/30/22 Pct Recovery = 66% Analysis Date = 04/30/22 Pct Recovery = 66% Analysis Date = 04/26/22 Pct Recovery = 66% Analysis Date = 04/26/22 Pct Recovery = 66% Analysis Date = 04/22/22 Pct Recovery = 66% Analysis Date = 04/22/22 Pct Recovery = 66% Analysis Date = 04/18/22 Pct Recovery = 66% Analysis Date = 04/18/22 Pct Recovery = 66% Analysis Date = 04/13/22 Pct Recovery = 66% Analysis Date = 04/13/22 Pct Recovery = 66% Analysis Date = 04/09/22 Pct Recovery = 67% Analysis Date = 04/09/22 Pct Recovery = 67% Analysis Date = 04/05/22 Pct Recovery = 67% Analysis Date = 04/05/22 Pct Recovery = 67% Analysis Date = 03/31/22 Pct Recovery = 67% Analysis Date = 03/31/22 Pct Recovery = 67% Analysis Date = 03/27/22 Pct Recovery = 67% Analysis Date = 03/27/22 Pct Recovery = 67% Analysis Date = 03/23/22 Pct Recovery = 67% Analysis Date = 03/23/22 Pct Recovery = 67% Analysis Date = 03/18/22 Pct Recovery = 67% Analysis Date = 03/18/22 Pct Recovery = 67% Analysis Date = 03/14/22 Pct Recovery = 67% Analysis Date = 03/14/22 Pct Recovery = 67% Analysis Date = 03/10/22 Pct Recovery = 68% Analysis Date = 03/10/22 Pct Recovery = 68% Analysis Date = 03/05/22 Pct Recovery = 68% Analysis Date = 03/05/22 Pct Recovery = 68% Analysis Date = 03/01/22 Pct Recovery = 68% Analysis Date = 03/01/22 Pct Recovery = 68% Analysis Date = 02/25/22 Pct Recovery = 68% Analysis Date = 02/25/22 Pct Recovery = 68% Analysis Date = 02/20/22 Pct Recovery = 68% Analysis Date = 02/20/22 Pct Recovery = 68% Analysis Date = 02/16/22 Pct Recovery = 68% Analysis Date = 02/16/22 Pct Recovery = 68% Analysis Date = 02/12/22 Pct Recovery = 68% Analysis Date = 02/12/22 Pct Recovery = 68% Analysis Date = 02/07/22 Pct Recovery = 69% Analysis Date = 02/07/22 Pct Recovery = 69% Analysis Date = 02/03/22 Pct Recovery = 69% Analysis Date = 02/03/22 Pct Recovery = 69% Analysis Date = 01/30/22 Pct Recovery = 69% Analysis Date = 01/30/22 Pct Recovery = 69% Analysis Date = 01/26/22 Pct Recovery = 69% Analysis Date = 01/26/22 Pct Recovery = 69% Analysis Date = 01/21/22 Pct Recovery = 69% Analysis Date = 01/21/22 Pct Recovery = 69% Analysis Date = 01/17/22 Pct Recovery = 69% Analysis Date = 01/17/22 Pct Recovery = 69% Analysis Date = 01/13/22 Pct Recovery = 69% Analysis Date = 01/13/22 Pct Recovery = 69% Analysis Date = 01/08/22 Pct Recovery = 70% Analysis Date = 01/08/22 Pct Recovery = 70% Analysis Date = 01/04/22 Pct Recovery = 70% Analysis Date = 01/04/22 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 70% Analysis Date = 12/31/21 Pct Recovery = 70% Analysis Date = 12/26/21 Pct Recovery = 70% Analysis Date = 12/26/21 Pct Recovery = 70% Analysis Date = 12/22/21 Pct Recovery = 70% Analysis Date = 12/22/21 Pct Recovery = 70% Analysis Date = 12/18/21 Pct Recovery = 70% Analysis Date = 12/18/21 Pct Recovery = 70% Analysis Date = 12/13/21 Pct Recovery = 71% Analysis Date = 12/13/21 Pct Recovery = 71% Analysis Date = 12/09/21 Pct Recovery = 71% Analysis Date = 12/09/21 Pct Recovery = 71% Analysis Date = 12/05/21 Pct Recovery = 71% Analysis Date = 12/05/21 Pct Recovery = 71% Analysis Date = 11/30/21 Pct Recovery = 71% Analysis Date = 11/30/21 Pct Recovery = 71% Analysis Date = 11/26/21 Pct Recovery = 71% Analysis Date = 11/26/21 Pct Recovery = 71% Analysis Date = 11/22/21 Pct Recovery = 71% Analysis Date = 11/22/21 Pct Recovery = 71% Analysis Date = 11/18/21 Pct Recovery = 71% Analysis Date = 11/18/21 Pct Recovery = 71% Analysis Date = 11/13/21 Pct Recovery = 71% Analysis Date = 11/13/21 Pct Recovery = 71% Analysis Date = 11/09/21 Pct Recovery = 72% Analysis Date = 11/09/21 Pct Recovery = 72% Analysis Date = 11/05/21 Pct Recovery = 72% Analysis Date = 11/05/21 Pct Recovery = 72% Analysis Date = 10/31/21 Pct Recovery = 72% Analysis Date = 10/31/21 Pct Recovery = 72% Analysis Date = 10/27/21 Pct Recovery = 72% Analysis Date = 10/27/21 Pct Recovery = 72% Analysis Date = 10/23/21 Pct Recovery = 72% Analysis Date = 10/23/21 Pct Recovery = 72% Analysis Date = 10/18/21 Pct Recovery = 72% Analysis Date = 10/18/21 Pct Recovery = 72% Analysis Date = 10/14/21 Pct Recovery = 72% Analysis Date = 10/14/21 Pct Recovery = 72% Analysis Date = 10/10/21 Pct Recovery = 72% Analysis Date = 10/10/21 Pct Recovery = 72% Analysis Date = 10/05/21 Pct Recovery = 72% Analysis Date = 10/05/21 Pct Recovery = 72% Analysis Date = 10/01/21 Pct Recovery = 72% Analysis Date = 10/01/21 Pct Recovery = 72% Analysis Date = 09/27/21 Pct Recovery = 72% Analysis Date = 09/27/21 Pct Recovery = 72% Analysis Date = 09/22/21 Pct Recovery = 72% Analysis Date = 09/22/21 Pct Recovery = 72% Analysis Date = 09/18/21 Pct Recovery = 72% Analysis Date = 09/18/21 Pct Recovery = 72% Analysis Date = 09/14/21 Pct Recovery = 72% Analysis Date = 09/14/21 Pct Recovery = 72% Analysis Date = 09/09/21 Pct Recovery = 72% Analysis Date = 09/09/21 Pct Recovery = 72% Analysis Date = 09/05/21 Pct Recovery = 72% Analysis Date = 09/05/21 Pct Recovery = 72% Analysis Date = 09/01/21 Pct Recovery = 72% Analysis Date = 09/01/21 Pct Recovery = 72% Analysis Date = 08/28/21 Pct Recovery = 73% Analysis Date = 08/28/21 Pct Recovery = 73% Analysis Date = 08/23/21 Pct Recovery = 73% Analysis Date = 08/23/21 Pct Recovery = 73% Analysis Date = 08/19/21 Pct Recovery = 73% Analysis Date = 08/19/21 Pct Recovery = 73% Analysis Date = 08/15/21 Pct Recovery = 73% Analysis Date = 08/15/21 Pct Recovery = 73% Analysis Date = 08/10/21 Pct Recovery = 73% Analysis Date = 08/10/21 Pct Recovery = 73% Analysis Date = 08/06/21 Pct Recovery = 73% Analysis Date = 08/06/21 Pct Recovery = 73% Analysis Date = 08/02/21 Pct Recovery = 73% Analysis Date = 08/02/21 Pct Recovery = 73% Analysis Date = 07/28/21 Pct Recovery = 73% Analysis Date = 07/28/21 Pct Recovery = 73% Analysis Date = 07/24/21 Pct Recovery = 73% Analysis Date = 07/24/21 Pct Recovery = 73% Analysis Date = 07/20/21 Pct Recovery = 73% Analysis Date = 07/20/21 Pct Recovery = 73% Analysis Date = 07/15/21 Pct Recovery = 73% Analysis Date = 07/15/21 Pct Recovery = 73% Analysis Date = 07/11/21 Pct Recovery = 73% Analysis Date = 07/11/21 Pct Recovery = 73% Analysis Date = 07/07/21 Pct Recovery = 73% Analysis Date = 07/07/21 Pct Recovery = 73% Analysis Date = 07/02/21 Pct Recovery = 73% Analysis Date = 07/02/21 Pct Recovery = 73% Analysis Date = 06/28/21 Pct Recovery = 73% Analysis Date = 06/28/21 Pct Recovery = 73% Analysis Date = 06/24/21 Pct Recovery = 73% Analysis Date = 06/24/21 Pct Recovery = 73% Analysis Date = 06/19/21 Pct Recovery = 73% Analysis Date = 06/19/21 Pct Recovery = 73% Analysis Date = 06/15/21 Pct Recovery = 73% Analysis Date = 06/15/21 Pct Recovery = 73% Analysis Date = 06/11/21 Pct Recovery = 73% Analysis Date = 06/11/21 Pct Recovery = 73% Analysis Date = 06/07/21 Pct Recovery = 73% Analysis Date = 06/07/21 Pct Recovery = 73% Analysis Date = 06/02/21 Pct Recovery = 73% Analysis Date = 06/02/21 Pct Recovery = 73% Analysis Date = 05/29/21 Pct Recovery = 74% Analysis Date = 05/29/21 Pct Recovery = 74% Analysis Date = 05/25/21 Pct Recovery = 74% Analysis Date = 05/25/21 Pct Recovery = 74% Analysis Date = 05/20/21 Pct Recovery = 74% Analysis Date = 05/20/21 Pct Recovery = 74% Analysis Date = 05/16/21 Pct Recovery = 74% Analysis Date = 05/16/21 Pct Recovery = 74% Analysis Date = 05/12/21 Pct Recovery = 74% Analysis Date = 05/12/21 Pct Recovery = 74% Analysis Date = 05/07/21 Pct Recovery = 74% Analysis Date = 05/07/21 Pct Recovery = 74% Analysis Date = 05/03/21 Pct Recovery = 74% Analysis Date = 05/03/21 Pct Recovery = 74% Analysis Date = 04/29/21 Pct Recovery = 74% Analysis Date = 04/29/21 Pct Recovery = 74% Analysis Date = 04/24/21 Pct Recovery = 74% Analysis Date = 04/24/21 Pct Recovery = 74% Analysis Date = 04/20/21 Pct Recovery = 74% Analysis Date = 04/20/21 Pct Recovery = 74% Analysis Date = 04/16/21 Pct Recovery = 74% Analysis Date = 04/16/21 Pct Recovery = 74% Analysis Date = 04/11/21 Pct Recovery = 74% Analysis Date = 04/11/21 Pct Recovery = 74% Analysis Date = 04/07/21 Pct Recovery = 74% Analysis Date = 04/07/21 Pct Recovery = 74% Analysis Date = 04/03/21 Pct Recovery = 74% Analysis Date = 04/03/21 Pct Recovery = 74% Analysis Date = 03/29/21 Pct Recovery = 74% Analysis Date = 03/29/21 Pct Recovery = 74% Analysis Date = 03/25/21 Pct Recovery = 74% Analysis Date = 03/25/21 Pct Recovery = 74% Analysis Date = 03/21/21 Pct Recovery = 74% Analysis Date = 03/21/21 Pct Recovery = 74% Analysis Date = 03/17/21 Pct Recovery = 74% Analysis Date = 03/17/21 Pct Recovery = 74% Analysis Date = 03/12/21 Pct Recovery = 74% Analysis Date = 03/12/21 Pct Recovery = 74% Analysis Date = 03/08/21 Pct Recovery = 74% Analysis Date = 03/08/21 Pct Recovery = 74% Analysis Date = 03/04/21 Pct Recovery = 75% Analysis Date = 03/04/21 Pct Recovery = 75% Analysis Date = 02/27/21 Pct Recovery = 75% Analysis Date = 02/27/21 Pct Recovery = 75% Analysis Date = 02/23/21 Pct Recovery = 75% Analysis Date = 02/23/21 Pct Recovery = 75% Analysis Date = 02/19/21 Pct Recovery = 75% Analysis Date = 02/19/21 Pct Recovery = 75% Analysis Date = 02/14/21 Pct Recovery = 75% Analysis Date = 02/14/21 Pct Recovery = 75% Analysis Date = 02/10/21 Pct Recovery = 75% Analysis Date = 02/10/21 Pct Recovery = 75% Analysis Date = 02/06/21 Pct Recovery = 75% Analysis Date = 02/06/21 Pct Recovery = 75% Analysis Date = 02/01/21 Pct Recovery = 75% Analysis Date = 02/01/21 Pct Recovery = 75% Analysis Date = 01/28/21 Pct Recovery = 76% Analysis Date = 01/28/21 Pct Recovery = 76% Analysis Date = 01/24/21 Pct Recovery = 76% Analysis Date = 01/24/21 Pct Recovery = 76% Analysis Date = 01/19/21 Pct Recovery = 76% Analysis Date = 01/19/21 Pct Recovery = 76% Analysis Date = 01/15/21 Pct Recovery = 77% Analysis Date = 01/15/21 Pct Recovery = 77% Analysis Date = 01/11/21 Pct Recovery = 77% Analysis Date = 01/11/21 Pct Recovery = 77% Analysis Date = 01/07/21 Pct Recovery = 77% Analysis Date = 01/07/21 Pct Recovery = 77% Analysis Date = 01/02/21 Pct Recovery = 78% Analysis Date = 01/02/21 Pct Recovery = 78% Analysis Date = 12/29/20 Pct Recovery = 78% Analysis Date = 12/29/20 Pct Recovery = 78% Analysis Date = 12/25/20 Pct Recovery = 78% Analysis Date = 12/25/20 Pct Recovery = 78% Analysis Date = 12/20/20 Pct Recovery = 79% Analysis Date = 12/20/20 Pct Recovery = 79% Analysis Date = 12/16/20 Pct Recovery = 79% Analysis Date = 12/16/20 Pct Recovery = 79% Analysis Date = 12/12/20 Pct Recovery = 79% Analysis Date = 12/12/20 Pct Recovery = 79% Analysis Date = 12/07/20 Pct Recovery = 80% Analysis Date = 12/07/20 Pct Recovery = 80% Analysis Date = 12/03/20 Pct Recovery = 80% Analysis Date = 12/03/20 Pct Recovery = 80% Analysis Date = 11/29/20 Pct Recovery = 80% Analysis Date = 11/29/20 Pct Recovery = 80% Analysis Date = 11/24/20 Pct Recovery = 81% Analysis Date = 11/24/20 Pct Recovery = 81% Analysis Date = 11/20/20 Pct Recovery = 81% Analysis Date = 11/20/20 Pct Recovery = 81% Analysis Date = 11/16/20 Pct Recovery = 81% Analysis Date = 11/16/20 Pct Recovery = 81% Analysis Date = 11/11/20 Pct Recovery = 81% Analysis Date = 11/11/20 Pct Recovery = 81% Analysis Date = 11/07/20 Pct Recovery = 82% Analysis Date = 11/07/20 Pct Recovery = 82% Analysis Date = 11/03/20 Pct Recovery = 82% Analysis Date = 11/03/20 Pct Recovery = 82% Analysis Date = 10/29/20 Pct Recovery = 82% Analysis Date = 10/29/20 Pct Recovery = 82% Analysis Date = 10/25/20 Pct Recovery = 83% Analysis Date = 10/25/20 Pct Recovery = 83% Analysis Date = 10/21/20 Pct Recovery = 83% Analysis Date = 10/21/20 Pct Recovery = 83% Analysis Date = 10/17/20 Pct Recovery = 83% Analysis Date = 10/17/20 Pct Recovery = 83% Analysis Date = 10/12/20 Pct Recovery = 83% Analysis Date = 10/12/20 Pct Recovery = 83% Analysis Date = 10/08/20 Pct Recovery = 83% Analysis Date = 10/08/20 Pct Recovery = 83% Analysis Date = 10/04/20 Pct Recovery = 84% Analysis Date = 10/04/20 Pct Recovery = 84% Analysis Date = 09/29/20 Pct Recovery = 84% Analysis Date = 09/29/20 Pct Recovery = 84% Analysis Date = 09/25/20 Pct Recovery = 84% Analysis Date = 09/25/20 Pct Recovery = 84% Analysis Date = 09/21/20 Pct Recovery = 84% Analysis Date = 09/21/20 Pct Recovery = 84% Analysis Date = 09/16/20 Pct Recovery = 84% Analysis Date = 09/16/20 Pct Recovery = 84% Analysis Date = 09/12/20 Pct Recovery = 84% Analysis Date = 09/12/20 Pct Recovery = 84% Analysis Date = 09/08/20 Pct Recovery = 85% Analysis Date = 09/08/20 Pct Recovery = 85% Analysis Date = 09/03/20 Pct Recovery = 85% Analysis Date = 09/03/20 Pct Recovery = 85% Analysis Date = 08/30/20 Pct Recovery = 85% Analysis Date = 08/30/20 Pct Recovery = 85% Analysis Date = 08/26/20 Pct Recovery = 85% Analysis Date = 08/26/20 Pct Recovery = 85% Analysis Date = 08/21/20 Pct Recovery = 85% Analysis Date = 08/21/20 Pct Recovery = 85% Analysis Date = 08/17/20 Pct Recovery = 85% Analysis Date = 08/17/20 Pct Recovery = 85% Analysis Date = 08/13/20 Pct Recovery = 85% Analysis Date = 08/13/20 Pct Recovery = 85% Analysis Date = 08/08/20 Pct Recovery = 85% Analysis Date = 08/08/20 Pct Recovery = 85% Analysis Date = 08/04/20 Pct Recovery = 85% Analysis Date = 08/04/20 Pct Recovery = 85% Analysis Date = 07/31/20 Pct Recovery = 85% Analysis Date = 07/31/20 Pct Recovery = 85% Analysis Date = 07/27/20 Pct Recovery = 85% Analysis Date = 07/27/20 Pct Recovery = 85% Analysis Date = 07/22/20 Pct Recovery = 85% Analysis Date = 07/22/20 Pct Recovery = 85% Analysis Date = 07/18/20 Pct Recovery = 85% Analysis Date = 07/18/20 Pct Recovery = 85% Analysis Date = 07/14/20 Pct Recovery = 85% Analysis Date = 07/14/20 Pct Recovery = 85% Analysis Date = 07/09/20 Pct Recovery = 85% Analysis Date = 07/09/20 Pct Recovery = 85% Analysis Date = 07/05/20 Pct Recovery = 85% Analysis Date = 07/05/20 Pct Recovery = 85% Analysis Date = 07/01/20 Pct Recovery = 85% Analysis Date = 07/01/20 Pct Recovery = 85% Analysis Date = 06/26/20 Pct Recovery = 85% Analysis Date = 06/26/20 Pct Recovery = 85% Analysis Date = 06/22/20 Pct Recovery = 85% Analysis Date = 06/22/20 Pct Recovery = 85% Analysis Date = 06/18/20 Pct Recovery = 85% Analysis Date = 06/18/20 Pct Recovery = 85% Analysis Date = 06/13/20 Pct Recovery = 85% Analysis Date = 06/13/20 Pct Recovery = 85% Analysis Date = 06/09/20 Pct Recovery = 85% Analysis Date = 06/09/20 Pct Recovery = 85% Analysis Date = 06/05/20 Pct Recovery = 85% Analysis Date = 06/05/20 Pct Recovery = 85% Analysis Date = 05/31/20 Pct Recovery = 85% Analysis Date = 05/31/20 Pct Recovery = 85% Analysis Date = 05/27/20 Pct Recovery = 85% Analysis Date = 05/27/20 Pct Recovery = 85% Analysis Date = 05/23/20 Pct Recovery = 85% Analysis Date = 05/23/20 Pct Recovery = 85% Analysis Date = 05/19/20 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIFLOXYSTROBIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 42 76% 23% 73% 16%
Total 42 76% 23% 73% 16%

Sample Statistics
TRIFLOXYSTROBIN

Characteristic N % % Basis
Plotted 42 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 42 .  
False Negatives 0 0% 0 out of 42
Not Spiked 74 .  
False Positives 0 0% 0 out of 74