OBSP Determination:
1-NAPHTHOL
METHOD: 2033 , TESTIDCODE: 49295GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 58% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 42% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 65% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 51% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 56% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 50% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 25% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 84% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 49% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 62% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 54% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 55% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 71% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 33% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 33% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 50% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 36% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 24% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 36% Analysis Date = 05/10/17 Pct Recovery = 63% Analysis Date = 05/08/17 Pct Recovery = 62% Analysis Date = 05/08/17 Pct Recovery = 62% Analysis Date = 05/06/17 Pct Recovery = 62% Analysis Date = 05/06/17 Pct Recovery = 62% Analysis Date = 05/04/17 Pct Recovery = 62% Analysis Date = 05/04/17 Pct Recovery = 62% Analysis Date = 05/01/17 Pct Recovery = 61% Analysis Date = 05/01/17 Pct Recovery = 61% Analysis Date = 04/29/17 Pct Recovery = 61% Analysis Date = 04/29/17 Pct Recovery = 61% Analysis Date = 04/27/17 Pct Recovery = 61% Analysis Date = 04/27/17 Pct Recovery = 61% Analysis Date = 04/25/17 Pct Recovery = 61% Analysis Date = 04/25/17 Pct Recovery = 61% Analysis Date = 04/22/17 Pct Recovery = 60% Analysis Date = 04/22/17 Pct Recovery = 60% Analysis Date = 04/20/17 Pct Recovery = 60% Analysis Date = 04/20/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 60% Analysis Date = 04/15/17 Pct Recovery = 60% Analysis Date = 04/15/17 Pct Recovery = 60% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/11/17 Pct Recovery = 59% Analysis Date = 04/11/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 58% Analysis Date = 04/04/17 Pct Recovery = 58% Analysis Date = 04/02/17 Pct Recovery = 58% Analysis Date = 04/02/17 Pct Recovery = 58% Analysis Date = 03/30/17 Pct Recovery = 58% Analysis Date = 03/30/17 Pct Recovery = 58% Analysis Date = 03/28/17 Pct Recovery = 58% Analysis Date = 03/28/17 Pct Recovery = 58% Analysis Date = 03/26/17 Pct Recovery = 58% Analysis Date = 03/26/17 Pct Recovery = 58% Analysis Date = 03/24/17 Pct Recovery = 57% Analysis Date = 03/24/17 Pct Recovery = 57% Analysis Date = 03/21/17 Pct Recovery = 57% Analysis Date = 03/21/17 Pct Recovery = 57% Analysis Date = 03/19/17 Pct Recovery = 57% Analysis Date = 03/19/17 Pct Recovery = 57% Analysis Date = 03/17/17 Pct Recovery = 57% Analysis Date = 03/17/17 Pct Recovery = 57% Analysis Date = 03/14/17 Pct Recovery = 56% Analysis Date = 03/14/17 Pct Recovery = 56% Analysis Date = 03/12/17 Pct Recovery = 56% Analysis Date = 03/12/17 Pct Recovery = 56% Analysis Date = 03/10/17 Pct Recovery = 56% Analysis Date = 03/10/17 Pct Recovery = 56% Analysis Date = 03/08/17 Pct Recovery = 56% Analysis Date = 03/08/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 55% Analysis Date = 03/05/17 Pct Recovery = 55% Analysis Date = 03/03/17 Pct Recovery = 55% Analysis Date = 03/03/17 Pct Recovery = 55% Analysis Date = 03/01/17 Pct Recovery = 55% Analysis Date = 03/01/17 Pct Recovery = 55% Analysis Date = 02/26/17 Pct Recovery = 55% Analysis Date = 02/26/17 Pct Recovery = 55% Analysis Date = 02/24/17 Pct Recovery = 54% Analysis Date = 02/24/17 Pct Recovery = 54% Analysis Date = 02/22/17 Pct Recovery = 54% Analysis Date = 02/22/17 Pct Recovery = 54% Analysis Date = 02/20/17 Pct Recovery = 54% Analysis Date = 02/20/17 Pct Recovery = 54% Analysis Date = 02/17/17 Pct Recovery = 54% Analysis Date = 02/17/17 Pct Recovery = 54% Analysis Date = 02/15/17 Pct Recovery = 54% Analysis Date = 02/15/17 Pct Recovery = 54% Analysis Date = 02/13/17 Pct Recovery = 53% Analysis Date = 02/13/17 Pct Recovery = 53% Analysis Date = 02/10/17 Pct Recovery = 53% Analysis Date = 02/10/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/06/17 Pct Recovery = 53% Analysis Date = 02/06/17 Pct Recovery = 53% Analysis Date = 02/04/17 Pct Recovery = 53% Analysis Date = 02/04/17 Pct Recovery = 53% Analysis Date = 02/01/17 Pct Recovery = 52% Analysis Date = 02/01/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 52% Analysis Date = 01/30/17 Pct Recovery = 52% Analysis Date = 01/28/17 Pct Recovery = 52% Analysis Date = 01/28/17 Pct Recovery = 52% Analysis Date = 01/25/17 Pct Recovery = 52% Analysis Date = 01/25/17 Pct Recovery = 52% Analysis Date = 01/23/17 Pct Recovery = 52% Analysis Date = 01/23/17 Pct Recovery = 52% Analysis Date = 01/21/17 Pct Recovery = 51% Analysis Date = 01/21/17 Pct Recovery = 51% Analysis Date = 01/19/17 Pct Recovery = 51% Analysis Date = 01/19/17 Pct Recovery = 51% Analysis Date = 01/16/17 Pct Recovery = 51% Analysis Date = 01/16/17 Pct Recovery = 51% Analysis Date = 01/14/17 Pct Recovery = 51% Analysis Date = 01/14/17 Pct Recovery = 51% Analysis Date = 01/12/17 Pct Recovery = 52% Analysis Date = 01/12/17 Pct Recovery = 52% Analysis Date = 01/09/17 Pct Recovery = 52% Analysis Date = 01/09/17 Pct Recovery = 52% Analysis Date = 01/07/17 Pct Recovery = 52% Analysis Date = 01/07/17 Pct Recovery = 52% Analysis Date = 01/05/17 Pct Recovery = 53% Analysis Date = 01/05/17 Pct Recovery = 53% Analysis Date = 01/03/17 Pct Recovery = 53% Analysis Date = 01/03/17 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/29/16 Pct Recovery = 53% Analysis Date = 12/29/16 Pct Recovery = 53% Analysis Date = 12/27/16 Pct Recovery = 54% Analysis Date = 12/27/16 Pct Recovery = 54% Analysis Date = 12/24/16 Pct Recovery = 54% Analysis Date = 12/24/16 Pct Recovery = 54% Analysis Date = 12/22/16 Pct Recovery = 54% Analysis Date = 12/22/16 Pct Recovery = 54% Analysis Date = 12/20/16 Pct Recovery = 54% Analysis Date = 12/20/16 Pct Recovery = 54% Analysis Date = 12/18/16 Pct Recovery = 54% Analysis Date = 12/18/16 Pct Recovery = 54% Analysis Date = 12/15/16 Pct Recovery = 55% Analysis Date = 12/15/16 Pct Recovery = 55% Analysis Date = 12/13/16 Pct Recovery = 55% Analysis Date = 12/13/16 Pct Recovery = 55% Analysis Date = 12/11/16 Pct Recovery = 55% Analysis Date = 12/11/16 Pct Recovery = 55% Analysis Date = 12/08/16 Pct Recovery = 55% Analysis Date = 12/08/16 Pct Recovery = 55% Analysis Date = 12/06/16 Pct Recovery = 55% Analysis Date = 12/06/16 Pct Recovery = 55% Analysis Date = 12/04/16 Pct Recovery = 55% Analysis Date = 12/04/16 Pct Recovery = 55% Analysis Date = 12/02/16 Pct Recovery = 55% Analysis Date = 12/02/16 Pct Recovery = 55% Analysis Date = 11/29/16 Pct Recovery = 55% Analysis Date = 11/29/16 Pct Recovery = 55% Analysis Date = 11/27/16 Pct Recovery = 55% Analysis Date = 11/27/16 Pct Recovery = 55% Analysis Date = 11/25/16 Pct Recovery = 56% Analysis Date = 11/25/16 Pct Recovery = 56% Analysis Date = 11/22/16 Pct Recovery = 56% Analysis Date = 11/22/16 Pct Recovery = 56% Analysis Date = 11/20/16 Pct Recovery = 56% Analysis Date = 11/20/16 Pct Recovery = 56% Analysis Date = 11/18/16 Pct Recovery = 56% Analysis Date = 11/18/16 Pct Recovery = 56% Analysis Date = 11/16/16 Pct Recovery = 56% Analysis Date = 11/16/16 Pct Recovery = 56% Analysis Date = 11/13/16 Pct Recovery = 56% Analysis Date = 11/13/16 Pct Recovery = 56% Analysis Date = 11/11/16 Pct Recovery = 56% Analysis Date = 11/11/16 Pct Recovery = 56% Analysis Date = 11/09/16 Pct Recovery = 56% Analysis Date = 11/09/16 Pct Recovery = 56% Analysis Date = 11/06/16 Pct Recovery = 56% Analysis Date = 11/06/16 Pct Recovery = 56% Analysis Date = 11/04/16 Pct Recovery = 57% Analysis Date = 11/04/16 Pct Recovery = 57% Analysis Date = 11/02/16 Pct Recovery = 57% Analysis Date = 11/02/16 Pct Recovery = 57% Analysis Date = 10/31/16 Pct Recovery = 57% Analysis Date = 10/31/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/26/16 Pct Recovery = 57% Analysis Date = 10/26/16 Pct Recovery = 57% Analysis Date = 10/24/16 Pct Recovery = 57% Analysis Date = 10/24/16 Pct Recovery = 57% Analysis Date = 10/21/16 Pct Recovery = 57% Analysis Date = 10/21/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 58% Analysis Date = 10/15/16 Pct Recovery = 58% Analysis Date = 10/12/16 Pct Recovery = 58% Analysis Date = 10/12/16 Pct Recovery = 58% Analysis Date = 10/10/16 Pct Recovery = 58% Analysis Date = 10/10/16 Pct Recovery = 58% Analysis Date = 10/08/16 Pct Recovery = 58% Analysis Date = 10/08/16 Pct Recovery = 58% Analysis Date = 10/05/16 Pct Recovery = 58% Analysis Date = 10/05/16 Pct Recovery = 58% Analysis Date = 10/03/16 Pct Recovery = 58% Analysis Date = 10/03/16 Pct Recovery = 58% Analysis Date = 10/01/16 Pct Recovery = 58% Analysis Date = 10/01/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 58% Analysis Date = 09/26/16 Pct Recovery = 58% Analysis Date = 09/26/16 Pct Recovery = 58% Analysis Date = 09/24/16 Pct Recovery = 58% Analysis Date = 09/24/16 Pct Recovery = 58% Analysis Date = 09/22/16 Pct Recovery = 59% Analysis Date = 09/22/16 Pct Recovery = 59% Analysis Date = 09/19/16 Pct Recovery = 59% Analysis Date = 09/19/16 Pct Recovery = 59% Analysis Date = 09/17/16 Pct Recovery = 59% Analysis Date = 09/17/16 Pct Recovery = 59% Analysis Date = 09/15/16 Pct Recovery = 59% Analysis Date = 09/15/16 Pct Recovery = 59% Analysis Date = 09/13/16 Pct Recovery = 59% Analysis Date = 09/13/16 Pct Recovery = 59% Analysis Date = 09/10/16 Pct Recovery = 59% Analysis Date = 09/10/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/06/16 Pct Recovery = 59% Analysis Date = 09/06/16 Pct Recovery = 59% Analysis Date = 09/03/16 Pct Recovery = 59% Analysis Date = 09/03/16 Pct Recovery = 59% Analysis Date = 09/01/16 Pct Recovery = 59% Analysis Date = 09/01/16 Pct Recovery = 59% Analysis Date = 08/30/16 Pct Recovery = 58% Analysis Date = 08/30/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/23/16 Pct Recovery = 58% Analysis Date = 08/23/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/18/16 Pct Recovery = 58% Analysis Date = 08/18/16 Pct Recovery = 58% Analysis Date = 08/16/16 Pct Recovery = 57% Analysis Date = 08/16/16 Pct Recovery = 57% Analysis Date = 08/14/16 Pct Recovery = 56% Analysis Date = 08/14/16 Pct Recovery = 56% Analysis Date = 08/12/16 Pct Recovery = 56% Analysis Date = 08/12/16 Pct Recovery = 56% Analysis Date = 08/09/16 Pct Recovery = 55% Analysis Date = 08/09/16 Pct Recovery = 55% Analysis Date = 08/07/16 Pct Recovery = 55% Analysis Date = 08/07/16 Pct Recovery = 55% Analysis Date = 08/05/16 Pct Recovery = 54% Analysis Date = 08/05/16 Pct Recovery = 54% Analysis Date = 08/02/16 Pct Recovery = 53% Analysis Date = 08/02/16 Pct Recovery = 53% Analysis Date = 07/31/16 Pct Recovery = 53% Analysis Date = 07/31/16 Pct Recovery = 53% Analysis Date = 07/29/16 Pct Recovery = 52% Analysis Date = 07/29/16 Pct Recovery = 52% Analysis Date = 07/27/16 Pct Recovery = 52% Analysis Date = 07/27/16 Pct Recovery = 52% Analysis Date = 07/24/16 Pct Recovery = 51% Analysis Date = 07/24/16 Pct Recovery = 51% Analysis Date = 07/22/16 Pct Recovery = 51% Analysis Date = 07/22/16 Pct Recovery = 51% Analysis Date = 07/20/16 Pct Recovery = 50% Analysis Date = 07/20/16 Pct Recovery = 50% Analysis Date = 07/17/16 Pct Recovery = 49% Analysis Date = 07/17/16 Pct Recovery = 49% Analysis Date = 07/15/16 Pct Recovery = 49% Analysis Date = 07/15/16 Pct Recovery = 49% Analysis Date = 07/13/16 Pct Recovery = 48% Analysis Date = 07/13/16 Pct Recovery = 48% Analysis Date = 07/11/16 Pct Recovery = 48% Analysis Date = 07/11/16 Pct Recovery = 48% Analysis Date = 07/08/16 Pct Recovery = 47% Analysis Date = 07/08/16 Pct Recovery = 47% Analysis Date = 07/06/16 Pct Recovery = 46% Analysis Date = 07/06/16 Pct Recovery = 46% Analysis Date = 07/04/16 Pct Recovery = 46% Analysis Date = 07/04/16 Pct Recovery = 46% Analysis Date = 07/01/16 Pct Recovery = 45% Analysis Date = 07/01/16 Pct Recovery = 45% Analysis Date = 06/29/16 Pct Recovery = 45% Analysis Date = 06/29/16 Pct Recovery = 45% Analysis Date = 06/27/16 Pct Recovery = 44% Analysis Date = 06/27/16 Pct Recovery = 44% Analysis Date = 06/25/16 Pct Recovery = 44% Analysis Date = 06/25/16 Pct Recovery = 44% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/22/16 Pct Recovery = 43% Analysis Date = 06/20/16 Pct Recovery = 42% Analysis Date = 06/20/16 Pct Recovery = 42% Analysis Date = 06/18/16 Pct Recovery = 42% Analysis Date = 06/18/16 Pct Recovery = 42% Analysis Date = 06/15/16 Pct Recovery = 41% Analysis Date = 06/15/16 Pct Recovery = 41% Analysis Date = 06/13/16 Pct Recovery = 41% Analysis Date = 06/13/16 Pct Recovery = 41% Analysis Date = 06/11/16 Pct Recovery = 40% Analysis Date = 06/11/16 Pct Recovery = 40% Analysis Date = 06/09/16 Pct Recovery = 39% Analysis Date = 06/09/16 Pct Recovery = 39% Analysis Date = 06/06/16 Pct Recovery = 39% Analysis Date = 06/06/16 Pct Recovery = 39% Analysis Date = 06/04/16 Pct Recovery = 38% Analysis Date = 06/04/16 Pct Recovery = 38% Analysis Date = 06/02/16 Pct Recovery = 38% Analysis Date = 06/02/16 Pct Recovery = 38% Analysis Date = 05/30/16 Pct Recovery = 37% Analysis Date = 05/30/16 Pct Recovery = 37% Analysis Date = 05/28/16 Pct Recovery = 37% Analysis Date = 05/28/16 Pct Recovery = 37% Analysis Date = 05/26/16 Pct Recovery = 36% Analysis Date = 05/26/16 Pct Recovery = 36% Analysis Date = 05/24/16 Pct Recovery = 36% Analysis Date = 05/24/16 Pct Recovery = 36% Analysis Date = 05/21/16 Pct Recovery = 36% Analysis Date = 05/21/16 Pct Recovery = 36% Analysis Date = 05/19/16 Pct Recovery = 35% Analysis Date = 05/19/16 Pct Recovery = 35% Analysis Date = 05/17/16 Pct Recovery = 35% Analysis Date = 05/17/16 Pct Recovery = 35% Analysis Date = 05/14/16 Pct Recovery = 35% Analysis Date = 05/14/16 Pct Recovery = 35% Analysis Date = 05/12/16 Pct Recovery = 35% Analysis Date = 05/12/16 Pct Recovery = 35% Analysis Date = 05/10/16 Pct Recovery = 34% Analysis Date = 05/10/16 Pct Recovery = 34% Analysis Date = 05/08/16 Pct Recovery = 34% Analysis Date = 05/08/16 Pct Recovery = 34% Analysis Date = 05/05/16 Pct Recovery = 34% Analysis Date = 05/05/16 Pct Recovery = 34% Analysis Date = 05/03/16 Pct Recovery = 34% Analysis Date = 05/03/16 Pct Recovery = 34% Analysis Date = 05/01/16 Pct Recovery = 34% Analysis Date = 05/01/16 Pct Recovery = 34% Analysis Date = 04/28/16 Pct Recovery = 34% Analysis Date = 04/28/16 Pct Recovery = 34% Analysis Date = 04/26/16 Pct Recovery = 34% Analysis Date = 04/26/16 Pct Recovery = 34% Analysis Date = 04/24/16 Pct Recovery = 34% Analysis Date = 04/24/16 Pct Recovery = 34% Analysis Date = 04/22/16 Pct Recovery = 34% Analysis Date = 04/22/16 Pct Recovery = 34% Analysis Date = 04/19/16 Pct Recovery = 34% Analysis Date = 04/19/16 Pct Recovery = 34% Analysis Date = 04/17/16 Pct Recovery = 34% Analysis Date = 04/17/16 Pct Recovery = 34% Analysis Date = 04/15/16 Pct Recovery = 34% Analysis Date = 04/15/16 Pct Recovery = 34% Analysis Date = 04/12/16 Pct Recovery = 34% Analysis Date = 04/12/16 Pct Recovery = 34% Analysis Date = 04/10/16 Pct Recovery = 34% Analysis Date = 04/10/16 Pct Recovery = 34% Analysis Date = 04/08/16 Pct Recovery = 34% Analysis Date = 04/08/16 Pct Recovery = 34% Analysis Date = 04/06/16 Pct Recovery = 34% Analysis Date = 04/06/16 Pct Recovery = 34% Analysis Date = 04/03/16 Pct Recovery = 35% Analysis Date = 04/03/16 Pct Recovery = 35% Analysis Date = 04/01/16 Pct Recovery = 35% Analysis Date = 04/01/16 Pct Recovery = 35% Analysis Date = 03/30/16 Pct Recovery = 35% Analysis Date = 03/30/16 Pct Recovery = 35% Analysis Date = 03/27/16 Pct Recovery = 35% Analysis Date = 03/27/16 Pct Recovery = 35% Analysis Date = 03/25/16 Pct Recovery = 35% Analysis Date = 03/25/16 Pct Recovery = 35% Analysis Date = 03/23/16 Pct Recovery = 35% Analysis Date = 03/23/16 Pct Recovery = 35% Analysis Date = 03/21/16 Pct Recovery = 36% Analysis Date = 03/21/16 Pct Recovery = 36% Analysis Date = 03/18/16 Pct Recovery = 36% Analysis Date = 03/18/16 Pct Recovery = 36% Analysis Date = 03/16/16 Pct Recovery = 36% Analysis Date = 03/16/16 Pct Recovery = 36% Analysis Date = 03/14/16 Pct Recovery = 36% Analysis Date = 03/14/16 Pct Recovery = 36% Analysis Date = 03/11/16 Pct Recovery = 36% Analysis Date = 03/11/16 Pct Recovery = 36% Analysis Date = 03/09/16 Pct Recovery = 36% Analysis Date = 03/09/16 Pct Recovery = 36% Analysis Date = 03/07/16 Pct Recovery = 37% Analysis Date = 03/07/16 Pct Recovery = 37% Analysis Date = 03/05/16 Pct Recovery = 37% Analysis Date = 03/05/16 Pct Recovery = 37% Analysis Date = 03/02/16 Pct Recovery = 37% Analysis Date = 03/02/16 Pct Recovery = 37% Analysis Date = 02/29/16 Pct Recovery = 37% Analysis Date = 02/29/16 Pct Recovery = 37% Analysis Date = 02/27/16 Pct Recovery = 37% Analysis Date = 02/27/16 Pct Recovery = 37% Analysis Date = 02/24/16 Pct Recovery = 38% Analysis Date = 02/24/16 Pct Recovery = 38% Analysis Date = 02/22/16 Pct Recovery = 38% Analysis Date = 02/22/16 Pct Recovery = 38% Analysis Date = 02/20/16 Pct Recovery = 38% Analysis Date = 02/20/16 Pct Recovery = 38% Analysis Date = 02/18/16 Pct Recovery = 38% Analysis Date = 02/18/16 Pct Recovery = 38% Analysis Date = 02/15/16 Pct Recovery = 38% Analysis Date = 02/15/16 Pct Recovery = 38% Analysis Date = 02/13/16 Pct Recovery = 39% Analysis Date = 02/13/16 Pct Recovery = 39% Analysis Date = 02/11/16 Pct Recovery = 39% Analysis Date = 02/11/16 Pct Recovery = 39% Analysis Date = 02/09/16 Pct Recovery = 39% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
1-NAPHTHOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 49% 16% 50% 16%
Total 19 49% 16% 50% 16%

Sample Statistics
1-NAPHTHOL

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 1 11% 1 out of 9

OBSP Determination:
2,6-DIETHYLANILINE
METHOD: 2033 , TESTIDCODE: 82660GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 105% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 109% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 85% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 102% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 91% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 92% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 108% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 104% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 94% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 05/10/17 Pct Recovery = 85% Analysis Date = 05/08/17 Pct Recovery = 86% Analysis Date = 05/08/17 Pct Recovery = 86% Analysis Date = 05/06/17 Pct Recovery = 86% Analysis Date = 05/06/17 Pct Recovery = 86% Analysis Date = 05/04/17 Pct Recovery = 87% Analysis Date = 05/04/17 Pct Recovery = 87% Analysis Date = 05/01/17 Pct Recovery = 87% Analysis Date = 05/01/17 Pct Recovery = 87% Analysis Date = 04/29/17 Pct Recovery = 88% Analysis Date = 04/29/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/25/17 Pct Recovery = 89% Analysis Date = 04/25/17 Pct Recovery = 89% Analysis Date = 04/22/17 Pct Recovery = 89% Analysis Date = 04/22/17 Pct Recovery = 89% Analysis Date = 04/20/17 Pct Recovery = 90% Analysis Date = 04/20/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/15/17 Pct Recovery = 91% Analysis Date = 04/15/17 Pct Recovery = 91% Analysis Date = 04/13/17 Pct Recovery = 91% Analysis Date = 04/13/17 Pct Recovery = 91% Analysis Date = 04/11/17 Pct Recovery = 91% Analysis Date = 04/11/17 Pct Recovery = 91% Analysis Date = 04/09/17 Pct Recovery = 92% Analysis Date = 04/09/17 Pct Recovery = 92% Analysis Date = 04/06/17 Pct Recovery = 92% Analysis Date = 04/06/17 Pct Recovery = 92% Analysis Date = 04/04/17 Pct Recovery = 93% Analysis Date = 04/04/17 Pct Recovery = 93% Analysis Date = 04/02/17 Pct Recovery = 93% Analysis Date = 04/02/17 Pct Recovery = 93% Analysis Date = 03/30/17 Pct Recovery = 94% Analysis Date = 03/30/17 Pct Recovery = 94% Analysis Date = 03/28/17 Pct Recovery = 94% Analysis Date = 03/28/17 Pct Recovery = 94% Analysis Date = 03/26/17 Pct Recovery = 95% Analysis Date = 03/26/17 Pct Recovery = 95% Analysis Date = 03/24/17 Pct Recovery = 95% Analysis Date = 03/24/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 97% Analysis Date = 03/10/17 Pct Recovery = 98% Analysis Date = 03/10/17 Pct Recovery = 98% Analysis Date = 03/08/17 Pct Recovery = 98% Analysis Date = 03/08/17 Pct Recovery = 98% Analysis Date = 03/05/17 Pct Recovery = 99% Analysis Date = 03/05/17 Pct Recovery = 99% Analysis Date = 03/03/17 Pct Recovery = 99% Analysis Date = 03/03/17 Pct Recovery = 99% Analysis Date = 03/01/17 Pct Recovery = 100% Analysis Date = 03/01/17 Pct Recovery = 100% Analysis Date = 02/26/17 Pct Recovery = 100% Analysis Date = 02/26/17 Pct Recovery = 100% Analysis Date = 02/24/17 Pct Recovery = 100% Analysis Date = 02/24/17 Pct Recovery = 100% Analysis Date = 02/22/17 Pct Recovery = 101% Analysis Date = 02/22/17 Pct Recovery = 101% Analysis Date = 02/20/17 Pct Recovery = 101% Analysis Date = 02/20/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/10/17 Pct Recovery = 101% Analysis Date = 02/10/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 101% Analysis Date = 02/04/17 Pct Recovery = 101% Analysis Date = 02/04/17 Pct Recovery = 101% Analysis Date = 02/01/17 Pct Recovery = 101% Analysis Date = 02/01/17 Pct Recovery = 101% Analysis Date = 01/30/17 Pct Recovery = 101% Analysis Date = 01/30/17 Pct Recovery = 101% Analysis Date = 01/28/17 Pct Recovery = 101% Analysis Date = 01/28/17 Pct Recovery = 101% Analysis Date = 01/25/17 Pct Recovery = 101% Analysis Date = 01/25/17 Pct Recovery = 101% Analysis Date = 01/23/17 Pct Recovery = 102% Analysis Date = 01/23/17 Pct Recovery = 102% Analysis Date = 01/21/17 Pct Recovery = 102% Analysis Date = 01/21/17 Pct Recovery = 102% Analysis Date = 01/19/17 Pct Recovery = 102% Analysis Date = 01/19/17 Pct Recovery = 102% Analysis Date = 01/16/17 Pct Recovery = 101% Analysis Date = 01/16/17 Pct Recovery = 101% Analysis Date = 01/14/17 Pct Recovery = 101% Analysis Date = 01/14/17 Pct Recovery = 101% Analysis Date = 01/12/17 Pct Recovery = 101% Analysis Date = 01/12/17 Pct Recovery = 101% Analysis Date = 01/09/17 Pct Recovery = 101% Analysis Date = 01/09/17 Pct Recovery = 101% Analysis Date = 01/07/17 Pct Recovery = 101% Analysis Date = 01/07/17 Pct Recovery = 101% Analysis Date = 01/05/17 Pct Recovery = 100% Analysis Date = 01/05/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 100% Analysis Date = 12/29/16 Pct Recovery = 100% Analysis Date = 12/29/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 99% Analysis Date = 12/27/16 Pct Recovery = 99% Analysis Date = 12/24/16 Pct Recovery = 99% Analysis Date = 12/24/16 Pct Recovery = 99% Analysis Date = 12/22/16 Pct Recovery = 99% Analysis Date = 12/22/16 Pct Recovery = 99% Analysis Date = 12/20/16 Pct Recovery = 99% Analysis Date = 12/20/16 Pct Recovery = 99% Analysis Date = 12/18/16 Pct Recovery = 98% Analysis Date = 12/18/16 Pct Recovery = 98% Analysis Date = 12/15/16 Pct Recovery = 98% Analysis Date = 12/15/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 98% Analysis Date = 12/11/16 Pct Recovery = 98% Analysis Date = 12/08/16 Pct Recovery = 97% Analysis Date = 12/08/16 Pct Recovery = 97% Analysis Date = 12/06/16 Pct Recovery = 97% Analysis Date = 12/06/16 Pct Recovery = 97% Analysis Date = 12/04/16 Pct Recovery = 97% Analysis Date = 12/04/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 11/29/16 Pct Recovery = 97% Analysis Date = 11/29/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 96% Analysis Date = 11/27/16 Pct Recovery = 96% Analysis Date = 11/25/16 Pct Recovery = 96% Analysis Date = 11/25/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 96% Analysis Date = 11/20/16 Pct Recovery = 96% Analysis Date = 11/20/16 Pct Recovery = 96% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 95% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 10/31/16 Pct Recovery = 93% Analysis Date = 10/31/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/26/16 Pct Recovery = 93% Analysis Date = 10/26/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 93% Analysis Date = 10/21/16 Pct Recovery = 93% Analysis Date = 10/21/16 Pct Recovery = 93% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/26/16 Pct Recovery = 90% Analysis Date = 09/26/16 Pct Recovery = 90% Analysis Date = 09/24/16 Pct Recovery = 90% Analysis Date = 09/24/16 Pct Recovery = 90% Analysis Date = 09/22/16 Pct Recovery = 89% Analysis Date = 09/22/16 Pct Recovery = 89% Analysis Date = 09/19/16 Pct Recovery = 89% Analysis Date = 09/19/16 Pct Recovery = 89% Analysis Date = 09/17/16 Pct Recovery = 89% Analysis Date = 09/17/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/15/16 Pct Recovery = 89% Analysis Date = 09/13/16 Pct Recovery = 89% Analysis Date = 09/13/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/10/16 Pct Recovery = 89% Analysis Date = 09/08/16 Pct Recovery = 89% Analysis Date = 09/08/16 Pct Recovery = 89% Analysis Date = 09/06/16 Pct Recovery = 89% Analysis Date = 09/06/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 09/01/16 Pct Recovery = 89% Analysis Date = 09/01/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 89% Analysis Date = 08/12/16 Pct Recovery = 90% Analysis Date = 08/12/16 Pct Recovery = 90% Analysis Date = 08/09/16 Pct Recovery = 90% Analysis Date = 08/09/16 Pct Recovery = 90% Analysis Date = 08/07/16 Pct Recovery = 90% Analysis Date = 08/07/16 Pct Recovery = 90% Analysis Date = 08/05/16 Pct Recovery = 90% Analysis Date = 08/05/16 Pct Recovery = 90% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 90% Analysis Date = 07/22/16 Pct Recovery = 90% Analysis Date = 07/22/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/17/16 Pct Recovery = 91% Analysis Date = 07/17/16 Pct Recovery = 91% Analysis Date = 07/15/16 Pct Recovery = 91% Analysis Date = 07/15/16 Pct Recovery = 91% Analysis Date = 07/13/16 Pct Recovery = 91% Analysis Date = 07/13/16 Pct Recovery = 91% Analysis Date = 07/11/16 Pct Recovery = 91% Analysis Date = 07/11/16 Pct Recovery = 91% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/06/16 Pct Recovery = 91% Analysis Date = 07/06/16 Pct Recovery = 91% Analysis Date = 07/04/16 Pct Recovery = 91% Analysis Date = 07/04/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 06/29/16 Pct Recovery = 91% Analysis Date = 06/29/16 Pct Recovery = 91% Analysis Date = 06/27/16 Pct Recovery = 91% Analysis Date = 06/27/16 Pct Recovery = 91% Analysis Date = 06/25/16 Pct Recovery = 91% Analysis Date = 06/25/16 Pct Recovery = 91% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/15/16 Pct Recovery = 92% Analysis Date = 06/15/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/09/16 Pct Recovery = 92% Analysis Date = 06/09/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/04/16 Pct Recovery = 92% Analysis Date = 06/04/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 06/02/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/30/16 Pct Recovery = 92% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/28/16 Pct Recovery = 93% Analysis Date = 05/26/16 Pct Recovery = 93% Analysis Date = 05/26/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/24/16 Pct Recovery = 93% Analysis Date = 05/21/16 Pct Recovery = 93% Analysis Date = 05/21/16 Pct Recovery = 93% Analysis Date = 05/19/16 Pct Recovery = 93% Analysis Date = 05/19/16 Pct Recovery = 93% Analysis Date = 05/17/16 Pct Recovery = 93% Analysis Date = 05/17/16 Pct Recovery = 93% Analysis Date = 05/14/16 Pct Recovery = 93% Analysis Date = 05/14/16 Pct Recovery = 93% Analysis Date = 05/12/16 Pct Recovery = 93% Analysis Date = 05/12/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/08/16 Pct Recovery = 93% Analysis Date = 05/08/16 Pct Recovery = 93% Analysis Date = 05/05/16 Pct Recovery = 93% Analysis Date = 05/05/16 Pct Recovery = 93% Analysis Date = 05/03/16 Pct Recovery = 93% Analysis Date = 05/03/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 05/01/16 Pct Recovery = 93% Analysis Date = 04/28/16 Pct Recovery = 93% Analysis Date = 04/28/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/26/16 Pct Recovery = 93% Analysis Date = 04/24/16 Pct Recovery = 93% Analysis Date = 04/24/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 93% Analysis Date = 04/22/16 Pct Recovery = 93% Analysis Date = 04/19/16 Pct Recovery = 93% Analysis Date = 04/19/16 Pct Recovery = 93% Analysis Date = 04/17/16 Pct Recovery = 93% Analysis Date = 04/17/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/12/16 Pct Recovery = 93% Analysis Date = 04/12/16 Pct Recovery = 93% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/23/16 Pct Recovery = 91% Analysis Date = 03/23/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/11/16 Pct Recovery = 90% Analysis Date = 03/11/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/09/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/07/16 Pct Recovery = 89% Analysis Date = 03/05/16 Pct Recovery = 89% Analysis Date = 03/05/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/22/16 Pct Recovery = 87% Analysis Date = 02/22/16 Pct Recovery = 87% Analysis Date = 02/20/16 Pct Recovery = 87% Analysis Date = 02/20/16 Pct Recovery = 87% Analysis Date = 02/18/16 Pct Recovery = 87% Analysis Date = 02/18/16 Pct Recovery = 87% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/09/16 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2,6-DIETHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 93% 11% 92% 13%
Total 18 93% 11% 92% 13%

Sample Statistics
2,6-DIETHYLANILINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
2-CHLORO-2,6-DIETHYLACETANILIDE
METHOD: 2033 , TESTIDCODE: 61618GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 111% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 98% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 97% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 80% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 131% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 95% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 111% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 95% Analysis Date = 04/30/17 Pct Recovery = 96% Analysis Date = 04/30/17 Pct Recovery = 96% Analysis Date = 04/28/17 Pct Recovery = 97% Analysis Date = 04/28/17 Pct Recovery = 97% Analysis Date = 04/26/17 Pct Recovery = 99% Analysis Date = 04/26/17 Pct Recovery = 99% Analysis Date = 04/24/17 Pct Recovery = 100% Analysis Date = 04/24/17 Pct Recovery = 100% Analysis Date = 04/22/17 Pct Recovery = 102% Analysis Date = 04/22/17 Pct Recovery = 102% Analysis Date = 04/20/17 Pct Recovery = 103% Analysis Date = 04/20/17 Pct Recovery = 103% Analysis Date = 04/18/17 Pct Recovery = 104% Analysis Date = 04/18/17 Pct Recovery = 104% Analysis Date = 04/15/17 Pct Recovery = 106% Analysis Date = 04/15/17 Pct Recovery = 106% Analysis Date = 04/13/17 Pct Recovery = 107% Analysis Date = 04/13/17 Pct Recovery = 107% Analysis Date = 04/11/17 Pct Recovery = 109% Analysis Date = 04/11/17 Pct Recovery = 109% Analysis Date = 04/09/17 Pct Recovery = 110% Analysis Date = 04/09/17 Pct Recovery = 110% Analysis Date = 04/07/17 Pct Recovery = 111% Analysis Date = 04/07/17 Pct Recovery = 111% Analysis Date = 04/05/17 Pct Recovery = 113% Analysis Date = 04/05/17 Pct Recovery = 113% Analysis Date = 04/03/17 Pct Recovery = 114% Analysis Date = 04/03/17 Pct Recovery = 114% Analysis Date = 03/31/17 Pct Recovery = 116% Analysis Date = 03/31/17 Pct Recovery = 116% Analysis Date = 03/29/17 Pct Recovery = 117% Analysis Date = 03/29/17 Pct Recovery = 117% Analysis Date = 03/27/17 Pct Recovery = 118% Analysis Date = 03/27/17 Pct Recovery = 118% Analysis Date = 03/25/17 Pct Recovery = 120% Analysis Date = 03/25/17 Pct Recovery = 120% Analysis Date = 03/23/17 Pct Recovery = 121% Analysis Date = 03/23/17 Pct Recovery = 121% Analysis Date = 03/21/17 Pct Recovery = 123% Analysis Date = 03/21/17 Pct Recovery = 123% Analysis Date = 03/19/17 Pct Recovery = 124% Analysis Date = 03/19/17 Pct Recovery = 124% Analysis Date = 03/17/17 Pct Recovery = 125% Analysis Date = 03/17/17 Pct Recovery = 125% Analysis Date = 03/14/17 Pct Recovery = 125% Analysis Date = 03/14/17 Pct Recovery = 125% Analysis Date = 03/12/17 Pct Recovery = 122% Analysis Date = 03/12/17 Pct Recovery = 122% Analysis Date = 03/10/17 Pct Recovery = 120% Analysis Date = 03/10/17 Pct Recovery = 120% Analysis Date = 03/08/17 Pct Recovery = 117% Analysis Date = 03/08/17 Pct Recovery = 117% Analysis Date = 03/06/17 Pct Recovery = 115% Analysis Date = 03/06/17 Pct Recovery = 115% Analysis Date = 03/04/17 Pct Recovery = 112% Analysis Date = 03/04/17 Pct Recovery = 112% Analysis Date = 03/02/17 Pct Recovery = 110% Analysis Date = 03/02/17 Pct Recovery = 110% Analysis Date = 02/27/17 Pct Recovery = 107% Analysis Date = 02/27/17 Pct Recovery = 107% Analysis Date = 02/25/17 Pct Recovery = 105% Analysis Date = 02/25/17 Pct Recovery = 105% Analysis Date = 02/23/17 Pct Recovery = 102% Analysis Date = 02/23/17 Pct Recovery = 102% Analysis Date = 02/21/17 Pct Recovery = 100% Analysis Date = 02/21/17 Pct Recovery = 100% Analysis Date = 02/19/17 Pct Recovery = 98% Analysis Date = 02/19/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/15/17 Pct Recovery = 95% Analysis Date = 02/15/17 Pct Recovery = 95% Analysis Date = 02/13/17 Pct Recovery = 96% Analysis Date = 02/13/17 Pct Recovery = 96% Analysis Date = 02/10/17 Pct Recovery = 96% Analysis Date = 02/10/17 Pct Recovery = 96% Analysis Date = 02/08/17 Pct Recovery = 97% Analysis Date = 02/08/17 Pct Recovery = 97% Analysis Date = 02/06/17 Pct Recovery = 97% Analysis Date = 02/06/17 Pct Recovery = 97% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/02/17 Pct Recovery = 98% Analysis Date = 02/02/17 Pct Recovery = 98% Analysis Date = 01/31/17 Pct Recovery = 99% Analysis Date = 01/31/17 Pct Recovery = 99% Analysis Date = 01/29/17 Pct Recovery = 100% Analysis Date = 01/29/17 Pct Recovery = 100% Analysis Date = 01/26/17 Pct Recovery = 100% Analysis Date = 01/26/17 Pct Recovery = 100% Analysis Date = 01/24/17 Pct Recovery = 101% Analysis Date = 01/24/17 Pct Recovery = 101% Analysis Date = 01/22/17 Pct Recovery = 101% Analysis Date = 01/22/17 Pct Recovery = 101% Analysis Date = 01/20/17 Pct Recovery = 102% Analysis Date = 01/20/17 Pct Recovery = 102% Analysis Date = 01/18/17 Pct Recovery = 103% Analysis Date = 01/18/17 Pct Recovery = 103% Analysis Date = 01/16/17 Pct Recovery = 103% Analysis Date = 01/16/17 Pct Recovery = 103% Analysis Date = 01/14/17 Pct Recovery = 104% Analysis Date = 01/14/17 Pct Recovery = 104% Analysis Date = 01/11/17 Pct Recovery = 104% Analysis Date = 01/11/17 Pct Recovery = 104% Analysis Date = 01/09/17 Pct Recovery = 105% Analysis Date = 01/09/17 Pct Recovery = 105% Analysis Date = 01/07/17 Pct Recovery = 106% Analysis Date = 01/07/17 Pct Recovery = 106% Analysis Date = 01/05/17 Pct Recovery = 106% Analysis Date = 01/05/17 Pct Recovery = 106% Analysis Date = 01/03/17 Pct Recovery = 107% Analysis Date = 01/03/17 Pct Recovery = 107% Analysis Date = 01/01/17 Pct Recovery = 107% Analysis Date = 01/01/17 Pct Recovery = 107% Analysis Date = 12/30/16 Pct Recovery = 108% Analysis Date = 12/30/16 Pct Recovery = 108% Analysis Date = 12/28/16 Pct Recovery = 108% Analysis Date = 12/28/16 Pct Recovery = 108% Analysis Date = 12/25/16 Pct Recovery = 109% Analysis Date = 12/25/16 Pct Recovery = 109% Analysis Date = 12/23/16 Pct Recovery = 110% Analysis Date = 12/23/16 Pct Recovery = 110% Analysis Date = 12/21/16 Pct Recovery = 110% Analysis Date = 12/21/16 Pct Recovery = 110% Analysis Date = 12/19/16 Pct Recovery = 111% Analysis Date = 12/19/16 Pct Recovery = 111% Analysis Date = 12/17/16 Pct Recovery = 110% Analysis Date = 12/17/16 Pct Recovery = 110% Analysis Date = 12/15/16 Pct Recovery = 110% Analysis Date = 12/15/16 Pct Recovery = 110% Analysis Date = 12/13/16 Pct Recovery = 110% Analysis Date = 12/13/16 Pct Recovery = 110% Analysis Date = 12/10/16 Pct Recovery = 110% Analysis Date = 12/10/16 Pct Recovery = 110% Analysis Date = 12/08/16 Pct Recovery = 110% Analysis Date = 12/08/16 Pct Recovery = 110% Analysis Date = 12/06/16 Pct Recovery = 109% Analysis Date = 12/06/16 Pct Recovery = 109% Analysis Date = 12/04/16 Pct Recovery = 109% Analysis Date = 12/04/16 Pct Recovery = 109% Analysis Date = 12/02/16 Pct Recovery = 109% Analysis Date = 12/02/16 Pct Recovery = 109% Analysis Date = 11/30/16 Pct Recovery = 109% Analysis Date = 11/30/16 Pct Recovery = 109% Analysis Date = 11/28/16 Pct Recovery = 108% Analysis Date = 11/28/16 Pct Recovery = 108% Analysis Date = 11/26/16 Pct Recovery = 108% Analysis Date = 11/26/16 Pct Recovery = 108% Analysis Date = 11/23/16 Pct Recovery = 108% Analysis Date = 11/23/16 Pct Recovery = 108% Analysis Date = 11/21/16 Pct Recovery = 108% Analysis Date = 11/21/16 Pct Recovery = 108% Analysis Date = 11/19/16 Pct Recovery = 108% Analysis Date = 11/19/16 Pct Recovery = 108% Analysis Date = 11/17/16 Pct Recovery = 107% Analysis Date = 11/17/16 Pct Recovery = 107% Analysis Date = 11/15/16 Pct Recovery = 107% Analysis Date = 11/15/16 Pct Recovery = 107% Analysis Date = 11/13/16 Pct Recovery = 107% Analysis Date = 11/13/16 Pct Recovery = 107% Analysis Date = 11/11/16 Pct Recovery = 107% Analysis Date = 11/11/16 Pct Recovery = 107% Analysis Date = 11/08/16 Pct Recovery = 107% Analysis Date = 11/08/16 Pct Recovery = 107% Analysis Date = 11/06/16 Pct Recovery = 106% Analysis Date = 11/06/16 Pct Recovery = 106% Analysis Date = 11/04/16 Pct Recovery = 106% Analysis Date = 11/04/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/31/16 Pct Recovery = 106% Analysis Date = 10/31/16 Pct Recovery = 106% Analysis Date = 10/29/16 Pct Recovery = 105% Analysis Date = 10/29/16 Pct Recovery = 105% Analysis Date = 10/27/16 Pct Recovery = 105% Analysis Date = 10/27/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/24/16 Pct Recovery = 105% Analysis Date = 10/22/16 Pct Recovery = 105% Analysis Date = 10/22/16 Pct Recovery = 105% Analysis Date = 10/20/16 Pct Recovery = 105% Analysis Date = 10/20/16 Pct Recovery = 105% Analysis Date = 10/18/16 Pct Recovery = 104% Analysis Date = 10/18/16 Pct Recovery = 104% Analysis Date = 10/16/16 Pct Recovery = 104% Analysis Date = 10/16/16 Pct Recovery = 104% Analysis Date = 10/14/16 Pct Recovery = 104% Analysis Date = 10/14/16 Pct Recovery = 104% Analysis Date = 10/12/16 Pct Recovery = 104% Analysis Date = 10/12/16 Pct Recovery = 104% Analysis Date = 10/10/16 Pct Recovery = 103% Analysis Date = 10/10/16 Pct Recovery = 103% Analysis Date = 10/07/16 Pct Recovery = 103% Analysis Date = 10/07/16 Pct Recovery = 103% Analysis Date = 10/05/16 Pct Recovery = 103% Analysis Date = 10/05/16 Pct Recovery = 103% Analysis Date = 10/03/16 Pct Recovery = 103% Analysis Date = 10/03/16 Pct Recovery = 103% Analysis Date = 10/01/16 Pct Recovery = 103% Analysis Date = 10/01/16 Pct Recovery = 103% Analysis Date = 09/29/16 Pct Recovery = 102% Analysis Date = 09/29/16 Pct Recovery = 102% Analysis Date = 09/27/16 Pct Recovery = 102% Analysis Date = 09/27/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/25/16 Pct Recovery = 102% Analysis Date = 09/22/16 Pct Recovery = 102% Analysis Date = 09/22/16 Pct Recovery = 102% Analysis Date = 09/20/16 Pct Recovery = 102% Analysis Date = 09/20/16 Pct Recovery = 102% Analysis Date = 09/18/16 Pct Recovery = 101% Analysis Date = 09/18/16 Pct Recovery = 101% Analysis Date = 09/16/16 Pct Recovery = 101% Analysis Date = 09/16/16 Pct Recovery = 101% Analysis Date = 09/14/16 Pct Recovery = 101% Analysis Date = 09/14/16 Pct Recovery = 101% Analysis Date = 09/12/16 Pct Recovery = 101% Analysis Date = 09/12/16 Pct Recovery = 101% Analysis Date = 09/10/16 Pct Recovery = 100% Analysis Date = 09/10/16 Pct Recovery = 100% Analysis Date = 09/08/16 Pct Recovery = 100% Analysis Date = 09/08/16 Pct Recovery = 100% Analysis Date = 09/05/16 Pct Recovery = 100% Analysis Date = 09/05/16 Pct Recovery = 100% Analysis Date = 09/03/16 Pct Recovery = 100% Analysis Date = 09/03/16 Pct Recovery = 100% Analysis Date = 09/01/16 Pct Recovery = 100% Analysis Date = 09/01/16 Pct Recovery = 100% Analysis Date = 08/30/16 Pct Recovery = 99% Analysis Date = 08/30/16 Pct Recovery = 99% Analysis Date = 08/28/16 Pct Recovery = 99% Analysis Date = 08/28/16 Pct Recovery = 99% Analysis Date = 08/26/16 Pct Recovery = 99% Analysis Date = 08/26/16 Pct Recovery = 99% Analysis Date = 08/24/16 Pct Recovery = 99% Analysis Date = 08/24/16 Pct Recovery = 99% Analysis Date = 08/21/16 Pct Recovery = 99% Analysis Date = 08/21/16 Pct Recovery = 99% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/19/16 Pct Recovery = 98% Analysis Date = 08/17/16 Pct Recovery = 98% Analysis Date = 08/17/16 Pct Recovery = 98% Analysis Date = 08/15/16 Pct Recovery = 98% Analysis Date = 08/15/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/13/16 Pct Recovery = 98% Analysis Date = 08/11/16 Pct Recovery = 97% Analysis Date = 08/11/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/06/16 Pct Recovery = 97% Analysis Date = 08/06/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 08/04/16 Pct Recovery = 97% Analysis Date = 08/02/16 Pct Recovery = 97% Analysis Date = 08/02/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 96% Analysis Date = 07/29/16 Pct Recovery = 96% Analysis Date = 07/29/16 Pct Recovery = 96% Analysis Date = 07/27/16 Pct Recovery = 96% Analysis Date = 07/27/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/23/16 Pct Recovery = 95% Analysis Date = 07/23/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/20/16 Pct Recovery = 95% Analysis Date = 07/18/16 Pct Recovery = 95% Analysis Date = 07/18/16 Pct Recovery = 95% Analysis Date = 07/16/16 Pct Recovery = 95% Analysis Date = 07/16/16 Pct Recovery = 95% Analysis Date = 07/14/16 Pct Recovery = 95% Analysis Date = 07/14/16 Pct Recovery = 95% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/08/16 Pct Recovery = 94% Analysis Date = 07/08/16 Pct Recovery = 94% Analysis Date = 07/05/16 Pct Recovery = 94% Analysis Date = 07/05/16 Pct Recovery = 94% Analysis Date = 07/03/16 Pct Recovery = 94% Analysis Date = 07/03/16 Pct Recovery = 94% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/23/16 Pct Recovery = 92% Analysis Date = 06/23/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/21/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 92% Analysis Date = 06/14/16 Pct Recovery = 92% Analysis Date = 06/12/16 Pct Recovery = 91% Analysis Date = 06/12/16 Pct Recovery = 91% Analysis Date = 06/10/16 Pct Recovery = 91% Analysis Date = 06/10/16 Pct Recovery = 91% Analysis Date = 06/08/16 Pct Recovery = 91% Analysis Date = 06/08/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/03/16 Pct Recovery = 90% Analysis Date = 06/03/16 Pct Recovery = 90% Analysis Date = 06/01/16 Pct Recovery = 90% Analysis Date = 06/01/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 89% Analysis Date = 05/24/16 Pct Recovery = 89% Analysis Date = 05/22/16 Pct Recovery = 89% Analysis Date = 05/22/16 Pct Recovery = 89% Analysis Date = 05/19/16 Pct Recovery = 89% Analysis Date = 05/19/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/13/16 Pct Recovery = 88% Analysis Date = 05/13/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 88% Analysis Date = 05/11/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/09/16 Pct Recovery = 88% Analysis Date = 05/07/16 Pct Recovery = 88% Analysis Date = 05/07/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/02/16 Pct Recovery = 87% Analysis Date = 05/02/16 Pct Recovery = 87% Analysis Date = 04/30/16 Pct Recovery = 87% Analysis Date = 04/30/16 Pct Recovery = 87% Analysis Date = 04/28/16 Pct Recovery = 87% Analysis Date = 04/28/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/20/16 Pct Recovery = 86% Analysis Date = 04/20/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/13/16 Pct Recovery = 86% Analysis Date = 04/11/16 Pct Recovery = 85% Analysis Date = 04/11/16 Pct Recovery = 85% Analysis Date = 04/09/16 Pct Recovery = 85% Analysis Date = 04/09/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/29/16 Pct Recovery = 84% Analysis Date = 03/29/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/19/16 Pct Recovery = 83% Analysis Date = 03/16/16 Pct Recovery = 83% Analysis Date = 03/16/16 Pct Recovery = 83% Analysis Date = 03/14/16 Pct Recovery = 83% Analysis Date = 03/14/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/10/16 Pct Recovery = 83% Analysis Date = 03/10/16 Pct Recovery = 83% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 82% Analysis Date = 03/04/16 Pct Recovery = 82% Analysis Date = 03/04/16 Pct Recovery = 82% Analysis Date = 03/02/16 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 11 98% 15% 95% 19%
Total 11 98% 15% 95% 19%

Sample Statistics
2-CHLORO-2,6-DIETHYLACETANILIDE

Characteristic N % % Basis
Plotted 11 92% Spiked
Estimated Values 1 8% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 8% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 12
Not Spiked 16 .  
False Positives 0 0% 0 out of 16

OBSP Determination:
2-ETHYL-6-METHYLANILINE
METHOD: 2033 , TESTIDCODE: 61620GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 95% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 105% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 85% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 74% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 81% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 90% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 86% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 84% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 99% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 83% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 94% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 87% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 73% Analysis Date = 05/10/17 Pct Recovery = 78% Analysis Date = 05/08/17 Pct Recovery = 79% Analysis Date = 05/08/17 Pct Recovery = 79% Analysis Date = 05/06/17 Pct Recovery = 79% Analysis Date = 05/06/17 Pct Recovery = 79% Analysis Date = 05/04/17 Pct Recovery = 80% Analysis Date = 05/04/17 Pct Recovery = 80% Analysis Date = 05/01/17 Pct Recovery = 80% Analysis Date = 05/01/17 Pct Recovery = 80% Analysis Date = 04/29/17 Pct Recovery = 80% Analysis Date = 04/29/17 Pct Recovery = 80% Analysis Date = 04/27/17 Pct Recovery = 81% Analysis Date = 04/27/17 Pct Recovery = 81% Analysis Date = 04/25/17 Pct Recovery = 81% Analysis Date = 04/25/17 Pct Recovery = 81% Analysis Date = 04/22/17 Pct Recovery = 82% Analysis Date = 04/22/17 Pct Recovery = 82% Analysis Date = 04/20/17 Pct Recovery = 82% Analysis Date = 04/20/17 Pct Recovery = 82% Analysis Date = 04/18/17 Pct Recovery = 82% Analysis Date = 04/18/17 Pct Recovery = 82% Analysis Date = 04/15/17 Pct Recovery = 83% Analysis Date = 04/15/17 Pct Recovery = 83% Analysis Date = 04/13/17 Pct Recovery = 83% Analysis Date = 04/13/17 Pct Recovery = 83% Analysis Date = 04/11/17 Pct Recovery = 83% Analysis Date = 04/11/17 Pct Recovery = 83% Analysis Date = 04/09/17 Pct Recovery = 84% Analysis Date = 04/09/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/04/17 Pct Recovery = 85% Analysis Date = 04/04/17 Pct Recovery = 85% Analysis Date = 04/02/17 Pct Recovery = 85% Analysis Date = 04/02/17 Pct Recovery = 85% Analysis Date = 03/30/17 Pct Recovery = 85% Analysis Date = 03/30/17 Pct Recovery = 85% Analysis Date = 03/28/17 Pct Recovery = 86% Analysis Date = 03/28/17 Pct Recovery = 86% Analysis Date = 03/26/17 Pct Recovery = 86% Analysis Date = 03/26/17 Pct Recovery = 86% Analysis Date = 03/24/17 Pct Recovery = 87% Analysis Date = 03/24/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/19/17 Pct Recovery = 87% Analysis Date = 03/19/17 Pct Recovery = 87% Analysis Date = 03/17/17 Pct Recovery = 88% Analysis Date = 03/17/17 Pct Recovery = 88% Analysis Date = 03/14/17 Pct Recovery = 88% Analysis Date = 03/14/17 Pct Recovery = 88% Analysis Date = 03/12/17 Pct Recovery = 88% Analysis Date = 03/12/17 Pct Recovery = 88% Analysis Date = 03/10/17 Pct Recovery = 89% Analysis Date = 03/10/17 Pct Recovery = 89% Analysis Date = 03/08/17 Pct Recovery = 89% Analysis Date = 03/08/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 91% Analysis Date = 02/24/17 Pct Recovery = 91% Analysis Date = 02/22/17 Pct Recovery = 91% Analysis Date = 02/22/17 Pct Recovery = 91% Analysis Date = 02/20/17 Pct Recovery = 91% Analysis Date = 02/20/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 92% Analysis Date = 02/15/17 Pct Recovery = 92% Analysis Date = 02/13/17 Pct Recovery = 92% Analysis Date = 02/13/17 Pct Recovery = 92% Analysis Date = 02/10/17 Pct Recovery = 92% Analysis Date = 02/10/17 Pct Recovery = 92% Analysis Date = 02/08/17 Pct Recovery = 92% Analysis Date = 02/08/17 Pct Recovery = 92% Analysis Date = 02/06/17 Pct Recovery = 92% Analysis Date = 02/06/17 Pct Recovery = 92% Analysis Date = 02/04/17 Pct Recovery = 93% Analysis Date = 02/04/17 Pct Recovery = 93% Analysis Date = 02/01/17 Pct Recovery = 93% Analysis Date = 02/01/17 Pct Recovery = 93% Analysis Date = 01/30/17 Pct Recovery = 93% Analysis Date = 01/30/17 Pct Recovery = 93% Analysis Date = 01/28/17 Pct Recovery = 93% Analysis Date = 01/28/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/23/17 Pct Recovery = 93% Analysis Date = 01/23/17 Pct Recovery = 93% Analysis Date = 01/21/17 Pct Recovery = 94% Analysis Date = 01/21/17 Pct Recovery = 94% Analysis Date = 01/19/17 Pct Recovery = 94% Analysis Date = 01/19/17 Pct Recovery = 94% Analysis Date = 01/16/17 Pct Recovery = 94% Analysis Date = 01/16/17 Pct Recovery = 94% Analysis Date = 01/14/17 Pct Recovery = 94% Analysis Date = 01/14/17 Pct Recovery = 94% Analysis Date = 01/12/17 Pct Recovery = 93% Analysis Date = 01/12/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 92% Analysis Date = 12/22/16 Pct Recovery = 91% Analysis Date = 12/22/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 11/29/16 Pct Recovery = 89% Analysis Date = 11/29/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/27/16 Pct Recovery = 89% Analysis Date = 11/25/16 Pct Recovery = 89% Analysis Date = 11/25/16 Pct Recovery = 89% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/22/16 Pct Recovery = 88% Analysis Date = 11/20/16 Pct Recovery = 88% Analysis Date = 11/20/16 Pct Recovery = 88% Analysis Date = 11/18/16 Pct Recovery = 88% Analysis Date = 11/18/16 Pct Recovery = 88% Analysis Date = 11/16/16 Pct Recovery = 88% Analysis Date = 11/16/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/11/16 Pct Recovery = 87% Analysis Date = 11/11/16 Pct Recovery = 87% Analysis Date = 11/09/16 Pct Recovery = 87% Analysis Date = 11/09/16 Pct Recovery = 87% Analysis Date = 11/06/16 Pct Recovery = 87% Analysis Date = 11/06/16 Pct Recovery = 87% Analysis Date = 11/04/16 Pct Recovery = 87% Analysis Date = 11/04/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/28/16 Pct Recovery = 86% Analysis Date = 10/28/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 85% Analysis Date = 10/24/16 Pct Recovery = 85% Analysis Date = 10/21/16 Pct Recovery = 85% Analysis Date = 10/21/16 Pct Recovery = 85% Analysis Date = 10/19/16 Pct Recovery = 85% Analysis Date = 10/19/16 Pct Recovery = 85% Analysis Date = 10/17/16 Pct Recovery = 85% Analysis Date = 10/17/16 Pct Recovery = 85% Analysis Date = 10/15/16 Pct Recovery = 85% Analysis Date = 10/15/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/08/16 Pct Recovery = 84% Analysis Date = 10/08/16 Pct Recovery = 84% Analysis Date = 10/05/16 Pct Recovery = 84% Analysis Date = 10/05/16 Pct Recovery = 84% Analysis Date = 10/03/16 Pct Recovery = 83% Analysis Date = 10/03/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/24/16 Pct Recovery = 83% Analysis Date = 09/24/16 Pct Recovery = 83% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/10/16 Pct Recovery = 81% Analysis Date = 09/08/16 Pct Recovery = 81% Analysis Date = 09/08/16 Pct Recovery = 81% Analysis Date = 09/06/16 Pct Recovery = 81% Analysis Date = 09/06/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 08/30/16 Pct Recovery = 81% Analysis Date = 08/30/16 Pct Recovery = 81% Analysis Date = 08/28/16 Pct Recovery = 81% Analysis Date = 08/28/16 Pct Recovery = 81% Analysis Date = 08/25/16 Pct Recovery = 81% Analysis Date = 08/25/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 82% Analysis Date = 08/18/16 Pct Recovery = 82% Analysis Date = 08/18/16 Pct Recovery = 82% Analysis Date = 08/16/16 Pct Recovery = 82% Analysis Date = 08/16/16 Pct Recovery = 82% Analysis Date = 08/14/16 Pct Recovery = 82% Analysis Date = 08/14/16 Pct Recovery = 82% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 83% Analysis Date = 08/05/16 Pct Recovery = 83% Analysis Date = 08/02/16 Pct Recovery = 83% Analysis Date = 08/02/16 Pct Recovery = 83% Analysis Date = 07/31/16 Pct Recovery = 83% Analysis Date = 07/31/16 Pct Recovery = 83% Analysis Date = 07/29/16 Pct Recovery = 83% Analysis Date = 07/29/16 Pct Recovery = 83% Analysis Date = 07/27/16 Pct Recovery = 83% Analysis Date = 07/27/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/22/16 Pct Recovery = 83% Analysis Date = 07/22/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 84% Analysis Date = 07/15/16 Pct Recovery = 84% Analysis Date = 07/15/16 Pct Recovery = 84% Analysis Date = 07/13/16 Pct Recovery = 84% Analysis Date = 07/13/16 Pct Recovery = 84% Analysis Date = 07/11/16 Pct Recovery = 84% Analysis Date = 07/11/16 Pct Recovery = 84% Analysis Date = 07/08/16 Pct Recovery = 84% Analysis Date = 07/08/16 Pct Recovery = 84% Analysis Date = 07/06/16 Pct Recovery = 84% Analysis Date = 07/06/16 Pct Recovery = 84% Analysis Date = 07/04/16 Pct Recovery = 84% Analysis Date = 07/04/16 Pct Recovery = 84% Analysis Date = 07/01/16 Pct Recovery = 84% Analysis Date = 07/01/16 Pct Recovery = 84% Analysis Date = 06/29/16 Pct Recovery = 85% Analysis Date = 06/29/16 Pct Recovery = 85% Analysis Date = 06/27/16 Pct Recovery = 85% Analysis Date = 06/27/16 Pct Recovery = 85% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/15/16 Pct Recovery = 85% Analysis Date = 06/15/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/30/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/28/16 Pct Recovery = 86% Analysis Date = 05/26/16 Pct Recovery = 86% Analysis Date = 05/26/16 Pct Recovery = 86% Analysis Date = 05/24/16 Pct Recovery = 87% Analysis Date = 05/24/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/03/16 Pct Recovery = 88% Analysis Date = 05/03/16 Pct Recovery = 88% Analysis Date = 05/01/16 Pct Recovery = 88% Analysis Date = 05/01/16 Pct Recovery = 88% Analysis Date = 04/28/16 Pct Recovery = 87% Analysis Date = 04/28/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/26/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/24/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/22/16 Pct Recovery = 87% Analysis Date = 04/19/16 Pct Recovery = 87% Analysis Date = 04/19/16 Pct Recovery = 87% Analysis Date = 04/17/16 Pct Recovery = 87% Analysis Date = 04/17/16 Pct Recovery = 87% Analysis Date = 04/15/16 Pct Recovery = 87% Analysis Date = 04/15/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/08/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/01/16 Pct Recovery = 86% Analysis Date = 04/01/16 Pct Recovery = 86% Analysis Date = 03/30/16 Pct Recovery = 86% Analysis Date = 03/30/16 Pct Recovery = 86% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 84% Analysis Date = 03/21/16 Pct Recovery = 84% Analysis Date = 03/18/16 Pct Recovery = 84% Analysis Date = 03/18/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/11/16 Pct Recovery = 83% Analysis Date = 03/11/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 82% Analysis Date = 03/02/16 Pct Recovery = 82% Analysis Date = 02/29/16 Pct Recovery = 82% Analysis Date = 02/29/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/24/16 Pct Recovery = 82% Analysis Date = 02/24/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 81% Analysis Date = 02/22/16 Pct Recovery = 81% Analysis Date = 02/20/16 Pct Recovery = 81% Analysis Date = 02/20/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 81% Analysis Date = 02/15/16 Pct Recovery = 81% Analysis Date = 02/15/16 Pct Recovery = 81% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 80% Analysis Date = 02/09/16 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
2-ETHYL-6-METHYLANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 86% 9% 85% 11%
Total 19 86% 9% 85% 11%

Sample Statistics
2-ETHYL-6-METHYLANILINE

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
3,4-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61625GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 92% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 66% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 67% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 51% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 70% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 89% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 80% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 79% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 65% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 74% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 75% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 05/02/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 69% Analysis Date = 04/28/17 Pct Recovery = 69% Analysis Date = 04/28/17 Pct Recovery = 69% Analysis Date = 04/26/17 Pct Recovery = 69% Analysis Date = 04/26/17 Pct Recovery = 69% Analysis Date = 04/24/17 Pct Recovery = 70% Analysis Date = 04/24/17 Pct Recovery = 70% Analysis Date = 04/22/17 Pct Recovery = 70% Analysis Date = 04/22/17 Pct Recovery = 70% Analysis Date = 04/20/17 Pct Recovery = 70% Analysis Date = 04/20/17 Pct Recovery = 70% Analysis Date = 04/18/17 Pct Recovery = 70% Analysis Date = 04/18/17 Pct Recovery = 70% Analysis Date = 04/15/17 Pct Recovery = 71% Analysis Date = 04/15/17 Pct Recovery = 71% Analysis Date = 04/13/17 Pct Recovery = 71% Analysis Date = 04/13/17 Pct Recovery = 71% Analysis Date = 04/11/17 Pct Recovery = 71% Analysis Date = 04/11/17 Pct Recovery = 71% Analysis Date = 04/09/17 Pct Recovery = 72% Analysis Date = 04/09/17 Pct Recovery = 72% Analysis Date = 04/07/17 Pct Recovery = 72% Analysis Date = 04/07/17 Pct Recovery = 72% Analysis Date = 04/05/17 Pct Recovery = 72% Analysis Date = 04/05/17 Pct Recovery = 72% Analysis Date = 04/03/17 Pct Recovery = 72% Analysis Date = 04/03/17 Pct Recovery = 72% Analysis Date = 03/31/17 Pct Recovery = 73% Analysis Date = 03/31/17 Pct Recovery = 73% Analysis Date = 03/29/17 Pct Recovery = 73% Analysis Date = 03/29/17 Pct Recovery = 73% Analysis Date = 03/27/17 Pct Recovery = 73% Analysis Date = 03/27/17 Pct Recovery = 73% Analysis Date = 03/25/17 Pct Recovery = 73% Analysis Date = 03/25/17 Pct Recovery = 73% Analysis Date = 03/23/17 Pct Recovery = 74% Analysis Date = 03/23/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 75% Analysis Date = 03/17/17 Pct Recovery = 75% Analysis Date = 03/14/17 Pct Recovery = 75% Analysis Date = 03/14/17 Pct Recovery = 75% Analysis Date = 03/12/17 Pct Recovery = 75% Analysis Date = 03/12/17 Pct Recovery = 75% Analysis Date = 03/10/17 Pct Recovery = 75% Analysis Date = 03/10/17 Pct Recovery = 75% Analysis Date = 03/08/17 Pct Recovery = 76% Analysis Date = 03/08/17 Pct Recovery = 76% Analysis Date = 03/06/17 Pct Recovery = 76% Analysis Date = 03/06/17 Pct Recovery = 76% Analysis Date = 03/04/17 Pct Recovery = 76% Analysis Date = 03/04/17 Pct Recovery = 76% Analysis Date = 03/02/17 Pct Recovery = 77% Analysis Date = 03/02/17 Pct Recovery = 77% Analysis Date = 02/27/17 Pct Recovery = 77% Analysis Date = 02/27/17 Pct Recovery = 77% Analysis Date = 02/25/17 Pct Recovery = 77% Analysis Date = 02/25/17 Pct Recovery = 77% Analysis Date = 02/23/17 Pct Recovery = 77% Analysis Date = 02/23/17 Pct Recovery = 77% Analysis Date = 02/21/17 Pct Recovery = 78% Analysis Date = 02/21/17 Pct Recovery = 78% Analysis Date = 02/19/17 Pct Recovery = 78% Analysis Date = 02/19/17 Pct Recovery = 78% Analysis Date = 02/17/17 Pct Recovery = 78% Analysis Date = 02/17/17 Pct Recovery = 78% Analysis Date = 02/15/17 Pct Recovery = 79% Analysis Date = 02/15/17 Pct Recovery = 79% Analysis Date = 02/13/17 Pct Recovery = 79% Analysis Date = 02/13/17 Pct Recovery = 79% Analysis Date = 02/10/17 Pct Recovery = 79% Analysis Date = 02/10/17 Pct Recovery = 79% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/04/17 Pct Recovery = 80% Analysis Date = 02/04/17 Pct Recovery = 80% Analysis Date = 02/02/17 Pct Recovery = 80% Analysis Date = 02/02/17 Pct Recovery = 80% Analysis Date = 01/31/17 Pct Recovery = 80% Analysis Date = 01/31/17 Pct Recovery = 80% Analysis Date = 01/29/17 Pct Recovery = 80% Analysis Date = 01/29/17 Pct Recovery = 80% Analysis Date = 01/26/17 Pct Recovery = 81% Analysis Date = 01/26/17 Pct Recovery = 81% Analysis Date = 01/24/17 Pct Recovery = 81% Analysis Date = 01/24/17 Pct Recovery = 81% Analysis Date = 01/22/17 Pct Recovery = 81% Analysis Date = 01/22/17 Pct Recovery = 81% Analysis Date = 01/20/17 Pct Recovery = 81% Analysis Date = 01/20/17 Pct Recovery = 81% Analysis Date = 01/18/17 Pct Recovery = 82% Analysis Date = 01/18/17 Pct Recovery = 82% Analysis Date = 01/16/17 Pct Recovery = 82% Analysis Date = 01/16/17 Pct Recovery = 82% Analysis Date = 01/14/17 Pct Recovery = 82% Analysis Date = 01/14/17 Pct Recovery = 82% Analysis Date = 01/11/17 Pct Recovery = 82% Analysis Date = 01/11/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/05/17 Pct Recovery = 83% Analysis Date = 01/05/17 Pct Recovery = 83% Analysis Date = 01/03/17 Pct Recovery = 83% Analysis Date = 01/03/17 Pct Recovery = 83% Analysis Date = 01/01/17 Pct Recovery = 83% Analysis Date = 01/01/17 Pct Recovery = 83% Analysis Date = 12/30/16 Pct Recovery = 84% Analysis Date = 12/30/16 Pct Recovery = 84% Analysis Date = 12/28/16 Pct Recovery = 84% Analysis Date = 12/28/16 Pct Recovery = 84% Analysis Date = 12/25/16 Pct Recovery = 84% Analysis Date = 12/25/16 Pct Recovery = 84% Analysis Date = 12/23/16 Pct Recovery = 84% Analysis Date = 12/23/16 Pct Recovery = 84% Analysis Date = 12/21/16 Pct Recovery = 85% Analysis Date = 12/21/16 Pct Recovery = 85% Analysis Date = 12/19/16 Pct Recovery = 85% Analysis Date = 12/19/16 Pct Recovery = 85% Analysis Date = 12/17/16 Pct Recovery = 84% Analysis Date = 12/17/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 84% Analysis Date = 12/13/16 Pct Recovery = 84% Analysis Date = 12/13/16 Pct Recovery = 84% Analysis Date = 12/10/16 Pct Recovery = 83% Analysis Date = 12/10/16 Pct Recovery = 83% Analysis Date = 12/08/16 Pct Recovery = 83% Analysis Date = 12/08/16 Pct Recovery = 83% Analysis Date = 12/06/16 Pct Recovery = 83% Analysis Date = 12/06/16 Pct Recovery = 83% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 82% Analysis Date = 11/30/16 Pct Recovery = 82% Analysis Date = 11/30/16 Pct Recovery = 82% Analysis Date = 11/28/16 Pct Recovery = 81% Analysis Date = 11/28/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/23/16 Pct Recovery = 81% Analysis Date = 11/23/16 Pct Recovery = 81% Analysis Date = 11/21/16 Pct Recovery = 81% Analysis Date = 11/21/16 Pct Recovery = 81% Analysis Date = 11/19/16 Pct Recovery = 80% Analysis Date = 11/19/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 79% Analysis Date = 11/13/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/11/16 Pct Recovery = 79% Analysis Date = 11/08/16 Pct Recovery = 79% Analysis Date = 11/08/16 Pct Recovery = 79% Analysis Date = 11/06/16 Pct Recovery = 78% Analysis Date = 11/06/16 Pct Recovery = 78% Analysis Date = 11/04/16 Pct Recovery = 78% Analysis Date = 11/04/16 Pct Recovery = 78% Analysis Date = 11/02/16 Pct Recovery = 78% Analysis Date = 11/02/16 Pct Recovery = 78% Analysis Date = 10/31/16 Pct Recovery = 77% Analysis Date = 10/31/16 Pct Recovery = 77% Analysis Date = 10/29/16 Pct Recovery = 77% Analysis Date = 10/29/16 Pct Recovery = 77% Analysis Date = 10/27/16 Pct Recovery = 77% Analysis Date = 10/27/16 Pct Recovery = 77% Analysis Date = 10/24/16 Pct Recovery = 76% Analysis Date = 10/24/16 Pct Recovery = 76% Analysis Date = 10/22/16 Pct Recovery = 76% Analysis Date = 10/22/16 Pct Recovery = 76% Analysis Date = 10/20/16 Pct Recovery = 76% Analysis Date = 10/20/16 Pct Recovery = 76% Analysis Date = 10/18/16 Pct Recovery = 75% Analysis Date = 10/18/16 Pct Recovery = 75% Analysis Date = 10/16/16 Pct Recovery = 75% Analysis Date = 10/16/16 Pct Recovery = 75% Analysis Date = 10/14/16 Pct Recovery = 75% Analysis Date = 10/14/16 Pct Recovery = 75% Analysis Date = 10/12/16 Pct Recovery = 74% Analysis Date = 10/12/16 Pct Recovery = 74% Analysis Date = 10/10/16 Pct Recovery = 74% Analysis Date = 10/10/16 Pct Recovery = 74% Analysis Date = 10/07/16 Pct Recovery = 74% Analysis Date = 10/07/16 Pct Recovery = 74% Analysis Date = 10/05/16 Pct Recovery = 74% Analysis Date = 10/05/16 Pct Recovery = 74% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/01/16 Pct Recovery = 73% Analysis Date = 10/01/16 Pct Recovery = 73% Analysis Date = 09/29/16 Pct Recovery = 73% Analysis Date = 09/29/16 Pct Recovery = 73% Analysis Date = 09/27/16 Pct Recovery = 72% Analysis Date = 09/27/16 Pct Recovery = 72% Analysis Date = 09/25/16 Pct Recovery = 72% Analysis Date = 09/25/16 Pct Recovery = 72% Analysis Date = 09/22/16 Pct Recovery = 72% Analysis Date = 09/22/16 Pct Recovery = 72% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/20/16 Pct Recovery = 71% Analysis Date = 09/18/16 Pct Recovery = 71% Analysis Date = 09/18/16 Pct Recovery = 71% Analysis Date = 09/16/16 Pct Recovery = 71% Analysis Date = 09/16/16 Pct Recovery = 71% Analysis Date = 09/14/16 Pct Recovery = 70% Analysis Date = 09/14/16 Pct Recovery = 70% Analysis Date = 09/12/16 Pct Recovery = 70% Analysis Date = 09/12/16 Pct Recovery = 70% Analysis Date = 09/10/16 Pct Recovery = 70% Analysis Date = 09/10/16 Pct Recovery = 70% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 09/08/16 Pct Recovery = 69% Analysis Date = 09/05/16 Pct Recovery = 69% Analysis Date = 09/05/16 Pct Recovery = 69% Analysis Date = 09/03/16 Pct Recovery = 69% Analysis Date = 09/03/16 Pct Recovery = 69% Analysis Date = 09/01/16 Pct Recovery = 68% Analysis Date = 09/01/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 68% Analysis Date = 08/28/16 Pct Recovery = 68% Analysis Date = 08/28/16 Pct Recovery = 68% Analysis Date = 08/26/16 Pct Recovery = 69% Analysis Date = 08/26/16 Pct Recovery = 69% Analysis Date = 08/24/16 Pct Recovery = 69% Analysis Date = 08/24/16 Pct Recovery = 69% Analysis Date = 08/21/16 Pct Recovery = 69% Analysis Date = 08/21/16 Pct Recovery = 69% Analysis Date = 08/19/16 Pct Recovery = 69% Analysis Date = 08/19/16 Pct Recovery = 69% Analysis Date = 08/17/16 Pct Recovery = 69% Analysis Date = 08/17/16 Pct Recovery = 69% Analysis Date = 08/15/16 Pct Recovery = 69% Analysis Date = 08/15/16 Pct Recovery = 69% Analysis Date = 08/13/16 Pct Recovery = 69% Analysis Date = 08/13/16 Pct Recovery = 69% Analysis Date = 08/11/16 Pct Recovery = 69% Analysis Date = 08/11/16 Pct Recovery = 69% Analysis Date = 08/09/16 Pct Recovery = 69% Analysis Date = 08/09/16 Pct Recovery = 69% Analysis Date = 08/06/16 Pct Recovery = 69% Analysis Date = 08/06/16 Pct Recovery = 69% Analysis Date = 08/04/16 Pct Recovery = 69% Analysis Date = 08/04/16 Pct Recovery = 69% Analysis Date = 08/02/16 Pct Recovery = 69% Analysis Date = 08/02/16 Pct Recovery = 69% Analysis Date = 07/31/16 Pct Recovery = 70% Analysis Date = 07/31/16 Pct Recovery = 70% Analysis Date = 07/29/16 Pct Recovery = 70% Analysis Date = 07/29/16 Pct Recovery = 70% Analysis Date = 07/27/16 Pct Recovery = 70% Analysis Date = 07/27/16 Pct Recovery = 70% Analysis Date = 07/25/16 Pct Recovery = 70% Analysis Date = 07/25/16 Pct Recovery = 70% Analysis Date = 07/23/16 Pct Recovery = 70% Analysis Date = 07/23/16 Pct Recovery = 70% Analysis Date = 07/20/16 Pct Recovery = 70% Analysis Date = 07/20/16 Pct Recovery = 70% Analysis Date = 07/18/16 Pct Recovery = 70% Analysis Date = 07/18/16 Pct Recovery = 70% Analysis Date = 07/16/16 Pct Recovery = 70% Analysis Date = 07/16/16 Pct Recovery = 70% Analysis Date = 07/14/16 Pct Recovery = 70% Analysis Date = 07/14/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 70% Analysis Date = 07/10/16 Pct Recovery = 70% Analysis Date = 07/10/16 Pct Recovery = 70% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/05/16 Pct Recovery = 71% Analysis Date = 07/05/16 Pct Recovery = 71% Analysis Date = 07/03/16 Pct Recovery = 71% Analysis Date = 07/03/16 Pct Recovery = 71% Analysis Date = 07/01/16 Pct Recovery = 71% Analysis Date = 07/01/16 Pct Recovery = 71% Analysis Date = 06/29/16 Pct Recovery = 71% Analysis Date = 06/29/16 Pct Recovery = 71% Analysis Date = 06/27/16 Pct Recovery = 71% Analysis Date = 06/27/16 Pct Recovery = 71% Analysis Date = 06/25/16 Pct Recovery = 71% Analysis Date = 06/25/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/21/16 Pct Recovery = 71% Analysis Date = 06/21/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/18/16 Pct Recovery = 71% Analysis Date = 06/16/16 Pct Recovery = 71% Analysis Date = 06/16/16 Pct Recovery = 71% Analysis Date = 06/14/16 Pct Recovery = 71% Analysis Date = 06/14/16 Pct Recovery = 71% Analysis Date = 06/12/16 Pct Recovery = 72% Analysis Date = 06/12/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/06/16 Pct Recovery = 72% Analysis Date = 06/06/16 Pct Recovery = 72% Analysis Date = 06/03/16 Pct Recovery = 72% Analysis Date = 06/03/16 Pct Recovery = 72% Analysis Date = 06/01/16 Pct Recovery = 72% Analysis Date = 06/01/16 Pct Recovery = 72% Analysis Date = 05/30/16 Pct Recovery = 72% Analysis Date = 05/30/16 Pct Recovery = 72% Analysis Date = 05/28/16 Pct Recovery = 72% Analysis Date = 05/28/16 Pct Recovery = 72% Analysis Date = 05/26/16 Pct Recovery = 72% Analysis Date = 05/26/16 Pct Recovery = 72% Analysis Date = 05/24/16 Pct Recovery = 72% Analysis Date = 05/24/16 Pct Recovery = 72% Analysis Date = 05/22/16 Pct Recovery = 73% Analysis Date = 05/22/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/15/16 Pct Recovery = 73% Analysis Date = 05/15/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/11/16 Pct Recovery = 73% Analysis Date = 05/11/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/09/16 Pct Recovery = 73% Analysis Date = 05/07/16 Pct Recovery = 73% Analysis Date = 05/07/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 04/30/16 Pct Recovery = 73% Analysis Date = 04/30/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/26/16 Pct Recovery = 73% Analysis Date = 04/26/16 Pct Recovery = 73% Analysis Date = 04/24/16 Pct Recovery = 73% Analysis Date = 04/24/16 Pct Recovery = 73% Analysis Date = 04/22/16 Pct Recovery = 73% Analysis Date = 04/22/16 Pct Recovery = 73% Analysis Date = 04/20/16 Pct Recovery = 73% Analysis Date = 04/20/16 Pct Recovery = 73% Analysis Date = 04/17/16 Pct Recovery = 73% Analysis Date = 04/17/16 Pct Recovery = 73% Analysis Date = 04/15/16 Pct Recovery = 73% Analysis Date = 04/15/16 Pct Recovery = 73% Analysis Date = 04/13/16 Pct Recovery = 73% Analysis Date = 04/13/16 Pct Recovery = 73% Analysis Date = 04/11/16 Pct Recovery = 73% Analysis Date = 04/11/16 Pct Recovery = 73% Analysis Date = 04/09/16 Pct Recovery = 73% Analysis Date = 04/09/16 Pct Recovery = 73% Analysis Date = 04/07/16 Pct Recovery = 73% Analysis Date = 04/07/16 Pct Recovery = 73% Analysis Date = 04/05/16 Pct Recovery = 73% Analysis Date = 04/05/16 Pct Recovery = 73% Analysis Date = 04/03/16 Pct Recovery = 73% Analysis Date = 04/03/16 Pct Recovery = 73% Analysis Date = 03/31/16 Pct Recovery = 73% Analysis Date = 03/31/16 Pct Recovery = 73% Analysis Date = 03/29/16 Pct Recovery = 73% Analysis Date = 03/29/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/27/16 Pct Recovery = 73% Analysis Date = 03/25/16 Pct Recovery = 73% Analysis Date = 03/25/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/21/16 Pct Recovery = 73% Analysis Date = 03/21/16 Pct Recovery = 73% Analysis Date = 03/19/16 Pct Recovery = 73% Analysis Date = 03/19/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/16/16 Pct Recovery = 73% Analysis Date = 03/14/16 Pct Recovery = 73% Analysis Date = 03/14/16 Pct Recovery = 73% Analysis Date = 03/12/16 Pct Recovery = 73% Analysis Date = 03/12/16 Pct Recovery = 73% Analysis Date = 03/10/16 Pct Recovery = 73% Analysis Date = 03/10/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/08/16 Pct Recovery = 73% Analysis Date = 03/06/16 Pct Recovery = 73% Analysis Date = 03/06/16 Pct Recovery = 73% Analysis Date = 03/04/16 Pct Recovery = 73% Analysis Date = 03/04/16 Pct Recovery = 73% Analysis Date = 03/02/16 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,4-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 73% 10% 71% 10%
Total 18 73% 10% 71% 10%

Sample Statistics
3,4-DICHLOROANILINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
3,5-DICHLOROANILINE
METHOD: 2033 , TESTIDCODE: 61627GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 104% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 93% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 82% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 76% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 88% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 77% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 92% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 107% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 95% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 96% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 05/10/17 Pct Recovery = 81% Analysis Date = 05/08/17 Pct Recovery = 81% Analysis Date = 05/08/17 Pct Recovery = 81% Analysis Date = 05/06/17 Pct Recovery = 82% Analysis Date = 05/06/17 Pct Recovery = 82% Analysis Date = 05/04/17 Pct Recovery = 82% Analysis Date = 05/04/17 Pct Recovery = 82% Analysis Date = 05/01/17 Pct Recovery = 82% Analysis Date = 05/01/17 Pct Recovery = 82% Analysis Date = 04/29/17 Pct Recovery = 83% Analysis Date = 04/29/17 Pct Recovery = 83% Analysis Date = 04/27/17 Pct Recovery = 83% Analysis Date = 04/27/17 Pct Recovery = 83% Analysis Date = 04/25/17 Pct Recovery = 84% Analysis Date = 04/25/17 Pct Recovery = 84% Analysis Date = 04/22/17 Pct Recovery = 84% Analysis Date = 04/22/17 Pct Recovery = 84% Analysis Date = 04/20/17 Pct Recovery = 84% Analysis Date = 04/20/17 Pct Recovery = 84% Analysis Date = 04/18/17 Pct Recovery = 85% Analysis Date = 04/18/17 Pct Recovery = 85% Analysis Date = 04/15/17 Pct Recovery = 85% Analysis Date = 04/15/17 Pct Recovery = 85% Analysis Date = 04/13/17 Pct Recovery = 85% Analysis Date = 04/13/17 Pct Recovery = 85% Analysis Date = 04/11/17 Pct Recovery = 86% Analysis Date = 04/11/17 Pct Recovery = 86% Analysis Date = 04/09/17 Pct Recovery = 86% Analysis Date = 04/09/17 Pct Recovery = 86% Analysis Date = 04/06/17 Pct Recovery = 86% Analysis Date = 04/06/17 Pct Recovery = 86% Analysis Date = 04/04/17 Pct Recovery = 87% Analysis Date = 04/04/17 Pct Recovery = 87% Analysis Date = 04/02/17 Pct Recovery = 87% Analysis Date = 04/02/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/28/17 Pct Recovery = 88% Analysis Date = 03/28/17 Pct Recovery = 88% Analysis Date = 03/26/17 Pct Recovery = 88% Analysis Date = 03/26/17 Pct Recovery = 88% Analysis Date = 03/24/17 Pct Recovery = 88% Analysis Date = 03/24/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 90% Analysis Date = 03/14/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 91% Analysis Date = 03/08/17 Pct Recovery = 91% Analysis Date = 03/05/17 Pct Recovery = 91% Analysis Date = 03/05/17 Pct Recovery = 91% Analysis Date = 03/03/17 Pct Recovery = 91% Analysis Date = 03/03/17 Pct Recovery = 91% Analysis Date = 03/01/17 Pct Recovery = 92% Analysis Date = 03/01/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/24/17 Pct Recovery = 92% Analysis Date = 02/24/17 Pct Recovery = 92% Analysis Date = 02/22/17 Pct Recovery = 93% Analysis Date = 02/22/17 Pct Recovery = 93% Analysis Date = 02/20/17 Pct Recovery = 93% Analysis Date = 02/20/17 Pct Recovery = 93% Analysis Date = 02/17/17 Pct Recovery = 93% Analysis Date = 02/17/17 Pct Recovery = 93% Analysis Date = 02/15/17 Pct Recovery = 93% Analysis Date = 02/15/17 Pct Recovery = 93% Analysis Date = 02/13/17 Pct Recovery = 93% Analysis Date = 02/13/17 Pct Recovery = 93% Analysis Date = 02/10/17 Pct Recovery = 93% Analysis Date = 02/10/17 Pct Recovery = 93% Analysis Date = 02/08/17 Pct Recovery = 93% Analysis Date = 02/08/17 Pct Recovery = 93% Analysis Date = 02/06/17 Pct Recovery = 93% Analysis Date = 02/06/17 Pct Recovery = 93% Analysis Date = 02/04/17 Pct Recovery = 93% Analysis Date = 02/04/17 Pct Recovery = 93% Analysis Date = 02/01/17 Pct Recovery = 93% Analysis Date = 02/01/17 Pct Recovery = 93% Analysis Date = 01/30/17 Pct Recovery = 93% Analysis Date = 01/30/17 Pct Recovery = 93% Analysis Date = 01/28/17 Pct Recovery = 93% Analysis Date = 01/28/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/23/17 Pct Recovery = 93% Analysis Date = 01/23/17 Pct Recovery = 93% Analysis Date = 01/21/17 Pct Recovery = 93% Analysis Date = 01/21/17 Pct Recovery = 93% Analysis Date = 01/19/17 Pct Recovery = 93% Analysis Date = 01/19/17 Pct Recovery = 93% Analysis Date = 01/16/17 Pct Recovery = 93% Analysis Date = 01/16/17 Pct Recovery = 93% Analysis Date = 01/14/17 Pct Recovery = 93% Analysis Date = 01/14/17 Pct Recovery = 93% Analysis Date = 01/12/17 Pct Recovery = 93% Analysis Date = 01/12/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 92% Analysis Date = 12/22/16 Pct Recovery = 91% Analysis Date = 12/22/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/11/16 Pct Recovery = 91% Analysis Date = 12/08/16 Pct Recovery = 91% Analysis Date = 12/08/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 11/29/16 Pct Recovery = 90% Analysis Date = 11/29/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 90% Analysis Date = 11/25/16 Pct Recovery = 90% Analysis Date = 11/25/16 Pct Recovery = 90% Analysis Date = 11/22/16 Pct Recovery = 90% Analysis Date = 11/22/16 Pct Recovery = 90% Analysis Date = 11/20/16 Pct Recovery = 90% Analysis Date = 11/20/16 Pct Recovery = 90% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/16/16 Pct Recovery = 89% Analysis Date = 11/16/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/09/16 Pct Recovery = 89% Analysis Date = 11/09/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/04/16 Pct Recovery = 89% Analysis Date = 11/04/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/28/16 Pct Recovery = 88% Analysis Date = 10/28/16 Pct Recovery = 88% Analysis Date = 10/26/16 Pct Recovery = 88% Analysis Date = 10/26/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/21/16 Pct Recovery = 88% Analysis Date = 10/21/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 88% Analysis Date = 10/17/16 Pct Recovery = 88% Analysis Date = 10/17/16 Pct Recovery = 88% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/08/16 Pct Recovery = 87% Analysis Date = 10/08/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/29/16 Pct Recovery = 86% Analysis Date = 09/29/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 86% Analysis Date = 09/26/16 Pct Recovery = 86% Analysis Date = 09/24/16 Pct Recovery = 86% Analysis Date = 09/24/16 Pct Recovery = 86% Analysis Date = 09/22/16 Pct Recovery = 86% Analysis Date = 09/22/16 Pct Recovery = 86% Analysis Date = 09/19/16 Pct Recovery = 86% Analysis Date = 09/19/16 Pct Recovery = 86% Analysis Date = 09/17/16 Pct Recovery = 86% Analysis Date = 09/17/16 Pct Recovery = 86% Analysis Date = 09/15/16 Pct Recovery = 86% Analysis Date = 09/15/16 Pct Recovery = 86% Analysis Date = 09/13/16 Pct Recovery = 86% Analysis Date = 09/13/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 09/08/16 Pct Recovery = 85% Analysis Date = 09/08/16 Pct Recovery = 85% Analysis Date = 09/06/16 Pct Recovery = 85% Analysis Date = 09/06/16 Pct Recovery = 85% Analysis Date = 09/03/16 Pct Recovery = 86% Analysis Date = 09/03/16 Pct Recovery = 86% Analysis Date = 09/01/16 Pct Recovery = 86% Analysis Date = 09/01/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/30/16 Pct Recovery = 86% Analysis Date = 08/28/16 Pct Recovery = 86% Analysis Date = 08/28/16 Pct Recovery = 86% Analysis Date = 08/25/16 Pct Recovery = 86% Analysis Date = 08/25/16 Pct Recovery = 86% Analysis Date = 08/23/16 Pct Recovery = 86% Analysis Date = 08/23/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 86% Analysis Date = 08/21/16 Pct Recovery = 86% Analysis Date = 08/18/16 Pct Recovery = 86% Analysis Date = 08/18/16 Pct Recovery = 86% Analysis Date = 08/16/16 Pct Recovery = 86% Analysis Date = 08/16/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 87% Analysis Date = 07/29/16 Pct Recovery = 87% Analysis Date = 07/29/16 Pct Recovery = 87% Analysis Date = 07/27/16 Pct Recovery = 87% Analysis Date = 07/27/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 88% Analysis Date = 07/08/16 Pct Recovery = 88% Analysis Date = 07/08/16 Pct Recovery = 88% Analysis Date = 07/06/16 Pct Recovery = 88% Analysis Date = 07/06/16 Pct Recovery = 88% Analysis Date = 07/04/16 Pct Recovery = 88% Analysis Date = 07/04/16 Pct Recovery = 88% Analysis Date = 07/01/16 Pct Recovery = 88% Analysis Date = 07/01/16 Pct Recovery = 88% Analysis Date = 06/29/16 Pct Recovery = 88% Analysis Date = 06/29/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/25/16 Pct Recovery = 89% Analysis Date = 06/25/16 Pct Recovery = 89% Analysis Date = 06/22/16 Pct Recovery = 89% Analysis Date = 06/22/16 Pct Recovery = 89% Analysis Date = 06/20/16 Pct Recovery = 89% Analysis Date = 06/20/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/15/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/13/16 Pct Recovery = 89% Analysis Date = 06/11/16 Pct Recovery = 89% Analysis Date = 06/11/16 Pct Recovery = 89% Analysis Date = 06/09/16 Pct Recovery = 89% Analysis Date = 06/09/16 Pct Recovery = 89% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/21/16 Pct Recovery = 90% Analysis Date = 05/21/16 Pct Recovery = 90% Analysis Date = 05/19/16 Pct Recovery = 90% Analysis Date = 05/19/16 Pct Recovery = 90% Analysis Date = 05/17/16 Pct Recovery = 90% Analysis Date = 05/17/16 Pct Recovery = 90% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/14/16 Pct Recovery = 91% Analysis Date = 05/12/16 Pct Recovery = 91% Analysis Date = 05/12/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/08/16 Pct Recovery = 91% Analysis Date = 05/08/16 Pct Recovery = 91% Analysis Date = 05/05/16 Pct Recovery = 91% Analysis Date = 05/05/16 Pct Recovery = 91% Analysis Date = 05/03/16 Pct Recovery = 91% Analysis Date = 05/03/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 05/01/16 Pct Recovery = 91% Analysis Date = 04/28/16 Pct Recovery = 91% Analysis Date = 04/28/16 Pct Recovery = 91% Analysis Date = 04/26/16 Pct Recovery = 91% Analysis Date = 04/26/16 Pct Recovery = 91% Analysis Date = 04/24/16 Pct Recovery = 92% Analysis Date = 04/24/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/22/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/19/16 Pct Recovery = 92% Analysis Date = 04/17/16 Pct Recovery = 92% Analysis Date = 04/17/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/15/16 Pct Recovery = 92% Analysis Date = 04/12/16 Pct Recovery = 92% Analysis Date = 04/12/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/10/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 92% Analysis Date = 04/08/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/06/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 93% Analysis Date = 04/01/16 Pct Recovery = 93% Analysis Date = 03/30/16 Pct Recovery = 93% Analysis Date = 03/30/16 Pct Recovery = 93% Analysis Date = 03/27/16 Pct Recovery = 93% Analysis Date = 03/27/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/23/16 Pct Recovery = 93% Analysis Date = 03/23/16 Pct Recovery = 93% Analysis Date = 03/21/16 Pct Recovery = 93% Analysis Date = 03/21/16 Pct Recovery = 93% Analysis Date = 03/18/16 Pct Recovery = 93% Analysis Date = 03/18/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 93% Analysis Date = 03/14/16 Pct Recovery = 93% Analysis Date = 03/14/16 Pct Recovery = 93% Analysis Date = 03/11/16 Pct Recovery = 94% Analysis Date = 03/11/16 Pct Recovery = 94% Analysis Date = 03/09/16 Pct Recovery = 94% Analysis Date = 03/09/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 94% Analysis Date = 02/22/16 Pct Recovery = 94% Analysis Date = 02/22/16 Pct Recovery = 94% Analysis Date = 02/20/16 Pct Recovery = 94% Analysis Date = 02/20/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 95% Analysis Date = 02/18/16 Pct Recovery = 95% Analysis Date = 02/15/16 Pct Recovery = 95% Analysis Date = 02/15/16 Pct Recovery = 95% Analysis Date = 02/13/16 Pct Recovery = 95% Analysis Date = 02/13/16 Pct Recovery = 95% Analysis Date = 02/11/16 Pct Recovery = 95% Analysis Date = 02/11/16 Pct Recovery = 95% Analysis Date = 02/09/16 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
3,5-DICHLOROANILINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 15 89% 10% 92% 10%
Total 15 89% 10% 92% 10%

Sample Statistics
3,5-DICHLOROANILINE

Characteristic N % % Basis
Plotted 15 83% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 6% Spiked
Spiked 18 .  
False Negatives 2 11% 2 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
4-CHLORO-2-METHYLPHENOL
METHOD: 2033 , TESTIDCODE: 61633GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 74% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 60% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 61% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 32% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 39% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 58% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 50% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 57% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 77% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 58% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 59% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 66% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 46% Analysis Date = 05/10/17 Pct Recovery = 56% Analysis Date = 05/08/17 Pct Recovery = 57% Analysis Date = 05/08/17 Pct Recovery = 57% Analysis Date = 05/06/17 Pct Recovery = 57% Analysis Date = 05/06/17 Pct Recovery = 57% Analysis Date = 05/04/17 Pct Recovery = 57% Analysis Date = 05/04/17 Pct Recovery = 57% Analysis Date = 05/01/17 Pct Recovery = 57% Analysis Date = 05/01/17 Pct Recovery = 57% Analysis Date = 04/29/17 Pct Recovery = 57% Analysis Date = 04/29/17 Pct Recovery = 57% Analysis Date = 04/27/17 Pct Recovery = 57% Analysis Date = 04/27/17 Pct Recovery = 57% Analysis Date = 04/25/17 Pct Recovery = 58% Analysis Date = 04/25/17 Pct Recovery = 58% Analysis Date = 04/22/17 Pct Recovery = 58% Analysis Date = 04/22/17 Pct Recovery = 58% Analysis Date = 04/20/17 Pct Recovery = 58% Analysis Date = 04/20/17 Pct Recovery = 58% Analysis Date = 04/18/17 Pct Recovery = 58% Analysis Date = 04/18/17 Pct Recovery = 58% Analysis Date = 04/15/17 Pct Recovery = 58% Analysis Date = 04/15/17 Pct Recovery = 58% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/13/17 Pct Recovery = 59% Analysis Date = 04/11/17 Pct Recovery = 59% Analysis Date = 04/11/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/09/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 59% Analysis Date = 04/04/17 Pct Recovery = 59% Analysis Date = 04/02/17 Pct Recovery = 60% Analysis Date = 04/02/17 Pct Recovery = 60% Analysis Date = 03/30/17 Pct Recovery = 60% Analysis Date = 03/30/17 Pct Recovery = 60% Analysis Date = 03/28/17 Pct Recovery = 60% Analysis Date = 03/28/17 Pct Recovery = 60% Analysis Date = 03/26/17 Pct Recovery = 60% Analysis Date = 03/26/17 Pct Recovery = 60% Analysis Date = 03/24/17 Pct Recovery = 60% Analysis Date = 03/24/17 Pct Recovery = 60% Analysis Date = 03/21/17 Pct Recovery = 60% Analysis Date = 03/21/17 Pct Recovery = 60% Analysis Date = 03/19/17 Pct Recovery = 61% Analysis Date = 03/19/17 Pct Recovery = 61% Analysis Date = 03/17/17 Pct Recovery = 61% Analysis Date = 03/17/17 Pct Recovery = 61% Analysis Date = 03/14/17 Pct Recovery = 61% Analysis Date = 03/14/17 Pct Recovery = 61% Analysis Date = 03/12/17 Pct Recovery = 61% Analysis Date = 03/12/17 Pct Recovery = 61% Analysis Date = 03/10/17 Pct Recovery = 61% Analysis Date = 03/10/17 Pct Recovery = 61% Analysis Date = 03/08/17 Pct Recovery = 62% Analysis Date = 03/08/17 Pct Recovery = 62% Analysis Date = 03/05/17 Pct Recovery = 62% Analysis Date = 03/05/17 Pct Recovery = 62% Analysis Date = 03/03/17 Pct Recovery = 62% Analysis Date = 03/03/17 Pct Recovery = 62% Analysis Date = 03/01/17 Pct Recovery = 62% Analysis Date = 03/01/17 Pct Recovery = 62% Analysis Date = 02/26/17 Pct Recovery = 62% Analysis Date = 02/26/17 Pct Recovery = 62% Analysis Date = 02/24/17 Pct Recovery = 62% Analysis Date = 02/24/17 Pct Recovery = 62% Analysis Date = 02/22/17 Pct Recovery = 63% Analysis Date = 02/22/17 Pct Recovery = 63% Analysis Date = 02/20/17 Pct Recovery = 63% Analysis Date = 02/20/17 Pct Recovery = 63% Analysis Date = 02/17/17 Pct Recovery = 63% Analysis Date = 02/17/17 Pct Recovery = 63% Analysis Date = 02/15/17 Pct Recovery = 63% Analysis Date = 02/15/17 Pct Recovery = 63% Analysis Date = 02/13/17 Pct Recovery = 64% Analysis Date = 02/13/17 Pct Recovery = 64% Analysis Date = 02/10/17 Pct Recovery = 64% Analysis Date = 02/10/17 Pct Recovery = 64% Analysis Date = 02/08/17 Pct Recovery = 64% Analysis Date = 02/08/17 Pct Recovery = 64% Analysis Date = 02/06/17 Pct Recovery = 64% Analysis Date = 02/06/17 Pct Recovery = 64% Analysis Date = 02/04/17 Pct Recovery = 64% Analysis Date = 02/04/17 Pct Recovery = 64% Analysis Date = 02/01/17 Pct Recovery = 65% Analysis Date = 02/01/17 Pct Recovery = 65% Analysis Date = 01/30/17 Pct Recovery = 65% Analysis Date = 01/30/17 Pct Recovery = 65% Analysis Date = 01/28/17 Pct Recovery = 65% Analysis Date = 01/28/17 Pct Recovery = 65% Analysis Date = 01/25/17 Pct Recovery = 65% Analysis Date = 01/25/17 Pct Recovery = 65% Analysis Date = 01/23/17 Pct Recovery = 66% Analysis Date = 01/23/17 Pct Recovery = 66% Analysis Date = 01/21/17 Pct Recovery = 66% Analysis Date = 01/21/17 Pct Recovery = 66% Analysis Date = 01/19/17 Pct Recovery = 66% Analysis Date = 01/19/17 Pct Recovery = 66% Analysis Date = 01/16/17 Pct Recovery = 66% Analysis Date = 01/16/17 Pct Recovery = 66% Analysis Date = 01/14/17 Pct Recovery = 66% Analysis Date = 01/14/17 Pct Recovery = 66% Analysis Date = 01/12/17 Pct Recovery = 66% Analysis Date = 01/12/17 Pct Recovery = 66% Analysis Date = 01/09/17 Pct Recovery = 66% Analysis Date = 01/09/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 65% Analysis Date = 01/07/17 Pct Recovery = 65% Analysis Date = 01/05/17 Pct Recovery = 65% Analysis Date = 01/05/17 Pct Recovery = 65% Analysis Date = 01/03/17 Pct Recovery = 65% Analysis Date = 01/03/17 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/29/16 Pct Recovery = 65% Analysis Date = 12/29/16 Pct Recovery = 65% Analysis Date = 12/27/16 Pct Recovery = 65% Analysis Date = 12/27/16 Pct Recovery = 65% Analysis Date = 12/24/16 Pct Recovery = 64% Analysis Date = 12/24/16 Pct Recovery = 64% Analysis Date = 12/22/16 Pct Recovery = 64% Analysis Date = 12/22/16 Pct Recovery = 64% Analysis Date = 12/20/16 Pct Recovery = 64% Analysis Date = 12/20/16 Pct Recovery = 64% Analysis Date = 12/18/16 Pct Recovery = 64% Analysis Date = 12/18/16 Pct Recovery = 64% Analysis Date = 12/15/16 Pct Recovery = 64% Analysis Date = 12/15/16 Pct Recovery = 64% Analysis Date = 12/13/16 Pct Recovery = 63% Analysis Date = 12/13/16 Pct Recovery = 63% Analysis Date = 12/11/16 Pct Recovery = 63% Analysis Date = 12/11/16 Pct Recovery = 63% Analysis Date = 12/08/16 Pct Recovery = 63% Analysis Date = 12/08/16 Pct Recovery = 63% Analysis Date = 12/06/16 Pct Recovery = 63% Analysis Date = 12/06/16 Pct Recovery = 63% Analysis Date = 12/04/16 Pct Recovery = 63% Analysis Date = 12/04/16 Pct Recovery = 63% Analysis Date = 12/02/16 Pct Recovery = 63% Analysis Date = 12/02/16 Pct Recovery = 63% Analysis Date = 11/29/16 Pct Recovery = 62% Analysis Date = 11/29/16 Pct Recovery = 62% Analysis Date = 11/27/16 Pct Recovery = 62% Analysis Date = 11/27/16 Pct Recovery = 62% Analysis Date = 11/25/16 Pct Recovery = 62% Analysis Date = 11/25/16 Pct Recovery = 62% Analysis Date = 11/22/16 Pct Recovery = 62% Analysis Date = 11/22/16 Pct Recovery = 62% Analysis Date = 11/20/16 Pct Recovery = 62% Analysis Date = 11/20/16 Pct Recovery = 62% Analysis Date = 11/18/16 Pct Recovery = 61% Analysis Date = 11/18/16 Pct Recovery = 61% Analysis Date = 11/16/16 Pct Recovery = 61% Analysis Date = 11/16/16 Pct Recovery = 61% Analysis Date = 11/13/16 Pct Recovery = 61% Analysis Date = 11/13/16 Pct Recovery = 61% Analysis Date = 11/11/16 Pct Recovery = 61% Analysis Date = 11/11/16 Pct Recovery = 61% Analysis Date = 11/09/16 Pct Recovery = 61% Analysis Date = 11/09/16 Pct Recovery = 61% Analysis Date = 11/06/16 Pct Recovery = 61% Analysis Date = 11/06/16 Pct Recovery = 61% Analysis Date = 11/04/16 Pct Recovery = 60% Analysis Date = 11/04/16 Pct Recovery = 60% Analysis Date = 11/02/16 Pct Recovery = 60% Analysis Date = 11/02/16 Pct Recovery = 60% Analysis Date = 10/31/16 Pct Recovery = 60% Analysis Date = 10/31/16 Pct Recovery = 60% Analysis Date = 10/28/16 Pct Recovery = 60% Analysis Date = 10/28/16 Pct Recovery = 60% Analysis Date = 10/26/16 Pct Recovery = 60% Analysis Date = 10/26/16 Pct Recovery = 60% Analysis Date = 10/24/16 Pct Recovery = 59% Analysis Date = 10/24/16 Pct Recovery = 59% Analysis Date = 10/21/16 Pct Recovery = 59% Analysis Date = 10/21/16 Pct Recovery = 59% Analysis Date = 10/19/16 Pct Recovery = 59% Analysis Date = 10/19/16 Pct Recovery = 59% Analysis Date = 10/17/16 Pct Recovery = 59% Analysis Date = 10/17/16 Pct Recovery = 59% Analysis Date = 10/15/16 Pct Recovery = 59% Analysis Date = 10/15/16 Pct Recovery = 59% Analysis Date = 10/12/16 Pct Recovery = 59% Analysis Date = 10/12/16 Pct Recovery = 59% Analysis Date = 10/10/16 Pct Recovery = 58% Analysis Date = 10/10/16 Pct Recovery = 58% Analysis Date = 10/08/16 Pct Recovery = 58% Analysis Date = 10/08/16 Pct Recovery = 58% Analysis Date = 10/05/16 Pct Recovery = 58% Analysis Date = 10/05/16 Pct Recovery = 58% Analysis Date = 10/03/16 Pct Recovery = 58% Analysis Date = 10/03/16 Pct Recovery = 58% Analysis Date = 10/01/16 Pct Recovery = 58% Analysis Date = 10/01/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 57% Analysis Date = 09/29/16 Pct Recovery = 57% Analysis Date = 09/26/16 Pct Recovery = 57% Analysis Date = 09/26/16 Pct Recovery = 57% Analysis Date = 09/24/16 Pct Recovery = 57% Analysis Date = 09/24/16 Pct Recovery = 57% Analysis Date = 09/22/16 Pct Recovery = 57% Analysis Date = 09/22/16 Pct Recovery = 57% Analysis Date = 09/19/16 Pct Recovery = 57% Analysis Date = 09/19/16 Pct Recovery = 57% Analysis Date = 09/17/16 Pct Recovery = 57% Analysis Date = 09/17/16 Pct Recovery = 57% Analysis Date = 09/15/16 Pct Recovery = 56% Analysis Date = 09/15/16 Pct Recovery = 56% Analysis Date = 09/13/16 Pct Recovery = 56% Analysis Date = 09/13/16 Pct Recovery = 56% Analysis Date = 09/10/16 Pct Recovery = 56% Analysis Date = 09/10/16 Pct Recovery = 56% Analysis Date = 09/08/16 Pct Recovery = 56% Analysis Date = 09/08/16 Pct Recovery = 56% Analysis Date = 09/06/16 Pct Recovery = 56% Analysis Date = 09/06/16 Pct Recovery = 56% Analysis Date = 09/03/16 Pct Recovery = 56% Analysis Date = 09/03/16 Pct Recovery = 56% Analysis Date = 09/01/16 Pct Recovery = 56% Analysis Date = 09/01/16 Pct Recovery = 56% Analysis Date = 08/30/16 Pct Recovery = 56% Analysis Date = 08/30/16 Pct Recovery = 56% Analysis Date = 08/28/16 Pct Recovery = 56% Analysis Date = 08/28/16 Pct Recovery = 56% Analysis Date = 08/25/16 Pct Recovery = 57% Analysis Date = 08/25/16 Pct Recovery = 57% Analysis Date = 08/23/16 Pct Recovery = 57% Analysis Date = 08/23/16 Pct Recovery = 57% Analysis Date = 08/21/16 Pct Recovery = 57% Analysis Date = 08/21/16 Pct Recovery = 57% Analysis Date = 08/18/16 Pct Recovery = 57% Analysis Date = 08/18/16 Pct Recovery = 57% Analysis Date = 08/16/16 Pct Recovery = 57% Analysis Date = 08/16/16 Pct Recovery = 57% Analysis Date = 08/14/16 Pct Recovery = 57% Analysis Date = 08/14/16 Pct Recovery = 57% Analysis Date = 08/12/16 Pct Recovery = 57% Analysis Date = 08/12/16 Pct Recovery = 57% Analysis Date = 08/09/16 Pct Recovery = 57% Analysis Date = 08/09/16 Pct Recovery = 57% Analysis Date = 08/07/16 Pct Recovery = 57% Analysis Date = 08/07/16 Pct Recovery = 57% Analysis Date = 08/05/16 Pct Recovery = 57% Analysis Date = 08/05/16 Pct Recovery = 57% Analysis Date = 08/02/16 Pct Recovery = 57% Analysis Date = 08/02/16 Pct Recovery = 57% Analysis Date = 07/31/16 Pct Recovery = 57% Analysis Date = 07/31/16 Pct Recovery = 57% Analysis Date = 07/29/16 Pct Recovery = 57% Analysis Date = 07/29/16 Pct Recovery = 57% Analysis Date = 07/27/16 Pct Recovery = 57% Analysis Date = 07/27/16 Pct Recovery = 57% Analysis Date = 07/24/16 Pct Recovery = 57% Analysis Date = 07/24/16 Pct Recovery = 57% Analysis Date = 07/22/16 Pct Recovery = 57% Analysis Date = 07/22/16 Pct Recovery = 57% Analysis Date = 07/20/16 Pct Recovery = 57% Analysis Date = 07/20/16 Pct Recovery = 57% Analysis Date = 07/17/16 Pct Recovery = 57% Analysis Date = 07/17/16 Pct Recovery = 57% Analysis Date = 07/15/16 Pct Recovery = 57% Analysis Date = 07/15/16 Pct Recovery = 57% Analysis Date = 07/13/16 Pct Recovery = 57% Analysis Date = 07/13/16 Pct Recovery = 57% Analysis Date = 07/11/16 Pct Recovery = 57% Analysis Date = 07/11/16 Pct Recovery = 57% Analysis Date = 07/08/16 Pct Recovery = 57% Analysis Date = 07/08/16 Pct Recovery = 57% Analysis Date = 07/06/16 Pct Recovery = 57% Analysis Date = 07/06/16 Pct Recovery = 57% Analysis Date = 07/04/16 Pct Recovery = 57% Analysis Date = 07/04/16 Pct Recovery = 57% Analysis Date = 07/01/16 Pct Recovery = 57% Analysis Date = 07/01/16 Pct Recovery = 57% Analysis Date = 06/29/16 Pct Recovery = 57% Analysis Date = 06/29/16 Pct Recovery = 57% Analysis Date = 06/27/16 Pct Recovery = 57% Analysis Date = 06/27/16 Pct Recovery = 57% Analysis Date = 06/25/16 Pct Recovery = 57% Analysis Date = 06/25/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/20/16 Pct Recovery = 57% Analysis Date = 06/20/16 Pct Recovery = 57% Analysis Date = 06/18/16 Pct Recovery = 57% Analysis Date = 06/18/16 Pct Recovery = 57% Analysis Date = 06/15/16 Pct Recovery = 57% Analysis Date = 06/15/16 Pct Recovery = 57% Analysis Date = 06/13/16 Pct Recovery = 57% Analysis Date = 06/13/16 Pct Recovery = 57% Analysis Date = 06/11/16 Pct Recovery = 57% Analysis Date = 06/11/16 Pct Recovery = 57% Analysis Date = 06/09/16 Pct Recovery = 57% Analysis Date = 06/09/16 Pct Recovery = 57% Analysis Date = 06/06/16 Pct Recovery = 57% Analysis Date = 06/06/16 Pct Recovery = 57% Analysis Date = 06/04/16 Pct Recovery = 57% Analysis Date = 06/04/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 05/30/16 Pct Recovery = 57% Analysis Date = 05/30/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 57% Analysis Date = 05/26/16 Pct Recovery = 57% Analysis Date = 05/26/16 Pct Recovery = 57% Analysis Date = 05/24/16 Pct Recovery = 57% Analysis Date = 05/24/16 Pct Recovery = 57% Analysis Date = 05/21/16 Pct Recovery = 57% Analysis Date = 05/21/16 Pct Recovery = 57% Analysis Date = 05/19/16 Pct Recovery = 57% Analysis Date = 05/19/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 57% Analysis Date = 05/14/16 Pct Recovery = 57% Analysis Date = 05/14/16 Pct Recovery = 57% Analysis Date = 05/12/16 Pct Recovery = 57% Analysis Date = 05/12/16 Pct Recovery = 57% Analysis Date = 05/10/16 Pct Recovery = 57% Analysis Date = 05/10/16 Pct Recovery = 57% Analysis Date = 05/08/16 Pct Recovery = 57% Analysis Date = 05/08/16 Pct Recovery = 57% Analysis Date = 05/05/16 Pct Recovery = 57% Analysis Date = 05/05/16 Pct Recovery = 57% Analysis Date = 05/03/16 Pct Recovery = 57% Analysis Date = 05/03/16 Pct Recovery = 57% Analysis Date = 05/01/16 Pct Recovery = 57% Analysis Date = 05/01/16 Pct Recovery = 57% Analysis Date = 04/28/16 Pct Recovery = 57% Analysis Date = 04/28/16 Pct Recovery = 57% Analysis Date = 04/26/16 Pct Recovery = 57% Analysis Date = 04/26/16 Pct Recovery = 57% Analysis Date = 04/24/16 Pct Recovery = 57% Analysis Date = 04/24/16 Pct Recovery = 57% Analysis Date = 04/22/16 Pct Recovery = 57% Analysis Date = 04/22/16 Pct Recovery = 57% Analysis Date = 04/19/16 Pct Recovery = 57% Analysis Date = 04/19/16 Pct Recovery = 57% Analysis Date = 04/17/16 Pct Recovery = 56% Analysis Date = 04/17/16 Pct Recovery = 56% Analysis Date = 04/15/16 Pct Recovery = 56% Analysis Date = 04/15/16 Pct Recovery = 56% Analysis Date = 04/12/16 Pct Recovery = 56% Analysis Date = 04/12/16 Pct Recovery = 56% Analysis Date = 04/10/16 Pct Recovery = 56% Analysis Date = 04/10/16 Pct Recovery = 56% Analysis Date = 04/08/16 Pct Recovery = 56% Analysis Date = 04/08/16 Pct Recovery = 56% Analysis Date = 04/06/16 Pct Recovery = 56% Analysis Date = 04/06/16 Pct Recovery = 56% Analysis Date = 04/03/16 Pct Recovery = 55% Analysis Date = 04/03/16 Pct Recovery = 55% Analysis Date = 04/01/16 Pct Recovery = 55% Analysis Date = 04/01/16 Pct Recovery = 55% Analysis Date = 03/30/16 Pct Recovery = 55% Analysis Date = 03/30/16 Pct Recovery = 55% Analysis Date = 03/27/16 Pct Recovery = 55% Analysis Date = 03/27/16 Pct Recovery = 55% Analysis Date = 03/25/16 Pct Recovery = 54% Analysis Date = 03/25/16 Pct Recovery = 54% Analysis Date = 03/23/16 Pct Recovery = 54% Analysis Date = 03/23/16 Pct Recovery = 54% Analysis Date = 03/21/16 Pct Recovery = 54% Analysis Date = 03/21/16 Pct Recovery = 54% Analysis Date = 03/18/16 Pct Recovery = 54% Analysis Date = 03/18/16 Pct Recovery = 54% Analysis Date = 03/16/16 Pct Recovery = 53% Analysis Date = 03/16/16 Pct Recovery = 53% Analysis Date = 03/14/16 Pct Recovery = 53% Analysis Date = 03/14/16 Pct Recovery = 53% Analysis Date = 03/11/16 Pct Recovery = 53% Analysis Date = 03/11/16 Pct Recovery = 53% Analysis Date = 03/09/16 Pct Recovery = 52% Analysis Date = 03/09/16 Pct Recovery = 52% Analysis Date = 03/07/16 Pct Recovery = 52% Analysis Date = 03/07/16 Pct Recovery = 52% Analysis Date = 03/05/16 Pct Recovery = 52% Analysis Date = 03/05/16 Pct Recovery = 52% Analysis Date = 03/02/16 Pct Recovery = 52% Analysis Date = 03/02/16 Pct Recovery = 52% Analysis Date = 02/29/16 Pct Recovery = 51% Analysis Date = 02/29/16 Pct Recovery = 51% Analysis Date = 02/27/16 Pct Recovery = 51% Analysis Date = 02/27/16 Pct Recovery = 51% Analysis Date = 02/24/16 Pct Recovery = 51% Analysis Date = 02/24/16 Pct Recovery = 51% Analysis Date = 02/22/16 Pct Recovery = 50% Analysis Date = 02/22/16 Pct Recovery = 50% Analysis Date = 02/20/16 Pct Recovery = 50% Analysis Date = 02/20/16 Pct Recovery = 50% Analysis Date = 02/18/16 Pct Recovery = 50% Analysis Date = 02/18/16 Pct Recovery = 50% Analysis Date = 02/15/16 Pct Recovery = 49% Analysis Date = 02/15/16 Pct Recovery = 49% Analysis Date = 02/13/16 Pct Recovery = 49% Analysis Date = 02/13/16 Pct Recovery = 49% Analysis Date = 02/11/16 Pct Recovery = 49% Analysis Date = 02/11/16 Pct Recovery = 49% Analysis Date = 02/09/16 Pct Recovery = 48% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLORO-2-METHYLPHENOL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 58% 12% 58% 8%
Total 18 58% 12% 58% 8%

Sample Statistics
4-CHLORO-2-METHYLPHENOL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
ACETOCHLOR
METHOD: 2033 , TESTIDCODE: 49260GCM33

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 102% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 96% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 89% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 96% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 110% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 97% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 83% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 101% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 87% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 98% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 83% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 77% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 05/10/17 Pct Recovery = 93% Analysis Date = 05/08/17 Pct Recovery = 93% Analysis Date = 05/08/17 Pct Recovery = 93% Analysis Date = 05/06/17 Pct Recovery = 93% Analysis Date = 05/06/17 Pct Recovery = 93% Analysis Date = 05/04/17 Pct Recovery = 93% Analysis Date = 05/04/17 Pct Recovery = 93% Analysis Date = 05/01/17 Pct Recovery = 93% Analysis Date = 05/01/17 Pct Recovery = 93% Analysis Date = 04/29/17 Pct Recovery = 93% Analysis Date = 04/29/17 Pct Recovery = 93% Analysis Date = 04/27/17 Pct Recovery = 93% Analysis Date = 04/27/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/20/17 Pct Recovery = 93% Analysis Date = 04/20/17 Pct Recovery = 93% Analysis Date = 04/18/17 Pct Recovery = 93% Analysis Date = 04/18/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/09/17 Pct Recovery = 93% Analysis Date = 04/09/17 Pct Recovery = 93% Analysis Date = 04/06/17 Pct Recovery = 93% Analysis Date = 04/06/17 Pct Recovery = 93% Analysis Date = 04/04/17 Pct Recovery = 93% Analysis Date = 04/04/17 Pct Recovery = 93% Analysis Date = 04/02/17 Pct Recovery = 93% Analysis Date = 04/02/17 Pct Recovery = 93% Analysis Date = 03/30/17 Pct Recovery = 93% Analysis Date = 03/30/17 Pct Recovery = 93% Analysis Date = 03/28/17 Pct Recovery = 93% Analysis Date = 03/28/17 Pct Recovery = 93% Analysis Date = 03/26/17 Pct Recovery = 93% Analysis Date = 03/26/17 Pct Recovery = 93% Analysis Date = 03/24/17 Pct Recovery = 94% Analysis Date = 03/24/17 Pct Recovery = 94% Analysis Date = 03/21/17 Pct Recovery = 94% Analysis Date = 03/21/17 Pct Recovery = 94% Analysis Date = 03/19/17 Pct Recovery = 94% Analysis Date = 03/19/17 Pct Recovery = 94% Analysis Date = 03/17/17 Pct Recovery = 94% Analysis Date = 03/17/17 Pct Recovery = 94% Analysis Date = 03/14/17 Pct Recovery = 94% Analysis Date = 03/14/17 Pct Recovery = 94% Analysis Date = 03/12/17 Pct Recovery = 94% Analysis Date = 03/12/17 Pct Recovery = 94% Analysis Date = 03/10/17 Pct Recovery = 94% Analysis Date = 03/10/17 Pct Recovery = 94% Analysis Date = 03/08/17 Pct Recovery = 94% Analysis Date = 03/08/17 Pct Recovery = 94% Analysis Date = 03/05/17 Pct Recovery = 94% Analysis Date = 03/05/17 Pct Recovery = 94% Analysis Date = 03/03/17 Pct Recovery = 94% Analysis Date = 03/03/17 Pct Recovery = 94% Analysis Date = 03/01/17 Pct Recovery = 94% Analysis Date = 03/01/17 Pct Recovery = 94% Analysis Date = 02/26/17 Pct Recovery = 94% Analysis Date = 02/26/17 Pct Recovery = 94% Analysis Date = 02/24/17 Pct Recovery = 94% Analysis Date = 02/24/17 Pct Recovery = 94% Analysis Date = 02/22/17 Pct Recovery = 94% Analysis Date = 02/22/17 Pct Recovery = 94% Analysis Date = 02/20/17 Pct Recovery = 94% Analysis Date = 02/20/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/15/17 Pct Recovery = 94% Analysis Date = 02/15/17 Pct Recovery = 94% Analysis Date = 02/13/17 Pct Recovery = 94% Analysis Date = 02/13/17 Pct Recovery = 94% Analysis Date = 02/10/17 Pct Recovery = 94% Analysis Date = 02/10/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 94% Analysis Date = 02/06/17 Pct Recovery = 94% Analysis Date = 02/06/17 Pct Recovery = 94% Analysis Date = 02/04/17 Pct Recovery = 94% Analysis Date = 02/04/17 Pct Recovery = 94% Analysis Date = 02/01/17 Pct Recovery = 94% Analysis Date = 02/01/17 Pct Recovery = 94% Analysis Date = 01/30/17 Pct Recovery = 94% Analysis Date = 01/30/17 Pct Recovery = 94% Analysis Date = 01/28/17 Pct Recovery = 94% Analysis Date = 01/28/17 Pct Recovery = 94% Analysis Date = 01/25/17 Pct Recovery = 94% Analysis Date = 01/25/17 Pct Recovery = 94% Analysis Date = 01/23/17 Pct Recovery = 94% Analysis Date = 01/23/17 Pct Recovery = 94% Analysis Date = 01/21/17 Pct Recovery = 94% Analysis Date = 01/21/17 Pct Recovery = 94% Analysis Date = 01/19/17 Pct Recovery = 94% Analysis Date = 01/19/17 Pct Recovery = 94% Analysis Date = 01/16/17 Pct Recovery = 94% Analysis Date = 01/16/17 Pct Recovery = 94% Analysis Date = 01/14/17 Pct Recovery = 95% Analysis Date = 01/14/17 Pct Recovery = 95% Analysis Date = 01/12/17 Pct Recovery = 95% Analysis Date = 01/12/17 Pct Recovery = 95% Analysis Date = 01/09/17 Pct Recovery = 95% Analysis Date = 01/09/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/05/17 Pct Recovery = 95% Analysis Date = 01/05/17 Pct Recovery = 95% Analysis Date = 01/03/17 Pct Recovery = 95% Analysis Date = 01/03/17 Pct Recovery = 95% Analysis Date = 12/31/16 Pct Recovery = 95% Analysis Date = 12/31/16 Pct Recovery = 95% Analysis Date = 12/29/16 Pct Recovery = 95% Analysis Date = 12/29/16 Pct Recovery = 95% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/24/16 Pct Recovery = 96% Analysis Date = 12/24/16 Pct Recovery = 96% Analysis Date = 12/22/16 Pct Recovery = 96% Analysis Date = 12/22/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/18/16 Pct Recovery = 96% Analysis Date = 12/18/16 Pct Recovery = 96% Analysis Date = 12/15/16 Pct Recovery = 96% Analysis Date = 12/15/16 Pct Recovery = 96% Analysis Date = 12/13/16 Pct Recovery = 96% Analysis Date = 12/13/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/08/16 Pct Recovery = 97% Analysis Date = 12/08/16 Pct Recovery = 97% Analysis Date = 12/06/16 Pct Recovery = 97% Analysis Date = 12/06/16 Pct Recovery = 97% Analysis Date = 12/04/16 Pct Recovery = 97% Analysis Date = 12/04/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 12/02/16 Pct Recovery = 97% Analysis Date = 11/29/16 Pct Recovery = 97% Analysis Date = 11/29/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/27/16 Pct Recovery = 97% Analysis Date = 11/25/16 Pct Recovery = 97% Analysis Date = 11/25/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/20/16 Pct Recovery = 98% Analysis Date = 11/20/16 Pct Recovery = 98% Analysis Date = 11/18/16 Pct Recovery = 98% Analysis Date = 11/18/16 Pct Recovery = 98% Analysis Date = 11/16/16 Pct Recovery = 98% Analysis Date = 11/16/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/11/16 Pct Recovery = 98% Analysis Date = 11/11/16 Pct Recovery = 98% Analysis Date = 11/09/16 Pct Recovery = 98% Analysis Date = 11/09/16 Pct Recovery = 98% Analysis Date = 11/06/16 Pct Recovery = 98% Analysis Date = 11/06/16 Pct Recovery = 98% Analysis Date = 11/04/16 Pct Recovery = 99% Analysis Date = 11/04/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/28/16 Pct Recovery = 99% Analysis Date = 10/28/16 Pct Recovery = 99% Analysis Date = 10/26/16 Pct Recovery = 99% Analysis Date = 10/26/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/21/16 Pct Recovery = 99% Analysis Date = 10/21/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 100% Analysis Date = 10/17/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/12/16 Pct Recovery = 100% Analysis Date = 10/12/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/08/16 Pct Recovery = 100% Analysis Date = 10/08/16 Pct Recovery = 100% Analysis Date = 10/05/16 Pct Recovery = 100% Analysis Date = 10/05/16 Pct Recovery = 100% Analysis Date = 10/03/16 Pct Recovery = 100% Analysis Date = 10/03/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 09/29/16 Pct Recovery = 101% Analysis Date = 09/29/16 Pct Recovery = 101% Analysis Date = 09/26/16 Pct Recovery = 101% Analysis Date = 09/26/16 Pct Recovery = 101% Analysis Date = 09/24/16 Pct Recovery = 101% Analysis Date = 09/24/16 Pct Recovery = 101% Analysis Date = 09/22/16 Pct Recovery = 101% Analysis Date = 09/22/16 Pct Recovery = 101% Analysis Date = 09/19/16 Pct Recovery = 101% Analysis Date = 09/19/16 Pct Recovery = 101% Analysis Date = 09/17/16 Pct Recovery = 101% Analysis Date = 09/17/16 Pct Recovery = 101% Analysis Date = 09/15/16 Pct Recovery = 101% Analysis Date = 09/15/16 Pct Recovery = 101% Analysis Date = 09/13/16 Pct Recovery = 101% Analysis Date = 09/13/16 Pct Recovery = 101% Analysis Date = 09/10/16 Pct Recovery = 102% Analysis Date = 09/10/16 Pct Recovery = 102% Analysis Date = 09/08/16 Pct Recovery = 102% Analysis Date = 09/08/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/03/16 Pct Recovery = 101% Analysis Date = 09/03/16 Pct Recovery = 101% Analysis Date = 09/01/16 Pct Recovery = 101% Analysis Date = 09/01/16 Pct Recovery = 101% Analysis Date = 08/30/16 Pct Recovery = 101% Analysis Date = 08/30/16 Pct Recovery = 101% Analysis Date = 08/28/16 Pct Recovery = 101% Analysis Date = 08/28/16 Pct Recovery = 101% Analysis Date = 08/25/16 Pct Recovery = 101% Analysis Date = 08/25/16 Pct Recovery = 101% Analysis Date = 08/23/16 Pct Recovery = 101% Analysis Date = 08/23/16 Pct Recovery = 101% Analysis Date = 08/21/16 Pct Recovery = 101% Analysis Date = 08/21/16 Pct Recovery = 101% Analysis Date = 08/18/16 Pct Recovery = 101% Analysis Date = 08/18/16 Pct Recovery = 101% Analysis Date = 08/16/16 Pct Recovery = 101% Analysis Date = 08/16/16 Pct Recovery = 101% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/12/16 Pct Recovery = 100% Analysis Date = 08/12/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/07/16 Pct Recovery = 100% Analysis Date = 08/07/16 Pct Recovery = 100% Analysis Date = 08/05/16 Pct Recovery = 99% Analysis Date = 08/05/16 Pct Recovery = 99% Analysis Date = 08/02/16 Pct Recovery = 99% Analysis Date = 08/02/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/31/16 Pct Recovery = 99% Analysis Date = 07/29/16 Pct Recovery = 98% Analysis Date = 07/29/16 Pct Recovery = 98% Analysis Date = 07/27/16 Pct Recovery = 98% Analysis Date = 07/27/16 Pct Recovery = 98% Analysis Date = 07/24/16 Pct Recovery = 98% Analysis Date = 07/24/16 Pct Recovery = 98% Analysis Date = 07/22/16 Pct Recovery = 97% Analysis Date = 07/22/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/20/16 Pct Recovery = 97% Analysis Date = 07/17/16 Pct Recovery = 97% Analysis Date = 07/17/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/15/16 Pct Recovery = 97% Analysis Date = 07/13/16 Pct Recovery = 96% Analysis Date = 07/13/16 Pct Recovery = 96% Analysis Date = 07/11/16 Pct Recovery = 96% Analysis Date = 07/11/16 Pct Recovery = 96% Analysis Date = 07/08/16 Pct Recovery = 96% Analysis Date = 07/08/16 Pct Recovery = 96% Analysis Date = 07/06/16 Pct Recovery = 95% Analysis Date = 07/06/16 Pct Recovery = 95% Analysis Date = 07/04/16 Pct Recovery = 95% Analysis Date = 07/04/16 Pct Recovery = 95% Analysis Date = 07/01/16 Pct Recovery = 95% Analysis Date = 07/01/16 Pct Recovery = 95% Analysis Date = 06/29/16 Pct Recovery = 94% Analysis Date = 06/29/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 94% Analysis Date = 06/27/16 Pct Recovery = 94% Analysis Date = 06/25/16 Pct Recovery = 94% Analysis Date = 06/25/16 Pct Recovery = 94% Analysis Date = 06/22/16 Pct Recovery = 94% Analysis Date = 06/22/16 Pct Recovery = 94% Analysis Date = 06/20/16 Pct Recovery = 93% Analysis Date = 06/20/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 93% Analysis Date = 06/15/16 Pct Recovery = 93% Analysis Date = 06/15/16 Pct Recovery = 93% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 92% Analysis Date = 06/09/16 Pct Recovery = 92% Analysis Date = 06/09/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/06/16 Pct Recovery = 92% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 05/30/16 Pct Recovery = 91% Analysis Date = 05/30/16 Pct Recovery = 91% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/21/16 Pct Recovery = 89% Analysis Date = 05/21/16 Pct Recovery = 89% Analysis Date = 05/19/16 Pct Recovery = 89% Analysis Date = 05/19/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/12/16 Pct Recovery = 88% Analysis Date = 05/12/16 Pct Recovery = 88% Analysis Date = 05/10/16 Pct Recovery = 88% Analysis Date = 05/10/16 Pct Recovery = 88% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 87% Analysis Date = 05/03/16 Pct Recovery = 87% Analysis Date = 05/03/16 Pct Recovery = 87% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/24/16 Pct Recovery = 86% Analysis Date = 04/24/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/17/16 Pct Recovery = 85% Analysis Date = 04/17/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/08/16 Pct Recovery = 84% Analysis Date = 04/08/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 03/30/16 Pct Recovery = 83% Analysis Date = 03/30/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 82% Analysis Date = 03/18/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 82% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/05/16 Pct Recovery = 81% Analysis Date = 03/05/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/27/16 Pct Recovery = 81% Analysis Date = 02/27/16 Pct Recovery = 81% Analysis Date = 02/24/16 Pct Recovery = 81% Analysis Date = 02/24/16 Pct Recovery = 81% Analysis Date = 02/22/16 Pct Recovery = 80% Analysis Date = 02/22/16 Pct Recovery = 80% Analysis Date = 02/20/16 Pct Recovery = 80% Analysis Date = 02/20/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 80% Analysis Date = 02/18/16 Pct Recovery = 80% Analysis Date = 02/15/16 Pct Recovery = 80% Analysis Date = 02/15/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/13/16 Pct Recovery = 80% Analysis Date = 02/11/16 Pct Recovery = 79% Analysis Date = 02/11/16 Pct Recovery = 79% Analysis Date = 02/09/16 Pct Recovery = 79% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETOCHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 93% 10% 96% 10%
Total 19 93% 10% 96% 10%

Sample Statistics
ACETOCHLOR

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
ALACHLOR
METHOD: 2033 , TESTIDCODE: 46342GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 114% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 99% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 94% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 96% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 96% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 125% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 101% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 106% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 05/02/17 Pct Recovery = 101% Analysis Date = 04/30/17 Pct Recovery = 101% Analysis Date = 04/30/17 Pct Recovery = 101% Analysis Date = 04/28/17 Pct Recovery = 102% Analysis Date = 04/28/17 Pct Recovery = 102% Analysis Date = 04/26/17 Pct Recovery = 102% Analysis Date = 04/26/17 Pct Recovery = 102% Analysis Date = 04/24/17 Pct Recovery = 102% Analysis Date = 04/24/17 Pct Recovery = 102% Analysis Date = 04/21/17 Pct Recovery = 102% Analysis Date = 04/21/17 Pct Recovery = 102% Analysis Date = 04/19/17 Pct Recovery = 102% Analysis Date = 04/19/17 Pct Recovery = 102% Analysis Date = 04/17/17 Pct Recovery = 102% Analysis Date = 04/17/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/12/17 Pct Recovery = 102% Analysis Date = 04/12/17 Pct Recovery = 102% Analysis Date = 04/10/17 Pct Recovery = 102% Analysis Date = 04/10/17 Pct Recovery = 102% Analysis Date = 04/08/17 Pct Recovery = 102% Analysis Date = 04/08/17 Pct Recovery = 102% Analysis Date = 04/06/17 Pct Recovery = 102% Analysis Date = 04/06/17 Pct Recovery = 102% Analysis Date = 04/03/17 Pct Recovery = 102% Analysis Date = 04/03/17 Pct Recovery = 102% Analysis Date = 04/01/17 Pct Recovery = 102% Analysis Date = 04/01/17 Pct Recovery = 102% Analysis Date = 03/30/17 Pct Recovery = 102% Analysis Date = 03/30/17 Pct Recovery = 102% Analysis Date = 03/28/17 Pct Recovery = 103% Analysis Date = 03/28/17 Pct Recovery = 103% Analysis Date = 03/25/17 Pct Recovery = 103% Analysis Date = 03/25/17 Pct Recovery = 103% Analysis Date = 03/23/17 Pct Recovery = 103% Analysis Date = 03/23/17 Pct Recovery = 103% Analysis Date = 03/21/17 Pct Recovery = 103% Analysis Date = 03/21/17 Pct Recovery = 103% Analysis Date = 03/19/17 Pct Recovery = 103% Analysis Date = 03/19/17 Pct Recovery = 103% Analysis Date = 03/16/17 Pct Recovery = 103% Analysis Date = 03/16/17 Pct Recovery = 103% Analysis Date = 03/14/17 Pct Recovery = 103% Analysis Date = 03/14/17 Pct Recovery = 103% Analysis Date = 03/12/17 Pct Recovery = 103% Analysis Date = 03/12/17 Pct Recovery = 103% Analysis Date = 03/10/17 Pct Recovery = 103% Analysis Date = 03/10/17 Pct Recovery = 103% Analysis Date = 03/07/17 Pct Recovery = 103% Analysis Date = 03/07/17 Pct Recovery = 103% Analysis Date = 03/05/17 Pct Recovery = 103% Analysis Date = 03/05/17 Pct Recovery = 103% Analysis Date = 03/03/17 Pct Recovery = 103% Analysis Date = 03/03/17 Pct Recovery = 103% Analysis Date = 03/01/17 Pct Recovery = 103% Analysis Date = 03/01/17 Pct Recovery = 103% Analysis Date = 02/26/17 Pct Recovery = 103% Analysis Date = 02/26/17 Pct Recovery = 103% Analysis Date = 02/24/17 Pct Recovery = 103% Analysis Date = 02/24/17 Pct Recovery = 103% Analysis Date = 02/22/17 Pct Recovery = 103% Analysis Date = 02/22/17 Pct Recovery = 103% Analysis Date = 02/20/17 Pct Recovery = 103% Analysis Date = 02/20/17 Pct Recovery = 103% Analysis Date = 02/17/17 Pct Recovery = 103% Analysis Date = 02/17/17 Pct Recovery = 103% Analysis Date = 02/15/17 Pct Recovery = 103% Analysis Date = 02/15/17 Pct Recovery = 103% Analysis Date = 02/13/17 Pct Recovery = 103% Analysis Date = 02/13/17 Pct Recovery = 103% Analysis Date = 02/11/17 Pct Recovery = 103% Analysis Date = 02/11/17 Pct Recovery = 103% Analysis Date = 02/08/17 Pct Recovery = 103% Analysis Date = 02/08/17 Pct Recovery = 103% Analysis Date = 02/06/17 Pct Recovery = 103% Analysis Date = 02/06/17 Pct Recovery = 103% Analysis Date = 02/04/17 Pct Recovery = 102% Analysis Date = 02/04/17 Pct Recovery = 102% Analysis Date = 02/02/17 Pct Recovery = 102% Analysis Date = 02/02/17 Pct Recovery = 102% Analysis Date = 01/30/17 Pct Recovery = 102% Analysis Date = 01/30/17 Pct Recovery = 102% Analysis Date = 01/28/17 Pct Recovery = 102% Analysis Date = 01/28/17 Pct Recovery = 102% Analysis Date = 01/26/17 Pct Recovery = 102% Analysis Date = 01/26/17 Pct Recovery = 102% Analysis Date = 01/24/17 Pct Recovery = 102% Analysis Date = 01/24/17 Pct Recovery = 102% Analysis Date = 01/21/17 Pct Recovery = 101% Analysis Date = 01/21/17 Pct Recovery = 101% Analysis Date = 01/19/17 Pct Recovery = 101% Analysis Date = 01/19/17 Pct Recovery = 101% Analysis Date = 01/17/17 Pct Recovery = 101% Analysis Date = 01/17/17 Pct Recovery = 101% Analysis Date = 01/15/17 Pct Recovery = 101% Analysis Date = 01/15/17 Pct Recovery = 101% Analysis Date = 01/12/17 Pct Recovery = 101% Analysis Date = 01/12/17 Pct Recovery = 101% Analysis Date = 01/10/17 Pct Recovery = 101% Analysis Date = 01/10/17 Pct Recovery = 101% Analysis Date = 01/08/17 Pct Recovery = 100% Analysis Date = 01/08/17 Pct Recovery = 100% Analysis Date = 01/06/17 Pct Recovery = 100% Analysis Date = 01/06/17 Pct Recovery = 100% Analysis Date = 01/04/17 Pct Recovery = 100% Analysis Date = 01/04/17 Pct Recovery = 100% Analysis Date = 01/01/17 Pct Recovery = 100% Analysis Date = 01/01/17 Pct Recovery = 100% Analysis Date = 12/30/16 Pct Recovery = 100% Analysis Date = 12/30/16 Pct Recovery = 100% Analysis Date = 12/28/16 Pct Recovery = 100% Analysis Date = 12/28/16 Pct Recovery = 100% Analysis Date = 12/26/16 Pct Recovery = 99% Analysis Date = 12/26/16 Pct Recovery = 99% Analysis Date = 12/23/16 Pct Recovery = 99% Analysis Date = 12/23/16 Pct Recovery = 99% Analysis Date = 12/21/16 Pct Recovery = 99% Analysis Date = 12/21/16 Pct Recovery = 99% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/17/16 Pct Recovery = 99% Analysis Date = 12/17/16 Pct Recovery = 99% Analysis Date = 12/14/16 Pct Recovery = 98% Analysis Date = 12/14/16 Pct Recovery = 98% Analysis Date = 12/12/16 Pct Recovery = 98% Analysis Date = 12/12/16 Pct Recovery = 98% Analysis Date = 12/10/16 Pct Recovery = 98% Analysis Date = 12/10/16 Pct Recovery = 98% Analysis Date = 12/08/16 Pct Recovery = 97% Analysis Date = 12/08/16 Pct Recovery = 97% Analysis Date = 12/05/16 Pct Recovery = 97% Analysis Date = 12/05/16 Pct Recovery = 97% Analysis Date = 12/03/16 Pct Recovery = 97% Analysis Date = 12/03/16 Pct Recovery = 97% Analysis Date = 12/01/16 Pct Recovery = 97% Analysis Date = 12/01/16 Pct Recovery = 97% Analysis Date = 11/29/16 Pct Recovery = 96% Analysis Date = 11/29/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/24/16 Pct Recovery = 96% Analysis Date = 11/24/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/15/16 Pct Recovery = 95% Analysis Date = 11/15/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/04/16 Pct Recovery = 93% Analysis Date = 11/04/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/30/16 Pct Recovery = 93% Analysis Date = 10/30/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 90% Analysis Date = 10/12/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/06/16 Pct Recovery = 89% Analysis Date = 10/03/16 Pct Recovery = 89% Analysis Date = 10/03/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 88% Analysis Date = 09/27/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 88% Analysis Date = 09/22/16 Pct Recovery = 88% Analysis Date = 09/22/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/13/16 Pct Recovery = 86% Analysis Date = 09/13/16 Pct Recovery = 86% Analysis Date = 09/11/16 Pct Recovery = 86% Analysis Date = 09/11/16 Pct Recovery = 86% Analysis Date = 09/09/16 Pct Recovery = 86% Analysis Date = 09/09/16 Pct Recovery = 86% Analysis Date = 09/07/16 Pct Recovery = 86% Analysis Date = 09/07/16 Pct Recovery = 86% Analysis Date = 09/04/16 Pct Recovery = 85% Analysis Date = 09/04/16 Pct Recovery = 85% Analysis Date = 09/02/16 Pct Recovery = 85% Analysis Date = 09/02/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/29/16 Pct Recovery = 85% Analysis Date = 08/29/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/24/16 Pct Recovery = 85% Analysis Date = 08/24/16 Pct Recovery = 85% Analysis Date = 08/22/16 Pct Recovery = 85% Analysis Date = 08/22/16 Pct Recovery = 85% Analysis Date = 08/20/16 Pct Recovery = 85% Analysis Date = 08/20/16 Pct Recovery = 85% Analysis Date = 08/17/16 Pct Recovery = 85% Analysis Date = 08/17/16 Pct Recovery = 85% Analysis Date = 08/15/16 Pct Recovery = 85% Analysis Date = 08/15/16 Pct Recovery = 85% Analysis Date = 08/13/16 Pct Recovery = 85% Analysis Date = 08/13/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/11/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 08/08/16 Pct Recovery = 85% Analysis Date = 08/06/16 Pct Recovery = 85% Analysis Date = 08/06/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 08/04/16 Pct Recovery = 85% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 07/30/16 Pct Recovery = 85% Analysis Date = 07/30/16 Pct Recovery = 85% Analysis Date = 07/28/16 Pct Recovery = 85% Analysis Date = 07/28/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/26/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 85% Analysis Date = 07/21/16 Pct Recovery = 85% Analysis Date = 07/19/16 Pct Recovery = 86% Analysis Date = 07/19/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/12/16 Pct Recovery = 86% Analysis Date = 07/12/16 Pct Recovery = 86% Analysis Date = 07/10/16 Pct Recovery = 86% Analysis Date = 07/10/16 Pct Recovery = 86% Analysis Date = 07/08/16 Pct Recovery = 86% Analysis Date = 07/08/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/03/16 Pct Recovery = 86% Analysis Date = 07/03/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/24/16 Pct Recovery = 86% Analysis Date = 06/24/16 Pct Recovery = 86% Analysis Date = 06/22/16 Pct Recovery = 86% Analysis Date = 06/22/16 Pct Recovery = 86% Analysis Date = 06/20/16 Pct Recovery = 86% Analysis Date = 06/20/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 06/02/16 Pct Recovery = 86% Analysis Date = 05/31/16 Pct Recovery = 86% Analysis Date = 05/31/16 Pct Recovery = 86% Analysis Date = 05/29/16 Pct Recovery = 86% Analysis Date = 05/29/16 Pct Recovery = 86% Analysis Date = 05/26/16 Pct Recovery = 86% Analysis Date = 05/26/16 Pct Recovery = 86% Analysis Date = 05/24/16 Pct Recovery = 86% Analysis Date = 05/24/16 Pct Recovery = 86% Analysis Date = 05/22/16 Pct Recovery = 87% Analysis Date = 05/22/16 Pct Recovery = 87% Analysis Date = 05/20/16 Pct Recovery = 87% Analysis Date = 05/20/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/15/16 Pct Recovery = 87% Analysis Date = 05/15/16 Pct Recovery = 87% Analysis Date = 05/13/16 Pct Recovery = 87% Analysis Date = 05/13/16 Pct Recovery = 87% Analysis Date = 05/11/16 Pct Recovery = 87% Analysis Date = 05/11/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/06/16 Pct Recovery = 87% Analysis Date = 05/06/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 05/04/16 Pct Recovery = 87% Analysis Date = 05/02/16 Pct Recovery = 88% Analysis Date = 05/02/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/29/16 Pct Recovery = 88% Analysis Date = 04/27/16 Pct Recovery = 88% Analysis Date = 04/27/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 88% Analysis Date = 04/25/16 Pct Recovery = 88% Analysis Date = 04/23/16 Pct Recovery = 88% Analysis Date = 04/23/16 Pct Recovery = 88% Analysis Date = 04/20/16 Pct Recovery = 88% Analysis Date = 04/20/16 Pct Recovery = 88% Analysis Date = 04/18/16 Pct Recovery = 88% Analysis Date = 04/18/16 Pct Recovery = 88% Analysis Date = 04/16/16 Pct Recovery = 88% Analysis Date = 04/16/16 Pct Recovery = 88% Analysis Date = 04/14/16 Pct Recovery = 89% Analysis Date = 04/14/16 Pct Recovery = 89% Analysis Date = 04/11/16 Pct Recovery = 89% Analysis Date = 04/11/16 Pct Recovery = 89% Analysis Date = 04/09/16 Pct Recovery = 89% Analysis Date = 04/09/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/05/16 Pct Recovery = 89% Analysis Date = 04/05/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 04/02/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 89% Analysis Date = 03/31/16 Pct Recovery = 89% Analysis Date = 03/29/16 Pct Recovery = 89% Analysis Date = 03/29/16 Pct Recovery = 89% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/24/16 Pct Recovery = 90% Analysis Date = 03/22/16 Pct Recovery = 90% Analysis Date = 03/22/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/20/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/18/16 Pct Recovery = 90% Analysis Date = 03/15/16 Pct Recovery = 90% Analysis Date = 03/15/16 Pct Recovery = 90% Analysis Date = 03/13/16 Pct Recovery = 90% Analysis Date = 03/13/16 Pct Recovery = 90% Analysis Date = 03/11/16 Pct Recovery = 90% Analysis Date = 03/11/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/26/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/24/16 Pct Recovery = 91% Analysis Date = 02/22/16 Pct Recovery = 91% Analysis Date = 02/22/16 Pct Recovery = 91% Analysis Date = 02/20/16 Pct Recovery = 91% Analysis Date = 02/20/16 Pct Recovery = 91% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/17/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 92% Analysis Date = 02/13/16 Pct Recovery = 92% Analysis Date = 02/13/16 Pct Recovery = 92% Analysis Date = 02/11/16 Pct Recovery = 92% Analysis Date = 02/11/16 Pct Recovery = 92% Analysis Date = 02/09/16 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 94% 14% 95% 11%
Total 18 94% 14% 95% 11%

Sample Statistics
ALACHLOR

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
ALPHA-ENDOSULFAN (ENDOSULFAN I)
METHOD: 2033 , TESTIDCODE: 34362GCM39

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 108% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 109% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 72% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 78% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 85% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 66% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 79% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 90% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 99% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 108% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 101% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 94% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 05/10/17 Pct Recovery = 88% Analysis Date = 05/08/17 Pct Recovery = 88% Analysis Date = 05/08/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 05/04/17 Pct Recovery = 88% Analysis Date = 05/04/17 Pct Recovery = 88% Analysis Date = 05/01/17 Pct Recovery = 88% Analysis Date = 05/01/17 Pct Recovery = 88% Analysis Date = 04/29/17 Pct Recovery = 88% Analysis Date = 04/29/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/25/17 Pct Recovery = 88% Analysis Date = 04/25/17 Pct Recovery = 88% Analysis Date = 04/22/17 Pct Recovery = 88% Analysis Date = 04/22/17 Pct Recovery = 88% Analysis Date = 04/20/17 Pct Recovery = 89% Analysis Date = 04/20/17 Pct Recovery = 89% Analysis Date = 04/18/17 Pct Recovery = 89% Analysis Date = 04/18/17 Pct Recovery = 89% Analysis Date = 04/15/17 Pct Recovery = 89% Analysis Date = 04/15/17 Pct Recovery = 89% Analysis Date = 04/13/17 Pct Recovery = 89% Analysis Date = 04/13/17 Pct Recovery = 89% Analysis Date = 04/11/17 Pct Recovery = 89% Analysis Date = 04/11/17 Pct Recovery = 89% Analysis Date = 04/09/17 Pct Recovery = 89% Analysis Date = 04/09/17 Pct Recovery = 89% Analysis Date = 04/06/17 Pct Recovery = 89% Analysis Date = 04/06/17 Pct Recovery = 89% Analysis Date = 04/04/17 Pct Recovery = 89% Analysis Date = 04/04/17 Pct Recovery = 89% Analysis Date = 04/02/17 Pct Recovery = 89% Analysis Date = 04/02/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 90% Analysis Date = 03/14/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/01/17 Pct Recovery = 91% Analysis Date = 02/01/17 Pct Recovery = 91% Analysis Date = 01/30/17 Pct Recovery = 91% Analysis Date = 01/30/17 Pct Recovery = 91% Analysis Date = 01/28/17 Pct Recovery = 91% Analysis Date = 01/28/17 Pct Recovery = 91% Analysis Date = 01/25/17 Pct Recovery = 91% Analysis Date = 01/25/17 Pct Recovery = 91% Analysis Date = 01/23/17 Pct Recovery = 91% Analysis Date = 01/23/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/19/17 Pct Recovery = 92% Analysis Date = 01/19/17 Pct Recovery = 92% Analysis Date = 01/16/17 Pct Recovery = 92% Analysis Date = 01/16/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 92% Analysis Date = 01/12/17 Pct Recovery = 92% Analysis Date = 01/12/17 Pct Recovery = 92% Analysis Date = 01/09/17 Pct Recovery = 92% Analysis Date = 01/09/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 93% Analysis Date = 12/20/16 Pct Recovery = 93% Analysis Date = 12/20/16 Pct Recovery = 93% Analysis Date = 12/18/16 Pct Recovery = 93% Analysis Date = 12/18/16 Pct Recovery = 93% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/13/16 Pct Recovery = 93% Analysis Date = 12/13/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/08/16 Pct Recovery = 93% Analysis Date = 12/08/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 92% Analysis Date = 12/02/16 Pct Recovery = 92% Analysis Date = 12/02/16 Pct Recovery = 92% Analysis Date = 11/29/16 Pct Recovery = 92% Analysis Date = 11/29/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/27/16 Pct Recovery = 92% Analysis Date = 11/25/16 Pct Recovery = 92% Analysis Date = 11/25/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/22/16 Pct Recovery = 92% Analysis Date = 11/20/16 Pct Recovery = 92% Analysis Date = 11/20/16 Pct Recovery = 92% Analysis Date = 11/18/16 Pct Recovery = 92% Analysis Date = 11/18/16 Pct Recovery = 92% Analysis Date = 11/16/16 Pct Recovery = 92% Analysis Date = 11/16/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/13/16 Pct Recovery = 92% Analysis Date = 11/11/16 Pct Recovery = 92% Analysis Date = 11/11/16 Pct Recovery = 92% Analysis Date = 11/09/16 Pct Recovery = 92% Analysis Date = 11/09/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/24/16 Pct Recovery = 91% Analysis Date = 09/24/16 Pct Recovery = 91% Analysis Date = 09/22/16 Pct Recovery = 91% Analysis Date = 09/22/16 Pct Recovery = 91% Analysis Date = 09/19/16 Pct Recovery = 91% Analysis Date = 09/19/16 Pct Recovery = 91% Analysis Date = 09/17/16 Pct Recovery = 91% Analysis Date = 09/17/16 Pct Recovery = 91% Analysis Date = 09/15/16 Pct Recovery = 91% Analysis Date = 09/15/16 Pct Recovery = 91% Analysis Date = 09/13/16 Pct Recovery = 91% Analysis Date = 09/13/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/10/16 Pct Recovery = 91% Analysis Date = 09/08/16 Pct Recovery = 91% Analysis Date = 09/08/16 Pct Recovery = 91% Analysis Date = 09/06/16 Pct Recovery = 91% Analysis Date = 09/06/16 Pct Recovery = 91% Analysis Date = 09/03/16 Pct Recovery = 91% Analysis Date = 09/03/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 90% Analysis Date = 08/28/16 Pct Recovery = 90% Analysis Date = 08/25/16 Pct Recovery = 90% Analysis Date = 08/25/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/18/16 Pct Recovery = 90% Analysis Date = 08/18/16 Pct Recovery = 90% Analysis Date = 08/16/16 Pct Recovery = 90% Analysis Date = 08/16/16 Pct Recovery = 90% Analysis Date = 08/14/16 Pct Recovery = 90% Analysis Date = 08/14/16 Pct Recovery = 90% Analysis Date = 08/12/16 Pct Recovery = 89% Analysis Date = 08/12/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/07/16 Pct Recovery = 89% Analysis Date = 08/07/16 Pct Recovery = 89% Analysis Date = 08/05/16 Pct Recovery = 89% Analysis Date = 08/05/16 Pct Recovery = 89% Analysis Date = 08/02/16 Pct Recovery = 89% Analysis Date = 08/02/16 Pct Recovery = 89% Analysis Date = 07/31/16 Pct Recovery = 89% Analysis Date = 07/31/16 Pct Recovery = 89% Analysis Date = 07/29/16 Pct Recovery = 89% Analysis Date = 07/29/16 Pct Recovery = 89% Analysis Date = 07/27/16 Pct Recovery = 89% Analysis Date = 07/27/16 Pct Recovery = 89% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/24/16 Pct Recovery = 88% Analysis Date = 07/22/16 Pct Recovery = 88% Analysis Date = 07/22/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 88% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/04/16 Pct Recovery = 87% Analysis Date = 07/04/16 Pct Recovery = 87% Analysis Date = 07/01/16 Pct Recovery = 87% Analysis Date = 07/01/16 Pct Recovery = 87% Analysis Date = 06/29/16 Pct Recovery = 87% Analysis Date = 06/29/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/25/16 Pct Recovery = 87% Analysis Date = 06/25/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/20/16 Pct Recovery = 86% Analysis Date = 06/20/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/09/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/06/16 Pct Recovery = 86% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/26/16 Pct Recovery = 85% Analysis Date = 05/26/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 86% Analysis Date = 05/24/16 Pct Recovery = 86% Analysis Date = 05/21/16 Pct Recovery = 86% Analysis Date = 05/21/16 Pct Recovery = 86% Analysis Date = 05/19/16 Pct Recovery = 86% Analysis Date = 05/19/16 Pct Recovery = 86% Analysis Date = 05/17/16 Pct Recovery = 86% Analysis Date = 05/17/16 Pct Recovery = 86% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 88% Analysis Date = 05/08/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/05/16 Pct Recovery = 88% Analysis Date = 05/03/16 Pct Recovery = 88% Analysis Date = 05/03/16 Pct Recovery = 88% Analysis Date = 05/01/16 Pct Recovery = 88% Analysis Date = 05/01/16 Pct Recovery = 88% Analysis Date = 04/28/16 Pct Recovery = 88% Analysis Date = 04/28/16 Pct Recovery = 88% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/19/16 Pct Recovery = 89% Analysis Date = 04/19/16 Pct Recovery = 89% Analysis Date = 04/17/16 Pct Recovery = 89% Analysis Date = 04/17/16 Pct Recovery = 89% Analysis Date = 04/15/16 Pct Recovery = 89% Analysis Date = 04/15/16 Pct Recovery = 89% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/08/16 Pct Recovery = 90% Analysis Date = 04/08/16 Pct Recovery = 90% Analysis Date = 04/06/16 Pct Recovery = 90% Analysis Date = 04/06/16 Pct Recovery = 90% Analysis Date = 04/03/16 Pct Recovery = 90% Analysis Date = 04/03/16 Pct Recovery = 90% Analysis Date = 04/01/16 Pct Recovery = 90% Analysis Date = 04/01/16 Pct Recovery = 90% Analysis Date = 03/30/16 Pct Recovery = 90% Analysis Date = 03/30/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/27/16 Pct Recovery = 90% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/23/16 Pct Recovery = 91% Analysis Date = 03/23/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/18/16 Pct Recovery = 91% Analysis Date = 03/18/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/16/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/11/16 Pct Recovery = 91% Analysis Date = 03/11/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 91% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/07/16 Pct Recovery = 92% Analysis Date = 03/05/16 Pct Recovery = 92% Analysis Date = 03/05/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 03/02/16 Pct Recovery = 92% Analysis Date = 02/29/16 Pct Recovery = 92% Analysis Date = 02/29/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/27/16 Pct Recovery = 92% Analysis Date = 02/24/16 Pct Recovery = 92% Analysis Date = 02/24/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 92% Analysis Date = 02/20/16 Pct Recovery = 92% Analysis Date = 02/20/16 Pct Recovery = 92% Analysis Date = 02/18/16 Pct Recovery = 92% Analysis Date = 02/18/16 Pct Recovery = 92% Analysis Date = 02/15/16 Pct Recovery = 93% Analysis Date = 02/15/16 Pct Recovery = 93% Analysis Date = 02/13/16 Pct Recovery = 93% Analysis Date = 02/13/16 Pct Recovery = 93% Analysis Date = 02/11/16 Pct Recovery = 93% Analysis Date = 02/11/16 Pct Recovery = 93% Analysis Date = 02/09/16 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 94% 6% 92% 6%
>= Reporting Level 16 88% 13% 87% 14%
Total 20 89% 12% 89% 13%

Sample Statistics
ALPHA-ENDOSULFAN (ENDOSULFAN I)

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
ATRAZINE
METHOD: 2033 , TESTIDCODE: 39632GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 118% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 102% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 86% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 107% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 70% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 92% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 114% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 106% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 88% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 82% Analysis Date = 05/02/17 Pct Recovery = 94% Analysis Date = 04/30/17 Pct Recovery = 94% Analysis Date = 04/30/17 Pct Recovery = 94% Analysis Date = 04/28/17 Pct Recovery = 94% Analysis Date = 04/28/17 Pct Recovery = 94% Analysis Date = 04/26/17 Pct Recovery = 95% Analysis Date = 04/26/17 Pct Recovery = 95% Analysis Date = 04/24/17 Pct Recovery = 95% Analysis Date = 04/24/17 Pct Recovery = 95% Analysis Date = 04/22/17 Pct Recovery = 95% Analysis Date = 04/22/17 Pct Recovery = 95% Analysis Date = 04/20/17 Pct Recovery = 96% Analysis Date = 04/20/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/11/17 Pct Recovery = 97% Analysis Date = 04/11/17 Pct Recovery = 97% Analysis Date = 04/09/17 Pct Recovery = 97% Analysis Date = 04/09/17 Pct Recovery = 97% Analysis Date = 04/07/17 Pct Recovery = 97% Analysis Date = 04/07/17 Pct Recovery = 97% Analysis Date = 04/05/17 Pct Recovery = 98% Analysis Date = 04/05/17 Pct Recovery = 98% Analysis Date = 04/03/17 Pct Recovery = 98% Analysis Date = 04/03/17 Pct Recovery = 98% Analysis Date = 03/31/17 Pct Recovery = 98% Analysis Date = 03/31/17 Pct Recovery = 98% Analysis Date = 03/29/17 Pct Recovery = 98% Analysis Date = 03/29/17 Pct Recovery = 98% Analysis Date = 03/27/17 Pct Recovery = 99% Analysis Date = 03/27/17 Pct Recovery = 99% Analysis Date = 03/25/17 Pct Recovery = 99% Analysis Date = 03/25/17 Pct Recovery = 99% Analysis Date = 03/23/17 Pct Recovery = 99% Analysis Date = 03/23/17 Pct Recovery = 99% Analysis Date = 03/21/17 Pct Recovery = 99% Analysis Date = 03/21/17 Pct Recovery = 99% Analysis Date = 03/19/17 Pct Recovery = 100% Analysis Date = 03/19/17 Pct Recovery = 100% Analysis Date = 03/17/17 Pct Recovery = 100% Analysis Date = 03/17/17 Pct Recovery = 100% Analysis Date = 03/14/17 Pct Recovery = 100% Analysis Date = 03/14/17 Pct Recovery = 100% Analysis Date = 03/12/17 Pct Recovery = 101% Analysis Date = 03/12/17 Pct Recovery = 101% Analysis Date = 03/10/17 Pct Recovery = 101% Analysis Date = 03/10/17 Pct Recovery = 101% Analysis Date = 03/08/17 Pct Recovery = 101% Analysis Date = 03/08/17 Pct Recovery = 101% Analysis Date = 03/06/17 Pct Recovery = 101% Analysis Date = 03/06/17 Pct Recovery = 101% Analysis Date = 03/04/17 Pct Recovery = 102% Analysis Date = 03/04/17 Pct Recovery = 102% Analysis Date = 03/02/17 Pct Recovery = 102% Analysis Date = 03/02/17 Pct Recovery = 102% Analysis Date = 02/27/17 Pct Recovery = 102% Analysis Date = 02/27/17 Pct Recovery = 102% Analysis Date = 02/25/17 Pct Recovery = 102% Analysis Date = 02/25/17 Pct Recovery = 102% Analysis Date = 02/23/17 Pct Recovery = 102% Analysis Date = 02/23/17 Pct Recovery = 102% Analysis Date = 02/21/17 Pct Recovery = 103% Analysis Date = 02/21/17 Pct Recovery = 103% Analysis Date = 02/19/17 Pct Recovery = 103% Analysis Date = 02/19/17 Pct Recovery = 103% Analysis Date = 02/17/17 Pct Recovery = 103% Analysis Date = 02/17/17 Pct Recovery = 103% Analysis Date = 02/15/17 Pct Recovery = 103% Analysis Date = 02/15/17 Pct Recovery = 103% Analysis Date = 02/13/17 Pct Recovery = 103% Analysis Date = 02/13/17 Pct Recovery = 103% Analysis Date = 02/10/17 Pct Recovery = 103% Analysis Date = 02/10/17 Pct Recovery = 103% Analysis Date = 02/08/17 Pct Recovery = 103% Analysis Date = 02/08/17 Pct Recovery = 103% Analysis Date = 02/06/17 Pct Recovery = 103% Analysis Date = 02/06/17 Pct Recovery = 103% Analysis Date = 02/04/17 Pct Recovery = 103% Analysis Date = 02/04/17 Pct Recovery = 103% Analysis Date = 02/02/17 Pct Recovery = 103% Analysis Date = 02/02/17 Pct Recovery = 103% Analysis Date = 01/31/17 Pct Recovery = 103% Analysis Date = 01/31/17 Pct Recovery = 103% Analysis Date = 01/29/17 Pct Recovery = 103% Analysis Date = 01/29/17 Pct Recovery = 103% Analysis Date = 01/26/17 Pct Recovery = 103% Analysis Date = 01/26/17 Pct Recovery = 103% Analysis Date = 01/24/17 Pct Recovery = 104% Analysis Date = 01/24/17 Pct Recovery = 104% Analysis Date = 01/22/17 Pct Recovery = 104% Analysis Date = 01/22/17 Pct Recovery = 104% Analysis Date = 01/20/17 Pct Recovery = 104% Analysis Date = 01/20/17 Pct Recovery = 104% Analysis Date = 01/18/17 Pct Recovery = 104% Analysis Date = 01/18/17 Pct Recovery = 104% Analysis Date = 01/16/17 Pct Recovery = 104% Analysis Date = 01/16/17 Pct Recovery = 104% Analysis Date = 01/14/17 Pct Recovery = 104% Analysis Date = 01/14/17 Pct Recovery = 104% Analysis Date = 01/11/17 Pct Recovery = 104% Analysis Date = 01/11/17 Pct Recovery = 104% Analysis Date = 01/09/17 Pct Recovery = 104% Analysis Date = 01/09/17 Pct Recovery = 104% Analysis Date = 01/07/17 Pct Recovery = 104% Analysis Date = 01/07/17 Pct Recovery = 104% Analysis Date = 01/05/17 Pct Recovery = 104% Analysis Date = 01/05/17 Pct Recovery = 104% Analysis Date = 01/03/17 Pct Recovery = 104% Analysis Date = 01/03/17 Pct Recovery = 104% Analysis Date = 01/01/17 Pct Recovery = 104% Analysis Date = 01/01/17 Pct Recovery = 104% Analysis Date = 12/30/16 Pct Recovery = 104% Analysis Date = 12/30/16 Pct Recovery = 104% Analysis Date = 12/28/16 Pct Recovery = 104% Analysis Date = 12/28/16 Pct Recovery = 104% Analysis Date = 12/25/16 Pct Recovery = 104% Analysis Date = 12/25/16 Pct Recovery = 104% Analysis Date = 12/23/16 Pct Recovery = 104% Analysis Date = 12/23/16 Pct Recovery = 104% Analysis Date = 12/21/16 Pct Recovery = 104% Analysis Date = 12/21/16 Pct Recovery = 104% Analysis Date = 12/19/16 Pct Recovery = 104% Analysis Date = 12/19/16 Pct Recovery = 104% Analysis Date = 12/17/16 Pct Recovery = 103% Analysis Date = 12/17/16 Pct Recovery = 103% Analysis Date = 12/15/16 Pct Recovery = 103% Analysis Date = 12/15/16 Pct Recovery = 103% Analysis Date = 12/13/16 Pct Recovery = 103% Analysis Date = 12/13/16 Pct Recovery = 103% Analysis Date = 12/10/16 Pct Recovery = 102% Analysis Date = 12/10/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/06/16 Pct Recovery = 101% Analysis Date = 12/06/16 Pct Recovery = 101% Analysis Date = 12/04/16 Pct Recovery = 101% Analysis Date = 12/04/16 Pct Recovery = 101% Analysis Date = 12/02/16 Pct Recovery = 101% Analysis Date = 12/02/16 Pct Recovery = 101% Analysis Date = 11/30/16 Pct Recovery = 100% Analysis Date = 11/30/16 Pct Recovery = 100% Analysis Date = 11/28/16 Pct Recovery = 100% Analysis Date = 11/28/16 Pct Recovery = 100% Analysis Date = 11/26/16 Pct Recovery = 100% Analysis Date = 11/26/16 Pct Recovery = 100% Analysis Date = 11/23/16 Pct Recovery = 99% Analysis Date = 11/23/16 Pct Recovery = 99% Analysis Date = 11/21/16 Pct Recovery = 99% Analysis Date = 11/21/16 Pct Recovery = 99% Analysis Date = 11/19/16 Pct Recovery = 98% Analysis Date = 11/19/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/15/16 Pct Recovery = 98% Analysis Date = 11/15/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/11/16 Pct Recovery = 97% Analysis Date = 11/11/16 Pct Recovery = 97% Analysis Date = 11/08/16 Pct Recovery = 96% Analysis Date = 11/08/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 10/31/16 Pct Recovery = 95% Analysis Date = 10/31/16 Pct Recovery = 95% Analysis Date = 10/29/16 Pct Recovery = 95% Analysis Date = 10/29/16 Pct Recovery = 95% Analysis Date = 10/27/16 Pct Recovery = 94% Analysis Date = 10/27/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/22/16 Pct Recovery = 93% Analysis Date = 10/22/16 Pct Recovery = 93% Analysis Date = 10/20/16 Pct Recovery = 93% Analysis Date = 10/20/16 Pct Recovery = 93% Analysis Date = 10/18/16 Pct Recovery = 93% Analysis Date = 10/18/16 Pct Recovery = 93% Analysis Date = 10/16/16 Pct Recovery = 92% Analysis Date = 10/16/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/07/16 Pct Recovery = 91% Analysis Date = 10/07/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/25/16 Pct Recovery = 88% Analysis Date = 09/25/16 Pct Recovery = 88% Analysis Date = 09/22/16 Pct Recovery = 88% Analysis Date = 09/22/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/20/16 Pct Recovery = 88% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 86% Analysis Date = 09/12/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 09/10/16 Pct Recovery = 86% Analysis Date = 09/08/16 Pct Recovery = 85% Analysis Date = 09/08/16 Pct Recovery = 85% Analysis Date = 09/05/16 Pct Recovery = 85% Analysis Date = 09/05/16 Pct Recovery = 85% Analysis Date = 09/03/16 Pct Recovery = 85% Analysis Date = 09/03/16 Pct Recovery = 85% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/26/16 Pct Recovery = 84% Analysis Date = 08/26/16 Pct Recovery = 84% Analysis Date = 08/24/16 Pct Recovery = 84% Analysis Date = 08/24/16 Pct Recovery = 84% Analysis Date = 08/21/16 Pct Recovery = 84% Analysis Date = 08/21/16 Pct Recovery = 84% Analysis Date = 08/19/16 Pct Recovery = 83% Analysis Date = 08/19/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/17/16 Pct Recovery = 83% Analysis Date = 08/15/16 Pct Recovery = 83% Analysis Date = 08/15/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/13/16 Pct Recovery = 83% Analysis Date = 08/11/16 Pct Recovery = 83% Analysis Date = 08/11/16 Pct Recovery = 83% Analysis Date = 08/09/16 Pct Recovery = 83% Analysis Date = 08/09/16 Pct Recovery = 83% Analysis Date = 08/06/16 Pct Recovery = 83% Analysis Date = 08/06/16 Pct Recovery = 83% Analysis Date = 08/04/16 Pct Recovery = 83% Analysis Date = 08/04/16 Pct Recovery = 83% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/29/16 Pct Recovery = 82% Analysis Date = 07/29/16 Pct Recovery = 82% Analysis Date = 07/27/16 Pct Recovery = 82% Analysis Date = 07/27/16 Pct Recovery = 82% Analysis Date = 07/25/16 Pct Recovery = 82% Analysis Date = 07/25/16 Pct Recovery = 82% Analysis Date = 07/23/16 Pct Recovery = 82% Analysis Date = 07/23/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/18/16 Pct Recovery = 82% Analysis Date = 07/18/16 Pct Recovery = 82% Analysis Date = 07/16/16 Pct Recovery = 82% Analysis Date = 07/16/16 Pct Recovery = 82% Analysis Date = 07/14/16 Pct Recovery = 81% Analysis Date = 07/14/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/10/16 Pct Recovery = 81% Analysis Date = 07/10/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/05/16 Pct Recovery = 81% Analysis Date = 07/05/16 Pct Recovery = 81% Analysis Date = 07/03/16 Pct Recovery = 81% Analysis Date = 07/03/16 Pct Recovery = 81% Analysis Date = 07/01/16 Pct Recovery = 81% Analysis Date = 07/01/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 80% Analysis Date = 06/25/16 Pct Recovery = 80% Analysis Date = 06/25/16 Pct Recovery = 80% Analysis Date = 06/23/16 Pct Recovery = 80% Analysis Date = 06/23/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/21/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/16/16 Pct Recovery = 80% Analysis Date = 06/14/16 Pct Recovery = 80% Analysis Date = 06/14/16 Pct Recovery = 80% Analysis Date = 06/12/16 Pct Recovery = 80% Analysis Date = 06/12/16 Pct Recovery = 80% Analysis Date = 06/10/16 Pct Recovery = 80% Analysis Date = 06/10/16 Pct Recovery = 80% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/08/16 Pct Recovery = 79% Analysis Date = 06/06/16 Pct Recovery = 79% Analysis Date = 06/06/16 Pct Recovery = 79% Analysis Date = 06/03/16 Pct Recovery = 79% Analysis Date = 06/03/16 Pct Recovery = 79% Analysis Date = 06/01/16 Pct Recovery = 79% Analysis Date = 06/01/16 Pct Recovery = 79% Analysis Date = 05/30/16 Pct Recovery = 79% Analysis Date = 05/30/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/28/16 Pct Recovery = 79% Analysis Date = 05/26/16 Pct Recovery = 79% Analysis Date = 05/26/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/22/16 Pct Recovery = 80% Analysis Date = 05/22/16 Pct Recovery = 80% Analysis Date = 05/19/16 Pct Recovery = 80% Analysis Date = 05/19/16 Pct Recovery = 80% Analysis Date = 05/17/16 Pct Recovery = 80% Analysis Date = 05/17/16 Pct Recovery = 80% Analysis Date = 05/15/16 Pct Recovery = 80% Analysis Date = 05/15/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/13/16 Pct Recovery = 80% Analysis Date = 05/11/16 Pct Recovery = 80% Analysis Date = 05/11/16 Pct Recovery = 80% Analysis Date = 05/09/16 Pct Recovery = 81% Analysis Date = 05/09/16 Pct Recovery = 81% Analysis Date = 05/07/16 Pct Recovery = 81% Analysis Date = 05/07/16 Pct Recovery = 81% Analysis Date = 05/05/16 Pct Recovery = 81% Analysis Date = 05/05/16 Pct Recovery = 81% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/26/16 Pct Recovery = 82% Analysis Date = 04/26/16 Pct Recovery = 82% Analysis Date = 04/24/16 Pct Recovery = 82% Analysis Date = 04/24/16 Pct Recovery = 82% Analysis Date = 04/22/16 Pct Recovery = 82% Analysis Date = 04/22/16 Pct Recovery = 82% Analysis Date = 04/20/16 Pct Recovery = 82% Analysis Date = 04/20/16 Pct Recovery = 82% Analysis Date = 04/17/16 Pct Recovery = 82% Analysis Date = 04/17/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/15/16 Pct Recovery = 82% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/13/16 Pct Recovery = 83% Analysis Date = 04/11/16 Pct Recovery = 83% Analysis Date = 04/11/16 Pct Recovery = 83% Analysis Date = 04/09/16 Pct Recovery = 83% Analysis Date = 04/09/16 Pct Recovery = 83% Analysis Date = 04/07/16 Pct Recovery = 83% Analysis Date = 04/07/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/31/16 Pct Recovery = 84% Analysis Date = 03/29/16 Pct Recovery = 84% Analysis Date = 03/29/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/21/16 Pct Recovery = 84% Analysis Date = 03/21/16 Pct Recovery = 84% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/12/16 Pct Recovery = 85% Analysis Date = 03/10/16 Pct Recovery = 85% Analysis Date = 03/10/16 Pct Recovery = 85% Analysis Date = 03/08/16 Pct Recovery = 85% Analysis Date = 03/08/16 Pct Recovery = 85% Analysis Date = 03/06/16 Pct Recovery = 85% Analysis Date = 03/06/16 Pct Recovery = 85% Analysis Date = 03/04/16 Pct Recovery = 85% Analysis Date = 03/04/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 91% 15% 88% 20%
Total 18 91% 15% 88% 20%

Sample Statistics
ATRAZINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
AZINPHOS-METHYL
METHOD: 2033 , TESTIDCODE: 82686GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 66% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 92% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 68% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 74% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 86% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 66% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 89% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 66% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 81% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 56% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 77% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 45% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 63% Analysis Date = 05/10/17 Pct Recovery = 71% Analysis Date = 05/08/17 Pct Recovery = 71% Analysis Date = 05/08/17 Pct Recovery = 71% Analysis Date = 05/06/17 Pct Recovery = 71% Analysis Date = 05/06/17 Pct Recovery = 71% Analysis Date = 05/04/17 Pct Recovery = 71% Analysis Date = 05/04/17 Pct Recovery = 71% Analysis Date = 05/01/17 Pct Recovery = 71% Analysis Date = 05/01/17 Pct Recovery = 71% Analysis Date = 04/29/17 Pct Recovery = 71% Analysis Date = 04/29/17 Pct Recovery = 71% Analysis Date = 04/27/17 Pct Recovery = 71% Analysis Date = 04/27/17 Pct Recovery = 71% Analysis Date = 04/25/17 Pct Recovery = 71% Analysis Date = 04/25/17 Pct Recovery = 71% Analysis Date = 04/22/17 Pct Recovery = 71% Analysis Date = 04/22/17 Pct Recovery = 71% Analysis Date = 04/20/17 Pct Recovery = 71% Analysis Date = 04/20/17 Pct Recovery = 71% Analysis Date = 04/18/17 Pct Recovery = 71% Analysis Date = 04/18/17 Pct Recovery = 71% Analysis Date = 04/15/17 Pct Recovery = 71% Analysis Date = 04/15/17 Pct Recovery = 71% Analysis Date = 04/13/17 Pct Recovery = 71% Analysis Date = 04/13/17 Pct Recovery = 71% Analysis Date = 04/11/17 Pct Recovery = 71% Analysis Date = 04/11/17 Pct Recovery = 71% Analysis Date = 04/09/17 Pct Recovery = 71% Analysis Date = 04/09/17 Pct Recovery = 71% Analysis Date = 04/06/17 Pct Recovery = 70% Analysis Date = 04/06/17 Pct Recovery = 70% Analysis Date = 04/04/17 Pct Recovery = 70% Analysis Date = 04/04/17 Pct Recovery = 70% Analysis Date = 04/02/17 Pct Recovery = 70% Analysis Date = 04/02/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/26/17 Pct Recovery = 70% Analysis Date = 03/26/17 Pct Recovery = 70% Analysis Date = 03/24/17 Pct Recovery = 70% Analysis Date = 03/24/17 Pct Recovery = 70% Analysis Date = 03/21/17 Pct Recovery = 70% Analysis Date = 03/21/17 Pct Recovery = 70% Analysis Date = 03/19/17 Pct Recovery = 70% Analysis Date = 03/19/17 Pct Recovery = 70% Analysis Date = 03/17/17 Pct Recovery = 70% Analysis Date = 03/17/17 Pct Recovery = 70% Analysis Date = 03/14/17 Pct Recovery = 70% Analysis Date = 03/14/17 Pct Recovery = 70% Analysis Date = 03/12/17 Pct Recovery = 70% Analysis Date = 03/12/17 Pct Recovery = 70% Analysis Date = 03/10/17 Pct Recovery = 70% Analysis Date = 03/10/17 Pct Recovery = 70% Analysis Date = 03/08/17 Pct Recovery = 70% Analysis Date = 03/08/17 Pct Recovery = 70% Analysis Date = 03/05/17 Pct Recovery = 70% Analysis Date = 03/05/17 Pct Recovery = 70% Analysis Date = 03/03/17 Pct Recovery = 70% Analysis Date = 03/03/17 Pct Recovery = 70% Analysis Date = 03/01/17 Pct Recovery = 69% Analysis Date = 03/01/17 Pct Recovery = 69% Analysis Date = 02/26/17 Pct Recovery = 69% Analysis Date = 02/26/17 Pct Recovery = 69% Analysis Date = 02/24/17 Pct Recovery = 69% Analysis Date = 02/24/17 Pct Recovery = 69% Analysis Date = 02/22/17 Pct Recovery = 69% Analysis Date = 02/22/17 Pct Recovery = 69% Analysis Date = 02/20/17 Pct Recovery = 69% Analysis Date = 02/20/17 Pct Recovery = 69% Analysis Date = 02/17/17 Pct Recovery = 68% Analysis Date = 02/17/17 Pct Recovery = 68% Analysis Date = 02/15/17 Pct Recovery = 68% Analysis Date = 02/15/17 Pct Recovery = 68% Analysis Date = 02/13/17 Pct Recovery = 68% Analysis Date = 02/13/17 Pct Recovery = 68% Analysis Date = 02/10/17 Pct Recovery = 67% Analysis Date = 02/10/17 Pct Recovery = 67% Analysis Date = 02/08/17 Pct Recovery = 67% Analysis Date = 02/08/17 Pct Recovery = 67% Analysis Date = 02/06/17 Pct Recovery = 67% Analysis Date = 02/06/17 Pct Recovery = 67% Analysis Date = 02/04/17 Pct Recovery = 66% Analysis Date = 02/04/17 Pct Recovery = 66% Analysis Date = 02/01/17 Pct Recovery = 66% Analysis Date = 02/01/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 65% Analysis Date = 01/30/17 Pct Recovery = 65% Analysis Date = 01/28/17 Pct Recovery = 65% Analysis Date = 01/28/17 Pct Recovery = 65% Analysis Date = 01/25/17 Pct Recovery = 65% Analysis Date = 01/25/17 Pct Recovery = 65% Analysis Date = 01/23/17 Pct Recovery = 64% Analysis Date = 01/23/17 Pct Recovery = 64% Analysis Date = 01/21/17 Pct Recovery = 64% Analysis Date = 01/21/17 Pct Recovery = 64% Analysis Date = 01/19/17 Pct Recovery = 63% Analysis Date = 01/19/17 Pct Recovery = 63% Analysis Date = 01/16/17 Pct Recovery = 63% Analysis Date = 01/16/17 Pct Recovery = 63% Analysis Date = 01/14/17 Pct Recovery = 64% Analysis Date = 01/14/17 Pct Recovery = 64% Analysis Date = 01/12/17 Pct Recovery = 64% Analysis Date = 01/12/17 Pct Recovery = 64% Analysis Date = 01/09/17 Pct Recovery = 64% Analysis Date = 01/09/17 Pct Recovery = 64% Analysis Date = 01/07/17 Pct Recovery = 64% Analysis Date = 01/07/17 Pct Recovery = 64% Analysis Date = 01/05/17 Pct Recovery = 64% Analysis Date = 01/05/17 Pct Recovery = 64% Analysis Date = 01/03/17 Pct Recovery = 65% Analysis Date = 01/03/17 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/31/16 Pct Recovery = 65% Analysis Date = 12/29/16 Pct Recovery = 65% Analysis Date = 12/29/16 Pct Recovery = 65% Analysis Date = 12/27/16 Pct Recovery = 65% Analysis Date = 12/27/16 Pct Recovery = 65% Analysis Date = 12/24/16 Pct Recovery = 65% Analysis Date = 12/24/16 Pct Recovery = 65% Analysis Date = 12/22/16 Pct Recovery = 66% Analysis Date = 12/22/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/18/16 Pct Recovery = 66% Analysis Date = 12/18/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 66% Analysis Date = 12/13/16 Pct Recovery = 66% Analysis Date = 12/13/16 Pct Recovery = 66% Analysis Date = 12/11/16 Pct Recovery = 67% Analysis Date = 12/11/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/06/16 Pct Recovery = 67% Analysis Date = 12/06/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 67% Analysis Date = 12/02/16 Pct Recovery = 68% Analysis Date = 12/02/16 Pct Recovery = 68% Analysis Date = 11/29/16 Pct Recovery = 68% Analysis Date = 11/29/16 Pct Recovery = 68% Analysis Date = 11/27/16 Pct Recovery = 68% Analysis Date = 11/27/16 Pct Recovery = 68% Analysis Date = 11/25/16 Pct Recovery = 68% Analysis Date = 11/25/16 Pct Recovery = 68% Analysis Date = 11/22/16 Pct Recovery = 68% Analysis Date = 11/22/16 Pct Recovery = 68% Analysis Date = 11/20/16 Pct Recovery = 69% Analysis Date = 11/20/16 Pct Recovery = 69% Analysis Date = 11/18/16 Pct Recovery = 69% Analysis Date = 11/18/16 Pct Recovery = 69% Analysis Date = 11/16/16 Pct Recovery = 69% Analysis Date = 11/16/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/06/16 Pct Recovery = 70% Analysis Date = 11/06/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 70% Analysis Date = 11/02/16 Pct Recovery = 70% Analysis Date = 11/02/16 Pct Recovery = 70% Analysis Date = 10/31/16 Pct Recovery = 70% Analysis Date = 10/31/16 Pct Recovery = 70% Analysis Date = 10/28/16 Pct Recovery = 71% Analysis Date = 10/28/16 Pct Recovery = 71% Analysis Date = 10/26/16 Pct Recovery = 71% Analysis Date = 10/26/16 Pct Recovery = 71% Analysis Date = 10/24/16 Pct Recovery = 71% Analysis Date = 10/24/16 Pct Recovery = 71% Analysis Date = 10/21/16 Pct Recovery = 71% Analysis Date = 10/21/16 Pct Recovery = 71% Analysis Date = 10/19/16 Pct Recovery = 71% Analysis Date = 10/19/16 Pct Recovery = 71% Analysis Date = 10/17/16 Pct Recovery = 72% Analysis Date = 10/17/16 Pct Recovery = 72% Analysis Date = 10/15/16 Pct Recovery = 72% Analysis Date = 10/15/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/08/16 Pct Recovery = 72% Analysis Date = 10/08/16 Pct Recovery = 72% Analysis Date = 10/05/16 Pct Recovery = 73% Analysis Date = 10/05/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/01/16 Pct Recovery = 73% Analysis Date = 10/01/16 Pct Recovery = 73% Analysis Date = 09/29/16 Pct Recovery = 73% Analysis Date = 09/29/16 Pct Recovery = 73% Analysis Date = 09/26/16 Pct Recovery = 73% Analysis Date = 09/26/16 Pct Recovery = 73% Analysis Date = 09/24/16 Pct Recovery = 74% Analysis Date = 09/24/16 Pct Recovery = 74% Analysis Date = 09/22/16 Pct Recovery = 74% Analysis Date = 09/22/16 Pct Recovery = 74% Analysis Date = 09/19/16 Pct Recovery = 74% Analysis Date = 09/19/16 Pct Recovery = 74% Analysis Date = 09/17/16 Pct Recovery = 74% Analysis Date = 09/17/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 74% Analysis Date = 09/15/16 Pct Recovery = 74% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/10/16 Pct Recovery = 75% Analysis Date = 09/08/16 Pct Recovery = 75% Analysis Date = 09/08/16 Pct Recovery = 75% Analysis Date = 09/06/16 Pct Recovery = 75% Analysis Date = 09/06/16 Pct Recovery = 75% Analysis Date = 09/03/16 Pct Recovery = 75% Analysis Date = 09/03/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 75% Analysis Date = 08/30/16 Pct Recovery = 75% Analysis Date = 08/28/16 Pct Recovery = 75% Analysis Date = 08/28/16 Pct Recovery = 75% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/25/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/23/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/18/16 Pct Recovery = 74% Analysis Date = 08/16/16 Pct Recovery = 74% Analysis Date = 08/16/16 Pct Recovery = 74% Analysis Date = 08/14/16 Pct Recovery = 74% Analysis Date = 08/14/16 Pct Recovery = 74% Analysis Date = 08/12/16 Pct Recovery = 73% Analysis Date = 08/12/16 Pct Recovery = 73% Analysis Date = 08/09/16 Pct Recovery = 73% Analysis Date = 08/09/16 Pct Recovery = 73% Analysis Date = 08/07/16 Pct Recovery = 73% Analysis Date = 08/07/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/02/16 Pct Recovery = 73% Analysis Date = 08/02/16 Pct Recovery = 73% Analysis Date = 07/31/16 Pct Recovery = 72% Analysis Date = 07/31/16 Pct Recovery = 72% Analysis Date = 07/29/16 Pct Recovery = 72% Analysis Date = 07/29/16 Pct Recovery = 72% Analysis Date = 07/27/16 Pct Recovery = 72% Analysis Date = 07/27/16 Pct Recovery = 72% Analysis Date = 07/24/16 Pct Recovery = 72% Analysis Date = 07/24/16 Pct Recovery = 72% Analysis Date = 07/22/16 Pct Recovery = 72% Analysis Date = 07/22/16 Pct Recovery = 72% Analysis Date = 07/20/16 Pct Recovery = 72% Analysis Date = 07/20/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 71% Analysis Date = 07/15/16 Pct Recovery = 71% Analysis Date = 07/15/16 Pct Recovery = 71% Analysis Date = 07/13/16 Pct Recovery = 71% Analysis Date = 07/13/16 Pct Recovery = 71% Analysis Date = 07/11/16 Pct Recovery = 71% Analysis Date = 07/11/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/08/16 Pct Recovery = 71% Analysis Date = 07/06/16 Pct Recovery = 70% Analysis Date = 07/06/16 Pct Recovery = 70% Analysis Date = 07/04/16 Pct Recovery = 70% Analysis Date = 07/04/16 Pct Recovery = 70% Analysis Date = 07/01/16 Pct Recovery = 70% Analysis Date = 07/01/16 Pct Recovery = 70% Analysis Date = 06/29/16 Pct Recovery = 70% Analysis Date = 06/29/16 Pct Recovery = 70% Analysis Date = 06/27/16 Pct Recovery = 70% Analysis Date = 06/27/16 Pct Recovery = 70% Analysis Date = 06/25/16 Pct Recovery = 70% Analysis Date = 06/25/16 Pct Recovery = 70% Analysis Date = 06/22/16 Pct Recovery = 69% Analysis Date = 06/22/16 Pct Recovery = 69% Analysis Date = 06/20/16 Pct Recovery = 69% Analysis Date = 06/20/16 Pct Recovery = 69% Analysis Date = 06/18/16 Pct Recovery = 69% Analysis Date = 06/18/16 Pct Recovery = 69% Analysis Date = 06/15/16 Pct Recovery = 69% Analysis Date = 06/15/16 Pct Recovery = 69% Analysis Date = 06/13/16 Pct Recovery = 69% Analysis Date = 06/13/16 Pct Recovery = 69% Analysis Date = 06/11/16 Pct Recovery = 68% Analysis Date = 06/11/16 Pct Recovery = 68% Analysis Date = 06/09/16 Pct Recovery = 68% Analysis Date = 06/09/16 Pct Recovery = 68% Analysis Date = 06/06/16 Pct Recovery = 68% Analysis Date = 06/06/16 Pct Recovery = 68% Analysis Date = 06/04/16 Pct Recovery = 68% Analysis Date = 06/04/16 Pct Recovery = 68% Analysis Date = 06/02/16 Pct Recovery = 68% Analysis Date = 06/02/16 Pct Recovery = 68% Analysis Date = 05/30/16 Pct Recovery = 68% Analysis Date = 05/30/16 Pct Recovery = 68% Analysis Date = 05/28/16 Pct Recovery = 67% Analysis Date = 05/28/16 Pct Recovery = 67% Analysis Date = 05/26/16 Pct Recovery = 67% Analysis Date = 05/26/16 Pct Recovery = 67% Analysis Date = 05/24/16 Pct Recovery = 67% Analysis Date = 05/24/16 Pct Recovery = 67% Analysis Date = 05/21/16 Pct Recovery = 67% Analysis Date = 05/21/16 Pct Recovery = 67% Analysis Date = 05/19/16 Pct Recovery = 67% Analysis Date = 05/19/16 Pct Recovery = 67% Analysis Date = 05/17/16 Pct Recovery = 67% Analysis Date = 05/17/16 Pct Recovery = 67% Analysis Date = 05/14/16 Pct Recovery = 66% Analysis Date = 05/14/16 Pct Recovery = 66% Analysis Date = 05/12/16 Pct Recovery = 66% Analysis Date = 05/12/16 Pct Recovery = 66% Analysis Date = 05/10/16 Pct Recovery = 66% Analysis Date = 05/10/16 Pct Recovery = 66% Analysis Date = 05/08/16 Pct Recovery = 66% Analysis Date = 05/08/16 Pct Recovery = 66% Analysis Date = 05/05/16 Pct Recovery = 66% Analysis Date = 05/05/16 Pct Recovery = 66% Analysis Date = 05/03/16 Pct Recovery = 65% Analysis Date = 05/03/16 Pct Recovery = 65% Analysis Date = 05/01/16 Pct Recovery = 65% Analysis Date = 05/01/16 Pct Recovery = 65% Analysis Date = 04/28/16 Pct Recovery = 65% Analysis Date = 04/28/16 Pct Recovery = 65% Analysis Date = 04/26/16 Pct Recovery = 64% Analysis Date = 04/26/16 Pct Recovery = 64% Analysis Date = 04/24/16 Pct Recovery = 64% Analysis Date = 04/24/16 Pct Recovery = 64% Analysis Date = 04/22/16 Pct Recovery = 64% Analysis Date = 04/22/16 Pct Recovery = 64% Analysis Date = 04/19/16 Pct Recovery = 63% Analysis Date = 04/19/16 Pct Recovery = 63% Analysis Date = 04/17/16 Pct Recovery = 63% Analysis Date = 04/17/16 Pct Recovery = 63% Analysis Date = 04/15/16 Pct Recovery = 63% Analysis Date = 04/15/16 Pct Recovery = 63% Analysis Date = 04/12/16 Pct Recovery = 62% Analysis Date = 04/12/16 Pct Recovery = 62% Analysis Date = 04/10/16 Pct Recovery = 62% Analysis Date = 04/10/16 Pct Recovery = 62% Analysis Date = 04/08/16 Pct Recovery = 62% Analysis Date = 04/08/16 Pct Recovery = 62% Analysis Date = 04/06/16 Pct Recovery = 61% Analysis Date = 04/06/16 Pct Recovery = 61% Analysis Date = 04/03/16 Pct Recovery = 61% Analysis Date = 04/03/16 Pct Recovery = 61% Analysis Date = 04/01/16 Pct Recovery = 61% Analysis Date = 04/01/16 Pct Recovery = 61% Analysis Date = 03/30/16 Pct Recovery = 60% Analysis Date = 03/30/16 Pct Recovery = 60% Analysis Date = 03/27/16 Pct Recovery = 60% Analysis Date = 03/27/16 Pct Recovery = 60% Analysis Date = 03/25/16 Pct Recovery = 60% Analysis Date = 03/25/16 Pct Recovery = 60% Analysis Date = 03/23/16 Pct Recovery = 59% Analysis Date = 03/23/16 Pct Recovery = 59% Analysis Date = 03/21/16 Pct Recovery = 59% Analysis Date = 03/21/16 Pct Recovery = 59% Analysis Date = 03/18/16 Pct Recovery = 59% Analysis Date = 03/18/16 Pct Recovery = 59% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 57% Analysis Date = 03/09/16 Pct Recovery = 57% Analysis Date = 03/07/16 Pct Recovery = 57% Analysis Date = 03/07/16 Pct Recovery = 57% Analysis Date = 03/05/16 Pct Recovery = 57% Analysis Date = 03/05/16 Pct Recovery = 57% Analysis Date = 03/02/16 Pct Recovery = 56% Analysis Date = 03/02/16 Pct Recovery = 56% Analysis Date = 02/29/16 Pct Recovery = 56% Analysis Date = 02/29/16 Pct Recovery = 56% Analysis Date = 02/27/16 Pct Recovery = 55% Analysis Date = 02/27/16 Pct Recovery = 55% Analysis Date = 02/24/16 Pct Recovery = 55% Analysis Date = 02/24/16 Pct Recovery = 55% Analysis Date = 02/22/16 Pct Recovery = 55% Analysis Date = 02/22/16 Pct Recovery = 55% Analysis Date = 02/20/16 Pct Recovery = 54% Analysis Date = 02/20/16 Pct Recovery = 54% Analysis Date = 02/18/16 Pct Recovery = 54% Analysis Date = 02/18/16 Pct Recovery = 54% Analysis Date = 02/15/16 Pct Recovery = 54% Analysis Date = 02/15/16 Pct Recovery = 54% Analysis Date = 02/13/16 Pct Recovery = 53% Analysis Date = 02/13/16 Pct Recovery = 53% Analysis Date = 02/11/16 Pct Recovery = 53% Analysis Date = 02/11/16 Pct Recovery = 53% Analysis Date = 02/09/16 Pct Recovery = 53% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 69% 13% 66% 11%
Total 18 69% 13% 66% 11%

Sample Statistics
AZINPHOS-METHYL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
AZINPHOS-METHYL-OXON
METHOD: 2033 , TESTIDCODE: 61635GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 62% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 64% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 90% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 69% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 113% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 05/10/17 Pct Recovery = 70% Analysis Date = 05/08/17 Pct Recovery = 73% Analysis Date = 05/08/17 Pct Recovery = 73% Analysis Date = 05/06/17 Pct Recovery = 75% Analysis Date = 05/06/17 Pct Recovery = 75% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/02/17 Pct Recovery = 79% Analysis Date = 05/02/17 Pct Recovery = 79% Analysis Date = 04/30/17 Pct Recovery = 81% Analysis Date = 04/30/17 Pct Recovery = 81% Analysis Date = 04/27/17 Pct Recovery = 83% Analysis Date = 04/27/17 Pct Recovery = 83% Analysis Date = 04/25/17 Pct Recovery = 85% Analysis Date = 04/25/17 Pct Recovery = 85% Analysis Date = 04/23/17 Pct Recovery = 86% Analysis Date = 04/23/17 Pct Recovery = 86% Analysis Date = 04/21/17 Pct Recovery = 86% Analysis Date = 04/21/17 Pct Recovery = 86% Analysis Date = 04/19/17 Pct Recovery = 85% Analysis Date = 04/19/17 Pct Recovery = 85% Analysis Date = 04/17/17 Pct Recovery = 84% Analysis Date = 04/17/17 Pct Recovery = 84% Analysis Date = 04/14/17 Pct Recovery = 83% Analysis Date = 04/14/17 Pct Recovery = 83% Analysis Date = 04/12/17 Pct Recovery = 83% Analysis Date = 04/12/17 Pct Recovery = 83% Analysis Date = 04/10/17 Pct Recovery = 82% Analysis Date = 04/10/17 Pct Recovery = 82% Analysis Date = 04/08/17 Pct Recovery = 81% Analysis Date = 04/08/17 Pct Recovery = 81% Analysis Date = 04/06/17 Pct Recovery = 80% Analysis Date = 04/06/17 Pct Recovery = 80% Analysis Date = 04/04/17 Pct Recovery = 79% Analysis Date = 04/04/17 Pct Recovery = 79% Analysis Date = 04/01/17 Pct Recovery = 79% Analysis Date = 04/01/17 Pct Recovery = 79% Analysis Date = 03/30/17 Pct Recovery = 78% Analysis Date = 03/30/17 Pct Recovery = 78% Analysis Date = 03/28/17 Pct Recovery = 77% Analysis Date = 03/28/17 Pct Recovery = 77% Analysis Date = 03/26/17 Pct Recovery = 76% Analysis Date = 03/26/17 Pct Recovery = 76% Analysis Date = 03/24/17 Pct Recovery = 75% Analysis Date = 03/24/17 Pct Recovery = 75% Analysis Date = 03/21/17 Pct Recovery = 75% Analysis Date = 03/21/17 Pct Recovery = 75% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 73% Analysis Date = 03/17/17 Pct Recovery = 73% Analysis Date = 03/15/17 Pct Recovery = 72% Analysis Date = 03/15/17 Pct Recovery = 72% Analysis Date = 03/13/17 Pct Recovery = 72% Analysis Date = 03/13/17 Pct Recovery = 72% Analysis Date = 03/11/17 Pct Recovery = 71% Analysis Date = 03/11/17 Pct Recovery = 71% Analysis Date = 03/08/17 Pct Recovery = 70% Analysis Date = 03/08/17 Pct Recovery = 70% Analysis Date = 03/06/17 Pct Recovery = 69% Analysis Date = 03/06/17 Pct Recovery = 69% Analysis Date = 03/04/17 Pct Recovery = 68% Analysis Date = 03/04/17 Pct Recovery = 68% Analysis Date = 03/02/17 Pct Recovery = 68% Analysis Date = 03/02/17 Pct Recovery = 68% Analysis Date = 02/28/17 Pct Recovery = 67% Analysis Date = 02/28/17 Pct Recovery = 67% Analysis Date = 02/26/17 Pct Recovery = 66% Analysis Date = 02/26/17 Pct Recovery = 66% Analysis Date = 02/23/17 Pct Recovery = 65% Analysis Date = 02/23/17 Pct Recovery = 65% Analysis Date = 02/21/17 Pct Recovery = 64% Analysis Date = 02/21/17 Pct Recovery = 64% Analysis Date = 02/19/17 Pct Recovery = 64% Analysis Date = 02/19/17 Pct Recovery = 64% Analysis Date = 02/17/17 Pct Recovery = 64% Analysis Date = 02/17/17 Pct Recovery = 64% Analysis Date = 02/15/17 Pct Recovery = 64% Analysis Date = 02/15/17 Pct Recovery = 64% Analysis Date = 02/12/17 Pct Recovery = 64% Analysis Date = 02/12/17 Pct Recovery = 64% Analysis Date = 02/10/17 Pct Recovery = 64% Analysis Date = 02/10/17 Pct Recovery = 64% Analysis Date = 02/08/17 Pct Recovery = 64% Analysis Date = 02/08/17 Pct Recovery = 64% Analysis Date = 02/06/17 Pct Recovery = 64% Analysis Date = 02/06/17 Pct Recovery = 64% Analysis Date = 02/04/17 Pct Recovery = 64% Analysis Date = 02/04/17 Pct Recovery = 64% Analysis Date = 02/02/17 Pct Recovery = 64% Analysis Date = 02/02/17 Pct Recovery = 64% Analysis Date = 01/30/17 Pct Recovery = 64% Analysis Date = 01/30/17 Pct Recovery = 64% Analysis Date = 01/28/17 Pct Recovery = 64% Analysis Date = 01/28/17 Pct Recovery = 64% Analysis Date = 01/26/17 Pct Recovery = 64% Analysis Date = 01/26/17 Pct Recovery = 64% Analysis Date = 01/24/17 Pct Recovery = 64% Analysis Date = 01/24/17 Pct Recovery = 64% Analysis Date = 01/22/17 Pct Recovery = 64% Analysis Date = 01/22/17 Pct Recovery = 64% Analysis Date = 01/20/17 Pct Recovery = 64% Analysis Date = 01/20/17 Pct Recovery = 64% Analysis Date = 01/17/17 Pct Recovery = 64% Analysis Date = 01/17/17 Pct Recovery = 64% Analysis Date = 01/15/17 Pct Recovery = 64% Analysis Date = 01/15/17 Pct Recovery = 64% Analysis Date = 01/13/17 Pct Recovery = 64% Analysis Date = 01/13/17 Pct Recovery = 64% Analysis Date = 01/11/17 Pct Recovery = 64% Analysis Date = 01/11/17 Pct Recovery = 64% Analysis Date = 01/09/17 Pct Recovery = 64% Analysis Date = 01/09/17 Pct Recovery = 64% Analysis Date = 01/07/17 Pct Recovery = 64% Analysis Date = 01/07/17 Pct Recovery = 64% Analysis Date = 01/04/17 Pct Recovery = 64% Analysis Date = 01/04/17 Pct Recovery = 64% Analysis Date = 01/02/17 Pct Recovery = 64% Analysis Date = 01/02/17 Pct Recovery = 64% Analysis Date = 12/31/16 Pct Recovery = 64% Analysis Date = 12/31/16 Pct Recovery = 64% Analysis Date = 12/29/16 Pct Recovery = 64% Analysis Date = 12/29/16 Pct Recovery = 64% Analysis Date = 12/27/16 Pct Recovery = 64% Analysis Date = 12/27/16 Pct Recovery = 64% Analysis Date = 12/24/16 Pct Recovery = 64% Analysis Date = 12/24/16 Pct Recovery = 64% Analysis Date = 12/22/16 Pct Recovery = 64% Analysis Date = 12/22/16 Pct Recovery = 64% Analysis Date = 12/20/16 Pct Recovery = 64% Analysis Date = 12/20/16 Pct Recovery = 64% Analysis Date = 12/18/16 Pct Recovery = 64% Analysis Date = 12/18/16 Pct Recovery = 64% Analysis Date = 12/16/16 Pct Recovery = 64% Analysis Date = 12/16/16 Pct Recovery = 64% Analysis Date = 12/14/16 Pct Recovery = 64% Analysis Date = 12/14/16 Pct Recovery = 64% Analysis Date = 12/11/16 Pct Recovery = 64% Analysis Date = 12/11/16 Pct Recovery = 64% Analysis Date = 12/09/16 Pct Recovery = 64% Analysis Date = 12/09/16 Pct Recovery = 64% Analysis Date = 12/07/16 Pct Recovery = 64% Analysis Date = 12/07/16 Pct Recovery = 64% Analysis Date = 12/05/16 Pct Recovery = 64% Analysis Date = 12/05/16 Pct Recovery = 64% Analysis Date = 12/03/16 Pct Recovery = 64% Analysis Date = 12/03/16 Pct Recovery = 64% Analysis Date = 12/01/16 Pct Recovery = 64% Analysis Date = 12/01/16 Pct Recovery = 64% Analysis Date = 11/28/16 Pct Recovery = 64% Analysis Date = 11/28/16 Pct Recovery = 64% Analysis Date = 11/26/16 Pct Recovery = 64% Analysis Date = 11/26/16 Pct Recovery = 64% Analysis Date = 11/24/16 Pct Recovery = 64% Analysis Date = 11/24/16 Pct Recovery = 64% Analysis Date = 11/22/16 Pct Recovery = 64% Analysis Date = 11/22/16 Pct Recovery = 64% Analysis Date = 11/20/16 Pct Recovery = 64% Analysis Date = 11/20/16 Pct Recovery = 64% Analysis Date = 11/17/16 Pct Recovery = 64% Analysis Date = 11/17/16 Pct Recovery = 64% Analysis Date = 11/15/16 Pct Recovery = 64% Analysis Date = 11/15/16 Pct Recovery = 64% Analysis Date = 11/13/16 Pct Recovery = 64% Analysis Date = 11/13/16 Pct Recovery = 64% Analysis Date = 11/11/16 Pct Recovery = 64% Analysis Date = 11/11/16 Pct Recovery = 64% Analysis Date = 11/09/16 Pct Recovery = 64% Analysis Date = 11/09/16 Pct Recovery = 64% Analysis Date = 11/07/16 Pct Recovery = 64% Analysis Date = 11/07/16 Pct Recovery = 64% Analysis Date = 11/04/16 Pct Recovery = 64% Analysis Date = 11/04/16 Pct Recovery = 64% Analysis Date = 11/02/16 Pct Recovery = 64% Analysis Date = 11/02/16 Pct Recovery = 64% Analysis Date = 10/31/16 Pct Recovery = 64% Analysis Date = 10/31/16 Pct Recovery = 64% Analysis Date = 10/29/16 Pct Recovery = 64% Analysis Date = 10/29/16 Pct Recovery = 64% Analysis Date = 10/27/16 Pct Recovery = 64% Analysis Date = 10/27/16 Pct Recovery = 64% Analysis Date = 10/25/16 Pct Recovery = 64% Analysis Date = 10/25/16 Pct Recovery = 64% Analysis Date = 10/22/16 Pct Recovery = 64% Analysis Date = 10/22/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 64% Analysis Date = 10/12/16 Pct Recovery = 64% Analysis Date = 10/12/16 Pct Recovery = 64% Analysis Date = 10/09/16 Pct Recovery = 64% Analysis Date = 10/09/16 Pct Recovery = 64% Analysis Date = 10/07/16 Pct Recovery = 64% Analysis Date = 10/07/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/05/16 Pct Recovery = 64% Analysis Date = 10/03/16 Pct Recovery = 64% Analysis Date = 10/03/16 Pct Recovery = 64% Analysis Date = 10/01/16 Pct Recovery = 64% Analysis Date = 10/01/16 Pct Recovery = 64% Analysis Date = 09/28/16 Pct Recovery = 64% Analysis Date = 09/28/16 Pct Recovery = 64% Analysis Date = 09/26/16 Pct Recovery = 64% Analysis Date = 09/26/16 Pct Recovery = 64% Analysis Date = 09/24/16 Pct Recovery = 64% Analysis Date = 09/24/16 Pct Recovery = 64% Analysis Date = 09/22/16 Pct Recovery = 64% Analysis Date = 09/22/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/18/16 Pct Recovery = 64% Analysis Date = 09/18/16 Pct Recovery = 64% Analysis Date = 09/15/16 Pct Recovery = 64% Analysis Date = 09/15/16 Pct Recovery = 64% Analysis Date = 09/13/16 Pct Recovery = 64% Analysis Date = 09/13/16 Pct Recovery = 64% Analysis Date = 09/11/16 Pct Recovery = 64% Analysis Date = 09/11/16 Pct Recovery = 64% Analysis Date = 09/09/16 Pct Recovery = 64% Analysis Date = 09/09/16 Pct Recovery = 64% Analysis Date = 09/07/16 Pct Recovery = 64% Analysis Date = 09/07/16 Pct Recovery = 64% Analysis Date = 09/05/16 Pct Recovery = 64% Analysis Date = 09/05/16 Pct Recovery = 64% Analysis Date = 09/02/16 Pct Recovery = 64% Analysis Date = 09/02/16 Pct Recovery = 64% Analysis Date = 08/31/16 Pct Recovery = 64% Analysis Date = 08/31/16 Pct Recovery = 64% Analysis Date = 08/29/16 Pct Recovery = 64% Analysis Date = 08/29/16 Pct Recovery = 64% Analysis Date = 08/27/16 Pct Recovery = 64% Analysis Date = 08/27/16 Pct Recovery = 64% Analysis Date = 08/25/16 Pct Recovery = 65% Analysis Date = 08/25/16 Pct Recovery = 65% Analysis Date = 08/22/16 Pct Recovery = 65% Analysis Date = 08/22/16 Pct Recovery = 65% Analysis Date = 08/20/16 Pct Recovery = 66% Analysis Date = 08/20/16 Pct Recovery = 66% Analysis Date = 08/18/16 Pct Recovery = 67% Analysis Date = 08/18/16 Pct Recovery = 67% Analysis Date = 08/16/16 Pct Recovery = 68% Analysis Date = 08/16/16 Pct Recovery = 68% Analysis Date = 08/14/16 Pct Recovery = 69% Analysis Date = 08/14/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 70% Analysis Date = 08/12/16 Pct Recovery = 70% Analysis Date = 08/09/16 Pct Recovery = 71% Analysis Date = 08/09/16 Pct Recovery = 71% Analysis Date = 08/07/16 Pct Recovery = 72% Analysis Date = 08/07/16 Pct Recovery = 72% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/03/16 Pct Recovery = 73% Analysis Date = 08/03/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 74% Analysis Date = 07/30/16 Pct Recovery = 75% Analysis Date = 07/30/16 Pct Recovery = 75% Analysis Date = 07/27/16 Pct Recovery = 76% Analysis Date = 07/27/16 Pct Recovery = 76% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 78% Analysis Date = 07/23/16 Pct Recovery = 78% Analysis Date = 07/21/16 Pct Recovery = 79% Analysis Date = 07/21/16 Pct Recovery = 79% Analysis Date = 07/19/16 Pct Recovery = 80% Analysis Date = 07/19/16 Pct Recovery = 80% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/14/16 Pct Recovery = 81% Analysis Date = 07/14/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 82% Analysis Date = 07/12/16 Pct Recovery = 82% Analysis Date = 07/10/16 Pct Recovery = 83% Analysis Date = 07/10/16 Pct Recovery = 83% Analysis Date = 07/08/16 Pct Recovery = 84% Analysis Date = 07/08/16 Pct Recovery = 84% Analysis Date = 07/06/16 Pct Recovery = 85% Analysis Date = 07/06/16 Pct Recovery = 85% Analysis Date = 07/03/16 Pct Recovery = 86% Analysis Date = 07/03/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 87% Analysis Date = 07/01/16 Pct Recovery = 87% Analysis Date = 06/29/16 Pct Recovery = 88% Analysis Date = 06/29/16 Pct Recovery = 88% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/27/16 Pct Recovery = 89% Analysis Date = 06/25/16 Pct Recovery = 89% Analysis Date = 06/25/16 Pct Recovery = 89% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/16/16 Pct Recovery = 93% Analysis Date = 06/14/16 Pct Recovery = 94% Analysis Date = 06/14/16 Pct Recovery = 94% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 96% Analysis Date = 06/10/16 Pct Recovery = 96% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/07/16 Pct Recovery = 97% Analysis Date = 06/05/16 Pct Recovery = 97% Analysis Date = 06/05/16 Pct Recovery = 97% Analysis Date = 06/03/16 Pct Recovery = 98% Analysis Date = 06/03/16 Pct Recovery = 98% Analysis Date = 06/01/16 Pct Recovery = 99% Analysis Date = 06/01/16 Pct Recovery = 99% Analysis Date = 05/30/16 Pct Recovery = 100% Analysis Date = 05/30/16 Pct Recovery = 100% Analysis Date = 05/27/16 Pct Recovery = 101% Analysis Date = 05/27/16 Pct Recovery = 101% Analysis Date = 05/25/16 Pct Recovery = 102% Analysis Date = 05/25/16 Pct Recovery = 102% Analysis Date = 05/23/16 Pct Recovery = 103% Analysis Date = 05/23/16 Pct Recovery = 103% Analysis Date = 05/21/16 Pct Recovery = 104% Analysis Date = 05/21/16 Pct Recovery = 104% Analysis Date = 05/19/16 Pct Recovery = 105% Analysis Date = 05/19/16 Pct Recovery = 105% Analysis Date = 05/17/16 Pct Recovery = 105% Analysis Date = 05/17/16 Pct Recovery = 105% Analysis Date = 05/14/16 Pct Recovery = 106% Analysis Date = 05/14/16 Pct Recovery = 106% Analysis Date = 05/12/16 Pct Recovery = 107% Analysis Date = 05/12/16 Pct Recovery = 107% Analysis Date = 05/10/16 Pct Recovery = 108% Analysis Date = 05/10/16 Pct Recovery = 108% Analysis Date = 05/08/16 Pct Recovery = 109% Analysis Date = 05/08/16 Pct Recovery = 109% Analysis Date = 05/06/16 Pct Recovery = 110% Analysis Date = 05/06/16 Pct Recovery = 110% Analysis Date = 05/04/16 Pct Recovery = 111% Analysis Date = 05/04/16 Pct Recovery = 111% Analysis Date = 05/01/16 Pct Recovery = 110% Analysis Date = 05/01/16 Pct Recovery = 110% Analysis Date = 04/29/16 Pct Recovery = 108% Analysis Date = 04/29/16 Pct Recovery = 108% Analysis Date = 04/27/16 Pct Recovery = 107% Analysis Date = 04/27/16 Pct Recovery = 107% Analysis Date = 04/25/16 Pct Recovery = 106% Analysis Date = 04/25/16 Pct Recovery = 106% Analysis Date = 04/23/16 Pct Recovery = 105% Analysis Date = 04/23/16 Pct Recovery = 105% Analysis Date = 04/21/16 Pct Recovery = 103% Analysis Date = 04/21/16 Pct Recovery = 103% Analysis Date = 04/18/16 Pct Recovery = 102% Analysis Date = 04/18/16 Pct Recovery = 102% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/14/16 Pct Recovery = 100% Analysis Date = 04/14/16 Pct Recovery = 100% Analysis Date = 04/12/16 Pct Recovery = 98% Analysis Date = 04/12/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 97% Analysis Date = 04/10/16 Pct Recovery = 97% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/07/16 Pct Recovery = 96% Analysis Date = 04/05/16 Pct Recovery = 95% Analysis Date = 04/05/16 Pct Recovery = 95% Analysis Date = 04/03/16 Pct Recovery = 93% Analysis Date = 04/03/16 Pct Recovery = 93% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 04/01/16 Pct Recovery = 92% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/30/16 Pct Recovery = 91% Analysis Date = 03/28/16 Pct Recovery = 89% Analysis Date = 03/28/16 Pct Recovery = 89% Analysis Date = 03/25/16 Pct Recovery = 88% Analysis Date = 03/25/16 Pct Recovery = 88% Analysis Date = 03/23/16 Pct Recovery = 86% Analysis Date = 03/23/16 Pct Recovery = 86% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/19/16 Pct Recovery = 84% Analysis Date = 03/17/16 Pct Recovery = 82% Analysis Date = 03/17/16 Pct Recovery = 82% Analysis Date = 03/15/16 Pct Recovery = 81% Analysis Date = 03/15/16 Pct Recovery = 81% Analysis Date = 03/12/16 Pct Recovery = 79% Analysis Date = 03/12/16 Pct Recovery = 79% Analysis Date = 03/10/16 Pct Recovery = 78% Analysis Date = 03/10/16 Pct Recovery = 78% Analysis Date = 03/08/16 Pct Recovery = 77% Analysis Date = 03/08/16 Pct Recovery = 77% Analysis Date = 03/06/16 Pct Recovery = 75% Analysis Date = 03/06/16 Pct Recovery = 75% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
AZINPHOS-METHYL-OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 8 79% 20% 69% 23%
Total 8 79% 20% 69% 23%

Sample Statistics
AZINPHOS-METHYL-OXON

Characteristic N % % Basis
Plotted 8 80% Spiked
Estimated Values 8 80% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 10 .  
False Negatives 2 20% 2 out of 10
Not Spiked 18 .  
False Positives 2 11% 2 out of 18

OBSP Determination:
BENFLURALIN
METHOD: 2033 , TESTIDCODE: 82673GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 80% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 73% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 78% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 72% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 68% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 68% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 74% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 105% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 72% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 64% Analysis Date = 05/02/17 Pct Recovery = 83% Analysis Date = 04/30/17 Pct Recovery = 83% Analysis Date = 04/30/17 Pct Recovery = 83% Analysis Date = 04/28/17 Pct Recovery = 83% Analysis Date = 04/28/17 Pct Recovery = 83% Analysis Date = 04/26/17 Pct Recovery = 83% Analysis Date = 04/26/17 Pct Recovery = 83% Analysis Date = 04/24/17 Pct Recovery = 83% Analysis Date = 04/24/17 Pct Recovery = 83% Analysis Date = 04/22/17 Pct Recovery = 83% Analysis Date = 04/22/17 Pct Recovery = 83% Analysis Date = 04/20/17 Pct Recovery = 82% Analysis Date = 04/20/17 Pct Recovery = 82% Analysis Date = 04/18/17 Pct Recovery = 82% Analysis Date = 04/18/17 Pct Recovery = 82% Analysis Date = 04/15/17 Pct Recovery = 82% Analysis Date = 04/15/17 Pct Recovery = 82% Analysis Date = 04/13/17 Pct Recovery = 82% Analysis Date = 04/13/17 Pct Recovery = 82% Analysis Date = 04/11/17 Pct Recovery = 82% Analysis Date = 04/11/17 Pct Recovery = 82% Analysis Date = 04/09/17 Pct Recovery = 82% Analysis Date = 04/09/17 Pct Recovery = 82% Analysis Date = 04/07/17 Pct Recovery = 82% Analysis Date = 04/07/17 Pct Recovery = 82% Analysis Date = 04/05/17 Pct Recovery = 82% Analysis Date = 04/05/17 Pct Recovery = 82% Analysis Date = 04/03/17 Pct Recovery = 82% Analysis Date = 04/03/17 Pct Recovery = 82% Analysis Date = 03/31/17 Pct Recovery = 82% Analysis Date = 03/31/17 Pct Recovery = 82% Analysis Date = 03/29/17 Pct Recovery = 81% Analysis Date = 03/29/17 Pct Recovery = 81% Analysis Date = 03/27/17 Pct Recovery = 81% Analysis Date = 03/27/17 Pct Recovery = 81% Analysis Date = 03/25/17 Pct Recovery = 81% Analysis Date = 03/25/17 Pct Recovery = 81% Analysis Date = 03/23/17 Pct Recovery = 81% Analysis Date = 03/23/17 Pct Recovery = 81% Analysis Date = 03/21/17 Pct Recovery = 81% Analysis Date = 03/21/17 Pct Recovery = 81% Analysis Date = 03/19/17 Pct Recovery = 81% Analysis Date = 03/19/17 Pct Recovery = 81% Analysis Date = 03/17/17 Pct Recovery = 81% Analysis Date = 03/17/17 Pct Recovery = 81% Analysis Date = 03/14/17 Pct Recovery = 81% Analysis Date = 03/14/17 Pct Recovery = 81% Analysis Date = 03/12/17 Pct Recovery = 81% Analysis Date = 03/12/17 Pct Recovery = 81% Analysis Date = 03/10/17 Pct Recovery = 80% Analysis Date = 03/10/17 Pct Recovery = 80% Analysis Date = 03/08/17 Pct Recovery = 80% Analysis Date = 03/08/17 Pct Recovery = 80% Analysis Date = 03/06/17 Pct Recovery = 80% Analysis Date = 03/06/17 Pct Recovery = 80% Analysis Date = 03/04/17 Pct Recovery = 80% Analysis Date = 03/04/17 Pct Recovery = 80% Analysis Date = 03/02/17 Pct Recovery = 80% Analysis Date = 03/02/17 Pct Recovery = 80% Analysis Date = 02/27/17 Pct Recovery = 80% Analysis Date = 02/27/17 Pct Recovery = 80% Analysis Date = 02/25/17 Pct Recovery = 80% Analysis Date = 02/25/17 Pct Recovery = 80% Analysis Date = 02/23/17 Pct Recovery = 80% Analysis Date = 02/23/17 Pct Recovery = 80% Analysis Date = 02/21/17 Pct Recovery = 79% Analysis Date = 02/21/17 Pct Recovery = 79% Analysis Date = 02/19/17 Pct Recovery = 79% Analysis Date = 02/19/17 Pct Recovery = 79% Analysis Date = 02/17/17 Pct Recovery = 79% Analysis Date = 02/17/17 Pct Recovery = 79% Analysis Date = 02/15/17 Pct Recovery = 79% Analysis Date = 02/15/17 Pct Recovery = 79% Analysis Date = 02/13/17 Pct Recovery = 79% Analysis Date = 02/13/17 Pct Recovery = 79% Analysis Date = 02/10/17 Pct Recovery = 78% Analysis Date = 02/10/17 Pct Recovery = 78% Analysis Date = 02/08/17 Pct Recovery = 78% Analysis Date = 02/08/17 Pct Recovery = 78% Analysis Date = 02/06/17 Pct Recovery = 78% Analysis Date = 02/06/17 Pct Recovery = 78% Analysis Date = 02/04/17 Pct Recovery = 78% Analysis Date = 02/04/17 Pct Recovery = 78% Analysis Date = 02/02/17 Pct Recovery = 77% Analysis Date = 02/02/17 Pct Recovery = 77% Analysis Date = 01/31/17 Pct Recovery = 77% Analysis Date = 01/31/17 Pct Recovery = 77% Analysis Date = 01/29/17 Pct Recovery = 77% Analysis Date = 01/29/17 Pct Recovery = 77% Analysis Date = 01/26/17 Pct Recovery = 77% Analysis Date = 01/26/17 Pct Recovery = 77% Analysis Date = 01/24/17 Pct Recovery = 76% Analysis Date = 01/24/17 Pct Recovery = 76% Analysis Date = 01/22/17 Pct Recovery = 76% Analysis Date = 01/22/17 Pct Recovery = 76% Analysis Date = 01/20/17 Pct Recovery = 76% Analysis Date = 01/20/17 Pct Recovery = 76% Analysis Date = 01/18/17 Pct Recovery = 75% Analysis Date = 01/18/17 Pct Recovery = 75% Analysis Date = 01/16/17 Pct Recovery = 75% Analysis Date = 01/16/17 Pct Recovery = 75% Analysis Date = 01/14/17 Pct Recovery = 75% Analysis Date = 01/14/17 Pct Recovery = 75% Analysis Date = 01/11/17 Pct Recovery = 75% Analysis Date = 01/11/17 Pct Recovery = 75% Analysis Date = 01/09/17 Pct Recovery = 74% Analysis Date = 01/09/17 Pct Recovery = 74% Analysis Date = 01/07/17 Pct Recovery = 74% Analysis Date = 01/07/17 Pct Recovery = 74% Analysis Date = 01/05/17 Pct Recovery = 74% Analysis Date = 01/05/17 Pct Recovery = 74% Analysis Date = 01/03/17 Pct Recovery = 74% Analysis Date = 01/03/17 Pct Recovery = 74% Analysis Date = 01/01/17 Pct Recovery = 73% Analysis Date = 01/01/17 Pct Recovery = 73% Analysis Date = 12/30/16 Pct Recovery = 73% Analysis Date = 12/30/16 Pct Recovery = 73% Analysis Date = 12/28/16 Pct Recovery = 73% Analysis Date = 12/28/16 Pct Recovery = 73% Analysis Date = 12/25/16 Pct Recovery = 73% Analysis Date = 12/25/16 Pct Recovery = 73% Analysis Date = 12/23/16 Pct Recovery = 72% Analysis Date = 12/23/16 Pct Recovery = 72% Analysis Date = 12/21/16 Pct Recovery = 72% Analysis Date = 12/21/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/17/16 Pct Recovery = 72% Analysis Date = 12/17/16 Pct Recovery = 72% Analysis Date = 12/15/16 Pct Recovery = 72% Analysis Date = 12/15/16 Pct Recovery = 72% Analysis Date = 12/13/16 Pct Recovery = 71% Analysis Date = 12/13/16 Pct Recovery = 71% Analysis Date = 12/10/16 Pct Recovery = 71% Analysis Date = 12/10/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 71% Analysis Date = 12/02/16 Pct Recovery = 71% Analysis Date = 12/02/16 Pct Recovery = 71% Analysis Date = 11/30/16 Pct Recovery = 71% Analysis Date = 11/30/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/28/16 Pct Recovery = 71% Analysis Date = 11/26/16 Pct Recovery = 71% Analysis Date = 11/26/16 Pct Recovery = 71% Analysis Date = 11/23/16 Pct Recovery = 71% Analysis Date = 11/23/16 Pct Recovery = 71% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/21/16 Pct Recovery = 70% Analysis Date = 11/19/16 Pct Recovery = 70% Analysis Date = 11/19/16 Pct Recovery = 70% Analysis Date = 11/17/16 Pct Recovery = 70% Analysis Date = 11/17/16 Pct Recovery = 70% Analysis Date = 11/15/16 Pct Recovery = 70% Analysis Date = 11/15/16 Pct Recovery = 70% Analysis Date = 11/13/16 Pct Recovery = 70% Analysis Date = 11/13/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 70% Analysis Date = 11/08/16 Pct Recovery = 70% Analysis Date = 11/08/16 Pct Recovery = 70% Analysis Date = 11/06/16 Pct Recovery = 70% Analysis Date = 11/06/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 70% Analysis Date = 11/02/16 Pct Recovery = 70% Analysis Date = 11/02/16 Pct Recovery = 70% Analysis Date = 10/31/16 Pct Recovery = 69% Analysis Date = 10/31/16 Pct Recovery = 69% Analysis Date = 10/29/16 Pct Recovery = 69% Analysis Date = 10/29/16 Pct Recovery = 69% Analysis Date = 10/27/16 Pct Recovery = 69% Analysis Date = 10/27/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/22/16 Pct Recovery = 69% Analysis Date = 10/22/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/20/16 Pct Recovery = 69% Analysis Date = 10/18/16 Pct Recovery = 69% Analysis Date = 10/18/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/16/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/14/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/10/16 Pct Recovery = 68% Analysis Date = 10/07/16 Pct Recovery = 68% Analysis Date = 10/07/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 10/05/16 Pct Recovery = 68% Analysis Date = 10/03/16 Pct Recovery = 68% Analysis Date = 10/03/16 Pct Recovery = 68% Analysis Date = 10/01/16 Pct Recovery = 68% Analysis Date = 10/01/16 Pct Recovery = 68% Analysis Date = 09/29/16 Pct Recovery = 68% Analysis Date = 09/29/16 Pct Recovery = 68% Analysis Date = 09/27/16 Pct Recovery = 68% Analysis Date = 09/27/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/25/16 Pct Recovery = 68% Analysis Date = 09/22/16 Pct Recovery = 68% Analysis Date = 09/22/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/20/16 Pct Recovery = 67% Analysis Date = 09/18/16 Pct Recovery = 67% Analysis Date = 09/18/16 Pct Recovery = 67% Analysis Date = 09/16/16 Pct Recovery = 67% Analysis Date = 09/16/16 Pct Recovery = 67% Analysis Date = 09/14/16 Pct Recovery = 67% Analysis Date = 09/14/16 Pct Recovery = 67% Analysis Date = 09/12/16 Pct Recovery = 67% Analysis Date = 09/12/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/10/16 Pct Recovery = 67% Analysis Date = 09/08/16 Pct Recovery = 67% Analysis Date = 09/08/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 67% Analysis Date = 09/05/16 Pct Recovery = 67% Analysis Date = 09/03/16 Pct Recovery = 67% Analysis Date = 09/03/16 Pct Recovery = 67% Analysis Date = 09/01/16 Pct Recovery = 67% Analysis Date = 09/01/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/30/16 Pct Recovery = 67% Analysis Date = 08/28/16 Pct Recovery = 67% Analysis Date = 08/28/16 Pct Recovery = 67% Analysis Date = 08/26/16 Pct Recovery = 66% Analysis Date = 08/26/16 Pct Recovery = 66% Analysis Date = 08/24/16 Pct Recovery = 66% Analysis Date = 08/24/16 Pct Recovery = 66% Analysis Date = 08/21/16 Pct Recovery = 66% Analysis Date = 08/21/16 Pct Recovery = 66% Analysis Date = 08/19/16 Pct Recovery = 66% Analysis Date = 08/19/16 Pct Recovery = 66% Analysis Date = 08/17/16 Pct Recovery = 66% Analysis Date = 08/17/16 Pct Recovery = 66% Analysis Date = 08/15/16 Pct Recovery = 66% Analysis Date = 08/15/16 Pct Recovery = 66% Analysis Date = 08/13/16 Pct Recovery = 66% Analysis Date = 08/13/16 Pct Recovery = 66% Analysis Date = 08/11/16 Pct Recovery = 66% Analysis Date = 08/11/16 Pct Recovery = 66% Analysis Date = 08/09/16 Pct Recovery = 66% Analysis Date = 08/09/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/04/16 Pct Recovery = 66% Analysis Date = 08/04/16 Pct Recovery = 66% Analysis Date = 08/02/16 Pct Recovery = 66% Analysis Date = 08/02/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/29/16 Pct Recovery = 66% Analysis Date = 07/29/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/25/16 Pct Recovery = 66% Analysis Date = 07/25/16 Pct Recovery = 66% Analysis Date = 07/23/16 Pct Recovery = 66% Analysis Date = 07/23/16 Pct Recovery = 66% Analysis Date = 07/20/16 Pct Recovery = 66% Analysis Date = 07/20/16 Pct Recovery = 66% Analysis Date = 07/18/16 Pct Recovery = 66% Analysis Date = 07/18/16 Pct Recovery = 66% Analysis Date = 07/16/16 Pct Recovery = 66% Analysis Date = 07/16/16 Pct Recovery = 66% Analysis Date = 07/14/16 Pct Recovery = 66% Analysis Date = 07/14/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/12/16 Pct Recovery = 66% Analysis Date = 07/10/16 Pct Recovery = 66% Analysis Date = 07/10/16 Pct Recovery = 66% Analysis Date = 07/08/16 Pct Recovery = 66% Analysis Date = 07/08/16 Pct Recovery = 66% Analysis Date = 07/05/16 Pct Recovery = 66% Analysis Date = 07/05/16 Pct Recovery = 66% Analysis Date = 07/03/16 Pct Recovery = 66% Analysis Date = 07/03/16 Pct Recovery = 66% Analysis Date = 07/01/16 Pct Recovery = 66% Analysis Date = 07/01/16 Pct Recovery = 66% Analysis Date = 06/29/16 Pct Recovery = 66% Analysis Date = 06/29/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/23/16 Pct Recovery = 66% Analysis Date = 06/23/16 Pct Recovery = 66% Analysis Date = 06/21/16 Pct Recovery = 66% Analysis Date = 06/21/16 Pct Recovery = 66% Analysis Date = 06/18/16 Pct Recovery = 66% Analysis Date = 06/18/16 Pct Recovery = 66% Analysis Date = 06/16/16 Pct Recovery = 66% Analysis Date = 06/16/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/14/16 Pct Recovery = 66% Analysis Date = 06/12/16 Pct Recovery = 66% Analysis Date = 06/12/16 Pct Recovery = 66% Analysis Date = 06/10/16 Pct Recovery = 66% Analysis Date = 06/10/16 Pct Recovery = 66% Analysis Date = 06/08/16 Pct Recovery = 66% Analysis Date = 06/08/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/03/16 Pct Recovery = 66% Analysis Date = 06/03/16 Pct Recovery = 66% Analysis Date = 06/01/16 Pct Recovery = 66% Analysis Date = 06/01/16 Pct Recovery = 66% Analysis Date = 05/30/16 Pct Recovery = 66% Analysis Date = 05/30/16 Pct Recovery = 66% Analysis Date = 05/28/16 Pct Recovery = 66% Analysis Date = 05/28/16 Pct Recovery = 66% Analysis Date = 05/26/16 Pct Recovery = 66% Analysis Date = 05/26/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 66% Analysis Date = 05/24/16 Pct Recovery = 66% Analysis Date = 05/22/16 Pct Recovery = 66% Analysis Date = 05/22/16 Pct Recovery = 66% Analysis Date = 05/19/16 Pct Recovery = 67% Analysis Date = 05/19/16 Pct Recovery = 67% Analysis Date = 05/17/16 Pct Recovery = 67% Analysis Date = 05/17/16 Pct Recovery = 67% Analysis Date = 05/15/16 Pct Recovery = 67% Analysis Date = 05/15/16 Pct Recovery = 67% Analysis Date = 05/13/16 Pct Recovery = 67% Analysis Date = 05/13/16 Pct Recovery = 67% Analysis Date = 05/11/16 Pct Recovery = 67% Analysis Date = 05/11/16 Pct Recovery = 67% Analysis Date = 05/09/16 Pct Recovery = 67% Analysis Date = 05/09/16 Pct Recovery = 67% Analysis Date = 05/07/16 Pct Recovery = 67% Analysis Date = 05/07/16 Pct Recovery = 67% Analysis Date = 05/05/16 Pct Recovery = 67% Analysis Date = 05/05/16 Pct Recovery = 67% Analysis Date = 05/02/16 Pct Recovery = 67% Analysis Date = 05/02/16 Pct Recovery = 67% Analysis Date = 04/30/16 Pct Recovery = 67% Analysis Date = 04/30/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/26/16 Pct Recovery = 67% Analysis Date = 04/26/16 Pct Recovery = 67% Analysis Date = 04/24/16 Pct Recovery = 67% Analysis Date = 04/24/16 Pct Recovery = 67% Analysis Date = 04/22/16 Pct Recovery = 67% Analysis Date = 04/22/16 Pct Recovery = 67% Analysis Date = 04/20/16 Pct Recovery = 67% Analysis Date = 04/20/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 67% Analysis Date = 04/13/16 Pct Recovery = 67% Analysis Date = 04/13/16 Pct Recovery = 67% Analysis Date = 04/11/16 Pct Recovery = 66% Analysis Date = 04/11/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/07/16 Pct Recovery = 66% Analysis Date = 04/07/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 66% Analysis Date = 04/03/16 Pct Recovery = 66% Analysis Date = 04/03/16 Pct Recovery = 66% Analysis Date = 03/31/16 Pct Recovery = 66% Analysis Date = 03/31/16 Pct Recovery = 66% Analysis Date = 03/29/16 Pct Recovery = 66% Analysis Date = 03/29/16 Pct Recovery = 66% Analysis Date = 03/27/16 Pct Recovery = 66% Analysis Date = 03/27/16 Pct Recovery = 66% Analysis Date = 03/25/16 Pct Recovery = 66% Analysis Date = 03/25/16 Pct Recovery = 66% Analysis Date = 03/23/16 Pct Recovery = 66% Analysis Date = 03/23/16 Pct Recovery = 66% Analysis Date = 03/21/16 Pct Recovery = 66% Analysis Date = 03/21/16 Pct Recovery = 66% Analysis Date = 03/19/16 Pct Recovery = 66% Analysis Date = 03/19/16 Pct Recovery = 66% Analysis Date = 03/16/16 Pct Recovery = 66% Analysis Date = 03/16/16 Pct Recovery = 66% Analysis Date = 03/14/16 Pct Recovery = 66% Analysis Date = 03/14/16 Pct Recovery = 66% Analysis Date = 03/12/16 Pct Recovery = 66% Analysis Date = 03/12/16 Pct Recovery = 66% Analysis Date = 03/10/16 Pct Recovery = 66% Analysis Date = 03/10/16 Pct Recovery = 66% Analysis Date = 03/08/16 Pct Recovery = 66% Analysis Date = 03/08/16 Pct Recovery = 66% Analysis Date = 03/06/16 Pct Recovery = 66% Analysis Date = 03/06/16 Pct Recovery = 66% Analysis Date = 03/04/16 Pct Recovery = 66% Analysis Date = 03/04/16 Pct Recovery = 66% Analysis Date = 03/02/16 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BENFLURALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 72% 11% 72% 10%
Total 18 72% 11% 72% 10%

Sample Statistics
BENFLURALIN

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
CARBARYL
METHOD: 2033 , TESTIDCODE: 82680GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 71% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 71% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 94% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 84% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 75% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 50% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 67% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 60% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 53% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 54% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 64% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 53% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 44% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 74% Analysis Date = 05/10/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/04/17 Pct Recovery = 76% Analysis Date = 05/04/17 Pct Recovery = 76% Analysis Date = 05/01/17 Pct Recovery = 76% Analysis Date = 05/01/17 Pct Recovery = 76% Analysis Date = 04/29/17 Pct Recovery = 76% Analysis Date = 04/29/17 Pct Recovery = 76% Analysis Date = 04/27/17 Pct Recovery = 76% Analysis Date = 04/27/17 Pct Recovery = 76% Analysis Date = 04/25/17 Pct Recovery = 76% Analysis Date = 04/25/17 Pct Recovery = 76% Analysis Date = 04/22/17 Pct Recovery = 75% Analysis Date = 04/22/17 Pct Recovery = 75% Analysis Date = 04/20/17 Pct Recovery = 75% Analysis Date = 04/20/17 Pct Recovery = 75% Analysis Date = 04/18/17 Pct Recovery = 75% Analysis Date = 04/18/17 Pct Recovery = 75% Analysis Date = 04/15/17 Pct Recovery = 75% Analysis Date = 04/15/17 Pct Recovery = 75% Analysis Date = 04/13/17 Pct Recovery = 75% Analysis Date = 04/13/17 Pct Recovery = 75% Analysis Date = 04/11/17 Pct Recovery = 75% Analysis Date = 04/11/17 Pct Recovery = 75% Analysis Date = 04/09/17 Pct Recovery = 75% Analysis Date = 04/09/17 Pct Recovery = 75% Analysis Date = 04/06/17 Pct Recovery = 75% Analysis Date = 04/06/17 Pct Recovery = 75% Analysis Date = 04/04/17 Pct Recovery = 75% Analysis Date = 04/04/17 Pct Recovery = 75% Analysis Date = 04/02/17 Pct Recovery = 75% Analysis Date = 04/02/17 Pct Recovery = 75% Analysis Date = 03/30/17 Pct Recovery = 74% Analysis Date = 03/30/17 Pct Recovery = 74% Analysis Date = 03/28/17 Pct Recovery = 74% Analysis Date = 03/28/17 Pct Recovery = 74% Analysis Date = 03/26/17 Pct Recovery = 74% Analysis Date = 03/26/17 Pct Recovery = 74% Analysis Date = 03/24/17 Pct Recovery = 74% Analysis Date = 03/24/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 74% Analysis Date = 03/14/17 Pct Recovery = 74% Analysis Date = 03/14/17 Pct Recovery = 74% Analysis Date = 03/12/17 Pct Recovery = 74% Analysis Date = 03/12/17 Pct Recovery = 74% Analysis Date = 03/10/17 Pct Recovery = 73% Analysis Date = 03/10/17 Pct Recovery = 73% Analysis Date = 03/08/17 Pct Recovery = 73% Analysis Date = 03/08/17 Pct Recovery = 73% Analysis Date = 03/05/17 Pct Recovery = 73% Analysis Date = 03/05/17 Pct Recovery = 73% Analysis Date = 03/03/17 Pct Recovery = 73% Analysis Date = 03/03/17 Pct Recovery = 73% Analysis Date = 03/01/17 Pct Recovery = 73% Analysis Date = 03/01/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/22/17 Pct Recovery = 73% Analysis Date = 02/22/17 Pct Recovery = 73% Analysis Date = 02/20/17 Pct Recovery = 73% Analysis Date = 02/20/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/15/17 Pct Recovery = 73% Analysis Date = 02/15/17 Pct Recovery = 73% Analysis Date = 02/13/17 Pct Recovery = 72% Analysis Date = 02/13/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/08/17 Pct Recovery = 72% Analysis Date = 02/08/17 Pct Recovery = 72% Analysis Date = 02/06/17 Pct Recovery = 72% Analysis Date = 02/06/17 Pct Recovery = 72% Analysis Date = 02/04/17 Pct Recovery = 72% Analysis Date = 02/04/17 Pct Recovery = 72% Analysis Date = 02/01/17 Pct Recovery = 72% Analysis Date = 02/01/17 Pct Recovery = 72% Analysis Date = 01/30/17 Pct Recovery = 72% Analysis Date = 01/30/17 Pct Recovery = 72% Analysis Date = 01/28/17 Pct Recovery = 72% Analysis Date = 01/28/17 Pct Recovery = 72% Analysis Date = 01/25/17 Pct Recovery = 72% Analysis Date = 01/25/17 Pct Recovery = 72% Analysis Date = 01/23/17 Pct Recovery = 72% Analysis Date = 01/23/17 Pct Recovery = 72% Analysis Date = 01/21/17 Pct Recovery = 72% Analysis Date = 01/21/17 Pct Recovery = 72% Analysis Date = 01/19/17 Pct Recovery = 72% Analysis Date = 01/19/17 Pct Recovery = 72% Analysis Date = 01/16/17 Pct Recovery = 72% Analysis Date = 01/16/17 Pct Recovery = 72% Analysis Date = 01/14/17 Pct Recovery = 72% Analysis Date = 01/14/17 Pct Recovery = 72% Analysis Date = 01/12/17 Pct Recovery = 72% Analysis Date = 01/12/17 Pct Recovery = 72% Analysis Date = 01/09/17 Pct Recovery = 72% Analysis Date = 01/09/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/05/17 Pct Recovery = 72% Analysis Date = 01/05/17 Pct Recovery = 72% Analysis Date = 01/03/17 Pct Recovery = 71% Analysis Date = 01/03/17 Pct Recovery = 71% Analysis Date = 12/31/16 Pct Recovery = 71% Analysis Date = 12/31/16 Pct Recovery = 71% Analysis Date = 12/29/16 Pct Recovery = 71% Analysis Date = 12/29/16 Pct Recovery = 71% Analysis Date = 12/27/16 Pct Recovery = 71% Analysis Date = 12/27/16 Pct Recovery = 71% Analysis Date = 12/24/16 Pct Recovery = 71% Analysis Date = 12/24/16 Pct Recovery = 71% Analysis Date = 12/22/16 Pct Recovery = 71% Analysis Date = 12/22/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/18/16 Pct Recovery = 71% Analysis Date = 12/18/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/13/16 Pct Recovery = 71% Analysis Date = 12/13/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/06/16 Pct Recovery = 71% Analysis Date = 12/04/16 Pct Recovery = 72% Analysis Date = 12/04/16 Pct Recovery = 72% Analysis Date = 12/02/16 Pct Recovery = 72% Analysis Date = 12/02/16 Pct Recovery = 72% Analysis Date = 11/29/16 Pct Recovery = 72% Analysis Date = 11/29/16 Pct Recovery = 72% Analysis Date = 11/27/16 Pct Recovery = 72% Analysis Date = 11/27/16 Pct Recovery = 72% Analysis Date = 11/25/16 Pct Recovery = 72% Analysis Date = 11/25/16 Pct Recovery = 72% Analysis Date = 11/22/16 Pct Recovery = 72% Analysis Date = 11/22/16 Pct Recovery = 72% Analysis Date = 11/20/16 Pct Recovery = 72% Analysis Date = 11/20/16 Pct Recovery = 72% Analysis Date = 11/18/16 Pct Recovery = 72% Analysis Date = 11/18/16 Pct Recovery = 72% Analysis Date = 11/16/16 Pct Recovery = 72% Analysis Date = 11/16/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/13/16 Pct Recovery = 72% Analysis Date = 11/11/16 Pct Recovery = 72% Analysis Date = 11/11/16 Pct Recovery = 72% Analysis Date = 11/09/16 Pct Recovery = 72% Analysis Date = 11/09/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/04/16 Pct Recovery = 72% Analysis Date = 11/04/16 Pct Recovery = 72% Analysis Date = 11/02/16 Pct Recovery = 72% Analysis Date = 11/02/16 Pct Recovery = 72% Analysis Date = 10/31/16 Pct Recovery = 72% Analysis Date = 10/31/16 Pct Recovery = 72% Analysis Date = 10/28/16 Pct Recovery = 72% Analysis Date = 10/28/16 Pct Recovery = 72% Analysis Date = 10/26/16 Pct Recovery = 72% Analysis Date = 10/26/16 Pct Recovery = 72% Analysis Date = 10/24/16 Pct Recovery = 72% Analysis Date = 10/24/16 Pct Recovery = 72% Analysis Date = 10/21/16 Pct Recovery = 72% Analysis Date = 10/21/16 Pct Recovery = 72% Analysis Date = 10/19/16 Pct Recovery = 72% Analysis Date = 10/19/16 Pct Recovery = 72% Analysis Date = 10/17/16 Pct Recovery = 72% Analysis Date = 10/17/16 Pct Recovery = 72% Analysis Date = 10/15/16 Pct Recovery = 72% Analysis Date = 10/15/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/12/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/10/16 Pct Recovery = 72% Analysis Date = 10/08/16 Pct Recovery = 73% Analysis Date = 10/08/16 Pct Recovery = 73% Analysis Date = 10/05/16 Pct Recovery = 73% Analysis Date = 10/05/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/03/16 Pct Recovery = 73% Analysis Date = 10/01/16 Pct Recovery = 73% Analysis Date = 10/01/16 Pct Recovery = 73% Analysis Date = 09/29/16 Pct Recovery = 73% Analysis Date = 09/29/16 Pct Recovery = 73% Analysis Date = 09/26/16 Pct Recovery = 73% Analysis Date = 09/26/16 Pct Recovery = 73% Analysis Date = 09/24/16 Pct Recovery = 73% Analysis Date = 09/24/16 Pct Recovery = 73% Analysis Date = 09/22/16 Pct Recovery = 73% Analysis Date = 09/22/16 Pct Recovery = 73% Analysis Date = 09/19/16 Pct Recovery = 73% Analysis Date = 09/19/16 Pct Recovery = 73% Analysis Date = 09/17/16 Pct Recovery = 73% Analysis Date = 09/17/16 Pct Recovery = 73% Analysis Date = 09/15/16 Pct Recovery = 73% Analysis Date = 09/15/16 Pct Recovery = 73% Analysis Date = 09/13/16 Pct Recovery = 73% Analysis Date = 09/13/16 Pct Recovery = 73% Analysis Date = 09/10/16 Pct Recovery = 73% Analysis Date = 09/10/16 Pct Recovery = 73% Analysis Date = 09/08/16 Pct Recovery = 73% Analysis Date = 09/08/16 Pct Recovery = 73% Analysis Date = 09/06/16 Pct Recovery = 73% Analysis Date = 09/06/16 Pct Recovery = 73% Analysis Date = 09/03/16 Pct Recovery = 73% Analysis Date = 09/03/16 Pct Recovery = 73% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 08/30/16 Pct Recovery = 72% Analysis Date = 08/30/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/23/16 Pct Recovery = 72% Analysis Date = 08/23/16 Pct Recovery = 72% Analysis Date = 08/21/16 Pct Recovery = 72% Analysis Date = 08/21/16 Pct Recovery = 72% Analysis Date = 08/18/16 Pct Recovery = 71% Analysis Date = 08/18/16 Pct Recovery = 71% Analysis Date = 08/16/16 Pct Recovery = 71% Analysis Date = 08/16/16 Pct Recovery = 71% Analysis Date = 08/14/16 Pct Recovery = 71% Analysis Date = 08/14/16 Pct Recovery = 71% Analysis Date = 08/12/16 Pct Recovery = 71% Analysis Date = 08/12/16 Pct Recovery = 71% Analysis Date = 08/09/16 Pct Recovery = 70% Analysis Date = 08/09/16 Pct Recovery = 70% Analysis Date = 08/07/16 Pct Recovery = 70% Analysis Date = 08/07/16 Pct Recovery = 70% Analysis Date = 08/05/16 Pct Recovery = 70% Analysis Date = 08/05/16 Pct Recovery = 70% Analysis Date = 08/02/16 Pct Recovery = 70% Analysis Date = 08/02/16 Pct Recovery = 70% Analysis Date = 07/31/16 Pct Recovery = 69% Analysis Date = 07/31/16 Pct Recovery = 69% Analysis Date = 07/29/16 Pct Recovery = 69% Analysis Date = 07/29/16 Pct Recovery = 69% Analysis Date = 07/27/16 Pct Recovery = 69% Analysis Date = 07/27/16 Pct Recovery = 69% Analysis Date = 07/24/16 Pct Recovery = 69% Analysis Date = 07/24/16 Pct Recovery = 69% Analysis Date = 07/22/16 Pct Recovery = 68% Analysis Date = 07/22/16 Pct Recovery = 68% Analysis Date = 07/20/16 Pct Recovery = 68% Analysis Date = 07/20/16 Pct Recovery = 68% Analysis Date = 07/17/16 Pct Recovery = 68% Analysis Date = 07/17/16 Pct Recovery = 68% Analysis Date = 07/15/16 Pct Recovery = 67% Analysis Date = 07/15/16 Pct Recovery = 67% Analysis Date = 07/13/16 Pct Recovery = 67% Analysis Date = 07/13/16 Pct Recovery = 67% Analysis Date = 07/11/16 Pct Recovery = 67% Analysis Date = 07/11/16 Pct Recovery = 67% Analysis Date = 07/08/16 Pct Recovery = 67% Analysis Date = 07/08/16 Pct Recovery = 67% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 07/04/16 Pct Recovery = 66% Analysis Date = 07/04/16 Pct Recovery = 66% Analysis Date = 07/01/16 Pct Recovery = 66% Analysis Date = 07/01/16 Pct Recovery = 66% Analysis Date = 06/29/16 Pct Recovery = 66% Analysis Date = 06/29/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/25/16 Pct Recovery = 65% Analysis Date = 06/25/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 64% Analysis Date = 06/18/16 Pct Recovery = 64% Analysis Date = 06/15/16 Pct Recovery = 64% Analysis Date = 06/15/16 Pct Recovery = 64% Analysis Date = 06/13/16 Pct Recovery = 64% Analysis Date = 06/13/16 Pct Recovery = 64% Analysis Date = 06/11/16 Pct Recovery = 63% Analysis Date = 06/11/16 Pct Recovery = 63% Analysis Date = 06/09/16 Pct Recovery = 63% Analysis Date = 06/09/16 Pct Recovery = 63% Analysis Date = 06/06/16 Pct Recovery = 63% Analysis Date = 06/06/16 Pct Recovery = 63% Analysis Date = 06/04/16 Pct Recovery = 63% Analysis Date = 06/04/16 Pct Recovery = 63% Analysis Date = 06/02/16 Pct Recovery = 62% Analysis Date = 06/02/16 Pct Recovery = 62% Analysis Date = 05/30/16 Pct Recovery = 62% Analysis Date = 05/30/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/26/16 Pct Recovery = 62% Analysis Date = 05/26/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 61% Analysis Date = 05/24/16 Pct Recovery = 61% Analysis Date = 05/21/16 Pct Recovery = 61% Analysis Date = 05/21/16 Pct Recovery = 61% Analysis Date = 05/19/16 Pct Recovery = 61% Analysis Date = 05/19/16 Pct Recovery = 61% Analysis Date = 05/17/16 Pct Recovery = 60% Analysis Date = 05/17/16 Pct Recovery = 60% Analysis Date = 05/14/16 Pct Recovery = 60% Analysis Date = 05/14/16 Pct Recovery = 60% Analysis Date = 05/12/16 Pct Recovery = 60% Analysis Date = 05/12/16 Pct Recovery = 60% Analysis Date = 05/10/16 Pct Recovery = 59% Analysis Date = 05/10/16 Pct Recovery = 59% Analysis Date = 05/08/16 Pct Recovery = 59% Analysis Date = 05/08/16 Pct Recovery = 59% Analysis Date = 05/05/16 Pct Recovery = 59% Analysis Date = 05/05/16 Pct Recovery = 59% Analysis Date = 05/03/16 Pct Recovery = 59% Analysis Date = 05/03/16 Pct Recovery = 59% Analysis Date = 05/01/16 Pct Recovery = 58% Analysis Date = 05/01/16 Pct Recovery = 58% Analysis Date = 04/28/16 Pct Recovery = 58% Analysis Date = 04/28/16 Pct Recovery = 58% Analysis Date = 04/26/16 Pct Recovery = 58% Analysis Date = 04/26/16 Pct Recovery = 58% Analysis Date = 04/24/16 Pct Recovery = 58% Analysis Date = 04/24/16 Pct Recovery = 58% Analysis Date = 04/22/16 Pct Recovery = 58% Analysis Date = 04/22/16 Pct Recovery = 58% Analysis Date = 04/19/16 Pct Recovery = 58% Analysis Date = 04/19/16 Pct Recovery = 58% Analysis Date = 04/17/16 Pct Recovery = 58% Analysis Date = 04/17/16 Pct Recovery = 58% Analysis Date = 04/15/16 Pct Recovery = 58% Analysis Date = 04/15/16 Pct Recovery = 58% Analysis Date = 04/12/16 Pct Recovery = 58% Analysis Date = 04/12/16 Pct Recovery = 58% Analysis Date = 04/10/16 Pct Recovery = 58% Analysis Date = 04/10/16 Pct Recovery = 58% Analysis Date = 04/08/16 Pct Recovery = 58% Analysis Date = 04/08/16 Pct Recovery = 58% Analysis Date = 04/06/16 Pct Recovery = 58% Analysis Date = 04/06/16 Pct Recovery = 58% Analysis Date = 04/03/16 Pct Recovery = 58% Analysis Date = 04/03/16 Pct Recovery = 58% Analysis Date = 04/01/16 Pct Recovery = 58% Analysis Date = 04/01/16 Pct Recovery = 58% Analysis Date = 03/30/16 Pct Recovery = 58% Analysis Date = 03/30/16 Pct Recovery = 58% Analysis Date = 03/27/16 Pct Recovery = 58% Analysis Date = 03/27/16 Pct Recovery = 58% Analysis Date = 03/25/16 Pct Recovery = 58% Analysis Date = 03/25/16 Pct Recovery = 58% Analysis Date = 03/23/16 Pct Recovery = 58% Analysis Date = 03/23/16 Pct Recovery = 58% Analysis Date = 03/21/16 Pct Recovery = 58% Analysis Date = 03/21/16 Pct Recovery = 58% Analysis Date = 03/18/16 Pct Recovery = 58% Analysis Date = 03/18/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/05/16 Pct Recovery = 58% Analysis Date = 03/05/16 Pct Recovery = 58% Analysis Date = 03/02/16 Pct Recovery = 58% Analysis Date = 03/02/16 Pct Recovery = 58% Analysis Date = 02/29/16 Pct Recovery = 58% Analysis Date = 02/29/16 Pct Recovery = 58% Analysis Date = 02/27/16 Pct Recovery = 58% Analysis Date = 02/27/16 Pct Recovery = 58% Analysis Date = 02/24/16 Pct Recovery = 58% Analysis Date = 02/24/16 Pct Recovery = 58% Analysis Date = 02/22/16 Pct Recovery = 58% Analysis Date = 02/22/16 Pct Recovery = 58% Analysis Date = 02/20/16 Pct Recovery = 58% Analysis Date = 02/20/16 Pct Recovery = 58% Analysis Date = 02/18/16 Pct Recovery = 58% Analysis Date = 02/18/16 Pct Recovery = 58% Analysis Date = 02/15/16 Pct Recovery = 58% Analysis Date = 02/15/16 Pct Recovery = 58% Analysis Date = 02/13/16 Pct Recovery = 58% Analysis Date = 02/13/16 Pct Recovery = 58% Analysis Date = 02/11/16 Pct Recovery = 58% Analysis Date = 02/11/16 Pct Recovery = 58% Analysis Date = 02/09/16 Pct Recovery = 58% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBARYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 68% 13% 68% 18%
Total 19 68% 13% 68% 18%

Sample Statistics
CARBARYL

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 2 22% 2 out of 9

OBSP Determination:
CARBOFURAN
METHOD: 2033 , TESTIDCODE: 82674GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 80% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 82% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 30% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 77% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 65% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 75% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 96% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 70% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 97% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 86% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 64% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 05/02/17 Pct Recovery = 63% Analysis Date = 04/30/17 Pct Recovery = 63% Analysis Date = 04/30/17 Pct Recovery = 63% Analysis Date = 04/28/17 Pct Recovery = 64% Analysis Date = 04/28/17 Pct Recovery = 64% Analysis Date = 04/26/17 Pct Recovery = 64% Analysis Date = 04/26/17 Pct Recovery = 64% Analysis Date = 04/24/17 Pct Recovery = 65% Analysis Date = 04/24/17 Pct Recovery = 65% Analysis Date = 04/21/17 Pct Recovery = 65% Analysis Date = 04/21/17 Pct Recovery = 65% Analysis Date = 04/19/17 Pct Recovery = 65% Analysis Date = 04/19/17 Pct Recovery = 65% Analysis Date = 04/17/17 Pct Recovery = 66% Analysis Date = 04/17/17 Pct Recovery = 66% Analysis Date = 04/15/17 Pct Recovery = 66% Analysis Date = 04/15/17 Pct Recovery = 66% Analysis Date = 04/12/17 Pct Recovery = 67% Analysis Date = 04/12/17 Pct Recovery = 67% Analysis Date = 04/10/17 Pct Recovery = 67% Analysis Date = 04/10/17 Pct Recovery = 67% Analysis Date = 04/08/17 Pct Recovery = 68% Analysis Date = 04/08/17 Pct Recovery = 68% Analysis Date = 04/06/17 Pct Recovery = 68% Analysis Date = 04/06/17 Pct Recovery = 68% Analysis Date = 04/03/17 Pct Recovery = 69% Analysis Date = 04/03/17 Pct Recovery = 69% Analysis Date = 04/01/17 Pct Recovery = 69% Analysis Date = 04/01/17 Pct Recovery = 69% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/25/17 Pct Recovery = 71% Analysis Date = 03/25/17 Pct Recovery = 71% Analysis Date = 03/23/17 Pct Recovery = 71% Analysis Date = 03/23/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/19/17 Pct Recovery = 72% Analysis Date = 03/19/17 Pct Recovery = 72% Analysis Date = 03/16/17 Pct Recovery = 72% Analysis Date = 03/16/17 Pct Recovery = 72% Analysis Date = 03/14/17 Pct Recovery = 73% Analysis Date = 03/14/17 Pct Recovery = 73% Analysis Date = 03/12/17 Pct Recovery = 73% Analysis Date = 03/12/17 Pct Recovery = 73% Analysis Date = 03/10/17 Pct Recovery = 74% Analysis Date = 03/10/17 Pct Recovery = 74% Analysis Date = 03/07/17 Pct Recovery = 74% Analysis Date = 03/07/17 Pct Recovery = 74% Analysis Date = 03/05/17 Pct Recovery = 75% Analysis Date = 03/05/17 Pct Recovery = 75% Analysis Date = 03/03/17 Pct Recovery = 75% Analysis Date = 03/03/17 Pct Recovery = 75% Analysis Date = 03/01/17 Pct Recovery = 76% Analysis Date = 03/01/17 Pct Recovery = 76% Analysis Date = 02/26/17 Pct Recovery = 76% Analysis Date = 02/26/17 Pct Recovery = 76% Analysis Date = 02/24/17 Pct Recovery = 77% Analysis Date = 02/24/17 Pct Recovery = 77% Analysis Date = 02/22/17 Pct Recovery = 77% Analysis Date = 02/22/17 Pct Recovery = 77% Analysis Date = 02/20/17 Pct Recovery = 78% Analysis Date = 02/20/17 Pct Recovery = 78% Analysis Date = 02/17/17 Pct Recovery = 78% Analysis Date = 02/17/17 Pct Recovery = 78% Analysis Date = 02/15/17 Pct Recovery = 79% Analysis Date = 02/15/17 Pct Recovery = 79% Analysis Date = 02/13/17 Pct Recovery = 79% Analysis Date = 02/13/17 Pct Recovery = 79% Analysis Date = 02/11/17 Pct Recovery = 79% Analysis Date = 02/11/17 Pct Recovery = 79% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/04/17 Pct Recovery = 80% Analysis Date = 02/04/17 Pct Recovery = 80% Analysis Date = 02/02/17 Pct Recovery = 80% Analysis Date = 02/02/17 Pct Recovery = 80% Analysis Date = 01/30/17 Pct Recovery = 80% Analysis Date = 01/30/17 Pct Recovery = 80% Analysis Date = 01/28/17 Pct Recovery = 80% Analysis Date = 01/28/17 Pct Recovery = 80% Analysis Date = 01/26/17 Pct Recovery = 80% Analysis Date = 01/26/17 Pct Recovery = 80% Analysis Date = 01/24/17 Pct Recovery = 80% Analysis Date = 01/24/17 Pct Recovery = 80% Analysis Date = 01/21/17 Pct Recovery = 81% Analysis Date = 01/21/17 Pct Recovery = 81% Analysis Date = 01/19/17 Pct Recovery = 81% Analysis Date = 01/19/17 Pct Recovery = 81% Analysis Date = 01/17/17 Pct Recovery = 81% Analysis Date = 01/17/17 Pct Recovery = 81% Analysis Date = 01/15/17 Pct Recovery = 81% Analysis Date = 01/15/17 Pct Recovery = 81% Analysis Date = 01/12/17 Pct Recovery = 81% Analysis Date = 01/12/17 Pct Recovery = 81% Analysis Date = 01/10/17 Pct Recovery = 82% Analysis Date = 01/10/17 Pct Recovery = 82% Analysis Date = 01/08/17 Pct Recovery = 82% Analysis Date = 01/08/17 Pct Recovery = 82% Analysis Date = 01/06/17 Pct Recovery = 82% Analysis Date = 01/06/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/01/17 Pct Recovery = 82% Analysis Date = 01/01/17 Pct Recovery = 82% Analysis Date = 12/30/16 Pct Recovery = 82% Analysis Date = 12/30/16 Pct Recovery = 82% Analysis Date = 12/28/16 Pct Recovery = 83% Analysis Date = 12/28/16 Pct Recovery = 83% Analysis Date = 12/26/16 Pct Recovery = 83% Analysis Date = 12/26/16 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/23/16 Pct Recovery = 83% Analysis Date = 12/21/16 Pct Recovery = 83% Analysis Date = 12/21/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/17/16 Pct Recovery = 83% Analysis Date = 12/17/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/12/16 Pct Recovery = 83% Analysis Date = 12/12/16 Pct Recovery = 83% Analysis Date = 12/10/16 Pct Recovery = 82% Analysis Date = 12/10/16 Pct Recovery = 82% Analysis Date = 12/08/16 Pct Recovery = 82% Analysis Date = 12/08/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/03/16 Pct Recovery = 82% Analysis Date = 12/03/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 11/29/16 Pct Recovery = 81% Analysis Date = 11/29/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/20/16 Pct Recovery = 81% Analysis Date = 11/20/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/08/16 Pct Recovery = 80% Analysis Date = 11/08/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 79% Analysis Date = 11/04/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 10/30/16 Pct Recovery = 79% Analysis Date = 10/30/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/26/16 Pct Recovery = 79% Analysis Date = 10/26/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/21/16 Pct Recovery = 78% Analysis Date = 10/21/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/10/16 Pct Recovery = 77% Analysis Date = 10/10/16 Pct Recovery = 77% Analysis Date = 10/08/16 Pct Recovery = 77% Analysis Date = 10/08/16 Pct Recovery = 77% Analysis Date = 10/06/16 Pct Recovery = 77% Analysis Date = 10/06/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 77% Analysis Date = 10/01/16 Pct Recovery = 76% Analysis Date = 10/01/16 Pct Recovery = 76% Analysis Date = 09/29/16 Pct Recovery = 76% Analysis Date = 09/29/16 Pct Recovery = 76% Analysis Date = 09/27/16 Pct Recovery = 76% Analysis Date = 09/27/16 Pct Recovery = 76% Analysis Date = 09/24/16 Pct Recovery = 76% Analysis Date = 09/24/16 Pct Recovery = 76% Analysis Date = 09/22/16 Pct Recovery = 76% Analysis Date = 09/22/16 Pct Recovery = 76% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/20/16 Pct Recovery = 75% Analysis Date = 09/18/16 Pct Recovery = 75% Analysis Date = 09/18/16 Pct Recovery = 75% Analysis Date = 09/16/16 Pct Recovery = 75% Analysis Date = 09/16/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/13/16 Pct Recovery = 75% Analysis Date = 09/11/16 Pct Recovery = 75% Analysis Date = 09/11/16 Pct Recovery = 75% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/09/16 Pct Recovery = 74% Analysis Date = 09/07/16 Pct Recovery = 74% Analysis Date = 09/07/16 Pct Recovery = 74% Analysis Date = 09/04/16 Pct Recovery = 74% Analysis Date = 09/04/16 Pct Recovery = 74% Analysis Date = 09/02/16 Pct Recovery = 74% Analysis Date = 09/02/16 Pct Recovery = 74% Analysis Date = 08/31/16 Pct Recovery = 74% Analysis Date = 08/31/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 74% Analysis Date = 08/29/16 Pct Recovery = 74% Analysis Date = 08/26/16 Pct Recovery = 73% Analysis Date = 08/26/16 Pct Recovery = 73% Analysis Date = 08/24/16 Pct Recovery = 73% Analysis Date = 08/24/16 Pct Recovery = 73% Analysis Date = 08/22/16 Pct Recovery = 73% Analysis Date = 08/22/16 Pct Recovery = 73% Analysis Date = 08/20/16 Pct Recovery = 73% Analysis Date = 08/20/16 Pct Recovery = 73% Analysis Date = 08/17/16 Pct Recovery = 73% Analysis Date = 08/17/16 Pct Recovery = 73% Analysis Date = 08/15/16 Pct Recovery = 73% Analysis Date = 08/15/16 Pct Recovery = 73% Analysis Date = 08/13/16 Pct Recovery = 73% Analysis Date = 08/13/16 Pct Recovery = 73% Analysis Date = 08/11/16 Pct Recovery = 73% Analysis Date = 08/11/16 Pct Recovery = 73% Analysis Date = 08/08/16 Pct Recovery = 73% Analysis Date = 08/08/16 Pct Recovery = 73% Analysis Date = 08/06/16 Pct Recovery = 73% Analysis Date = 08/06/16 Pct Recovery = 73% Analysis Date = 08/04/16 Pct Recovery = 73% Analysis Date = 08/04/16 Pct Recovery = 73% Analysis Date = 08/02/16 Pct Recovery = 73% Analysis Date = 08/02/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/28/16 Pct Recovery = 73% Analysis Date = 07/28/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/26/16 Pct Recovery = 73% Analysis Date = 07/24/16 Pct Recovery = 73% Analysis Date = 07/24/16 Pct Recovery = 73% Analysis Date = 07/21/16 Pct Recovery = 73% Analysis Date = 07/21/16 Pct Recovery = 73% Analysis Date = 07/19/16 Pct Recovery = 72% Analysis Date = 07/19/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/15/16 Pct Recovery = 72% Analysis Date = 07/15/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/10/16 Pct Recovery = 72% Analysis Date = 07/10/16 Pct Recovery = 72% Analysis Date = 07/08/16 Pct Recovery = 72% Analysis Date = 07/08/16 Pct Recovery = 72% Analysis Date = 07/06/16 Pct Recovery = 72% Analysis Date = 07/06/16 Pct Recovery = 72% Analysis Date = 07/03/16 Pct Recovery = 72% Analysis Date = 07/03/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 72% Analysis Date = 07/01/16 Pct Recovery = 72% Analysis Date = 06/29/16 Pct Recovery = 72% Analysis Date = 06/29/16 Pct Recovery = 72% Analysis Date = 06/27/16 Pct Recovery = 72% Analysis Date = 06/27/16 Pct Recovery = 72% Analysis Date = 06/24/16 Pct Recovery = 72% Analysis Date = 06/24/16 Pct Recovery = 72% Analysis Date = 06/22/16 Pct Recovery = 72% Analysis Date = 06/22/16 Pct Recovery = 72% Analysis Date = 06/20/16 Pct Recovery = 72% Analysis Date = 06/20/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/15/16 Pct Recovery = 72% Analysis Date = 06/15/16 Pct Recovery = 72% Analysis Date = 06/13/16 Pct Recovery = 72% Analysis Date = 06/13/16 Pct Recovery = 72% Analysis Date = 06/11/16 Pct Recovery = 72% Analysis Date = 06/11/16 Pct Recovery = 72% Analysis Date = 06/09/16 Pct Recovery = 71% Analysis Date = 06/09/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 71% Analysis Date = 06/02/16 Pct Recovery = 71% Analysis Date = 06/02/16 Pct Recovery = 71% Analysis Date = 05/31/16 Pct Recovery = 71% Analysis Date = 05/31/16 Pct Recovery = 71% Analysis Date = 05/29/16 Pct Recovery = 71% Analysis Date = 05/29/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/22/16 Pct Recovery = 72% Analysis Date = 05/22/16 Pct Recovery = 72% Analysis Date = 05/20/16 Pct Recovery = 72% Analysis Date = 05/20/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/15/16 Pct Recovery = 72% Analysis Date = 05/15/16 Pct Recovery = 72% Analysis Date = 05/13/16 Pct Recovery = 72% Analysis Date = 05/13/16 Pct Recovery = 72% Analysis Date = 05/11/16 Pct Recovery = 73% Analysis Date = 05/11/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/06/16 Pct Recovery = 73% Analysis Date = 05/06/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 05/02/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 73% Analysis Date = 04/27/16 Pct Recovery = 74% Analysis Date = 04/27/16 Pct Recovery = 74% Analysis Date = 04/25/16 Pct Recovery = 74% Analysis Date = 04/25/16 Pct Recovery = 74% Analysis Date = 04/23/16 Pct Recovery = 74% Analysis Date = 04/23/16 Pct Recovery = 74% Analysis Date = 04/20/16 Pct Recovery = 74% Analysis Date = 04/20/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/11/16 Pct Recovery = 74% Analysis Date = 04/09/16 Pct Recovery = 74% Analysis Date = 04/09/16 Pct Recovery = 74% Analysis Date = 04/07/16 Pct Recovery = 74% Analysis Date = 04/07/16 Pct Recovery = 74% Analysis Date = 04/05/16 Pct Recovery = 74% Analysis Date = 04/05/16 Pct Recovery = 74% Analysis Date = 04/02/16 Pct Recovery = 75% Analysis Date = 04/02/16 Pct Recovery = 75% Analysis Date = 03/31/16 Pct Recovery = 75% Analysis Date = 03/31/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 75% Analysis Date = 03/29/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/27/16 Pct Recovery = 75% Analysis Date = 03/24/16 Pct Recovery = 75% Analysis Date = 03/24/16 Pct Recovery = 75% Analysis Date = 03/22/16 Pct Recovery = 75% Analysis Date = 03/22/16 Pct Recovery = 75% Analysis Date = 03/20/16 Pct Recovery = 75% Analysis Date = 03/20/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/18/16 Pct Recovery = 75% Analysis Date = 03/15/16 Pct Recovery = 75% Analysis Date = 03/15/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/13/16 Pct Recovery = 75% Analysis Date = 03/11/16 Pct Recovery = 75% Analysis Date = 03/11/16 Pct Recovery = 75% Analysis Date = 03/09/16 Pct Recovery = 75% Analysis Date = 03/09/16 Pct Recovery = 75% Analysis Date = 03/06/16 Pct Recovery = 75% Analysis Date = 03/06/16 Pct Recovery = 75% Analysis Date = 03/04/16 Pct Recovery = 75% Analysis Date = 03/04/16 Pct Recovery = 75% Analysis Date = 03/02/16 Pct Recovery = 75% Analysis Date = 03/02/16 Pct Recovery = 75% Analysis Date = 02/29/16 Pct Recovery = 75% Analysis Date = 02/29/16 Pct Recovery = 75% Analysis Date = 02/26/16 Pct Recovery = 76% Analysis Date = 02/26/16 Pct Recovery = 76% Analysis Date = 02/24/16 Pct Recovery = 76% Analysis Date = 02/24/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/22/16 Pct Recovery = 76% Analysis Date = 02/20/16 Pct Recovery = 76% Analysis Date = 02/20/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/17/16 Pct Recovery = 76% Analysis Date = 02/15/16 Pct Recovery = 76% Analysis Date = 02/15/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 76% Analysis Date = 02/09/16 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CARBOFURAN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 74% 15% 75% 10%
Total 19 74% 15% 75% 10%

Sample Statistics
CARBOFURAN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
CHLORPYRIFOS
METHOD: 2033 , TESTIDCODE: 38933GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 96% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 91% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 133% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 101% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 98% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 53% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 71% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 79% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 100% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 79% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 84% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 05/10/17 Pct Recovery = 95% Analysis Date = 05/08/17 Pct Recovery = 95% Analysis Date = 05/08/17 Pct Recovery = 95% Analysis Date = 05/06/17 Pct Recovery = 95% Analysis Date = 05/06/17 Pct Recovery = 95% Analysis Date = 05/04/17 Pct Recovery = 94% Analysis Date = 05/04/17 Pct Recovery = 94% Analysis Date = 05/02/17 Pct Recovery = 94% Analysis Date = 05/02/17 Pct Recovery = 94% Analysis Date = 04/30/17 Pct Recovery = 94% Analysis Date = 04/30/17 Pct Recovery = 94% Analysis Date = 04/27/17 Pct Recovery = 93% Analysis Date = 04/27/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/23/17 Pct Recovery = 93% Analysis Date = 04/23/17 Pct Recovery = 93% Analysis Date = 04/21/17 Pct Recovery = 92% Analysis Date = 04/21/17 Pct Recovery = 92% Analysis Date = 04/19/17 Pct Recovery = 92% Analysis Date = 04/19/17 Pct Recovery = 92% Analysis Date = 04/17/17 Pct Recovery = 92% Analysis Date = 04/17/17 Pct Recovery = 92% Analysis Date = 04/14/17 Pct Recovery = 91% Analysis Date = 04/14/17 Pct Recovery = 91% Analysis Date = 04/12/17 Pct Recovery = 91% Analysis Date = 04/12/17 Pct Recovery = 91% Analysis Date = 04/10/17 Pct Recovery = 91% Analysis Date = 04/10/17 Pct Recovery = 91% Analysis Date = 04/08/17 Pct Recovery = 90% Analysis Date = 04/08/17 Pct Recovery = 90% Analysis Date = 04/06/17 Pct Recovery = 90% Analysis Date = 04/06/17 Pct Recovery = 90% Analysis Date = 04/04/17 Pct Recovery = 90% Analysis Date = 04/04/17 Pct Recovery = 90% Analysis Date = 04/01/17 Pct Recovery = 89% Analysis Date = 04/01/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 88% Analysis Date = 03/26/17 Pct Recovery = 88% Analysis Date = 03/24/17 Pct Recovery = 88% Analysis Date = 03/24/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 88% Analysis Date = 03/19/17 Pct Recovery = 88% Analysis Date = 03/19/17 Pct Recovery = 88% Analysis Date = 03/17/17 Pct Recovery = 87% Analysis Date = 03/17/17 Pct Recovery = 87% Analysis Date = 03/15/17 Pct Recovery = 87% Analysis Date = 03/15/17 Pct Recovery = 87% Analysis Date = 03/13/17 Pct Recovery = 87% Analysis Date = 03/13/17 Pct Recovery = 87% Analysis Date = 03/11/17 Pct Recovery = 86% Analysis Date = 03/11/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 03/06/17 Pct Recovery = 86% Analysis Date = 03/06/17 Pct Recovery = 86% Analysis Date = 03/04/17 Pct Recovery = 85% Analysis Date = 03/04/17 Pct Recovery = 85% Analysis Date = 03/02/17 Pct Recovery = 85% Analysis Date = 03/02/17 Pct Recovery = 85% Analysis Date = 02/28/17 Pct Recovery = 85% Analysis Date = 02/28/17 Pct Recovery = 85% Analysis Date = 02/26/17 Pct Recovery = 84% Analysis Date = 02/26/17 Pct Recovery = 84% Analysis Date = 02/23/17 Pct Recovery = 84% Analysis Date = 02/23/17 Pct Recovery = 84% Analysis Date = 02/21/17 Pct Recovery = 84% Analysis Date = 02/21/17 Pct Recovery = 84% Analysis Date = 02/19/17 Pct Recovery = 84% Analysis Date = 02/19/17 Pct Recovery = 84% Analysis Date = 02/17/17 Pct Recovery = 84% Analysis Date = 02/17/17 Pct Recovery = 84% Analysis Date = 02/15/17 Pct Recovery = 84% Analysis Date = 02/15/17 Pct Recovery = 84% Analysis Date = 02/12/17 Pct Recovery = 84% Analysis Date = 02/12/17 Pct Recovery = 84% Analysis Date = 02/10/17 Pct Recovery = 84% Analysis Date = 02/10/17 Pct Recovery = 84% Analysis Date = 02/08/17 Pct Recovery = 84% Analysis Date = 02/08/17 Pct Recovery = 84% Analysis Date = 02/06/17 Pct Recovery = 83% Analysis Date = 02/06/17 Pct Recovery = 83% Analysis Date = 02/04/17 Pct Recovery = 83% Analysis Date = 02/04/17 Pct Recovery = 83% Analysis Date = 02/02/17 Pct Recovery = 83% Analysis Date = 02/02/17 Pct Recovery = 83% Analysis Date = 01/30/17 Pct Recovery = 83% Analysis Date = 01/30/17 Pct Recovery = 83% Analysis Date = 01/28/17 Pct Recovery = 83% Analysis Date = 01/28/17 Pct Recovery = 83% Analysis Date = 01/26/17 Pct Recovery = 83% Analysis Date = 01/26/17 Pct Recovery = 83% Analysis Date = 01/24/17 Pct Recovery = 83% Analysis Date = 01/24/17 Pct Recovery = 83% Analysis Date = 01/22/17 Pct Recovery = 83% Analysis Date = 01/22/17 Pct Recovery = 83% Analysis Date = 01/20/17 Pct Recovery = 83% Analysis Date = 01/20/17 Pct Recovery = 83% Analysis Date = 01/17/17 Pct Recovery = 83% Analysis Date = 01/17/17 Pct Recovery = 83% Analysis Date = 01/15/17 Pct Recovery = 83% Analysis Date = 01/15/17 Pct Recovery = 83% Analysis Date = 01/13/17 Pct Recovery = 83% Analysis Date = 01/13/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/11/17 Pct Recovery = 83% Analysis Date = 01/09/17 Pct Recovery = 83% Analysis Date = 01/09/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/04/17 Pct Recovery = 84% Analysis Date = 01/04/17 Pct Recovery = 84% Analysis Date = 01/02/17 Pct Recovery = 84% Analysis Date = 01/02/17 Pct Recovery = 84% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/22/16 Pct Recovery = 84% Analysis Date = 12/22/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/18/16 Pct Recovery = 84% Analysis Date = 12/18/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/16/16 Pct Recovery = 84% Analysis Date = 12/14/16 Pct Recovery = 84% Analysis Date = 12/14/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/09/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/07/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 12/05/16 Pct Recovery = 85% Analysis Date = 12/03/16 Pct Recovery = 85% Analysis Date = 12/03/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 85% Analysis Date = 11/22/16 Pct Recovery = 85% Analysis Date = 11/22/16 Pct Recovery = 85% Analysis Date = 11/20/16 Pct Recovery = 85% Analysis Date = 11/20/16 Pct Recovery = 85% Analysis Date = 11/17/16 Pct Recovery = 85% Analysis Date = 11/17/16 Pct Recovery = 85% Analysis Date = 11/15/16 Pct Recovery = 85% Analysis Date = 11/15/16 Pct Recovery = 85% Analysis Date = 11/13/16 Pct Recovery = 85% Analysis Date = 11/13/16 Pct Recovery = 85% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/07/16 Pct Recovery = 86% Analysis Date = 11/07/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/25/16 Pct Recovery = 86% Analysis Date = 10/25/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/16/16 Pct Recovery = 86% Analysis Date = 10/16/16 Pct Recovery = 86% Analysis Date = 10/14/16 Pct Recovery = 87% Analysis Date = 10/14/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/09/16 Pct Recovery = 87% Analysis Date = 10/07/16 Pct Recovery = 87% Analysis Date = 10/07/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/28/16 Pct Recovery = 87% Analysis Date = 09/28/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/26/16 Pct Recovery = 87% Analysis Date = 09/24/16 Pct Recovery = 87% Analysis Date = 09/24/16 Pct Recovery = 87% Analysis Date = 09/22/16 Pct Recovery = 87% Analysis Date = 09/22/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/11/16 Pct Recovery = 88% Analysis Date = 09/11/16 Pct Recovery = 88% Analysis Date = 09/09/16 Pct Recovery = 88% Analysis Date = 09/09/16 Pct Recovery = 88% Analysis Date = 09/07/16 Pct Recovery = 88% Analysis Date = 09/07/16 Pct Recovery = 88% Analysis Date = 09/05/16 Pct Recovery = 88% Analysis Date = 09/05/16 Pct Recovery = 88% Analysis Date = 09/02/16 Pct Recovery = 88% Analysis Date = 09/02/16 Pct Recovery = 88% Analysis Date = 08/31/16 Pct Recovery = 88% Analysis Date = 08/31/16 Pct Recovery = 88% Analysis Date = 08/29/16 Pct Recovery = 88% Analysis Date = 08/29/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/27/16 Pct Recovery = 88% Analysis Date = 08/25/16 Pct Recovery = 87% Analysis Date = 08/25/16 Pct Recovery = 87% Analysis Date = 08/22/16 Pct Recovery = 87% Analysis Date = 08/22/16 Pct Recovery = 87% Analysis Date = 08/20/16 Pct Recovery = 87% Analysis Date = 08/20/16 Pct Recovery = 87% Analysis Date = 08/18/16 Pct Recovery = 86% Analysis Date = 08/18/16 Pct Recovery = 86% Analysis Date = 08/16/16 Pct Recovery = 86% Analysis Date = 08/16/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/14/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/12/16 Pct Recovery = 86% Analysis Date = 08/09/16 Pct Recovery = 85% Analysis Date = 08/09/16 Pct Recovery = 85% Analysis Date = 08/07/16 Pct Recovery = 85% Analysis Date = 08/07/16 Pct Recovery = 85% Analysis Date = 08/05/16 Pct Recovery = 85% Analysis Date = 08/05/16 Pct Recovery = 85% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 08/03/16 Pct Recovery = 84% Analysis Date = 08/01/16 Pct Recovery = 84% Analysis Date = 08/01/16 Pct Recovery = 84% Analysis Date = 07/30/16 Pct Recovery = 84% Analysis Date = 07/30/16 Pct Recovery = 84% Analysis Date = 07/27/16 Pct Recovery = 83% Analysis Date = 07/27/16 Pct Recovery = 83% Analysis Date = 07/25/16 Pct Recovery = 83% Analysis Date = 07/25/16 Pct Recovery = 83% Analysis Date = 07/23/16 Pct Recovery = 83% Analysis Date = 07/23/16 Pct Recovery = 83% Analysis Date = 07/21/16 Pct Recovery = 83% Analysis Date = 07/21/16 Pct Recovery = 83% Analysis Date = 07/19/16 Pct Recovery = 82% Analysis Date = 07/19/16 Pct Recovery = 82% Analysis Date = 07/17/16 Pct Recovery = 82% Analysis Date = 07/17/16 Pct Recovery = 82% Analysis Date = 07/14/16 Pct Recovery = 82% Analysis Date = 07/14/16 Pct Recovery = 82% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/10/16 Pct Recovery = 81% Analysis Date = 07/10/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 07/03/16 Pct Recovery = 80% Analysis Date = 07/03/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 06/29/16 Pct Recovery = 80% Analysis Date = 06/29/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/25/16 Pct Recovery = 79% Analysis Date = 06/25/16 Pct Recovery = 79% Analysis Date = 06/23/16 Pct Recovery = 79% Analysis Date = 06/23/16 Pct Recovery = 79% Analysis Date = 06/20/16 Pct Recovery = 79% Analysis Date = 06/20/16 Pct Recovery = 79% Analysis Date = 06/18/16 Pct Recovery = 78% Analysis Date = 06/18/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/16/16 Pct Recovery = 78% Analysis Date = 06/14/16 Pct Recovery = 78% Analysis Date = 06/14/16 Pct Recovery = 78% Analysis Date = 06/12/16 Pct Recovery = 77% Analysis Date = 06/12/16 Pct Recovery = 77% Analysis Date = 06/10/16 Pct Recovery = 77% Analysis Date = 06/10/16 Pct Recovery = 77% Analysis Date = 06/07/16 Pct Recovery = 77% Analysis Date = 06/07/16 Pct Recovery = 77% Analysis Date = 06/05/16 Pct Recovery = 77% Analysis Date = 06/05/16 Pct Recovery = 77% Analysis Date = 06/03/16 Pct Recovery = 76% Analysis Date = 06/03/16 Pct Recovery = 76% Analysis Date = 06/01/16 Pct Recovery = 76% Analysis Date = 06/01/16 Pct Recovery = 76% Analysis Date = 05/30/16 Pct Recovery = 76% Analysis Date = 05/30/16 Pct Recovery = 76% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/23/16 Pct Recovery = 75% Analysis Date = 05/23/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 74% Analysis Date = 05/21/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 74% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/06/16 Pct Recovery = 72% Analysis Date = 05/06/16 Pct Recovery = 72% Analysis Date = 05/04/16 Pct Recovery = 72% Analysis Date = 05/04/16 Pct Recovery = 72% Analysis Date = 05/01/16 Pct Recovery = 71% Analysis Date = 05/01/16 Pct Recovery = 71% Analysis Date = 04/29/16 Pct Recovery = 71% Analysis Date = 04/29/16 Pct Recovery = 71% Analysis Date = 04/27/16 Pct Recovery = 71% Analysis Date = 04/27/16 Pct Recovery = 71% Analysis Date = 04/25/16 Pct Recovery = 70% Analysis Date = 04/25/16 Pct Recovery = 70% Analysis Date = 04/23/16 Pct Recovery = 70% Analysis Date = 04/23/16 Pct Recovery = 70% Analysis Date = 04/21/16 Pct Recovery = 70% Analysis Date = 04/21/16 Pct Recovery = 70% Analysis Date = 04/18/16 Pct Recovery = 69% Analysis Date = 04/18/16 Pct Recovery = 69% Analysis Date = 04/16/16 Pct Recovery = 69% Analysis Date = 04/16/16 Pct Recovery = 69% Analysis Date = 04/14/16 Pct Recovery = 69% Analysis Date = 04/14/16 Pct Recovery = 69% Analysis Date = 04/12/16 Pct Recovery = 68% Analysis Date = 04/12/16 Pct Recovery = 68% Analysis Date = 04/10/16 Pct Recovery = 68% Analysis Date = 04/10/16 Pct Recovery = 68% Analysis Date = 04/07/16 Pct Recovery = 67% Analysis Date = 04/07/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/03/16 Pct Recovery = 67% Analysis Date = 04/03/16 Pct Recovery = 67% Analysis Date = 04/01/16 Pct Recovery = 66% Analysis Date = 04/01/16 Pct Recovery = 66% Analysis Date = 03/30/16 Pct Recovery = 66% Analysis Date = 03/30/16 Pct Recovery = 66% Analysis Date = 03/28/16 Pct Recovery = 66% Analysis Date = 03/28/16 Pct Recovery = 66% Analysis Date = 03/25/16 Pct Recovery = 65% Analysis Date = 03/25/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/21/16 Pct Recovery = 65% Analysis Date = 03/21/16 Pct Recovery = 65% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/17/16 Pct Recovery = 64% Analysis Date = 03/17/16 Pct Recovery = 64% Analysis Date = 03/15/16 Pct Recovery = 64% Analysis Date = 03/15/16 Pct Recovery = 64% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/10/16 Pct Recovery = 63% Analysis Date = 03/10/16 Pct Recovery = 63% Analysis Date = 03/08/16 Pct Recovery = 63% Analysis Date = 03/08/16 Pct Recovery = 63% Analysis Date = 03/06/16 Pct Recovery = 62% Analysis Date = 03/06/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/02/16 Pct Recovery = 62% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 82% 19% 79% 23%
Total 18 82% 19% 79% 23%

Sample Statistics
CHLORPYRIFOS

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
CHLORPYRIFOS, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61636GCM39

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 50% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 42% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 46% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 45% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 34% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 31% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 63% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 54% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 50% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 63% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 66% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 58% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 56% Analysis Date = 05/10/17 Pct Recovery = 35% Analysis Date = 05/08/17 Pct Recovery = 35% Analysis Date = 05/08/17 Pct Recovery = 35% Analysis Date = 05/06/17 Pct Recovery = 35% Analysis Date = 05/06/17 Pct Recovery = 35% Analysis Date = 05/04/17 Pct Recovery = 35% Analysis Date = 05/04/17 Pct Recovery = 35% Analysis Date = 05/01/17 Pct Recovery = 35% Analysis Date = 05/01/17 Pct Recovery = 35% Analysis Date = 04/29/17 Pct Recovery = 35% Analysis Date = 04/29/17 Pct Recovery = 35% Analysis Date = 04/27/17 Pct Recovery = 36% Analysis Date = 04/27/17 Pct Recovery = 36% Analysis Date = 04/25/17 Pct Recovery = 36% Analysis Date = 04/25/17 Pct Recovery = 36% Analysis Date = 04/22/17 Pct Recovery = 36% Analysis Date = 04/22/17 Pct Recovery = 36% Analysis Date = 04/20/17 Pct Recovery = 36% Analysis Date = 04/20/17 Pct Recovery = 36% Analysis Date = 04/18/17 Pct Recovery = 36% Analysis Date = 04/18/17 Pct Recovery = 36% Analysis Date = 04/15/17 Pct Recovery = 36% Analysis Date = 04/15/17 Pct Recovery = 36% Analysis Date = 04/13/17 Pct Recovery = 36% Analysis Date = 04/13/17 Pct Recovery = 36% Analysis Date = 04/11/17 Pct Recovery = 36% Analysis Date = 04/11/17 Pct Recovery = 36% Analysis Date = 04/09/17 Pct Recovery = 37% Analysis Date = 04/09/17 Pct Recovery = 37% Analysis Date = 04/06/17 Pct Recovery = 37% Analysis Date = 04/06/17 Pct Recovery = 37% Analysis Date = 04/04/17 Pct Recovery = 37% Analysis Date = 04/04/17 Pct Recovery = 37% Analysis Date = 04/02/17 Pct Recovery = 37% Analysis Date = 04/02/17 Pct Recovery = 37% Analysis Date = 03/30/17 Pct Recovery = 37% Analysis Date = 03/30/17 Pct Recovery = 37% Analysis Date = 03/28/17 Pct Recovery = 37% Analysis Date = 03/28/17 Pct Recovery = 37% Analysis Date = 03/26/17 Pct Recovery = 37% Analysis Date = 03/26/17 Pct Recovery = 37% Analysis Date = 03/24/17 Pct Recovery = 38% Analysis Date = 03/24/17 Pct Recovery = 38% Analysis Date = 03/21/17 Pct Recovery = 38% Analysis Date = 03/21/17 Pct Recovery = 38% Analysis Date = 03/19/17 Pct Recovery = 38% Analysis Date = 03/19/17 Pct Recovery = 38% Analysis Date = 03/17/17 Pct Recovery = 38% Analysis Date = 03/17/17 Pct Recovery = 38% Analysis Date = 03/14/17 Pct Recovery = 38% Analysis Date = 03/14/17 Pct Recovery = 38% Analysis Date = 03/12/17 Pct Recovery = 38% Analysis Date = 03/12/17 Pct Recovery = 38% Analysis Date = 03/10/17 Pct Recovery = 38% Analysis Date = 03/10/17 Pct Recovery = 38% Analysis Date = 03/08/17 Pct Recovery = 39% Analysis Date = 03/08/17 Pct Recovery = 39% Analysis Date = 03/05/17 Pct Recovery = 39% Analysis Date = 03/05/17 Pct Recovery = 39% Analysis Date = 03/03/17 Pct Recovery = 39% Analysis Date = 03/03/17 Pct Recovery = 39% Analysis Date = 03/01/17 Pct Recovery = 39% Analysis Date = 03/01/17 Pct Recovery = 39% Analysis Date = 02/26/17 Pct Recovery = 39% Analysis Date = 02/26/17 Pct Recovery = 39% Analysis Date = 02/24/17 Pct Recovery = 39% Analysis Date = 02/24/17 Pct Recovery = 39% Analysis Date = 02/22/17 Pct Recovery = 39% Analysis Date = 02/22/17 Pct Recovery = 39% Analysis Date = 02/20/17 Pct Recovery = 40% Analysis Date = 02/20/17 Pct Recovery = 40% Analysis Date = 02/17/17 Pct Recovery = 40% Analysis Date = 02/17/17 Pct Recovery = 40% Analysis Date = 02/15/17 Pct Recovery = 40% Analysis Date = 02/15/17 Pct Recovery = 40% Analysis Date = 02/13/17 Pct Recovery = 40% Analysis Date = 02/13/17 Pct Recovery = 40% Analysis Date = 02/10/17 Pct Recovery = 40% Analysis Date = 02/10/17 Pct Recovery = 40% Analysis Date = 02/08/17 Pct Recovery = 40% Analysis Date = 02/08/17 Pct Recovery = 40% Analysis Date = 02/06/17 Pct Recovery = 40% Analysis Date = 02/06/17 Pct Recovery = 40% Analysis Date = 02/04/17 Pct Recovery = 40% Analysis Date = 02/04/17 Pct Recovery = 40% Analysis Date = 02/01/17 Pct Recovery = 41% Analysis Date = 02/01/17 Pct Recovery = 41% Analysis Date = 01/30/17 Pct Recovery = 41% Analysis Date = 01/30/17 Pct Recovery = 41% Analysis Date = 01/28/17 Pct Recovery = 41% Analysis Date = 01/28/17 Pct Recovery = 41% Analysis Date = 01/25/17 Pct Recovery = 41% Analysis Date = 01/25/17 Pct Recovery = 41% Analysis Date = 01/23/17 Pct Recovery = 41% Analysis Date = 01/23/17 Pct Recovery = 41% Analysis Date = 01/21/17 Pct Recovery = 41% Analysis Date = 01/21/17 Pct Recovery = 41% Analysis Date = 01/19/17 Pct Recovery = 41% Analysis Date = 01/19/17 Pct Recovery = 41% Analysis Date = 01/16/17 Pct Recovery = 42% Analysis Date = 01/16/17 Pct Recovery = 42% Analysis Date = 01/14/17 Pct Recovery = 42% Analysis Date = 01/14/17 Pct Recovery = 42% Analysis Date = 01/12/17 Pct Recovery = 42% Analysis Date = 01/12/17 Pct Recovery = 42% Analysis Date = 01/09/17 Pct Recovery = 42% Analysis Date = 01/09/17 Pct Recovery = 42% Analysis Date = 01/07/17 Pct Recovery = 43% Analysis Date = 01/07/17 Pct Recovery = 43% Analysis Date = 01/05/17 Pct Recovery = 43% Analysis Date = 01/05/17 Pct Recovery = 43% Analysis Date = 01/03/17 Pct Recovery = 43% Analysis Date = 01/03/17 Pct Recovery = 43% Analysis Date = 12/31/16 Pct Recovery = 43% Analysis Date = 12/31/16 Pct Recovery = 43% Analysis Date = 12/29/16 Pct Recovery = 44% Analysis Date = 12/29/16 Pct Recovery = 44% Analysis Date = 12/27/16 Pct Recovery = 44% Analysis Date = 12/27/16 Pct Recovery = 44% Analysis Date = 12/24/16 Pct Recovery = 44% Analysis Date = 12/24/16 Pct Recovery = 44% Analysis Date = 12/22/16 Pct Recovery = 44% Analysis Date = 12/22/16 Pct Recovery = 44% Analysis Date = 12/20/16 Pct Recovery = 45% Analysis Date = 12/20/16 Pct Recovery = 45% Analysis Date = 12/18/16 Pct Recovery = 45% Analysis Date = 12/18/16 Pct Recovery = 45% Analysis Date = 12/15/16 Pct Recovery = 45% Analysis Date = 12/15/16 Pct Recovery = 45% Analysis Date = 12/13/16 Pct Recovery = 46% Analysis Date = 12/13/16 Pct Recovery = 46% Analysis Date = 12/11/16 Pct Recovery = 46% Analysis Date = 12/11/16 Pct Recovery = 46% Analysis Date = 12/08/16 Pct Recovery = 46% Analysis Date = 12/08/16 Pct Recovery = 46% Analysis Date = 12/06/16 Pct Recovery = 46% Analysis Date = 12/06/16 Pct Recovery = 46% Analysis Date = 12/04/16 Pct Recovery = 47% Analysis Date = 12/04/16 Pct Recovery = 47% Analysis Date = 12/02/16 Pct Recovery = 47% Analysis Date = 12/02/16 Pct Recovery = 47% Analysis Date = 11/29/16 Pct Recovery = 47% Analysis Date = 11/29/16 Pct Recovery = 47% Analysis Date = 11/27/16 Pct Recovery = 47% Analysis Date = 11/27/16 Pct Recovery = 47% Analysis Date = 11/25/16 Pct Recovery = 48% Analysis Date = 11/25/16 Pct Recovery = 48% Analysis Date = 11/22/16 Pct Recovery = 48% Analysis Date = 11/22/16 Pct Recovery = 48% Analysis Date = 11/20/16 Pct Recovery = 48% Analysis Date = 11/20/16 Pct Recovery = 48% Analysis Date = 11/18/16 Pct Recovery = 48% Analysis Date = 11/18/16 Pct Recovery = 48% Analysis Date = 11/16/16 Pct Recovery = 49% Analysis Date = 11/16/16 Pct Recovery = 49% Analysis Date = 11/13/16 Pct Recovery = 49% Analysis Date = 11/13/16 Pct Recovery = 49% Analysis Date = 11/11/16 Pct Recovery = 49% Analysis Date = 11/11/16 Pct Recovery = 49% Analysis Date = 11/09/16 Pct Recovery = 49% Analysis Date = 11/09/16 Pct Recovery = 49% Analysis Date = 11/06/16 Pct Recovery = 50% Analysis Date = 11/06/16 Pct Recovery = 50% Analysis Date = 11/04/16 Pct Recovery = 50% Analysis Date = 11/04/16 Pct Recovery = 50% Analysis Date = 11/02/16 Pct Recovery = 50% Analysis Date = 11/02/16 Pct Recovery = 50% Analysis Date = 10/31/16 Pct Recovery = 50% Analysis Date = 10/31/16 Pct Recovery = 50% Analysis Date = 10/28/16 Pct Recovery = 51% Analysis Date = 10/28/16 Pct Recovery = 51% Analysis Date = 10/26/16 Pct Recovery = 51% Analysis Date = 10/26/16 Pct Recovery = 51% Analysis Date = 10/24/16 Pct Recovery = 51% Analysis Date = 10/24/16 Pct Recovery = 51% Analysis Date = 10/21/16 Pct Recovery = 51% Analysis Date = 10/21/16 Pct Recovery = 51% Analysis Date = 10/19/16 Pct Recovery = 52% Analysis Date = 10/19/16 Pct Recovery = 52% Analysis Date = 10/17/16 Pct Recovery = 52% Analysis Date = 10/17/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/15/16 Pct Recovery = 52% Analysis Date = 10/12/16 Pct Recovery = 52% Analysis Date = 10/12/16 Pct Recovery = 52% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/08/16 Pct Recovery = 53% Analysis Date = 10/08/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/03/16 Pct Recovery = 53% Analysis Date = 10/03/16 Pct Recovery = 53% Analysis Date = 10/01/16 Pct Recovery = 54% Analysis Date = 10/01/16 Pct Recovery = 54% Analysis Date = 09/29/16 Pct Recovery = 54% Analysis Date = 09/29/16 Pct Recovery = 54% Analysis Date = 09/26/16 Pct Recovery = 54% Analysis Date = 09/26/16 Pct Recovery = 54% Analysis Date = 09/24/16 Pct Recovery = 55% Analysis Date = 09/24/16 Pct Recovery = 55% Analysis Date = 09/22/16 Pct Recovery = 55% Analysis Date = 09/22/16 Pct Recovery = 55% Analysis Date = 09/19/16 Pct Recovery = 55% Analysis Date = 09/19/16 Pct Recovery = 55% Analysis Date = 09/17/16 Pct Recovery = 55% Analysis Date = 09/17/16 Pct Recovery = 55% Analysis Date = 09/15/16 Pct Recovery = 56% Analysis Date = 09/15/16 Pct Recovery = 56% Analysis Date = 09/13/16 Pct Recovery = 56% Analysis Date = 09/13/16 Pct Recovery = 56% Analysis Date = 09/10/16 Pct Recovery = 56% Analysis Date = 09/10/16 Pct Recovery = 56% Analysis Date = 09/08/16 Pct Recovery = 56% Analysis Date = 09/08/16 Pct Recovery = 56% Analysis Date = 09/06/16 Pct Recovery = 56% Analysis Date = 09/06/16 Pct Recovery = 56% Analysis Date = 09/03/16 Pct Recovery = 56% Analysis Date = 09/03/16 Pct Recovery = 56% Analysis Date = 09/01/16 Pct Recovery = 56% Analysis Date = 09/01/16 Pct Recovery = 56% Analysis Date = 08/30/16 Pct Recovery = 56% Analysis Date = 08/30/16 Pct Recovery = 56% Analysis Date = 08/28/16 Pct Recovery = 56% Analysis Date = 08/28/16 Pct Recovery = 56% Analysis Date = 08/25/16 Pct Recovery = 56% Analysis Date = 08/25/16 Pct Recovery = 56% Analysis Date = 08/23/16 Pct Recovery = 55% Analysis Date = 08/23/16 Pct Recovery = 55% Analysis Date = 08/21/16 Pct Recovery = 55% Analysis Date = 08/21/16 Pct Recovery = 55% Analysis Date = 08/18/16 Pct Recovery = 55% Analysis Date = 08/18/16 Pct Recovery = 55% Analysis Date = 08/16/16 Pct Recovery = 55% Analysis Date = 08/16/16 Pct Recovery = 55% Analysis Date = 08/14/16 Pct Recovery = 55% Analysis Date = 08/14/16 Pct Recovery = 55% Analysis Date = 08/12/16 Pct Recovery = 55% Analysis Date = 08/12/16 Pct Recovery = 55% Analysis Date = 08/09/16 Pct Recovery = 55% Analysis Date = 08/09/16 Pct Recovery = 55% Analysis Date = 08/07/16 Pct Recovery = 55% Analysis Date = 08/07/16 Pct Recovery = 55% Analysis Date = 08/05/16 Pct Recovery = 54% Analysis Date = 08/05/16 Pct Recovery = 54% Analysis Date = 08/02/16 Pct Recovery = 54% Analysis Date = 08/02/16 Pct Recovery = 54% Analysis Date = 07/31/16 Pct Recovery = 54% Analysis Date = 07/31/16 Pct Recovery = 54% Analysis Date = 07/29/16 Pct Recovery = 54% Analysis Date = 07/29/16 Pct Recovery = 54% Analysis Date = 07/27/16 Pct Recovery = 54% Analysis Date = 07/27/16 Pct Recovery = 54% Analysis Date = 07/24/16 Pct Recovery = 54% Analysis Date = 07/24/16 Pct Recovery = 54% Analysis Date = 07/22/16 Pct Recovery = 54% Analysis Date = 07/22/16 Pct Recovery = 54% Analysis Date = 07/20/16 Pct Recovery = 54% Analysis Date = 07/20/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 53% Analysis Date = 07/17/16 Pct Recovery = 53% Analysis Date = 07/15/16 Pct Recovery = 53% Analysis Date = 07/15/16 Pct Recovery = 53% Analysis Date = 07/13/16 Pct Recovery = 53% Analysis Date = 07/13/16 Pct Recovery = 53% Analysis Date = 07/11/16 Pct Recovery = 53% Analysis Date = 07/11/16 Pct Recovery = 53% Analysis Date = 07/08/16 Pct Recovery = 53% Analysis Date = 07/08/16 Pct Recovery = 53% Analysis Date = 07/06/16 Pct Recovery = 53% Analysis Date = 07/06/16 Pct Recovery = 53% Analysis Date = 07/04/16 Pct Recovery = 53% Analysis Date = 07/04/16 Pct Recovery = 53% Analysis Date = 07/01/16 Pct Recovery = 52% Analysis Date = 07/01/16 Pct Recovery = 52% Analysis Date = 06/29/16 Pct Recovery = 52% Analysis Date = 06/29/16 Pct Recovery = 52% Analysis Date = 06/27/16 Pct Recovery = 52% Analysis Date = 06/27/16 Pct Recovery = 52% Analysis Date = 06/25/16 Pct Recovery = 52% Analysis Date = 06/25/16 Pct Recovery = 52% Analysis Date = 06/22/16 Pct Recovery = 52% Analysis Date = 06/22/16 Pct Recovery = 52% Analysis Date = 06/20/16 Pct Recovery = 52% Analysis Date = 06/20/16 Pct Recovery = 52% Analysis Date = 06/18/16 Pct Recovery = 52% Analysis Date = 06/18/16 Pct Recovery = 52% Analysis Date = 06/15/16 Pct Recovery = 52% Analysis Date = 06/15/16 Pct Recovery = 52% Analysis Date = 06/13/16 Pct Recovery = 51% Analysis Date = 06/13/16 Pct Recovery = 51% Analysis Date = 06/11/16 Pct Recovery = 51% Analysis Date = 06/11/16 Pct Recovery = 51% Analysis Date = 06/09/16 Pct Recovery = 51% Analysis Date = 06/09/16 Pct Recovery = 51% Analysis Date = 06/06/16 Pct Recovery = 51% Analysis Date = 06/06/16 Pct Recovery = 51% Analysis Date = 06/04/16 Pct Recovery = 51% Analysis Date = 06/04/16 Pct Recovery = 51% Analysis Date = 06/02/16 Pct Recovery = 51% Analysis Date = 06/02/16 Pct Recovery = 51% Analysis Date = 05/30/16 Pct Recovery = 51% Analysis Date = 05/30/16 Pct Recovery = 51% Analysis Date = 05/28/16 Pct Recovery = 50% Analysis Date = 05/28/16 Pct Recovery = 50% Analysis Date = 05/26/16 Pct Recovery = 51% Analysis Date = 05/26/16 Pct Recovery = 51% Analysis Date = 05/24/16 Pct Recovery = 51% Analysis Date = 05/24/16 Pct Recovery = 51% Analysis Date = 05/21/16 Pct Recovery = 52% Analysis Date = 05/21/16 Pct Recovery = 52% Analysis Date = 05/19/16 Pct Recovery = 52% Analysis Date = 05/19/16 Pct Recovery = 52% Analysis Date = 05/17/16 Pct Recovery = 53% Analysis Date = 05/17/16 Pct Recovery = 53% Analysis Date = 05/14/16 Pct Recovery = 53% Analysis Date = 05/14/16 Pct Recovery = 53% Analysis Date = 05/12/16 Pct Recovery = 53% Analysis Date = 05/12/16 Pct Recovery = 53% Analysis Date = 05/10/16 Pct Recovery = 54% Analysis Date = 05/10/16 Pct Recovery = 54% Analysis Date = 05/08/16 Pct Recovery = 54% Analysis Date = 05/08/16 Pct Recovery = 54% Analysis Date = 05/05/16 Pct Recovery = 54% Analysis Date = 05/05/16 Pct Recovery = 54% Analysis Date = 05/03/16 Pct Recovery = 55% Analysis Date = 05/03/16 Pct Recovery = 55% Analysis Date = 05/01/16 Pct Recovery = 55% Analysis Date = 05/01/16 Pct Recovery = 55% Analysis Date = 04/28/16 Pct Recovery = 55% Analysis Date = 04/28/16 Pct Recovery = 55% Analysis Date = 04/26/16 Pct Recovery = 56% Analysis Date = 04/26/16 Pct Recovery = 56% Analysis Date = 04/24/16 Pct Recovery = 56% Analysis Date = 04/24/16 Pct Recovery = 56% Analysis Date = 04/22/16 Pct Recovery = 57% Analysis Date = 04/22/16 Pct Recovery = 57% Analysis Date = 04/19/16 Pct Recovery = 57% Analysis Date = 04/19/16 Pct Recovery = 57% Analysis Date = 04/17/16 Pct Recovery = 57% Analysis Date = 04/17/16 Pct Recovery = 57% Analysis Date = 04/15/16 Pct Recovery = 57% Analysis Date = 04/15/16 Pct Recovery = 57% Analysis Date = 04/12/16 Pct Recovery = 57% Analysis Date = 04/12/16 Pct Recovery = 57% Analysis Date = 04/10/16 Pct Recovery = 57% Analysis Date = 04/10/16 Pct Recovery = 57% Analysis Date = 04/08/16 Pct Recovery = 57% Analysis Date = 04/08/16 Pct Recovery = 57% Analysis Date = 04/06/16 Pct Recovery = 57% Analysis Date = 04/06/16 Pct Recovery = 57% Analysis Date = 04/03/16 Pct Recovery = 57% Analysis Date = 04/03/16 Pct Recovery = 57% Analysis Date = 04/01/16 Pct Recovery = 57% Analysis Date = 04/01/16 Pct Recovery = 57% Analysis Date = 03/30/16 Pct Recovery = 57% Analysis Date = 03/30/16 Pct Recovery = 57% Analysis Date = 03/27/16 Pct Recovery = 57% Analysis Date = 03/27/16 Pct Recovery = 57% Analysis Date = 03/25/16 Pct Recovery = 57% Analysis Date = 03/25/16 Pct Recovery = 57% Analysis Date = 03/23/16 Pct Recovery = 57% Analysis Date = 03/23/16 Pct Recovery = 57% Analysis Date = 03/21/16 Pct Recovery = 57% Analysis Date = 03/21/16 Pct Recovery = 57% Analysis Date = 03/18/16 Pct Recovery = 57% Analysis Date = 03/18/16 Pct Recovery = 57% Analysis Date = 03/16/16 Pct Recovery = 57% Analysis Date = 03/16/16 Pct Recovery = 57% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/05/16 Pct Recovery = 58% Analysis Date = 03/05/16 Pct Recovery = 58% Analysis Date = 03/02/16 Pct Recovery = 58% Analysis Date = 03/02/16 Pct Recovery = 58% Analysis Date = 02/29/16 Pct Recovery = 58% Analysis Date = 02/29/16 Pct Recovery = 58% Analysis Date = 02/27/16 Pct Recovery = 58% Analysis Date = 02/27/16 Pct Recovery = 58% Analysis Date = 02/24/16 Pct Recovery = 58% Analysis Date = 02/24/16 Pct Recovery = 58% Analysis Date = 02/22/16 Pct Recovery = 58% Analysis Date = 02/22/16 Pct Recovery = 58% Analysis Date = 02/20/16 Pct Recovery = 58% Analysis Date = 02/20/16 Pct Recovery = 58% Analysis Date = 02/18/16 Pct Recovery = 58% Analysis Date = 02/18/16 Pct Recovery = 58% Analysis Date = 02/15/16 Pct Recovery = 58% Analysis Date = 02/15/16 Pct Recovery = 58% Analysis Date = 02/13/16 Pct Recovery = 58% Analysis Date = 02/13/16 Pct Recovery = 58% Analysis Date = 02/11/16 Pct Recovery = 58% Analysis Date = 02/11/16 Pct Recovery = 58% Analysis Date = 02/09/16 Pct Recovery = 58% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CHLORPYRIFOS, OXYGEN ANALOG

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 51% 11% 50% 9%
Total 13 51% 11% 50% 9%

Sample Statistics
CHLORPYRIFOS, OXYGEN ANALOG

Characteristic N % % Basis
Plotted 13 100% Spiked
Estimated Values 13 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 13 .  
False Negatives 0 0% 0 out of 13
Not Spiked 15 .  
False Positives 0 0% 0 out of 15

OBSP Determination:
CIS-PERMETHRIN
METHOD: 2033 , TESTIDCODE: 82687GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 37% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 33% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 115% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 26% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 51% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 66% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 66% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 36% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 42% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 38% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 68% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 78% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 81% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 66% Analysis Date = 05/10/17 Pct Recovery = 52% Analysis Date = 05/08/17 Pct Recovery = 52% Analysis Date = 05/08/17 Pct Recovery = 52% Analysis Date = 05/06/17 Pct Recovery = 52% Analysis Date = 05/06/17 Pct Recovery = 52% Analysis Date = 05/04/17 Pct Recovery = 52% Analysis Date = 05/04/17 Pct Recovery = 52% Analysis Date = 05/02/17 Pct Recovery = 52% Analysis Date = 05/02/17 Pct Recovery = 52% Analysis Date = 04/30/17 Pct Recovery = 51% Analysis Date = 04/30/17 Pct Recovery = 51% Analysis Date = 04/27/17 Pct Recovery = 51% Analysis Date = 04/27/17 Pct Recovery = 51% Analysis Date = 04/25/17 Pct Recovery = 51% Analysis Date = 04/25/17 Pct Recovery = 51% Analysis Date = 04/23/17 Pct Recovery = 51% Analysis Date = 04/23/17 Pct Recovery = 51% Analysis Date = 04/21/17 Pct Recovery = 51% Analysis Date = 04/21/17 Pct Recovery = 51% Analysis Date = 04/19/17 Pct Recovery = 51% Analysis Date = 04/19/17 Pct Recovery = 51% Analysis Date = 04/17/17 Pct Recovery = 51% Analysis Date = 04/17/17 Pct Recovery = 51% Analysis Date = 04/14/17 Pct Recovery = 51% Analysis Date = 04/14/17 Pct Recovery = 51% Analysis Date = 04/12/17 Pct Recovery = 51% Analysis Date = 04/12/17 Pct Recovery = 51% Analysis Date = 04/10/17 Pct Recovery = 51% Analysis Date = 04/10/17 Pct Recovery = 51% Analysis Date = 04/08/17 Pct Recovery = 51% Analysis Date = 04/08/17 Pct Recovery = 51% Analysis Date = 04/06/17 Pct Recovery = 51% Analysis Date = 04/06/17 Pct Recovery = 51% Analysis Date = 04/04/17 Pct Recovery = 50% Analysis Date = 04/04/17 Pct Recovery = 50% Analysis Date = 04/01/17 Pct Recovery = 50% Analysis Date = 04/01/17 Pct Recovery = 50% Analysis Date = 03/30/17 Pct Recovery = 50% Analysis Date = 03/30/17 Pct Recovery = 50% Analysis Date = 03/28/17 Pct Recovery = 50% Analysis Date = 03/28/17 Pct Recovery = 50% Analysis Date = 03/26/17 Pct Recovery = 50% Analysis Date = 03/26/17 Pct Recovery = 50% Analysis Date = 03/24/17 Pct Recovery = 50% Analysis Date = 03/24/17 Pct Recovery = 50% Analysis Date = 03/21/17 Pct Recovery = 50% Analysis Date = 03/21/17 Pct Recovery = 50% Analysis Date = 03/19/17 Pct Recovery = 50% Analysis Date = 03/19/17 Pct Recovery = 50% Analysis Date = 03/17/17 Pct Recovery = 50% Analysis Date = 03/17/17 Pct Recovery = 50% Analysis Date = 03/15/17 Pct Recovery = 50% Analysis Date = 03/15/17 Pct Recovery = 50% Analysis Date = 03/13/17 Pct Recovery = 50% Analysis Date = 03/13/17 Pct Recovery = 50% Analysis Date = 03/11/17 Pct Recovery = 50% Analysis Date = 03/11/17 Pct Recovery = 50% Analysis Date = 03/08/17 Pct Recovery = 50% Analysis Date = 03/08/17 Pct Recovery = 50% Analysis Date = 03/06/17 Pct Recovery = 50% Analysis Date = 03/06/17 Pct Recovery = 50% Analysis Date = 03/04/17 Pct Recovery = 49% Analysis Date = 03/04/17 Pct Recovery = 49% Analysis Date = 03/02/17 Pct Recovery = 49% Analysis Date = 03/02/17 Pct Recovery = 49% Analysis Date = 02/28/17 Pct Recovery = 49% Analysis Date = 02/28/17 Pct Recovery = 49% Analysis Date = 02/26/17 Pct Recovery = 49% Analysis Date = 02/26/17 Pct Recovery = 49% Analysis Date = 02/23/17 Pct Recovery = 49% Analysis Date = 02/23/17 Pct Recovery = 49% Analysis Date = 02/21/17 Pct Recovery = 49% Analysis Date = 02/21/17 Pct Recovery = 49% Analysis Date = 02/19/17 Pct Recovery = 49% Analysis Date = 02/19/17 Pct Recovery = 49% Analysis Date = 02/17/17 Pct Recovery = 49% Analysis Date = 02/17/17 Pct Recovery = 49% Analysis Date = 02/15/17 Pct Recovery = 49% Analysis Date = 02/15/17 Pct Recovery = 49% Analysis Date = 02/12/17 Pct Recovery = 49% Analysis Date = 02/12/17 Pct Recovery = 49% Analysis Date = 02/10/17 Pct Recovery = 49% Analysis Date = 02/10/17 Pct Recovery = 49% Analysis Date = 02/08/17 Pct Recovery = 49% Analysis Date = 02/08/17 Pct Recovery = 49% Analysis Date = 02/06/17 Pct Recovery = 49% Analysis Date = 02/06/17 Pct Recovery = 49% Analysis Date = 02/04/17 Pct Recovery = 49% Analysis Date = 02/04/17 Pct Recovery = 49% Analysis Date = 02/02/17 Pct Recovery = 49% Analysis Date = 02/02/17 Pct Recovery = 49% Analysis Date = 01/30/17 Pct Recovery = 49% Analysis Date = 01/30/17 Pct Recovery = 49% Analysis Date = 01/28/17 Pct Recovery = 49% Analysis Date = 01/28/17 Pct Recovery = 49% Analysis Date = 01/26/17 Pct Recovery = 49% Analysis Date = 01/26/17 Pct Recovery = 49% Analysis Date = 01/24/17 Pct Recovery = 49% Analysis Date = 01/24/17 Pct Recovery = 49% Analysis Date = 01/22/17 Pct Recovery = 50% Analysis Date = 01/22/17 Pct Recovery = 50% Analysis Date = 01/20/17 Pct Recovery = 50% Analysis Date = 01/20/17 Pct Recovery = 50% Analysis Date = 01/17/17 Pct Recovery = 50% Analysis Date = 01/17/17 Pct Recovery = 50% Analysis Date = 01/15/17 Pct Recovery = 50% Analysis Date = 01/15/17 Pct Recovery = 50% Analysis Date = 01/13/17 Pct Recovery = 50% Analysis Date = 01/13/17 Pct Recovery = 50% Analysis Date = 01/11/17 Pct Recovery = 51% Analysis Date = 01/11/17 Pct Recovery = 51% Analysis Date = 01/09/17 Pct Recovery = 51% Analysis Date = 01/09/17 Pct Recovery = 51% Analysis Date = 01/07/17 Pct Recovery = 52% Analysis Date = 01/07/17 Pct Recovery = 52% Analysis Date = 01/04/17 Pct Recovery = 52% Analysis Date = 01/04/17 Pct Recovery = 52% Analysis Date = 01/02/17 Pct Recovery = 53% Analysis Date = 01/02/17 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/31/16 Pct Recovery = 53% Analysis Date = 12/29/16 Pct Recovery = 53% Analysis Date = 12/29/16 Pct Recovery = 53% Analysis Date = 12/27/16 Pct Recovery = 54% Analysis Date = 12/27/16 Pct Recovery = 54% Analysis Date = 12/24/16 Pct Recovery = 54% Analysis Date = 12/24/16 Pct Recovery = 54% Analysis Date = 12/22/16 Pct Recovery = 55% Analysis Date = 12/22/16 Pct Recovery = 55% Analysis Date = 12/20/16 Pct Recovery = 55% Analysis Date = 12/20/16 Pct Recovery = 55% Analysis Date = 12/18/16 Pct Recovery = 55% Analysis Date = 12/18/16 Pct Recovery = 55% Analysis Date = 12/16/16 Pct Recovery = 56% Analysis Date = 12/16/16 Pct Recovery = 56% Analysis Date = 12/14/16 Pct Recovery = 56% Analysis Date = 12/14/16 Pct Recovery = 56% Analysis Date = 12/11/16 Pct Recovery = 56% Analysis Date = 12/11/16 Pct Recovery = 56% Analysis Date = 12/09/16 Pct Recovery = 57% Analysis Date = 12/09/16 Pct Recovery = 57% Analysis Date = 12/07/16 Pct Recovery = 57% Analysis Date = 12/07/16 Pct Recovery = 57% Analysis Date = 12/05/16 Pct Recovery = 57% Analysis Date = 12/05/16 Pct Recovery = 57% Analysis Date = 12/03/16 Pct Recovery = 58% Analysis Date = 12/03/16 Pct Recovery = 58% Analysis Date = 12/01/16 Pct Recovery = 58% Analysis Date = 12/01/16 Pct Recovery = 58% Analysis Date = 11/28/16 Pct Recovery = 58% Analysis Date = 11/28/16 Pct Recovery = 58% Analysis Date = 11/26/16 Pct Recovery = 58% Analysis Date = 11/26/16 Pct Recovery = 58% Analysis Date = 11/24/16 Pct Recovery = 59% Analysis Date = 11/24/16 Pct Recovery = 59% Analysis Date = 11/22/16 Pct Recovery = 59% Analysis Date = 11/22/16 Pct Recovery = 59% Analysis Date = 11/20/16 Pct Recovery = 59% Analysis Date = 11/20/16 Pct Recovery = 59% Analysis Date = 11/17/16 Pct Recovery = 60% Analysis Date = 11/17/16 Pct Recovery = 60% Analysis Date = 11/15/16 Pct Recovery = 60% Analysis Date = 11/15/16 Pct Recovery = 60% Analysis Date = 11/13/16 Pct Recovery = 60% Analysis Date = 11/13/16 Pct Recovery = 60% Analysis Date = 11/11/16 Pct Recovery = 61% Analysis Date = 11/11/16 Pct Recovery = 61% Analysis Date = 11/09/16 Pct Recovery = 61% Analysis Date = 11/09/16 Pct Recovery = 61% Analysis Date = 11/07/16 Pct Recovery = 61% Analysis Date = 11/07/16 Pct Recovery = 61% Analysis Date = 11/04/16 Pct Recovery = 62% Analysis Date = 11/04/16 Pct Recovery = 62% Analysis Date = 11/02/16 Pct Recovery = 62% Analysis Date = 11/02/16 Pct Recovery = 62% Analysis Date = 10/31/16 Pct Recovery = 62% Analysis Date = 10/31/16 Pct Recovery = 62% Analysis Date = 10/29/16 Pct Recovery = 62% Analysis Date = 10/29/16 Pct Recovery = 62% Analysis Date = 10/27/16 Pct Recovery = 63% Analysis Date = 10/27/16 Pct Recovery = 63% Analysis Date = 10/25/16 Pct Recovery = 63% Analysis Date = 10/25/16 Pct Recovery = 63% Analysis Date = 10/22/16 Pct Recovery = 63% Analysis Date = 10/22/16 Pct Recovery = 63% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/20/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/18/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/16/16 Pct Recovery = 64% Analysis Date = 10/14/16 Pct Recovery = 65% Analysis Date = 10/14/16 Pct Recovery = 65% Analysis Date = 10/12/16 Pct Recovery = 65% Analysis Date = 10/12/16 Pct Recovery = 65% Analysis Date = 10/09/16 Pct Recovery = 65% Analysis Date = 10/09/16 Pct Recovery = 65% Analysis Date = 10/07/16 Pct Recovery = 65% Analysis Date = 10/07/16 Pct Recovery = 65% Analysis Date = 10/05/16 Pct Recovery = 66% Analysis Date = 10/05/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 10/03/16 Pct Recovery = 66% Analysis Date = 10/01/16 Pct Recovery = 66% Analysis Date = 10/01/16 Pct Recovery = 66% Analysis Date = 09/28/16 Pct Recovery = 67% Analysis Date = 09/28/16 Pct Recovery = 67% Analysis Date = 09/26/16 Pct Recovery = 67% Analysis Date = 09/26/16 Pct Recovery = 67% Analysis Date = 09/24/16 Pct Recovery = 67% Analysis Date = 09/24/16 Pct Recovery = 67% Analysis Date = 09/22/16 Pct Recovery = 68% Analysis Date = 09/22/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 68% Analysis Date = 09/20/16 Pct Recovery = 68% Analysis Date = 09/18/16 Pct Recovery = 68% Analysis Date = 09/18/16 Pct Recovery = 68% Analysis Date = 09/15/16 Pct Recovery = 69% Analysis Date = 09/15/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/11/16 Pct Recovery = 69% Analysis Date = 09/11/16 Pct Recovery = 69% Analysis Date = 09/09/16 Pct Recovery = 69% Analysis Date = 09/09/16 Pct Recovery = 69% Analysis Date = 09/07/16 Pct Recovery = 70% Analysis Date = 09/07/16 Pct Recovery = 70% Analysis Date = 09/05/16 Pct Recovery = 70% Analysis Date = 09/05/16 Pct Recovery = 70% Analysis Date = 09/02/16 Pct Recovery = 70% Analysis Date = 09/02/16 Pct Recovery = 70% Analysis Date = 08/31/16 Pct Recovery = 71% Analysis Date = 08/31/16 Pct Recovery = 71% Analysis Date = 08/29/16 Pct Recovery = 71% Analysis Date = 08/29/16 Pct Recovery = 71% Analysis Date = 08/27/16 Pct Recovery = 71% Analysis Date = 08/27/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/25/16 Pct Recovery = 72% Analysis Date = 08/22/16 Pct Recovery = 72% Analysis Date = 08/22/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/18/16 Pct Recovery = 73% Analysis Date = 08/18/16 Pct Recovery = 73% Analysis Date = 08/16/16 Pct Recovery = 73% Analysis Date = 08/16/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/14/16 Pct Recovery = 73% Analysis Date = 08/12/16 Pct Recovery = 73% Analysis Date = 08/12/16 Pct Recovery = 73% Analysis Date = 08/09/16 Pct Recovery = 73% Analysis Date = 08/09/16 Pct Recovery = 73% Analysis Date = 08/07/16 Pct Recovery = 73% Analysis Date = 08/07/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/05/16 Pct Recovery = 73% Analysis Date = 08/03/16 Pct Recovery = 73% Analysis Date = 08/03/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/27/16 Pct Recovery = 73% Analysis Date = 07/27/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 73% Analysis Date = 07/25/16 Pct Recovery = 73% Analysis Date = 07/23/16 Pct Recovery = 73% Analysis Date = 07/23/16 Pct Recovery = 73% Analysis Date = 07/21/16 Pct Recovery = 73% Analysis Date = 07/21/16 Pct Recovery = 73% Analysis Date = 07/19/16 Pct Recovery = 73% Analysis Date = 07/19/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/17/16 Pct Recovery = 73% Analysis Date = 07/14/16 Pct Recovery = 73% Analysis Date = 07/14/16 Pct Recovery = 73% Analysis Date = 07/12/16 Pct Recovery = 73% Analysis Date = 07/12/16 Pct Recovery = 73% Analysis Date = 07/10/16 Pct Recovery = 73% Analysis Date = 07/10/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/23/16 Pct Recovery = 73% Analysis Date = 06/23/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/16/16 Pct Recovery = 73% Analysis Date = 06/16/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/12/16 Pct Recovery = 73% Analysis Date = 06/12/16 Pct Recovery = 73% Analysis Date = 06/10/16 Pct Recovery = 73% Analysis Date = 06/10/16 Pct Recovery = 73% Analysis Date = 06/07/16 Pct Recovery = 73% Analysis Date = 06/07/16 Pct Recovery = 73% Analysis Date = 06/05/16 Pct Recovery = 73% Analysis Date = 06/05/16 Pct Recovery = 73% Analysis Date = 06/03/16 Pct Recovery = 73% Analysis Date = 06/03/16 Pct Recovery = 73% Analysis Date = 06/01/16 Pct Recovery = 73% Analysis Date = 06/01/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/27/16 Pct Recovery = 73% Analysis Date = 05/27/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/23/16 Pct Recovery = 73% Analysis Date = 05/23/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/06/16 Pct Recovery = 73% Analysis Date = 05/06/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 05/04/16 Pct Recovery = 73% Analysis Date = 05/01/16 Pct Recovery = 73% Analysis Date = 05/01/16 Pct Recovery = 73% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/27/16 Pct Recovery = 72% Analysis Date = 04/27/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 72% Analysis Date = 04/18/16 Pct Recovery = 72% Analysis Date = 04/18/16 Pct Recovery = 72% Analysis Date = 04/16/16 Pct Recovery = 72% Analysis Date = 04/16/16 Pct Recovery = 72% Analysis Date = 04/14/16 Pct Recovery = 72% Analysis Date = 04/14/16 Pct Recovery = 72% Analysis Date = 04/12/16 Pct Recovery = 72% Analysis Date = 04/12/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/03/16 Pct Recovery = 71% Analysis Date = 04/03/16 Pct Recovery = 71% Analysis Date = 04/01/16 Pct Recovery = 71% Analysis Date = 04/01/16 Pct Recovery = 71% Analysis Date = 03/30/16 Pct Recovery = 71% Analysis Date = 03/30/16 Pct Recovery = 71% Analysis Date = 03/28/16 Pct Recovery = 70% Analysis Date = 03/28/16 Pct Recovery = 70% Analysis Date = 03/25/16 Pct Recovery = 70% Analysis Date = 03/25/16 Pct Recovery = 70% Analysis Date = 03/23/16 Pct Recovery = 70% Analysis Date = 03/23/16 Pct Recovery = 70% Analysis Date = 03/21/16 Pct Recovery = 70% Analysis Date = 03/21/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/17/16 Pct Recovery = 70% Analysis Date = 03/17/16 Pct Recovery = 70% Analysis Date = 03/15/16 Pct Recovery = 69% Analysis Date = 03/15/16 Pct Recovery = 69% Analysis Date = 03/12/16 Pct Recovery = 69% Analysis Date = 03/12/16 Pct Recovery = 69% Analysis Date = 03/10/16 Pct Recovery = 69% Analysis Date = 03/10/16 Pct Recovery = 69% Analysis Date = 03/08/16 Pct Recovery = 69% Analysis Date = 03/08/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/04/16 Pct Recovery = 69% Analysis Date = 03/04/16 Pct Recovery = 69% Analysis Date = 03/02/16 Pct Recovery = 68% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CIS-PERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 63% 23% 66% 31%
Total 19 63% 23% 66% 31%

Sample Statistics
CIS-PERMETHRIN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 4 21% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
CYANAZINE
METHOD: 2033 , TESTIDCODE: 04041GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 101% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 86% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 21% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 94% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 105% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 83% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 92% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 56% Analysis Date = 05/02/17 Pct Recovery = 75% Analysis Date = 04/30/17 Pct Recovery = 75% Analysis Date = 04/30/17 Pct Recovery = 75% Analysis Date = 04/28/17 Pct Recovery = 75% Analysis Date = 04/28/17 Pct Recovery = 75% Analysis Date = 04/26/17 Pct Recovery = 76% Analysis Date = 04/26/17 Pct Recovery = 76% Analysis Date = 04/24/17 Pct Recovery = 76% Analysis Date = 04/24/17 Pct Recovery = 76% Analysis Date = 04/22/17 Pct Recovery = 76% Analysis Date = 04/22/17 Pct Recovery = 76% Analysis Date = 04/20/17 Pct Recovery = 77% Analysis Date = 04/20/17 Pct Recovery = 77% Analysis Date = 04/18/17 Pct Recovery = 77% Analysis Date = 04/18/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/13/17 Pct Recovery = 78% Analysis Date = 04/13/17 Pct Recovery = 78% Analysis Date = 04/11/17 Pct Recovery = 78% Analysis Date = 04/11/17 Pct Recovery = 78% Analysis Date = 04/09/17 Pct Recovery = 78% Analysis Date = 04/09/17 Pct Recovery = 78% Analysis Date = 04/07/17 Pct Recovery = 78% Analysis Date = 04/07/17 Pct Recovery = 78% Analysis Date = 04/05/17 Pct Recovery = 79% Analysis Date = 04/05/17 Pct Recovery = 79% Analysis Date = 04/03/17 Pct Recovery = 79% Analysis Date = 04/03/17 Pct Recovery = 79% Analysis Date = 03/31/17 Pct Recovery = 79% Analysis Date = 03/31/17 Pct Recovery = 79% Analysis Date = 03/29/17 Pct Recovery = 80% Analysis Date = 03/29/17 Pct Recovery = 80% Analysis Date = 03/27/17 Pct Recovery = 80% Analysis Date = 03/27/17 Pct Recovery = 80% Analysis Date = 03/25/17 Pct Recovery = 80% Analysis Date = 03/25/17 Pct Recovery = 80% Analysis Date = 03/23/17 Pct Recovery = 81% Analysis Date = 03/23/17 Pct Recovery = 81% Analysis Date = 03/21/17 Pct Recovery = 81% Analysis Date = 03/21/17 Pct Recovery = 81% Analysis Date = 03/19/17 Pct Recovery = 81% Analysis Date = 03/19/17 Pct Recovery = 81% Analysis Date = 03/17/17 Pct Recovery = 82% Analysis Date = 03/17/17 Pct Recovery = 82% Analysis Date = 03/14/17 Pct Recovery = 82% Analysis Date = 03/14/17 Pct Recovery = 82% Analysis Date = 03/12/17 Pct Recovery = 82% Analysis Date = 03/12/17 Pct Recovery = 82% Analysis Date = 03/10/17 Pct Recovery = 82% Analysis Date = 03/10/17 Pct Recovery = 82% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/06/17 Pct Recovery = 83% Analysis Date = 03/06/17 Pct Recovery = 83% Analysis Date = 03/04/17 Pct Recovery = 83% Analysis Date = 03/04/17 Pct Recovery = 83% Analysis Date = 03/02/17 Pct Recovery = 84% Analysis Date = 03/02/17 Pct Recovery = 84% Analysis Date = 02/27/17 Pct Recovery = 84% Analysis Date = 02/27/17 Pct Recovery = 84% Analysis Date = 02/25/17 Pct Recovery = 84% Analysis Date = 02/25/17 Pct Recovery = 84% Analysis Date = 02/23/17 Pct Recovery = 85% Analysis Date = 02/23/17 Pct Recovery = 85% Analysis Date = 02/21/17 Pct Recovery = 85% Analysis Date = 02/21/17 Pct Recovery = 85% Analysis Date = 02/19/17 Pct Recovery = 85% Analysis Date = 02/19/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/15/17 Pct Recovery = 86% Analysis Date = 02/15/17 Pct Recovery = 86% Analysis Date = 02/13/17 Pct Recovery = 86% Analysis Date = 02/13/17 Pct Recovery = 86% Analysis Date = 02/10/17 Pct Recovery = 86% Analysis Date = 02/10/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 87% Analysis Date = 02/06/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 02/02/17 Pct Recovery = 87% Analysis Date = 02/02/17 Pct Recovery = 87% Analysis Date = 01/31/17 Pct Recovery = 87% Analysis Date = 01/31/17 Pct Recovery = 87% Analysis Date = 01/29/17 Pct Recovery = 87% Analysis Date = 01/29/17 Pct Recovery = 87% Analysis Date = 01/26/17 Pct Recovery = 88% Analysis Date = 01/26/17 Pct Recovery = 88% Analysis Date = 01/24/17 Pct Recovery = 88% Analysis Date = 01/24/17 Pct Recovery = 88% Analysis Date = 01/22/17 Pct Recovery = 88% Analysis Date = 01/22/17 Pct Recovery = 88% Analysis Date = 01/20/17 Pct Recovery = 88% Analysis Date = 01/20/17 Pct Recovery = 88% Analysis Date = 01/18/17 Pct Recovery = 88% Analysis Date = 01/18/17 Pct Recovery = 88% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/11/17 Pct Recovery = 89% Analysis Date = 01/11/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 90% Analysis Date = 01/05/17 Pct Recovery = 90% Analysis Date = 01/03/17 Pct Recovery = 90% Analysis Date = 01/03/17 Pct Recovery = 90% Analysis Date = 01/01/17 Pct Recovery = 90% Analysis Date = 01/01/17 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 90% Analysis Date = 12/30/16 Pct Recovery = 90% Analysis Date = 12/28/16 Pct Recovery = 90% Analysis Date = 12/28/16 Pct Recovery = 90% Analysis Date = 12/25/16 Pct Recovery = 91% Analysis Date = 12/25/16 Pct Recovery = 91% Analysis Date = 12/23/16 Pct Recovery = 91% Analysis Date = 12/23/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/19/16 Pct Recovery = 91% Analysis Date = 12/19/16 Pct Recovery = 91% Analysis Date = 12/17/16 Pct Recovery = 91% Analysis Date = 12/17/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/10/16 Pct Recovery = 90% Analysis Date = 12/10/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 11/30/16 Pct Recovery = 90% Analysis Date = 11/30/16 Pct Recovery = 90% Analysis Date = 11/28/16 Pct Recovery = 89% Analysis Date = 11/28/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/23/16 Pct Recovery = 89% Analysis Date = 11/23/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/19/16 Pct Recovery = 89% Analysis Date = 11/19/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/17/16 Pct Recovery = 89% Analysis Date = 11/15/16 Pct Recovery = 88% Analysis Date = 11/15/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/13/16 Pct Recovery = 88% Analysis Date = 11/11/16 Pct Recovery = 88% Analysis Date = 11/11/16 Pct Recovery = 88% Analysis Date = 11/08/16 Pct Recovery = 88% Analysis Date = 11/08/16 Pct Recovery = 88% Analysis Date = 11/06/16 Pct Recovery = 88% Analysis Date = 11/06/16 Pct Recovery = 88% Analysis Date = 11/04/16 Pct Recovery = 87% Analysis Date = 11/04/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 10/31/16 Pct Recovery = 87% Analysis Date = 10/31/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/16/16 Pct Recovery = 86% Analysis Date = 10/16/16 Pct Recovery = 86% Analysis Date = 10/14/16 Pct Recovery = 86% Analysis Date = 10/14/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/10/16 Pct Recovery = 85% Analysis Date = 10/10/16 Pct Recovery = 85% Analysis Date = 10/07/16 Pct Recovery = 85% Analysis Date = 10/07/16 Pct Recovery = 85% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 10/03/16 Pct Recovery = 85% Analysis Date = 10/03/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 09/29/16 Pct Recovery = 84% Analysis Date = 09/29/16 Pct Recovery = 84% Analysis Date = 09/27/16 Pct Recovery = 84% Analysis Date = 09/27/16 Pct Recovery = 84% Analysis Date = 09/25/16 Pct Recovery = 84% Analysis Date = 09/25/16 Pct Recovery = 84% Analysis Date = 09/22/16 Pct Recovery = 84% Analysis Date = 09/22/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/16/16 Pct Recovery = 83% Analysis Date = 09/16/16 Pct Recovery = 83% Analysis Date = 09/14/16 Pct Recovery = 83% Analysis Date = 09/14/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/05/16 Pct Recovery = 82% Analysis Date = 09/05/16 Pct Recovery = 82% Analysis Date = 09/03/16 Pct Recovery = 82% Analysis Date = 09/03/16 Pct Recovery = 82% Analysis Date = 09/01/16 Pct Recovery = 82% Analysis Date = 09/01/16 Pct Recovery = 82% Analysis Date = 08/30/16 Pct Recovery = 82% Analysis Date = 08/30/16 Pct Recovery = 82% Analysis Date = 08/28/16 Pct Recovery = 82% Analysis Date = 08/28/16 Pct Recovery = 82% Analysis Date = 08/26/16 Pct Recovery = 81% Analysis Date = 08/26/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/24/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/19/16 Pct Recovery = 81% Analysis Date = 08/19/16 Pct Recovery = 81% Analysis Date = 08/17/16 Pct Recovery = 80% Analysis Date = 08/17/16 Pct Recovery = 80% Analysis Date = 08/15/16 Pct Recovery = 80% Analysis Date = 08/15/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 79% Analysis Date = 08/09/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/04/16 Pct Recovery = 79% Analysis Date = 08/04/16 Pct Recovery = 79% Analysis Date = 08/02/16 Pct Recovery = 79% Analysis Date = 08/02/16 Pct Recovery = 79% Analysis Date = 07/31/16 Pct Recovery = 78% Analysis Date = 07/31/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/18/16 Pct Recovery = 77% Analysis Date = 07/18/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/16/16 Pct Recovery = 77% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/10/16 Pct Recovery = 76% Analysis Date = 07/10/16 Pct Recovery = 76% Analysis Date = 07/08/16 Pct Recovery = 76% Analysis Date = 07/08/16 Pct Recovery = 76% Analysis Date = 07/05/16 Pct Recovery = 75% Analysis Date = 07/05/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 07/03/16 Pct Recovery = 75% Analysis Date = 07/01/16 Pct Recovery = 75% Analysis Date = 07/01/16 Pct Recovery = 75% Analysis Date = 06/29/16 Pct Recovery = 75% Analysis Date = 06/29/16 Pct Recovery = 75% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/25/16 Pct Recovery = 74% Analysis Date = 06/25/16 Pct Recovery = 74% Analysis Date = 06/23/16 Pct Recovery = 74% Analysis Date = 06/23/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/16/16 Pct Recovery = 73% Analysis Date = 06/16/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/14/16 Pct Recovery = 73% Analysis Date = 06/12/16 Pct Recovery = 73% Analysis Date = 06/12/16 Pct Recovery = 73% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/06/16 Pct Recovery = 72% Analysis Date = 06/06/16 Pct Recovery = 72% Analysis Date = 06/03/16 Pct Recovery = 72% Analysis Date = 06/03/16 Pct Recovery = 72% Analysis Date = 06/01/16 Pct Recovery = 71% Analysis Date = 06/01/16 Pct Recovery = 71% Analysis Date = 05/30/16 Pct Recovery = 71% Analysis Date = 05/30/16 Pct Recovery = 71% Analysis Date = 05/28/16 Pct Recovery = 71% Analysis Date = 05/28/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/22/16 Pct Recovery = 71% Analysis Date = 05/22/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/17/16 Pct Recovery = 70% Analysis Date = 05/17/16 Pct Recovery = 70% Analysis Date = 05/15/16 Pct Recovery = 70% Analysis Date = 05/15/16 Pct Recovery = 70% Analysis Date = 05/13/16 Pct Recovery = 70% Analysis Date = 05/13/16 Pct Recovery = 70% Analysis Date = 05/11/16 Pct Recovery = 70% Analysis Date = 05/11/16 Pct Recovery = 70% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/09/16 Pct Recovery = 69% Analysis Date = 05/07/16 Pct Recovery = 69% Analysis Date = 05/07/16 Pct Recovery = 69% Analysis Date = 05/05/16 Pct Recovery = 69% Analysis Date = 05/05/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 69% Analysis Date = 04/30/16 Pct Recovery = 69% Analysis Date = 04/30/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/28/16 Pct Recovery = 68% Analysis Date = 04/26/16 Pct Recovery = 68% Analysis Date = 04/26/16 Pct Recovery = 68% Analysis Date = 04/24/16 Pct Recovery = 68% Analysis Date = 04/24/16 Pct Recovery = 68% Analysis Date = 04/22/16 Pct Recovery = 68% Analysis Date = 04/22/16 Pct Recovery = 68% Analysis Date = 04/20/16 Pct Recovery = 67% Analysis Date = 04/20/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 67% Analysis Date = 04/13/16 Pct Recovery = 67% Analysis Date = 04/13/16 Pct Recovery = 67% Analysis Date = 04/11/16 Pct Recovery = 67% Analysis Date = 04/11/16 Pct Recovery = 67% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/09/16 Pct Recovery = 66% Analysis Date = 04/07/16 Pct Recovery = 66% Analysis Date = 04/07/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 66% Analysis Date = 04/05/16 Pct Recovery = 66% Analysis Date = 04/03/16 Pct Recovery = 65% Analysis Date = 04/03/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/29/16 Pct Recovery = 65% Analysis Date = 03/29/16 Pct Recovery = 65% Analysis Date = 03/27/16 Pct Recovery = 65% Analysis Date = 03/27/16 Pct Recovery = 65% Analysis Date = 03/25/16 Pct Recovery = 64% Analysis Date = 03/25/16 Pct Recovery = 64% Analysis Date = 03/23/16 Pct Recovery = 64% Analysis Date = 03/23/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/16/16 Pct Recovery = 63% Analysis Date = 03/16/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/10/16 Pct Recovery = 62% Analysis Date = 03/10/16 Pct Recovery = 62% Analysis Date = 03/08/16 Pct Recovery = 62% Analysis Date = 03/08/16 Pct Recovery = 62% Analysis Date = 03/06/16 Pct Recovery = 62% Analysis Date = 03/06/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/02/16 Pct Recovery = 61% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYANAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 78% 20% 77% 19%
Total 18 78% 20% 77% 19%

Sample Statistics
CYANAZINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
CYFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61585GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 62% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 89% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 89% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 53% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 85% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 98% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 67% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 58% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 94% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 109% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 32% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 05/10/17 Pct Recovery = 61% Analysis Date = 05/08/17 Pct Recovery = 61% Analysis Date = 05/08/17 Pct Recovery = 61% Analysis Date = 05/06/17 Pct Recovery = 62% Analysis Date = 05/06/17 Pct Recovery = 62% Analysis Date = 05/04/17 Pct Recovery = 62% Analysis Date = 05/04/17 Pct Recovery = 62% Analysis Date = 05/01/17 Pct Recovery = 63% Analysis Date = 05/01/17 Pct Recovery = 63% Analysis Date = 04/29/17 Pct Recovery = 63% Analysis Date = 04/29/17 Pct Recovery = 63% Analysis Date = 04/27/17 Pct Recovery = 64% Analysis Date = 04/27/17 Pct Recovery = 64% Analysis Date = 04/25/17 Pct Recovery = 64% Analysis Date = 04/25/17 Pct Recovery = 64% Analysis Date = 04/22/17 Pct Recovery = 64% Analysis Date = 04/22/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 65% Analysis Date = 04/20/17 Pct Recovery = 65% Analysis Date = 04/18/17 Pct Recovery = 65% Analysis Date = 04/18/17 Pct Recovery = 65% Analysis Date = 04/15/17 Pct Recovery = 66% Analysis Date = 04/15/17 Pct Recovery = 66% Analysis Date = 04/13/17 Pct Recovery = 66% Analysis Date = 04/13/17 Pct Recovery = 66% Analysis Date = 04/11/17 Pct Recovery = 66% Analysis Date = 04/11/17 Pct Recovery = 66% Analysis Date = 04/09/17 Pct Recovery = 67% Analysis Date = 04/09/17 Pct Recovery = 67% Analysis Date = 04/06/17 Pct Recovery = 67% Analysis Date = 04/06/17 Pct Recovery = 67% Analysis Date = 04/04/17 Pct Recovery = 67% Analysis Date = 04/04/17 Pct Recovery = 67% Analysis Date = 04/02/17 Pct Recovery = 68% Analysis Date = 04/02/17 Pct Recovery = 68% Analysis Date = 03/30/17 Pct Recovery = 68% Analysis Date = 03/30/17 Pct Recovery = 68% Analysis Date = 03/28/17 Pct Recovery = 69% Analysis Date = 03/28/17 Pct Recovery = 69% Analysis Date = 03/26/17 Pct Recovery = 69% Analysis Date = 03/26/17 Pct Recovery = 69% Analysis Date = 03/24/17 Pct Recovery = 69% Analysis Date = 03/24/17 Pct Recovery = 69% Analysis Date = 03/21/17 Pct Recovery = 70% Analysis Date = 03/21/17 Pct Recovery = 70% Analysis Date = 03/19/17 Pct Recovery = 70% Analysis Date = 03/19/17 Pct Recovery = 70% Analysis Date = 03/17/17 Pct Recovery = 70% Analysis Date = 03/17/17 Pct Recovery = 70% Analysis Date = 03/14/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/10/17 Pct Recovery = 71% Analysis Date = 03/10/17 Pct Recovery = 71% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/05/17 Pct Recovery = 72% Analysis Date = 03/05/17 Pct Recovery = 72% Analysis Date = 03/03/17 Pct Recovery = 72% Analysis Date = 03/03/17 Pct Recovery = 72% Analysis Date = 03/01/17 Pct Recovery = 73% Analysis Date = 03/01/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/22/17 Pct Recovery = 74% Analysis Date = 02/22/17 Pct Recovery = 74% Analysis Date = 02/20/17 Pct Recovery = 73% Analysis Date = 02/20/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/15/17 Pct Recovery = 72% Analysis Date = 02/15/17 Pct Recovery = 72% Analysis Date = 02/13/17 Pct Recovery = 72% Analysis Date = 02/13/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/10/17 Pct Recovery = 72% Analysis Date = 02/08/17 Pct Recovery = 71% Analysis Date = 02/08/17 Pct Recovery = 71% Analysis Date = 02/06/17 Pct Recovery = 71% Analysis Date = 02/06/17 Pct Recovery = 71% Analysis Date = 02/04/17 Pct Recovery = 70% Analysis Date = 02/04/17 Pct Recovery = 70% Analysis Date = 02/01/17 Pct Recovery = 70% Analysis Date = 02/01/17 Pct Recovery = 70% Analysis Date = 01/30/17 Pct Recovery = 69% Analysis Date = 01/30/17 Pct Recovery = 69% Analysis Date = 01/28/17 Pct Recovery = 69% Analysis Date = 01/28/17 Pct Recovery = 69% Analysis Date = 01/25/17 Pct Recovery = 68% Analysis Date = 01/25/17 Pct Recovery = 68% Analysis Date = 01/23/17 Pct Recovery = 68% Analysis Date = 01/23/17 Pct Recovery = 68% Analysis Date = 01/21/17 Pct Recovery = 68% Analysis Date = 01/21/17 Pct Recovery = 68% Analysis Date = 01/19/17 Pct Recovery = 67% Analysis Date = 01/19/17 Pct Recovery = 67% Analysis Date = 01/16/17 Pct Recovery = 67% Analysis Date = 01/16/17 Pct Recovery = 67% Analysis Date = 01/14/17 Pct Recovery = 67% Analysis Date = 01/14/17 Pct Recovery = 67% Analysis Date = 01/12/17 Pct Recovery = 68% Analysis Date = 01/12/17 Pct Recovery = 68% Analysis Date = 01/09/17 Pct Recovery = 68% Analysis Date = 01/09/17 Pct Recovery = 68% Analysis Date = 01/07/17 Pct Recovery = 68% Analysis Date = 01/07/17 Pct Recovery = 68% Analysis Date = 01/05/17 Pct Recovery = 69% Analysis Date = 01/05/17 Pct Recovery = 69% Analysis Date = 01/03/17 Pct Recovery = 69% Analysis Date = 01/03/17 Pct Recovery = 69% Analysis Date = 12/31/16 Pct Recovery = 69% Analysis Date = 12/31/16 Pct Recovery = 69% Analysis Date = 12/29/16 Pct Recovery = 69% Analysis Date = 12/29/16 Pct Recovery = 69% Analysis Date = 12/27/16 Pct Recovery = 70% Analysis Date = 12/27/16 Pct Recovery = 70% Analysis Date = 12/24/16 Pct Recovery = 70% Analysis Date = 12/24/16 Pct Recovery = 70% Analysis Date = 12/22/16 Pct Recovery = 70% Analysis Date = 12/22/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/20/16 Pct Recovery = 71% Analysis Date = 12/18/16 Pct Recovery = 71% Analysis Date = 12/18/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/15/16 Pct Recovery = 71% Analysis Date = 12/13/16 Pct Recovery = 71% Analysis Date = 12/13/16 Pct Recovery = 71% Analysis Date = 12/11/16 Pct Recovery = 72% Analysis Date = 12/11/16 Pct Recovery = 72% Analysis Date = 12/08/16 Pct Recovery = 72% Analysis Date = 12/08/16 Pct Recovery = 72% Analysis Date = 12/06/16 Pct Recovery = 72% Analysis Date = 12/06/16 Pct Recovery = 72% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 12/04/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 12/02/16 Pct Recovery = 73% Analysis Date = 11/29/16 Pct Recovery = 73% Analysis Date = 11/29/16 Pct Recovery = 73% Analysis Date = 11/27/16 Pct Recovery = 73% Analysis Date = 11/27/16 Pct Recovery = 73% Analysis Date = 11/25/16 Pct Recovery = 74% Analysis Date = 11/25/16 Pct Recovery = 74% Analysis Date = 11/22/16 Pct Recovery = 74% Analysis Date = 11/22/16 Pct Recovery = 74% Analysis Date = 11/20/16 Pct Recovery = 74% Analysis Date = 11/20/16 Pct Recovery = 74% Analysis Date = 11/18/16 Pct Recovery = 74% Analysis Date = 11/18/16 Pct Recovery = 74% Analysis Date = 11/16/16 Pct Recovery = 75% Analysis Date = 11/16/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/11/16 Pct Recovery = 75% Analysis Date = 11/11/16 Pct Recovery = 75% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/06/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 77% Analysis Date = 10/31/16 Pct Recovery = 77% Analysis Date = 10/28/16 Pct Recovery = 77% Analysis Date = 10/28/16 Pct Recovery = 77% Analysis Date = 10/26/16 Pct Recovery = 77% Analysis Date = 10/26/16 Pct Recovery = 77% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/24/16 Pct Recovery = 78% Analysis Date = 10/21/16 Pct Recovery = 78% Analysis Date = 10/21/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 79% Analysis Date = 10/15/16 Pct Recovery = 79% Analysis Date = 10/12/16 Pct Recovery = 79% Analysis Date = 10/12/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/01/16 Pct Recovery = 80% Analysis Date = 10/01/16 Pct Recovery = 80% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/26/16 Pct Recovery = 81% Analysis Date = 09/26/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 81% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 82% Analysis Date = 09/06/16 Pct Recovery = 82% Analysis Date = 09/06/16 Pct Recovery = 82% Analysis Date = 09/03/16 Pct Recovery = 82% Analysis Date = 09/03/16 Pct Recovery = 82% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 08/30/16 Pct Recovery = 81% Analysis Date = 08/30/16 Pct Recovery = 81% Analysis Date = 08/28/16 Pct Recovery = 81% Analysis Date = 08/28/16 Pct Recovery = 81% Analysis Date = 08/25/16 Pct Recovery = 80% Analysis Date = 08/25/16 Pct Recovery = 80% Analysis Date = 08/23/16 Pct Recovery = 80% Analysis Date = 08/23/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 80% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/12/16 Pct Recovery = 79% Analysis Date = 08/12/16 Pct Recovery = 79% Analysis Date = 08/09/16 Pct Recovery = 79% Analysis Date = 08/09/16 Pct Recovery = 79% Analysis Date = 08/07/16 Pct Recovery = 79% Analysis Date = 08/07/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/02/16 Pct Recovery = 78% Analysis Date = 08/02/16 Pct Recovery = 78% Analysis Date = 07/31/16 Pct Recovery = 78% Analysis Date = 07/31/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/24/16 Pct Recovery = 78% Analysis Date = 07/24/16 Pct Recovery = 78% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/15/16 Pct Recovery = 77% Analysis Date = 07/15/16 Pct Recovery = 77% Analysis Date = 07/13/16 Pct Recovery = 77% Analysis Date = 07/13/16 Pct Recovery = 77% Analysis Date = 07/11/16 Pct Recovery = 77% Analysis Date = 07/11/16 Pct Recovery = 77% Analysis Date = 07/08/16 Pct Recovery = 76% Analysis Date = 07/08/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/04/16 Pct Recovery = 76% Analysis Date = 07/04/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/20/16 Pct Recovery = 75% Analysis Date = 06/20/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/15/16 Pct Recovery = 75% Analysis Date = 06/15/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/11/16 Pct Recovery = 74% Analysis Date = 06/11/16 Pct Recovery = 74% Analysis Date = 06/09/16 Pct Recovery = 74% Analysis Date = 06/09/16 Pct Recovery = 74% Analysis Date = 06/06/16 Pct Recovery = 74% Analysis Date = 06/06/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/30/16 Pct Recovery = 73% Analysis Date = 05/28/16 Pct Recovery = 73% Analysis Date = 05/28/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 72% Analysis Date = 05/12/16 Pct Recovery = 72% Analysis Date = 05/12/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/05/16 Pct Recovery = 72% Analysis Date = 05/03/16 Pct Recovery = 71% Analysis Date = 05/03/16 Pct Recovery = 71% Analysis Date = 05/01/16 Pct Recovery = 71% Analysis Date = 05/01/16 Pct Recovery = 71% Analysis Date = 04/28/16 Pct Recovery = 71% Analysis Date = 04/28/16 Pct Recovery = 71% Analysis Date = 04/26/16 Pct Recovery = 71% Analysis Date = 04/26/16 Pct Recovery = 71% Analysis Date = 04/24/16 Pct Recovery = 71% Analysis Date = 04/24/16 Pct Recovery = 71% Analysis Date = 04/22/16 Pct Recovery = 71% Analysis Date = 04/22/16 Pct Recovery = 71% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/17/16 Pct Recovery = 70% Analysis Date = 04/17/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/12/16 Pct Recovery = 70% Analysis Date = 04/12/16 Pct Recovery = 70% Analysis Date = 04/10/16 Pct Recovery = 70% Analysis Date = 04/10/16 Pct Recovery = 70% Analysis Date = 04/08/16 Pct Recovery = 70% Analysis Date = 04/08/16 Pct Recovery = 70% Analysis Date = 04/06/16 Pct Recovery = 69% Analysis Date = 04/06/16 Pct Recovery = 69% Analysis Date = 04/03/16 Pct Recovery = 69% Analysis Date = 04/03/16 Pct Recovery = 69% Analysis Date = 04/01/16 Pct Recovery = 69% Analysis Date = 04/01/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 69% Analysis Date = 03/27/16 Pct Recovery = 69% Analysis Date = 03/27/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 69% Analysis Date = 03/21/16 Pct Recovery = 68% Analysis Date = 03/21/16 Pct Recovery = 68% Analysis Date = 03/18/16 Pct Recovery = 68% Analysis Date = 03/18/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/14/16 Pct Recovery = 68% Analysis Date = 03/14/16 Pct Recovery = 68% Analysis Date = 03/11/16 Pct Recovery = 68% Analysis Date = 03/11/16 Pct Recovery = 68% Analysis Date = 03/09/16 Pct Recovery = 68% Analysis Date = 03/09/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 68% Analysis Date = 03/07/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 02/29/16 Pct Recovery = 67% Analysis Date = 02/29/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 67% Analysis Date = 02/24/16 Pct Recovery = 67% Analysis Date = 02/24/16 Pct Recovery = 67% Analysis Date = 02/22/16 Pct Recovery = 67% Analysis Date = 02/22/16 Pct Recovery = 67% Analysis Date = 02/20/16 Pct Recovery = 67% Analysis Date = 02/20/16 Pct Recovery = 67% Analysis Date = 02/18/16 Pct Recovery = 67% Analysis Date = 02/18/16 Pct Recovery = 67% Analysis Date = 02/15/16 Pct Recovery = 66% Analysis Date = 02/15/16 Pct Recovery = 66% Analysis Date = 02/13/16 Pct Recovery = 66% Analysis Date = 02/13/16 Pct Recovery = 66% Analysis Date = 02/11/16 Pct Recovery = 66% Analysis Date = 02/11/16 Pct Recovery = 66% Analysis Date = 02/09/16 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYFLUTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 16 74% 20% 68% 20%
Total 16 74% 20% 68% 20%

Sample Statistics
CYFLUTHRIN

Characteristic N % % Basis
Plotted 16 89% Spiked
Estimated Values 16 89% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 2 11% 2 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
CYHALOTHRIN
METHOD: 2033 , TESTIDCODE: 61595GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 58% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 64% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 51% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 71% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 65% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 79% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 83% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 57% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 83% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 89% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 65% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 60% Analysis Date = 05/02/17 Pct Recovery = 72% Analysis Date = 04/30/17 Pct Recovery = 72% Analysis Date = 04/30/17 Pct Recovery = 72% Analysis Date = 04/28/17 Pct Recovery = 72% Analysis Date = 04/28/17 Pct Recovery = 72% Analysis Date = 04/26/17 Pct Recovery = 71% Analysis Date = 04/26/17 Pct Recovery = 71% Analysis Date = 04/24/17 Pct Recovery = 71% Analysis Date = 04/24/17 Pct Recovery = 71% Analysis Date = 04/21/17 Pct Recovery = 71% Analysis Date = 04/21/17 Pct Recovery = 71% Analysis Date = 04/19/17 Pct Recovery = 71% Analysis Date = 04/19/17 Pct Recovery = 71% Analysis Date = 04/17/17 Pct Recovery = 71% Analysis Date = 04/17/17 Pct Recovery = 71% Analysis Date = 04/15/17 Pct Recovery = 70% Analysis Date = 04/15/17 Pct Recovery = 70% Analysis Date = 04/12/17 Pct Recovery = 70% Analysis Date = 04/12/17 Pct Recovery = 70% Analysis Date = 04/10/17 Pct Recovery = 70% Analysis Date = 04/10/17 Pct Recovery = 70% Analysis Date = 04/08/17 Pct Recovery = 70% Analysis Date = 04/08/17 Pct Recovery = 70% Analysis Date = 04/06/17 Pct Recovery = 70% Analysis Date = 04/06/17 Pct Recovery = 70% Analysis Date = 04/03/17 Pct Recovery = 69% Analysis Date = 04/03/17 Pct Recovery = 69% Analysis Date = 04/01/17 Pct Recovery = 69% Analysis Date = 04/01/17 Pct Recovery = 69% Analysis Date = 03/30/17 Pct Recovery = 69% Analysis Date = 03/30/17 Pct Recovery = 69% Analysis Date = 03/28/17 Pct Recovery = 69% Analysis Date = 03/28/17 Pct Recovery = 69% Analysis Date = 03/25/17 Pct Recovery = 69% Analysis Date = 03/25/17 Pct Recovery = 69% Analysis Date = 03/23/17 Pct Recovery = 68% Analysis Date = 03/23/17 Pct Recovery = 68% Analysis Date = 03/21/17 Pct Recovery = 68% Analysis Date = 03/21/17 Pct Recovery = 68% Analysis Date = 03/19/17 Pct Recovery = 68% Analysis Date = 03/19/17 Pct Recovery = 68% Analysis Date = 03/16/17 Pct Recovery = 68% Analysis Date = 03/16/17 Pct Recovery = 68% Analysis Date = 03/14/17 Pct Recovery = 68% Analysis Date = 03/14/17 Pct Recovery = 68% Analysis Date = 03/12/17 Pct Recovery = 67% Analysis Date = 03/12/17 Pct Recovery = 67% Analysis Date = 03/10/17 Pct Recovery = 67% Analysis Date = 03/10/17 Pct Recovery = 67% Analysis Date = 03/07/17 Pct Recovery = 67% Analysis Date = 03/07/17 Pct Recovery = 67% Analysis Date = 03/05/17 Pct Recovery = 67% Analysis Date = 03/05/17 Pct Recovery = 67% Analysis Date = 03/03/17 Pct Recovery = 67% Analysis Date = 03/03/17 Pct Recovery = 67% Analysis Date = 03/01/17 Pct Recovery = 66% Analysis Date = 03/01/17 Pct Recovery = 66% Analysis Date = 02/26/17 Pct Recovery = 66% Analysis Date = 02/26/17 Pct Recovery = 66% Analysis Date = 02/24/17 Pct Recovery = 66% Analysis Date = 02/24/17 Pct Recovery = 66% Analysis Date = 02/22/17 Pct Recovery = 66% Analysis Date = 02/22/17 Pct Recovery = 66% Analysis Date = 02/20/17 Pct Recovery = 66% Analysis Date = 02/20/17 Pct Recovery = 66% Analysis Date = 02/17/17 Pct Recovery = 65% Analysis Date = 02/17/17 Pct Recovery = 65% Analysis Date = 02/15/17 Pct Recovery = 65% Analysis Date = 02/15/17 Pct Recovery = 65% Analysis Date = 02/13/17 Pct Recovery = 65% Analysis Date = 02/13/17 Pct Recovery = 65% Analysis Date = 02/11/17 Pct Recovery = 65% Analysis Date = 02/11/17 Pct Recovery = 65% Analysis Date = 02/08/17 Pct Recovery = 65% Analysis Date = 02/08/17 Pct Recovery = 65% Analysis Date = 02/06/17 Pct Recovery = 65% Analysis Date = 02/06/17 Pct Recovery = 65% Analysis Date = 02/04/17 Pct Recovery = 65% Analysis Date = 02/04/17 Pct Recovery = 65% Analysis Date = 02/02/17 Pct Recovery = 66% Analysis Date = 02/02/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/28/17 Pct Recovery = 66% Analysis Date = 01/28/17 Pct Recovery = 66% Analysis Date = 01/26/17 Pct Recovery = 66% Analysis Date = 01/26/17 Pct Recovery = 66% Analysis Date = 01/24/17 Pct Recovery = 66% Analysis Date = 01/24/17 Pct Recovery = 66% Analysis Date = 01/21/17 Pct Recovery = 66% Analysis Date = 01/21/17 Pct Recovery = 66% Analysis Date = 01/19/17 Pct Recovery = 66% Analysis Date = 01/19/17 Pct Recovery = 66% Analysis Date = 01/17/17 Pct Recovery = 66% Analysis Date = 01/17/17 Pct Recovery = 66% Analysis Date = 01/15/17 Pct Recovery = 66% Analysis Date = 01/15/17 Pct Recovery = 66% Analysis Date = 01/12/17 Pct Recovery = 66% Analysis Date = 01/12/17 Pct Recovery = 66% Analysis Date = 01/10/17 Pct Recovery = 66% Analysis Date = 01/10/17 Pct Recovery = 66% Analysis Date = 01/08/17 Pct Recovery = 66% Analysis Date = 01/08/17 Pct Recovery = 66% Analysis Date = 01/06/17 Pct Recovery = 66% Analysis Date = 01/06/17 Pct Recovery = 66% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 01/04/17 Pct Recovery = 66% Analysis Date = 01/01/17 Pct Recovery = 67% Analysis Date = 01/01/17 Pct Recovery = 67% Analysis Date = 12/30/16 Pct Recovery = 67% Analysis Date = 12/30/16 Pct Recovery = 67% Analysis Date = 12/28/16 Pct Recovery = 67% Analysis Date = 12/28/16 Pct Recovery = 67% Analysis Date = 12/26/16 Pct Recovery = 67% Analysis Date = 12/26/16 Pct Recovery = 67% Analysis Date = 12/23/16 Pct Recovery = 67% Analysis Date = 12/23/16 Pct Recovery = 67% Analysis Date = 12/21/16 Pct Recovery = 67% Analysis Date = 12/21/16 Pct Recovery = 67% Analysis Date = 12/19/16 Pct Recovery = 67% Analysis Date = 12/19/16 Pct Recovery = 67% Analysis Date = 12/17/16 Pct Recovery = 67% Analysis Date = 12/17/16 Pct Recovery = 67% Analysis Date = 12/14/16 Pct Recovery = 67% Analysis Date = 12/14/16 Pct Recovery = 67% Analysis Date = 12/12/16 Pct Recovery = 67% Analysis Date = 12/12/16 Pct Recovery = 67% Analysis Date = 12/10/16 Pct Recovery = 67% Analysis Date = 12/10/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/05/16 Pct Recovery = 67% Analysis Date = 12/03/16 Pct Recovery = 67% Analysis Date = 12/03/16 Pct Recovery = 67% Analysis Date = 12/01/16 Pct Recovery = 67% Analysis Date = 12/01/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 68% Analysis Date = 11/29/16 Pct Recovery = 68% Analysis Date = 11/26/16 Pct Recovery = 68% Analysis Date = 11/26/16 Pct Recovery = 68% Analysis Date = 11/24/16 Pct Recovery = 68% Analysis Date = 11/24/16 Pct Recovery = 68% Analysis Date = 11/22/16 Pct Recovery = 68% Analysis Date = 11/22/16 Pct Recovery = 68% Analysis Date = 11/20/16 Pct Recovery = 68% Analysis Date = 11/20/16 Pct Recovery = 68% Analysis Date = 11/17/16 Pct Recovery = 68% Analysis Date = 11/17/16 Pct Recovery = 68% Analysis Date = 11/15/16 Pct Recovery = 68% Analysis Date = 11/15/16 Pct Recovery = 68% Analysis Date = 11/13/16 Pct Recovery = 68% Analysis Date = 11/13/16 Pct Recovery = 68% Analysis Date = 11/11/16 Pct Recovery = 68% Analysis Date = 11/11/16 Pct Recovery = 68% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 10/30/16 Pct Recovery = 68% Analysis Date = 10/30/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 68% Analysis Date = 10/26/16 Pct Recovery = 69% Analysis Date = 10/26/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/21/16 Pct Recovery = 69% Analysis Date = 10/21/16 Pct Recovery = 69% Analysis Date = 10/19/16 Pct Recovery = 69% Analysis Date = 10/19/16 Pct Recovery = 69% Analysis Date = 10/17/16 Pct Recovery = 69% Analysis Date = 10/17/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 69% Analysis Date = 10/08/16 Pct Recovery = 69% Analysis Date = 10/08/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 10/06/16 Pct Recovery = 69% Analysis Date = 10/03/16 Pct Recovery = 69% Analysis Date = 10/03/16 Pct Recovery = 69% Analysis Date = 10/01/16 Pct Recovery = 69% Analysis Date = 10/01/16 Pct Recovery = 69% Analysis Date = 09/29/16 Pct Recovery = 69% Analysis Date = 09/29/16 Pct Recovery = 69% Analysis Date = 09/27/16 Pct Recovery = 69% Analysis Date = 09/27/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/24/16 Pct Recovery = 69% Analysis Date = 09/22/16 Pct Recovery = 70% Analysis Date = 09/22/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/16/16 Pct Recovery = 70% Analysis Date = 09/16/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 70% Analysis Date = 09/11/16 Pct Recovery = 70% Analysis Date = 09/11/16 Pct Recovery = 70% Analysis Date = 09/09/16 Pct Recovery = 70% Analysis Date = 09/09/16 Pct Recovery = 70% Analysis Date = 09/07/16 Pct Recovery = 71% Analysis Date = 09/07/16 Pct Recovery = 71% Analysis Date = 09/04/16 Pct Recovery = 71% Analysis Date = 09/04/16 Pct Recovery = 71% Analysis Date = 09/02/16 Pct Recovery = 71% Analysis Date = 09/02/16 Pct Recovery = 71% Analysis Date = 08/31/16 Pct Recovery = 71% Analysis Date = 08/31/16 Pct Recovery = 71% Analysis Date = 08/29/16 Pct Recovery = 71% Analysis Date = 08/29/16 Pct Recovery = 71% Analysis Date = 08/26/16 Pct Recovery = 72% Analysis Date = 08/26/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/24/16 Pct Recovery = 72% Analysis Date = 08/22/16 Pct Recovery = 72% Analysis Date = 08/22/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/20/16 Pct Recovery = 72% Analysis Date = 08/17/16 Pct Recovery = 72% Analysis Date = 08/17/16 Pct Recovery = 72% Analysis Date = 08/15/16 Pct Recovery = 72% Analysis Date = 08/15/16 Pct Recovery = 72% Analysis Date = 08/13/16 Pct Recovery = 72% Analysis Date = 08/13/16 Pct Recovery = 72% Analysis Date = 08/11/16 Pct Recovery = 72% Analysis Date = 08/11/16 Pct Recovery = 72% Analysis Date = 08/08/16 Pct Recovery = 72% Analysis Date = 08/08/16 Pct Recovery = 72% Analysis Date = 08/06/16 Pct Recovery = 72% Analysis Date = 08/06/16 Pct Recovery = 72% Analysis Date = 08/04/16 Pct Recovery = 72% Analysis Date = 08/04/16 Pct Recovery = 72% Analysis Date = 08/02/16 Pct Recovery = 72% Analysis Date = 08/02/16 Pct Recovery = 72% Analysis Date = 07/30/16 Pct Recovery = 72% Analysis Date = 07/30/16 Pct Recovery = 72% Analysis Date = 07/28/16 Pct Recovery = 72% Analysis Date = 07/28/16 Pct Recovery = 72% Analysis Date = 07/26/16 Pct Recovery = 72% Analysis Date = 07/26/16 Pct Recovery = 72% Analysis Date = 07/24/16 Pct Recovery = 72% Analysis Date = 07/24/16 Pct Recovery = 72% Analysis Date = 07/21/16 Pct Recovery = 72% Analysis Date = 07/21/16 Pct Recovery = 72% Analysis Date = 07/19/16 Pct Recovery = 72% Analysis Date = 07/19/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/17/16 Pct Recovery = 72% Analysis Date = 07/15/16 Pct Recovery = 72% Analysis Date = 07/15/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/12/16 Pct Recovery = 72% Analysis Date = 07/10/16 Pct Recovery = 72% Analysis Date = 07/10/16 Pct Recovery = 72% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/06/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/24/16 Pct Recovery = 73% Analysis Date = 06/24/16 Pct Recovery = 73% Analysis Date = 06/22/16 Pct Recovery = 73% Analysis Date = 06/22/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/20/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/18/16 Pct Recovery = 73% Analysis Date = 06/15/16 Pct Recovery = 73% Analysis Date = 06/15/16 Pct Recovery = 73% Analysis Date = 06/13/16 Pct Recovery = 73% Analysis Date = 06/13/16 Pct Recovery = 73% Analysis Date = 06/11/16 Pct Recovery = 73% Analysis Date = 06/11/16 Pct Recovery = 73% Analysis Date = 06/09/16 Pct Recovery = 73% Analysis Date = 06/09/16 Pct Recovery = 73% Analysis Date = 06/06/16 Pct Recovery = 73% Analysis Date = 06/06/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 06/04/16 Pct Recovery = 73% Analysis Date = 06/02/16 Pct Recovery = 73% Analysis Date = 06/02/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/31/16 Pct Recovery = 73% Analysis Date = 05/29/16 Pct Recovery = 73% Analysis Date = 05/29/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/22/16 Pct Recovery = 73% Analysis Date = 05/22/16 Pct Recovery = 73% Analysis Date = 05/20/16 Pct Recovery = 73% Analysis Date = 05/20/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/15/16 Pct Recovery = 73% Analysis Date = 05/15/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/13/16 Pct Recovery = 73% Analysis Date = 05/11/16 Pct Recovery = 72% Analysis Date = 05/11/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/06/16 Pct Recovery = 72% Analysis Date = 05/06/16 Pct Recovery = 72% Analysis Date = 05/04/16 Pct Recovery = 72% Analysis Date = 05/04/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 05/02/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/27/16 Pct Recovery = 72% Analysis Date = 04/27/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/20/16 Pct Recovery = 71% Analysis Date = 04/20/16 Pct Recovery = 71% Analysis Date = 04/18/16 Pct Recovery = 71% Analysis Date = 04/18/16 Pct Recovery = 71% Analysis Date = 04/16/16 Pct Recovery = 71% Analysis Date = 04/16/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/11/16 Pct Recovery = 71% Analysis Date = 04/11/16 Pct Recovery = 71% Analysis Date = 04/09/16 Pct Recovery = 71% Analysis Date = 04/09/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/02/16 Pct Recovery = 70% Analysis Date = 04/02/16 Pct Recovery = 70% Analysis Date = 03/31/16 Pct Recovery = 70% Analysis Date = 03/31/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 70% Analysis Date = 03/29/16 Pct Recovery = 70% Analysis Date = 03/27/16 Pct Recovery = 70% Analysis Date = 03/27/16 Pct Recovery = 70% Analysis Date = 03/24/16 Pct Recovery = 70% Analysis Date = 03/24/16 Pct Recovery = 70% Analysis Date = 03/22/16 Pct Recovery = 70% Analysis Date = 03/22/16 Pct Recovery = 70% Analysis Date = 03/20/16 Pct Recovery = 69% Analysis Date = 03/20/16 Pct Recovery = 69% Analysis Date = 03/18/16 Pct Recovery = 69% Analysis Date = 03/18/16 Pct Recovery = 69% Analysis Date = 03/15/16 Pct Recovery = 69% Analysis Date = 03/15/16 Pct Recovery = 69% Analysis Date = 03/13/16 Pct Recovery = 69% Analysis Date = 03/13/16 Pct Recovery = 69% Analysis Date = 03/11/16 Pct Recovery = 69% Analysis Date = 03/11/16 Pct Recovery = 69% Analysis Date = 03/09/16 Pct Recovery = 69% Analysis Date = 03/09/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/04/16 Pct Recovery = 68% Analysis Date = 03/04/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 02/29/16 Pct Recovery = 68% Analysis Date = 02/29/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/26/16 Pct Recovery = 68% Analysis Date = 02/24/16 Pct Recovery = 68% Analysis Date = 02/24/16 Pct Recovery = 68% Analysis Date = 02/22/16 Pct Recovery = 68% Analysis Date = 02/22/16 Pct Recovery = 68% Analysis Date = 02/20/16 Pct Recovery = 67% Analysis Date = 02/20/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/17/16 Pct Recovery = 67% Analysis Date = 02/15/16 Pct Recovery = 67% Analysis Date = 02/15/16 Pct Recovery = 67% Analysis Date = 02/13/16 Pct Recovery = 67% Analysis Date = 02/13/16 Pct Recovery = 67% Analysis Date = 02/11/16 Pct Recovery = 67% Analysis Date = 02/11/16 Pct Recovery = 67% Analysis Date = 02/09/16 Pct Recovery = 66% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYHALOTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 17 69% 11% 69% 13%
Total 17 69% 11% 69% 13%

Sample Statistics
CYHALOTHRIN

Characteristic N % % Basis
Plotted 17 94% Spiked
Estimated Values 17 94% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 1 6% 1 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
CYPERMETHRIN
METHOD: 2033 , TESTIDCODE: 61586GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 63% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 62% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 52% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 70% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 92% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 53% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 82% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 115% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 107% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 63% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 62% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 66% Analysis Date = 05/10/17 Pct Recovery = 62% Analysis Date = 05/08/17 Pct Recovery = 62% Analysis Date = 05/08/17 Pct Recovery = 62% Analysis Date = 05/06/17 Pct Recovery = 62% Analysis Date = 05/06/17 Pct Recovery = 62% Analysis Date = 05/04/17 Pct Recovery = 63% Analysis Date = 05/04/17 Pct Recovery = 63% Analysis Date = 05/01/17 Pct Recovery = 63% Analysis Date = 05/01/17 Pct Recovery = 63% Analysis Date = 04/29/17 Pct Recovery = 63% Analysis Date = 04/29/17 Pct Recovery = 63% Analysis Date = 04/27/17 Pct Recovery = 64% Analysis Date = 04/27/17 Pct Recovery = 64% Analysis Date = 04/25/17 Pct Recovery = 64% Analysis Date = 04/25/17 Pct Recovery = 64% Analysis Date = 04/22/17 Pct Recovery = 64% Analysis Date = 04/22/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 64% Analysis Date = 04/20/17 Pct Recovery = 64% Analysis Date = 04/18/17 Pct Recovery = 65% Analysis Date = 04/18/17 Pct Recovery = 65% Analysis Date = 04/15/17 Pct Recovery = 65% Analysis Date = 04/15/17 Pct Recovery = 65% Analysis Date = 04/13/17 Pct Recovery = 65% Analysis Date = 04/13/17 Pct Recovery = 65% Analysis Date = 04/11/17 Pct Recovery = 65% Analysis Date = 04/11/17 Pct Recovery = 65% Analysis Date = 04/09/17 Pct Recovery = 66% Analysis Date = 04/09/17 Pct Recovery = 66% Analysis Date = 04/06/17 Pct Recovery = 66% Analysis Date = 04/06/17 Pct Recovery = 66% Analysis Date = 04/04/17 Pct Recovery = 66% Analysis Date = 04/04/17 Pct Recovery = 66% Analysis Date = 04/02/17 Pct Recovery = 67% Analysis Date = 04/02/17 Pct Recovery = 67% Analysis Date = 03/30/17 Pct Recovery = 67% Analysis Date = 03/30/17 Pct Recovery = 67% Analysis Date = 03/28/17 Pct Recovery = 67% Analysis Date = 03/28/17 Pct Recovery = 67% Analysis Date = 03/26/17 Pct Recovery = 67% Analysis Date = 03/26/17 Pct Recovery = 67% Analysis Date = 03/24/17 Pct Recovery = 68% Analysis Date = 03/24/17 Pct Recovery = 68% Analysis Date = 03/21/17 Pct Recovery = 68% Analysis Date = 03/21/17 Pct Recovery = 68% Analysis Date = 03/19/17 Pct Recovery = 68% Analysis Date = 03/19/17 Pct Recovery = 68% Analysis Date = 03/17/17 Pct Recovery = 68% Analysis Date = 03/17/17 Pct Recovery = 68% Analysis Date = 03/14/17 Pct Recovery = 69% Analysis Date = 03/14/17 Pct Recovery = 69% Analysis Date = 03/12/17 Pct Recovery = 69% Analysis Date = 03/12/17 Pct Recovery = 69% Analysis Date = 03/10/17 Pct Recovery = 69% Analysis Date = 03/10/17 Pct Recovery = 69% Analysis Date = 03/08/17 Pct Recovery = 69% Analysis Date = 03/08/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/03/17 Pct Recovery = 70% Analysis Date = 03/03/17 Pct Recovery = 70% Analysis Date = 03/01/17 Pct Recovery = 70% Analysis Date = 03/01/17 Pct Recovery = 70% Analysis Date = 02/26/17 Pct Recovery = 70% Analysis Date = 02/26/17 Pct Recovery = 70% Analysis Date = 02/24/17 Pct Recovery = 70% Analysis Date = 02/24/17 Pct Recovery = 70% Analysis Date = 02/22/17 Pct Recovery = 70% Analysis Date = 02/22/17 Pct Recovery = 70% Analysis Date = 02/20/17 Pct Recovery = 70% Analysis Date = 02/20/17 Pct Recovery = 70% Analysis Date = 02/17/17 Pct Recovery = 70% Analysis Date = 02/17/17 Pct Recovery = 70% Analysis Date = 02/15/17 Pct Recovery = 69% Analysis Date = 02/15/17 Pct Recovery = 69% Analysis Date = 02/13/17 Pct Recovery = 69% Analysis Date = 02/13/17 Pct Recovery = 69% Analysis Date = 02/10/17 Pct Recovery = 68% Analysis Date = 02/10/17 Pct Recovery = 68% Analysis Date = 02/08/17 Pct Recovery = 68% Analysis Date = 02/08/17 Pct Recovery = 68% Analysis Date = 02/06/17 Pct Recovery = 67% Analysis Date = 02/06/17 Pct Recovery = 67% Analysis Date = 02/04/17 Pct Recovery = 67% Analysis Date = 02/04/17 Pct Recovery = 67% Analysis Date = 02/01/17 Pct Recovery = 66% Analysis Date = 02/01/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/28/17 Pct Recovery = 65% Analysis Date = 01/28/17 Pct Recovery = 65% Analysis Date = 01/25/17 Pct Recovery = 65% Analysis Date = 01/25/17 Pct Recovery = 65% Analysis Date = 01/23/17 Pct Recovery = 65% Analysis Date = 01/23/17 Pct Recovery = 65% Analysis Date = 01/21/17 Pct Recovery = 64% Analysis Date = 01/21/17 Pct Recovery = 64% Analysis Date = 01/19/17 Pct Recovery = 64% Analysis Date = 01/19/17 Pct Recovery = 64% Analysis Date = 01/16/17 Pct Recovery = 64% Analysis Date = 01/16/17 Pct Recovery = 64% Analysis Date = 01/14/17 Pct Recovery = 64% Analysis Date = 01/14/17 Pct Recovery = 64% Analysis Date = 01/12/17 Pct Recovery = 64% Analysis Date = 01/12/17 Pct Recovery = 64% Analysis Date = 01/09/17 Pct Recovery = 65% Analysis Date = 01/09/17 Pct Recovery = 65% Analysis Date = 01/07/17 Pct Recovery = 65% Analysis Date = 01/07/17 Pct Recovery = 65% Analysis Date = 01/05/17 Pct Recovery = 65% Analysis Date = 01/05/17 Pct Recovery = 65% Analysis Date = 01/03/17 Pct Recovery = 66% Analysis Date = 01/03/17 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 67% Analysis Date = 12/29/16 Pct Recovery = 67% Analysis Date = 12/27/16 Pct Recovery = 67% Analysis Date = 12/27/16 Pct Recovery = 67% Analysis Date = 12/24/16 Pct Recovery = 67% Analysis Date = 12/24/16 Pct Recovery = 67% Analysis Date = 12/22/16 Pct Recovery = 68% Analysis Date = 12/22/16 Pct Recovery = 68% Analysis Date = 12/20/16 Pct Recovery = 68% Analysis Date = 12/20/16 Pct Recovery = 68% Analysis Date = 12/18/16 Pct Recovery = 68% Analysis Date = 12/18/16 Pct Recovery = 68% Analysis Date = 12/15/16 Pct Recovery = 69% Analysis Date = 12/15/16 Pct Recovery = 69% Analysis Date = 12/13/16 Pct Recovery = 69% Analysis Date = 12/13/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/11/16 Pct Recovery = 69% Analysis Date = 12/08/16 Pct Recovery = 70% Analysis Date = 12/08/16 Pct Recovery = 70% Analysis Date = 12/06/16 Pct Recovery = 70% Analysis Date = 12/06/16 Pct Recovery = 70% Analysis Date = 12/04/16 Pct Recovery = 70% Analysis Date = 12/04/16 Pct Recovery = 70% Analysis Date = 12/02/16 Pct Recovery = 71% Analysis Date = 12/02/16 Pct Recovery = 71% Analysis Date = 11/29/16 Pct Recovery = 71% Analysis Date = 11/29/16 Pct Recovery = 71% Analysis Date = 11/27/16 Pct Recovery = 72% Analysis Date = 11/27/16 Pct Recovery = 72% Analysis Date = 11/25/16 Pct Recovery = 72% Analysis Date = 11/25/16 Pct Recovery = 72% Analysis Date = 11/22/16 Pct Recovery = 72% Analysis Date = 11/22/16 Pct Recovery = 72% Analysis Date = 11/20/16 Pct Recovery = 73% Analysis Date = 11/20/16 Pct Recovery = 73% Analysis Date = 11/18/16 Pct Recovery = 73% Analysis Date = 11/18/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/13/16 Pct Recovery = 74% Analysis Date = 11/13/16 Pct Recovery = 74% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/11/16 Pct Recovery = 74% Analysis Date = 11/09/16 Pct Recovery = 74% Analysis Date = 11/09/16 Pct Recovery = 74% Analysis Date = 11/06/16 Pct Recovery = 75% Analysis Date = 11/06/16 Pct Recovery = 75% Analysis Date = 11/04/16 Pct Recovery = 75% Analysis Date = 11/04/16 Pct Recovery = 75% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 76% Analysis Date = 10/28/16 Pct Recovery = 76% Analysis Date = 10/28/16 Pct Recovery = 76% Analysis Date = 10/26/16 Pct Recovery = 77% Analysis Date = 10/26/16 Pct Recovery = 77% Analysis Date = 10/24/16 Pct Recovery = 77% Analysis Date = 10/24/16 Pct Recovery = 77% Analysis Date = 10/21/16 Pct Recovery = 77% Analysis Date = 10/21/16 Pct Recovery = 77% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/12/16 Pct Recovery = 79% Analysis Date = 10/12/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/10/16 Pct Recovery = 79% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/08/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/05/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/03/16 Pct Recovery = 80% Analysis Date = 10/01/16 Pct Recovery = 81% Analysis Date = 10/01/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/26/16 Pct Recovery = 81% Analysis Date = 09/26/16 Pct Recovery = 81% Analysis Date = 09/24/16 Pct Recovery = 82% Analysis Date = 09/24/16 Pct Recovery = 82% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/13/16 Pct Recovery = 83% Analysis Date = 09/13/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/03/16 Pct Recovery = 83% Analysis Date = 09/03/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/28/16 Pct Recovery = 83% Analysis Date = 08/28/16 Pct Recovery = 83% Analysis Date = 08/25/16 Pct Recovery = 83% Analysis Date = 08/25/16 Pct Recovery = 83% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 82% Analysis Date = 08/18/16 Pct Recovery = 82% Analysis Date = 08/18/16 Pct Recovery = 82% Analysis Date = 08/16/16 Pct Recovery = 82% Analysis Date = 08/16/16 Pct Recovery = 82% Analysis Date = 08/14/16 Pct Recovery = 81% Analysis Date = 08/14/16 Pct Recovery = 81% Analysis Date = 08/12/16 Pct Recovery = 81% Analysis Date = 08/12/16 Pct Recovery = 81% Analysis Date = 08/09/16 Pct Recovery = 81% Analysis Date = 08/09/16 Pct Recovery = 81% Analysis Date = 08/07/16 Pct Recovery = 81% Analysis Date = 08/07/16 Pct Recovery = 81% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/02/16 Pct Recovery = 80% Analysis Date = 08/02/16 Pct Recovery = 80% Analysis Date = 07/31/16 Pct Recovery = 80% Analysis Date = 07/31/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 79% Analysis Date = 07/24/16 Pct Recovery = 79% Analysis Date = 07/24/16 Pct Recovery = 79% Analysis Date = 07/22/16 Pct Recovery = 79% Analysis Date = 07/22/16 Pct Recovery = 79% Analysis Date = 07/20/16 Pct Recovery = 79% Analysis Date = 07/20/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/15/16 Pct Recovery = 78% Analysis Date = 07/15/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/13/16 Pct Recovery = 78% Analysis Date = 07/11/16 Pct Recovery = 78% Analysis Date = 07/11/16 Pct Recovery = 78% Analysis Date = 07/08/16 Pct Recovery = 78% Analysis Date = 07/08/16 Pct Recovery = 78% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/04/16 Pct Recovery = 77% Analysis Date = 07/04/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 06/29/16 Pct Recovery = 77% Analysis Date = 06/29/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 76% Analysis Date = 06/22/16 Pct Recovery = 76% Analysis Date = 06/22/16 Pct Recovery = 76% Analysis Date = 06/20/16 Pct Recovery = 76% Analysis Date = 06/20/16 Pct Recovery = 76% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/15/16 Pct Recovery = 75% Analysis Date = 06/15/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/13/16 Pct Recovery = 75% Analysis Date = 06/11/16 Pct Recovery = 75% Analysis Date = 06/11/16 Pct Recovery = 75% Analysis Date = 06/09/16 Pct Recovery = 74% Analysis Date = 06/09/16 Pct Recovery = 74% Analysis Date = 06/06/16 Pct Recovery = 74% Analysis Date = 06/06/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/04/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 73% Analysis Date = 05/28/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 72% Analysis Date = 05/12/16 Pct Recovery = 72% Analysis Date = 05/12/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 71% Analysis Date = 05/10/16 Pct Recovery = 71% Analysis Date = 05/08/16 Pct Recovery = 71% Analysis Date = 05/08/16 Pct Recovery = 71% Analysis Date = 05/05/16 Pct Recovery = 71% Analysis Date = 05/05/16 Pct Recovery = 71% Analysis Date = 05/03/16 Pct Recovery = 71% Analysis Date = 05/03/16 Pct Recovery = 71% Analysis Date = 05/01/16 Pct Recovery = 71% Analysis Date = 05/01/16 Pct Recovery = 71% Analysis Date = 04/28/16 Pct Recovery = 70% Analysis Date = 04/28/16 Pct Recovery = 70% Analysis Date = 04/26/16 Pct Recovery = 70% Analysis Date = 04/26/16 Pct Recovery = 70% Analysis Date = 04/24/16 Pct Recovery = 70% Analysis Date = 04/24/16 Pct Recovery = 70% Analysis Date = 04/22/16 Pct Recovery = 70% Analysis Date = 04/22/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/19/16 Pct Recovery = 70% Analysis Date = 04/17/16 Pct Recovery = 70% Analysis Date = 04/17/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/15/16 Pct Recovery = 70% Analysis Date = 04/12/16 Pct Recovery = 69% Analysis Date = 04/12/16 Pct Recovery = 69% Analysis Date = 04/10/16 Pct Recovery = 69% Analysis Date = 04/10/16 Pct Recovery = 69% Analysis Date = 04/08/16 Pct Recovery = 69% Analysis Date = 04/08/16 Pct Recovery = 69% Analysis Date = 04/06/16 Pct Recovery = 69% Analysis Date = 04/06/16 Pct Recovery = 69% Analysis Date = 04/03/16 Pct Recovery = 69% Analysis Date = 04/03/16 Pct Recovery = 69% Analysis Date = 04/01/16 Pct Recovery = 69% Analysis Date = 04/01/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/27/16 Pct Recovery = 68% Analysis Date = 03/25/16 Pct Recovery = 68% Analysis Date = 03/25/16 Pct Recovery = 68% Analysis Date = 03/23/16 Pct Recovery = 68% Analysis Date = 03/23/16 Pct Recovery = 68% Analysis Date = 03/21/16 Pct Recovery = 68% Analysis Date = 03/21/16 Pct Recovery = 68% Analysis Date = 03/18/16 Pct Recovery = 68% Analysis Date = 03/18/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/16/16 Pct Recovery = 68% Analysis Date = 03/14/16 Pct Recovery = 67% Analysis Date = 03/14/16 Pct Recovery = 67% Analysis Date = 03/11/16 Pct Recovery = 67% Analysis Date = 03/11/16 Pct Recovery = 67% Analysis Date = 03/09/16 Pct Recovery = 67% Analysis Date = 03/09/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/07/16 Pct Recovery = 67% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 03/05/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 03/02/16 Pct Recovery = 67% Analysis Date = 02/29/16 Pct Recovery = 66% Analysis Date = 02/29/16 Pct Recovery = 66% Analysis Date = 02/27/16 Pct Recovery = 66% Analysis Date = 02/27/16 Pct Recovery = 66% Analysis Date = 02/24/16 Pct Recovery = 66% Analysis Date = 02/24/16 Pct Recovery = 66% Analysis Date = 02/22/16 Pct Recovery = 66% Analysis Date = 02/22/16 Pct Recovery = 66% Analysis Date = 02/20/16 Pct Recovery = 66% Analysis Date = 02/20/16 Pct Recovery = 66% Analysis Date = 02/18/16 Pct Recovery = 66% Analysis Date = 02/18/16 Pct Recovery = 66% Analysis Date = 02/15/16 Pct Recovery = 66% Analysis Date = 02/15/16 Pct Recovery = 66% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/13/16 Pct Recovery = 65% Analysis Date = 02/11/16 Pct Recovery = 65% Analysis Date = 02/11/16 Pct Recovery = 65% Analysis Date = 02/09/16 Pct Recovery = 65% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
CYPERMETHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 73% 18% 66% 14%
Total 19 73% 18% 66% 14%

Sample Statistics
CYPERMETHRIN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
DACTHAL
METHOD: 2033 , TESTIDCODE: 82682GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 114% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 102% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 92% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 104% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 93% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 89% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 100% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 102% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 91% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 93% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 84% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 80% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 97% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 106% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 05/02/17 Pct Recovery = 99% Analysis Date = 04/30/17 Pct Recovery = 99% Analysis Date = 04/30/17 Pct Recovery = 99% Analysis Date = 04/28/17 Pct Recovery = 99% Analysis Date = 04/28/17 Pct Recovery = 99% Analysis Date = 04/26/17 Pct Recovery = 99% Analysis Date = 04/26/17 Pct Recovery = 99% Analysis Date = 04/24/17 Pct Recovery = 99% Analysis Date = 04/24/17 Pct Recovery = 99% Analysis Date = 04/21/17 Pct Recovery = 99% Analysis Date = 04/21/17 Pct Recovery = 99% Analysis Date = 04/19/17 Pct Recovery = 99% Analysis Date = 04/19/17 Pct Recovery = 99% Analysis Date = 04/17/17 Pct Recovery = 99% Analysis Date = 04/17/17 Pct Recovery = 99% Analysis Date = 04/15/17 Pct Recovery = 99% Analysis Date = 04/15/17 Pct Recovery = 99% Analysis Date = 04/12/17 Pct Recovery = 99% Analysis Date = 04/12/17 Pct Recovery = 99% Analysis Date = 04/10/17 Pct Recovery = 99% Analysis Date = 04/10/17 Pct Recovery = 99% Analysis Date = 04/08/17 Pct Recovery = 99% Analysis Date = 04/08/17 Pct Recovery = 99% Analysis Date = 04/06/17 Pct Recovery = 100% Analysis Date = 04/06/17 Pct Recovery = 100% Analysis Date = 04/03/17 Pct Recovery = 100% Analysis Date = 04/03/17 Pct Recovery = 100% Analysis Date = 04/01/17 Pct Recovery = 100% Analysis Date = 04/01/17 Pct Recovery = 100% Analysis Date = 03/30/17 Pct Recovery = 100% Analysis Date = 03/30/17 Pct Recovery = 100% Analysis Date = 03/28/17 Pct Recovery = 100% Analysis Date = 03/28/17 Pct Recovery = 100% Analysis Date = 03/25/17 Pct Recovery = 100% Analysis Date = 03/25/17 Pct Recovery = 100% Analysis Date = 03/23/17 Pct Recovery = 100% Analysis Date = 03/23/17 Pct Recovery = 100% Analysis Date = 03/21/17 Pct Recovery = 100% Analysis Date = 03/21/17 Pct Recovery = 100% Analysis Date = 03/19/17 Pct Recovery = 100% Analysis Date = 03/19/17 Pct Recovery = 100% Analysis Date = 03/16/17 Pct Recovery = 100% Analysis Date = 03/16/17 Pct Recovery = 100% Analysis Date = 03/14/17 Pct Recovery = 100% Analysis Date = 03/14/17 Pct Recovery = 100% Analysis Date = 03/12/17 Pct Recovery = 100% Analysis Date = 03/12/17 Pct Recovery = 100% Analysis Date = 03/10/17 Pct Recovery = 100% Analysis Date = 03/10/17 Pct Recovery = 100% Analysis Date = 03/07/17 Pct Recovery = 101% Analysis Date = 03/07/17 Pct Recovery = 101% Analysis Date = 03/05/17 Pct Recovery = 101% Analysis Date = 03/05/17 Pct Recovery = 101% Analysis Date = 03/03/17 Pct Recovery = 101% Analysis Date = 03/03/17 Pct Recovery = 101% Analysis Date = 03/01/17 Pct Recovery = 101% Analysis Date = 03/01/17 Pct Recovery = 101% Analysis Date = 02/26/17 Pct Recovery = 101% Analysis Date = 02/26/17 Pct Recovery = 101% Analysis Date = 02/24/17 Pct Recovery = 101% Analysis Date = 02/24/17 Pct Recovery = 101% Analysis Date = 02/22/17 Pct Recovery = 101% Analysis Date = 02/22/17 Pct Recovery = 101% Analysis Date = 02/20/17 Pct Recovery = 101% Analysis Date = 02/20/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/11/17 Pct Recovery = 101% Analysis Date = 02/11/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 100% Analysis Date = 02/06/17 Pct Recovery = 100% Analysis Date = 02/04/17 Pct Recovery = 100% Analysis Date = 02/04/17 Pct Recovery = 100% Analysis Date = 02/02/17 Pct Recovery = 100% Analysis Date = 02/02/17 Pct Recovery = 100% Analysis Date = 01/30/17 Pct Recovery = 100% Analysis Date = 01/30/17 Pct Recovery = 100% Analysis Date = 01/28/17 Pct Recovery = 100% Analysis Date = 01/28/17 Pct Recovery = 100% Analysis Date = 01/26/17 Pct Recovery = 100% Analysis Date = 01/26/17 Pct Recovery = 100% Analysis Date = 01/24/17 Pct Recovery = 100% Analysis Date = 01/24/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 100% Analysis Date = 01/19/17 Pct Recovery = 99% Analysis Date = 01/19/17 Pct Recovery = 99% Analysis Date = 01/17/17 Pct Recovery = 99% Analysis Date = 01/17/17 Pct Recovery = 99% Analysis Date = 01/15/17 Pct Recovery = 99% Analysis Date = 01/15/17 Pct Recovery = 99% Analysis Date = 01/12/17 Pct Recovery = 99% Analysis Date = 01/12/17 Pct Recovery = 99% Analysis Date = 01/10/17 Pct Recovery = 99% Analysis Date = 01/10/17 Pct Recovery = 99% Analysis Date = 01/08/17 Pct Recovery = 99% Analysis Date = 01/08/17 Pct Recovery = 99% Analysis Date = 01/06/17 Pct Recovery = 99% Analysis Date = 01/06/17 Pct Recovery = 99% Analysis Date = 01/04/17 Pct Recovery = 99% Analysis Date = 01/04/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 98% Analysis Date = 01/01/17 Pct Recovery = 98% Analysis Date = 12/30/16 Pct Recovery = 98% Analysis Date = 12/30/16 Pct Recovery = 98% Analysis Date = 12/28/16 Pct Recovery = 98% Analysis Date = 12/28/16 Pct Recovery = 98% Analysis Date = 12/26/16 Pct Recovery = 98% Analysis Date = 12/26/16 Pct Recovery = 98% Analysis Date = 12/23/16 Pct Recovery = 98% Analysis Date = 12/23/16 Pct Recovery = 98% Analysis Date = 12/21/16 Pct Recovery = 98% Analysis Date = 12/21/16 Pct Recovery = 98% Analysis Date = 12/19/16 Pct Recovery = 98% Analysis Date = 12/19/16 Pct Recovery = 98% Analysis Date = 12/17/16 Pct Recovery = 97% Analysis Date = 12/17/16 Pct Recovery = 97% Analysis Date = 12/14/16 Pct Recovery = 97% Analysis Date = 12/14/16 Pct Recovery = 97% Analysis Date = 12/12/16 Pct Recovery = 97% Analysis Date = 12/12/16 Pct Recovery = 97% Analysis Date = 12/10/16 Pct Recovery = 97% Analysis Date = 12/10/16 Pct Recovery = 97% Analysis Date = 12/08/16 Pct Recovery = 96% Analysis Date = 12/08/16 Pct Recovery = 96% Analysis Date = 12/05/16 Pct Recovery = 96% Analysis Date = 12/05/16 Pct Recovery = 96% Analysis Date = 12/03/16 Pct Recovery = 96% Analysis Date = 12/03/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 11/29/16 Pct Recovery = 96% Analysis Date = 11/29/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 95% Analysis Date = 11/26/16 Pct Recovery = 95% Analysis Date = 11/24/16 Pct Recovery = 95% Analysis Date = 11/24/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/17/16 Pct Recovery = 94% Analysis Date = 11/15/16 Pct Recovery = 94% Analysis Date = 11/15/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/08/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/06/16 Pct Recovery = 93% Analysis Date = 11/04/16 Pct Recovery = 93% Analysis Date = 11/04/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 11/02/16 Pct Recovery = 93% Analysis Date = 10/30/16 Pct Recovery = 93% Analysis Date = 10/30/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/06/16 Pct Recovery = 90% Analysis Date = 10/06/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/27/16 Pct Recovery = 89% Analysis Date = 09/24/16 Pct Recovery = 89% Analysis Date = 09/24/16 Pct Recovery = 89% Analysis Date = 09/22/16 Pct Recovery = 89% Analysis Date = 09/22/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/20/16 Pct Recovery = 89% Analysis Date = 09/18/16 Pct Recovery = 88% Analysis Date = 09/18/16 Pct Recovery = 88% Analysis Date = 09/16/16 Pct Recovery = 88% Analysis Date = 09/16/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/11/16 Pct Recovery = 88% Analysis Date = 09/11/16 Pct Recovery = 88% Analysis Date = 09/09/16 Pct Recovery = 87% Analysis Date = 09/09/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/07/16 Pct Recovery = 87% Analysis Date = 09/04/16 Pct Recovery = 87% Analysis Date = 09/04/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 87% Analysis Date = 09/02/16 Pct Recovery = 87% Analysis Date = 08/31/16 Pct Recovery = 87% Analysis Date = 08/31/16 Pct Recovery = 87% Analysis Date = 08/29/16 Pct Recovery = 87% Analysis Date = 08/29/16 Pct Recovery = 87% Analysis Date = 08/26/16 Pct Recovery = 87% Analysis Date = 08/26/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 87% Analysis Date = 08/22/16 Pct Recovery = 87% Analysis Date = 08/22/16 Pct Recovery = 87% Analysis Date = 08/20/16 Pct Recovery = 87% Analysis Date = 08/20/16 Pct Recovery = 87% Analysis Date = 08/17/16 Pct Recovery = 87% Analysis Date = 08/17/16 Pct Recovery = 87% Analysis Date = 08/15/16 Pct Recovery = 87% Analysis Date = 08/15/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 87% Analysis Date = 08/13/16 Pct Recovery = 87% Analysis Date = 08/11/16 Pct Recovery = 87% Analysis Date = 08/11/16 Pct Recovery = 87% Analysis Date = 08/08/16 Pct Recovery = 87% Analysis Date = 08/08/16 Pct Recovery = 87% Analysis Date = 08/06/16 Pct Recovery = 87% Analysis Date = 08/06/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 07/30/16 Pct Recovery = 87% Analysis Date = 07/30/16 Pct Recovery = 87% Analysis Date = 07/28/16 Pct Recovery = 87% Analysis Date = 07/28/16 Pct Recovery = 87% Analysis Date = 07/26/16 Pct Recovery = 87% Analysis Date = 07/26/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/21/16 Pct Recovery = 87% Analysis Date = 07/21/16 Pct Recovery = 87% Analysis Date = 07/19/16 Pct Recovery = 87% Analysis Date = 07/19/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/12/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/10/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/03/16 Pct Recovery = 87% Analysis Date = 07/03/16 Pct Recovery = 87% Analysis Date = 07/01/16 Pct Recovery = 87% Analysis Date = 07/01/16 Pct Recovery = 87% Analysis Date = 06/29/16 Pct Recovery = 87% Analysis Date = 06/29/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/27/16 Pct Recovery = 87% Analysis Date = 06/24/16 Pct Recovery = 87% Analysis Date = 06/24/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/22/16 Pct Recovery = 87% Analysis Date = 06/20/16 Pct Recovery = 87% Analysis Date = 06/20/16 Pct Recovery = 87% Analysis Date = 06/18/16 Pct Recovery = 87% Analysis Date = 06/18/16 Pct Recovery = 87% Analysis Date = 06/15/16 Pct Recovery = 87% Analysis Date = 06/15/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/13/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/09/16 Pct Recovery = 87% Analysis Date = 06/09/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 87% Analysis Date = 06/04/16 Pct Recovery = 87% Analysis Date = 06/04/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 87% Analysis Date = 05/31/16 Pct Recovery = 87% Analysis Date = 05/31/16 Pct Recovery = 87% Analysis Date = 05/29/16 Pct Recovery = 87% Analysis Date = 05/29/16 Pct Recovery = 87% Analysis Date = 05/26/16 Pct Recovery = 88% Analysis Date = 05/26/16 Pct Recovery = 88% Analysis Date = 05/24/16 Pct Recovery = 88% Analysis Date = 05/24/16 Pct Recovery = 88% Analysis Date = 05/22/16 Pct Recovery = 88% Analysis Date = 05/22/16 Pct Recovery = 88% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/20/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/15/16 Pct Recovery = 89% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/13/16 Pct Recovery = 90% Analysis Date = 05/11/16 Pct Recovery = 90% Analysis Date = 05/11/16 Pct Recovery = 90% Analysis Date = 05/08/16 Pct Recovery = 91% Analysis Date = 05/08/16 Pct Recovery = 91% Analysis Date = 05/06/16 Pct Recovery = 91% Analysis Date = 05/06/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/04/16 Pct Recovery = 91% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 05/02/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/27/16 Pct Recovery = 92% Analysis Date = 04/27/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 92% Analysis Date = 04/23/16 Pct Recovery = 92% Analysis Date = 04/23/16 Pct Recovery = 92% Analysis Date = 04/20/16 Pct Recovery = 93% Analysis Date = 04/20/16 Pct Recovery = 93% Analysis Date = 04/18/16 Pct Recovery = 93% Analysis Date = 04/18/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/16/16 Pct Recovery = 93% Analysis Date = 04/14/16 Pct Recovery = 93% Analysis Date = 04/14/16 Pct Recovery = 93% Analysis Date = 04/11/16 Pct Recovery = 93% Analysis Date = 04/11/16 Pct Recovery = 93% Analysis Date = 04/09/16 Pct Recovery = 94% Analysis Date = 04/09/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/05/16 Pct Recovery = 94% Analysis Date = 04/05/16 Pct Recovery = 94% Analysis Date = 04/02/16 Pct Recovery = 94% Analysis Date = 04/02/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/29/16 Pct Recovery = 95% Analysis Date = 03/29/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/24/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/22/16 Pct Recovery = 95% Analysis Date = 03/20/16 Pct Recovery = 95% Analysis Date = 03/20/16 Pct Recovery = 95% Analysis Date = 03/18/16 Pct Recovery = 95% Analysis Date = 03/18/16 Pct Recovery = 95% Analysis Date = 03/15/16 Pct Recovery = 96% Analysis Date = 03/15/16 Pct Recovery = 96% Analysis Date = 03/13/16 Pct Recovery = 96% Analysis Date = 03/13/16 Pct Recovery = 96% Analysis Date = 03/11/16 Pct Recovery = 96% Analysis Date = 03/11/16 Pct Recovery = 96% Analysis Date = 03/09/16 Pct Recovery = 96% Analysis Date = 03/09/16 Pct Recovery = 96% Analysis Date = 03/06/16 Pct Recovery = 96% Analysis Date = 03/06/16 Pct Recovery = 96% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/26/16 Pct Recovery = 97% Analysis Date = 02/26/16 Pct Recovery = 97% Analysis Date = 02/24/16 Pct Recovery = 97% Analysis Date = 02/24/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/22/16 Pct Recovery = 97% Analysis Date = 02/20/16 Pct Recovery = 98% Analysis Date = 02/20/16 Pct Recovery = 98% Analysis Date = 02/17/16 Pct Recovery = 98% Analysis Date = 02/17/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/15/16 Pct Recovery = 98% Analysis Date = 02/13/16 Pct Recovery = 98% Analysis Date = 02/13/16 Pct Recovery = 98% Analysis Date = 02/11/16 Pct Recovery = 98% Analysis Date = 02/11/16 Pct Recovery = 98% Analysis Date = 02/09/16 Pct Recovery = 98% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DACTHAL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 95% 9% 93% 9%
Total 19 95% 9% 93% 9%

Sample Statistics
DACTHAL

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
DEETHYLATRAZINE
METHOD: 2033 , TESTIDCODE: 04040GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 51% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 55% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 52% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 11% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 50% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 49% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 33% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 47% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 70% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 58% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 62% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 55% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 55% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 69% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 64% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 61% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 54% Analysis Date = 05/10/17 Pct Recovery = 46% Analysis Date = 05/08/17 Pct Recovery = 47% Analysis Date = 05/08/17 Pct Recovery = 47% Analysis Date = 05/06/17 Pct Recovery = 47% Analysis Date = 05/06/17 Pct Recovery = 47% Analysis Date = 05/04/17 Pct Recovery = 47% Analysis Date = 05/04/17 Pct Recovery = 47% Analysis Date = 05/01/17 Pct Recovery = 47% Analysis Date = 05/01/17 Pct Recovery = 47% Analysis Date = 04/29/17 Pct Recovery = 47% Analysis Date = 04/29/17 Pct Recovery = 47% Analysis Date = 04/27/17 Pct Recovery = 47% Analysis Date = 04/27/17 Pct Recovery = 47% Analysis Date = 04/25/17 Pct Recovery = 47% Analysis Date = 04/25/17 Pct Recovery = 47% Analysis Date = 04/22/17 Pct Recovery = 48% Analysis Date = 04/22/17 Pct Recovery = 48% Analysis Date = 04/20/17 Pct Recovery = 48% Analysis Date = 04/20/17 Pct Recovery = 48% Analysis Date = 04/18/17 Pct Recovery = 48% Analysis Date = 04/18/17 Pct Recovery = 48% Analysis Date = 04/15/17 Pct Recovery = 48% Analysis Date = 04/15/17 Pct Recovery = 48% Analysis Date = 04/13/17 Pct Recovery = 48% Analysis Date = 04/13/17 Pct Recovery = 48% Analysis Date = 04/11/17 Pct Recovery = 48% Analysis Date = 04/11/17 Pct Recovery = 48% Analysis Date = 04/09/17 Pct Recovery = 49% Analysis Date = 04/09/17 Pct Recovery = 49% Analysis Date = 04/06/17 Pct Recovery = 49% Analysis Date = 04/06/17 Pct Recovery = 49% Analysis Date = 04/04/17 Pct Recovery = 49% Analysis Date = 04/04/17 Pct Recovery = 49% Analysis Date = 04/02/17 Pct Recovery = 49% Analysis Date = 04/02/17 Pct Recovery = 49% Analysis Date = 03/30/17 Pct Recovery = 49% Analysis Date = 03/30/17 Pct Recovery = 49% Analysis Date = 03/28/17 Pct Recovery = 49% Analysis Date = 03/28/17 Pct Recovery = 49% Analysis Date = 03/26/17 Pct Recovery = 49% Analysis Date = 03/26/17 Pct Recovery = 49% Analysis Date = 03/24/17 Pct Recovery = 50% Analysis Date = 03/24/17 Pct Recovery = 50% Analysis Date = 03/21/17 Pct Recovery = 50% Analysis Date = 03/21/17 Pct Recovery = 50% Analysis Date = 03/19/17 Pct Recovery = 50% Analysis Date = 03/19/17 Pct Recovery = 50% Analysis Date = 03/17/17 Pct Recovery = 50% Analysis Date = 03/17/17 Pct Recovery = 50% Analysis Date = 03/14/17 Pct Recovery = 50% Analysis Date = 03/14/17 Pct Recovery = 50% Analysis Date = 03/12/17 Pct Recovery = 50% Analysis Date = 03/12/17 Pct Recovery = 50% Analysis Date = 03/10/17 Pct Recovery = 51% Analysis Date = 03/10/17 Pct Recovery = 51% Analysis Date = 03/08/17 Pct Recovery = 51% Analysis Date = 03/08/17 Pct Recovery = 51% Analysis Date = 03/05/17 Pct Recovery = 51% Analysis Date = 03/05/17 Pct Recovery = 51% Analysis Date = 03/03/17 Pct Recovery = 51% Analysis Date = 03/03/17 Pct Recovery = 51% Analysis Date = 03/01/17 Pct Recovery = 51% Analysis Date = 03/01/17 Pct Recovery = 51% Analysis Date = 02/26/17 Pct Recovery = 52% Analysis Date = 02/26/17 Pct Recovery = 52% Analysis Date = 02/24/17 Pct Recovery = 52% Analysis Date = 02/24/17 Pct Recovery = 52% Analysis Date = 02/22/17 Pct Recovery = 52% Analysis Date = 02/22/17 Pct Recovery = 52% Analysis Date = 02/20/17 Pct Recovery = 52% Analysis Date = 02/20/17 Pct Recovery = 52% Analysis Date = 02/17/17 Pct Recovery = 53% Analysis Date = 02/17/17 Pct Recovery = 53% Analysis Date = 02/15/17 Pct Recovery = 53% Analysis Date = 02/15/17 Pct Recovery = 53% Analysis Date = 02/13/17 Pct Recovery = 54% Analysis Date = 02/13/17 Pct Recovery = 54% Analysis Date = 02/10/17 Pct Recovery = 54% Analysis Date = 02/10/17 Pct Recovery = 54% Analysis Date = 02/08/17 Pct Recovery = 55% Analysis Date = 02/08/17 Pct Recovery = 55% Analysis Date = 02/06/17 Pct Recovery = 55% Analysis Date = 02/06/17 Pct Recovery = 55% Analysis Date = 02/04/17 Pct Recovery = 56% Analysis Date = 02/04/17 Pct Recovery = 56% Analysis Date = 02/01/17 Pct Recovery = 56% Analysis Date = 02/01/17 Pct Recovery = 56% Analysis Date = 01/30/17 Pct Recovery = 57% Analysis Date = 01/30/17 Pct Recovery = 57% Analysis Date = 01/28/17 Pct Recovery = 57% Analysis Date = 01/28/17 Pct Recovery = 57% Analysis Date = 01/25/17 Pct Recovery = 58% Analysis Date = 01/25/17 Pct Recovery = 58% Analysis Date = 01/23/17 Pct Recovery = 58% Analysis Date = 01/23/17 Pct Recovery = 58% Analysis Date = 01/21/17 Pct Recovery = 59% Analysis Date = 01/21/17 Pct Recovery = 59% Analysis Date = 01/19/17 Pct Recovery = 59% Analysis Date = 01/19/17 Pct Recovery = 59% Analysis Date = 01/16/17 Pct Recovery = 59% Analysis Date = 01/16/17 Pct Recovery = 59% Analysis Date = 01/14/17 Pct Recovery = 59% Analysis Date = 01/14/17 Pct Recovery = 59% Analysis Date = 01/12/17 Pct Recovery = 59% Analysis Date = 01/12/17 Pct Recovery = 59% Analysis Date = 01/09/17 Pct Recovery = 59% Analysis Date = 01/09/17 Pct Recovery = 59% Analysis Date = 01/07/17 Pct Recovery = 59% Analysis Date = 01/07/17 Pct Recovery = 59% Analysis Date = 01/05/17 Pct Recovery = 58% Analysis Date = 01/05/17 Pct Recovery = 58% Analysis Date = 01/03/17 Pct Recovery = 58% Analysis Date = 01/03/17 Pct Recovery = 58% Analysis Date = 12/31/16 Pct Recovery = 58% Analysis Date = 12/31/16 Pct Recovery = 58% Analysis Date = 12/29/16 Pct Recovery = 58% Analysis Date = 12/29/16 Pct Recovery = 58% Analysis Date = 12/27/16 Pct Recovery = 58% Analysis Date = 12/27/16 Pct Recovery = 58% Analysis Date = 12/24/16 Pct Recovery = 58% Analysis Date = 12/24/16 Pct Recovery = 58% Analysis Date = 12/22/16 Pct Recovery = 58% Analysis Date = 12/22/16 Pct Recovery = 58% Analysis Date = 12/20/16 Pct Recovery = 57% Analysis Date = 12/20/16 Pct Recovery = 57% Analysis Date = 12/18/16 Pct Recovery = 57% Analysis Date = 12/18/16 Pct Recovery = 57% Analysis Date = 12/15/16 Pct Recovery = 57% Analysis Date = 12/15/16 Pct Recovery = 57% Analysis Date = 12/13/16 Pct Recovery = 57% Analysis Date = 12/13/16 Pct Recovery = 57% Analysis Date = 12/11/16 Pct Recovery = 57% Analysis Date = 12/11/16 Pct Recovery = 57% Analysis Date = 12/08/16 Pct Recovery = 57% Analysis Date = 12/08/16 Pct Recovery = 57% Analysis Date = 12/06/16 Pct Recovery = 57% Analysis Date = 12/06/16 Pct Recovery = 57% Analysis Date = 12/04/16 Pct Recovery = 56% Analysis Date = 12/04/16 Pct Recovery = 56% Analysis Date = 12/02/16 Pct Recovery = 56% Analysis Date = 12/02/16 Pct Recovery = 56% Analysis Date = 11/29/16 Pct Recovery = 56% Analysis Date = 11/29/16 Pct Recovery = 56% Analysis Date = 11/27/16 Pct Recovery = 56% Analysis Date = 11/27/16 Pct Recovery = 56% Analysis Date = 11/25/16 Pct Recovery = 56% Analysis Date = 11/25/16 Pct Recovery = 56% Analysis Date = 11/22/16 Pct Recovery = 56% Analysis Date = 11/22/16 Pct Recovery = 56% Analysis Date = 11/20/16 Pct Recovery = 56% Analysis Date = 11/20/16 Pct Recovery = 56% Analysis Date = 11/18/16 Pct Recovery = 55% Analysis Date = 11/18/16 Pct Recovery = 55% Analysis Date = 11/16/16 Pct Recovery = 55% Analysis Date = 11/16/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/11/16 Pct Recovery = 55% Analysis Date = 11/11/16 Pct Recovery = 55% Analysis Date = 11/09/16 Pct Recovery = 55% Analysis Date = 11/09/16 Pct Recovery = 55% Analysis Date = 11/06/16 Pct Recovery = 55% Analysis Date = 11/06/16 Pct Recovery = 55% Analysis Date = 11/04/16 Pct Recovery = 55% Analysis Date = 11/04/16 Pct Recovery = 55% Analysis Date = 11/02/16 Pct Recovery = 54% Analysis Date = 11/02/16 Pct Recovery = 54% Analysis Date = 10/31/16 Pct Recovery = 54% Analysis Date = 10/31/16 Pct Recovery = 54% Analysis Date = 10/28/16 Pct Recovery = 54% Analysis Date = 10/28/16 Pct Recovery = 54% Analysis Date = 10/26/16 Pct Recovery = 54% Analysis Date = 10/26/16 Pct Recovery = 54% Analysis Date = 10/24/16 Pct Recovery = 54% Analysis Date = 10/24/16 Pct Recovery = 54% Analysis Date = 10/21/16 Pct Recovery = 54% Analysis Date = 10/21/16 Pct Recovery = 54% Analysis Date = 10/19/16 Pct Recovery = 54% Analysis Date = 10/19/16 Pct Recovery = 54% Analysis Date = 10/17/16 Pct Recovery = 54% Analysis Date = 10/17/16 Pct Recovery = 54% Analysis Date = 10/15/16 Pct Recovery = 53% Analysis Date = 10/15/16 Pct Recovery = 53% Analysis Date = 10/12/16 Pct Recovery = 53% Analysis Date = 10/12/16 Pct Recovery = 53% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/10/16 Pct Recovery = 53% Analysis Date = 10/08/16 Pct Recovery = 53% Analysis Date = 10/08/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/05/16 Pct Recovery = 53% Analysis Date = 10/03/16 Pct Recovery = 53% Analysis Date = 10/03/16 Pct Recovery = 53% Analysis Date = 10/01/16 Pct Recovery = 53% Analysis Date = 10/01/16 Pct Recovery = 53% Analysis Date = 09/29/16 Pct Recovery = 52% Analysis Date = 09/29/16 Pct Recovery = 52% Analysis Date = 09/26/16 Pct Recovery = 52% Analysis Date = 09/26/16 Pct Recovery = 52% Analysis Date = 09/24/16 Pct Recovery = 52% Analysis Date = 09/24/16 Pct Recovery = 52% Analysis Date = 09/22/16 Pct Recovery = 52% Analysis Date = 09/22/16 Pct Recovery = 52% Analysis Date = 09/19/16 Pct Recovery = 52% Analysis Date = 09/19/16 Pct Recovery = 52% Analysis Date = 09/17/16 Pct Recovery = 52% Analysis Date = 09/17/16 Pct Recovery = 52% Analysis Date = 09/15/16 Pct Recovery = 52% Analysis Date = 09/15/16 Pct Recovery = 52% Analysis Date = 09/13/16 Pct Recovery = 52% Analysis Date = 09/13/16 Pct Recovery = 52% Analysis Date = 09/10/16 Pct Recovery = 52% Analysis Date = 09/10/16 Pct Recovery = 52% Analysis Date = 09/08/16 Pct Recovery = 52% Analysis Date = 09/08/16 Pct Recovery = 52% Analysis Date = 09/06/16 Pct Recovery = 52% Analysis Date = 09/06/16 Pct Recovery = 52% Analysis Date = 09/03/16 Pct Recovery = 52% Analysis Date = 09/03/16 Pct Recovery = 52% Analysis Date = 09/01/16 Pct Recovery = 52% Analysis Date = 09/01/16 Pct Recovery = 52% Analysis Date = 08/30/16 Pct Recovery = 52% Analysis Date = 08/30/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 52% Analysis Date = 08/28/16 Pct Recovery = 52% Analysis Date = 08/25/16 Pct Recovery = 52% Analysis Date = 08/25/16 Pct Recovery = 52% Analysis Date = 08/23/16 Pct Recovery = 52% Analysis Date = 08/23/16 Pct Recovery = 52% Analysis Date = 08/21/16 Pct Recovery = 52% Analysis Date = 08/21/16 Pct Recovery = 52% Analysis Date = 08/18/16 Pct Recovery = 52% Analysis Date = 08/18/16 Pct Recovery = 52% Analysis Date = 08/16/16 Pct Recovery = 53% Analysis Date = 08/16/16 Pct Recovery = 53% Analysis Date = 08/14/16 Pct Recovery = 53% Analysis Date = 08/14/16 Pct Recovery = 53% Analysis Date = 08/12/16 Pct Recovery = 53% Analysis Date = 08/12/16 Pct Recovery = 53% Analysis Date = 08/09/16 Pct Recovery = 53% Analysis Date = 08/09/16 Pct Recovery = 53% Analysis Date = 08/07/16 Pct Recovery = 53% Analysis Date = 08/07/16 Pct Recovery = 53% Analysis Date = 08/05/16 Pct Recovery = 53% Analysis Date = 08/05/16 Pct Recovery = 53% Analysis Date = 08/02/16 Pct Recovery = 53% Analysis Date = 08/02/16 Pct Recovery = 53% Analysis Date = 07/31/16 Pct Recovery = 53% Analysis Date = 07/31/16 Pct Recovery = 53% Analysis Date = 07/29/16 Pct Recovery = 54% Analysis Date = 07/29/16 Pct Recovery = 54% Analysis Date = 07/27/16 Pct Recovery = 54% Analysis Date = 07/27/16 Pct Recovery = 54% Analysis Date = 07/24/16 Pct Recovery = 54% Analysis Date = 07/24/16 Pct Recovery = 54% Analysis Date = 07/22/16 Pct Recovery = 54% Analysis Date = 07/22/16 Pct Recovery = 54% Analysis Date = 07/20/16 Pct Recovery = 54% Analysis Date = 07/20/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/15/16 Pct Recovery = 54% Analysis Date = 07/15/16 Pct Recovery = 54% Analysis Date = 07/13/16 Pct Recovery = 54% Analysis Date = 07/13/16 Pct Recovery = 54% Analysis Date = 07/11/16 Pct Recovery = 55% Analysis Date = 07/11/16 Pct Recovery = 55% Analysis Date = 07/08/16 Pct Recovery = 55% Analysis Date = 07/08/16 Pct Recovery = 55% Analysis Date = 07/06/16 Pct Recovery = 55% Analysis Date = 07/06/16 Pct Recovery = 55% Analysis Date = 07/04/16 Pct Recovery = 55% Analysis Date = 07/04/16 Pct Recovery = 55% Analysis Date = 07/01/16 Pct Recovery = 55% Analysis Date = 07/01/16 Pct Recovery = 55% Analysis Date = 06/29/16 Pct Recovery = 55% Analysis Date = 06/29/16 Pct Recovery = 55% Analysis Date = 06/27/16 Pct Recovery = 55% Analysis Date = 06/27/16 Pct Recovery = 55% Analysis Date = 06/25/16 Pct Recovery = 55% Analysis Date = 06/25/16 Pct Recovery = 55% Analysis Date = 06/22/16 Pct Recovery = 56% Analysis Date = 06/22/16 Pct Recovery = 56% Analysis Date = 06/20/16 Pct Recovery = 56% Analysis Date = 06/20/16 Pct Recovery = 56% Analysis Date = 06/18/16 Pct Recovery = 56% Analysis Date = 06/18/16 Pct Recovery = 56% Analysis Date = 06/15/16 Pct Recovery = 56% Analysis Date = 06/15/16 Pct Recovery = 56% Analysis Date = 06/13/16 Pct Recovery = 56% Analysis Date = 06/13/16 Pct Recovery = 56% Analysis Date = 06/11/16 Pct Recovery = 56% Analysis Date = 06/11/16 Pct Recovery = 56% Analysis Date = 06/09/16 Pct Recovery = 56% Analysis Date = 06/09/16 Pct Recovery = 56% Analysis Date = 06/06/16 Pct Recovery = 56% Analysis Date = 06/06/16 Pct Recovery = 56% Analysis Date = 06/04/16 Pct Recovery = 57% Analysis Date = 06/04/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 05/30/16 Pct Recovery = 57% Analysis Date = 05/30/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 57% Analysis Date = 05/28/16 Pct Recovery = 57% Analysis Date = 05/26/16 Pct Recovery = 57% Analysis Date = 05/26/16 Pct Recovery = 57% Analysis Date = 05/24/16 Pct Recovery = 57% Analysis Date = 05/24/16 Pct Recovery = 57% Analysis Date = 05/21/16 Pct Recovery = 57% Analysis Date = 05/21/16 Pct Recovery = 57% Analysis Date = 05/19/16 Pct Recovery = 57% Analysis Date = 05/19/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 57% Analysis Date = 05/17/16 Pct Recovery = 57% Analysis Date = 05/14/16 Pct Recovery = 58% Analysis Date = 05/14/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/10/16 Pct Recovery = 58% Analysis Date = 05/10/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/05/16 Pct Recovery = 58% Analysis Date = 05/05/16 Pct Recovery = 58% Analysis Date = 05/03/16 Pct Recovery = 58% Analysis Date = 05/03/16 Pct Recovery = 58% Analysis Date = 05/01/16 Pct Recovery = 58% Analysis Date = 05/01/16 Pct Recovery = 58% Analysis Date = 04/28/16 Pct Recovery = 58% Analysis Date = 04/28/16 Pct Recovery = 58% Analysis Date = 04/26/16 Pct Recovery = 58% Analysis Date = 04/26/16 Pct Recovery = 58% Analysis Date = 04/24/16 Pct Recovery = 58% Analysis Date = 04/24/16 Pct Recovery = 58% Analysis Date = 04/22/16 Pct Recovery = 58% Analysis Date = 04/22/16 Pct Recovery = 58% Analysis Date = 04/19/16 Pct Recovery = 58% Analysis Date = 04/19/16 Pct Recovery = 58% Analysis Date = 04/17/16 Pct Recovery = 58% Analysis Date = 04/17/16 Pct Recovery = 58% Analysis Date = 04/15/16 Pct Recovery = 59% Analysis Date = 04/15/16 Pct Recovery = 59% Analysis Date = 04/12/16 Pct Recovery = 59% Analysis Date = 04/12/16 Pct Recovery = 59% Analysis Date = 04/10/16 Pct Recovery = 59% Analysis Date = 04/10/16 Pct Recovery = 59% Analysis Date = 04/08/16 Pct Recovery = 59% Analysis Date = 04/08/16 Pct Recovery = 59% Analysis Date = 04/06/16 Pct Recovery = 59% Analysis Date = 04/06/16 Pct Recovery = 59% Analysis Date = 04/03/16 Pct Recovery = 59% Analysis Date = 04/03/16 Pct Recovery = 59% Analysis Date = 04/01/16 Pct Recovery = 59% Analysis Date = 04/01/16 Pct Recovery = 59% Analysis Date = 03/30/16 Pct Recovery = 58% Analysis Date = 03/30/16 Pct Recovery = 58% Analysis Date = 03/27/16 Pct Recovery = 58% Analysis Date = 03/27/16 Pct Recovery = 58% Analysis Date = 03/25/16 Pct Recovery = 58% Analysis Date = 03/25/16 Pct Recovery = 58% Analysis Date = 03/23/16 Pct Recovery = 58% Analysis Date = 03/23/16 Pct Recovery = 58% Analysis Date = 03/21/16 Pct Recovery = 58% Analysis Date = 03/21/16 Pct Recovery = 58% Analysis Date = 03/18/16 Pct Recovery = 58% Analysis Date = 03/18/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/16/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/14/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/11/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 58% Analysis Date = 03/09/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/07/16 Pct Recovery = 58% Analysis Date = 03/05/16 Pct Recovery = 58% Analysis Date = 03/05/16 Pct Recovery = 58% Analysis Date = 03/02/16 Pct Recovery = 58% Analysis Date = 03/02/16 Pct Recovery = 58% Analysis Date = 02/29/16 Pct Recovery = 57% Analysis Date = 02/29/16 Pct Recovery = 57% Analysis Date = 02/27/16 Pct Recovery = 57% Analysis Date = 02/27/16 Pct Recovery = 57% Analysis Date = 02/24/16 Pct Recovery = 57% Analysis Date = 02/24/16 Pct Recovery = 57% Analysis Date = 02/22/16 Pct Recovery = 57% Analysis Date = 02/22/16 Pct Recovery = 57% Analysis Date = 02/20/16 Pct Recovery = 57% Analysis Date = 02/20/16 Pct Recovery = 57% Analysis Date = 02/18/16 Pct Recovery = 57% Analysis Date = 02/18/16 Pct Recovery = 57% Analysis Date = 02/15/16 Pct Recovery = 57% Analysis Date = 02/15/16 Pct Recovery = 57% Analysis Date = 02/13/16 Pct Recovery = 57% Analysis Date = 02/13/16 Pct Recovery = 57% Analysis Date = 02/11/16 Pct Recovery = 56% Analysis Date = 02/11/16 Pct Recovery = 56% Analysis Date = 02/09/16 Pct Recovery = 56% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DEETHYLATRAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 53% 13% 55% 8%
Total 18 53% 13% 55% 8%

Sample Statistics
DEETHYLATRAZINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
DESULFINYLFIPRONIL
METHOD: 2033 , TESTIDCODE: 62170GCM29

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 100% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 135% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 102% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 93% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 78% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 73% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 85% Analysis Date = 05/10/17 Pct Recovery = 98% Analysis Date = 05/08/17 Pct Recovery = 98% Analysis Date = 05/08/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 98% Analysis Date = 05/04/17 Pct Recovery = 98% Analysis Date = 05/04/17 Pct Recovery = 98% Analysis Date = 05/01/17 Pct Recovery = 97% Analysis Date = 05/01/17 Pct Recovery = 97% Analysis Date = 04/29/17 Pct Recovery = 97% Analysis Date = 04/29/17 Pct Recovery = 97% Analysis Date = 04/27/17 Pct Recovery = 97% Analysis Date = 04/27/17 Pct Recovery = 97% Analysis Date = 04/25/17 Pct Recovery = 96% Analysis Date = 04/25/17 Pct Recovery = 96% Analysis Date = 04/22/17 Pct Recovery = 96% Analysis Date = 04/22/17 Pct Recovery = 96% Analysis Date = 04/20/17 Pct Recovery = 96% Analysis Date = 04/20/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/13/17 Pct Recovery = 95% Analysis Date = 04/13/17 Pct Recovery = 95% Analysis Date = 04/11/17 Pct Recovery = 95% Analysis Date = 04/11/17 Pct Recovery = 95% Analysis Date = 04/09/17 Pct Recovery = 95% Analysis Date = 04/09/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 94% Analysis Date = 04/06/17 Pct Recovery = 94% Analysis Date = 04/04/17 Pct Recovery = 94% Analysis Date = 04/04/17 Pct Recovery = 94% Analysis Date = 04/02/17 Pct Recovery = 94% Analysis Date = 04/02/17 Pct Recovery = 94% Analysis Date = 03/30/17 Pct Recovery = 94% Analysis Date = 03/30/17 Pct Recovery = 94% Analysis Date = 03/28/17 Pct Recovery = 93% Analysis Date = 03/28/17 Pct Recovery = 93% Analysis Date = 03/26/17 Pct Recovery = 93% Analysis Date = 03/26/17 Pct Recovery = 93% Analysis Date = 03/24/17 Pct Recovery = 93% Analysis Date = 03/24/17 Pct Recovery = 93% Analysis Date = 03/21/17 Pct Recovery = 93% Analysis Date = 03/21/17 Pct Recovery = 93% Analysis Date = 03/19/17 Pct Recovery = 92% Analysis Date = 03/19/17 Pct Recovery = 92% Analysis Date = 03/17/17 Pct Recovery = 92% Analysis Date = 03/17/17 Pct Recovery = 92% Analysis Date = 03/14/17 Pct Recovery = 92% Analysis Date = 03/14/17 Pct Recovery = 92% Analysis Date = 03/12/17 Pct Recovery = 92% Analysis Date = 03/12/17 Pct Recovery = 92% Analysis Date = 03/10/17 Pct Recovery = 91% Analysis Date = 03/10/17 Pct Recovery = 91% Analysis Date = 03/08/17 Pct Recovery = 91% Analysis Date = 03/08/17 Pct Recovery = 91% Analysis Date = 03/05/17 Pct Recovery = 91% Analysis Date = 03/05/17 Pct Recovery = 91% Analysis Date = 03/03/17 Pct Recovery = 91% Analysis Date = 03/03/17 Pct Recovery = 91% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 90% Analysis Date = 02/08/17 Pct Recovery = 90% Analysis Date = 02/08/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/28/17 Pct Recovery = 91% Analysis Date = 01/28/17 Pct Recovery = 91% Analysis Date = 01/25/17 Pct Recovery = 91% Analysis Date = 01/25/17 Pct Recovery = 91% Analysis Date = 01/23/17 Pct Recovery = 91% Analysis Date = 01/23/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/19/17 Pct Recovery = 91% Analysis Date = 01/19/17 Pct Recovery = 91% Analysis Date = 01/16/17 Pct Recovery = 91% Analysis Date = 01/16/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/12/17 Pct Recovery = 91% Analysis Date = 01/12/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/05/17 Pct Recovery = 91% Analysis Date = 01/05/17 Pct Recovery = 91% Analysis Date = 01/03/17 Pct Recovery = 91% Analysis Date = 01/03/17 Pct Recovery = 91% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/29/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/27/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 92% Analysis Date = 12/24/16 Pct Recovery = 92% Analysis Date = 12/22/16 Pct Recovery = 92% Analysis Date = 12/22/16 Pct Recovery = 92% Analysis Date = 12/20/16 Pct Recovery = 92% Analysis Date = 12/20/16 Pct Recovery = 92% Analysis Date = 12/18/16 Pct Recovery = 92% Analysis Date = 12/18/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/08/16 Pct Recovery = 92% Analysis Date = 12/08/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 93% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 93% Analysis Date = 11/29/16 Pct Recovery = 93% Analysis Date = 11/29/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 93% Analysis Date = 11/22/16 Pct Recovery = 93% Analysis Date = 11/22/16 Pct Recovery = 93% Analysis Date = 11/20/16 Pct Recovery = 93% Analysis Date = 11/20/16 Pct Recovery = 93% Analysis Date = 11/18/16 Pct Recovery = 93% Analysis Date = 11/18/16 Pct Recovery = 93% Analysis Date = 11/16/16 Pct Recovery = 93% Analysis Date = 11/16/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/13/16 Pct Recovery = 93% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 10/31/16 Pct Recovery = 94% Analysis Date = 10/31/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 94% Analysis Date = 10/26/16 Pct Recovery = 94% Analysis Date = 10/26/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/21/16 Pct Recovery = 94% Analysis Date = 10/21/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/17/16 Pct Recovery = 94% Analysis Date = 10/17/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 95% Analysis Date = 10/15/16 Pct Recovery = 95% Analysis Date = 10/12/16 Pct Recovery = 95% Analysis Date = 10/12/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/08/16 Pct Recovery = 95% Analysis Date = 10/08/16 Pct Recovery = 95% Analysis Date = 10/05/16 Pct Recovery = 95% Analysis Date = 10/05/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 95% Analysis Date = 09/29/16 Pct Recovery = 95% Analysis Date = 09/29/16 Pct Recovery = 95% Analysis Date = 09/26/16 Pct Recovery = 95% Analysis Date = 09/26/16 Pct Recovery = 95% Analysis Date = 09/24/16 Pct Recovery = 95% Analysis Date = 09/24/16 Pct Recovery = 95% Analysis Date = 09/22/16 Pct Recovery = 95% Analysis Date = 09/22/16 Pct Recovery = 95% Analysis Date = 09/19/16 Pct Recovery = 95% Analysis Date = 09/19/16 Pct Recovery = 95% Analysis Date = 09/17/16 Pct Recovery = 95% Analysis Date = 09/17/16 Pct Recovery = 95% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/03/16 Pct Recovery = 92% Analysis Date = 09/03/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 90% Analysis Date = 08/28/16 Pct Recovery = 90% Analysis Date = 08/25/16 Pct Recovery = 90% Analysis Date = 08/25/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/13/16 Pct Recovery = 82% Analysis Date = 07/13/16 Pct Recovery = 82% Analysis Date = 07/11/16 Pct Recovery = 82% Analysis Date = 07/11/16 Pct Recovery = 82% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 81% Analysis Date = 07/04/16 Pct Recovery = 81% Analysis Date = 07/04/16 Pct Recovery = 81% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 06/29/16 Pct Recovery = 80% Analysis Date = 06/29/16 Pct Recovery = 80% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/25/16 Pct Recovery = 79% Analysis Date = 06/25/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/20/16 Pct Recovery = 78% Analysis Date = 06/20/16 Pct Recovery = 78% Analysis Date = 06/18/16 Pct Recovery = 78% Analysis Date = 06/18/16 Pct Recovery = 78% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 77% Analysis Date = 06/11/16 Pct Recovery = 76% Analysis Date = 06/11/16 Pct Recovery = 76% Analysis Date = 06/09/16 Pct Recovery = 76% Analysis Date = 06/09/16 Pct Recovery = 76% Analysis Date = 06/06/16 Pct Recovery = 76% Analysis Date = 06/06/16 Pct Recovery = 76% Analysis Date = 06/04/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 75% Analysis Date = 06/02/16 Pct Recovery = 75% Analysis Date = 06/02/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/26/16 Pct Recovery = 74% Analysis Date = 05/26/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/19/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/17/16 Pct Recovery = 72% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 75% Analysis Date = 04/19/16 Pct Recovery = 76% Analysis Date = 04/19/16 Pct Recovery = 76% Analysis Date = 04/17/16 Pct Recovery = 76% Analysis Date = 04/17/16 Pct Recovery = 76% Analysis Date = 04/15/16 Pct Recovery = 76% Analysis Date = 04/15/16 Pct Recovery = 76% Analysis Date = 04/12/16 Pct Recovery = 76% Analysis Date = 04/12/16 Pct Recovery = 76% Analysis Date = 04/10/16 Pct Recovery = 77% Analysis Date = 04/10/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 77% Analysis Date = 04/06/16 Pct Recovery = 77% Analysis Date = 04/06/16 Pct Recovery = 77% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 78% Analysis Date = 03/30/16 Pct Recovery = 78% Analysis Date = 03/30/16 Pct Recovery = 78% Analysis Date = 03/27/16 Pct Recovery = 78% Analysis Date = 03/27/16 Pct Recovery = 78% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/18/16 Pct Recovery = 80% Analysis Date = 03/18/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/11/16 Pct Recovery = 80% Analysis Date = 03/11/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/05/16 Pct Recovery = 81% Analysis Date = 03/05/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 82% Analysis Date = 02/29/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/27/16 Pct Recovery = 82% Analysis Date = 02/24/16 Pct Recovery = 82% Analysis Date = 02/24/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/22/16 Pct Recovery = 83% Analysis Date = 02/20/16 Pct Recovery = 83% Analysis Date = 02/20/16 Pct Recovery = 83% Analysis Date = 02/18/16 Pct Recovery = 83% Analysis Date = 02/18/16 Pct Recovery = 83% Analysis Date = 02/15/16 Pct Recovery = 83% Analysis Date = 02/15/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/09/16 Pct Recovery = 84% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 85% 19% 82% 15%
Total 13 85% 19% 82% 15%

Sample Statistics
DESULFINYLFIPRONIL

Characteristic N % % Basis
Plotted 13 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 13 .  
False Negatives 0 0% 0 out of 13
Not Spiked 15 .  
False Positives 0 0% 0 out of 15

OBSP Determination:
DESULFINYLFIPRONIL AMIDE
METHOD: 2033 , TESTIDCODE: 62169GCM29

Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 11% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DESULFINYLFIPRONIL AMIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 1 11% . 11% 0%
Total 1 11% . 11% 0%

Sample Statistics
DESULFINYLFIPRONIL AMIDE

Characteristic N % % Basis
Plotted 1 50% Spiked
Estimated Values 1 50% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 2 .  
False Negatives 1 50% 1 out of 2
Not Spiked 26 .  
False Positives 0 0% 0 out of 26

OBSP Determination:
DIAZINON
METHOD: 2033 , TESTIDCODE: 39572GCM35

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 97% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 95% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 95% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 97% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 92% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 93% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 106% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 95% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 111% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 96% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 89% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 105% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 98% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 91% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 100% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 91% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 104% Analysis Date = 05/10/17 Pct Recovery = 101% Analysis Date = 05/08/17 Pct Recovery = 101% Analysis Date = 05/08/17 Pct Recovery = 101% Analysis Date = 05/06/17 Pct Recovery = 101% Analysis Date = 05/06/17 Pct Recovery = 101% Analysis Date = 05/04/17 Pct Recovery = 101% Analysis Date = 05/04/17 Pct Recovery = 101% Analysis Date = 05/01/17 Pct Recovery = 101% Analysis Date = 05/01/17 Pct Recovery = 101% Analysis Date = 04/29/17 Pct Recovery = 101% Analysis Date = 04/29/17 Pct Recovery = 101% Analysis Date = 04/27/17 Pct Recovery = 101% Analysis Date = 04/27/17 Pct Recovery = 101% Analysis Date = 04/25/17 Pct Recovery = 101% Analysis Date = 04/25/17 Pct Recovery = 101% Analysis Date = 04/22/17 Pct Recovery = 100% Analysis Date = 04/22/17 Pct Recovery = 100% Analysis Date = 04/20/17 Pct Recovery = 100% Analysis Date = 04/20/17 Pct Recovery = 100% Analysis Date = 04/18/17 Pct Recovery = 100% Analysis Date = 04/18/17 Pct Recovery = 100% Analysis Date = 04/15/17 Pct Recovery = 100% Analysis Date = 04/15/17 Pct Recovery = 100% Analysis Date = 04/13/17 Pct Recovery = 100% Analysis Date = 04/13/17 Pct Recovery = 100% Analysis Date = 04/11/17 Pct Recovery = 100% Analysis Date = 04/11/17 Pct Recovery = 100% Analysis Date = 04/09/17 Pct Recovery = 100% Analysis Date = 04/09/17 Pct Recovery = 100% Analysis Date = 04/06/17 Pct Recovery = 100% Analysis Date = 04/06/17 Pct Recovery = 100% Analysis Date = 04/04/17 Pct Recovery = 100% Analysis Date = 04/04/17 Pct Recovery = 100% Analysis Date = 04/02/17 Pct Recovery = 100% Analysis Date = 04/02/17 Pct Recovery = 100% Analysis Date = 03/30/17 Pct Recovery = 100% Analysis Date = 03/30/17 Pct Recovery = 100% Analysis Date = 03/28/17 Pct Recovery = 99% Analysis Date = 03/28/17 Pct Recovery = 99% Analysis Date = 03/26/17 Pct Recovery = 99% Analysis Date = 03/26/17 Pct Recovery = 99% Analysis Date = 03/24/17 Pct Recovery = 99% Analysis Date = 03/24/17 Pct Recovery = 99% Analysis Date = 03/21/17 Pct Recovery = 99% Analysis Date = 03/21/17 Pct Recovery = 99% Analysis Date = 03/19/17 Pct Recovery = 99% Analysis Date = 03/19/17 Pct Recovery = 99% Analysis Date = 03/17/17 Pct Recovery = 99% Analysis Date = 03/17/17 Pct Recovery = 99% Analysis Date = 03/14/17 Pct Recovery = 99% Analysis Date = 03/14/17 Pct Recovery = 99% Analysis Date = 03/12/17 Pct Recovery = 99% Analysis Date = 03/12/17 Pct Recovery = 99% Analysis Date = 03/10/17 Pct Recovery = 99% Analysis Date = 03/10/17 Pct Recovery = 99% Analysis Date = 03/08/17 Pct Recovery = 99% Analysis Date = 03/08/17 Pct Recovery = 99% Analysis Date = 03/05/17 Pct Recovery = 99% Analysis Date = 03/05/17 Pct Recovery = 99% Analysis Date = 03/03/17 Pct Recovery = 98% Analysis Date = 03/03/17 Pct Recovery = 98% Analysis Date = 03/01/17 Pct Recovery = 98% Analysis Date = 03/01/17 Pct Recovery = 98% Analysis Date = 02/26/17 Pct Recovery = 98% Analysis Date = 02/26/17 Pct Recovery = 98% Analysis Date = 02/24/17 Pct Recovery = 98% Analysis Date = 02/24/17 Pct Recovery = 98% Analysis Date = 02/22/17 Pct Recovery = 98% Analysis Date = 02/22/17 Pct Recovery = 98% Analysis Date = 02/20/17 Pct Recovery = 98% Analysis Date = 02/20/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/10/17 Pct Recovery = 98% Analysis Date = 02/10/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/01/17 Pct Recovery = 98% Analysis Date = 02/01/17 Pct Recovery = 98% Analysis Date = 01/30/17 Pct Recovery = 98% Analysis Date = 01/30/17 Pct Recovery = 98% Analysis Date = 01/28/17 Pct Recovery = 98% Analysis Date = 01/28/17 Pct Recovery = 98% Analysis Date = 01/25/17 Pct Recovery = 98% Analysis Date = 01/25/17 Pct Recovery = 98% Analysis Date = 01/23/17 Pct Recovery = 98% Analysis Date = 01/23/17 Pct Recovery = 98% Analysis Date = 01/21/17 Pct Recovery = 98% Analysis Date = 01/21/17 Pct Recovery = 98% Analysis Date = 01/19/17 Pct Recovery = 98% Analysis Date = 01/19/17 Pct Recovery = 98% Analysis Date = 01/16/17 Pct Recovery = 98% Analysis Date = 01/16/17 Pct Recovery = 98% Analysis Date = 01/14/17 Pct Recovery = 98% Analysis Date = 01/14/17 Pct Recovery = 98% Analysis Date = 01/12/17 Pct Recovery = 98% Analysis Date = 01/12/17 Pct Recovery = 98% Analysis Date = 01/09/17 Pct Recovery = 98% Analysis Date = 01/09/17 Pct Recovery = 98% Analysis Date = 01/07/17 Pct Recovery = 98% Analysis Date = 01/07/17 Pct Recovery = 98% Analysis Date = 01/05/17 Pct Recovery = 98% Analysis Date = 01/05/17 Pct Recovery = 98% Analysis Date = 01/03/17 Pct Recovery = 98% Analysis Date = 01/03/17 Pct Recovery = 98% Analysis Date = 12/31/16 Pct Recovery = 98% Analysis Date = 12/31/16 Pct Recovery = 98% Analysis Date = 12/29/16 Pct Recovery = 98% Analysis Date = 12/29/16 Pct Recovery = 98% Analysis Date = 12/27/16 Pct Recovery = 98% Analysis Date = 12/27/16 Pct Recovery = 98% Analysis Date = 12/24/16 Pct Recovery = 98% Analysis Date = 12/24/16 Pct Recovery = 98% Analysis Date = 12/22/16 Pct Recovery = 98% Analysis Date = 12/22/16 Pct Recovery = 98% Analysis Date = 12/20/16 Pct Recovery = 98% Analysis Date = 12/20/16 Pct Recovery = 98% Analysis Date = 12/18/16 Pct Recovery = 99% Analysis Date = 12/18/16 Pct Recovery = 99% Analysis Date = 12/15/16 Pct Recovery = 99% Analysis Date = 12/15/16 Pct Recovery = 99% Analysis Date = 12/13/16 Pct Recovery = 99% Analysis Date = 12/13/16 Pct Recovery = 99% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/08/16 Pct Recovery = 99% Analysis Date = 12/08/16 Pct Recovery = 99% Analysis Date = 12/06/16 Pct Recovery = 99% Analysis Date = 12/06/16 Pct Recovery = 99% Analysis Date = 12/04/16 Pct Recovery = 99% Analysis Date = 12/04/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 11/29/16 Pct Recovery = 99% Analysis Date = 11/29/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/25/16 Pct Recovery = 100% Analysis Date = 11/25/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 100% Analysis Date = 11/20/16 Pct Recovery = 100% Analysis Date = 11/20/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/18/16 Pct Recovery = 100% Analysis Date = 11/16/16 Pct Recovery = 100% Analysis Date = 11/16/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/13/16 Pct Recovery = 100% Analysis Date = 11/11/16 Pct Recovery = 100% Analysis Date = 11/11/16 Pct Recovery = 100% Analysis Date = 11/09/16 Pct Recovery = 100% Analysis Date = 11/09/16 Pct Recovery = 100% Analysis Date = 11/06/16 Pct Recovery = 101% Analysis Date = 11/06/16 Pct Recovery = 101% Analysis Date = 11/04/16 Pct Recovery = 101% Analysis Date = 11/04/16 Pct Recovery = 101% Analysis Date = 11/02/16 Pct Recovery = 101% Analysis Date = 11/02/16 Pct Recovery = 101% Analysis Date = 10/31/16 Pct Recovery = 101% Analysis Date = 10/31/16 Pct Recovery = 101% Analysis Date = 10/28/16 Pct Recovery = 101% Analysis Date = 10/28/16 Pct Recovery = 101% Analysis Date = 10/26/16 Pct Recovery = 101% Analysis Date = 10/26/16 Pct Recovery = 101% Analysis Date = 10/24/16 Pct Recovery = 101% Analysis Date = 10/24/16 Pct Recovery = 101% Analysis Date = 10/21/16 Pct Recovery = 101% Analysis Date = 10/21/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/17/16 Pct Recovery = 102% Analysis Date = 10/17/16 Pct Recovery = 102% Analysis Date = 10/15/16 Pct Recovery = 102% Analysis Date = 10/15/16 Pct Recovery = 102% Analysis Date = 10/12/16 Pct Recovery = 102% Analysis Date = 10/12/16 Pct Recovery = 102% Analysis Date = 10/10/16 Pct Recovery = 102% Analysis Date = 10/10/16 Pct Recovery = 102% Analysis Date = 10/08/16 Pct Recovery = 102% Analysis Date = 10/08/16 Pct Recovery = 102% Analysis Date = 10/05/16 Pct Recovery = 102% Analysis Date = 10/05/16 Pct Recovery = 102% Analysis Date = 10/03/16 Pct Recovery = 102% Analysis Date = 10/03/16 Pct Recovery = 102% Analysis Date = 10/01/16 Pct Recovery = 102% Analysis Date = 10/01/16 Pct Recovery = 102% Analysis Date = 09/29/16 Pct Recovery = 102% Analysis Date = 09/29/16 Pct Recovery = 102% Analysis Date = 09/26/16 Pct Recovery = 103% Analysis Date = 09/26/16 Pct Recovery = 103% Analysis Date = 09/24/16 Pct Recovery = 103% Analysis Date = 09/24/16 Pct Recovery = 103% Analysis Date = 09/22/16 Pct Recovery = 103% Analysis Date = 09/22/16 Pct Recovery = 103% Analysis Date = 09/19/16 Pct Recovery = 103% Analysis Date = 09/19/16 Pct Recovery = 103% Analysis Date = 09/17/16 Pct Recovery = 103% Analysis Date = 09/17/16 Pct Recovery = 103% Analysis Date = 09/15/16 Pct Recovery = 103% Analysis Date = 09/15/16 Pct Recovery = 103% Analysis Date = 09/13/16 Pct Recovery = 103% Analysis Date = 09/13/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/08/16 Pct Recovery = 103% Analysis Date = 09/08/16 Pct Recovery = 103% Analysis Date = 09/06/16 Pct Recovery = 103% Analysis Date = 09/06/16 Pct Recovery = 103% Analysis Date = 09/03/16 Pct Recovery = 103% Analysis Date = 09/03/16 Pct Recovery = 103% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 09/01/16 Pct Recovery = 104% Analysis Date = 08/30/16 Pct Recovery = 103% Analysis Date = 08/30/16 Pct Recovery = 103% Analysis Date = 08/28/16 Pct Recovery = 103% Analysis Date = 08/28/16 Pct Recovery = 103% Analysis Date = 08/25/16 Pct Recovery = 103% Analysis Date = 08/25/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 103% Analysis Date = 08/21/16 Pct Recovery = 103% Analysis Date = 08/21/16 Pct Recovery = 103% Analysis Date = 08/18/16 Pct Recovery = 103% Analysis Date = 08/18/16 Pct Recovery = 103% Analysis Date = 08/16/16 Pct Recovery = 102% Analysis Date = 08/16/16 Pct Recovery = 102% Analysis Date = 08/14/16 Pct Recovery = 102% Analysis Date = 08/14/16 Pct Recovery = 102% Analysis Date = 08/12/16 Pct Recovery = 102% Analysis Date = 08/12/16 Pct Recovery = 102% Analysis Date = 08/09/16 Pct Recovery = 102% Analysis Date = 08/09/16 Pct Recovery = 102% Analysis Date = 08/07/16 Pct Recovery = 102% Analysis Date = 08/07/16 Pct Recovery = 102% Analysis Date = 08/05/16 Pct Recovery = 102% Analysis Date = 08/05/16 Pct Recovery = 102% Analysis Date = 08/02/16 Pct Recovery = 101% Analysis Date = 08/02/16 Pct Recovery = 101% Analysis Date = 07/31/16 Pct Recovery = 101% Analysis Date = 07/31/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 101% Analysis Date = 07/29/16 Pct Recovery = 101% Analysis Date = 07/27/16 Pct Recovery = 101% Analysis Date = 07/27/16 Pct Recovery = 101% Analysis Date = 07/24/16 Pct Recovery = 101% Analysis Date = 07/24/16 Pct Recovery = 101% Analysis Date = 07/22/16 Pct Recovery = 101% Analysis Date = 07/22/16 Pct Recovery = 101% Analysis Date = 07/20/16 Pct Recovery = 100% Analysis Date = 07/20/16 Pct Recovery = 100% Analysis Date = 07/17/16 Pct Recovery = 100% Analysis Date = 07/17/16 Pct Recovery = 100% Analysis Date = 07/15/16 Pct Recovery = 100% Analysis Date = 07/15/16 Pct Recovery = 100% Analysis Date = 07/13/16 Pct Recovery = 100% Analysis Date = 07/13/16 Pct Recovery = 100% Analysis Date = 07/11/16 Pct Recovery = 100% Analysis Date = 07/11/16 Pct Recovery = 100% Analysis Date = 07/08/16 Pct Recovery = 100% Analysis Date = 07/08/16 Pct Recovery = 100% Analysis Date = 07/06/16 Pct Recovery = 99% Analysis Date = 07/06/16 Pct Recovery = 99% Analysis Date = 07/04/16 Pct Recovery = 99% Analysis Date = 07/04/16 Pct Recovery = 99% Analysis Date = 07/01/16 Pct Recovery = 99% Analysis Date = 07/01/16 Pct Recovery = 99% Analysis Date = 06/29/16 Pct Recovery = 99% Analysis Date = 06/29/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/25/16 Pct Recovery = 99% Analysis Date = 06/25/16 Pct Recovery = 99% Analysis Date = 06/22/16 Pct Recovery = 98% Analysis Date = 06/22/16 Pct Recovery = 98% Analysis Date = 06/20/16 Pct Recovery = 98% Analysis Date = 06/20/16 Pct Recovery = 98% Analysis Date = 06/18/16 Pct Recovery = 98% Analysis Date = 06/18/16 Pct Recovery = 98% Analysis Date = 06/15/16 Pct Recovery = 98% Analysis Date = 06/15/16 Pct Recovery = 98% Analysis Date = 06/13/16 Pct Recovery = 98% Analysis Date = 06/13/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/09/16 Pct Recovery = 97% Analysis Date = 06/09/16 Pct Recovery = 97% Analysis Date = 06/06/16 Pct Recovery = 97% Analysis Date = 06/06/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 06/04/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 06/02/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 97% Analysis Date = 05/30/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/26/16 Pct Recovery = 96% Analysis Date = 05/26/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/21/16 Pct Recovery = 96% Analysis Date = 05/21/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/17/16 Pct Recovery = 96% Analysis Date = 05/17/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/12/16 Pct Recovery = 96% Analysis Date = 05/12/16 Pct Recovery = 96% Analysis Date = 05/10/16 Pct Recovery = 96% Analysis Date = 05/10/16 Pct Recovery = 96% Analysis Date = 05/08/16 Pct Recovery = 96% Analysis Date = 05/08/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/03/16 Pct Recovery = 96% Analysis Date = 05/03/16 Pct Recovery = 96% Analysis Date = 05/01/16 Pct Recovery = 97% Analysis Date = 05/01/16 Pct Recovery = 97% Analysis Date = 04/28/16 Pct Recovery = 97% Analysis Date = 04/28/16 Pct Recovery = 97% Analysis Date = 04/26/16 Pct Recovery = 97% Analysis Date = 04/26/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/22/16 Pct Recovery = 97% Analysis Date = 04/22/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 97% Analysis Date = 04/19/16 Pct Recovery = 97% Analysis Date = 04/17/16 Pct Recovery = 97% Analysis Date = 04/17/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/12/16 Pct Recovery = 98% Analysis Date = 04/12/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/08/16 Pct Recovery = 98% Analysis Date = 04/08/16 Pct Recovery = 98% Analysis Date = 04/06/16 Pct Recovery = 98% Analysis Date = 04/06/16 Pct Recovery = 98% Analysis Date = 04/03/16 Pct Recovery = 98% Analysis Date = 04/03/16 Pct Recovery = 98% Analysis Date = 04/01/16 Pct Recovery = 98% Analysis Date = 04/01/16 Pct Recovery = 98% Analysis Date = 03/30/16 Pct Recovery = 98% Analysis Date = 03/30/16 Pct Recovery = 98% Analysis Date = 03/27/16 Pct Recovery = 99% Analysis Date = 03/27/16 Pct Recovery = 99% Analysis Date = 03/25/16 Pct Recovery = 99% Analysis Date = 03/25/16 Pct Recovery = 99% Analysis Date = 03/23/16 Pct Recovery = 99% Analysis Date = 03/23/16 Pct Recovery = 99% Analysis Date = 03/21/16 Pct Recovery = 99% Analysis Date = 03/21/16 Pct Recovery = 99% Analysis Date = 03/18/16 Pct Recovery = 99% Analysis Date = 03/18/16 Pct Recovery = 99% Analysis Date = 03/16/16 Pct Recovery = 99% Analysis Date = 03/16/16 Pct Recovery = 99% Analysis Date = 03/14/16 Pct Recovery = 100% Analysis Date = 03/14/16 Pct Recovery = 100% Analysis Date = 03/11/16 Pct Recovery = 100% Analysis Date = 03/11/16 Pct Recovery = 100% Analysis Date = 03/09/16 Pct Recovery = 100% Analysis Date = 03/09/16 Pct Recovery = 100% Analysis Date = 03/07/16 Pct Recovery = 100% Analysis Date = 03/07/16 Pct Recovery = 100% Analysis Date = 03/05/16 Pct Recovery = 100% Analysis Date = 03/05/16 Pct Recovery = 100% Analysis Date = 03/02/16 Pct Recovery = 100% Analysis Date = 03/02/16 Pct Recovery = 100% Analysis Date = 02/29/16 Pct Recovery = 101% Analysis Date = 02/29/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/27/16 Pct Recovery = 101% Analysis Date = 02/24/16 Pct Recovery = 101% Analysis Date = 02/24/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/20/16 Pct Recovery = 101% Analysis Date = 02/20/16 Pct Recovery = 101% Analysis Date = 02/18/16 Pct Recovery = 101% Analysis Date = 02/18/16 Pct Recovery = 101% Analysis Date = 02/15/16 Pct Recovery = 102% Analysis Date = 02/15/16 Pct Recovery = 102% Analysis Date = 02/13/16 Pct Recovery = 102% Analysis Date = 02/13/16 Pct Recovery = 102% Analysis Date = 02/11/16 Pct Recovery = 102% Analysis Date = 02/11/16 Pct Recovery = 102% Analysis Date = 02/09/16 Pct Recovery = 102% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 99% 8% 97% 8%
Total 20 99% 8% 97% 8%

Sample Statistics
DIAZINON

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
DIAZINON, OXYGEN ANALOG
METHOD: 2033 , TESTIDCODE: 61638GCM14

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 122% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 124% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 120% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 96% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 101% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 102% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 119% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 152% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 102% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 106% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 112% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 182% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 125% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 144% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 132% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 95% Analysis Date = 05/02/17 Pct Recovery = 121% Analysis Date = 04/30/17 Pct Recovery = 121% Analysis Date = 04/30/17 Pct Recovery = 121% Analysis Date = 04/28/17 Pct Recovery = 121% Analysis Date = 04/28/17 Pct Recovery = 121% Analysis Date = 04/26/17 Pct Recovery = 122% Analysis Date = 04/26/17 Pct Recovery = 122% Analysis Date = 04/24/17 Pct Recovery = 122% Analysis Date = 04/24/17 Pct Recovery = 122% Analysis Date = 04/21/17 Pct Recovery = 122% Analysis Date = 04/21/17 Pct Recovery = 122% Analysis Date = 04/19/17 Pct Recovery = 123% Analysis Date = 04/19/17 Pct Recovery = 123% Analysis Date = 04/17/17 Pct Recovery = 123% Analysis Date = 04/17/17 Pct Recovery = 123% Analysis Date = 04/15/17 Pct Recovery = 123% Analysis Date = 04/15/17 Pct Recovery = 123% Analysis Date = 04/12/17 Pct Recovery = 123% Analysis Date = 04/12/17 Pct Recovery = 123% Analysis Date = 04/10/17 Pct Recovery = 124% Analysis Date = 04/10/17 Pct Recovery = 124% Analysis Date = 04/08/17 Pct Recovery = 124% Analysis Date = 04/08/17 Pct Recovery = 124% Analysis Date = 04/06/17 Pct Recovery = 124% Analysis Date = 04/06/17 Pct Recovery = 124% Analysis Date = 04/03/17 Pct Recovery = 124% Analysis Date = 04/03/17 Pct Recovery = 124% Analysis Date = 04/01/17 Pct Recovery = 125% Analysis Date = 04/01/17 Pct Recovery = 125% Analysis Date = 03/30/17 Pct Recovery = 125% Analysis Date = 03/30/17 Pct Recovery = 125% Analysis Date = 03/28/17 Pct Recovery = 125% Analysis Date = 03/28/17 Pct Recovery = 125% Analysis Date = 03/25/17 Pct Recovery = 126% Analysis Date = 03/25/17 Pct Recovery = 126% Analysis Date = 03/23/17 Pct Recovery = 126% Analysis Date = 03/23/17 Pct Recovery = 126% Analysis Date = 03/21/17 Pct Recovery = 126% Analysis Date = 03/21/17 Pct Recovery = 126% Analysis Date = 03/19/17 Pct Recovery = 126% Analysis Date = 03/19/17 Pct Recovery = 126% Analysis Date = 03/16/17 Pct Recovery = 127% Analysis Date = 03/16/17 Pct Recovery = 127% Analysis Date = 03/14/17 Pct Recovery = 127% Analysis Date = 03/14/17 Pct Recovery = 127% Analysis Date = 03/12/17 Pct Recovery = 127% Analysis Date = 03/12/17 Pct Recovery = 127% Analysis Date = 03/10/17 Pct Recovery = 128% Analysis Date = 03/10/17 Pct Recovery = 128% Analysis Date = 03/07/17 Pct Recovery = 128% Analysis Date = 03/07/17 Pct Recovery = 128% Analysis Date = 03/05/17 Pct Recovery = 128% Analysis Date = 03/05/17 Pct Recovery = 128% Analysis Date = 03/03/17 Pct Recovery = 128% Analysis Date = 03/03/17 Pct Recovery = 128% Analysis Date = 03/01/17 Pct Recovery = 129% Analysis Date = 03/01/17 Pct Recovery = 129% Analysis Date = 02/26/17 Pct Recovery = 129% Analysis Date = 02/26/17 Pct Recovery = 129% Analysis Date = 02/24/17 Pct Recovery = 129% Analysis Date = 02/24/17 Pct Recovery = 129% Analysis Date = 02/22/17 Pct Recovery = 130% Analysis Date = 02/22/17 Pct Recovery = 130% Analysis Date = 02/20/17 Pct Recovery = 130% Analysis Date = 02/20/17 Pct Recovery = 130% Analysis Date = 02/17/17 Pct Recovery = 130% Analysis Date = 02/17/17 Pct Recovery = 130% Analysis Date = 02/15/17 Pct Recovery = 130% Analysis Date = 02/15/17 Pct Recovery = 130% Analysis Date = 02/13/17 Pct Recovery = 131% Analysis Date = 02/13/17 Pct Recovery = 131% Analysis Date = 02/11/17 Pct Recovery = 131% Analysis Date = 02/11/17 Pct Recovery = 131% Analysis Date = 02/08/17 Pct Recovery = 131% Analysis Date = 02/08/17 Pct Recovery = 131% Analysis Date = 02/06/17 Pct Recovery = 131% Analysis Date = 02/06/17 Pct Recovery = 131% Analysis Date = 02/04/17 Pct Recovery = 132% Analysis Date = 02/04/17 Pct Recovery = 132% Analysis Date = 02/02/17 Pct Recovery = 132% Analysis Date = 02/02/17 Pct Recovery = 132% Analysis Date = 01/30/17 Pct Recovery = 132% Analysis Date = 01/30/17 Pct Recovery = 132% Analysis Date = 01/28/17 Pct Recovery = 132% Analysis Date = 01/28/17 Pct Recovery = 132% Analysis Date = 01/26/17 Pct Recovery = 133% Analysis Date = 01/26/17 Pct Recovery = 133% Analysis Date = 01/24/17 Pct Recovery = 133% Analysis Date = 01/24/17 Pct Recovery = 133% Analysis Date = 01/21/17 Pct Recovery = 133% Analysis Date = 01/21/17 Pct Recovery = 133% Analysis Date = 01/19/17 Pct Recovery = 133% Analysis Date = 01/19/17 Pct Recovery = 133% Analysis Date = 01/17/17 Pct Recovery = 133% Analysis Date = 01/17/17 Pct Recovery = 133% Analysis Date = 01/15/17 Pct Recovery = 134% Analysis Date = 01/15/17 Pct Recovery = 134% Analysis Date = 01/12/17 Pct Recovery = 134% Analysis Date = 01/12/17 Pct Recovery = 134% Analysis Date = 01/10/17 Pct Recovery = 134% Analysis Date = 01/10/17 Pct Recovery = 134% Analysis Date = 01/08/17 Pct Recovery = 134% Analysis Date = 01/08/17 Pct Recovery = 134% Analysis Date = 01/06/17 Pct Recovery = 135% Analysis Date = 01/06/17 Pct Recovery = 135% Analysis Date = 01/04/17 Pct Recovery = 135% Analysis Date = 01/04/17 Pct Recovery = 135% Analysis Date = 01/01/17 Pct Recovery = 135% Analysis Date = 01/01/17 Pct Recovery = 135% Analysis Date = 12/30/16 Pct Recovery = 135% Analysis Date = 12/30/16 Pct Recovery = 135% Analysis Date = 12/28/16 Pct Recovery = 136% Analysis Date = 12/28/16 Pct Recovery = 136% Analysis Date = 12/26/16 Pct Recovery = 136% Analysis Date = 12/26/16 Pct Recovery = 136% Analysis Date = 12/23/16 Pct Recovery = 136% Analysis Date = 12/23/16 Pct Recovery = 136% Analysis Date = 12/21/16 Pct Recovery = 136% Analysis Date = 12/21/16 Pct Recovery = 136% Analysis Date = 12/19/16 Pct Recovery = 136% Analysis Date = 12/19/16 Pct Recovery = 136% Analysis Date = 12/17/16 Pct Recovery = 136% Analysis Date = 12/17/16 Pct Recovery = 136% Analysis Date = 12/14/16 Pct Recovery = 136% Analysis Date = 12/14/16 Pct Recovery = 136% Analysis Date = 12/12/16 Pct Recovery = 135% Analysis Date = 12/12/16 Pct Recovery = 135% Analysis Date = 12/10/16 Pct Recovery = 135% Analysis Date = 12/10/16 Pct Recovery = 135% Analysis Date = 12/08/16 Pct Recovery = 135% Analysis Date = 12/08/16 Pct Recovery = 135% Analysis Date = 12/05/16 Pct Recovery = 135% Analysis Date = 12/05/16 Pct Recovery = 135% Analysis Date = 12/03/16 Pct Recovery = 134% Analysis Date = 12/03/16 Pct Recovery = 134% Analysis Date = 12/01/16 Pct Recovery = 134% Analysis Date = 12/01/16 Pct Recovery = 134% Analysis Date = 11/29/16 Pct Recovery = 134% Analysis Date = 11/29/16 Pct Recovery = 134% Analysis Date = 11/26/16 Pct Recovery = 134% Analysis Date = 11/26/16 Pct Recovery = 134% Analysis Date = 11/24/16 Pct Recovery = 133% Analysis Date = 11/24/16 Pct Recovery = 133% Analysis Date = 11/22/16 Pct Recovery = 133% Analysis Date = 11/22/16 Pct Recovery = 133% Analysis Date = 11/20/16 Pct Recovery = 133% Analysis Date = 11/20/16 Pct Recovery = 133% Analysis Date = 11/17/16 Pct Recovery = 132% Analysis Date = 11/17/16 Pct Recovery = 132% Analysis Date = 11/15/16 Pct Recovery = 132% Analysis Date = 11/15/16 Pct Recovery = 132% Analysis Date = 11/13/16 Pct Recovery = 132% Analysis Date = 11/13/16 Pct Recovery = 132% Analysis Date = 11/11/16 Pct Recovery = 132% Analysis Date = 11/11/16 Pct Recovery = 132% Analysis Date = 11/08/16 Pct Recovery = 131% Analysis Date = 11/08/16 Pct Recovery = 131% Analysis Date = 11/06/16 Pct Recovery = 131% Analysis Date = 11/06/16 Pct Recovery = 131% Analysis Date = 11/04/16 Pct Recovery = 131% Analysis Date = 11/04/16 Pct Recovery = 131% Analysis Date = 11/02/16 Pct Recovery = 131% Analysis Date = 11/02/16 Pct Recovery = 131% Analysis Date = 10/30/16 Pct Recovery = 130% Analysis Date = 10/30/16 Pct Recovery = 130% Analysis Date = 10/28/16 Pct Recovery = 130% Analysis Date = 10/28/16 Pct Recovery = 130% Analysis Date = 10/26/16 Pct Recovery = 130% Analysis Date = 10/26/16 Pct Recovery = 130% Analysis Date = 10/24/16 Pct Recovery = 129% Analysis Date = 10/24/16 Pct Recovery = 129% Analysis Date = 10/21/16 Pct Recovery = 129% Analysis Date = 10/21/16 Pct Recovery = 129% Analysis Date = 10/19/16 Pct Recovery = 129% Analysis Date = 10/19/16 Pct Recovery = 129% Analysis Date = 10/17/16 Pct Recovery = 129% Analysis Date = 10/17/16 Pct Recovery = 129% Analysis Date = 10/15/16 Pct Recovery = 128% Analysis Date = 10/15/16 Pct Recovery = 128% Analysis Date = 10/12/16 Pct Recovery = 128% Analysis Date = 10/12/16 Pct Recovery = 128% Analysis Date = 10/10/16 Pct Recovery = 128% Analysis Date = 10/10/16 Pct Recovery = 128% Analysis Date = 10/08/16 Pct Recovery = 128% Analysis Date = 10/08/16 Pct Recovery = 128% Analysis Date = 10/06/16 Pct Recovery = 127% Analysis Date = 10/06/16 Pct Recovery = 127% Analysis Date = 10/03/16 Pct Recovery = 127% Analysis Date = 10/03/16 Pct Recovery = 127% Analysis Date = 10/01/16 Pct Recovery = 127% Analysis Date = 10/01/16 Pct Recovery = 127% Analysis Date = 09/29/16 Pct Recovery = 126% Analysis Date = 09/29/16 Pct Recovery = 126% Analysis Date = 09/27/16 Pct Recovery = 126% Analysis Date = 09/27/16 Pct Recovery = 126% Analysis Date = 09/24/16 Pct Recovery = 126% Analysis Date = 09/24/16 Pct Recovery = 126% Analysis Date = 09/22/16 Pct Recovery = 126% Analysis Date = 09/22/16 Pct Recovery = 126% Analysis Date = 09/20/16 Pct Recovery = 125% Analysis Date = 09/20/16 Pct Recovery = 125% Analysis Date = 09/18/16 Pct Recovery = 125% Analysis Date = 09/18/16 Pct Recovery = 125% Analysis Date = 09/16/16 Pct Recovery = 125% Analysis Date = 09/16/16 Pct Recovery = 125% Analysis Date = 09/13/16 Pct Recovery = 125% Analysis Date = 09/13/16 Pct Recovery = 125% Analysis Date = 09/11/16 Pct Recovery = 124% Analysis Date = 09/11/16 Pct Recovery = 124% Analysis Date = 09/09/16 Pct Recovery = 124% Analysis Date = 09/09/16 Pct Recovery = 124% Analysis Date = 09/07/16 Pct Recovery = 124% Analysis Date = 09/07/16 Pct Recovery = 124% Analysis Date = 09/04/16 Pct Recovery = 123% Analysis Date = 09/04/16 Pct Recovery = 123% Analysis Date = 09/02/16 Pct Recovery = 123% Analysis Date = 09/02/16 Pct Recovery = 123% Analysis Date = 08/31/16 Pct Recovery = 123% Analysis Date = 08/31/16 Pct Recovery = 123% Analysis Date = 08/29/16 Pct Recovery = 123% Analysis Date = 08/29/16 Pct Recovery = 123% Analysis Date = 08/26/16 Pct Recovery = 122% Analysis Date = 08/26/16 Pct Recovery = 122% Analysis Date = 08/24/16 Pct Recovery = 122% Analysis Date = 08/24/16 Pct Recovery = 122% Analysis Date = 08/22/16 Pct Recovery = 122% Analysis Date = 08/22/16 Pct Recovery = 122% Analysis Date = 08/20/16 Pct Recovery = 121% Analysis Date = 08/20/16 Pct Recovery = 121% Analysis Date = 08/17/16 Pct Recovery = 121% Analysis Date = 08/17/16 Pct Recovery = 121% Analysis Date = 08/15/16 Pct Recovery = 121% Analysis Date = 08/15/16 Pct Recovery = 121% Analysis Date = 08/13/16 Pct Recovery = 120% Analysis Date = 08/13/16 Pct Recovery = 120% Analysis Date = 08/11/16 Pct Recovery = 120% Analysis Date = 08/11/16 Pct Recovery = 120% Analysis Date = 08/08/16 Pct Recovery = 120% Analysis Date = 08/08/16 Pct Recovery = 120% Analysis Date = 08/06/16 Pct Recovery = 120% Analysis Date = 08/06/16 Pct Recovery = 120% Analysis Date = 08/04/16 Pct Recovery = 119% Analysis Date = 08/04/16 Pct Recovery = 119% Analysis Date = 08/02/16 Pct Recovery = 119% Analysis Date = 08/02/16 Pct Recovery = 119% Analysis Date = 07/30/16 Pct Recovery = 119% Analysis Date = 07/30/16 Pct Recovery = 119% Analysis Date = 07/28/16 Pct Recovery = 118% Analysis Date = 07/28/16 Pct Recovery = 118% Analysis Date = 07/26/16 Pct Recovery = 118% Analysis Date = 07/26/16 Pct Recovery = 118% Analysis Date = 07/24/16 Pct Recovery = 118% Analysis Date = 07/24/16 Pct Recovery = 118% Analysis Date = 07/21/16 Pct Recovery = 118% Analysis Date = 07/21/16 Pct Recovery = 118% Analysis Date = 07/19/16 Pct Recovery = 117% Analysis Date = 07/19/16 Pct Recovery = 117% Analysis Date = 07/17/16 Pct Recovery = 117% Analysis Date = 07/17/16 Pct Recovery = 117% Analysis Date = 07/15/16 Pct Recovery = 117% Analysis Date = 07/15/16 Pct Recovery = 117% Analysis Date = 07/12/16 Pct Recovery = 116% Analysis Date = 07/12/16 Pct Recovery = 116% Analysis Date = 07/10/16 Pct Recovery = 116% Analysis Date = 07/10/16 Pct Recovery = 116% Analysis Date = 07/08/16 Pct Recovery = 116% Analysis Date = 07/08/16 Pct Recovery = 116% Analysis Date = 07/06/16 Pct Recovery = 115% Analysis Date = 07/06/16 Pct Recovery = 115% Analysis Date = 07/03/16 Pct Recovery = 115% Analysis Date = 07/03/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 06/29/16 Pct Recovery = 115% Analysis Date = 06/29/16 Pct Recovery = 115% Analysis Date = 06/27/16 Pct Recovery = 114% Analysis Date = 06/27/16 Pct Recovery = 114% Analysis Date = 06/24/16 Pct Recovery = 114% Analysis Date = 06/24/16 Pct Recovery = 114% Analysis Date = 06/22/16 Pct Recovery = 114% Analysis Date = 06/22/16 Pct Recovery = 114% Analysis Date = 06/20/16 Pct Recovery = 113% Analysis Date = 06/20/16 Pct Recovery = 113% Analysis Date = 06/18/16 Pct Recovery = 113% Analysis Date = 06/18/16 Pct Recovery = 113% Analysis Date = 06/15/16 Pct Recovery = 113% Analysis Date = 06/15/16 Pct Recovery = 113% Analysis Date = 06/13/16 Pct Recovery = 112% Analysis Date = 06/13/16 Pct Recovery = 112% Analysis Date = 06/11/16 Pct Recovery = 112% Analysis Date = 06/11/16 Pct Recovery = 112% Analysis Date = 06/09/16 Pct Recovery = 112% Analysis Date = 06/09/16 Pct Recovery = 112% Analysis Date = 06/06/16 Pct Recovery = 112% Analysis Date = 06/06/16 Pct Recovery = 112% Analysis Date = 06/04/16 Pct Recovery = 111% Analysis Date = 06/04/16 Pct Recovery = 111% Analysis Date = 06/02/16 Pct Recovery = 111% Analysis Date = 06/02/16 Pct Recovery = 111% Analysis Date = 05/31/16 Pct Recovery = 111% Analysis Date = 05/31/16 Pct Recovery = 111% Analysis Date = 05/29/16 Pct Recovery = 110% Analysis Date = 05/29/16 Pct Recovery = 110% Analysis Date = 05/26/16 Pct Recovery = 110% Analysis Date = 05/26/16 Pct Recovery = 110% Analysis Date = 05/24/16 Pct Recovery = 110% Analysis Date = 05/24/16 Pct Recovery = 110% Analysis Date = 05/22/16 Pct Recovery = 110% Analysis Date = 05/22/16 Pct Recovery = 110% Analysis Date = 05/20/16 Pct Recovery = 109% Analysis Date = 05/20/16 Pct Recovery = 109% Analysis Date = 05/17/16 Pct Recovery = 109% Analysis Date = 05/17/16 Pct Recovery = 109% Analysis Date = 05/15/16 Pct Recovery = 109% Analysis Date = 05/15/16 Pct Recovery = 109% Analysis Date = 05/13/16 Pct Recovery = 109% Analysis Date = 05/13/16 Pct Recovery = 109% Analysis Date = 05/11/16 Pct Recovery = 108% Analysis Date = 05/11/16 Pct Recovery = 108% Analysis Date = 05/08/16 Pct Recovery = 108% Analysis Date = 05/08/16 Pct Recovery = 108% Analysis Date = 05/06/16 Pct Recovery = 108% Analysis Date = 05/06/16 Pct Recovery = 108% Analysis Date = 05/04/16 Pct Recovery = 108% Analysis Date = 05/04/16 Pct Recovery = 108% Analysis Date = 05/02/16 Pct Recovery = 107% Analysis Date = 05/02/16 Pct Recovery = 107% Analysis Date = 04/29/16 Pct Recovery = 107% Analysis Date = 04/29/16 Pct Recovery = 107% Analysis Date = 04/27/16 Pct Recovery = 107% Analysis Date = 04/27/16 Pct Recovery = 107% Analysis Date = 04/25/16 Pct Recovery = 106% Analysis Date = 04/25/16 Pct Recovery = 106% Analysis Date = 04/23/16 Pct Recovery = 106% Analysis Date = 04/23/16 Pct Recovery = 106% Analysis Date = 04/20/16 Pct Recovery = 106% Analysis Date = 04/20/16 Pct Recovery = 106% Analysis Date = 04/18/16 Pct Recovery = 105% Analysis Date = 04/18/16 Pct Recovery = 105% Analysis Date = 04/16/16 Pct Recovery = 105% Analysis Date = 04/16/16 Pct Recovery = 105% Analysis Date = 04/14/16 Pct Recovery = 104% Analysis Date = 04/14/16 Pct Recovery = 104% Analysis Date = 04/11/16 Pct Recovery = 104% Analysis Date = 04/11/16 Pct Recovery = 104% Analysis Date = 04/09/16 Pct Recovery = 104% Analysis Date = 04/09/16 Pct Recovery = 104% Analysis Date = 04/07/16 Pct Recovery = 103% Analysis Date = 04/07/16 Pct Recovery = 103% Analysis Date = 04/05/16 Pct Recovery = 103% Analysis Date = 04/05/16 Pct Recovery = 103% Analysis Date = 04/02/16 Pct Recovery = 103% Analysis Date = 04/02/16 Pct Recovery = 103% Analysis Date = 03/31/16 Pct Recovery = 102% Analysis Date = 03/31/16 Pct Recovery = 102% Analysis Date = 03/29/16 Pct Recovery = 102% Analysis Date = 03/29/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 101% Analysis Date = 03/27/16 Pct Recovery = 101% Analysis Date = 03/24/16 Pct Recovery = 101% Analysis Date = 03/24/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/22/16 Pct Recovery = 101% Analysis Date = 03/20/16 Pct Recovery = 100% Analysis Date = 03/20/16 Pct Recovery = 100% Analysis Date = 03/18/16 Pct Recovery = 100% Analysis Date = 03/18/16 Pct Recovery = 100% Analysis Date = 03/15/16 Pct Recovery = 99% Analysis Date = 03/15/16 Pct Recovery = 99% Analysis Date = 03/13/16 Pct Recovery = 99% Analysis Date = 03/13/16 Pct Recovery = 99% Analysis Date = 03/11/16 Pct Recovery = 99% Analysis Date = 03/11/16 Pct Recovery = 99% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/06/16 Pct Recovery = 98% Analysis Date = 03/06/16 Pct Recovery = 98% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 03/04/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 96% Analysis Date = 02/29/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 96% Analysis Date = 02/26/16 Pct Recovery = 96% Analysis Date = 02/24/16 Pct Recovery = 96% Analysis Date = 02/24/16 Pct Recovery = 96% Analysis Date = 02/22/16 Pct Recovery = 95% Analysis Date = 02/22/16 Pct Recovery = 95% Analysis Date = 02/20/16 Pct Recovery = 95% Analysis Date = 02/20/16 Pct Recovery = 95% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 93% Analysis Date = 02/13/16 Pct Recovery = 93% Analysis Date = 02/11/16 Pct Recovery = 93% Analysis Date = 02/11/16 Pct Recovery = 93% Analysis Date = 02/09/16 Pct Recovery = 93% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIAZINON, OXYGEN ANALOG

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 118% 23% 116% 17%
Total 18 118% 23% 116% 17%

Sample Statistics
DIAZINON, OXYGEN ANALOG

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 3 17% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
DICHLOROVOS (DICHLORVOS)
METHOD: 2033 , TESTIDCODE: 38775GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 49% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 32% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 26% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 43% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 26% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 47% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 86% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 122% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 40% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 45% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 43% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 23% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 18% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 33% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 30% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 18% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 25% Analysis Date = 05/02/17 Pct Recovery = 60% Analysis Date = 04/30/17 Pct Recovery = 60% Analysis Date = 04/30/17 Pct Recovery = 60% Analysis Date = 04/28/17 Pct Recovery = 60% Analysis Date = 04/28/17 Pct Recovery = 60% Analysis Date = 04/26/17 Pct Recovery = 60% Analysis Date = 04/26/17 Pct Recovery = 60% Analysis Date = 04/24/17 Pct Recovery = 59% Analysis Date = 04/24/17 Pct Recovery = 59% Analysis Date = 04/21/17 Pct Recovery = 59% Analysis Date = 04/21/17 Pct Recovery = 59% Analysis Date = 04/19/17 Pct Recovery = 59% Analysis Date = 04/19/17 Pct Recovery = 59% Analysis Date = 04/17/17 Pct Recovery = 59% Analysis Date = 04/17/17 Pct Recovery = 59% Analysis Date = 04/15/17 Pct Recovery = 59% Analysis Date = 04/15/17 Pct Recovery = 59% Analysis Date = 04/12/17 Pct Recovery = 59% Analysis Date = 04/12/17 Pct Recovery = 59% Analysis Date = 04/10/17 Pct Recovery = 59% Analysis Date = 04/10/17 Pct Recovery = 59% Analysis Date = 04/08/17 Pct Recovery = 59% Analysis Date = 04/08/17 Pct Recovery = 59% Analysis Date = 04/06/17 Pct Recovery = 58% Analysis Date = 04/06/17 Pct Recovery = 58% Analysis Date = 04/03/17 Pct Recovery = 58% Analysis Date = 04/03/17 Pct Recovery = 58% Analysis Date = 04/01/17 Pct Recovery = 58% Analysis Date = 04/01/17 Pct Recovery = 58% Analysis Date = 03/30/17 Pct Recovery = 58% Analysis Date = 03/30/17 Pct Recovery = 58% Analysis Date = 03/28/17 Pct Recovery = 58% Analysis Date = 03/28/17 Pct Recovery = 58% Analysis Date = 03/25/17 Pct Recovery = 58% Analysis Date = 03/25/17 Pct Recovery = 58% Analysis Date = 03/23/17 Pct Recovery = 58% Analysis Date = 03/23/17 Pct Recovery = 58% Analysis Date = 03/21/17 Pct Recovery = 57% Analysis Date = 03/21/17 Pct Recovery = 57% Analysis Date = 03/19/17 Pct Recovery = 57% Analysis Date = 03/19/17 Pct Recovery = 57% Analysis Date = 03/16/17 Pct Recovery = 57% Analysis Date = 03/16/17 Pct Recovery = 57% Analysis Date = 03/14/17 Pct Recovery = 57% Analysis Date = 03/14/17 Pct Recovery = 57% Analysis Date = 03/12/17 Pct Recovery = 57% Analysis Date = 03/12/17 Pct Recovery = 57% Analysis Date = 03/10/17 Pct Recovery = 57% Analysis Date = 03/10/17 Pct Recovery = 57% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 56% Analysis Date = 03/03/17 Pct Recovery = 56% Analysis Date = 03/03/17 Pct Recovery = 56% Analysis Date = 03/01/17 Pct Recovery = 56% Analysis Date = 03/01/17 Pct Recovery = 56% Analysis Date = 02/26/17 Pct Recovery = 56% Analysis Date = 02/26/17 Pct Recovery = 56% Analysis Date = 02/24/17 Pct Recovery = 55% Analysis Date = 02/24/17 Pct Recovery = 55% Analysis Date = 02/22/17 Pct Recovery = 55% Analysis Date = 02/22/17 Pct Recovery = 55% Analysis Date = 02/20/17 Pct Recovery = 55% Analysis Date = 02/20/17 Pct Recovery = 55% Analysis Date = 02/17/17 Pct Recovery = 55% Analysis Date = 02/17/17 Pct Recovery = 55% Analysis Date = 02/15/17 Pct Recovery = 54% Analysis Date = 02/15/17 Pct Recovery = 54% Analysis Date = 02/13/17 Pct Recovery = 54% Analysis Date = 02/13/17 Pct Recovery = 54% Analysis Date = 02/11/17 Pct Recovery = 53% Analysis Date = 02/11/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/08/17 Pct Recovery = 53% Analysis Date = 02/06/17 Pct Recovery = 52% Analysis Date = 02/06/17 Pct Recovery = 52% Analysis Date = 02/04/17 Pct Recovery = 52% Analysis Date = 02/04/17 Pct Recovery = 52% Analysis Date = 02/02/17 Pct Recovery = 51% Analysis Date = 02/02/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/30/17 Pct Recovery = 51% Analysis Date = 01/28/17 Pct Recovery = 50% Analysis Date = 01/28/17 Pct Recovery = 50% Analysis Date = 01/26/17 Pct Recovery = 50% Analysis Date = 01/26/17 Pct Recovery = 50% Analysis Date = 01/24/17 Pct Recovery = 49% Analysis Date = 01/24/17 Pct Recovery = 49% Analysis Date = 01/21/17 Pct Recovery = 49% Analysis Date = 01/21/17 Pct Recovery = 49% Analysis Date = 01/19/17 Pct Recovery = 48% Analysis Date = 01/19/17 Pct Recovery = 48% Analysis Date = 01/17/17 Pct Recovery = 48% Analysis Date = 01/17/17 Pct Recovery = 48% Analysis Date = 01/15/17 Pct Recovery = 47% Analysis Date = 01/15/17 Pct Recovery = 47% Analysis Date = 01/12/17 Pct Recovery = 47% Analysis Date = 01/12/17 Pct Recovery = 47% Analysis Date = 01/10/17 Pct Recovery = 46% Analysis Date = 01/10/17 Pct Recovery = 46% Analysis Date = 01/08/17 Pct Recovery = 46% Analysis Date = 01/08/17 Pct Recovery = 46% Analysis Date = 01/06/17 Pct Recovery = 45% Analysis Date = 01/06/17 Pct Recovery = 45% Analysis Date = 01/04/17 Pct Recovery = 45% Analysis Date = 01/04/17 Pct Recovery = 45% Analysis Date = 01/01/17 Pct Recovery = 44% Analysis Date = 01/01/17 Pct Recovery = 44% Analysis Date = 12/30/16 Pct Recovery = 44% Analysis Date = 12/30/16 Pct Recovery = 44% Analysis Date = 12/28/16 Pct Recovery = 43% Analysis Date = 12/28/16 Pct Recovery = 43% Analysis Date = 12/26/16 Pct Recovery = 43% Analysis Date = 12/26/16 Pct Recovery = 43% Analysis Date = 12/23/16 Pct Recovery = 42% Analysis Date = 12/23/16 Pct Recovery = 42% Analysis Date = 12/21/16 Pct Recovery = 42% Analysis Date = 12/21/16 Pct Recovery = 42% Analysis Date = 12/19/16 Pct Recovery = 41% Analysis Date = 12/19/16 Pct Recovery = 41% Analysis Date = 12/17/16 Pct Recovery = 41% Analysis Date = 12/17/16 Pct Recovery = 41% Analysis Date = 12/14/16 Pct Recovery = 41% Analysis Date = 12/14/16 Pct Recovery = 41% Analysis Date = 12/12/16 Pct Recovery = 41% Analysis Date = 12/12/16 Pct Recovery = 41% Analysis Date = 12/10/16 Pct Recovery = 41% Analysis Date = 12/10/16 Pct Recovery = 41% Analysis Date = 12/08/16 Pct Recovery = 41% Analysis Date = 12/08/16 Pct Recovery = 41% Analysis Date = 12/05/16 Pct Recovery = 42% Analysis Date = 12/05/16 Pct Recovery = 42% Analysis Date = 12/03/16 Pct Recovery = 42% Analysis Date = 12/03/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 12/01/16 Pct Recovery = 42% Analysis Date = 11/29/16 Pct Recovery = 42% Analysis Date = 11/29/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/26/16 Pct Recovery = 42% Analysis Date = 11/24/16 Pct Recovery = 42% Analysis Date = 11/24/16 Pct Recovery = 42% Analysis Date = 11/22/16 Pct Recovery = 42% Analysis Date = 11/22/16 Pct Recovery = 42% Analysis Date = 11/20/16 Pct Recovery = 42% Analysis Date = 11/20/16 Pct Recovery = 42% Analysis Date = 11/17/16 Pct Recovery = 42% Analysis Date = 11/17/16 Pct Recovery = 42% Analysis Date = 11/15/16 Pct Recovery = 42% Analysis Date = 11/15/16 Pct Recovery = 42% Analysis Date = 11/13/16 Pct Recovery = 42% Analysis Date = 11/13/16 Pct Recovery = 42% Analysis Date = 11/11/16 Pct Recovery = 42% Analysis Date = 11/11/16 Pct Recovery = 42% Analysis Date = 11/08/16 Pct Recovery = 42% Analysis Date = 11/08/16 Pct Recovery = 42% Analysis Date = 11/06/16 Pct Recovery = 42% Analysis Date = 11/06/16 Pct Recovery = 42% Analysis Date = 11/04/16 Pct Recovery = 42% Analysis Date = 11/04/16 Pct Recovery = 42% Analysis Date = 11/02/16 Pct Recovery = 42% Analysis Date = 11/02/16 Pct Recovery = 42% Analysis Date = 10/30/16 Pct Recovery = 42% Analysis Date = 10/30/16 Pct Recovery = 42% Analysis Date = 10/28/16 Pct Recovery = 42% Analysis Date = 10/28/16 Pct Recovery = 42% Analysis Date = 10/26/16 Pct Recovery = 43% Analysis Date = 10/26/16 Pct Recovery = 43% Analysis Date = 10/24/16 Pct Recovery = 43% Analysis Date = 10/24/16 Pct Recovery = 43% Analysis Date = 10/21/16 Pct Recovery = 43% Analysis Date = 10/21/16 Pct Recovery = 43% Analysis Date = 10/19/16 Pct Recovery = 43% Analysis Date = 10/19/16 Pct Recovery = 43% Analysis Date = 10/17/16 Pct Recovery = 43% Analysis Date = 10/17/16 Pct Recovery = 43% Analysis Date = 10/15/16 Pct Recovery = 43% Analysis Date = 10/15/16 Pct Recovery = 43% Analysis Date = 10/12/16 Pct Recovery = 43% Analysis Date = 10/12/16 Pct Recovery = 43% Analysis Date = 10/10/16 Pct Recovery = 43% Analysis Date = 10/10/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/08/16 Pct Recovery = 43% Analysis Date = 10/06/16 Pct Recovery = 43% Analysis Date = 10/06/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 10/03/16 Pct Recovery = 43% Analysis Date = 10/01/16 Pct Recovery = 43% Analysis Date = 10/01/16 Pct Recovery = 43% Analysis Date = 09/29/16 Pct Recovery = 43% Analysis Date = 09/29/16 Pct Recovery = 43% Analysis Date = 09/27/16 Pct Recovery = 43% Analysis Date = 09/27/16 Pct Recovery = 43% Analysis Date = 09/24/16 Pct Recovery = 43% Analysis Date = 09/24/16 Pct Recovery = 43% Analysis Date = 09/22/16 Pct Recovery = 43% Analysis Date = 09/22/16 Pct Recovery = 43% Analysis Date = 09/20/16 Pct Recovery = 43% Analysis Date = 09/20/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/18/16 Pct Recovery = 43% Analysis Date = 09/16/16 Pct Recovery = 44% Analysis Date = 09/16/16 Pct Recovery = 44% Analysis Date = 09/13/16 Pct Recovery = 44% Analysis Date = 09/13/16 Pct Recovery = 44% Analysis Date = 09/11/16 Pct Recovery = 44% Analysis Date = 09/11/16 Pct Recovery = 44% Analysis Date = 09/09/16 Pct Recovery = 44% Analysis Date = 09/09/16 Pct Recovery = 44% Analysis Date = 09/07/16 Pct Recovery = 44% Analysis Date = 09/07/16 Pct Recovery = 44% Analysis Date = 09/04/16 Pct Recovery = 44% Analysis Date = 09/04/16 Pct Recovery = 44% Analysis Date = 09/02/16 Pct Recovery = 44% Analysis Date = 09/02/16 Pct Recovery = 44% Analysis Date = 08/31/16 Pct Recovery = 44% Analysis Date = 08/31/16 Pct Recovery = 44% Analysis Date = 08/29/16 Pct Recovery = 43% Analysis Date = 08/29/16 Pct Recovery = 43% Analysis Date = 08/26/16 Pct Recovery = 43% Analysis Date = 08/26/16 Pct Recovery = 43% Analysis Date = 08/24/16 Pct Recovery = 43% Analysis Date = 08/24/16 Pct Recovery = 43% Analysis Date = 08/22/16 Pct Recovery = 42% Analysis Date = 08/22/16 Pct Recovery = 42% Analysis Date = 08/20/16 Pct Recovery = 42% Analysis Date = 08/20/16 Pct Recovery = 42% Analysis Date = 08/17/16 Pct Recovery = 41% Analysis Date = 08/17/16 Pct Recovery = 41% Analysis Date = 08/15/16 Pct Recovery = 41% Analysis Date = 08/15/16 Pct Recovery = 41% Analysis Date = 08/13/16 Pct Recovery = 41% Analysis Date = 08/13/16 Pct Recovery = 41% Analysis Date = 08/11/16 Pct Recovery = 40% Analysis Date = 08/11/16 Pct Recovery = 40% Analysis Date = 08/08/16 Pct Recovery = 40% Analysis Date = 08/08/16 Pct Recovery = 40% Analysis Date = 08/06/16 Pct Recovery = 39% Analysis Date = 08/06/16 Pct Recovery = 39% Analysis Date = 08/04/16 Pct Recovery = 39% Analysis Date = 08/04/16 Pct Recovery = 39% Analysis Date = 08/02/16 Pct Recovery = 39% Analysis Date = 08/02/16 Pct Recovery = 39% Analysis Date = 07/30/16 Pct Recovery = 38% Analysis Date = 07/30/16 Pct Recovery = 38% Analysis Date = 07/28/16 Pct Recovery = 38% Analysis Date = 07/28/16 Pct Recovery = 38% Analysis Date = 07/26/16 Pct Recovery = 37% Analysis Date = 07/26/16 Pct Recovery = 37% Analysis Date = 07/24/16 Pct Recovery = 37% Analysis Date = 07/24/16 Pct Recovery = 37% Analysis Date = 07/21/16 Pct Recovery = 36% Analysis Date = 07/21/16 Pct Recovery = 36% Analysis Date = 07/19/16 Pct Recovery = 36% Analysis Date = 07/19/16 Pct Recovery = 36% Analysis Date = 07/17/16 Pct Recovery = 36% Analysis Date = 07/17/16 Pct Recovery = 36% Analysis Date = 07/15/16 Pct Recovery = 35% Analysis Date = 07/15/16 Pct Recovery = 35% Analysis Date = 07/12/16 Pct Recovery = 35% Analysis Date = 07/12/16 Pct Recovery = 35% Analysis Date = 07/10/16 Pct Recovery = 34% Analysis Date = 07/10/16 Pct Recovery = 34% Analysis Date = 07/08/16 Pct Recovery = 34% Analysis Date = 07/08/16 Pct Recovery = 34% Analysis Date = 07/06/16 Pct Recovery = 34% Analysis Date = 07/06/16 Pct Recovery = 34% Analysis Date = 07/03/16 Pct Recovery = 33% Analysis Date = 07/03/16 Pct Recovery = 33% Analysis Date = 07/01/16 Pct Recovery = 33% Analysis Date = 07/01/16 Pct Recovery = 33% Analysis Date = 06/29/16 Pct Recovery = 32% Analysis Date = 06/29/16 Pct Recovery = 32% Analysis Date = 06/27/16 Pct Recovery = 32% Analysis Date = 06/27/16 Pct Recovery = 32% Analysis Date = 06/24/16 Pct Recovery = 32% Analysis Date = 06/24/16 Pct Recovery = 32% Analysis Date = 06/22/16 Pct Recovery = 31% Analysis Date = 06/22/16 Pct Recovery = 31% Analysis Date = 06/20/16 Pct Recovery = 31% Analysis Date = 06/20/16 Pct Recovery = 31% Analysis Date = 06/18/16 Pct Recovery = 30% Analysis Date = 06/18/16 Pct Recovery = 30% Analysis Date = 06/15/16 Pct Recovery = 30% Analysis Date = 06/15/16 Pct Recovery = 30% Analysis Date = 06/13/16 Pct Recovery = 30% Analysis Date = 06/13/16 Pct Recovery = 30% Analysis Date = 06/11/16 Pct Recovery = 29% Analysis Date = 06/11/16 Pct Recovery = 29% Analysis Date = 06/09/16 Pct Recovery = 29% Analysis Date = 06/09/16 Pct Recovery = 29% Analysis Date = 06/06/16 Pct Recovery = 28% Analysis Date = 06/06/16 Pct Recovery = 28% Analysis Date = 06/04/16 Pct Recovery = 28% Analysis Date = 06/04/16 Pct Recovery = 28% Analysis Date = 06/02/16 Pct Recovery = 28% Analysis Date = 06/02/16 Pct Recovery = 28% Analysis Date = 05/31/16 Pct Recovery = 27% Analysis Date = 05/31/16 Pct Recovery = 27% Analysis Date = 05/29/16 Pct Recovery = 27% Analysis Date = 05/29/16 Pct Recovery = 27% Analysis Date = 05/26/16 Pct Recovery = 27% Analysis Date = 05/26/16 Pct Recovery = 27% Analysis Date = 05/24/16 Pct Recovery = 27% Analysis Date = 05/24/16 Pct Recovery = 27% Analysis Date = 05/22/16 Pct Recovery = 26% Analysis Date = 05/22/16 Pct Recovery = 26% Analysis Date = 05/20/16 Pct Recovery = 26% Analysis Date = 05/20/16 Pct Recovery = 26% Analysis Date = 05/17/16 Pct Recovery = 26% Analysis Date = 05/17/16 Pct Recovery = 26% Analysis Date = 05/15/16 Pct Recovery = 26% Analysis Date = 05/15/16 Pct Recovery = 26% Analysis Date = 05/13/16 Pct Recovery = 26% Analysis Date = 05/13/16 Pct Recovery = 26% Analysis Date = 05/11/16 Pct Recovery = 26% Analysis Date = 05/11/16 Pct Recovery = 26% Analysis Date = 05/08/16 Pct Recovery = 26% Analysis Date = 05/08/16 Pct Recovery = 26% Analysis Date = 05/06/16 Pct Recovery = 26% Analysis Date = 05/06/16 Pct Recovery = 26% Analysis Date = 05/04/16 Pct Recovery = 26% Analysis Date = 05/04/16 Pct Recovery = 26% Analysis Date = 05/02/16 Pct Recovery = 26% Analysis Date = 05/02/16 Pct Recovery = 26% Analysis Date = 04/29/16 Pct Recovery = 26% Analysis Date = 04/29/16 Pct Recovery = 26% Analysis Date = 04/27/16 Pct Recovery = 25% Analysis Date = 04/27/16 Pct Recovery = 25% Analysis Date = 04/25/16 Pct Recovery = 25% Analysis Date = 04/25/16 Pct Recovery = 25% Analysis Date = 04/23/16 Pct Recovery = 25% Analysis Date = 04/23/16 Pct Recovery = 25% Analysis Date = 04/20/16 Pct Recovery = 25% Analysis Date = 04/20/16 Pct Recovery = 25% Analysis Date = 04/18/16 Pct Recovery = 25% Analysis Date = 04/18/16 Pct Recovery = 25% Analysis Date = 04/16/16 Pct Recovery = 25% Analysis Date = 04/16/16 Pct Recovery = 25% Analysis Date = 04/14/16 Pct Recovery = 25% Analysis Date = 04/14/16 Pct Recovery = 25% Analysis Date = 04/11/16 Pct Recovery = 25% Analysis Date = 04/11/16 Pct Recovery = 25% Analysis Date = 04/09/16 Pct Recovery = 25% Analysis Date = 04/09/16 Pct Recovery = 25% Analysis Date = 04/07/16 Pct Recovery = 25% Analysis Date = 04/07/16 Pct Recovery = 25% Analysis Date = 04/05/16 Pct Recovery = 25% Analysis Date = 04/05/16 Pct Recovery = 25% Analysis Date = 04/02/16 Pct Recovery = 25% Analysis Date = 04/02/16 Pct Recovery = 25% Analysis Date = 03/31/16 Pct Recovery = 25% Analysis Date = 03/31/16 Pct Recovery = 25% Analysis Date = 03/29/16 Pct Recovery = 25% Analysis Date = 03/29/16 Pct Recovery = 25% Analysis Date = 03/27/16 Pct Recovery = 25% Analysis Date = 03/27/16 Pct Recovery = 25% Analysis Date = 03/24/16 Pct Recovery = 25% Analysis Date = 03/24/16 Pct Recovery = 25% Analysis Date = 03/22/16 Pct Recovery = 25% Analysis Date = 03/22/16 Pct Recovery = 25% Analysis Date = 03/20/16 Pct Recovery = 25% Analysis Date = 03/20/16 Pct Recovery = 25% Analysis Date = 03/18/16 Pct Recovery = 25% Analysis Date = 03/18/16 Pct Recovery = 25% Analysis Date = 03/15/16 Pct Recovery = 24% Analysis Date = 03/15/16 Pct Recovery = 24% Analysis Date = 03/13/16 Pct Recovery = 24% Analysis Date = 03/13/16 Pct Recovery = 24% Analysis Date = 03/11/16 Pct Recovery = 24% Analysis Date = 03/11/16 Pct Recovery = 24% Analysis Date = 03/09/16 Pct Recovery = 24% Analysis Date = 03/09/16 Pct Recovery = 24% Analysis Date = 03/06/16 Pct Recovery = 24% Analysis Date = 03/06/16 Pct Recovery = 24% Analysis Date = 03/04/16 Pct Recovery = 24% Analysis Date = 03/04/16 Pct Recovery = 24% Analysis Date = 03/02/16 Pct Recovery = 24% Analysis Date = 03/02/16 Pct Recovery = 24% Analysis Date = 02/29/16 Pct Recovery = 24% Analysis Date = 02/29/16 Pct Recovery = 24% Analysis Date = 02/26/16 Pct Recovery = 24% Analysis Date = 02/26/16 Pct Recovery = 24% Analysis Date = 02/24/16 Pct Recovery = 24% Analysis Date = 02/24/16 Pct Recovery = 24% Analysis Date = 02/22/16 Pct Recovery = 24% Analysis Date = 02/22/16 Pct Recovery = 24% Analysis Date = 02/20/16 Pct Recovery = 24% Analysis Date = 02/20/16 Pct Recovery = 24% Analysis Date = 02/17/16 Pct Recovery = 24% Analysis Date = 02/17/16 Pct Recovery = 24% Analysis Date = 02/15/16 Pct Recovery = 24% Analysis Date = 02/15/16 Pct Recovery = 24% Analysis Date = 02/13/16 Pct Recovery = 24% Analysis Date = 02/13/16 Pct Recovery = 24% Analysis Date = 02/11/16 Pct Recovery = 24% Analysis Date = 02/11/16 Pct Recovery = 24% Analysis Date = 02/09/16 Pct Recovery = 24% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICHLOROVOS (DICHLORVOS)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 43% 26% 36% 16%
Total 18 43% 26% 36% 16%

Sample Statistics
DICHLOROVOS (DICHLORVOS)

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
DICROTOPHOS
METHOD: 2033 , TESTIDCODE: 38454GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 21% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 21% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 19% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 17% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 16% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 21% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 14% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 13% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 25% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 17% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 17% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 24% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 14% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 12% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 11% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 10% Analysis Date = 05/10/17 Pct Recovery = 19% Analysis Date = 05/09/17 Pct Recovery = 19% Analysis Date = 05/09/17 Pct Recovery = 19% Analysis Date = 05/07/17 Pct Recovery = 19% Analysis Date = 05/07/17 Pct Recovery = 19% Analysis Date = 05/05/17 Pct Recovery = 19% Analysis Date = 05/05/17 Pct Recovery = 19% Analysis Date = 05/03/17 Pct Recovery = 19% Analysis Date = 05/03/17 Pct Recovery = 19% Analysis Date = 05/01/17 Pct Recovery = 19% Analysis Date = 05/01/17 Pct Recovery = 19% Analysis Date = 04/29/17 Pct Recovery = 19% Analysis Date = 04/29/17 Pct Recovery = 19% Analysis Date = 04/27/17 Pct Recovery = 19% Analysis Date = 04/27/17 Pct Recovery = 19% Analysis Date = 04/25/17 Pct Recovery = 19% Analysis Date = 04/25/17 Pct Recovery = 19% Analysis Date = 04/23/17 Pct Recovery = 19% Analysis Date = 04/23/17 Pct Recovery = 19% Analysis Date = 04/21/17 Pct Recovery = 19% Analysis Date = 04/21/17 Pct Recovery = 19% Analysis Date = 04/19/17 Pct Recovery = 19% Analysis Date = 04/19/17 Pct Recovery = 19% Analysis Date = 04/17/17 Pct Recovery = 19% Analysis Date = 04/17/17 Pct Recovery = 19% Analysis Date = 04/15/17 Pct Recovery = 19% Analysis Date = 04/15/17 Pct Recovery = 19% Analysis Date = 04/13/17 Pct Recovery = 19% Analysis Date = 04/13/17 Pct Recovery = 19% Analysis Date = 04/11/17 Pct Recovery = 19% Analysis Date = 04/11/17 Pct Recovery = 19% Analysis Date = 04/09/17 Pct Recovery = 19% Analysis Date = 04/09/17 Pct Recovery = 19% Analysis Date = 04/07/17 Pct Recovery = 19% Analysis Date = 04/07/17 Pct Recovery = 19% Analysis Date = 04/05/17 Pct Recovery = 19% Analysis Date = 04/05/17 Pct Recovery = 19% Analysis Date = 04/03/17 Pct Recovery = 19% Analysis Date = 04/03/17 Pct Recovery = 19% Analysis Date = 04/01/17 Pct Recovery = 19% Analysis Date = 04/01/17 Pct Recovery = 19% Analysis Date = 03/30/17 Pct Recovery = 19% Analysis Date = 03/30/17 Pct Recovery = 19% Analysis Date = 03/28/17 Pct Recovery = 19% Analysis Date = 03/28/17 Pct Recovery = 19% Analysis Date = 03/26/17 Pct Recovery = 19% Analysis Date = 03/26/17 Pct Recovery = 19% Analysis Date = 03/24/17 Pct Recovery = 19% Analysis Date = 03/24/17 Pct Recovery = 19% Analysis Date = 03/22/17 Pct Recovery = 20% Analysis Date = 03/22/17 Pct Recovery = 20% Analysis Date = 03/20/17 Pct Recovery = 20% Analysis Date = 03/20/17 Pct Recovery = 20% Analysis Date = 03/18/17 Pct Recovery = 20% Analysis Date = 03/18/17 Pct Recovery = 20% Analysis Date = 03/16/17 Pct Recovery = 20% Analysis Date = 03/16/17 Pct Recovery = 20% Analysis Date = 03/14/17 Pct Recovery = 20% Analysis Date = 03/14/17 Pct Recovery = 20% Analysis Date = 03/12/17 Pct Recovery = 20% Analysis Date = 03/12/17 Pct Recovery = 20% Analysis Date = 03/10/17 Pct Recovery = 20% Analysis Date = 03/10/17 Pct Recovery = 20% Analysis Date = 03/08/17 Pct Recovery = 20% Analysis Date = 03/08/17 Pct Recovery = 20% Analysis Date = 03/06/17 Pct Recovery = 20% Analysis Date = 03/06/17 Pct Recovery = 20% Analysis Date = 03/04/17 Pct Recovery = 20% Analysis Date = 03/04/17 Pct Recovery = 20% Analysis Date = 03/02/17 Pct Recovery = 20% Analysis Date = 03/02/17 Pct Recovery = 20% Analysis Date = 02/28/17 Pct Recovery = 20% Analysis Date = 02/28/17 Pct Recovery = 20% Analysis Date = 02/26/17 Pct Recovery = 20% Analysis Date = 02/26/17 Pct Recovery = 20% Analysis Date = 02/24/17 Pct Recovery = 20% Analysis Date = 02/24/17 Pct Recovery = 20% Analysis Date = 02/22/17 Pct Recovery = 20% Analysis Date = 02/22/17 Pct Recovery = 20% Analysis Date = 02/20/17 Pct Recovery = 20% Analysis Date = 02/20/17 Pct Recovery = 20% Analysis Date = 02/18/17 Pct Recovery = 20% Analysis Date = 02/18/17 Pct Recovery = 20% Analysis Date = 02/16/17 Pct Recovery = 20% Analysis Date = 02/16/17 Pct Recovery = 20% Analysis Date = 02/14/17 Pct Recovery = 20% Analysis Date = 02/14/17 Pct Recovery = 20% Analysis Date = 02/12/17 Pct Recovery = 20% Analysis Date = 02/12/17 Pct Recovery = 20% Analysis Date = 02/10/17 Pct Recovery = 20% Analysis Date = 02/10/17 Pct Recovery = 20% Analysis Date = 02/08/17 Pct Recovery = 20% Analysis Date = 02/08/17 Pct Recovery = 20% Analysis Date = 02/06/17 Pct Recovery = 20% Analysis Date = 02/06/17 Pct Recovery = 20% Analysis Date = 02/04/17 Pct Recovery = 20% Analysis Date = 02/04/17 Pct Recovery = 20% Analysis Date = 02/02/17 Pct Recovery = 20% Analysis Date = 02/02/17 Pct Recovery = 20% Analysis Date = 01/31/17 Pct Recovery = 20% Analysis Date = 01/31/17 Pct Recovery = 20% Analysis Date = 01/29/17 Pct Recovery = 20% Analysis Date = 01/29/17 Pct Recovery = 20% Analysis Date = 01/27/17 Pct Recovery = 20% Analysis Date = 01/27/17 Pct Recovery = 20% Analysis Date = 01/25/17 Pct Recovery = 21% Analysis Date = 01/25/17 Pct Recovery = 21% Analysis Date = 01/23/17 Pct Recovery = 21% Analysis Date = 01/23/17 Pct Recovery = 21% Analysis Date = 01/21/17 Pct Recovery = 21% Analysis Date = 01/21/17 Pct Recovery = 21% Analysis Date = 01/19/17 Pct Recovery = 21% Analysis Date = 01/19/17 Pct Recovery = 21% Analysis Date = 01/17/17 Pct Recovery = 21% Analysis Date = 01/17/17 Pct Recovery = 21% Analysis Date = 01/15/17 Pct Recovery = 21% Analysis Date = 01/15/17 Pct Recovery = 21% Analysis Date = 01/13/17 Pct Recovery = 21% Analysis Date = 01/13/17 Pct Recovery = 21% Analysis Date = 01/11/17 Pct Recovery = 21% Analysis Date = 01/11/17 Pct Recovery = 21% Analysis Date = 01/09/17 Pct Recovery = 20% Analysis Date = 01/09/17 Pct Recovery = 20% Analysis Date = 01/07/17 Pct Recovery = 20% Analysis Date = 01/07/17 Pct Recovery = 20% Analysis Date = 01/05/17 Pct Recovery = 20% Analysis Date = 01/05/17 Pct Recovery = 20% Analysis Date = 01/03/17 Pct Recovery = 20% Analysis Date = 01/03/17 Pct Recovery = 20% Analysis Date = 01/01/17 Pct Recovery = 20% Analysis Date = 01/01/17 Pct Recovery = 20% Analysis Date = 12/30/16 Pct Recovery = 20% Analysis Date = 12/30/16 Pct Recovery = 20% Analysis Date = 12/28/16 Pct Recovery = 20% Analysis Date = 12/28/16 Pct Recovery = 20% Analysis Date = 12/26/16 Pct Recovery = 20% Analysis Date = 12/26/16 Pct Recovery = 20% Analysis Date = 12/24/16 Pct Recovery = 20% Analysis Date = 12/24/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/22/16 Pct Recovery = 20% Analysis Date = 12/20/16 Pct Recovery = 20% Analysis Date = 12/20/16 Pct Recovery = 20% Analysis Date = 12/18/16 Pct Recovery = 20% Analysis Date = 12/18/16 Pct Recovery = 20% Analysis Date = 12/16/16 Pct Recovery = 20% Analysis Date = 12/16/16 Pct Recovery = 20% Analysis Date = 12/14/16 Pct Recovery = 20% Analysis Date = 12/14/16 Pct Recovery = 20% Analysis Date = 12/12/16 Pct Recovery = 20% Analysis Date = 12/12/16 Pct Recovery = 20% Analysis Date = 12/10/16 Pct Recovery = 20% Analysis Date = 12/10/16 Pct Recovery = 20% Analysis Date = 12/08/16 Pct Recovery = 20% Analysis Date = 12/08/16 Pct Recovery = 20% Analysis Date = 12/06/16 Pct Recovery = 19% Analysis Date = 12/06/16 Pct Recovery = 19% Analysis Date = 12/04/16 Pct Recovery = 19% Analysis Date = 12/04/16 Pct Recovery = 19% Analysis Date = 12/02/16 Pct Recovery = 19% Analysis Date = 12/02/16 Pct Recovery = 19% Analysis Date = 11/30/16 Pct Recovery = 19% Analysis Date = 11/30/16 Pct Recovery = 19% Analysis Date = 11/28/16 Pct Recovery = 19% Analysis Date = 11/28/16 Pct Recovery = 19% Analysis Date = 11/26/16 Pct Recovery = 19% Analysis Date = 11/26/16 Pct Recovery = 19% Analysis Date = 11/24/16 Pct Recovery = 19% Analysis Date = 11/24/16 Pct Recovery = 19% Analysis Date = 11/22/16 Pct Recovery = 19% Analysis Date = 11/22/16 Pct Recovery = 19% Analysis Date = 11/20/16 Pct Recovery = 19% Analysis Date = 11/20/16 Pct Recovery = 19% Analysis Date = 11/18/16 Pct Recovery = 19% Analysis Date = 11/18/16 Pct Recovery = 19% Analysis Date = 11/16/16 Pct Recovery = 19% Analysis Date = 11/16/16 Pct Recovery = 19% Analysis Date = 11/14/16 Pct Recovery = 19% Analysis Date = 11/14/16 Pct Recovery = 19% Analysis Date = 11/12/16 Pct Recovery = 19% Analysis Date = 11/12/16 Pct Recovery = 19% Analysis Date = 11/10/16 Pct Recovery = 19% Analysis Date = 11/10/16 Pct Recovery = 19% Analysis Date = 11/08/16 Pct Recovery = 19% Analysis Date = 11/08/16 Pct Recovery = 19% Analysis Date = 11/06/16 Pct Recovery = 19% Analysis Date = 11/06/16 Pct Recovery = 19% Analysis Date = 11/04/16 Pct Recovery = 19% Analysis Date = 11/04/16 Pct Recovery = 19% Analysis Date = 11/02/16 Pct Recovery = 19% Analysis Date = 11/02/16 Pct Recovery = 19% Analysis Date = 10/31/16 Pct Recovery = 19% Analysis Date = 10/31/16 Pct Recovery = 19% Analysis Date = 10/29/16 Pct Recovery = 18% Analysis Date = 10/29/16 Pct Recovery = 18% Analysis Date = 10/27/16 Pct Recovery = 18% Analysis Date = 10/27/16 Pct Recovery = 18% Analysis Date = 10/25/16 Pct Recovery = 18% Analysis Date = 10/25/16 Pct Recovery = 18% Analysis Date = 10/23/16 Pct Recovery = 18% Analysis Date = 10/23/16 Pct Recovery = 18% Analysis Date = 10/21/16 Pct Recovery = 18% Analysis Date = 10/21/16 Pct Recovery = 18% Analysis Date = 10/19/16 Pct Recovery = 18% Analysis Date = 10/19/16 Pct Recovery = 18% Analysis Date = 10/17/16 Pct Recovery = 18% Analysis Date = 10/17/16 Pct Recovery = 18% Analysis Date = 10/15/16 Pct Recovery = 18% Analysis Date = 10/15/16 Pct Recovery = 18% Analysis Date = 10/13/16 Pct Recovery = 18% Analysis Date = 10/13/16 Pct Recovery = 18% Analysis Date = 10/11/16 Pct Recovery = 18% Analysis Date = 10/11/16 Pct Recovery = 18% Analysis Date = 10/09/16 Pct Recovery = 18% Analysis Date = 10/09/16 Pct Recovery = 18% Analysis Date = 10/07/16 Pct Recovery = 18% Analysis Date = 10/07/16 Pct Recovery = 18% Analysis Date = 10/05/16 Pct Recovery = 18% Analysis Date = 10/05/16 Pct Recovery = 18% Analysis Date = 10/03/16 Pct Recovery = 18% Analysis Date = 10/03/16 Pct Recovery = 18% Analysis Date = 10/01/16 Pct Recovery = 18% Analysis Date = 10/01/16 Pct Recovery = 18% Analysis Date = 09/29/16 Pct Recovery = 18% Analysis Date = 09/29/16 Pct Recovery = 18% Analysis Date = 09/27/16 Pct Recovery = 18% Analysis Date = 09/27/16 Pct Recovery = 18% Analysis Date = 09/25/16 Pct Recovery = 18% Analysis Date = 09/25/16 Pct Recovery = 18% Analysis Date = 09/23/16 Pct Recovery = 18% Analysis Date = 09/23/16 Pct Recovery = 18% Analysis Date = 09/21/16 Pct Recovery = 17% Analysis Date = 09/21/16 Pct Recovery = 17% Analysis Date = 09/19/16 Pct Recovery = 17% Analysis Date = 09/19/16 Pct Recovery = 17% Analysis Date = 09/17/16 Pct Recovery = 17% Analysis Date = 09/17/16 Pct Recovery = 17% Analysis Date = 09/15/16 Pct Recovery = 17% Analysis Date = 09/15/16 Pct Recovery = 17% Analysis Date = 09/13/16 Pct Recovery = 17% Analysis Date = 09/13/16 Pct Recovery = 17% Analysis Date = 09/11/16 Pct Recovery = 17% Analysis Date = 09/11/16 Pct Recovery = 17% Analysis Date = 09/09/16 Pct Recovery = 17% Analysis Date = 09/09/16 Pct Recovery = 17% Analysis Date = 09/07/16 Pct Recovery = 17% Analysis Date = 09/07/16 Pct Recovery = 17% Analysis Date = 09/05/16 Pct Recovery = 17% Analysis Date = 09/05/16 Pct Recovery = 17% Analysis Date = 09/03/16 Pct Recovery = 17% Analysis Date = 09/03/16 Pct Recovery = 17% Analysis Date = 09/01/16 Pct Recovery = 17% Analysis Date = 09/01/16 Pct Recovery = 17% Analysis Date = 08/30/16 Pct Recovery = 16% Analysis Date = 08/30/16 Pct Recovery = 16% Analysis Date = 08/28/16 Pct Recovery = 16% Analysis Date = 08/28/16 Pct Recovery = 16% Analysis Date = 08/26/16 Pct Recovery = 16% Analysis Date = 08/26/16 Pct Recovery = 16% Analysis Date = 08/24/16 Pct Recovery = 16% Analysis Date = 08/24/16 Pct Recovery = 16% Analysis Date = 08/22/16 Pct Recovery = 16% Analysis Date = 08/22/16 Pct Recovery = 16% Analysis Date = 08/20/16 Pct Recovery = 16% Analysis Date = 08/20/16 Pct Recovery = 16% Analysis Date = 08/18/16 Pct Recovery = 16% Analysis Date = 08/18/16 Pct Recovery = 16% Analysis Date = 08/16/16 Pct Recovery = 16% Analysis Date = 08/16/16 Pct Recovery = 16% Analysis Date = 08/14/16 Pct Recovery = 16% Analysis Date = 08/14/16 Pct Recovery = 16% Analysis Date = 08/12/16 Pct Recovery = 16% Analysis Date = 08/12/16 Pct Recovery = 16% Analysis Date = 08/10/16 Pct Recovery = 16% Analysis Date = 08/10/16 Pct Recovery = 16% Analysis Date = 08/08/16 Pct Recovery = 15% Analysis Date = 08/08/16 Pct Recovery = 15% Analysis Date = 08/06/16 Pct Recovery = 15% Analysis Date = 08/06/16 Pct Recovery = 15% Analysis Date = 08/04/16 Pct Recovery = 15% Analysis Date = 08/04/16 Pct Recovery = 15% Analysis Date = 08/02/16 Pct Recovery = 15% Analysis Date = 08/02/16 Pct Recovery = 15% Analysis Date = 07/31/16 Pct Recovery = 15% Analysis Date = 07/31/16 Pct Recovery = 15% Analysis Date = 07/29/16 Pct Recovery = 15% Analysis Date = 07/29/16 Pct Recovery = 15% Analysis Date = 07/27/16 Pct Recovery = 15% Analysis Date = 07/27/16 Pct Recovery = 15% Analysis Date = 07/25/16 Pct Recovery = 15% Analysis Date = 07/25/16 Pct Recovery = 15% Analysis Date = 07/23/16 Pct Recovery = 15% Analysis Date = 07/23/16 Pct Recovery = 15% Analysis Date = 07/21/16 Pct Recovery = 15% Analysis Date = 07/21/16 Pct Recovery = 15% Analysis Date = 07/19/16 Pct Recovery = 15% Analysis Date = 07/19/16 Pct Recovery = 15% Analysis Date = 07/17/16 Pct Recovery = 15% Analysis Date = 07/17/16 Pct Recovery = 15% Analysis Date = 07/15/16 Pct Recovery = 15% Analysis Date = 07/15/16 Pct Recovery = 15% Analysis Date = 07/13/16 Pct Recovery = 15% Analysis Date = 07/13/16 Pct Recovery = 15% Analysis Date = 07/11/16 Pct Recovery = 15% Analysis Date = 07/11/16 Pct Recovery = 15% Analysis Date = 07/09/16 Pct Recovery = 15% Analysis Date = 07/09/16 Pct Recovery = 15% Analysis Date = 07/07/16 Pct Recovery = 15% Analysis Date = 07/07/16 Pct Recovery = 15% Analysis Date = 07/05/16 Pct Recovery = 15% Analysis Date = 07/05/16 Pct Recovery = 15% Analysis Date = 07/03/16 Pct Recovery = 14% Analysis Date = 07/03/16 Pct Recovery = 14% Analysis Date = 07/01/16 Pct Recovery = 14% Analysis Date = 07/01/16 Pct Recovery = 14% Analysis Date = 06/29/16 Pct Recovery = 14% Analysis Date = 06/29/16 Pct Recovery = 14% Analysis Date = 06/27/16 Pct Recovery = 14% Analysis Date = 06/27/16 Pct Recovery = 14% Analysis Date = 06/25/16 Pct Recovery = 14% Analysis Date = 06/25/16 Pct Recovery = 14% Analysis Date = 06/23/16 Pct Recovery = 14% Analysis Date = 06/23/16 Pct Recovery = 14% Analysis Date = 06/21/16 Pct Recovery = 14% Analysis Date = 06/21/16 Pct Recovery = 14% Analysis Date = 06/19/16 Pct Recovery = 14% Analysis Date = 06/19/16 Pct Recovery = 14% Analysis Date = 06/17/16 Pct Recovery = 14% Analysis Date = 06/17/16 Pct Recovery = 14% Analysis Date = 06/15/16 Pct Recovery = 14% Analysis Date = 06/15/16 Pct Recovery = 14% Analysis Date = 06/13/16 Pct Recovery = 14% Analysis Date = 06/13/16 Pct Recovery = 14% Analysis Date = 06/11/16 Pct Recovery = 14% Analysis Date = 06/11/16 Pct Recovery = 14% Analysis Date = 06/09/16 Pct Recovery = 14% Analysis Date = 06/09/16 Pct Recovery = 14% Analysis Date = 06/07/16 Pct Recovery = 14% Analysis Date = 06/07/16 Pct Recovery = 14% Analysis Date = 06/05/16 Pct Recovery = 14% Analysis Date = 06/05/16 Pct Recovery = 14% Analysis Date = 06/03/16 Pct Recovery = 14% Analysis Date = 06/03/16 Pct Recovery = 14% Analysis Date = 06/01/16 Pct Recovery = 14% Analysis Date = 06/01/16 Pct Recovery = 14% Analysis Date = 05/30/16 Pct Recovery = 13% Analysis Date = 05/30/16 Pct Recovery = 13% Analysis Date = 05/28/16 Pct Recovery = 13% Analysis Date = 05/28/16 Pct Recovery = 13% Analysis Date = 05/26/16 Pct Recovery = 13% Analysis Date = 05/26/16 Pct Recovery = 13% Analysis Date = 05/24/16 Pct Recovery = 13% Analysis Date = 05/24/16 Pct Recovery = 13% Analysis Date = 05/22/16 Pct Recovery = 13% Analysis Date = 05/22/16 Pct Recovery = 13% Analysis Date = 05/20/16 Pct Recovery = 13% Analysis Date = 05/20/16 Pct Recovery = 13% Analysis Date = 05/18/16 Pct Recovery = 13% Analysis Date = 05/18/16 Pct Recovery = 13% Analysis Date = 05/16/16 Pct Recovery = 13% Analysis Date = 05/16/16 Pct Recovery = 13% Analysis Date = 05/14/16 Pct Recovery = 13% Analysis Date = 05/14/16 Pct Recovery = 13% Analysis Date = 05/12/16 Pct Recovery = 13% Analysis Date = 05/12/16 Pct Recovery = 13% Analysis Date = 05/10/16 Pct Recovery = 13% Analysis Date = 05/10/16 Pct Recovery = 13% Analysis Date = 05/08/16 Pct Recovery = 13% Analysis Date = 05/08/16 Pct Recovery = 13% Analysis Date = 05/06/16 Pct Recovery = 13% Analysis Date = 05/06/16 Pct Recovery = 13% Analysis Date = 05/04/16 Pct Recovery = 13% Analysis Date = 05/04/16 Pct Recovery = 13% Analysis Date = 05/02/16 Pct Recovery = 13% Analysis Date = 05/02/16 Pct Recovery = 13% Analysis Date = 04/30/16 Pct Recovery = 13% Analysis Date = 04/30/16 Pct Recovery = 13% Analysis Date = 04/28/16 Pct Recovery = 13% Analysis Date = 04/28/16 Pct Recovery = 13% Analysis Date = 04/26/16 Pct Recovery = 13% Analysis Date = 04/26/16 Pct Recovery = 13% Analysis Date = 04/24/16 Pct Recovery = 12% Analysis Date = 04/24/16 Pct Recovery = 12% Analysis Date = 04/22/16 Pct Recovery = 12% Analysis Date = 04/22/16 Pct Recovery = 12% Analysis Date = 04/20/16 Pct Recovery = 12% Analysis Date = 04/20/16 Pct Recovery = 12% Analysis Date = 04/18/16 Pct Recovery = 12% Analysis Date = 04/18/16 Pct Recovery = 12% Analysis Date = 04/16/16 Pct Recovery = 12% Analysis Date = 04/16/16 Pct Recovery = 12% Analysis Date = 04/14/16 Pct Recovery = 12% Analysis Date = 04/14/16 Pct Recovery = 12% Analysis Date = 04/12/16 Pct Recovery = 12% Analysis Date = 04/12/16 Pct Recovery = 12% Analysis Date = 04/10/16 Pct Recovery = 12% Analysis Date = 04/10/16 Pct Recovery = 12% Analysis Date = 04/08/16 Pct Recovery = 12% Analysis Date = 04/08/16 Pct Recovery = 12% Analysis Date = 04/07/16 Pct Recovery = 12% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DICROTOPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 16 17% 4% 17% 5%
Total 16 17% 4% 17% 5%

Sample Statistics
DICROTOPHOS

Characteristic N % % Basis
Plotted 16 100% Spiked
Estimated Values 16 100% Spiked
Deleted Values 1 4% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 16 .  
False Negatives 0 0% 0 out of 16
Not Spiked 9 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
DIELDRIN
METHOD: 2033 , TESTIDCODE: 39381GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 114% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 83% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 86% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 72% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 93% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 116% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 79% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 83% Analysis Date = 05/10/17 Pct Recovery = 94% Analysis Date = 05/08/17 Pct Recovery = 94% Analysis Date = 05/08/17 Pct Recovery = 94% Analysis Date = 05/06/17 Pct Recovery = 94% Analysis Date = 05/06/17 Pct Recovery = 94% Analysis Date = 05/04/17 Pct Recovery = 94% Analysis Date = 05/04/17 Pct Recovery = 94% Analysis Date = 05/01/17 Pct Recovery = 94% Analysis Date = 05/01/17 Pct Recovery = 94% Analysis Date = 04/29/17 Pct Recovery = 94% Analysis Date = 04/29/17 Pct Recovery = 94% Analysis Date = 04/27/17 Pct Recovery = 94% Analysis Date = 04/27/17 Pct Recovery = 94% Analysis Date = 04/25/17 Pct Recovery = 94% Analysis Date = 04/25/17 Pct Recovery = 94% Analysis Date = 04/22/17 Pct Recovery = 94% Analysis Date = 04/22/17 Pct Recovery = 94% Analysis Date = 04/20/17 Pct Recovery = 94% Analysis Date = 04/20/17 Pct Recovery = 94% Analysis Date = 04/18/17 Pct Recovery = 94% Analysis Date = 04/18/17 Pct Recovery = 94% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/09/17 Pct Recovery = 93% Analysis Date = 04/09/17 Pct Recovery = 93% Analysis Date = 04/06/17 Pct Recovery = 93% Analysis Date = 04/06/17 Pct Recovery = 93% Analysis Date = 04/04/17 Pct Recovery = 93% Analysis Date = 04/04/17 Pct Recovery = 93% Analysis Date = 04/02/17 Pct Recovery = 93% Analysis Date = 04/02/17 Pct Recovery = 93% Analysis Date = 03/30/17 Pct Recovery = 93% Analysis Date = 03/30/17 Pct Recovery = 93% Analysis Date = 03/28/17 Pct Recovery = 93% Analysis Date = 03/28/17 Pct Recovery = 93% Analysis Date = 03/26/17 Pct Recovery = 93% Analysis Date = 03/26/17 Pct Recovery = 93% Analysis Date = 03/24/17 Pct Recovery = 93% Analysis Date = 03/24/17 Pct Recovery = 93% Analysis Date = 03/21/17 Pct Recovery = 93% Analysis Date = 03/21/17 Pct Recovery = 93% Analysis Date = 03/19/17 Pct Recovery = 92% Analysis Date = 03/19/17 Pct Recovery = 92% Analysis Date = 03/17/17 Pct Recovery = 92% Analysis Date = 03/17/17 Pct Recovery = 92% Analysis Date = 03/14/17 Pct Recovery = 92% Analysis Date = 03/14/17 Pct Recovery = 92% Analysis Date = 03/12/17 Pct Recovery = 92% Analysis Date = 03/12/17 Pct Recovery = 92% Analysis Date = 03/10/17 Pct Recovery = 92% Analysis Date = 03/10/17 Pct Recovery = 92% Analysis Date = 03/08/17 Pct Recovery = 92% Analysis Date = 03/08/17 Pct Recovery = 92% Analysis Date = 03/05/17 Pct Recovery = 92% Analysis Date = 03/05/17 Pct Recovery = 92% Analysis Date = 03/03/17 Pct Recovery = 92% Analysis Date = 03/03/17 Pct Recovery = 92% Analysis Date = 03/01/17 Pct Recovery = 92% Analysis Date = 03/01/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/24/17 Pct Recovery = 92% Analysis Date = 02/24/17 Pct Recovery = 92% Analysis Date = 02/22/17 Pct Recovery = 92% Analysis Date = 02/22/17 Pct Recovery = 92% Analysis Date = 02/20/17 Pct Recovery = 92% Analysis Date = 02/20/17 Pct Recovery = 92% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/01/17 Pct Recovery = 91% Analysis Date = 02/01/17 Pct Recovery = 91% Analysis Date = 01/30/17 Pct Recovery = 91% Analysis Date = 01/30/17 Pct Recovery = 91% Analysis Date = 01/28/17 Pct Recovery = 91% Analysis Date = 01/28/17 Pct Recovery = 91% Analysis Date = 01/25/17 Pct Recovery = 91% Analysis Date = 01/25/17 Pct Recovery = 91% Analysis Date = 01/23/17 Pct Recovery = 91% Analysis Date = 01/23/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/19/17 Pct Recovery = 91% Analysis Date = 01/19/17 Pct Recovery = 91% Analysis Date = 01/16/17 Pct Recovery = 91% Analysis Date = 01/16/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/14/17 Pct Recovery = 91% Analysis Date = 01/12/17 Pct Recovery = 91% Analysis Date = 01/12/17 Pct Recovery = 91% Analysis Date = 01/09/17 Pct Recovery = 92% Analysis Date = 01/09/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/05/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 01/03/17 Pct Recovery = 92% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 94% Analysis Date = 12/24/16 Pct Recovery = 94% Analysis Date = 12/22/16 Pct Recovery = 94% Analysis Date = 12/22/16 Pct Recovery = 94% Analysis Date = 12/20/16 Pct Recovery = 94% Analysis Date = 12/20/16 Pct Recovery = 94% Analysis Date = 12/18/16 Pct Recovery = 94% Analysis Date = 12/18/16 Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/08/16 Pct Recovery = 94% Analysis Date = 12/08/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/29/16 Pct Recovery = 94% Analysis Date = 11/29/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/16/16 Pct Recovery = 94% Analysis Date = 11/16/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 10/31/16 Pct Recovery = 94% Analysis Date = 10/31/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 94% Analysis Date = 10/26/16 Pct Recovery = 94% Analysis Date = 10/26/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/24/16 Pct Recovery = 94% Analysis Date = 10/21/16 Pct Recovery = 94% Analysis Date = 10/21/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/19/16 Pct Recovery = 94% Analysis Date = 10/17/16 Pct Recovery = 94% Analysis Date = 10/17/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/15/16 Pct Recovery = 94% Analysis Date = 10/12/16 Pct Recovery = 94% Analysis Date = 10/12/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/10/16 Pct Recovery = 94% Analysis Date = 10/08/16 Pct Recovery = 94% Analysis Date = 10/08/16 Pct Recovery = 94% Analysis Date = 10/05/16 Pct Recovery = 94% Analysis Date = 10/05/16 Pct Recovery = 94% Analysis Date = 10/03/16 Pct Recovery = 94% Analysis Date = 10/03/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 94% Analysis Date = 10/01/16 Pct Recovery = 94% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/13/16 Pct Recovery = 93% Analysis Date = 09/13/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/10/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/03/16 Pct Recovery = 93% Analysis Date = 09/03/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 93% Analysis Date = 08/30/16 Pct Recovery = 93% Analysis Date = 08/30/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/25/16 Pct Recovery = 93% Analysis Date = 08/25/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/21/16 Pct Recovery = 93% Analysis Date = 08/21/16 Pct Recovery = 93% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/16/16 Pct Recovery = 92% Analysis Date = 08/16/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/12/16 Pct Recovery = 92% Analysis Date = 08/12/16 Pct Recovery = 92% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/07/16 Pct Recovery = 91% Analysis Date = 08/07/16 Pct Recovery = 91% Analysis Date = 08/05/16 Pct Recovery = 91% Analysis Date = 08/05/16 Pct Recovery = 91% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 90% Analysis Date = 07/24/16 Pct Recovery = 89% Analysis Date = 07/24/16 Pct Recovery = 89% Analysis Date = 07/22/16 Pct Recovery = 89% Analysis Date = 07/22/16 Pct Recovery = 89% Analysis Date = 07/20/16 Pct Recovery = 89% Analysis Date = 07/20/16 Pct Recovery = 89% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 87% Analysis Date = 07/11/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/04/16 Pct Recovery = 87% Analysis Date = 07/04/16 Pct Recovery = 87% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/09/16 Pct Recovery = 83% Analysis Date = 06/09/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/04/16 Pct Recovery = 83% Analysis Date = 06/04/16 Pct Recovery = 83% Analysis Date = 06/02/16 Pct Recovery = 82% Analysis Date = 06/02/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/26/16 Pct Recovery = 82% Analysis Date = 05/26/16 Pct Recovery = 82% Analysis Date = 05/24/16 Pct Recovery = 82% Analysis Date = 05/24/16 Pct Recovery = 82% Analysis Date = 05/21/16 Pct Recovery = 82% Analysis Date = 05/21/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/17/16 Pct Recovery = 82% Analysis Date = 05/17/16 Pct Recovery = 82% Analysis Date = 05/14/16 Pct Recovery = 82% Analysis Date = 05/14/16 Pct Recovery = 82% Analysis Date = 05/12/16 Pct Recovery = 82% Analysis Date = 05/12/16 Pct Recovery = 82% Analysis Date = 05/10/16 Pct Recovery = 82% Analysis Date = 05/10/16 Pct Recovery = 82% Analysis Date = 05/08/16 Pct Recovery = 83% Analysis Date = 05/08/16 Pct Recovery = 83% Analysis Date = 05/05/16 Pct Recovery = 83% Analysis Date = 05/05/16 Pct Recovery = 83% Analysis Date = 05/03/16 Pct Recovery = 83% Analysis Date = 05/03/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/24/16 Pct Recovery = 83% Analysis Date = 04/24/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 83% Analysis Date = 04/17/16 Pct Recovery = 84% Analysis Date = 04/17/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/08/16 Pct Recovery = 84% Analysis Date = 04/08/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 03/30/16 Pct Recovery = 84% Analysis Date = 03/30/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/18/16 Pct Recovery = 85% Analysis Date = 03/18/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/11/16 Pct Recovery = 85% Analysis Date = 03/11/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/05/16 Pct Recovery = 86% Analysis Date = 03/05/16 Pct Recovery = 86% Analysis Date = 03/02/16 Pct Recovery = 86% Analysis Date = 03/02/16 Pct Recovery = 86% Analysis Date = 02/29/16 Pct Recovery = 86% Analysis Date = 02/29/16 Pct Recovery = 86% Analysis Date = 02/27/16 Pct Recovery = 86% Analysis Date = 02/27/16 Pct Recovery = 86% Analysis Date = 02/24/16 Pct Recovery = 86% Analysis Date = 02/24/16 Pct Recovery = 86% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 87% Analysis Date = 02/15/16 Pct Recovery = 87% Analysis Date = 02/13/16 Pct Recovery = 87% Analysis Date = 02/13/16 Pct Recovery = 87% Analysis Date = 02/11/16 Pct Recovery = 87% Analysis Date = 02/11/16 Pct Recovery = 87% Analysis Date = 02/09/16 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIELDRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 89% 13% 86% 13%
Total 19 89% 13% 86% 13%

Sample Statistics
DIELDRIN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 1 11% 1 out of 9

OBSP Determination:
DIMETHOATE
METHOD: 2033 , TESTIDCODE: 82662GCM40

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 34% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 30% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 25% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 24% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 35% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 42% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 36% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 36% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 57% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 51% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 42% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 38% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 35% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 38% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 57% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 46% Analysis Date = 05/02/17 Pct Recovery = 36% Analysis Date = 04/30/17 Pct Recovery = 36% Analysis Date = 04/30/17 Pct Recovery = 36% Analysis Date = 04/28/17 Pct Recovery = 36% Analysis Date = 04/28/17 Pct Recovery = 36% Analysis Date = 04/26/17 Pct Recovery = 36% Analysis Date = 04/26/17 Pct Recovery = 36% Analysis Date = 04/24/17 Pct Recovery = 36% Analysis Date = 04/24/17 Pct Recovery = 36% Analysis Date = 04/22/17 Pct Recovery = 36% Analysis Date = 04/22/17 Pct Recovery = 36% Analysis Date = 04/20/17 Pct Recovery = 37% Analysis Date = 04/20/17 Pct Recovery = 37% Analysis Date = 04/18/17 Pct Recovery = 37% Analysis Date = 04/18/17 Pct Recovery = 37% Analysis Date = 04/15/17 Pct Recovery = 37% Analysis Date = 04/15/17 Pct Recovery = 37% Analysis Date = 04/13/17 Pct Recovery = 37% Analysis Date = 04/13/17 Pct Recovery = 37% Analysis Date = 04/11/17 Pct Recovery = 37% Analysis Date = 04/11/17 Pct Recovery = 37% Analysis Date = 04/09/17 Pct Recovery = 37% Analysis Date = 04/09/17 Pct Recovery = 37% Analysis Date = 04/07/17 Pct Recovery = 37% Analysis Date = 04/07/17 Pct Recovery = 37% Analysis Date = 04/05/17 Pct Recovery = 37% Analysis Date = 04/05/17 Pct Recovery = 37% Analysis Date = 04/03/17 Pct Recovery = 37% Analysis Date = 04/03/17 Pct Recovery = 37% Analysis Date = 03/31/17 Pct Recovery = 37% Analysis Date = 03/31/17 Pct Recovery = 37% Analysis Date = 03/29/17 Pct Recovery = 37% Analysis Date = 03/29/17 Pct Recovery = 37% Analysis Date = 03/27/17 Pct Recovery = 37% Analysis Date = 03/27/17 Pct Recovery = 37% Analysis Date = 03/25/17 Pct Recovery = 37% Analysis Date = 03/25/17 Pct Recovery = 37% Analysis Date = 03/23/17 Pct Recovery = 37% Analysis Date = 03/23/17 Pct Recovery = 37% Analysis Date = 03/21/17 Pct Recovery = 38% Analysis Date = 03/21/17 Pct Recovery = 38% Analysis Date = 03/19/17 Pct Recovery = 38% Analysis Date = 03/19/17 Pct Recovery = 38% Analysis Date = 03/17/17 Pct Recovery = 38% Analysis Date = 03/17/17 Pct Recovery = 38% Analysis Date = 03/14/17 Pct Recovery = 38% Analysis Date = 03/14/17 Pct Recovery = 38% Analysis Date = 03/12/17 Pct Recovery = 38% Analysis Date = 03/12/17 Pct Recovery = 38% Analysis Date = 03/10/17 Pct Recovery = 38% Analysis Date = 03/10/17 Pct Recovery = 38% Analysis Date = 03/08/17 Pct Recovery = 38% Analysis Date = 03/08/17 Pct Recovery = 38% Analysis Date = 03/06/17 Pct Recovery = 38% Analysis Date = 03/06/17 Pct Recovery = 38% Analysis Date = 03/04/17 Pct Recovery = 38% Analysis Date = 03/04/17 Pct Recovery = 38% Analysis Date = 03/02/17 Pct Recovery = 38% Analysis Date = 03/02/17 Pct Recovery = 38% Analysis Date = 02/27/17 Pct Recovery = 39% Analysis Date = 02/27/17 Pct Recovery = 39% Analysis Date = 02/25/17 Pct Recovery = 39% Analysis Date = 02/25/17 Pct Recovery = 39% Analysis Date = 02/23/17 Pct Recovery = 39% Analysis Date = 02/23/17 Pct Recovery = 39% Analysis Date = 02/21/17 Pct Recovery = 39% Analysis Date = 02/21/17 Pct Recovery = 39% Analysis Date = 02/19/17 Pct Recovery = 39% Analysis Date = 02/19/17 Pct Recovery = 39% Analysis Date = 02/17/17 Pct Recovery = 39% Analysis Date = 02/17/17 Pct Recovery = 39% Analysis Date = 02/15/17 Pct Recovery = 39% Analysis Date = 02/15/17 Pct Recovery = 39% Analysis Date = 02/13/17 Pct Recovery = 39% Analysis Date = 02/13/17 Pct Recovery = 39% Analysis Date = 02/10/17 Pct Recovery = 39% Analysis Date = 02/10/17 Pct Recovery = 39% Analysis Date = 02/08/17 Pct Recovery = 39% Analysis Date = 02/08/17 Pct Recovery = 39% Analysis Date = 02/06/17 Pct Recovery = 39% Analysis Date = 02/06/17 Pct Recovery = 39% Analysis Date = 02/04/17 Pct Recovery = 40% Analysis Date = 02/04/17 Pct Recovery = 40% Analysis Date = 02/02/17 Pct Recovery = 40% Analysis Date = 02/02/17 Pct Recovery = 40% Analysis Date = 01/31/17 Pct Recovery = 40% Analysis Date = 01/31/17 Pct Recovery = 40% Analysis Date = 01/29/17 Pct Recovery = 40% Analysis Date = 01/29/17 Pct Recovery = 40% Analysis Date = 01/26/17 Pct Recovery = 40% Analysis Date = 01/26/17 Pct Recovery = 40% Analysis Date = 01/24/17 Pct Recovery = 40% Analysis Date = 01/24/17 Pct Recovery = 40% Analysis Date = 01/22/17 Pct Recovery = 40% Analysis Date = 01/22/17 Pct Recovery = 40% Analysis Date = 01/20/17 Pct Recovery = 40% Analysis Date = 01/20/17 Pct Recovery = 40% Analysis Date = 01/18/17 Pct Recovery = 40% Analysis Date = 01/18/17 Pct Recovery = 40% Analysis Date = 01/16/17 Pct Recovery = 40% Analysis Date = 01/16/17 Pct Recovery = 40% Analysis Date = 01/14/17 Pct Recovery = 40% Analysis Date = 01/14/17 Pct Recovery = 40% Analysis Date = 01/11/17 Pct Recovery = 40% Analysis Date = 01/11/17 Pct Recovery = 40% Analysis Date = 01/09/17 Pct Recovery = 40% Analysis Date = 01/09/17 Pct Recovery = 40% Analysis Date = 01/07/17 Pct Recovery = 40% Analysis Date = 01/07/17 Pct Recovery = 40% Analysis Date = 01/05/17 Pct Recovery = 40% Analysis Date = 01/05/17 Pct Recovery = 40% Analysis Date = 01/03/17 Pct Recovery = 40% Analysis Date = 01/03/17 Pct Recovery = 40% Analysis Date = 01/01/17 Pct Recovery = 40% Analysis Date = 01/01/17 Pct Recovery = 40% Analysis Date = 12/30/16 Pct Recovery = 40% Analysis Date = 12/30/16 Pct Recovery = 40% Analysis Date = 12/28/16 Pct Recovery = 41% Analysis Date = 12/28/16 Pct Recovery = 41% Analysis Date = 12/25/16 Pct Recovery = 41% Analysis Date = 12/25/16 Pct Recovery = 41% Analysis Date = 12/23/16 Pct Recovery = 41% Analysis Date = 12/23/16 Pct Recovery = 41% Analysis Date = 12/21/16 Pct Recovery = 41% Analysis Date = 12/21/16 Pct Recovery = 41% Analysis Date = 12/19/16 Pct Recovery = 41% Analysis Date = 12/19/16 Pct Recovery = 41% Analysis Date = 12/17/16 Pct Recovery = 41% Analysis Date = 12/17/16 Pct Recovery = 41% Analysis Date = 12/15/16 Pct Recovery = 41% Analysis Date = 12/15/16 Pct Recovery = 41% Analysis Date = 12/13/16 Pct Recovery = 41% Analysis Date = 12/13/16 Pct Recovery = 41% Analysis Date = 12/10/16 Pct Recovery = 40% Analysis Date = 12/10/16 Pct Recovery = 40% Analysis Date = 12/08/16 Pct Recovery = 40% Analysis Date = 12/08/16 Pct Recovery = 40% Analysis Date = 12/06/16 Pct Recovery = 40% Analysis Date = 12/06/16 Pct Recovery = 40% Analysis Date = 12/04/16 Pct Recovery = 40% Analysis Date = 12/04/16 Pct Recovery = 40% Analysis Date = 12/02/16 Pct Recovery = 40% Analysis Date = 12/02/16 Pct Recovery = 40% Analysis Date = 11/30/16 Pct Recovery = 40% Analysis Date = 11/30/16 Pct Recovery = 40% Analysis Date = 11/28/16 Pct Recovery = 40% Analysis Date = 11/28/16 Pct Recovery = 40% Analysis Date = 11/26/16 Pct Recovery = 40% Analysis Date = 11/26/16 Pct Recovery = 40% Analysis Date = 11/23/16 Pct Recovery = 40% Analysis Date = 11/23/16 Pct Recovery = 40% Analysis Date = 11/21/16 Pct Recovery = 40% Analysis Date = 11/21/16 Pct Recovery = 40% Analysis Date = 11/19/16 Pct Recovery = 40% Analysis Date = 11/19/16 Pct Recovery = 40% Analysis Date = 11/17/16 Pct Recovery = 40% Analysis Date = 11/17/16 Pct Recovery = 40% Analysis Date = 11/15/16 Pct Recovery = 40% Analysis Date = 11/15/16 Pct Recovery = 40% Analysis Date = 11/13/16 Pct Recovery = 40% Analysis Date = 11/13/16 Pct Recovery = 40% Analysis Date = 11/11/16 Pct Recovery = 40% Analysis Date = 11/11/16 Pct Recovery = 40% Analysis Date = 11/08/16 Pct Recovery = 39% Analysis Date = 11/08/16 Pct Recovery = 39% Analysis Date = 11/06/16 Pct Recovery = 39% Analysis Date = 11/06/16 Pct Recovery = 39% Analysis Date = 11/04/16 Pct Recovery = 39% Analysis Date = 11/04/16 Pct Recovery = 39% Analysis Date = 11/02/16 Pct Recovery = 39% Analysis Date = 11/02/16 Pct Recovery = 39% Analysis Date = 10/31/16 Pct Recovery = 39% Analysis Date = 10/31/16 Pct Recovery = 39% Analysis Date = 10/29/16 Pct Recovery = 39% Analysis Date = 10/29/16 Pct Recovery = 39% Analysis Date = 10/27/16 Pct Recovery = 39% Analysis Date = 10/27/16 Pct Recovery = 39% Analysis Date = 10/24/16 Pct Recovery = 39% Analysis Date = 10/24/16 Pct Recovery = 39% Analysis Date = 10/22/16 Pct Recovery = 39% Analysis Date = 10/22/16 Pct Recovery = 39% Analysis Date = 10/20/16 Pct Recovery = 39% Analysis Date = 10/20/16 Pct Recovery = 39% Analysis Date = 10/18/16 Pct Recovery = 39% Analysis Date = 10/18/16 Pct Recovery = 39% Analysis Date = 10/16/16 Pct Recovery = 39% Analysis Date = 10/16/16 Pct Recovery = 39% Analysis Date = 10/14/16 Pct Recovery = 39% Analysis Date = 10/14/16 Pct Recovery = 39% Analysis Date = 10/12/16 Pct Recovery = 39% Analysis Date = 10/12/16 Pct Recovery = 39% Analysis Date = 10/10/16 Pct Recovery = 39% Analysis Date = 10/10/16 Pct Recovery = 39% Analysis Date = 10/07/16 Pct Recovery = 39% Analysis Date = 10/07/16 Pct Recovery = 39% Analysis Date = 10/05/16 Pct Recovery = 38% Analysis Date = 10/05/16 Pct Recovery = 38% Analysis Date = 10/03/16 Pct Recovery = 38% Analysis Date = 10/03/16 Pct Recovery = 38% Analysis Date = 10/01/16 Pct Recovery = 38% Analysis Date = 10/01/16 Pct Recovery = 38% Analysis Date = 09/29/16 Pct Recovery = 38% Analysis Date = 09/29/16 Pct Recovery = 38% Analysis Date = 09/27/16 Pct Recovery = 38% Analysis Date = 09/27/16 Pct Recovery = 38% Analysis Date = 09/25/16 Pct Recovery = 38% Analysis Date = 09/25/16 Pct Recovery = 38% Analysis Date = 09/22/16 Pct Recovery = 38% Analysis Date = 09/22/16 Pct Recovery = 38% Analysis Date = 09/20/16 Pct Recovery = 38% Analysis Date = 09/20/16 Pct Recovery = 38% Analysis Date = 09/18/16 Pct Recovery = 38% Analysis Date = 09/18/16 Pct Recovery = 38% Analysis Date = 09/16/16 Pct Recovery = 38% Analysis Date = 09/16/16 Pct Recovery = 38% Analysis Date = 09/14/16 Pct Recovery = 38% Analysis Date = 09/14/16 Pct Recovery = 38% Analysis Date = 09/12/16 Pct Recovery = 38% Analysis Date = 09/12/16 Pct Recovery = 38% Analysis Date = 09/10/16 Pct Recovery = 37% Analysis Date = 09/10/16 Pct Recovery = 37% Analysis Date = 09/08/16 Pct Recovery = 37% Analysis Date = 09/08/16 Pct Recovery = 37% Analysis Date = 09/05/16 Pct Recovery = 37% Analysis Date = 09/05/16 Pct Recovery = 37% Analysis Date = 09/03/16 Pct Recovery = 37% Analysis Date = 09/03/16 Pct Recovery = 37% Analysis Date = 09/01/16 Pct Recovery = 36% Analysis Date = 09/01/16 Pct Recovery = 36% Analysis Date = 08/30/16 Pct Recovery = 36% Analysis Date = 08/30/16 Pct Recovery = 36% Analysis Date = 08/28/16 Pct Recovery = 36% Analysis Date = 08/28/16 Pct Recovery = 36% Analysis Date = 08/26/16 Pct Recovery = 36% Analysis Date = 08/26/16 Pct Recovery = 36% Analysis Date = 08/24/16 Pct Recovery = 36% Analysis Date = 08/24/16 Pct Recovery = 36% Analysis Date = 08/21/16 Pct Recovery = 36% Analysis Date = 08/21/16 Pct Recovery = 36% Analysis Date = 08/19/16 Pct Recovery = 36% Analysis Date = 08/19/16 Pct Recovery = 36% Analysis Date = 08/17/16 Pct Recovery = 36% Analysis Date = 08/17/16 Pct Recovery = 36% Analysis Date = 08/15/16 Pct Recovery = 36% Analysis Date = 08/15/16 Pct Recovery = 36% Analysis Date = 08/13/16 Pct Recovery = 36% Analysis Date = 08/13/16 Pct Recovery = 36% Analysis Date = 08/11/16 Pct Recovery = 36% Analysis Date = 08/11/16 Pct Recovery = 36% Analysis Date = 08/09/16 Pct Recovery = 36% Analysis Date = 08/09/16 Pct Recovery = 36% Analysis Date = 08/06/16 Pct Recovery = 36% Analysis Date = 08/06/16 Pct Recovery = 36% Analysis Date = 08/04/16 Pct Recovery = 36% Analysis Date = 08/04/16 Pct Recovery = 36% Analysis Date = 08/02/16 Pct Recovery = 36% Analysis Date = 08/02/16 Pct Recovery = 36% Analysis Date = 07/31/16 Pct Recovery = 36% Analysis Date = 07/31/16 Pct Recovery = 36% Analysis Date = 07/29/16 Pct Recovery = 36% Analysis Date = 07/29/16 Pct Recovery = 36% Analysis Date = 07/27/16 Pct Recovery = 36% Analysis Date = 07/27/16 Pct Recovery = 36% Analysis Date = 07/25/16 Pct Recovery = 36% Analysis Date = 07/25/16 Pct Recovery = 36% Analysis Date = 07/23/16 Pct Recovery = 36% Analysis Date = 07/23/16 Pct Recovery = 36% Analysis Date = 07/20/16 Pct Recovery = 36% Analysis Date = 07/20/16 Pct Recovery = 36% Analysis Date = 07/18/16 Pct Recovery = 36% Analysis Date = 07/18/16 Pct Recovery = 36% Analysis Date = 07/16/16 Pct Recovery = 36% Analysis Date = 07/16/16 Pct Recovery = 36% Analysis Date = 07/14/16 Pct Recovery = 36% Analysis Date = 07/14/16 Pct Recovery = 36% Analysis Date = 07/12/16 Pct Recovery = 36% Analysis Date = 07/12/16 Pct Recovery = 36% Analysis Date = 07/10/16 Pct Recovery = 36% Analysis Date = 07/10/16 Pct Recovery = 36% Analysis Date = 07/08/16 Pct Recovery = 36% Analysis Date = 07/08/16 Pct Recovery = 36% Analysis Date = 07/05/16 Pct Recovery = 36% Analysis Date = 07/05/16 Pct Recovery = 36% Analysis Date = 07/03/16 Pct Recovery = 36% Analysis Date = 07/03/16 Pct Recovery = 36% Analysis Date = 07/01/16 Pct Recovery = 36% Analysis Date = 07/01/16 Pct Recovery = 36% Analysis Date = 06/29/16 Pct Recovery = 36% Analysis Date = 06/29/16 Pct Recovery = 36% Analysis Date = 06/27/16 Pct Recovery = 36% Analysis Date = 06/27/16 Pct Recovery = 36% Analysis Date = 06/25/16 Pct Recovery = 36% Analysis Date = 06/25/16 Pct Recovery = 36% Analysis Date = 06/23/16 Pct Recovery = 36% Analysis Date = 06/23/16 Pct Recovery = 36% Analysis Date = 06/21/16 Pct Recovery = 36% Analysis Date = 06/21/16 Pct Recovery = 36% Analysis Date = 06/18/16 Pct Recovery = 36% Analysis Date = 06/18/16 Pct Recovery = 36% Analysis Date = 06/16/16 Pct Recovery = 36% Analysis Date = 06/16/16 Pct Recovery = 36% Analysis Date = 06/14/16 Pct Recovery = 36% Analysis Date = 06/14/16 Pct Recovery = 36% Analysis Date = 06/12/16 Pct Recovery = 36% Analysis Date = 06/12/16 Pct Recovery = 36% Analysis Date = 06/10/16 Pct Recovery = 36% Analysis Date = 06/10/16 Pct Recovery = 36% Analysis Date = 06/08/16 Pct Recovery = 36% Analysis Date = 06/08/16 Pct Recovery = 36% Analysis Date = 06/06/16 Pct Recovery = 36% Analysis Date = 06/06/16 Pct Recovery = 36% Analysis Date = 06/03/16 Pct Recovery = 36% Analysis Date = 06/03/16 Pct Recovery = 36% Analysis Date = 06/01/16 Pct Recovery = 36% Analysis Date = 06/01/16 Pct Recovery = 36% Analysis Date = 05/30/16 Pct Recovery = 36% Analysis Date = 05/30/16 Pct Recovery = 36% Analysis Date = 05/28/16 Pct Recovery = 36% Analysis Date = 05/28/16 Pct Recovery = 36% Analysis Date = 05/26/16 Pct Recovery = 36% Analysis Date = 05/26/16 Pct Recovery = 36% Analysis Date = 05/24/16 Pct Recovery = 36% Analysis Date = 05/24/16 Pct Recovery = 36% Analysis Date = 05/22/16 Pct Recovery = 37% Analysis Date = 05/22/16 Pct Recovery = 37% Analysis Date = 05/19/16 Pct Recovery = 37% Analysis Date = 05/19/16 Pct Recovery = 37% Analysis Date = 05/17/16 Pct Recovery = 38% Analysis Date = 05/17/16 Pct Recovery = 38% Analysis Date = 05/15/16 Pct Recovery = 38% Analysis Date = 05/15/16 Pct Recovery = 38% Analysis Date = 05/13/16 Pct Recovery = 38% Analysis Date = 05/13/16 Pct Recovery = 38% Analysis Date = 05/11/16 Pct Recovery = 39% Analysis Date = 05/11/16 Pct Recovery = 39% Analysis Date = 05/09/16 Pct Recovery = 39% Analysis Date = 05/09/16 Pct Recovery = 39% Analysis Date = 05/07/16 Pct Recovery = 39% Analysis Date = 05/07/16 Pct Recovery = 39% Analysis Date = 05/05/16 Pct Recovery = 40% Analysis Date = 05/05/16 Pct Recovery = 40% Analysis Date = 05/02/16 Pct Recovery = 40% Analysis Date = 05/02/16 Pct Recovery = 40% Analysis Date = 04/30/16 Pct Recovery = 40% Analysis Date = 04/30/16 Pct Recovery = 40% Analysis Date = 04/28/16 Pct Recovery = 40% Analysis Date = 04/28/16 Pct Recovery = 40% Analysis Date = 04/26/16 Pct Recovery = 41% Analysis Date = 04/26/16 Pct Recovery = 41% Analysis Date = 04/24/16 Pct Recovery = 41% Analysis Date = 04/24/16 Pct Recovery = 41% Analysis Date = 04/22/16 Pct Recovery = 41% Analysis Date = 04/22/16 Pct Recovery = 41% Analysis Date = 04/20/16 Pct Recovery = 42% Analysis Date = 04/20/16 Pct Recovery = 42% Analysis Date = 04/17/16 Pct Recovery = 42% Analysis Date = 04/17/16 Pct Recovery = 42% Analysis Date = 04/15/16 Pct Recovery = 42% Analysis Date = 04/15/16 Pct Recovery = 42% Analysis Date = 04/13/16 Pct Recovery = 43% Analysis Date = 04/13/16 Pct Recovery = 43% Analysis Date = 04/11/16 Pct Recovery = 43% Analysis Date = 04/11/16 Pct Recovery = 43% Analysis Date = 04/09/16 Pct Recovery = 43% Analysis Date = 04/09/16 Pct Recovery = 43% Analysis Date = 04/07/16 Pct Recovery = 43% Analysis Date = 04/07/16 Pct Recovery = 43% Analysis Date = 04/05/16 Pct Recovery = 44% Analysis Date = 04/05/16 Pct Recovery = 44% Analysis Date = 04/03/16 Pct Recovery = 44% Analysis Date = 04/03/16 Pct Recovery = 44% Analysis Date = 03/31/16 Pct Recovery = 44% Analysis Date = 03/31/16 Pct Recovery = 44% Analysis Date = 03/29/16 Pct Recovery = 44% Analysis Date = 03/29/16 Pct Recovery = 44% Analysis Date = 03/27/16 Pct Recovery = 45% Analysis Date = 03/27/16 Pct Recovery = 45% Analysis Date = 03/25/16 Pct Recovery = 45% Analysis Date = 03/25/16 Pct Recovery = 45% Analysis Date = 03/23/16 Pct Recovery = 45% Analysis Date = 03/23/16 Pct Recovery = 45% Analysis Date = 03/21/16 Pct Recovery = 46% Analysis Date = 03/21/16 Pct Recovery = 46% Analysis Date = 03/19/16 Pct Recovery = 46% Analysis Date = 03/19/16 Pct Recovery = 46% Analysis Date = 03/16/16 Pct Recovery = 46% Analysis Date = 03/16/16 Pct Recovery = 46% Analysis Date = 03/14/16 Pct Recovery = 46% Analysis Date = 03/14/16 Pct Recovery = 46% Analysis Date = 03/12/16 Pct Recovery = 47% Analysis Date = 03/12/16 Pct Recovery = 47% Analysis Date = 03/10/16 Pct Recovery = 47% Analysis Date = 03/10/16 Pct Recovery = 47% Analysis Date = 03/08/16 Pct Recovery = 47% Analysis Date = 03/08/16 Pct Recovery = 47% Analysis Date = 03/06/16 Pct Recovery = 47% Analysis Date = 03/06/16 Pct Recovery = 47% Analysis Date = 03/04/16 Pct Recovery = 48% Analysis Date = 03/04/16 Pct Recovery = 48% Analysis Date = 03/02/16 Pct Recovery = 48% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DIMETHOATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 16 39% 10% 37% 7%
Total 16 39% 10% 37% 7%

Sample Statistics
DIMETHOATE

Characteristic N % % Basis
Plotted 16 89% Spiked
Estimated Values 16 89% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 2 11% 2 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
DISULFOTON
METHOD: 2033 , TESTIDCODE: 82677GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 76% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 70% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 91% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 80% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 68% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 42% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 60% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 65% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 66% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 60% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 44% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 58% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 60% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 48% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 51% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 40% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 60% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 32% Analysis Date = 05/10/17 Pct Recovery = 66% Analysis Date = 05/08/17 Pct Recovery = 66% Analysis Date = 05/08/17 Pct Recovery = 66% Analysis Date = 05/06/17 Pct Recovery = 66% Analysis Date = 05/06/17 Pct Recovery = 66% Analysis Date = 05/04/17 Pct Recovery = 66% Analysis Date = 05/04/17 Pct Recovery = 66% Analysis Date = 05/01/17 Pct Recovery = 66% Analysis Date = 05/01/17 Pct Recovery = 66% Analysis Date = 04/29/17 Pct Recovery = 66% Analysis Date = 04/29/17 Pct Recovery = 66% Analysis Date = 04/27/17 Pct Recovery = 66% Analysis Date = 04/27/17 Pct Recovery = 66% Analysis Date = 04/25/17 Pct Recovery = 66% Analysis Date = 04/25/17 Pct Recovery = 66% Analysis Date = 04/22/17 Pct Recovery = 66% Analysis Date = 04/22/17 Pct Recovery = 66% Analysis Date = 04/20/17 Pct Recovery = 66% Analysis Date = 04/20/17 Pct Recovery = 66% Analysis Date = 04/18/17 Pct Recovery = 66% Analysis Date = 04/18/17 Pct Recovery = 66% Analysis Date = 04/15/17 Pct Recovery = 66% Analysis Date = 04/15/17 Pct Recovery = 66% Analysis Date = 04/13/17 Pct Recovery = 66% Analysis Date = 04/13/17 Pct Recovery = 66% Analysis Date = 04/11/17 Pct Recovery = 66% Analysis Date = 04/11/17 Pct Recovery = 66% Analysis Date = 04/09/17 Pct Recovery = 66% Analysis Date = 04/09/17 Pct Recovery = 66% Analysis Date = 04/06/17 Pct Recovery = 66% Analysis Date = 04/06/17 Pct Recovery = 66% Analysis Date = 04/04/17 Pct Recovery = 66% Analysis Date = 04/04/17 Pct Recovery = 66% Analysis Date = 04/02/17 Pct Recovery = 66% Analysis Date = 04/02/17 Pct Recovery = 66% Analysis Date = 03/30/17 Pct Recovery = 66% Analysis Date = 03/30/17 Pct Recovery = 66% Analysis Date = 03/28/17 Pct Recovery = 66% Analysis Date = 03/28/17 Pct Recovery = 66% Analysis Date = 03/26/17 Pct Recovery = 66% Analysis Date = 03/26/17 Pct Recovery = 66% Analysis Date = 03/24/17 Pct Recovery = 66% Analysis Date = 03/24/17 Pct Recovery = 66% Analysis Date = 03/21/17 Pct Recovery = 65% Analysis Date = 03/21/17 Pct Recovery = 65% Analysis Date = 03/19/17 Pct Recovery = 65% Analysis Date = 03/19/17 Pct Recovery = 65% Analysis Date = 03/17/17 Pct Recovery = 65% Analysis Date = 03/17/17 Pct Recovery = 65% Analysis Date = 03/14/17 Pct Recovery = 65% Analysis Date = 03/14/17 Pct Recovery = 65% Analysis Date = 03/12/17 Pct Recovery = 65% Analysis Date = 03/12/17 Pct Recovery = 65% Analysis Date = 03/10/17 Pct Recovery = 65% Analysis Date = 03/10/17 Pct Recovery = 65% Analysis Date = 03/08/17 Pct Recovery = 65% Analysis Date = 03/08/17 Pct Recovery = 65% Analysis Date = 03/05/17 Pct Recovery = 65% Analysis Date = 03/05/17 Pct Recovery = 65% Analysis Date = 03/03/17 Pct Recovery = 65% Analysis Date = 03/03/17 Pct Recovery = 65% Analysis Date = 03/01/17 Pct Recovery = 65% Analysis Date = 03/01/17 Pct Recovery = 65% Analysis Date = 02/26/17 Pct Recovery = 65% Analysis Date = 02/26/17 Pct Recovery = 65% Analysis Date = 02/24/17 Pct Recovery = 65% Analysis Date = 02/24/17 Pct Recovery = 65% Analysis Date = 02/22/17 Pct Recovery = 65% Analysis Date = 02/22/17 Pct Recovery = 65% Analysis Date = 02/20/17 Pct Recovery = 65% Analysis Date = 02/20/17 Pct Recovery = 65% Analysis Date = 02/17/17 Pct Recovery = 65% Analysis Date = 02/17/17 Pct Recovery = 65% Analysis Date = 02/15/17 Pct Recovery = 65% Analysis Date = 02/15/17 Pct Recovery = 65% Analysis Date = 02/13/17 Pct Recovery = 65% Analysis Date = 02/13/17 Pct Recovery = 65% Analysis Date = 02/10/17 Pct Recovery = 65% Analysis Date = 02/10/17 Pct Recovery = 65% Analysis Date = 02/08/17 Pct Recovery = 65% Analysis Date = 02/08/17 Pct Recovery = 65% Analysis Date = 02/06/17 Pct Recovery = 65% Analysis Date = 02/06/17 Pct Recovery = 65% Analysis Date = 02/04/17 Pct Recovery = 65% Analysis Date = 02/04/17 Pct Recovery = 65% Analysis Date = 02/01/17 Pct Recovery = 65% Analysis Date = 02/01/17 Pct Recovery = 65% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/30/17 Pct Recovery = 66% Analysis Date = 01/28/17 Pct Recovery = 66% Analysis Date = 01/28/17 Pct Recovery = 66% Analysis Date = 01/25/17 Pct Recovery = 66% Analysis Date = 01/25/17 Pct Recovery = 66% Analysis Date = 01/23/17 Pct Recovery = 66% Analysis Date = 01/23/17 Pct Recovery = 66% Analysis Date = 01/21/17 Pct Recovery = 66% Analysis Date = 01/21/17 Pct Recovery = 66% Analysis Date = 01/19/17 Pct Recovery = 66% Analysis Date = 01/19/17 Pct Recovery = 66% Analysis Date = 01/16/17 Pct Recovery = 66% Analysis Date = 01/16/17 Pct Recovery = 66% Analysis Date = 01/14/17 Pct Recovery = 66% Analysis Date = 01/14/17 Pct Recovery = 66% Analysis Date = 01/12/17 Pct Recovery = 66% Analysis Date = 01/12/17 Pct Recovery = 66% Analysis Date = 01/09/17 Pct Recovery = 66% Analysis Date = 01/09/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 66% Analysis Date = 01/07/17 Pct Recovery = 66% Analysis Date = 01/05/17 Pct Recovery = 66% Analysis Date = 01/05/17 Pct Recovery = 66% Analysis Date = 01/03/17 Pct Recovery = 66% Analysis Date = 01/03/17 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/31/16 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 66% Analysis Date = 12/29/16 Pct Recovery = 66% Analysis Date = 12/27/16 Pct Recovery = 66% Analysis Date = 12/27/16 Pct Recovery = 66% Analysis Date = 12/24/16 Pct Recovery = 66% Analysis Date = 12/24/16 Pct Recovery = 66% Analysis Date = 12/22/16 Pct Recovery = 66% Analysis Date = 12/22/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/20/16 Pct Recovery = 66% Analysis Date = 12/18/16 Pct Recovery = 66% Analysis Date = 12/18/16 Pct Recovery = 66% Analysis Date = 12/15/16 Pct Recovery = 67% Analysis Date = 12/15/16 Pct Recovery = 67% Analysis Date = 12/13/16 Pct Recovery = 67% Analysis Date = 12/13/16 Pct Recovery = 67% Analysis Date = 12/11/16 Pct Recovery = 67% Analysis Date = 12/11/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/08/16 Pct Recovery = 67% Analysis Date = 12/06/16 Pct Recovery = 67% Analysis Date = 12/06/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 67% Analysis Date = 12/04/16 Pct Recovery = 67% Analysis Date = 12/02/16 Pct Recovery = 67% Analysis Date = 12/02/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 67% Analysis Date = 11/29/16 Pct Recovery = 67% Analysis Date = 11/27/16 Pct Recovery = 67% Analysis Date = 11/27/16 Pct Recovery = 67% Analysis Date = 11/25/16 Pct Recovery = 67% Analysis Date = 11/25/16 Pct Recovery = 67% Analysis Date = 11/22/16 Pct Recovery = 68% Analysis Date = 11/22/16 Pct Recovery = 68% Analysis Date = 11/20/16 Pct Recovery = 68% Analysis Date = 11/20/16 Pct Recovery = 68% Analysis Date = 11/18/16 Pct Recovery = 68% Analysis Date = 11/18/16 Pct Recovery = 68% Analysis Date = 11/16/16 Pct Recovery = 68% Analysis Date = 11/16/16 Pct Recovery = 68% Analysis Date = 11/13/16 Pct Recovery = 68% Analysis Date = 11/13/16 Pct Recovery = 68% Analysis Date = 11/11/16 Pct Recovery = 68% Analysis Date = 11/11/16 Pct Recovery = 68% Analysis Date = 11/09/16 Pct Recovery = 68% Analysis Date = 11/09/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 10/31/16 Pct Recovery = 69% Analysis Date = 10/31/16 Pct Recovery = 69% Analysis Date = 10/28/16 Pct Recovery = 69% Analysis Date = 10/28/16 Pct Recovery = 69% Analysis Date = 10/26/16 Pct Recovery = 69% Analysis Date = 10/26/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/24/16 Pct Recovery = 69% Analysis Date = 10/21/16 Pct Recovery = 69% Analysis Date = 10/21/16 Pct Recovery = 69% Analysis Date = 10/19/16 Pct Recovery = 69% Analysis Date = 10/19/16 Pct Recovery = 69% Analysis Date = 10/17/16 Pct Recovery = 69% Analysis Date = 10/17/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/15/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/12/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 69% Analysis Date = 10/10/16 Pct Recovery = 69% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/08/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 09/29/16 Pct Recovery = 70% Analysis Date = 09/29/16 Pct Recovery = 70% Analysis Date = 09/26/16 Pct Recovery = 70% Analysis Date = 09/26/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/22/16 Pct Recovery = 70% Analysis Date = 09/22/16 Pct Recovery = 70% Analysis Date = 09/19/16 Pct Recovery = 70% Analysis Date = 09/19/16 Pct Recovery = 70% Analysis Date = 09/17/16 Pct Recovery = 71% Analysis Date = 09/17/16 Pct Recovery = 71% Analysis Date = 09/15/16 Pct Recovery = 71% Analysis Date = 09/15/16 Pct Recovery = 71% Analysis Date = 09/13/16 Pct Recovery = 71% Analysis Date = 09/13/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/10/16 Pct Recovery = 71% Analysis Date = 09/08/16 Pct Recovery = 71% Analysis Date = 09/08/16 Pct Recovery = 71% Analysis Date = 09/06/16 Pct Recovery = 72% Analysis Date = 09/06/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 09/03/16 Pct Recovery = 72% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 09/01/16 Pct Recovery = 72% Analysis Date = 08/30/16 Pct Recovery = 72% Analysis Date = 08/30/16 Pct Recovery = 72% Analysis Date = 08/28/16 Pct Recovery = 71% Analysis Date = 08/28/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 71% Analysis Date = 08/25/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/23/16 Pct Recovery = 71% Analysis Date = 08/21/16 Pct Recovery = 70% Analysis Date = 08/21/16 Pct Recovery = 70% Analysis Date = 08/18/16 Pct Recovery = 70% Analysis Date = 08/18/16 Pct Recovery = 70% Analysis Date = 08/16/16 Pct Recovery = 69% Analysis Date = 08/16/16 Pct Recovery = 69% Analysis Date = 08/14/16 Pct Recovery = 69% Analysis Date = 08/14/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 69% Analysis Date = 08/09/16 Pct Recovery = 68% Analysis Date = 08/09/16 Pct Recovery = 68% Analysis Date = 08/07/16 Pct Recovery = 68% Analysis Date = 08/07/16 Pct Recovery = 68% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 08/05/16 Pct Recovery = 67% Analysis Date = 08/02/16 Pct Recovery = 67% Analysis Date = 08/02/16 Pct Recovery = 67% Analysis Date = 07/31/16 Pct Recovery = 67% Analysis Date = 07/31/16 Pct Recovery = 67% Analysis Date = 07/29/16 Pct Recovery = 66% Analysis Date = 07/29/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/24/16 Pct Recovery = 66% Analysis Date = 07/24/16 Pct Recovery = 66% Analysis Date = 07/22/16 Pct Recovery = 65% Analysis Date = 07/22/16 Pct Recovery = 65% Analysis Date = 07/20/16 Pct Recovery = 65% Analysis Date = 07/20/16 Pct Recovery = 65% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/15/16 Pct Recovery = 64% Analysis Date = 07/15/16 Pct Recovery = 64% Analysis Date = 07/13/16 Pct Recovery = 64% Analysis Date = 07/13/16 Pct Recovery = 64% Analysis Date = 07/11/16 Pct Recovery = 63% Analysis Date = 07/11/16 Pct Recovery = 63% Analysis Date = 07/08/16 Pct Recovery = 63% Analysis Date = 07/08/16 Pct Recovery = 63% Analysis Date = 07/06/16 Pct Recovery = 62% Analysis Date = 07/06/16 Pct Recovery = 62% Analysis Date = 07/04/16 Pct Recovery = 62% Analysis Date = 07/04/16 Pct Recovery = 62% Analysis Date = 07/01/16 Pct Recovery = 62% Analysis Date = 07/01/16 Pct Recovery = 62% Analysis Date = 06/29/16 Pct Recovery = 61% Analysis Date = 06/29/16 Pct Recovery = 61% Analysis Date = 06/27/16 Pct Recovery = 61% Analysis Date = 06/27/16 Pct Recovery = 61% Analysis Date = 06/25/16 Pct Recovery = 61% Analysis Date = 06/25/16 Pct Recovery = 61% Analysis Date = 06/22/16 Pct Recovery = 60% Analysis Date = 06/22/16 Pct Recovery = 60% Analysis Date = 06/20/16 Pct Recovery = 60% Analysis Date = 06/20/16 Pct Recovery = 60% Analysis Date = 06/18/16 Pct Recovery = 59% Analysis Date = 06/18/16 Pct Recovery = 59% Analysis Date = 06/15/16 Pct Recovery = 59% Analysis Date = 06/15/16 Pct Recovery = 59% Analysis Date = 06/13/16 Pct Recovery = 59% Analysis Date = 06/13/16 Pct Recovery = 59% Analysis Date = 06/11/16 Pct Recovery = 58% Analysis Date = 06/11/16 Pct Recovery = 58% Analysis Date = 06/09/16 Pct Recovery = 58% Analysis Date = 06/09/16 Pct Recovery = 58% Analysis Date = 06/06/16 Pct Recovery = 57% Analysis Date = 06/06/16 Pct Recovery = 57% Analysis Date = 06/04/16 Pct Recovery = 57% Analysis Date = 06/04/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 06/02/16 Pct Recovery = 57% Analysis Date = 05/30/16 Pct Recovery = 56% Analysis Date = 05/30/16 Pct Recovery = 56% Analysis Date = 05/28/16 Pct Recovery = 56% Analysis Date = 05/28/16 Pct Recovery = 56% Analysis Date = 05/26/16 Pct Recovery = 55% Analysis Date = 05/26/16 Pct Recovery = 55% Analysis Date = 05/24/16 Pct Recovery = 55% Analysis Date = 05/24/16 Pct Recovery = 55% Analysis Date = 05/21/16 Pct Recovery = 54% Analysis Date = 05/21/16 Pct Recovery = 54% Analysis Date = 05/19/16 Pct Recovery = 54% Analysis Date = 05/19/16 Pct Recovery = 54% Analysis Date = 05/17/16 Pct Recovery = 53% Analysis Date = 05/17/16 Pct Recovery = 53% Analysis Date = 05/14/16 Pct Recovery = 52% Analysis Date = 05/14/16 Pct Recovery = 52% Analysis Date = 05/12/16 Pct Recovery = 52% Analysis Date = 05/12/16 Pct Recovery = 52% Analysis Date = 05/10/16 Pct Recovery = 51% Analysis Date = 05/10/16 Pct Recovery = 51% Analysis Date = 05/08/16 Pct Recovery = 51% Analysis Date = 05/08/16 Pct Recovery = 51% Analysis Date = 05/05/16 Pct Recovery = 50% Analysis Date = 05/05/16 Pct Recovery = 50% Analysis Date = 05/03/16 Pct Recovery = 50% Analysis Date = 05/03/16 Pct Recovery = 50% Analysis Date = 05/01/16 Pct Recovery = 50% Analysis Date = 05/01/16 Pct Recovery = 50% Analysis Date = 04/28/16 Pct Recovery = 49% Analysis Date = 04/28/16 Pct Recovery = 49% Analysis Date = 04/26/16 Pct Recovery = 49% Analysis Date = 04/26/16 Pct Recovery = 49% Analysis Date = 04/24/16 Pct Recovery = 49% Analysis Date = 04/24/16 Pct Recovery = 49% Analysis Date = 04/22/16 Pct Recovery = 49% Analysis Date = 04/22/16 Pct Recovery = 49% Analysis Date = 04/19/16 Pct Recovery = 49% Analysis Date = 04/19/16 Pct Recovery = 49% Analysis Date = 04/17/16 Pct Recovery = 49% Analysis Date = 04/17/16 Pct Recovery = 49% Analysis Date = 04/15/16 Pct Recovery = 48% Analysis Date = 04/15/16 Pct Recovery = 48% Analysis Date = 04/12/16 Pct Recovery = 48% Analysis Date = 04/12/16 Pct Recovery = 48% Analysis Date = 04/10/16 Pct Recovery = 48% Analysis Date = 04/10/16 Pct Recovery = 48% Analysis Date = 04/08/16 Pct Recovery = 48% Analysis Date = 04/08/16 Pct Recovery = 48% Analysis Date = 04/06/16 Pct Recovery = 48% Analysis Date = 04/06/16 Pct Recovery = 48% Analysis Date = 04/03/16 Pct Recovery = 48% Analysis Date = 04/03/16 Pct Recovery = 48% Analysis Date = 04/01/16 Pct Recovery = 48% Analysis Date = 04/01/16 Pct Recovery = 48% Analysis Date = 03/30/16 Pct Recovery = 48% Analysis Date = 03/30/16 Pct Recovery = 48% Analysis Date = 03/27/16 Pct Recovery = 48% Analysis Date = 03/27/16 Pct Recovery = 48% Analysis Date = 03/25/16 Pct Recovery = 48% Analysis Date = 03/25/16 Pct Recovery = 48% Analysis Date = 03/23/16 Pct Recovery = 47% Analysis Date = 03/23/16 Pct Recovery = 47% Analysis Date = 03/21/16 Pct Recovery = 47% Analysis Date = 03/21/16 Pct Recovery = 47% Analysis Date = 03/18/16 Pct Recovery = 47% Analysis Date = 03/18/16 Pct Recovery = 47% Analysis Date = 03/16/16 Pct Recovery = 47% Analysis Date = 03/16/16 Pct Recovery = 47% Analysis Date = 03/14/16 Pct Recovery = 47% Analysis Date = 03/14/16 Pct Recovery = 47% Analysis Date = 03/11/16 Pct Recovery = 47% Analysis Date = 03/11/16 Pct Recovery = 47% Analysis Date = 03/09/16 Pct Recovery = 47% Analysis Date = 03/09/16 Pct Recovery = 47% Analysis Date = 03/07/16 Pct Recovery = 47% Analysis Date = 03/07/16 Pct Recovery = 47% Analysis Date = 03/05/16 Pct Recovery = 47% Analysis Date = 03/05/16 Pct Recovery = 47% Analysis Date = 03/02/16 Pct Recovery = 47% Analysis Date = 03/02/16 Pct Recovery = 47% Analysis Date = 02/29/16 Pct Recovery = 47% Analysis Date = 02/29/16 Pct Recovery = 47% Analysis Date = 02/27/16 Pct Recovery = 47% Analysis Date = 02/27/16 Pct Recovery = 47% Analysis Date = 02/24/16 Pct Recovery = 47% Analysis Date = 02/24/16 Pct Recovery = 47% Analysis Date = 02/22/16 Pct Recovery = 47% Analysis Date = 02/22/16 Pct Recovery = 47% Analysis Date = 02/20/16 Pct Recovery = 47% Analysis Date = 02/20/16 Pct Recovery = 47% Analysis Date = 02/18/16 Pct Recovery = 47% Analysis Date = 02/18/16 Pct Recovery = 47% Analysis Date = 02/15/16 Pct Recovery = 47% Analysis Date = 02/15/16 Pct Recovery = 47% Analysis Date = 02/13/16 Pct Recovery = 46% Analysis Date = 02/13/16 Pct Recovery = 46% Analysis Date = 02/11/16 Pct Recovery = 46% Analysis Date = 02/11/16 Pct Recovery = 46% Analysis Date = 02/09/16 Pct Recovery = 46% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 61% 15% 60% 14%
Total 20 61% 15% 60% 14%

Sample Statistics
DISULFOTON

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 20 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
DISULFOTON SULFONE
METHOD: 2033 , TESTIDCODE: 61640GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 101% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 93% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 99% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 69% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 98% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 97% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 96% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 130% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 113% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 76% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 97% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 98% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 100% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 94% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 05/02/17 Pct Recovery = 106% Analysis Date = 04/30/17 Pct Recovery = 106% Analysis Date = 04/30/17 Pct Recovery = 106% Analysis Date = 04/28/17 Pct Recovery = 106% Analysis Date = 04/28/17 Pct Recovery = 106% Analysis Date = 04/26/17 Pct Recovery = 106% Analysis Date = 04/26/17 Pct Recovery = 106% Analysis Date = 04/24/17 Pct Recovery = 105% Analysis Date = 04/24/17 Pct Recovery = 105% Analysis Date = 04/22/17 Pct Recovery = 105% Analysis Date = 04/22/17 Pct Recovery = 105% Analysis Date = 04/20/17 Pct Recovery = 105% Analysis Date = 04/20/17 Pct Recovery = 105% Analysis Date = 04/18/17 Pct Recovery = 105% Analysis Date = 04/18/17 Pct Recovery = 105% Analysis Date = 04/15/17 Pct Recovery = 105% Analysis Date = 04/15/17 Pct Recovery = 105% Analysis Date = 04/13/17 Pct Recovery = 105% Analysis Date = 04/13/17 Pct Recovery = 105% Analysis Date = 04/11/17 Pct Recovery = 105% Analysis Date = 04/11/17 Pct Recovery = 105% Analysis Date = 04/09/17 Pct Recovery = 104% Analysis Date = 04/09/17 Pct Recovery = 104% Analysis Date = 04/07/17 Pct Recovery = 104% Analysis Date = 04/07/17 Pct Recovery = 104% Analysis Date = 04/05/17 Pct Recovery = 104% Analysis Date = 04/05/17 Pct Recovery = 104% Analysis Date = 04/03/17 Pct Recovery = 104% Analysis Date = 04/03/17 Pct Recovery = 104% Analysis Date = 03/31/17 Pct Recovery = 104% Analysis Date = 03/31/17 Pct Recovery = 104% Analysis Date = 03/29/17 Pct Recovery = 104% Analysis Date = 03/29/17 Pct Recovery = 104% Analysis Date = 03/27/17 Pct Recovery = 104% Analysis Date = 03/27/17 Pct Recovery = 104% Analysis Date = 03/25/17 Pct Recovery = 104% Analysis Date = 03/25/17 Pct Recovery = 104% Analysis Date = 03/23/17 Pct Recovery = 103% Analysis Date = 03/23/17 Pct Recovery = 103% Analysis Date = 03/21/17 Pct Recovery = 103% Analysis Date = 03/21/17 Pct Recovery = 103% Analysis Date = 03/19/17 Pct Recovery = 103% Analysis Date = 03/19/17 Pct Recovery = 103% Analysis Date = 03/17/17 Pct Recovery = 103% Analysis Date = 03/17/17 Pct Recovery = 103% Analysis Date = 03/14/17 Pct Recovery = 103% Analysis Date = 03/14/17 Pct Recovery = 103% Analysis Date = 03/12/17 Pct Recovery = 103% Analysis Date = 03/12/17 Pct Recovery = 103% Analysis Date = 03/10/17 Pct Recovery = 103% Analysis Date = 03/10/17 Pct Recovery = 103% Analysis Date = 03/08/17 Pct Recovery = 102% Analysis Date = 03/08/17 Pct Recovery = 102% Analysis Date = 03/06/17 Pct Recovery = 102% Analysis Date = 03/06/17 Pct Recovery = 102% Analysis Date = 03/04/17 Pct Recovery = 102% Analysis Date = 03/04/17 Pct Recovery = 102% Analysis Date = 03/02/17 Pct Recovery = 102% Analysis Date = 03/02/17 Pct Recovery = 102% Analysis Date = 02/27/17 Pct Recovery = 102% Analysis Date = 02/27/17 Pct Recovery = 102% Analysis Date = 02/25/17 Pct Recovery = 102% Analysis Date = 02/25/17 Pct Recovery = 102% Analysis Date = 02/23/17 Pct Recovery = 101% Analysis Date = 02/23/17 Pct Recovery = 101% Analysis Date = 02/21/17 Pct Recovery = 101% Analysis Date = 02/21/17 Pct Recovery = 101% Analysis Date = 02/19/17 Pct Recovery = 101% Analysis Date = 02/19/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 100% Analysis Date = 02/13/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 100% Analysis Date = 02/06/17 Pct Recovery = 99% Analysis Date = 02/06/17 Pct Recovery = 99% Analysis Date = 02/04/17 Pct Recovery = 99% Analysis Date = 02/04/17 Pct Recovery = 99% Analysis Date = 02/02/17 Pct Recovery = 99% Analysis Date = 02/02/17 Pct Recovery = 99% Analysis Date = 01/31/17 Pct Recovery = 98% Analysis Date = 01/31/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/26/17 Pct Recovery = 98% Analysis Date = 01/26/17 Pct Recovery = 98% Analysis Date = 01/24/17 Pct Recovery = 97% Analysis Date = 01/24/17 Pct Recovery = 97% Analysis Date = 01/22/17 Pct Recovery = 97% Analysis Date = 01/22/17 Pct Recovery = 97% Analysis Date = 01/20/17 Pct Recovery = 97% Analysis Date = 01/20/17 Pct Recovery = 97% Analysis Date = 01/18/17 Pct Recovery = 96% Analysis Date = 01/18/17 Pct Recovery = 96% Analysis Date = 01/16/17 Pct Recovery = 96% Analysis Date = 01/16/17 Pct Recovery = 96% Analysis Date = 01/14/17 Pct Recovery = 96% Analysis Date = 01/14/17 Pct Recovery = 96% Analysis Date = 01/11/17 Pct Recovery = 96% Analysis Date = 01/11/17 Pct Recovery = 96% Analysis Date = 01/09/17 Pct Recovery = 95% Analysis Date = 01/09/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/05/17 Pct Recovery = 95% Analysis Date = 01/05/17 Pct Recovery = 95% Analysis Date = 01/03/17 Pct Recovery = 94% Analysis Date = 01/03/17 Pct Recovery = 94% Analysis Date = 01/01/17 Pct Recovery = 94% Analysis Date = 01/01/17 Pct Recovery = 94% Analysis Date = 12/30/16 Pct Recovery = 94% Analysis Date = 12/30/16 Pct Recovery = 94% Analysis Date = 12/28/16 Pct Recovery = 93% Analysis Date = 12/28/16 Pct Recovery = 93% Analysis Date = 12/25/16 Pct Recovery = 93% Analysis Date = 12/25/16 Pct Recovery = 93% Analysis Date = 12/23/16 Pct Recovery = 93% Analysis Date = 12/23/16 Pct Recovery = 93% Analysis Date = 12/21/16 Pct Recovery = 92% Analysis Date = 12/21/16 Pct Recovery = 92% Analysis Date = 12/19/16 Pct Recovery = 92% Analysis Date = 12/19/16 Pct Recovery = 92% Analysis Date = 12/17/16 Pct Recovery = 92% Analysis Date = 12/17/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/10/16 Pct Recovery = 91% Analysis Date = 12/10/16 Pct Recovery = 91% Analysis Date = 12/08/16 Pct Recovery = 91% Analysis Date = 12/08/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 11/30/16 Pct Recovery = 91% Analysis Date = 11/30/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 90% Analysis Date = 11/28/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/26/16 Pct Recovery = 90% Analysis Date = 11/23/16 Pct Recovery = 90% Analysis Date = 11/23/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/21/16 Pct Recovery = 90% Analysis Date = 11/19/16 Pct Recovery = 90% Analysis Date = 11/19/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 90% Analysis Date = 11/17/16 Pct Recovery = 90% Analysis Date = 11/15/16 Pct Recovery = 89% Analysis Date = 11/15/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/11/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/08/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/04/16 Pct Recovery = 89% Analysis Date = 11/04/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 89% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 88% Analysis Date = 10/27/16 Pct Recovery = 88% Analysis Date = 10/27/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/22/16 Pct Recovery = 88% Analysis Date = 10/22/16 Pct Recovery = 88% Analysis Date = 10/20/16 Pct Recovery = 88% Analysis Date = 10/20/16 Pct Recovery = 88% Analysis Date = 10/18/16 Pct Recovery = 87% Analysis Date = 10/18/16 Pct Recovery = 87% Analysis Date = 10/16/16 Pct Recovery = 87% Analysis Date = 10/16/16 Pct Recovery = 87% Analysis Date = 10/14/16 Pct Recovery = 87% Analysis Date = 10/14/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/07/16 Pct Recovery = 87% Analysis Date = 10/07/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 10/05/16 Pct Recovery = 86% Analysis Date = 10/03/16 Pct Recovery = 86% Analysis Date = 10/03/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 10/01/16 Pct Recovery = 86% Analysis Date = 09/29/16 Pct Recovery = 86% Analysis Date = 09/29/16 Pct Recovery = 86% Analysis Date = 09/27/16 Pct Recovery = 86% Analysis Date = 09/27/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 86% Analysis Date = 09/25/16 Pct Recovery = 86% Analysis Date = 09/22/16 Pct Recovery = 86% Analysis Date = 09/22/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/16/16 Pct Recovery = 85% Analysis Date = 09/16/16 Pct Recovery = 85% Analysis Date = 09/14/16 Pct Recovery = 85% Analysis Date = 09/14/16 Pct Recovery = 85% Analysis Date = 09/12/16 Pct Recovery = 85% Analysis Date = 09/12/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/10/16 Pct Recovery = 85% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/05/16 Pct Recovery = 84% Analysis Date = 09/05/16 Pct Recovery = 84% Analysis Date = 09/03/16 Pct Recovery = 84% Analysis Date = 09/03/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/26/16 Pct Recovery = 85% Analysis Date = 08/24/16 Pct Recovery = 85% Analysis Date = 08/24/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/19/16 Pct Recovery = 86% Analysis Date = 08/17/16 Pct Recovery = 86% Analysis Date = 08/17/16 Pct Recovery = 86% Analysis Date = 08/15/16 Pct Recovery = 86% Analysis Date = 08/15/16 Pct Recovery = 86% Analysis Date = 08/13/16 Pct Recovery = 86% Analysis Date = 08/13/16 Pct Recovery = 86% Analysis Date = 08/11/16 Pct Recovery = 87% Analysis Date = 08/11/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/06/16 Pct Recovery = 87% Analysis Date = 08/06/16 Pct Recovery = 87% Analysis Date = 08/04/16 Pct Recovery = 88% Analysis Date = 08/04/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/27/16 Pct Recovery = 89% Analysis Date = 07/27/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/25/16 Pct Recovery = 89% Analysis Date = 07/23/16 Pct Recovery = 89% Analysis Date = 07/23/16 Pct Recovery = 89% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/20/16 Pct Recovery = 90% Analysis Date = 07/18/16 Pct Recovery = 90% Analysis Date = 07/18/16 Pct Recovery = 90% Analysis Date = 07/16/16 Pct Recovery = 90% Analysis Date = 07/16/16 Pct Recovery = 90% Analysis Date = 07/14/16 Pct Recovery = 90% Analysis Date = 07/14/16 Pct Recovery = 90% Analysis Date = 07/12/16 Pct Recovery = 91% Analysis Date = 07/12/16 Pct Recovery = 91% Analysis Date = 07/10/16 Pct Recovery = 91% Analysis Date = 07/10/16 Pct Recovery = 91% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/05/16 Pct Recovery = 91% Analysis Date = 07/05/16 Pct Recovery = 91% Analysis Date = 07/03/16 Pct Recovery = 92% Analysis Date = 07/03/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/23/16 Pct Recovery = 93% Analysis Date = 06/23/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/21/16 Pct Recovery = 93% Analysis Date = 06/18/16 Pct Recovery = 94% Analysis Date = 06/18/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/14/16 Pct Recovery = 94% Analysis Date = 06/14/16 Pct Recovery = 94% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 96% Analysis Date = 06/03/16 Pct Recovery = 96% Analysis Date = 06/01/16 Pct Recovery = 96% Analysis Date = 06/01/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/28/16 Pct Recovery = 97% Analysis Date = 05/26/16 Pct Recovery = 97% Analysis Date = 05/26/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/24/16 Pct Recovery = 97% Analysis Date = 05/22/16 Pct Recovery = 97% Analysis Date = 05/22/16 Pct Recovery = 97% Analysis Date = 05/19/16 Pct Recovery = 97% Analysis Date = 05/19/16 Pct Recovery = 97% Analysis Date = 05/17/16 Pct Recovery = 97% Analysis Date = 05/17/16 Pct Recovery = 97% Analysis Date = 05/15/16 Pct Recovery = 97% Analysis Date = 05/15/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/13/16 Pct Recovery = 97% Analysis Date = 05/11/16 Pct Recovery = 96% Analysis Date = 05/11/16 Pct Recovery = 96% Analysis Date = 05/09/16 Pct Recovery = 96% Analysis Date = 05/09/16 Pct Recovery = 96% Analysis Date = 05/07/16 Pct Recovery = 96% Analysis Date = 05/07/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/02/16 Pct Recovery = 96% Analysis Date = 05/02/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/30/16 Pct Recovery = 96% Analysis Date = 04/28/16 Pct Recovery = 96% Analysis Date = 04/28/16 Pct Recovery = 96% Analysis Date = 04/26/16 Pct Recovery = 96% Analysis Date = 04/26/16 Pct Recovery = 96% Analysis Date = 04/24/16 Pct Recovery = 95% Analysis Date = 04/24/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/22/16 Pct Recovery = 95% Analysis Date = 04/20/16 Pct Recovery = 95% Analysis Date = 04/20/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/17/16 Pct Recovery = 95% Analysis Date = 04/15/16 Pct Recovery = 95% Analysis Date = 04/15/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/13/16 Pct Recovery = 95% Analysis Date = 04/11/16 Pct Recovery = 95% Analysis Date = 04/11/16 Pct Recovery = 95% Analysis Date = 04/09/16 Pct Recovery = 94% Analysis Date = 04/09/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/07/16 Pct Recovery = 94% Analysis Date = 04/05/16 Pct Recovery = 94% Analysis Date = 04/05/16 Pct Recovery = 94% Analysis Date = 04/03/16 Pct Recovery = 94% Analysis Date = 04/03/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/31/16 Pct Recovery = 94% Analysis Date = 03/29/16 Pct Recovery = 93% Analysis Date = 03/29/16 Pct Recovery = 93% Analysis Date = 03/27/16 Pct Recovery = 93% Analysis Date = 03/27/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/25/16 Pct Recovery = 93% Analysis Date = 03/23/16 Pct Recovery = 93% Analysis Date = 03/23/16 Pct Recovery = 93% Analysis Date = 03/21/16 Pct Recovery = 93% Analysis Date = 03/21/16 Pct Recovery = 93% Analysis Date = 03/19/16 Pct Recovery = 92% Analysis Date = 03/19/16 Pct Recovery = 92% Analysis Date = 03/16/16 Pct Recovery = 92% Analysis Date = 03/16/16 Pct Recovery = 92% Analysis Date = 03/14/16 Pct Recovery = 92% Analysis Date = 03/14/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/12/16 Pct Recovery = 92% Analysis Date = 03/10/16 Pct Recovery = 92% Analysis Date = 03/10/16 Pct Recovery = 92% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/08/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/06/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
DISULFOTON SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 96% 13% 97% 6%
Total 18 96% 13% 97% 6%

Sample Statistics
DISULFOTON SULFONE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
ENDOSULFAN SULFATE
METHOD: 2033 , TESTIDCODE: 61590GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 101% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 80% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 96% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 71% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 88% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 69% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 100% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 77% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 117% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 73% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 71% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 05/10/17 Pct Recovery = 83% Analysis Date = 05/08/17 Pct Recovery = 83% Analysis Date = 05/08/17 Pct Recovery = 83% Analysis Date = 05/06/17 Pct Recovery = 83% Analysis Date = 05/06/17 Pct Recovery = 83% Analysis Date = 05/04/17 Pct Recovery = 84% Analysis Date = 05/04/17 Pct Recovery = 84% Analysis Date = 05/01/17 Pct Recovery = 84% Analysis Date = 05/01/17 Pct Recovery = 84% Analysis Date = 04/29/17 Pct Recovery = 84% Analysis Date = 04/29/17 Pct Recovery = 84% Analysis Date = 04/27/17 Pct Recovery = 84% Analysis Date = 04/27/17 Pct Recovery = 84% Analysis Date = 04/25/17 Pct Recovery = 84% Analysis Date = 04/25/17 Pct Recovery = 84% Analysis Date = 04/22/17 Pct Recovery = 84% Analysis Date = 04/22/17 Pct Recovery = 84% Analysis Date = 04/20/17 Pct Recovery = 84% Analysis Date = 04/20/17 Pct Recovery = 84% Analysis Date = 04/18/17 Pct Recovery = 84% Analysis Date = 04/18/17 Pct Recovery = 84% Analysis Date = 04/15/17 Pct Recovery = 85% Analysis Date = 04/15/17 Pct Recovery = 85% Analysis Date = 04/13/17 Pct Recovery = 85% Analysis Date = 04/13/17 Pct Recovery = 85% Analysis Date = 04/11/17 Pct Recovery = 85% Analysis Date = 04/11/17 Pct Recovery = 85% Analysis Date = 04/09/17 Pct Recovery = 85% Analysis Date = 04/09/17 Pct Recovery = 85% Analysis Date = 04/06/17 Pct Recovery = 85% Analysis Date = 04/06/17 Pct Recovery = 85% Analysis Date = 04/04/17 Pct Recovery = 85% Analysis Date = 04/04/17 Pct Recovery = 85% Analysis Date = 04/02/17 Pct Recovery = 85% Analysis Date = 04/02/17 Pct Recovery = 85% Analysis Date = 03/30/17 Pct Recovery = 86% Analysis Date = 03/30/17 Pct Recovery = 86% Analysis Date = 03/28/17 Pct Recovery = 86% Analysis Date = 03/28/17 Pct Recovery = 86% Analysis Date = 03/26/17 Pct Recovery = 86% Analysis Date = 03/26/17 Pct Recovery = 86% Analysis Date = 03/24/17 Pct Recovery = 86% Analysis Date = 03/24/17 Pct Recovery = 86% Analysis Date = 03/21/17 Pct Recovery = 86% Analysis Date = 03/21/17 Pct Recovery = 86% Analysis Date = 03/19/17 Pct Recovery = 86% Analysis Date = 03/19/17 Pct Recovery = 86% Analysis Date = 03/17/17 Pct Recovery = 86% Analysis Date = 03/17/17 Pct Recovery = 86% Analysis Date = 03/14/17 Pct Recovery = 87% Analysis Date = 03/14/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/10/17 Pct Recovery = 87% Analysis Date = 03/10/17 Pct Recovery = 87% Analysis Date = 03/08/17 Pct Recovery = 87% Analysis Date = 03/08/17 Pct Recovery = 87% Analysis Date = 03/05/17 Pct Recovery = 87% Analysis Date = 03/05/17 Pct Recovery = 87% Analysis Date = 03/03/17 Pct Recovery = 87% Analysis Date = 03/03/17 Pct Recovery = 87% Analysis Date = 03/01/17 Pct Recovery = 87% Analysis Date = 03/01/17 Pct Recovery = 87% Analysis Date = 02/26/17 Pct Recovery = 88% Analysis Date = 02/26/17 Pct Recovery = 88% Analysis Date = 02/24/17 Pct Recovery = 88% Analysis Date = 02/24/17 Pct Recovery = 88% Analysis Date = 02/22/17 Pct Recovery = 88% Analysis Date = 02/22/17 Pct Recovery = 88% Analysis Date = 02/20/17 Pct Recovery = 88% Analysis Date = 02/20/17 Pct Recovery = 88% Analysis Date = 02/17/17 Pct Recovery = 88% Analysis Date = 02/17/17 Pct Recovery = 88% Analysis Date = 02/15/17 Pct Recovery = 88% Analysis Date = 02/15/17 Pct Recovery = 88% Analysis Date = 02/13/17 Pct Recovery = 88% Analysis Date = 02/13/17 Pct Recovery = 88% Analysis Date = 02/10/17 Pct Recovery = 89% Analysis Date = 02/10/17 Pct Recovery = 89% Analysis Date = 02/08/17 Pct Recovery = 89% Analysis Date = 02/08/17 Pct Recovery = 89% Analysis Date = 02/06/17 Pct Recovery = 89% Analysis Date = 02/06/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/01/17 Pct Recovery = 89% Analysis Date = 02/01/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/23/17 Pct Recovery = 90% Analysis Date = 01/23/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/19/17 Pct Recovery = 90% Analysis Date = 01/19/17 Pct Recovery = 90% Analysis Date = 01/16/17 Pct Recovery = 90% Analysis Date = 01/16/17 Pct Recovery = 90% Analysis Date = 01/14/17 Pct Recovery = 90% Analysis Date = 01/14/17 Pct Recovery = 90% Analysis Date = 01/12/17 Pct Recovery = 90% Analysis Date = 01/12/17 Pct Recovery = 90% Analysis Date = 01/09/17 Pct Recovery = 90% Analysis Date = 01/09/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/05/17 Pct Recovery = 91% Analysis Date = 01/05/17 Pct Recovery = 91% Analysis Date = 01/03/17 Pct Recovery = 91% Analysis Date = 01/03/17 Pct Recovery = 91% Analysis Date = 12/31/16 Pct Recovery = 91% Analysis Date = 12/31/16 Pct Recovery = 91% Analysis Date = 12/29/16 Pct Recovery = 91% Analysis Date = 12/29/16 Pct Recovery = 91% Analysis Date = 12/27/16 Pct Recovery = 91% Analysis Date = 12/27/16 Pct Recovery = 91% Analysis Date = 12/24/16 Pct Recovery = 91% Analysis Date = 12/24/16 Pct Recovery = 91% Analysis Date = 12/22/16 Pct Recovery = 92% Analysis Date = 12/22/16 Pct Recovery = 92% Analysis Date = 12/20/16 Pct Recovery = 92% Analysis Date = 12/20/16 Pct Recovery = 92% Analysis Date = 12/18/16 Pct Recovery = 92% Analysis Date = 12/18/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/08/16 Pct Recovery = 92% Analysis Date = 12/08/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 11/29/16 Pct Recovery = 91% Analysis Date = 11/29/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/04/16 Pct Recovery = 91% Analysis Date = 11/04/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 11/02/16 Pct Recovery = 91% Analysis Date = 10/31/16 Pct Recovery = 91% Analysis Date = 10/31/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/26/16 Pct Recovery = 91% Analysis Date = 10/26/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/24/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/21/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/10/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/08/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 91% Analysis Date = 09/24/16 Pct Recovery = 90% Analysis Date = 09/24/16 Pct Recovery = 90% Analysis Date = 09/22/16 Pct Recovery = 90% Analysis Date = 09/22/16 Pct Recovery = 90% Analysis Date = 09/19/16 Pct Recovery = 90% Analysis Date = 09/19/16 Pct Recovery = 90% Analysis Date = 09/17/16 Pct Recovery = 90% Analysis Date = 09/17/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/13/16 Pct Recovery = 90% Analysis Date = 09/13/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/08/16 Pct Recovery = 90% Analysis Date = 09/08/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 91% Analysis Date = 09/06/16 Pct Recovery = 91% Analysis Date = 09/03/16 Pct Recovery = 91% Analysis Date = 09/03/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 90% Analysis Date = 08/30/16 Pct Recovery = 90% Analysis Date = 08/28/16 Pct Recovery = 90% Analysis Date = 08/28/16 Pct Recovery = 90% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 88% Analysis Date = 08/18/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 84% Analysis Date = 07/27/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 83% Analysis Date = 07/22/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 82% Analysis Date = 07/17/16 Pct Recovery = 82% Analysis Date = 07/15/16 Pct Recovery = 82% Analysis Date = 07/15/16 Pct Recovery = 82% Analysis Date = 07/13/16 Pct Recovery = 82% Analysis Date = 07/13/16 Pct Recovery = 82% Analysis Date = 07/11/16 Pct Recovery = 81% Analysis Date = 07/11/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/08/16 Pct Recovery = 81% Analysis Date = 07/06/16 Pct Recovery = 80% Analysis Date = 07/06/16 Pct Recovery = 80% Analysis Date = 07/04/16 Pct Recovery = 80% Analysis Date = 07/04/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 80% Analysis Date = 06/29/16 Pct Recovery = 79% Analysis Date = 06/29/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/25/16 Pct Recovery = 78% Analysis Date = 06/25/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/22/16 Pct Recovery = 78% Analysis Date = 06/20/16 Pct Recovery = 78% Analysis Date = 06/20/16 Pct Recovery = 78% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 77% Analysis Date = 06/13/16 Pct Recovery = 76% Analysis Date = 06/13/16 Pct Recovery = 76% Analysis Date = 06/11/16 Pct Recovery = 76% Analysis Date = 06/11/16 Pct Recovery = 76% Analysis Date = 06/09/16 Pct Recovery = 76% Analysis Date = 06/09/16 Pct Recovery = 76% Analysis Date = 06/06/16 Pct Recovery = 75% Analysis Date = 06/06/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 75% Analysis Date = 06/04/16 Pct Recovery = 75% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 06/02/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 73% Analysis Date = 05/28/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/26/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/24/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 74% Analysis Date = 05/21/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 74% Analysis Date = 05/19/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 74% Analysis Date = 05/17/16 Pct Recovery = 74% Analysis Date = 05/14/16 Pct Recovery = 74% Analysis Date = 05/14/16 Pct Recovery = 74% Analysis Date = 05/12/16 Pct Recovery = 74% Analysis Date = 05/12/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/10/16 Pct Recovery = 74% Analysis Date = 05/08/16 Pct Recovery = 74% Analysis Date = 05/08/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/05/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 75% Analysis Date = 05/03/16 Pct Recovery = 75% Analysis Date = 05/01/16 Pct Recovery = 75% Analysis Date = 05/01/16 Pct Recovery = 75% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 76% Analysis Date = 04/24/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/19/16 Pct Recovery = 76% Analysis Date = 04/19/16 Pct Recovery = 76% Analysis Date = 04/17/16 Pct Recovery = 77% Analysis Date = 04/17/16 Pct Recovery = 77% Analysis Date = 04/15/16 Pct Recovery = 77% Analysis Date = 04/15/16 Pct Recovery = 77% Analysis Date = 04/12/16 Pct Recovery = 77% Analysis Date = 04/12/16 Pct Recovery = 77% Analysis Date = 04/10/16 Pct Recovery = 77% Analysis Date = 04/10/16 Pct Recovery = 77% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 79% Analysis Date = 04/01/16 Pct Recovery = 79% Analysis Date = 03/30/16 Pct Recovery = 79% Analysis Date = 03/30/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 80% Analysis Date = 03/27/16 Pct Recovery = 80% Analysis Date = 03/25/16 Pct Recovery = 80% Analysis Date = 03/25/16 Pct Recovery = 80% Analysis Date = 03/23/16 Pct Recovery = 80% Analysis Date = 03/23/16 Pct Recovery = 80% Analysis Date = 03/21/16 Pct Recovery = 81% Analysis Date = 03/21/16 Pct Recovery = 81% Analysis Date = 03/18/16 Pct Recovery = 81% Analysis Date = 03/18/16 Pct Recovery = 81% Analysis Date = 03/16/16 Pct Recovery = 81% Analysis Date = 03/16/16 Pct Recovery = 81% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/09/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/07/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 03/05/16 Pct Recovery = 83% Analysis Date = 03/02/16 Pct Recovery = 84% Analysis Date = 03/02/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 87% Analysis Date = 02/13/16 Pct Recovery = 87% Analysis Date = 02/11/16 Pct Recovery = 87% Analysis Date = 02/11/16 Pct Recovery = 87% Analysis Date = 02/09/16 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ENDOSULFAN SULFATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 83% 13% 81% 13%
Total 20 83% 13% 81% 13%

Sample Statistics
ENDOSULFAN SULFATE

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
EPTC
METHOD: 2033 , TESTIDCODE: 82668GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 121% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 107% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 97% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 100% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 80% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 98% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 97% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 105% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 137% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 110% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 112% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 104% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 96% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 98% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 101% Analysis Date = 05/02/17 Pct Recovery = 109% Analysis Date = 04/30/17 Pct Recovery = 109% Analysis Date = 04/30/17 Pct Recovery = 109% Analysis Date = 04/28/17 Pct Recovery = 109% Analysis Date = 04/28/17 Pct Recovery = 109% Analysis Date = 04/26/17 Pct Recovery = 109% Analysis Date = 04/26/17 Pct Recovery = 109% Analysis Date = 04/24/17 Pct Recovery = 109% Analysis Date = 04/24/17 Pct Recovery = 109% Analysis Date = 04/21/17 Pct Recovery = 109% Analysis Date = 04/21/17 Pct Recovery = 109% Analysis Date = 04/19/17 Pct Recovery = 109% Analysis Date = 04/19/17 Pct Recovery = 109% Analysis Date = 04/17/17 Pct Recovery = 109% Analysis Date = 04/17/17 Pct Recovery = 109% Analysis Date = 04/15/17 Pct Recovery = 109% Analysis Date = 04/15/17 Pct Recovery = 109% Analysis Date = 04/12/17 Pct Recovery = 110% Analysis Date = 04/12/17 Pct Recovery = 110% Analysis Date = 04/10/17 Pct Recovery = 110% Analysis Date = 04/10/17 Pct Recovery = 110% Analysis Date = 04/08/17 Pct Recovery = 110% Analysis Date = 04/08/17 Pct Recovery = 110% Analysis Date = 04/06/17 Pct Recovery = 110% Analysis Date = 04/06/17 Pct Recovery = 110% Analysis Date = 04/03/17 Pct Recovery = 110% Analysis Date = 04/03/17 Pct Recovery = 110% Analysis Date = 04/01/17 Pct Recovery = 110% Analysis Date = 04/01/17 Pct Recovery = 110% Analysis Date = 03/30/17 Pct Recovery = 110% Analysis Date = 03/30/17 Pct Recovery = 110% Analysis Date = 03/28/17 Pct Recovery = 110% Analysis Date = 03/28/17 Pct Recovery = 110% Analysis Date = 03/25/17 Pct Recovery = 110% Analysis Date = 03/25/17 Pct Recovery = 110% Analysis Date = 03/23/17 Pct Recovery = 110% Analysis Date = 03/23/17 Pct Recovery = 110% Analysis Date = 03/21/17 Pct Recovery = 110% Analysis Date = 03/21/17 Pct Recovery = 110% Analysis Date = 03/19/17 Pct Recovery = 111% Analysis Date = 03/19/17 Pct Recovery = 111% Analysis Date = 03/16/17 Pct Recovery = 111% Analysis Date = 03/16/17 Pct Recovery = 111% Analysis Date = 03/14/17 Pct Recovery = 111% Analysis Date = 03/14/17 Pct Recovery = 111% Analysis Date = 03/12/17 Pct Recovery = 111% Analysis Date = 03/12/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 111% Analysis Date = 03/07/17 Pct Recovery = 111% Analysis Date = 03/07/17 Pct Recovery = 111% Analysis Date = 03/05/17 Pct Recovery = 111% Analysis Date = 03/05/17 Pct Recovery = 111% Analysis Date = 03/03/17 Pct Recovery = 111% Analysis Date = 03/03/17 Pct Recovery = 111% Analysis Date = 03/01/17 Pct Recovery = 111% Analysis Date = 03/01/17 Pct Recovery = 111% Analysis Date = 02/26/17 Pct Recovery = 111% Analysis Date = 02/26/17 Pct Recovery = 111% Analysis Date = 02/24/17 Pct Recovery = 111% Analysis Date = 02/24/17 Pct Recovery = 111% Analysis Date = 02/22/17 Pct Recovery = 111% Analysis Date = 02/22/17 Pct Recovery = 111% Analysis Date = 02/20/17 Pct Recovery = 112% Analysis Date = 02/20/17 Pct Recovery = 112% Analysis Date = 02/17/17 Pct Recovery = 112% Analysis Date = 02/17/17 Pct Recovery = 112% Analysis Date = 02/15/17 Pct Recovery = 112% Analysis Date = 02/15/17 Pct Recovery = 112% Analysis Date = 02/13/17 Pct Recovery = 111% Analysis Date = 02/13/17 Pct Recovery = 111% Analysis Date = 02/11/17 Pct Recovery = 111% Analysis Date = 02/11/17 Pct Recovery = 111% Analysis Date = 02/08/17 Pct Recovery = 111% Analysis Date = 02/08/17 Pct Recovery = 111% Analysis Date = 02/06/17 Pct Recovery = 111% Analysis Date = 02/06/17 Pct Recovery = 111% Analysis Date = 02/04/17 Pct Recovery = 111% Analysis Date = 02/04/17 Pct Recovery = 111% Analysis Date = 02/02/17 Pct Recovery = 111% Analysis Date = 02/02/17 Pct Recovery = 111% Analysis Date = 01/30/17 Pct Recovery = 111% Analysis Date = 01/30/17 Pct Recovery = 111% Analysis Date = 01/28/17 Pct Recovery = 111% Analysis Date = 01/28/17 Pct Recovery = 111% Analysis Date = 01/26/17 Pct Recovery = 110% Analysis Date = 01/26/17 Pct Recovery = 110% Analysis Date = 01/24/17 Pct Recovery = 110% Analysis Date = 01/24/17 Pct Recovery = 110% Analysis Date = 01/21/17 Pct Recovery = 110% Analysis Date = 01/21/17 Pct Recovery = 110% Analysis Date = 01/19/17 Pct Recovery = 110% Analysis Date = 01/19/17 Pct Recovery = 110% Analysis Date = 01/17/17 Pct Recovery = 110% Analysis Date = 01/17/17 Pct Recovery = 110% Analysis Date = 01/15/17 Pct Recovery = 110% Analysis Date = 01/15/17 Pct Recovery = 110% Analysis Date = 01/12/17 Pct Recovery = 110% Analysis Date = 01/12/17 Pct Recovery = 110% Analysis Date = 01/10/17 Pct Recovery = 110% Analysis Date = 01/10/17 Pct Recovery = 110% Analysis Date = 01/08/17 Pct Recovery = 109% Analysis Date = 01/08/17 Pct Recovery = 109% Analysis Date = 01/06/17 Pct Recovery = 109% Analysis Date = 01/06/17 Pct Recovery = 109% Analysis Date = 01/04/17 Pct Recovery = 109% Analysis Date = 01/04/17 Pct Recovery = 109% Analysis Date = 01/01/17 Pct Recovery = 109% Analysis Date = 01/01/17 Pct Recovery = 109% Analysis Date = 12/30/16 Pct Recovery = 109% Analysis Date = 12/30/16 Pct Recovery = 109% Analysis Date = 12/28/16 Pct Recovery = 109% Analysis Date = 12/28/16 Pct Recovery = 109% Analysis Date = 12/26/16 Pct Recovery = 109% Analysis Date = 12/26/16 Pct Recovery = 109% Analysis Date = 12/23/16 Pct Recovery = 109% Analysis Date = 12/23/16 Pct Recovery = 109% Analysis Date = 12/21/16 Pct Recovery = 108% Analysis Date = 12/21/16 Pct Recovery = 108% Analysis Date = 12/19/16 Pct Recovery = 108% Analysis Date = 12/19/16 Pct Recovery = 108% Analysis Date = 12/17/16 Pct Recovery = 108% Analysis Date = 12/17/16 Pct Recovery = 108% Analysis Date = 12/14/16 Pct Recovery = 108% Analysis Date = 12/14/16 Pct Recovery = 108% Analysis Date = 12/12/16 Pct Recovery = 107% Analysis Date = 12/12/16 Pct Recovery = 107% Analysis Date = 12/10/16 Pct Recovery = 107% Analysis Date = 12/10/16 Pct Recovery = 107% Analysis Date = 12/08/16 Pct Recovery = 107% Analysis Date = 12/08/16 Pct Recovery = 107% Analysis Date = 12/05/16 Pct Recovery = 107% Analysis Date = 12/05/16 Pct Recovery = 107% Analysis Date = 12/03/16 Pct Recovery = 106% Analysis Date = 12/03/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 12/01/16 Pct Recovery = 106% Analysis Date = 11/29/16 Pct Recovery = 106% Analysis Date = 11/29/16 Pct Recovery = 106% Analysis Date = 11/26/16 Pct Recovery = 105% Analysis Date = 11/26/16 Pct Recovery = 105% Analysis Date = 11/24/16 Pct Recovery = 105% Analysis Date = 11/24/16 Pct Recovery = 105% Analysis Date = 11/22/16 Pct Recovery = 105% Analysis Date = 11/22/16 Pct Recovery = 105% Analysis Date = 11/20/16 Pct Recovery = 105% Analysis Date = 11/20/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/15/16 Pct Recovery = 104% Analysis Date = 11/15/16 Pct Recovery = 104% Analysis Date = 11/13/16 Pct Recovery = 104% Analysis Date = 11/13/16 Pct Recovery = 104% Analysis Date = 11/11/16 Pct Recovery = 104% Analysis Date = 11/11/16 Pct Recovery = 104% Analysis Date = 11/08/16 Pct Recovery = 103% Analysis Date = 11/08/16 Pct Recovery = 103% Analysis Date = 11/06/16 Pct Recovery = 103% Analysis Date = 11/06/16 Pct Recovery = 103% Analysis Date = 11/04/16 Pct Recovery = 103% Analysis Date = 11/04/16 Pct Recovery = 103% Analysis Date = 11/02/16 Pct Recovery = 102% Analysis Date = 11/02/16 Pct Recovery = 102% Analysis Date = 10/30/16 Pct Recovery = 102% Analysis Date = 10/30/16 Pct Recovery = 102% Analysis Date = 10/28/16 Pct Recovery = 102% Analysis Date = 10/28/16 Pct Recovery = 102% Analysis Date = 10/26/16 Pct Recovery = 102% Analysis Date = 10/26/16 Pct Recovery = 102% Analysis Date = 10/24/16 Pct Recovery = 101% Analysis Date = 10/24/16 Pct Recovery = 101% Analysis Date = 10/21/16 Pct Recovery = 101% Analysis Date = 10/21/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/19/16 Pct Recovery = 101% Analysis Date = 10/17/16 Pct Recovery = 101% Analysis Date = 10/17/16 Pct Recovery = 101% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/15/16 Pct Recovery = 100% Analysis Date = 10/12/16 Pct Recovery = 100% Analysis Date = 10/12/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/10/16 Pct Recovery = 100% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/06/16 Pct Recovery = 99% Analysis Date = 10/06/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 98% Analysis Date = 09/29/16 Pct Recovery = 98% Analysis Date = 09/27/16 Pct Recovery = 98% Analysis Date = 09/27/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 98% Analysis Date = 09/22/16 Pct Recovery = 97% Analysis Date = 09/22/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/20/16 Pct Recovery = 97% Analysis Date = 09/18/16 Pct Recovery = 97% Analysis Date = 09/18/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/11/16 Pct Recovery = 96% Analysis Date = 09/11/16 Pct Recovery = 96% Analysis Date = 09/09/16 Pct Recovery = 96% Analysis Date = 09/09/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/04/16 Pct Recovery = 95% Analysis Date = 09/04/16 Pct Recovery = 95% Analysis Date = 09/02/16 Pct Recovery = 95% Analysis Date = 09/02/16 Pct Recovery = 95% Analysis Date = 08/31/16 Pct Recovery = 95% Analysis Date = 08/31/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 95% Analysis Date = 08/29/16 Pct Recovery = 95% Analysis Date = 08/26/16 Pct Recovery = 95% Analysis Date = 08/26/16 Pct Recovery = 95% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/24/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/22/16 Pct Recovery = 94% Analysis Date = 08/20/16 Pct Recovery = 94% Analysis Date = 08/20/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/17/16 Pct Recovery = 94% Analysis Date = 08/15/16 Pct Recovery = 94% Analysis Date = 08/15/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/13/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/11/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/08/16 Pct Recovery = 94% Analysis Date = 08/06/16 Pct Recovery = 94% Analysis Date = 08/06/16 Pct Recovery = 94% Analysis Date = 08/04/16 Pct Recovery = 94% Analysis Date = 08/04/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 93% Analysis Date = 07/30/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/28/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/26/16 Pct Recovery = 93% Analysis Date = 07/24/16 Pct Recovery = 93% Analysis Date = 07/24/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/19/16 Pct Recovery = 93% Analysis Date = 07/19/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/15/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/12/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/10/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 92% Analysis Date = 07/03/16 Pct Recovery = 92% Analysis Date = 07/03/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/24/16 Pct Recovery = 92% Analysis Date = 06/24/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/15/16 Pct Recovery = 92% Analysis Date = 06/15/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 91% Analysis Date = 06/11/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 91% Analysis Date = 05/31/16 Pct Recovery = 91% Analysis Date = 05/31/16 Pct Recovery = 91% Analysis Date = 05/29/16 Pct Recovery = 91% Analysis Date = 05/29/16 Pct Recovery = 91% Analysis Date = 05/26/16 Pct Recovery = 91% Analysis Date = 05/26/16 Pct Recovery = 91% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/24/16 Pct Recovery = 92% Analysis Date = 05/22/16 Pct Recovery = 92% Analysis Date = 05/22/16 Pct Recovery = 92% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/20/16 Pct Recovery = 93% Analysis Date = 05/17/16 Pct Recovery = 93% Analysis Date = 05/17/16 Pct Recovery = 93% Analysis Date = 05/15/16 Pct Recovery = 94% Analysis Date = 05/15/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/13/16 Pct Recovery = 94% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/08/16 Pct Recovery = 95% Analysis Date = 05/08/16 Pct Recovery = 95% Analysis Date = 05/06/16 Pct Recovery = 96% Analysis Date = 05/06/16 Pct Recovery = 96% Analysis Date = 05/04/16 Pct Recovery = 96% Analysis Date = 05/04/16 Pct Recovery = 96% Analysis Date = 05/02/16 Pct Recovery = 97% Analysis Date = 05/02/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 97% Analysis Date = 04/29/16 Pct Recovery = 97% Analysis Date = 04/27/16 Pct Recovery = 97% Analysis Date = 04/27/16 Pct Recovery = 97% Analysis Date = 04/25/16 Pct Recovery = 98% Analysis Date = 04/25/16 Pct Recovery = 98% Analysis Date = 04/23/16 Pct Recovery = 98% Analysis Date = 04/23/16 Pct Recovery = 98% Analysis Date = 04/20/16 Pct Recovery = 98% Analysis Date = 04/20/16 Pct Recovery = 98% Analysis Date = 04/18/16 Pct Recovery = 99% Analysis Date = 04/18/16 Pct Recovery = 99% Analysis Date = 04/16/16 Pct Recovery = 99% Analysis Date = 04/16/16 Pct Recovery = 99% Analysis Date = 04/14/16 Pct Recovery = 99% Analysis Date = 04/14/16 Pct Recovery = 99% Analysis Date = 04/11/16 Pct Recovery = 100% Analysis Date = 04/11/16 Pct Recovery = 100% Analysis Date = 04/09/16 Pct Recovery = 100% Analysis Date = 04/09/16 Pct Recovery = 100% Analysis Date = 04/07/16 Pct Recovery = 100% Analysis Date = 04/07/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 04/02/16 Pct Recovery = 101% Analysis Date = 04/02/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/29/16 Pct Recovery = 101% Analysis Date = 03/29/16 Pct Recovery = 101% Analysis Date = 03/27/16 Pct Recovery = 101% Analysis Date = 03/27/16 Pct Recovery = 101% Analysis Date = 03/24/16 Pct Recovery = 102% Analysis Date = 03/24/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/22/16 Pct Recovery = 102% Analysis Date = 03/20/16 Pct Recovery = 102% Analysis Date = 03/20/16 Pct Recovery = 102% Analysis Date = 03/18/16 Pct Recovery = 102% Analysis Date = 03/18/16 Pct Recovery = 102% Analysis Date = 03/15/16 Pct Recovery = 103% Analysis Date = 03/15/16 Pct Recovery = 103% Analysis Date = 03/13/16 Pct Recovery = 103% Analysis Date = 03/13/16 Pct Recovery = 103% Analysis Date = 03/11/16 Pct Recovery = 103% Analysis Date = 03/11/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/09/16 Pct Recovery = 103% Analysis Date = 03/06/16 Pct Recovery = 104% Analysis Date = 03/06/16 Pct Recovery = 104% Analysis Date = 03/04/16 Pct Recovery = 104% Analysis Date = 03/04/16 Pct Recovery = 104% Analysis Date = 03/02/16 Pct Recovery = 104% Analysis Date = 03/02/16 Pct Recovery = 104% Analysis Date = 02/29/16 Pct Recovery = 104% Analysis Date = 02/29/16 Pct Recovery = 104% Analysis Date = 02/26/16 Pct Recovery = 105% Analysis Date = 02/26/16 Pct Recovery = 105% Analysis Date = 02/24/16 Pct Recovery = 105% Analysis Date = 02/24/16 Pct Recovery = 105% Analysis Date = 02/22/16 Pct Recovery = 105% Analysis Date = 02/22/16 Pct Recovery = 105% Analysis Date = 02/20/16 Pct Recovery = 105% Analysis Date = 02/20/16 Pct Recovery = 105% Analysis Date = 02/17/16 Pct Recovery = 106% Analysis Date = 02/17/16 Pct Recovery = 106% Analysis Date = 02/15/16 Pct Recovery = 106% Analysis Date = 02/15/16 Pct Recovery = 106% Analysis Date = 02/13/16 Pct Recovery = 106% Analysis Date = 02/13/16 Pct Recovery = 106% Analysis Date = 02/11/16 Pct Recovery = 106% Analysis Date = 02/11/16 Pct Recovery = 106% Analysis Date = 02/09/16 Pct Recovery = 107% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
EPTC

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 103% 13% 101% 10%
Total 19 103% 13% 101% 10%

Sample Statistics
EPTC

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
ETHION
METHOD: 2033 , TESTIDCODE: 82346GCM40

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 95% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 113% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 115% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 89% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 97% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 109% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 94% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 113% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 97% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 136% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 193% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 122% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 102% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 110% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 111% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 121% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 141% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 103% Analysis Date = 05/10/17 Pct Recovery = 97% Analysis Date = 05/08/17 Pct Recovery = 98% Analysis Date = 05/08/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 98% Analysis Date = 05/06/17 Pct Recovery = 98% Analysis Date = 05/04/17 Pct Recovery = 98% Analysis Date = 05/04/17 Pct Recovery = 98% Analysis Date = 05/01/17 Pct Recovery = 99% Analysis Date = 05/01/17 Pct Recovery = 99% Analysis Date = 04/29/17 Pct Recovery = 99% Analysis Date = 04/29/17 Pct Recovery = 99% Analysis Date = 04/27/17 Pct Recovery = 100% Analysis Date = 04/27/17 Pct Recovery = 100% Analysis Date = 04/25/17 Pct Recovery = 100% Analysis Date = 04/25/17 Pct Recovery = 100% Analysis Date = 04/22/17 Pct Recovery = 101% Analysis Date = 04/22/17 Pct Recovery = 101% Analysis Date = 04/20/17 Pct Recovery = 101% Analysis Date = 04/20/17 Pct Recovery = 101% Analysis Date = 04/18/17 Pct Recovery = 102% Analysis Date = 04/18/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/15/17 Pct Recovery = 102% Analysis Date = 04/13/17 Pct Recovery = 102% Analysis Date = 04/13/17 Pct Recovery = 102% Analysis Date = 04/11/17 Pct Recovery = 103% Analysis Date = 04/11/17 Pct Recovery = 103% Analysis Date = 04/09/17 Pct Recovery = 103% Analysis Date = 04/09/17 Pct Recovery = 103% Analysis Date = 04/06/17 Pct Recovery = 104% Analysis Date = 04/06/17 Pct Recovery = 104% Analysis Date = 04/04/17 Pct Recovery = 104% Analysis Date = 04/04/17 Pct Recovery = 104% Analysis Date = 04/02/17 Pct Recovery = 105% Analysis Date = 04/02/17 Pct Recovery = 105% Analysis Date = 03/30/17 Pct Recovery = 105% Analysis Date = 03/30/17 Pct Recovery = 105% Analysis Date = 03/28/17 Pct Recovery = 106% Analysis Date = 03/28/17 Pct Recovery = 106% Analysis Date = 03/26/17 Pct Recovery = 106% Analysis Date = 03/26/17 Pct Recovery = 106% Analysis Date = 03/24/17 Pct Recovery = 106% Analysis Date = 03/24/17 Pct Recovery = 106% Analysis Date = 03/21/17 Pct Recovery = 107% Analysis Date = 03/21/17 Pct Recovery = 107% Analysis Date = 03/19/17 Pct Recovery = 107% Analysis Date = 03/19/17 Pct Recovery = 107% Analysis Date = 03/17/17 Pct Recovery = 108% Analysis Date = 03/17/17 Pct Recovery = 108% Analysis Date = 03/14/17 Pct Recovery = 108% Analysis Date = 03/14/17 Pct Recovery = 108% Analysis Date = 03/12/17 Pct Recovery = 108% Analysis Date = 03/12/17 Pct Recovery = 108% Analysis Date = 03/10/17 Pct Recovery = 109% Analysis Date = 03/10/17 Pct Recovery = 109% Analysis Date = 03/08/17 Pct Recovery = 109% Analysis Date = 03/08/17 Pct Recovery = 109% Analysis Date = 03/05/17 Pct Recovery = 109% Analysis Date = 03/05/17 Pct Recovery = 109% Analysis Date = 03/03/17 Pct Recovery = 110% Analysis Date = 03/03/17 Pct Recovery = 110% Analysis Date = 03/01/17 Pct Recovery = 110% Analysis Date = 03/01/17 Pct Recovery = 110% Analysis Date = 02/26/17 Pct Recovery = 111% Analysis Date = 02/26/17 Pct Recovery = 111% Analysis Date = 02/24/17 Pct Recovery = 111% Analysis Date = 02/24/17 Pct Recovery = 111% Analysis Date = 02/22/17 Pct Recovery = 111% Analysis Date = 02/22/17 Pct Recovery = 111% Analysis Date = 02/20/17 Pct Recovery = 111% Analysis Date = 02/20/17 Pct Recovery = 111% Analysis Date = 02/17/17 Pct Recovery = 111% Analysis Date = 02/17/17 Pct Recovery = 111% Analysis Date = 02/15/17 Pct Recovery = 111% Analysis Date = 02/15/17 Pct Recovery = 111% Analysis Date = 02/13/17 Pct Recovery = 110% Analysis Date = 02/13/17 Pct Recovery = 110% Analysis Date = 02/10/17 Pct Recovery = 110% Analysis Date = 02/10/17 Pct Recovery = 110% Analysis Date = 02/08/17 Pct Recovery = 110% Analysis Date = 02/08/17 Pct Recovery = 110% Analysis Date = 02/06/17 Pct Recovery = 110% Analysis Date = 02/06/17 Pct Recovery = 110% Analysis Date = 02/04/17 Pct Recovery = 110% Analysis Date = 02/04/17 Pct Recovery = 110% Analysis Date = 02/01/17 Pct Recovery = 109% Analysis Date = 02/01/17 Pct Recovery = 109% Analysis Date = 01/30/17 Pct Recovery = 109% Analysis Date = 01/30/17 Pct Recovery = 109% Analysis Date = 01/28/17 Pct Recovery = 109% Analysis Date = 01/28/17 Pct Recovery = 109% Analysis Date = 01/25/17 Pct Recovery = 109% Analysis Date = 01/25/17 Pct Recovery = 109% Analysis Date = 01/23/17 Pct Recovery = 109% Analysis Date = 01/23/17 Pct Recovery = 109% Analysis Date = 01/21/17 Pct Recovery = 108% Analysis Date = 01/21/17 Pct Recovery = 108% Analysis Date = 01/19/17 Pct Recovery = 108% Analysis Date = 01/19/17 Pct Recovery = 108% Analysis Date = 01/16/17 Pct Recovery = 108% Analysis Date = 01/16/17 Pct Recovery = 108% Analysis Date = 01/14/17 Pct Recovery = 108% Analysis Date = 01/14/17 Pct Recovery = 108% Analysis Date = 01/12/17 Pct Recovery = 109% Analysis Date = 01/12/17 Pct Recovery = 109% Analysis Date = 01/09/17 Pct Recovery = 109% Analysis Date = 01/09/17 Pct Recovery = 109% Analysis Date = 01/07/17 Pct Recovery = 109% Analysis Date = 01/07/17 Pct Recovery = 109% Analysis Date = 01/05/17 Pct Recovery = 110% Analysis Date = 01/05/17 Pct Recovery = 110% Analysis Date = 01/03/17 Pct Recovery = 110% Analysis Date = 01/03/17 Pct Recovery = 110% Analysis Date = 12/31/16 Pct Recovery = 110% Analysis Date = 12/31/16 Pct Recovery = 110% Analysis Date = 12/29/16 Pct Recovery = 110% Analysis Date = 12/29/16 Pct Recovery = 110% Analysis Date = 12/27/16 Pct Recovery = 111% Analysis Date = 12/27/16 Pct Recovery = 111% Analysis Date = 12/24/16 Pct Recovery = 111% Analysis Date = 12/24/16 Pct Recovery = 111% Analysis Date = 12/22/16 Pct Recovery = 111% Analysis Date = 12/22/16 Pct Recovery = 111% Analysis Date = 12/20/16 Pct Recovery = 111% Analysis Date = 12/20/16 Pct Recovery = 111% Analysis Date = 12/18/16 Pct Recovery = 112% Analysis Date = 12/18/16 Pct Recovery = 112% Analysis Date = 12/15/16 Pct Recovery = 112% Analysis Date = 12/15/16 Pct Recovery = 112% Analysis Date = 12/13/16 Pct Recovery = 112% Analysis Date = 12/13/16 Pct Recovery = 112% Analysis Date = 12/11/16 Pct Recovery = 112% Analysis Date = 12/11/16 Pct Recovery = 112% Analysis Date = 12/08/16 Pct Recovery = 113% Analysis Date = 12/08/16 Pct Recovery = 113% Analysis Date = 12/06/16 Pct Recovery = 113% Analysis Date = 12/06/16 Pct Recovery = 113% Analysis Date = 12/04/16 Pct Recovery = 113% Analysis Date = 12/04/16 Pct Recovery = 113% Analysis Date = 12/02/16 Pct Recovery = 114% Analysis Date = 12/02/16 Pct Recovery = 114% Analysis Date = 11/29/16 Pct Recovery = 114% Analysis Date = 11/29/16 Pct Recovery = 114% Analysis Date = 11/27/16 Pct Recovery = 114% Analysis Date = 11/27/16 Pct Recovery = 114% Analysis Date = 11/25/16 Pct Recovery = 114% Analysis Date = 11/25/16 Pct Recovery = 114% Analysis Date = 11/22/16 Pct Recovery = 115% Analysis Date = 11/22/16 Pct Recovery = 115% Analysis Date = 11/20/16 Pct Recovery = 115% Analysis Date = 11/20/16 Pct Recovery = 115% Analysis Date = 11/18/16 Pct Recovery = 115% Analysis Date = 11/18/16 Pct Recovery = 115% Analysis Date = 11/16/16 Pct Recovery = 115% Analysis Date = 11/16/16 Pct Recovery = 115% Analysis Date = 11/13/16 Pct Recovery = 116% Analysis Date = 11/13/16 Pct Recovery = 116% Analysis Date = 11/11/16 Pct Recovery = 116% Analysis Date = 11/11/16 Pct Recovery = 116% Analysis Date = 11/09/16 Pct Recovery = 116% Analysis Date = 11/09/16 Pct Recovery = 116% Analysis Date = 11/06/16 Pct Recovery = 117% Analysis Date = 11/06/16 Pct Recovery = 117% Analysis Date = 11/04/16 Pct Recovery = 117% Analysis Date = 11/04/16 Pct Recovery = 117% Analysis Date = 11/02/16 Pct Recovery = 117% Analysis Date = 11/02/16 Pct Recovery = 117% Analysis Date = 10/31/16 Pct Recovery = 117% Analysis Date = 10/31/16 Pct Recovery = 117% Analysis Date = 10/28/16 Pct Recovery = 118% Analysis Date = 10/28/16 Pct Recovery = 118% Analysis Date = 10/26/16 Pct Recovery = 118% Analysis Date = 10/26/16 Pct Recovery = 118% Analysis Date = 10/24/16 Pct Recovery = 118% Analysis Date = 10/24/16 Pct Recovery = 118% Analysis Date = 10/21/16 Pct Recovery = 118% Analysis Date = 10/21/16 Pct Recovery = 118% Analysis Date = 10/19/16 Pct Recovery = 119% Analysis Date = 10/19/16 Pct Recovery = 119% Analysis Date = 10/17/16 Pct Recovery = 119% Analysis Date = 10/17/16 Pct Recovery = 119% Analysis Date = 10/15/16 Pct Recovery = 119% Analysis Date = 10/15/16 Pct Recovery = 119% Analysis Date = 10/12/16 Pct Recovery = 119% Analysis Date = 10/12/16 Pct Recovery = 119% Analysis Date = 10/10/16 Pct Recovery = 120% Analysis Date = 10/10/16 Pct Recovery = 120% Analysis Date = 10/08/16 Pct Recovery = 120% Analysis Date = 10/08/16 Pct Recovery = 120% Analysis Date = 10/05/16 Pct Recovery = 120% Analysis Date = 10/05/16 Pct Recovery = 120% Analysis Date = 10/03/16 Pct Recovery = 121% Analysis Date = 10/03/16 Pct Recovery = 121% Analysis Date = 10/01/16 Pct Recovery = 121% Analysis Date = 10/01/16 Pct Recovery = 121% Analysis Date = 09/29/16 Pct Recovery = 121% Analysis Date = 09/29/16 Pct Recovery = 121% Analysis Date = 09/26/16 Pct Recovery = 121% Analysis Date = 09/26/16 Pct Recovery = 121% Analysis Date = 09/24/16 Pct Recovery = 122% Analysis Date = 09/24/16 Pct Recovery = 122% Analysis Date = 09/22/16 Pct Recovery = 122% Analysis Date = 09/22/16 Pct Recovery = 122% Analysis Date = 09/19/16 Pct Recovery = 122% Analysis Date = 09/19/16 Pct Recovery = 122% Analysis Date = 09/17/16 Pct Recovery = 122% Analysis Date = 09/17/16 Pct Recovery = 122% Analysis Date = 09/15/16 Pct Recovery = 123% Analysis Date = 09/15/16 Pct Recovery = 123% Analysis Date = 09/13/16 Pct Recovery = 123% Analysis Date = 09/13/16 Pct Recovery = 123% Analysis Date = 09/10/16 Pct Recovery = 122% Analysis Date = 09/10/16 Pct Recovery = 122% Analysis Date = 09/08/16 Pct Recovery = 122% Analysis Date = 09/08/16 Pct Recovery = 122% Analysis Date = 09/06/16 Pct Recovery = 122% Analysis Date = 09/06/16 Pct Recovery = 122% Analysis Date = 09/03/16 Pct Recovery = 122% Analysis Date = 09/03/16 Pct Recovery = 122% Analysis Date = 09/01/16 Pct Recovery = 121% Analysis Date = 09/01/16 Pct Recovery = 121% Analysis Date = 08/30/16 Pct Recovery = 121% Analysis Date = 08/30/16 Pct Recovery = 121% Analysis Date = 08/28/16 Pct Recovery = 121% Analysis Date = 08/28/16 Pct Recovery = 121% Analysis Date = 08/25/16 Pct Recovery = 120% Analysis Date = 08/25/16 Pct Recovery = 120% Analysis Date = 08/23/16 Pct Recovery = 120% Analysis Date = 08/23/16 Pct Recovery = 120% Analysis Date = 08/21/16 Pct Recovery = 120% Analysis Date = 08/21/16 Pct Recovery = 120% Analysis Date = 08/18/16 Pct Recovery = 120% Analysis Date = 08/18/16 Pct Recovery = 120% Analysis Date = 08/16/16 Pct Recovery = 120% Analysis Date = 08/16/16 Pct Recovery = 120% Analysis Date = 08/14/16 Pct Recovery = 120% Analysis Date = 08/14/16 Pct Recovery = 120% Analysis Date = 08/12/16 Pct Recovery = 120% Analysis Date = 08/12/16 Pct Recovery = 120% Analysis Date = 08/09/16 Pct Recovery = 119% Analysis Date = 08/09/16 Pct Recovery = 119% Analysis Date = 08/07/16 Pct Recovery = 119% Analysis Date = 08/07/16 Pct Recovery = 119% Analysis Date = 08/05/16 Pct Recovery = 119% Analysis Date = 08/05/16 Pct Recovery = 119% Analysis Date = 08/02/16 Pct Recovery = 119% Analysis Date = 08/02/16 Pct Recovery = 119% Analysis Date = 07/31/16 Pct Recovery = 119% Analysis Date = 07/31/16 Pct Recovery = 119% Analysis Date = 07/29/16 Pct Recovery = 119% Analysis Date = 07/29/16 Pct Recovery = 119% Analysis Date = 07/27/16 Pct Recovery = 119% Analysis Date = 07/27/16 Pct Recovery = 119% Analysis Date = 07/24/16 Pct Recovery = 118% Analysis Date = 07/24/16 Pct Recovery = 118% Analysis Date = 07/22/16 Pct Recovery = 118% Analysis Date = 07/22/16 Pct Recovery = 118% Analysis Date = 07/20/16 Pct Recovery = 118% Analysis Date = 07/20/16 Pct Recovery = 118% Analysis Date = 07/17/16 Pct Recovery = 118% Analysis Date = 07/17/16 Pct Recovery = 118% Analysis Date = 07/15/16 Pct Recovery = 118% Analysis Date = 07/15/16 Pct Recovery = 118% Analysis Date = 07/13/16 Pct Recovery = 118% Analysis Date = 07/13/16 Pct Recovery = 118% Analysis Date = 07/11/16 Pct Recovery = 118% Analysis Date = 07/11/16 Pct Recovery = 118% Analysis Date = 07/08/16 Pct Recovery = 117% Analysis Date = 07/08/16 Pct Recovery = 117% Analysis Date = 07/06/16 Pct Recovery = 117% Analysis Date = 07/06/16 Pct Recovery = 117% Analysis Date = 07/04/16 Pct Recovery = 117% Analysis Date = 07/04/16 Pct Recovery = 117% Analysis Date = 07/01/16 Pct Recovery = 117% Analysis Date = 07/01/16 Pct Recovery = 117% Analysis Date = 06/29/16 Pct Recovery = 117% Analysis Date = 06/29/16 Pct Recovery = 117% Analysis Date = 06/27/16 Pct Recovery = 117% Analysis Date = 06/27/16 Pct Recovery = 117% Analysis Date = 06/25/16 Pct Recovery = 117% Analysis Date = 06/25/16 Pct Recovery = 117% Analysis Date = 06/22/16 Pct Recovery = 117% Analysis Date = 06/22/16 Pct Recovery = 117% Analysis Date = 06/20/16 Pct Recovery = 116% Analysis Date = 06/20/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/15/16 Pct Recovery = 116% Analysis Date = 06/15/16 Pct Recovery = 116% Analysis Date = 06/13/16 Pct Recovery = 116% Analysis Date = 06/13/16 Pct Recovery = 116% Analysis Date = 06/11/16 Pct Recovery = 116% Analysis Date = 06/11/16 Pct Recovery = 116% Analysis Date = 06/09/16 Pct Recovery = 116% Analysis Date = 06/09/16 Pct Recovery = 116% Analysis Date = 06/06/16 Pct Recovery = 116% Analysis Date = 06/06/16 Pct Recovery = 116% Analysis Date = 06/04/16 Pct Recovery = 115% Analysis Date = 06/04/16 Pct Recovery = 115% Analysis Date = 06/02/16 Pct Recovery = 115% Analysis Date = 06/02/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 115% Analysis Date = 05/30/16 Pct Recovery = 115% Analysis Date = 05/28/16 Pct Recovery = 115% Analysis Date = 05/28/16 Pct Recovery = 115% Analysis Date = 05/26/16 Pct Recovery = 115% Analysis Date = 05/26/16 Pct Recovery = 115% Analysis Date = 05/24/16 Pct Recovery = 115% Analysis Date = 05/24/16 Pct Recovery = 115% Analysis Date = 05/21/16 Pct Recovery = 115% Analysis Date = 05/21/16 Pct Recovery = 115% Analysis Date = 05/19/16 Pct Recovery = 114% Analysis Date = 05/19/16 Pct Recovery = 114% Analysis Date = 05/17/16 Pct Recovery = 114% Analysis Date = 05/17/16 Pct Recovery = 114% Analysis Date = 05/14/16 Pct Recovery = 114% Analysis Date = 05/14/16 Pct Recovery = 114% Analysis Date = 05/12/16 Pct Recovery = 114% Analysis Date = 05/12/16 Pct Recovery = 114% Analysis Date = 05/10/16 Pct Recovery = 114% Analysis Date = 05/10/16 Pct Recovery = 114% Analysis Date = 05/08/16 Pct Recovery = 114% Analysis Date = 05/08/16 Pct Recovery = 114% Analysis Date = 05/05/16 Pct Recovery = 114% Analysis Date = 05/05/16 Pct Recovery = 114% Analysis Date = 05/03/16 Pct Recovery = 114% Analysis Date = 05/03/16 Pct Recovery = 114% Analysis Date = 05/01/16 Pct Recovery = 114% Analysis Date = 05/01/16 Pct Recovery = 114% Analysis Date = 04/28/16 Pct Recovery = 114% Analysis Date = 04/28/16 Pct Recovery = 114% Analysis Date = 04/26/16 Pct Recovery = 114% Analysis Date = 04/26/16 Pct Recovery = 114% Analysis Date = 04/24/16 Pct Recovery = 115% Analysis Date = 04/24/16 Pct Recovery = 115% Analysis Date = 04/22/16 Pct Recovery = 115% Analysis Date = 04/22/16 Pct Recovery = 115% Analysis Date = 04/19/16 Pct Recovery = 115% Analysis Date = 04/19/16 Pct Recovery = 115% Analysis Date = 04/17/16 Pct Recovery = 115% Analysis Date = 04/17/16 Pct Recovery = 115% Analysis Date = 04/15/16 Pct Recovery = 116% Analysis Date = 04/15/16 Pct Recovery = 116% Analysis Date = 04/12/16 Pct Recovery = 116% Analysis Date = 04/12/16 Pct Recovery = 116% Analysis Date = 04/10/16 Pct Recovery = 116% Analysis Date = 04/10/16 Pct Recovery = 116% Analysis Date = 04/08/16 Pct Recovery = 117% Analysis Date = 04/08/16 Pct Recovery = 117% Analysis Date = 04/06/16 Pct Recovery = 117% Analysis Date = 04/06/16 Pct Recovery = 117% Analysis Date = 04/03/16 Pct Recovery = 117% Analysis Date = 04/03/16 Pct Recovery = 117% Analysis Date = 04/01/16 Pct Recovery = 117% Analysis Date = 04/01/16 Pct Recovery = 117% Analysis Date = 03/30/16 Pct Recovery = 117% Analysis Date = 03/30/16 Pct Recovery = 117% Analysis Date = 03/27/16 Pct Recovery = 118% Analysis Date = 03/27/16 Pct Recovery = 118% Analysis Date = 03/25/16 Pct Recovery = 118% Analysis Date = 03/25/16 Pct Recovery = 118% Analysis Date = 03/23/16 Pct Recovery = 118% Analysis Date = 03/23/16 Pct Recovery = 118% Analysis Date = 03/21/16 Pct Recovery = 118% Analysis Date = 03/21/16 Pct Recovery = 118% Analysis Date = 03/18/16 Pct Recovery = 118% Analysis Date = 03/18/16 Pct Recovery = 118% Analysis Date = 03/16/16 Pct Recovery = 118% Analysis Date = 03/16/16 Pct Recovery = 118% Analysis Date = 03/14/16 Pct Recovery = 119% Analysis Date = 03/14/16 Pct Recovery = 119% Analysis Date = 03/11/16 Pct Recovery = 119% Analysis Date = 03/11/16 Pct Recovery = 119% Analysis Date = 03/09/16 Pct Recovery = 119% Analysis Date = 03/09/16 Pct Recovery = 119% Analysis Date = 03/07/16 Pct Recovery = 119% Analysis Date = 03/07/16 Pct Recovery = 119% Analysis Date = 03/05/16 Pct Recovery = 119% Analysis Date = 03/05/16 Pct Recovery = 119% Analysis Date = 03/02/16 Pct Recovery = 119% Analysis Date = 03/02/16 Pct Recovery = 119% Analysis Date = 02/29/16 Pct Recovery = 119% Analysis Date = 02/29/16 Pct Recovery = 119% Analysis Date = 02/27/16 Pct Recovery = 120% Analysis Date = 02/27/16 Pct Recovery = 120% Analysis Date = 02/24/16 Pct Recovery = 120% Analysis Date = 02/24/16 Pct Recovery = 120% Analysis Date = 02/22/16 Pct Recovery = 120% Analysis Date = 02/22/16 Pct Recovery = 120% Analysis Date = 02/20/16 Pct Recovery = 120% Analysis Date = 02/20/16 Pct Recovery = 120% Analysis Date = 02/18/16 Pct Recovery = 120% Analysis Date = 02/18/16 Pct Recovery = 120% Analysis Date = 02/15/16 Pct Recovery = 120% Analysis Date = 02/15/16 Pct Recovery = 120% Analysis Date = 02/13/16 Pct Recovery = 120% Analysis Date = 02/13/16 Pct Recovery = 120% Analysis Date = 02/11/16 Pct Recovery = 120% Analysis Date = 02/11/16 Pct Recovery = 120% Analysis Date = 02/09/16 Pct Recovery = 121% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 114% 24% 111% 18%
Total 18 114% 24% 111% 18%

Sample Statistics
ETHION

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
ETHION MONOXON
METHOD: 2033 , TESTIDCODE: 61644GCM39

The SGPlot Procedure

Sample Statistics
ETHION MONOXON

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 13 46% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 28 .  
False Positives 0 0% 0 out of 15

OBSP Determination:
ETHOPROPHOS
METHOD: 2033 , TESTIDCODE: 82672GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 98% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 92% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 92% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 85% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 86% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 91% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 139% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 95% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 05/02/17 Pct Recovery = 98% Analysis Date = 04/30/17 Pct Recovery = 98% Analysis Date = 04/30/17 Pct Recovery = 98% Analysis Date = 04/28/17 Pct Recovery = 98% Analysis Date = 04/28/17 Pct Recovery = 98% Analysis Date = 04/26/17 Pct Recovery = 98% Analysis Date = 04/26/17 Pct Recovery = 98% Analysis Date = 04/24/17 Pct Recovery = 98% Analysis Date = 04/24/17 Pct Recovery = 98% Analysis Date = 04/21/17 Pct Recovery = 98% Analysis Date = 04/21/17 Pct Recovery = 98% Analysis Date = 04/19/17 Pct Recovery = 98% Analysis Date = 04/19/17 Pct Recovery = 98% Analysis Date = 04/17/17 Pct Recovery = 99% Analysis Date = 04/17/17 Pct Recovery = 99% Analysis Date = 04/15/17 Pct Recovery = 99% Analysis Date = 04/15/17 Pct Recovery = 99% Analysis Date = 04/12/17 Pct Recovery = 99% Analysis Date = 04/12/17 Pct Recovery = 99% Analysis Date = 04/10/17 Pct Recovery = 99% Analysis Date = 04/10/17 Pct Recovery = 99% Analysis Date = 04/08/17 Pct Recovery = 99% Analysis Date = 04/08/17 Pct Recovery = 99% Analysis Date = 04/06/17 Pct Recovery = 99% Analysis Date = 04/06/17 Pct Recovery = 99% Analysis Date = 04/03/17 Pct Recovery = 99% Analysis Date = 04/03/17 Pct Recovery = 99% Analysis Date = 04/01/17 Pct Recovery = 100% Analysis Date = 04/01/17 Pct Recovery = 100% Analysis Date = 03/30/17 Pct Recovery = 100% Analysis Date = 03/30/17 Pct Recovery = 100% Analysis Date = 03/28/17 Pct Recovery = 100% Analysis Date = 03/28/17 Pct Recovery = 100% Analysis Date = 03/25/17 Pct Recovery = 100% Analysis Date = 03/25/17 Pct Recovery = 100% Analysis Date = 03/23/17 Pct Recovery = 100% Analysis Date = 03/23/17 Pct Recovery = 100% Analysis Date = 03/21/17 Pct Recovery = 100% Analysis Date = 03/21/17 Pct Recovery = 100% Analysis Date = 03/19/17 Pct Recovery = 100% Analysis Date = 03/19/17 Pct Recovery = 100% Analysis Date = 03/16/17 Pct Recovery = 100% Analysis Date = 03/16/17 Pct Recovery = 100% Analysis Date = 03/14/17 Pct Recovery = 100% Analysis Date = 03/14/17 Pct Recovery = 100% Analysis Date = 03/12/17 Pct Recovery = 100% Analysis Date = 03/12/17 Pct Recovery = 100% Analysis Date = 03/10/17 Pct Recovery = 100% Analysis Date = 03/10/17 Pct Recovery = 100% Analysis Date = 03/07/17 Pct Recovery = 100% Analysis Date = 03/07/17 Pct Recovery = 100% Analysis Date = 03/05/17 Pct Recovery = 100% Analysis Date = 03/05/17 Pct Recovery = 100% Analysis Date = 03/03/17 Pct Recovery = 99% Analysis Date = 03/03/17 Pct Recovery = 99% Analysis Date = 03/01/17 Pct Recovery = 99% Analysis Date = 03/01/17 Pct Recovery = 99% Analysis Date = 02/26/17 Pct Recovery = 98% Analysis Date = 02/26/17 Pct Recovery = 98% Analysis Date = 02/24/17 Pct Recovery = 97% Analysis Date = 02/24/17 Pct Recovery = 97% Analysis Date = 02/22/17 Pct Recovery = 96% Analysis Date = 02/22/17 Pct Recovery = 96% Analysis Date = 02/20/17 Pct Recovery = 96% Analysis Date = 02/20/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/11/17 Pct Recovery = 98% Analysis Date = 02/11/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 99% Analysis Date = 02/08/17 Pct Recovery = 99% Analysis Date = 02/06/17 Pct Recovery = 99% Analysis Date = 02/06/17 Pct Recovery = 99% Analysis Date = 02/04/17 Pct Recovery = 99% Analysis Date = 02/04/17 Pct Recovery = 99% Analysis Date = 02/02/17 Pct Recovery = 99% Analysis Date = 02/02/17 Pct Recovery = 99% Analysis Date = 01/30/17 Pct Recovery = 100% Analysis Date = 01/30/17 Pct Recovery = 100% Analysis Date = 01/28/17 Pct Recovery = 100% Analysis Date = 01/28/17 Pct Recovery = 100% Analysis Date = 01/26/17 Pct Recovery = 100% Analysis Date = 01/26/17 Pct Recovery = 100% Analysis Date = 01/24/17 Pct Recovery = 101% Analysis Date = 01/24/17 Pct Recovery = 101% Analysis Date = 01/21/17 Pct Recovery = 101% Analysis Date = 01/21/17 Pct Recovery = 101% Analysis Date = 01/19/17 Pct Recovery = 101% Analysis Date = 01/19/17 Pct Recovery = 101% Analysis Date = 01/17/17 Pct Recovery = 102% Analysis Date = 01/17/17 Pct Recovery = 102% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/12/17 Pct Recovery = 102% Analysis Date = 01/12/17 Pct Recovery = 102% Analysis Date = 01/10/17 Pct Recovery = 102% Analysis Date = 01/10/17 Pct Recovery = 102% Analysis Date = 01/08/17 Pct Recovery = 103% Analysis Date = 01/08/17 Pct Recovery = 103% Analysis Date = 01/06/17 Pct Recovery = 103% Analysis Date = 01/06/17 Pct Recovery = 103% Analysis Date = 01/04/17 Pct Recovery = 103% Analysis Date = 01/04/17 Pct Recovery = 103% Analysis Date = 01/01/17 Pct Recovery = 104% Analysis Date = 01/01/17 Pct Recovery = 104% Analysis Date = 12/30/16 Pct Recovery = 104% Analysis Date = 12/30/16 Pct Recovery = 104% Analysis Date = 12/28/16 Pct Recovery = 104% Analysis Date = 12/28/16 Pct Recovery = 104% Analysis Date = 12/26/16 Pct Recovery = 104% Analysis Date = 12/26/16 Pct Recovery = 104% Analysis Date = 12/23/16 Pct Recovery = 105% Analysis Date = 12/23/16 Pct Recovery = 105% Analysis Date = 12/21/16 Pct Recovery = 105% Analysis Date = 12/21/16 Pct Recovery = 105% Analysis Date = 12/19/16 Pct Recovery = 105% Analysis Date = 12/19/16 Pct Recovery = 105% Analysis Date = 12/17/16 Pct Recovery = 105% Analysis Date = 12/17/16 Pct Recovery = 105% Analysis Date = 12/14/16 Pct Recovery = 104% Analysis Date = 12/14/16 Pct Recovery = 104% Analysis Date = 12/12/16 Pct Recovery = 104% Analysis Date = 12/12/16 Pct Recovery = 104% Analysis Date = 12/10/16 Pct Recovery = 103% Analysis Date = 12/10/16 Pct Recovery = 103% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/05/16 Pct Recovery = 102% Analysis Date = 12/05/16 Pct Recovery = 102% Analysis Date = 12/03/16 Pct Recovery = 101% Analysis Date = 12/03/16 Pct Recovery = 101% Analysis Date = 12/01/16 Pct Recovery = 101% Analysis Date = 12/01/16 Pct Recovery = 101% Analysis Date = 11/29/16 Pct Recovery = 100% Analysis Date = 11/29/16 Pct Recovery = 100% Analysis Date = 11/26/16 Pct Recovery = 100% Analysis Date = 11/26/16 Pct Recovery = 100% Analysis Date = 11/24/16 Pct Recovery = 99% Analysis Date = 11/24/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/20/16 Pct Recovery = 98% Analysis Date = 11/20/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/17/16 Pct Recovery = 98% Analysis Date = 11/15/16 Pct Recovery = 97% Analysis Date = 11/15/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/13/16 Pct Recovery = 97% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/08/16 Pct Recovery = 96% Analysis Date = 11/08/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 95% Analysis Date = 11/06/16 Pct Recovery = 95% Analysis Date = 11/04/16 Pct Recovery = 95% Analysis Date = 11/04/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 94% Analysis Date = 10/30/16 Pct Recovery = 94% Analysis Date = 10/30/16 Pct Recovery = 94% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/28/16 Pct Recovery = 93% Analysis Date = 10/26/16 Pct Recovery = 93% Analysis Date = 10/26/16 Pct Recovery = 93% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 91% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/12/16 Pct Recovery = 89% Analysis Date = 10/12/16 Pct Recovery = 89% Analysis Date = 10/10/16 Pct Recovery = 89% Analysis Date = 10/10/16 Pct Recovery = 89% Analysis Date = 10/08/16 Pct Recovery = 88% Analysis Date = 10/08/16 Pct Recovery = 88% Analysis Date = 10/06/16 Pct Recovery = 88% Analysis Date = 10/06/16 Pct Recovery = 88% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/29/16 Pct Recovery = 86% Analysis Date = 09/29/16 Pct Recovery = 86% Analysis Date = 09/27/16 Pct Recovery = 86% Analysis Date = 09/27/16 Pct Recovery = 86% Analysis Date = 09/24/16 Pct Recovery = 85% Analysis Date = 09/24/16 Pct Recovery = 85% Analysis Date = 09/22/16 Pct Recovery = 85% Analysis Date = 09/22/16 Pct Recovery = 85% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/16/16 Pct Recovery = 83% Analysis Date = 09/16/16 Pct Recovery = 83% Analysis Date = 09/13/16 Pct Recovery = 83% Analysis Date = 09/13/16 Pct Recovery = 83% Analysis Date = 09/11/16 Pct Recovery = 82% Analysis Date = 09/11/16 Pct Recovery = 82% Analysis Date = 09/09/16 Pct Recovery = 82% Analysis Date = 09/09/16 Pct Recovery = 82% Analysis Date = 09/07/16 Pct Recovery = 81% Analysis Date = 09/07/16 Pct Recovery = 81% Analysis Date = 09/04/16 Pct Recovery = 81% Analysis Date = 09/04/16 Pct Recovery = 81% Analysis Date = 09/02/16 Pct Recovery = 80% Analysis Date = 09/02/16 Pct Recovery = 80% Analysis Date = 08/31/16 Pct Recovery = 80% Analysis Date = 08/31/16 Pct Recovery = 80% Analysis Date = 08/29/16 Pct Recovery = 80% Analysis Date = 08/29/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 80% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/24/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/17/16 Pct Recovery = 79% Analysis Date = 08/17/16 Pct Recovery = 79% Analysis Date = 08/15/16 Pct Recovery = 79% Analysis Date = 08/15/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 79% Analysis Date = 08/13/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/11/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/08/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/06/16 Pct Recovery = 79% Analysis Date = 08/04/16 Pct Recovery = 79% Analysis Date = 08/04/16 Pct Recovery = 79% Analysis Date = 08/02/16 Pct Recovery = 79% Analysis Date = 08/02/16 Pct Recovery = 79% Analysis Date = 07/30/16 Pct Recovery = 79% Analysis Date = 07/30/16 Pct Recovery = 79% Analysis Date = 07/28/16 Pct Recovery = 79% Analysis Date = 07/28/16 Pct Recovery = 79% Analysis Date = 07/26/16 Pct Recovery = 79% Analysis Date = 07/26/16 Pct Recovery = 79% Analysis Date = 07/24/16 Pct Recovery = 79% Analysis Date = 07/24/16 Pct Recovery = 79% Analysis Date = 07/21/16 Pct Recovery = 79% Analysis Date = 07/21/16 Pct Recovery = 79% Analysis Date = 07/19/16 Pct Recovery = 79% Analysis Date = 07/19/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/17/16 Pct Recovery = 79% Analysis Date = 07/15/16 Pct Recovery = 79% Analysis Date = 07/15/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/12/16 Pct Recovery = 79% Analysis Date = 07/10/16 Pct Recovery = 79% Analysis Date = 07/10/16 Pct Recovery = 79% Analysis Date = 07/08/16 Pct Recovery = 79% Analysis Date = 07/08/16 Pct Recovery = 79% Analysis Date = 07/06/16 Pct Recovery = 79% Analysis Date = 07/06/16 Pct Recovery = 79% Analysis Date = 07/03/16 Pct Recovery = 79% Analysis Date = 07/03/16 Pct Recovery = 79% Analysis Date = 07/01/16 Pct Recovery = 79% Analysis Date = 07/01/16 Pct Recovery = 79% Analysis Date = 06/29/16 Pct Recovery = 79% Analysis Date = 06/29/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/27/16 Pct Recovery = 79% Analysis Date = 06/24/16 Pct Recovery = 79% Analysis Date = 06/24/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/22/16 Pct Recovery = 79% Analysis Date = 06/20/16 Pct Recovery = 79% Analysis Date = 06/20/16 Pct Recovery = 79% Analysis Date = 06/18/16 Pct Recovery = 79% Analysis Date = 06/18/16 Pct Recovery = 79% Analysis Date = 06/15/16 Pct Recovery = 79% Analysis Date = 06/15/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/11/16 Pct Recovery = 79% Analysis Date = 06/11/16 Pct Recovery = 79% Analysis Date = 06/09/16 Pct Recovery = 79% Analysis Date = 06/09/16 Pct Recovery = 79% Analysis Date = 06/06/16 Pct Recovery = 79% Analysis Date = 06/06/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 79% Analysis Date = 06/04/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 06/02/16 Pct Recovery = 79% Analysis Date = 05/31/16 Pct Recovery = 79% Analysis Date = 05/31/16 Pct Recovery = 79% Analysis Date = 05/29/16 Pct Recovery = 79% Analysis Date = 05/29/16 Pct Recovery = 79% Analysis Date = 05/26/16 Pct Recovery = 79% Analysis Date = 05/26/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/24/16 Pct Recovery = 79% Analysis Date = 05/22/16 Pct Recovery = 79% Analysis Date = 05/22/16 Pct Recovery = 79% Analysis Date = 05/20/16 Pct Recovery = 79% Analysis Date = 05/20/16 Pct Recovery = 79% Analysis Date = 05/17/16 Pct Recovery = 79% Analysis Date = 05/17/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/08/16 Pct Recovery = 79% Analysis Date = 05/06/16 Pct Recovery = 79% Analysis Date = 05/06/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 79% Analysis Date = 05/04/16 Pct Recovery = 79% Analysis Date = 05/02/16 Pct Recovery = 79% Analysis Date = 05/02/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/27/16 Pct Recovery = 79% Analysis Date = 04/27/16 Pct Recovery = 79% Analysis Date = 04/25/16 Pct Recovery = 80% Analysis Date = 04/25/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/23/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/18/16 Pct Recovery = 80% Analysis Date = 04/18/16 Pct Recovery = 80% Analysis Date = 04/16/16 Pct Recovery = 80% Analysis Date = 04/16/16 Pct Recovery = 80% Analysis Date = 04/14/16 Pct Recovery = 80% Analysis Date = 04/14/16 Pct Recovery = 80% Analysis Date = 04/11/16 Pct Recovery = 80% Analysis Date = 04/11/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 04/07/16 Pct Recovery = 80% Analysis Date = 04/07/16 Pct Recovery = 80% Analysis Date = 04/05/16 Pct Recovery = 80% Analysis Date = 04/05/16 Pct Recovery = 80% Analysis Date = 04/02/16 Pct Recovery = 80% Analysis Date = 04/02/16 Pct Recovery = 80% Analysis Date = 03/31/16 Pct Recovery = 80% Analysis Date = 03/31/16 Pct Recovery = 80% Analysis Date = 03/29/16 Pct Recovery = 80% Analysis Date = 03/29/16 Pct Recovery = 80% Analysis Date = 03/27/16 Pct Recovery = 80% Analysis Date = 03/27/16 Pct Recovery = 80% Analysis Date = 03/24/16 Pct Recovery = 81% Analysis Date = 03/24/16 Pct Recovery = 81% Analysis Date = 03/22/16 Pct Recovery = 81% Analysis Date = 03/22/16 Pct Recovery = 81% Analysis Date = 03/20/16 Pct Recovery = 81% Analysis Date = 03/20/16 Pct Recovery = 81% Analysis Date = 03/18/16 Pct Recovery = 81% Analysis Date = 03/18/16 Pct Recovery = 81% Analysis Date = 03/15/16 Pct Recovery = 81% Analysis Date = 03/15/16 Pct Recovery = 81% Analysis Date = 03/13/16 Pct Recovery = 81% Analysis Date = 03/13/16 Pct Recovery = 81% Analysis Date = 03/11/16 Pct Recovery = 81% Analysis Date = 03/11/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/06/16 Pct Recovery = 81% Analysis Date = 03/06/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/26/16 Pct Recovery = 82% Analysis Date = 02/26/16 Pct Recovery = 82% Analysis Date = 02/24/16 Pct Recovery = 82% Analysis Date = 02/24/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 82% Analysis Date = 02/22/16 Pct Recovery = 82% Analysis Date = 02/20/16 Pct Recovery = 82% Analysis Date = 02/20/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/17/16 Pct Recovery = 82% Analysis Date = 02/15/16 Pct Recovery = 82% Analysis Date = 02/15/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/11/16 Pct Recovery = 82% Analysis Date = 02/11/16 Pct Recovery = 82% Analysis Date = 02/09/16 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ETHOPROPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 14 91% 18% 90% 7%
Total 14 91% 18% 90% 7%

Sample Statistics
ETHOPROPHOS

Characteristic N % % Basis
Plotted 14 74% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 1 5% Spiked
Spiked 19 .  
False Negatives 4 21% 4 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
FENAMIPHOS
METHOD: 2033 , TESTIDCODE: 61591GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 67% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 95% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 88% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 81% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 81% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 85% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 80% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 115% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 86% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 87% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 113% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 143% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 106% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 87% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 79% Analysis Date = 05/10/17 Pct Recovery = 85% Analysis Date = 05/08/17 Pct Recovery = 85% Analysis Date = 05/08/17 Pct Recovery = 85% Analysis Date = 05/06/17 Pct Recovery = 86% Analysis Date = 05/06/17 Pct Recovery = 86% Analysis Date = 05/04/17 Pct Recovery = 86% Analysis Date = 05/04/17 Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 86% Analysis Date = 04/30/17 Pct Recovery = 86% Analysis Date = 04/30/17 Pct Recovery = 86% Analysis Date = 04/27/17 Pct Recovery = 86% Analysis Date = 04/27/17 Pct Recovery = 86% Analysis Date = 04/25/17 Pct Recovery = 87% Analysis Date = 04/25/17 Pct Recovery = 87% Analysis Date = 04/23/17 Pct Recovery = 87% Analysis Date = 04/23/17 Pct Recovery = 87% Analysis Date = 04/21/17 Pct Recovery = 87% Analysis Date = 04/21/17 Pct Recovery = 87% Analysis Date = 04/19/17 Pct Recovery = 87% Analysis Date = 04/19/17 Pct Recovery = 87% Analysis Date = 04/17/17 Pct Recovery = 87% Analysis Date = 04/17/17 Pct Recovery = 87% Analysis Date = 04/14/17 Pct Recovery = 87% Analysis Date = 04/14/17 Pct Recovery = 87% Analysis Date = 04/12/17 Pct Recovery = 88% Analysis Date = 04/12/17 Pct Recovery = 88% Analysis Date = 04/10/17 Pct Recovery = 88% Analysis Date = 04/10/17 Pct Recovery = 88% Analysis Date = 04/08/17 Pct Recovery = 88% Analysis Date = 04/08/17 Pct Recovery = 88% Analysis Date = 04/06/17 Pct Recovery = 88% Analysis Date = 04/06/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/01/17 Pct Recovery = 89% Analysis Date = 04/01/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/15/17 Pct Recovery = 90% Analysis Date = 03/15/17 Pct Recovery = 90% Analysis Date = 03/13/17 Pct Recovery = 90% Analysis Date = 03/13/17 Pct Recovery = 90% Analysis Date = 03/11/17 Pct Recovery = 90% Analysis Date = 03/11/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 91% Analysis Date = 03/08/17 Pct Recovery = 91% Analysis Date = 03/06/17 Pct Recovery = 91% Analysis Date = 03/06/17 Pct Recovery = 91% Analysis Date = 03/04/17 Pct Recovery = 91% Analysis Date = 03/04/17 Pct Recovery = 91% Analysis Date = 03/02/17 Pct Recovery = 91% Analysis Date = 03/02/17 Pct Recovery = 91% Analysis Date = 02/28/17 Pct Recovery = 91% Analysis Date = 02/28/17 Pct Recovery = 91% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/23/17 Pct Recovery = 92% Analysis Date = 02/23/17 Pct Recovery = 92% Analysis Date = 02/21/17 Pct Recovery = 92% Analysis Date = 02/21/17 Pct Recovery = 92% Analysis Date = 02/19/17 Pct Recovery = 92% Analysis Date = 02/19/17 Pct Recovery = 92% Analysis Date = 02/17/17 Pct Recovery = 92% Analysis Date = 02/17/17 Pct Recovery = 92% Analysis Date = 02/15/17 Pct Recovery = 92% Analysis Date = 02/15/17 Pct Recovery = 92% Analysis Date = 02/12/17 Pct Recovery = 92% Analysis Date = 02/12/17 Pct Recovery = 92% Analysis Date = 02/10/17 Pct Recovery = 92% Analysis Date = 02/10/17 Pct Recovery = 92% Analysis Date = 02/08/17 Pct Recovery = 92% Analysis Date = 02/08/17 Pct Recovery = 92% Analysis Date = 02/06/17 Pct Recovery = 92% Analysis Date = 02/06/17 Pct Recovery = 92% Analysis Date = 02/04/17 Pct Recovery = 92% Analysis Date = 02/04/17 Pct Recovery = 92% Analysis Date = 02/02/17 Pct Recovery = 92% Analysis Date = 02/02/17 Pct Recovery = 92% Analysis Date = 01/30/17 Pct Recovery = 92% Analysis Date = 01/30/17 Pct Recovery = 92% Analysis Date = 01/28/17 Pct Recovery = 92% Analysis Date = 01/28/17 Pct Recovery = 92% Analysis Date = 01/26/17 Pct Recovery = 92% Analysis Date = 01/26/17 Pct Recovery = 92% Analysis Date = 01/24/17 Pct Recovery = 92% Analysis Date = 01/24/17 Pct Recovery = 92% Analysis Date = 01/22/17 Pct Recovery = 92% Analysis Date = 01/22/17 Pct Recovery = 92% Analysis Date = 01/20/17 Pct Recovery = 92% Analysis Date = 01/20/17 Pct Recovery = 92% Analysis Date = 01/17/17 Pct Recovery = 92% Analysis Date = 01/17/17 Pct Recovery = 92% Analysis Date = 01/15/17 Pct Recovery = 92% Analysis Date = 01/15/17 Pct Recovery = 92% Analysis Date = 01/13/17 Pct Recovery = 92% Analysis Date = 01/13/17 Pct Recovery = 92% Analysis Date = 01/11/17 Pct Recovery = 92% Analysis Date = 01/11/17 Pct Recovery = 92% Analysis Date = 01/09/17 Pct Recovery = 92% Analysis Date = 01/09/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/07/17 Pct Recovery = 92% Analysis Date = 01/04/17 Pct Recovery = 93% Analysis Date = 01/04/17 Pct Recovery = 93% Analysis Date = 01/02/17 Pct Recovery = 93% Analysis Date = 01/02/17 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 93% Analysis Date = 12/20/16 Pct Recovery = 93% Analysis Date = 12/20/16 Pct Recovery = 93% Analysis Date = 12/18/16 Pct Recovery = 94% Analysis Date = 12/18/16 Pct Recovery = 94% Analysis Date = 12/16/16 Pct Recovery = 94% Analysis Date = 12/16/16 Pct Recovery = 94% Analysis Date = 12/14/16 Pct Recovery = 94% Analysis Date = 12/14/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/09/16 Pct Recovery = 94% Analysis Date = 12/09/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/07/16 Pct Recovery = 94% Analysis Date = 12/05/16 Pct Recovery = 94% Analysis Date = 12/05/16 Pct Recovery = 94% Analysis Date = 12/03/16 Pct Recovery = 94% Analysis Date = 12/03/16 Pct Recovery = 94% Analysis Date = 12/01/16 Pct Recovery = 95% Analysis Date = 12/01/16 Pct Recovery = 95% Analysis Date = 11/28/16 Pct Recovery = 95% Analysis Date = 11/28/16 Pct Recovery = 95% Analysis Date = 11/26/16 Pct Recovery = 95% Analysis Date = 11/26/16 Pct Recovery = 95% Analysis Date = 11/24/16 Pct Recovery = 95% Analysis Date = 11/24/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/17/16 Pct Recovery = 95% Analysis Date = 11/15/16 Pct Recovery = 95% Analysis Date = 11/15/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 96% Analysis Date = 11/13/16 Pct Recovery = 96% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/07/16 Pct Recovery = 96% Analysis Date = 11/07/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/25/16 Pct Recovery = 97% Analysis Date = 10/22/16 Pct Recovery = 97% Analysis Date = 10/22/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/20/16 Pct Recovery = 97% Analysis Date = 10/18/16 Pct Recovery = 97% Analysis Date = 10/18/16 Pct Recovery = 97% Analysis Date = 10/16/16 Pct Recovery = 97% Analysis Date = 10/16/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/14/16 Pct Recovery = 97% Analysis Date = 10/12/16 Pct Recovery = 97% Analysis Date = 10/12/16 Pct Recovery = 97% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/09/16 Pct Recovery = 98% Analysis Date = 10/07/16 Pct Recovery = 98% Analysis Date = 10/07/16 Pct Recovery = 98% Analysis Date = 10/05/16 Pct Recovery = 98% Analysis Date = 10/05/16 Pct Recovery = 98% Analysis Date = 10/03/16 Pct Recovery = 98% Analysis Date = 10/03/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 09/28/16 Pct Recovery = 98% Analysis Date = 09/28/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 98% Analysis Date = 09/22/16 Pct Recovery = 99% Analysis Date = 09/22/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/20/16 Pct Recovery = 99% Analysis Date = 09/18/16 Pct Recovery = 99% Analysis Date = 09/18/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/13/16 Pct Recovery = 99% Analysis Date = 09/13/16 Pct Recovery = 99% Analysis Date = 09/11/16 Pct Recovery = 99% Analysis Date = 09/11/16 Pct Recovery = 99% Analysis Date = 09/09/16 Pct Recovery = 99% Analysis Date = 09/09/16 Pct Recovery = 99% Analysis Date = 09/07/16 Pct Recovery = 99% Analysis Date = 09/07/16 Pct Recovery = 99% Analysis Date = 09/05/16 Pct Recovery = 99% Analysis Date = 09/05/16 Pct Recovery = 99% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 08/31/16 Pct Recovery = 98% Analysis Date = 08/31/16 Pct Recovery = 98% Analysis Date = 08/29/16 Pct Recovery = 98% Analysis Date = 08/29/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/27/16 Pct Recovery = 98% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/22/16 Pct Recovery = 98% Analysis Date = 08/22/16 Pct Recovery = 98% Analysis Date = 08/20/16 Pct Recovery = 98% Analysis Date = 08/20/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 98% Analysis Date = 08/16/16 Pct Recovery = 97% Analysis Date = 08/16/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/12/16 Pct Recovery = 97% Analysis Date = 08/12/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/09/16 Pct Recovery = 97% Analysis Date = 08/07/16 Pct Recovery = 97% Analysis Date = 08/07/16 Pct Recovery = 97% Analysis Date = 08/05/16 Pct Recovery = 97% Analysis Date = 08/05/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 08/01/16 Pct Recovery = 97% Analysis Date = 08/01/16 Pct Recovery = 97% Analysis Date = 07/30/16 Pct Recovery = 97% Analysis Date = 07/30/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 97% Analysis Date = 07/25/16 Pct Recovery = 97% Analysis Date = 07/25/16 Pct Recovery = 97% Analysis Date = 07/23/16 Pct Recovery = 97% Analysis Date = 07/23/16 Pct Recovery = 97% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/19/16 Pct Recovery = 96% Analysis Date = 07/19/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 96% Analysis Date = 07/14/16 Pct Recovery = 96% Analysis Date = 07/14/16 Pct Recovery = 96% Analysis Date = 07/12/16 Pct Recovery = 96% Analysis Date = 07/12/16 Pct Recovery = 96% Analysis Date = 07/10/16 Pct Recovery = 96% Analysis Date = 07/10/16 Pct Recovery = 96% Analysis Date = 07/08/16 Pct Recovery = 96% Analysis Date = 07/08/16 Pct Recovery = 96% Analysis Date = 07/06/16 Pct Recovery = 96% Analysis Date = 07/06/16 Pct Recovery = 96% Analysis Date = 07/03/16 Pct Recovery = 96% Analysis Date = 07/03/16 Pct Recovery = 96% Analysis Date = 07/01/16 Pct Recovery = 96% Analysis Date = 07/01/16 Pct Recovery = 96% Analysis Date = 06/29/16 Pct Recovery = 96% Analysis Date = 06/29/16 Pct Recovery = 96% Analysis Date = 06/27/16 Pct Recovery = 95% Analysis Date = 06/27/16 Pct Recovery = 95% Analysis Date = 06/25/16 Pct Recovery = 95% Analysis Date = 06/25/16 Pct Recovery = 95% Analysis Date = 06/23/16 Pct Recovery = 95% Analysis Date = 06/23/16 Pct Recovery = 95% Analysis Date = 06/20/16 Pct Recovery = 95% Analysis Date = 06/20/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/16/16 Pct Recovery = 95% Analysis Date = 06/16/16 Pct Recovery = 95% Analysis Date = 06/14/16 Pct Recovery = 95% Analysis Date = 06/14/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 95% Analysis Date = 06/07/16 Pct Recovery = 95% Analysis Date = 06/07/16 Pct Recovery = 95% Analysis Date = 06/05/16 Pct Recovery = 95% Analysis Date = 06/05/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 94% Analysis Date = 06/03/16 Pct Recovery = 94% Analysis Date = 06/01/16 Pct Recovery = 94% Analysis Date = 06/01/16 Pct Recovery = 94% Analysis Date = 05/30/16 Pct Recovery = 94% Analysis Date = 05/30/16 Pct Recovery = 94% Analysis Date = 05/27/16 Pct Recovery = 94% Analysis Date = 05/27/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/25/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/23/16 Pct Recovery = 94% Analysis Date = 05/21/16 Pct Recovery = 94% Analysis Date = 05/21/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/19/16 Pct Recovery = 94% Analysis Date = 05/17/16 Pct Recovery = 94% Analysis Date = 05/17/16 Pct Recovery = 94% Analysis Date = 05/14/16 Pct Recovery = 93% Analysis Date = 05/14/16 Pct Recovery = 93% Analysis Date = 05/12/16 Pct Recovery = 93% Analysis Date = 05/12/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/10/16 Pct Recovery = 93% Analysis Date = 05/08/16 Pct Recovery = 93% Analysis Date = 05/08/16 Pct Recovery = 93% Analysis Date = 05/06/16 Pct Recovery = 93% Analysis Date = 05/06/16 Pct Recovery = 93% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/04/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 05/01/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/29/16 Pct Recovery = 92% Analysis Date = 04/27/16 Pct Recovery = 92% Analysis Date = 04/27/16 Pct Recovery = 92% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/25/16 Pct Recovery = 91% Analysis Date = 04/23/16 Pct Recovery = 91% Analysis Date = 04/23/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/21/16 Pct Recovery = 91% Analysis Date = 04/18/16 Pct Recovery = 91% Analysis Date = 04/18/16 Pct Recovery = 91% Analysis Date = 04/16/16 Pct Recovery = 90% Analysis Date = 04/16/16 Pct Recovery = 90% Analysis Date = 04/14/16 Pct Recovery = 90% Analysis Date = 04/14/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/12/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/10/16 Pct Recovery = 90% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/07/16 Pct Recovery = 89% Analysis Date = 04/05/16 Pct Recovery = 89% Analysis Date = 04/05/16 Pct Recovery = 89% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 88% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/25/16 Pct Recovery = 86% Analysis Date = 03/23/16 Pct Recovery = 86% Analysis Date = 03/23/16 Pct Recovery = 86% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 85% Analysis Date = 03/17/16 Pct Recovery = 84% Analysis Date = 03/17/16 Pct Recovery = 84% Analysis Date = 03/15/16 Pct Recovery = 84% Analysis Date = 03/15/16 Pct Recovery = 84% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/12/16 Pct Recovery = 83% Analysis Date = 03/10/16 Pct Recovery = 82% Analysis Date = 03/10/16 Pct Recovery = 82% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/08/16 Pct Recovery = 82% Analysis Date = 03/06/16 Pct Recovery = 81% Analysis Date = 03/06/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/04/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 80% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 92% 18% 87% 11%
Total 18 92% 18% 87% 11%

Sample Statistics
FENAMIPHOS

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
FENAMIPHOS SULFONE
METHOD: 2033 , TESTIDCODE: 61645GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 64% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 64% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 79% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 36% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 68% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 67% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 71% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 87% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 91% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 104% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 85% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 80% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 96% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 95% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 96% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 81% Analysis Date = 05/10/17 Pct Recovery = 69% Analysis Date = 05/08/17 Pct Recovery = 70% Analysis Date = 05/08/17 Pct Recovery = 70% Analysis Date = 05/06/17 Pct Recovery = 70% Analysis Date = 05/06/17 Pct Recovery = 70% Analysis Date = 05/04/17 Pct Recovery = 70% Analysis Date = 05/04/17 Pct Recovery = 70% Analysis Date = 05/02/17 Pct Recovery = 70% Analysis Date = 05/02/17 Pct Recovery = 70% Analysis Date = 04/30/17 Pct Recovery = 70% Analysis Date = 04/30/17 Pct Recovery = 70% Analysis Date = 04/27/17 Pct Recovery = 71% Analysis Date = 04/27/17 Pct Recovery = 71% Analysis Date = 04/25/17 Pct Recovery = 71% Analysis Date = 04/25/17 Pct Recovery = 71% Analysis Date = 04/23/17 Pct Recovery = 71% Analysis Date = 04/23/17 Pct Recovery = 71% Analysis Date = 04/21/17 Pct Recovery = 71% Analysis Date = 04/21/17 Pct Recovery = 71% Analysis Date = 04/19/17 Pct Recovery = 71% Analysis Date = 04/19/17 Pct Recovery = 71% Analysis Date = 04/17/17 Pct Recovery = 72% Analysis Date = 04/17/17 Pct Recovery = 72% Analysis Date = 04/14/17 Pct Recovery = 72% Analysis Date = 04/14/17 Pct Recovery = 72% Analysis Date = 04/12/17 Pct Recovery = 72% Analysis Date = 04/12/17 Pct Recovery = 72% Analysis Date = 04/10/17 Pct Recovery = 72% Analysis Date = 04/10/17 Pct Recovery = 72% Analysis Date = 04/08/17 Pct Recovery = 72% Analysis Date = 04/08/17 Pct Recovery = 72% Analysis Date = 04/06/17 Pct Recovery = 73% Analysis Date = 04/06/17 Pct Recovery = 73% Analysis Date = 04/04/17 Pct Recovery = 73% Analysis Date = 04/04/17 Pct Recovery = 73% Analysis Date = 04/01/17 Pct Recovery = 73% Analysis Date = 04/01/17 Pct Recovery = 73% Analysis Date = 03/30/17 Pct Recovery = 73% Analysis Date = 03/30/17 Pct Recovery = 73% Analysis Date = 03/28/17 Pct Recovery = 73% Analysis Date = 03/28/17 Pct Recovery = 73% Analysis Date = 03/26/17 Pct Recovery = 73% Analysis Date = 03/26/17 Pct Recovery = 73% Analysis Date = 03/24/17 Pct Recovery = 74% Analysis Date = 03/24/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/21/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/19/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 74% Analysis Date = 03/17/17 Pct Recovery = 74% Analysis Date = 03/15/17 Pct Recovery = 74% Analysis Date = 03/15/17 Pct Recovery = 74% Analysis Date = 03/13/17 Pct Recovery = 75% Analysis Date = 03/13/17 Pct Recovery = 75% Analysis Date = 03/11/17 Pct Recovery = 75% Analysis Date = 03/11/17 Pct Recovery = 75% Analysis Date = 03/08/17 Pct Recovery = 75% Analysis Date = 03/08/17 Pct Recovery = 75% Analysis Date = 03/06/17 Pct Recovery = 75% Analysis Date = 03/06/17 Pct Recovery = 75% Analysis Date = 03/04/17 Pct Recovery = 75% Analysis Date = 03/04/17 Pct Recovery = 75% Analysis Date = 03/02/17 Pct Recovery = 76% Analysis Date = 03/02/17 Pct Recovery = 76% Analysis Date = 02/28/17 Pct Recovery = 76% Analysis Date = 02/28/17 Pct Recovery = 76% Analysis Date = 02/26/17 Pct Recovery = 76% Analysis Date = 02/26/17 Pct Recovery = 76% Analysis Date = 02/23/17 Pct Recovery = 76% Analysis Date = 02/23/17 Pct Recovery = 76% Analysis Date = 02/21/17 Pct Recovery = 77% Analysis Date = 02/21/17 Pct Recovery = 77% Analysis Date = 02/19/17 Pct Recovery = 77% Analysis Date = 02/19/17 Pct Recovery = 77% Analysis Date = 02/17/17 Pct Recovery = 77% Analysis Date = 02/17/17 Pct Recovery = 77% Analysis Date = 02/15/17 Pct Recovery = 78% Analysis Date = 02/15/17 Pct Recovery = 78% Analysis Date = 02/12/17 Pct Recovery = 78% Analysis Date = 02/12/17 Pct Recovery = 78% Analysis Date = 02/10/17 Pct Recovery = 78% Analysis Date = 02/10/17 Pct Recovery = 78% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/04/17 Pct Recovery = 79% Analysis Date = 02/04/17 Pct Recovery = 79% Analysis Date = 02/02/17 Pct Recovery = 80% Analysis Date = 02/02/17 Pct Recovery = 80% Analysis Date = 01/30/17 Pct Recovery = 80% Analysis Date = 01/30/17 Pct Recovery = 80% Analysis Date = 01/28/17 Pct Recovery = 80% Analysis Date = 01/28/17 Pct Recovery = 80% Analysis Date = 01/26/17 Pct Recovery = 81% Analysis Date = 01/26/17 Pct Recovery = 81% Analysis Date = 01/24/17 Pct Recovery = 81% Analysis Date = 01/24/17 Pct Recovery = 81% Analysis Date = 01/22/17 Pct Recovery = 82% Analysis Date = 01/22/17 Pct Recovery = 82% Analysis Date = 01/20/17 Pct Recovery = 82% Analysis Date = 01/20/17 Pct Recovery = 82% Analysis Date = 01/17/17 Pct Recovery = 82% Analysis Date = 01/17/17 Pct Recovery = 82% Analysis Date = 01/15/17 Pct Recovery = 82% Analysis Date = 01/15/17 Pct Recovery = 82% Analysis Date = 01/13/17 Pct Recovery = 82% Analysis Date = 01/13/17 Pct Recovery = 82% Analysis Date = 01/11/17 Pct Recovery = 82% Analysis Date = 01/11/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/09/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/02/17 Pct Recovery = 82% Analysis Date = 01/02/17 Pct Recovery = 82% Analysis Date = 12/31/16 Pct Recovery = 82% Analysis Date = 12/31/16 Pct Recovery = 82% Analysis Date = 12/29/16 Pct Recovery = 82% Analysis Date = 12/29/16 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/24/16 Pct Recovery = 81% Analysis Date = 12/24/16 Pct Recovery = 81% Analysis Date = 12/22/16 Pct Recovery = 81% Analysis Date = 12/22/16 Pct Recovery = 81% Analysis Date = 12/20/16 Pct Recovery = 81% Analysis Date = 12/20/16 Pct Recovery = 81% Analysis Date = 12/18/16 Pct Recovery = 81% Analysis Date = 12/18/16 Pct Recovery = 81% Analysis Date = 12/16/16 Pct Recovery = 81% Analysis Date = 12/16/16 Pct Recovery = 81% Analysis Date = 12/14/16 Pct Recovery = 81% Analysis Date = 12/14/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/09/16 Pct Recovery = 81% Analysis Date = 12/09/16 Pct Recovery = 81% Analysis Date = 12/07/16 Pct Recovery = 81% Analysis Date = 12/07/16 Pct Recovery = 81% Analysis Date = 12/05/16 Pct Recovery = 81% Analysis Date = 12/05/16 Pct Recovery = 81% Analysis Date = 12/03/16 Pct Recovery = 81% Analysis Date = 12/03/16 Pct Recovery = 81% Analysis Date = 12/01/16 Pct Recovery = 81% Analysis Date = 12/01/16 Pct Recovery = 81% Analysis Date = 11/28/16 Pct Recovery = 81% Analysis Date = 11/28/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/20/16 Pct Recovery = 80% Analysis Date = 11/20/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/17/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/09/16 Pct Recovery = 80% Analysis Date = 11/09/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/02/16 Pct Recovery = 80% Analysis Date = 11/02/16 Pct Recovery = 80% Analysis Date = 10/31/16 Pct Recovery = 80% Analysis Date = 10/31/16 Pct Recovery = 80% Analysis Date = 10/29/16 Pct Recovery = 80% Analysis Date = 10/29/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 80% Analysis Date = 10/27/16 Pct Recovery = 80% Analysis Date = 10/25/16 Pct Recovery = 80% Analysis Date = 10/25/16 Pct Recovery = 80% Analysis Date = 10/22/16 Pct Recovery = 80% Analysis Date = 10/22/16 Pct Recovery = 80% Analysis Date = 10/20/16 Pct Recovery = 80% Analysis Date = 10/20/16 Pct Recovery = 80% Analysis Date = 10/18/16 Pct Recovery = 80% Analysis Date = 10/18/16 Pct Recovery = 80% Analysis Date = 10/16/16 Pct Recovery = 79% Analysis Date = 10/16/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/14/16 Pct Recovery = 79% Analysis Date = 10/12/16 Pct Recovery = 79% Analysis Date = 10/12/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/09/16 Pct Recovery = 79% Analysis Date = 10/07/16 Pct Recovery = 79% Analysis Date = 10/07/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/11/16 Pct Recovery = 78% Analysis Date = 09/11/16 Pct Recovery = 78% Analysis Date = 09/09/16 Pct Recovery = 78% Analysis Date = 09/09/16 Pct Recovery = 78% Analysis Date = 09/07/16 Pct Recovery = 78% Analysis Date = 09/07/16 Pct Recovery = 78% Analysis Date = 09/05/16 Pct Recovery = 78% Analysis Date = 09/05/16 Pct Recovery = 78% Analysis Date = 09/02/16 Pct Recovery = 78% Analysis Date = 09/02/16 Pct Recovery = 78% Analysis Date = 08/31/16 Pct Recovery = 78% Analysis Date = 08/31/16 Pct Recovery = 78% Analysis Date = 08/29/16 Pct Recovery = 78% Analysis Date = 08/29/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 78% Analysis Date = 08/25/16 Pct Recovery = 78% Analysis Date = 08/25/16 Pct Recovery = 78% Analysis Date = 08/22/16 Pct Recovery = 78% Analysis Date = 08/22/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/20/16 Pct Recovery = 78% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/12/16 Pct Recovery = 79% Analysis Date = 08/12/16 Pct Recovery = 79% Analysis Date = 08/09/16 Pct Recovery = 79% Analysis Date = 08/09/16 Pct Recovery = 79% Analysis Date = 08/07/16 Pct Recovery = 79% Analysis Date = 08/07/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/05/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/23/16 Pct Recovery = 81% Analysis Date = 07/23/16 Pct Recovery = 81% Analysis Date = 07/21/16 Pct Recovery = 81% Analysis Date = 07/21/16 Pct Recovery = 81% Analysis Date = 07/19/16 Pct Recovery = 81% Analysis Date = 07/19/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/14/16 Pct Recovery = 81% Analysis Date = 07/14/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/12/16 Pct Recovery = 81% Analysis Date = 07/10/16 Pct Recovery = 82% Analysis Date = 07/10/16 Pct Recovery = 82% Analysis Date = 07/08/16 Pct Recovery = 82% Analysis Date = 07/08/16 Pct Recovery = 82% Analysis Date = 07/06/16 Pct Recovery = 82% Analysis Date = 07/06/16 Pct Recovery = 82% Analysis Date = 07/03/16 Pct Recovery = 82% Analysis Date = 07/03/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 82% Analysis Date = 06/29/16 Pct Recovery = 82% Analysis Date = 06/29/16 Pct Recovery = 82% Analysis Date = 06/27/16 Pct Recovery = 83% Analysis Date = 06/27/16 Pct Recovery = 83% Analysis Date = 06/25/16 Pct Recovery = 83% Analysis Date = 06/25/16 Pct Recovery = 83% Analysis Date = 06/23/16 Pct Recovery = 83% Analysis Date = 06/23/16 Pct Recovery = 83% Analysis Date = 06/20/16 Pct Recovery = 83% Analysis Date = 06/20/16 Pct Recovery = 83% Analysis Date = 06/18/16 Pct Recovery = 83% Analysis Date = 06/18/16 Pct Recovery = 83% Analysis Date = 06/16/16 Pct Recovery = 83% Analysis Date = 06/16/16 Pct Recovery = 83% Analysis Date = 06/14/16 Pct Recovery = 84% Analysis Date = 06/14/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/12/16 Pct Recovery = 84% Analysis Date = 06/10/16 Pct Recovery = 84% Analysis Date = 06/10/16 Pct Recovery = 84% Analysis Date = 06/07/16 Pct Recovery = 84% Analysis Date = 06/07/16 Pct Recovery = 84% Analysis Date = 06/05/16 Pct Recovery = 84% Analysis Date = 06/05/16 Pct Recovery = 84% Analysis Date = 06/03/16 Pct Recovery = 84% Analysis Date = 06/03/16 Pct Recovery = 84% Analysis Date = 06/01/16 Pct Recovery = 85% Analysis Date = 06/01/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/27/16 Pct Recovery = 85% Analysis Date = 05/27/16 Pct Recovery = 85% Analysis Date = 05/25/16 Pct Recovery = 85% Analysis Date = 05/25/16 Pct Recovery = 85% Analysis Date = 05/23/16 Pct Recovery = 85% Analysis Date = 05/23/16 Pct Recovery = 85% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/17/16 Pct Recovery = 86% Analysis Date = 05/17/16 Pct Recovery = 86% Analysis Date = 05/14/16 Pct Recovery = 86% Analysis Date = 05/14/16 Pct Recovery = 86% Analysis Date = 05/12/16 Pct Recovery = 86% Analysis Date = 05/12/16 Pct Recovery = 86% Analysis Date = 05/10/16 Pct Recovery = 86% Analysis Date = 05/10/16 Pct Recovery = 86% Analysis Date = 05/08/16 Pct Recovery = 86% Analysis Date = 05/08/16 Pct Recovery = 86% Analysis Date = 05/06/16 Pct Recovery = 86% Analysis Date = 05/06/16 Pct Recovery = 86% Analysis Date = 05/04/16 Pct Recovery = 86% Analysis Date = 05/04/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/29/16 Pct Recovery = 86% Analysis Date = 04/29/16 Pct Recovery = 86% Analysis Date = 04/27/16 Pct Recovery = 87% Analysis Date = 04/27/16 Pct Recovery = 87% Analysis Date = 04/25/16 Pct Recovery = 87% Analysis Date = 04/25/16 Pct Recovery = 87% Analysis Date = 04/23/16 Pct Recovery = 87% Analysis Date = 04/23/16 Pct Recovery = 87% Analysis Date = 04/21/16 Pct Recovery = 87% Analysis Date = 04/21/16 Pct Recovery = 87% Analysis Date = 04/18/16 Pct Recovery = 87% Analysis Date = 04/18/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 87% Analysis Date = 04/16/16 Pct Recovery = 87% Analysis Date = 04/14/16 Pct Recovery = 87% Analysis Date = 04/14/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/12/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/07/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 87% Analysis Date = 04/05/16 Pct Recovery = 87% Analysis Date = 04/03/16 Pct Recovery = 87% Analysis Date = 04/03/16 Pct Recovery = 87% Analysis Date = 04/01/16 Pct Recovery = 87% Analysis Date = 04/01/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/28/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/19/16 Pct Recovery = 87% Analysis Date = 03/19/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/17/16 Pct Recovery = 87% Analysis Date = 03/15/16 Pct Recovery = 87% Analysis Date = 03/15/16 Pct Recovery = 87% Analysis Date = 03/12/16 Pct Recovery = 86% Analysis Date = 03/12/16 Pct Recovery = 86% Analysis Date = 03/10/16 Pct Recovery = 86% Analysis Date = 03/10/16 Pct Recovery = 86% Analysis Date = 03/08/16 Pct Recovery = 86% Analysis Date = 03/08/16 Pct Recovery = 86% Analysis Date = 03/06/16 Pct Recovery = 86% Analysis Date = 03/06/16 Pct Recovery = 86% Analysis Date = 03/04/16 Pct Recovery = 86% Analysis Date = 03/04/16 Pct Recovery = 86% Analysis Date = 03/02/16 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 79% 16% 81% 17%
Total 18 79% 16% 81% 17%

Sample Statistics
FENAMIPHOS SULFONE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 1 10% 1 out of 10

OBSP Determination:
FENAMIPHOS SULFOXIDE
METHOD: 2033 , TESTIDCODE: 61646GCM39

Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 17% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 16% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 15% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 32% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 13% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 8% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 12% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 10% Analysis Date = 05/02/17 Pct Recovery = 32% Analysis Date = 04/30/17 Pct Recovery = 31% Analysis Date = 04/30/17 Pct Recovery = 31% Analysis Date = 04/28/17 Pct Recovery = 31% Analysis Date = 04/28/17 Pct Recovery = 31% Analysis Date = 04/26/17 Pct Recovery = 30% Analysis Date = 04/26/17 Pct Recovery = 30% Analysis Date = 04/24/17 Pct Recovery = 30% Analysis Date = 04/24/17 Pct Recovery = 30% Analysis Date = 04/21/17 Pct Recovery = 29% Analysis Date = 04/21/17 Pct Recovery = 29% Analysis Date = 04/19/17 Pct Recovery = 29% Analysis Date = 04/19/17 Pct Recovery = 29% Analysis Date = 04/17/17 Pct Recovery = 28% Analysis Date = 04/17/17 Pct Recovery = 28% Analysis Date = 04/15/17 Pct Recovery = 28% Analysis Date = 04/15/17 Pct Recovery = 28% Analysis Date = 04/12/17 Pct Recovery = 27% Analysis Date = 04/12/17 Pct Recovery = 27% Analysis Date = 04/10/17 Pct Recovery = 27% Analysis Date = 04/10/17 Pct Recovery = 27% Analysis Date = 04/08/17 Pct Recovery = 26% Analysis Date = 04/08/17 Pct Recovery = 26% Analysis Date = 04/06/17 Pct Recovery = 25% Analysis Date = 04/06/17 Pct Recovery = 25% Analysis Date = 04/03/17 Pct Recovery = 25% Analysis Date = 04/03/17 Pct Recovery = 25% Analysis Date = 04/01/17 Pct Recovery = 24% Analysis Date = 04/01/17 Pct Recovery = 24% Analysis Date = 03/30/17 Pct Recovery = 24% Analysis Date = 03/30/17 Pct Recovery = 24% Analysis Date = 03/28/17 Pct Recovery = 23% Analysis Date = 03/28/17 Pct Recovery = 23% Analysis Date = 03/25/17 Pct Recovery = 23% Analysis Date = 03/25/17 Pct Recovery = 23% Analysis Date = 03/23/17 Pct Recovery = 22% Analysis Date = 03/23/17 Pct Recovery = 22% Analysis Date = 03/21/17 Pct Recovery = 22% Analysis Date = 03/21/17 Pct Recovery = 22% Analysis Date = 03/19/17 Pct Recovery = 21% Analysis Date = 03/19/17 Pct Recovery = 21% Analysis Date = 03/16/17 Pct Recovery = 21% Analysis Date = 03/16/17 Pct Recovery = 21% Analysis Date = 03/14/17 Pct Recovery = 20% Analysis Date = 03/14/17 Pct Recovery = 20% Analysis Date = 03/12/17 Pct Recovery = 20% Analysis Date = 03/12/17 Pct Recovery = 20% Analysis Date = 03/10/17 Pct Recovery = 19% Analysis Date = 03/10/17 Pct Recovery = 19% Analysis Date = 03/07/17 Pct Recovery = 19% Analysis Date = 03/07/17 Pct Recovery = 19% Analysis Date = 03/05/17 Pct Recovery = 18% Analysis Date = 03/05/17 Pct Recovery = 18% Analysis Date = 03/03/17 Pct Recovery = 18% Analysis Date = 03/03/17 Pct Recovery = 18% Analysis Date = 03/01/17 Pct Recovery = 17% Analysis Date = 03/01/17 Pct Recovery = 17% Analysis Date = 02/26/17 Pct Recovery = 17% Analysis Date = 02/26/17 Pct Recovery = 17% Analysis Date = 02/24/17 Pct Recovery = 17% Analysis Date = 02/24/17 Pct Recovery = 17% Analysis Date = 02/22/17 Pct Recovery = 17% Analysis Date = 02/22/17 Pct Recovery = 17% Analysis Date = 02/20/17 Pct Recovery = 16% Analysis Date = 02/20/17 Pct Recovery = 16% Analysis Date = 02/17/17 Pct Recovery = 16% Analysis Date = 02/17/17 Pct Recovery = 16% Analysis Date = 02/15/17 Pct Recovery = 16% Analysis Date = 02/15/17 Pct Recovery = 16% Analysis Date = 02/13/17 Pct Recovery = 16% Analysis Date = 02/13/17 Pct Recovery = 16% Analysis Date = 02/11/17 Pct Recovery = 16% Analysis Date = 02/11/17 Pct Recovery = 16% Analysis Date = 02/08/17 Pct Recovery = 16% Analysis Date = 02/08/17 Pct Recovery = 16% Analysis Date = 02/06/17 Pct Recovery = 16% Analysis Date = 02/06/17 Pct Recovery = 16% Analysis Date = 02/04/17 Pct Recovery = 15% Analysis Date = 02/04/17 Pct Recovery = 15% Analysis Date = 02/02/17 Pct Recovery = 15% Analysis Date = 02/02/17 Pct Recovery = 15% Analysis Date = 01/30/17 Pct Recovery = 15% Analysis Date = 01/30/17 Pct Recovery = 15% Analysis Date = 01/28/17 Pct Recovery = 15% Analysis Date = 01/28/17 Pct Recovery = 15% Analysis Date = 01/26/17 Pct Recovery = 15% Analysis Date = 01/26/17 Pct Recovery = 15% Analysis Date = 01/24/17 Pct Recovery = 15% Analysis Date = 01/24/17 Pct Recovery = 15% Analysis Date = 01/21/17 Pct Recovery = 15% Analysis Date = 01/21/17 Pct Recovery = 15% Analysis Date = 01/19/17 Pct Recovery = 15% Analysis Date = 01/19/17 Pct Recovery = 15% Analysis Date = 01/17/17 Pct Recovery = 14% Analysis Date = 01/17/17 Pct Recovery = 14% Analysis Date = 01/15/17 Pct Recovery = 14% Analysis Date = 01/15/17 Pct Recovery = 14% Analysis Date = 01/12/17 Pct Recovery = 14% Analysis Date = 01/12/17 Pct Recovery = 14% Analysis Date = 01/10/17 Pct Recovery = 14% Analysis Date = 01/10/17 Pct Recovery = 14% Analysis Date = 01/08/17 Pct Recovery = 14% Analysis Date = 01/08/17 Pct Recovery = 14% Analysis Date = 01/06/17 Pct Recovery = 14% Analysis Date = 01/06/17 Pct Recovery = 14% Analysis Date = 01/04/17 Pct Recovery = 14% Analysis Date = 01/04/17 Pct Recovery = 14% Analysis Date = 01/01/17 Pct Recovery = 13% Analysis Date = 01/01/17 Pct Recovery = 13% Analysis Date = 12/30/16 Pct Recovery = 13% Analysis Date = 12/30/16 Pct Recovery = 13% Analysis Date = 12/28/16 Pct Recovery = 13% Analysis Date = 12/28/16 Pct Recovery = 13% Analysis Date = 12/26/16 Pct Recovery = 13% Analysis Date = 12/26/16 Pct Recovery = 13% Analysis Date = 12/23/16 Pct Recovery = 13% Analysis Date = 12/23/16 Pct Recovery = 13% Analysis Date = 12/21/16 Pct Recovery = 13% Analysis Date = 12/21/16 Pct Recovery = 13% Analysis Date = 12/19/16 Pct Recovery = 13% Analysis Date = 12/19/16 Pct Recovery = 13% Analysis Date = 12/17/16 Pct Recovery = 13% Analysis Date = 12/17/16 Pct Recovery = 13% Analysis Date = 12/14/16 Pct Recovery = 12% Analysis Date = 12/14/16 Pct Recovery = 12% Analysis Date = 12/12/16 Pct Recovery = 12% Analysis Date = 12/12/16 Pct Recovery = 12% Analysis Date = 12/10/16 Pct Recovery = 12% Analysis Date = 12/10/16 Pct Recovery = 12% Analysis Date = 12/08/16 Pct Recovery = 12% Analysis Date = 12/08/16 Pct Recovery = 12% Analysis Date = 12/05/16 Pct Recovery = 12% Analysis Date = 12/05/16 Pct Recovery = 12% Analysis Date = 12/03/16 Pct Recovery = 12% Analysis Date = 12/03/16 Pct Recovery = 12% Analysis Date = 12/01/16 Pct Recovery = 12% Analysis Date = 12/01/16 Pct Recovery = 12% Analysis Date = 11/29/16 Pct Recovery = 12% Analysis Date = 11/29/16 Pct Recovery = 12% Analysis Date = 11/26/16 Pct Recovery = 12% Analysis Date = 11/26/16 Pct Recovery = 12% Analysis Date = 11/24/16 Pct Recovery = 12% Analysis Date = 11/24/16 Pct Recovery = 12% Analysis Date = 11/22/16 Pct Recovery = 12% Analysis Date = 11/22/16 Pct Recovery = 12% Analysis Date = 11/20/16 Pct Recovery = 12% Analysis Date = 11/20/16 Pct Recovery = 12% Analysis Date = 11/17/16 Pct Recovery = 12% Analysis Date = 11/17/16 Pct Recovery = 12% Analysis Date = 11/15/16 Pct Recovery = 11% Analysis Date = 11/15/16 Pct Recovery = 11% Analysis Date = 11/13/16 Pct Recovery = 11% Analysis Date = 11/13/16 Pct Recovery = 11% Analysis Date = 11/11/16 Pct Recovery = 11% Analysis Date = 11/11/16 Pct Recovery = 11% Analysis Date = 11/08/16 Pct Recovery = 11% Analysis Date = 11/08/16 Pct Recovery = 11% Analysis Date = 11/06/16 Pct Recovery = 11% Analysis Date = 11/06/16 Pct Recovery = 11% Analysis Date = 11/04/16 Pct Recovery = 11% Analysis Date = 11/04/16 Pct Recovery = 11% Analysis Date = 11/02/16 Pct Recovery = 11% Analysis Date = 11/02/16 Pct Recovery = 11% Analysis Date = 10/30/16 Pct Recovery = 11% Analysis Date = 10/30/16 Pct Recovery = 11% Analysis Date = 10/28/16 Pct Recovery = 11% Analysis Date = 10/28/16 Pct Recovery = 11% Analysis Date = 10/26/16 Pct Recovery = 11% Analysis Date = 10/26/16 Pct Recovery = 11% Analysis Date = 10/24/16 Pct Recovery = 11% Analysis Date = 10/24/16 Pct Recovery = 11% Analysis Date = 10/21/16 Pct Recovery = 11% Analysis Date = 10/21/16 Pct Recovery = 11% Analysis Date = 10/19/16 Pct Recovery = 11% Analysis Date = 10/19/16 Pct Recovery = 11% Analysis Date = 10/17/16 Pct Recovery = 11% Analysis Date = 10/17/16 Pct Recovery = 11% Analysis Date = 10/15/16 Pct Recovery = 10% Analysis Date = 10/15/16 Pct Recovery = 10% Analysis Date = 10/12/16 Pct Recovery = 10% Analysis Date = 10/12/16 Pct Recovery = 10% Analysis Date = 10/10/16 Pct Recovery = 10% Analysis Date = 10/10/16 Pct Recovery = 10% Analysis Date = 10/08/16 Pct Recovery = 10% Analysis Date = 10/08/16 Pct Recovery = 10% Analysis Date = 10/06/16 Pct Recovery = 10% Analysis Date = 10/06/16 Pct Recovery = 10% Analysis Date = 10/03/16 Pct Recovery = 10% Analysis Date = 10/03/16 Pct Recovery = 10% Analysis Date = 10/01/16 Pct Recovery = 10% Analysis Date = 10/01/16 Pct Recovery = 10% Analysis Date = 09/29/16 Pct Recovery = 10% Analysis Date = 09/29/16 Pct Recovery = 10% Analysis Date = 09/27/16 Pct Recovery = 10% Analysis Date = 09/27/16 Pct Recovery = 10% Analysis Date = 09/24/16 Pct Recovery = 10% Analysis Date = 09/24/16 Pct Recovery = 10% Analysis Date = 09/22/16 Pct Recovery = 10% Analysis Date = 09/22/16 Pct Recovery = 10% Analysis Date = 09/20/16 Pct Recovery = 10% Analysis Date = 09/20/16 Pct Recovery = 10% Analysis Date = 09/18/16 Pct Recovery = 10% Analysis Date = 09/18/16 Pct Recovery = 10% Analysis Date = 09/16/16 Pct Recovery = 9% Analysis Date = 09/16/16 Pct Recovery = 9% Analysis Date = 09/13/16 Pct Recovery = 9% Analysis Date = 09/13/16 Pct Recovery = 9% Analysis Date = 09/11/16 Pct Recovery = 9% Analysis Date = 09/11/16 Pct Recovery = 9% Analysis Date = 09/09/16 Pct Recovery = 9% Analysis Date = 09/09/16 Pct Recovery = 9% Analysis Date = 09/07/16 Pct Recovery = 9% Analysis Date = 09/07/16 Pct Recovery = 9% Analysis Date = 09/04/16 Pct Recovery = 9% Analysis Date = 09/04/16 Pct Recovery = 9% Analysis Date = 09/02/16 Pct Recovery = 9% Analysis Date = 09/02/16 Pct Recovery = 9% Analysis Date = 08/31/16 Pct Recovery = 9% Analysis Date = 08/31/16 Pct Recovery = 9% Analysis Date = 08/29/16 Pct Recovery = 9% Analysis Date = 08/29/16 Pct Recovery = 9% Analysis Date = 08/26/16 Pct Recovery = 9% Analysis Date = 08/26/16 Pct Recovery = 9% Analysis Date = 08/24/16 Pct Recovery = 9% Analysis Date = 08/24/16 Pct Recovery = 9% Analysis Date = 08/22/16 Pct Recovery = 9% Analysis Date = 08/22/16 Pct Recovery = 9% Analysis Date = 08/20/16 Pct Recovery = 9% Analysis Date = 08/20/16 Pct Recovery = 9% Analysis Date = 08/17/16 Pct Recovery = 10% Analysis Date = 08/17/16 Pct Recovery = 10% Analysis Date = 08/15/16 Pct Recovery = 10% Analysis Date = 08/15/16 Pct Recovery = 10% Analysis Date = 08/13/16 Pct Recovery = 10% Analysis Date = 08/13/16 Pct Recovery = 10% Analysis Date = 08/11/16 Pct Recovery = 10% Analysis Date = 08/11/16 Pct Recovery = 10% Analysis Date = 08/08/16 Pct Recovery = 10% Analysis Date = 08/08/16 Pct Recovery = 10% Analysis Date = 08/06/16 Pct Recovery = 10% Analysis Date = 08/06/16 Pct Recovery = 10% Analysis Date = 08/04/16 Pct Recovery = 10% Analysis Date = 08/04/16 Pct Recovery = 10% Analysis Date = 08/02/16 Pct Recovery = 10% Analysis Date = 08/02/16 Pct Recovery = 10% Analysis Date = 07/30/16 Pct Recovery = 10% Analysis Date = 07/30/16 Pct Recovery = 10% Analysis Date = 07/28/16 Pct Recovery = 10% Analysis Date = 07/28/16 Pct Recovery = 10% Analysis Date = 07/26/16 Pct Recovery = 10% Analysis Date = 07/26/16 Pct Recovery = 10% Analysis Date = 07/24/16 Pct Recovery = 11% Analysis Date = 07/24/16 Pct Recovery = 11% Analysis Date = 07/21/16 Pct Recovery = 11% Analysis Date = 07/21/16 Pct Recovery = 11% Analysis Date = 07/19/16 Pct Recovery = 11% Analysis Date = 07/19/16 Pct Recovery = 11% Analysis Date = 07/17/16 Pct Recovery = 11% Analysis Date = 07/17/16 Pct Recovery = 11% Analysis Date = 07/15/16 Pct Recovery = 11% Analysis Date = 07/15/16 Pct Recovery = 11% Analysis Date = 07/12/16 Pct Recovery = 11% Analysis Date = 07/12/16 Pct Recovery = 11% Analysis Date = 07/10/16 Pct Recovery = 11% Analysis Date = 07/10/16 Pct Recovery = 11% Analysis Date = 07/08/16 Pct Recovery = 11% Analysis Date = 07/08/16 Pct Recovery = 11% Analysis Date = 07/06/16 Pct Recovery = 11% Analysis Date = 07/06/16 Pct Recovery = 11% Analysis Date = 07/03/16 Pct Recovery = 11% Analysis Date = 07/03/16 Pct Recovery = 11% Analysis Date = 07/01/16 Pct Recovery = 11% Analysis Date = 07/01/16 Pct Recovery = 11% Analysis Date = 06/29/16 Pct Recovery = 12% Analysis Date = 06/29/16 Pct Recovery = 12% Analysis Date = 06/27/16 Pct Recovery = 12% Analysis Date = 06/27/16 Pct Recovery = 12% Analysis Date = 06/24/16 Pct Recovery = 12% Analysis Date = 06/24/16 Pct Recovery = 12% Analysis Date = 06/22/16 Pct Recovery = 12% Analysis Date = 06/22/16 Pct Recovery = 12% Analysis Date = 06/20/16 Pct Recovery = 12% Analysis Date = 06/20/16 Pct Recovery = 12% Analysis Date = 06/18/16 Pct Recovery = 12% Analysis Date = 06/18/16 Pct Recovery = 12% Analysis Date = 06/15/16 Pct Recovery = 12% Analysis Date = 06/15/16 Pct Recovery = 12% Analysis Date = 06/13/16 Pct Recovery = 12% Analysis Date = 06/13/16 Pct Recovery = 12% Analysis Date = 06/11/16 Pct Recovery = 12% Analysis Date = 06/11/16 Pct Recovery = 12% Analysis Date = 06/09/16 Pct Recovery = 12% Analysis Date = 06/09/16 Pct Recovery = 12% Analysis Date = 06/06/16 Pct Recovery = 12% Analysis Date = 06/06/16 Pct Recovery = 12% Analysis Date = 06/04/16 Pct Recovery = 12% Analysis Date = 06/04/16 Pct Recovery = 12% Analysis Date = 06/02/16 Pct Recovery = 13% Analysis Date = 06/02/16 Pct Recovery = 13% Analysis Date = 05/31/16 Pct Recovery = 13% Analysis Date = 05/31/16 Pct Recovery = 13% Analysis Date = 05/29/16 Pct Recovery = 13% Analysis Date = 05/29/16 Pct Recovery = 13% Analysis Date = 05/26/16 Pct Recovery = 13% Analysis Date = 05/26/16 Pct Recovery = 13% Analysis Date = 05/24/16 Pct Recovery = 13% Analysis Date = 05/24/16 Pct Recovery = 13% Analysis Date = 05/22/16 Pct Recovery = 13% Analysis Date = 05/22/16 Pct Recovery = 13% Analysis Date = 05/20/16 Pct Recovery = 13% Analysis Date = 05/20/16 Pct Recovery = 13% Analysis Date = 05/17/16 Pct Recovery = 13% Analysis Date = 05/17/16 Pct Recovery = 13% Analysis Date = 05/15/16 Pct Recovery = 13% Analysis Date = 05/15/16 Pct Recovery = 13% Analysis Date = 05/13/16 Pct Recovery = 13% Analysis Date = 05/13/16 Pct Recovery = 13% Analysis Date = 05/11/16 Pct Recovery = 13% Analysis Date = 05/11/16 Pct Recovery = 13% Analysis Date = 05/08/16 Pct Recovery = 14% Analysis Date = 05/08/16 Pct Recovery = 14% Analysis Date = 05/06/16 Pct Recovery = 14% Analysis Date = 05/06/16 Pct Recovery = 14% Analysis Date = 05/04/16 Pct Recovery = 14% Analysis Date = 05/04/16 Pct Recovery = 14% Analysis Date = 05/02/16 Pct Recovery = 14% Analysis Date = 05/02/16 Pct Recovery = 14% Analysis Date = 04/29/16 Pct Recovery = 14% Analysis Date = 04/29/16 Pct Recovery = 14% Analysis Date = 04/27/16 Pct Recovery = 14% Analysis Date = 04/27/16 Pct Recovery = 14% Analysis Date = 04/25/16 Pct Recovery = 14% Analysis Date = 04/25/16 Pct Recovery = 14% Analysis Date = 04/23/16 Pct Recovery = 13% Analysis Date = 04/23/16 Pct Recovery = 13% Analysis Date = 04/20/16 Pct Recovery = 13% Analysis Date = 04/20/16 Pct Recovery = 13% Analysis Date = 04/18/16 Pct Recovery = 13% Analysis Date = 04/18/16 Pct Recovery = 13% Analysis Date = 04/16/16 Pct Recovery = 13% Analysis Date = 04/16/16 Pct Recovery = 13% Analysis Date = 04/14/16 Pct Recovery = 13% Analysis Date = 04/14/16 Pct Recovery = 13% Analysis Date = 04/11/16 Pct Recovery = 13% Analysis Date = 04/11/16 Pct Recovery = 13% Analysis Date = 04/09/16 Pct Recovery = 13% Analysis Date = 04/09/16 Pct Recovery = 13% Analysis Date = 04/07/16 Pct Recovery = 13% Analysis Date = 04/07/16 Pct Recovery = 13% Analysis Date = 04/05/16 Pct Recovery = 13% Analysis Date = 04/05/16 Pct Recovery = 13% Analysis Date = 04/02/16 Pct Recovery = 13% Analysis Date = 04/02/16 Pct Recovery = 13% Analysis Date = 03/31/16 Pct Recovery = 13% Analysis Date = 03/31/16 Pct Recovery = 13% Analysis Date = 03/29/16 Pct Recovery = 13% Analysis Date = 03/29/16 Pct Recovery = 13% Analysis Date = 03/27/16 Pct Recovery = 13% Analysis Date = 03/27/16 Pct Recovery = 13% Analysis Date = 03/24/16 Pct Recovery = 13% Analysis Date = 03/24/16 Pct Recovery = 13% Analysis Date = 03/22/16 Pct Recovery = 12% Analysis Date = 03/22/16 Pct Recovery = 12% Analysis Date = 03/20/16 Pct Recovery = 12% Analysis Date = 03/20/16 Pct Recovery = 12% Analysis Date = 03/18/16 Pct Recovery = 12% Analysis Date = 03/18/16 Pct Recovery = 12% Analysis Date = 03/15/16 Pct Recovery = 12% Analysis Date = 03/15/16 Pct Recovery = 12% Analysis Date = 03/13/16 Pct Recovery = 12% Analysis Date = 03/13/16 Pct Recovery = 12% Analysis Date = 03/11/16 Pct Recovery = 12% Analysis Date = 03/11/16 Pct Recovery = 12% Analysis Date = 03/09/16 Pct Recovery = 12% Analysis Date = 03/09/16 Pct Recovery = 12% Analysis Date = 03/06/16 Pct Recovery = 12% Analysis Date = 03/06/16 Pct Recovery = 12% Analysis Date = 03/04/16 Pct Recovery = 12% Analysis Date = 03/04/16 Pct Recovery = 12% Analysis Date = 03/02/16 Pct Recovery = 12% Analysis Date = 03/02/16 Pct Recovery = 12% Analysis Date = 02/29/16 Pct Recovery = 12% Analysis Date = 02/29/16 Pct Recovery = 12% Analysis Date = 02/26/16 Pct Recovery = 11% Analysis Date = 02/26/16 Pct Recovery = 11% Analysis Date = 02/24/16 Pct Recovery = 11% Analysis Date = 02/24/16 Pct Recovery = 11% Analysis Date = 02/22/16 Pct Recovery = 11% Analysis Date = 02/22/16 Pct Recovery = 11% Analysis Date = 02/20/16 Pct Recovery = 11% Analysis Date = 02/20/16 Pct Recovery = 11% Analysis Date = 02/17/16 Pct Recovery = 11% Analysis Date = 02/17/16 Pct Recovery = 11% Analysis Date = 02/15/16 Pct Recovery = 11% Analysis Date = 02/15/16 Pct Recovery = 11% Analysis Date = 02/13/16 Pct Recovery = 11% Analysis Date = 02/13/16 Pct Recovery = 11% Analysis Date = 02/11/16 Pct Recovery = 11% Analysis Date = 02/11/16 Pct Recovery = 11% Analysis Date = 02/09/16 Pct Recovery = 11% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FENAMIPHOS SULFOXIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 8 15% 7% 14% 4%
Total 8 15% 7% 14% 4%

Sample Statistics
FENAMIPHOS SULFOXIDE

Characteristic N % % Basis
Plotted 8 89% Spiked
Estimated Values 8 89% Spiked
Deleted Values 1 10% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 10 .  
False Negatives 1 11% 1 out of 9
Not Spiked 0 .  
False Positives 0 . 0 out of 0

OBSP Determination:
FIPRONIL
METHOD: 2033 , TESTIDCODE: 62166GCM29

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 92% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 99% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 94% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 100% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 95% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 111% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 108% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 130% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 104% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 95% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 101% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 126% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 136% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 123% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 121% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 118% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 122% Analysis Date = 05/02/17 Pct Recovery = 112% Analysis Date = 04/30/17 Pct Recovery = 112% Analysis Date = 04/30/17 Pct Recovery = 112% Analysis Date = 04/28/17 Pct Recovery = 111% Analysis Date = 04/28/17 Pct Recovery = 111% Analysis Date = 04/26/17 Pct Recovery = 111% Analysis Date = 04/26/17 Pct Recovery = 111% Analysis Date = 04/24/17 Pct Recovery = 111% Analysis Date = 04/24/17 Pct Recovery = 111% Analysis Date = 04/21/17 Pct Recovery = 110% Analysis Date = 04/21/17 Pct Recovery = 110% Analysis Date = 04/19/17 Pct Recovery = 110% Analysis Date = 04/19/17 Pct Recovery = 110% Analysis Date = 04/17/17 Pct Recovery = 110% Analysis Date = 04/17/17 Pct Recovery = 110% Analysis Date = 04/15/17 Pct Recovery = 109% Analysis Date = 04/15/17 Pct Recovery = 109% Analysis Date = 04/12/17 Pct Recovery = 109% Analysis Date = 04/12/17 Pct Recovery = 109% Analysis Date = 04/10/17 Pct Recovery = 109% Analysis Date = 04/10/17 Pct Recovery = 109% Analysis Date = 04/08/17 Pct Recovery = 108% Analysis Date = 04/08/17 Pct Recovery = 108% Analysis Date = 04/06/17 Pct Recovery = 108% Analysis Date = 04/06/17 Pct Recovery = 108% Analysis Date = 04/03/17 Pct Recovery = 108% Analysis Date = 04/03/17 Pct Recovery = 108% Analysis Date = 04/01/17 Pct Recovery = 107% Analysis Date = 04/01/17 Pct Recovery = 107% Analysis Date = 03/30/17 Pct Recovery = 107% Analysis Date = 03/30/17 Pct Recovery = 107% Analysis Date = 03/28/17 Pct Recovery = 107% Analysis Date = 03/28/17 Pct Recovery = 107% Analysis Date = 03/25/17 Pct Recovery = 106% Analysis Date = 03/25/17 Pct Recovery = 106% Analysis Date = 03/23/17 Pct Recovery = 106% Analysis Date = 03/23/17 Pct Recovery = 106% Analysis Date = 03/21/17 Pct Recovery = 106% Analysis Date = 03/21/17 Pct Recovery = 106% Analysis Date = 03/19/17 Pct Recovery = 105% Analysis Date = 03/19/17 Pct Recovery = 105% Analysis Date = 03/16/17 Pct Recovery = 105% Analysis Date = 03/16/17 Pct Recovery = 105% Analysis Date = 03/14/17 Pct Recovery = 105% Analysis Date = 03/14/17 Pct Recovery = 105% Analysis Date = 03/12/17 Pct Recovery = 104% Analysis Date = 03/12/17 Pct Recovery = 104% Analysis Date = 03/10/17 Pct Recovery = 104% Analysis Date = 03/10/17 Pct Recovery = 104% Analysis Date = 03/07/17 Pct Recovery = 104% Analysis Date = 03/07/17 Pct Recovery = 104% Analysis Date = 03/05/17 Pct Recovery = 104% Analysis Date = 03/05/17 Pct Recovery = 104% Analysis Date = 03/03/17 Pct Recovery = 103% Analysis Date = 03/03/17 Pct Recovery = 103% Analysis Date = 03/01/17 Pct Recovery = 103% Analysis Date = 03/01/17 Pct Recovery = 103% Analysis Date = 02/26/17 Pct Recovery = 103% Analysis Date = 02/26/17 Pct Recovery = 103% Analysis Date = 02/24/17 Pct Recovery = 102% Analysis Date = 02/24/17 Pct Recovery = 102% Analysis Date = 02/22/17 Pct Recovery = 102% Analysis Date = 02/22/17 Pct Recovery = 102% Analysis Date = 02/20/17 Pct Recovery = 102% Analysis Date = 02/20/17 Pct Recovery = 102% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/11/17 Pct Recovery = 101% Analysis Date = 02/11/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 101% Analysis Date = 02/04/17 Pct Recovery = 102% Analysis Date = 02/04/17 Pct Recovery = 102% Analysis Date = 02/02/17 Pct Recovery = 102% Analysis Date = 02/02/17 Pct Recovery = 102% Analysis Date = 01/30/17 Pct Recovery = 102% Analysis Date = 01/30/17 Pct Recovery = 102% Analysis Date = 01/28/17 Pct Recovery = 102% Analysis Date = 01/28/17 Pct Recovery = 102% Analysis Date = 01/26/17 Pct Recovery = 102% Analysis Date = 01/26/17 Pct Recovery = 102% Analysis Date = 01/24/17 Pct Recovery = 102% Analysis Date = 01/24/17 Pct Recovery = 102% Analysis Date = 01/21/17 Pct Recovery = 102% Analysis Date = 01/21/17 Pct Recovery = 102% Analysis Date = 01/19/17 Pct Recovery = 102% Analysis Date = 01/19/17 Pct Recovery = 102% Analysis Date = 01/17/17 Pct Recovery = 102% Analysis Date = 01/17/17 Pct Recovery = 102% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/12/17 Pct Recovery = 102% Analysis Date = 01/12/17 Pct Recovery = 102% Analysis Date = 01/10/17 Pct Recovery = 103% Analysis Date = 01/10/17 Pct Recovery = 103% Analysis Date = 01/08/17 Pct Recovery = 103% Analysis Date = 01/08/17 Pct Recovery = 103% Analysis Date = 01/06/17 Pct Recovery = 103% Analysis Date = 01/06/17 Pct Recovery = 103% Analysis Date = 01/04/17 Pct Recovery = 103% Analysis Date = 01/04/17 Pct Recovery = 103% Analysis Date = 01/01/17 Pct Recovery = 103% Analysis Date = 01/01/17 Pct Recovery = 103% Analysis Date = 12/30/16 Pct Recovery = 103% Analysis Date = 12/30/16 Pct Recovery = 103% Analysis Date = 12/28/16 Pct Recovery = 103% Analysis Date = 12/28/16 Pct Recovery = 103% Analysis Date = 12/26/16 Pct Recovery = 103% Analysis Date = 12/26/16 Pct Recovery = 103% Analysis Date = 12/23/16 Pct Recovery = 103% Analysis Date = 12/23/16 Pct Recovery = 103% Analysis Date = 12/21/16 Pct Recovery = 103% Analysis Date = 12/21/16 Pct Recovery = 103% Analysis Date = 12/19/16 Pct Recovery = 103% Analysis Date = 12/19/16 Pct Recovery = 103% Analysis Date = 12/17/16 Pct Recovery = 104% Analysis Date = 12/17/16 Pct Recovery = 104% Analysis Date = 12/14/16 Pct Recovery = 104% Analysis Date = 12/14/16 Pct Recovery = 104% Analysis Date = 12/12/16 Pct Recovery = 104% Analysis Date = 12/12/16 Pct Recovery = 104% Analysis Date = 12/10/16 Pct Recovery = 104% Analysis Date = 12/10/16 Pct Recovery = 104% Analysis Date = 12/08/16 Pct Recovery = 104% Analysis Date = 12/08/16 Pct Recovery = 104% Analysis Date = 12/05/16 Pct Recovery = 104% Analysis Date = 12/05/16 Pct Recovery = 104% Analysis Date = 12/03/16 Pct Recovery = 104% Analysis Date = 12/03/16 Pct Recovery = 104% Analysis Date = 12/01/16 Pct Recovery = 104% Analysis Date = 12/01/16 Pct Recovery = 104% Analysis Date = 11/29/16 Pct Recovery = 104% Analysis Date = 11/29/16 Pct Recovery = 104% Analysis Date = 11/26/16 Pct Recovery = 104% Analysis Date = 11/26/16 Pct Recovery = 104% Analysis Date = 11/24/16 Pct Recovery = 104% Analysis Date = 11/24/16 Pct Recovery = 104% Analysis Date = 11/22/16 Pct Recovery = 104% Analysis Date = 11/22/16 Pct Recovery = 104% Analysis Date = 11/20/16 Pct Recovery = 105% Analysis Date = 11/20/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 105% Analysis Date = 11/15/16 Pct Recovery = 105% Analysis Date = 11/15/16 Pct Recovery = 105% Analysis Date = 11/13/16 Pct Recovery = 105% Analysis Date = 11/13/16 Pct Recovery = 105% Analysis Date = 11/11/16 Pct Recovery = 105% Analysis Date = 11/11/16 Pct Recovery = 105% Analysis Date = 11/08/16 Pct Recovery = 105% Analysis Date = 11/08/16 Pct Recovery = 105% Analysis Date = 11/06/16 Pct Recovery = 105% Analysis Date = 11/06/16 Pct Recovery = 105% Analysis Date = 11/04/16 Pct Recovery = 105% Analysis Date = 11/04/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 105% Analysis Date = 11/02/16 Pct Recovery = 105% Analysis Date = 10/30/16 Pct Recovery = 105% Analysis Date = 10/30/16 Pct Recovery = 105% Analysis Date = 10/28/16 Pct Recovery = 105% Analysis Date = 10/28/16 Pct Recovery = 105% Analysis Date = 10/26/16 Pct Recovery = 106% Analysis Date = 10/26/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/24/16 Pct Recovery = 106% Analysis Date = 10/21/16 Pct Recovery = 106% Analysis Date = 10/21/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 106% Analysis Date = 10/19/16 Pct Recovery = 106% Analysis Date = 10/17/16 Pct Recovery = 106% Analysis Date = 10/17/16 Pct Recovery = 106% Analysis Date = 10/15/16 Pct Recovery = 106% Analysis Date = 10/15/16 Pct Recovery = 106% Analysis Date = 10/12/16 Pct Recovery = 106% Analysis Date = 10/12/16 Pct Recovery = 106% Analysis Date = 10/10/16 Pct Recovery = 106% Analysis Date = 10/10/16 Pct Recovery = 106% Analysis Date = 10/08/16 Pct Recovery = 106% Analysis Date = 10/08/16 Pct Recovery = 106% Analysis Date = 10/06/16 Pct Recovery = 106% Analysis Date = 10/06/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 106% Analysis Date = 10/01/16 Pct Recovery = 107% Analysis Date = 10/01/16 Pct Recovery = 107% Analysis Date = 09/29/16 Pct Recovery = 107% Analysis Date = 09/29/16 Pct Recovery = 107% Analysis Date = 09/27/16 Pct Recovery = 107% Analysis Date = 09/27/16 Pct Recovery = 107% Analysis Date = 09/24/16 Pct Recovery = 107% Analysis Date = 09/24/16 Pct Recovery = 107% Analysis Date = 09/22/16 Pct Recovery = 107% Analysis Date = 09/22/16 Pct Recovery = 107% Analysis Date = 09/20/16 Pct Recovery = 107% Analysis Date = 09/20/16 Pct Recovery = 107% Analysis Date = 09/18/16 Pct Recovery = 107% Analysis Date = 09/18/16 Pct Recovery = 107% Analysis Date = 09/16/16 Pct Recovery = 107% Analysis Date = 09/16/16 Pct Recovery = 107% Analysis Date = 09/13/16 Pct Recovery = 107% Analysis Date = 09/13/16 Pct Recovery = 107% Analysis Date = 09/11/16 Pct Recovery = 108% Analysis Date = 09/11/16 Pct Recovery = 108% Analysis Date = 09/09/16 Pct Recovery = 108% Analysis Date = 09/09/16 Pct Recovery = 108% Analysis Date = 09/07/16 Pct Recovery = 108% Analysis Date = 09/07/16 Pct Recovery = 108% Analysis Date = 09/04/16 Pct Recovery = 109% Analysis Date = 09/04/16 Pct Recovery = 109% Analysis Date = 09/02/16 Pct Recovery = 109% Analysis Date = 09/02/16 Pct Recovery = 109% Analysis Date = 08/31/16 Pct Recovery = 109% Analysis Date = 08/31/16 Pct Recovery = 109% Analysis Date = 08/29/16 Pct Recovery = 110% Analysis Date = 08/29/16 Pct Recovery = 110% Analysis Date = 08/26/16 Pct Recovery = 110% Analysis Date = 08/26/16 Pct Recovery = 110% Analysis Date = 08/24/16 Pct Recovery = 110% Analysis Date = 08/24/16 Pct Recovery = 110% Analysis Date = 08/22/16 Pct Recovery = 110% Analysis Date = 08/22/16 Pct Recovery = 110% Analysis Date = 08/20/16 Pct Recovery = 111% Analysis Date = 08/20/16 Pct Recovery = 111% Analysis Date = 08/17/16 Pct Recovery = 111% Analysis Date = 08/17/16 Pct Recovery = 111% Analysis Date = 08/15/16 Pct Recovery = 111% Analysis Date = 08/15/16 Pct Recovery = 111% Analysis Date = 08/13/16 Pct Recovery = 111% Analysis Date = 08/13/16 Pct Recovery = 111% Analysis Date = 08/11/16 Pct Recovery = 111% Analysis Date = 08/11/16 Pct Recovery = 111% Analysis Date = 08/08/16 Pct Recovery = 112% Analysis Date = 08/08/16 Pct Recovery = 112% Analysis Date = 08/06/16 Pct Recovery = 112% Analysis Date = 08/06/16 Pct Recovery = 112% Analysis Date = 08/04/16 Pct Recovery = 112% Analysis Date = 08/04/16 Pct Recovery = 112% Analysis Date = 08/02/16 Pct Recovery = 112% Analysis Date = 08/02/16 Pct Recovery = 112% Analysis Date = 07/30/16 Pct Recovery = 112% Analysis Date = 07/30/16 Pct Recovery = 112% Analysis Date = 07/28/16 Pct Recovery = 113% Analysis Date = 07/28/16 Pct Recovery = 113% Analysis Date = 07/26/16 Pct Recovery = 113% Analysis Date = 07/26/16 Pct Recovery = 113% Analysis Date = 07/24/16 Pct Recovery = 113% Analysis Date = 07/24/16 Pct Recovery = 113% Analysis Date = 07/21/16 Pct Recovery = 113% Analysis Date = 07/21/16 Pct Recovery = 113% Analysis Date = 07/19/16 Pct Recovery = 113% Analysis Date = 07/19/16 Pct Recovery = 113% Analysis Date = 07/17/16 Pct Recovery = 114% Analysis Date = 07/17/16 Pct Recovery = 114% Analysis Date = 07/15/16 Pct Recovery = 114% Analysis Date = 07/15/16 Pct Recovery = 114% Analysis Date = 07/12/16 Pct Recovery = 114% Analysis Date = 07/12/16 Pct Recovery = 114% Analysis Date = 07/10/16 Pct Recovery = 114% Analysis Date = 07/10/16 Pct Recovery = 114% Analysis Date = 07/08/16 Pct Recovery = 114% Analysis Date = 07/08/16 Pct Recovery = 114% Analysis Date = 07/06/16 Pct Recovery = 115% Analysis Date = 07/06/16 Pct Recovery = 115% Analysis Date = 07/03/16 Pct Recovery = 115% Analysis Date = 07/03/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 07/01/16 Pct Recovery = 115% Analysis Date = 06/29/16 Pct Recovery = 115% Analysis Date = 06/29/16 Pct Recovery = 115% Analysis Date = 06/27/16 Pct Recovery = 115% Analysis Date = 06/27/16 Pct Recovery = 115% Analysis Date = 06/24/16 Pct Recovery = 116% Analysis Date = 06/24/16 Pct Recovery = 116% Analysis Date = 06/22/16 Pct Recovery = 116% Analysis Date = 06/22/16 Pct Recovery = 116% Analysis Date = 06/20/16 Pct Recovery = 116% Analysis Date = 06/20/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/18/16 Pct Recovery = 116% Analysis Date = 06/15/16 Pct Recovery = 116% Analysis Date = 06/15/16 Pct Recovery = 116% Analysis Date = 06/13/16 Pct Recovery = 117% Analysis Date = 06/13/16 Pct Recovery = 117% Analysis Date = 06/11/16 Pct Recovery = 117% Analysis Date = 06/11/16 Pct Recovery = 117% Analysis Date = 06/09/16 Pct Recovery = 117% Analysis Date = 06/09/16 Pct Recovery = 117% Analysis Date = 06/06/16 Pct Recovery = 117% Analysis Date = 06/06/16 Pct Recovery = 117% Analysis Date = 06/04/16 Pct Recovery = 117% Analysis Date = 06/04/16 Pct Recovery = 117% Analysis Date = 06/02/16 Pct Recovery = 118% Analysis Date = 06/02/16 Pct Recovery = 118% Analysis Date = 05/31/16 Pct Recovery = 118% Analysis Date = 05/31/16 Pct Recovery = 118% Analysis Date = 05/29/16 Pct Recovery = 118% Analysis Date = 05/29/16 Pct Recovery = 118% Analysis Date = 05/26/16 Pct Recovery = 118% Analysis Date = 05/26/16 Pct Recovery = 118% Analysis Date = 05/24/16 Pct Recovery = 118% Analysis Date = 05/24/16 Pct Recovery = 118% Analysis Date = 05/22/16 Pct Recovery = 118% Analysis Date = 05/22/16 Pct Recovery = 118% Analysis Date = 05/20/16 Pct Recovery = 119% Analysis Date = 05/20/16 Pct Recovery = 119% Analysis Date = 05/17/16 Pct Recovery = 119% Analysis Date = 05/17/16 Pct Recovery = 119% Analysis Date = 05/15/16 Pct Recovery = 119% Analysis Date = 05/15/16 Pct Recovery = 119% Analysis Date = 05/13/16 Pct Recovery = 119% Analysis Date = 05/13/16 Pct Recovery = 119% Analysis Date = 05/11/16 Pct Recovery = 119% Analysis Date = 05/11/16 Pct Recovery = 119% Analysis Date = 05/08/16 Pct Recovery = 119% Analysis Date = 05/08/16 Pct Recovery = 119% Analysis Date = 05/06/16 Pct Recovery = 119% Analysis Date = 05/06/16 Pct Recovery = 119% Analysis Date = 05/04/16 Pct Recovery = 119% Analysis Date = 05/04/16 Pct Recovery = 119% Analysis Date = 05/02/16 Pct Recovery = 120% Analysis Date = 05/02/16 Pct Recovery = 120% Analysis Date = 04/29/16 Pct Recovery = 120% Analysis Date = 04/29/16 Pct Recovery = 120% Analysis Date = 04/27/16 Pct Recovery = 120% Analysis Date = 04/27/16 Pct Recovery = 120% Analysis Date = 04/25/16 Pct Recovery = 120% Analysis Date = 04/25/16 Pct Recovery = 120% Analysis Date = 04/23/16 Pct Recovery = 120% Analysis Date = 04/23/16 Pct Recovery = 120% Analysis Date = 04/20/16 Pct Recovery = 120% Analysis Date = 04/20/16 Pct Recovery = 120% Analysis Date = 04/18/16 Pct Recovery = 120% Analysis Date = 04/18/16 Pct Recovery = 120% Analysis Date = 04/16/16 Pct Recovery = 120% Analysis Date = 04/16/16 Pct Recovery = 120% Analysis Date = 04/14/16 Pct Recovery = 121% Analysis Date = 04/14/16 Pct Recovery = 121% Analysis Date = 04/11/16 Pct Recovery = 121% Analysis Date = 04/11/16 Pct Recovery = 121% Analysis Date = 04/09/16 Pct Recovery = 121% Analysis Date = 04/09/16 Pct Recovery = 121% Analysis Date = 04/07/16 Pct Recovery = 121% Analysis Date = 04/07/16 Pct Recovery = 121% Analysis Date = 04/05/16 Pct Recovery = 121% Analysis Date = 04/05/16 Pct Recovery = 121% Analysis Date = 04/02/16 Pct Recovery = 121% Analysis Date = 04/02/16 Pct Recovery = 121% Analysis Date = 03/31/16 Pct Recovery = 121% Analysis Date = 03/31/16 Pct Recovery = 121% Analysis Date = 03/29/16 Pct Recovery = 121% Analysis Date = 03/29/16 Pct Recovery = 121% Analysis Date = 03/27/16 Pct Recovery = 121% Analysis Date = 03/27/16 Pct Recovery = 121% Analysis Date = 03/24/16 Pct Recovery = 121% Analysis Date = 03/24/16 Pct Recovery = 121% Analysis Date = 03/22/16 Pct Recovery = 122% Analysis Date = 03/22/16 Pct Recovery = 122% Analysis Date = 03/20/16 Pct Recovery = 122% Analysis Date = 03/20/16 Pct Recovery = 122% Analysis Date = 03/18/16 Pct Recovery = 122% Analysis Date = 03/18/16 Pct Recovery = 122% Analysis Date = 03/15/16 Pct Recovery = 122% Analysis Date = 03/15/16 Pct Recovery = 122% Analysis Date = 03/13/16 Pct Recovery = 122% Analysis Date = 03/13/16 Pct Recovery = 122% Analysis Date = 03/11/16 Pct Recovery = 122% Analysis Date = 03/11/16 Pct Recovery = 122% Analysis Date = 03/09/16 Pct Recovery = 122% Analysis Date = 03/09/16 Pct Recovery = 122% Analysis Date = 03/06/16 Pct Recovery = 122% Analysis Date = 03/06/16 Pct Recovery = 122% Analysis Date = 03/04/16 Pct Recovery = 122% Analysis Date = 03/04/16 Pct Recovery = 122% Analysis Date = 03/02/16 Pct Recovery = 122% Analysis Date = 03/02/16 Pct Recovery = 122% Analysis Date = 02/29/16 Pct Recovery = 122% Analysis Date = 02/29/16 Pct Recovery = 122% Analysis Date = 02/26/16 Pct Recovery = 122% Analysis Date = 02/26/16 Pct Recovery = 122% Analysis Date = 02/24/16 Pct Recovery = 123% Analysis Date = 02/24/16 Pct Recovery = 123% Analysis Date = 02/22/16 Pct Recovery = 123% Analysis Date = 02/22/16 Pct Recovery = 123% Analysis Date = 02/20/16 Pct Recovery = 123% Analysis Date = 02/20/16 Pct Recovery = 123% Analysis Date = 02/17/16 Pct Recovery = 123% Analysis Date = 02/17/16 Pct Recovery = 123% Analysis Date = 02/15/16 Pct Recovery = 123% Analysis Date = 02/15/16 Pct Recovery = 123% Analysis Date = 02/13/16 Pct Recovery = 123% Analysis Date = 02/13/16 Pct Recovery = 123% Analysis Date = 02/11/16 Pct Recovery = 123% Analysis Date = 02/11/16 Pct Recovery = 123% Analysis Date = 02/09/16 Pct Recovery = 123% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 17 110% 14% 108% 17%
Total 17 110% 14% 108% 17%

Sample Statistics
FIPRONIL

Characteristic N % % Basis
Plotted 17 94% Spiked
Estimated Values 17 94% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 1 6% 1 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
FIPRONIL SULFIDE
METHOD: 2033 , TESTIDCODE: 62167GCM29

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 75% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 94% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 86% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 103% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 80% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 73% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 87% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 89% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 113% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 89% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 85% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 84% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 94% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 102% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 110% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 97% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 104% Analysis Date = 05/10/17 Pct Recovery = 85% Analysis Date = 05/08/17 Pct Recovery = 85% Analysis Date = 05/08/17 Pct Recovery = 85% Analysis Date = 05/06/17 Pct Recovery = 86% Analysis Date = 05/06/17 Pct Recovery = 86% Analysis Date = 05/04/17 Pct Recovery = 86% Analysis Date = 05/04/17 Pct Recovery = 86% Analysis Date = 05/01/17 Pct Recovery = 86% Analysis Date = 05/01/17 Pct Recovery = 86% Analysis Date = 04/29/17 Pct Recovery = 86% Analysis Date = 04/29/17 Pct Recovery = 86% Analysis Date = 04/27/17 Pct Recovery = 86% Analysis Date = 04/27/17 Pct Recovery = 86% Analysis Date = 04/25/17 Pct Recovery = 86% Analysis Date = 04/25/17 Pct Recovery = 86% Analysis Date = 04/22/17 Pct Recovery = 86% Analysis Date = 04/22/17 Pct Recovery = 86% Analysis Date = 04/20/17 Pct Recovery = 87% Analysis Date = 04/20/17 Pct Recovery = 87% Analysis Date = 04/18/17 Pct Recovery = 87% Analysis Date = 04/18/17 Pct Recovery = 87% Analysis Date = 04/15/17 Pct Recovery = 87% Analysis Date = 04/15/17 Pct Recovery = 87% Analysis Date = 04/13/17 Pct Recovery = 87% Analysis Date = 04/13/17 Pct Recovery = 87% Analysis Date = 04/11/17 Pct Recovery = 87% Analysis Date = 04/11/17 Pct Recovery = 87% Analysis Date = 04/09/17 Pct Recovery = 87% Analysis Date = 04/09/17 Pct Recovery = 87% Analysis Date = 04/06/17 Pct Recovery = 87% Analysis Date = 04/06/17 Pct Recovery = 87% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/02/17 Pct Recovery = 88% Analysis Date = 04/02/17 Pct Recovery = 88% Analysis Date = 03/30/17 Pct Recovery = 88% Analysis Date = 03/30/17 Pct Recovery = 88% Analysis Date = 03/28/17 Pct Recovery = 88% Analysis Date = 03/28/17 Pct Recovery = 88% Analysis Date = 03/26/17 Pct Recovery = 88% Analysis Date = 03/26/17 Pct Recovery = 88% Analysis Date = 03/24/17 Pct Recovery = 88% Analysis Date = 03/24/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 88% Analysis Date = 03/21/17 Pct Recovery = 88% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 89% Analysis Date = 03/10/17 Pct Recovery = 89% Analysis Date = 03/10/17 Pct Recovery = 89% Analysis Date = 03/08/17 Pct Recovery = 89% Analysis Date = 03/08/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 90% Analysis Date = 02/08/17 Pct Recovery = 90% Analysis Date = 02/08/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/01/17 Pct Recovery = 89% Analysis Date = 02/01/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/23/17 Pct Recovery = 89% Analysis Date = 01/23/17 Pct Recovery = 89% Analysis Date = 01/21/17 Pct Recovery = 89% Analysis Date = 01/21/17 Pct Recovery = 89% Analysis Date = 01/19/17 Pct Recovery = 89% Analysis Date = 01/19/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/12/17 Pct Recovery = 89% Analysis Date = 01/12/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 89% Analysis Date = 01/03/17 Pct Recovery = 89% Analysis Date = 01/03/17 Pct Recovery = 89% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 11/29/16 Pct Recovery = 91% Analysis Date = 11/29/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 92% Analysis Date = 11/09/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/08/16 Pct Recovery = 93% Analysis Date = 10/08/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/03/16 Pct Recovery = 93% Analysis Date = 10/03/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/03/16 Pct Recovery = 94% Analysis Date = 09/03/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/30/16 Pct Recovery = 94% Analysis Date = 08/30/16 Pct Recovery = 94% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/25/16 Pct Recovery = 93% Analysis Date = 08/25/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 94% Analysis Date = 08/23/16 Pct Recovery = 94% Analysis Date = 08/21/16 Pct Recovery = 94% Analysis Date = 08/21/16 Pct Recovery = 94% Analysis Date = 08/18/16 Pct Recovery = 94% Analysis Date = 08/18/16 Pct Recovery = 94% Analysis Date = 08/16/16 Pct Recovery = 94% Analysis Date = 08/16/16 Pct Recovery = 94% Analysis Date = 08/14/16 Pct Recovery = 94% Analysis Date = 08/14/16 Pct Recovery = 94% Analysis Date = 08/12/16 Pct Recovery = 94% Analysis Date = 08/12/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/07/16 Pct Recovery = 94% Analysis Date = 08/07/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 07/31/16 Pct Recovery = 94% Analysis Date = 07/31/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 94% Analysis Date = 07/29/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/24/16 Pct Recovery = 94% Analysis Date = 07/22/16 Pct Recovery = 94% Analysis Date = 07/22/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/17/16 Pct Recovery = 94% Analysis Date = 07/17/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/13/16 Pct Recovery = 95% Analysis Date = 07/13/16 Pct Recovery = 95% Analysis Date = 07/11/16 Pct Recovery = 95% Analysis Date = 07/11/16 Pct Recovery = 95% Analysis Date = 07/08/16 Pct Recovery = 95% Analysis Date = 07/08/16 Pct Recovery = 95% Analysis Date = 07/06/16 Pct Recovery = 95% Analysis Date = 07/06/16 Pct Recovery = 95% Analysis Date = 07/04/16 Pct Recovery = 95% Analysis Date = 07/04/16 Pct Recovery = 95% Analysis Date = 07/01/16 Pct Recovery = 95% Analysis Date = 07/01/16 Pct Recovery = 95% Analysis Date = 06/29/16 Pct Recovery = 95% Analysis Date = 06/29/16 Pct Recovery = 95% Analysis Date = 06/27/16 Pct Recovery = 95% Analysis Date = 06/27/16 Pct Recovery = 95% Analysis Date = 06/25/16 Pct Recovery = 95% Analysis Date = 06/25/16 Pct Recovery = 95% Analysis Date = 06/22/16 Pct Recovery = 95% Analysis Date = 06/22/16 Pct Recovery = 95% Analysis Date = 06/20/16 Pct Recovery = 95% Analysis Date = 06/20/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/18/16 Pct Recovery = 95% Analysis Date = 06/15/16 Pct Recovery = 95% Analysis Date = 06/15/16 Pct Recovery = 95% Analysis Date = 06/13/16 Pct Recovery = 95% Analysis Date = 06/13/16 Pct Recovery = 95% Analysis Date = 06/11/16 Pct Recovery = 95% Analysis Date = 06/11/16 Pct Recovery = 95% Analysis Date = 06/09/16 Pct Recovery = 96% Analysis Date = 06/09/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 96% Analysis Date = 06/02/16 Pct Recovery = 96% Analysis Date = 06/02/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/26/16 Pct Recovery = 96% Analysis Date = 05/26/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/21/16 Pct Recovery = 96% Analysis Date = 05/21/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/17/16 Pct Recovery = 96% Analysis Date = 05/17/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/14/16 Pct Recovery = 96% Analysis Date = 05/12/16 Pct Recovery = 96% Analysis Date = 05/12/16 Pct Recovery = 96% Analysis Date = 05/10/16 Pct Recovery = 96% Analysis Date = 05/10/16 Pct Recovery = 96% Analysis Date = 05/08/16 Pct Recovery = 96% Analysis Date = 05/08/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/05/16 Pct Recovery = 96% Analysis Date = 05/03/16 Pct Recovery = 97% Analysis Date = 05/03/16 Pct Recovery = 97% Analysis Date = 05/01/16 Pct Recovery = 97% Analysis Date = 05/01/16 Pct Recovery = 97% Analysis Date = 04/28/16 Pct Recovery = 97% Analysis Date = 04/28/16 Pct Recovery = 97% Analysis Date = 04/26/16 Pct Recovery = 97% Analysis Date = 04/26/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/24/16 Pct Recovery = 97% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/19/16 Pct Recovery = 98% Analysis Date = 04/19/16 Pct Recovery = 98% Analysis Date = 04/17/16 Pct Recovery = 98% Analysis Date = 04/17/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/15/16 Pct Recovery = 98% Analysis Date = 04/12/16 Pct Recovery = 98% Analysis Date = 04/12/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 99% Analysis Date = 04/10/16 Pct Recovery = 99% Analysis Date = 04/08/16 Pct Recovery = 99% Analysis Date = 04/08/16 Pct Recovery = 99% Analysis Date = 04/06/16 Pct Recovery = 99% Analysis Date = 04/06/16 Pct Recovery = 99% Analysis Date = 04/03/16 Pct Recovery = 99% Analysis Date = 04/03/16 Pct Recovery = 99% Analysis Date = 04/01/16 Pct Recovery = 99% Analysis Date = 04/01/16 Pct Recovery = 99% Analysis Date = 03/30/16 Pct Recovery = 100% Analysis Date = 03/30/16 Pct Recovery = 100% Analysis Date = 03/27/16 Pct Recovery = 100% Analysis Date = 03/27/16 Pct Recovery = 100% Analysis Date = 03/25/16 Pct Recovery = 100% Analysis Date = 03/25/16 Pct Recovery = 100% Analysis Date = 03/23/16 Pct Recovery = 100% Analysis Date = 03/23/16 Pct Recovery = 100% Analysis Date = 03/21/16 Pct Recovery = 101% Analysis Date = 03/21/16 Pct Recovery = 101% Analysis Date = 03/18/16 Pct Recovery = 101% Analysis Date = 03/18/16 Pct Recovery = 101% Analysis Date = 03/16/16 Pct Recovery = 101% Analysis Date = 03/16/16 Pct Recovery = 101% Analysis Date = 03/14/16 Pct Recovery = 101% Analysis Date = 03/14/16 Pct Recovery = 101% Analysis Date = 03/11/16 Pct Recovery = 102% Analysis Date = 03/11/16 Pct Recovery = 102% Analysis Date = 03/09/16 Pct Recovery = 102% Analysis Date = 03/09/16 Pct Recovery = 102% Analysis Date = 03/07/16 Pct Recovery = 102% Analysis Date = 03/07/16 Pct Recovery = 102% Analysis Date = 03/05/16 Pct Recovery = 102% Analysis Date = 03/05/16 Pct Recovery = 102% Analysis Date = 03/02/16 Pct Recovery = 103% Analysis Date = 03/02/16 Pct Recovery = 103% Analysis Date = 02/29/16 Pct Recovery = 103% Analysis Date = 02/29/16 Pct Recovery = 103% Analysis Date = 02/27/16 Pct Recovery = 103% Analysis Date = 02/27/16 Pct Recovery = 103% Analysis Date = 02/24/16 Pct Recovery = 103% Analysis Date = 02/24/16 Pct Recovery = 103% Analysis Date = 02/22/16 Pct Recovery = 103% Analysis Date = 02/22/16 Pct Recovery = 103% Analysis Date = 02/20/16 Pct Recovery = 104% Analysis Date = 02/20/16 Pct Recovery = 104% Analysis Date = 02/18/16 Pct Recovery = 104% Analysis Date = 02/18/16 Pct Recovery = 104% Analysis Date = 02/15/16 Pct Recovery = 104% Analysis Date = 02/15/16 Pct Recovery = 104% Analysis Date = 02/13/16 Pct Recovery = 104% Analysis Date = 02/13/16 Pct Recovery = 104% Analysis Date = 02/11/16 Pct Recovery = 105% Analysis Date = 02/11/16 Pct Recovery = 105% Analysis Date = 02/09/16 Pct Recovery = 105% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 93% 12% 92% 13%
Total 19 93% 12% 92% 13%

Sample Statistics
FIPRONIL SULFIDE

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 2 22% 2 out of 9

OBSP Determination:
FIPRONIL SULFONE
METHOD: 2033 , TESTIDCODE: 62168GCM29

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 82% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 95% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 74% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 75% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 92% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 78% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 78% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 103% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 122% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 102% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 89% Analysis Date = 05/10/17 Pct Recovery = 83% Analysis Date = 05/08/17 Pct Recovery = 83% Analysis Date = 05/08/17 Pct Recovery = 83% Analysis Date = 05/06/17 Pct Recovery = 83% Analysis Date = 05/06/17 Pct Recovery = 83% Analysis Date = 05/04/17 Pct Recovery = 84% Analysis Date = 05/04/17 Pct Recovery = 84% Analysis Date = 05/02/17 Pct Recovery = 84% Analysis Date = 05/02/17 Pct Recovery = 84% Analysis Date = 04/30/17 Pct Recovery = 84% Analysis Date = 04/30/17 Pct Recovery = 84% Analysis Date = 04/27/17 Pct Recovery = 84% Analysis Date = 04/27/17 Pct Recovery = 84% Analysis Date = 04/25/17 Pct Recovery = 84% Analysis Date = 04/25/17 Pct Recovery = 84% Analysis Date = 04/23/17 Pct Recovery = 84% Analysis Date = 04/23/17 Pct Recovery = 84% Analysis Date = 04/21/17 Pct Recovery = 84% Analysis Date = 04/21/17 Pct Recovery = 84% Analysis Date = 04/19/17 Pct Recovery = 84% Analysis Date = 04/19/17 Pct Recovery = 84% Analysis Date = 04/17/17 Pct Recovery = 84% Analysis Date = 04/17/17 Pct Recovery = 84% Analysis Date = 04/14/17 Pct Recovery = 84% Analysis Date = 04/14/17 Pct Recovery = 84% Analysis Date = 04/12/17 Pct Recovery = 84% Analysis Date = 04/12/17 Pct Recovery = 84% Analysis Date = 04/10/17 Pct Recovery = 84% Analysis Date = 04/10/17 Pct Recovery = 84% Analysis Date = 04/08/17 Pct Recovery = 84% Analysis Date = 04/08/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/04/17 Pct Recovery = 83% Analysis Date = 04/04/17 Pct Recovery = 83% Analysis Date = 04/01/17 Pct Recovery = 83% Analysis Date = 04/01/17 Pct Recovery = 83% Analysis Date = 03/30/17 Pct Recovery = 83% Analysis Date = 03/30/17 Pct Recovery = 83% Analysis Date = 03/28/17 Pct Recovery = 83% Analysis Date = 03/28/17 Pct Recovery = 83% Analysis Date = 03/26/17 Pct Recovery = 83% Analysis Date = 03/26/17 Pct Recovery = 83% Analysis Date = 03/24/17 Pct Recovery = 83% Analysis Date = 03/24/17 Pct Recovery = 83% Analysis Date = 03/21/17 Pct Recovery = 83% Analysis Date = 03/21/17 Pct Recovery = 83% Analysis Date = 03/19/17 Pct Recovery = 83% Analysis Date = 03/19/17 Pct Recovery = 83% Analysis Date = 03/17/17 Pct Recovery = 83% Analysis Date = 03/17/17 Pct Recovery = 83% Analysis Date = 03/15/17 Pct Recovery = 83% Analysis Date = 03/15/17 Pct Recovery = 83% Analysis Date = 03/13/17 Pct Recovery = 83% Analysis Date = 03/13/17 Pct Recovery = 83% Analysis Date = 03/11/17 Pct Recovery = 83% Analysis Date = 03/11/17 Pct Recovery = 83% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/06/17 Pct Recovery = 83% Analysis Date = 03/06/17 Pct Recovery = 83% Analysis Date = 03/04/17 Pct Recovery = 83% Analysis Date = 03/04/17 Pct Recovery = 83% Analysis Date = 03/02/17 Pct Recovery = 83% Analysis Date = 03/02/17 Pct Recovery = 83% Analysis Date = 02/28/17 Pct Recovery = 83% Analysis Date = 02/28/17 Pct Recovery = 83% Analysis Date = 02/26/17 Pct Recovery = 83% Analysis Date = 02/26/17 Pct Recovery = 83% Analysis Date = 02/23/17 Pct Recovery = 83% Analysis Date = 02/23/17 Pct Recovery = 83% Analysis Date = 02/21/17 Pct Recovery = 83% Analysis Date = 02/21/17 Pct Recovery = 83% Analysis Date = 02/19/17 Pct Recovery = 83% Analysis Date = 02/19/17 Pct Recovery = 83% Analysis Date = 02/17/17 Pct Recovery = 83% Analysis Date = 02/17/17 Pct Recovery = 83% Analysis Date = 02/15/17 Pct Recovery = 83% Analysis Date = 02/15/17 Pct Recovery = 83% Analysis Date = 02/12/17 Pct Recovery = 83% Analysis Date = 02/12/17 Pct Recovery = 83% Analysis Date = 02/10/17 Pct Recovery = 83% Analysis Date = 02/10/17 Pct Recovery = 83% Analysis Date = 02/08/17 Pct Recovery = 83% Analysis Date = 02/08/17 Pct Recovery = 83% Analysis Date = 02/06/17 Pct Recovery = 82% Analysis Date = 02/06/17 Pct Recovery = 82% Analysis Date = 02/04/17 Pct Recovery = 82% Analysis Date = 02/04/17 Pct Recovery = 82% Analysis Date = 02/02/17 Pct Recovery = 82% Analysis Date = 02/02/17 Pct Recovery = 82% Analysis Date = 01/30/17 Pct Recovery = 82% Analysis Date = 01/30/17 Pct Recovery = 82% Analysis Date = 01/28/17 Pct Recovery = 82% Analysis Date = 01/28/17 Pct Recovery = 82% Analysis Date = 01/26/17 Pct Recovery = 82% Analysis Date = 01/26/17 Pct Recovery = 82% Analysis Date = 01/24/17 Pct Recovery = 81% Analysis Date = 01/24/17 Pct Recovery = 81% Analysis Date = 01/22/17 Pct Recovery = 81% Analysis Date = 01/22/17 Pct Recovery = 81% Analysis Date = 01/20/17 Pct Recovery = 81% Analysis Date = 01/20/17 Pct Recovery = 81% Analysis Date = 01/17/17 Pct Recovery = 81% Analysis Date = 01/17/17 Pct Recovery = 81% Analysis Date = 01/15/17 Pct Recovery = 81% Analysis Date = 01/15/17 Pct Recovery = 81% Analysis Date = 01/13/17 Pct Recovery = 81% Analysis Date = 01/13/17 Pct Recovery = 81% Analysis Date = 01/11/17 Pct Recovery = 81% Analysis Date = 01/11/17 Pct Recovery = 81% Analysis Date = 01/09/17 Pct Recovery = 81% Analysis Date = 01/09/17 Pct Recovery = 81% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 01/07/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/04/17 Pct Recovery = 82% Analysis Date = 01/02/17 Pct Recovery = 82% Analysis Date = 01/02/17 Pct Recovery = 82% Analysis Date = 12/31/16 Pct Recovery = 82% Analysis Date = 12/31/16 Pct Recovery = 82% Analysis Date = 12/29/16 Pct Recovery = 82% Analysis Date = 12/29/16 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/27/16 Pct Recovery = 82% Analysis Date = 12/24/16 Pct Recovery = 82% Analysis Date = 12/24/16 Pct Recovery = 82% Analysis Date = 12/22/16 Pct Recovery = 82% Analysis Date = 12/22/16 Pct Recovery = 82% Analysis Date = 12/20/16 Pct Recovery = 83% Analysis Date = 12/20/16 Pct Recovery = 83% Analysis Date = 12/18/16 Pct Recovery = 83% Analysis Date = 12/18/16 Pct Recovery = 83% Analysis Date = 12/16/16 Pct Recovery = 83% Analysis Date = 12/16/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 84% Analysis Date = 12/09/16 Pct Recovery = 84% Analysis Date = 12/07/16 Pct Recovery = 84% Analysis Date = 12/07/16 Pct Recovery = 84% Analysis Date = 12/05/16 Pct Recovery = 84% Analysis Date = 12/05/16 Pct Recovery = 84% Analysis Date = 12/03/16 Pct Recovery = 85% Analysis Date = 12/03/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 12/01/16 Pct Recovery = 85% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/28/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/26/16 Pct Recovery = 85% Analysis Date = 11/24/16 Pct Recovery = 86% Analysis Date = 11/24/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/20/16 Pct Recovery = 86% Analysis Date = 11/20/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/15/16 Pct Recovery = 87% Analysis Date = 11/15/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/11/16 Pct Recovery = 87% Analysis Date = 11/11/16 Pct Recovery = 87% Analysis Date = 11/09/16 Pct Recovery = 87% Analysis Date = 11/09/16 Pct Recovery = 87% Analysis Date = 11/07/16 Pct Recovery = 88% Analysis Date = 11/07/16 Pct Recovery = 88% Analysis Date = 11/04/16 Pct Recovery = 88% Analysis Date = 11/04/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/29/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/27/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 89% Analysis Date = 10/25/16 Pct Recovery = 89% Analysis Date = 10/22/16 Pct Recovery = 89% Analysis Date = 10/22/16 Pct Recovery = 89% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/20/16 Pct Recovery = 90% Analysis Date = 10/18/16 Pct Recovery = 90% Analysis Date = 10/18/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 90% Analysis Date = 10/16/16 Pct Recovery = 90% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/14/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/12/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/09/16 Pct Recovery = 91% Analysis Date = 10/07/16 Pct Recovery = 91% Analysis Date = 10/07/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 10/05/16 Pct Recovery = 92% Analysis Date = 10/03/16 Pct Recovery = 92% Analysis Date = 10/03/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 10/01/16 Pct Recovery = 92% Analysis Date = 09/28/16 Pct Recovery = 92% Analysis Date = 09/28/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/18/16 Pct Recovery = 94% Analysis Date = 09/18/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/11/16 Pct Recovery = 95% Analysis Date = 09/11/16 Pct Recovery = 95% Analysis Date = 09/09/16 Pct Recovery = 95% Analysis Date = 09/09/16 Pct Recovery = 95% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/05/16 Pct Recovery = 96% Analysis Date = 09/05/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 08/31/16 Pct Recovery = 97% Analysis Date = 08/31/16 Pct Recovery = 97% Analysis Date = 08/29/16 Pct Recovery = 97% Analysis Date = 08/29/16 Pct Recovery = 97% Analysis Date = 08/27/16 Pct Recovery = 97% Analysis Date = 08/27/16 Pct Recovery = 97% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/22/16 Pct Recovery = 98% Analysis Date = 08/22/16 Pct Recovery = 98% Analysis Date = 08/20/16 Pct Recovery = 98% Analysis Date = 08/20/16 Pct Recovery = 98% Analysis Date = 08/18/16 Pct Recovery = 99% Analysis Date = 08/18/16 Pct Recovery = 99% Analysis Date = 08/16/16 Pct Recovery = 99% Analysis Date = 08/16/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/12/16 Pct Recovery = 99% Analysis Date = 08/12/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 99% Analysis Date = 08/07/16 Pct Recovery = 99% Analysis Date = 08/07/16 Pct Recovery = 99% Analysis Date = 08/05/16 Pct Recovery = 99% Analysis Date = 08/05/16 Pct Recovery = 99% Analysis Date = 08/03/16 Pct Recovery = 99% Analysis Date = 08/03/16 Pct Recovery = 99% Analysis Date = 08/01/16 Pct Recovery = 99% Analysis Date = 08/01/16 Pct Recovery = 99% Analysis Date = 07/30/16 Pct Recovery = 99% Analysis Date = 07/30/16 Pct Recovery = 99% Analysis Date = 07/27/16 Pct Recovery = 100% Analysis Date = 07/27/16 Pct Recovery = 100% Analysis Date = 07/25/16 Pct Recovery = 100% Analysis Date = 07/25/16 Pct Recovery = 100% Analysis Date = 07/23/16 Pct Recovery = 100% Analysis Date = 07/23/16 Pct Recovery = 100% Analysis Date = 07/21/16 Pct Recovery = 100% Analysis Date = 07/21/16 Pct Recovery = 100% Analysis Date = 07/19/16 Pct Recovery = 100% Analysis Date = 07/19/16 Pct Recovery = 100% Analysis Date = 07/17/16 Pct Recovery = 100% Analysis Date = 07/17/16 Pct Recovery = 100% Analysis Date = 07/14/16 Pct Recovery = 100% Analysis Date = 07/14/16 Pct Recovery = 100% Analysis Date = 07/12/16 Pct Recovery = 100% Analysis Date = 07/12/16 Pct Recovery = 100% Analysis Date = 07/10/16 Pct Recovery = 100% Analysis Date = 07/10/16 Pct Recovery = 100% Analysis Date = 07/08/16 Pct Recovery = 100% Analysis Date = 07/08/16 Pct Recovery = 100% Analysis Date = 07/06/16 Pct Recovery = 100% Analysis Date = 07/06/16 Pct Recovery = 100% Analysis Date = 07/03/16 Pct Recovery = 100% Analysis Date = 07/03/16 Pct Recovery = 100% Analysis Date = 07/01/16 Pct Recovery = 100% Analysis Date = 07/01/16 Pct Recovery = 100% Analysis Date = 06/29/16 Pct Recovery = 101% Analysis Date = 06/29/16 Pct Recovery = 101% Analysis Date = 06/27/16 Pct Recovery = 101% Analysis Date = 06/27/16 Pct Recovery = 101% Analysis Date = 06/25/16 Pct Recovery = 101% Analysis Date = 06/25/16 Pct Recovery = 101% Analysis Date = 06/23/16 Pct Recovery = 101% Analysis Date = 06/23/16 Pct Recovery = 101% Analysis Date = 06/20/16 Pct Recovery = 101% Analysis Date = 06/20/16 Pct Recovery = 101% Analysis Date = 06/18/16 Pct Recovery = 101% Analysis Date = 06/18/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/16/16 Pct Recovery = 101% Analysis Date = 06/14/16 Pct Recovery = 101% Analysis Date = 06/14/16 Pct Recovery = 101% Analysis Date = 06/12/16 Pct Recovery = 101% Analysis Date = 06/12/16 Pct Recovery = 101% Analysis Date = 06/10/16 Pct Recovery = 101% Analysis Date = 06/10/16 Pct Recovery = 101% Analysis Date = 06/07/16 Pct Recovery = 101% Analysis Date = 06/07/16 Pct Recovery = 101% Analysis Date = 06/05/16 Pct Recovery = 101% Analysis Date = 06/05/16 Pct Recovery = 101% Analysis Date = 06/03/16 Pct Recovery = 101% Analysis Date = 06/03/16 Pct Recovery = 101% Analysis Date = 06/01/16 Pct Recovery = 102% Analysis Date = 06/01/16 Pct Recovery = 102% Analysis Date = 05/30/16 Pct Recovery = 102% Analysis Date = 05/30/16 Pct Recovery = 102% Analysis Date = 05/27/16 Pct Recovery = 102% Analysis Date = 05/27/16 Pct Recovery = 102% Analysis Date = 05/25/16 Pct Recovery = 102% Analysis Date = 05/25/16 Pct Recovery = 102% Analysis Date = 05/23/16 Pct Recovery = 102% Analysis Date = 05/23/16 Pct Recovery = 102% Analysis Date = 05/21/16 Pct Recovery = 102% Analysis Date = 05/21/16 Pct Recovery = 102% Analysis Date = 05/19/16 Pct Recovery = 102% Analysis Date = 05/19/16 Pct Recovery = 102% Analysis Date = 05/17/16 Pct Recovery = 102% Analysis Date = 05/17/16 Pct Recovery = 102% Analysis Date = 05/14/16 Pct Recovery = 102% Analysis Date = 05/14/16 Pct Recovery = 102% Analysis Date = 05/12/16 Pct Recovery = 102% Analysis Date = 05/12/16 Pct Recovery = 102% Analysis Date = 05/10/16 Pct Recovery = 102% Analysis Date = 05/10/16 Pct Recovery = 102% Analysis Date = 05/08/16 Pct Recovery = 101% Analysis Date = 05/08/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/06/16 Pct Recovery = 101% Analysis Date = 05/04/16 Pct Recovery = 101% Analysis Date = 05/04/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 101% Analysis Date = 05/01/16 Pct Recovery = 101% Analysis Date = 04/29/16 Pct Recovery = 101% Analysis Date = 04/29/16 Pct Recovery = 101% Analysis Date = 04/27/16 Pct Recovery = 101% Analysis Date = 04/27/16 Pct Recovery = 101% Analysis Date = 04/25/16 Pct Recovery = 101% Analysis Date = 04/25/16 Pct Recovery = 101% Analysis Date = 04/23/16 Pct Recovery = 101% Analysis Date = 04/23/16 Pct Recovery = 101% Analysis Date = 04/21/16 Pct Recovery = 101% Analysis Date = 04/21/16 Pct Recovery = 101% Analysis Date = 04/18/16 Pct Recovery = 101% Analysis Date = 04/18/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/16/16 Pct Recovery = 101% Analysis Date = 04/14/16 Pct Recovery = 101% Analysis Date = 04/14/16 Pct Recovery = 101% Analysis Date = 04/12/16 Pct Recovery = 101% Analysis Date = 04/12/16 Pct Recovery = 101% Analysis Date = 04/10/16 Pct Recovery = 101% Analysis Date = 04/10/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/07/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 04/05/16 Pct Recovery = 101% Analysis Date = 04/03/16 Pct Recovery = 101% Analysis Date = 04/03/16 Pct Recovery = 101% Analysis Date = 04/01/16 Pct Recovery = 101% Analysis Date = 04/01/16 Pct Recovery = 101% Analysis Date = 03/30/16 Pct Recovery = 101% Analysis Date = 03/30/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 101% Analysis Date = 03/25/16 Pct Recovery = 101% Analysis Date = 03/25/16 Pct Recovery = 101% Analysis Date = 03/23/16 Pct Recovery = 101% Analysis Date = 03/23/16 Pct Recovery = 101% Analysis Date = 03/21/16 Pct Recovery = 101% Analysis Date = 03/21/16 Pct Recovery = 101% Analysis Date = 03/19/16 Pct Recovery = 101% Analysis Date = 03/19/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/15/16 Pct Recovery = 101% Analysis Date = 03/15/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/10/16 Pct Recovery = 101% Analysis Date = 03/10/16 Pct Recovery = 101% Analysis Date = 03/08/16 Pct Recovery = 100% Analysis Date = 03/08/16 Pct Recovery = 100% Analysis Date = 03/06/16 Pct Recovery = 100% Analysis Date = 03/06/16 Pct Recovery = 100% Analysis Date = 03/04/16 Pct Recovery = 100% Analysis Date = 03/04/16 Pct Recovery = 100% Analysis Date = 03/02/16 Pct Recovery = 100% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FIPRONIL SULFONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 16 92% 13% 92% 15%
Total 16 92% 13% 92% 15%

Sample Statistics
FIPRONIL SULFONE

Characteristic N % % Basis
Plotted 16 100% Spiked
Estimated Values 3 19% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 16 .  
False Negatives 0 0% 0 out of 16
Not Spiked 7 .  
False Positives 1 14% 1 out of 7

OBSP Determination:
FONOFOS
METHOD: 2033 , TESTIDCODE: 04095GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 98% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 108% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 76% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 103% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 56% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 83% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 76% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 97% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 105% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 101% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 77% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 82% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 69% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 84% Analysis Date = 05/02/17 Pct Recovery = 92% Analysis Date = 04/30/17 Pct Recovery = 92% Analysis Date = 04/30/17 Pct Recovery = 92% Analysis Date = 04/28/17 Pct Recovery = 92% Analysis Date = 04/28/17 Pct Recovery = 92% Analysis Date = 04/26/17 Pct Recovery = 93% Analysis Date = 04/26/17 Pct Recovery = 93% Analysis Date = 04/24/17 Pct Recovery = 93% Analysis Date = 04/24/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/20/17 Pct Recovery = 93% Analysis Date = 04/20/17 Pct Recovery = 93% Analysis Date = 04/18/17 Pct Recovery = 93% Analysis Date = 04/18/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 94% Analysis Date = 04/13/17 Pct Recovery = 94% Analysis Date = 04/11/17 Pct Recovery = 94% Analysis Date = 04/11/17 Pct Recovery = 94% Analysis Date = 04/09/17 Pct Recovery = 94% Analysis Date = 04/09/17 Pct Recovery = 94% Analysis Date = 04/07/17 Pct Recovery = 94% Analysis Date = 04/07/17 Pct Recovery = 94% Analysis Date = 04/05/17 Pct Recovery = 94% Analysis Date = 04/05/17 Pct Recovery = 94% Analysis Date = 04/03/17 Pct Recovery = 94% Analysis Date = 04/03/17 Pct Recovery = 94% Analysis Date = 03/31/17 Pct Recovery = 95% Analysis Date = 03/31/17 Pct Recovery = 95% Analysis Date = 03/29/17 Pct Recovery = 95% Analysis Date = 03/29/17 Pct Recovery = 95% Analysis Date = 03/27/17 Pct Recovery = 95% Analysis Date = 03/27/17 Pct Recovery = 95% Analysis Date = 03/25/17 Pct Recovery = 95% Analysis Date = 03/25/17 Pct Recovery = 95% Analysis Date = 03/23/17 Pct Recovery = 95% Analysis Date = 03/23/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/14/17 Pct Recovery = 96% Analysis Date = 03/14/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/10/17 Pct Recovery = 96% Analysis Date = 03/10/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/06/17 Pct Recovery = 96% Analysis Date = 03/06/17 Pct Recovery = 96% Analysis Date = 03/04/17 Pct Recovery = 97% Analysis Date = 03/04/17 Pct Recovery = 97% Analysis Date = 03/02/17 Pct Recovery = 97% Analysis Date = 03/02/17 Pct Recovery = 97% Analysis Date = 02/27/17 Pct Recovery = 97% Analysis Date = 02/27/17 Pct Recovery = 97% Analysis Date = 02/25/17 Pct Recovery = 97% Analysis Date = 02/25/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/21/17 Pct Recovery = 97% Analysis Date = 02/21/17 Pct Recovery = 97% Analysis Date = 02/19/17 Pct Recovery = 98% Analysis Date = 02/19/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/10/17 Pct Recovery = 98% Analysis Date = 02/10/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/02/17 Pct Recovery = 98% Analysis Date = 02/02/17 Pct Recovery = 98% Analysis Date = 01/31/17 Pct Recovery = 98% Analysis Date = 01/31/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/29/17 Pct Recovery = 98% Analysis Date = 01/26/17 Pct Recovery = 98% Analysis Date = 01/26/17 Pct Recovery = 98% Analysis Date = 01/24/17 Pct Recovery = 98% Analysis Date = 01/24/17 Pct Recovery = 98% Analysis Date = 01/22/17 Pct Recovery = 98% Analysis Date = 01/22/17 Pct Recovery = 98% Analysis Date = 01/20/17 Pct Recovery = 98% Analysis Date = 01/20/17 Pct Recovery = 98% Analysis Date = 01/18/17 Pct Recovery = 98% Analysis Date = 01/18/17 Pct Recovery = 98% Analysis Date = 01/16/17 Pct Recovery = 98% Analysis Date = 01/16/17 Pct Recovery = 98% Analysis Date = 01/14/17 Pct Recovery = 98% Analysis Date = 01/14/17 Pct Recovery = 98% Analysis Date = 01/11/17 Pct Recovery = 98% Analysis Date = 01/11/17 Pct Recovery = 98% Analysis Date = 01/09/17 Pct Recovery = 98% Analysis Date = 01/09/17 Pct Recovery = 98% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/05/17 Pct Recovery = 99% Analysis Date = 01/05/17 Pct Recovery = 99% Analysis Date = 01/03/17 Pct Recovery = 99% Analysis Date = 01/03/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 01/01/17 Pct Recovery = 99% Analysis Date = 12/30/16 Pct Recovery = 99% Analysis Date = 12/30/16 Pct Recovery = 99% Analysis Date = 12/28/16 Pct Recovery = 99% Analysis Date = 12/28/16 Pct Recovery = 99% Analysis Date = 12/25/16 Pct Recovery = 99% Analysis Date = 12/25/16 Pct Recovery = 99% Analysis Date = 12/23/16 Pct Recovery = 99% Analysis Date = 12/23/16 Pct Recovery = 99% Analysis Date = 12/21/16 Pct Recovery = 99% Analysis Date = 12/21/16 Pct Recovery = 99% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/19/16 Pct Recovery = 99% Analysis Date = 12/17/16 Pct Recovery = 98% Analysis Date = 12/17/16 Pct Recovery = 98% Analysis Date = 12/15/16 Pct Recovery = 98% Analysis Date = 12/15/16 Pct Recovery = 98% Analysis Date = 12/13/16 Pct Recovery = 97% Analysis Date = 12/13/16 Pct Recovery = 97% Analysis Date = 12/10/16 Pct Recovery = 97% Analysis Date = 12/10/16 Pct Recovery = 97% Analysis Date = 12/08/16 Pct Recovery = 96% Analysis Date = 12/08/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/06/16 Pct Recovery = 96% Analysis Date = 12/04/16 Pct Recovery = 95% Analysis Date = 12/04/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 11/30/16 Pct Recovery = 94% Analysis Date = 11/30/16 Pct Recovery = 94% Analysis Date = 11/28/16 Pct Recovery = 94% Analysis Date = 11/28/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/26/16 Pct Recovery = 94% Analysis Date = 11/23/16 Pct Recovery = 93% Analysis Date = 11/23/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/21/16 Pct Recovery = 93% Analysis Date = 11/19/16 Pct Recovery = 92% Analysis Date = 11/19/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/17/16 Pct Recovery = 92% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/15/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 90% Analysis Date = 11/11/16 Pct Recovery = 90% Analysis Date = 11/08/16 Pct Recovery = 90% Analysis Date = 11/08/16 Pct Recovery = 90% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/06/16 Pct Recovery = 89% Analysis Date = 11/04/16 Pct Recovery = 89% Analysis Date = 11/04/16 Pct Recovery = 89% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 11/02/16 Pct Recovery = 88% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/31/16 Pct Recovery = 88% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/29/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/27/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 85% Analysis Date = 10/20/16 Pct Recovery = 85% Analysis Date = 10/18/16 Pct Recovery = 85% Analysis Date = 10/18/16 Pct Recovery = 85% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/16/16 Pct Recovery = 84% Analysis Date = 10/14/16 Pct Recovery = 84% Analysis Date = 10/14/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 83% Analysis Date = 10/12/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/07/16 Pct Recovery = 83% Analysis Date = 10/07/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 82% Analysis Date = 10/05/16 Pct Recovery = 82% Analysis Date = 10/03/16 Pct Recovery = 82% Analysis Date = 10/03/16 Pct Recovery = 82% Analysis Date = 10/01/16 Pct Recovery = 81% Analysis Date = 10/01/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/29/16 Pct Recovery = 81% Analysis Date = 09/27/16 Pct Recovery = 80% Analysis Date = 09/27/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 80% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/16/16 Pct Recovery = 78% Analysis Date = 09/16/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 77% Analysis Date = 09/14/16 Pct Recovery = 77% Analysis Date = 09/12/16 Pct Recovery = 77% Analysis Date = 09/12/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 76% Analysis Date = 09/10/16 Pct Recovery = 76% Analysis Date = 09/08/16 Pct Recovery = 76% Analysis Date = 09/08/16 Pct Recovery = 76% Analysis Date = 09/05/16 Pct Recovery = 75% Analysis Date = 09/05/16 Pct Recovery = 75% Analysis Date = 09/03/16 Pct Recovery = 75% Analysis Date = 09/03/16 Pct Recovery = 75% Analysis Date = 09/01/16 Pct Recovery = 74% Analysis Date = 09/01/16 Pct Recovery = 74% Analysis Date = 08/30/16 Pct Recovery = 74% Analysis Date = 08/30/16 Pct Recovery = 74% Analysis Date = 08/28/16 Pct Recovery = 74% Analysis Date = 08/28/16 Pct Recovery = 74% Analysis Date = 08/26/16 Pct Recovery = 74% Analysis Date = 08/26/16 Pct Recovery = 74% Analysis Date = 08/24/16 Pct Recovery = 74% Analysis Date = 08/24/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/21/16 Pct Recovery = 74% Analysis Date = 08/19/16 Pct Recovery = 74% Analysis Date = 08/19/16 Pct Recovery = 74% Analysis Date = 08/17/16 Pct Recovery = 74% Analysis Date = 08/17/16 Pct Recovery = 74% Analysis Date = 08/15/16 Pct Recovery = 74% Analysis Date = 08/15/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/13/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/11/16 Pct Recovery = 74% Analysis Date = 08/09/16 Pct Recovery = 74% Analysis Date = 08/09/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/06/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 07/31/16 Pct Recovery = 74% Analysis Date = 07/31/16 Pct Recovery = 74% Analysis Date = 07/29/16 Pct Recovery = 74% Analysis Date = 07/29/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/20/16 Pct Recovery = 74% Analysis Date = 07/20/16 Pct Recovery = 74% Analysis Date = 07/18/16 Pct Recovery = 74% Analysis Date = 07/18/16 Pct Recovery = 74% Analysis Date = 07/16/16 Pct Recovery = 74% Analysis Date = 07/16/16 Pct Recovery = 74% Analysis Date = 07/14/16 Pct Recovery = 74% Analysis Date = 07/14/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/12/16 Pct Recovery = 74% Analysis Date = 07/10/16 Pct Recovery = 74% Analysis Date = 07/10/16 Pct Recovery = 74% Analysis Date = 07/08/16 Pct Recovery = 74% Analysis Date = 07/08/16 Pct Recovery = 74% Analysis Date = 07/05/16 Pct Recovery = 74% Analysis Date = 07/05/16 Pct Recovery = 74% Analysis Date = 07/03/16 Pct Recovery = 74% Analysis Date = 07/03/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 06/29/16 Pct Recovery = 74% Analysis Date = 06/29/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/27/16 Pct Recovery = 74% Analysis Date = 06/25/16 Pct Recovery = 74% Analysis Date = 06/25/16 Pct Recovery = 74% Analysis Date = 06/23/16 Pct Recovery = 74% Analysis Date = 06/23/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/21/16 Pct Recovery = 74% Analysis Date = 06/18/16 Pct Recovery = 74% Analysis Date = 06/18/16 Pct Recovery = 74% Analysis Date = 06/16/16 Pct Recovery = 74% Analysis Date = 06/16/16 Pct Recovery = 74% Analysis Date = 06/14/16 Pct Recovery = 74% Analysis Date = 06/14/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/08/16 Pct Recovery = 74% Analysis Date = 06/08/16 Pct Recovery = 74% Analysis Date = 06/06/16 Pct Recovery = 74% Analysis Date = 06/06/16 Pct Recovery = 74% Analysis Date = 06/03/16 Pct Recovery = 74% Analysis Date = 06/03/16 Pct Recovery = 74% Analysis Date = 06/01/16 Pct Recovery = 74% Analysis Date = 06/01/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/28/16 Pct Recovery = 74% Analysis Date = 05/26/16 Pct Recovery = 74% Analysis Date = 05/26/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 74% Analysis Date = 05/24/16 Pct Recovery = 74% Analysis Date = 05/22/16 Pct Recovery = 75% Analysis Date = 05/22/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/17/16 Pct Recovery = 76% Analysis Date = 05/17/16 Pct Recovery = 76% Analysis Date = 05/15/16 Pct Recovery = 76% Analysis Date = 05/15/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/13/16 Pct Recovery = 76% Analysis Date = 05/11/16 Pct Recovery = 77% Analysis Date = 05/11/16 Pct Recovery = 77% Analysis Date = 05/09/16 Pct Recovery = 77% Analysis Date = 05/09/16 Pct Recovery = 77% Analysis Date = 05/07/16 Pct Recovery = 77% Analysis Date = 05/07/16 Pct Recovery = 77% Analysis Date = 05/05/16 Pct Recovery = 78% Analysis Date = 05/05/16 Pct Recovery = 78% Analysis Date = 05/02/16 Pct Recovery = 78% Analysis Date = 05/02/16 Pct Recovery = 78% Analysis Date = 04/30/16 Pct Recovery = 78% Analysis Date = 04/30/16 Pct Recovery = 78% Analysis Date = 04/28/16 Pct Recovery = 79% Analysis Date = 04/28/16 Pct Recovery = 79% Analysis Date = 04/26/16 Pct Recovery = 79% Analysis Date = 04/26/16 Pct Recovery = 79% Analysis Date = 04/24/16 Pct Recovery = 79% Analysis Date = 04/24/16 Pct Recovery = 79% Analysis Date = 04/22/16 Pct Recovery = 80% Analysis Date = 04/22/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/20/16 Pct Recovery = 80% Analysis Date = 04/17/16 Pct Recovery = 81% Analysis Date = 04/17/16 Pct Recovery = 81% Analysis Date = 04/15/16 Pct Recovery = 81% Analysis Date = 04/15/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 81% Analysis Date = 04/11/16 Pct Recovery = 82% Analysis Date = 04/11/16 Pct Recovery = 82% Analysis Date = 04/09/16 Pct Recovery = 82% Analysis Date = 04/09/16 Pct Recovery = 82% Analysis Date = 04/07/16 Pct Recovery = 82% Analysis Date = 04/07/16 Pct Recovery = 82% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/05/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 04/03/16 Pct Recovery = 83% Analysis Date = 03/31/16 Pct Recovery = 83% Analysis Date = 03/31/16 Pct Recovery = 83% Analysis Date = 03/29/16 Pct Recovery = 84% Analysis Date = 03/29/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 85% Analysis Date = 03/19/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/12/16 Pct Recovery = 86% Analysis Date = 03/12/16 Pct Recovery = 86% Analysis Date = 03/10/16 Pct Recovery = 86% Analysis Date = 03/10/16 Pct Recovery = 86% Analysis Date = 03/08/16 Pct Recovery = 87% Analysis Date = 03/08/16 Pct Recovery = 87% Analysis Date = 03/06/16 Pct Recovery = 87% Analysis Date = 03/06/16 Pct Recovery = 87% Analysis Date = 03/04/16 Pct Recovery = 87% Analysis Date = 03/04/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 88% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
FONOFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 86% 14% 83% 16%
Total 18 86% 14% 83% 16%

Sample Statistics
FONOFOS

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
HEXAZINONE
METHOD: 2033 , TESTIDCODE: 04025GCM39

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 77% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 65% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 63% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 60% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 59% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 64% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 56% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 62% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 60% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 60% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 61% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 87% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 63% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 75% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 68% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 05/10/17 Pct Recovery = 67% Analysis Date = 05/08/17 Pct Recovery = 67% Analysis Date = 05/08/17 Pct Recovery = 67% Analysis Date = 05/06/17 Pct Recovery = 67% Analysis Date = 05/06/17 Pct Recovery = 67% Analysis Date = 05/04/17 Pct Recovery = 67% Analysis Date = 05/04/17 Pct Recovery = 67% Analysis Date = 05/02/17 Pct Recovery = 67% Analysis Date = 05/02/17 Pct Recovery = 67% Analysis Date = 04/30/17 Pct Recovery = 67% Analysis Date = 04/30/17 Pct Recovery = 67% Analysis Date = 04/27/17 Pct Recovery = 67% Analysis Date = 04/27/17 Pct Recovery = 67% Analysis Date = 04/25/17 Pct Recovery = 67% Analysis Date = 04/25/17 Pct Recovery = 67% Analysis Date = 04/23/17 Pct Recovery = 67% Analysis Date = 04/23/17 Pct Recovery = 67% Analysis Date = 04/21/17 Pct Recovery = 67% Analysis Date = 04/21/17 Pct Recovery = 67% Analysis Date = 04/19/17 Pct Recovery = 67% Analysis Date = 04/19/17 Pct Recovery = 67% Analysis Date = 04/17/17 Pct Recovery = 67% Analysis Date = 04/17/17 Pct Recovery = 67% Analysis Date = 04/14/17 Pct Recovery = 67% Analysis Date = 04/14/17 Pct Recovery = 67% Analysis Date = 04/12/17 Pct Recovery = 67% Analysis Date = 04/12/17 Pct Recovery = 67% Analysis Date = 04/10/17 Pct Recovery = 67% Analysis Date = 04/10/17 Pct Recovery = 67% Analysis Date = 04/08/17 Pct Recovery = 67% Analysis Date = 04/08/17 Pct Recovery = 67% Analysis Date = 04/06/17 Pct Recovery = 67% Analysis Date = 04/06/17 Pct Recovery = 67% Analysis Date = 04/04/17 Pct Recovery = 67% Analysis Date = 04/04/17 Pct Recovery = 67% Analysis Date = 04/01/17 Pct Recovery = 67% Analysis Date = 04/01/17 Pct Recovery = 67% Analysis Date = 03/30/17 Pct Recovery = 67% Analysis Date = 03/30/17 Pct Recovery = 67% Analysis Date = 03/28/17 Pct Recovery = 67% Analysis Date = 03/28/17 Pct Recovery = 67% Analysis Date = 03/26/17 Pct Recovery = 67% Analysis Date = 03/26/17 Pct Recovery = 67% Analysis Date = 03/24/17 Pct Recovery = 68% Analysis Date = 03/24/17 Pct Recovery = 68% Analysis Date = 03/21/17 Pct Recovery = 68% Analysis Date = 03/21/17 Pct Recovery = 68% Analysis Date = 03/19/17 Pct Recovery = 68% Analysis Date = 03/19/17 Pct Recovery = 68% Analysis Date = 03/17/17 Pct Recovery = 68% Analysis Date = 03/17/17 Pct Recovery = 68% Analysis Date = 03/15/17 Pct Recovery = 68% Analysis Date = 03/15/17 Pct Recovery = 68% Analysis Date = 03/13/17 Pct Recovery = 68% Analysis Date = 03/13/17 Pct Recovery = 68% Analysis Date = 03/11/17 Pct Recovery = 68% Analysis Date = 03/11/17 Pct Recovery = 68% Analysis Date = 03/08/17 Pct Recovery = 68% Analysis Date = 03/08/17 Pct Recovery = 68% Analysis Date = 03/06/17 Pct Recovery = 68% Analysis Date = 03/06/17 Pct Recovery = 68% Analysis Date = 03/04/17 Pct Recovery = 68% Analysis Date = 03/04/17 Pct Recovery = 68% Analysis Date = 03/02/17 Pct Recovery = 68% Analysis Date = 03/02/17 Pct Recovery = 68% Analysis Date = 02/28/17 Pct Recovery = 68% Analysis Date = 02/28/17 Pct Recovery = 68% Analysis Date = 02/26/17 Pct Recovery = 68% Analysis Date = 02/26/17 Pct Recovery = 68% Analysis Date = 02/23/17 Pct Recovery = 68% Analysis Date = 02/23/17 Pct Recovery = 68% Analysis Date = 02/21/17 Pct Recovery = 68% Analysis Date = 02/21/17 Pct Recovery = 68% Analysis Date = 02/19/17 Pct Recovery = 68% Analysis Date = 02/19/17 Pct Recovery = 68% Analysis Date = 02/17/17 Pct Recovery = 68% Analysis Date = 02/17/17 Pct Recovery = 68% Analysis Date = 02/15/17 Pct Recovery = 68% Analysis Date = 02/15/17 Pct Recovery = 68% Analysis Date = 02/12/17 Pct Recovery = 68% Analysis Date = 02/12/17 Pct Recovery = 68% Analysis Date = 02/10/17 Pct Recovery = 68% Analysis Date = 02/10/17 Pct Recovery = 68% Analysis Date = 02/08/17 Pct Recovery = 68% Analysis Date = 02/08/17 Pct Recovery = 68% Analysis Date = 02/06/17 Pct Recovery = 68% Analysis Date = 02/06/17 Pct Recovery = 68% Analysis Date = 02/04/17 Pct Recovery = 68% Analysis Date = 02/04/17 Pct Recovery = 68% Analysis Date = 02/02/17 Pct Recovery = 68% Analysis Date = 02/02/17 Pct Recovery = 68% Analysis Date = 01/30/17 Pct Recovery = 68% Analysis Date = 01/30/17 Pct Recovery = 68% Analysis Date = 01/28/17 Pct Recovery = 68% Analysis Date = 01/28/17 Pct Recovery = 68% Analysis Date = 01/26/17 Pct Recovery = 68% Analysis Date = 01/26/17 Pct Recovery = 68% Analysis Date = 01/24/17 Pct Recovery = 68% Analysis Date = 01/24/17 Pct Recovery = 68% Analysis Date = 01/22/17 Pct Recovery = 68% Analysis Date = 01/22/17 Pct Recovery = 68% Analysis Date = 01/20/17 Pct Recovery = 68% Analysis Date = 01/20/17 Pct Recovery = 68% Analysis Date = 01/17/17 Pct Recovery = 69% Analysis Date = 01/17/17 Pct Recovery = 69% Analysis Date = 01/15/17 Pct Recovery = 69% Analysis Date = 01/15/17 Pct Recovery = 69% Analysis Date = 01/13/17 Pct Recovery = 69% Analysis Date = 01/13/17 Pct Recovery = 69% Analysis Date = 01/11/17 Pct Recovery = 69% Analysis Date = 01/11/17 Pct Recovery = 69% Analysis Date = 01/09/17 Pct Recovery = 69% Analysis Date = 01/09/17 Pct Recovery = 69% Analysis Date = 01/07/17 Pct Recovery = 69% Analysis Date = 01/07/17 Pct Recovery = 69% Analysis Date = 01/04/17 Pct Recovery = 69% Analysis Date = 01/04/17 Pct Recovery = 69% Analysis Date = 01/02/17 Pct Recovery = 69% Analysis Date = 01/02/17 Pct Recovery = 69% Analysis Date = 12/31/16 Pct Recovery = 69% Analysis Date = 12/31/16 Pct Recovery = 69% Analysis Date = 12/29/16 Pct Recovery = 70% Analysis Date = 12/29/16 Pct Recovery = 70% Analysis Date = 12/27/16 Pct Recovery = 70% Analysis Date = 12/27/16 Pct Recovery = 70% Analysis Date = 12/24/16 Pct Recovery = 70% Analysis Date = 12/24/16 Pct Recovery = 70% Analysis Date = 12/22/16 Pct Recovery = 70% Analysis Date = 12/22/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 70% Analysis Date = 12/20/16 Pct Recovery = 70% Analysis Date = 12/18/16 Pct Recovery = 70% Analysis Date = 12/18/16 Pct Recovery = 70% Analysis Date = 12/16/16 Pct Recovery = 70% Analysis Date = 12/16/16 Pct Recovery = 70% Analysis Date = 12/14/16 Pct Recovery = 70% Analysis Date = 12/14/16 Pct Recovery = 70% Analysis Date = 12/11/16 Pct Recovery = 70% Analysis Date = 12/11/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/09/16 Pct Recovery = 70% Analysis Date = 12/07/16 Pct Recovery = 70% Analysis Date = 12/07/16 Pct Recovery = 70% Analysis Date = 12/05/16 Pct Recovery = 70% Analysis Date = 12/05/16 Pct Recovery = 70% Analysis Date = 12/03/16 Pct Recovery = 70% Analysis Date = 12/03/16 Pct Recovery = 70% Analysis Date = 12/01/16 Pct Recovery = 70% Analysis Date = 12/01/16 Pct Recovery = 70% Analysis Date = 11/28/16 Pct Recovery = 70% Analysis Date = 11/28/16 Pct Recovery = 70% Analysis Date = 11/26/16 Pct Recovery = 70% Analysis Date = 11/26/16 Pct Recovery = 70% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/22/16 Pct Recovery = 70% Analysis Date = 11/22/16 Pct Recovery = 70% Analysis Date = 11/20/16 Pct Recovery = 70% Analysis Date = 11/20/16 Pct Recovery = 70% Analysis Date = 11/17/16 Pct Recovery = 70% Analysis Date = 11/17/16 Pct Recovery = 70% Analysis Date = 11/15/16 Pct Recovery = 70% Analysis Date = 11/15/16 Pct Recovery = 70% Analysis Date = 11/13/16 Pct Recovery = 70% Analysis Date = 11/13/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 70% Analysis Date = 11/11/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/09/16 Pct Recovery = 70% Analysis Date = 11/07/16 Pct Recovery = 70% Analysis Date = 11/07/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 70% Analysis Date = 11/04/16 Pct Recovery = 70% Analysis Date = 11/02/16 Pct Recovery = 70% Analysis Date = 11/02/16 Pct Recovery = 70% Analysis Date = 10/31/16 Pct Recovery = 70% Analysis Date = 10/31/16 Pct Recovery = 70% Analysis Date = 10/29/16 Pct Recovery = 70% Analysis Date = 10/29/16 Pct Recovery = 70% Analysis Date = 10/27/16 Pct Recovery = 70% Analysis Date = 10/27/16 Pct Recovery = 70% Analysis Date = 10/25/16 Pct Recovery = 70% Analysis Date = 10/25/16 Pct Recovery = 70% Analysis Date = 10/22/16 Pct Recovery = 70% Analysis Date = 10/22/16 Pct Recovery = 70% Analysis Date = 10/20/16 Pct Recovery = 70% Analysis Date = 10/20/16 Pct Recovery = 70% Analysis Date = 10/18/16 Pct Recovery = 70% Analysis Date = 10/18/16 Pct Recovery = 70% Analysis Date = 10/16/16 Pct Recovery = 70% Analysis Date = 10/16/16 Pct Recovery = 70% Analysis Date = 10/14/16 Pct Recovery = 70% Analysis Date = 10/14/16 Pct Recovery = 70% Analysis Date = 10/12/16 Pct Recovery = 70% Analysis Date = 10/12/16 Pct Recovery = 70% Analysis Date = 10/09/16 Pct Recovery = 70% Analysis Date = 10/09/16 Pct Recovery = 70% Analysis Date = 10/07/16 Pct Recovery = 70% Analysis Date = 10/07/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/28/16 Pct Recovery = 70% Analysis Date = 09/26/16 Pct Recovery = 70% Analysis Date = 09/26/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/24/16 Pct Recovery = 70% Analysis Date = 09/22/16 Pct Recovery = 70% Analysis Date = 09/22/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/20/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/18/16 Pct Recovery = 70% Analysis Date = 09/15/16 Pct Recovery = 70% Analysis Date = 09/15/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 70% Analysis Date = 09/13/16 Pct Recovery = 70% Analysis Date = 09/11/16 Pct Recovery = 70% Analysis Date = 09/11/16 Pct Recovery = 70% Analysis Date = 09/09/16 Pct Recovery = 70% Analysis Date = 09/09/16 Pct Recovery = 70% Analysis Date = 09/07/16 Pct Recovery = 70% Analysis Date = 09/07/16 Pct Recovery = 70% Analysis Date = 09/05/16 Pct Recovery = 70% Analysis Date = 09/05/16 Pct Recovery = 70% Analysis Date = 09/02/16 Pct Recovery = 70% Analysis Date = 09/02/16 Pct Recovery = 70% Analysis Date = 08/31/16 Pct Recovery = 70% Analysis Date = 08/31/16 Pct Recovery = 70% Analysis Date = 08/29/16 Pct Recovery = 70% Analysis Date = 08/29/16 Pct Recovery = 70% Analysis Date = 08/27/16 Pct Recovery = 70% Analysis Date = 08/27/16 Pct Recovery = 70% Analysis Date = 08/25/16 Pct Recovery = 70% Analysis Date = 08/25/16 Pct Recovery = 70% Analysis Date = 08/22/16 Pct Recovery = 70% Analysis Date = 08/22/16 Pct Recovery = 70% Analysis Date = 08/20/16 Pct Recovery = 70% Analysis Date = 08/20/16 Pct Recovery = 70% Analysis Date = 08/18/16 Pct Recovery = 69% Analysis Date = 08/18/16 Pct Recovery = 69% Analysis Date = 08/16/16 Pct Recovery = 69% Analysis Date = 08/16/16 Pct Recovery = 69% Analysis Date = 08/14/16 Pct Recovery = 69% Analysis Date = 08/14/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 69% Analysis Date = 08/12/16 Pct Recovery = 69% Analysis Date = 08/09/16 Pct Recovery = 69% Analysis Date = 08/09/16 Pct Recovery = 69% Analysis Date = 08/07/16 Pct Recovery = 69% Analysis Date = 08/07/16 Pct Recovery = 69% Analysis Date = 08/05/16 Pct Recovery = 69% Analysis Date = 08/05/16 Pct Recovery = 69% Analysis Date = 08/03/16 Pct Recovery = 68% Analysis Date = 08/03/16 Pct Recovery = 68% Analysis Date = 08/01/16 Pct Recovery = 68% Analysis Date = 08/01/16 Pct Recovery = 68% Analysis Date = 07/30/16 Pct Recovery = 68% Analysis Date = 07/30/16 Pct Recovery = 68% Analysis Date = 07/27/16 Pct Recovery = 68% Analysis Date = 07/27/16 Pct Recovery = 68% Analysis Date = 07/25/16 Pct Recovery = 68% Analysis Date = 07/25/16 Pct Recovery = 68% Analysis Date = 07/23/16 Pct Recovery = 68% Analysis Date = 07/23/16 Pct Recovery = 68% Analysis Date = 07/21/16 Pct Recovery = 67% Analysis Date = 07/21/16 Pct Recovery = 67% Analysis Date = 07/19/16 Pct Recovery = 67% Analysis Date = 07/19/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/17/16 Pct Recovery = 67% Analysis Date = 07/14/16 Pct Recovery = 67% Analysis Date = 07/14/16 Pct Recovery = 67% Analysis Date = 07/12/16 Pct Recovery = 67% Analysis Date = 07/12/16 Pct Recovery = 67% Analysis Date = 07/10/16 Pct Recovery = 67% Analysis Date = 07/10/16 Pct Recovery = 67% Analysis Date = 07/08/16 Pct Recovery = 66% Analysis Date = 07/08/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 07/06/16 Pct Recovery = 66% Analysis Date = 07/03/16 Pct Recovery = 66% Analysis Date = 07/03/16 Pct Recovery = 66% Analysis Date = 07/01/16 Pct Recovery = 66% Analysis Date = 07/01/16 Pct Recovery = 66% Analysis Date = 06/29/16 Pct Recovery = 66% Analysis Date = 06/29/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 65% Analysis Date = 06/25/16 Pct Recovery = 65% Analysis Date = 06/23/16 Pct Recovery = 65% Analysis Date = 06/23/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 65% Analysis Date = 06/16/16 Pct Recovery = 65% Analysis Date = 06/16/16 Pct Recovery = 65% Analysis Date = 06/14/16 Pct Recovery = 65% Analysis Date = 06/14/16 Pct Recovery = 65% Analysis Date = 06/12/16 Pct Recovery = 64% Analysis Date = 06/12/16 Pct Recovery = 64% Analysis Date = 06/10/16 Pct Recovery = 64% Analysis Date = 06/10/16 Pct Recovery = 64% Analysis Date = 06/07/16 Pct Recovery = 64% Analysis Date = 06/07/16 Pct Recovery = 64% Analysis Date = 06/05/16 Pct Recovery = 64% Analysis Date = 06/05/16 Pct Recovery = 64% Analysis Date = 06/03/16 Pct Recovery = 64% Analysis Date = 06/03/16 Pct Recovery = 64% Analysis Date = 06/01/16 Pct Recovery = 64% Analysis Date = 06/01/16 Pct Recovery = 64% Analysis Date = 05/30/16 Pct Recovery = 63% Analysis Date = 05/30/16 Pct Recovery = 63% Analysis Date = 05/27/16 Pct Recovery = 63% Analysis Date = 05/27/16 Pct Recovery = 63% Analysis Date = 05/25/16 Pct Recovery = 63% Analysis Date = 05/25/16 Pct Recovery = 63% Analysis Date = 05/23/16 Pct Recovery = 63% Analysis Date = 05/23/16 Pct Recovery = 63% Analysis Date = 05/21/16 Pct Recovery = 63% Analysis Date = 05/21/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/17/16 Pct Recovery = 63% Analysis Date = 05/17/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/14/16 Pct Recovery = 63% Analysis Date = 05/12/16 Pct Recovery = 63% Analysis Date = 05/12/16 Pct Recovery = 63% Analysis Date = 05/10/16 Pct Recovery = 63% Analysis Date = 05/10/16 Pct Recovery = 63% Analysis Date = 05/08/16 Pct Recovery = 63% Analysis Date = 05/08/16 Pct Recovery = 63% Analysis Date = 05/06/16 Pct Recovery = 63% Analysis Date = 05/06/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 63% Analysis Date = 05/04/16 Pct Recovery = 63% Analysis Date = 05/01/16 Pct Recovery = 63% Analysis Date = 05/01/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 63% Analysis Date = 04/29/16 Pct Recovery = 63% Analysis Date = 04/27/16 Pct Recovery = 63% Analysis Date = 04/27/16 Pct Recovery = 63% Analysis Date = 04/25/16 Pct Recovery = 64% Analysis Date = 04/25/16 Pct Recovery = 64% Analysis Date = 04/23/16 Pct Recovery = 64% Analysis Date = 04/23/16 Pct Recovery = 64% Analysis Date = 04/21/16 Pct Recovery = 64% Analysis Date = 04/21/16 Pct Recovery = 64% Analysis Date = 04/18/16 Pct Recovery = 64% Analysis Date = 04/18/16 Pct Recovery = 64% Analysis Date = 04/16/16 Pct Recovery = 64% Analysis Date = 04/16/16 Pct Recovery = 64% Analysis Date = 04/14/16 Pct Recovery = 64% Analysis Date = 04/14/16 Pct Recovery = 64% Analysis Date = 04/12/16 Pct Recovery = 64% Analysis Date = 04/12/16 Pct Recovery = 64% Analysis Date = 04/10/16 Pct Recovery = 64% Analysis Date = 04/10/16 Pct Recovery = 64% Analysis Date = 04/07/16 Pct Recovery = 64% Analysis Date = 04/07/16 Pct Recovery = 64% Analysis Date = 04/05/16 Pct Recovery = 64% Analysis Date = 04/05/16 Pct Recovery = 64% Analysis Date = 04/03/16 Pct Recovery = 64% Analysis Date = 04/03/16 Pct Recovery = 64% Analysis Date = 04/01/16 Pct Recovery = 64% Analysis Date = 04/01/16 Pct Recovery = 64% Analysis Date = 03/30/16 Pct Recovery = 64% Analysis Date = 03/30/16 Pct Recovery = 64% Analysis Date = 03/28/16 Pct Recovery = 64% Analysis Date = 03/28/16 Pct Recovery = 64% Analysis Date = 03/25/16 Pct Recovery = 64% Analysis Date = 03/25/16 Pct Recovery = 64% Analysis Date = 03/23/16 Pct Recovery = 64% Analysis Date = 03/23/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/17/16 Pct Recovery = 64% Analysis Date = 03/17/16 Pct Recovery = 64% Analysis Date = 03/15/16 Pct Recovery = 64% Analysis Date = 03/15/16 Pct Recovery = 64% Analysis Date = 03/12/16 Pct Recovery = 65% Analysis Date = 03/12/16 Pct Recovery = 65% Analysis Date = 03/10/16 Pct Recovery = 65% Analysis Date = 03/10/16 Pct Recovery = 65% Analysis Date = 03/08/16 Pct Recovery = 65% Analysis Date = 03/08/16 Pct Recovery = 65% Analysis Date = 03/06/16 Pct Recovery = 65% Analysis Date = 03/06/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 03/04/16 Pct Recovery = 65% Analysis Date = 03/02/16 Pct Recovery = 65% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
HEXAZINONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 67% 9% 64% 7%
Total 19 67% 9% 64% 7%

Sample Statistics
HEXAZINONE

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
IPRODIONE
METHOD: 2033 , TESTIDCODE: 61593GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 96% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 92% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 112% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 96% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 100% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 93% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 76% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 92% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 112% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 105% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 82% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 97% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 93% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 71% Analysis Date = 05/10/17 Pct Recovery = 96% Analysis Date = 05/08/17 Pct Recovery = 96% Analysis Date = 05/08/17 Pct Recovery = 96% Analysis Date = 05/06/17 Pct Recovery = 96% Analysis Date = 05/06/17 Pct Recovery = 96% Analysis Date = 05/04/17 Pct Recovery = 96% Analysis Date = 05/04/17 Pct Recovery = 96% Analysis Date = 05/02/17 Pct Recovery = 96% Analysis Date = 05/02/17 Pct Recovery = 96% Analysis Date = 04/30/17 Pct Recovery = 96% Analysis Date = 04/30/17 Pct Recovery = 96% Analysis Date = 04/27/17 Pct Recovery = 96% Analysis Date = 04/27/17 Pct Recovery = 96% Analysis Date = 04/25/17 Pct Recovery = 96% Analysis Date = 04/25/17 Pct Recovery = 96% Analysis Date = 04/23/17 Pct Recovery = 96% Analysis Date = 04/23/17 Pct Recovery = 96% Analysis Date = 04/21/17 Pct Recovery = 96% Analysis Date = 04/21/17 Pct Recovery = 96% Analysis Date = 04/19/17 Pct Recovery = 96% Analysis Date = 04/19/17 Pct Recovery = 96% Analysis Date = 04/17/17 Pct Recovery = 96% Analysis Date = 04/17/17 Pct Recovery = 96% Analysis Date = 04/14/17 Pct Recovery = 96% Analysis Date = 04/14/17 Pct Recovery = 96% Analysis Date = 04/12/17 Pct Recovery = 96% Analysis Date = 04/12/17 Pct Recovery = 96% Analysis Date = 04/10/17 Pct Recovery = 96% Analysis Date = 04/10/17 Pct Recovery = 96% Analysis Date = 04/08/17 Pct Recovery = 95% Analysis Date = 04/08/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/04/17 Pct Recovery = 95% Analysis Date = 04/04/17 Pct Recovery = 95% Analysis Date = 04/01/17 Pct Recovery = 95% Analysis Date = 04/01/17 Pct Recovery = 95% Analysis Date = 03/30/17 Pct Recovery = 95% Analysis Date = 03/30/17 Pct Recovery = 95% Analysis Date = 03/28/17 Pct Recovery = 95% Analysis Date = 03/28/17 Pct Recovery = 95% Analysis Date = 03/26/17 Pct Recovery = 95% Analysis Date = 03/26/17 Pct Recovery = 95% Analysis Date = 03/24/17 Pct Recovery = 95% Analysis Date = 03/24/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/21/17 Pct Recovery = 95% Analysis Date = 03/19/17 Pct Recovery = 95% Analysis Date = 03/19/17 Pct Recovery = 95% Analysis Date = 03/17/17 Pct Recovery = 95% Analysis Date = 03/17/17 Pct Recovery = 95% Analysis Date = 03/15/17 Pct Recovery = 95% Analysis Date = 03/15/17 Pct Recovery = 95% Analysis Date = 03/13/17 Pct Recovery = 95% Analysis Date = 03/13/17 Pct Recovery = 95% Analysis Date = 03/11/17 Pct Recovery = 95% Analysis Date = 03/11/17 Pct Recovery = 95% Analysis Date = 03/08/17 Pct Recovery = 95% Analysis Date = 03/08/17 Pct Recovery = 95% Analysis Date = 03/06/17 Pct Recovery = 95% Analysis Date = 03/06/17 Pct Recovery = 95% Analysis Date = 03/04/17 Pct Recovery = 95% Analysis Date = 03/04/17 Pct Recovery = 95% Analysis Date = 03/02/17 Pct Recovery = 94% Analysis Date = 03/02/17 Pct Recovery = 94% Analysis Date = 02/28/17 Pct Recovery = 94% Analysis Date = 02/28/17 Pct Recovery = 94% Analysis Date = 02/26/17 Pct Recovery = 94% Analysis Date = 02/26/17 Pct Recovery = 94% Analysis Date = 02/23/17 Pct Recovery = 94% Analysis Date = 02/23/17 Pct Recovery = 94% Analysis Date = 02/21/17 Pct Recovery = 94% Analysis Date = 02/21/17 Pct Recovery = 94% Analysis Date = 02/19/17 Pct Recovery = 94% Analysis Date = 02/19/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/17/17 Pct Recovery = 94% Analysis Date = 02/15/17 Pct Recovery = 94% Analysis Date = 02/15/17 Pct Recovery = 94% Analysis Date = 02/12/17 Pct Recovery = 94% Analysis Date = 02/12/17 Pct Recovery = 94% Analysis Date = 02/10/17 Pct Recovery = 94% Analysis Date = 02/10/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 94% Analysis Date = 02/08/17 Pct Recovery = 94% Analysis Date = 02/06/17 Pct Recovery = 94% Analysis Date = 02/06/17 Pct Recovery = 94% Analysis Date = 02/04/17 Pct Recovery = 94% Analysis Date = 02/04/17 Pct Recovery = 94% Analysis Date = 02/02/17 Pct Recovery = 94% Analysis Date = 02/02/17 Pct Recovery = 94% Analysis Date = 01/30/17 Pct Recovery = 94% Analysis Date = 01/30/17 Pct Recovery = 94% Analysis Date = 01/28/17 Pct Recovery = 94% Analysis Date = 01/28/17 Pct Recovery = 94% Analysis Date = 01/26/17 Pct Recovery = 94% Analysis Date = 01/26/17 Pct Recovery = 94% Analysis Date = 01/24/17 Pct Recovery = 94% Analysis Date = 01/24/17 Pct Recovery = 94% Analysis Date = 01/22/17 Pct Recovery = 94% Analysis Date = 01/22/17 Pct Recovery = 94% Analysis Date = 01/20/17 Pct Recovery = 94% Analysis Date = 01/20/17 Pct Recovery = 94% Analysis Date = 01/17/17 Pct Recovery = 94% Analysis Date = 01/17/17 Pct Recovery = 94% Analysis Date = 01/15/17 Pct Recovery = 94% Analysis Date = 01/15/17 Pct Recovery = 94% Analysis Date = 01/13/17 Pct Recovery = 94% Analysis Date = 01/13/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/09/17 Pct Recovery = 94% Analysis Date = 01/09/17 Pct Recovery = 94% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/07/17 Pct Recovery = 95% Analysis Date = 01/04/17 Pct Recovery = 95% Analysis Date = 01/04/17 Pct Recovery = 95% Analysis Date = 01/02/17 Pct Recovery = 95% Analysis Date = 01/02/17 Pct Recovery = 95% Analysis Date = 12/31/16 Pct Recovery = 95% Analysis Date = 12/31/16 Pct Recovery = 95% Analysis Date = 12/29/16 Pct Recovery = 95% Analysis Date = 12/29/16 Pct Recovery = 95% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/27/16 Pct Recovery = 96% Analysis Date = 12/24/16 Pct Recovery = 96% Analysis Date = 12/24/16 Pct Recovery = 96% Analysis Date = 12/22/16 Pct Recovery = 96% Analysis Date = 12/22/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/18/16 Pct Recovery = 96% Analysis Date = 12/18/16 Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/14/16 Pct Recovery = 96% Analysis Date = 12/14/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 97% Analysis Date = 12/11/16 Pct Recovery = 97% Analysis Date = 12/09/16 Pct Recovery = 97% Analysis Date = 12/09/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/07/16 Pct Recovery = 97% Analysis Date = 12/05/16 Pct Recovery = 97% Analysis Date = 12/05/16 Pct Recovery = 97% Analysis Date = 12/03/16 Pct Recovery = 97% Analysis Date = 12/03/16 Pct Recovery = 97% Analysis Date = 12/01/16 Pct Recovery = 97% Analysis Date = 12/01/16 Pct Recovery = 97% Analysis Date = 11/28/16 Pct Recovery = 97% Analysis Date = 11/28/16 Pct Recovery = 97% Analysis Date = 11/26/16 Pct Recovery = 97% Analysis Date = 11/26/16 Pct Recovery = 97% Analysis Date = 11/24/16 Pct Recovery = 97% Analysis Date = 11/24/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/22/16 Pct Recovery = 97% Analysis Date = 11/20/16 Pct Recovery = 97% Analysis Date = 11/20/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/17/16 Pct Recovery = 97% Analysis Date = 11/15/16 Pct Recovery = 98% Analysis Date = 11/15/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/13/16 Pct Recovery = 98% Analysis Date = 11/11/16 Pct Recovery = 98% Analysis Date = 11/11/16 Pct Recovery = 98% Analysis Date = 11/09/16 Pct Recovery = 98% Analysis Date = 11/09/16 Pct Recovery = 98% Analysis Date = 11/07/16 Pct Recovery = 98% Analysis Date = 11/07/16 Pct Recovery = 98% Analysis Date = 11/04/16 Pct Recovery = 98% Analysis Date = 11/04/16 Pct Recovery = 98% Analysis Date = 11/02/16 Pct Recovery = 98% Analysis Date = 11/02/16 Pct Recovery = 98% Analysis Date = 10/31/16 Pct Recovery = 98% Analysis Date = 10/31/16 Pct Recovery = 98% Analysis Date = 10/29/16 Pct Recovery = 98% Analysis Date = 10/29/16 Pct Recovery = 98% Analysis Date = 10/27/16 Pct Recovery = 98% Analysis Date = 10/27/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/25/16 Pct Recovery = 98% Analysis Date = 10/22/16 Pct Recovery = 98% Analysis Date = 10/22/16 Pct Recovery = 98% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/20/16 Pct Recovery = 99% Analysis Date = 10/18/16 Pct Recovery = 99% Analysis Date = 10/18/16 Pct Recovery = 99% Analysis Date = 10/16/16 Pct Recovery = 99% Analysis Date = 10/16/16 Pct Recovery = 99% Analysis Date = 10/14/16 Pct Recovery = 99% Analysis Date = 10/14/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/09/16 Pct Recovery = 99% Analysis Date = 10/07/16 Pct Recovery = 99% Analysis Date = 10/07/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/28/16 Pct Recovery = 99% Analysis Date = 09/28/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 99% Analysis Date = 09/24/16 Pct Recovery = 100% Analysis Date = 09/24/16 Pct Recovery = 100% Analysis Date = 09/22/16 Pct Recovery = 100% Analysis Date = 09/22/16 Pct Recovery = 100% Analysis Date = 09/20/16 Pct Recovery = 100% Analysis Date = 09/20/16 Pct Recovery = 100% Analysis Date = 09/18/16 Pct Recovery = 100% Analysis Date = 09/18/16 Pct Recovery = 100% Analysis Date = 09/15/16 Pct Recovery = 100% Analysis Date = 09/15/16 Pct Recovery = 100% Analysis Date = 09/13/16 Pct Recovery = 100% Analysis Date = 09/13/16 Pct Recovery = 100% Analysis Date = 09/11/16 Pct Recovery = 100% Analysis Date = 09/11/16 Pct Recovery = 100% Analysis Date = 09/09/16 Pct Recovery = 100% Analysis Date = 09/09/16 Pct Recovery = 100% Analysis Date = 09/07/16 Pct Recovery = 100% Analysis Date = 09/07/16 Pct Recovery = 100% Analysis Date = 09/05/16 Pct Recovery = 100% Analysis Date = 09/05/16 Pct Recovery = 100% Analysis Date = 09/02/16 Pct Recovery = 100% Analysis Date = 09/02/16 Pct Recovery = 100% Analysis Date = 08/31/16 Pct Recovery = 100% Analysis Date = 08/31/16 Pct Recovery = 100% Analysis Date = 08/29/16 Pct Recovery = 100% Analysis Date = 08/29/16 Pct Recovery = 100% Analysis Date = 08/27/16 Pct Recovery = 100% Analysis Date = 08/27/16 Pct Recovery = 100% Analysis Date = 08/25/16 Pct Recovery = 100% Analysis Date = 08/25/16 Pct Recovery = 100% Analysis Date = 08/22/16 Pct Recovery = 100% Analysis Date = 08/22/16 Pct Recovery = 100% Analysis Date = 08/20/16 Pct Recovery = 100% Analysis Date = 08/20/16 Pct Recovery = 100% Analysis Date = 08/18/16 Pct Recovery = 100% Analysis Date = 08/18/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 99% Analysis Date = 08/16/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/12/16 Pct Recovery = 99% Analysis Date = 08/12/16 Pct Recovery = 99% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/07/16 Pct Recovery = 98% Analysis Date = 08/07/16 Pct Recovery = 98% Analysis Date = 08/05/16 Pct Recovery = 98% Analysis Date = 08/05/16 Pct Recovery = 98% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 08/03/16 Pct Recovery = 97% Analysis Date = 08/01/16 Pct Recovery = 97% Analysis Date = 08/01/16 Pct Recovery = 97% Analysis Date = 07/30/16 Pct Recovery = 97% Analysis Date = 07/30/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 97% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/25/16 Pct Recovery = 96% Analysis Date = 07/23/16 Pct Recovery = 96% Analysis Date = 07/23/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/21/16 Pct Recovery = 96% Analysis Date = 07/19/16 Pct Recovery = 95% Analysis Date = 07/19/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/14/16 Pct Recovery = 95% Analysis Date = 07/14/16 Pct Recovery = 95% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/12/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/10/16 Pct Recovery = 94% Analysis Date = 07/08/16 Pct Recovery = 94% Analysis Date = 07/08/16 Pct Recovery = 94% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/23/16 Pct Recovery = 92% Analysis Date = 06/23/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/18/16 Pct Recovery = 91% Analysis Date = 06/18/16 Pct Recovery = 91% Analysis Date = 06/16/16 Pct Recovery = 91% Analysis Date = 06/16/16 Pct Recovery = 91% Analysis Date = 06/14/16 Pct Recovery = 90% Analysis Date = 06/14/16 Pct Recovery = 90% Analysis Date = 06/12/16 Pct Recovery = 90% Analysis Date = 06/12/16 Pct Recovery = 90% Analysis Date = 06/10/16 Pct Recovery = 90% Analysis Date = 06/10/16 Pct Recovery = 90% Analysis Date = 06/07/16 Pct Recovery = 89% Analysis Date = 06/07/16 Pct Recovery = 89% Analysis Date = 06/05/16 Pct Recovery = 89% Analysis Date = 06/05/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 06/03/16 Pct Recovery = 89% Analysis Date = 06/01/16 Pct Recovery = 88% Analysis Date = 06/01/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/27/16 Pct Recovery = 88% Analysis Date = 05/27/16 Pct Recovery = 88% Analysis Date = 05/25/16 Pct Recovery = 88% Analysis Date = 05/25/16 Pct Recovery = 88% Analysis Date = 05/23/16 Pct Recovery = 87% Analysis Date = 05/23/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 86% Analysis Date = 05/14/16 Pct Recovery = 86% Analysis Date = 05/12/16 Pct Recovery = 86% Analysis Date = 05/12/16 Pct Recovery = 86% Analysis Date = 05/10/16 Pct Recovery = 86% Analysis Date = 05/10/16 Pct Recovery = 86% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/06/16 Pct Recovery = 85% Analysis Date = 05/06/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 05/04/16 Pct Recovery = 85% Analysis Date = 05/01/16 Pct Recovery = 85% Analysis Date = 05/01/16 Pct Recovery = 85% Analysis Date = 04/29/16 Pct Recovery = 84% Analysis Date = 04/29/16 Pct Recovery = 84% Analysis Date = 04/27/16 Pct Recovery = 84% Analysis Date = 04/27/16 Pct Recovery = 84% Analysis Date = 04/25/16 Pct Recovery = 84% Analysis Date = 04/25/16 Pct Recovery = 84% Analysis Date = 04/23/16 Pct Recovery = 83% Analysis Date = 04/23/16 Pct Recovery = 83% Analysis Date = 04/21/16 Pct Recovery = 83% Analysis Date = 04/21/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 82% Analysis Date = 04/16/16 Pct Recovery = 82% Analysis Date = 04/14/16 Pct Recovery = 82% Analysis Date = 04/14/16 Pct Recovery = 82% Analysis Date = 04/12/16 Pct Recovery = 82% Analysis Date = 04/12/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/10/16 Pct Recovery = 82% Analysis Date = 04/07/16 Pct Recovery = 81% Analysis Date = 04/07/16 Pct Recovery = 81% Analysis Date = 04/05/16 Pct Recovery = 81% Analysis Date = 04/05/16 Pct Recovery = 81% Analysis Date = 04/03/16 Pct Recovery = 81% Analysis Date = 04/03/16 Pct Recovery = 81% Analysis Date = 04/01/16 Pct Recovery = 80% Analysis Date = 04/01/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/30/16 Pct Recovery = 80% Analysis Date = 03/28/16 Pct Recovery = 80% Analysis Date = 03/28/16 Pct Recovery = 80% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/17/16 Pct Recovery = 78% Analysis Date = 03/17/16 Pct Recovery = 78% Analysis Date = 03/15/16 Pct Recovery = 78% Analysis Date = 03/15/16 Pct Recovery = 78% Analysis Date = 03/12/16 Pct Recovery = 77% Analysis Date = 03/12/16 Pct Recovery = 77% Analysis Date = 03/10/16 Pct Recovery = 77% Analysis Date = 03/10/16 Pct Recovery = 77% Analysis Date = 03/08/16 Pct Recovery = 77% Analysis Date = 03/08/16 Pct Recovery = 77% Analysis Date = 03/06/16 Pct Recovery = 76% Analysis Date = 03/06/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 03/04/16 Pct Recovery = 76% Analysis Date = 03/02/16 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
IPRODIONE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 92% 11% 92% 9%
Total 19 92% 11% 92% 9%

Sample Statistics
IPRODIONE

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
ISOFENPHOS
METHOD: 2033 , TESTIDCODE: 61594GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 106% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 88% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 84% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 74% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 98% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 107% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 74% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 100% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 128% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 103% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 94% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 93% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 87% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 70% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 05/10/17 Pct Recovery = 90% Analysis Date = 05/08/17 Pct Recovery = 91% Analysis Date = 05/08/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 05/06/17 Pct Recovery = 91% Analysis Date = 05/04/17 Pct Recovery = 91% Analysis Date = 05/04/17 Pct Recovery = 91% Analysis Date = 05/01/17 Pct Recovery = 92% Analysis Date = 05/01/17 Pct Recovery = 92% Analysis Date = 04/29/17 Pct Recovery = 92% Analysis Date = 04/29/17 Pct Recovery = 92% Analysis Date = 04/27/17 Pct Recovery = 92% Analysis Date = 04/27/17 Pct Recovery = 92% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/25/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/22/17 Pct Recovery = 93% Analysis Date = 04/20/17 Pct Recovery = 93% Analysis Date = 04/20/17 Pct Recovery = 93% Analysis Date = 04/18/17 Pct Recovery = 94% Analysis Date = 04/18/17 Pct Recovery = 94% Analysis Date = 04/15/17 Pct Recovery = 94% Analysis Date = 04/15/17 Pct Recovery = 94% Analysis Date = 04/13/17 Pct Recovery = 94% Analysis Date = 04/13/17 Pct Recovery = 94% Analysis Date = 04/11/17 Pct Recovery = 95% Analysis Date = 04/11/17 Pct Recovery = 95% Analysis Date = 04/09/17 Pct Recovery = 95% Analysis Date = 04/09/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/04/17 Pct Recovery = 96% Analysis Date = 04/04/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/28/17 Pct Recovery = 97% Analysis Date = 03/28/17 Pct Recovery = 97% Analysis Date = 03/26/17 Pct Recovery = 97% Analysis Date = 03/26/17 Pct Recovery = 97% Analysis Date = 03/24/17 Pct Recovery = 97% Analysis Date = 03/24/17 Pct Recovery = 97% Analysis Date = 03/21/17 Pct Recovery = 98% Analysis Date = 03/21/17 Pct Recovery = 98% Analysis Date = 03/19/17 Pct Recovery = 98% Analysis Date = 03/19/17 Pct Recovery = 98% Analysis Date = 03/17/17 Pct Recovery = 98% Analysis Date = 03/17/17 Pct Recovery = 98% Analysis Date = 03/14/17 Pct Recovery = 98% Analysis Date = 03/14/17 Pct Recovery = 98% Analysis Date = 03/12/17 Pct Recovery = 99% Analysis Date = 03/12/17 Pct Recovery = 99% Analysis Date = 03/10/17 Pct Recovery = 99% Analysis Date = 03/10/17 Pct Recovery = 99% Analysis Date = 03/08/17 Pct Recovery = 99% Analysis Date = 03/08/17 Pct Recovery = 99% Analysis Date = 03/05/17 Pct Recovery = 100% Analysis Date = 03/05/17 Pct Recovery = 100% Analysis Date = 03/03/17 Pct Recovery = 100% Analysis Date = 03/03/17 Pct Recovery = 100% Analysis Date = 03/01/17 Pct Recovery = 100% Analysis Date = 03/01/17 Pct Recovery = 100% Analysis Date = 02/26/17 Pct Recovery = 101% Analysis Date = 02/26/17 Pct Recovery = 101% Analysis Date = 02/24/17 Pct Recovery = 101% Analysis Date = 02/24/17 Pct Recovery = 101% Analysis Date = 02/22/17 Pct Recovery = 101% Analysis Date = 02/22/17 Pct Recovery = 101% Analysis Date = 02/20/17 Pct Recovery = 101% Analysis Date = 02/20/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/17/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/15/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/13/17 Pct Recovery = 101% Analysis Date = 02/10/17 Pct Recovery = 101% Analysis Date = 02/10/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 100% Analysis Date = 02/06/17 Pct Recovery = 100% Analysis Date = 02/04/17 Pct Recovery = 100% Analysis Date = 02/04/17 Pct Recovery = 100% Analysis Date = 02/01/17 Pct Recovery = 100% Analysis Date = 02/01/17 Pct Recovery = 100% Analysis Date = 01/30/17 Pct Recovery = 100% Analysis Date = 01/30/17 Pct Recovery = 100% Analysis Date = 01/28/17 Pct Recovery = 100% Analysis Date = 01/28/17 Pct Recovery = 100% Analysis Date = 01/25/17 Pct Recovery = 100% Analysis Date = 01/25/17 Pct Recovery = 100% Analysis Date = 01/23/17 Pct Recovery = 100% Analysis Date = 01/23/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 100% Analysis Date = 01/19/17 Pct Recovery = 100% Analysis Date = 01/19/17 Pct Recovery = 100% Analysis Date = 01/16/17 Pct Recovery = 100% Analysis Date = 01/16/17 Pct Recovery = 100% Analysis Date = 01/14/17 Pct Recovery = 100% Analysis Date = 01/14/17 Pct Recovery = 100% Analysis Date = 01/12/17 Pct Recovery = 100% Analysis Date = 01/12/17 Pct Recovery = 100% Analysis Date = 01/09/17 Pct Recovery = 100% Analysis Date = 01/09/17 Pct Recovery = 100% Analysis Date = 01/07/17 Pct Recovery = 100% Analysis Date = 01/07/17 Pct Recovery = 100% Analysis Date = 01/05/17 Pct Recovery = 100% Analysis Date = 01/05/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 100% Analysis Date = 12/29/16 Pct Recovery = 100% Analysis Date = 12/29/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/24/16 Pct Recovery = 100% Analysis Date = 12/24/16 Pct Recovery = 100% Analysis Date = 12/22/16 Pct Recovery = 100% Analysis Date = 12/22/16 Pct Recovery = 100% Analysis Date = 12/20/16 Pct Recovery = 100% Analysis Date = 12/20/16 Pct Recovery = 100% Analysis Date = 12/18/16 Pct Recovery = 100% Analysis Date = 12/18/16 Pct Recovery = 100% Analysis Date = 12/15/16 Pct Recovery = 100% Analysis Date = 12/15/16 Pct Recovery = 100% Analysis Date = 12/13/16 Pct Recovery = 100% Analysis Date = 12/13/16 Pct Recovery = 100% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/11/16 Pct Recovery = 100% Analysis Date = 12/08/16 Pct Recovery = 100% Analysis Date = 12/08/16 Pct Recovery = 100% Analysis Date = 12/06/16 Pct Recovery = 100% Analysis Date = 12/06/16 Pct Recovery = 100% Analysis Date = 12/04/16 Pct Recovery = 100% Analysis Date = 12/04/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 12/02/16 Pct Recovery = 100% Analysis Date = 11/29/16 Pct Recovery = 100% Analysis Date = 11/29/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/27/16 Pct Recovery = 100% Analysis Date = 11/25/16 Pct Recovery = 100% Analysis Date = 11/25/16 Pct Recovery = 100% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/20/16 Pct Recovery = 99% Analysis Date = 11/20/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/16/16 Pct Recovery = 99% Analysis Date = 11/16/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/11/16 Pct Recovery = 99% Analysis Date = 11/11/16 Pct Recovery = 99% Analysis Date = 11/09/16 Pct Recovery = 99% Analysis Date = 11/09/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 99% Analysis Date = 11/04/16 Pct Recovery = 99% Analysis Date = 11/04/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/28/16 Pct Recovery = 99% Analysis Date = 10/28/16 Pct Recovery = 99% Analysis Date = 10/26/16 Pct Recovery = 99% Analysis Date = 10/26/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/21/16 Pct Recovery = 99% Analysis Date = 10/21/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 99% Analysis Date = 09/24/16 Pct Recovery = 99% Analysis Date = 09/24/16 Pct Recovery = 99% Analysis Date = 09/22/16 Pct Recovery = 99% Analysis Date = 09/22/16 Pct Recovery = 99% Analysis Date = 09/19/16 Pct Recovery = 99% Analysis Date = 09/19/16 Pct Recovery = 99% Analysis Date = 09/17/16 Pct Recovery = 99% Analysis Date = 09/17/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/13/16 Pct Recovery = 99% Analysis Date = 09/13/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 99% Analysis Date = 09/08/16 Pct Recovery = 99% Analysis Date = 09/08/16 Pct Recovery = 99% Analysis Date = 09/06/16 Pct Recovery = 99% Analysis Date = 09/06/16 Pct Recovery = 99% Analysis Date = 09/03/16 Pct Recovery = 98% Analysis Date = 09/03/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 09/01/16 Pct Recovery = 98% Analysis Date = 08/30/16 Pct Recovery = 98% Analysis Date = 08/30/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/28/16 Pct Recovery = 98% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/25/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/23/16 Pct Recovery = 98% Analysis Date = 08/21/16 Pct Recovery = 97% Analysis Date = 08/21/16 Pct Recovery = 97% Analysis Date = 08/18/16 Pct Recovery = 97% Analysis Date = 08/18/16 Pct Recovery = 97% Analysis Date = 08/16/16 Pct Recovery = 97% Analysis Date = 08/16/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/14/16 Pct Recovery = 97% Analysis Date = 08/12/16 Pct Recovery = 96% Analysis Date = 08/12/16 Pct Recovery = 96% Analysis Date = 08/09/16 Pct Recovery = 96% Analysis Date = 08/09/16 Pct Recovery = 96% Analysis Date = 08/07/16 Pct Recovery = 96% Analysis Date = 08/07/16 Pct Recovery = 96% Analysis Date = 08/05/16 Pct Recovery = 96% Analysis Date = 08/05/16 Pct Recovery = 96% Analysis Date = 08/02/16 Pct Recovery = 96% Analysis Date = 08/02/16 Pct Recovery = 96% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/27/16 Pct Recovery = 95% Analysis Date = 07/27/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/24/16 Pct Recovery = 95% Analysis Date = 07/22/16 Pct Recovery = 94% Analysis Date = 07/22/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/20/16 Pct Recovery = 94% Analysis Date = 07/17/16 Pct Recovery = 94% Analysis Date = 07/17/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/15/16 Pct Recovery = 94% Analysis Date = 07/13/16 Pct Recovery = 94% Analysis Date = 07/13/16 Pct Recovery = 94% Analysis Date = 07/11/16 Pct Recovery = 93% Analysis Date = 07/11/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/08/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/06/16 Pct Recovery = 93% Analysis Date = 07/04/16 Pct Recovery = 93% Analysis Date = 07/04/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 07/01/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/29/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/27/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/25/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/22/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/20/16 Pct Recovery = 91% Analysis Date = 06/18/16 Pct Recovery = 91% Analysis Date = 06/18/16 Pct Recovery = 91% Analysis Date = 06/15/16 Pct Recovery = 91% Analysis Date = 06/15/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/13/16 Pct Recovery = 91% Analysis Date = 06/11/16 Pct Recovery = 90% Analysis Date = 06/11/16 Pct Recovery = 90% Analysis Date = 06/09/16 Pct Recovery = 90% Analysis Date = 06/09/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/06/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/04/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 89% Analysis Date = 06/02/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 89% Analysis Date = 05/28/16 Pct Recovery = 89% Analysis Date = 05/28/16 Pct Recovery = 89% Analysis Date = 05/26/16 Pct Recovery = 89% Analysis Date = 05/26/16 Pct Recovery = 89% Analysis Date = 05/24/16 Pct Recovery = 89% Analysis Date = 05/24/16 Pct Recovery = 89% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/19/16 Pct Recovery = 88% Analysis Date = 05/19/16 Pct Recovery = 88% Analysis Date = 05/17/16 Pct Recovery = 88% Analysis Date = 05/17/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 87% Analysis Date = 05/03/16 Pct Recovery = 87% Analysis Date = 05/03/16 Pct Recovery = 87% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/24/16 Pct Recovery = 86% Analysis Date = 04/24/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/19/16 Pct Recovery = 86% Analysis Date = 04/19/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/08/16 Pct Recovery = 85% Analysis Date = 04/08/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/18/16 Pct Recovery = 85% Analysis Date = 03/18/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/11/16 Pct Recovery = 85% Analysis Date = 03/11/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/05/16 Pct Recovery = 84% Analysis Date = 03/05/16 Pct Recovery = 84% Analysis Date = 03/02/16 Pct Recovery = 84% Analysis Date = 03/02/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 84% Analysis Date = 02/29/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/27/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/20/16 Pct Recovery = 84% Analysis Date = 02/20/16 Pct Recovery = 84% Analysis Date = 02/18/16 Pct Recovery = 84% Analysis Date = 02/18/16 Pct Recovery = 84% Analysis Date = 02/15/16 Pct Recovery = 84% Analysis Date = 02/15/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/11/16 Pct Recovery = 84% Analysis Date = 02/09/16 Pct Recovery = 84% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ISOFENPHOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 95% 15% 94% 12%
Total 18 95% 15% 94% 12%

Sample Statistics
ISOFENPHOS

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
MALAOXON
METHOD: 2033 , TESTIDCODE: 61652GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 87% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 104% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 44% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 52% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 100% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 90% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 92% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 120% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 91% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 125% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 68% Analysis Date = 05/02/17 Pct Recovery = 78% Analysis Date = 04/30/17 Pct Recovery = 79% Analysis Date = 04/30/17 Pct Recovery = 79% Analysis Date = 04/28/17 Pct Recovery = 79% Analysis Date = 04/28/17 Pct Recovery = 79% Analysis Date = 04/26/17 Pct Recovery = 80% Analysis Date = 04/26/17 Pct Recovery = 80% Analysis Date = 04/24/17 Pct Recovery = 80% Analysis Date = 04/24/17 Pct Recovery = 80% Analysis Date = 04/22/17 Pct Recovery = 81% Analysis Date = 04/22/17 Pct Recovery = 81% Analysis Date = 04/20/17 Pct Recovery = 81% Analysis Date = 04/20/17 Pct Recovery = 81% Analysis Date = 04/18/17 Pct Recovery = 82% Analysis Date = 04/18/17 Pct Recovery = 82% Analysis Date = 04/15/17 Pct Recovery = 83% Analysis Date = 04/15/17 Pct Recovery = 83% Analysis Date = 04/13/17 Pct Recovery = 83% Analysis Date = 04/13/17 Pct Recovery = 83% Analysis Date = 04/11/17 Pct Recovery = 84% Analysis Date = 04/11/17 Pct Recovery = 84% Analysis Date = 04/09/17 Pct Recovery = 84% Analysis Date = 04/09/17 Pct Recovery = 84% Analysis Date = 04/07/17 Pct Recovery = 85% Analysis Date = 04/07/17 Pct Recovery = 85% Analysis Date = 04/05/17 Pct Recovery = 85% Analysis Date = 04/05/17 Pct Recovery = 85% Analysis Date = 04/03/17 Pct Recovery = 86% Analysis Date = 04/03/17 Pct Recovery = 86% Analysis Date = 03/31/17 Pct Recovery = 87% Analysis Date = 03/31/17 Pct Recovery = 87% Analysis Date = 03/29/17 Pct Recovery = 87% Analysis Date = 03/29/17 Pct Recovery = 87% Analysis Date = 03/27/17 Pct Recovery = 88% Analysis Date = 03/27/17 Pct Recovery = 88% Analysis Date = 03/25/17 Pct Recovery = 88% Analysis Date = 03/25/17 Pct Recovery = 88% Analysis Date = 03/23/17 Pct Recovery = 89% Analysis Date = 03/23/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/14/17 Pct Recovery = 91% Analysis Date = 03/14/17 Pct Recovery = 91% Analysis Date = 03/12/17 Pct Recovery = 92% Analysis Date = 03/12/17 Pct Recovery = 92% Analysis Date = 03/10/17 Pct Recovery = 92% Analysis Date = 03/10/17 Pct Recovery = 92% Analysis Date = 03/08/17 Pct Recovery = 93% Analysis Date = 03/08/17 Pct Recovery = 93% Analysis Date = 03/06/17 Pct Recovery = 93% Analysis Date = 03/06/17 Pct Recovery = 93% Analysis Date = 03/04/17 Pct Recovery = 94% Analysis Date = 03/04/17 Pct Recovery = 94% Analysis Date = 03/02/17 Pct Recovery = 95% Analysis Date = 03/02/17 Pct Recovery = 95% Analysis Date = 02/27/17 Pct Recovery = 95% Analysis Date = 02/27/17 Pct Recovery = 95% Analysis Date = 02/25/17 Pct Recovery = 96% Analysis Date = 02/25/17 Pct Recovery = 96% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/23/17 Pct Recovery = 97% Analysis Date = 02/21/17 Pct Recovery = 97% Analysis Date = 02/21/17 Pct Recovery = 97% Analysis Date = 02/19/17 Pct Recovery = 98% Analysis Date = 02/19/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 99% Analysis Date = 02/15/17 Pct Recovery = 99% Analysis Date = 02/13/17 Pct Recovery = 100% Analysis Date = 02/13/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/08/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 101% Analysis Date = 02/06/17 Pct Recovery = 101% Analysis Date = 02/04/17 Pct Recovery = 102% Analysis Date = 02/04/17 Pct Recovery = 102% Analysis Date = 02/02/17 Pct Recovery = 102% Analysis Date = 02/02/17 Pct Recovery = 102% Analysis Date = 01/31/17 Pct Recovery = 103% Analysis Date = 01/31/17 Pct Recovery = 103% Analysis Date = 01/29/17 Pct Recovery = 104% Analysis Date = 01/29/17 Pct Recovery = 104% Analysis Date = 01/26/17 Pct Recovery = 104% Analysis Date = 01/26/17 Pct Recovery = 104% Analysis Date = 01/24/17 Pct Recovery = 105% Analysis Date = 01/24/17 Pct Recovery = 105% Analysis Date = 01/22/17 Pct Recovery = 105% Analysis Date = 01/22/17 Pct Recovery = 105% Analysis Date = 01/20/17 Pct Recovery = 106% Analysis Date = 01/20/17 Pct Recovery = 106% Analysis Date = 01/18/17 Pct Recovery = 106% Analysis Date = 01/18/17 Pct Recovery = 106% Analysis Date = 01/16/17 Pct Recovery = 107% Analysis Date = 01/16/17 Pct Recovery = 107% Analysis Date = 01/14/17 Pct Recovery = 108% Analysis Date = 01/14/17 Pct Recovery = 108% Analysis Date = 01/11/17 Pct Recovery = 108% Analysis Date = 01/11/17 Pct Recovery = 108% Analysis Date = 01/09/17 Pct Recovery = 109% Analysis Date = 01/09/17 Pct Recovery = 109% Analysis Date = 01/07/17 Pct Recovery = 109% Analysis Date = 01/07/17 Pct Recovery = 109% Analysis Date = 01/05/17 Pct Recovery = 110% Analysis Date = 01/05/17 Pct Recovery = 110% Analysis Date = 01/03/17 Pct Recovery = 110% Analysis Date = 01/03/17 Pct Recovery = 110% Analysis Date = 01/01/17 Pct Recovery = 111% Analysis Date = 01/01/17 Pct Recovery = 111% Analysis Date = 12/30/16 Pct Recovery = 112% Analysis Date = 12/30/16 Pct Recovery = 112% Analysis Date = 12/28/16 Pct Recovery = 112% Analysis Date = 12/28/16 Pct Recovery = 112% Analysis Date = 12/25/16 Pct Recovery = 113% Analysis Date = 12/25/16 Pct Recovery = 113% Analysis Date = 12/23/16 Pct Recovery = 113% Analysis Date = 12/23/16 Pct Recovery = 113% Analysis Date = 12/21/16 Pct Recovery = 114% Analysis Date = 12/21/16 Pct Recovery = 114% Analysis Date = 12/19/16 Pct Recovery = 114% Analysis Date = 12/19/16 Pct Recovery = 114% Analysis Date = 12/17/16 Pct Recovery = 114% Analysis Date = 12/17/16 Pct Recovery = 114% Analysis Date = 12/15/16 Pct Recovery = 113% Analysis Date = 12/15/16 Pct Recovery = 113% Analysis Date = 12/13/16 Pct Recovery = 112% Analysis Date = 12/13/16 Pct Recovery = 112% Analysis Date = 12/10/16 Pct Recovery = 111% Analysis Date = 12/10/16 Pct Recovery = 111% Analysis Date = 12/08/16 Pct Recovery = 111% Analysis Date = 12/08/16 Pct Recovery = 111% Analysis Date = 12/06/16 Pct Recovery = 110% Analysis Date = 12/06/16 Pct Recovery = 110% Analysis Date = 12/04/16 Pct Recovery = 109% Analysis Date = 12/04/16 Pct Recovery = 109% Analysis Date = 12/02/16 Pct Recovery = 109% Analysis Date = 12/02/16 Pct Recovery = 109% Analysis Date = 11/30/16 Pct Recovery = 108% Analysis Date = 11/30/16 Pct Recovery = 108% Analysis Date = 11/28/16 Pct Recovery = 107% Analysis Date = 11/28/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/26/16 Pct Recovery = 107% Analysis Date = 11/23/16 Pct Recovery = 106% Analysis Date = 11/23/16 Pct Recovery = 106% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/21/16 Pct Recovery = 105% Analysis Date = 11/19/16 Pct Recovery = 105% Analysis Date = 11/19/16 Pct Recovery = 105% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/17/16 Pct Recovery = 104% Analysis Date = 11/15/16 Pct Recovery = 103% Analysis Date = 11/15/16 Pct Recovery = 103% Analysis Date = 11/13/16 Pct Recovery = 103% Analysis Date = 11/13/16 Pct Recovery = 103% Analysis Date = 11/11/16 Pct Recovery = 102% Analysis Date = 11/11/16 Pct Recovery = 102% Analysis Date = 11/08/16 Pct Recovery = 101% Analysis Date = 11/08/16 Pct Recovery = 101% Analysis Date = 11/06/16 Pct Recovery = 101% Analysis Date = 11/06/16 Pct Recovery = 101% Analysis Date = 11/04/16 Pct Recovery = 100% Analysis Date = 11/04/16 Pct Recovery = 100% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/29/16 Pct Recovery = 98% Analysis Date = 10/29/16 Pct Recovery = 98% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/27/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 97% Analysis Date = 10/22/16 Pct Recovery = 96% Analysis Date = 10/22/16 Pct Recovery = 96% Analysis Date = 10/20/16 Pct Recovery = 95% Analysis Date = 10/20/16 Pct Recovery = 95% Analysis Date = 10/18/16 Pct Recovery = 95% Analysis Date = 10/18/16 Pct Recovery = 95% Analysis Date = 10/16/16 Pct Recovery = 94% Analysis Date = 10/16/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/10/16 Pct Recovery = 92% Analysis Date = 10/07/16 Pct Recovery = 91% Analysis Date = 10/07/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/05/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 10/01/16 Pct Recovery = 89% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/27/16 Pct Recovery = 88% Analysis Date = 09/27/16 Pct Recovery = 88% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/22/16 Pct Recovery = 86% Analysis Date = 09/22/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/20/16 Pct Recovery = 86% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/18/16 Pct Recovery = 85% Analysis Date = 09/16/16 Pct Recovery = 84% Analysis Date = 09/16/16 Pct Recovery = 84% Analysis Date = 09/14/16 Pct Recovery = 84% Analysis Date = 09/14/16 Pct Recovery = 84% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/12/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 82% Analysis Date = 09/05/16 Pct Recovery = 81% Analysis Date = 09/05/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 80% Analysis Date = 09/03/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 09/01/16 Pct Recovery = 80% Analysis Date = 08/30/16 Pct Recovery = 80% Analysis Date = 08/30/16 Pct Recovery = 80% Analysis Date = 08/28/16 Pct Recovery = 80% Analysis Date = 08/28/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 80% Analysis Date = 08/26/16 Pct Recovery = 80% Analysis Date = 08/24/16 Pct Recovery = 80% Analysis Date = 08/24/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 80% Analysis Date = 08/21/16 Pct Recovery = 80% Analysis Date = 08/19/16 Pct Recovery = 80% Analysis Date = 08/19/16 Pct Recovery = 80% Analysis Date = 08/17/16 Pct Recovery = 80% Analysis Date = 08/17/16 Pct Recovery = 80% Analysis Date = 08/15/16 Pct Recovery = 80% Analysis Date = 08/15/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/13/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/11/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/06/16 Pct Recovery = 80% Analysis Date = 08/06/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 08/04/16 Pct Recovery = 80% Analysis Date = 08/02/16 Pct Recovery = 80% Analysis Date = 08/02/16 Pct Recovery = 80% Analysis Date = 07/31/16 Pct Recovery = 80% Analysis Date = 07/31/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/29/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/27/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/25/16 Pct Recovery = 80% Analysis Date = 07/23/16 Pct Recovery = 80% Analysis Date = 07/23/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/20/16 Pct Recovery = 80% Analysis Date = 07/18/16 Pct Recovery = 80% Analysis Date = 07/18/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 80% Analysis Date = 07/16/16 Pct Recovery = 80% Analysis Date = 07/14/16 Pct Recovery = 80% Analysis Date = 07/14/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 80% Analysis Date = 07/12/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/10/16 Pct Recovery = 80% Analysis Date = 07/08/16 Pct Recovery = 80% Analysis Date = 07/08/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 07/05/16 Pct Recovery = 80% Analysis Date = 07/03/16 Pct Recovery = 80% Analysis Date = 07/03/16 Pct Recovery = 80% Analysis Date = 07/01/16 Pct Recovery = 81% Analysis Date = 07/01/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 81% Analysis Date = 06/23/16 Pct Recovery = 81% Analysis Date = 06/23/16 Pct Recovery = 81% Analysis Date = 06/21/16 Pct Recovery = 81% Analysis Date = 06/21/16 Pct Recovery = 81% Analysis Date = 06/18/16 Pct Recovery = 81% Analysis Date = 06/18/16 Pct Recovery = 81% Analysis Date = 06/16/16 Pct Recovery = 81% Analysis Date = 06/16/16 Pct Recovery = 81% Analysis Date = 06/14/16 Pct Recovery = 81% Analysis Date = 06/14/16 Pct Recovery = 81% Analysis Date = 06/12/16 Pct Recovery = 81% Analysis Date = 06/12/16 Pct Recovery = 81% Analysis Date = 06/10/16 Pct Recovery = 81% Analysis Date = 06/10/16 Pct Recovery = 81% Analysis Date = 06/08/16 Pct Recovery = 81% Analysis Date = 06/08/16 Pct Recovery = 81% Analysis Date = 06/06/16 Pct Recovery = 81% Analysis Date = 06/06/16 Pct Recovery = 81% Analysis Date = 06/03/16 Pct Recovery = 81% Analysis Date = 06/03/16 Pct Recovery = 81% Analysis Date = 06/01/16 Pct Recovery = 81% Analysis Date = 06/01/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/30/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/28/16 Pct Recovery = 81% Analysis Date = 05/26/16 Pct Recovery = 81% Analysis Date = 05/26/16 Pct Recovery = 81% Analysis Date = 05/24/16 Pct Recovery = 81% Analysis Date = 05/24/16 Pct Recovery = 81% Analysis Date = 05/22/16 Pct Recovery = 82% Analysis Date = 05/22/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/17/16 Pct Recovery = 82% Analysis Date = 05/17/16 Pct Recovery = 82% Analysis Date = 05/15/16 Pct Recovery = 82% Analysis Date = 05/15/16 Pct Recovery = 82% Analysis Date = 05/13/16 Pct Recovery = 82% Analysis Date = 05/13/16 Pct Recovery = 82% Analysis Date = 05/11/16 Pct Recovery = 82% Analysis Date = 05/11/16 Pct Recovery = 82% Analysis Date = 05/09/16 Pct Recovery = 82% Analysis Date = 05/09/16 Pct Recovery = 82% Analysis Date = 05/07/16 Pct Recovery = 81% Analysis Date = 05/07/16 Pct Recovery = 81% Analysis Date = 05/05/16 Pct Recovery = 81% Analysis Date = 05/05/16 Pct Recovery = 81% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 05/02/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/30/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/26/16 Pct Recovery = 81% Analysis Date = 04/26/16 Pct Recovery = 81% Analysis Date = 04/24/16 Pct Recovery = 81% Analysis Date = 04/24/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 81% Analysis Date = 04/20/16 Pct Recovery = 81% Analysis Date = 04/20/16 Pct Recovery = 81% Analysis Date = 04/17/16 Pct Recovery = 81% Analysis Date = 04/17/16 Pct Recovery = 81% Analysis Date = 04/15/16 Pct Recovery = 81% Analysis Date = 04/15/16 Pct Recovery = 81% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/13/16 Pct Recovery = 80% Analysis Date = 04/11/16 Pct Recovery = 80% Analysis Date = 04/11/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 04/09/16 Pct Recovery = 80% Analysis Date = 04/07/16 Pct Recovery = 80% Analysis Date = 04/07/16 Pct Recovery = 80% Analysis Date = 04/05/16 Pct Recovery = 80% Analysis Date = 04/05/16 Pct Recovery = 80% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 04/03/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/31/16 Pct Recovery = 79% Analysis Date = 03/29/16 Pct Recovery = 79% Analysis Date = 03/29/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 78% Analysis Date = 03/23/16 Pct Recovery = 78% Analysis Date = 03/21/16 Pct Recovery = 78% Analysis Date = 03/21/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/19/16 Pct Recovery = 78% Analysis Date = 03/16/16 Pct Recovery = 78% Analysis Date = 03/16/16 Pct Recovery = 78% Analysis Date = 03/14/16 Pct Recovery = 78% Analysis Date = 03/14/16 Pct Recovery = 78% Analysis Date = 03/12/16 Pct Recovery = 77% Analysis Date = 03/12/16 Pct Recovery = 77% Analysis Date = 03/10/16 Pct Recovery = 77% Analysis Date = 03/10/16 Pct Recovery = 77% Analysis Date = 03/08/16 Pct Recovery = 77% Analysis Date = 03/08/16 Pct Recovery = 77% Analysis Date = 03/06/16 Pct Recovery = 77% Analysis Date = 03/06/16 Pct Recovery = 77% Analysis Date = 03/04/16 Pct Recovery = 77% Analysis Date = 03/04/16 Pct Recovery = 77% Analysis Date = 03/02/16 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALAOXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 86% 21% 89% 20%
Total 18 86% 21% 89% 20%

Sample Statistics
MALAOXON

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
MALATHION
METHOD: 2033 , TESTIDCODE: 39532GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 89% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 87% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 119% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 105% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 90% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 90% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 91% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 104% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 78% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 100% Analysis Date = 05/10/17 Pct Recovery = 90% Analysis Date = 05/08/17 Pct Recovery = 90% Analysis Date = 05/08/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/04/17 Pct Recovery = 90% Analysis Date = 05/04/17 Pct Recovery = 90% Analysis Date = 05/01/17 Pct Recovery = 90% Analysis Date = 05/01/17 Pct Recovery = 90% Analysis Date = 04/29/17 Pct Recovery = 90% Analysis Date = 04/29/17 Pct Recovery = 90% Analysis Date = 04/27/17 Pct Recovery = 90% Analysis Date = 04/27/17 Pct Recovery = 90% Analysis Date = 04/25/17 Pct Recovery = 90% Analysis Date = 04/25/17 Pct Recovery = 90% Analysis Date = 04/22/17 Pct Recovery = 90% Analysis Date = 04/22/17 Pct Recovery = 90% Analysis Date = 04/20/17 Pct Recovery = 90% Analysis Date = 04/20/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/18/17 Pct Recovery = 90% Analysis Date = 04/15/17 Pct Recovery = 90% Analysis Date = 04/15/17 Pct Recovery = 90% Analysis Date = 04/13/17 Pct Recovery = 90% Analysis Date = 04/13/17 Pct Recovery = 90% Analysis Date = 04/11/17 Pct Recovery = 90% Analysis Date = 04/11/17 Pct Recovery = 90% Analysis Date = 04/09/17 Pct Recovery = 90% Analysis Date = 04/09/17 Pct Recovery = 90% Analysis Date = 04/06/17 Pct Recovery = 90% Analysis Date = 04/06/17 Pct Recovery = 90% Analysis Date = 04/04/17 Pct Recovery = 89% Analysis Date = 04/04/17 Pct Recovery = 89% Analysis Date = 04/02/17 Pct Recovery = 89% Analysis Date = 04/02/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 89% Analysis Date = 03/10/17 Pct Recovery = 89% Analysis Date = 03/10/17 Pct Recovery = 89% Analysis Date = 03/08/17 Pct Recovery = 89% Analysis Date = 03/08/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/03/17 Pct Recovery = 89% Analysis Date = 03/03/17 Pct Recovery = 89% Analysis Date = 03/01/17 Pct Recovery = 89% Analysis Date = 03/01/17 Pct Recovery = 89% Analysis Date = 02/26/17 Pct Recovery = 89% Analysis Date = 02/26/17 Pct Recovery = 89% Analysis Date = 02/24/17 Pct Recovery = 89% Analysis Date = 02/24/17 Pct Recovery = 89% Analysis Date = 02/22/17 Pct Recovery = 89% Analysis Date = 02/22/17 Pct Recovery = 89% Analysis Date = 02/20/17 Pct Recovery = 89% Analysis Date = 02/20/17 Pct Recovery = 89% Analysis Date = 02/17/17 Pct Recovery = 89% Analysis Date = 02/17/17 Pct Recovery = 89% Analysis Date = 02/15/17 Pct Recovery = 89% Analysis Date = 02/15/17 Pct Recovery = 89% Analysis Date = 02/13/17 Pct Recovery = 89% Analysis Date = 02/13/17 Pct Recovery = 89% Analysis Date = 02/10/17 Pct Recovery = 89% Analysis Date = 02/10/17 Pct Recovery = 89% Analysis Date = 02/08/17 Pct Recovery = 89% Analysis Date = 02/08/17 Pct Recovery = 89% Analysis Date = 02/06/17 Pct Recovery = 89% Analysis Date = 02/06/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/01/17 Pct Recovery = 89% Analysis Date = 02/01/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/25/17 Pct Recovery = 89% Analysis Date = 01/23/17 Pct Recovery = 89% Analysis Date = 01/23/17 Pct Recovery = 89% Analysis Date = 01/21/17 Pct Recovery = 89% Analysis Date = 01/21/17 Pct Recovery = 89% Analysis Date = 01/19/17 Pct Recovery = 89% Analysis Date = 01/19/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/12/17 Pct Recovery = 89% Analysis Date = 01/12/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 90% Analysis Date = 01/05/17 Pct Recovery = 90% Analysis Date = 01/03/17 Pct Recovery = 90% Analysis Date = 01/03/17 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 91% Analysis Date = 12/22/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/20/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/13/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/11/16 Pct Recovery = 92% Analysis Date = 12/08/16 Pct Recovery = 92% Analysis Date = 12/08/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 92% Analysis Date = 12/06/16 Pct Recovery = 92% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 12/04/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 93% Analysis Date = 12/02/16 Pct Recovery = 93% Analysis Date = 11/29/16 Pct Recovery = 93% Analysis Date = 11/29/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/27/16 Pct Recovery = 93% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 95% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 97% Analysis Date = 10/31/16 Pct Recovery = 97% Analysis Date = 10/28/16 Pct Recovery = 97% Analysis Date = 10/28/16 Pct Recovery = 97% Analysis Date = 10/26/16 Pct Recovery = 97% Analysis Date = 10/26/16 Pct Recovery = 97% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/24/16 Pct Recovery = 98% Analysis Date = 10/21/16 Pct Recovery = 98% Analysis Date = 10/21/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/19/16 Pct Recovery = 98% Analysis Date = 10/17/16 Pct Recovery = 98% Analysis Date = 10/17/16 Pct Recovery = 98% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 100% Analysis Date = 10/05/16 Pct Recovery = 100% Analysis Date = 10/03/16 Pct Recovery = 100% Analysis Date = 10/03/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 10/01/16 Pct Recovery = 100% Analysis Date = 09/29/16 Pct Recovery = 100% Analysis Date = 09/29/16 Pct Recovery = 100% Analysis Date = 09/26/16 Pct Recovery = 101% Analysis Date = 09/26/16 Pct Recovery = 101% Analysis Date = 09/24/16 Pct Recovery = 101% Analysis Date = 09/24/16 Pct Recovery = 101% Analysis Date = 09/22/16 Pct Recovery = 101% Analysis Date = 09/22/16 Pct Recovery = 101% Analysis Date = 09/19/16 Pct Recovery = 102% Analysis Date = 09/19/16 Pct Recovery = 102% Analysis Date = 09/17/16 Pct Recovery = 102% Analysis Date = 09/17/16 Pct Recovery = 102% Analysis Date = 09/15/16 Pct Recovery = 102% Analysis Date = 09/15/16 Pct Recovery = 102% Analysis Date = 09/13/16 Pct Recovery = 102% Analysis Date = 09/13/16 Pct Recovery = 102% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/10/16 Pct Recovery = 103% Analysis Date = 09/08/16 Pct Recovery = 103% Analysis Date = 09/08/16 Pct Recovery = 103% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/06/16 Pct Recovery = 102% Analysis Date = 09/03/16 Pct Recovery = 102% Analysis Date = 09/03/16 Pct Recovery = 102% Analysis Date = 09/01/16 Pct Recovery = 102% Analysis Date = 09/01/16 Pct Recovery = 102% Analysis Date = 08/30/16 Pct Recovery = 101% Analysis Date = 08/30/16 Pct Recovery = 101% Analysis Date = 08/28/16 Pct Recovery = 101% Analysis Date = 08/28/16 Pct Recovery = 101% Analysis Date = 08/25/16 Pct Recovery = 100% Analysis Date = 08/25/16 Pct Recovery = 100% Analysis Date = 08/23/16 Pct Recovery = 100% Analysis Date = 08/23/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 99% Analysis Date = 08/21/16 Pct Recovery = 99% Analysis Date = 08/18/16 Pct Recovery = 99% Analysis Date = 08/18/16 Pct Recovery = 99% Analysis Date = 08/16/16 Pct Recovery = 99% Analysis Date = 08/16/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/14/16 Pct Recovery = 99% Analysis Date = 08/12/16 Pct Recovery = 98% Analysis Date = 08/12/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/09/16 Pct Recovery = 98% Analysis Date = 08/07/16 Pct Recovery = 98% Analysis Date = 08/07/16 Pct Recovery = 98% Analysis Date = 08/05/16 Pct Recovery = 98% Analysis Date = 08/05/16 Pct Recovery = 98% Analysis Date = 08/02/16 Pct Recovery = 97% Analysis Date = 08/02/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/31/16 Pct Recovery = 97% Analysis Date = 07/29/16 Pct Recovery = 97% Analysis Date = 07/29/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 97% Analysis Date = 07/27/16 Pct Recovery = 97% Analysis Date = 07/24/16 Pct Recovery = 96% Analysis Date = 07/24/16 Pct Recovery = 96% Analysis Date = 07/22/16 Pct Recovery = 96% Analysis Date = 07/22/16 Pct Recovery = 96% Analysis Date = 07/20/16 Pct Recovery = 96% Analysis Date = 07/20/16 Pct Recovery = 96% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/17/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/15/16 Pct Recovery = 95% Analysis Date = 07/13/16 Pct Recovery = 95% Analysis Date = 07/13/16 Pct Recovery = 95% Analysis Date = 07/11/16 Pct Recovery = 95% Analysis Date = 07/11/16 Pct Recovery = 95% Analysis Date = 07/08/16 Pct Recovery = 94% Analysis Date = 07/08/16 Pct Recovery = 94% Analysis Date = 07/06/16 Pct Recovery = 94% Analysis Date = 07/06/16 Pct Recovery = 94% Analysis Date = 07/04/16 Pct Recovery = 94% Analysis Date = 07/04/16 Pct Recovery = 94% Analysis Date = 07/01/16 Pct Recovery = 94% Analysis Date = 07/01/16 Pct Recovery = 94% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/22/16 Pct Recovery = 93% Analysis Date = 06/20/16 Pct Recovery = 92% Analysis Date = 06/20/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/18/16 Pct Recovery = 92% Analysis Date = 06/15/16 Pct Recovery = 92% Analysis Date = 06/15/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/13/16 Pct Recovery = 92% Analysis Date = 06/11/16 Pct Recovery = 91% Analysis Date = 06/11/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/09/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/06/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/04/16 Pct Recovery = 91% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 06/02/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/30/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/28/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/26/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/24/16 Pct Recovery = 90% Analysis Date = 05/21/16 Pct Recovery = 90% Analysis Date = 05/21/16 Pct Recovery = 90% Analysis Date = 05/19/16 Pct Recovery = 90% Analysis Date = 05/19/16 Pct Recovery = 90% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/17/16 Pct Recovery = 89% Analysis Date = 05/14/16 Pct Recovery = 89% Analysis Date = 05/14/16 Pct Recovery = 89% Analysis Date = 05/12/16 Pct Recovery = 89% Analysis Date = 05/12/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/10/16 Pct Recovery = 89% Analysis Date = 05/08/16 Pct Recovery = 89% Analysis Date = 05/08/16 Pct Recovery = 89% Analysis Date = 05/05/16 Pct Recovery = 89% Analysis Date = 05/05/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/28/16 Pct Recovery = 89% Analysis Date = 04/28/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/17/16 Pct Recovery = 88% Analysis Date = 04/17/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/12/16 Pct Recovery = 88% Analysis Date = 04/12/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/08/16 Pct Recovery = 88% Analysis Date = 04/08/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 88% Analysis Date = 03/30/16 Pct Recovery = 88% Analysis Date = 03/30/16 Pct Recovery = 88% Analysis Date = 03/27/16 Pct Recovery = 88% Analysis Date = 03/27/16 Pct Recovery = 88% Analysis Date = 03/25/16 Pct Recovery = 88% Analysis Date = 03/25/16 Pct Recovery = 88% Analysis Date = 03/23/16 Pct Recovery = 88% Analysis Date = 03/23/16 Pct Recovery = 88% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/18/16 Pct Recovery = 87% Analysis Date = 03/18/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/14/16 Pct Recovery = 87% Analysis Date = 03/14/16 Pct Recovery = 87% Analysis Date = 03/11/16 Pct Recovery = 87% Analysis Date = 03/11/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/05/16 Pct Recovery = 87% Analysis Date = 03/05/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 02/29/16 Pct Recovery = 87% Analysis Date = 02/29/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/22/16 Pct Recovery = 87% Analysis Date = 02/22/16 Pct Recovery = 87% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/09/16 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MALATHION

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 16 92% 11% 90% 6%
Total 16 92% 11% 90% 6%

Sample Statistics
MALATHION

Characteristic N % % Basis
Plotted 16 84% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 3 16% 3 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
METALAXYL
METHOD: 2033 , TESTIDCODE: 61596GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 107% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 126% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 97% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 91% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 72% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 106% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 73% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 93% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 118% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 87% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 90% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 96% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 76% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 92% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 88% Analysis Date = 05/10/17 Pct Recovery = 94% Analysis Date = 05/08/17 Pct Recovery = 94% Analysis Date = 05/08/17 Pct Recovery = 94% Analysis Date = 05/06/17 Pct Recovery = 94% Analysis Date = 05/06/17 Pct Recovery = 94% Analysis Date = 05/04/17 Pct Recovery = 94% Analysis Date = 05/04/17 Pct Recovery = 94% Analysis Date = 05/01/17 Pct Recovery = 94% Analysis Date = 05/01/17 Pct Recovery = 94% Analysis Date = 04/29/17 Pct Recovery = 94% Analysis Date = 04/29/17 Pct Recovery = 94% Analysis Date = 04/27/17 Pct Recovery = 94% Analysis Date = 04/27/17 Pct Recovery = 94% Analysis Date = 04/25/17 Pct Recovery = 95% Analysis Date = 04/25/17 Pct Recovery = 95% Analysis Date = 04/22/17 Pct Recovery = 95% Analysis Date = 04/22/17 Pct Recovery = 95% Analysis Date = 04/20/17 Pct Recovery = 95% Analysis Date = 04/20/17 Pct Recovery = 95% Analysis Date = 04/18/17 Pct Recovery = 95% Analysis Date = 04/18/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/13/17 Pct Recovery = 95% Analysis Date = 04/13/17 Pct Recovery = 95% Analysis Date = 04/11/17 Pct Recovery = 95% Analysis Date = 04/11/17 Pct Recovery = 95% Analysis Date = 04/09/17 Pct Recovery = 95% Analysis Date = 04/09/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/04/17 Pct Recovery = 96% Analysis Date = 04/04/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/28/17 Pct Recovery = 96% Analysis Date = 03/28/17 Pct Recovery = 96% Analysis Date = 03/26/17 Pct Recovery = 96% Analysis Date = 03/26/17 Pct Recovery = 96% Analysis Date = 03/24/17 Pct Recovery = 96% Analysis Date = 03/24/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 97% Analysis Date = 03/10/17 Pct Recovery = 97% Analysis Date = 03/10/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/05/17 Pct Recovery = 97% Analysis Date = 03/05/17 Pct Recovery = 97% Analysis Date = 03/03/17 Pct Recovery = 97% Analysis Date = 03/03/17 Pct Recovery = 97% Analysis Date = 03/01/17 Pct Recovery = 97% Analysis Date = 03/01/17 Pct Recovery = 97% Analysis Date = 02/26/17 Pct Recovery = 97% Analysis Date = 02/26/17 Pct Recovery = 97% Analysis Date = 02/24/17 Pct Recovery = 97% Analysis Date = 02/24/17 Pct Recovery = 97% Analysis Date = 02/22/17 Pct Recovery = 97% Analysis Date = 02/22/17 Pct Recovery = 97% Analysis Date = 02/20/17 Pct Recovery = 97% Analysis Date = 02/20/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/17/17 Pct Recovery = 97% Analysis Date = 02/15/17 Pct Recovery = 96% Analysis Date = 02/15/17 Pct Recovery = 96% Analysis Date = 02/13/17 Pct Recovery = 96% Analysis Date = 02/13/17 Pct Recovery = 96% Analysis Date = 02/10/17 Pct Recovery = 96% Analysis Date = 02/10/17 Pct Recovery = 96% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/06/17 Pct Recovery = 95% Analysis Date = 02/06/17 Pct Recovery = 95% Analysis Date = 02/04/17 Pct Recovery = 95% Analysis Date = 02/04/17 Pct Recovery = 95% Analysis Date = 02/01/17 Pct Recovery = 94% Analysis Date = 02/01/17 Pct Recovery = 94% Analysis Date = 01/30/17 Pct Recovery = 94% Analysis Date = 01/30/17 Pct Recovery = 94% Analysis Date = 01/28/17 Pct Recovery = 94% Analysis Date = 01/28/17 Pct Recovery = 94% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/25/17 Pct Recovery = 93% Analysis Date = 01/23/17 Pct Recovery = 93% Analysis Date = 01/23/17 Pct Recovery = 93% Analysis Date = 01/21/17 Pct Recovery = 93% Analysis Date = 01/21/17 Pct Recovery = 93% Analysis Date = 01/19/17 Pct Recovery = 92% Analysis Date = 01/19/17 Pct Recovery = 92% Analysis Date = 01/16/17 Pct Recovery = 92% Analysis Date = 01/16/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 92% Analysis Date = 01/12/17 Pct Recovery = 92% Analysis Date = 01/12/17 Pct Recovery = 92% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 93% Analysis Date = 12/20/16 Pct Recovery = 93% Analysis Date = 12/20/16 Pct Recovery = 93% Analysis Date = 12/18/16 Pct Recovery = 93% Analysis Date = 12/18/16 Pct Recovery = 93% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/15/16 Pct Recovery = 93% Analysis Date = 12/13/16 Pct Recovery = 93% Analysis Date = 12/13/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/11/16 Pct Recovery = 93% Analysis Date = 12/08/16 Pct Recovery = 93% Analysis Date = 12/08/16 Pct Recovery = 93% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 94% Analysis Date = 11/29/16 Pct Recovery = 94% Analysis Date = 11/29/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/27/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/25/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/22/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/20/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/18/16 Pct Recovery = 94% Analysis Date = 11/16/16 Pct Recovery = 94% Analysis Date = 11/16/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/13/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/11/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/09/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/06/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/04/16 Pct Recovery = 94% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 11/02/16 Pct Recovery = 95% Analysis Date = 10/31/16 Pct Recovery = 95% Analysis Date = 10/31/16 Pct Recovery = 95% Analysis Date = 10/28/16 Pct Recovery = 95% Analysis Date = 10/28/16 Pct Recovery = 95% Analysis Date = 10/26/16 Pct Recovery = 95% Analysis Date = 10/26/16 Pct Recovery = 95% Analysis Date = 10/24/16 Pct Recovery = 95% Analysis Date = 10/24/16 Pct Recovery = 95% Analysis Date = 10/21/16 Pct Recovery = 95% Analysis Date = 10/21/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 95% Analysis Date = 10/19/16 Pct Recovery = 95% Analysis Date = 10/17/16 Pct Recovery = 95% Analysis Date = 10/17/16 Pct Recovery = 95% Analysis Date = 10/15/16 Pct Recovery = 95% Analysis Date = 10/15/16 Pct Recovery = 95% Analysis Date = 10/12/16 Pct Recovery = 95% Analysis Date = 10/12/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/10/16 Pct Recovery = 95% Analysis Date = 10/08/16 Pct Recovery = 95% Analysis Date = 10/08/16 Pct Recovery = 95% Analysis Date = 10/05/16 Pct Recovery = 95% Analysis Date = 10/05/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/29/16 Pct Recovery = 96% Analysis Date = 09/26/16 Pct Recovery = 96% Analysis Date = 09/26/16 Pct Recovery = 96% Analysis Date = 09/24/16 Pct Recovery = 96% Analysis Date = 09/24/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/19/16 Pct Recovery = 96% Analysis Date = 09/19/16 Pct Recovery = 96% Analysis Date = 09/17/16 Pct Recovery = 96% Analysis Date = 09/17/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/10/16 Pct Recovery = 96% Analysis Date = 09/08/16 Pct Recovery = 96% Analysis Date = 09/08/16 Pct Recovery = 96% Analysis Date = 09/06/16 Pct Recovery = 96% Analysis Date = 09/06/16 Pct Recovery = 96% Analysis Date = 09/03/16 Pct Recovery = 96% Analysis Date = 09/03/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 09/01/16 Pct Recovery = 96% Analysis Date = 08/30/16 Pct Recovery = 96% Analysis Date = 08/30/16 Pct Recovery = 96% Analysis Date = 08/28/16 Pct Recovery = 96% Analysis Date = 08/28/16 Pct Recovery = 96% Analysis Date = 08/25/16 Pct Recovery = 95% Analysis Date = 08/25/16 Pct Recovery = 95% Analysis Date = 08/23/16 Pct Recovery = 95% Analysis Date = 08/23/16 Pct Recovery = 95% Analysis Date = 08/21/16 Pct Recovery = 95% Analysis Date = 08/21/16 Pct Recovery = 95% Analysis Date = 08/18/16 Pct Recovery = 95% Analysis Date = 08/18/16 Pct Recovery = 95% Analysis Date = 08/16/16 Pct Recovery = 95% Analysis Date = 08/16/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/12/16 Pct Recovery = 94% Analysis Date = 08/12/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/09/16 Pct Recovery = 94% Analysis Date = 08/07/16 Pct Recovery = 94% Analysis Date = 08/07/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/05/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 08/02/16 Pct Recovery = 94% Analysis Date = 07/31/16 Pct Recovery = 93% Analysis Date = 07/31/16 Pct Recovery = 93% Analysis Date = 07/29/16 Pct Recovery = 93% Analysis Date = 07/29/16 Pct Recovery = 93% Analysis Date = 07/27/16 Pct Recovery = 93% Analysis Date = 07/27/16 Pct Recovery = 93% Analysis Date = 07/24/16 Pct Recovery = 93% Analysis Date = 07/24/16 Pct Recovery = 93% Analysis Date = 07/22/16 Pct Recovery = 93% Analysis Date = 07/22/16 Pct Recovery = 93% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/20/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/15/16 Pct Recovery = 92% Analysis Date = 07/13/16 Pct Recovery = 92% Analysis Date = 07/13/16 Pct Recovery = 92% Analysis Date = 07/11/16 Pct Recovery = 92% Analysis Date = 07/11/16 Pct Recovery = 92% Analysis Date = 07/08/16 Pct Recovery = 92% Analysis Date = 07/08/16 Pct Recovery = 92% Analysis Date = 07/06/16 Pct Recovery = 91% Analysis Date = 07/06/16 Pct Recovery = 91% Analysis Date = 07/04/16 Pct Recovery = 91% Analysis Date = 07/04/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 06/29/16 Pct Recovery = 91% Analysis Date = 06/29/16 Pct Recovery = 91% Analysis Date = 06/27/16 Pct Recovery = 91% Analysis Date = 06/27/16 Pct Recovery = 91% Analysis Date = 06/25/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 90% Analysis Date = 06/22/16 Pct Recovery = 90% Analysis Date = 06/22/16 Pct Recovery = 90% Analysis Date = 06/20/16 Pct Recovery = 90% Analysis Date = 06/20/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/18/16 Pct Recovery = 90% Analysis Date = 06/15/16 Pct Recovery = 90% Analysis Date = 06/15/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/13/16 Pct Recovery = 90% Analysis Date = 06/11/16 Pct Recovery = 89% Analysis Date = 06/11/16 Pct Recovery = 89% Analysis Date = 06/09/16 Pct Recovery = 89% Analysis Date = 06/09/16 Pct Recovery = 89% Analysis Date = 06/06/16 Pct Recovery = 89% Analysis Date = 06/06/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 06/04/16 Pct Recovery = 89% Analysis Date = 06/02/16 Pct Recovery = 89% Analysis Date = 06/02/16 Pct Recovery = 89% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/30/16 Pct Recovery = 88% Analysis Date = 05/28/16 Pct Recovery = 88% Analysis Date = 05/28/16 Pct Recovery = 88% Analysis Date = 05/26/16 Pct Recovery = 88% Analysis Date = 05/26/16 Pct Recovery = 88% Analysis Date = 05/24/16 Pct Recovery = 88% Analysis Date = 05/24/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/21/16 Pct Recovery = 88% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/14/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/12/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/10/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/08/16 Pct Recovery = 87% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/03/16 Pct Recovery = 86% Analysis Date = 05/03/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/26/16 Pct Recovery = 86% Analysis Date = 04/24/16 Pct Recovery = 86% Analysis Date = 04/24/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/19/16 Pct Recovery = 86% Analysis Date = 04/19/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/12/16 Pct Recovery = 86% Analysis Date = 04/12/16 Pct Recovery = 86% Analysis Date = 04/10/16 Pct Recovery = 86% Analysis Date = 04/10/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 85% Analysis Date = 04/08/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/21/16 Pct Recovery = 85% Analysis Date = 03/18/16 Pct Recovery = 85% Analysis Date = 03/18/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/16/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/14/16 Pct Recovery = 85% Analysis Date = 03/11/16 Pct Recovery = 85% Analysis Date = 03/11/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/09/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/05/16 Pct Recovery = 85% Analysis Date = 03/05/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/20/16 Pct Recovery = 85% Analysis Date = 02/20/16 Pct Recovery = 85% Analysis Date = 02/18/16 Pct Recovery = 85% Analysis Date = 02/18/16 Pct Recovery = 85% Analysis Date = 02/15/16 Pct Recovery = 85% Analysis Date = 02/15/16 Pct Recovery = 85% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/09/16 Pct Recovery = 86% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METALAXYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 93% 14% 91% 7%
Total 18 93% 14% 91% 7%

Sample Statistics
METALAXYL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
METHIDATHION (SUPRACIDE)
METHOD: 2033 , TESTIDCODE: 61598GCM39

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 97% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 99% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 76% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 84% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 84% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 59% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 95% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 105% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 86% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 95% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 96% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 125% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 72% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 57% Analysis Date = 05/10/17 Pct Recovery = 88% Analysis Date = 05/08/17 Pct Recovery = 89% Analysis Date = 05/08/17 Pct Recovery = 89% Analysis Date = 05/06/17 Pct Recovery = 89% Analysis Date = 05/06/17 Pct Recovery = 89% Analysis Date = 05/04/17 Pct Recovery = 89% Analysis Date = 05/04/17 Pct Recovery = 89% Analysis Date = 05/02/17 Pct Recovery = 89% Analysis Date = 05/02/17 Pct Recovery = 89% Analysis Date = 04/30/17 Pct Recovery = 89% Analysis Date = 04/30/17 Pct Recovery = 89% Analysis Date = 04/27/17 Pct Recovery = 89% Analysis Date = 04/27/17 Pct Recovery = 89% Analysis Date = 04/25/17 Pct Recovery = 89% Analysis Date = 04/25/17 Pct Recovery = 89% Analysis Date = 04/23/17 Pct Recovery = 89% Analysis Date = 04/23/17 Pct Recovery = 89% Analysis Date = 04/21/17 Pct Recovery = 89% Analysis Date = 04/21/17 Pct Recovery = 89% Analysis Date = 04/19/17 Pct Recovery = 89% Analysis Date = 04/19/17 Pct Recovery = 89% Analysis Date = 04/17/17 Pct Recovery = 89% Analysis Date = 04/17/17 Pct Recovery = 89% Analysis Date = 04/14/17 Pct Recovery = 89% Analysis Date = 04/14/17 Pct Recovery = 89% Analysis Date = 04/12/17 Pct Recovery = 89% Analysis Date = 04/12/17 Pct Recovery = 89% Analysis Date = 04/10/17 Pct Recovery = 89% Analysis Date = 04/10/17 Pct Recovery = 89% Analysis Date = 04/08/17 Pct Recovery = 89% Analysis Date = 04/08/17 Pct Recovery = 89% Analysis Date = 04/06/17 Pct Recovery = 89% Analysis Date = 04/06/17 Pct Recovery = 89% Analysis Date = 04/04/17 Pct Recovery = 90% Analysis Date = 04/04/17 Pct Recovery = 90% Analysis Date = 04/01/17 Pct Recovery = 90% Analysis Date = 04/01/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/28/17 Pct Recovery = 90% Analysis Date = 03/28/17 Pct Recovery = 90% Analysis Date = 03/26/17 Pct Recovery = 90% Analysis Date = 03/26/17 Pct Recovery = 90% Analysis Date = 03/24/17 Pct Recovery = 90% Analysis Date = 03/24/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/15/17 Pct Recovery = 90% Analysis Date = 03/15/17 Pct Recovery = 90% Analysis Date = 03/13/17 Pct Recovery = 90% Analysis Date = 03/13/17 Pct Recovery = 90% Analysis Date = 03/11/17 Pct Recovery = 90% Analysis Date = 03/11/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/06/17 Pct Recovery = 90% Analysis Date = 03/06/17 Pct Recovery = 90% Analysis Date = 03/04/17 Pct Recovery = 90% Analysis Date = 03/04/17 Pct Recovery = 90% Analysis Date = 03/02/17 Pct Recovery = 91% Analysis Date = 03/02/17 Pct Recovery = 91% Analysis Date = 02/28/17 Pct Recovery = 91% Analysis Date = 02/28/17 Pct Recovery = 91% Analysis Date = 02/26/17 Pct Recovery = 91% Analysis Date = 02/26/17 Pct Recovery = 91% Analysis Date = 02/23/17 Pct Recovery = 91% Analysis Date = 02/23/17 Pct Recovery = 91% Analysis Date = 02/21/17 Pct Recovery = 91% Analysis Date = 02/21/17 Pct Recovery = 91% Analysis Date = 02/19/17 Pct Recovery = 91% Analysis Date = 02/19/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/12/17 Pct Recovery = 91% Analysis Date = 02/12/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 92% Analysis Date = 02/04/17 Pct Recovery = 92% Analysis Date = 02/02/17 Pct Recovery = 92% Analysis Date = 02/02/17 Pct Recovery = 92% Analysis Date = 01/30/17 Pct Recovery = 92% Analysis Date = 01/30/17 Pct Recovery = 92% Analysis Date = 01/28/17 Pct Recovery = 92% Analysis Date = 01/28/17 Pct Recovery = 92% Analysis Date = 01/26/17 Pct Recovery = 92% Analysis Date = 01/26/17 Pct Recovery = 92% Analysis Date = 01/24/17 Pct Recovery = 92% Analysis Date = 01/24/17 Pct Recovery = 92% Analysis Date = 01/22/17 Pct Recovery = 92% Analysis Date = 01/22/17 Pct Recovery = 92% Analysis Date = 01/20/17 Pct Recovery = 92% Analysis Date = 01/20/17 Pct Recovery = 92% Analysis Date = 01/17/17 Pct Recovery = 92% Analysis Date = 01/17/17 Pct Recovery = 92% Analysis Date = 01/15/17 Pct Recovery = 93% Analysis Date = 01/15/17 Pct Recovery = 93% Analysis Date = 01/13/17 Pct Recovery = 93% Analysis Date = 01/13/17 Pct Recovery = 93% Analysis Date = 01/11/17 Pct Recovery = 93% Analysis Date = 01/11/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 94% Analysis Date = 01/07/17 Pct Recovery = 94% Analysis Date = 01/04/17 Pct Recovery = 94% Analysis Date = 01/04/17 Pct Recovery = 94% Analysis Date = 01/02/17 Pct Recovery = 94% Analysis Date = 01/02/17 Pct Recovery = 94% Analysis Date = 12/31/16 Pct Recovery = 95% Analysis Date = 12/31/16 Pct Recovery = 95% Analysis Date = 12/29/16 Pct Recovery = 95% Analysis Date = 12/29/16 Pct Recovery = 95% Analysis Date = 12/27/16 Pct Recovery = 95% Analysis Date = 12/27/16 Pct Recovery = 95% Analysis Date = 12/24/16 Pct Recovery = 95% Analysis Date = 12/24/16 Pct Recovery = 95% Analysis Date = 12/22/16 Pct Recovery = 96% Analysis Date = 12/22/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/20/16 Pct Recovery = 96% Analysis Date = 12/18/16 Pct Recovery = 96% Analysis Date = 12/18/16 Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/16/16 Pct Recovery = 96% Analysis Date = 12/14/16 Pct Recovery = 96% Analysis Date = 12/14/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/11/16 Pct Recovery = 96% Analysis Date = 12/09/16 Pct Recovery = 96% Analysis Date = 12/09/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 96% Analysis Date = 12/07/16 Pct Recovery = 96% Analysis Date = 12/05/16 Pct Recovery = 96% Analysis Date = 12/05/16 Pct Recovery = 96% Analysis Date = 12/03/16 Pct Recovery = 96% Analysis Date = 12/03/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 12/01/16 Pct Recovery = 96% Analysis Date = 11/28/16 Pct Recovery = 96% Analysis Date = 11/28/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/26/16 Pct Recovery = 96% Analysis Date = 11/24/16 Pct Recovery = 96% Analysis Date = 11/24/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 96% Analysis Date = 11/22/16 Pct Recovery = 96% Analysis Date = 11/20/16 Pct Recovery = 96% Analysis Date = 11/20/16 Pct Recovery = 96% Analysis Date = 11/17/16 Pct Recovery = 96% Analysis Date = 11/17/16 Pct Recovery = 96% Analysis Date = 11/15/16 Pct Recovery = 96% Analysis Date = 11/15/16 Pct Recovery = 96% Analysis Date = 11/13/16 Pct Recovery = 96% Analysis Date = 11/13/16 Pct Recovery = 96% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/07/16 Pct Recovery = 96% Analysis Date = 11/07/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/29/16 Pct Recovery = 96% Analysis Date = 10/27/16 Pct Recovery = 96% Analysis Date = 10/27/16 Pct Recovery = 96% Analysis Date = 10/25/16 Pct Recovery = 96% Analysis Date = 10/25/16 Pct Recovery = 96% Analysis Date = 10/22/16 Pct Recovery = 96% Analysis Date = 10/22/16 Pct Recovery = 96% Analysis Date = 10/20/16 Pct Recovery = 96% Analysis Date = 10/20/16 Pct Recovery = 96% Analysis Date = 10/18/16 Pct Recovery = 96% Analysis Date = 10/18/16 Pct Recovery = 96% Analysis Date = 10/16/16 Pct Recovery = 96% Analysis Date = 10/16/16 Pct Recovery = 96% Analysis Date = 10/14/16 Pct Recovery = 96% Analysis Date = 10/14/16 Pct Recovery = 96% Analysis Date = 10/12/16 Pct Recovery = 96% Analysis Date = 10/12/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 10/09/16 Pct Recovery = 96% Analysis Date = 10/07/16 Pct Recovery = 96% Analysis Date = 10/07/16 Pct Recovery = 96% Analysis Date = 10/05/16 Pct Recovery = 96% Analysis Date = 10/05/16 Pct Recovery = 96% Analysis Date = 10/03/16 Pct Recovery = 96% Analysis Date = 10/03/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 10/01/16 Pct Recovery = 96% Analysis Date = 09/28/16 Pct Recovery = 96% Analysis Date = 09/28/16 Pct Recovery = 96% Analysis Date = 09/26/16 Pct Recovery = 96% Analysis Date = 09/26/16 Pct Recovery = 96% Analysis Date = 09/24/16 Pct Recovery = 96% Analysis Date = 09/24/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/20/16 Pct Recovery = 96% Analysis Date = 09/18/16 Pct Recovery = 96% Analysis Date = 09/18/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 96% Analysis Date = 09/11/16 Pct Recovery = 96% Analysis Date = 09/11/16 Pct Recovery = 96% Analysis Date = 09/09/16 Pct Recovery = 96% Analysis Date = 09/09/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/07/16 Pct Recovery = 96% Analysis Date = 09/05/16 Pct Recovery = 96% Analysis Date = 09/05/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 09/02/16 Pct Recovery = 96% Analysis Date = 08/31/16 Pct Recovery = 96% Analysis Date = 08/31/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/29/16 Pct Recovery = 96% Analysis Date = 08/27/16 Pct Recovery = 96% Analysis Date = 08/27/16 Pct Recovery = 96% Analysis Date = 08/25/16 Pct Recovery = 96% Analysis Date = 08/25/16 Pct Recovery = 96% Analysis Date = 08/22/16 Pct Recovery = 96% Analysis Date = 08/22/16 Pct Recovery = 96% Analysis Date = 08/20/16 Pct Recovery = 96% Analysis Date = 08/20/16 Pct Recovery = 96% Analysis Date = 08/18/16 Pct Recovery = 96% Analysis Date = 08/18/16 Pct Recovery = 96% Analysis Date = 08/16/16 Pct Recovery = 96% Analysis Date = 08/16/16 Pct Recovery = 96% Analysis Date = 08/14/16 Pct Recovery = 96% Analysis Date = 08/14/16 Pct Recovery = 96% Analysis Date = 08/12/16 Pct Recovery = 95% Analysis Date = 08/12/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/09/16 Pct Recovery = 95% Analysis Date = 08/07/16 Pct Recovery = 95% Analysis Date = 08/07/16 Pct Recovery = 95% Analysis Date = 08/05/16 Pct Recovery = 95% Analysis Date = 08/05/16 Pct Recovery = 95% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 08/03/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 94% Analysis Date = 08/01/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 94% Analysis Date = 07/30/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/27/16 Pct Recovery = 94% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/25/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/23/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/21/16 Pct Recovery = 93% Analysis Date = 07/19/16 Pct Recovery = 93% Analysis Date = 07/19/16 Pct Recovery = 93% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/17/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/08/16 Pct Recovery = 91% Analysis Date = 07/06/16 Pct Recovery = 91% Analysis Date = 07/06/16 Pct Recovery = 91% Analysis Date = 07/03/16 Pct Recovery = 91% Analysis Date = 07/03/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 07/01/16 Pct Recovery = 91% Analysis Date = 06/29/16 Pct Recovery = 90% Analysis Date = 06/29/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/27/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 90% Analysis Date = 06/25/16 Pct Recovery = 90% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/23/16 Pct Recovery = 90% Analysis Date = 06/20/16 Pct Recovery = 89% Analysis Date = 06/20/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/18/16 Pct Recovery = 89% Analysis Date = 06/16/16 Pct Recovery = 89% Analysis Date = 06/16/16 Pct Recovery = 89% Analysis Date = 06/14/16 Pct Recovery = 89% Analysis Date = 06/14/16 Pct Recovery = 89% Analysis Date = 06/12/16 Pct Recovery = 88% Analysis Date = 06/12/16 Pct Recovery = 88% Analysis Date = 06/10/16 Pct Recovery = 88% Analysis Date = 06/10/16 Pct Recovery = 88% Analysis Date = 06/07/16 Pct Recovery = 88% Analysis Date = 06/07/16 Pct Recovery = 88% Analysis Date = 06/05/16 Pct Recovery = 88% Analysis Date = 06/05/16 Pct Recovery = 88% Analysis Date = 06/03/16 Pct Recovery = 87% Analysis Date = 06/03/16 Pct Recovery = 87% Analysis Date = 06/01/16 Pct Recovery = 87% Analysis Date = 06/01/16 Pct Recovery = 87% Analysis Date = 05/30/16 Pct Recovery = 87% Analysis Date = 05/30/16 Pct Recovery = 87% Analysis Date = 05/27/16 Pct Recovery = 87% Analysis Date = 05/27/16 Pct Recovery = 87% Analysis Date = 05/25/16 Pct Recovery = 86% Analysis Date = 05/25/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/23/16 Pct Recovery = 86% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/17/16 Pct Recovery = 84% Analysis Date = 05/17/16 Pct Recovery = 84% Analysis Date = 05/14/16 Pct Recovery = 83% Analysis Date = 05/14/16 Pct Recovery = 83% Analysis Date = 05/12/16 Pct Recovery = 83% Analysis Date = 05/12/16 Pct Recovery = 83% Analysis Date = 05/10/16 Pct Recovery = 82% Analysis Date = 05/10/16 Pct Recovery = 82% Analysis Date = 05/08/16 Pct Recovery = 81% Analysis Date = 05/08/16 Pct Recovery = 81% Analysis Date = 05/06/16 Pct Recovery = 81% Analysis Date = 05/06/16 Pct Recovery = 81% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 05/01/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/29/16 Pct Recovery = 79% Analysis Date = 04/27/16 Pct Recovery = 78% Analysis Date = 04/27/16 Pct Recovery = 78% Analysis Date = 04/25/16 Pct Recovery = 77% Analysis Date = 04/25/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/23/16 Pct Recovery = 77% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/21/16 Pct Recovery = 76% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 75% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/12/16 Pct Recovery = 73% Analysis Date = 04/12/16 Pct Recovery = 73% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/10/16 Pct Recovery = 72% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 70% Analysis Date = 04/05/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 70% Analysis Date = 04/03/16 Pct Recovery = 70% Analysis Date = 04/01/16 Pct Recovery = 69% Analysis Date = 04/01/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 68% Analysis Date = 03/28/16 Pct Recovery = 67% Analysis Date = 03/28/16 Pct Recovery = 67% Analysis Date = 03/25/16 Pct Recovery = 66% Analysis Date = 03/25/16 Pct Recovery = 66% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 63% Analysis Date = 03/19/16 Pct Recovery = 63% Analysis Date = 03/17/16 Pct Recovery = 62% Analysis Date = 03/17/16 Pct Recovery = 62% Analysis Date = 03/15/16 Pct Recovery = 61% Analysis Date = 03/15/16 Pct Recovery = 61% Analysis Date = 03/12/16 Pct Recovery = 61% Analysis Date = 03/12/16 Pct Recovery = 61% Analysis Date = 03/10/16 Pct Recovery = 60% Analysis Date = 03/10/16 Pct Recovery = 60% Analysis Date = 03/08/16 Pct Recovery = 59% Analysis Date = 03/08/16 Pct Recovery = 59% Analysis Date = 03/06/16 Pct Recovery = 58% Analysis Date = 03/06/16 Pct Recovery = 58% Analysis Date = 03/04/16 Pct Recovery = 57% Analysis Date = 03/04/16 Pct Recovery = 57% Analysis Date = 03/02/16 Pct Recovery = 56% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHIDATHION (SUPRACIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 87% 16% 88% 13%
Total 19 87% 16% 88% 13%

Sample Statistics
METHIDATHION (SUPRACIDE)

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 3 16% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
METOLACHLOR
METHOD: 2033 , TESTIDCODE: 39415GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 91% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 85% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 116% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 85% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 89% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 81% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 76% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 85% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 85% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 88% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 90% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 81% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 72% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 88% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 81% Analysis Date = 05/10/17 Pct Recovery = 82% Analysis Date = 05/08/17 Pct Recovery = 82% Analysis Date = 05/08/17 Pct Recovery = 82% Analysis Date = 05/06/17 Pct Recovery = 82% Analysis Date = 05/06/17 Pct Recovery = 82% Analysis Date = 05/04/17 Pct Recovery = 82% Analysis Date = 05/04/17 Pct Recovery = 82% Analysis Date = 05/01/17 Pct Recovery = 83% Analysis Date = 05/01/17 Pct Recovery = 83% Analysis Date = 04/29/17 Pct Recovery = 83% Analysis Date = 04/29/17 Pct Recovery = 83% Analysis Date = 04/27/17 Pct Recovery = 83% Analysis Date = 04/27/17 Pct Recovery = 83% Analysis Date = 04/25/17 Pct Recovery = 83% Analysis Date = 04/25/17 Pct Recovery = 83% Analysis Date = 04/22/17 Pct Recovery = 83% Analysis Date = 04/22/17 Pct Recovery = 83% Analysis Date = 04/20/17 Pct Recovery = 83% Analysis Date = 04/20/17 Pct Recovery = 83% Analysis Date = 04/18/17 Pct Recovery = 83% Analysis Date = 04/18/17 Pct Recovery = 83% Analysis Date = 04/15/17 Pct Recovery = 83% Analysis Date = 04/15/17 Pct Recovery = 83% Analysis Date = 04/13/17 Pct Recovery = 84% Analysis Date = 04/13/17 Pct Recovery = 84% Analysis Date = 04/11/17 Pct Recovery = 84% Analysis Date = 04/11/17 Pct Recovery = 84% Analysis Date = 04/09/17 Pct Recovery = 84% Analysis Date = 04/09/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/04/17 Pct Recovery = 84% Analysis Date = 04/04/17 Pct Recovery = 84% Analysis Date = 04/02/17 Pct Recovery = 84% Analysis Date = 04/02/17 Pct Recovery = 84% Analysis Date = 03/30/17 Pct Recovery = 84% Analysis Date = 03/30/17 Pct Recovery = 84% Analysis Date = 03/28/17 Pct Recovery = 84% Analysis Date = 03/28/17 Pct Recovery = 84% Analysis Date = 03/26/17 Pct Recovery = 85% Analysis Date = 03/26/17 Pct Recovery = 85% Analysis Date = 03/24/17 Pct Recovery = 85% Analysis Date = 03/24/17 Pct Recovery = 85% Analysis Date = 03/21/17 Pct Recovery = 85% Analysis Date = 03/21/17 Pct Recovery = 85% Analysis Date = 03/19/17 Pct Recovery = 85% Analysis Date = 03/19/17 Pct Recovery = 85% Analysis Date = 03/17/17 Pct Recovery = 85% Analysis Date = 03/17/17 Pct Recovery = 85% Analysis Date = 03/14/17 Pct Recovery = 85% Analysis Date = 03/14/17 Pct Recovery = 85% Analysis Date = 03/12/17 Pct Recovery = 85% Analysis Date = 03/12/17 Pct Recovery = 85% Analysis Date = 03/10/17 Pct Recovery = 85% Analysis Date = 03/10/17 Pct Recovery = 85% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 86% Analysis Date = 03/05/17 Pct Recovery = 86% Analysis Date = 03/05/17 Pct Recovery = 86% Analysis Date = 03/03/17 Pct Recovery = 86% Analysis Date = 03/03/17 Pct Recovery = 86% Analysis Date = 03/01/17 Pct Recovery = 86% Analysis Date = 03/01/17 Pct Recovery = 86% Analysis Date = 02/26/17 Pct Recovery = 86% Analysis Date = 02/26/17 Pct Recovery = 86% Analysis Date = 02/24/17 Pct Recovery = 86% Analysis Date = 02/24/17 Pct Recovery = 86% Analysis Date = 02/22/17 Pct Recovery = 86% Analysis Date = 02/22/17 Pct Recovery = 86% Analysis Date = 02/20/17 Pct Recovery = 86% Analysis Date = 02/20/17 Pct Recovery = 86% Analysis Date = 02/17/17 Pct Recovery = 87% Analysis Date = 02/17/17 Pct Recovery = 87% Analysis Date = 02/15/17 Pct Recovery = 87% Analysis Date = 02/15/17 Pct Recovery = 87% Analysis Date = 02/13/17 Pct Recovery = 87% Analysis Date = 02/13/17 Pct Recovery = 87% Analysis Date = 02/10/17 Pct Recovery = 87% Analysis Date = 02/10/17 Pct Recovery = 87% Analysis Date = 02/08/17 Pct Recovery = 87% Analysis Date = 02/08/17 Pct Recovery = 87% Analysis Date = 02/06/17 Pct Recovery = 87% Analysis Date = 02/06/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 02/04/17 Pct Recovery = 87% Analysis Date = 02/01/17 Pct Recovery = 87% Analysis Date = 02/01/17 Pct Recovery = 87% Analysis Date = 01/30/17 Pct Recovery = 88% Analysis Date = 01/30/17 Pct Recovery = 88% Analysis Date = 01/28/17 Pct Recovery = 88% Analysis Date = 01/28/17 Pct Recovery = 88% Analysis Date = 01/25/17 Pct Recovery = 88% Analysis Date = 01/25/17 Pct Recovery = 88% Analysis Date = 01/23/17 Pct Recovery = 88% Analysis Date = 01/23/17 Pct Recovery = 88% Analysis Date = 01/21/17 Pct Recovery = 88% Analysis Date = 01/21/17 Pct Recovery = 88% Analysis Date = 01/19/17 Pct Recovery = 88% Analysis Date = 01/19/17 Pct Recovery = 88% Analysis Date = 01/16/17 Pct Recovery = 88% Analysis Date = 01/16/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 89% Analysis Date = 01/12/17 Pct Recovery = 89% Analysis Date = 01/12/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/09/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/07/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 89% Analysis Date = 01/05/17 Pct Recovery = 89% Analysis Date = 01/03/17 Pct Recovery = 89% Analysis Date = 01/03/17 Pct Recovery = 89% Analysis Date = 12/31/16 Pct Recovery = 89% Analysis Date = 12/31/16 Pct Recovery = 89% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 91% Analysis Date = 12/08/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/06/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 12/02/16 Pct Recovery = 91% Analysis Date = 11/29/16 Pct Recovery = 91% Analysis Date = 11/29/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/27/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/25/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/22/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/18/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/16/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/13/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/11/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 92% Analysis Date = 11/09/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/06/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/04/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 11/02/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/24/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/21/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/19/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/15/16 Pct Recovery = 92% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/12/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/10/16 Pct Recovery = 93% Analysis Date = 10/08/16 Pct Recovery = 93% Analysis Date = 10/08/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/05/16 Pct Recovery = 93% Analysis Date = 10/03/16 Pct Recovery = 93% Analysis Date = 10/03/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/29/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/26/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/24/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/22/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 94% Analysis Date = 09/03/16 Pct Recovery = 94% Analysis Date = 09/03/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/30/16 Pct Recovery = 94% Analysis Date = 08/30/16 Pct Recovery = 94% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/28/16 Pct Recovery = 93% Analysis Date = 08/25/16 Pct Recovery = 93% Analysis Date = 08/25/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/23/16 Pct Recovery = 93% Analysis Date = 08/21/16 Pct Recovery = 93% Analysis Date = 08/21/16 Pct Recovery = 93% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/18/16 Pct Recovery = 92% Analysis Date = 08/16/16 Pct Recovery = 92% Analysis Date = 08/16/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/14/16 Pct Recovery = 92% Analysis Date = 08/12/16 Pct Recovery = 91% Analysis Date = 08/12/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/09/16 Pct Recovery = 91% Analysis Date = 08/07/16 Pct Recovery = 91% Analysis Date = 08/07/16 Pct Recovery = 91% Analysis Date = 08/05/16 Pct Recovery = 91% Analysis Date = 08/05/16 Pct Recovery = 91% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 89% Analysis Date = 07/27/16 Pct Recovery = 89% Analysis Date = 07/24/16 Pct Recovery = 89% Analysis Date = 07/24/16 Pct Recovery = 89% Analysis Date = 07/22/16 Pct Recovery = 89% Analysis Date = 07/22/16 Pct Recovery = 89% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/20/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/17/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/15/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/13/16 Pct Recovery = 88% Analysis Date = 07/11/16 Pct Recovery = 87% Analysis Date = 07/11/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/06/16 Pct Recovery = 87% Analysis Date = 07/04/16 Pct Recovery = 86% Analysis Date = 07/04/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/25/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/22/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/09/16 Pct Recovery = 83% Analysis Date = 06/09/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/04/16 Pct Recovery = 83% Analysis Date = 06/04/16 Pct Recovery = 83% Analysis Date = 06/02/16 Pct Recovery = 82% Analysis Date = 06/02/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/26/16 Pct Recovery = 82% Analysis Date = 05/26/16 Pct Recovery = 82% Analysis Date = 05/24/16 Pct Recovery = 82% Analysis Date = 05/24/16 Pct Recovery = 82% Analysis Date = 05/21/16 Pct Recovery = 82% Analysis Date = 05/21/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 82% Analysis Date = 05/17/16 Pct Recovery = 82% Analysis Date = 05/17/16 Pct Recovery = 82% Analysis Date = 05/14/16 Pct Recovery = 82% Analysis Date = 05/14/16 Pct Recovery = 82% Analysis Date = 05/12/16 Pct Recovery = 82% Analysis Date = 05/12/16 Pct Recovery = 82% Analysis Date = 05/10/16 Pct Recovery = 82% Analysis Date = 05/10/16 Pct Recovery = 82% Analysis Date = 05/08/16 Pct Recovery = 82% Analysis Date = 05/08/16 Pct Recovery = 82% Analysis Date = 05/05/16 Pct Recovery = 82% Analysis Date = 05/05/16 Pct Recovery = 82% Analysis Date = 05/03/16 Pct Recovery = 82% Analysis Date = 05/03/16 Pct Recovery = 82% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 05/01/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/28/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/26/16 Pct Recovery = 83% Analysis Date = 04/24/16 Pct Recovery = 83% Analysis Date = 04/24/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/22/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 83% Analysis Date = 04/19/16 Pct Recovery = 83% Analysis Date = 04/17/16 Pct Recovery = 84% Analysis Date = 04/17/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/15/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 84% Analysis Date = 04/12/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/10/16 Pct Recovery = 84% Analysis Date = 04/08/16 Pct Recovery = 84% Analysis Date = 04/08/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/03/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 85% Analysis Date = 03/23/16 Pct Recovery = 86% Analysis Date = 03/23/16 Pct Recovery = 86% Analysis Date = 03/21/16 Pct Recovery = 86% Analysis Date = 03/21/16 Pct Recovery = 86% Analysis Date = 03/18/16 Pct Recovery = 86% Analysis Date = 03/18/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/11/16 Pct Recovery = 87% Analysis Date = 03/11/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/09/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/07/16 Pct Recovery = 87% Analysis Date = 03/05/16 Pct Recovery = 87% Analysis Date = 03/05/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 03/02/16 Pct Recovery = 87% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/22/16 Pct Recovery = 88% Analysis Date = 02/22/16 Pct Recovery = 88% Analysis Date = 02/20/16 Pct Recovery = 88% Analysis Date = 02/20/16 Pct Recovery = 88% Analysis Date = 02/18/16 Pct Recovery = 89% Analysis Date = 02/18/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/13/16 Pct Recovery = 89% Analysis Date = 02/13/16 Pct Recovery = 89% Analysis Date = 02/11/16 Pct Recovery = 89% Analysis Date = 02/11/16 Pct Recovery = 89% Analysis Date = 02/09/16 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METOLACHLOR

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 86% 9% 85% 7%
Total 20 86% 9% 85% 7%

Sample Statistics
METOLACHLOR

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
METRIBUZIN
METHOD: 2033 , TESTIDCODE: 82630GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 75% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 65% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 76% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 73% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 68% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 77% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 80% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 69% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 81% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 76% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 64% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 77% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 69% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 67% Analysis Date = 05/10/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/04/17 Pct Recovery = 75% Analysis Date = 05/04/17 Pct Recovery = 75% Analysis Date = 05/02/17 Pct Recovery = 75% Analysis Date = 05/02/17 Pct Recovery = 75% Analysis Date = 04/30/17 Pct Recovery = 75% Analysis Date = 04/30/17 Pct Recovery = 75% Analysis Date = 04/27/17 Pct Recovery = 75% Analysis Date = 04/27/17 Pct Recovery = 75% Analysis Date = 04/25/17 Pct Recovery = 75% Analysis Date = 04/25/17 Pct Recovery = 75% Analysis Date = 04/23/17 Pct Recovery = 75% Analysis Date = 04/23/17 Pct Recovery = 75% Analysis Date = 04/21/17 Pct Recovery = 75% Analysis Date = 04/21/17 Pct Recovery = 75% Analysis Date = 04/19/17 Pct Recovery = 74% Analysis Date = 04/19/17 Pct Recovery = 74% Analysis Date = 04/17/17 Pct Recovery = 74% Analysis Date = 04/17/17 Pct Recovery = 74% Analysis Date = 04/14/17 Pct Recovery = 74% Analysis Date = 04/14/17 Pct Recovery = 74% Analysis Date = 04/12/17 Pct Recovery = 74% Analysis Date = 04/12/17 Pct Recovery = 74% Analysis Date = 04/10/17 Pct Recovery = 74% Analysis Date = 04/10/17 Pct Recovery = 74% Analysis Date = 04/08/17 Pct Recovery = 74% Analysis Date = 04/08/17 Pct Recovery = 74% Analysis Date = 04/06/17 Pct Recovery = 74% Analysis Date = 04/06/17 Pct Recovery = 74% Analysis Date = 04/04/17 Pct Recovery = 74% Analysis Date = 04/04/17 Pct Recovery = 74% Analysis Date = 04/01/17 Pct Recovery = 74% Analysis Date = 04/01/17 Pct Recovery = 74% Analysis Date = 03/30/17 Pct Recovery = 73% Analysis Date = 03/30/17 Pct Recovery = 73% Analysis Date = 03/28/17 Pct Recovery = 73% Analysis Date = 03/28/17 Pct Recovery = 73% Analysis Date = 03/26/17 Pct Recovery = 73% Analysis Date = 03/26/17 Pct Recovery = 73% Analysis Date = 03/24/17 Pct Recovery = 73% Analysis Date = 03/24/17 Pct Recovery = 73% Analysis Date = 03/21/17 Pct Recovery = 73% Analysis Date = 03/21/17 Pct Recovery = 73% Analysis Date = 03/19/17 Pct Recovery = 73% Analysis Date = 03/19/17 Pct Recovery = 73% Analysis Date = 03/17/17 Pct Recovery = 73% Analysis Date = 03/17/17 Pct Recovery = 73% Analysis Date = 03/15/17 Pct Recovery = 73% Analysis Date = 03/15/17 Pct Recovery = 73% Analysis Date = 03/13/17 Pct Recovery = 73% Analysis Date = 03/13/17 Pct Recovery = 73% Analysis Date = 03/11/17 Pct Recovery = 72% Analysis Date = 03/11/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/04/17 Pct Recovery = 72% Analysis Date = 03/04/17 Pct Recovery = 72% Analysis Date = 03/02/17 Pct Recovery = 72% Analysis Date = 03/02/17 Pct Recovery = 72% Analysis Date = 02/28/17 Pct Recovery = 72% Analysis Date = 02/28/17 Pct Recovery = 72% Analysis Date = 02/26/17 Pct Recovery = 72% Analysis Date = 02/26/17 Pct Recovery = 72% Analysis Date = 02/23/17 Pct Recovery = 72% Analysis Date = 02/23/17 Pct Recovery = 72% Analysis Date = 02/21/17 Pct Recovery = 71% Analysis Date = 02/21/17 Pct Recovery = 71% Analysis Date = 02/19/17 Pct Recovery = 71% Analysis Date = 02/19/17 Pct Recovery = 71% Analysis Date = 02/17/17 Pct Recovery = 71% Analysis Date = 02/17/17 Pct Recovery = 71% Analysis Date = 02/15/17 Pct Recovery = 71% Analysis Date = 02/15/17 Pct Recovery = 71% Analysis Date = 02/12/17 Pct Recovery = 71% Analysis Date = 02/12/17 Pct Recovery = 71% Analysis Date = 02/10/17 Pct Recovery = 71% Analysis Date = 02/10/17 Pct Recovery = 71% Analysis Date = 02/08/17 Pct Recovery = 71% Analysis Date = 02/08/17 Pct Recovery = 71% Analysis Date = 02/06/17 Pct Recovery = 71% Analysis Date = 02/06/17 Pct Recovery = 71% Analysis Date = 02/04/17 Pct Recovery = 71% Analysis Date = 02/04/17 Pct Recovery = 71% Analysis Date = 02/02/17 Pct Recovery = 71% Analysis Date = 02/02/17 Pct Recovery = 71% Analysis Date = 01/30/17 Pct Recovery = 71% Analysis Date = 01/30/17 Pct Recovery = 71% Analysis Date = 01/28/17 Pct Recovery = 71% Analysis Date = 01/28/17 Pct Recovery = 71% Analysis Date = 01/26/17 Pct Recovery = 71% Analysis Date = 01/26/17 Pct Recovery = 71% Analysis Date = 01/24/17 Pct Recovery = 71% Analysis Date = 01/24/17 Pct Recovery = 71% Analysis Date = 01/22/17 Pct Recovery = 71% Analysis Date = 01/22/17 Pct Recovery = 71% Analysis Date = 01/20/17 Pct Recovery = 71% Analysis Date = 01/20/17 Pct Recovery = 71% Analysis Date = 01/17/17 Pct Recovery = 71% Analysis Date = 01/17/17 Pct Recovery = 71% Analysis Date = 01/15/17 Pct Recovery = 71% Analysis Date = 01/15/17 Pct Recovery = 71% Analysis Date = 01/13/17 Pct Recovery = 71% Analysis Date = 01/13/17 Pct Recovery = 71% Analysis Date = 01/11/17 Pct Recovery = 71% Analysis Date = 01/11/17 Pct Recovery = 71% Analysis Date = 01/09/17 Pct Recovery = 71% Analysis Date = 01/09/17 Pct Recovery = 71% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/07/17 Pct Recovery = 72% Analysis Date = 01/04/17 Pct Recovery = 72% Analysis Date = 01/04/17 Pct Recovery = 72% Analysis Date = 01/02/17 Pct Recovery = 72% Analysis Date = 01/02/17 Pct Recovery = 72% Analysis Date = 12/31/16 Pct Recovery = 72% Analysis Date = 12/31/16 Pct Recovery = 72% Analysis Date = 12/29/16 Pct Recovery = 72% Analysis Date = 12/29/16 Pct Recovery = 72% Analysis Date = 12/27/16 Pct Recovery = 73% Analysis Date = 12/27/16 Pct Recovery = 73% Analysis Date = 12/24/16 Pct Recovery = 73% Analysis Date = 12/24/16 Pct Recovery = 73% Analysis Date = 12/22/16 Pct Recovery = 73% Analysis Date = 12/22/16 Pct Recovery = 73% Analysis Date = 12/20/16 Pct Recovery = 73% Analysis Date = 12/20/16 Pct Recovery = 73% Analysis Date = 12/18/16 Pct Recovery = 73% Analysis Date = 12/18/16 Pct Recovery = 73% Analysis Date = 12/16/16 Pct Recovery = 73% Analysis Date = 12/16/16 Pct Recovery = 73% Analysis Date = 12/14/16 Pct Recovery = 74% Analysis Date = 12/14/16 Pct Recovery = 74% Analysis Date = 12/11/16 Pct Recovery = 74% Analysis Date = 12/11/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 12/09/16 Pct Recovery = 74% Analysis Date = 12/07/16 Pct Recovery = 74% Analysis Date = 12/07/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/05/16 Pct Recovery = 74% Analysis Date = 12/03/16 Pct Recovery = 74% Analysis Date = 12/03/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 74% Analysis Date = 12/01/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 75% Analysis Date = 11/26/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/24/16 Pct Recovery = 75% Analysis Date = 11/22/16 Pct Recovery = 75% Analysis Date = 11/22/16 Pct Recovery = 75% Analysis Date = 11/20/16 Pct Recovery = 75% Analysis Date = 11/20/16 Pct Recovery = 75% Analysis Date = 11/17/16 Pct Recovery = 75% Analysis Date = 11/17/16 Pct Recovery = 75% Analysis Date = 11/15/16 Pct Recovery = 75% Analysis Date = 11/15/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/13/16 Pct Recovery = 75% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 11/02/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 76% Analysis Date = 10/31/16 Pct Recovery = 76% Analysis Date = 10/29/16 Pct Recovery = 76% Analysis Date = 10/29/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/27/16 Pct Recovery = 76% Analysis Date = 10/25/16 Pct Recovery = 77% Analysis Date = 10/25/16 Pct Recovery = 77% Analysis Date = 10/22/16 Pct Recovery = 77% Analysis Date = 10/22/16 Pct Recovery = 77% Analysis Date = 10/20/16 Pct Recovery = 77% Analysis Date = 10/20/16 Pct Recovery = 77% Analysis Date = 10/18/16 Pct Recovery = 77% Analysis Date = 10/18/16 Pct Recovery = 77% Analysis Date = 10/16/16 Pct Recovery = 77% Analysis Date = 10/16/16 Pct Recovery = 77% Analysis Date = 10/14/16 Pct Recovery = 77% Analysis Date = 10/14/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/09/16 Pct Recovery = 77% Analysis Date = 10/09/16 Pct Recovery = 77% Analysis Date = 10/07/16 Pct Recovery = 78% Analysis Date = 10/07/16 Pct Recovery = 78% Analysis Date = 10/05/16 Pct Recovery = 78% Analysis Date = 10/05/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/01/16 Pct Recovery = 78% Analysis Date = 10/01/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/26/16 Pct Recovery = 78% Analysis Date = 09/26/16 Pct Recovery = 78% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/22/16 Pct Recovery = 78% Analysis Date = 09/22/16 Pct Recovery = 78% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/13/16 Pct Recovery = 79% Analysis Date = 09/13/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/09/16 Pct Recovery = 79% Analysis Date = 09/09/16 Pct Recovery = 79% Analysis Date = 09/07/16 Pct Recovery = 79% Analysis Date = 09/07/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 09/02/16 Pct Recovery = 79% Analysis Date = 09/02/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/14/16 Pct Recovery = 79% Analysis Date = 08/12/16 Pct Recovery = 79% Analysis Date = 08/12/16 Pct Recovery = 79% Analysis Date = 08/09/16 Pct Recovery = 78% Analysis Date = 08/09/16 Pct Recovery = 78% Analysis Date = 08/07/16 Pct Recovery = 78% Analysis Date = 08/07/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 78% Analysis Date = 07/30/16 Pct Recovery = 78% Analysis Date = 07/30/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/19/16 Pct Recovery = 77% Analysis Date = 07/19/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 77% Analysis Date = 07/14/16 Pct Recovery = 77% Analysis Date = 07/14/16 Pct Recovery = 77% Analysis Date = 07/12/16 Pct Recovery = 77% Analysis Date = 07/12/16 Pct Recovery = 77% Analysis Date = 07/10/16 Pct Recovery = 77% Analysis Date = 07/10/16 Pct Recovery = 77% Analysis Date = 07/08/16 Pct Recovery = 77% Analysis Date = 07/08/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/03/16 Pct Recovery = 76% Analysis Date = 07/03/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 76% Analysis Date = 06/23/16 Pct Recovery = 76% Analysis Date = 06/23/16 Pct Recovery = 76% Analysis Date = 06/20/16 Pct Recovery = 76% Analysis Date = 06/20/16 Pct Recovery = 76% Analysis Date = 06/18/16 Pct Recovery = 76% Analysis Date = 06/18/16 Pct Recovery = 76% Analysis Date = 06/16/16 Pct Recovery = 76% Analysis Date = 06/16/16 Pct Recovery = 76% Analysis Date = 06/14/16 Pct Recovery = 75% Analysis Date = 06/14/16 Pct Recovery = 75% Analysis Date = 06/12/16 Pct Recovery = 75% Analysis Date = 06/12/16 Pct Recovery = 75% Analysis Date = 06/10/16 Pct Recovery = 75% Analysis Date = 06/10/16 Pct Recovery = 75% Analysis Date = 06/07/16 Pct Recovery = 75% Analysis Date = 06/07/16 Pct Recovery = 75% Analysis Date = 06/05/16 Pct Recovery = 75% Analysis Date = 06/05/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 06/03/16 Pct Recovery = 75% Analysis Date = 06/01/16 Pct Recovery = 75% Analysis Date = 06/01/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 75% Analysis Date = 05/30/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/27/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/25/16 Pct Recovery = 75% Analysis Date = 05/23/16 Pct Recovery = 75% Analysis Date = 05/23/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/17/16 Pct Recovery = 75% Analysis Date = 05/17/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 75% Analysis Date = 05/12/16 Pct Recovery = 75% Analysis Date = 05/12/16 Pct Recovery = 75% Analysis Date = 05/10/16 Pct Recovery = 75% Analysis Date = 05/10/16 Pct Recovery = 75% Analysis Date = 05/08/16 Pct Recovery = 75% Analysis Date = 05/08/16 Pct Recovery = 75% Analysis Date = 05/06/16 Pct Recovery = 75% Analysis Date = 05/06/16 Pct Recovery = 75% Analysis Date = 05/04/16 Pct Recovery = 75% Analysis Date = 05/04/16 Pct Recovery = 75% Analysis Date = 05/01/16 Pct Recovery = 75% Analysis Date = 05/01/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/29/16 Pct Recovery = 75% Analysis Date = 04/27/16 Pct Recovery = 75% Analysis Date = 04/27/16 Pct Recovery = 75% Analysis Date = 04/25/16 Pct Recovery = 75% Analysis Date = 04/25/16 Pct Recovery = 75% Analysis Date = 04/23/16 Pct Recovery = 75% Analysis Date = 04/23/16 Pct Recovery = 75% Analysis Date = 04/21/16 Pct Recovery = 75% Analysis Date = 04/21/16 Pct Recovery = 75% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/18/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/16/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/14/16 Pct Recovery = 74% Analysis Date = 04/12/16 Pct Recovery = 74% Analysis Date = 04/12/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/10/16 Pct Recovery = 74% Analysis Date = 04/07/16 Pct Recovery = 74% Analysis Date = 04/07/16 Pct Recovery = 74% Analysis Date = 04/05/16 Pct Recovery = 74% Analysis Date = 04/05/16 Pct Recovery = 74% Analysis Date = 04/03/16 Pct Recovery = 74% Analysis Date = 04/03/16 Pct Recovery = 74% Analysis Date = 04/01/16 Pct Recovery = 74% Analysis Date = 04/01/16 Pct Recovery = 74% Analysis Date = 03/30/16 Pct Recovery = 74% Analysis Date = 03/30/16 Pct Recovery = 74% Analysis Date = 03/28/16 Pct Recovery = 74% Analysis Date = 03/28/16 Pct Recovery = 74% Analysis Date = 03/25/16 Pct Recovery = 74% Analysis Date = 03/25/16 Pct Recovery = 74% Analysis Date = 03/23/16 Pct Recovery = 74% Analysis Date = 03/23/16 Pct Recovery = 74% Analysis Date = 03/21/16 Pct Recovery = 74% Analysis Date = 03/21/16 Pct Recovery = 74% Analysis Date = 03/19/16 Pct Recovery = 74% Analysis Date = 03/19/16 Pct Recovery = 74% Analysis Date = 03/17/16 Pct Recovery = 74% Analysis Date = 03/17/16 Pct Recovery = 74% Analysis Date = 03/15/16 Pct Recovery = 74% Analysis Date = 03/15/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/12/16 Pct Recovery = 74% Analysis Date = 03/10/16 Pct Recovery = 74% Analysis Date = 03/10/16 Pct Recovery = 74% Analysis Date = 03/08/16 Pct Recovery = 74% Analysis Date = 03/08/16 Pct Recovery = 74% Analysis Date = 03/06/16 Pct Recovery = 74% Analysis Date = 03/06/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
METRIBUZIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 75% 7% 75% 8%
Total 19 75% 7% 75% 8%

Sample Statistics
METRIBUZIN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
MOLINATE
METHOD: 2033 , TESTIDCODE: 82671GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 112% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 115% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 123% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 119% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 103% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 115% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 135% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 117% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 105% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 122% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 113% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 98% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 108% Analysis Date = 05/10/17 Pct Recovery = 120% Analysis Date = 05/08/17 Pct Recovery = 120% Analysis Date = 05/08/17 Pct Recovery = 120% Analysis Date = 05/06/17 Pct Recovery = 120% Analysis Date = 05/06/17 Pct Recovery = 120% Analysis Date = 05/04/17 Pct Recovery = 120% Analysis Date = 05/04/17 Pct Recovery = 120% Analysis Date = 05/01/17 Pct Recovery = 120% Analysis Date = 05/01/17 Pct Recovery = 120% Analysis Date = 04/29/17 Pct Recovery = 120% Analysis Date = 04/29/17 Pct Recovery = 120% Analysis Date = 04/27/17 Pct Recovery = 120% Analysis Date = 04/27/17 Pct Recovery = 120% Analysis Date = 04/25/17 Pct Recovery = 120% Analysis Date = 04/25/17 Pct Recovery = 120% Analysis Date = 04/22/17 Pct Recovery = 120% Analysis Date = 04/22/17 Pct Recovery = 120% Analysis Date = 04/20/17 Pct Recovery = 120% Analysis Date = 04/20/17 Pct Recovery = 120% Analysis Date = 04/18/17 Pct Recovery = 120% Analysis Date = 04/18/17 Pct Recovery = 120% Analysis Date = 04/15/17 Pct Recovery = 120% Analysis Date = 04/15/17 Pct Recovery = 120% Analysis Date = 04/13/17 Pct Recovery = 119% Analysis Date = 04/13/17 Pct Recovery = 119% Analysis Date = 04/11/17 Pct Recovery = 119% Analysis Date = 04/11/17 Pct Recovery = 119% Analysis Date = 04/09/17 Pct Recovery = 119% Analysis Date = 04/09/17 Pct Recovery = 119% Analysis Date = 04/06/17 Pct Recovery = 119% Analysis Date = 04/06/17 Pct Recovery = 119% Analysis Date = 04/04/17 Pct Recovery = 119% Analysis Date = 04/04/17 Pct Recovery = 119% Analysis Date = 04/02/17 Pct Recovery = 119% Analysis Date = 04/02/17 Pct Recovery = 119% Analysis Date = 03/30/17 Pct Recovery = 119% Analysis Date = 03/30/17 Pct Recovery = 119% Analysis Date = 03/28/17 Pct Recovery = 119% Analysis Date = 03/28/17 Pct Recovery = 119% Analysis Date = 03/26/17 Pct Recovery = 119% Analysis Date = 03/26/17 Pct Recovery = 119% Analysis Date = 03/24/17 Pct Recovery = 119% Analysis Date = 03/24/17 Pct Recovery = 119% Analysis Date = 03/21/17 Pct Recovery = 119% Analysis Date = 03/21/17 Pct Recovery = 119% Analysis Date = 03/19/17 Pct Recovery = 119% Analysis Date = 03/19/17 Pct Recovery = 119% Analysis Date = 03/17/17 Pct Recovery = 119% Analysis Date = 03/17/17 Pct Recovery = 119% Analysis Date = 03/14/17 Pct Recovery = 119% Analysis Date = 03/14/17 Pct Recovery = 119% Analysis Date = 03/12/17 Pct Recovery = 118% Analysis Date = 03/12/17 Pct Recovery = 118% Analysis Date = 03/10/17 Pct Recovery = 118% Analysis Date = 03/10/17 Pct Recovery = 118% Analysis Date = 03/08/17 Pct Recovery = 118% Analysis Date = 03/08/17 Pct Recovery = 118% Analysis Date = 03/05/17 Pct Recovery = 118% Analysis Date = 03/05/17 Pct Recovery = 118% Analysis Date = 03/03/17 Pct Recovery = 118% Analysis Date = 03/03/17 Pct Recovery = 118% Analysis Date = 03/01/17 Pct Recovery = 118% Analysis Date = 03/01/17 Pct Recovery = 118% Analysis Date = 02/26/17 Pct Recovery = 118% Analysis Date = 02/26/17 Pct Recovery = 118% Analysis Date = 02/24/17 Pct Recovery = 118% Analysis Date = 02/24/17 Pct Recovery = 118% Analysis Date = 02/22/17 Pct Recovery = 118% Analysis Date = 02/22/17 Pct Recovery = 118% Analysis Date = 02/20/17 Pct Recovery = 117% Analysis Date = 02/20/17 Pct Recovery = 117% Analysis Date = 02/17/17 Pct Recovery = 117% Analysis Date = 02/17/17 Pct Recovery = 117% Analysis Date = 02/15/17 Pct Recovery = 117% Analysis Date = 02/15/17 Pct Recovery = 117% Analysis Date = 02/13/17 Pct Recovery = 117% Analysis Date = 02/13/17 Pct Recovery = 117% Analysis Date = 02/10/17 Pct Recovery = 116% Analysis Date = 02/10/17 Pct Recovery = 116% Analysis Date = 02/08/17 Pct Recovery = 116% Analysis Date = 02/08/17 Pct Recovery = 116% Analysis Date = 02/06/17 Pct Recovery = 116% Analysis Date = 02/06/17 Pct Recovery = 116% Analysis Date = 02/04/17 Pct Recovery = 115% Analysis Date = 02/04/17 Pct Recovery = 115% Analysis Date = 02/01/17 Pct Recovery = 115% Analysis Date = 02/01/17 Pct Recovery = 115% Analysis Date = 01/30/17 Pct Recovery = 115% Analysis Date = 01/30/17 Pct Recovery = 115% Analysis Date = 01/28/17 Pct Recovery = 115% Analysis Date = 01/28/17 Pct Recovery = 115% Analysis Date = 01/25/17 Pct Recovery = 114% Analysis Date = 01/25/17 Pct Recovery = 114% Analysis Date = 01/23/17 Pct Recovery = 114% Analysis Date = 01/23/17 Pct Recovery = 114% Analysis Date = 01/21/17 Pct Recovery = 114% Analysis Date = 01/21/17 Pct Recovery = 114% Analysis Date = 01/19/17 Pct Recovery = 113% Analysis Date = 01/19/17 Pct Recovery = 113% Analysis Date = 01/16/17 Pct Recovery = 113% Analysis Date = 01/16/17 Pct Recovery = 113% Analysis Date = 01/14/17 Pct Recovery = 113% Analysis Date = 01/14/17 Pct Recovery = 113% Analysis Date = 01/12/17 Pct Recovery = 113% Analysis Date = 01/12/17 Pct Recovery = 113% Analysis Date = 01/09/17 Pct Recovery = 113% Analysis Date = 01/09/17 Pct Recovery = 113% Analysis Date = 01/07/17 Pct Recovery = 112% Analysis Date = 01/07/17 Pct Recovery = 112% Analysis Date = 01/05/17 Pct Recovery = 112% Analysis Date = 01/05/17 Pct Recovery = 112% Analysis Date = 01/03/17 Pct Recovery = 112% Analysis Date = 01/03/17 Pct Recovery = 112% Analysis Date = 12/31/16 Pct Recovery = 112% Analysis Date = 12/31/16 Pct Recovery = 112% Analysis Date = 12/29/16 Pct Recovery = 112% Analysis Date = 12/29/16 Pct Recovery = 112% Analysis Date = 12/27/16 Pct Recovery = 112% Analysis Date = 12/27/16 Pct Recovery = 112% Analysis Date = 12/24/16 Pct Recovery = 111% Analysis Date = 12/24/16 Pct Recovery = 111% Analysis Date = 12/22/16 Pct Recovery = 111% Analysis Date = 12/22/16 Pct Recovery = 111% Analysis Date = 12/20/16 Pct Recovery = 111% Analysis Date = 12/20/16 Pct Recovery = 111% Analysis Date = 12/18/16 Pct Recovery = 111% Analysis Date = 12/18/16 Pct Recovery = 111% Analysis Date = 12/15/16 Pct Recovery = 111% Analysis Date = 12/15/16 Pct Recovery = 111% Analysis Date = 12/13/16 Pct Recovery = 111% Analysis Date = 12/13/16 Pct Recovery = 111% Analysis Date = 12/11/16 Pct Recovery = 110% Analysis Date = 12/11/16 Pct Recovery = 110% Analysis Date = 12/08/16 Pct Recovery = 110% Analysis Date = 12/08/16 Pct Recovery = 110% Analysis Date = 12/06/16 Pct Recovery = 110% Analysis Date = 12/06/16 Pct Recovery = 110% Analysis Date = 12/04/16 Pct Recovery = 110% Analysis Date = 12/04/16 Pct Recovery = 110% Analysis Date = 12/02/16 Pct Recovery = 110% Analysis Date = 12/02/16 Pct Recovery = 110% Analysis Date = 11/29/16 Pct Recovery = 110% Analysis Date = 11/29/16 Pct Recovery = 110% Analysis Date = 11/27/16 Pct Recovery = 109% Analysis Date = 11/27/16 Pct Recovery = 109% Analysis Date = 11/25/16 Pct Recovery = 109% Analysis Date = 11/25/16 Pct Recovery = 109% Analysis Date = 11/22/16 Pct Recovery = 109% Analysis Date = 11/22/16 Pct Recovery = 109% Analysis Date = 11/20/16 Pct Recovery = 109% Analysis Date = 11/20/16 Pct Recovery = 109% Analysis Date = 11/18/16 Pct Recovery = 109% Analysis Date = 11/18/16 Pct Recovery = 109% Analysis Date = 11/16/16 Pct Recovery = 109% Analysis Date = 11/16/16 Pct Recovery = 109% Analysis Date = 11/13/16 Pct Recovery = 108% Analysis Date = 11/13/16 Pct Recovery = 108% Analysis Date = 11/11/16 Pct Recovery = 108% Analysis Date = 11/11/16 Pct Recovery = 108% Analysis Date = 11/09/16 Pct Recovery = 108% Analysis Date = 11/09/16 Pct Recovery = 108% Analysis Date = 11/06/16 Pct Recovery = 108% Analysis Date = 11/06/16 Pct Recovery = 108% Analysis Date = 11/04/16 Pct Recovery = 108% Analysis Date = 11/04/16 Pct Recovery = 108% Analysis Date = 11/02/16 Pct Recovery = 108% Analysis Date = 11/02/16 Pct Recovery = 108% Analysis Date = 10/31/16 Pct Recovery = 107% Analysis Date = 10/31/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/26/16 Pct Recovery = 107% Analysis Date = 10/26/16 Pct Recovery = 107% Analysis Date = 10/24/16 Pct Recovery = 107% Analysis Date = 10/24/16 Pct Recovery = 107% Analysis Date = 10/21/16 Pct Recovery = 107% Analysis Date = 10/21/16 Pct Recovery = 107% Analysis Date = 10/19/16 Pct Recovery = 107% Analysis Date = 10/19/16 Pct Recovery = 107% Analysis Date = 10/17/16 Pct Recovery = 106% Analysis Date = 10/17/16 Pct Recovery = 106% Analysis Date = 10/15/16 Pct Recovery = 106% Analysis Date = 10/15/16 Pct Recovery = 106% Analysis Date = 10/12/16 Pct Recovery = 106% Analysis Date = 10/12/16 Pct Recovery = 106% Analysis Date = 10/10/16 Pct Recovery = 106% Analysis Date = 10/10/16 Pct Recovery = 106% Analysis Date = 10/08/16 Pct Recovery = 106% Analysis Date = 10/08/16 Pct Recovery = 106% Analysis Date = 10/05/16 Pct Recovery = 106% Analysis Date = 10/05/16 Pct Recovery = 106% Analysis Date = 10/03/16 Pct Recovery = 105% Analysis Date = 10/03/16 Pct Recovery = 105% Analysis Date = 10/01/16 Pct Recovery = 105% Analysis Date = 10/01/16 Pct Recovery = 105% Analysis Date = 09/29/16 Pct Recovery = 105% Analysis Date = 09/29/16 Pct Recovery = 105% Analysis Date = 09/26/16 Pct Recovery = 105% Analysis Date = 09/26/16 Pct Recovery = 105% Analysis Date = 09/24/16 Pct Recovery = 105% Analysis Date = 09/24/16 Pct Recovery = 105% Analysis Date = 09/22/16 Pct Recovery = 105% Analysis Date = 09/22/16 Pct Recovery = 105% Analysis Date = 09/19/16 Pct Recovery = 104% Analysis Date = 09/19/16 Pct Recovery = 104% Analysis Date = 09/17/16 Pct Recovery = 104% Analysis Date = 09/17/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/15/16 Pct Recovery = 104% Analysis Date = 09/13/16 Pct Recovery = 104% Analysis Date = 09/13/16 Pct Recovery = 104% Analysis Date = 09/10/16 Pct Recovery = 104% Analysis Date = 09/10/16 Pct Recovery = 104% Analysis Date = 09/08/16 Pct Recovery = 103% Analysis Date = 09/08/16 Pct Recovery = 103% Analysis Date = 09/06/16 Pct Recovery = 103% Analysis Date = 09/06/16 Pct Recovery = 103% Analysis Date = 09/03/16 Pct Recovery = 103% Analysis Date = 09/03/16 Pct Recovery = 103% Analysis Date = 09/01/16 Pct Recovery = 103% Analysis Date = 09/01/16 Pct Recovery = 103% Analysis Date = 08/30/16 Pct Recovery = 103% Analysis Date = 08/30/16 Pct Recovery = 103% Analysis Date = 08/28/16 Pct Recovery = 103% Analysis Date = 08/28/16 Pct Recovery = 103% Analysis Date = 08/25/16 Pct Recovery = 103% Analysis Date = 08/25/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 103% Analysis Date = 08/23/16 Pct Recovery = 103% Analysis Date = 08/21/16 Pct Recovery = 103% Analysis Date = 08/21/16 Pct Recovery = 103% Analysis Date = 08/18/16 Pct Recovery = 103% Analysis Date = 08/18/16 Pct Recovery = 103% Analysis Date = 08/16/16 Pct Recovery = 103% Analysis Date = 08/16/16 Pct Recovery = 103% Analysis Date = 08/14/16 Pct Recovery = 103% Analysis Date = 08/14/16 Pct Recovery = 103% Analysis Date = 08/12/16 Pct Recovery = 103% Analysis Date = 08/12/16 Pct Recovery = 103% Analysis Date = 08/09/16 Pct Recovery = 103% Analysis Date = 08/09/16 Pct Recovery = 103% Analysis Date = 08/07/16 Pct Recovery = 104% Analysis Date = 08/07/16 Pct Recovery = 104% Analysis Date = 08/05/16 Pct Recovery = 104% Analysis Date = 08/05/16 Pct Recovery = 104% Analysis Date = 08/02/16 Pct Recovery = 104% Analysis Date = 08/02/16 Pct Recovery = 104% Analysis Date = 07/31/16 Pct Recovery = 104% Analysis Date = 07/31/16 Pct Recovery = 104% Analysis Date = 07/29/16 Pct Recovery = 104% Analysis Date = 07/29/16 Pct Recovery = 104% Analysis Date = 07/27/16 Pct Recovery = 104% Analysis Date = 07/27/16 Pct Recovery = 104% Analysis Date = 07/24/16 Pct Recovery = 104% Analysis Date = 07/24/16 Pct Recovery = 104% Analysis Date = 07/22/16 Pct Recovery = 104% Analysis Date = 07/22/16 Pct Recovery = 104% Analysis Date = 07/20/16 Pct Recovery = 104% Analysis Date = 07/20/16 Pct Recovery = 104% Analysis Date = 07/17/16 Pct Recovery = 104% Analysis Date = 07/17/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 104% Analysis Date = 07/15/16 Pct Recovery = 104% Analysis Date = 07/13/16 Pct Recovery = 104% Analysis Date = 07/13/16 Pct Recovery = 104% Analysis Date = 07/11/16 Pct Recovery = 104% Analysis Date = 07/11/16 Pct Recovery = 104% Analysis Date = 07/08/16 Pct Recovery = 104% Analysis Date = 07/08/16 Pct Recovery = 104% Analysis Date = 07/06/16 Pct Recovery = 104% Analysis Date = 07/06/16 Pct Recovery = 104% Analysis Date = 07/04/16 Pct Recovery = 104% Analysis Date = 07/04/16 Pct Recovery = 104% Analysis Date = 07/01/16 Pct Recovery = 104% Analysis Date = 07/01/16 Pct Recovery = 104% Analysis Date = 06/29/16 Pct Recovery = 105% Analysis Date = 06/29/16 Pct Recovery = 105% Analysis Date = 06/27/16 Pct Recovery = 105% Analysis Date = 06/27/16 Pct Recovery = 105% Analysis Date = 06/25/16 Pct Recovery = 105% Analysis Date = 06/25/16 Pct Recovery = 105% Analysis Date = 06/22/16 Pct Recovery = 105% Analysis Date = 06/22/16 Pct Recovery = 105% Analysis Date = 06/20/16 Pct Recovery = 105% Analysis Date = 06/20/16 Pct Recovery = 105% Analysis Date = 06/18/16 Pct Recovery = 105% Analysis Date = 06/18/16 Pct Recovery = 105% Analysis Date = 06/15/16 Pct Recovery = 105% Analysis Date = 06/15/16 Pct Recovery = 105% Analysis Date = 06/13/16 Pct Recovery = 105% Analysis Date = 06/13/16 Pct Recovery = 105% Analysis Date = 06/11/16 Pct Recovery = 105% Analysis Date = 06/11/16 Pct Recovery = 105% Analysis Date = 06/09/16 Pct Recovery = 105% Analysis Date = 06/09/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/04/16 Pct Recovery = 105% Analysis Date = 06/04/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/26/16 Pct Recovery = 105% Analysis Date = 05/26/16 Pct Recovery = 105% Analysis Date = 05/24/16 Pct Recovery = 105% Analysis Date = 05/24/16 Pct Recovery = 105% Analysis Date = 05/21/16 Pct Recovery = 106% Analysis Date = 05/21/16 Pct Recovery = 106% Analysis Date = 05/19/16 Pct Recovery = 106% Analysis Date = 05/19/16 Pct Recovery = 106% Analysis Date = 05/17/16 Pct Recovery = 106% Analysis Date = 05/17/16 Pct Recovery = 106% Analysis Date = 05/14/16 Pct Recovery = 106% Analysis Date = 05/14/16 Pct Recovery = 106% Analysis Date = 05/12/16 Pct Recovery = 106% Analysis Date = 05/12/16 Pct Recovery = 106% Analysis Date = 05/10/16 Pct Recovery = 106% Analysis Date = 05/10/16 Pct Recovery = 106% Analysis Date = 05/08/16 Pct Recovery = 106% Analysis Date = 05/08/16 Pct Recovery = 106% Analysis Date = 05/05/16 Pct Recovery = 106% Analysis Date = 05/05/16 Pct Recovery = 106% Analysis Date = 05/03/16 Pct Recovery = 106% Analysis Date = 05/03/16 Pct Recovery = 106% Analysis Date = 05/01/16 Pct Recovery = 106% Analysis Date = 05/01/16 Pct Recovery = 106% Analysis Date = 04/28/16 Pct Recovery = 106% Analysis Date = 04/28/16 Pct Recovery = 106% Analysis Date = 04/26/16 Pct Recovery = 106% Analysis Date = 04/26/16 Pct Recovery = 106% Analysis Date = 04/24/16 Pct Recovery = 106% Analysis Date = 04/24/16 Pct Recovery = 106% Analysis Date = 04/22/16 Pct Recovery = 106% Analysis Date = 04/22/16 Pct Recovery = 106% Analysis Date = 04/19/16 Pct Recovery = 106% Analysis Date = 04/19/16 Pct Recovery = 106% Analysis Date = 04/17/16 Pct Recovery = 106% Analysis Date = 04/17/16 Pct Recovery = 106% Analysis Date = 04/15/16 Pct Recovery = 106% Analysis Date = 04/15/16 Pct Recovery = 106% Analysis Date = 04/12/16 Pct Recovery = 107% Analysis Date = 04/12/16 Pct Recovery = 107% Analysis Date = 04/10/16 Pct Recovery = 107% Analysis Date = 04/10/16 Pct Recovery = 107% Analysis Date = 04/08/16 Pct Recovery = 107% Analysis Date = 04/08/16 Pct Recovery = 107% Analysis Date = 04/06/16 Pct Recovery = 107% Analysis Date = 04/06/16 Pct Recovery = 107% Analysis Date = 04/03/16 Pct Recovery = 107% Analysis Date = 04/03/16 Pct Recovery = 107% Analysis Date = 04/01/16 Pct Recovery = 107% Analysis Date = 04/01/16 Pct Recovery = 107% Analysis Date = 03/30/16 Pct Recovery = 107% Analysis Date = 03/30/16 Pct Recovery = 107% Analysis Date = 03/27/16 Pct Recovery = 107% Analysis Date = 03/27/16 Pct Recovery = 107% Analysis Date = 03/25/16 Pct Recovery = 107% Analysis Date = 03/25/16 Pct Recovery = 107% Analysis Date = 03/23/16 Pct Recovery = 107% Analysis Date = 03/23/16 Pct Recovery = 107% Analysis Date = 03/21/16 Pct Recovery = 107% Analysis Date = 03/21/16 Pct Recovery = 107% Analysis Date = 03/18/16 Pct Recovery = 107% Analysis Date = 03/18/16 Pct Recovery = 107% Analysis Date = 03/16/16 Pct Recovery = 107% Analysis Date = 03/16/16 Pct Recovery = 107% Analysis Date = 03/14/16 Pct Recovery = 107% Analysis Date = 03/14/16 Pct Recovery = 107% Analysis Date = 03/11/16 Pct Recovery = 107% Analysis Date = 03/11/16 Pct Recovery = 107% Analysis Date = 03/09/16 Pct Recovery = 107% Analysis Date = 03/09/16 Pct Recovery = 107% Analysis Date = 03/07/16 Pct Recovery = 108% Analysis Date = 03/07/16 Pct Recovery = 108% Analysis Date = 03/05/16 Pct Recovery = 108% Analysis Date = 03/05/16 Pct Recovery = 108% Analysis Date = 03/02/16 Pct Recovery = 108% Analysis Date = 03/02/16 Pct Recovery = 108% Analysis Date = 02/29/16 Pct Recovery = 108% Analysis Date = 02/29/16 Pct Recovery = 108% Analysis Date = 02/27/16 Pct Recovery = 108% Analysis Date = 02/27/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/24/16 Pct Recovery = 108% Analysis Date = 02/22/16 Pct Recovery = 108% Analysis Date = 02/22/16 Pct Recovery = 108% Analysis Date = 02/20/16 Pct Recovery = 108% Analysis Date = 02/20/16 Pct Recovery = 108% Analysis Date = 02/18/16 Pct Recovery = 108% Analysis Date = 02/18/16 Pct Recovery = 108% Analysis Date = 02/15/16 Pct Recovery = 108% Analysis Date = 02/15/16 Pct Recovery = 108% Analysis Date = 02/13/16 Pct Recovery = 108% Analysis Date = 02/13/16 Pct Recovery = 108% Analysis Date = 02/11/16 Pct Recovery = 108% Analysis Date = 02/11/16 Pct Recovery = 108% Analysis Date = 02/09/16 Pct Recovery = 108% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MOLINATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 15 112% 12% 113% 10%
Total 15 112% 12% 113% 10%

Sample Statistics
MOLINATE

Characteristic N % % Basis
Plotted 15 83% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 2 11% Spiked
Spiked 18 .  
False Negatives 1 6% 1 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
MYCLOBUTANIL
METHOD: 2033 , TESTIDCODE: 61599GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 100% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 80% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 95% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 87% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 67% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 77% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 92% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 88% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 117% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 76% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 71% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 84% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 79% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 91% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 85% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 05/02/17 Pct Recovery = 97% Analysis Date = 04/30/17 Pct Recovery = 97% Analysis Date = 04/30/17 Pct Recovery = 97% Analysis Date = 04/28/17 Pct Recovery = 96% Analysis Date = 04/28/17 Pct Recovery = 96% Analysis Date = 04/26/17 Pct Recovery = 96% Analysis Date = 04/26/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 96% Analysis Date = 04/21/17 Pct Recovery = 96% Analysis Date = 04/21/17 Pct Recovery = 96% Analysis Date = 04/19/17 Pct Recovery = 96% Analysis Date = 04/19/17 Pct Recovery = 96% Analysis Date = 04/17/17 Pct Recovery = 96% Analysis Date = 04/17/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 95% Analysis Date = 04/12/17 Pct Recovery = 95% Analysis Date = 04/12/17 Pct Recovery = 95% Analysis Date = 04/10/17 Pct Recovery = 95% Analysis Date = 04/10/17 Pct Recovery = 95% Analysis Date = 04/08/17 Pct Recovery = 95% Analysis Date = 04/08/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/06/17 Pct Recovery = 95% Analysis Date = 04/03/17 Pct Recovery = 95% Analysis Date = 04/03/17 Pct Recovery = 95% Analysis Date = 04/01/17 Pct Recovery = 95% Analysis Date = 04/01/17 Pct Recovery = 95% Analysis Date = 03/30/17 Pct Recovery = 94% Analysis Date = 03/30/17 Pct Recovery = 94% Analysis Date = 03/28/17 Pct Recovery = 94% Analysis Date = 03/28/17 Pct Recovery = 94% Analysis Date = 03/25/17 Pct Recovery = 94% Analysis Date = 03/25/17 Pct Recovery = 94% Analysis Date = 03/23/17 Pct Recovery = 94% Analysis Date = 03/23/17 Pct Recovery = 94% Analysis Date = 03/21/17 Pct Recovery = 94% Analysis Date = 03/21/17 Pct Recovery = 94% Analysis Date = 03/19/17 Pct Recovery = 94% Analysis Date = 03/19/17 Pct Recovery = 94% Analysis Date = 03/16/17 Pct Recovery = 93% Analysis Date = 03/16/17 Pct Recovery = 93% Analysis Date = 03/14/17 Pct Recovery = 93% Analysis Date = 03/14/17 Pct Recovery = 93% Analysis Date = 03/12/17 Pct Recovery = 93% Analysis Date = 03/12/17 Pct Recovery = 93% Analysis Date = 03/10/17 Pct Recovery = 93% Analysis Date = 03/10/17 Pct Recovery = 93% Analysis Date = 03/07/17 Pct Recovery = 93% Analysis Date = 03/07/17 Pct Recovery = 93% Analysis Date = 03/05/17 Pct Recovery = 92% Analysis Date = 03/05/17 Pct Recovery = 92% Analysis Date = 03/03/17 Pct Recovery = 92% Analysis Date = 03/03/17 Pct Recovery = 92% Analysis Date = 03/01/17 Pct Recovery = 92% Analysis Date = 03/01/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/26/17 Pct Recovery = 92% Analysis Date = 02/24/17 Pct Recovery = 92% Analysis Date = 02/24/17 Pct Recovery = 92% Analysis Date = 02/22/17 Pct Recovery = 91% Analysis Date = 02/22/17 Pct Recovery = 91% Analysis Date = 02/20/17 Pct Recovery = 91% Analysis Date = 02/20/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/11/17 Pct Recovery = 90% Analysis Date = 02/11/17 Pct Recovery = 90% Analysis Date = 02/08/17 Pct Recovery = 90% Analysis Date = 02/08/17 Pct Recovery = 90% Analysis Date = 02/06/17 Pct Recovery = 89% Analysis Date = 02/06/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/04/17 Pct Recovery = 89% Analysis Date = 02/02/17 Pct Recovery = 89% Analysis Date = 02/02/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/30/17 Pct Recovery = 89% Analysis Date = 01/28/17 Pct Recovery = 88% Analysis Date = 01/28/17 Pct Recovery = 88% Analysis Date = 01/26/17 Pct Recovery = 88% Analysis Date = 01/26/17 Pct Recovery = 88% Analysis Date = 01/24/17 Pct Recovery = 88% Analysis Date = 01/24/17 Pct Recovery = 88% Analysis Date = 01/21/17 Pct Recovery = 87% Analysis Date = 01/21/17 Pct Recovery = 87% Analysis Date = 01/19/17 Pct Recovery = 87% Analysis Date = 01/19/17 Pct Recovery = 87% Analysis Date = 01/17/17 Pct Recovery = 87% Analysis Date = 01/17/17 Pct Recovery = 87% Analysis Date = 01/15/17 Pct Recovery = 86% Analysis Date = 01/15/17 Pct Recovery = 86% Analysis Date = 01/12/17 Pct Recovery = 86% Analysis Date = 01/12/17 Pct Recovery = 86% Analysis Date = 01/10/17 Pct Recovery = 86% Analysis Date = 01/10/17 Pct Recovery = 86% Analysis Date = 01/08/17 Pct Recovery = 86% Analysis Date = 01/08/17 Pct Recovery = 86% Analysis Date = 01/06/17 Pct Recovery = 85% Analysis Date = 01/06/17 Pct Recovery = 85% Analysis Date = 01/04/17 Pct Recovery = 85% Analysis Date = 01/04/17 Pct Recovery = 85% Analysis Date = 01/01/17 Pct Recovery = 85% Analysis Date = 01/01/17 Pct Recovery = 85% Analysis Date = 12/30/16 Pct Recovery = 84% Analysis Date = 12/30/16 Pct Recovery = 84% Analysis Date = 12/28/16 Pct Recovery = 84% Analysis Date = 12/28/16 Pct Recovery = 84% Analysis Date = 12/26/16 Pct Recovery = 84% Analysis Date = 12/26/16 Pct Recovery = 84% Analysis Date = 12/23/16 Pct Recovery = 84% Analysis Date = 12/23/16 Pct Recovery = 84% Analysis Date = 12/21/16 Pct Recovery = 83% Analysis Date = 12/21/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/19/16 Pct Recovery = 83% Analysis Date = 12/17/16 Pct Recovery = 83% Analysis Date = 12/17/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/14/16 Pct Recovery = 83% Analysis Date = 12/12/16 Pct Recovery = 82% Analysis Date = 12/12/16 Pct Recovery = 82% Analysis Date = 12/10/16 Pct Recovery = 82% Analysis Date = 12/10/16 Pct Recovery = 82% Analysis Date = 12/08/16 Pct Recovery = 82% Analysis Date = 12/08/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/05/16 Pct Recovery = 82% Analysis Date = 12/03/16 Pct Recovery = 82% Analysis Date = 12/03/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 12/01/16 Pct Recovery = 82% Analysis Date = 11/29/16 Pct Recovery = 81% Analysis Date = 11/29/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/26/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/24/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/22/16 Pct Recovery = 81% Analysis Date = 11/20/16 Pct Recovery = 81% Analysis Date = 11/20/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/17/16 Pct Recovery = 81% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/08/16 Pct Recovery = 80% Analysis Date = 11/08/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 80% Analysis Date = 11/06/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 11/02/16 Pct Recovery = 79% Analysis Date = 10/30/16 Pct Recovery = 79% Analysis Date = 10/30/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/28/16 Pct Recovery = 79% Analysis Date = 10/26/16 Pct Recovery = 79% Analysis Date = 10/26/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/24/16 Pct Recovery = 79% Analysis Date = 10/21/16 Pct Recovery = 79% Analysis Date = 10/21/16 Pct Recovery = 79% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/19/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/17/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/15/16 Pct Recovery = 78% Analysis Date = 10/12/16 Pct Recovery = 78% Analysis Date = 10/12/16 Pct Recovery = 78% Analysis Date = 10/10/16 Pct Recovery = 78% Analysis Date = 10/10/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/08/16 Pct Recovery = 78% Analysis Date = 10/06/16 Pct Recovery = 77% Analysis Date = 10/06/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 77% Analysis Date = 10/03/16 Pct Recovery = 77% Analysis Date = 10/01/16 Pct Recovery = 77% Analysis Date = 10/01/16 Pct Recovery = 77% Analysis Date = 09/29/16 Pct Recovery = 77% Analysis Date = 09/29/16 Pct Recovery = 77% Analysis Date = 09/27/16 Pct Recovery = 77% Analysis Date = 09/27/16 Pct Recovery = 77% Analysis Date = 09/24/16 Pct Recovery = 77% Analysis Date = 09/24/16 Pct Recovery = 77% Analysis Date = 09/22/16 Pct Recovery = 76% Analysis Date = 09/22/16 Pct Recovery = 76% Analysis Date = 09/20/16 Pct Recovery = 76% Analysis Date = 09/20/16 Pct Recovery = 76% Analysis Date = 09/18/16 Pct Recovery = 76% Analysis Date = 09/18/16 Pct Recovery = 76% Analysis Date = 09/16/16 Pct Recovery = 76% Analysis Date = 09/16/16 Pct Recovery = 76% Analysis Date = 09/13/16 Pct Recovery = 76% Analysis Date = 09/13/16 Pct Recovery = 76% Analysis Date = 09/11/16 Pct Recovery = 75% Analysis Date = 09/11/16 Pct Recovery = 75% Analysis Date = 09/09/16 Pct Recovery = 75% Analysis Date = 09/09/16 Pct Recovery = 75% Analysis Date = 09/07/16 Pct Recovery = 75% Analysis Date = 09/07/16 Pct Recovery = 75% Analysis Date = 09/04/16 Pct Recovery = 75% Analysis Date = 09/04/16 Pct Recovery = 75% Analysis Date = 09/02/16 Pct Recovery = 75% Analysis Date = 09/02/16 Pct Recovery = 75% Analysis Date = 08/31/16 Pct Recovery = 75% Analysis Date = 08/31/16 Pct Recovery = 75% Analysis Date = 08/29/16 Pct Recovery = 75% Analysis Date = 08/29/16 Pct Recovery = 75% Analysis Date = 08/26/16 Pct Recovery = 75% Analysis Date = 08/26/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/22/16 Pct Recovery = 75% Analysis Date = 08/22/16 Pct Recovery = 75% Analysis Date = 08/20/16 Pct Recovery = 75% Analysis Date = 08/20/16 Pct Recovery = 75% Analysis Date = 08/17/16 Pct Recovery = 75% Analysis Date = 08/17/16 Pct Recovery = 75% Analysis Date = 08/15/16 Pct Recovery = 75% Analysis Date = 08/15/16 Pct Recovery = 75% Analysis Date = 08/13/16 Pct Recovery = 75% Analysis Date = 08/13/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/08/16 Pct Recovery = 76% Analysis Date = 08/08/16 Pct Recovery = 76% Analysis Date = 08/06/16 Pct Recovery = 76% Analysis Date = 08/06/16 Pct Recovery = 76% Analysis Date = 08/04/16 Pct Recovery = 76% Analysis Date = 08/04/16 Pct Recovery = 76% Analysis Date = 08/02/16 Pct Recovery = 76% Analysis Date = 08/02/16 Pct Recovery = 76% Analysis Date = 07/30/16 Pct Recovery = 76% Analysis Date = 07/30/16 Pct Recovery = 76% Analysis Date = 07/28/16 Pct Recovery = 76% Analysis Date = 07/28/16 Pct Recovery = 76% Analysis Date = 07/26/16 Pct Recovery = 76% Analysis Date = 07/26/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 76% Analysis Date = 07/24/16 Pct Recovery = 76% Analysis Date = 07/21/16 Pct Recovery = 76% Analysis Date = 07/21/16 Pct Recovery = 76% Analysis Date = 07/19/16 Pct Recovery = 76% Analysis Date = 07/19/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/15/16 Pct Recovery = 76% Analysis Date = 07/15/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 77% Analysis Date = 07/12/16 Pct Recovery = 77% Analysis Date = 07/10/16 Pct Recovery = 77% Analysis Date = 07/10/16 Pct Recovery = 77% Analysis Date = 07/08/16 Pct Recovery = 77% Analysis Date = 07/08/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/06/16 Pct Recovery = 77% Analysis Date = 07/03/16 Pct Recovery = 77% Analysis Date = 07/03/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 06/29/16 Pct Recovery = 77% Analysis Date = 06/29/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/27/16 Pct Recovery = 77% Analysis Date = 06/24/16 Pct Recovery = 77% Analysis Date = 06/24/16 Pct Recovery = 77% Analysis Date = 06/22/16 Pct Recovery = 77% Analysis Date = 06/22/16 Pct Recovery = 77% Analysis Date = 06/20/16 Pct Recovery = 77% Analysis Date = 06/20/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/18/16 Pct Recovery = 77% Analysis Date = 06/15/16 Pct Recovery = 78% Analysis Date = 06/15/16 Pct Recovery = 78% Analysis Date = 06/13/16 Pct Recovery = 78% Analysis Date = 06/13/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/09/16 Pct Recovery = 78% Analysis Date = 06/09/16 Pct Recovery = 78% Analysis Date = 06/06/16 Pct Recovery = 78% Analysis Date = 06/06/16 Pct Recovery = 78% Analysis Date = 06/04/16 Pct Recovery = 78% Analysis Date = 06/04/16 Pct Recovery = 78% Analysis Date = 06/02/16 Pct Recovery = 78% Analysis Date = 06/02/16 Pct Recovery = 78% Analysis Date = 05/31/16 Pct Recovery = 78% Analysis Date = 05/31/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 78% Analysis Date = 05/29/16 Pct Recovery = 78% Analysis Date = 05/26/16 Pct Recovery = 78% Analysis Date = 05/26/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/24/16 Pct Recovery = 78% Analysis Date = 05/22/16 Pct Recovery = 79% Analysis Date = 05/22/16 Pct Recovery = 79% Analysis Date = 05/20/16 Pct Recovery = 79% Analysis Date = 05/20/16 Pct Recovery = 79% Analysis Date = 05/17/16 Pct Recovery = 79% Analysis Date = 05/17/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 79% Analysis Date = 05/15/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/13/16 Pct Recovery = 79% Analysis Date = 05/11/16 Pct Recovery = 80% Analysis Date = 05/11/16 Pct Recovery = 80% Analysis Date = 05/08/16 Pct Recovery = 80% Analysis Date = 05/08/16 Pct Recovery = 80% Analysis Date = 05/06/16 Pct Recovery = 80% Analysis Date = 05/06/16 Pct Recovery = 80% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/04/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 05/02/16 Pct Recovery = 80% Analysis Date = 04/29/16 Pct Recovery = 81% Analysis Date = 04/29/16 Pct Recovery = 81% Analysis Date = 04/27/16 Pct Recovery = 81% Analysis Date = 04/27/16 Pct Recovery = 81% Analysis Date = 04/25/16 Pct Recovery = 82% Analysis Date = 04/25/16 Pct Recovery = 82% Analysis Date = 04/23/16 Pct Recovery = 82% Analysis Date = 04/23/16 Pct Recovery = 82% Analysis Date = 04/20/16 Pct Recovery = 82% Analysis Date = 04/20/16 Pct Recovery = 82% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/18/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 83% Analysis Date = 04/16/16 Pct Recovery = 83% Analysis Date = 04/14/16 Pct Recovery = 83% Analysis Date = 04/14/16 Pct Recovery = 83% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/11/16 Pct Recovery = 84% Analysis Date = 04/09/16 Pct Recovery = 84% Analysis Date = 04/09/16 Pct Recovery = 84% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/07/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/05/16 Pct Recovery = 85% Analysis Date = 04/02/16 Pct Recovery = 85% Analysis Date = 04/02/16 Pct Recovery = 85% Analysis Date = 03/31/16 Pct Recovery = 86% Analysis Date = 03/31/16 Pct Recovery = 86% Analysis Date = 03/29/16 Pct Recovery = 86% Analysis Date = 03/29/16 Pct Recovery = 86% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 87% Analysis Date = 03/24/16 Pct Recovery = 87% Analysis Date = 03/22/16 Pct Recovery = 88% Analysis Date = 03/22/16 Pct Recovery = 88% Analysis Date = 03/20/16 Pct Recovery = 88% Analysis Date = 03/20/16 Pct Recovery = 88% Analysis Date = 03/18/16 Pct Recovery = 88% Analysis Date = 03/18/16 Pct Recovery = 88% Analysis Date = 03/15/16 Pct Recovery = 89% Analysis Date = 03/15/16 Pct Recovery = 89% Analysis Date = 03/13/16 Pct Recovery = 89% Analysis Date = 03/13/16 Pct Recovery = 89% Analysis Date = 03/11/16 Pct Recovery = 90% Analysis Date = 03/11/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/06/16 Pct Recovery = 90% Analysis Date = 03/06/16 Pct Recovery = 90% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/04/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Analysis Date = 03/02/16 Pct Recovery = 91% Analysis Date = 02/29/16 Pct Recovery = 92% Analysis Date = 02/29/16 Pct Recovery = 92% Analysis Date = 02/26/16 Pct Recovery = 92% Analysis Date = 02/26/16 Pct Recovery = 92% Analysis Date = 02/24/16 Pct Recovery = 92% Analysis Date = 02/24/16 Pct Recovery = 92% Analysis Date = 02/22/16 Pct Recovery = 93% Analysis Date = 02/22/16 Pct Recovery = 93% Analysis Date = 02/20/16 Pct Recovery = 93% Analysis Date = 02/20/16 Pct Recovery = 93% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/17/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 95% Analysis Date = 02/13/16 Pct Recovery = 95% Analysis Date = 02/11/16 Pct Recovery = 95% Analysis Date = 02/11/16 Pct Recovery = 95% Analysis Date = 02/09/16 Pct Recovery = 95% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
MYCLOBUTANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 85% 12% 84% 12%
Total 19 85% 12% 84% 12%

Sample Statistics
MYCLOBUTANIL

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
OXYFLUORFEN
METHOD: 2033 , TESTIDCODE: 61600GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 97% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 86% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 103% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 90% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 73% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 89% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 102% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 103% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 78% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 86% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 94% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 101% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 137% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 178% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 93% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 95% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 71% Analysis Date = 05/10/17 Pct Recovery = 94% Analysis Date = 05/08/17 Pct Recovery = 94% Analysis Date = 05/08/17 Pct Recovery = 94% Analysis Date = 05/06/17 Pct Recovery = 95% Analysis Date = 05/06/17 Pct Recovery = 95% Analysis Date = 05/04/17 Pct Recovery = 95% Analysis Date = 05/04/17 Pct Recovery = 95% Analysis Date = 05/01/17 Pct Recovery = 95% Analysis Date = 05/01/17 Pct Recovery = 95% Analysis Date = 04/29/17 Pct Recovery = 95% Analysis Date = 04/29/17 Pct Recovery = 95% Analysis Date = 04/27/17 Pct Recovery = 95% Analysis Date = 04/27/17 Pct Recovery = 95% Analysis Date = 04/25/17 Pct Recovery = 95% Analysis Date = 04/25/17 Pct Recovery = 95% Analysis Date = 04/22/17 Pct Recovery = 95% Analysis Date = 04/22/17 Pct Recovery = 95% Analysis Date = 04/20/17 Pct Recovery = 95% Analysis Date = 04/20/17 Pct Recovery = 95% Analysis Date = 04/18/17 Pct Recovery = 95% Analysis Date = 04/18/17 Pct Recovery = 95% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/11/17 Pct Recovery = 96% Analysis Date = 04/11/17 Pct Recovery = 96% Analysis Date = 04/09/17 Pct Recovery = 96% Analysis Date = 04/09/17 Pct Recovery = 96% Analysis Date = 04/06/17 Pct Recovery = 96% Analysis Date = 04/06/17 Pct Recovery = 96% Analysis Date = 04/04/17 Pct Recovery = 96% Analysis Date = 04/04/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 96% Analysis Date = 04/02/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/30/17 Pct Recovery = 96% Analysis Date = 03/28/17 Pct Recovery = 96% Analysis Date = 03/28/17 Pct Recovery = 96% Analysis Date = 03/26/17 Pct Recovery = 97% Analysis Date = 03/26/17 Pct Recovery = 97% Analysis Date = 03/24/17 Pct Recovery = 97% Analysis Date = 03/24/17 Pct Recovery = 97% Analysis Date = 03/21/17 Pct Recovery = 97% Analysis Date = 03/21/17 Pct Recovery = 97% Analysis Date = 03/19/17 Pct Recovery = 97% Analysis Date = 03/19/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 97% Analysis Date = 03/10/17 Pct Recovery = 97% Analysis Date = 03/10/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/08/17 Pct Recovery = 97% Analysis Date = 03/05/17 Pct Recovery = 97% Analysis Date = 03/05/17 Pct Recovery = 97% Analysis Date = 03/03/17 Pct Recovery = 98% Analysis Date = 03/03/17 Pct Recovery = 98% Analysis Date = 03/01/17 Pct Recovery = 98% Analysis Date = 03/01/17 Pct Recovery = 98% Analysis Date = 02/26/17 Pct Recovery = 98% Analysis Date = 02/26/17 Pct Recovery = 98% Analysis Date = 02/24/17 Pct Recovery = 98% Analysis Date = 02/24/17 Pct Recovery = 98% Analysis Date = 02/22/17 Pct Recovery = 98% Analysis Date = 02/22/17 Pct Recovery = 98% Analysis Date = 02/20/17 Pct Recovery = 98% Analysis Date = 02/20/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/17/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/15/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/13/17 Pct Recovery = 98% Analysis Date = 02/10/17 Pct Recovery = 98% Analysis Date = 02/10/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/08/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/06/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/04/17 Pct Recovery = 98% Analysis Date = 02/01/17 Pct Recovery = 98% Analysis Date = 02/01/17 Pct Recovery = 98% Analysis Date = 01/30/17 Pct Recovery = 98% Analysis Date = 01/30/17 Pct Recovery = 98% Analysis Date = 01/28/17 Pct Recovery = 98% Analysis Date = 01/28/17 Pct Recovery = 98% Analysis Date = 01/25/17 Pct Recovery = 98% Analysis Date = 01/25/17 Pct Recovery = 98% Analysis Date = 01/23/17 Pct Recovery = 98% Analysis Date = 01/23/17 Pct Recovery = 98% Analysis Date = 01/21/17 Pct Recovery = 98% Analysis Date = 01/21/17 Pct Recovery = 98% Analysis Date = 01/19/17 Pct Recovery = 98% Analysis Date = 01/19/17 Pct Recovery = 98% Analysis Date = 01/16/17 Pct Recovery = 98% Analysis Date = 01/16/17 Pct Recovery = 98% Analysis Date = 01/14/17 Pct Recovery = 98% Analysis Date = 01/14/17 Pct Recovery = 98% Analysis Date = 01/12/17 Pct Recovery = 99% Analysis Date = 01/12/17 Pct Recovery = 99% Analysis Date = 01/09/17 Pct Recovery = 99% Analysis Date = 01/09/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/05/17 Pct Recovery = 99% Analysis Date = 01/05/17 Pct Recovery = 99% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 100% Analysis Date = 12/31/16 Pct Recovery = 100% Analysis Date = 12/29/16 Pct Recovery = 100% Analysis Date = 12/29/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/27/16 Pct Recovery = 100% Analysis Date = 12/24/16 Pct Recovery = 101% Analysis Date = 12/24/16 Pct Recovery = 101% Analysis Date = 12/22/16 Pct Recovery = 101% Analysis Date = 12/22/16 Pct Recovery = 101% Analysis Date = 12/20/16 Pct Recovery = 101% Analysis Date = 12/20/16 Pct Recovery = 101% Analysis Date = 12/18/16 Pct Recovery = 101% Analysis Date = 12/18/16 Pct Recovery = 101% Analysis Date = 12/15/16 Pct Recovery = 102% Analysis Date = 12/15/16 Pct Recovery = 102% Analysis Date = 12/13/16 Pct Recovery = 102% Analysis Date = 12/13/16 Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 102% Analysis Date = 12/11/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/08/16 Pct Recovery = 102% Analysis Date = 12/06/16 Pct Recovery = 103% Analysis Date = 12/06/16 Pct Recovery = 103% Analysis Date = 12/04/16 Pct Recovery = 103% Analysis Date = 12/04/16 Pct Recovery = 103% Analysis Date = 12/02/16 Pct Recovery = 103% Analysis Date = 12/02/16 Pct Recovery = 103% Analysis Date = 11/29/16 Pct Recovery = 103% Analysis Date = 11/29/16 Pct Recovery = 103% Analysis Date = 11/27/16 Pct Recovery = 104% Analysis Date = 11/27/16 Pct Recovery = 104% Analysis Date = 11/25/16 Pct Recovery = 104% Analysis Date = 11/25/16 Pct Recovery = 104% Analysis Date = 11/22/16 Pct Recovery = 104% Analysis Date = 11/22/16 Pct Recovery = 104% Analysis Date = 11/20/16 Pct Recovery = 104% Analysis Date = 11/20/16 Pct Recovery = 104% Analysis Date = 11/18/16 Pct Recovery = 105% Analysis Date = 11/18/16 Pct Recovery = 105% Analysis Date = 11/16/16 Pct Recovery = 105% Analysis Date = 11/16/16 Pct Recovery = 105% Analysis Date = 11/13/16 Pct Recovery = 105% Analysis Date = 11/13/16 Pct Recovery = 105% Analysis Date = 11/11/16 Pct Recovery = 105% Analysis Date = 11/11/16 Pct Recovery = 105% Analysis Date = 11/09/16 Pct Recovery = 105% Analysis Date = 11/09/16 Pct Recovery = 105% Analysis Date = 11/06/16 Pct Recovery = 106% Analysis Date = 11/06/16 Pct Recovery = 106% Analysis Date = 11/04/16 Pct Recovery = 106% Analysis Date = 11/04/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 11/02/16 Pct Recovery = 106% Analysis Date = 10/31/16 Pct Recovery = 106% Analysis Date = 10/31/16 Pct Recovery = 106% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/26/16 Pct Recovery = 107% Analysis Date = 10/26/16 Pct Recovery = 107% Analysis Date = 10/24/16 Pct Recovery = 107% Analysis Date = 10/24/16 Pct Recovery = 107% Analysis Date = 10/21/16 Pct Recovery = 107% Analysis Date = 10/21/16 Pct Recovery = 107% Analysis Date = 10/19/16 Pct Recovery = 108% Analysis Date = 10/19/16 Pct Recovery = 108% Analysis Date = 10/17/16 Pct Recovery = 108% Analysis Date = 10/17/16 Pct Recovery = 108% Analysis Date = 10/15/16 Pct Recovery = 108% Analysis Date = 10/15/16 Pct Recovery = 108% Analysis Date = 10/12/16 Pct Recovery = 108% Analysis Date = 10/12/16 Pct Recovery = 108% Analysis Date = 10/10/16 Pct Recovery = 109% Analysis Date = 10/10/16 Pct Recovery = 109% Analysis Date = 10/08/16 Pct Recovery = 109% Analysis Date = 10/08/16 Pct Recovery = 109% Analysis Date = 10/05/16 Pct Recovery = 109% Analysis Date = 10/05/16 Pct Recovery = 109% Analysis Date = 10/03/16 Pct Recovery = 109% Analysis Date = 10/03/16 Pct Recovery = 109% Analysis Date = 10/01/16 Pct Recovery = 110% Analysis Date = 10/01/16 Pct Recovery = 110% Analysis Date = 09/29/16 Pct Recovery = 110% Analysis Date = 09/29/16 Pct Recovery = 110% Analysis Date = 09/26/16 Pct Recovery = 110% Analysis Date = 09/26/16 Pct Recovery = 110% Analysis Date = 09/24/16 Pct Recovery = 110% Analysis Date = 09/24/16 Pct Recovery = 110% Analysis Date = 09/22/16 Pct Recovery = 111% Analysis Date = 09/22/16 Pct Recovery = 111% Analysis Date = 09/19/16 Pct Recovery = 111% Analysis Date = 09/19/16 Pct Recovery = 111% Analysis Date = 09/17/16 Pct Recovery = 111% Analysis Date = 09/17/16 Pct Recovery = 111% Analysis Date = 09/15/16 Pct Recovery = 111% Analysis Date = 09/15/16 Pct Recovery = 111% Analysis Date = 09/13/16 Pct Recovery = 111% Analysis Date = 09/13/16 Pct Recovery = 111% Analysis Date = 09/10/16 Pct Recovery = 111% Analysis Date = 09/10/16 Pct Recovery = 111% Analysis Date = 09/08/16 Pct Recovery = 111% Analysis Date = 09/08/16 Pct Recovery = 111% Analysis Date = 09/06/16 Pct Recovery = 110% Analysis Date = 09/06/16 Pct Recovery = 110% Analysis Date = 09/03/16 Pct Recovery = 110% Analysis Date = 09/03/16 Pct Recovery = 110% Analysis Date = 09/01/16 Pct Recovery = 110% Analysis Date = 09/01/16 Pct Recovery = 110% Analysis Date = 08/30/16 Pct Recovery = 109% Analysis Date = 08/30/16 Pct Recovery = 109% Analysis Date = 08/28/16 Pct Recovery = 109% Analysis Date = 08/28/16 Pct Recovery = 109% Analysis Date = 08/25/16 Pct Recovery = 109% Analysis Date = 08/25/16 Pct Recovery = 109% Analysis Date = 08/23/16 Pct Recovery = 108% Analysis Date = 08/23/16 Pct Recovery = 108% Analysis Date = 08/21/16 Pct Recovery = 108% Analysis Date = 08/21/16 Pct Recovery = 108% Analysis Date = 08/18/16 Pct Recovery = 108% Analysis Date = 08/18/16 Pct Recovery = 108% Analysis Date = 08/16/16 Pct Recovery = 107% Analysis Date = 08/16/16 Pct Recovery = 107% Analysis Date = 08/14/16 Pct Recovery = 107% Analysis Date = 08/14/16 Pct Recovery = 107% Analysis Date = 08/12/16 Pct Recovery = 107% Analysis Date = 08/12/16 Pct Recovery = 107% Analysis Date = 08/09/16 Pct Recovery = 106% Analysis Date = 08/09/16 Pct Recovery = 106% Analysis Date = 08/07/16 Pct Recovery = 106% Analysis Date = 08/07/16 Pct Recovery = 106% Analysis Date = 08/05/16 Pct Recovery = 106% Analysis Date = 08/05/16 Pct Recovery = 106% Analysis Date = 08/02/16 Pct Recovery = 105% Analysis Date = 08/02/16 Pct Recovery = 105% Analysis Date = 07/31/16 Pct Recovery = 105% Analysis Date = 07/31/16 Pct Recovery = 105% Analysis Date = 07/29/16 Pct Recovery = 104% Analysis Date = 07/29/16 Pct Recovery = 104% Analysis Date = 07/27/16 Pct Recovery = 104% Analysis Date = 07/27/16 Pct Recovery = 104% Analysis Date = 07/24/16 Pct Recovery = 104% Analysis Date = 07/24/16 Pct Recovery = 104% Analysis Date = 07/22/16 Pct Recovery = 103% Analysis Date = 07/22/16 Pct Recovery = 103% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/20/16 Pct Recovery = 103% Analysis Date = 07/17/16 Pct Recovery = 103% Analysis Date = 07/17/16 Pct Recovery = 103% Analysis Date = 07/15/16 Pct Recovery = 102% Analysis Date = 07/15/16 Pct Recovery = 102% Analysis Date = 07/13/16 Pct Recovery = 102% Analysis Date = 07/13/16 Pct Recovery = 102% Analysis Date = 07/11/16 Pct Recovery = 101% Analysis Date = 07/11/16 Pct Recovery = 101% Analysis Date = 07/08/16 Pct Recovery = 101% Analysis Date = 07/08/16 Pct Recovery = 101% Analysis Date = 07/06/16 Pct Recovery = 101% Analysis Date = 07/06/16 Pct Recovery = 101% Analysis Date = 07/04/16 Pct Recovery = 100% Analysis Date = 07/04/16 Pct Recovery = 100% Analysis Date = 07/01/16 Pct Recovery = 100% Analysis Date = 07/01/16 Pct Recovery = 100% Analysis Date = 06/29/16 Pct Recovery = 100% Analysis Date = 06/29/16 Pct Recovery = 100% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/25/16 Pct Recovery = 99% Analysis Date = 06/25/16 Pct Recovery = 99% Analysis Date = 06/22/16 Pct Recovery = 98% Analysis Date = 06/22/16 Pct Recovery = 98% Analysis Date = 06/20/16 Pct Recovery = 98% Analysis Date = 06/20/16 Pct Recovery = 98% Analysis Date = 06/18/16 Pct Recovery = 98% Analysis Date = 06/18/16 Pct Recovery = 98% Analysis Date = 06/15/16 Pct Recovery = 97% Analysis Date = 06/15/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/13/16 Pct Recovery = 97% Analysis Date = 06/11/16 Pct Recovery = 97% Analysis Date = 06/11/16 Pct Recovery = 97% Analysis Date = 06/09/16 Pct Recovery = 96% Analysis Date = 06/09/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 96% Analysis Date = 06/06/16 Pct Recovery = 96% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 06/04/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 95% Analysis Date = 06/02/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/30/16 Pct Recovery = 95% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/28/16 Pct Recovery = 94% Analysis Date = 05/26/16 Pct Recovery = 94% Analysis Date = 05/26/16 Pct Recovery = 94% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/24/16 Pct Recovery = 94% Analysis Date = 05/21/16 Pct Recovery = 93% Analysis Date = 05/21/16 Pct Recovery = 93% Analysis Date = 05/19/16 Pct Recovery = 93% Analysis Date = 05/19/16 Pct Recovery = 93% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/17/16 Pct Recovery = 92% Analysis Date = 05/14/16 Pct Recovery = 92% Analysis Date = 05/14/16 Pct Recovery = 92% Analysis Date = 05/12/16 Pct Recovery = 92% Analysis Date = 05/12/16 Pct Recovery = 92% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/10/16 Pct Recovery = 91% Analysis Date = 05/08/16 Pct Recovery = 91% Analysis Date = 05/08/16 Pct Recovery = 91% Analysis Date = 05/05/16 Pct Recovery = 91% Analysis Date = 05/05/16 Pct Recovery = 91% Analysis Date = 05/03/16 Pct Recovery = 90% Analysis Date = 05/03/16 Pct Recovery = 90% Analysis Date = 05/01/16 Pct Recovery = 90% Analysis Date = 05/01/16 Pct Recovery = 90% Analysis Date = 04/28/16 Pct Recovery = 90% Analysis Date = 04/28/16 Pct Recovery = 90% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/19/16 Pct Recovery = 88% Analysis Date = 04/17/16 Pct Recovery = 88% Analysis Date = 04/17/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/12/16 Pct Recovery = 88% Analysis Date = 04/12/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/10/16 Pct Recovery = 87% Analysis Date = 04/08/16 Pct Recovery = 87% Analysis Date = 04/08/16 Pct Recovery = 87% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 04/01/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/30/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/27/16 Pct Recovery = 85% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/25/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/23/16 Pct Recovery = 84% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 83% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 81% Analysis Date = 03/11/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/05/16 Pct Recovery = 80% Analysis Date = 03/05/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 80% Analysis Date = 02/29/16 Pct Recovery = 79% Analysis Date = 02/29/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/27/16 Pct Recovery = 79% Analysis Date = 02/24/16 Pct Recovery = 78% Analysis Date = 02/24/16 Pct Recovery = 78% Analysis Date = 02/22/16 Pct Recovery = 78% Analysis Date = 02/22/16 Pct Recovery = 78% Analysis Date = 02/20/16 Pct Recovery = 77% Analysis Date = 02/20/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/18/16 Pct Recovery = 77% Analysis Date = 02/15/16 Pct Recovery = 76% Analysis Date = 02/15/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 75% Analysis Date = 02/11/16 Pct Recovery = 75% Analysis Date = 02/09/16 Pct Recovery = 75% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
OXYFLUORFEN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 98% 24% 93% 11%
Total 19 98% 24% 93% 11%

Sample Statistics
OXYFLUORFEN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
PARAOXON-METHYL
METHOD: 2033 , TESTIDCODE: 61664GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 83% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 83% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 76% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 81% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 93% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 77% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 86% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 80% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 107% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 77% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 74% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 81% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 80% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 77% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 114% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 109% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 05/10/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/01/17 Pct Recovery = 77% Analysis Date = 05/01/17 Pct Recovery = 77% Analysis Date = 04/29/17 Pct Recovery = 77% Analysis Date = 04/29/17 Pct Recovery = 77% Analysis Date = 04/27/17 Pct Recovery = 77% Analysis Date = 04/27/17 Pct Recovery = 77% Analysis Date = 04/25/17 Pct Recovery = 77% Analysis Date = 04/25/17 Pct Recovery = 77% Analysis Date = 04/22/17 Pct Recovery = 78% Analysis Date = 04/22/17 Pct Recovery = 78% Analysis Date = 04/20/17 Pct Recovery = 78% Analysis Date = 04/20/17 Pct Recovery = 78% Analysis Date = 04/18/17 Pct Recovery = 78% Analysis Date = 04/18/17 Pct Recovery = 78% Analysis Date = 04/15/17 Pct Recovery = 78% Analysis Date = 04/15/17 Pct Recovery = 78% Analysis Date = 04/13/17 Pct Recovery = 79% Analysis Date = 04/13/17 Pct Recovery = 79% Analysis Date = 04/11/17 Pct Recovery = 79% Analysis Date = 04/11/17 Pct Recovery = 79% Analysis Date = 04/09/17 Pct Recovery = 79% Analysis Date = 04/09/17 Pct Recovery = 79% Analysis Date = 04/06/17 Pct Recovery = 79% Analysis Date = 04/06/17 Pct Recovery = 79% Analysis Date = 04/04/17 Pct Recovery = 80% Analysis Date = 04/04/17 Pct Recovery = 80% Analysis Date = 04/02/17 Pct Recovery = 80% Analysis Date = 04/02/17 Pct Recovery = 80% Analysis Date = 03/30/17 Pct Recovery = 80% Analysis Date = 03/30/17 Pct Recovery = 80% Analysis Date = 03/28/17 Pct Recovery = 80% Analysis Date = 03/28/17 Pct Recovery = 80% Analysis Date = 03/26/17 Pct Recovery = 80% Analysis Date = 03/26/17 Pct Recovery = 80% Analysis Date = 03/24/17 Pct Recovery = 81% Analysis Date = 03/24/17 Pct Recovery = 81% Analysis Date = 03/21/17 Pct Recovery = 81% Analysis Date = 03/21/17 Pct Recovery = 81% Analysis Date = 03/19/17 Pct Recovery = 81% Analysis Date = 03/19/17 Pct Recovery = 81% Analysis Date = 03/17/17 Pct Recovery = 81% Analysis Date = 03/17/17 Pct Recovery = 81% Analysis Date = 03/14/17 Pct Recovery = 82% Analysis Date = 03/14/17 Pct Recovery = 82% Analysis Date = 03/12/17 Pct Recovery = 82% Analysis Date = 03/12/17 Pct Recovery = 82% Analysis Date = 03/10/17 Pct Recovery = 82% Analysis Date = 03/10/17 Pct Recovery = 82% Analysis Date = 03/08/17 Pct Recovery = 82% Analysis Date = 03/08/17 Pct Recovery = 82% Analysis Date = 03/05/17 Pct Recovery = 83% Analysis Date = 03/05/17 Pct Recovery = 83% Analysis Date = 03/03/17 Pct Recovery = 83% Analysis Date = 03/03/17 Pct Recovery = 83% Analysis Date = 03/01/17 Pct Recovery = 83% Analysis Date = 03/01/17 Pct Recovery = 83% Analysis Date = 02/26/17 Pct Recovery = 83% Analysis Date = 02/26/17 Pct Recovery = 83% Analysis Date = 02/24/17 Pct Recovery = 84% Analysis Date = 02/24/17 Pct Recovery = 84% Analysis Date = 02/22/17 Pct Recovery = 84% Analysis Date = 02/22/17 Pct Recovery = 84% Analysis Date = 02/20/17 Pct Recovery = 84% Analysis Date = 02/20/17 Pct Recovery = 84% Analysis Date = 02/17/17 Pct Recovery = 84% Analysis Date = 02/17/17 Pct Recovery = 84% Analysis Date = 02/15/17 Pct Recovery = 85% Analysis Date = 02/15/17 Pct Recovery = 85% Analysis Date = 02/13/17 Pct Recovery = 85% Analysis Date = 02/13/17 Pct Recovery = 85% Analysis Date = 02/10/17 Pct Recovery = 85% Analysis Date = 02/10/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 85% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/04/17 Pct Recovery = 86% Analysis Date = 02/04/17 Pct Recovery = 86% Analysis Date = 02/01/17 Pct Recovery = 86% Analysis Date = 02/01/17 Pct Recovery = 86% Analysis Date = 01/30/17 Pct Recovery = 86% Analysis Date = 01/30/17 Pct Recovery = 86% Analysis Date = 01/28/17 Pct Recovery = 87% Analysis Date = 01/28/17 Pct Recovery = 87% Analysis Date = 01/25/17 Pct Recovery = 87% Analysis Date = 01/25/17 Pct Recovery = 87% Analysis Date = 01/23/17 Pct Recovery = 87% Analysis Date = 01/23/17 Pct Recovery = 87% Analysis Date = 01/21/17 Pct Recovery = 87% Analysis Date = 01/21/17 Pct Recovery = 87% Analysis Date = 01/19/17 Pct Recovery = 88% Analysis Date = 01/19/17 Pct Recovery = 88% Analysis Date = 01/16/17 Pct Recovery = 88% Analysis Date = 01/16/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/12/17 Pct Recovery = 88% Analysis Date = 01/12/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/09/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 01/07/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 87% Analysis Date = 12/29/16 Pct Recovery = 87% Analysis Date = 12/29/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/27/16 Pct Recovery = 87% Analysis Date = 12/24/16 Pct Recovery = 87% Analysis Date = 12/24/16 Pct Recovery = 87% Analysis Date = 12/22/16 Pct Recovery = 87% Analysis Date = 12/22/16 Pct Recovery = 87% Analysis Date = 12/20/16 Pct Recovery = 87% Analysis Date = 12/20/16 Pct Recovery = 87% Analysis Date = 12/18/16 Pct Recovery = 87% Analysis Date = 12/18/16 Pct Recovery = 87% Analysis Date = 12/15/16 Pct Recovery = 87% Analysis Date = 12/15/16 Pct Recovery = 87% Analysis Date = 12/13/16 Pct Recovery = 87% Analysis Date = 12/13/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/11/16 Pct Recovery = 87% Analysis Date = 12/08/16 Pct Recovery = 86% Analysis Date = 12/08/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 11/29/16 Pct Recovery = 86% Analysis Date = 11/29/16 Pct Recovery = 86% Analysis Date = 11/27/16 Pct Recovery = 86% Analysis Date = 11/27/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 86% Analysis Date = 11/25/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/22/16 Pct Recovery = 86% Analysis Date = 11/20/16 Pct Recovery = 86% Analysis Date = 11/20/16 Pct Recovery = 86% Analysis Date = 11/18/16 Pct Recovery = 86% Analysis Date = 11/18/16 Pct Recovery = 86% Analysis Date = 11/16/16 Pct Recovery = 86% Analysis Date = 11/16/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/28/16 Pct Recovery = 86% Analysis Date = 10/28/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 85% Analysis Date = 10/26/16 Pct Recovery = 85% Analysis Date = 10/24/16 Pct Recovery = 85% Analysis Date = 10/24/16 Pct Recovery = 85% Analysis Date = 10/21/16 Pct Recovery = 85% Analysis Date = 10/21/16 Pct Recovery = 85% Analysis Date = 10/19/16 Pct Recovery = 85% Analysis Date = 10/19/16 Pct Recovery = 85% Analysis Date = 10/17/16 Pct Recovery = 85% Analysis Date = 10/17/16 Pct Recovery = 85% Analysis Date = 10/15/16 Pct Recovery = 85% Analysis Date = 10/15/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/12/16 Pct Recovery = 85% Analysis Date = 10/10/16 Pct Recovery = 85% Analysis Date = 10/10/16 Pct Recovery = 85% Analysis Date = 10/08/16 Pct Recovery = 85% Analysis Date = 10/08/16 Pct Recovery = 85% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 10/05/16 Pct Recovery = 85% Analysis Date = 10/03/16 Pct Recovery = 85% Analysis Date = 10/03/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 10/01/16 Pct Recovery = 85% Analysis Date = 09/29/16 Pct Recovery = 85% Analysis Date = 09/29/16 Pct Recovery = 85% Analysis Date = 09/26/16 Pct Recovery = 85% Analysis Date = 09/26/16 Pct Recovery = 85% Analysis Date = 09/24/16 Pct Recovery = 85% Analysis Date = 09/24/16 Pct Recovery = 85% Analysis Date = 09/22/16 Pct Recovery = 85% Analysis Date = 09/22/16 Pct Recovery = 85% Analysis Date = 09/19/16 Pct Recovery = 85% Analysis Date = 09/19/16 Pct Recovery = 85% Analysis Date = 09/17/16 Pct Recovery = 85% Analysis Date = 09/17/16 Pct Recovery = 85% Analysis Date = 09/15/16 Pct Recovery = 85% Analysis Date = 09/15/16 Pct Recovery = 85% Analysis Date = 09/13/16 Pct Recovery = 84% Analysis Date = 09/13/16 Pct Recovery = 84% Analysis Date = 09/10/16 Pct Recovery = 84% Analysis Date = 09/10/16 Pct Recovery = 84% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/08/16 Pct Recovery = 84% Analysis Date = 09/06/16 Pct Recovery = 84% Analysis Date = 09/06/16 Pct Recovery = 84% Analysis Date = 09/03/16 Pct Recovery = 84% Analysis Date = 09/03/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 09/01/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/30/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/28/16 Pct Recovery = 84% Analysis Date = 08/25/16 Pct Recovery = 84% Analysis Date = 08/25/16 Pct Recovery = 84% Analysis Date = 08/23/16 Pct Recovery = 84% Analysis Date = 08/23/16 Pct Recovery = 84% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/21/16 Pct Recovery = 85% Analysis Date = 08/18/16 Pct Recovery = 85% Analysis Date = 08/18/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/16/16 Pct Recovery = 85% Analysis Date = 08/14/16 Pct Recovery = 85% Analysis Date = 08/14/16 Pct Recovery = 85% Analysis Date = 08/12/16 Pct Recovery = 85% Analysis Date = 08/12/16 Pct Recovery = 85% Analysis Date = 08/09/16 Pct Recovery = 85% Analysis Date = 08/09/16 Pct Recovery = 85% Analysis Date = 08/07/16 Pct Recovery = 85% Analysis Date = 08/07/16 Pct Recovery = 85% Analysis Date = 08/05/16 Pct Recovery = 85% Analysis Date = 08/05/16 Pct Recovery = 85% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 85% Analysis Date = 07/22/16 Pct Recovery = 85% Analysis Date = 07/22/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/20/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/15/16 Pct Recovery = 86% Analysis Date = 07/13/16 Pct Recovery = 86% Analysis Date = 07/13/16 Pct Recovery = 86% Analysis Date = 07/11/16 Pct Recovery = 86% Analysis Date = 07/11/16 Pct Recovery = 86% Analysis Date = 07/08/16 Pct Recovery = 86% Analysis Date = 07/08/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/04/16 Pct Recovery = 86% Analysis Date = 07/04/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/22/16 Pct Recovery = 86% Analysis Date = 06/22/16 Pct Recovery = 86% Analysis Date = 06/20/16 Pct Recovery = 86% Analysis Date = 06/20/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/18/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/15/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/13/16 Pct Recovery = 86% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/11/16 Pct Recovery = 87% Analysis Date = 06/09/16 Pct Recovery = 87% Analysis Date = 06/09/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 87% Analysis Date = 06/06/16 Pct Recovery = 87% Analysis Date = 06/04/16 Pct Recovery = 87% Analysis Date = 06/04/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 87% Analysis Date = 06/02/16 Pct Recovery = 87% Analysis Date = 05/30/16 Pct Recovery = 87% Analysis Date = 05/30/16 Pct Recovery = 87% Analysis Date = 05/28/16 Pct Recovery = 87% Analysis Date = 05/28/16 Pct Recovery = 87% Analysis Date = 05/26/16 Pct Recovery = 87% Analysis Date = 05/26/16 Pct Recovery = 87% Analysis Date = 05/24/16 Pct Recovery = 87% Analysis Date = 05/24/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/21/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/19/16 Pct Recovery = 87% Analysis Date = 05/17/16 Pct Recovery = 88% Analysis Date = 05/17/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/14/16 Pct Recovery = 88% Analysis Date = 05/12/16 Pct Recovery = 88% Analysis Date = 05/12/16 Pct Recovery = 88% Analysis Date = 05/10/16 Pct Recovery = 88% Analysis Date = 05/10/16 Pct Recovery = 88% Analysis Date = 05/08/16 Pct Recovery = 89% Analysis Date = 05/08/16 Pct Recovery = 89% Analysis Date = 05/05/16 Pct Recovery = 89% Analysis Date = 05/05/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 05/03/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 05/01/16 Pct Recovery = 89% Analysis Date = 04/28/16 Pct Recovery = 89% Analysis Date = 04/28/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/26/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/24/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/22/16 Pct Recovery = 89% Analysis Date = 04/19/16 Pct Recovery = 89% Analysis Date = 04/19/16 Pct Recovery = 89% Analysis Date = 04/17/16 Pct Recovery = 88% Analysis Date = 04/17/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/15/16 Pct Recovery = 88% Analysis Date = 04/12/16 Pct Recovery = 88% Analysis Date = 04/12/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/10/16 Pct Recovery = 88% Analysis Date = 04/08/16 Pct Recovery = 88% Analysis Date = 04/08/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/06/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/03/16 Pct Recovery = 88% Analysis Date = 04/01/16 Pct Recovery = 87% Analysis Date = 04/01/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 86% Analysis Date = 03/21/16 Pct Recovery = 86% Analysis Date = 03/18/16 Pct Recovery = 86% Analysis Date = 03/18/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/16/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/14/16 Pct Recovery = 86% Analysis Date = 03/11/16 Pct Recovery = 86% Analysis Date = 03/11/16 Pct Recovery = 86% Analysis Date = 03/09/16 Pct Recovery = 86% Analysis Date = 03/09/16 Pct Recovery = 86% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/07/16 Pct Recovery = 85% Analysis Date = 03/05/16 Pct Recovery = 85% Analysis Date = 03/05/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/24/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/22/16 Pct Recovery = 84% Analysis Date = 02/20/16 Pct Recovery = 84% Analysis Date = 02/20/16 Pct Recovery = 84% Analysis Date = 02/18/16 Pct Recovery = 84% Analysis Date = 02/18/16 Pct Recovery = 84% Analysis Date = 02/15/16 Pct Recovery = 84% Analysis Date = 02/15/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/11/16 Pct Recovery = 83% Analysis Date = 02/11/16 Pct Recovery = 83% Analysis Date = 02/09/16 Pct Recovery = 83% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PARAOXON-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 85% 12% 81% 9%
Total 19 85% 12% 81% 9%

Sample Statistics
PARAOXON-METHYL

Characteristic N % % Basis
Plotted 19 95% Spiked
Estimated Values 19 95% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 1 5% 1 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
PARATHION-METHYL
METHOD: 2033 , TESTIDCODE: 82667GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 111% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 94% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 133% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 101% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 123% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 105% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 90% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 96% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 142% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 103% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 108% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 110% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 116% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 135% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 116% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 112% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 93% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 93% Analysis Date = 05/10/17 Pct Recovery = 112% Analysis Date = 05/08/17 Pct Recovery = 112% Analysis Date = 05/08/17 Pct Recovery = 112% Analysis Date = 05/06/17 Pct Recovery = 111% Analysis Date = 05/06/17 Pct Recovery = 111% Analysis Date = 05/04/17 Pct Recovery = 111% Analysis Date = 05/04/17 Pct Recovery = 111% Analysis Date = 05/01/17 Pct Recovery = 111% Analysis Date = 05/01/17 Pct Recovery = 111% Analysis Date = 04/29/17 Pct Recovery = 111% Analysis Date = 04/29/17 Pct Recovery = 111% Analysis Date = 04/27/17 Pct Recovery = 111% Analysis Date = 04/27/17 Pct Recovery = 111% Analysis Date = 04/25/17 Pct Recovery = 111% Analysis Date = 04/25/17 Pct Recovery = 111% Analysis Date = 04/22/17 Pct Recovery = 111% Analysis Date = 04/22/17 Pct Recovery = 111% Analysis Date = 04/20/17 Pct Recovery = 111% Analysis Date = 04/20/17 Pct Recovery = 111% Analysis Date = 04/18/17 Pct Recovery = 111% Analysis Date = 04/18/17 Pct Recovery = 111% Analysis Date = 04/15/17 Pct Recovery = 111% Analysis Date = 04/15/17 Pct Recovery = 111% Analysis Date = 04/13/17 Pct Recovery = 111% Analysis Date = 04/13/17 Pct Recovery = 111% Analysis Date = 04/11/17 Pct Recovery = 111% Analysis Date = 04/11/17 Pct Recovery = 111% Analysis Date = 04/09/17 Pct Recovery = 111% Analysis Date = 04/09/17 Pct Recovery = 111% Analysis Date = 04/06/17 Pct Recovery = 111% Analysis Date = 04/06/17 Pct Recovery = 111% Analysis Date = 04/04/17 Pct Recovery = 111% Analysis Date = 04/04/17 Pct Recovery = 111% Analysis Date = 04/02/17 Pct Recovery = 111% Analysis Date = 04/02/17 Pct Recovery = 111% Analysis Date = 03/30/17 Pct Recovery = 111% Analysis Date = 03/30/17 Pct Recovery = 111% Analysis Date = 03/28/17 Pct Recovery = 111% Analysis Date = 03/28/17 Pct Recovery = 111% Analysis Date = 03/26/17 Pct Recovery = 111% Analysis Date = 03/26/17 Pct Recovery = 111% Analysis Date = 03/24/17 Pct Recovery = 111% Analysis Date = 03/24/17 Pct Recovery = 111% Analysis Date = 03/21/17 Pct Recovery = 111% Analysis Date = 03/21/17 Pct Recovery = 111% Analysis Date = 03/19/17 Pct Recovery = 111% Analysis Date = 03/19/17 Pct Recovery = 111% Analysis Date = 03/17/17 Pct Recovery = 110% Analysis Date = 03/17/17 Pct Recovery = 110% Analysis Date = 03/14/17 Pct Recovery = 110% Analysis Date = 03/14/17 Pct Recovery = 110% Analysis Date = 03/12/17 Pct Recovery = 110% Analysis Date = 03/12/17 Pct Recovery = 110% Analysis Date = 03/10/17 Pct Recovery = 110% Analysis Date = 03/10/17 Pct Recovery = 110% Analysis Date = 03/08/17 Pct Recovery = 110% Analysis Date = 03/08/17 Pct Recovery = 110% Analysis Date = 03/05/17 Pct Recovery = 110% Analysis Date = 03/05/17 Pct Recovery = 110% Analysis Date = 03/03/17 Pct Recovery = 110% Analysis Date = 03/03/17 Pct Recovery = 110% Analysis Date = 03/01/17 Pct Recovery = 110% Analysis Date = 03/01/17 Pct Recovery = 110% Analysis Date = 02/26/17 Pct Recovery = 110% Analysis Date = 02/26/17 Pct Recovery = 110% Analysis Date = 02/24/17 Pct Recovery = 110% Analysis Date = 02/24/17 Pct Recovery = 110% Analysis Date = 02/22/17 Pct Recovery = 110% Analysis Date = 02/22/17 Pct Recovery = 110% Analysis Date = 02/20/17 Pct Recovery = 109% Analysis Date = 02/20/17 Pct Recovery = 109% Analysis Date = 02/17/17 Pct Recovery = 109% Analysis Date = 02/17/17 Pct Recovery = 109% Analysis Date = 02/15/17 Pct Recovery = 108% Analysis Date = 02/15/17 Pct Recovery = 108% Analysis Date = 02/13/17 Pct Recovery = 108% Analysis Date = 02/13/17 Pct Recovery = 108% Analysis Date = 02/10/17 Pct Recovery = 107% Analysis Date = 02/10/17 Pct Recovery = 107% Analysis Date = 02/08/17 Pct Recovery = 107% Analysis Date = 02/08/17 Pct Recovery = 107% Analysis Date = 02/06/17 Pct Recovery = 107% Analysis Date = 02/06/17 Pct Recovery = 107% Analysis Date = 02/04/17 Pct Recovery = 106% Analysis Date = 02/04/17 Pct Recovery = 106% Analysis Date = 02/01/17 Pct Recovery = 106% Analysis Date = 02/01/17 Pct Recovery = 106% Analysis Date = 01/30/17 Pct Recovery = 105% Analysis Date = 01/30/17 Pct Recovery = 105% Analysis Date = 01/28/17 Pct Recovery = 105% Analysis Date = 01/28/17 Pct Recovery = 105% Analysis Date = 01/25/17 Pct Recovery = 104% Analysis Date = 01/25/17 Pct Recovery = 104% Analysis Date = 01/23/17 Pct Recovery = 104% Analysis Date = 01/23/17 Pct Recovery = 104% Analysis Date = 01/21/17 Pct Recovery = 103% Analysis Date = 01/21/17 Pct Recovery = 103% Analysis Date = 01/19/17 Pct Recovery = 103% Analysis Date = 01/19/17 Pct Recovery = 103% Analysis Date = 01/16/17 Pct Recovery = 103% Analysis Date = 01/16/17 Pct Recovery = 103% Analysis Date = 01/14/17 Pct Recovery = 103% Analysis Date = 01/14/17 Pct Recovery = 103% Analysis Date = 01/12/17 Pct Recovery = 103% Analysis Date = 01/12/17 Pct Recovery = 103% Analysis Date = 01/09/17 Pct Recovery = 104% Analysis Date = 01/09/17 Pct Recovery = 104% Analysis Date = 01/07/17 Pct Recovery = 104% Analysis Date = 01/07/17 Pct Recovery = 104% Analysis Date = 01/05/17 Pct Recovery = 104% Analysis Date = 01/05/17 Pct Recovery = 104% Analysis Date = 01/03/17 Pct Recovery = 104% Analysis Date = 01/03/17 Pct Recovery = 104% Analysis Date = 12/31/16 Pct Recovery = 105% Analysis Date = 12/31/16 Pct Recovery = 105% Analysis Date = 12/29/16 Pct Recovery = 105% Analysis Date = 12/29/16 Pct Recovery = 105% Analysis Date = 12/27/16 Pct Recovery = 105% Analysis Date = 12/27/16 Pct Recovery = 105% Analysis Date = 12/24/16 Pct Recovery = 106% Analysis Date = 12/24/16 Pct Recovery = 106% Analysis Date = 12/22/16 Pct Recovery = 106% Analysis Date = 12/22/16 Pct Recovery = 106% Analysis Date = 12/20/16 Pct Recovery = 106% Analysis Date = 12/20/16 Pct Recovery = 106% Analysis Date = 12/18/16 Pct Recovery = 106% Analysis Date = 12/18/16 Pct Recovery = 106% Analysis Date = 12/15/16 Pct Recovery = 107% Analysis Date = 12/15/16 Pct Recovery = 107% Analysis Date = 12/13/16 Pct Recovery = 107% Analysis Date = 12/13/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/11/16 Pct Recovery = 107% Analysis Date = 12/08/16 Pct Recovery = 107% Analysis Date = 12/08/16 Pct Recovery = 107% Analysis Date = 12/06/16 Pct Recovery = 108% Analysis Date = 12/06/16 Pct Recovery = 108% Analysis Date = 12/04/16 Pct Recovery = 108% Analysis Date = 12/04/16 Pct Recovery = 108% Analysis Date = 12/02/16 Pct Recovery = 108% Analysis Date = 12/02/16 Pct Recovery = 108% Analysis Date = 11/29/16 Pct Recovery = 108% Analysis Date = 11/29/16 Pct Recovery = 108% Analysis Date = 11/27/16 Pct Recovery = 109% Analysis Date = 11/27/16 Pct Recovery = 109% Analysis Date = 11/25/16 Pct Recovery = 109% Analysis Date = 11/25/16 Pct Recovery = 109% Analysis Date = 11/22/16 Pct Recovery = 109% Analysis Date = 11/22/16 Pct Recovery = 109% Analysis Date = 11/20/16 Pct Recovery = 110% Analysis Date = 11/20/16 Pct Recovery = 110% Analysis Date = 11/18/16 Pct Recovery = 110% Analysis Date = 11/18/16 Pct Recovery = 110% Analysis Date = 11/16/16 Pct Recovery = 110% Analysis Date = 11/16/16 Pct Recovery = 110% Analysis Date = 11/13/16 Pct Recovery = 110% Analysis Date = 11/13/16 Pct Recovery = 110% Analysis Date = 11/11/16 Pct Recovery = 111% Analysis Date = 11/11/16 Pct Recovery = 111% Analysis Date = 11/09/16 Pct Recovery = 111% Analysis Date = 11/09/16 Pct Recovery = 111% Analysis Date = 11/06/16 Pct Recovery = 111% Analysis Date = 11/06/16 Pct Recovery = 111% Analysis Date = 11/04/16 Pct Recovery = 111% Analysis Date = 11/04/16 Pct Recovery = 111% Analysis Date = 11/02/16 Pct Recovery = 112% Analysis Date = 11/02/16 Pct Recovery = 112% Analysis Date = 10/31/16 Pct Recovery = 112% Analysis Date = 10/31/16 Pct Recovery = 112% Analysis Date = 10/28/16 Pct Recovery = 112% Analysis Date = 10/28/16 Pct Recovery = 112% Analysis Date = 10/26/16 Pct Recovery = 113% Analysis Date = 10/26/16 Pct Recovery = 113% Analysis Date = 10/24/16 Pct Recovery = 113% Analysis Date = 10/24/16 Pct Recovery = 113% Analysis Date = 10/21/16 Pct Recovery = 113% Analysis Date = 10/21/16 Pct Recovery = 113% Analysis Date = 10/19/16 Pct Recovery = 113% Analysis Date = 10/19/16 Pct Recovery = 113% Analysis Date = 10/17/16 Pct Recovery = 114% Analysis Date = 10/17/16 Pct Recovery = 114% Analysis Date = 10/15/16 Pct Recovery = 114% Analysis Date = 10/15/16 Pct Recovery = 114% Analysis Date = 10/12/16 Pct Recovery = 114% Analysis Date = 10/12/16 Pct Recovery = 114% Analysis Date = 10/10/16 Pct Recovery = 114% Analysis Date = 10/10/16 Pct Recovery = 114% Analysis Date = 10/08/16 Pct Recovery = 115% Analysis Date = 10/08/16 Pct Recovery = 115% Analysis Date = 10/05/16 Pct Recovery = 115% Analysis Date = 10/05/16 Pct Recovery = 115% Analysis Date = 10/03/16 Pct Recovery = 115% Analysis Date = 10/03/16 Pct Recovery = 115% Analysis Date = 10/01/16 Pct Recovery = 116% Analysis Date = 10/01/16 Pct Recovery = 116% Analysis Date = 09/29/16 Pct Recovery = 116% Analysis Date = 09/29/16 Pct Recovery = 116% Analysis Date = 09/26/16 Pct Recovery = 116% Analysis Date = 09/26/16 Pct Recovery = 116% Analysis Date = 09/24/16 Pct Recovery = 116% Analysis Date = 09/24/16 Pct Recovery = 116% Analysis Date = 09/22/16 Pct Recovery = 117% Analysis Date = 09/22/16 Pct Recovery = 117% Analysis Date = 09/19/16 Pct Recovery = 117% Analysis Date = 09/19/16 Pct Recovery = 117% Analysis Date = 09/17/16 Pct Recovery = 117% Analysis Date = 09/17/16 Pct Recovery = 117% Analysis Date = 09/15/16 Pct Recovery = 117% Analysis Date = 09/15/16 Pct Recovery = 117% Analysis Date = 09/13/16 Pct Recovery = 118% Analysis Date = 09/13/16 Pct Recovery = 118% Analysis Date = 09/10/16 Pct Recovery = 118% Analysis Date = 09/10/16 Pct Recovery = 118% Analysis Date = 09/08/16 Pct Recovery = 117% Analysis Date = 09/08/16 Pct Recovery = 117% Analysis Date = 09/06/16 Pct Recovery = 117% Analysis Date = 09/06/16 Pct Recovery = 117% Analysis Date = 09/03/16 Pct Recovery = 117% Analysis Date = 09/03/16 Pct Recovery = 117% Analysis Date = 09/01/16 Pct Recovery = 117% Analysis Date = 09/01/16 Pct Recovery = 117% Analysis Date = 08/30/16 Pct Recovery = 117% Analysis Date = 08/30/16 Pct Recovery = 117% Analysis Date = 08/28/16 Pct Recovery = 117% Analysis Date = 08/28/16 Pct Recovery = 117% Analysis Date = 08/25/16 Pct Recovery = 117% Analysis Date = 08/25/16 Pct Recovery = 117% Analysis Date = 08/23/16 Pct Recovery = 117% Analysis Date = 08/23/16 Pct Recovery = 117% Analysis Date = 08/21/16 Pct Recovery = 117% Analysis Date = 08/21/16 Pct Recovery = 117% Analysis Date = 08/18/16 Pct Recovery = 116% Analysis Date = 08/18/16 Pct Recovery = 116% Analysis Date = 08/16/16 Pct Recovery = 116% Analysis Date = 08/16/16 Pct Recovery = 116% Analysis Date = 08/14/16 Pct Recovery = 116% Analysis Date = 08/14/16 Pct Recovery = 116% Analysis Date = 08/12/16 Pct Recovery = 116% Analysis Date = 08/12/16 Pct Recovery = 116% Analysis Date = 08/09/16 Pct Recovery = 116% Analysis Date = 08/09/16 Pct Recovery = 116% Analysis Date = 08/07/16 Pct Recovery = 115% Analysis Date = 08/07/16 Pct Recovery = 115% Analysis Date = 08/05/16 Pct Recovery = 115% Analysis Date = 08/05/16 Pct Recovery = 115% Analysis Date = 08/02/16 Pct Recovery = 115% Analysis Date = 08/02/16 Pct Recovery = 115% Analysis Date = 07/31/16 Pct Recovery = 115% Analysis Date = 07/31/16 Pct Recovery = 115% Analysis Date = 07/29/16 Pct Recovery = 115% Analysis Date = 07/29/16 Pct Recovery = 115% Analysis Date = 07/27/16 Pct Recovery = 115% Analysis Date = 07/27/16 Pct Recovery = 115% Analysis Date = 07/24/16 Pct Recovery = 114% Analysis Date = 07/24/16 Pct Recovery = 114% Analysis Date = 07/22/16 Pct Recovery = 114% Analysis Date = 07/22/16 Pct Recovery = 114% Analysis Date = 07/20/16 Pct Recovery = 114% Analysis Date = 07/20/16 Pct Recovery = 114% Analysis Date = 07/17/16 Pct Recovery = 114% Analysis Date = 07/17/16 Pct Recovery = 114% Analysis Date = 07/15/16 Pct Recovery = 114% Analysis Date = 07/15/16 Pct Recovery = 114% Analysis Date = 07/13/16 Pct Recovery = 113% Analysis Date = 07/13/16 Pct Recovery = 113% Analysis Date = 07/11/16 Pct Recovery = 113% Analysis Date = 07/11/16 Pct Recovery = 113% Analysis Date = 07/08/16 Pct Recovery = 113% Analysis Date = 07/08/16 Pct Recovery = 113% Analysis Date = 07/06/16 Pct Recovery = 113% Analysis Date = 07/06/16 Pct Recovery = 113% Analysis Date = 07/04/16 Pct Recovery = 113% Analysis Date = 07/04/16 Pct Recovery = 113% Analysis Date = 07/01/16 Pct Recovery = 113% Analysis Date = 07/01/16 Pct Recovery = 113% Analysis Date = 06/29/16 Pct Recovery = 112% Analysis Date = 06/29/16 Pct Recovery = 112% Analysis Date = 06/27/16 Pct Recovery = 112% Analysis Date = 06/27/16 Pct Recovery = 112% Analysis Date = 06/25/16 Pct Recovery = 112% Analysis Date = 06/25/16 Pct Recovery = 112% Analysis Date = 06/22/16 Pct Recovery = 112% Analysis Date = 06/22/16 Pct Recovery = 112% Analysis Date = 06/20/16 Pct Recovery = 112% Analysis Date = 06/20/16 Pct Recovery = 112% Analysis Date = 06/18/16 Pct Recovery = 111% Analysis Date = 06/18/16 Pct Recovery = 111% Analysis Date = 06/15/16 Pct Recovery = 111% Analysis Date = 06/15/16 Pct Recovery = 111% Analysis Date = 06/13/16 Pct Recovery = 111% Analysis Date = 06/13/16 Pct Recovery = 111% Analysis Date = 06/11/16 Pct Recovery = 111% Analysis Date = 06/11/16 Pct Recovery = 111% Analysis Date = 06/09/16 Pct Recovery = 111% Analysis Date = 06/09/16 Pct Recovery = 111% Analysis Date = 06/06/16 Pct Recovery = 111% Analysis Date = 06/06/16 Pct Recovery = 111% Analysis Date = 06/04/16 Pct Recovery = 110% Analysis Date = 06/04/16 Pct Recovery = 110% Analysis Date = 06/02/16 Pct Recovery = 110% Analysis Date = 06/02/16 Pct Recovery = 110% Analysis Date = 05/30/16 Pct Recovery = 110% Analysis Date = 05/30/16 Pct Recovery = 110% Analysis Date = 05/28/16 Pct Recovery = 110% Analysis Date = 05/28/16 Pct Recovery = 110% Analysis Date = 05/26/16 Pct Recovery = 110% Analysis Date = 05/26/16 Pct Recovery = 110% Analysis Date = 05/24/16 Pct Recovery = 109% Analysis Date = 05/24/16 Pct Recovery = 109% Analysis Date = 05/21/16 Pct Recovery = 109% Analysis Date = 05/21/16 Pct Recovery = 109% Analysis Date = 05/19/16 Pct Recovery = 109% Analysis Date = 05/19/16 Pct Recovery = 109% Analysis Date = 05/17/16 Pct Recovery = 109% Analysis Date = 05/17/16 Pct Recovery = 109% Analysis Date = 05/14/16 Pct Recovery = 109% Analysis Date = 05/14/16 Pct Recovery = 109% Analysis Date = 05/12/16 Pct Recovery = 109% Analysis Date = 05/12/16 Pct Recovery = 109% Analysis Date = 05/10/16 Pct Recovery = 108% Analysis Date = 05/10/16 Pct Recovery = 108% Analysis Date = 05/08/16 Pct Recovery = 108% Analysis Date = 05/08/16 Pct Recovery = 108% Analysis Date = 05/05/16 Pct Recovery = 108% Analysis Date = 05/05/16 Pct Recovery = 108% Analysis Date = 05/03/16 Pct Recovery = 108% Analysis Date = 05/03/16 Pct Recovery = 108% Analysis Date = 05/01/16 Pct Recovery = 107% Analysis Date = 05/01/16 Pct Recovery = 107% Analysis Date = 04/28/16 Pct Recovery = 107% Analysis Date = 04/28/16 Pct Recovery = 107% Analysis Date = 04/26/16 Pct Recovery = 107% Analysis Date = 04/26/16 Pct Recovery = 107% Analysis Date = 04/24/16 Pct Recovery = 106% Analysis Date = 04/24/16 Pct Recovery = 106% Analysis Date = 04/22/16 Pct Recovery = 106% Analysis Date = 04/22/16 Pct Recovery = 106% Analysis Date = 04/19/16 Pct Recovery = 106% Analysis Date = 04/19/16 Pct Recovery = 106% Analysis Date = 04/17/16 Pct Recovery = 105% Analysis Date = 04/17/16 Pct Recovery = 105% Analysis Date = 04/15/16 Pct Recovery = 105% Analysis Date = 04/15/16 Pct Recovery = 105% Analysis Date = 04/12/16 Pct Recovery = 105% Analysis Date = 04/12/16 Pct Recovery = 105% Analysis Date = 04/10/16 Pct Recovery = 104% Analysis Date = 04/10/16 Pct Recovery = 104% Analysis Date = 04/08/16 Pct Recovery = 104% Analysis Date = 04/08/16 Pct Recovery = 104% Analysis Date = 04/06/16 Pct Recovery = 104% Analysis Date = 04/06/16 Pct Recovery = 104% Analysis Date = 04/03/16 Pct Recovery = 103% Analysis Date = 04/03/16 Pct Recovery = 103% Analysis Date = 04/01/16 Pct Recovery = 103% Analysis Date = 04/01/16 Pct Recovery = 103% Analysis Date = 03/30/16 Pct Recovery = 102% Analysis Date = 03/30/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 102% Analysis Date = 03/27/16 Pct Recovery = 102% Analysis Date = 03/25/16 Pct Recovery = 101% Analysis Date = 03/25/16 Pct Recovery = 101% Analysis Date = 03/23/16 Pct Recovery = 101% Analysis Date = 03/23/16 Pct Recovery = 101% Analysis Date = 03/21/16 Pct Recovery = 101% Analysis Date = 03/21/16 Pct Recovery = 101% Analysis Date = 03/18/16 Pct Recovery = 100% Analysis Date = 03/18/16 Pct Recovery = 100% Analysis Date = 03/16/16 Pct Recovery = 100% Analysis Date = 03/16/16 Pct Recovery = 100% Analysis Date = 03/14/16 Pct Recovery = 99% Analysis Date = 03/14/16 Pct Recovery = 99% Analysis Date = 03/11/16 Pct Recovery = 99% Analysis Date = 03/11/16 Pct Recovery = 99% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/09/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/07/16 Pct Recovery = 98% Analysis Date = 03/05/16 Pct Recovery = 97% Analysis Date = 03/05/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 03/02/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/29/16 Pct Recovery = 97% Analysis Date = 02/27/16 Pct Recovery = 96% Analysis Date = 02/27/16 Pct Recovery = 96% Analysis Date = 02/24/16 Pct Recovery = 96% Analysis Date = 02/24/16 Pct Recovery = 96% Analysis Date = 02/22/16 Pct Recovery = 95% Analysis Date = 02/22/16 Pct Recovery = 95% Analysis Date = 02/20/16 Pct Recovery = 95% Analysis Date = 02/20/16 Pct Recovery = 95% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/18/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/15/16 Pct Recovery = 94% Analysis Date = 02/13/16 Pct Recovery = 93% Analysis Date = 02/13/16 Pct Recovery = 93% Analysis Date = 02/11/16 Pct Recovery = 93% Analysis Date = 02/11/16 Pct Recovery = 93% Analysis Date = 02/09/16 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PARATHION-METHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 110% 15% 109% 15%
Total 18 110% 15% 109% 15%

Sample Statistics
PARATHION-METHYL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
PENDIMETHALIN
METHOD: 2033 , TESTIDCODE: 82683GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 79% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 80% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 87% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 98% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 90% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 102% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 96% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 99% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 99% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 120% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 92% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 98% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 101% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 102% Analysis Date = 04/30/17 Pct Recovery = 102% Analysis Date = 04/30/17 Pct Recovery = 102% Analysis Date = 04/28/17 Pct Recovery = 102% Analysis Date = 04/28/17 Pct Recovery = 102% Analysis Date = 04/26/17 Pct Recovery = 101% Analysis Date = 04/26/17 Pct Recovery = 101% Analysis Date = 04/24/17 Pct Recovery = 101% Analysis Date = 04/24/17 Pct Recovery = 101% Analysis Date = 04/22/17 Pct Recovery = 101% Analysis Date = 04/22/17 Pct Recovery = 101% Analysis Date = 04/20/17 Pct Recovery = 100% Analysis Date = 04/20/17 Pct Recovery = 100% Analysis Date = 04/18/17 Pct Recovery = 100% Analysis Date = 04/18/17 Pct Recovery = 100% Analysis Date = 04/15/17 Pct Recovery = 100% Analysis Date = 04/15/17 Pct Recovery = 100% Analysis Date = 04/13/17 Pct Recovery = 99% Analysis Date = 04/13/17 Pct Recovery = 99% Analysis Date = 04/11/17 Pct Recovery = 99% Analysis Date = 04/11/17 Pct Recovery = 99% Analysis Date = 04/09/17 Pct Recovery = 99% Analysis Date = 04/09/17 Pct Recovery = 99% Analysis Date = 04/07/17 Pct Recovery = 99% Analysis Date = 04/07/17 Pct Recovery = 99% Analysis Date = 04/05/17 Pct Recovery = 98% Analysis Date = 04/05/17 Pct Recovery = 98% Analysis Date = 04/03/17 Pct Recovery = 98% Analysis Date = 04/03/17 Pct Recovery = 98% Analysis Date = 03/31/17 Pct Recovery = 98% Analysis Date = 03/31/17 Pct Recovery = 98% Analysis Date = 03/29/17 Pct Recovery = 97% Analysis Date = 03/29/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 97% Analysis Date = 03/27/17 Pct Recovery = 97% Analysis Date = 03/25/17 Pct Recovery = 97% Analysis Date = 03/25/17 Pct Recovery = 97% Analysis Date = 03/23/17 Pct Recovery = 96% Analysis Date = 03/23/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/14/17 Pct Recovery = 95% Analysis Date = 03/14/17 Pct Recovery = 95% Analysis Date = 03/12/17 Pct Recovery = 95% Analysis Date = 03/12/17 Pct Recovery = 95% Analysis Date = 03/10/17 Pct Recovery = 95% Analysis Date = 03/10/17 Pct Recovery = 95% Analysis Date = 03/08/17 Pct Recovery = 94% Analysis Date = 03/08/17 Pct Recovery = 94% Analysis Date = 03/06/17 Pct Recovery = 94% Analysis Date = 03/06/17 Pct Recovery = 94% Analysis Date = 03/04/17 Pct Recovery = 94% Analysis Date = 03/04/17 Pct Recovery = 94% Analysis Date = 03/02/17 Pct Recovery = 94% Analysis Date = 03/02/17 Pct Recovery = 94% Analysis Date = 02/27/17 Pct Recovery = 93% Analysis Date = 02/27/17 Pct Recovery = 93% Analysis Date = 02/25/17 Pct Recovery = 93% Analysis Date = 02/25/17 Pct Recovery = 93% Analysis Date = 02/23/17 Pct Recovery = 93% Analysis Date = 02/23/17 Pct Recovery = 93% Analysis Date = 02/21/17 Pct Recovery = 92% Analysis Date = 02/21/17 Pct Recovery = 92% Analysis Date = 02/19/17 Pct Recovery = 92% Analysis Date = 02/19/17 Pct Recovery = 92% Analysis Date = 02/17/17 Pct Recovery = 92% Analysis Date = 02/17/17 Pct Recovery = 92% Analysis Date = 02/15/17 Pct Recovery = 92% Analysis Date = 02/15/17 Pct Recovery = 92% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/02/17 Pct Recovery = 90% Analysis Date = 02/02/17 Pct Recovery = 90% Analysis Date = 01/31/17 Pct Recovery = 90% Analysis Date = 01/31/17 Pct Recovery = 90% Analysis Date = 01/29/17 Pct Recovery = 90% Analysis Date = 01/29/17 Pct Recovery = 90% Analysis Date = 01/26/17 Pct Recovery = 90% Analysis Date = 01/26/17 Pct Recovery = 90% Analysis Date = 01/24/17 Pct Recovery = 89% Analysis Date = 01/24/17 Pct Recovery = 89% Analysis Date = 01/22/17 Pct Recovery = 89% Analysis Date = 01/22/17 Pct Recovery = 89% Analysis Date = 01/20/17 Pct Recovery = 89% Analysis Date = 01/20/17 Pct Recovery = 89% Analysis Date = 01/18/17 Pct Recovery = 89% Analysis Date = 01/18/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/16/17 Pct Recovery = 89% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/14/17 Pct Recovery = 88% Analysis Date = 01/11/17 Pct Recovery = 88% Analysis Date = 01/11/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 88% Analysis Date = 01/09/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 01/07/17 Pct Recovery = 88% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 01/03/17 Pct Recovery = 87% Analysis Date = 01/01/17 Pct Recovery = 87% Analysis Date = 01/01/17 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/30/16 Pct Recovery = 87% Analysis Date = 12/28/16 Pct Recovery = 87% Analysis Date = 12/28/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 86% Analysis Date = 12/25/16 Pct Recovery = 86% Analysis Date = 12/23/16 Pct Recovery = 86% Analysis Date = 12/23/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/21/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/19/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/17/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/15/16 Pct Recovery = 86% Analysis Date = 12/13/16 Pct Recovery = 86% Analysis Date = 12/13/16 Pct Recovery = 86% Analysis Date = 12/10/16 Pct Recovery = 86% Analysis Date = 12/10/16 Pct Recovery = 86% Analysis Date = 12/08/16 Pct Recovery = 86% Analysis Date = 12/08/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/06/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 12/04/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 12/02/16 Pct Recovery = 86% Analysis Date = 11/30/16 Pct Recovery = 86% Analysis Date = 11/30/16 Pct Recovery = 86% Analysis Date = 11/28/16 Pct Recovery = 86% Analysis Date = 11/28/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/26/16 Pct Recovery = 86% Analysis Date = 11/23/16 Pct Recovery = 86% Analysis Date = 11/23/16 Pct Recovery = 86% Analysis Date = 11/21/16 Pct Recovery = 86% Analysis Date = 11/21/16 Pct Recovery = 86% Analysis Date = 11/19/16 Pct Recovery = 86% Analysis Date = 11/19/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/17/16 Pct Recovery = 86% Analysis Date = 11/15/16 Pct Recovery = 86% Analysis Date = 11/15/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 86% Analysis Date = 10/29/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/27/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/22/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 86% Analysis Date = 10/20/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/18/16 Pct Recovery = 86% Analysis Date = 10/16/16 Pct Recovery = 86% Analysis Date = 10/16/16 Pct Recovery = 86% Analysis Date = 10/14/16 Pct Recovery = 86% Analysis Date = 10/14/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 86% Analysis Date = 10/12/16 Pct Recovery = 86% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/07/16 Pct Recovery = 87% Analysis Date = 10/07/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 10/01/16 Pct Recovery = 87% Analysis Date = 09/29/16 Pct Recovery = 87% Analysis Date = 09/29/16 Pct Recovery = 87% Analysis Date = 09/27/16 Pct Recovery = 87% Analysis Date = 09/27/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/25/16 Pct Recovery = 87% Analysis Date = 09/22/16 Pct Recovery = 87% Analysis Date = 09/22/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/20/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/18/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/16/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/14/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/12/16 Pct Recovery = 87% Analysis Date = 09/10/16 Pct Recovery = 87% Analysis Date = 09/10/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/08/16 Pct Recovery = 87% Analysis Date = 09/05/16 Pct Recovery = 87% Analysis Date = 09/05/16 Pct Recovery = 87% Analysis Date = 09/03/16 Pct Recovery = 87% Analysis Date = 09/03/16 Pct Recovery = 87% Analysis Date = 09/01/16 Pct Recovery = 87% Analysis Date = 09/01/16 Pct Recovery = 87% Analysis Date = 08/30/16 Pct Recovery = 87% Analysis Date = 08/30/16 Pct Recovery = 87% Analysis Date = 08/28/16 Pct Recovery = 87% Analysis Date = 08/28/16 Pct Recovery = 87% Analysis Date = 08/26/16 Pct Recovery = 87% Analysis Date = 08/26/16 Pct Recovery = 87% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/24/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/19/16 Pct Recovery = 88% Analysis Date = 08/19/16 Pct Recovery = 88% Analysis Date = 08/17/16 Pct Recovery = 88% Analysis Date = 08/17/16 Pct Recovery = 88% Analysis Date = 08/15/16 Pct Recovery = 89% Analysis Date = 08/15/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/13/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 89% Analysis Date = 08/11/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/09/16 Pct Recovery = 89% Analysis Date = 08/06/16 Pct Recovery = 89% Analysis Date = 08/06/16 Pct Recovery = 89% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 08/04/16 Pct Recovery = 90% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 08/02/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/31/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/29/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 90% Analysis Date = 07/27/16 Pct Recovery = 90% Analysis Date = 07/25/16 Pct Recovery = 91% Analysis Date = 07/25/16 Pct Recovery = 91% Analysis Date = 07/23/16 Pct Recovery = 91% Analysis Date = 07/23/16 Pct Recovery = 91% Analysis Date = 07/20/16 Pct Recovery = 91% Analysis Date = 07/20/16 Pct Recovery = 91% Analysis Date = 07/18/16 Pct Recovery = 91% Analysis Date = 07/18/16 Pct Recovery = 91% Analysis Date = 07/16/16 Pct Recovery = 91% Analysis Date = 07/16/16 Pct Recovery = 91% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/14/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/12/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/10/16 Pct Recovery = 92% Analysis Date = 07/08/16 Pct Recovery = 92% Analysis Date = 07/08/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/05/16 Pct Recovery = 92% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 07/03/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 07/01/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/29/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/27/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/25/16 Pct Recovery = 93% Analysis Date = 06/23/16 Pct Recovery = 94% Analysis Date = 06/23/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/21/16 Pct Recovery = 94% Analysis Date = 06/18/16 Pct Recovery = 94% Analysis Date = 06/18/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/16/16 Pct Recovery = 94% Analysis Date = 06/14/16 Pct Recovery = 94% Analysis Date = 06/14/16 Pct Recovery = 94% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/12/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 95% Analysis Date = 06/10/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/08/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/06/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 95% Analysis Date = 06/03/16 Pct Recovery = 95% Analysis Date = 06/01/16 Pct Recovery = 96% Analysis Date = 06/01/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/30/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/28/16 Pct Recovery = 96% Analysis Date = 05/26/16 Pct Recovery = 96% Analysis Date = 05/26/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/24/16 Pct Recovery = 96% Analysis Date = 05/22/16 Pct Recovery = 96% Analysis Date = 05/22/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/19/16 Pct Recovery = 96% Analysis Date = 05/17/16 Pct Recovery = 96% Analysis Date = 05/17/16 Pct Recovery = 96% Analysis Date = 05/15/16 Pct Recovery = 96% Analysis Date = 05/15/16 Pct Recovery = 96% Analysis Date = 05/13/16 Pct Recovery = 96% Analysis Date = 05/13/16 Pct Recovery = 96% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/11/16 Pct Recovery = 95% Analysis Date = 05/09/16 Pct Recovery = 95% Analysis Date = 05/09/16 Pct Recovery = 95% Analysis Date = 05/07/16 Pct Recovery = 95% Analysis Date = 05/07/16 Pct Recovery = 95% Analysis Date = 05/05/16 Pct Recovery = 95% Analysis Date = 05/05/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 05/02/16 Pct Recovery = 95% Analysis Date = 04/30/16 Pct Recovery = 95% Analysis Date = 04/30/16 Pct Recovery = 95% Analysis Date = 04/28/16 Pct Recovery = 94% Analysis Date = 04/28/16 Pct Recovery = 94% Analysis Date = 04/26/16 Pct Recovery = 94% Analysis Date = 04/26/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/24/16 Pct Recovery = 94% Analysis Date = 04/22/16 Pct Recovery = 94% Analysis Date = 04/22/16 Pct Recovery = 94% Analysis Date = 04/20/16 Pct Recovery = 94% Analysis Date = 04/20/16 Pct Recovery = 94% Analysis Date = 04/17/16 Pct Recovery = 94% Analysis Date = 04/17/16 Pct Recovery = 94% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/15/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/13/16 Pct Recovery = 93% Analysis Date = 04/11/16 Pct Recovery = 93% Analysis Date = 04/11/16 Pct Recovery = 93% Analysis Date = 04/09/16 Pct Recovery = 93% Analysis Date = 04/09/16 Pct Recovery = 93% Analysis Date = 04/07/16 Pct Recovery = 93% Analysis Date = 04/07/16 Pct Recovery = 93% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 04/05/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 04/03/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/31/16 Pct Recovery = 92% Analysis Date = 03/29/16 Pct Recovery = 92% Analysis Date = 03/29/16 Pct Recovery = 92% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/27/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/25/16 Pct Recovery = 91% Analysis Date = 03/23/16 Pct Recovery = 91% Analysis Date = 03/23/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/21/16 Pct Recovery = 91% Analysis Date = 03/19/16 Pct Recovery = 90% Analysis Date = 03/19/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/16/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/14/16 Pct Recovery = 90% Analysis Date = 03/12/16 Pct Recovery = 90% Analysis Date = 03/12/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/10/16 Pct Recovery = 90% Analysis Date = 03/08/16 Pct Recovery = 89% Analysis Date = 03/08/16 Pct Recovery = 89% Analysis Date = 03/06/16 Pct Recovery = 89% Analysis Date = 03/06/16 Pct Recovery = 89% Analysis Date = 03/04/16 Pct Recovery = 89% Analysis Date = 03/04/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PENDIMETHALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 92% 10% 91% 10%
Total 18 92% 10% 91% 10%

Sample Statistics
PENDIMETHALIN

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
PHORATE
METHOD: 2033 , TESTIDCODE: 82664GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 82% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 76% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 79% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 88% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 71% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 70% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 55% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 43% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 72% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 80% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 57% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 78% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 64% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 63% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 50% Analysis Date = 05/10/17 Pct Recovery = 69% Analysis Date = 05/08/17 Pct Recovery = 69% Analysis Date = 05/08/17 Pct Recovery = 69% Analysis Date = 05/06/17 Pct Recovery = 69% Analysis Date = 05/06/17 Pct Recovery = 69% Analysis Date = 05/04/17 Pct Recovery = 69% Analysis Date = 05/04/17 Pct Recovery = 69% Analysis Date = 05/02/17 Pct Recovery = 69% Analysis Date = 05/02/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 69% Analysis Date = 04/30/17 Pct Recovery = 69% Analysis Date = 04/27/17 Pct Recovery = 69% Analysis Date = 04/27/17 Pct Recovery = 69% Analysis Date = 04/25/17 Pct Recovery = 69% Analysis Date = 04/25/17 Pct Recovery = 69% Analysis Date = 04/23/17 Pct Recovery = 69% Analysis Date = 04/23/17 Pct Recovery = 69% Analysis Date = 04/21/17 Pct Recovery = 70% Analysis Date = 04/21/17 Pct Recovery = 70% Analysis Date = 04/19/17 Pct Recovery = 70% Analysis Date = 04/19/17 Pct Recovery = 70% Analysis Date = 04/17/17 Pct Recovery = 70% Analysis Date = 04/17/17 Pct Recovery = 70% Analysis Date = 04/14/17 Pct Recovery = 70% Analysis Date = 04/14/17 Pct Recovery = 70% Analysis Date = 04/12/17 Pct Recovery = 70% Analysis Date = 04/12/17 Pct Recovery = 70% Analysis Date = 04/10/17 Pct Recovery = 70% Analysis Date = 04/10/17 Pct Recovery = 70% Analysis Date = 04/08/17 Pct Recovery = 70% Analysis Date = 04/08/17 Pct Recovery = 70% Analysis Date = 04/06/17 Pct Recovery = 70% Analysis Date = 04/06/17 Pct Recovery = 70% Analysis Date = 04/04/17 Pct Recovery = 70% Analysis Date = 04/04/17 Pct Recovery = 70% Analysis Date = 04/01/17 Pct Recovery = 70% Analysis Date = 04/01/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 71% Analysis Date = 03/30/17 Pct Recovery = 71% Analysis Date = 03/28/17 Pct Recovery = 71% Analysis Date = 03/28/17 Pct Recovery = 71% Analysis Date = 03/26/17 Pct Recovery = 71% Analysis Date = 03/26/17 Pct Recovery = 71% Analysis Date = 03/24/17 Pct Recovery = 71% Analysis Date = 03/24/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/19/17 Pct Recovery = 71% Analysis Date = 03/19/17 Pct Recovery = 71% Analysis Date = 03/17/17 Pct Recovery = 71% Analysis Date = 03/17/17 Pct Recovery = 71% Analysis Date = 03/15/17 Pct Recovery = 71% Analysis Date = 03/15/17 Pct Recovery = 71% Analysis Date = 03/13/17 Pct Recovery = 71% Analysis Date = 03/13/17 Pct Recovery = 71% Analysis Date = 03/11/17 Pct Recovery = 71% Analysis Date = 03/11/17 Pct Recovery = 71% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/04/17 Pct Recovery = 72% Analysis Date = 03/04/17 Pct Recovery = 72% Analysis Date = 03/02/17 Pct Recovery = 72% Analysis Date = 03/02/17 Pct Recovery = 72% Analysis Date = 02/28/17 Pct Recovery = 72% Analysis Date = 02/28/17 Pct Recovery = 72% Analysis Date = 02/26/17 Pct Recovery = 72% Analysis Date = 02/26/17 Pct Recovery = 72% Analysis Date = 02/23/17 Pct Recovery = 72% Analysis Date = 02/23/17 Pct Recovery = 72% Analysis Date = 02/21/17 Pct Recovery = 72% Analysis Date = 02/21/17 Pct Recovery = 72% Analysis Date = 02/19/17 Pct Recovery = 72% Analysis Date = 02/19/17 Pct Recovery = 72% Analysis Date = 02/17/17 Pct Recovery = 72% Analysis Date = 02/17/17 Pct Recovery = 72% Analysis Date = 02/15/17 Pct Recovery = 72% Analysis Date = 02/15/17 Pct Recovery = 72% Analysis Date = 02/12/17 Pct Recovery = 73% Analysis Date = 02/12/17 Pct Recovery = 73% Analysis Date = 02/10/17 Pct Recovery = 73% Analysis Date = 02/10/17 Pct Recovery = 73% Analysis Date = 02/08/17 Pct Recovery = 73% Analysis Date = 02/08/17 Pct Recovery = 73% Analysis Date = 02/06/17 Pct Recovery = 73% Analysis Date = 02/06/17 Pct Recovery = 73% Analysis Date = 02/04/17 Pct Recovery = 73% Analysis Date = 02/04/17 Pct Recovery = 73% Analysis Date = 02/02/17 Pct Recovery = 73% Analysis Date = 02/02/17 Pct Recovery = 73% Analysis Date = 01/30/17 Pct Recovery = 73% Analysis Date = 01/30/17 Pct Recovery = 73% Analysis Date = 01/28/17 Pct Recovery = 73% Analysis Date = 01/28/17 Pct Recovery = 73% Analysis Date = 01/26/17 Pct Recovery = 73% Analysis Date = 01/26/17 Pct Recovery = 73% Analysis Date = 01/24/17 Pct Recovery = 73% Analysis Date = 01/24/17 Pct Recovery = 73% Analysis Date = 01/22/17 Pct Recovery = 73% Analysis Date = 01/22/17 Pct Recovery = 73% Analysis Date = 01/20/17 Pct Recovery = 73% Analysis Date = 01/20/17 Pct Recovery = 73% Analysis Date = 01/17/17 Pct Recovery = 74% Analysis Date = 01/17/17 Pct Recovery = 74% Analysis Date = 01/15/17 Pct Recovery = 74% Analysis Date = 01/15/17 Pct Recovery = 74% Analysis Date = 01/13/17 Pct Recovery = 74% Analysis Date = 01/13/17 Pct Recovery = 74% Analysis Date = 01/11/17 Pct Recovery = 74% Analysis Date = 01/11/17 Pct Recovery = 74% Analysis Date = 01/09/17 Pct Recovery = 75% Analysis Date = 01/09/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 01/04/17 Pct Recovery = 75% Analysis Date = 01/04/17 Pct Recovery = 75% Analysis Date = 01/02/17 Pct Recovery = 75% Analysis Date = 01/02/17 Pct Recovery = 75% Analysis Date = 12/31/16 Pct Recovery = 75% Analysis Date = 12/31/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 76% Analysis Date = 12/29/16 Pct Recovery = 76% Analysis Date = 12/27/16 Pct Recovery = 76% Analysis Date = 12/27/16 Pct Recovery = 76% Analysis Date = 12/24/16 Pct Recovery = 76% Analysis Date = 12/24/16 Pct Recovery = 76% Analysis Date = 12/22/16 Pct Recovery = 76% Analysis Date = 12/22/16 Pct Recovery = 76% Analysis Date = 12/20/16 Pct Recovery = 77% Analysis Date = 12/20/16 Pct Recovery = 77% Analysis Date = 12/18/16 Pct Recovery = 77% Analysis Date = 12/18/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 77% Analysis Date = 12/16/16 Pct Recovery = 77% Analysis Date = 12/14/16 Pct Recovery = 77% Analysis Date = 12/14/16 Pct Recovery = 77% Analysis Date = 12/11/16 Pct Recovery = 77% Analysis Date = 12/11/16 Pct Recovery = 77% Analysis Date = 12/09/16 Pct Recovery = 78% Analysis Date = 12/09/16 Pct Recovery = 78% Analysis Date = 12/07/16 Pct Recovery = 78% Analysis Date = 12/07/16 Pct Recovery = 78% Analysis Date = 12/05/16 Pct Recovery = 78% Analysis Date = 12/05/16 Pct Recovery = 78% Analysis Date = 12/03/16 Pct Recovery = 78% Analysis Date = 12/03/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 78% Analysis Date = 12/01/16 Pct Recovery = 78% Analysis Date = 11/28/16 Pct Recovery = 78% Analysis Date = 11/28/16 Pct Recovery = 78% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/26/16 Pct Recovery = 79% Analysis Date = 11/24/16 Pct Recovery = 79% Analysis Date = 11/24/16 Pct Recovery = 79% Analysis Date = 11/22/16 Pct Recovery = 79% Analysis Date = 11/22/16 Pct Recovery = 79% Analysis Date = 11/20/16 Pct Recovery = 79% Analysis Date = 11/20/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/17/16 Pct Recovery = 79% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/15/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/13/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/11/16 Pct Recovery = 80% Analysis Date = 11/09/16 Pct Recovery = 80% Analysis Date = 11/09/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/07/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/04/16 Pct Recovery = 80% Analysis Date = 11/02/16 Pct Recovery = 81% Analysis Date = 11/02/16 Pct Recovery = 81% Analysis Date = 10/31/16 Pct Recovery = 81% Analysis Date = 10/31/16 Pct Recovery = 81% Analysis Date = 10/29/16 Pct Recovery = 81% Analysis Date = 10/29/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/27/16 Pct Recovery = 81% Analysis Date = 10/25/16 Pct Recovery = 81% Analysis Date = 10/25/16 Pct Recovery = 81% Analysis Date = 10/22/16 Pct Recovery = 82% Analysis Date = 10/22/16 Pct Recovery = 82% Analysis Date = 10/20/16 Pct Recovery = 82% Analysis Date = 10/20/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/18/16 Pct Recovery = 82% Analysis Date = 10/16/16 Pct Recovery = 82% Analysis Date = 10/16/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/12/16 Pct Recovery = 82% Analysis Date = 10/12/16 Pct Recovery = 82% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/09/16 Pct Recovery = 83% Analysis Date = 10/07/16 Pct Recovery = 83% Analysis Date = 10/07/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/03/16 Pct Recovery = 83% Analysis Date = 10/03/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/28/16 Pct Recovery = 83% Analysis Date = 09/28/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 84% Analysis Date = 09/26/16 Pct Recovery = 84% Analysis Date = 09/24/16 Pct Recovery = 84% Analysis Date = 09/24/16 Pct Recovery = 84% Analysis Date = 09/22/16 Pct Recovery = 84% Analysis Date = 09/22/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/20/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/18/16 Pct Recovery = 84% Analysis Date = 09/15/16 Pct Recovery = 85% Analysis Date = 09/15/16 Pct Recovery = 85% Analysis Date = 09/13/16 Pct Recovery = 85% Analysis Date = 09/13/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/11/16 Pct Recovery = 85% Analysis Date = 09/09/16 Pct Recovery = 85% Analysis Date = 09/09/16 Pct Recovery = 85% Analysis Date = 09/07/16 Pct Recovery = 85% Analysis Date = 09/07/16 Pct Recovery = 85% Analysis Date = 09/05/16 Pct Recovery = 85% Analysis Date = 09/05/16 Pct Recovery = 85% Analysis Date = 09/02/16 Pct Recovery = 85% Analysis Date = 09/02/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/31/16 Pct Recovery = 85% Analysis Date = 08/29/16 Pct Recovery = 85% Analysis Date = 08/29/16 Pct Recovery = 85% Analysis Date = 08/27/16 Pct Recovery = 85% Analysis Date = 08/27/16 Pct Recovery = 85% Analysis Date = 08/25/16 Pct Recovery = 84% Analysis Date = 08/25/16 Pct Recovery = 84% Analysis Date = 08/22/16 Pct Recovery = 84% Analysis Date = 08/22/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/20/16 Pct Recovery = 84% Analysis Date = 08/18/16 Pct Recovery = 84% Analysis Date = 08/18/16 Pct Recovery = 84% Analysis Date = 08/16/16 Pct Recovery = 84% Analysis Date = 08/16/16 Pct Recovery = 84% Analysis Date = 08/14/16 Pct Recovery = 83% Analysis Date = 08/14/16 Pct Recovery = 83% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 81% Analysis Date = 08/07/16 Pct Recovery = 81% Analysis Date = 08/05/16 Pct Recovery = 81% Analysis Date = 08/05/16 Pct Recovery = 81% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 08/03/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 08/01/16 Pct Recovery = 80% Analysis Date = 07/30/16 Pct Recovery = 79% Analysis Date = 07/30/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 79% Analysis Date = 07/27/16 Pct Recovery = 79% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/25/16 Pct Recovery = 78% Analysis Date = 07/23/16 Pct Recovery = 78% Analysis Date = 07/23/16 Pct Recovery = 78% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/19/16 Pct Recovery = 77% Analysis Date = 07/19/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 75% Analysis Date = 07/12/16 Pct Recovery = 75% Analysis Date = 07/10/16 Pct Recovery = 75% Analysis Date = 07/10/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 74% Analysis Date = 07/08/16 Pct Recovery = 74% Analysis Date = 07/06/16 Pct Recovery = 74% Analysis Date = 07/06/16 Pct Recovery = 74% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 72% Analysis Date = 06/29/16 Pct Recovery = 72% Analysis Date = 06/27/16 Pct Recovery = 72% Analysis Date = 06/27/16 Pct Recovery = 72% Analysis Date = 06/25/16 Pct Recovery = 71% Analysis Date = 06/25/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/23/16 Pct Recovery = 71% Analysis Date = 06/20/16 Pct Recovery = 70% Analysis Date = 06/20/16 Pct Recovery = 70% Analysis Date = 06/18/16 Pct Recovery = 70% Analysis Date = 06/18/16 Pct Recovery = 70% Analysis Date = 06/16/16 Pct Recovery = 69% Analysis Date = 06/16/16 Pct Recovery = 69% Analysis Date = 06/14/16 Pct Recovery = 69% Analysis Date = 06/14/16 Pct Recovery = 69% Analysis Date = 06/12/16 Pct Recovery = 68% Analysis Date = 06/12/16 Pct Recovery = 68% Analysis Date = 06/10/16 Pct Recovery = 68% Analysis Date = 06/10/16 Pct Recovery = 68% Analysis Date = 06/07/16 Pct Recovery = 67% Analysis Date = 06/07/16 Pct Recovery = 67% Analysis Date = 06/05/16 Pct Recovery = 67% Analysis Date = 06/05/16 Pct Recovery = 67% Analysis Date = 06/03/16 Pct Recovery = 66% Analysis Date = 06/03/16 Pct Recovery = 66% Analysis Date = 06/01/16 Pct Recovery = 66% Analysis Date = 06/01/16 Pct Recovery = 66% Analysis Date = 05/30/16 Pct Recovery = 65% Analysis Date = 05/30/16 Pct Recovery = 65% Analysis Date = 05/27/16 Pct Recovery = 65% Analysis Date = 05/27/16 Pct Recovery = 65% Analysis Date = 05/25/16 Pct Recovery = 64% Analysis Date = 05/25/16 Pct Recovery = 64% Analysis Date = 05/23/16 Pct Recovery = 64% Analysis Date = 05/23/16 Pct Recovery = 64% Analysis Date = 05/21/16 Pct Recovery = 63% Analysis Date = 05/21/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/19/16 Pct Recovery = 63% Analysis Date = 05/17/16 Pct Recovery = 62% Analysis Date = 05/17/16 Pct Recovery = 62% Analysis Date = 05/14/16 Pct Recovery = 62% Analysis Date = 05/14/16 Pct Recovery = 62% Analysis Date = 05/12/16 Pct Recovery = 61% Analysis Date = 05/12/16 Pct Recovery = 61% Analysis Date = 05/10/16 Pct Recovery = 61% Analysis Date = 05/10/16 Pct Recovery = 61% Analysis Date = 05/08/16 Pct Recovery = 60% Analysis Date = 05/08/16 Pct Recovery = 60% Analysis Date = 05/06/16 Pct Recovery = 60% Analysis Date = 05/06/16 Pct Recovery = 60% Analysis Date = 05/04/16 Pct Recovery = 60% Analysis Date = 05/04/16 Pct Recovery = 60% Analysis Date = 05/01/16 Pct Recovery = 59% Analysis Date = 05/01/16 Pct Recovery = 59% Analysis Date = 04/29/16 Pct Recovery = 59% Analysis Date = 04/29/16 Pct Recovery = 59% Analysis Date = 04/27/16 Pct Recovery = 58% Analysis Date = 04/27/16 Pct Recovery = 58% Analysis Date = 04/25/16 Pct Recovery = 58% Analysis Date = 04/25/16 Pct Recovery = 58% Analysis Date = 04/23/16 Pct Recovery = 57% Analysis Date = 04/23/16 Pct Recovery = 57% Analysis Date = 04/21/16 Pct Recovery = 57% Analysis Date = 04/21/16 Pct Recovery = 57% Analysis Date = 04/18/16 Pct Recovery = 56% Analysis Date = 04/18/16 Pct Recovery = 56% Analysis Date = 04/16/16 Pct Recovery = 56% Analysis Date = 04/16/16 Pct Recovery = 56% Analysis Date = 04/14/16 Pct Recovery = 56% Analysis Date = 04/14/16 Pct Recovery = 56% Analysis Date = 04/12/16 Pct Recovery = 55% Analysis Date = 04/12/16 Pct Recovery = 55% Analysis Date = 04/10/16 Pct Recovery = 55% Analysis Date = 04/10/16 Pct Recovery = 55% Analysis Date = 04/07/16 Pct Recovery = 54% Analysis Date = 04/07/16 Pct Recovery = 54% Analysis Date = 04/05/16 Pct Recovery = 54% Analysis Date = 04/05/16 Pct Recovery = 54% Analysis Date = 04/03/16 Pct Recovery = 53% Analysis Date = 04/03/16 Pct Recovery = 53% Analysis Date = 04/01/16 Pct Recovery = 53% Analysis Date = 04/01/16 Pct Recovery = 53% Analysis Date = 03/30/16 Pct Recovery = 53% Analysis Date = 03/30/16 Pct Recovery = 53% Analysis Date = 03/28/16 Pct Recovery = 52% Analysis Date = 03/28/16 Pct Recovery = 52% Analysis Date = 03/25/16 Pct Recovery = 52% Analysis Date = 03/25/16 Pct Recovery = 52% Analysis Date = 03/23/16 Pct Recovery = 51% Analysis Date = 03/23/16 Pct Recovery = 51% Analysis Date = 03/21/16 Pct Recovery = 51% Analysis Date = 03/21/16 Pct Recovery = 51% Analysis Date = 03/19/16 Pct Recovery = 50% Analysis Date = 03/19/16 Pct Recovery = 50% Analysis Date = 03/17/16 Pct Recovery = 50% Analysis Date = 03/17/16 Pct Recovery = 50% Analysis Date = 03/15/16 Pct Recovery = 50% Analysis Date = 03/15/16 Pct Recovery = 50% Analysis Date = 03/12/16 Pct Recovery = 49% Analysis Date = 03/12/16 Pct Recovery = 49% Analysis Date = 03/10/16 Pct Recovery = 49% Analysis Date = 03/10/16 Pct Recovery = 49% Analysis Date = 03/08/16 Pct Recovery = 48% Analysis Date = 03/08/16 Pct Recovery = 48% Analysis Date = 03/06/16 Pct Recovery = 48% Analysis Date = 03/06/16 Pct Recovery = 48% Analysis Date = 03/04/16 Pct Recovery = 47% Analysis Date = 03/04/16 Pct Recovery = 47% Analysis Date = 03/02/16 Pct Recovery = 47% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHORATE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 70% 15% 71% 16%
Total 19 70% 15% 71% 16%

Sample Statistics
PHORATE

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
PHORATE OXON
METHOD: 2033 , TESTIDCODE: 61666GCM39

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 95% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 69% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 55% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 69% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 92% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 73% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 65% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 83% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 108% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 62% Analysis Date = 05/10/17 Pct Recovery = 66% Analysis Date = 05/08/17 Pct Recovery = 66% Analysis Date = 05/08/17 Pct Recovery = 66% Analysis Date = 05/06/17 Pct Recovery = 67% Analysis Date = 05/06/17 Pct Recovery = 67% Analysis Date = 05/04/17 Pct Recovery = 67% Analysis Date = 05/04/17 Pct Recovery = 67% Analysis Date = 05/01/17 Pct Recovery = 67% Analysis Date = 05/01/17 Pct Recovery = 67% Analysis Date = 04/29/17 Pct Recovery = 67% Analysis Date = 04/29/17 Pct Recovery = 67% Analysis Date = 04/27/17 Pct Recovery = 67% Analysis Date = 04/27/17 Pct Recovery = 67% Analysis Date = 04/25/17 Pct Recovery = 68% Analysis Date = 04/25/17 Pct Recovery = 68% Analysis Date = 04/22/17 Pct Recovery = 68% Analysis Date = 04/22/17 Pct Recovery = 68% Analysis Date = 04/20/17 Pct Recovery = 68% Analysis Date = 04/20/17 Pct Recovery = 68% Analysis Date = 04/18/17 Pct Recovery = 68% Analysis Date = 04/18/17 Pct Recovery = 68% Analysis Date = 04/15/17 Pct Recovery = 68% Analysis Date = 04/15/17 Pct Recovery = 68% Analysis Date = 04/13/17 Pct Recovery = 69% Analysis Date = 04/13/17 Pct Recovery = 69% Analysis Date = 04/11/17 Pct Recovery = 69% Analysis Date = 04/11/17 Pct Recovery = 69% Analysis Date = 04/09/17 Pct Recovery = 69% Analysis Date = 04/09/17 Pct Recovery = 69% Analysis Date = 04/06/17 Pct Recovery = 69% Analysis Date = 04/06/17 Pct Recovery = 69% Analysis Date = 04/04/17 Pct Recovery = 69% Analysis Date = 04/04/17 Pct Recovery = 69% Analysis Date = 04/02/17 Pct Recovery = 70% Analysis Date = 04/02/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/26/17 Pct Recovery = 70% Analysis Date = 03/26/17 Pct Recovery = 70% Analysis Date = 03/24/17 Pct Recovery = 70% Analysis Date = 03/24/17 Pct Recovery = 70% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/21/17 Pct Recovery = 71% Analysis Date = 03/19/17 Pct Recovery = 71% Analysis Date = 03/19/17 Pct Recovery = 71% Analysis Date = 03/17/17 Pct Recovery = 71% Analysis Date = 03/17/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 71% Analysis Date = 03/10/17 Pct Recovery = 72% Analysis Date = 03/10/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/05/17 Pct Recovery = 72% Analysis Date = 03/05/17 Pct Recovery = 72% Analysis Date = 03/03/17 Pct Recovery = 72% Analysis Date = 03/03/17 Pct Recovery = 72% Analysis Date = 03/01/17 Pct Recovery = 72% Analysis Date = 03/01/17 Pct Recovery = 72% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/22/17 Pct Recovery = 73% Analysis Date = 02/22/17 Pct Recovery = 73% Analysis Date = 02/20/17 Pct Recovery = 73% Analysis Date = 02/20/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/17/17 Pct Recovery = 73% Analysis Date = 02/15/17 Pct Recovery = 74% Analysis Date = 02/15/17 Pct Recovery = 74% Analysis Date = 02/13/17 Pct Recovery = 74% Analysis Date = 02/13/17 Pct Recovery = 74% Analysis Date = 02/10/17 Pct Recovery = 74% Analysis Date = 02/10/17 Pct Recovery = 74% Analysis Date = 02/08/17 Pct Recovery = 74% Analysis Date = 02/08/17 Pct Recovery = 74% Analysis Date = 02/06/17 Pct Recovery = 74% Analysis Date = 02/06/17 Pct Recovery = 74% Analysis Date = 02/04/17 Pct Recovery = 75% Analysis Date = 02/04/17 Pct Recovery = 75% Analysis Date = 02/01/17 Pct Recovery = 75% Analysis Date = 02/01/17 Pct Recovery = 75% Analysis Date = 01/30/17 Pct Recovery = 75% Analysis Date = 01/30/17 Pct Recovery = 75% Analysis Date = 01/28/17 Pct Recovery = 75% Analysis Date = 01/28/17 Pct Recovery = 75% Analysis Date = 01/25/17 Pct Recovery = 75% Analysis Date = 01/25/17 Pct Recovery = 75% Analysis Date = 01/23/17 Pct Recovery = 76% Analysis Date = 01/23/17 Pct Recovery = 76% Analysis Date = 01/21/17 Pct Recovery = 76% Analysis Date = 01/21/17 Pct Recovery = 76% Analysis Date = 01/19/17 Pct Recovery = 76% Analysis Date = 01/19/17 Pct Recovery = 76% Analysis Date = 01/16/17 Pct Recovery = 76% Analysis Date = 01/16/17 Pct Recovery = 76% Analysis Date = 01/14/17 Pct Recovery = 77% Analysis Date = 01/14/17 Pct Recovery = 77% Analysis Date = 01/12/17 Pct Recovery = 77% Analysis Date = 01/12/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 78% Analysis Date = 01/07/17 Pct Recovery = 78% Analysis Date = 01/05/17 Pct Recovery = 78% Analysis Date = 01/05/17 Pct Recovery = 78% Analysis Date = 01/03/17 Pct Recovery = 78% Analysis Date = 01/03/17 Pct Recovery = 78% Analysis Date = 12/31/16 Pct Recovery = 79% Analysis Date = 12/31/16 Pct Recovery = 79% Analysis Date = 12/29/16 Pct Recovery = 79% Analysis Date = 12/29/16 Pct Recovery = 79% Analysis Date = 12/27/16 Pct Recovery = 79% Analysis Date = 12/27/16 Pct Recovery = 79% Analysis Date = 12/24/16 Pct Recovery = 79% Analysis Date = 12/24/16 Pct Recovery = 79% Analysis Date = 12/22/16 Pct Recovery = 80% Analysis Date = 12/22/16 Pct Recovery = 80% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/20/16 Pct Recovery = 80% Analysis Date = 12/18/16 Pct Recovery = 80% Analysis Date = 12/18/16 Pct Recovery = 80% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/15/16 Pct Recovery = 81% Analysis Date = 12/13/16 Pct Recovery = 81% Analysis Date = 12/13/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/11/16 Pct Recovery = 81% Analysis Date = 12/08/16 Pct Recovery = 82% Analysis Date = 12/08/16 Pct Recovery = 82% Analysis Date = 12/06/16 Pct Recovery = 82% Analysis Date = 12/06/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/04/16 Pct Recovery = 82% Analysis Date = 12/02/16 Pct Recovery = 83% Analysis Date = 12/02/16 Pct Recovery = 83% Analysis Date = 11/29/16 Pct Recovery = 83% Analysis Date = 11/29/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/27/16 Pct Recovery = 83% Analysis Date = 11/25/16 Pct Recovery = 84% Analysis Date = 11/25/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/20/16 Pct Recovery = 84% Analysis Date = 11/20/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 85% Analysis Date = 11/13/16 Pct Recovery = 85% Analysis Date = 11/13/16 Pct Recovery = 85% Analysis Date = 11/11/16 Pct Recovery = 85% Analysis Date = 11/11/16 Pct Recovery = 85% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 11/02/16 Pct Recovery = 87% Analysis Date = 10/31/16 Pct Recovery = 87% Analysis Date = 10/31/16 Pct Recovery = 87% Analysis Date = 10/28/16 Pct Recovery = 87% Analysis Date = 10/28/16 Pct Recovery = 87% Analysis Date = 10/26/16 Pct Recovery = 88% Analysis Date = 10/26/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/24/16 Pct Recovery = 88% Analysis Date = 10/21/16 Pct Recovery = 88% Analysis Date = 10/21/16 Pct Recovery = 88% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/19/16 Pct Recovery = 89% Analysis Date = 10/17/16 Pct Recovery = 89% Analysis Date = 10/17/16 Pct Recovery = 89% Analysis Date = 10/15/16 Pct Recovery = 89% Analysis Date = 10/15/16 Pct Recovery = 89% Analysis Date = 10/12/16 Pct Recovery = 89% Analysis Date = 10/12/16 Pct Recovery = 89% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/03/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 10/01/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/29/16 Pct Recovery = 91% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/26/16 Pct Recovery = 92% Analysis Date = 09/24/16 Pct Recovery = 92% Analysis Date = 09/24/16 Pct Recovery = 92% Analysis Date = 09/22/16 Pct Recovery = 92% Analysis Date = 09/22/16 Pct Recovery = 92% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/19/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/15/16 Pct Recovery = 93% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/13/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 94% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 93% Analysis Date = 09/03/16 Pct Recovery = 93% Analysis Date = 09/03/16 Pct Recovery = 93% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 92% Analysis Date = 08/30/16 Pct Recovery = 92% Analysis Date = 08/30/16 Pct Recovery = 92% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/28/16 Pct Recovery = 91% Analysis Date = 08/25/16 Pct Recovery = 91% Analysis Date = 08/25/16 Pct Recovery = 91% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/23/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/21/16 Pct Recovery = 90% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 08/02/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 84% Analysis Date = 07/31/16 Pct Recovery = 84% Analysis Date = 07/29/16 Pct Recovery = 84% Analysis Date = 07/29/16 Pct Recovery = 84% Analysis Date = 07/27/16 Pct Recovery = 83% Analysis Date = 07/27/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/24/16 Pct Recovery = 83% Analysis Date = 07/22/16 Pct Recovery = 82% Analysis Date = 07/22/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 82% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/17/16 Pct Recovery = 81% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/15/16 Pct Recovery = 80% Analysis Date = 07/13/16 Pct Recovery = 80% Analysis Date = 07/13/16 Pct Recovery = 80% Analysis Date = 07/11/16 Pct Recovery = 79% Analysis Date = 07/11/16 Pct Recovery = 79% Analysis Date = 07/08/16 Pct Recovery = 79% Analysis Date = 07/08/16 Pct Recovery = 79% Analysis Date = 07/06/16 Pct Recovery = 78% Analysis Date = 07/06/16 Pct Recovery = 78% Analysis Date = 07/04/16 Pct Recovery = 78% Analysis Date = 07/04/16 Pct Recovery = 78% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 07/01/16 Pct Recovery = 77% Analysis Date = 06/29/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/27/16 Pct Recovery = 76% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/22/16 Pct Recovery = 75% Analysis Date = 06/20/16 Pct Recovery = 74% Analysis Date = 06/20/16 Pct Recovery = 74% Analysis Date = 06/18/16 Pct Recovery = 74% Analysis Date = 06/18/16 Pct Recovery = 74% Analysis Date = 06/15/16 Pct Recovery = 73% Analysis Date = 06/15/16 Pct Recovery = 73% Analysis Date = 06/13/16 Pct Recovery = 72% Analysis Date = 06/13/16 Pct Recovery = 72% Analysis Date = 06/11/16 Pct Recovery = 72% Analysis Date = 06/11/16 Pct Recovery = 72% Analysis Date = 06/09/16 Pct Recovery = 71% Analysis Date = 06/09/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/06/16 Pct Recovery = 71% Analysis Date = 06/04/16 Pct Recovery = 70% Analysis Date = 06/04/16 Pct Recovery = 70% Analysis Date = 06/02/16 Pct Recovery = 70% Analysis Date = 06/02/16 Pct Recovery = 70% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/28/16 Pct Recovery = 68% Analysis Date = 05/28/16 Pct Recovery = 68% Analysis Date = 05/26/16 Pct Recovery = 69% Analysis Date = 05/26/16 Pct Recovery = 69% Analysis Date = 05/24/16 Pct Recovery = 69% Analysis Date = 05/24/16 Pct Recovery = 69% Analysis Date = 05/21/16 Pct Recovery = 70% Analysis Date = 05/21/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 70% Analysis Date = 05/19/16 Pct Recovery = 70% Analysis Date = 05/17/16 Pct Recovery = 71% Analysis Date = 05/17/16 Pct Recovery = 71% Analysis Date = 05/14/16 Pct Recovery = 71% Analysis Date = 05/14/16 Pct Recovery = 71% Analysis Date = 05/12/16 Pct Recovery = 72% Analysis Date = 05/12/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/08/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 73% Analysis Date = 05/05/16 Pct Recovery = 73% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/03/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 05/01/16 Pct Recovery = 74% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/28/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/26/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 76% Analysis Date = 04/24/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/19/16 Pct Recovery = 77% Analysis Date = 04/19/16 Pct Recovery = 77% Analysis Date = 04/17/16 Pct Recovery = 77% Analysis Date = 04/17/16 Pct Recovery = 77% Analysis Date = 04/15/16 Pct Recovery = 77% Analysis Date = 04/15/16 Pct Recovery = 77% Analysis Date = 04/12/16 Pct Recovery = 77% Analysis Date = 04/12/16 Pct Recovery = 77% Analysis Date = 04/10/16 Pct Recovery = 76% Analysis Date = 04/10/16 Pct Recovery = 76% Analysis Date = 04/08/16 Pct Recovery = 76% Analysis Date = 04/08/16 Pct Recovery = 76% Analysis Date = 04/06/16 Pct Recovery = 76% Analysis Date = 04/06/16 Pct Recovery = 76% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 04/03/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 04/01/16 Pct Recovery = 75% Analysis Date = 03/30/16 Pct Recovery = 74% Analysis Date = 03/30/16 Pct Recovery = 74% Analysis Date = 03/27/16 Pct Recovery = 74% Analysis Date = 03/27/16 Pct Recovery = 74% Analysis Date = 03/25/16 Pct Recovery = 73% Analysis Date = 03/25/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/23/16 Pct Recovery = 73% Analysis Date = 03/21/16 Pct Recovery = 72% Analysis Date = 03/21/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/18/16 Pct Recovery = 72% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/16/16 Pct Recovery = 71% Analysis Date = 03/14/16 Pct Recovery = 70% Analysis Date = 03/14/16 Pct Recovery = 70% Analysis Date = 03/11/16 Pct Recovery = 70% Analysis Date = 03/11/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 69% Analysis Date = 03/09/16 Pct Recovery = 69% Analysis Date = 03/07/16 Pct Recovery = 69% Analysis Date = 03/07/16 Pct Recovery = 69% Analysis Date = 03/05/16 Pct Recovery = 68% Analysis Date = 03/05/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 03/02/16 Pct Recovery = 68% Analysis Date = 02/29/16 Pct Recovery = 67% Analysis Date = 02/29/16 Pct Recovery = 67% Analysis Date = 02/27/16 Pct Recovery = 66% Analysis Date = 02/27/16 Pct Recovery = 66% Analysis Date = 02/24/16 Pct Recovery = 66% Analysis Date = 02/24/16 Pct Recovery = 66% Analysis Date = 02/22/16 Pct Recovery = 65% Analysis Date = 02/22/16 Pct Recovery = 65% Analysis Date = 02/20/16 Pct Recovery = 65% Analysis Date = 02/20/16 Pct Recovery = 65% Analysis Date = 02/18/16 Pct Recovery = 64% Analysis Date = 02/18/16 Pct Recovery = 64% Analysis Date = 02/15/16 Pct Recovery = 64% Analysis Date = 02/15/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 63% Analysis Date = 02/13/16 Pct Recovery = 63% Analysis Date = 02/11/16 Pct Recovery = 63% Analysis Date = 02/11/16 Pct Recovery = 63% Analysis Date = 02/09/16 Pct Recovery = 62% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHORATE OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 74% 15% 69% 14%
Total 13 74% 15% 69% 14%

Sample Statistics
PHORATE OXON

Characteristic N % % Basis
Plotted 13 100% Spiked
Estimated Values 13 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 13 .  
False Negatives 0 0% 0 out of 13
Not Spiked 15 .  
False Positives 0 0% 0 out of 15

OBSP Determination:
PHOSMET (IMIDAN)
METHOD: 2033 , TESTIDCODE: 61601GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 56% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 57% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 71% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 58% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 57% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 49% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 56% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 59% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 50% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 47% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 50% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 53% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 50% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 58% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 55% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 49% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 50% Analysis Date = 05/02/17 Pct Recovery = 55% Analysis Date = 04/30/17 Pct Recovery = 55% Analysis Date = 04/30/17 Pct Recovery = 55% Analysis Date = 04/28/17 Pct Recovery = 55% Analysis Date = 04/28/17 Pct Recovery = 55% Analysis Date = 04/26/17 Pct Recovery = 55% Analysis Date = 04/26/17 Pct Recovery = 55% Analysis Date = 04/24/17 Pct Recovery = 55% Analysis Date = 04/24/17 Pct Recovery = 55% Analysis Date = 04/21/17 Pct Recovery = 55% Analysis Date = 04/21/17 Pct Recovery = 55% Analysis Date = 04/19/17 Pct Recovery = 55% Analysis Date = 04/19/17 Pct Recovery = 55% Analysis Date = 04/17/17 Pct Recovery = 55% Analysis Date = 04/17/17 Pct Recovery = 55% Analysis Date = 04/15/17 Pct Recovery = 55% Analysis Date = 04/15/17 Pct Recovery = 55% Analysis Date = 04/12/17 Pct Recovery = 55% Analysis Date = 04/12/17 Pct Recovery = 55% Analysis Date = 04/10/17 Pct Recovery = 55% Analysis Date = 04/10/17 Pct Recovery = 55% Analysis Date = 04/08/17 Pct Recovery = 55% Analysis Date = 04/08/17 Pct Recovery = 55% Analysis Date = 04/06/17 Pct Recovery = 56% Analysis Date = 04/06/17 Pct Recovery = 56% Analysis Date = 04/03/17 Pct Recovery = 56% Analysis Date = 04/03/17 Pct Recovery = 56% Analysis Date = 04/01/17 Pct Recovery = 56% Analysis Date = 04/01/17 Pct Recovery = 56% Analysis Date = 03/30/17 Pct Recovery = 56% Analysis Date = 03/30/17 Pct Recovery = 56% Analysis Date = 03/28/17 Pct Recovery = 56% Analysis Date = 03/28/17 Pct Recovery = 56% Analysis Date = 03/25/17 Pct Recovery = 56% Analysis Date = 03/25/17 Pct Recovery = 56% Analysis Date = 03/23/17 Pct Recovery = 56% Analysis Date = 03/23/17 Pct Recovery = 56% Analysis Date = 03/21/17 Pct Recovery = 56% Analysis Date = 03/21/17 Pct Recovery = 56% Analysis Date = 03/19/17 Pct Recovery = 56% Analysis Date = 03/19/17 Pct Recovery = 56% Analysis Date = 03/16/17 Pct Recovery = 56% Analysis Date = 03/16/17 Pct Recovery = 56% Analysis Date = 03/14/17 Pct Recovery = 56% Analysis Date = 03/14/17 Pct Recovery = 56% Analysis Date = 03/12/17 Pct Recovery = 56% Analysis Date = 03/12/17 Pct Recovery = 56% Analysis Date = 03/10/17 Pct Recovery = 56% Analysis Date = 03/10/17 Pct Recovery = 56% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/07/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 56% Analysis Date = 03/05/17 Pct Recovery = 56% Analysis Date = 03/03/17 Pct Recovery = 57% Analysis Date = 03/03/17 Pct Recovery = 57% Analysis Date = 03/01/17 Pct Recovery = 57% Analysis Date = 03/01/17 Pct Recovery = 57% Analysis Date = 02/26/17 Pct Recovery = 57% Analysis Date = 02/26/17 Pct Recovery = 57% Analysis Date = 02/24/17 Pct Recovery = 57% Analysis Date = 02/24/17 Pct Recovery = 57% Analysis Date = 02/22/17 Pct Recovery = 57% Analysis Date = 02/22/17 Pct Recovery = 57% Analysis Date = 02/20/17 Pct Recovery = 57% Analysis Date = 02/20/17 Pct Recovery = 57% Analysis Date = 02/17/17 Pct Recovery = 57% Analysis Date = 02/17/17 Pct Recovery = 57% Analysis Date = 02/15/17 Pct Recovery = 57% Analysis Date = 02/15/17 Pct Recovery = 57% Analysis Date = 02/13/17 Pct Recovery = 57% Analysis Date = 02/13/17 Pct Recovery = 57% Analysis Date = 02/11/17 Pct Recovery = 57% Analysis Date = 02/11/17 Pct Recovery = 57% Analysis Date = 02/08/17 Pct Recovery = 57% Analysis Date = 02/08/17 Pct Recovery = 57% Analysis Date = 02/06/17 Pct Recovery = 57% Analysis Date = 02/06/17 Pct Recovery = 57% Analysis Date = 02/04/17 Pct Recovery = 57% Analysis Date = 02/04/17 Pct Recovery = 57% Analysis Date = 02/02/17 Pct Recovery = 57% Analysis Date = 02/02/17 Pct Recovery = 57% Analysis Date = 01/30/17 Pct Recovery = 57% Analysis Date = 01/30/17 Pct Recovery = 57% Analysis Date = 01/28/17 Pct Recovery = 57% Analysis Date = 01/28/17 Pct Recovery = 57% Analysis Date = 01/26/17 Pct Recovery = 57% Analysis Date = 01/26/17 Pct Recovery = 57% Analysis Date = 01/24/17 Pct Recovery = 57% Analysis Date = 01/24/17 Pct Recovery = 57% Analysis Date = 01/21/17 Pct Recovery = 57% Analysis Date = 01/21/17 Pct Recovery = 57% Analysis Date = 01/19/17 Pct Recovery = 57% Analysis Date = 01/19/17 Pct Recovery = 57% Analysis Date = 01/17/17 Pct Recovery = 57% Analysis Date = 01/17/17 Pct Recovery = 57% Analysis Date = 01/15/17 Pct Recovery = 57% Analysis Date = 01/15/17 Pct Recovery = 57% Analysis Date = 01/12/17 Pct Recovery = 57% Analysis Date = 01/12/17 Pct Recovery = 57% Analysis Date = 01/10/17 Pct Recovery = 57% Analysis Date = 01/10/17 Pct Recovery = 57% Analysis Date = 01/08/17 Pct Recovery = 57% Analysis Date = 01/08/17 Pct Recovery = 57% Analysis Date = 01/06/17 Pct Recovery = 57% Analysis Date = 01/06/17 Pct Recovery = 57% Analysis Date = 01/04/17 Pct Recovery = 57% Analysis Date = 01/04/17 Pct Recovery = 57% Analysis Date = 01/01/17 Pct Recovery = 57% Analysis Date = 01/01/17 Pct Recovery = 57% Analysis Date = 12/30/16 Pct Recovery = 57% Analysis Date = 12/30/16 Pct Recovery = 57% Analysis Date = 12/28/16 Pct Recovery = 57% Analysis Date = 12/28/16 Pct Recovery = 57% Analysis Date = 12/26/16 Pct Recovery = 57% Analysis Date = 12/26/16 Pct Recovery = 57% Analysis Date = 12/23/16 Pct Recovery = 57% Analysis Date = 12/23/16 Pct Recovery = 57% Analysis Date = 12/21/16 Pct Recovery = 57% Analysis Date = 12/21/16 Pct Recovery = 57% Analysis Date = 12/19/16 Pct Recovery = 57% Analysis Date = 12/19/16 Pct Recovery = 57% Analysis Date = 12/17/16 Pct Recovery = 57% Analysis Date = 12/17/16 Pct Recovery = 57% Analysis Date = 12/14/16 Pct Recovery = 57% Analysis Date = 12/14/16 Pct Recovery = 57% Analysis Date = 12/12/16 Pct Recovery = 57% Analysis Date = 12/12/16 Pct Recovery = 57% Analysis Date = 12/10/16 Pct Recovery = 57% Analysis Date = 12/10/16 Pct Recovery = 57% Analysis Date = 12/08/16 Pct Recovery = 57% Analysis Date = 12/08/16 Pct Recovery = 57% Analysis Date = 12/05/16 Pct Recovery = 57% Analysis Date = 12/05/16 Pct Recovery = 57% Analysis Date = 12/03/16 Pct Recovery = 57% Analysis Date = 12/03/16 Pct Recovery = 57% Analysis Date = 12/01/16 Pct Recovery = 57% Analysis Date = 12/01/16 Pct Recovery = 57% Analysis Date = 11/29/16 Pct Recovery = 57% Analysis Date = 11/29/16 Pct Recovery = 57% Analysis Date = 11/26/16 Pct Recovery = 57% Analysis Date = 11/26/16 Pct Recovery = 57% Analysis Date = 11/24/16 Pct Recovery = 57% Analysis Date = 11/24/16 Pct Recovery = 57% Analysis Date = 11/22/16 Pct Recovery = 57% Analysis Date = 11/22/16 Pct Recovery = 57% Analysis Date = 11/20/16 Pct Recovery = 57% Analysis Date = 11/20/16 Pct Recovery = 57% Analysis Date = 11/17/16 Pct Recovery = 57% Analysis Date = 11/17/16 Pct Recovery = 57% Analysis Date = 11/15/16 Pct Recovery = 57% Analysis Date = 11/15/16 Pct Recovery = 57% Analysis Date = 11/13/16 Pct Recovery = 57% Analysis Date = 11/13/16 Pct Recovery = 57% Analysis Date = 11/11/16 Pct Recovery = 57% Analysis Date = 11/11/16 Pct Recovery = 57% Analysis Date = 11/08/16 Pct Recovery = 57% Analysis Date = 11/08/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/04/16 Pct Recovery = 57% Analysis Date = 11/04/16 Pct Recovery = 57% Analysis Date = 11/02/16 Pct Recovery = 57% Analysis Date = 11/02/16 Pct Recovery = 57% Analysis Date = 10/30/16 Pct Recovery = 57% Analysis Date = 10/30/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/26/16 Pct Recovery = 57% Analysis Date = 10/26/16 Pct Recovery = 57% Analysis Date = 10/24/16 Pct Recovery = 57% Analysis Date = 10/24/16 Pct Recovery = 57% Analysis Date = 10/21/16 Pct Recovery = 57% Analysis Date = 10/21/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 57% Analysis Date = 10/10/16 Pct Recovery = 57% Analysis Date = 10/10/16 Pct Recovery = 57% Analysis Date = 10/08/16 Pct Recovery = 57% Analysis Date = 10/08/16 Pct Recovery = 57% Analysis Date = 10/06/16 Pct Recovery = 57% Analysis Date = 10/06/16 Pct Recovery = 57% Analysis Date = 10/03/16 Pct Recovery = 57% Analysis Date = 10/03/16 Pct Recovery = 57% Analysis Date = 10/01/16 Pct Recovery = 57% Analysis Date = 10/01/16 Pct Recovery = 57% Analysis Date = 09/29/16 Pct Recovery = 57% Analysis Date = 09/29/16 Pct Recovery = 57% Analysis Date = 09/27/16 Pct Recovery = 57% Analysis Date = 09/27/16 Pct Recovery = 57% Analysis Date = 09/24/16 Pct Recovery = 57% Analysis Date = 09/24/16 Pct Recovery = 57% Analysis Date = 09/22/16 Pct Recovery = 57% Analysis Date = 09/22/16 Pct Recovery = 57% Analysis Date = 09/20/16 Pct Recovery = 57% Analysis Date = 09/20/16 Pct Recovery = 57% Analysis Date = 09/18/16 Pct Recovery = 57% Analysis Date = 09/18/16 Pct Recovery = 57% Analysis Date = 09/16/16 Pct Recovery = 57% Analysis Date = 09/16/16 Pct Recovery = 57% Analysis Date = 09/13/16 Pct Recovery = 57% Analysis Date = 09/13/16 Pct Recovery = 57% Analysis Date = 09/11/16 Pct Recovery = 57% Analysis Date = 09/11/16 Pct Recovery = 57% Analysis Date = 09/09/16 Pct Recovery = 57% Analysis Date = 09/09/16 Pct Recovery = 57% Analysis Date = 09/07/16 Pct Recovery = 57% Analysis Date = 09/07/16 Pct Recovery = 57% Analysis Date = 09/04/16 Pct Recovery = 57% Analysis Date = 09/04/16 Pct Recovery = 57% Analysis Date = 09/02/16 Pct Recovery = 57% Analysis Date = 09/02/16 Pct Recovery = 57% Analysis Date = 08/31/16 Pct Recovery = 57% Analysis Date = 08/31/16 Pct Recovery = 57% Analysis Date = 08/29/16 Pct Recovery = 57% Analysis Date = 08/29/16 Pct Recovery = 57% Analysis Date = 08/26/16 Pct Recovery = 57% Analysis Date = 08/26/16 Pct Recovery = 57% Analysis Date = 08/24/16 Pct Recovery = 57% Analysis Date = 08/24/16 Pct Recovery = 57% Analysis Date = 08/22/16 Pct Recovery = 57% Analysis Date = 08/22/16 Pct Recovery = 57% Analysis Date = 08/20/16 Pct Recovery = 57% Analysis Date = 08/20/16 Pct Recovery = 57% Analysis Date = 08/17/16 Pct Recovery = 57% Analysis Date = 08/17/16 Pct Recovery = 57% Analysis Date = 08/15/16 Pct Recovery = 57% Analysis Date = 08/15/16 Pct Recovery = 57% Analysis Date = 08/13/16 Pct Recovery = 56% Analysis Date = 08/13/16 Pct Recovery = 56% Analysis Date = 08/11/16 Pct Recovery = 56% Analysis Date = 08/11/16 Pct Recovery = 56% Analysis Date = 08/08/16 Pct Recovery = 56% Analysis Date = 08/08/16 Pct Recovery = 56% Analysis Date = 08/06/16 Pct Recovery = 56% Analysis Date = 08/06/16 Pct Recovery = 56% Analysis Date = 08/04/16 Pct Recovery = 56% Analysis Date = 08/04/16 Pct Recovery = 56% Analysis Date = 08/02/16 Pct Recovery = 56% Analysis Date = 08/02/16 Pct Recovery = 56% Analysis Date = 07/30/16 Pct Recovery = 55% Analysis Date = 07/30/16 Pct Recovery = 55% Analysis Date = 07/28/16 Pct Recovery = 55% Analysis Date = 07/28/16 Pct Recovery = 55% Analysis Date = 07/26/16 Pct Recovery = 55% Analysis Date = 07/26/16 Pct Recovery = 55% Analysis Date = 07/24/16 Pct Recovery = 55% Analysis Date = 07/24/16 Pct Recovery = 55% Analysis Date = 07/21/16 Pct Recovery = 55% Analysis Date = 07/21/16 Pct Recovery = 55% Analysis Date = 07/19/16 Pct Recovery = 55% Analysis Date = 07/19/16 Pct Recovery = 55% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/17/16 Pct Recovery = 54% Analysis Date = 07/15/16 Pct Recovery = 54% Analysis Date = 07/15/16 Pct Recovery = 54% Analysis Date = 07/12/16 Pct Recovery = 54% Analysis Date = 07/12/16 Pct Recovery = 54% Analysis Date = 07/10/16 Pct Recovery = 54% Analysis Date = 07/10/16 Pct Recovery = 54% Analysis Date = 07/08/16 Pct Recovery = 54% Analysis Date = 07/08/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/06/16 Pct Recovery = 54% Analysis Date = 07/03/16 Pct Recovery = 53% Analysis Date = 07/03/16 Pct Recovery = 53% Analysis Date = 07/01/16 Pct Recovery = 53% Analysis Date = 07/01/16 Pct Recovery = 53% Analysis Date = 06/29/16 Pct Recovery = 53% Analysis Date = 06/29/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/27/16 Pct Recovery = 53% Analysis Date = 06/24/16 Pct Recovery = 53% Analysis Date = 06/24/16 Pct Recovery = 53% Analysis Date = 06/22/16 Pct Recovery = 53% Analysis Date = 06/22/16 Pct Recovery = 53% Analysis Date = 06/20/16 Pct Recovery = 52% Analysis Date = 06/20/16 Pct Recovery = 52% Analysis Date = 06/18/16 Pct Recovery = 52% Analysis Date = 06/18/16 Pct Recovery = 52% Analysis Date = 06/15/16 Pct Recovery = 52% Analysis Date = 06/15/16 Pct Recovery = 52% Analysis Date = 06/13/16 Pct Recovery = 52% Analysis Date = 06/13/16 Pct Recovery = 52% Analysis Date = 06/11/16 Pct Recovery = 52% Analysis Date = 06/11/16 Pct Recovery = 52% Analysis Date = 06/09/16 Pct Recovery = 52% Analysis Date = 06/09/16 Pct Recovery = 52% Analysis Date = 06/06/16 Pct Recovery = 51% Analysis Date = 06/06/16 Pct Recovery = 51% Analysis Date = 06/04/16 Pct Recovery = 51% Analysis Date = 06/04/16 Pct Recovery = 51% Analysis Date = 06/02/16 Pct Recovery = 51% Analysis Date = 06/02/16 Pct Recovery = 51% Analysis Date = 05/31/16 Pct Recovery = 51% Analysis Date = 05/31/16 Pct Recovery = 51% Analysis Date = 05/29/16 Pct Recovery = 51% Analysis Date = 05/29/16 Pct Recovery = 51% Analysis Date = 05/26/16 Pct Recovery = 51% Analysis Date = 05/26/16 Pct Recovery = 51% Analysis Date = 05/24/16 Pct Recovery = 51% Analysis Date = 05/24/16 Pct Recovery = 51% Analysis Date = 05/22/16 Pct Recovery = 51% Analysis Date = 05/22/16 Pct Recovery = 51% Analysis Date = 05/20/16 Pct Recovery = 51% Analysis Date = 05/20/16 Pct Recovery = 51% Analysis Date = 05/17/16 Pct Recovery = 51% Analysis Date = 05/17/16 Pct Recovery = 51% Analysis Date = 05/15/16 Pct Recovery = 51% Analysis Date = 05/15/16 Pct Recovery = 51% Analysis Date = 05/13/16 Pct Recovery = 51% Analysis Date = 05/13/16 Pct Recovery = 51% Analysis Date = 05/11/16 Pct Recovery = 51% Analysis Date = 05/11/16 Pct Recovery = 51% Analysis Date = 05/08/16 Pct Recovery = 51% Analysis Date = 05/08/16 Pct Recovery = 51% Analysis Date = 05/06/16 Pct Recovery = 52% Analysis Date = 05/06/16 Pct Recovery = 52% Analysis Date = 05/04/16 Pct Recovery = 52% Analysis Date = 05/04/16 Pct Recovery = 52% Analysis Date = 05/02/16 Pct Recovery = 52% Analysis Date = 05/02/16 Pct Recovery = 52% Analysis Date = 04/29/16 Pct Recovery = 52% Analysis Date = 04/29/16 Pct Recovery = 52% Analysis Date = 04/27/16 Pct Recovery = 52% Analysis Date = 04/27/16 Pct Recovery = 52% Analysis Date = 04/25/16 Pct Recovery = 52% Analysis Date = 04/25/16 Pct Recovery = 52% Analysis Date = 04/23/16 Pct Recovery = 52% Analysis Date = 04/23/16 Pct Recovery = 52% Analysis Date = 04/20/16 Pct Recovery = 52% Analysis Date = 04/20/16 Pct Recovery = 52% Analysis Date = 04/18/16 Pct Recovery = 52% Analysis Date = 04/18/16 Pct Recovery = 52% Analysis Date = 04/16/16 Pct Recovery = 52% Analysis Date = 04/16/16 Pct Recovery = 52% Analysis Date = 04/14/16 Pct Recovery = 52% Analysis Date = 04/14/16 Pct Recovery = 52% Analysis Date = 04/11/16 Pct Recovery = 52% Analysis Date = 04/11/16 Pct Recovery = 52% Analysis Date = 04/09/16 Pct Recovery = 52% Analysis Date = 04/09/16 Pct Recovery = 52% Analysis Date = 04/07/16 Pct Recovery = 52% Analysis Date = 04/07/16 Pct Recovery = 52% Analysis Date = 04/05/16 Pct Recovery = 52% Analysis Date = 04/05/16 Pct Recovery = 52% Analysis Date = 04/02/16 Pct Recovery = 52% Analysis Date = 04/02/16 Pct Recovery = 52% Analysis Date = 03/31/16 Pct Recovery = 52% Analysis Date = 03/31/16 Pct Recovery = 52% Analysis Date = 03/29/16 Pct Recovery = 52% Analysis Date = 03/29/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/27/16 Pct Recovery = 52% Analysis Date = 03/24/16 Pct Recovery = 52% Analysis Date = 03/24/16 Pct Recovery = 52% Analysis Date = 03/22/16 Pct Recovery = 52% Analysis Date = 03/22/16 Pct Recovery = 52% Analysis Date = 03/20/16 Pct Recovery = 52% Analysis Date = 03/20/16 Pct Recovery = 52% Analysis Date = 03/18/16 Pct Recovery = 52% Analysis Date = 03/18/16 Pct Recovery = 52% Analysis Date = 03/15/16 Pct Recovery = 52% Analysis Date = 03/15/16 Pct Recovery = 52% Analysis Date = 03/13/16 Pct Recovery = 52% Analysis Date = 03/13/16 Pct Recovery = 52% Analysis Date = 03/11/16 Pct Recovery = 52% Analysis Date = 03/11/16 Pct Recovery = 52% Analysis Date = 03/09/16 Pct Recovery = 52% Analysis Date = 03/09/16 Pct Recovery = 52% Analysis Date = 03/06/16 Pct Recovery = 52% Analysis Date = 03/06/16 Pct Recovery = 52% Analysis Date = 03/04/16 Pct Recovery = 52% Analysis Date = 03/04/16 Pct Recovery = 52% Analysis Date = 03/02/16 Pct Recovery = 52% Analysis Date = 03/02/16 Pct Recovery = 52% Analysis Date = 02/29/16 Pct Recovery = 52% Analysis Date = 02/29/16 Pct Recovery = 52% Analysis Date = 02/26/16 Pct Recovery = 52% Analysis Date = 02/26/16 Pct Recovery = 52% Analysis Date = 02/24/16 Pct Recovery = 52% Analysis Date = 02/24/16 Pct Recovery = 52% Analysis Date = 02/22/16 Pct Recovery = 51% Analysis Date = 02/22/16 Pct Recovery = 51% Analysis Date = 02/20/16 Pct Recovery = 51% Analysis Date = 02/20/16 Pct Recovery = 51% Analysis Date = 02/17/16 Pct Recovery = 51% Analysis Date = 02/17/16 Pct Recovery = 51% Analysis Date = 02/15/16 Pct Recovery = 51% Analysis Date = 02/15/16 Pct Recovery = 51% Analysis Date = 02/13/16 Pct Recovery = 51% Analysis Date = 02/13/16 Pct Recovery = 51% Analysis Date = 02/11/16 Pct Recovery = 51% Analysis Date = 02/11/16 Pct Recovery = 51% Analysis Date = 02/09/16 Pct Recovery = 51% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET (IMIDAN)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 55% 6% 55% 5%
Total 18 55% 6% 55% 5%

Sample Statistics
PHOSMET (IMIDAN)

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 2 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 18
Not Spiked 9 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
PHOSMET OXON
METHOD: 2033 , TESTIDCODE: 61668GCM39

Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 61% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 81% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 73% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 76% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 57% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 76% Analysis Date = 05/10/17 Pct Recovery = 66% Analysis Date = 05/09/17 Pct Recovery = 66% Analysis Date = 05/09/17 Pct Recovery = 66% Analysis Date = 05/07/17 Pct Recovery = 66% Analysis Date = 05/07/17 Pct Recovery = 66% Analysis Date = 05/05/17 Pct Recovery = 66% Analysis Date = 05/05/17 Pct Recovery = 66% Analysis Date = 05/03/17 Pct Recovery = 67% Analysis Date = 05/03/17 Pct Recovery = 67% Analysis Date = 05/01/17 Pct Recovery = 67% Analysis Date = 05/01/17 Pct Recovery = 67% Analysis Date = 04/29/17 Pct Recovery = 67% Analysis Date = 04/29/17 Pct Recovery = 67% Analysis Date = 04/27/17 Pct Recovery = 67% Analysis Date = 04/27/17 Pct Recovery = 67% Analysis Date = 04/25/17 Pct Recovery = 67% Analysis Date = 04/25/17 Pct Recovery = 67% Analysis Date = 04/23/17 Pct Recovery = 68% Analysis Date = 04/23/17 Pct Recovery = 68% Analysis Date = 04/21/17 Pct Recovery = 68% Analysis Date = 04/21/17 Pct Recovery = 68% Analysis Date = 04/19/17 Pct Recovery = 68% Analysis Date = 04/19/17 Pct Recovery = 68% Analysis Date = 04/17/17 Pct Recovery = 68% Analysis Date = 04/17/17 Pct Recovery = 68% Analysis Date = 04/15/17 Pct Recovery = 68% Analysis Date = 04/15/17 Pct Recovery = 68% Analysis Date = 04/13/17 Pct Recovery = 69% Analysis Date = 04/13/17 Pct Recovery = 69% Analysis Date = 04/11/17 Pct Recovery = 69% Analysis Date = 04/11/17 Pct Recovery = 69% Analysis Date = 04/09/17 Pct Recovery = 69% Analysis Date = 04/09/17 Pct Recovery = 69% Analysis Date = 04/07/17 Pct Recovery = 69% Analysis Date = 04/07/17 Pct Recovery = 69% Analysis Date = 04/05/17 Pct Recovery = 69% Analysis Date = 04/05/17 Pct Recovery = 69% Analysis Date = 04/03/17 Pct Recovery = 70% Analysis Date = 04/03/17 Pct Recovery = 70% Analysis Date = 04/01/17 Pct Recovery = 70% Analysis Date = 04/01/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/30/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/28/17 Pct Recovery = 70% Analysis Date = 03/26/17 Pct Recovery = 70% Analysis Date = 03/26/17 Pct Recovery = 70% Analysis Date = 03/24/17 Pct Recovery = 71% Analysis Date = 03/24/17 Pct Recovery = 71% Analysis Date = 03/22/17 Pct Recovery = 71% Analysis Date = 03/22/17 Pct Recovery = 71% Analysis Date = 03/20/17 Pct Recovery = 71% Analysis Date = 03/20/17 Pct Recovery = 71% Analysis Date = 03/18/17 Pct Recovery = 71% Analysis Date = 03/18/17 Pct Recovery = 71% Analysis Date = 03/16/17 Pct Recovery = 71% Analysis Date = 03/16/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 72% Analysis Date = 03/14/17 Pct Recovery = 72% Analysis Date = 03/12/17 Pct Recovery = 72% Analysis Date = 03/12/17 Pct Recovery = 72% Analysis Date = 03/10/17 Pct Recovery = 72% Analysis Date = 03/10/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/08/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/06/17 Pct Recovery = 72% Analysis Date = 03/04/17 Pct Recovery = 73% Analysis Date = 03/04/17 Pct Recovery = 73% Analysis Date = 03/02/17 Pct Recovery = 73% Analysis Date = 03/02/17 Pct Recovery = 73% Analysis Date = 02/28/17 Pct Recovery = 73% Analysis Date = 02/28/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/26/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/24/17 Pct Recovery = 73% Analysis Date = 02/22/17 Pct Recovery = 74% Analysis Date = 02/22/17 Pct Recovery = 74% Analysis Date = 02/20/17 Pct Recovery = 74% Analysis Date = 02/20/17 Pct Recovery = 74% Analysis Date = 02/18/17 Pct Recovery = 74% Analysis Date = 02/18/17 Pct Recovery = 74% Analysis Date = 02/16/17 Pct Recovery = 74% Analysis Date = 02/16/17 Pct Recovery = 74% Analysis Date = 02/14/17 Pct Recovery = 74% Analysis Date = 02/14/17 Pct Recovery = 74% Analysis Date = 02/12/17 Pct Recovery = 75% Analysis Date = 02/12/17 Pct Recovery = 75% Analysis Date = 02/10/17 Pct Recovery = 75% Analysis Date = 02/10/17 Pct Recovery = 75% Analysis Date = 02/08/17 Pct Recovery = 75% Analysis Date = 02/08/17 Pct Recovery = 75% Analysis Date = 02/06/17 Pct Recovery = 75% Analysis Date = 02/06/17 Pct Recovery = 75% Analysis Date = 02/04/17 Pct Recovery = 75% Analysis Date = 02/04/17 Pct Recovery = 75% Analysis Date = 02/02/17 Pct Recovery = 76% Analysis Date = 02/02/17 Pct Recovery = 76% Analysis Date = 01/31/17 Pct Recovery = 76% Analysis Date = 01/31/17 Pct Recovery = 76% Analysis Date = 01/29/17 Pct Recovery = 76% Analysis Date = 01/29/17 Pct Recovery = 76% Analysis Date = 01/27/17 Pct Recovery = 76% Analysis Date = 01/27/17 Pct Recovery = 76% Analysis Date = 01/25/17 Pct Recovery = 76% Analysis Date = 01/25/17 Pct Recovery = 76% Analysis Date = 01/23/17 Pct Recovery = 77% Analysis Date = 01/23/17 Pct Recovery = 77% Analysis Date = 01/21/17 Pct Recovery = 77% Analysis Date = 01/21/17 Pct Recovery = 77% Analysis Date = 01/19/17 Pct Recovery = 77% Analysis Date = 01/19/17 Pct Recovery = 77% Analysis Date = 01/17/17 Pct Recovery = 77% Analysis Date = 01/17/17 Pct Recovery = 77% Analysis Date = 01/15/17 Pct Recovery = 77% Analysis Date = 01/15/17 Pct Recovery = 77% Analysis Date = 01/13/17 Pct Recovery = 77% Analysis Date = 01/13/17 Pct Recovery = 77% Analysis Date = 01/11/17 Pct Recovery = 77% Analysis Date = 01/11/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 77% Analysis Date = 01/09/17 Pct Recovery = 77% Analysis Date = 01/07/17 Pct Recovery = 76% Analysis Date = 01/07/17 Pct Recovery = 76% Analysis Date = 01/05/17 Pct Recovery = 76% Analysis Date = 01/05/17 Pct Recovery = 76% Analysis Date = 01/03/17 Pct Recovery = 76% Analysis Date = 01/03/17 Pct Recovery = 76% Analysis Date = 01/01/17 Pct Recovery = 76% Analysis Date = 01/01/17 Pct Recovery = 76% Analysis Date = 12/30/16 Pct Recovery = 76% Analysis Date = 12/30/16 Pct Recovery = 76% Analysis Date = 12/28/16 Pct Recovery = 76% Analysis Date = 12/28/16 Pct Recovery = 76% Analysis Date = 12/26/16 Pct Recovery = 76% Analysis Date = 12/26/16 Pct Recovery = 76% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/22/16 Pct Recovery = 75% Analysis Date = 12/22/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 75% Analysis Date = 12/18/16 Pct Recovery = 75% Analysis Date = 12/18/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/12/16 Pct Recovery = 75% Analysis Date = 12/12/16 Pct Recovery = 75% Analysis Date = 12/10/16 Pct Recovery = 75% Analysis Date = 12/10/16 Pct Recovery = 75% Analysis Date = 12/08/16 Pct Recovery = 74% Analysis Date = 12/08/16 Pct Recovery = 74% Analysis Date = 12/06/16 Pct Recovery = 74% Analysis Date = 12/06/16 Pct Recovery = 74% Analysis Date = 12/04/16 Pct Recovery = 74% Analysis Date = 12/04/16 Pct Recovery = 74% Analysis Date = 12/02/16 Pct Recovery = 74% Analysis Date = 12/02/16 Pct Recovery = 74% Analysis Date = 11/30/16 Pct Recovery = 74% Analysis Date = 11/30/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/28/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 74% Analysis Date = 11/26/16 Pct Recovery = 74% Analysis Date = 11/24/16 Pct Recovery = 74% Analysis Date = 11/24/16 Pct Recovery = 74% Analysis Date = 11/22/16 Pct Recovery = 73% Analysis Date = 11/22/16 Pct Recovery = 73% Analysis Date = 11/20/16 Pct Recovery = 73% Analysis Date = 11/20/16 Pct Recovery = 73% Analysis Date = 11/18/16 Pct Recovery = 73% Analysis Date = 11/18/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/16/16 Pct Recovery = 73% Analysis Date = 11/14/16 Pct Recovery = 73% Analysis Date = 11/14/16 Pct Recovery = 73% Analysis Date = 11/12/16 Pct Recovery = 73% Analysis Date = 11/12/16 Pct Recovery = 73% Analysis Date = 11/10/16 Pct Recovery = 73% Analysis Date = 11/10/16 Pct Recovery = 73% Analysis Date = 11/08/16 Pct Recovery = 73% Analysis Date = 11/08/16 Pct Recovery = 73% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/06/16 Pct Recovery = 72% Analysis Date = 11/04/16 Pct Recovery = 72% Analysis Date = 11/04/16 Pct Recovery = 72% Analysis Date = 11/02/16 Pct Recovery = 72% Analysis Date = 11/02/16 Pct Recovery = 72% Analysis Date = 10/31/16 Pct Recovery = 72% Analysis Date = 10/31/16 Pct Recovery = 72% Analysis Date = 10/29/16 Pct Recovery = 72% Analysis Date = 10/29/16 Pct Recovery = 72% Analysis Date = 10/27/16 Pct Recovery = 72% Analysis Date = 10/27/16 Pct Recovery = 72% Analysis Date = 10/25/16 Pct Recovery = 72% Analysis Date = 10/25/16 Pct Recovery = 72% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/23/16 Pct Recovery = 71% Analysis Date = 10/21/16 Pct Recovery = 71% Analysis Date = 10/21/16 Pct Recovery = 71% Analysis Date = 10/19/16 Pct Recovery = 71% Analysis Date = 10/19/16 Pct Recovery = 71% Analysis Date = 10/17/16 Pct Recovery = 71% Analysis Date = 10/17/16 Pct Recovery = 71% Analysis Date = 10/15/16 Pct Recovery = 71% Analysis Date = 10/15/16 Pct Recovery = 71% Analysis Date = 10/13/16 Pct Recovery = 71% Analysis Date = 10/13/16 Pct Recovery = 71% Analysis Date = 10/11/16 Pct Recovery = 71% Analysis Date = 10/11/16 Pct Recovery = 71% Analysis Date = 10/09/16 Pct Recovery = 71% Analysis Date = 10/09/16 Pct Recovery = 71% Analysis Date = 10/07/16 Pct Recovery = 70% Analysis Date = 10/07/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/05/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/03/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 10/01/16 Pct Recovery = 70% Analysis Date = 09/29/16 Pct Recovery = 70% Analysis Date = 09/29/16 Pct Recovery = 70% Analysis Date = 09/27/16 Pct Recovery = 70% Analysis Date = 09/27/16 Pct Recovery = 70% Analysis Date = 09/25/16 Pct Recovery = 70% Analysis Date = 09/25/16 Pct Recovery = 70% Analysis Date = 09/23/16 Pct Recovery = 70% Analysis Date = 09/23/16 Pct Recovery = 70% Analysis Date = 09/21/16 Pct Recovery = 69% Analysis Date = 09/21/16 Pct Recovery = 69% Analysis Date = 09/19/16 Pct Recovery = 69% Analysis Date = 09/19/16 Pct Recovery = 69% Analysis Date = 09/17/16 Pct Recovery = 69% Analysis Date = 09/17/16 Pct Recovery = 69% Analysis Date = 09/15/16 Pct Recovery = 69% Analysis Date = 09/15/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/13/16 Pct Recovery = 69% Analysis Date = 09/11/16 Pct Recovery = 69% Analysis Date = 09/11/16 Pct Recovery = 69% Analysis Date = 09/09/16 Pct Recovery = 69% Analysis Date = 09/09/16 Pct Recovery = 69% Analysis Date = 09/07/16 Pct Recovery = 68% Analysis Date = 09/07/16 Pct Recovery = 68% Analysis Date = 09/05/16 Pct Recovery = 68% Analysis Date = 09/05/16 Pct Recovery = 68% Analysis Date = 09/03/16 Pct Recovery = 68% Analysis Date = 09/03/16 Pct Recovery = 68% Analysis Date = 09/01/16 Pct Recovery = 68% Analysis Date = 09/01/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 68% Analysis Date = 08/30/16 Pct Recovery = 68% Analysis Date = 08/28/16 Pct Recovery = 68% Analysis Date = 08/28/16 Pct Recovery = 68% Analysis Date = 08/26/16 Pct Recovery = 68% Analysis Date = 08/26/16 Pct Recovery = 68% Analysis Date = 08/24/16 Pct Recovery = 68% Analysis Date = 08/24/16 Pct Recovery = 68% Analysis Date = 08/22/16 Pct Recovery = 67% Analysis Date = 08/22/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/20/16 Pct Recovery = 67% Analysis Date = 08/18/16 Pct Recovery = 67% Analysis Date = 08/18/16 Pct Recovery = 67% Analysis Date = 08/16/16 Pct Recovery = 67% Analysis Date = 08/16/16 Pct Recovery = 67% Analysis Date = 08/14/16 Pct Recovery = 67% Analysis Date = 08/14/16 Pct Recovery = 67% Analysis Date = 08/12/16 Pct Recovery = 67% Analysis Date = 08/12/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 67% Analysis Date = 08/10/16 Pct Recovery = 67% Analysis Date = 08/08/16 Pct Recovery = 67% Analysis Date = 08/08/16 Pct Recovery = 67% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/06/16 Pct Recovery = 66% Analysis Date = 08/04/16 Pct Recovery = 66% Analysis Date = 08/04/16 Pct Recovery = 66% Analysis Date = 08/02/16 Pct Recovery = 66% Analysis Date = 08/02/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/31/16 Pct Recovery = 66% Analysis Date = 07/29/16 Pct Recovery = 66% Analysis Date = 07/29/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/27/16 Pct Recovery = 66% Analysis Date = 07/25/16 Pct Recovery = 66% Analysis Date = 07/25/16 Pct Recovery = 66% Analysis Date = 07/23/16 Pct Recovery = 66% Analysis Date = 07/23/16 Pct Recovery = 66% Analysis Date = 07/21/16 Pct Recovery = 65% Analysis Date = 07/21/16 Pct Recovery = 65% Analysis Date = 07/19/16 Pct Recovery = 65% Analysis Date = 07/19/16 Pct Recovery = 65% Analysis Date = 07/17/16 Pct Recovery = 65% Analysis Date = 07/17/16 Pct Recovery = 65% Analysis Date = 07/15/16 Pct Recovery = 65% Analysis Date = 07/15/16 Pct Recovery = 65% Analysis Date = 07/13/16 Pct Recovery = 65% Analysis Date = 07/13/16 Pct Recovery = 65% Analysis Date = 07/11/16 Pct Recovery = 65% Analysis Date = 07/11/16 Pct Recovery = 65% Analysis Date = 07/09/16 Pct Recovery = 65% Analysis Date = 07/09/16 Pct Recovery = 65% Analysis Date = 07/07/16 Pct Recovery = 64% Analysis Date = 07/07/16 Pct Recovery = 64% Analysis Date = 07/05/16 Pct Recovery = 64% Analysis Date = 07/05/16 Pct Recovery = 64% Analysis Date = 07/03/16 Pct Recovery = 64% Analysis Date = 07/03/16 Pct Recovery = 64% Analysis Date = 07/01/16 Pct Recovery = 64% Analysis Date = 07/01/16 Pct Recovery = 64% Analysis Date = 06/29/16 Pct Recovery = 64% Analysis Date = 06/29/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/25/16 Pct Recovery = 64% Analysis Date = 06/25/16 Pct Recovery = 64% Analysis Date = 06/23/16 Pct Recovery = 64% Analysis Date = 06/23/16 Pct Recovery = 64% Analysis Date = 06/21/16 Pct Recovery = 63% Analysis Date = 06/21/16 Pct Recovery = 63% Analysis Date = 06/19/16 Pct Recovery = 63% Analysis Date = 06/19/16 Pct Recovery = 63% Analysis Date = 06/17/16 Pct Recovery = 63% Analysis Date = 06/17/16 Pct Recovery = 63% Analysis Date = 06/15/16 Pct Recovery = 63% Analysis Date = 06/15/16 Pct Recovery = 63% Analysis Date = 06/13/16 Pct Recovery = 63% Analysis Date = 06/13/16 Pct Recovery = 63% Analysis Date = 06/11/16 Pct Recovery = 63% Analysis Date = 06/11/16 Pct Recovery = 63% Analysis Date = 06/09/16 Pct Recovery = 63% Analysis Date = 06/09/16 Pct Recovery = 63% Analysis Date = 06/07/16 Pct Recovery = 63% Analysis Date = 06/07/16 Pct Recovery = 63% Analysis Date = 06/05/16 Pct Recovery = 62% Analysis Date = 06/05/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 06/01/16 Pct Recovery = 62% Analysis Date = 06/01/16 Pct Recovery = 62% Analysis Date = 05/30/16 Pct Recovery = 62% Analysis Date = 05/30/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/28/16 Pct Recovery = 62% Analysis Date = 05/26/16 Pct Recovery = 62% Analysis Date = 05/26/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 62% Analysis Date = 05/24/16 Pct Recovery = 62% Analysis Date = 05/22/16 Pct Recovery = 63% Analysis Date = 05/22/16 Pct Recovery = 63% Analysis Date = 05/20/16 Pct Recovery = 63% Analysis Date = 05/20/16 Pct Recovery = 63% Analysis Date = 05/18/16 Pct Recovery = 64% Analysis Date = 05/18/16 Pct Recovery = 64% Analysis Date = 05/16/16 Pct Recovery = 65% Analysis Date = 05/16/16 Pct Recovery = 65% Analysis Date = 05/14/16 Pct Recovery = 66% Analysis Date = 05/14/16 Pct Recovery = 66% Analysis Date = 05/12/16 Pct Recovery = 67% Analysis Date = 05/12/16 Pct Recovery = 67% Analysis Date = 05/10/16 Pct Recovery = 68% Analysis Date = 05/10/16 Pct Recovery = 68% Analysis Date = 05/08/16 Pct Recovery = 68% Analysis Date = 05/08/16 Pct Recovery = 68% Analysis Date = 05/06/16 Pct Recovery = 69% Analysis Date = 05/06/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 70% Analysis Date = 05/04/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 71% Analysis Date = 05/02/16 Pct Recovery = 71% Analysis Date = 04/30/16 Pct Recovery = 72% Analysis Date = 04/30/16 Pct Recovery = 72% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/28/16 Pct Recovery = 73% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/26/16 Pct Recovery = 74% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/24/16 Pct Recovery = 75% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/22/16 Pct Recovery = 76% Analysis Date = 04/20/16 Pct Recovery = 77% Analysis Date = 04/20/16 Pct Recovery = 77% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/18/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/16/16 Pct Recovery = 78% Analysis Date = 04/14/16 Pct Recovery = 79% Analysis Date = 04/14/16 Pct Recovery = 79% Analysis Date = 04/12/16 Pct Recovery = 79% Analysis Date = 04/12/16 Pct Recovery = 79% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/10/16 Pct Recovery = 80% Analysis Date = 04/08/16 Pct Recovery = 80% Analysis Date = 04/08/16 Pct Recovery = 80% Analysis Date = 04/07/16 Pct Recovery = 81% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PHOSMET OXON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 9 71% 9% 73% 10%
Total 9 71% 9% 73% 10%

Sample Statistics
PHOSMET OXON

Characteristic N % % Basis
Plotted 9 100% Spiked
Estimated Values 9 100% Spiked
Deleted Values 7 25% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 12 .  
False Negatives 0 0% 0 out of 9
Not Spiked 16 .  
False Positives 0 0% 0 out of 12

OBSP Determination:
PROMETON
METHOD: 2033 , TESTIDCODE: 04037GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 106% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 91% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 94% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 94% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 50% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 67% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 90% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 119% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 78% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 85% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 87% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 72% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 54% Analysis Date = 05/02/17 Pct Recovery = 97% Analysis Date = 04/30/17 Pct Recovery = 97% Analysis Date = 04/30/17 Pct Recovery = 97% Analysis Date = 04/28/17 Pct Recovery = 96% Analysis Date = 04/28/17 Pct Recovery = 96% Analysis Date = 04/26/17 Pct Recovery = 96% Analysis Date = 04/26/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 96% Analysis Date = 04/24/17 Pct Recovery = 96% Analysis Date = 04/22/17 Pct Recovery = 96% Analysis Date = 04/22/17 Pct Recovery = 96% Analysis Date = 04/20/17 Pct Recovery = 96% Analysis Date = 04/20/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/18/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/15/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/13/17 Pct Recovery = 96% Analysis Date = 04/11/17 Pct Recovery = 96% Analysis Date = 04/11/17 Pct Recovery = 96% Analysis Date = 04/09/17 Pct Recovery = 96% Analysis Date = 04/09/17 Pct Recovery = 96% Analysis Date = 04/07/17 Pct Recovery = 96% Analysis Date = 04/07/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 04/05/17 Pct Recovery = 96% Analysis Date = 04/03/17 Pct Recovery = 96% Analysis Date = 04/03/17 Pct Recovery = 96% Analysis Date = 03/31/17 Pct Recovery = 96% Analysis Date = 03/31/17 Pct Recovery = 96% Analysis Date = 03/29/17 Pct Recovery = 96% Analysis Date = 03/29/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/27/17 Pct Recovery = 96% Analysis Date = 03/25/17 Pct Recovery = 96% Analysis Date = 03/25/17 Pct Recovery = 96% Analysis Date = 03/23/17 Pct Recovery = 96% Analysis Date = 03/23/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/17/17 Pct Recovery = 96% Analysis Date = 03/14/17 Pct Recovery = 96% Analysis Date = 03/14/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/12/17 Pct Recovery = 96% Analysis Date = 03/10/17 Pct Recovery = 96% Analysis Date = 03/10/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/08/17 Pct Recovery = 96% Analysis Date = 03/06/17 Pct Recovery = 96% Analysis Date = 03/06/17 Pct Recovery = 96% Analysis Date = 03/04/17 Pct Recovery = 96% Analysis Date = 03/04/17 Pct Recovery = 96% Analysis Date = 03/02/17 Pct Recovery = 96% Analysis Date = 03/02/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 96% Analysis Date = 02/27/17 Pct Recovery = 96% Analysis Date = 02/25/17 Pct Recovery = 96% Analysis Date = 02/25/17 Pct Recovery = 96% Analysis Date = 02/23/17 Pct Recovery = 96% Analysis Date = 02/23/17 Pct Recovery = 96% Analysis Date = 02/21/17 Pct Recovery = 96% Analysis Date = 02/21/17 Pct Recovery = 96% Analysis Date = 02/19/17 Pct Recovery = 96% Analysis Date = 02/19/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/17/17 Pct Recovery = 96% Analysis Date = 02/15/17 Pct Recovery = 96% Analysis Date = 02/15/17 Pct Recovery = 96% Analysis Date = 02/13/17 Pct Recovery = 96% Analysis Date = 02/13/17 Pct Recovery = 96% Analysis Date = 02/10/17 Pct Recovery = 95% Analysis Date = 02/10/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/08/17 Pct Recovery = 95% Analysis Date = 02/06/17 Pct Recovery = 95% Analysis Date = 02/06/17 Pct Recovery = 95% Analysis Date = 02/04/17 Pct Recovery = 95% Analysis Date = 02/04/17 Pct Recovery = 95% Analysis Date = 02/02/17 Pct Recovery = 95% Analysis Date = 02/02/17 Pct Recovery = 95% Analysis Date = 01/31/17 Pct Recovery = 95% Analysis Date = 01/31/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/29/17 Pct Recovery = 95% Analysis Date = 01/26/17 Pct Recovery = 94% Analysis Date = 01/26/17 Pct Recovery = 94% Analysis Date = 01/24/17 Pct Recovery = 94% Analysis Date = 01/24/17 Pct Recovery = 94% Analysis Date = 01/22/17 Pct Recovery = 94% Analysis Date = 01/22/17 Pct Recovery = 94% Analysis Date = 01/20/17 Pct Recovery = 94% Analysis Date = 01/20/17 Pct Recovery = 94% Analysis Date = 01/18/17 Pct Recovery = 94% Analysis Date = 01/18/17 Pct Recovery = 94% Analysis Date = 01/16/17 Pct Recovery = 94% Analysis Date = 01/16/17 Pct Recovery = 94% Analysis Date = 01/14/17 Pct Recovery = 94% Analysis Date = 01/14/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/11/17 Pct Recovery = 94% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 01/01/17 Pct Recovery = 93% Analysis Date = 01/01/17 Pct Recovery = 93% Analysis Date = 12/30/16 Pct Recovery = 93% Analysis Date = 12/30/16 Pct Recovery = 93% Analysis Date = 12/28/16 Pct Recovery = 93% Analysis Date = 12/28/16 Pct Recovery = 93% Analysis Date = 12/25/16 Pct Recovery = 92% Analysis Date = 12/25/16 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/23/16 Pct Recovery = 92% Analysis Date = 12/21/16 Pct Recovery = 92% Analysis Date = 12/21/16 Pct Recovery = 92% Analysis Date = 12/19/16 Pct Recovery = 92% Analysis Date = 12/19/16 Pct Recovery = 92% Analysis Date = 12/17/16 Pct Recovery = 92% Analysis Date = 12/17/16 Pct Recovery = 92% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/10/16 Pct Recovery = 91% Analysis Date = 12/10/16 Pct Recovery = 91% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 12/02/16 Pct Recovery = 89% Analysis Date = 11/30/16 Pct Recovery = 89% Analysis Date = 11/30/16 Pct Recovery = 89% Analysis Date = 11/28/16 Pct Recovery = 89% Analysis Date = 11/28/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/26/16 Pct Recovery = 89% Analysis Date = 11/23/16 Pct Recovery = 88% Analysis Date = 11/23/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/21/16 Pct Recovery = 88% Analysis Date = 11/19/16 Pct Recovery = 88% Analysis Date = 11/19/16 Pct Recovery = 88% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/17/16 Pct Recovery = 87% Analysis Date = 11/15/16 Pct Recovery = 87% Analysis Date = 11/15/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/13/16 Pct Recovery = 87% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/08/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 85% Analysis Date = 11/04/16 Pct Recovery = 85% Analysis Date = 11/02/16 Pct Recovery = 85% Analysis Date = 11/02/16 Pct Recovery = 85% Analysis Date = 10/31/16 Pct Recovery = 85% Analysis Date = 10/31/16 Pct Recovery = 85% Analysis Date = 10/29/16 Pct Recovery = 84% Analysis Date = 10/29/16 Pct Recovery = 84% Analysis Date = 10/27/16 Pct Recovery = 84% Analysis Date = 10/27/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/22/16 Pct Recovery = 83% Analysis Date = 10/22/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/20/16 Pct Recovery = 83% Analysis Date = 10/18/16 Pct Recovery = 83% Analysis Date = 10/18/16 Pct Recovery = 83% Analysis Date = 10/16/16 Pct Recovery = 82% Analysis Date = 10/16/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/14/16 Pct Recovery = 82% Analysis Date = 10/12/16 Pct Recovery = 82% Analysis Date = 10/12/16 Pct Recovery = 82% Analysis Date = 10/10/16 Pct Recovery = 82% Analysis Date = 10/10/16 Pct Recovery = 82% Analysis Date = 10/07/16 Pct Recovery = 81% Analysis Date = 10/07/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 10/05/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 81% Analysis Date = 10/03/16 Pct Recovery = 81% Analysis Date = 10/01/16 Pct Recovery = 80% Analysis Date = 10/01/16 Pct Recovery = 80% Analysis Date = 09/29/16 Pct Recovery = 80% Analysis Date = 09/29/16 Pct Recovery = 80% Analysis Date = 09/27/16 Pct Recovery = 80% Analysis Date = 09/27/16 Pct Recovery = 80% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/25/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/16/16 Pct Recovery = 78% Analysis Date = 09/16/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 78% Analysis Date = 09/14/16 Pct Recovery = 78% Analysis Date = 09/12/16 Pct Recovery = 77% Analysis Date = 09/12/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 77% Analysis Date = 09/10/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 09/08/16 Pct Recovery = 77% Analysis Date = 09/05/16 Pct Recovery = 76% Analysis Date = 09/05/16 Pct Recovery = 76% Analysis Date = 09/03/16 Pct Recovery = 76% Analysis Date = 09/03/16 Pct Recovery = 76% Analysis Date = 09/01/16 Pct Recovery = 76% Analysis Date = 09/01/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/30/16 Pct Recovery = 76% Analysis Date = 08/28/16 Pct Recovery = 76% Analysis Date = 08/28/16 Pct Recovery = 76% Analysis Date = 08/26/16 Pct Recovery = 75% Analysis Date = 08/26/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/24/16 Pct Recovery = 75% Analysis Date = 08/21/16 Pct Recovery = 75% Analysis Date = 08/21/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/19/16 Pct Recovery = 75% Analysis Date = 08/17/16 Pct Recovery = 75% Analysis Date = 08/17/16 Pct Recovery = 75% Analysis Date = 08/15/16 Pct Recovery = 75% Analysis Date = 08/15/16 Pct Recovery = 75% Analysis Date = 08/13/16 Pct Recovery = 75% Analysis Date = 08/13/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/11/16 Pct Recovery = 75% Analysis Date = 08/09/16 Pct Recovery = 75% Analysis Date = 08/09/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/06/16 Pct Recovery = 75% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 08/04/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 08/02/16 Pct Recovery = 74% Analysis Date = 07/31/16 Pct Recovery = 74% Analysis Date = 07/31/16 Pct Recovery = 74% Analysis Date = 07/29/16 Pct Recovery = 74% Analysis Date = 07/29/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/27/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/25/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/23/16 Pct Recovery = 74% Analysis Date = 07/20/16 Pct Recovery = 74% Analysis Date = 07/20/16 Pct Recovery = 74% Analysis Date = 07/18/16 Pct Recovery = 74% Analysis Date = 07/18/16 Pct Recovery = 74% Analysis Date = 07/16/16 Pct Recovery = 74% Analysis Date = 07/16/16 Pct Recovery = 74% Analysis Date = 07/14/16 Pct Recovery = 73% Analysis Date = 07/14/16 Pct Recovery = 73% Analysis Date = 07/12/16 Pct Recovery = 73% Analysis Date = 07/12/16 Pct Recovery = 73% Analysis Date = 07/10/16 Pct Recovery = 73% Analysis Date = 07/10/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/08/16 Pct Recovery = 73% Analysis Date = 07/05/16 Pct Recovery = 73% Analysis Date = 07/05/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/03/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 07/01/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/23/16 Pct Recovery = 72% Analysis Date = 06/23/16 Pct Recovery = 72% Analysis Date = 06/21/16 Pct Recovery = 72% Analysis Date = 06/21/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/16/16 Pct Recovery = 72% Analysis Date = 06/16/16 Pct Recovery = 72% Analysis Date = 06/14/16 Pct Recovery = 72% Analysis Date = 06/14/16 Pct Recovery = 72% Analysis Date = 06/12/16 Pct Recovery = 72% Analysis Date = 06/12/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/10/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/08/16 Pct Recovery = 72% Analysis Date = 06/06/16 Pct Recovery = 72% Analysis Date = 06/06/16 Pct Recovery = 72% Analysis Date = 06/03/16 Pct Recovery = 71% Analysis Date = 06/03/16 Pct Recovery = 71% Analysis Date = 06/01/16 Pct Recovery = 71% Analysis Date = 06/01/16 Pct Recovery = 71% Analysis Date = 05/30/16 Pct Recovery = 71% Analysis Date = 05/30/16 Pct Recovery = 71% Analysis Date = 05/28/16 Pct Recovery = 71% Analysis Date = 05/28/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 71% Analysis Date = 05/26/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/24/16 Pct Recovery = 71% Analysis Date = 05/22/16 Pct Recovery = 71% Analysis Date = 05/22/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/19/16 Pct Recovery = 71% Analysis Date = 05/17/16 Pct Recovery = 71% Analysis Date = 05/17/16 Pct Recovery = 71% Analysis Date = 05/15/16 Pct Recovery = 71% Analysis Date = 05/15/16 Pct Recovery = 71% Analysis Date = 05/13/16 Pct Recovery = 71% Analysis Date = 05/13/16 Pct Recovery = 71% Analysis Date = 05/11/16 Pct Recovery = 71% Analysis Date = 05/11/16 Pct Recovery = 71% Analysis Date = 05/09/16 Pct Recovery = 70% Analysis Date = 05/09/16 Pct Recovery = 70% Analysis Date = 05/07/16 Pct Recovery = 70% Analysis Date = 05/07/16 Pct Recovery = 70% Analysis Date = 05/05/16 Pct Recovery = 70% Analysis Date = 05/05/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 04/30/16 Pct Recovery = 70% Analysis Date = 04/30/16 Pct Recovery = 70% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/28/16 Pct Recovery = 69% Analysis Date = 04/26/16 Pct Recovery = 69% Analysis Date = 04/26/16 Pct Recovery = 69% Analysis Date = 04/24/16 Pct Recovery = 69% Analysis Date = 04/24/16 Pct Recovery = 69% Analysis Date = 04/22/16 Pct Recovery = 69% Analysis Date = 04/22/16 Pct Recovery = 69% Analysis Date = 04/20/16 Pct Recovery = 68% Analysis Date = 04/20/16 Pct Recovery = 68% Analysis Date = 04/17/16 Pct Recovery = 68% Analysis Date = 04/17/16 Pct Recovery = 68% Analysis Date = 04/15/16 Pct Recovery = 68% Analysis Date = 04/15/16 Pct Recovery = 68% Analysis Date = 04/13/16 Pct Recovery = 68% Analysis Date = 04/13/16 Pct Recovery = 68% Analysis Date = 04/11/16 Pct Recovery = 68% Analysis Date = 04/11/16 Pct Recovery = 68% Analysis Date = 04/09/16 Pct Recovery = 67% Analysis Date = 04/09/16 Pct Recovery = 67% Analysis Date = 04/07/16 Pct Recovery = 67% Analysis Date = 04/07/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/05/16 Pct Recovery = 67% Analysis Date = 04/03/16 Pct Recovery = 66% Analysis Date = 04/03/16 Pct Recovery = 66% Analysis Date = 03/31/16 Pct Recovery = 66% Analysis Date = 03/31/16 Pct Recovery = 66% Analysis Date = 03/29/16 Pct Recovery = 66% Analysis Date = 03/29/16 Pct Recovery = 66% Analysis Date = 03/27/16 Pct Recovery = 65% Analysis Date = 03/27/16 Pct Recovery = 65% Analysis Date = 03/25/16 Pct Recovery = 65% Analysis Date = 03/25/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/23/16 Pct Recovery = 65% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/21/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/19/16 Pct Recovery = 64% Analysis Date = 03/16/16 Pct Recovery = 64% Analysis Date = 03/16/16 Pct Recovery = 64% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/14/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/12/16 Pct Recovery = 63% Analysis Date = 03/10/16 Pct Recovery = 63% Analysis Date = 03/10/16 Pct Recovery = 63% Analysis Date = 03/08/16 Pct Recovery = 62% Analysis Date = 03/08/16 Pct Recovery = 62% Analysis Date = 03/06/16 Pct Recovery = 62% Analysis Date = 03/06/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/04/16 Pct Recovery = 62% Analysis Date = 03/02/16 Pct Recovery = 61% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 82% 18% 86% 19%
Total 18 82% 18% 86% 19%

Sample Statistics
PROMETON

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 2 11% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
PROMETRYN
METHOD: 2033 , TESTIDCODE: 04036GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 85% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 109% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 122% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 89% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 94% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 88% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 70% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 74% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 68% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 99% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 75% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 78% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 90% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 85% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 83% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 88% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 87% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 81% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 89% Analysis Date = 05/10/17 Pct Recovery = 92% Analysis Date = 05/08/17 Pct Recovery = 92% Analysis Date = 05/08/17 Pct Recovery = 92% Analysis Date = 05/06/17 Pct Recovery = 92% Analysis Date = 05/06/17 Pct Recovery = 92% Analysis Date = 05/04/17 Pct Recovery = 92% Analysis Date = 05/04/17 Pct Recovery = 92% Analysis Date = 05/01/17 Pct Recovery = 92% Analysis Date = 05/01/17 Pct Recovery = 92% Analysis Date = 04/29/17 Pct Recovery = 92% Analysis Date = 04/29/17 Pct Recovery = 92% Analysis Date = 04/27/17 Pct Recovery = 92% Analysis Date = 04/27/17 Pct Recovery = 92% Analysis Date = 04/25/17 Pct Recovery = 92% Analysis Date = 04/25/17 Pct Recovery = 92% Analysis Date = 04/22/17 Pct Recovery = 92% Analysis Date = 04/22/17 Pct Recovery = 92% Analysis Date = 04/20/17 Pct Recovery = 92% Analysis Date = 04/20/17 Pct Recovery = 92% Analysis Date = 04/18/17 Pct Recovery = 91% Analysis Date = 04/18/17 Pct Recovery = 91% Analysis Date = 04/15/17 Pct Recovery = 91% Analysis Date = 04/15/17 Pct Recovery = 91% Analysis Date = 04/13/17 Pct Recovery = 91% Analysis Date = 04/13/17 Pct Recovery = 91% Analysis Date = 04/11/17 Pct Recovery = 91% Analysis Date = 04/11/17 Pct Recovery = 91% Analysis Date = 04/09/17 Pct Recovery = 91% Analysis Date = 04/09/17 Pct Recovery = 91% Analysis Date = 04/06/17 Pct Recovery = 91% Analysis Date = 04/06/17 Pct Recovery = 91% Analysis Date = 04/04/17 Pct Recovery = 91% Analysis Date = 04/04/17 Pct Recovery = 91% Analysis Date = 04/02/17 Pct Recovery = 91% Analysis Date = 04/02/17 Pct Recovery = 91% Analysis Date = 03/30/17 Pct Recovery = 91% Analysis Date = 03/30/17 Pct Recovery = 91% Analysis Date = 03/28/17 Pct Recovery = 91% Analysis Date = 03/28/17 Pct Recovery = 91% Analysis Date = 03/26/17 Pct Recovery = 91% Analysis Date = 03/26/17 Pct Recovery = 91% Analysis Date = 03/24/17 Pct Recovery = 90% Analysis Date = 03/24/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/17/17 Pct Recovery = 90% Analysis Date = 03/14/17 Pct Recovery = 90% Analysis Date = 03/14/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/12/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/05/17 Pct Recovery = 89% Analysis Date = 03/03/17 Pct Recovery = 89% Analysis Date = 03/03/17 Pct Recovery = 89% Analysis Date = 03/01/17 Pct Recovery = 89% Analysis Date = 03/01/17 Pct Recovery = 89% Analysis Date = 02/26/17 Pct Recovery = 89% Analysis Date = 02/26/17 Pct Recovery = 89% Analysis Date = 02/24/17 Pct Recovery = 89% Analysis Date = 02/24/17 Pct Recovery = 89% Analysis Date = 02/22/17 Pct Recovery = 89% Analysis Date = 02/22/17 Pct Recovery = 89% Analysis Date = 02/20/17 Pct Recovery = 88% Analysis Date = 02/20/17 Pct Recovery = 88% Analysis Date = 02/17/17 Pct Recovery = 88% Analysis Date = 02/17/17 Pct Recovery = 88% Analysis Date = 02/15/17 Pct Recovery = 88% Analysis Date = 02/15/17 Pct Recovery = 88% Analysis Date = 02/13/17 Pct Recovery = 87% Analysis Date = 02/13/17 Pct Recovery = 87% Analysis Date = 02/10/17 Pct Recovery = 87% Analysis Date = 02/10/17 Pct Recovery = 87% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/04/17 Pct Recovery = 86% Analysis Date = 02/04/17 Pct Recovery = 86% Analysis Date = 02/01/17 Pct Recovery = 85% Analysis Date = 02/01/17 Pct Recovery = 85% Analysis Date = 01/30/17 Pct Recovery = 85% Analysis Date = 01/30/17 Pct Recovery = 85% Analysis Date = 01/28/17 Pct Recovery = 84% Analysis Date = 01/28/17 Pct Recovery = 84% Analysis Date = 01/25/17 Pct Recovery = 84% Analysis Date = 01/25/17 Pct Recovery = 84% Analysis Date = 01/23/17 Pct Recovery = 84% Analysis Date = 01/23/17 Pct Recovery = 84% Analysis Date = 01/21/17 Pct Recovery = 83% Analysis Date = 01/21/17 Pct Recovery = 83% Analysis Date = 01/19/17 Pct Recovery = 83% Analysis Date = 01/19/17 Pct Recovery = 83% Analysis Date = 01/16/17 Pct Recovery = 83% Analysis Date = 01/16/17 Pct Recovery = 83% Analysis Date = 01/14/17 Pct Recovery = 83% Analysis Date = 01/14/17 Pct Recovery = 83% Analysis Date = 01/12/17 Pct Recovery = 83% Analysis Date = 01/12/17 Pct Recovery = 83% Analysis Date = 01/09/17 Pct Recovery = 83% Analysis Date = 01/09/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/07/17 Pct Recovery = 83% Analysis Date = 01/05/17 Pct Recovery = 83% Analysis Date = 01/05/17 Pct Recovery = 83% Analysis Date = 01/03/17 Pct Recovery = 83% Analysis Date = 01/03/17 Pct Recovery = 83% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/22/16 Pct Recovery = 84% Analysis Date = 12/22/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/18/16 Pct Recovery = 84% Analysis Date = 12/18/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 84% Analysis Date = 12/13/16 Pct Recovery = 84% Analysis Date = 12/13/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/08/16 Pct Recovery = 85% Analysis Date = 12/08/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/06/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 12/04/16 Pct Recovery = 85% Analysis Date = 12/02/16 Pct Recovery = 85% Analysis Date = 12/02/16 Pct Recovery = 85% Analysis Date = 11/29/16 Pct Recovery = 85% Analysis Date = 11/29/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/27/16 Pct Recovery = 85% Analysis Date = 11/25/16 Pct Recovery = 85% Analysis Date = 11/25/16 Pct Recovery = 85% Analysis Date = 11/22/16 Pct Recovery = 85% Analysis Date = 11/22/16 Pct Recovery = 85% Analysis Date = 11/20/16 Pct Recovery = 85% Analysis Date = 11/20/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/18/16 Pct Recovery = 85% Analysis Date = 11/16/16 Pct Recovery = 86% Analysis Date = 11/16/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/13/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/11/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/09/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/06/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/04/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 11/02/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/31/16 Pct Recovery = 86% Analysis Date = 10/28/16 Pct Recovery = 86% Analysis Date = 10/28/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/26/16 Pct Recovery = 86% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/24/16 Pct Recovery = 87% Analysis Date = 10/21/16 Pct Recovery = 87% Analysis Date = 10/21/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/19/16 Pct Recovery = 87% Analysis Date = 10/17/16 Pct Recovery = 87% Analysis Date = 10/17/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/15/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/12/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/10/16 Pct Recovery = 87% Analysis Date = 10/08/16 Pct Recovery = 87% Analysis Date = 10/08/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/05/16 Pct Recovery = 87% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 10/03/16 Pct Recovery = 88% Analysis Date = 10/01/16 Pct Recovery = 88% Analysis Date = 10/01/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/29/16 Pct Recovery = 88% Analysis Date = 09/26/16 Pct Recovery = 88% Analysis Date = 09/26/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 88% Analysis Date = 09/24/16 Pct Recovery = 88% Analysis Date = 09/22/16 Pct Recovery = 88% Analysis Date = 09/22/16 Pct Recovery = 88% Analysis Date = 09/19/16 Pct Recovery = 88% Analysis Date = 09/19/16 Pct Recovery = 88% Analysis Date = 09/17/16 Pct Recovery = 88% Analysis Date = 09/17/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/15/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/13/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/10/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 09/08/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/06/16 Pct Recovery = 88% Analysis Date = 09/03/16 Pct Recovery = 88% Analysis Date = 09/03/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 09/01/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/30/16 Pct Recovery = 88% Analysis Date = 08/28/16 Pct Recovery = 88% Analysis Date = 08/28/16 Pct Recovery = 88% Analysis Date = 08/25/16 Pct Recovery = 88% Analysis Date = 08/25/16 Pct Recovery = 88% Analysis Date = 08/23/16 Pct Recovery = 88% Analysis Date = 08/23/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/18/16 Pct Recovery = 88% Analysis Date = 08/18/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 87% Analysis Date = 08/16/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 87% Analysis Date = 08/05/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 08/02/16 Pct Recovery = 87% Analysis Date = 07/31/16 Pct Recovery = 86% Analysis Date = 07/31/16 Pct Recovery = 86% Analysis Date = 07/29/16 Pct Recovery = 86% Analysis Date = 07/29/16 Pct Recovery = 86% Analysis Date = 07/27/16 Pct Recovery = 86% Analysis Date = 07/27/16 Pct Recovery = 86% Analysis Date = 07/24/16 Pct Recovery = 86% Analysis Date = 07/24/16 Pct Recovery = 86% Analysis Date = 07/22/16 Pct Recovery = 86% Analysis Date = 07/22/16 Pct Recovery = 86% Analysis Date = 07/20/16 Pct Recovery = 86% Analysis Date = 07/20/16 Pct Recovery = 86% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/17/16 Pct Recovery = 85% Analysis Date = 07/15/16 Pct Recovery = 85% Analysis Date = 07/15/16 Pct Recovery = 85% Analysis Date = 07/13/16 Pct Recovery = 85% Analysis Date = 07/13/16 Pct Recovery = 85% Analysis Date = 07/11/16 Pct Recovery = 85% Analysis Date = 07/11/16 Pct Recovery = 85% Analysis Date = 07/08/16 Pct Recovery = 85% Analysis Date = 07/08/16 Pct Recovery = 85% Analysis Date = 07/06/16 Pct Recovery = 85% Analysis Date = 07/06/16 Pct Recovery = 85% Analysis Date = 07/04/16 Pct Recovery = 85% Analysis Date = 07/04/16 Pct Recovery = 85% Analysis Date = 07/01/16 Pct Recovery = 84% Analysis Date = 07/01/16 Pct Recovery = 84% Analysis Date = 06/29/16 Pct Recovery = 84% Analysis Date = 06/29/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/27/16 Pct Recovery = 84% Analysis Date = 06/25/16 Pct Recovery = 84% Analysis Date = 06/25/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/20/16 Pct Recovery = 84% Analysis Date = 06/20/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 83% Analysis Date = 06/18/16 Pct Recovery = 83% Analysis Date = 06/15/16 Pct Recovery = 83% Analysis Date = 06/15/16 Pct Recovery = 83% Analysis Date = 06/13/16 Pct Recovery = 83% Analysis Date = 06/13/16 Pct Recovery = 83% Analysis Date = 06/11/16 Pct Recovery = 83% Analysis Date = 06/11/16 Pct Recovery = 83% Analysis Date = 06/09/16 Pct Recovery = 83% Analysis Date = 06/09/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/06/16 Pct Recovery = 83% Analysis Date = 06/04/16 Pct Recovery = 83% Analysis Date = 06/04/16 Pct Recovery = 83% Analysis Date = 06/02/16 Pct Recovery = 82% Analysis Date = 06/02/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/30/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/28/16 Pct Recovery = 82% Analysis Date = 05/26/16 Pct Recovery = 82% Analysis Date = 05/26/16 Pct Recovery = 82% Analysis Date = 05/24/16 Pct Recovery = 82% Analysis Date = 05/24/16 Pct Recovery = 82% Analysis Date = 05/21/16 Pct Recovery = 82% Analysis Date = 05/21/16 Pct Recovery = 82% Analysis Date = 05/19/16 Pct Recovery = 81% Analysis Date = 05/19/16 Pct Recovery = 81% Analysis Date = 05/17/16 Pct Recovery = 81% Analysis Date = 05/17/16 Pct Recovery = 81% Analysis Date = 05/14/16 Pct Recovery = 81% Analysis Date = 05/14/16 Pct Recovery = 81% Analysis Date = 05/12/16 Pct Recovery = 81% Analysis Date = 05/12/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 05/10/16 Pct Recovery = 81% Analysis Date = 05/08/16 Pct Recovery = 81% Analysis Date = 05/08/16 Pct Recovery = 81% Analysis Date = 05/05/16 Pct Recovery = 81% Analysis Date = 05/05/16 Pct Recovery = 81% Analysis Date = 05/03/16 Pct Recovery = 80% Analysis Date = 05/03/16 Pct Recovery = 80% Analysis Date = 05/01/16 Pct Recovery = 81% Analysis Date = 05/01/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/28/16 Pct Recovery = 81% Analysis Date = 04/26/16 Pct Recovery = 81% Analysis Date = 04/26/16 Pct Recovery = 81% Analysis Date = 04/24/16 Pct Recovery = 81% Analysis Date = 04/24/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 81% Analysis Date = 04/22/16 Pct Recovery = 81% Analysis Date = 04/19/16 Pct Recovery = 81% Analysis Date = 04/19/16 Pct Recovery = 81% Analysis Date = 04/17/16 Pct Recovery = 81% Analysis Date = 04/17/16 Pct Recovery = 81% Analysis Date = 04/15/16 Pct Recovery = 81% Analysis Date = 04/15/16 Pct Recovery = 81% Analysis Date = 04/12/16 Pct Recovery = 81% Analysis Date = 04/12/16 Pct Recovery = 81% Analysis Date = 04/10/16 Pct Recovery = 81% Analysis Date = 04/10/16 Pct Recovery = 81% Analysis Date = 04/08/16 Pct Recovery = 82% Analysis Date = 04/08/16 Pct Recovery = 82% Analysis Date = 04/06/16 Pct Recovery = 82% Analysis Date = 04/06/16 Pct Recovery = 82% Analysis Date = 04/03/16 Pct Recovery = 82% Analysis Date = 04/03/16 Pct Recovery = 82% Analysis Date = 04/01/16 Pct Recovery = 82% Analysis Date = 04/01/16 Pct Recovery = 82% Analysis Date = 03/30/16 Pct Recovery = 82% Analysis Date = 03/30/16 Pct Recovery = 82% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 83% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/16/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/14/16 Pct Recovery = 84% Analysis Date = 03/11/16 Pct Recovery = 84% Analysis Date = 03/11/16 Pct Recovery = 84% Analysis Date = 03/09/16 Pct Recovery = 84% Analysis Date = 03/09/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 03/07/16 Pct Recovery = 84% Analysis Date = 03/05/16 Pct Recovery = 84% Analysis Date = 03/05/16 Pct Recovery = 84% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 03/02/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/29/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/27/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/24/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/22/16 Pct Recovery = 85% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/20/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/18/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/15/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/13/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/11/16 Pct Recovery = 86% Analysis Date = 02/09/16 Pct Recovery = 87% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROMETRYN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 87% 13% 87% 9%
Total 19 87% 13% 87% 9%

Sample Statistics
PROMETRYN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
PROPANIL
METHOD: 2033 , TESTIDCODE: 82679GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 103% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 121% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 132% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 97% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 124% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 120% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 77% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 92% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 142% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 98% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 102% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 116% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 91% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 126% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 112% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 103% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 88% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 79% Analysis Date = 05/10/17 Pct Recovery = 121% Analysis Date = 05/08/17 Pct Recovery = 121% Analysis Date = 05/08/17 Pct Recovery = 121% Analysis Date = 05/06/17 Pct Recovery = 120% Analysis Date = 05/06/17 Pct Recovery = 120% Analysis Date = 05/04/17 Pct Recovery = 120% Analysis Date = 05/04/17 Pct Recovery = 120% Analysis Date = 05/01/17 Pct Recovery = 119% Analysis Date = 05/01/17 Pct Recovery = 119% Analysis Date = 04/29/17 Pct Recovery = 119% Analysis Date = 04/29/17 Pct Recovery = 119% Analysis Date = 04/27/17 Pct Recovery = 119% Analysis Date = 04/27/17 Pct Recovery = 119% Analysis Date = 04/25/17 Pct Recovery = 118% Analysis Date = 04/25/17 Pct Recovery = 118% Analysis Date = 04/22/17 Pct Recovery = 118% Analysis Date = 04/22/17 Pct Recovery = 118% Analysis Date = 04/20/17 Pct Recovery = 117% Analysis Date = 04/20/17 Pct Recovery = 117% Analysis Date = 04/18/17 Pct Recovery = 117% Analysis Date = 04/18/17 Pct Recovery = 117% Analysis Date = 04/15/17 Pct Recovery = 117% Analysis Date = 04/15/17 Pct Recovery = 117% Analysis Date = 04/13/17 Pct Recovery = 116% Analysis Date = 04/13/17 Pct Recovery = 116% Analysis Date = 04/11/17 Pct Recovery = 116% Analysis Date = 04/11/17 Pct Recovery = 116% Analysis Date = 04/09/17 Pct Recovery = 115% Analysis Date = 04/09/17 Pct Recovery = 115% Analysis Date = 04/06/17 Pct Recovery = 115% Analysis Date = 04/06/17 Pct Recovery = 115% Analysis Date = 04/04/17 Pct Recovery = 115% Analysis Date = 04/04/17 Pct Recovery = 115% Analysis Date = 04/02/17 Pct Recovery = 114% Analysis Date = 04/02/17 Pct Recovery = 114% Analysis Date = 03/30/17 Pct Recovery = 114% Analysis Date = 03/30/17 Pct Recovery = 114% Analysis Date = 03/28/17 Pct Recovery = 113% Analysis Date = 03/28/17 Pct Recovery = 113% Analysis Date = 03/26/17 Pct Recovery = 113% Analysis Date = 03/26/17 Pct Recovery = 113% Analysis Date = 03/24/17 Pct Recovery = 113% Analysis Date = 03/24/17 Pct Recovery = 113% Analysis Date = 03/21/17 Pct Recovery = 112% Analysis Date = 03/21/17 Pct Recovery = 112% Analysis Date = 03/19/17 Pct Recovery = 112% Analysis Date = 03/19/17 Pct Recovery = 112% Analysis Date = 03/17/17 Pct Recovery = 112% Analysis Date = 03/17/17 Pct Recovery = 112% Analysis Date = 03/14/17 Pct Recovery = 111% Analysis Date = 03/14/17 Pct Recovery = 111% Analysis Date = 03/12/17 Pct Recovery = 111% Analysis Date = 03/12/17 Pct Recovery = 111% Analysis Date = 03/10/17 Pct Recovery = 110% Analysis Date = 03/10/17 Pct Recovery = 110% Analysis Date = 03/08/17 Pct Recovery = 110% Analysis Date = 03/08/17 Pct Recovery = 110% Analysis Date = 03/05/17 Pct Recovery = 110% Analysis Date = 03/05/17 Pct Recovery = 110% Analysis Date = 03/03/17 Pct Recovery = 109% Analysis Date = 03/03/17 Pct Recovery = 109% Analysis Date = 03/01/17 Pct Recovery = 109% Analysis Date = 03/01/17 Pct Recovery = 109% Analysis Date = 02/26/17 Pct Recovery = 108% Analysis Date = 02/26/17 Pct Recovery = 108% Analysis Date = 02/24/17 Pct Recovery = 108% Analysis Date = 02/24/17 Pct Recovery = 108% Analysis Date = 02/22/17 Pct Recovery = 107% Analysis Date = 02/22/17 Pct Recovery = 107% Analysis Date = 02/20/17 Pct Recovery = 107% Analysis Date = 02/20/17 Pct Recovery = 107% Analysis Date = 02/17/17 Pct Recovery = 106% Analysis Date = 02/17/17 Pct Recovery = 106% Analysis Date = 02/15/17 Pct Recovery = 106% Analysis Date = 02/15/17 Pct Recovery = 106% Analysis Date = 02/13/17 Pct Recovery = 105% Analysis Date = 02/13/17 Pct Recovery = 105% Analysis Date = 02/10/17 Pct Recovery = 105% Analysis Date = 02/10/17 Pct Recovery = 105% Analysis Date = 02/08/17 Pct Recovery = 104% Analysis Date = 02/08/17 Pct Recovery = 104% Analysis Date = 02/06/17 Pct Recovery = 104% Analysis Date = 02/06/17 Pct Recovery = 104% Analysis Date = 02/04/17 Pct Recovery = 103% Analysis Date = 02/04/17 Pct Recovery = 103% Analysis Date = 02/01/17 Pct Recovery = 103% Analysis Date = 02/01/17 Pct Recovery = 103% Analysis Date = 01/30/17 Pct Recovery = 102% Analysis Date = 01/30/17 Pct Recovery = 102% Analysis Date = 01/28/17 Pct Recovery = 102% Analysis Date = 01/28/17 Pct Recovery = 102% Analysis Date = 01/25/17 Pct Recovery = 101% Analysis Date = 01/25/17 Pct Recovery = 101% Analysis Date = 01/23/17 Pct Recovery = 100% Analysis Date = 01/23/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 100% Analysis Date = 01/21/17 Pct Recovery = 100% Analysis Date = 01/19/17 Pct Recovery = 99% Analysis Date = 01/19/17 Pct Recovery = 99% Analysis Date = 01/16/17 Pct Recovery = 99% Analysis Date = 01/16/17 Pct Recovery = 99% Analysis Date = 01/14/17 Pct Recovery = 99% Analysis Date = 01/14/17 Pct Recovery = 99% Analysis Date = 01/12/17 Pct Recovery = 100% Analysis Date = 01/12/17 Pct Recovery = 100% Analysis Date = 01/09/17 Pct Recovery = 100% Analysis Date = 01/09/17 Pct Recovery = 100% Analysis Date = 01/07/17 Pct Recovery = 100% Analysis Date = 01/07/17 Pct Recovery = 100% Analysis Date = 01/05/17 Pct Recovery = 100% Analysis Date = 01/05/17 Pct Recovery = 100% Analysis Date = 01/03/17 Pct Recovery = 101% Analysis Date = 01/03/17 Pct Recovery = 101% Analysis Date = 12/31/16 Pct Recovery = 101% Analysis Date = 12/31/16 Pct Recovery = 101% Analysis Date = 12/29/16 Pct Recovery = 101% Analysis Date = 12/29/16 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 101% Analysis Date = 12/27/16 Pct Recovery = 101% Analysis Date = 12/24/16 Pct Recovery = 102% Analysis Date = 12/24/16 Pct Recovery = 102% Analysis Date = 12/22/16 Pct Recovery = 102% Analysis Date = 12/22/16 Pct Recovery = 102% Analysis Date = 12/20/16 Pct Recovery = 102% Analysis Date = 12/20/16 Pct Recovery = 102% Analysis Date = 12/18/16 Pct Recovery = 102% Analysis Date = 12/18/16 Pct Recovery = 102% Analysis Date = 12/15/16 Pct Recovery = 102% Analysis Date = 12/15/16 Pct Recovery = 102% Analysis Date = 12/13/16 Pct Recovery = 103% Analysis Date = 12/13/16 Pct Recovery = 103% Analysis Date = 12/11/16 Pct Recovery = 103% Analysis Date = 12/11/16 Pct Recovery = 103% Analysis Date = 12/08/16 Pct Recovery = 103% Analysis Date = 12/08/16 Pct Recovery = 103% Analysis Date = 12/06/16 Pct Recovery = 103% Analysis Date = 12/06/16 Pct Recovery = 103% Analysis Date = 12/04/16 Pct Recovery = 104% Analysis Date = 12/04/16 Pct Recovery = 104% Analysis Date = 12/02/16 Pct Recovery = 104% Analysis Date = 12/02/16 Pct Recovery = 104% Analysis Date = 11/29/16 Pct Recovery = 104% Analysis Date = 11/29/16 Pct Recovery = 104% Analysis Date = 11/27/16 Pct Recovery = 104% Analysis Date = 11/27/16 Pct Recovery = 104% Analysis Date = 11/25/16 Pct Recovery = 105% Analysis Date = 11/25/16 Pct Recovery = 105% Analysis Date = 11/22/16 Pct Recovery = 105% Analysis Date = 11/22/16 Pct Recovery = 105% Analysis Date = 11/20/16 Pct Recovery = 105% Analysis Date = 11/20/16 Pct Recovery = 105% Analysis Date = 11/18/16 Pct Recovery = 105% Analysis Date = 11/18/16 Pct Recovery = 105% Analysis Date = 11/16/16 Pct Recovery = 106% Analysis Date = 11/16/16 Pct Recovery = 106% Analysis Date = 11/13/16 Pct Recovery = 106% Analysis Date = 11/13/16 Pct Recovery = 106% Analysis Date = 11/11/16 Pct Recovery = 106% Analysis Date = 11/11/16 Pct Recovery = 106% Analysis Date = 11/09/16 Pct Recovery = 106% Analysis Date = 11/09/16 Pct Recovery = 106% Analysis Date = 11/06/16 Pct Recovery = 106% Analysis Date = 11/06/16 Pct Recovery = 106% Analysis Date = 11/04/16 Pct Recovery = 107% Analysis Date = 11/04/16 Pct Recovery = 107% Analysis Date = 11/02/16 Pct Recovery = 107% Analysis Date = 11/02/16 Pct Recovery = 107% Analysis Date = 10/31/16 Pct Recovery = 107% Analysis Date = 10/31/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/28/16 Pct Recovery = 107% Analysis Date = 10/26/16 Pct Recovery = 108% Analysis Date = 10/26/16 Pct Recovery = 108% Analysis Date = 10/24/16 Pct Recovery = 108% Analysis Date = 10/24/16 Pct Recovery = 108% Analysis Date = 10/21/16 Pct Recovery = 108% Analysis Date = 10/21/16 Pct Recovery = 108% Analysis Date = 10/19/16 Pct Recovery = 108% Analysis Date = 10/19/16 Pct Recovery = 108% Analysis Date = 10/17/16 Pct Recovery = 109% Analysis Date = 10/17/16 Pct Recovery = 109% Analysis Date = 10/15/16 Pct Recovery = 109% Analysis Date = 10/15/16 Pct Recovery = 109% Analysis Date = 10/12/16 Pct Recovery = 109% Analysis Date = 10/12/16 Pct Recovery = 109% Analysis Date = 10/10/16 Pct Recovery = 109% Analysis Date = 10/10/16 Pct Recovery = 109% Analysis Date = 10/08/16 Pct Recovery = 109% Analysis Date = 10/08/16 Pct Recovery = 109% Analysis Date = 10/05/16 Pct Recovery = 110% Analysis Date = 10/05/16 Pct Recovery = 110% Analysis Date = 10/03/16 Pct Recovery = 110% Analysis Date = 10/03/16 Pct Recovery = 110% Analysis Date = 10/01/16 Pct Recovery = 110% Analysis Date = 10/01/16 Pct Recovery = 110% Analysis Date = 09/29/16 Pct Recovery = 110% Analysis Date = 09/29/16 Pct Recovery = 110% Analysis Date = 09/26/16 Pct Recovery = 111% Analysis Date = 09/26/16 Pct Recovery = 111% Analysis Date = 09/24/16 Pct Recovery = 111% Analysis Date = 09/24/16 Pct Recovery = 111% Analysis Date = 09/22/16 Pct Recovery = 111% Analysis Date = 09/22/16 Pct Recovery = 111% Analysis Date = 09/19/16 Pct Recovery = 111% Analysis Date = 09/19/16 Pct Recovery = 111% Analysis Date = 09/17/16 Pct Recovery = 112% Analysis Date = 09/17/16 Pct Recovery = 112% Analysis Date = 09/15/16 Pct Recovery = 112% Analysis Date = 09/15/16 Pct Recovery = 112% Analysis Date = 09/13/16 Pct Recovery = 112% Analysis Date = 09/13/16 Pct Recovery = 112% Analysis Date = 09/10/16 Pct Recovery = 112% Analysis Date = 09/10/16 Pct Recovery = 112% Analysis Date = 09/08/16 Pct Recovery = 112% Analysis Date = 09/08/16 Pct Recovery = 112% Analysis Date = 09/06/16 Pct Recovery = 112% Analysis Date = 09/06/16 Pct Recovery = 112% Analysis Date = 09/03/16 Pct Recovery = 112% Analysis Date = 09/03/16 Pct Recovery = 112% Analysis Date = 09/01/16 Pct Recovery = 112% Analysis Date = 09/01/16 Pct Recovery = 112% Analysis Date = 08/30/16 Pct Recovery = 112% Analysis Date = 08/30/16 Pct Recovery = 112% Analysis Date = 08/28/16 Pct Recovery = 112% Analysis Date = 08/28/16 Pct Recovery = 112% Analysis Date = 08/25/16 Pct Recovery = 111% Analysis Date = 08/25/16 Pct Recovery = 111% Analysis Date = 08/23/16 Pct Recovery = 111% Analysis Date = 08/23/16 Pct Recovery = 111% Analysis Date = 08/21/16 Pct Recovery = 111% Analysis Date = 08/21/16 Pct Recovery = 111% Analysis Date = 08/18/16 Pct Recovery = 111% Analysis Date = 08/18/16 Pct Recovery = 111% Analysis Date = 08/16/16 Pct Recovery = 111% Analysis Date = 08/16/16 Pct Recovery = 111% Analysis Date = 08/14/16 Pct Recovery = 111% Analysis Date = 08/14/16 Pct Recovery = 111% Analysis Date = 08/12/16 Pct Recovery = 110% Analysis Date = 08/12/16 Pct Recovery = 110% Analysis Date = 08/09/16 Pct Recovery = 110% Analysis Date = 08/09/16 Pct Recovery = 110% Analysis Date = 08/07/16 Pct Recovery = 110% Analysis Date = 08/07/16 Pct Recovery = 110% Analysis Date = 08/05/16 Pct Recovery = 110% Analysis Date = 08/05/16 Pct Recovery = 110% Analysis Date = 08/02/16 Pct Recovery = 110% Analysis Date = 08/02/16 Pct Recovery = 110% Analysis Date = 07/31/16 Pct Recovery = 109% Analysis Date = 07/31/16 Pct Recovery = 109% Analysis Date = 07/29/16 Pct Recovery = 109% Analysis Date = 07/29/16 Pct Recovery = 109% Analysis Date = 07/27/16 Pct Recovery = 109% Analysis Date = 07/27/16 Pct Recovery = 109% Analysis Date = 07/24/16 Pct Recovery = 109% Analysis Date = 07/24/16 Pct Recovery = 109% Analysis Date = 07/22/16 Pct Recovery = 109% Analysis Date = 07/22/16 Pct Recovery = 109% Analysis Date = 07/20/16 Pct Recovery = 109% Analysis Date = 07/20/16 Pct Recovery = 109% Analysis Date = 07/17/16 Pct Recovery = 108% Analysis Date = 07/17/16 Pct Recovery = 108% Analysis Date = 07/15/16 Pct Recovery = 108% Analysis Date = 07/15/16 Pct Recovery = 108% Analysis Date = 07/13/16 Pct Recovery = 108% Analysis Date = 07/13/16 Pct Recovery = 108% Analysis Date = 07/11/16 Pct Recovery = 108% Analysis Date = 07/11/16 Pct Recovery = 108% Analysis Date = 07/08/16 Pct Recovery = 108% Analysis Date = 07/08/16 Pct Recovery = 108% Analysis Date = 07/06/16 Pct Recovery = 108% Analysis Date = 07/06/16 Pct Recovery = 108% Analysis Date = 07/04/16 Pct Recovery = 107% Analysis Date = 07/04/16 Pct Recovery = 107% Analysis Date = 07/01/16 Pct Recovery = 107% Analysis Date = 07/01/16 Pct Recovery = 107% Analysis Date = 06/29/16 Pct Recovery = 107% Analysis Date = 06/29/16 Pct Recovery = 107% Analysis Date = 06/27/16 Pct Recovery = 107% Analysis Date = 06/27/16 Pct Recovery = 107% Analysis Date = 06/25/16 Pct Recovery = 107% Analysis Date = 06/25/16 Pct Recovery = 107% Analysis Date = 06/22/16 Pct Recovery = 107% Analysis Date = 06/22/16 Pct Recovery = 107% Analysis Date = 06/20/16 Pct Recovery = 106% Analysis Date = 06/20/16 Pct Recovery = 106% Analysis Date = 06/18/16 Pct Recovery = 106% Analysis Date = 06/18/16 Pct Recovery = 106% Analysis Date = 06/15/16 Pct Recovery = 106% Analysis Date = 06/15/16 Pct Recovery = 106% Analysis Date = 06/13/16 Pct Recovery = 106% Analysis Date = 06/13/16 Pct Recovery = 106% Analysis Date = 06/11/16 Pct Recovery = 106% Analysis Date = 06/11/16 Pct Recovery = 106% Analysis Date = 06/09/16 Pct Recovery = 105% Analysis Date = 06/09/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/06/16 Pct Recovery = 105% Analysis Date = 06/04/16 Pct Recovery = 105% Analysis Date = 06/04/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 06/02/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/30/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/28/16 Pct Recovery = 105% Analysis Date = 05/26/16 Pct Recovery = 104% Analysis Date = 05/26/16 Pct Recovery = 104% Analysis Date = 05/24/16 Pct Recovery = 104% Analysis Date = 05/24/16 Pct Recovery = 104% Analysis Date = 05/21/16 Pct Recovery = 104% Analysis Date = 05/21/16 Pct Recovery = 104% Analysis Date = 05/19/16 Pct Recovery = 104% Analysis Date = 05/19/16 Pct Recovery = 104% Analysis Date = 05/17/16 Pct Recovery = 104% Analysis Date = 05/17/16 Pct Recovery = 104% Analysis Date = 05/14/16 Pct Recovery = 104% Analysis Date = 05/14/16 Pct Recovery = 104% Analysis Date = 05/12/16 Pct Recovery = 103% Analysis Date = 05/12/16 Pct Recovery = 103% Analysis Date = 05/10/16 Pct Recovery = 103% Analysis Date = 05/10/16 Pct Recovery = 103% Analysis Date = 05/08/16 Pct Recovery = 103% Analysis Date = 05/08/16 Pct Recovery = 103% Analysis Date = 05/05/16 Pct Recovery = 103% Analysis Date = 05/05/16 Pct Recovery = 103% Analysis Date = 05/03/16 Pct Recovery = 103% Analysis Date = 05/03/16 Pct Recovery = 103% Analysis Date = 05/01/16 Pct Recovery = 102% Analysis Date = 05/01/16 Pct Recovery = 102% Analysis Date = 04/28/16 Pct Recovery = 102% Analysis Date = 04/28/16 Pct Recovery = 102% Analysis Date = 04/26/16 Pct Recovery = 101% Analysis Date = 04/26/16 Pct Recovery = 101% Analysis Date = 04/24/16 Pct Recovery = 101% Analysis Date = 04/24/16 Pct Recovery = 101% Analysis Date = 04/22/16 Pct Recovery = 100% Analysis Date = 04/22/16 Pct Recovery = 100% Analysis Date = 04/19/16 Pct Recovery = 100% Analysis Date = 04/19/16 Pct Recovery = 100% Analysis Date = 04/17/16 Pct Recovery = 100% Analysis Date = 04/17/16 Pct Recovery = 100% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/15/16 Pct Recovery = 99% Analysis Date = 04/12/16 Pct Recovery = 99% Analysis Date = 04/12/16 Pct Recovery = 99% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/10/16 Pct Recovery = 98% Analysis Date = 04/08/16 Pct Recovery = 98% Analysis Date = 04/08/16 Pct Recovery = 98% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/03/16 Pct Recovery = 97% Analysis Date = 04/03/16 Pct Recovery = 97% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 03/30/16 Pct Recovery = 96% Analysis Date = 03/30/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/27/16 Pct Recovery = 95% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/25/16 Pct Recovery = 94% Analysis Date = 03/23/16 Pct Recovery = 94% Analysis Date = 03/23/16 Pct Recovery = 94% Analysis Date = 03/21/16 Pct Recovery = 93% Analysis Date = 03/21/16 Pct Recovery = 93% Analysis Date = 03/18/16 Pct Recovery = 93% Analysis Date = 03/18/16 Pct Recovery = 93% Analysis Date = 03/16/16 Pct Recovery = 92% Analysis Date = 03/16/16 Pct Recovery = 92% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/14/16 Pct Recovery = 91% Analysis Date = 03/11/16 Pct Recovery = 91% Analysis Date = 03/11/16 Pct Recovery = 91% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/09/16 Pct Recovery = 90% Analysis Date = 03/07/16 Pct Recovery = 90% Analysis Date = 03/07/16 Pct Recovery = 90% Analysis Date = 03/05/16 Pct Recovery = 89% Analysis Date = 03/05/16 Pct Recovery = 89% Analysis Date = 03/02/16 Pct Recovery = 88% Analysis Date = 03/02/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/27/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/24/16 Pct Recovery = 87% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/22/16 Pct Recovery = 86% Analysis Date = 02/20/16 Pct Recovery = 85% Analysis Date = 02/20/16 Pct Recovery = 85% Analysis Date = 02/18/16 Pct Recovery = 85% Analysis Date = 02/18/16 Pct Recovery = 85% Analysis Date = 02/15/16 Pct Recovery = 84% Analysis Date = 02/15/16 Pct Recovery = 84% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/13/16 Pct Recovery = 83% Analysis Date = 02/11/16 Pct Recovery = 83% Analysis Date = 02/11/16 Pct Recovery = 83% Analysis Date = 02/09/16 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPANIL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 107% 18% 103% 21%
Total 18 107% 18% 103% 21%

Sample Statistics
PROPANIL

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 1 6% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
PROPARGITE
METHOD: 2033 , TESTIDCODE: 82685GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 87% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 109% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 69% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 57% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 75% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 72% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 74% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 97% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 108% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 75% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 90% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 72% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 82% Analysis Date = 05/10/17 Pct Recovery = 70% Analysis Date = 05/08/17 Pct Recovery = 71% Analysis Date = 05/08/17 Pct Recovery = 71% Analysis Date = 05/06/17 Pct Recovery = 71% Analysis Date = 05/06/17 Pct Recovery = 71% Analysis Date = 05/04/17 Pct Recovery = 72% Analysis Date = 05/04/17 Pct Recovery = 72% Analysis Date = 05/01/17 Pct Recovery = 73% Analysis Date = 05/01/17 Pct Recovery = 73% Analysis Date = 04/29/17 Pct Recovery = 73% Analysis Date = 04/29/17 Pct Recovery = 73% Analysis Date = 04/27/17 Pct Recovery = 74% Analysis Date = 04/27/17 Pct Recovery = 74% Analysis Date = 04/25/17 Pct Recovery = 75% Analysis Date = 04/25/17 Pct Recovery = 75% Analysis Date = 04/22/17 Pct Recovery = 75% Analysis Date = 04/22/17 Pct Recovery = 75% Analysis Date = 04/20/17 Pct Recovery = 76% Analysis Date = 04/20/17 Pct Recovery = 76% Analysis Date = 04/18/17 Pct Recovery = 76% Analysis Date = 04/18/17 Pct Recovery = 76% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/13/17 Pct Recovery = 77% Analysis Date = 04/13/17 Pct Recovery = 77% Analysis Date = 04/11/17 Pct Recovery = 78% Analysis Date = 04/11/17 Pct Recovery = 78% Analysis Date = 04/09/17 Pct Recovery = 79% Analysis Date = 04/09/17 Pct Recovery = 79% Analysis Date = 04/06/17 Pct Recovery = 79% Analysis Date = 04/06/17 Pct Recovery = 79% Analysis Date = 04/04/17 Pct Recovery = 80% Analysis Date = 04/04/17 Pct Recovery = 80% Analysis Date = 04/02/17 Pct Recovery = 80% Analysis Date = 04/02/17 Pct Recovery = 80% Analysis Date = 03/30/17 Pct Recovery = 81% Analysis Date = 03/30/17 Pct Recovery = 81% Analysis Date = 03/28/17 Pct Recovery = 82% Analysis Date = 03/28/17 Pct Recovery = 82% Analysis Date = 03/26/17 Pct Recovery = 82% Analysis Date = 03/26/17 Pct Recovery = 82% Analysis Date = 03/24/17 Pct Recovery = 83% Analysis Date = 03/24/17 Pct Recovery = 83% Analysis Date = 03/21/17 Pct Recovery = 83% Analysis Date = 03/21/17 Pct Recovery = 83% Analysis Date = 03/19/17 Pct Recovery = 84% Analysis Date = 03/19/17 Pct Recovery = 84% Analysis Date = 03/17/17 Pct Recovery = 85% Analysis Date = 03/17/17 Pct Recovery = 85% Analysis Date = 03/14/17 Pct Recovery = 85% Analysis Date = 03/14/17 Pct Recovery = 85% Analysis Date = 03/12/17 Pct Recovery = 86% Analysis Date = 03/12/17 Pct Recovery = 86% Analysis Date = 03/10/17 Pct Recovery = 86% Analysis Date = 03/10/17 Pct Recovery = 86% Analysis Date = 03/08/17 Pct Recovery = 87% Analysis Date = 03/08/17 Pct Recovery = 87% Analysis Date = 03/05/17 Pct Recovery = 88% Analysis Date = 03/05/17 Pct Recovery = 88% Analysis Date = 03/03/17 Pct Recovery = 88% Analysis Date = 03/03/17 Pct Recovery = 88% Analysis Date = 03/01/17 Pct Recovery = 89% Analysis Date = 03/01/17 Pct Recovery = 89% Analysis Date = 02/26/17 Pct Recovery = 89% Analysis Date = 02/26/17 Pct Recovery = 89% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 91% Analysis Date = 02/20/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/17/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/01/17 Pct Recovery = 92% Analysis Date = 02/01/17 Pct Recovery = 92% Analysis Date = 01/30/17 Pct Recovery = 92% Analysis Date = 01/30/17 Pct Recovery = 92% Analysis Date = 01/28/17 Pct Recovery = 92% Analysis Date = 01/28/17 Pct Recovery = 92% Analysis Date = 01/25/17 Pct Recovery = 92% Analysis Date = 01/25/17 Pct Recovery = 92% Analysis Date = 01/23/17 Pct Recovery = 92% Analysis Date = 01/23/17 Pct Recovery = 92% Analysis Date = 01/21/17 Pct Recovery = 92% Analysis Date = 01/21/17 Pct Recovery = 92% Analysis Date = 01/19/17 Pct Recovery = 92% Analysis Date = 01/19/17 Pct Recovery = 92% Analysis Date = 01/16/17 Pct Recovery = 92% Analysis Date = 01/16/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 92% Analysis Date = 01/14/17 Pct Recovery = 92% Analysis Date = 01/12/17 Pct Recovery = 93% Analysis Date = 01/12/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/09/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/07/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/05/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 01/03/17 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/31/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/29/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/27/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/24/16 Pct Recovery = 93% Analysis Date = 12/22/16 Pct Recovery = 94% Analysis Date = 12/22/16 Pct Recovery = 94% Analysis Date = 12/20/16 Pct Recovery = 94% Analysis Date = 12/20/16 Pct Recovery = 94% Analysis Date = 12/18/16 Pct Recovery = 94% Analysis Date = 12/18/16 Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 94% Analysis Date = 12/15/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 94% Analysis Date = 12/13/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/11/16 Pct Recovery = 94% Analysis Date = 12/08/16 Pct Recovery = 94% Analysis Date = 12/08/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/06/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/04/16 Pct Recovery = 94% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 12/02/16 Pct Recovery = 95% Analysis Date = 11/29/16 Pct Recovery = 95% Analysis Date = 11/29/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/27/16 Pct Recovery = 95% Analysis Date = 11/25/16 Pct Recovery = 95% Analysis Date = 11/25/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/22/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/20/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/18/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/16/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/13/16 Pct Recovery = 95% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/11/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/09/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 96% Analysis Date = 11/06/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/04/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 11/02/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 96% Analysis Date = 10/31/16 Pct Recovery = 96% Analysis Date = 10/28/16 Pct Recovery = 96% Analysis Date = 10/28/16 Pct Recovery = 96% Analysis Date = 10/26/16 Pct Recovery = 96% Analysis Date = 10/26/16 Pct Recovery = 96% Analysis Date = 10/24/16 Pct Recovery = 96% Analysis Date = 10/24/16 Pct Recovery = 96% Analysis Date = 10/21/16 Pct Recovery = 97% Analysis Date = 10/21/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/19/16 Pct Recovery = 97% Analysis Date = 10/17/16 Pct Recovery = 97% Analysis Date = 10/17/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 97% Analysis Date = 10/15/16 Pct Recovery = 97% Analysis Date = 10/12/16 Pct Recovery = 97% Analysis Date = 10/12/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/10/16 Pct Recovery = 97% Analysis Date = 10/08/16 Pct Recovery = 97% Analysis Date = 10/08/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 10/05/16 Pct Recovery = 97% Analysis Date = 10/03/16 Pct Recovery = 97% Analysis Date = 10/03/16 Pct Recovery = 97% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 10/01/16 Pct Recovery = 98% Analysis Date = 09/29/16 Pct Recovery = 98% Analysis Date = 09/29/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/26/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 98% Analysis Date = 09/24/16 Pct Recovery = 98% Analysis Date = 09/22/16 Pct Recovery = 98% Analysis Date = 09/22/16 Pct Recovery = 98% Analysis Date = 09/19/16 Pct Recovery = 98% Analysis Date = 09/19/16 Pct Recovery = 98% Analysis Date = 09/17/16 Pct Recovery = 97% Analysis Date = 09/17/16 Pct Recovery = 97% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/15/16 Pct Recovery = 96% Analysis Date = 09/13/16 Pct Recovery = 95% Analysis Date = 09/13/16 Pct Recovery = 95% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/10/16 Pct Recovery = 94% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/08/16 Pct Recovery = 93% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/06/16 Pct Recovery = 92% Analysis Date = 09/03/16 Pct Recovery = 92% Analysis Date = 09/03/16 Pct Recovery = 92% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 09/01/16 Pct Recovery = 91% Analysis Date = 08/30/16 Pct Recovery = 90% Analysis Date = 08/30/16 Pct Recovery = 90% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/21/16 Pct Recovery = 88% Analysis Date = 08/18/16 Pct Recovery = 88% Analysis Date = 08/18/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/16/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/14/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/12/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/09/16 Pct Recovery = 87% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/07/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/05/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 08/02/16 Pct Recovery = 86% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/31/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/29/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/27/16 Pct Recovery = 85% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/24/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/22/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 84% Analysis Date = 07/20/16 Pct Recovery = 84% Analysis Date = 07/17/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/13/16 Pct Recovery = 83% Analysis Date = 07/13/16 Pct Recovery = 83% Analysis Date = 07/11/16 Pct Recovery = 83% Analysis Date = 07/11/16 Pct Recovery = 83% Analysis Date = 07/08/16 Pct Recovery = 82% Analysis Date = 07/08/16 Pct Recovery = 82% Analysis Date = 07/06/16 Pct Recovery = 82% Analysis Date = 07/06/16 Pct Recovery = 82% Analysis Date = 07/04/16 Pct Recovery = 82% Analysis Date = 07/04/16 Pct Recovery = 82% Analysis Date = 07/01/16 Pct Recovery = 81% Analysis Date = 07/01/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/29/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 81% Analysis Date = 06/27/16 Pct Recovery = 81% Analysis Date = 06/25/16 Pct Recovery = 80% Analysis Date = 06/25/16 Pct Recovery = 80% Analysis Date = 06/22/16 Pct Recovery = 80% Analysis Date = 06/22/16 Pct Recovery = 80% Analysis Date = 06/20/16 Pct Recovery = 80% Analysis Date = 06/20/16 Pct Recovery = 80% Analysis Date = 06/18/16 Pct Recovery = 79% Analysis Date = 06/18/16 Pct Recovery = 79% Analysis Date = 06/15/16 Pct Recovery = 79% Analysis Date = 06/15/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/13/16 Pct Recovery = 79% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/11/16 Pct Recovery = 78% Analysis Date = 06/09/16 Pct Recovery = 78% Analysis Date = 06/09/16 Pct Recovery = 78% Analysis Date = 06/06/16 Pct Recovery = 78% Analysis Date = 06/06/16 Pct Recovery = 78% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 06/04/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 77% Analysis Date = 06/02/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 77% Analysis Date = 05/30/16 Pct Recovery = 77% Analysis Date = 05/28/16 Pct Recovery = 76% Analysis Date = 05/28/16 Pct Recovery = 76% Analysis Date = 05/26/16 Pct Recovery = 76% Analysis Date = 05/26/16 Pct Recovery = 76% Analysis Date = 05/24/16 Pct Recovery = 76% Analysis Date = 05/24/16 Pct Recovery = 76% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/21/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/19/16 Pct Recovery = 75% Analysis Date = 05/17/16 Pct Recovery = 75% Analysis Date = 05/17/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 75% Analysis Date = 05/14/16 Pct Recovery = 75% Analysis Date = 05/12/16 Pct Recovery = 76% Analysis Date = 05/12/16 Pct Recovery = 76% Analysis Date = 05/10/16 Pct Recovery = 76% Analysis Date = 05/10/16 Pct Recovery = 76% Analysis Date = 05/08/16 Pct Recovery = 76% Analysis Date = 05/08/16 Pct Recovery = 76% Analysis Date = 05/05/16 Pct Recovery = 76% Analysis Date = 05/05/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 05/03/16 Pct Recovery = 76% Analysis Date = 05/01/16 Pct Recovery = 76% Analysis Date = 05/01/16 Pct Recovery = 76% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/28/16 Pct Recovery = 77% Analysis Date = 04/26/16 Pct Recovery = 77% Analysis Date = 04/26/16 Pct Recovery = 77% Analysis Date = 04/24/16 Pct Recovery = 77% Analysis Date = 04/24/16 Pct Recovery = 77% Analysis Date = 04/22/16 Pct Recovery = 77% Analysis Date = 04/22/16 Pct Recovery = 77% Analysis Date = 04/19/16 Pct Recovery = 77% Analysis Date = 04/19/16 Pct Recovery = 77% Analysis Date = 04/17/16 Pct Recovery = 77% Analysis Date = 04/17/16 Pct Recovery = 77% Analysis Date = 04/15/16 Pct Recovery = 78% Analysis Date = 04/15/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/12/16 Pct Recovery = 78% Analysis Date = 04/10/16 Pct Recovery = 78% Analysis Date = 04/10/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/08/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 78% Analysis Date = 04/06/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/03/16 Pct Recovery = 78% Analysis Date = 04/01/16 Pct Recovery = 79% Analysis Date = 04/01/16 Pct Recovery = 79% Analysis Date = 03/30/16 Pct Recovery = 79% Analysis Date = 03/30/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 79% Analysis Date = 03/27/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/25/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 79% Analysis Date = 03/23/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/21/16 Pct Recovery = 79% Analysis Date = 03/18/16 Pct Recovery = 80% Analysis Date = 03/18/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/16/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/14/16 Pct Recovery = 80% Analysis Date = 03/11/16 Pct Recovery = 80% Analysis Date = 03/11/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/09/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/07/16 Pct Recovery = 80% Analysis Date = 03/05/16 Pct Recovery = 80% Analysis Date = 03/05/16 Pct Recovery = 80% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 81% Analysis Date = 02/27/16 Pct Recovery = 81% Analysis Date = 02/27/16 Pct Recovery = 81% Analysis Date = 02/24/16 Pct Recovery = 81% Analysis Date = 02/24/16 Pct Recovery = 81% Analysis Date = 02/22/16 Pct Recovery = 81% Analysis Date = 02/22/16 Pct Recovery = 81% Analysis Date = 02/20/16 Pct Recovery = 81% Analysis Date = 02/20/16 Pct Recovery = 81% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/18/16 Pct Recovery = 82% Analysis Date = 02/15/16 Pct Recovery = 82% Analysis Date = 02/15/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/13/16 Pct Recovery = 82% Analysis Date = 02/11/16 Pct Recovery = 82% Analysis Date = 02/11/16 Pct Recovery = 82% Analysis Date = 02/09/16 Pct Recovery = 82% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPARGITE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 13 82% 16% 75% 13%
Total 13 82% 16% 75% 13%

Sample Statistics
PROPARGITE

Characteristic N % % Basis
Plotted 13 100% Spiked
Estimated Values 4 31% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 13 .  
False Negatives 0 0% 0 out of 13
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
PROPYZAMIDE (PRONAMIDE)
METHOD: 2033 , TESTIDCODE: 82676GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 91% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 101% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 83% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 79% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 63% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 83% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 83% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 64% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 60% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 73% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 86% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 77% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 77% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 95% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 71% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 75% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 69% Analysis Date = 05/10/17 Pct Recovery = 86% Analysis Date = 05/08/17 Pct Recovery = 86% Analysis Date = 05/08/17 Pct Recovery = 86% Analysis Date = 05/06/17 Pct Recovery = 85% Analysis Date = 05/06/17 Pct Recovery = 85% Analysis Date = 05/04/17 Pct Recovery = 85% Analysis Date = 05/04/17 Pct Recovery = 85% Analysis Date = 05/02/17 Pct Recovery = 85% Analysis Date = 05/02/17 Pct Recovery = 85% Analysis Date = 04/30/17 Pct Recovery = 85% Analysis Date = 04/30/17 Pct Recovery = 85% Analysis Date = 04/27/17 Pct Recovery = 85% Analysis Date = 04/27/17 Pct Recovery = 85% Analysis Date = 04/25/17 Pct Recovery = 85% Analysis Date = 04/25/17 Pct Recovery = 85% Analysis Date = 04/23/17 Pct Recovery = 85% Analysis Date = 04/23/17 Pct Recovery = 85% Analysis Date = 04/21/17 Pct Recovery = 85% Analysis Date = 04/21/17 Pct Recovery = 85% Analysis Date = 04/19/17 Pct Recovery = 85% Analysis Date = 04/19/17 Pct Recovery = 85% Analysis Date = 04/17/17 Pct Recovery = 85% Analysis Date = 04/17/17 Pct Recovery = 85% Analysis Date = 04/14/17 Pct Recovery = 85% Analysis Date = 04/14/17 Pct Recovery = 85% Analysis Date = 04/12/17 Pct Recovery = 85% Analysis Date = 04/12/17 Pct Recovery = 85% Analysis Date = 04/10/17 Pct Recovery = 84% Analysis Date = 04/10/17 Pct Recovery = 84% Analysis Date = 04/08/17 Pct Recovery = 84% Analysis Date = 04/08/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/06/17 Pct Recovery = 84% Analysis Date = 04/04/17 Pct Recovery = 84% Analysis Date = 04/04/17 Pct Recovery = 84% Analysis Date = 04/01/17 Pct Recovery = 84% Analysis Date = 04/01/17 Pct Recovery = 84% Analysis Date = 03/30/17 Pct Recovery = 84% Analysis Date = 03/30/17 Pct Recovery = 84% Analysis Date = 03/28/17 Pct Recovery = 84% Analysis Date = 03/28/17 Pct Recovery = 84% Analysis Date = 03/26/17 Pct Recovery = 84% Analysis Date = 03/26/17 Pct Recovery = 84% Analysis Date = 03/24/17 Pct Recovery = 84% Analysis Date = 03/24/17 Pct Recovery = 84% Analysis Date = 03/21/17 Pct Recovery = 84% Analysis Date = 03/21/17 Pct Recovery = 84% Analysis Date = 03/19/17 Pct Recovery = 84% Analysis Date = 03/19/17 Pct Recovery = 84% Analysis Date = 03/17/17 Pct Recovery = 83% Analysis Date = 03/17/17 Pct Recovery = 83% Analysis Date = 03/15/17 Pct Recovery = 83% Analysis Date = 03/15/17 Pct Recovery = 83% Analysis Date = 03/13/17 Pct Recovery = 83% Analysis Date = 03/13/17 Pct Recovery = 83% Analysis Date = 03/11/17 Pct Recovery = 83% Analysis Date = 03/11/17 Pct Recovery = 83% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/08/17 Pct Recovery = 83% Analysis Date = 03/06/17 Pct Recovery = 83% Analysis Date = 03/06/17 Pct Recovery = 83% Analysis Date = 03/04/17 Pct Recovery = 83% Analysis Date = 03/04/17 Pct Recovery = 83% Analysis Date = 03/02/17 Pct Recovery = 83% Analysis Date = 03/02/17 Pct Recovery = 83% Analysis Date = 02/28/17 Pct Recovery = 82% Analysis Date = 02/28/17 Pct Recovery = 82% Analysis Date = 02/26/17 Pct Recovery = 82% Analysis Date = 02/26/17 Pct Recovery = 82% Analysis Date = 02/23/17 Pct Recovery = 82% Analysis Date = 02/23/17 Pct Recovery = 82% Analysis Date = 02/21/17 Pct Recovery = 82% Analysis Date = 02/21/17 Pct Recovery = 82% Analysis Date = 02/19/17 Pct Recovery = 81% Analysis Date = 02/19/17 Pct Recovery = 81% Analysis Date = 02/17/17 Pct Recovery = 81% Analysis Date = 02/17/17 Pct Recovery = 81% Analysis Date = 02/15/17 Pct Recovery = 81% Analysis Date = 02/15/17 Pct Recovery = 81% Analysis Date = 02/12/17 Pct Recovery = 80% Analysis Date = 02/12/17 Pct Recovery = 80% Analysis Date = 02/10/17 Pct Recovery = 80% Analysis Date = 02/10/17 Pct Recovery = 80% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/08/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/06/17 Pct Recovery = 79% Analysis Date = 02/04/17 Pct Recovery = 78% Analysis Date = 02/04/17 Pct Recovery = 78% Analysis Date = 02/02/17 Pct Recovery = 78% Analysis Date = 02/02/17 Pct Recovery = 78% Analysis Date = 01/30/17 Pct Recovery = 77% Analysis Date = 01/30/17 Pct Recovery = 77% Analysis Date = 01/28/17 Pct Recovery = 77% Analysis Date = 01/28/17 Pct Recovery = 77% Analysis Date = 01/26/17 Pct Recovery = 76% Analysis Date = 01/26/17 Pct Recovery = 76% Analysis Date = 01/24/17 Pct Recovery = 76% Analysis Date = 01/24/17 Pct Recovery = 76% Analysis Date = 01/22/17 Pct Recovery = 75% Analysis Date = 01/22/17 Pct Recovery = 75% Analysis Date = 01/20/17 Pct Recovery = 75% Analysis Date = 01/20/17 Pct Recovery = 75% Analysis Date = 01/17/17 Pct Recovery = 74% Analysis Date = 01/17/17 Pct Recovery = 74% Analysis Date = 01/15/17 Pct Recovery = 75% Analysis Date = 01/15/17 Pct Recovery = 75% Analysis Date = 01/13/17 Pct Recovery = 75% Analysis Date = 01/13/17 Pct Recovery = 75% Analysis Date = 01/11/17 Pct Recovery = 75% Analysis Date = 01/11/17 Pct Recovery = 75% Analysis Date = 01/09/17 Pct Recovery = 75% Analysis Date = 01/09/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 01/07/17 Pct Recovery = 75% Analysis Date = 01/04/17 Pct Recovery = 75% Analysis Date = 01/04/17 Pct Recovery = 75% Analysis Date = 01/02/17 Pct Recovery = 75% Analysis Date = 01/02/17 Pct Recovery = 75% Analysis Date = 12/31/16 Pct Recovery = 75% Analysis Date = 12/31/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/22/16 Pct Recovery = 75% Analysis Date = 12/22/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 76% Analysis Date = 12/20/16 Pct Recovery = 76% Analysis Date = 12/18/16 Pct Recovery = 76% Analysis Date = 12/18/16 Pct Recovery = 76% Analysis Date = 12/16/16 Pct Recovery = 76% Analysis Date = 12/16/16 Pct Recovery = 76% Analysis Date = 12/14/16 Pct Recovery = 76% Analysis Date = 12/14/16 Pct Recovery = 76% Analysis Date = 12/11/16 Pct Recovery = 76% Analysis Date = 12/11/16 Pct Recovery = 76% Analysis Date = 12/09/16 Pct Recovery = 76% Analysis Date = 12/09/16 Pct Recovery = 76% Analysis Date = 12/07/16 Pct Recovery = 76% Analysis Date = 12/07/16 Pct Recovery = 76% Analysis Date = 12/05/16 Pct Recovery = 76% Analysis Date = 12/05/16 Pct Recovery = 76% Analysis Date = 12/03/16 Pct Recovery = 76% Analysis Date = 12/03/16 Pct Recovery = 76% Analysis Date = 12/01/16 Pct Recovery = 76% Analysis Date = 12/01/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/26/16 Pct Recovery = 76% Analysis Date = 11/26/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 77% Analysis Date = 11/24/16 Pct Recovery = 77% Analysis Date = 11/22/16 Pct Recovery = 77% Analysis Date = 11/22/16 Pct Recovery = 77% Analysis Date = 11/20/16 Pct Recovery = 77% Analysis Date = 11/20/16 Pct Recovery = 77% Analysis Date = 11/17/16 Pct Recovery = 77% Analysis Date = 11/17/16 Pct Recovery = 77% Analysis Date = 11/15/16 Pct Recovery = 77% Analysis Date = 11/15/16 Pct Recovery = 77% Analysis Date = 11/13/16 Pct Recovery = 77% Analysis Date = 11/13/16 Pct Recovery = 77% Analysis Date = 11/11/16 Pct Recovery = 77% Analysis Date = 11/11/16 Pct Recovery = 77% Analysis Date = 11/09/16 Pct Recovery = 77% Analysis Date = 11/09/16 Pct Recovery = 77% Analysis Date = 11/07/16 Pct Recovery = 77% Analysis Date = 11/07/16 Pct Recovery = 77% Analysis Date = 11/04/16 Pct Recovery = 77% Analysis Date = 11/04/16 Pct Recovery = 77% Analysis Date = 11/02/16 Pct Recovery = 77% Analysis Date = 11/02/16 Pct Recovery = 77% Analysis Date = 10/31/16 Pct Recovery = 78% Analysis Date = 10/31/16 Pct Recovery = 78% Analysis Date = 10/29/16 Pct Recovery = 78% Analysis Date = 10/29/16 Pct Recovery = 78% Analysis Date = 10/27/16 Pct Recovery = 78% Analysis Date = 10/27/16 Pct Recovery = 78% Analysis Date = 10/25/16 Pct Recovery = 78% Analysis Date = 10/25/16 Pct Recovery = 78% Analysis Date = 10/22/16 Pct Recovery = 78% Analysis Date = 10/22/16 Pct Recovery = 78% Analysis Date = 10/20/16 Pct Recovery = 78% Analysis Date = 10/20/16 Pct Recovery = 78% Analysis Date = 10/18/16 Pct Recovery = 78% Analysis Date = 10/18/16 Pct Recovery = 78% Analysis Date = 10/16/16 Pct Recovery = 78% Analysis Date = 10/16/16 Pct Recovery = 78% Analysis Date = 10/14/16 Pct Recovery = 78% Analysis Date = 10/14/16 Pct Recovery = 78% Analysis Date = 10/12/16 Pct Recovery = 78% Analysis Date = 10/12/16 Pct Recovery = 78% Analysis Date = 10/09/16 Pct Recovery = 78% Analysis Date = 10/09/16 Pct Recovery = 78% Analysis Date = 10/07/16 Pct Recovery = 78% Analysis Date = 10/07/16 Pct Recovery = 78% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 10/05/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 10/03/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 10/01/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/28/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/26/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 79% Analysis Date = 09/24/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/22/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/20/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 79% Analysis Date = 09/18/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/15/16 Pct Recovery = 79% Analysis Date = 09/13/16 Pct Recovery = 79% Analysis Date = 09/13/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/11/16 Pct Recovery = 79% Analysis Date = 09/09/16 Pct Recovery = 79% Analysis Date = 09/09/16 Pct Recovery = 79% Analysis Date = 09/07/16 Pct Recovery = 79% Analysis Date = 09/07/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 09/05/16 Pct Recovery = 79% Analysis Date = 09/02/16 Pct Recovery = 79% Analysis Date = 09/02/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/31/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/29/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/27/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/25/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/22/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/20/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/18/16 Pct Recovery = 79% Analysis Date = 08/16/16 Pct Recovery = 78% Analysis Date = 08/16/16 Pct Recovery = 78% Analysis Date = 08/14/16 Pct Recovery = 78% Analysis Date = 08/14/16 Pct Recovery = 78% Analysis Date = 08/12/16 Pct Recovery = 78% Analysis Date = 08/12/16 Pct Recovery = 78% Analysis Date = 08/09/16 Pct Recovery = 78% Analysis Date = 08/09/16 Pct Recovery = 78% Analysis Date = 08/07/16 Pct Recovery = 78% Analysis Date = 08/07/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/05/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 08/03/16 Pct Recovery = 78% Analysis Date = 08/01/16 Pct Recovery = 77% Analysis Date = 08/01/16 Pct Recovery = 77% Analysis Date = 07/30/16 Pct Recovery = 77% Analysis Date = 07/30/16 Pct Recovery = 77% Analysis Date = 07/27/16 Pct Recovery = 77% Analysis Date = 07/27/16 Pct Recovery = 77% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/25/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/23/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/21/16 Pct Recovery = 77% Analysis Date = 07/19/16 Pct Recovery = 77% Analysis Date = 07/19/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/14/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/12/16 Pct Recovery = 76% Analysis Date = 07/10/16 Pct Recovery = 76% Analysis Date = 07/10/16 Pct Recovery = 76% Analysis Date = 07/08/16 Pct Recovery = 76% Analysis Date = 07/08/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/06/16 Pct Recovery = 76% Analysis Date = 07/03/16 Pct Recovery = 76% Analysis Date = 07/03/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 07/01/16 Pct Recovery = 76% Analysis Date = 06/29/16 Pct Recovery = 75% Analysis Date = 06/29/16 Pct Recovery = 75% Analysis Date = 06/27/16 Pct Recovery = 75% Analysis Date = 06/27/16 Pct Recovery = 75% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/25/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/23/16 Pct Recovery = 75% Analysis Date = 06/20/16 Pct Recovery = 75% Analysis Date = 06/20/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/18/16 Pct Recovery = 75% Analysis Date = 06/16/16 Pct Recovery = 75% Analysis Date = 06/16/16 Pct Recovery = 75% Analysis Date = 06/14/16 Pct Recovery = 74% Analysis Date = 06/14/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/12/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/10/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/07/16 Pct Recovery = 74% Analysis Date = 06/05/16 Pct Recovery = 74% Analysis Date = 06/05/16 Pct Recovery = 74% Analysis Date = 06/03/16 Pct Recovery = 74% Analysis Date = 06/03/16 Pct Recovery = 74% Analysis Date = 06/01/16 Pct Recovery = 74% Analysis Date = 06/01/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/30/16 Pct Recovery = 74% Analysis Date = 05/27/16 Pct Recovery = 73% Analysis Date = 05/27/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/25/16 Pct Recovery = 73% Analysis Date = 05/23/16 Pct Recovery = 73% Analysis Date = 05/23/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/21/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/19/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/17/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/14/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/12/16 Pct Recovery = 73% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/10/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/08/16 Pct Recovery = 72% Analysis Date = 05/06/16 Pct Recovery = 72% Analysis Date = 05/06/16 Pct Recovery = 72% Analysis Date = 05/04/16 Pct Recovery = 72% Analysis Date = 05/04/16 Pct Recovery = 72% Analysis Date = 05/01/16 Pct Recovery = 72% Analysis Date = 05/01/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/29/16 Pct Recovery = 72% Analysis Date = 04/27/16 Pct Recovery = 72% Analysis Date = 04/27/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/25/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/23/16 Pct Recovery = 72% Analysis Date = 04/21/16 Pct Recovery = 71% Analysis Date = 04/21/16 Pct Recovery = 71% Analysis Date = 04/18/16 Pct Recovery = 71% Analysis Date = 04/18/16 Pct Recovery = 71% Analysis Date = 04/16/16 Pct Recovery = 71% Analysis Date = 04/16/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/12/16 Pct Recovery = 71% Analysis Date = 04/12/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/10/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/05/16 Pct Recovery = 71% Analysis Date = 04/03/16 Pct Recovery = 71% Analysis Date = 04/03/16 Pct Recovery = 71% Analysis Date = 04/01/16 Pct Recovery = 70% Analysis Date = 04/01/16 Pct Recovery = 70% Analysis Date = 03/30/16 Pct Recovery = 70% Analysis Date = 03/30/16 Pct Recovery = 70% Analysis Date = 03/28/16 Pct Recovery = 70% Analysis Date = 03/28/16 Pct Recovery = 70% Analysis Date = 03/25/16 Pct Recovery = 70% Analysis Date = 03/25/16 Pct Recovery = 70% Analysis Date = 03/23/16 Pct Recovery = 70% Analysis Date = 03/23/16 Pct Recovery = 70% Analysis Date = 03/21/16 Pct Recovery = 70% Analysis Date = 03/21/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/19/16 Pct Recovery = 70% Analysis Date = 03/17/16 Pct Recovery = 70% Analysis Date = 03/17/16 Pct Recovery = 70% Analysis Date = 03/15/16 Pct Recovery = 70% Analysis Date = 03/15/16 Pct Recovery = 70% Analysis Date = 03/12/16 Pct Recovery = 69% Analysis Date = 03/12/16 Pct Recovery = 69% Analysis Date = 03/10/16 Pct Recovery = 69% Analysis Date = 03/10/16 Pct Recovery = 69% Analysis Date = 03/08/16 Pct Recovery = 69% Analysis Date = 03/08/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/06/16 Pct Recovery = 69% Analysis Date = 03/04/16 Pct Recovery = 69% Analysis Date = 03/04/16 Pct Recovery = 69% Analysis Date = 03/02/16 Pct Recovery = 69% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
PROPYZAMIDE (PRONAMIDE)

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 79% 11% 78% 11%
Total 18 79% 11% 78% 11%

Sample Statistics
PROPYZAMIDE (PRONAMIDE)

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
SIMAZINE
METHOD: 2033 , TESTIDCODE: 04035GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 121% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 111% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 100% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 87% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 84% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 59% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 99% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 75% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 89% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 90% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 86% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 141% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 90% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 118% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 118% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 100% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 90% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 99% Analysis Date = 05/10/17 Pct Recovery = 89% Analysis Date = 05/08/17 Pct Recovery = 89% Analysis Date = 05/08/17 Pct Recovery = 89% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/04/17 Pct Recovery = 90% Analysis Date = 05/04/17 Pct Recovery = 90% Analysis Date = 05/01/17 Pct Recovery = 90% Analysis Date = 05/01/17 Pct Recovery = 90% Analysis Date = 04/29/17 Pct Recovery = 91% Analysis Date = 04/29/17 Pct Recovery = 91% Analysis Date = 04/27/17 Pct Recovery = 91% Analysis Date = 04/27/17 Pct Recovery = 91% Analysis Date = 04/25/17 Pct Recovery = 91% Analysis Date = 04/25/17 Pct Recovery = 91% Analysis Date = 04/22/17 Pct Recovery = 92% Analysis Date = 04/22/17 Pct Recovery = 92% Analysis Date = 04/20/17 Pct Recovery = 92% Analysis Date = 04/20/17 Pct Recovery = 92% Analysis Date = 04/18/17 Pct Recovery = 92% Analysis Date = 04/18/17 Pct Recovery = 92% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/15/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 93% Analysis Date = 04/13/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/11/17 Pct Recovery = 93% Analysis Date = 04/09/17 Pct Recovery = 94% Analysis Date = 04/09/17 Pct Recovery = 94% Analysis Date = 04/06/17 Pct Recovery = 94% Analysis Date = 04/06/17 Pct Recovery = 94% Analysis Date = 04/04/17 Pct Recovery = 94% Analysis Date = 04/04/17 Pct Recovery = 94% Analysis Date = 04/02/17 Pct Recovery = 95% Analysis Date = 04/02/17 Pct Recovery = 95% Analysis Date = 03/30/17 Pct Recovery = 95% Analysis Date = 03/30/17 Pct Recovery = 95% Analysis Date = 03/28/17 Pct Recovery = 95% Analysis Date = 03/28/17 Pct Recovery = 95% Analysis Date = 03/26/17 Pct Recovery = 96% Analysis Date = 03/26/17 Pct Recovery = 96% Analysis Date = 03/24/17 Pct Recovery = 96% Analysis Date = 03/24/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/21/17 Pct Recovery = 96% Analysis Date = 03/19/17 Pct Recovery = 97% Analysis Date = 03/19/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/17/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/14/17 Pct Recovery = 97% Analysis Date = 03/12/17 Pct Recovery = 98% Analysis Date = 03/12/17 Pct Recovery = 98% Analysis Date = 03/10/17 Pct Recovery = 98% Analysis Date = 03/10/17 Pct Recovery = 98% Analysis Date = 03/08/17 Pct Recovery = 98% Analysis Date = 03/08/17 Pct Recovery = 98% Analysis Date = 03/05/17 Pct Recovery = 98% Analysis Date = 03/05/17 Pct Recovery = 98% Analysis Date = 03/03/17 Pct Recovery = 99% Analysis Date = 03/03/17 Pct Recovery = 99% Analysis Date = 03/01/17 Pct Recovery = 99% Analysis Date = 03/01/17 Pct Recovery = 99% Analysis Date = 02/26/17 Pct Recovery = 99% Analysis Date = 02/26/17 Pct Recovery = 99% Analysis Date = 02/24/17 Pct Recovery = 100% Analysis Date = 02/24/17 Pct Recovery = 100% Analysis Date = 02/22/17 Pct Recovery = 100% Analysis Date = 02/22/17 Pct Recovery = 100% Analysis Date = 02/20/17 Pct Recovery = 100% Analysis Date = 02/20/17 Pct Recovery = 100% Analysis Date = 02/17/17 Pct Recovery = 100% Analysis Date = 02/17/17 Pct Recovery = 100% Analysis Date = 02/15/17 Pct Recovery = 100% Analysis Date = 02/15/17 Pct Recovery = 100% Analysis Date = 02/13/17 Pct Recovery = 100% Analysis Date = 02/13/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/10/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 100% Analysis Date = 02/08/17 Pct Recovery = 100% Analysis Date = 02/06/17 Pct Recovery = 100% Analysis Date = 02/06/17 Pct Recovery = 100% Analysis Date = 02/04/17 Pct Recovery = 99% Analysis Date = 02/04/17 Pct Recovery = 99% Analysis Date = 02/01/17 Pct Recovery = 99% Analysis Date = 02/01/17 Pct Recovery = 99% Analysis Date = 01/30/17 Pct Recovery = 99% Analysis Date = 01/30/17 Pct Recovery = 99% Analysis Date = 01/28/17 Pct Recovery = 99% Analysis Date = 01/28/17 Pct Recovery = 99% Analysis Date = 01/25/17 Pct Recovery = 99% Analysis Date = 01/25/17 Pct Recovery = 99% Analysis Date = 01/23/17 Pct Recovery = 99% Analysis Date = 01/23/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/21/17 Pct Recovery = 99% Analysis Date = 01/19/17 Pct Recovery = 99% Analysis Date = 01/19/17 Pct Recovery = 99% Analysis Date = 01/16/17 Pct Recovery = 99% Analysis Date = 01/16/17 Pct Recovery = 99% Analysis Date = 01/14/17 Pct Recovery = 99% Analysis Date = 01/14/17 Pct Recovery = 99% Analysis Date = 01/12/17 Pct Recovery = 99% Analysis Date = 01/12/17 Pct Recovery = 99% Analysis Date = 01/09/17 Pct Recovery = 99% Analysis Date = 01/09/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/07/17 Pct Recovery = 99% Analysis Date = 01/05/17 Pct Recovery = 99% Analysis Date = 01/05/17 Pct Recovery = 99% Analysis Date = 01/03/17 Pct Recovery = 99% Analysis Date = 01/03/17 Pct Recovery = 99% Analysis Date = 12/31/16 Pct Recovery = 99% Analysis Date = 12/31/16 Pct Recovery = 99% Analysis Date = 12/29/16 Pct Recovery = 99% Analysis Date = 12/29/16 Pct Recovery = 99% Analysis Date = 12/27/16 Pct Recovery = 99% Analysis Date = 12/27/16 Pct Recovery = 99% Analysis Date = 12/24/16 Pct Recovery = 99% Analysis Date = 12/24/16 Pct Recovery = 99% Analysis Date = 12/22/16 Pct Recovery = 99% Analysis Date = 12/22/16 Pct Recovery = 99% Analysis Date = 12/20/16 Pct Recovery = 99% Analysis Date = 12/20/16 Pct Recovery = 99% Analysis Date = 12/18/16 Pct Recovery = 99% Analysis Date = 12/18/16 Pct Recovery = 99% Analysis Date = 12/15/16 Pct Recovery = 99% Analysis Date = 12/15/16 Pct Recovery = 99% Analysis Date = 12/13/16 Pct Recovery = 99% Analysis Date = 12/13/16 Pct Recovery = 99% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/11/16 Pct Recovery = 99% Analysis Date = 12/08/16 Pct Recovery = 99% Analysis Date = 12/08/16 Pct Recovery = 99% Analysis Date = 12/06/16 Pct Recovery = 99% Analysis Date = 12/06/16 Pct Recovery = 99% Analysis Date = 12/04/16 Pct Recovery = 99% Analysis Date = 12/04/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 12/02/16 Pct Recovery = 99% Analysis Date = 11/29/16 Pct Recovery = 99% Analysis Date = 11/29/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 99% Analysis Date = 11/27/16 Pct Recovery = 99% Analysis Date = 11/25/16 Pct Recovery = 99% Analysis Date = 11/25/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/22/16 Pct Recovery = 99% Analysis Date = 11/20/16 Pct Recovery = 99% Analysis Date = 11/20/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/18/16 Pct Recovery = 99% Analysis Date = 11/16/16 Pct Recovery = 99% Analysis Date = 11/16/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/13/16 Pct Recovery = 99% Analysis Date = 11/11/16 Pct Recovery = 99% Analysis Date = 11/11/16 Pct Recovery = 99% Analysis Date = 11/09/16 Pct Recovery = 99% Analysis Date = 11/09/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 99% Analysis Date = 11/06/16 Pct Recovery = 99% Analysis Date = 11/04/16 Pct Recovery = 99% Analysis Date = 11/04/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 11/02/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/31/16 Pct Recovery = 99% Analysis Date = 10/28/16 Pct Recovery = 99% Analysis Date = 10/28/16 Pct Recovery = 99% Analysis Date = 10/26/16 Pct Recovery = 99% Analysis Date = 10/26/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/24/16 Pct Recovery = 99% Analysis Date = 10/21/16 Pct Recovery = 99% Analysis Date = 10/21/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/19/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 99% Analysis Date = 10/17/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/15/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/12/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/10/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/08/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/05/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/03/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 10/01/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/29/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 99% Analysis Date = 09/26/16 Pct Recovery = 99% Analysis Date = 09/24/16 Pct Recovery = 99% Analysis Date = 09/24/16 Pct Recovery = 99% Analysis Date = 09/22/16 Pct Recovery = 99% Analysis Date = 09/22/16 Pct Recovery = 99% Analysis Date = 09/19/16 Pct Recovery = 99% Analysis Date = 09/19/16 Pct Recovery = 99% Analysis Date = 09/17/16 Pct Recovery = 99% Analysis Date = 09/17/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/15/16 Pct Recovery = 99% Analysis Date = 09/13/16 Pct Recovery = 99% Analysis Date = 09/13/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 99% Analysis Date = 09/10/16 Pct Recovery = 99% Analysis Date = 09/08/16 Pct Recovery = 100% Analysis Date = 09/08/16 Pct Recovery = 100% Analysis Date = 09/06/16 Pct Recovery = 100% Analysis Date = 09/06/16 Pct Recovery = 100% Analysis Date = 09/03/16 Pct Recovery = 100% Analysis Date = 09/03/16 Pct Recovery = 100% Analysis Date = 09/01/16 Pct Recovery = 100% Analysis Date = 09/01/16 Pct Recovery = 100% Analysis Date = 08/30/16 Pct Recovery = 100% Analysis Date = 08/30/16 Pct Recovery = 100% Analysis Date = 08/28/16 Pct Recovery = 100% Analysis Date = 08/28/16 Pct Recovery = 100% Analysis Date = 08/25/16 Pct Recovery = 100% Analysis Date = 08/25/16 Pct Recovery = 100% Analysis Date = 08/23/16 Pct Recovery = 100% Analysis Date = 08/23/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 100% Analysis Date = 08/21/16 Pct Recovery = 100% Analysis Date = 08/18/16 Pct Recovery = 100% Analysis Date = 08/18/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/14/16 Pct Recovery = 100% Analysis Date = 08/12/16 Pct Recovery = 100% Analysis Date = 08/12/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/09/16 Pct Recovery = 100% Analysis Date = 08/07/16 Pct Recovery = 100% Analysis Date = 08/07/16 Pct Recovery = 100% Analysis Date = 08/05/16 Pct Recovery = 100% Analysis Date = 08/05/16 Pct Recovery = 100% Analysis Date = 08/02/16 Pct Recovery = 100% Analysis Date = 08/02/16 Pct Recovery = 100% Analysis Date = 07/31/16 Pct Recovery = 100% Analysis Date = 07/31/16 Pct Recovery = 100% Analysis Date = 07/29/16 Pct Recovery = 100% Analysis Date = 07/29/16 Pct Recovery = 100% Analysis Date = 07/27/16 Pct Recovery = 100% Analysis Date = 07/27/16 Pct Recovery = 100% Analysis Date = 07/24/16 Pct Recovery = 100% Analysis Date = 07/24/16 Pct Recovery = 100% Analysis Date = 07/22/16 Pct Recovery = 100% Analysis Date = 07/22/16 Pct Recovery = 100% Analysis Date = 07/20/16 Pct Recovery = 99% Analysis Date = 07/20/16 Pct Recovery = 99% Analysis Date = 07/17/16 Pct Recovery = 99% Analysis Date = 07/17/16 Pct Recovery = 99% Analysis Date = 07/15/16 Pct Recovery = 99% Analysis Date = 07/15/16 Pct Recovery = 99% Analysis Date = 07/13/16 Pct Recovery = 99% Analysis Date = 07/13/16 Pct Recovery = 99% Analysis Date = 07/11/16 Pct Recovery = 99% Analysis Date = 07/11/16 Pct Recovery = 99% Analysis Date = 07/08/16 Pct Recovery = 99% Analysis Date = 07/08/16 Pct Recovery = 99% Analysis Date = 07/06/16 Pct Recovery = 99% Analysis Date = 07/06/16 Pct Recovery = 99% Analysis Date = 07/04/16 Pct Recovery = 99% Analysis Date = 07/04/16 Pct Recovery = 99% Analysis Date = 07/01/16 Pct Recovery = 99% Analysis Date = 07/01/16 Pct Recovery = 99% Analysis Date = 06/29/16 Pct Recovery = 99% Analysis Date = 06/29/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/27/16 Pct Recovery = 99% Analysis Date = 06/25/16 Pct Recovery = 99% Analysis Date = 06/25/16 Pct Recovery = 99% Analysis Date = 06/22/16 Pct Recovery = 99% Analysis Date = 06/22/16 Pct Recovery = 99% Analysis Date = 06/20/16 Pct Recovery = 99% Analysis Date = 06/20/16 Pct Recovery = 99% Analysis Date = 06/18/16 Pct Recovery = 99% Analysis Date = 06/18/16 Pct Recovery = 99% Analysis Date = 06/15/16 Pct Recovery = 99% Analysis Date = 06/15/16 Pct Recovery = 99% Analysis Date = 06/13/16 Pct Recovery = 99% Analysis Date = 06/13/16 Pct Recovery = 99% Analysis Date = 06/11/16 Pct Recovery = 99% Analysis Date = 06/11/16 Pct Recovery = 99% Analysis Date = 06/09/16 Pct Recovery = 99% Analysis Date = 06/09/16 Pct Recovery = 99% Analysis Date = 06/06/16 Pct Recovery = 99% Analysis Date = 06/06/16 Pct Recovery = 99% Analysis Date = 06/04/16 Pct Recovery = 99% Analysis Date = 06/04/16 Pct Recovery = 99% Analysis Date = 06/02/16 Pct Recovery = 99% Analysis Date = 06/02/16 Pct Recovery = 99% Analysis Date = 05/30/16 Pct Recovery = 99% Analysis Date = 05/30/16 Pct Recovery = 99% Analysis Date = 05/28/16 Pct Recovery = 99% Analysis Date = 05/28/16 Pct Recovery = 99% Analysis Date = 05/26/16 Pct Recovery = 99% Analysis Date = 05/26/16 Pct Recovery = 99% Analysis Date = 05/24/16 Pct Recovery = 99% Analysis Date = 05/24/16 Pct Recovery = 99% Analysis Date = 05/21/16 Pct Recovery = 99% Analysis Date = 05/21/16 Pct Recovery = 99% Analysis Date = 05/19/16 Pct Recovery = 99% Analysis Date = 05/19/16 Pct Recovery = 99% Analysis Date = 05/17/16 Pct Recovery = 99% Analysis Date = 05/17/16 Pct Recovery = 99% Analysis Date = 05/14/16 Pct Recovery = 98% Analysis Date = 05/14/16 Pct Recovery = 98% Analysis Date = 05/12/16 Pct Recovery = 98% Analysis Date = 05/12/16 Pct Recovery = 98% Analysis Date = 05/10/16 Pct Recovery = 98% Analysis Date = 05/10/16 Pct Recovery = 98% Analysis Date = 05/08/16 Pct Recovery = 98% Analysis Date = 05/08/16 Pct Recovery = 98% Analysis Date = 05/05/16 Pct Recovery = 98% Analysis Date = 05/05/16 Pct Recovery = 98% Analysis Date = 05/03/16 Pct Recovery = 98% Analysis Date = 05/03/16 Pct Recovery = 98% Analysis Date = 05/01/16 Pct Recovery = 98% Analysis Date = 05/01/16 Pct Recovery = 98% Analysis Date = 04/28/16 Pct Recovery = 98% Analysis Date = 04/28/16 Pct Recovery = 98% Analysis Date = 04/26/16 Pct Recovery = 98% Analysis Date = 04/26/16 Pct Recovery = 98% Analysis Date = 04/24/16 Pct Recovery = 98% Analysis Date = 04/24/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/22/16 Pct Recovery = 98% Analysis Date = 04/19/16 Pct Recovery = 98% Analysis Date = 04/19/16 Pct Recovery = 98% Analysis Date = 04/17/16 Pct Recovery = 97% Analysis Date = 04/17/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/15/16 Pct Recovery = 97% Analysis Date = 04/12/16 Pct Recovery = 97% Analysis Date = 04/12/16 Pct Recovery = 97% Analysis Date = 04/10/16 Pct Recovery = 97% Analysis Date = 04/10/16 Pct Recovery = 97% Analysis Date = 04/08/16 Pct Recovery = 97% Analysis Date = 04/08/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/06/16 Pct Recovery = 97% Analysis Date = 04/03/16 Pct Recovery = 97% Analysis Date = 04/03/16 Pct Recovery = 97% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 04/01/16 Pct Recovery = 96% Analysis Date = 03/30/16 Pct Recovery = 96% Analysis Date = 03/30/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/27/16 Pct Recovery = 96% Analysis Date = 03/25/16 Pct Recovery = 96% Analysis Date = 03/25/16 Pct Recovery = 96% Analysis Date = 03/23/16 Pct Recovery = 96% Analysis Date = 03/23/16 Pct Recovery = 96% Analysis Date = 03/21/16 Pct Recovery = 95% Analysis Date = 03/21/16 Pct Recovery = 95% Analysis Date = 03/18/16 Pct Recovery = 95% Analysis Date = 03/18/16 Pct Recovery = 95% Analysis Date = 03/16/16 Pct Recovery = 95% Analysis Date = 03/16/16 Pct Recovery = 95% Analysis Date = 03/14/16 Pct Recovery = 95% Analysis Date = 03/14/16 Pct Recovery = 95% Analysis Date = 03/11/16 Pct Recovery = 95% Analysis Date = 03/11/16 Pct Recovery = 95% Analysis Date = 03/09/16 Pct Recovery = 95% Analysis Date = 03/09/16 Pct Recovery = 95% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/07/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 03/05/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 03/02/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/29/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/27/16 Pct Recovery = 94% Analysis Date = 02/24/16 Pct Recovery = 93% Analysis Date = 02/24/16 Pct Recovery = 93% Analysis Date = 02/22/16 Pct Recovery = 93% Analysis Date = 02/22/16 Pct Recovery = 93% Analysis Date = 02/20/16 Pct Recovery = 93% Analysis Date = 02/20/16 Pct Recovery = 93% Analysis Date = 02/18/16 Pct Recovery = 93% Analysis Date = 02/18/16 Pct Recovery = 93% Analysis Date = 02/15/16 Pct Recovery = 93% Analysis Date = 02/15/16 Pct Recovery = 93% Analysis Date = 02/13/16 Pct Recovery = 92% Analysis Date = 02/13/16 Pct Recovery = 92% Analysis Date = 02/11/16 Pct Recovery = 92% Analysis Date = 02/11/16 Pct Recovery = 92% Analysis Date = 02/09/16 Pct Recovery = 92% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
SIMAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 98% 19% 94% 18%
Total 18 98% 19% 94% 18%

Sample Statistics
SIMAZINE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
TEBUCONAZOLE
METHOD: 2033 , TESTIDCODE: 62852GCM14

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 54% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 61% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 83% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 53% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 61% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 64% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 55% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 66% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 71% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 82% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 52% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 62% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 48% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 78% Analysis Date = 05/02/17 Pct Recovery = 82% Analysis Date = 04/30/17 Pct Recovery = 82% Analysis Date = 04/30/17 Pct Recovery = 82% Analysis Date = 04/28/17 Pct Recovery = 81% Analysis Date = 04/28/17 Pct Recovery = 81% Analysis Date = 04/26/17 Pct Recovery = 81% Analysis Date = 04/26/17 Pct Recovery = 81% Analysis Date = 04/24/17 Pct Recovery = 80% Analysis Date = 04/24/17 Pct Recovery = 80% Analysis Date = 04/21/17 Pct Recovery = 80% Analysis Date = 04/21/17 Pct Recovery = 80% Analysis Date = 04/19/17 Pct Recovery = 79% Analysis Date = 04/19/17 Pct Recovery = 79% Analysis Date = 04/17/17 Pct Recovery = 79% Analysis Date = 04/17/17 Pct Recovery = 79% Analysis Date = 04/15/17 Pct Recovery = 78% Analysis Date = 04/15/17 Pct Recovery = 78% Analysis Date = 04/12/17 Pct Recovery = 78% Analysis Date = 04/12/17 Pct Recovery = 78% Analysis Date = 04/10/17 Pct Recovery = 77% Analysis Date = 04/10/17 Pct Recovery = 77% Analysis Date = 04/08/17 Pct Recovery = 77% Analysis Date = 04/08/17 Pct Recovery = 77% Analysis Date = 04/06/17 Pct Recovery = 76% Analysis Date = 04/06/17 Pct Recovery = 76% Analysis Date = 04/03/17 Pct Recovery = 76% Analysis Date = 04/03/17 Pct Recovery = 76% Analysis Date = 04/01/17 Pct Recovery = 75% Analysis Date = 04/01/17 Pct Recovery = 75% Analysis Date = 03/30/17 Pct Recovery = 75% Analysis Date = 03/30/17 Pct Recovery = 75% Analysis Date = 03/28/17 Pct Recovery = 74% Analysis Date = 03/28/17 Pct Recovery = 74% Analysis Date = 03/25/17 Pct Recovery = 73% Analysis Date = 03/25/17 Pct Recovery = 73% Analysis Date = 03/23/17 Pct Recovery = 73% Analysis Date = 03/23/17 Pct Recovery = 73% Analysis Date = 03/21/17 Pct Recovery = 72% Analysis Date = 03/21/17 Pct Recovery = 72% Analysis Date = 03/19/17 Pct Recovery = 72% Analysis Date = 03/19/17 Pct Recovery = 72% Analysis Date = 03/16/17 Pct Recovery = 71% Analysis Date = 03/16/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 71% Analysis Date = 03/14/17 Pct Recovery = 71% Analysis Date = 03/12/17 Pct Recovery = 70% Analysis Date = 03/12/17 Pct Recovery = 70% Analysis Date = 03/10/17 Pct Recovery = 70% Analysis Date = 03/10/17 Pct Recovery = 70% Analysis Date = 03/07/17 Pct Recovery = 69% Analysis Date = 03/07/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/05/17 Pct Recovery = 69% Analysis Date = 03/03/17 Pct Recovery = 68% Analysis Date = 03/03/17 Pct Recovery = 68% Analysis Date = 03/01/17 Pct Recovery = 68% Analysis Date = 03/01/17 Pct Recovery = 68% Analysis Date = 02/26/17 Pct Recovery = 67% Analysis Date = 02/26/17 Pct Recovery = 67% Analysis Date = 02/24/17 Pct Recovery = 67% Analysis Date = 02/24/17 Pct Recovery = 67% Analysis Date = 02/22/17 Pct Recovery = 66% Analysis Date = 02/22/17 Pct Recovery = 66% Analysis Date = 02/20/17 Pct Recovery = 66% Analysis Date = 02/20/17 Pct Recovery = 66% Analysis Date = 02/17/17 Pct Recovery = 65% Analysis Date = 02/17/17 Pct Recovery = 65% Analysis Date = 02/15/17 Pct Recovery = 65% Analysis Date = 02/15/17 Pct Recovery = 65% Analysis Date = 02/13/17 Pct Recovery = 64% Analysis Date = 02/13/17 Pct Recovery = 64% Analysis Date = 02/11/17 Pct Recovery = 64% Analysis Date = 02/11/17 Pct Recovery = 64% Analysis Date = 02/08/17 Pct Recovery = 63% Analysis Date = 02/08/17 Pct Recovery = 63% Analysis Date = 02/06/17 Pct Recovery = 63% Analysis Date = 02/06/17 Pct Recovery = 63% Analysis Date = 02/04/17 Pct Recovery = 63% Analysis Date = 02/04/17 Pct Recovery = 63% Analysis Date = 02/02/17 Pct Recovery = 62% Analysis Date = 02/02/17 Pct Recovery = 62% Analysis Date = 01/30/17 Pct Recovery = 62% Analysis Date = 01/30/17 Pct Recovery = 62% Analysis Date = 01/28/17 Pct Recovery = 61% Analysis Date = 01/28/17 Pct Recovery = 61% Analysis Date = 01/26/17 Pct Recovery = 61% Analysis Date = 01/26/17 Pct Recovery = 61% Analysis Date = 01/24/17 Pct Recovery = 60% Analysis Date = 01/24/17 Pct Recovery = 60% Analysis Date = 01/21/17 Pct Recovery = 60% Analysis Date = 01/21/17 Pct Recovery = 60% Analysis Date = 01/19/17 Pct Recovery = 60% Analysis Date = 01/19/17 Pct Recovery = 60% Analysis Date = 01/17/17 Pct Recovery = 59% Analysis Date = 01/17/17 Pct Recovery = 59% Analysis Date = 01/15/17 Pct Recovery = 59% Analysis Date = 01/15/17 Pct Recovery = 59% Analysis Date = 01/12/17 Pct Recovery = 58% Analysis Date = 01/12/17 Pct Recovery = 58% Analysis Date = 01/10/17 Pct Recovery = 58% Analysis Date = 01/10/17 Pct Recovery = 58% Analysis Date = 01/08/17 Pct Recovery = 57% Analysis Date = 01/08/17 Pct Recovery = 57% Analysis Date = 01/06/17 Pct Recovery = 57% Analysis Date = 01/06/17 Pct Recovery = 57% Analysis Date = 01/04/17 Pct Recovery = 56% Analysis Date = 01/04/17 Pct Recovery = 56% Analysis Date = 01/01/17 Pct Recovery = 56% Analysis Date = 01/01/17 Pct Recovery = 56% Analysis Date = 12/30/16 Pct Recovery = 56% Analysis Date = 12/30/16 Pct Recovery = 56% Analysis Date = 12/28/16 Pct Recovery = 55% Analysis Date = 12/28/16 Pct Recovery = 55% Analysis Date = 12/26/16 Pct Recovery = 55% Analysis Date = 12/26/16 Pct Recovery = 55% Analysis Date = 12/23/16 Pct Recovery = 54% Analysis Date = 12/23/16 Pct Recovery = 54% Analysis Date = 12/21/16 Pct Recovery = 54% Analysis Date = 12/21/16 Pct Recovery = 54% Analysis Date = 12/19/16 Pct Recovery = 54% Analysis Date = 12/19/16 Pct Recovery = 54% Analysis Date = 12/17/16 Pct Recovery = 54% Analysis Date = 12/17/16 Pct Recovery = 54% Analysis Date = 12/14/16 Pct Recovery = 54% Analysis Date = 12/14/16 Pct Recovery = 54% Analysis Date = 12/12/16 Pct Recovery = 54% Analysis Date = 12/12/16 Pct Recovery = 54% Analysis Date = 12/10/16 Pct Recovery = 54% Analysis Date = 12/10/16 Pct Recovery = 54% Analysis Date = 12/08/16 Pct Recovery = 54% Analysis Date = 12/08/16 Pct Recovery = 54% Analysis Date = 12/05/16 Pct Recovery = 54% Analysis Date = 12/05/16 Pct Recovery = 54% Analysis Date = 12/03/16 Pct Recovery = 54% Analysis Date = 12/03/16 Pct Recovery = 54% Analysis Date = 12/01/16 Pct Recovery = 54% Analysis Date = 12/01/16 Pct Recovery = 54% Analysis Date = 11/29/16 Pct Recovery = 55% Analysis Date = 11/29/16 Pct Recovery = 55% Analysis Date = 11/26/16 Pct Recovery = 55% Analysis Date = 11/26/16 Pct Recovery = 55% Analysis Date = 11/24/16 Pct Recovery = 55% Analysis Date = 11/24/16 Pct Recovery = 55% Analysis Date = 11/22/16 Pct Recovery = 55% Analysis Date = 11/22/16 Pct Recovery = 55% Analysis Date = 11/20/16 Pct Recovery = 55% Analysis Date = 11/20/16 Pct Recovery = 55% Analysis Date = 11/17/16 Pct Recovery = 55% Analysis Date = 11/17/16 Pct Recovery = 55% Analysis Date = 11/15/16 Pct Recovery = 55% Analysis Date = 11/15/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/13/16 Pct Recovery = 55% Analysis Date = 11/11/16 Pct Recovery = 55% Analysis Date = 11/11/16 Pct Recovery = 55% Analysis Date = 11/08/16 Pct Recovery = 56% Analysis Date = 11/08/16 Pct Recovery = 56% Analysis Date = 11/06/16 Pct Recovery = 56% Analysis Date = 11/06/16 Pct Recovery = 56% Analysis Date = 11/04/16 Pct Recovery = 56% Analysis Date = 11/04/16 Pct Recovery = 56% Analysis Date = 11/02/16 Pct Recovery = 56% Analysis Date = 11/02/16 Pct Recovery = 56% Analysis Date = 10/30/16 Pct Recovery = 56% Analysis Date = 10/30/16 Pct Recovery = 56% Analysis Date = 10/28/16 Pct Recovery = 56% Analysis Date = 10/28/16 Pct Recovery = 56% Analysis Date = 10/26/16 Pct Recovery = 56% Analysis Date = 10/26/16 Pct Recovery = 56% Analysis Date = 10/24/16 Pct Recovery = 56% Analysis Date = 10/24/16 Pct Recovery = 56% Analysis Date = 10/21/16 Pct Recovery = 56% Analysis Date = 10/21/16 Pct Recovery = 56% Analysis Date = 10/19/16 Pct Recovery = 56% Analysis Date = 10/19/16 Pct Recovery = 56% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 57% Analysis Date = 10/10/16 Pct Recovery = 57% Analysis Date = 10/10/16 Pct Recovery = 57% Analysis Date = 10/08/16 Pct Recovery = 57% Analysis Date = 10/08/16 Pct Recovery = 57% Analysis Date = 10/06/16 Pct Recovery = 57% Analysis Date = 10/06/16 Pct Recovery = 57% Analysis Date = 10/03/16 Pct Recovery = 57% Analysis Date = 10/03/16 Pct Recovery = 57% Analysis Date = 10/01/16 Pct Recovery = 57% Analysis Date = 10/01/16 Pct Recovery = 57% Analysis Date = 09/29/16 Pct Recovery = 57% Analysis Date = 09/29/16 Pct Recovery = 57% Analysis Date = 09/27/16 Pct Recovery = 58% Analysis Date = 09/27/16 Pct Recovery = 58% Analysis Date = 09/24/16 Pct Recovery = 58% Analysis Date = 09/24/16 Pct Recovery = 58% Analysis Date = 09/22/16 Pct Recovery = 58% Analysis Date = 09/22/16 Pct Recovery = 58% Analysis Date = 09/20/16 Pct Recovery = 58% Analysis Date = 09/20/16 Pct Recovery = 58% Analysis Date = 09/18/16 Pct Recovery = 58% Analysis Date = 09/18/16 Pct Recovery = 58% Analysis Date = 09/16/16 Pct Recovery = 58% Analysis Date = 09/16/16 Pct Recovery = 58% Analysis Date = 09/13/16 Pct Recovery = 58% Analysis Date = 09/13/16 Pct Recovery = 58% Analysis Date = 09/11/16 Pct Recovery = 58% Analysis Date = 09/11/16 Pct Recovery = 58% Analysis Date = 09/09/16 Pct Recovery = 58% Analysis Date = 09/09/16 Pct Recovery = 58% Analysis Date = 09/07/16 Pct Recovery = 59% Analysis Date = 09/07/16 Pct Recovery = 59% Analysis Date = 09/04/16 Pct Recovery = 59% Analysis Date = 09/04/16 Pct Recovery = 59% Analysis Date = 09/02/16 Pct Recovery = 59% Analysis Date = 09/02/16 Pct Recovery = 59% Analysis Date = 08/31/16 Pct Recovery = 59% Analysis Date = 08/31/16 Pct Recovery = 59% Analysis Date = 08/29/16 Pct Recovery = 59% Analysis Date = 08/29/16 Pct Recovery = 59% Analysis Date = 08/26/16 Pct Recovery = 59% Analysis Date = 08/26/16 Pct Recovery = 59% Analysis Date = 08/24/16 Pct Recovery = 59% Analysis Date = 08/24/16 Pct Recovery = 59% Analysis Date = 08/22/16 Pct Recovery = 60% Analysis Date = 08/22/16 Pct Recovery = 60% Analysis Date = 08/20/16 Pct Recovery = 60% Analysis Date = 08/20/16 Pct Recovery = 60% Analysis Date = 08/17/16 Pct Recovery = 60% Analysis Date = 08/17/16 Pct Recovery = 60% Analysis Date = 08/15/16 Pct Recovery = 60% Analysis Date = 08/15/16 Pct Recovery = 60% Analysis Date = 08/13/16 Pct Recovery = 60% Analysis Date = 08/13/16 Pct Recovery = 60% Analysis Date = 08/11/16 Pct Recovery = 61% Analysis Date = 08/11/16 Pct Recovery = 61% Analysis Date = 08/08/16 Pct Recovery = 61% Analysis Date = 08/08/16 Pct Recovery = 61% Analysis Date = 08/06/16 Pct Recovery = 61% Analysis Date = 08/06/16 Pct Recovery = 61% Analysis Date = 08/04/16 Pct Recovery = 61% Analysis Date = 08/04/16 Pct Recovery = 61% Analysis Date = 08/02/16 Pct Recovery = 61% Analysis Date = 08/02/16 Pct Recovery = 61% Analysis Date = 07/30/16 Pct Recovery = 62% Analysis Date = 07/30/16 Pct Recovery = 62% Analysis Date = 07/28/16 Pct Recovery = 62% Analysis Date = 07/28/16 Pct Recovery = 62% Analysis Date = 07/26/16 Pct Recovery = 62% Analysis Date = 07/26/16 Pct Recovery = 62% Analysis Date = 07/24/16 Pct Recovery = 62% Analysis Date = 07/24/16 Pct Recovery = 62% Analysis Date = 07/21/16 Pct Recovery = 62% Analysis Date = 07/21/16 Pct Recovery = 62% Analysis Date = 07/19/16 Pct Recovery = 63% Analysis Date = 07/19/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 63% Analysis Date = 07/17/16 Pct Recovery = 63% Analysis Date = 07/15/16 Pct Recovery = 63% Analysis Date = 07/15/16 Pct Recovery = 63% Analysis Date = 07/12/16 Pct Recovery = 63% Analysis Date = 07/12/16 Pct Recovery = 63% Analysis Date = 07/10/16 Pct Recovery = 63% Analysis Date = 07/10/16 Pct Recovery = 63% Analysis Date = 07/08/16 Pct Recovery = 63% Analysis Date = 07/08/16 Pct Recovery = 63% Analysis Date = 07/06/16 Pct Recovery = 64% Analysis Date = 07/06/16 Pct Recovery = 64% Analysis Date = 07/03/16 Pct Recovery = 64% Analysis Date = 07/03/16 Pct Recovery = 64% Analysis Date = 07/01/16 Pct Recovery = 64% Analysis Date = 07/01/16 Pct Recovery = 64% Analysis Date = 06/29/16 Pct Recovery = 64% Analysis Date = 06/29/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/27/16 Pct Recovery = 64% Analysis Date = 06/24/16 Pct Recovery = 65% Analysis Date = 06/24/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 65% Analysis Date = 06/15/16 Pct Recovery = 65% Analysis Date = 06/15/16 Pct Recovery = 65% Analysis Date = 06/13/16 Pct Recovery = 66% Analysis Date = 06/13/16 Pct Recovery = 66% Analysis Date = 06/11/16 Pct Recovery = 66% Analysis Date = 06/11/16 Pct Recovery = 66% Analysis Date = 06/09/16 Pct Recovery = 66% Analysis Date = 06/09/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/02/16 Pct Recovery = 67% Analysis Date = 06/02/16 Pct Recovery = 67% Analysis Date = 05/31/16 Pct Recovery = 67% Analysis Date = 05/31/16 Pct Recovery = 67% Analysis Date = 05/29/16 Pct Recovery = 67% Analysis Date = 05/29/16 Pct Recovery = 67% Analysis Date = 05/26/16 Pct Recovery = 67% Analysis Date = 05/26/16 Pct Recovery = 67% Analysis Date = 05/24/16 Pct Recovery = 67% Analysis Date = 05/24/16 Pct Recovery = 67% Analysis Date = 05/22/16 Pct Recovery = 67% Analysis Date = 05/22/16 Pct Recovery = 67% Analysis Date = 05/20/16 Pct Recovery = 66% Analysis Date = 05/20/16 Pct Recovery = 66% Analysis Date = 05/17/16 Pct Recovery = 66% Analysis Date = 05/17/16 Pct Recovery = 66% Analysis Date = 05/15/16 Pct Recovery = 66% Analysis Date = 05/15/16 Pct Recovery = 66% Analysis Date = 05/13/16 Pct Recovery = 66% Analysis Date = 05/13/16 Pct Recovery = 66% Analysis Date = 05/11/16 Pct Recovery = 66% Analysis Date = 05/11/16 Pct Recovery = 66% Analysis Date = 05/08/16 Pct Recovery = 66% Analysis Date = 05/08/16 Pct Recovery = 66% Analysis Date = 05/06/16 Pct Recovery = 66% Analysis Date = 05/06/16 Pct Recovery = 66% Analysis Date = 05/04/16 Pct Recovery = 65% Analysis Date = 05/04/16 Pct Recovery = 65% Analysis Date = 05/02/16 Pct Recovery = 65% Analysis Date = 05/02/16 Pct Recovery = 65% Analysis Date = 04/29/16 Pct Recovery = 65% Analysis Date = 04/29/16 Pct Recovery = 65% Analysis Date = 04/27/16 Pct Recovery = 65% Analysis Date = 04/27/16 Pct Recovery = 65% Analysis Date = 04/25/16 Pct Recovery = 65% Analysis Date = 04/25/16 Pct Recovery = 65% Analysis Date = 04/23/16 Pct Recovery = 65% Analysis Date = 04/23/16 Pct Recovery = 65% Analysis Date = 04/20/16 Pct Recovery = 65% Analysis Date = 04/20/16 Pct Recovery = 65% Analysis Date = 04/18/16 Pct Recovery = 65% Analysis Date = 04/18/16 Pct Recovery = 65% Analysis Date = 04/16/16 Pct Recovery = 65% Analysis Date = 04/16/16 Pct Recovery = 65% Analysis Date = 04/14/16 Pct Recovery = 65% Analysis Date = 04/14/16 Pct Recovery = 65% Analysis Date = 04/11/16 Pct Recovery = 65% Analysis Date = 04/11/16 Pct Recovery = 65% Analysis Date = 04/09/16 Pct Recovery = 65% Analysis Date = 04/09/16 Pct Recovery = 65% Analysis Date = 04/07/16 Pct Recovery = 65% Analysis Date = 04/07/16 Pct Recovery = 65% Analysis Date = 04/05/16 Pct Recovery = 65% Analysis Date = 04/05/16 Pct Recovery = 65% Analysis Date = 04/02/16 Pct Recovery = 65% Analysis Date = 04/02/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/31/16 Pct Recovery = 65% Analysis Date = 03/29/16 Pct Recovery = 64% Analysis Date = 03/29/16 Pct Recovery = 64% Analysis Date = 03/27/16 Pct Recovery = 64% Analysis Date = 03/27/16 Pct Recovery = 64% Analysis Date = 03/24/16 Pct Recovery = 64% Analysis Date = 03/24/16 Pct Recovery = 64% Analysis Date = 03/22/16 Pct Recovery = 64% Analysis Date = 03/22/16 Pct Recovery = 64% Analysis Date = 03/20/16 Pct Recovery = 64% Analysis Date = 03/20/16 Pct Recovery = 64% Analysis Date = 03/18/16 Pct Recovery = 64% Analysis Date = 03/18/16 Pct Recovery = 64% Analysis Date = 03/15/16 Pct Recovery = 64% Analysis Date = 03/15/16 Pct Recovery = 64% Analysis Date = 03/13/16 Pct Recovery = 64% Analysis Date = 03/13/16 Pct Recovery = 64% Analysis Date = 03/11/16 Pct Recovery = 64% Analysis Date = 03/11/16 Pct Recovery = 64% Analysis Date = 03/09/16 Pct Recovery = 64% Analysis Date = 03/09/16 Pct Recovery = 64% Analysis Date = 03/06/16 Pct Recovery = 64% Analysis Date = 03/06/16 Pct Recovery = 64% Analysis Date = 03/04/16 Pct Recovery = 64% Analysis Date = 03/04/16 Pct Recovery = 64% Analysis Date = 03/02/16 Pct Recovery = 64% Analysis Date = 03/02/16 Pct Recovery = 64% Analysis Date = 02/29/16 Pct Recovery = 64% Analysis Date = 02/29/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/26/16 Pct Recovery = 64% Analysis Date = 02/24/16 Pct Recovery = 64% Analysis Date = 02/24/16 Pct Recovery = 64% Analysis Date = 02/22/16 Pct Recovery = 64% Analysis Date = 02/22/16 Pct Recovery = 64% Analysis Date = 02/20/16 Pct Recovery = 64% Analysis Date = 02/20/16 Pct Recovery = 64% Analysis Date = 02/17/16 Pct Recovery = 64% Analysis Date = 02/17/16 Pct Recovery = 64% Analysis Date = 02/15/16 Pct Recovery = 64% Analysis Date = 02/15/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/13/16 Pct Recovery = 64% Analysis Date = 02/11/16 Pct Recovery = 64% Analysis Date = 02/11/16 Pct Recovery = 64% Analysis Date = 02/09/16 Pct Recovery = 64% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUCONAZOLE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 65% 10% 65% 12%
Total 18 65% 10% 65% 12%

Sample Statistics
TEBUCONAZOLE

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 3 17% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
TEBUTHIURON
METHOD: 2033 , TESTIDCODE: 82670GCM35

Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 244% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 226% Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 98% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 142% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 105% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 105% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 129% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 74% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 126% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 110% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 123% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 124% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 103% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 114% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 109% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 99% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 131% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 124% Analysis Date = 05/10/17 Pct Recovery = 122% Analysis Date = 05/08/17 Pct Recovery = 122% Analysis Date = 05/08/17 Pct Recovery = 122% Analysis Date = 05/06/17 Pct Recovery = 122% Analysis Date = 05/06/17 Pct Recovery = 122% Analysis Date = 05/04/17 Pct Recovery = 122% Analysis Date = 05/04/17 Pct Recovery = 122% Analysis Date = 05/02/17 Pct Recovery = 121% Analysis Date = 05/02/17 Pct Recovery = 121% Analysis Date = 04/30/17 Pct Recovery = 121% Analysis Date = 04/30/17 Pct Recovery = 121% Analysis Date = 04/27/17 Pct Recovery = 121% Analysis Date = 04/27/17 Pct Recovery = 121% Analysis Date = 04/25/17 Pct Recovery = 121% Analysis Date = 04/25/17 Pct Recovery = 121% Analysis Date = 04/23/17 Pct Recovery = 121% Analysis Date = 04/23/17 Pct Recovery = 121% Analysis Date = 04/21/17 Pct Recovery = 121% Analysis Date = 04/21/17 Pct Recovery = 121% Analysis Date = 04/19/17 Pct Recovery = 121% Analysis Date = 04/19/17 Pct Recovery = 121% Analysis Date = 04/17/17 Pct Recovery = 120% Analysis Date = 04/17/17 Pct Recovery = 120% Analysis Date = 04/14/17 Pct Recovery = 120% Analysis Date = 04/14/17 Pct Recovery = 120% Analysis Date = 04/12/17 Pct Recovery = 120% Analysis Date = 04/12/17 Pct Recovery = 120% Analysis Date = 04/10/17 Pct Recovery = 120% Analysis Date = 04/10/17 Pct Recovery = 120% Analysis Date = 04/08/17 Pct Recovery = 120% Analysis Date = 04/08/17 Pct Recovery = 120% Analysis Date = 04/06/17 Pct Recovery = 120% Analysis Date = 04/06/17 Pct Recovery = 120% Analysis Date = 04/04/17 Pct Recovery = 120% Analysis Date = 04/04/17 Pct Recovery = 120% Analysis Date = 04/01/17 Pct Recovery = 119% Analysis Date = 04/01/17 Pct Recovery = 119% Analysis Date = 03/30/17 Pct Recovery = 119% Analysis Date = 03/30/17 Pct Recovery = 119% Analysis Date = 03/28/17 Pct Recovery = 119% Analysis Date = 03/28/17 Pct Recovery = 119% Analysis Date = 03/26/17 Pct Recovery = 119% Analysis Date = 03/26/17 Pct Recovery = 119% Analysis Date = 03/24/17 Pct Recovery = 119% Analysis Date = 03/24/17 Pct Recovery = 119% Analysis Date = 03/21/17 Pct Recovery = 119% Analysis Date = 03/21/17 Pct Recovery = 119% Analysis Date = 03/19/17 Pct Recovery = 119% Analysis Date = 03/19/17 Pct Recovery = 119% Analysis Date = 03/17/17 Pct Recovery = 118% Analysis Date = 03/17/17 Pct Recovery = 118% Analysis Date = 03/15/17 Pct Recovery = 118% Analysis Date = 03/15/17 Pct Recovery = 118% Analysis Date = 03/13/17 Pct Recovery = 118% Analysis Date = 03/13/17 Pct Recovery = 118% Analysis Date = 03/11/17 Pct Recovery = 118% Analysis Date = 03/11/17 Pct Recovery = 118% Analysis Date = 03/08/17 Pct Recovery = 118% Analysis Date = 03/08/17 Pct Recovery = 118% Analysis Date = 03/06/17 Pct Recovery = 117% Analysis Date = 03/06/17 Pct Recovery = 117% Analysis Date = 03/04/17 Pct Recovery = 117% Analysis Date = 03/04/17 Pct Recovery = 117% Analysis Date = 03/02/17 Pct Recovery = 117% Analysis Date = 03/02/17 Pct Recovery = 117% Analysis Date = 02/28/17 Pct Recovery = 117% Analysis Date = 02/28/17 Pct Recovery = 117% Analysis Date = 02/26/17 Pct Recovery = 117% Analysis Date = 02/26/17 Pct Recovery = 117% Analysis Date = 02/23/17 Pct Recovery = 116% Analysis Date = 02/23/17 Pct Recovery = 116% Analysis Date = 02/21/17 Pct Recovery = 116% Analysis Date = 02/21/17 Pct Recovery = 116% Analysis Date = 02/19/17 Pct Recovery = 115% Analysis Date = 02/19/17 Pct Recovery = 115% Analysis Date = 02/17/17 Pct Recovery = 114% Analysis Date = 02/17/17 Pct Recovery = 114% Analysis Date = 02/15/17 Pct Recovery = 113% Analysis Date = 02/15/17 Pct Recovery = 113% Analysis Date = 02/12/17 Pct Recovery = 112% Analysis Date = 02/12/17 Pct Recovery = 112% Analysis Date = 02/10/17 Pct Recovery = 111% Analysis Date = 02/10/17 Pct Recovery = 111% Analysis Date = 02/08/17 Pct Recovery = 110% Analysis Date = 02/08/17 Pct Recovery = 110% Analysis Date = 02/06/17 Pct Recovery = 109% Analysis Date = 02/06/17 Pct Recovery = 109% Analysis Date = 02/04/17 Pct Recovery = 109% Analysis Date = 02/04/17 Pct Recovery = 109% Analysis Date = 02/02/17 Pct Recovery = 108% Analysis Date = 02/02/17 Pct Recovery = 108% Analysis Date = 01/30/17 Pct Recovery = 107% Analysis Date = 01/30/17 Pct Recovery = 107% Analysis Date = 01/28/17 Pct Recovery = 106% Analysis Date = 01/28/17 Pct Recovery = 106% Analysis Date = 01/26/17 Pct Recovery = 105% Analysis Date = 01/26/17 Pct Recovery = 105% Analysis Date = 01/24/17 Pct Recovery = 104% Analysis Date = 01/24/17 Pct Recovery = 104% Analysis Date = 01/22/17 Pct Recovery = 103% Analysis Date = 01/22/17 Pct Recovery = 103% Analysis Date = 01/20/17 Pct Recovery = 102% Analysis Date = 01/20/17 Pct Recovery = 102% Analysis Date = 01/17/17 Pct Recovery = 101% Analysis Date = 01/17/17 Pct Recovery = 101% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/15/17 Pct Recovery = 102% Analysis Date = 01/13/17 Pct Recovery = 102% Analysis Date = 01/13/17 Pct Recovery = 102% Analysis Date = 01/11/17 Pct Recovery = 103% Analysis Date = 01/11/17 Pct Recovery = 103% Analysis Date = 01/09/17 Pct Recovery = 104% Analysis Date = 01/09/17 Pct Recovery = 104% Analysis Date = 01/07/17 Pct Recovery = 104% Analysis Date = 01/07/17 Pct Recovery = 104% Analysis Date = 01/04/17 Pct Recovery = 105% Analysis Date = 01/04/17 Pct Recovery = 105% Analysis Date = 01/02/17 Pct Recovery = 106% Analysis Date = 01/02/17 Pct Recovery = 106% Analysis Date = 12/31/16 Pct Recovery = 106% Analysis Date = 12/31/16 Pct Recovery = 106% Analysis Date = 12/29/16 Pct Recovery = 107% Analysis Date = 12/29/16 Pct Recovery = 107% Analysis Date = 12/27/16 Pct Recovery = 108% Analysis Date = 12/27/16 Pct Recovery = 108% Analysis Date = 12/24/16 Pct Recovery = 108% Analysis Date = 12/24/16 Pct Recovery = 108% Analysis Date = 12/22/16 Pct Recovery = 109% Analysis Date = 12/22/16 Pct Recovery = 109% Analysis Date = 12/20/16 Pct Recovery = 110% Analysis Date = 12/20/16 Pct Recovery = 110% Analysis Date = 12/18/16 Pct Recovery = 110% Analysis Date = 12/18/16 Pct Recovery = 110% Analysis Date = 12/16/16 Pct Recovery = 111% Analysis Date = 12/16/16 Pct Recovery = 111% Analysis Date = 12/14/16 Pct Recovery = 112% Analysis Date = 12/14/16 Pct Recovery = 112% Analysis Date = 12/11/16 Pct Recovery = 112% Analysis Date = 12/11/16 Pct Recovery = 112% Analysis Date = 12/09/16 Pct Recovery = 113% Analysis Date = 12/09/16 Pct Recovery = 113% Analysis Date = 12/07/16 Pct Recovery = 114% Analysis Date = 12/07/16 Pct Recovery = 114% Analysis Date = 12/05/16 Pct Recovery = 114% Analysis Date = 12/05/16 Pct Recovery = 114% Analysis Date = 12/03/16 Pct Recovery = 115% Analysis Date = 12/03/16 Pct Recovery = 115% Analysis Date = 12/01/16 Pct Recovery = 116% Analysis Date = 12/01/16 Pct Recovery = 116% Analysis Date = 11/28/16 Pct Recovery = 116% Analysis Date = 11/28/16 Pct Recovery = 116% Analysis Date = 11/26/16 Pct Recovery = 117% Analysis Date = 11/26/16 Pct Recovery = 117% Analysis Date = 11/24/16 Pct Recovery = 118% Analysis Date = 11/24/16 Pct Recovery = 118% Analysis Date = 11/22/16 Pct Recovery = 118% Analysis Date = 11/22/16 Pct Recovery = 118% Analysis Date = 11/20/16 Pct Recovery = 119% Analysis Date = 11/20/16 Pct Recovery = 119% Analysis Date = 11/17/16 Pct Recovery = 119% Analysis Date = 11/17/16 Pct Recovery = 119% Analysis Date = 11/15/16 Pct Recovery = 120% Analysis Date = 11/15/16 Pct Recovery = 120% Analysis Date = 11/13/16 Pct Recovery = 121% Analysis Date = 11/13/16 Pct Recovery = 121% Analysis Date = 11/11/16 Pct Recovery = 121% Analysis Date = 11/11/16 Pct Recovery = 121% Analysis Date = 11/09/16 Pct Recovery = 122% Analysis Date = 11/09/16 Pct Recovery = 122% Analysis Date = 11/07/16 Pct Recovery = 123% Analysis Date = 11/07/16 Pct Recovery = 123% Analysis Date = 11/04/16 Pct Recovery = 123% Analysis Date = 11/04/16 Pct Recovery = 123% Analysis Date = 11/02/16 Pct Recovery = 124% Analysis Date = 11/02/16 Pct Recovery = 124% Analysis Date = 10/31/16 Pct Recovery = 125% Analysis Date = 10/31/16 Pct Recovery = 125% Analysis Date = 10/29/16 Pct Recovery = 125% Analysis Date = 10/29/16 Pct Recovery = 125% Analysis Date = 10/27/16 Pct Recovery = 126% Analysis Date = 10/27/16 Pct Recovery = 126% Analysis Date = 10/25/16 Pct Recovery = 127% Analysis Date = 10/25/16 Pct Recovery = 127% Analysis Date = 10/22/16 Pct Recovery = 127% Analysis Date = 10/22/16 Pct Recovery = 127% Analysis Date = 10/20/16 Pct Recovery = 128% Analysis Date = 10/20/16 Pct Recovery = 128% Analysis Date = 10/18/16 Pct Recovery = 129% Analysis Date = 10/18/16 Pct Recovery = 129% Analysis Date = 10/16/16 Pct Recovery = 129% Analysis Date = 10/16/16 Pct Recovery = 129% Analysis Date = 10/14/16 Pct Recovery = 130% Analysis Date = 10/14/16 Pct Recovery = 130% Analysis Date = 10/12/16 Pct Recovery = 131% Analysis Date = 10/12/16 Pct Recovery = 131% Analysis Date = 10/09/16 Pct Recovery = 131% Analysis Date = 10/09/16 Pct Recovery = 131% Analysis Date = 10/07/16 Pct Recovery = 132% Analysis Date = 10/07/16 Pct Recovery = 132% Analysis Date = 10/05/16 Pct Recovery = 133% Analysis Date = 10/05/16 Pct Recovery = 133% Analysis Date = 10/03/16 Pct Recovery = 133% Analysis Date = 10/03/16 Pct Recovery = 133% Analysis Date = 10/01/16 Pct Recovery = 134% Analysis Date = 10/01/16 Pct Recovery = 134% Analysis Date = 09/28/16 Pct Recovery = 135% Analysis Date = 09/28/16 Pct Recovery = 135% Analysis Date = 09/26/16 Pct Recovery = 135% Analysis Date = 09/26/16 Pct Recovery = 135% Analysis Date = 09/24/16 Pct Recovery = 136% Analysis Date = 09/24/16 Pct Recovery = 136% Analysis Date = 09/22/16 Pct Recovery = 137% Analysis Date = 09/22/16 Pct Recovery = 137% Analysis Date = 09/20/16 Pct Recovery = 137% Analysis Date = 09/20/16 Pct Recovery = 137% Analysis Date = 09/18/16 Pct Recovery = 138% Analysis Date = 09/18/16 Pct Recovery = 138% Analysis Date = 09/15/16 Pct Recovery = 139% Analysis Date = 09/15/16 Pct Recovery = 139% Analysis Date = 09/13/16 Pct Recovery = 139% Analysis Date = 09/13/16 Pct Recovery = 139% Analysis Date = 09/11/16 Pct Recovery = 140% Analysis Date = 09/11/16 Pct Recovery = 140% Analysis Date = 09/09/16 Pct Recovery = 141% Analysis Date = 09/09/16 Pct Recovery = 141% Analysis Date = 09/07/16 Pct Recovery = 141% Analysis Date = 09/07/16 Pct Recovery = 141% Analysis Date = 09/05/16 Pct Recovery = 142% Analysis Date = 09/05/16 Pct Recovery = 142% Analysis Date = 09/02/16 Pct Recovery = 143% Analysis Date = 09/02/16 Pct Recovery = 143% Analysis Date = 08/31/16 Pct Recovery = 144% Analysis Date = 08/31/16 Pct Recovery = 144% Analysis Date = 08/29/16 Pct Recovery = 144% Analysis Date = 08/29/16 Pct Recovery = 144% Analysis Date = 08/27/16 Pct Recovery = 145% Analysis Date = 08/27/16 Pct Recovery = 145% Analysis Date = 08/25/16 Pct Recovery = 145% Analysis Date = 08/25/16 Pct Recovery = 145% Analysis Date = 08/22/16 Pct Recovery = 145% Analysis Date = 08/22/16 Pct Recovery = 145% Analysis Date = 08/20/16 Pct Recovery = 145% Analysis Date = 08/20/16 Pct Recovery = 145% Analysis Date = 08/18/16 Pct Recovery = 145% Analysis Date = 08/18/16 Pct Recovery = 145% Analysis Date = 08/16/16 Pct Recovery = 145% Analysis Date = 08/16/16 Pct Recovery = 145% Analysis Date = 08/14/16 Pct Recovery = 144% Analysis Date = 08/14/16 Pct Recovery = 144% Analysis Date = 08/12/16 Pct Recovery = 144% Analysis Date = 08/12/16 Pct Recovery = 144% Analysis Date = 08/09/16 Pct Recovery = 144% Analysis Date = 08/09/16 Pct Recovery = 144% Analysis Date = 08/07/16 Pct Recovery = 144% Analysis Date = 08/07/16 Pct Recovery = 144% Analysis Date = 08/05/16 Pct Recovery = 144% Analysis Date = 08/05/16 Pct Recovery = 144% Analysis Date = 08/03/16 Pct Recovery = 144% Analysis Date = 08/03/16 Pct Recovery = 144% Analysis Date = 08/01/16 Pct Recovery = 143% Analysis Date = 08/01/16 Pct Recovery = 143% Analysis Date = 07/30/16 Pct Recovery = 143% Analysis Date = 07/30/16 Pct Recovery = 143% Analysis Date = 07/27/16 Pct Recovery = 143% Analysis Date = 07/27/16 Pct Recovery = 143% Analysis Date = 07/25/16 Pct Recovery = 143% Analysis Date = 07/25/16 Pct Recovery = 143% Analysis Date = 07/23/16 Pct Recovery = 143% Analysis Date = 07/23/16 Pct Recovery = 143% Analysis Date = 07/21/16 Pct Recovery = 143% Analysis Date = 07/21/16 Pct Recovery = 143% Analysis Date = 07/19/16 Pct Recovery = 142% Analysis Date = 07/19/16 Pct Recovery = 142% Analysis Date = 07/17/16 Pct Recovery = 142% Analysis Date = 07/17/16 Pct Recovery = 142% Analysis Date = 07/14/16 Pct Recovery = 142% Analysis Date = 07/14/16 Pct Recovery = 142% Analysis Date = 07/12/16 Pct Recovery = 142% Analysis Date = 07/12/16 Pct Recovery = 142% Analysis Date = 07/10/16 Pct Recovery = 142% Analysis Date = 07/10/16 Pct Recovery = 142% Analysis Date = 07/08/16 Pct Recovery = 142% Analysis Date = 07/08/16 Pct Recovery = 142% Analysis Date = 07/06/16 Pct Recovery = 141% Analysis Date = 07/06/16 Pct Recovery = 141% Analysis Date = 07/03/16 Pct Recovery = 141% Analysis Date = 07/03/16 Pct Recovery = 141% Analysis Date = 07/01/16 Pct Recovery = 141% Analysis Date = 07/01/16 Pct Recovery = 141% Analysis Date = 06/29/16 Pct Recovery = 141% Analysis Date = 06/29/16 Pct Recovery = 141% Analysis Date = 06/27/16 Pct Recovery = 141% Analysis Date = 06/27/16 Pct Recovery = 141% Analysis Date = 06/25/16 Pct Recovery = 141% Analysis Date = 06/25/16 Pct Recovery = 141% Analysis Date = 06/23/16 Pct Recovery = 140% Analysis Date = 06/23/16 Pct Recovery = 140% Analysis Date = 06/20/16 Pct Recovery = 140% Analysis Date = 06/20/16 Pct Recovery = 140% Analysis Date = 06/18/16 Pct Recovery = 140% Analysis Date = 06/18/16 Pct Recovery = 140% Analysis Date = 06/16/16 Pct Recovery = 140% Analysis Date = 06/16/16 Pct Recovery = 140% Analysis Date = 06/14/16 Pct Recovery = 140% Analysis Date = 06/14/16 Pct Recovery = 140% Analysis Date = 06/12/16 Pct Recovery = 140% Analysis Date = 06/12/16 Pct Recovery = 140% Analysis Date = 06/10/16 Pct Recovery = 139% Analysis Date = 06/10/16 Pct Recovery = 139% Analysis Date = 06/07/16 Pct Recovery = 139% Analysis Date = 06/07/16 Pct Recovery = 139% Analysis Date = 06/05/16 Pct Recovery = 139% Analysis Date = 06/05/16 Pct Recovery = 139% Analysis Date = 06/03/16 Pct Recovery = 139% Analysis Date = 06/03/16 Pct Recovery = 139% Analysis Date = 06/01/16 Pct Recovery = 139% Analysis Date = 06/01/16 Pct Recovery = 139% Analysis Date = 05/30/16 Pct Recovery = 139% Analysis Date = 05/30/16 Pct Recovery = 139% Analysis Date = 05/27/16 Pct Recovery = 139% Analysis Date = 05/27/16 Pct Recovery = 139% Analysis Date = 05/25/16 Pct Recovery = 138% Analysis Date = 05/25/16 Pct Recovery = 138% Analysis Date = 05/23/16 Pct Recovery = 138% Analysis Date = 05/23/16 Pct Recovery = 138% Analysis Date = 05/21/16 Pct Recovery = 138% Analysis Date = 05/21/16 Pct Recovery = 138% Analysis Date = 05/19/16 Pct Recovery = 138% Analysis Date = 05/19/16 Pct Recovery = 138% Analysis Date = 05/17/16 Pct Recovery = 137% Analysis Date = 05/17/16 Pct Recovery = 137% Analysis Date = 05/14/16 Pct Recovery = 136% Analysis Date = 05/14/16 Pct Recovery = 136% Analysis Date = 05/12/16 Pct Recovery = 135% Analysis Date = 05/12/16 Pct Recovery = 135% Analysis Date = 05/10/16 Pct Recovery = 135% Analysis Date = 05/10/16 Pct Recovery = 135% Analysis Date = 05/08/16 Pct Recovery = 134% Analysis Date = 05/08/16 Pct Recovery = 134% Analysis Date = 05/06/16 Pct Recovery = 133% Analysis Date = 05/06/16 Pct Recovery = 133% Analysis Date = 05/04/16 Pct Recovery = 132% Analysis Date = 05/04/16 Pct Recovery = 132% Analysis Date = 05/01/16 Pct Recovery = 131% Analysis Date = 05/01/16 Pct Recovery = 131% Analysis Date = 04/29/16 Pct Recovery = 131% Analysis Date = 04/29/16 Pct Recovery = 131% Analysis Date = 04/27/16 Pct Recovery = 130% Analysis Date = 04/27/16 Pct Recovery = 130% Analysis Date = 04/25/16 Pct Recovery = 129% Analysis Date = 04/25/16 Pct Recovery = 129% Analysis Date = 04/23/16 Pct Recovery = 128% Analysis Date = 04/23/16 Pct Recovery = 128% Analysis Date = 04/21/16 Pct Recovery = 127% Analysis Date = 04/21/16 Pct Recovery = 127% Analysis Date = 04/18/16 Pct Recovery = 127% Analysis Date = 04/18/16 Pct Recovery = 127% Analysis Date = 04/16/16 Pct Recovery = 126% Analysis Date = 04/16/16 Pct Recovery = 126% Analysis Date = 04/14/16 Pct Recovery = 125% Analysis Date = 04/14/16 Pct Recovery = 125% Analysis Date = 04/12/16 Pct Recovery = 124% Analysis Date = 04/12/16 Pct Recovery = 124% Analysis Date = 04/10/16 Pct Recovery = 124% Analysis Date = 04/10/16 Pct Recovery = 124% Analysis Date = 04/07/16 Pct Recovery = 123% Analysis Date = 04/07/16 Pct Recovery = 123% Analysis Date = 04/05/16 Pct Recovery = 122% Analysis Date = 04/05/16 Pct Recovery = 122% Analysis Date = 04/03/16 Pct Recovery = 122% Analysis Date = 04/03/16 Pct Recovery = 122% Analysis Date = 04/01/16 Pct Recovery = 121% Analysis Date = 04/01/16 Pct Recovery = 121% Analysis Date = 03/30/16 Pct Recovery = 121% Analysis Date = 03/30/16 Pct Recovery = 121% Analysis Date = 03/28/16 Pct Recovery = 121% Analysis Date = 03/28/16 Pct Recovery = 121% Analysis Date = 03/25/16 Pct Recovery = 120% Analysis Date = 03/25/16 Pct Recovery = 120% Analysis Date = 03/23/16 Pct Recovery = 120% Analysis Date = 03/23/16 Pct Recovery = 120% Analysis Date = 03/21/16 Pct Recovery = 119% Analysis Date = 03/21/16 Pct Recovery = 119% Analysis Date = 03/19/16 Pct Recovery = 119% Analysis Date = 03/19/16 Pct Recovery = 119% Analysis Date = 03/17/16 Pct Recovery = 118% Analysis Date = 03/17/16 Pct Recovery = 118% Analysis Date = 03/15/16 Pct Recovery = 118% Analysis Date = 03/15/16 Pct Recovery = 118% Analysis Date = 03/12/16 Pct Recovery = 117% Analysis Date = 03/12/16 Pct Recovery = 117% Analysis Date = 03/10/16 Pct Recovery = 117% Analysis Date = 03/10/16 Pct Recovery = 117% Analysis Date = 03/08/16 Pct Recovery = 116% Analysis Date = 03/08/16 Pct Recovery = 116% Analysis Date = 03/06/16 Pct Recovery = 116% Analysis Date = 03/06/16 Pct Recovery = 116% Analysis Date = 03/04/16 Pct Recovery = 115% Analysis Date = 03/04/16 Pct Recovery = 115% Analysis Date = 03/02/16 Pct Recovery = 115% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEBUTHIURON

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 127% 42% 118% 18%
Total 18 127% 42% 118% 18%

Sample Statistics
TEBUTHIURON

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 6 33% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
TEFLUTHRIN
METHOD: 2033 , TESTIDCODE: 61606GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 58% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 73% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 64% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 51% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 40% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 68% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 63% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 51% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 56% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 57% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 59% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 78% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 53% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 58% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 61% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 54% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 52% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 56% Analysis Date = 05/10/17 Pct Recovery = 59% Analysis Date = 05/08/17 Pct Recovery = 59% Analysis Date = 05/08/17 Pct Recovery = 59% Analysis Date = 05/06/17 Pct Recovery = 59% Analysis Date = 05/06/17 Pct Recovery = 59% Analysis Date = 05/04/17 Pct Recovery = 59% Analysis Date = 05/04/17 Pct Recovery = 59% Analysis Date = 05/01/17 Pct Recovery = 59% Analysis Date = 05/01/17 Pct Recovery = 59% Analysis Date = 04/29/17 Pct Recovery = 59% Analysis Date = 04/29/17 Pct Recovery = 59% Analysis Date = 04/27/17 Pct Recovery = 59% Analysis Date = 04/27/17 Pct Recovery = 59% Analysis Date = 04/25/17 Pct Recovery = 59% Analysis Date = 04/25/17 Pct Recovery = 59% Analysis Date = 04/22/17 Pct Recovery = 59% Analysis Date = 04/22/17 Pct Recovery = 59% Analysis Date = 04/20/17 Pct Recovery = 60% Analysis Date = 04/20/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 60% Analysis Date = 04/18/17 Pct Recovery = 60% Analysis Date = 04/15/17 Pct Recovery = 60% Analysis Date = 04/15/17 Pct Recovery = 60% Analysis Date = 04/13/17 Pct Recovery = 60% Analysis Date = 04/13/17 Pct Recovery = 60% Analysis Date = 04/11/17 Pct Recovery = 60% Analysis Date = 04/11/17 Pct Recovery = 60% Analysis Date = 04/09/17 Pct Recovery = 60% Analysis Date = 04/09/17 Pct Recovery = 60% Analysis Date = 04/06/17 Pct Recovery = 60% Analysis Date = 04/06/17 Pct Recovery = 60% Analysis Date = 04/04/17 Pct Recovery = 60% Analysis Date = 04/04/17 Pct Recovery = 60% Analysis Date = 04/02/17 Pct Recovery = 60% Analysis Date = 04/02/17 Pct Recovery = 60% Analysis Date = 03/30/17 Pct Recovery = 60% Analysis Date = 03/30/17 Pct Recovery = 60% Analysis Date = 03/28/17 Pct Recovery = 60% Analysis Date = 03/28/17 Pct Recovery = 60% Analysis Date = 03/26/17 Pct Recovery = 61% Analysis Date = 03/26/17 Pct Recovery = 61% Analysis Date = 03/24/17 Pct Recovery = 61% Analysis Date = 03/24/17 Pct Recovery = 61% Analysis Date = 03/21/17 Pct Recovery = 61% Analysis Date = 03/21/17 Pct Recovery = 61% Analysis Date = 03/19/17 Pct Recovery = 61% Analysis Date = 03/19/17 Pct Recovery = 61% Analysis Date = 03/17/17 Pct Recovery = 61% Analysis Date = 03/17/17 Pct Recovery = 61% Analysis Date = 03/14/17 Pct Recovery = 61% Analysis Date = 03/14/17 Pct Recovery = 61% Analysis Date = 03/12/17 Pct Recovery = 61% Analysis Date = 03/12/17 Pct Recovery = 61% Analysis Date = 03/10/17 Pct Recovery = 61% Analysis Date = 03/10/17 Pct Recovery = 61% Analysis Date = 03/08/17 Pct Recovery = 61% Analysis Date = 03/08/17 Pct Recovery = 61% Analysis Date = 03/05/17 Pct Recovery = 61% Analysis Date = 03/05/17 Pct Recovery = 61% Analysis Date = 03/03/17 Pct Recovery = 61% Analysis Date = 03/03/17 Pct Recovery = 61% Analysis Date = 03/01/17 Pct Recovery = 61% Analysis Date = 03/01/17 Pct Recovery = 61% Analysis Date = 02/26/17 Pct Recovery = 61% Analysis Date = 02/26/17 Pct Recovery = 61% Analysis Date = 02/24/17 Pct Recovery = 61% Analysis Date = 02/24/17 Pct Recovery = 61% Analysis Date = 02/22/17 Pct Recovery = 61% Analysis Date = 02/22/17 Pct Recovery = 61% Analysis Date = 02/20/17 Pct Recovery = 61% Analysis Date = 02/20/17 Pct Recovery = 61% Analysis Date = 02/17/17 Pct Recovery = 60% Analysis Date = 02/17/17 Pct Recovery = 60% Analysis Date = 02/15/17 Pct Recovery = 60% Analysis Date = 02/15/17 Pct Recovery = 60% Analysis Date = 02/13/17 Pct Recovery = 59% Analysis Date = 02/13/17 Pct Recovery = 59% Analysis Date = 02/10/17 Pct Recovery = 59% Analysis Date = 02/10/17 Pct Recovery = 59% Analysis Date = 02/08/17 Pct Recovery = 59% Analysis Date = 02/08/17 Pct Recovery = 59% Analysis Date = 02/06/17 Pct Recovery = 58% Analysis Date = 02/06/17 Pct Recovery = 58% Analysis Date = 02/04/17 Pct Recovery = 58% Analysis Date = 02/04/17 Pct Recovery = 58% Analysis Date = 02/01/17 Pct Recovery = 57% Analysis Date = 02/01/17 Pct Recovery = 57% Analysis Date = 01/30/17 Pct Recovery = 57% Analysis Date = 01/30/17 Pct Recovery = 57% Analysis Date = 01/28/17 Pct Recovery = 56% Analysis Date = 01/28/17 Pct Recovery = 56% Analysis Date = 01/25/17 Pct Recovery = 56% Analysis Date = 01/25/17 Pct Recovery = 56% Analysis Date = 01/23/17 Pct Recovery = 55% Analysis Date = 01/23/17 Pct Recovery = 55% Analysis Date = 01/21/17 Pct Recovery = 55% Analysis Date = 01/21/17 Pct Recovery = 55% Analysis Date = 01/19/17 Pct Recovery = 54% Analysis Date = 01/19/17 Pct Recovery = 54% Analysis Date = 01/16/17 Pct Recovery = 54% Analysis Date = 01/16/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/14/17 Pct Recovery = 54% Analysis Date = 01/12/17 Pct Recovery = 54% Analysis Date = 01/12/17 Pct Recovery = 54% Analysis Date = 01/09/17 Pct Recovery = 55% Analysis Date = 01/09/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 01/07/17 Pct Recovery = 55% Analysis Date = 01/05/17 Pct Recovery = 55% Analysis Date = 01/05/17 Pct Recovery = 55% Analysis Date = 01/03/17 Pct Recovery = 55% Analysis Date = 01/03/17 Pct Recovery = 55% Analysis Date = 12/31/16 Pct Recovery = 55% Analysis Date = 12/31/16 Pct Recovery = 55% Analysis Date = 12/29/16 Pct Recovery = 55% Analysis Date = 12/29/16 Pct Recovery = 55% Analysis Date = 12/27/16 Pct Recovery = 55% Analysis Date = 12/27/16 Pct Recovery = 55% Analysis Date = 12/24/16 Pct Recovery = 55% Analysis Date = 12/24/16 Pct Recovery = 55% Analysis Date = 12/22/16 Pct Recovery = 55% Analysis Date = 12/22/16 Pct Recovery = 55% Analysis Date = 12/20/16 Pct Recovery = 55% Analysis Date = 12/20/16 Pct Recovery = 55% Analysis Date = 12/18/16 Pct Recovery = 55% Analysis Date = 12/18/16 Pct Recovery = 55% Analysis Date = 12/15/16 Pct Recovery = 55% Analysis Date = 12/15/16 Pct Recovery = 55% Analysis Date = 12/13/16 Pct Recovery = 55% Analysis Date = 12/13/16 Pct Recovery = 55% Analysis Date = 12/11/16 Pct Recovery = 56% Analysis Date = 12/11/16 Pct Recovery = 56% Analysis Date = 12/08/16 Pct Recovery = 56% Analysis Date = 12/08/16 Pct Recovery = 56% Analysis Date = 12/06/16 Pct Recovery = 56% Analysis Date = 12/06/16 Pct Recovery = 56% Analysis Date = 12/04/16 Pct Recovery = 56% Analysis Date = 12/04/16 Pct Recovery = 56% Analysis Date = 12/02/16 Pct Recovery = 56% Analysis Date = 12/02/16 Pct Recovery = 56% Analysis Date = 11/29/16 Pct Recovery = 56% Analysis Date = 11/29/16 Pct Recovery = 56% Analysis Date = 11/27/16 Pct Recovery = 56% Analysis Date = 11/27/16 Pct Recovery = 56% Analysis Date = 11/25/16 Pct Recovery = 56% Analysis Date = 11/25/16 Pct Recovery = 56% Analysis Date = 11/22/16 Pct Recovery = 56% Analysis Date = 11/22/16 Pct Recovery = 56% Analysis Date = 11/20/16 Pct Recovery = 56% Analysis Date = 11/20/16 Pct Recovery = 56% Analysis Date = 11/18/16 Pct Recovery = 56% Analysis Date = 11/18/16 Pct Recovery = 56% Analysis Date = 11/16/16 Pct Recovery = 56% Analysis Date = 11/16/16 Pct Recovery = 56% Analysis Date = 11/13/16 Pct Recovery = 56% Analysis Date = 11/13/16 Pct Recovery = 56% Analysis Date = 11/11/16 Pct Recovery = 57% Analysis Date = 11/11/16 Pct Recovery = 57% Analysis Date = 11/09/16 Pct Recovery = 57% Analysis Date = 11/09/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/06/16 Pct Recovery = 57% Analysis Date = 11/04/16 Pct Recovery = 57% Analysis Date = 11/04/16 Pct Recovery = 57% Analysis Date = 11/02/16 Pct Recovery = 57% Analysis Date = 11/02/16 Pct Recovery = 57% Analysis Date = 10/31/16 Pct Recovery = 57% Analysis Date = 10/31/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/28/16 Pct Recovery = 57% Analysis Date = 10/26/16 Pct Recovery = 57% Analysis Date = 10/26/16 Pct Recovery = 57% Analysis Date = 10/24/16 Pct Recovery = 57% Analysis Date = 10/24/16 Pct Recovery = 57% Analysis Date = 10/21/16 Pct Recovery = 57% Analysis Date = 10/21/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/19/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/17/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/15/16 Pct Recovery = 57% Analysis Date = 10/12/16 Pct Recovery = 58% Analysis Date = 10/12/16 Pct Recovery = 58% Analysis Date = 10/10/16 Pct Recovery = 58% Analysis Date = 10/10/16 Pct Recovery = 58% Analysis Date = 10/08/16 Pct Recovery = 58% Analysis Date = 10/08/16 Pct Recovery = 58% Analysis Date = 10/05/16 Pct Recovery = 58% Analysis Date = 10/05/16 Pct Recovery = 58% Analysis Date = 10/03/16 Pct Recovery = 58% Analysis Date = 10/03/16 Pct Recovery = 58% Analysis Date = 10/01/16 Pct Recovery = 58% Analysis Date = 10/01/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 58% Analysis Date = 09/29/16 Pct Recovery = 58% Analysis Date = 09/26/16 Pct Recovery = 58% Analysis Date = 09/26/16 Pct Recovery = 58% Analysis Date = 09/24/16 Pct Recovery = 58% Analysis Date = 09/24/16 Pct Recovery = 58% Analysis Date = 09/22/16 Pct Recovery = 58% Analysis Date = 09/22/16 Pct Recovery = 58% Analysis Date = 09/19/16 Pct Recovery = 58% Analysis Date = 09/19/16 Pct Recovery = 58% Analysis Date = 09/17/16 Pct Recovery = 58% Analysis Date = 09/17/16 Pct Recovery = 58% Analysis Date = 09/15/16 Pct Recovery = 58% Analysis Date = 09/15/16 Pct Recovery = 58% Analysis Date = 09/13/16 Pct Recovery = 59% Analysis Date = 09/13/16 Pct Recovery = 59% Analysis Date = 09/10/16 Pct Recovery = 59% Analysis Date = 09/10/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/08/16 Pct Recovery = 59% Analysis Date = 09/06/16 Pct Recovery = 59% Analysis Date = 09/06/16 Pct Recovery = 59% Analysis Date = 09/03/16 Pct Recovery = 58% Analysis Date = 09/03/16 Pct Recovery = 58% Analysis Date = 09/01/16 Pct Recovery = 58% Analysis Date = 09/01/16 Pct Recovery = 58% Analysis Date = 08/30/16 Pct Recovery = 58% Analysis Date = 08/30/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/28/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/25/16 Pct Recovery = 58% Analysis Date = 08/23/16 Pct Recovery = 58% Analysis Date = 08/23/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/21/16 Pct Recovery = 58% Analysis Date = 08/18/16 Pct Recovery = 58% Analysis Date = 08/18/16 Pct Recovery = 58% Analysis Date = 08/16/16 Pct Recovery = 58% Analysis Date = 08/16/16 Pct Recovery = 58% Analysis Date = 08/14/16 Pct Recovery = 58% Analysis Date = 08/14/16 Pct Recovery = 58% Analysis Date = 08/12/16 Pct Recovery = 58% Analysis Date = 08/12/16 Pct Recovery = 58% Analysis Date = 08/09/16 Pct Recovery = 58% Analysis Date = 08/09/16 Pct Recovery = 58% Analysis Date = 08/07/16 Pct Recovery = 58% Analysis Date = 08/07/16 Pct Recovery = 58% Analysis Date = 08/05/16 Pct Recovery = 58% Analysis Date = 08/05/16 Pct Recovery = 58% Analysis Date = 08/02/16 Pct Recovery = 58% Analysis Date = 08/02/16 Pct Recovery = 58% Analysis Date = 07/31/16 Pct Recovery = 58% Analysis Date = 07/31/16 Pct Recovery = 58% Analysis Date = 07/29/16 Pct Recovery = 58% Analysis Date = 07/29/16 Pct Recovery = 58% Analysis Date = 07/27/16 Pct Recovery = 58% Analysis Date = 07/27/16 Pct Recovery = 58% Analysis Date = 07/24/16 Pct Recovery = 58% Analysis Date = 07/24/16 Pct Recovery = 58% Analysis Date = 07/22/16 Pct Recovery = 58% Analysis Date = 07/22/16 Pct Recovery = 58% Analysis Date = 07/20/16 Pct Recovery = 58% Analysis Date = 07/20/16 Pct Recovery = 58% Analysis Date = 07/17/16 Pct Recovery = 58% Analysis Date = 07/17/16 Pct Recovery = 58% Analysis Date = 07/15/16 Pct Recovery = 57% Analysis Date = 07/15/16 Pct Recovery = 57% Analysis Date = 07/13/16 Pct Recovery = 57% Analysis Date = 07/13/16 Pct Recovery = 57% Analysis Date = 07/11/16 Pct Recovery = 57% Analysis Date = 07/11/16 Pct Recovery = 57% Analysis Date = 07/08/16 Pct Recovery = 57% Analysis Date = 07/08/16 Pct Recovery = 57% Analysis Date = 07/06/16 Pct Recovery = 57% Analysis Date = 07/06/16 Pct Recovery = 57% Analysis Date = 07/04/16 Pct Recovery = 57% Analysis Date = 07/04/16 Pct Recovery = 57% Analysis Date = 07/01/16 Pct Recovery = 57% Analysis Date = 07/01/16 Pct Recovery = 57% Analysis Date = 06/29/16 Pct Recovery = 57% Analysis Date = 06/29/16 Pct Recovery = 57% Analysis Date = 06/27/16 Pct Recovery = 57% Analysis Date = 06/27/16 Pct Recovery = 57% Analysis Date = 06/25/16 Pct Recovery = 57% Analysis Date = 06/25/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/22/16 Pct Recovery = 57% Analysis Date = 06/20/16 Pct Recovery = 57% Analysis Date = 06/20/16 Pct Recovery = 57% Analysis Date = 06/18/16 Pct Recovery = 57% Analysis Date = 06/18/16 Pct Recovery = 57% Analysis Date = 06/15/16 Pct Recovery = 57% Analysis Date = 06/15/16 Pct Recovery = 57% Analysis Date = 06/13/16 Pct Recovery = 57% Analysis Date = 06/13/16 Pct Recovery = 57% Analysis Date = 06/11/16 Pct Recovery = 57% Analysis Date = 06/11/16 Pct Recovery = 57% Analysis Date = 06/09/16 Pct Recovery = 57% Analysis Date = 06/09/16 Pct Recovery = 57% Analysis Date = 06/06/16 Pct Recovery = 57% Analysis Date = 06/06/16 Pct Recovery = 57% Analysis Date = 06/04/16 Pct Recovery = 56% Analysis Date = 06/04/16 Pct Recovery = 56% Analysis Date = 06/02/16 Pct Recovery = 56% Analysis Date = 06/02/16 Pct Recovery = 56% Analysis Date = 05/30/16 Pct Recovery = 56% Analysis Date = 05/30/16 Pct Recovery = 56% Analysis Date = 05/28/16 Pct Recovery = 56% Analysis Date = 05/28/16 Pct Recovery = 56% Analysis Date = 05/26/16 Pct Recovery = 56% Analysis Date = 05/26/16 Pct Recovery = 56% Analysis Date = 05/24/16 Pct Recovery = 56% Analysis Date = 05/24/16 Pct Recovery = 56% Analysis Date = 05/21/16 Pct Recovery = 56% Analysis Date = 05/21/16 Pct Recovery = 56% Analysis Date = 05/19/16 Pct Recovery = 56% Analysis Date = 05/19/16 Pct Recovery = 56% Analysis Date = 05/17/16 Pct Recovery = 56% Analysis Date = 05/17/16 Pct Recovery = 56% Analysis Date = 05/14/16 Pct Recovery = 56% Analysis Date = 05/14/16 Pct Recovery = 56% Analysis Date = 05/12/16 Pct Recovery = 56% Analysis Date = 05/12/16 Pct Recovery = 56% Analysis Date = 05/10/16 Pct Recovery = 56% Analysis Date = 05/10/16 Pct Recovery = 56% Analysis Date = 05/08/16 Pct Recovery = 56% Analysis Date = 05/08/16 Pct Recovery = 56% Analysis Date = 05/05/16 Pct Recovery = 56% Analysis Date = 05/05/16 Pct Recovery = 56% Analysis Date = 05/03/16 Pct Recovery = 56% Analysis Date = 05/03/16 Pct Recovery = 56% Analysis Date = 05/01/16 Pct Recovery = 56% Analysis Date = 05/01/16 Pct Recovery = 56% Analysis Date = 04/28/16 Pct Recovery = 56% Analysis Date = 04/28/16 Pct Recovery = 56% Analysis Date = 04/26/16 Pct Recovery = 56% Analysis Date = 04/26/16 Pct Recovery = 56% Analysis Date = 04/24/16 Pct Recovery = 56% Analysis Date = 04/24/16 Pct Recovery = 56% Analysis Date = 04/22/16 Pct Recovery = 55% Analysis Date = 04/22/16 Pct Recovery = 55% Analysis Date = 04/19/16 Pct Recovery = 55% Analysis Date = 04/19/16 Pct Recovery = 55% Analysis Date = 04/17/16 Pct Recovery = 55% Analysis Date = 04/17/16 Pct Recovery = 55% Analysis Date = 04/15/16 Pct Recovery = 55% Analysis Date = 04/15/16 Pct Recovery = 55% Analysis Date = 04/12/16 Pct Recovery = 55% Analysis Date = 04/12/16 Pct Recovery = 55% Analysis Date = 04/10/16 Pct Recovery = 55% Analysis Date = 04/10/16 Pct Recovery = 55% Analysis Date = 04/08/16 Pct Recovery = 55% Analysis Date = 04/08/16 Pct Recovery = 55% Analysis Date = 04/06/16 Pct Recovery = 55% Analysis Date = 04/06/16 Pct Recovery = 55% Analysis Date = 04/03/16 Pct Recovery = 55% Analysis Date = 04/03/16 Pct Recovery = 55% Analysis Date = 04/01/16 Pct Recovery = 55% Analysis Date = 04/01/16 Pct Recovery = 55% Analysis Date = 03/30/16 Pct Recovery = 55% Analysis Date = 03/30/16 Pct Recovery = 55% Analysis Date = 03/27/16 Pct Recovery = 55% Analysis Date = 03/27/16 Pct Recovery = 55% Analysis Date = 03/25/16 Pct Recovery = 55% Analysis Date = 03/25/16 Pct Recovery = 55% Analysis Date = 03/23/16 Pct Recovery = 55% Analysis Date = 03/23/16 Pct Recovery = 55% Analysis Date = 03/21/16 Pct Recovery = 55% Analysis Date = 03/21/16 Pct Recovery = 55% Analysis Date = 03/18/16 Pct Recovery = 55% Analysis Date = 03/18/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 55% Analysis Date = 03/16/16 Pct Recovery = 55% Analysis Date = 03/14/16 Pct Recovery = 54% Analysis Date = 03/14/16 Pct Recovery = 54% Analysis Date = 03/11/16 Pct Recovery = 54% Analysis Date = 03/11/16 Pct Recovery = 54% Analysis Date = 03/09/16 Pct Recovery = 54% Analysis Date = 03/09/16 Pct Recovery = 54% Analysis Date = 03/07/16 Pct Recovery = 54% Analysis Date = 03/07/16 Pct Recovery = 54% Analysis Date = 03/05/16 Pct Recovery = 54% Analysis Date = 03/05/16 Pct Recovery = 54% Analysis Date = 03/02/16 Pct Recovery = 54% Analysis Date = 03/02/16 Pct Recovery = 54% Analysis Date = 02/29/16 Pct Recovery = 54% Analysis Date = 02/29/16 Pct Recovery = 54% Analysis Date = 02/27/16 Pct Recovery = 54% Analysis Date = 02/27/16 Pct Recovery = 54% Analysis Date = 02/24/16 Pct Recovery = 54% Analysis Date = 02/24/16 Pct Recovery = 54% Analysis Date = 02/22/16 Pct Recovery = 54% Analysis Date = 02/22/16 Pct Recovery = 54% Analysis Date = 02/20/16 Pct Recovery = 54% Analysis Date = 02/20/16 Pct Recovery = 54% Analysis Date = 02/18/16 Pct Recovery = 54% Analysis Date = 02/18/16 Pct Recovery = 54% Analysis Date = 02/15/16 Pct Recovery = 54% Analysis Date = 02/15/16 Pct Recovery = 54% Analysis Date = 02/13/16 Pct Recovery = 54% Analysis Date = 02/13/16 Pct Recovery = 54% Analysis Date = 02/11/16 Pct Recovery = 54% Analysis Date = 02/11/16 Pct Recovery = 54% Analysis Date = 02/09/16 Pct Recovery = 54% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TEFLUTHRIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 18 59% 9% 57% 7%
Total 18 59% 9% 57% 7%

Sample Statistics
TEFLUTHRIN

Characteristic N % % Basis
Plotted 18 100% Spiked
Estimated Values 18 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 18 .  
False Negatives 0 0% 0 out of 18
Not Spiked 10 .  
False Positives 0 0% 0 out of 10

OBSP Determination:
TERBUFOS
METHOD: 2033 , TESTIDCODE: 82675GCM35

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 73% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 82% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 82% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 74% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 90% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 68% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 60% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 57% Analysis Date = 04/07/16 SpikeMix = Spex Organics EN150514012: 40 µl & ERA 0406-15-01: 40 µl Pct Recovery = 49% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 93% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 79% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 72% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 63% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 57% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 85% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 58% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 56% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 61% Analysis Date = 03/02/16 SpikeMix = Abs 041415: 20 µl & ChemService 3851600: 20 µl Pct Recovery = 51% Analysis Date = 05/10/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/06/17 Pct Recovery = 76% Analysis Date = 05/04/17 Pct Recovery = 76% Analysis Date = 05/04/17 Pct Recovery = 76% Analysis Date = 05/02/17 Pct Recovery = 76% Analysis Date = 05/02/17 Pct Recovery = 76% Analysis Date = 04/30/17 Pct Recovery = 76% Analysis Date = 04/30/17 Pct Recovery = 76% Analysis Date = 04/27/17 Pct Recovery = 76% Analysis Date = 04/27/17 Pct Recovery = 76% Analysis Date = 04/25/17 Pct Recovery = 76% Analysis Date = 04/25/17 Pct Recovery = 76% Analysis Date = 04/23/17 Pct Recovery = 76% Analysis Date = 04/23/17 Pct Recovery = 76% Analysis Date = 04/21/17 Pct Recovery = 76% Analysis Date = 04/21/17 Pct Recovery = 76% Analysis Date = 04/19/17 Pct Recovery = 76% Analysis Date = 04/19/17 Pct Recovery = 76% Analysis Date = 04/17/17 Pct Recovery = 76% Analysis Date = 04/17/17 Pct Recovery = 76% Analysis Date = 04/14/17 Pct Recovery = 76% Analysis Date = 04/14/17 Pct Recovery = 76% Analysis Date = 04/12/17 Pct Recovery = 75% Analysis Date = 04/12/17 Pct Recovery = 75% Analysis Date = 04/10/17 Pct Recovery = 75% Analysis Date = 04/10/17 Pct Recovery = 75% Analysis Date = 04/08/17 Pct Recovery = 75% Analysis Date = 04/08/17 Pct Recovery = 75% Analysis Date = 04/06/17 Pct Recovery = 75% Analysis Date = 04/06/17 Pct Recovery = 75% Analysis Date = 04/04/17 Pct Recovery = 75% Analysis Date = 04/04/17 Pct Recovery = 75% Analysis Date = 04/01/17 Pct Recovery = 75% Analysis Date = 04/01/17 Pct Recovery = 75% Analysis Date = 03/30/17 Pct Recovery = 75% Analysis Date = 03/30/17 Pct Recovery = 75% Analysis Date = 03/28/17 Pct Recovery = 75% Analysis Date = 03/28/17 Pct Recovery = 75% Analysis Date = 03/26/17 Pct Recovery = 75% Analysis Date = 03/26/17 Pct Recovery = 75% Analysis Date = 03/24/17 Pct Recovery = 75% Analysis Date = 03/24/17 Pct Recovery = 75% Analysis Date = 03/21/17 Pct Recovery = 75% Analysis Date = 03/21/17 Pct Recovery = 75% Analysis Date = 03/19/17 Pct Recovery = 75% Analysis Date = 03/19/17 Pct Recovery = 75% Analysis Date = 03/17/17 Pct Recovery = 75% Analysis Date = 03/17/17 Pct Recovery = 75% Analysis Date = 03/15/17 Pct Recovery = 75% Analysis Date = 03/15/17 Pct Recovery = 75% Analysis Date = 03/13/17 Pct Recovery = 75% Analysis Date = 03/13/17 Pct Recovery = 75% Analysis Date = 03/11/17 Pct Recovery = 75% Analysis Date = 03/11/17 Pct Recovery = 75% Analysis Date = 03/08/17 Pct Recovery = 75% Analysis Date = 03/08/17 Pct Recovery = 75% Analysis Date = 03/06/17 Pct Recovery = 75% Analysis Date = 03/06/17 Pct Recovery = 75% Analysis Date = 03/04/17 Pct Recovery = 75% Analysis Date = 03/04/17 Pct Recovery = 75% Analysis Date = 03/02/17 Pct Recovery = 75% Analysis Date = 03/02/17 Pct Recovery = 75% Analysis Date = 02/28/17 Pct Recovery = 75% Analysis Date = 02/28/17 Pct Recovery = 75% Analysis Date = 02/26/17 Pct Recovery = 75% Analysis Date = 02/26/17 Pct Recovery = 75% Analysis Date = 02/23/17 Pct Recovery = 75% Analysis Date = 02/23/17 Pct Recovery = 75% Analysis Date = 02/21/17 Pct Recovery = 74% Analysis Date = 02/21/17 Pct Recovery = 74% Analysis Date = 02/19/17 Pct Recovery = 74% Analysis Date = 02/19/17 Pct Recovery = 74% Analysis Date = 02/17/17 Pct Recovery = 74% Analysis Date = 02/17/17 Pct Recovery = 74% Analysis Date = 02/15/17 Pct Recovery = 74% Analysis Date = 02/15/17 Pct Recovery = 74% Analysis Date = 02/12/17 Pct Recovery = 74% Analysis Date = 02/12/17 Pct Recovery = 74% Analysis Date = 02/10/17 Pct Recovery = 74% Analysis Date = 02/10/17 Pct Recovery = 74% Analysis Date = 02/08/17 Pct Recovery = 74% Analysis Date = 02/08/17 Pct Recovery = 74% Analysis Date = 02/06/17 Pct Recovery = 74% Analysis Date = 02/06/17 Pct Recovery = 74% Analysis Date = 02/04/17 Pct Recovery = 74% Analysis Date = 02/04/17 Pct Recovery = 74% Analysis Date = 02/02/17 Pct Recovery = 74% Analysis Date = 02/02/17 Pct Recovery = 74% Analysis Date = 01/30/17 Pct Recovery = 74% Analysis Date = 01/30/17 Pct Recovery = 74% Analysis Date = 01/28/17 Pct Recovery = 74% Analysis Date = 01/28/17 Pct Recovery = 74% Analysis Date = 01/26/17 Pct Recovery = 74% Analysis Date = 01/26/17 Pct Recovery = 74% Analysis Date = 01/24/17 Pct Recovery = 74% Analysis Date = 01/24/17 Pct Recovery = 74% Analysis Date = 01/22/17 Pct Recovery = 74% Analysis Date = 01/22/17 Pct Recovery = 74% Analysis Date = 01/20/17 Pct Recovery = 74% Analysis Date = 01/20/17 Pct Recovery = 74% Analysis Date = 01/17/17 Pct Recovery = 74% Analysis Date = 01/17/17 Pct Recovery = 74% Analysis Date = 01/15/17 Pct Recovery = 74% Analysis Date = 01/15/17 Pct Recovery = 74% Analysis Date = 01/13/17 Pct Recovery = 74% Analysis Date = 01/13/17 Pct Recovery = 74% Analysis Date = 01/11/17 Pct Recovery = 74% Analysis Date = 01/11/17 Pct Recovery = 74% Analysis Date = 01/09/17 Pct Recovery = 74% Analysis Date = 01/09/17 Pct Recovery = 74% Analysis Date = 01/07/17 Pct Recovery = 74% Analysis Date = 01/07/17 Pct Recovery = 74% Analysis Date = 01/04/17 Pct Recovery = 74% Analysis Date = 01/04/17 Pct Recovery = 74% Analysis Date = 01/02/17 Pct Recovery = 74% Analysis Date = 01/02/17 Pct Recovery = 74% Analysis Date = 12/31/16 Pct Recovery = 75% Analysis Date = 12/31/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/29/16 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/27/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/24/16 Pct Recovery = 75% Analysis Date = 12/22/16 Pct Recovery = 75% Analysis Date = 12/22/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 75% Analysis Date = 12/20/16 Pct Recovery = 75% Analysis Date = 12/18/16 Pct Recovery = 75% Analysis Date = 12/18/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/16/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/14/16 Pct Recovery = 75% Analysis Date = 12/11/16 Pct Recovery = 75% Analysis Date = 12/11/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/09/16 Pct Recovery = 75% Analysis Date = 12/07/16 Pct Recovery = 75% Analysis Date = 12/07/16 Pct Recovery = 75% Analysis Date = 12/05/16 Pct Recovery = 76% Analysis Date = 12/05/16 Pct Recovery = 76% Analysis Date = 12/03/16 Pct Recovery = 76% Analysis Date = 12/03/16 Pct Recovery = 76% Analysis Date = 12/01/16 Pct Recovery = 76% Analysis Date = 12/01/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/28/16 Pct Recovery = 76% Analysis Date = 11/26/16 Pct Recovery = 76% Analysis Date = 11/26/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/24/16 Pct Recovery = 76% Analysis Date = 11/22/16 Pct Recovery = 76% Analysis Date = 11/22/16 Pct Recovery = 76% Analysis Date = 11/20/16 Pct Recovery = 76% Analysis Date = 11/20/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 76% Analysis Date = 11/17/16 Pct Recovery = 76% Analysis Date = 11/15/16 Pct Recovery = 76% Analysis Date = 11/15/16 Pct Recovery = 76% Analysis Date = 11/13/16 Pct Recovery = 76% Analysis Date = 11/13/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/11/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/09/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 76% Analysis Date = 11/07/16 Pct Recovery = 76% Analysis Date = 11/04/16 Pct Recovery = 77% Analysis Date = 11/04/16 Pct Recovery = 77% Analysis Date = 11/02/16 Pct Recovery = 77% Analysis Date = 11/02/16 Pct Recovery = 77% Analysis Date = 10/31/16 Pct Recovery = 77% Analysis Date = 10/31/16 Pct Recovery = 77% Analysis Date = 10/29/16 Pct Recovery = 77% Analysis Date = 10/29/16 Pct Recovery = 77% Analysis Date = 10/27/16 Pct Recovery = 77% Analysis Date = 10/27/16 Pct Recovery = 77% Analysis Date = 10/25/16 Pct Recovery = 77% Analysis Date = 10/25/16 Pct Recovery = 77% Analysis Date = 10/22/16 Pct Recovery = 77% Analysis Date = 10/22/16 Pct Recovery = 77% Analysis Date = 10/20/16 Pct Recovery = 77% Analysis Date = 10/20/16 Pct Recovery = 77% Analysis Date = 10/18/16 Pct Recovery = 77% Analysis Date = 10/18/16 Pct Recovery = 77% Analysis Date = 10/16/16 Pct Recovery = 77% Analysis Date = 10/16/16 Pct Recovery = 77% Analysis Date = 10/14/16 Pct Recovery = 77% Analysis Date = 10/14/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/12/16 Pct Recovery = 77% Analysis Date = 10/09/16 Pct Recovery = 77% Analysis Date = 10/09/16 Pct Recovery = 77% Analysis Date = 10/07/16 Pct Recovery = 77% Analysis Date = 10/07/16 Pct Recovery = 77% Analysis Date = 10/05/16 Pct Recovery = 78% Analysis Date = 10/05/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/03/16 Pct Recovery = 78% Analysis Date = 10/01/16 Pct Recovery = 78% Analysis Date = 10/01/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/28/16 Pct Recovery = 78% Analysis Date = 09/26/16 Pct Recovery = 78% Analysis Date = 09/26/16 Pct Recovery = 78% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/24/16 Pct Recovery = 78% Analysis Date = 09/22/16 Pct Recovery = 78% Analysis Date = 09/22/16 Pct Recovery = 78% Analysis Date = 09/20/16 Pct Recovery = 78% Analysis Date = 09/20/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/18/16 Pct Recovery = 78% Analysis Date = 09/15/16 Pct Recovery = 78% Analysis Date = 09/15/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/13/16 Pct Recovery = 78% Analysis Date = 09/11/16 Pct Recovery = 78% Analysis Date = 09/11/16 Pct Recovery = 78% Analysis Date = 09/09/16 Pct Recovery = 78% Analysis Date = 09/09/16 Pct Recovery = 78% Analysis Date = 09/07/16 Pct Recovery = 78% Analysis Date = 09/07/16 Pct Recovery = 78% Analysis Date = 09/05/16 Pct Recovery = 78% Analysis Date = 09/05/16 Pct Recovery = 78% Analysis Date = 09/02/16 Pct Recovery = 78% Analysis Date = 09/02/16 Pct Recovery = 78% Analysis Date = 08/31/16 Pct Recovery = 78% Analysis Date = 08/31/16 Pct Recovery = 78% Analysis Date = 08/29/16 Pct Recovery = 78% Analysis Date = 08/29/16 Pct Recovery = 78% Analysis Date = 08/27/16 Pct Recovery = 77% Analysis Date = 08/27/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 77% Analysis Date = 08/25/16 Pct Recovery = 77% Analysis Date = 08/22/16 Pct Recovery = 77% Analysis Date = 08/22/16 Pct Recovery = 77% Analysis Date = 08/20/16 Pct Recovery = 77% Analysis Date = 08/20/16 Pct Recovery = 77% Analysis Date = 08/18/16 Pct Recovery = 77% Analysis Date = 08/18/16 Pct Recovery = 77% Analysis Date = 08/16/16 Pct Recovery = 76% Analysis Date = 08/16/16 Pct Recovery = 76% Analysis Date = 08/14/16 Pct Recovery = 76% Analysis Date = 08/14/16 Pct Recovery = 76% Analysis Date = 08/12/16 Pct Recovery = 75% Analysis Date = 08/12/16 Pct Recovery = 75% Analysis Date = 08/09/16 Pct Recovery = 75% Analysis Date = 08/09/16 Pct Recovery = 75% Analysis Date = 08/07/16 Pct Recovery = 75% Analysis Date = 08/07/16 Pct Recovery = 75% Analysis Date = 08/05/16 Pct Recovery = 74% Analysis Date = 08/05/16 Pct Recovery = 74% Analysis Date = 08/03/16 Pct Recovery = 74% Analysis Date = 08/03/16 Pct Recovery = 74% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 08/01/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/30/16 Pct Recovery = 73% Analysis Date = 07/27/16 Pct Recovery = 72% Analysis Date = 07/27/16 Pct Recovery = 72% Analysis Date = 07/25/16 Pct Recovery = 72% Analysis Date = 07/25/16 Pct Recovery = 72% Analysis Date = 07/23/16 Pct Recovery = 72% Analysis Date = 07/23/16 Pct Recovery = 72% Analysis Date = 07/21/16 Pct Recovery = 71% Analysis Date = 07/21/16 Pct Recovery = 71% Analysis Date = 07/19/16 Pct Recovery = 71% Analysis Date = 07/19/16 Pct Recovery = 71% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/17/16 Pct Recovery = 70% Analysis Date = 07/14/16 Pct Recovery = 70% Analysis Date = 07/14/16 Pct Recovery = 70% Analysis Date = 07/12/16 Pct Recovery = 69% Analysis Date = 07/12/16 Pct Recovery = 69% Analysis Date = 07/10/16 Pct Recovery = 69% Analysis Date = 07/10/16 Pct Recovery = 69% Analysis Date = 07/08/16 Pct Recovery = 69% Analysis Date = 07/08/16 Pct Recovery = 69% Analysis Date = 07/06/16 Pct Recovery = 68% Analysis Date = 07/06/16 Pct Recovery = 68% Analysis Date = 07/03/16 Pct Recovery = 68% Analysis Date = 07/03/16 Pct Recovery = 68% Analysis Date = 07/01/16 Pct Recovery = 67% Analysis Date = 07/01/16 Pct Recovery = 67% Analysis Date = 06/29/16 Pct Recovery = 67% Analysis Date = 06/29/16 Pct Recovery = 67% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/27/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/25/16 Pct Recovery = 66% Analysis Date = 06/23/16 Pct Recovery = 66% Analysis Date = 06/23/16 Pct Recovery = 66% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 65% Analysis Date = 06/18/16 Pct Recovery = 65% Analysis Date = 06/16/16 Pct Recovery = 64% Analysis Date = 06/16/16 Pct Recovery = 64% Analysis Date = 06/14/16 Pct Recovery = 64% Analysis Date = 06/14/16 Pct Recovery = 64% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/12/16 Pct Recovery = 63% Analysis Date = 06/10/16 Pct Recovery = 63% Analysis Date = 06/10/16 Pct Recovery = 63% Analysis Date = 06/07/16 Pct Recovery = 63% Analysis Date = 06/07/16 Pct Recovery = 63% Analysis Date = 06/05/16 Pct Recovery = 62% Analysis Date = 06/05/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 06/03/16 Pct Recovery = 62% Analysis Date = 06/01/16 Pct Recovery = 61% Analysis Date = 06/01/16 Pct Recovery = 61% Analysis Date = 05/30/16 Pct Recovery = 61% Analysis Date = 05/30/16 Pct Recovery = 61% Analysis Date = 05/27/16 Pct Recovery = 60% Analysis Date = 05/27/16 Pct Recovery = 60% Analysis Date = 05/25/16 Pct Recovery = 60% Analysis Date = 05/25/16 Pct Recovery = 60% Analysis Date = 05/23/16 Pct Recovery = 60% Analysis Date = 05/23/16 Pct Recovery = 60% Analysis Date = 05/21/16 Pct Recovery = 60% Analysis Date = 05/21/16 Pct Recovery = 60% Analysis Date = 05/19/16 Pct Recovery = 59% Analysis Date = 05/19/16 Pct Recovery = 59% Analysis Date = 05/17/16 Pct Recovery = 59% Analysis Date = 05/17/16 Pct Recovery = 59% Analysis Date = 05/14/16 Pct Recovery = 59% Analysis Date = 05/14/16 Pct Recovery = 59% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/12/16 Pct Recovery = 58% Analysis Date = 05/10/16 Pct Recovery = 58% Analysis Date = 05/10/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/08/16 Pct Recovery = 58% Analysis Date = 05/06/16 Pct Recovery = 58% Analysis Date = 05/06/16 Pct Recovery = 58% Analysis Date = 05/04/16 Pct Recovery = 57% Analysis Date = 05/04/16 Pct Recovery = 57% Analysis Date = 05/01/16 Pct Recovery = 57% Analysis Date = 05/01/16 Pct Recovery = 57% Analysis Date = 04/29/16 Pct Recovery = 57% Analysis Date = 04/29/16 Pct Recovery = 57% Analysis Date = 04/27/16 Pct Recovery = 57% Analysis Date = 04/27/16 Pct Recovery = 57% Analysis Date = 04/25/16 Pct Recovery = 56% Analysis Date = 04/25/16 Pct Recovery = 56% Analysis Date = 04/23/16 Pct Recovery = 56% Analysis Date = 04/23/16 Pct Recovery = 56% Analysis Date = 04/21/16 Pct Recovery = 56% Analysis Date = 04/21/16 Pct Recovery = 56% Analysis Date = 04/18/16 Pct Recovery = 56% Analysis Date = 04/18/16 Pct Recovery = 56% Analysis Date = 04/16/16 Pct Recovery = 55% Analysis Date = 04/16/16 Pct Recovery = 55% Analysis Date = 04/14/16 Pct Recovery = 55% Analysis Date = 04/14/16 Pct Recovery = 55% Analysis Date = 04/12/16 Pct Recovery = 55% Analysis Date = 04/12/16 Pct Recovery = 55% Analysis Date = 04/10/16 Pct Recovery = 55% Analysis Date = 04/10/16 Pct Recovery = 55% Analysis Date = 04/07/16 Pct Recovery = 54% Analysis Date = 04/07/16 Pct Recovery = 54% Analysis Date = 04/05/16 Pct Recovery = 54% Analysis Date = 04/05/16 Pct Recovery = 54% Analysis Date = 04/03/16 Pct Recovery = 54% Analysis Date = 04/03/16 Pct Recovery = 54% Analysis Date = 04/01/16 Pct Recovery = 54% Analysis Date = 04/01/16 Pct Recovery = 54% Analysis Date = 03/30/16 Pct Recovery = 54% Analysis Date = 03/30/16 Pct Recovery = 54% Analysis Date = 03/28/16 Pct Recovery = 53% Analysis Date = 03/28/16 Pct Recovery = 53% Analysis Date = 03/25/16 Pct Recovery = 53% Analysis Date = 03/25/16 Pct Recovery = 53% Analysis Date = 03/23/16 Pct Recovery = 53% Analysis Date = 03/23/16 Pct Recovery = 53% Analysis Date = 03/21/16 Pct Recovery = 53% Analysis Date = 03/21/16 Pct Recovery = 53% Analysis Date = 03/19/16 Pct Recovery = 53% Analysis Date = 03/19/16 Pct Recovery = 53% Analysis Date = 03/17/16 Pct Recovery = 52% Analysis Date = 03/17/16 Pct Recovery = 52% Analysis Date = 03/15/16 Pct Recovery = 52% Analysis Date = 03/15/16 Pct Recovery = 52% Analysis Date = 03/12/16 Pct Recovery = 52% Analysis Date = 03/12/16 Pct Recovery = 52% Analysis Date = 03/10/16 Pct Recovery = 52% Analysis Date = 03/10/16 Pct Recovery = 52% Analysis Date = 03/08/16 Pct Recovery = 51% Analysis Date = 03/08/16 Pct Recovery = 51% Analysis Date = 03/06/16 Pct Recovery = 51% Analysis Date = 03/06/16 Pct Recovery = 51% Analysis Date = 03/04/16 Pct Recovery = 51% Analysis Date = 03/04/16 Pct Recovery = 51% Analysis Date = 03/02/16 Pct Recovery = 51% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUFOS

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 69% 14% 68% 19%
Total 19 69% 14% 68% 19%

Sample Statistics
TERBUFOS

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
TERBUFOS-O-ANALOGUE SULFONE
METHOD: 2033 , TESTIDCODE: 61674GCM39

The SGPlot Procedure

Sample Statistics
TERBUFOS-O-ANALOGUE SULFONE

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 0 .  
False Negatives 0 . 0 out of 0
Not Spiked 28 .  
False Positives 0 0% 0 out of 28

OBSP Determination:
TERBUTHYLAZINE
METHOD: 2033 , TESTIDCODE: 04022GCM39

Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 95% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 96% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 105% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 100% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 95% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 84% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 97% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 99% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 74% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 79% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 75% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 88% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 77% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 75% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 92% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 104% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 83% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 86% Analysis Date = 05/10/17 Pct Recovery = 86% Analysis Date = 05/08/17 Pct Recovery = 87% Analysis Date = 05/08/17 Pct Recovery = 87% Analysis Date = 05/06/17 Pct Recovery = 87% Analysis Date = 05/06/17 Pct Recovery = 87% Analysis Date = 05/04/17 Pct Recovery = 87% Analysis Date = 05/04/17 Pct Recovery = 87% Analysis Date = 05/01/17 Pct Recovery = 87% Analysis Date = 05/01/17 Pct Recovery = 87% Analysis Date = 04/29/17 Pct Recovery = 87% Analysis Date = 04/29/17 Pct Recovery = 87% Analysis Date = 04/27/17 Pct Recovery = 87% Analysis Date = 04/27/17 Pct Recovery = 87% Analysis Date = 04/25/17 Pct Recovery = 87% Analysis Date = 04/25/17 Pct Recovery = 87% Analysis Date = 04/22/17 Pct Recovery = 87% Analysis Date = 04/22/17 Pct Recovery = 87% Analysis Date = 04/20/17 Pct Recovery = 88% Analysis Date = 04/20/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/15/17 Pct Recovery = 88% Analysis Date = 04/15/17 Pct Recovery = 88% Analysis Date = 04/13/17 Pct Recovery = 88% Analysis Date = 04/13/17 Pct Recovery = 88% Analysis Date = 04/11/17 Pct Recovery = 88% Analysis Date = 04/11/17 Pct Recovery = 88% Analysis Date = 04/09/17 Pct Recovery = 88% Analysis Date = 04/09/17 Pct Recovery = 88% Analysis Date = 04/06/17 Pct Recovery = 88% Analysis Date = 04/06/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/04/17 Pct Recovery = 88% Analysis Date = 04/02/17 Pct Recovery = 88% Analysis Date = 04/02/17 Pct Recovery = 88% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/28/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/26/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/24/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/21/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/19/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/17/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 89% Analysis Date = 03/14/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 89% Analysis Date = 03/12/17 Pct Recovery = 89% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/08/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/03/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 03/01/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/26/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/22/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/20/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/17/17 Pct Recovery = 90% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/15/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/13/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/10/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/08/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/06/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/04/17 Pct Recovery = 91% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/28/17 Pct Recovery = 90% Analysis Date = 01/28/17 Pct Recovery = 90% Analysis Date = 01/25/17 Pct Recovery = 90% Analysis Date = 01/25/17 Pct Recovery = 90% Analysis Date = 01/23/17 Pct Recovery = 90% Analysis Date = 01/23/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/21/17 Pct Recovery = 90% Analysis Date = 01/19/17 Pct Recovery = 90% Analysis Date = 01/19/17 Pct Recovery = 90% Analysis Date = 01/16/17 Pct Recovery = 90% Analysis Date = 01/16/17 Pct Recovery = 90% Analysis Date = 01/14/17 Pct Recovery = 90% Analysis Date = 01/14/17 Pct Recovery = 90% Analysis Date = 01/12/17 Pct Recovery = 90% Analysis Date = 01/12/17 Pct Recovery = 90% Analysis Date = 01/09/17 Pct Recovery = 90% Analysis Date = 01/09/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 90% Analysis Date = 01/07/17 Pct Recovery = 90% Analysis Date = 01/05/17 Pct Recovery = 90% Analysis Date = 01/05/17 Pct Recovery = 90% Analysis Date = 01/03/17 Pct Recovery = 90% Analysis Date = 01/03/17 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/31/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/29/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/27/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/24/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 90% Analysis Date = 12/22/16 Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 90% Analysis Date = 12/20/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/18/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/15/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/13/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/11/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/08/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/06/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/04/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 12/02/16 Pct Recovery = 90% Analysis Date = 11/29/16 Pct Recovery = 90% Analysis Date = 11/29/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 90% Analysis Date = 11/27/16 Pct Recovery = 90% Analysis Date = 11/25/16 Pct Recovery = 90% Analysis Date = 11/25/16 Pct Recovery = 90% Analysis Date = 11/22/16 Pct Recovery = 90% Analysis Date = 11/22/16 Pct Recovery = 90% Analysis Date = 11/20/16 Pct Recovery = 90% Analysis Date = 11/20/16 Pct Recovery = 90% Analysis Date = 11/18/16 Pct Recovery = 90% Analysis Date = 11/18/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/16/16 Pct Recovery = 90% Analysis Date = 11/13/16 Pct Recovery = 90% Analysis Date = 11/13/16 Pct Recovery = 90% Analysis Date = 11/11/16 Pct Recovery = 90% Analysis Date = 11/11/16 Pct Recovery = 90% Analysis Date = 11/09/16 Pct Recovery = 90% Analysis Date = 11/09/16 Pct Recovery = 90% Analysis Date = 11/06/16 Pct Recovery = 90% Analysis Date = 11/06/16 Pct Recovery = 90% Analysis Date = 11/04/16 Pct Recovery = 90% Analysis Date = 11/04/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 10/31/16 Pct Recovery = 90% Analysis Date = 10/31/16 Pct Recovery = 90% Analysis Date = 10/28/16 Pct Recovery = 90% Analysis Date = 10/28/16 Pct Recovery = 90% Analysis Date = 10/26/16 Pct Recovery = 90% Analysis Date = 10/26/16 Pct Recovery = 90% Analysis Date = 10/24/16 Pct Recovery = 90% Analysis Date = 10/24/16 Pct Recovery = 90% Analysis Date = 10/21/16 Pct Recovery = 90% Analysis Date = 10/21/16 Pct Recovery = 90% Analysis Date = 10/19/16 Pct Recovery = 90% Analysis Date = 10/19/16 Pct Recovery = 90% Analysis Date = 10/17/16 Pct Recovery = 90% Analysis Date = 10/17/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/15/16 Pct Recovery = 90% Analysis Date = 10/12/16 Pct Recovery = 90% Analysis Date = 10/12/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/10/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/08/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/05/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/03/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 10/01/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/29/16 Pct Recovery = 90% Analysis Date = 09/26/16 Pct Recovery = 90% Analysis Date = 09/26/16 Pct Recovery = 90% Analysis Date = 09/24/16 Pct Recovery = 90% Analysis Date = 09/24/16 Pct Recovery = 90% Analysis Date = 09/22/16 Pct Recovery = 90% Analysis Date = 09/22/16 Pct Recovery = 90% Analysis Date = 09/19/16 Pct Recovery = 90% Analysis Date = 09/19/16 Pct Recovery = 90% Analysis Date = 09/17/16 Pct Recovery = 90% Analysis Date = 09/17/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/15/16 Pct Recovery = 90% Analysis Date = 09/13/16 Pct Recovery = 90% Analysis Date = 09/13/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/10/16 Pct Recovery = 90% Analysis Date = 09/08/16 Pct Recovery = 90% Analysis Date = 09/08/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/06/16 Pct Recovery = 90% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 09/03/16 Pct Recovery = 89% Analysis Date = 09/01/16 Pct Recovery = 89% Analysis Date = 09/01/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/30/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/28/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/25/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/23/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/21/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/18/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 89% Analysis Date = 08/16/16 Pct Recovery = 89% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/14/16 Pct Recovery = 88% Analysis Date = 08/12/16 Pct Recovery = 88% Analysis Date = 08/12/16 Pct Recovery = 88% Analysis Date = 08/09/16 Pct Recovery = 88% Analysis Date = 08/09/16 Pct Recovery = 88% Analysis Date = 08/07/16 Pct Recovery = 88% Analysis Date = 08/07/16 Pct Recovery = 88% Analysis Date = 08/05/16 Pct Recovery = 88% Analysis Date = 08/05/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 08/02/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/31/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/29/16 Pct Recovery = 88% Analysis Date = 07/27/16 Pct Recovery = 87% Analysis Date = 07/27/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/24/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/22/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/20/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/17/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/15/16 Pct Recovery = 87% Analysis Date = 07/13/16 Pct Recovery = 87% Analysis Date = 07/13/16 Pct Recovery = 87% Analysis Date = 07/11/16 Pct Recovery = 87% Analysis Date = 07/11/16 Pct Recovery = 87% Analysis Date = 07/08/16 Pct Recovery = 86% Analysis Date = 07/08/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/06/16 Pct Recovery = 86% Analysis Date = 07/04/16 Pct Recovery = 86% Analysis Date = 07/04/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 07/01/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/29/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/27/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/25/16 Pct Recovery = 86% Analysis Date = 06/22/16 Pct Recovery = 86% Analysis Date = 06/22/16 Pct Recovery = 86% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/20/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/18/16 Pct Recovery = 85% Analysis Date = 06/15/16 Pct Recovery = 85% Analysis Date = 06/15/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 85% Analysis Date = 06/13/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/11/16 Pct Recovery = 85% Analysis Date = 06/09/16 Pct Recovery = 85% Analysis Date = 06/09/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/06/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/04/16 Pct Recovery = 85% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 05/30/16 Pct Recovery = 84% Analysis Date = 05/30/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/28/16 Pct Recovery = 84% Analysis Date = 05/26/16 Pct Recovery = 84% Analysis Date = 05/26/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/24/16 Pct Recovery = 84% Analysis Date = 05/21/16 Pct Recovery = 84% Analysis Date = 05/21/16 Pct Recovery = 84% Analysis Date = 05/19/16 Pct Recovery = 84% Analysis Date = 05/19/16 Pct Recovery = 84% Analysis Date = 05/17/16 Pct Recovery = 85% Analysis Date = 05/17/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/12/16 Pct Recovery = 85% Analysis Date = 05/12/16 Pct Recovery = 85% Analysis Date = 05/10/16 Pct Recovery = 85% Analysis Date = 05/10/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/05/16 Pct Recovery = 85% Analysis Date = 05/05/16 Pct Recovery = 85% Analysis Date = 05/03/16 Pct Recovery = 85% Analysis Date = 05/03/16 Pct Recovery = 85% Analysis Date = 05/01/16 Pct Recovery = 85% Analysis Date = 05/01/16 Pct Recovery = 85% Analysis Date = 04/28/16 Pct Recovery = 85% Analysis Date = 04/28/16 Pct Recovery = 85% Analysis Date = 04/26/16 Pct Recovery = 85% Analysis Date = 04/26/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/22/16 Pct Recovery = 86% Analysis Date = 04/19/16 Pct Recovery = 86% Analysis Date = 04/19/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/17/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/15/16 Pct Recovery = 86% Analysis Date = 04/12/16 Pct Recovery = 86% Analysis Date = 04/12/16 Pct Recovery = 86% Analysis Date = 04/10/16 Pct Recovery = 86% Analysis Date = 04/10/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 86% Analysis Date = 04/08/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/06/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/03/16 Pct Recovery = 86% Analysis Date = 04/01/16 Pct Recovery = 87% Analysis Date = 04/01/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/30/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/27/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/25/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/23/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/21/16 Pct Recovery = 87% Analysis Date = 03/18/16 Pct Recovery = 87% Analysis Date = 03/18/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/16/16 Pct Recovery = 87% Analysis Date = 03/14/16 Pct Recovery = 87% Analysis Date = 03/14/16 Pct Recovery = 87% Analysis Date = 03/11/16 Pct Recovery = 88% Analysis Date = 03/11/16 Pct Recovery = 88% Analysis Date = 03/09/16 Pct Recovery = 88% Analysis Date = 03/09/16 Pct Recovery = 88% Analysis Date = 03/07/16 Pct Recovery = 88% Analysis Date = 03/07/16 Pct Recovery = 88% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 03/05/16 Pct Recovery = 88% Analysis Date = 03/02/16 Pct Recovery = 88% Analysis Date = 03/02/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/29/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/27/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/24/16 Pct Recovery = 88% Analysis Date = 02/22/16 Pct Recovery = 89% Analysis Date = 02/22/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/20/16 Pct Recovery = 89% Analysis Date = 02/18/16 Pct Recovery = 89% Analysis Date = 02/18/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/15/16 Pct Recovery = 89% Analysis Date = 02/13/16 Pct Recovery = 89% Analysis Date = 02/13/16 Pct Recovery = 89% Analysis Date = 02/11/16 Pct Recovery = 89% Analysis Date = 02/11/16 Pct Recovery = 89% Analysis Date = 02/09/16 Pct Recovery = 89% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TERBUTHYLAZINE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 88% 10% 87% 13%
Total 20 88% 10% 87% 13%

Sample Statistics
TERBUTHYLAZINE

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
THIOBENCARB
METHOD: 2033 , TESTIDCODE: 82681GCM35

Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 107% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 97% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 84% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 85% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 94% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 102% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 65% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 86% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 74% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 71% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 62% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 56% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 88% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 86% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 64% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 70% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 82% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 60% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 75% Analysis Date = 05/10/17 Pct Recovery = 88% Analysis Date = 05/08/17 Pct Recovery = 88% Analysis Date = 05/08/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 05/06/17 Pct Recovery = 88% Analysis Date = 05/04/17 Pct Recovery = 88% Analysis Date = 05/04/17 Pct Recovery = 88% Analysis Date = 05/01/17 Pct Recovery = 88% Analysis Date = 05/01/17 Pct Recovery = 88% Analysis Date = 04/29/17 Pct Recovery = 88% Analysis Date = 04/29/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/27/17 Pct Recovery = 88% Analysis Date = 04/25/17 Pct Recovery = 88% Analysis Date = 04/25/17 Pct Recovery = 88% Analysis Date = 04/22/17 Pct Recovery = 88% Analysis Date = 04/22/17 Pct Recovery = 88% Analysis Date = 04/20/17 Pct Recovery = 88% Analysis Date = 04/20/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/18/17 Pct Recovery = 88% Analysis Date = 04/15/17 Pct Recovery = 88% Analysis Date = 04/15/17 Pct Recovery = 88% Analysis Date = 04/13/17 Pct Recovery = 88% Analysis Date = 04/13/17 Pct Recovery = 88% Analysis Date = 04/11/17 Pct Recovery = 87% Analysis Date = 04/11/17 Pct Recovery = 87% Analysis Date = 04/09/17 Pct Recovery = 87% Analysis Date = 04/09/17 Pct Recovery = 87% Analysis Date = 04/06/17 Pct Recovery = 87% Analysis Date = 04/06/17 Pct Recovery = 87% Analysis Date = 04/04/17 Pct Recovery = 87% Analysis Date = 04/04/17 Pct Recovery = 87% Analysis Date = 04/02/17 Pct Recovery = 87% Analysis Date = 04/02/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/30/17 Pct Recovery = 87% Analysis Date = 03/28/17 Pct Recovery = 87% Analysis Date = 03/28/17 Pct Recovery = 87% Analysis Date = 03/26/17 Pct Recovery = 87% Analysis Date = 03/26/17 Pct Recovery = 87% Analysis Date = 03/24/17 Pct Recovery = 87% Analysis Date = 03/24/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/21/17 Pct Recovery = 87% Analysis Date = 03/19/17 Pct Recovery = 87% Analysis Date = 03/19/17 Pct Recovery = 87% Analysis Date = 03/17/17 Pct Recovery = 87% Analysis Date = 03/17/17 Pct Recovery = 87% Analysis Date = 03/14/17 Pct Recovery = 87% Analysis Date = 03/14/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/12/17 Pct Recovery = 87% Analysis Date = 03/10/17 Pct Recovery = 87% Analysis Date = 03/10/17 Pct Recovery = 87% Analysis Date = 03/08/17 Pct Recovery = 87% Analysis Date = 03/08/17 Pct Recovery = 87% Analysis Date = 03/05/17 Pct Recovery = 86% Analysis Date = 03/05/17 Pct Recovery = 86% Analysis Date = 03/03/17 Pct Recovery = 86% Analysis Date = 03/03/17 Pct Recovery = 86% Analysis Date = 03/01/17 Pct Recovery = 86% Analysis Date = 03/01/17 Pct Recovery = 86% Analysis Date = 02/26/17 Pct Recovery = 86% Analysis Date = 02/26/17 Pct Recovery = 86% Analysis Date = 02/24/17 Pct Recovery = 86% Analysis Date = 02/24/17 Pct Recovery = 86% Analysis Date = 02/22/17 Pct Recovery = 86% Analysis Date = 02/22/17 Pct Recovery = 86% Analysis Date = 02/20/17 Pct Recovery = 86% Analysis Date = 02/20/17 Pct Recovery = 86% Analysis Date = 02/17/17 Pct Recovery = 86% Analysis Date = 02/17/17 Pct Recovery = 86% Analysis Date = 02/15/17 Pct Recovery = 86% Analysis Date = 02/15/17 Pct Recovery = 86% Analysis Date = 02/13/17 Pct Recovery = 86% Analysis Date = 02/13/17 Pct Recovery = 86% Analysis Date = 02/10/17 Pct Recovery = 86% Analysis Date = 02/10/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/08/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/04/17 Pct Recovery = 85% Analysis Date = 02/04/17 Pct Recovery = 85% Analysis Date = 02/01/17 Pct Recovery = 85% Analysis Date = 02/01/17 Pct Recovery = 85% Analysis Date = 01/30/17 Pct Recovery = 85% Analysis Date = 01/30/17 Pct Recovery = 85% Analysis Date = 01/28/17 Pct Recovery = 85% Analysis Date = 01/28/17 Pct Recovery = 85% Analysis Date = 01/25/17 Pct Recovery = 85% Analysis Date = 01/25/17 Pct Recovery = 85% Analysis Date = 01/23/17 Pct Recovery = 85% Analysis Date = 01/23/17 Pct Recovery = 85% Analysis Date = 01/21/17 Pct Recovery = 85% Analysis Date = 01/21/17 Pct Recovery = 85% Analysis Date = 01/19/17 Pct Recovery = 85% Analysis Date = 01/19/17 Pct Recovery = 85% Analysis Date = 01/16/17 Pct Recovery = 85% Analysis Date = 01/16/17 Pct Recovery = 85% Analysis Date = 01/14/17 Pct Recovery = 85% Analysis Date = 01/14/17 Pct Recovery = 85% Analysis Date = 01/12/17 Pct Recovery = 85% Analysis Date = 01/12/17 Pct Recovery = 85% Analysis Date = 01/09/17 Pct Recovery = 85% Analysis Date = 01/09/17 Pct Recovery = 85% Analysis Date = 01/07/17 Pct Recovery = 84% Analysis Date = 01/07/17 Pct Recovery = 84% Analysis Date = 01/05/17 Pct Recovery = 84% Analysis Date = 01/05/17 Pct Recovery = 84% Analysis Date = 01/03/17 Pct Recovery = 84% Analysis Date = 01/03/17 Pct Recovery = 84% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/31/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/29/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/27/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/24/16 Pct Recovery = 84% Analysis Date = 12/22/16 Pct Recovery = 84% Analysis Date = 12/22/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/20/16 Pct Recovery = 84% Analysis Date = 12/18/16 Pct Recovery = 84% Analysis Date = 12/18/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 84% Analysis Date = 12/15/16 Pct Recovery = 84% Analysis Date = 12/13/16 Pct Recovery = 84% Analysis Date = 12/13/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/08/16 Pct Recovery = 84% Analysis Date = 12/08/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 84% Analysis Date = 12/04/16 Pct Recovery = 84% Analysis Date = 12/04/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 11/29/16 Pct Recovery = 84% Analysis Date = 11/29/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/25/16 Pct Recovery = 84% Analysis Date = 11/25/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/20/16 Pct Recovery = 84% Analysis Date = 11/20/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/04/16 Pct Recovery = 84% Analysis Date = 11/04/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 84% Analysis Date = 10/31/16 Pct Recovery = 84% Analysis Date = 10/31/16 Pct Recovery = 84% Analysis Date = 10/28/16 Pct Recovery = 84% Analysis Date = 10/28/16 Pct Recovery = 84% Analysis Date = 10/26/16 Pct Recovery = 84% Analysis Date = 10/26/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/24/16 Pct Recovery = 84% Analysis Date = 10/21/16 Pct Recovery = 84% Analysis Date = 10/21/16 Pct Recovery = 84% Analysis Date = 10/19/16 Pct Recovery = 84% Analysis Date = 10/19/16 Pct Recovery = 84% Analysis Date = 10/17/16 Pct Recovery = 84% Analysis Date = 10/17/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/15/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/12/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/10/16 Pct Recovery = 84% Analysis Date = 10/08/16 Pct Recovery = 84% Analysis Date = 10/08/16 Pct Recovery = 84% Analysis Date = 10/05/16 Pct Recovery = 84% Analysis Date = 10/05/16 Pct Recovery = 84% Analysis Date = 10/03/16 Pct Recovery = 84% Analysis Date = 10/03/16 Pct Recovery = 84% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 83% Analysis Date = 09/24/16 Pct Recovery = 83% Analysis Date = 09/24/16 Pct Recovery = 83% Analysis Date = 09/22/16 Pct Recovery = 83% Analysis Date = 09/22/16 Pct Recovery = 83% Analysis Date = 09/19/16 Pct Recovery = 83% Analysis Date = 09/19/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/17/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/15/16 Pct Recovery = 83% Analysis Date = 09/13/16 Pct Recovery = 83% Analysis Date = 09/13/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/10/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/08/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/06/16 Pct Recovery = 83% Analysis Date = 09/03/16 Pct Recovery = 83% Analysis Date = 09/03/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 09/01/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/30/16 Pct Recovery = 83% Analysis Date = 08/28/16 Pct Recovery = 83% Analysis Date = 08/28/16 Pct Recovery = 83% Analysis Date = 08/25/16 Pct Recovery = 82% Analysis Date = 08/25/16 Pct Recovery = 82% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/23/16 Pct Recovery = 82% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/18/16 Pct Recovery = 81% Analysis Date = 08/18/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/14/16 Pct Recovery = 80% Analysis Date = 08/14/16 Pct Recovery = 80% Analysis Date = 08/12/16 Pct Recovery = 80% Analysis Date = 08/12/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/09/16 Pct Recovery = 80% Analysis Date = 08/07/16 Pct Recovery = 79% Analysis Date = 08/07/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 79% Analysis Date = 08/05/16 Pct Recovery = 79% Analysis Date = 08/02/16 Pct Recovery = 79% Analysis Date = 08/02/16 Pct Recovery = 79% Analysis Date = 07/31/16 Pct Recovery = 78% Analysis Date = 07/31/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/29/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/27/16 Pct Recovery = 78% Analysis Date = 07/24/16 Pct Recovery = 77% Analysis Date = 07/24/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/22/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/20/16 Pct Recovery = 77% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/17/16 Pct Recovery = 76% Analysis Date = 07/15/16 Pct Recovery = 76% Analysis Date = 07/15/16 Pct Recovery = 76% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/13/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/11/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 75% Analysis Date = 07/08/16 Pct Recovery = 75% Analysis Date = 07/06/16 Pct Recovery = 74% Analysis Date = 07/06/16 Pct Recovery = 74% Analysis Date = 07/04/16 Pct Recovery = 74% Analysis Date = 07/04/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 07/01/16 Pct Recovery = 74% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/29/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/27/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/25/16 Pct Recovery = 73% Analysis Date = 06/22/16 Pct Recovery = 72% Analysis Date = 06/22/16 Pct Recovery = 72% Analysis Date = 06/20/16 Pct Recovery = 72% Analysis Date = 06/20/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/18/16 Pct Recovery = 72% Analysis Date = 06/15/16 Pct Recovery = 71% Analysis Date = 06/15/16 Pct Recovery = 71% Analysis Date = 06/13/16 Pct Recovery = 71% Analysis Date = 06/13/16 Pct Recovery = 71% Analysis Date = 06/11/16 Pct Recovery = 71% Analysis Date = 06/11/16 Pct Recovery = 71% Analysis Date = 06/09/16 Pct Recovery = 70% Analysis Date = 06/09/16 Pct Recovery = 70% Analysis Date = 06/06/16 Pct Recovery = 70% Analysis Date = 06/06/16 Pct Recovery = 70% Analysis Date = 06/04/16 Pct Recovery = 69% Analysis Date = 06/04/16 Pct Recovery = 69% Analysis Date = 06/02/16 Pct Recovery = 69% Analysis Date = 06/02/16 Pct Recovery = 69% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/30/16 Pct Recovery = 69% Analysis Date = 05/28/16 Pct Recovery = 68% Analysis Date = 05/28/16 Pct Recovery = 68% Analysis Date = 05/26/16 Pct Recovery = 68% Analysis Date = 05/26/16 Pct Recovery = 68% Analysis Date = 05/24/16 Pct Recovery = 68% Analysis Date = 05/24/16 Pct Recovery = 68% Analysis Date = 05/21/16 Pct Recovery = 68% Analysis Date = 05/21/16 Pct Recovery = 68% Analysis Date = 05/19/16 Pct Recovery = 68% Analysis Date = 05/19/16 Pct Recovery = 68% Analysis Date = 05/17/16 Pct Recovery = 68% Analysis Date = 05/17/16 Pct Recovery = 68% Analysis Date = 05/14/16 Pct Recovery = 67% Analysis Date = 05/14/16 Pct Recovery = 67% Analysis Date = 05/12/16 Pct Recovery = 67% Analysis Date = 05/12/16 Pct Recovery = 67% Analysis Date = 05/10/16 Pct Recovery = 67% Analysis Date = 05/10/16 Pct Recovery = 67% Analysis Date = 05/08/16 Pct Recovery = 67% Analysis Date = 05/08/16 Pct Recovery = 67% Analysis Date = 05/05/16 Pct Recovery = 67% Analysis Date = 05/05/16 Pct Recovery = 67% Analysis Date = 05/03/16 Pct Recovery = 67% Analysis Date = 05/03/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 05/01/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/28/16 Pct Recovery = 67% Analysis Date = 04/26/16 Pct Recovery = 67% Analysis Date = 04/26/16 Pct Recovery = 67% Analysis Date = 04/24/16 Pct Recovery = 67% Analysis Date = 04/24/16 Pct Recovery = 67% Analysis Date = 04/22/16 Pct Recovery = 67% Analysis Date = 04/22/16 Pct Recovery = 67% Analysis Date = 04/19/16 Pct Recovery = 67% Analysis Date = 04/19/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/17/16 Pct Recovery = 67% Analysis Date = 04/15/16 Pct Recovery = 68% Analysis Date = 04/15/16 Pct Recovery = 68% Analysis Date = 04/12/16 Pct Recovery = 68% Analysis Date = 04/12/16 Pct Recovery = 68% Analysis Date = 04/10/16 Pct Recovery = 68% Analysis Date = 04/10/16 Pct Recovery = 68% Analysis Date = 04/08/16 Pct Recovery = 68% Analysis Date = 04/08/16 Pct Recovery = 68% Analysis Date = 04/06/16 Pct Recovery = 68% Analysis Date = 04/06/16 Pct Recovery = 68% Analysis Date = 04/03/16 Pct Recovery = 68% Analysis Date = 04/03/16 Pct Recovery = 68% Analysis Date = 04/01/16 Pct Recovery = 68% Analysis Date = 04/01/16 Pct Recovery = 68% Analysis Date = 03/30/16 Pct Recovery = 69% Analysis Date = 03/30/16 Pct Recovery = 69% Analysis Date = 03/27/16 Pct Recovery = 69% Analysis Date = 03/27/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/25/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 69% Analysis Date = 03/23/16 Pct Recovery = 69% Analysis Date = 03/21/16 Pct Recovery = 69% Analysis Date = 03/21/16 Pct Recovery = 69% Analysis Date = 03/18/16 Pct Recovery = 70% Analysis Date = 03/18/16 Pct Recovery = 70% Analysis Date = 03/16/16 Pct Recovery = 70% Analysis Date = 03/16/16 Pct Recovery = 70% Analysis Date = 03/14/16 Pct Recovery = 70% Analysis Date = 03/14/16 Pct Recovery = 70% Analysis Date = 03/11/16 Pct Recovery = 70% Analysis Date = 03/11/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 70% Analysis Date = 03/09/16 Pct Recovery = 70% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/07/16 Pct Recovery = 71% Analysis Date = 03/05/16 Pct Recovery = 71% Analysis Date = 03/05/16 Pct Recovery = 71% Analysis Date = 03/02/16 Pct Recovery = 71% Analysis Date = 03/02/16 Pct Recovery = 71% Analysis Date = 02/29/16 Pct Recovery = 71% Analysis Date = 02/29/16 Pct Recovery = 71% Analysis Date = 02/27/16 Pct Recovery = 71% Analysis Date = 02/27/16 Pct Recovery = 71% Analysis Date = 02/24/16 Pct Recovery = 72% Analysis Date = 02/24/16 Pct Recovery = 72% Analysis Date = 02/22/16 Pct Recovery = 72% Analysis Date = 02/22/16 Pct Recovery = 72% Analysis Date = 02/20/16 Pct Recovery = 72% Analysis Date = 02/20/16 Pct Recovery = 72% Analysis Date = 02/18/16 Pct Recovery = 72% Analysis Date = 02/18/16 Pct Recovery = 72% Analysis Date = 02/15/16 Pct Recovery = 72% Analysis Date = 02/15/16 Pct Recovery = 72% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/13/16 Pct Recovery = 73% Analysis Date = 02/11/16 Pct Recovery = 73% Analysis Date = 02/11/16 Pct Recovery = 73% Analysis Date = 02/09/16 Pct Recovery = 73% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
THIOBENCARB

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 20 78% 15% 78% 17%
Total 20 78% 15% 78% 17%

Sample Statistics
THIOBENCARB

Characteristic N % % Basis
Plotted 20 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 20 .  
False Negatives 0 0% 0 out of 20
Not Spiked 8 .  
False Positives 0 0% 0 out of 8

OBSP Determination:
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))
METHOD: 2033 , TESTIDCODE: 61610GCM39

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 66% Analysis Date = 02/16/17 SpikeMix = Abs 060916: 100 µl & Phenova B20160331: 100 µl Pct Recovery = 61% Analysis Date = 02/28/17 SpikeMix = Abs 060916: 80 µl & Phenova B20160331: 80 µl Pct Recovery = 68% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 70% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 50% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 71% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 63% Analysis Date = 05/03/17 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 87% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 95% Analysis Date = 12/20/16 SpikeMix = Abs 060916: 40 µl & Phenova B20160331: 40 µl Pct Recovery = 78% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 67% Analysis Date = 09/01/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 61% Analysis Date = 05/28/16 SpikeMix = Crescent 03FF076: 40 µl & NSI 041816: 40 µl Pct Recovery = 66% Analysis Date = 05/26/16 SpikeMix = NSI 041816: 40 µl & Crescent 03FF076: 40 µl Pct Recovery = 68% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 67% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 74% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 74% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 80% Analysis Date = 05/02/17 Pct Recovery = 77% Analysis Date = 04/30/17 Pct Recovery = 77% Analysis Date = 04/30/17 Pct Recovery = 77% Analysis Date = 04/28/17 Pct Recovery = 77% Analysis Date = 04/28/17 Pct Recovery = 77% Analysis Date = 04/26/17 Pct Recovery = 77% Analysis Date = 04/26/17 Pct Recovery = 77% Analysis Date = 04/24/17 Pct Recovery = 77% Analysis Date = 04/24/17 Pct Recovery = 77% Analysis Date = 04/21/17 Pct Recovery = 77% Analysis Date = 04/21/17 Pct Recovery = 77% Analysis Date = 04/19/17 Pct Recovery = 77% Analysis Date = 04/19/17 Pct Recovery = 77% Analysis Date = 04/17/17 Pct Recovery = 77% Analysis Date = 04/17/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/15/17 Pct Recovery = 77% Analysis Date = 04/12/17 Pct Recovery = 77% Analysis Date = 04/12/17 Pct Recovery = 77% Analysis Date = 04/10/17 Pct Recovery = 77% Analysis Date = 04/10/17 Pct Recovery = 77% Analysis Date = 04/08/17 Pct Recovery = 77% Analysis Date = 04/08/17 Pct Recovery = 77% Analysis Date = 04/06/17 Pct Recovery = 76% Analysis Date = 04/06/17 Pct Recovery = 76% Analysis Date = 04/03/17 Pct Recovery = 76% Analysis Date = 04/03/17 Pct Recovery = 76% Analysis Date = 04/01/17 Pct Recovery = 76% Analysis Date = 04/01/17 Pct Recovery = 76% Analysis Date = 03/30/17 Pct Recovery = 76% Analysis Date = 03/30/17 Pct Recovery = 76% Analysis Date = 03/28/17 Pct Recovery = 76% Analysis Date = 03/28/17 Pct Recovery = 76% Analysis Date = 03/25/17 Pct Recovery = 76% Analysis Date = 03/25/17 Pct Recovery = 76% Analysis Date = 03/23/17 Pct Recovery = 76% Analysis Date = 03/23/17 Pct Recovery = 76% Analysis Date = 03/21/17 Pct Recovery = 76% Analysis Date = 03/21/17 Pct Recovery = 76% Analysis Date = 03/19/17 Pct Recovery = 76% Analysis Date = 03/19/17 Pct Recovery = 76% Analysis Date = 03/16/17 Pct Recovery = 76% Analysis Date = 03/16/17 Pct Recovery = 76% Analysis Date = 03/14/17 Pct Recovery = 76% Analysis Date = 03/14/17 Pct Recovery = 76% Analysis Date = 03/12/17 Pct Recovery = 76% Analysis Date = 03/12/17 Pct Recovery = 76% Analysis Date = 03/10/17 Pct Recovery = 75% Analysis Date = 03/10/17 Pct Recovery = 75% Analysis Date = 03/07/17 Pct Recovery = 75% Analysis Date = 03/07/17 Pct Recovery = 75% Analysis Date = 03/05/17 Pct Recovery = 75% Analysis Date = 03/05/17 Pct Recovery = 75% Analysis Date = 03/03/17 Pct Recovery = 75% Analysis Date = 03/03/17 Pct Recovery = 75% Analysis Date = 03/01/17 Pct Recovery = 75% Analysis Date = 03/01/17 Pct Recovery = 75% Analysis Date = 02/26/17 Pct Recovery = 75% Analysis Date = 02/26/17 Pct Recovery = 75% Analysis Date = 02/24/17 Pct Recovery = 75% Analysis Date = 02/24/17 Pct Recovery = 75% Analysis Date = 02/22/17 Pct Recovery = 75% Analysis Date = 02/22/17 Pct Recovery = 75% Analysis Date = 02/20/17 Pct Recovery = 75% Analysis Date = 02/20/17 Pct Recovery = 75% Analysis Date = 02/17/17 Pct Recovery = 75% Analysis Date = 02/17/17 Pct Recovery = 75% Analysis Date = 02/15/17 Pct Recovery = 75% Analysis Date = 02/15/17 Pct Recovery = 75% Analysis Date = 02/13/17 Pct Recovery = 75% Analysis Date = 02/13/17 Pct Recovery = 75% Analysis Date = 02/11/17 Pct Recovery = 75% Analysis Date = 02/11/17 Pct Recovery = 75% Analysis Date = 02/08/17 Pct Recovery = 75% Analysis Date = 02/08/17 Pct Recovery = 75% Analysis Date = 02/06/17 Pct Recovery = 74% Analysis Date = 02/06/17 Pct Recovery = 74% Analysis Date = 02/04/17 Pct Recovery = 74% Analysis Date = 02/04/17 Pct Recovery = 74% Analysis Date = 02/02/17 Pct Recovery = 74% Analysis Date = 02/02/17 Pct Recovery = 74% Analysis Date = 01/30/17 Pct Recovery = 74% Analysis Date = 01/30/17 Pct Recovery = 74% Analysis Date = 01/28/17 Pct Recovery = 74% Analysis Date = 01/28/17 Pct Recovery = 74% Analysis Date = 01/26/17 Pct Recovery = 74% Analysis Date = 01/26/17 Pct Recovery = 74% Analysis Date = 01/24/17 Pct Recovery = 74% Analysis Date = 01/24/17 Pct Recovery = 74% Analysis Date = 01/21/17 Pct Recovery = 74% Analysis Date = 01/21/17 Pct Recovery = 74% Analysis Date = 01/19/17 Pct Recovery = 73% Analysis Date = 01/19/17 Pct Recovery = 73% Analysis Date = 01/17/17 Pct Recovery = 73% Analysis Date = 01/17/17 Pct Recovery = 73% Analysis Date = 01/15/17 Pct Recovery = 73% Analysis Date = 01/15/17 Pct Recovery = 73% Analysis Date = 01/12/17 Pct Recovery = 73% Analysis Date = 01/12/17 Pct Recovery = 73% Analysis Date = 01/10/17 Pct Recovery = 73% Analysis Date = 01/10/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/08/17 Pct Recovery = 73% Analysis Date = 01/06/17 Pct Recovery = 73% Analysis Date = 01/06/17 Pct Recovery = 73% Analysis Date = 01/04/17 Pct Recovery = 73% Analysis Date = 01/04/17 Pct Recovery = 73% Analysis Date = 01/01/17 Pct Recovery = 73% Analysis Date = 01/01/17 Pct Recovery = 73% Analysis Date = 12/30/16 Pct Recovery = 72% Analysis Date = 12/30/16 Pct Recovery = 72% Analysis Date = 12/28/16 Pct Recovery = 72% Analysis Date = 12/28/16 Pct Recovery = 72% Analysis Date = 12/26/16 Pct Recovery = 72% Analysis Date = 12/26/16 Pct Recovery = 72% Analysis Date = 12/23/16 Pct Recovery = 72% Analysis Date = 12/23/16 Pct Recovery = 72% Analysis Date = 12/21/16 Pct Recovery = 72% Analysis Date = 12/21/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/19/16 Pct Recovery = 72% Analysis Date = 12/17/16 Pct Recovery = 72% Analysis Date = 12/17/16 Pct Recovery = 72% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/14/16 Pct Recovery = 71% Analysis Date = 12/12/16 Pct Recovery = 71% Analysis Date = 12/12/16 Pct Recovery = 71% Analysis Date = 12/10/16 Pct Recovery = 71% Analysis Date = 12/10/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/08/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 12/05/16 Pct Recovery = 71% Analysis Date = 12/03/16 Pct Recovery = 70% Analysis Date = 12/03/16 Pct Recovery = 70% Analysis Date = 12/01/16 Pct Recovery = 70% Analysis Date = 12/01/16 Pct Recovery = 70% Analysis Date = 11/29/16 Pct Recovery = 70% Analysis Date = 11/29/16 Pct Recovery = 70% Analysis Date = 11/26/16 Pct Recovery = 70% Analysis Date = 11/26/16 Pct Recovery = 70% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/24/16 Pct Recovery = 70% Analysis Date = 11/22/16 Pct Recovery = 70% Analysis Date = 11/22/16 Pct Recovery = 70% Analysis Date = 11/20/16 Pct Recovery = 69% Analysis Date = 11/20/16 Pct Recovery = 69% Analysis Date = 11/17/16 Pct Recovery = 69% Analysis Date = 11/17/16 Pct Recovery = 69% Analysis Date = 11/15/16 Pct Recovery = 69% Analysis Date = 11/15/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 69% Analysis Date = 11/13/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/11/16 Pct Recovery = 69% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/08/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/06/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/04/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 11/02/16 Pct Recovery = 68% Analysis Date = 10/30/16 Pct Recovery = 68% Analysis Date = 10/30/16 Pct Recovery = 68% Analysis Date = 10/28/16 Pct Recovery = 67% Analysis Date = 10/28/16 Pct Recovery = 67% Analysis Date = 10/26/16 Pct Recovery = 67% Analysis Date = 10/26/16 Pct Recovery = 67% Analysis Date = 10/24/16 Pct Recovery = 67% Analysis Date = 10/24/16 Pct Recovery = 67% Analysis Date = 10/21/16 Pct Recovery = 67% Analysis Date = 10/21/16 Pct Recovery = 67% Analysis Date = 10/19/16 Pct Recovery = 67% Analysis Date = 10/19/16 Pct Recovery = 67% Analysis Date = 10/17/16 Pct Recovery = 66% Analysis Date = 10/17/16 Pct Recovery = 66% Analysis Date = 10/15/16 Pct Recovery = 66% Analysis Date = 10/15/16 Pct Recovery = 66% Analysis Date = 10/12/16 Pct Recovery = 66% Analysis Date = 10/12/16 Pct Recovery = 66% Analysis Date = 10/10/16 Pct Recovery = 66% Analysis Date = 10/10/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 66% Analysis Date = 10/08/16 Pct Recovery = 66% Analysis Date = 10/06/16 Pct Recovery = 65% Analysis Date = 10/06/16 Pct Recovery = 65% Analysis Date = 10/03/16 Pct Recovery = 65% Analysis Date = 10/03/16 Pct Recovery = 65% Analysis Date = 10/01/16 Pct Recovery = 65% Analysis Date = 10/01/16 Pct Recovery = 65% Analysis Date = 09/29/16 Pct Recovery = 65% Analysis Date = 09/29/16 Pct Recovery = 65% Analysis Date = 09/27/16 Pct Recovery = 65% Analysis Date = 09/27/16 Pct Recovery = 65% Analysis Date = 09/24/16 Pct Recovery = 65% Analysis Date = 09/24/16 Pct Recovery = 65% Analysis Date = 09/22/16 Pct Recovery = 64% Analysis Date = 09/22/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/20/16 Pct Recovery = 64% Analysis Date = 09/18/16 Pct Recovery = 64% Analysis Date = 09/18/16 Pct Recovery = 64% Analysis Date = 09/16/16 Pct Recovery = 64% Analysis Date = 09/16/16 Pct Recovery = 64% Analysis Date = 09/13/16 Pct Recovery = 64% Analysis Date = 09/13/16 Pct Recovery = 64% Analysis Date = 09/11/16 Pct Recovery = 63% Analysis Date = 09/11/16 Pct Recovery = 63% Analysis Date = 09/09/16 Pct Recovery = 63% Analysis Date = 09/09/16 Pct Recovery = 63% Analysis Date = 09/07/16 Pct Recovery = 63% Analysis Date = 09/07/16 Pct Recovery = 63% Analysis Date = 09/04/16 Pct Recovery = 63% Analysis Date = 09/04/16 Pct Recovery = 63% Analysis Date = 09/02/16 Pct Recovery = 63% Analysis Date = 09/02/16 Pct Recovery = 63% Analysis Date = 08/31/16 Pct Recovery = 62% Analysis Date = 08/31/16 Pct Recovery = 62% Analysis Date = 08/29/16 Pct Recovery = 63% Analysis Date = 08/29/16 Pct Recovery = 63% Analysis Date = 08/26/16 Pct Recovery = 63% Analysis Date = 08/26/16 Pct Recovery = 63% Analysis Date = 08/24/16 Pct Recovery = 63% Analysis Date = 08/24/16 Pct Recovery = 63% Analysis Date = 08/22/16 Pct Recovery = 63% Analysis Date = 08/22/16 Pct Recovery = 63% Analysis Date = 08/20/16 Pct Recovery = 63% Analysis Date = 08/20/16 Pct Recovery = 63% Analysis Date = 08/17/16 Pct Recovery = 63% Analysis Date = 08/17/16 Pct Recovery = 63% Analysis Date = 08/15/16 Pct Recovery = 63% Analysis Date = 08/15/16 Pct Recovery = 63% Analysis Date = 08/13/16 Pct Recovery = 63% Analysis Date = 08/13/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/11/16 Pct Recovery = 63% Analysis Date = 08/08/16 Pct Recovery = 63% Analysis Date = 08/08/16 Pct Recovery = 63% Analysis Date = 08/06/16 Pct Recovery = 64% Analysis Date = 08/06/16 Pct Recovery = 64% Analysis Date = 08/04/16 Pct Recovery = 64% Analysis Date = 08/04/16 Pct Recovery = 64% Analysis Date = 08/02/16 Pct Recovery = 64% Analysis Date = 08/02/16 Pct Recovery = 64% Analysis Date = 07/30/16 Pct Recovery = 64% Analysis Date = 07/30/16 Pct Recovery = 64% Analysis Date = 07/28/16 Pct Recovery = 64% Analysis Date = 07/28/16 Pct Recovery = 64% Analysis Date = 07/26/16 Pct Recovery = 64% Analysis Date = 07/26/16 Pct Recovery = 64% Analysis Date = 07/24/16 Pct Recovery = 64% Analysis Date = 07/24/16 Pct Recovery = 64% Analysis Date = 07/21/16 Pct Recovery = 64% Analysis Date = 07/21/16 Pct Recovery = 64% Analysis Date = 07/19/16 Pct Recovery = 64% Analysis Date = 07/19/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/17/16 Pct Recovery = 64% Analysis Date = 07/15/16 Pct Recovery = 64% Analysis Date = 07/15/16 Pct Recovery = 64% Analysis Date = 07/12/16 Pct Recovery = 65% Analysis Date = 07/12/16 Pct Recovery = 65% Analysis Date = 07/10/16 Pct Recovery = 65% Analysis Date = 07/10/16 Pct Recovery = 65% Analysis Date = 07/08/16 Pct Recovery = 65% Analysis Date = 07/08/16 Pct Recovery = 65% Analysis Date = 07/06/16 Pct Recovery = 65% Analysis Date = 07/06/16 Pct Recovery = 65% Analysis Date = 07/03/16 Pct Recovery = 65% Analysis Date = 07/03/16 Pct Recovery = 65% Analysis Date = 07/01/16 Pct Recovery = 65% Analysis Date = 07/01/16 Pct Recovery = 65% Analysis Date = 06/29/16 Pct Recovery = 65% Analysis Date = 06/29/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/27/16 Pct Recovery = 65% Analysis Date = 06/24/16 Pct Recovery = 65% Analysis Date = 06/24/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/22/16 Pct Recovery = 65% Analysis Date = 06/20/16 Pct Recovery = 66% Analysis Date = 06/20/16 Pct Recovery = 66% Analysis Date = 06/18/16 Pct Recovery = 66% Analysis Date = 06/18/16 Pct Recovery = 66% Analysis Date = 06/15/16 Pct Recovery = 66% Analysis Date = 06/15/16 Pct Recovery = 66% Analysis Date = 06/13/16 Pct Recovery = 66% Analysis Date = 06/13/16 Pct Recovery = 66% Analysis Date = 06/11/16 Pct Recovery = 66% Analysis Date = 06/11/16 Pct Recovery = 66% Analysis Date = 06/09/16 Pct Recovery = 66% Analysis Date = 06/09/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/06/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/04/16 Pct Recovery = 66% Analysis Date = 06/02/16 Pct Recovery = 66% Analysis Date = 06/02/16 Pct Recovery = 66% Analysis Date = 05/31/16 Pct Recovery = 66% Analysis Date = 05/31/16 Pct Recovery = 66% Analysis Date = 05/29/16 Pct Recovery = 66% Analysis Date = 05/29/16 Pct Recovery = 66% Analysis Date = 05/26/16 Pct Recovery = 67% Analysis Date = 05/26/16 Pct Recovery = 67% Analysis Date = 05/24/16 Pct Recovery = 67% Analysis Date = 05/24/16 Pct Recovery = 67% Analysis Date = 05/22/16 Pct Recovery = 67% Analysis Date = 05/22/16 Pct Recovery = 67% Analysis Date = 05/20/16 Pct Recovery = 68% Analysis Date = 05/20/16 Pct Recovery = 68% Analysis Date = 05/17/16 Pct Recovery = 68% Analysis Date = 05/17/16 Pct Recovery = 68% Analysis Date = 05/15/16 Pct Recovery = 68% Analysis Date = 05/15/16 Pct Recovery = 68% Analysis Date = 05/13/16 Pct Recovery = 68% Analysis Date = 05/13/16 Pct Recovery = 68% Analysis Date = 05/11/16 Pct Recovery = 69% Analysis Date = 05/11/16 Pct Recovery = 69% Analysis Date = 05/08/16 Pct Recovery = 69% Analysis Date = 05/08/16 Pct Recovery = 69% Analysis Date = 05/06/16 Pct Recovery = 69% Analysis Date = 05/06/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 69% Analysis Date = 05/04/16 Pct Recovery = 69% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 05/02/16 Pct Recovery = 70% Analysis Date = 04/29/16 Pct Recovery = 70% Analysis Date = 04/29/16 Pct Recovery = 70% Analysis Date = 04/27/16 Pct Recovery = 70% Analysis Date = 04/27/16 Pct Recovery = 70% Analysis Date = 04/25/16 Pct Recovery = 70% Analysis Date = 04/25/16 Pct Recovery = 70% Analysis Date = 04/23/16 Pct Recovery = 70% Analysis Date = 04/23/16 Pct Recovery = 70% Analysis Date = 04/20/16 Pct Recovery = 71% Analysis Date = 04/20/16 Pct Recovery = 71% Analysis Date = 04/18/16 Pct Recovery = 71% Analysis Date = 04/18/16 Pct Recovery = 71% Analysis Date = 04/16/16 Pct Recovery = 71% Analysis Date = 04/16/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/14/16 Pct Recovery = 71% Analysis Date = 04/11/16 Pct Recovery = 71% Analysis Date = 04/11/16 Pct Recovery = 71% Analysis Date = 04/09/16 Pct Recovery = 71% Analysis Date = 04/09/16 Pct Recovery = 71% Analysis Date = 04/07/16 Pct Recovery = 72% Analysis Date = 04/07/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 72% Analysis Date = 04/05/16 Pct Recovery = 72% Analysis Date = 04/02/16 Pct Recovery = 72% Analysis Date = 04/02/16 Pct Recovery = 72% Analysis Date = 03/31/16 Pct Recovery = 72% Analysis Date = 03/31/16 Pct Recovery = 72% Analysis Date = 03/29/16 Pct Recovery = 72% Analysis Date = 03/29/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/27/16 Pct Recovery = 72% Analysis Date = 03/24/16 Pct Recovery = 73% Analysis Date = 03/24/16 Pct Recovery = 73% Analysis Date = 03/22/16 Pct Recovery = 73% Analysis Date = 03/22/16 Pct Recovery = 73% Analysis Date = 03/20/16 Pct Recovery = 73% Analysis Date = 03/20/16 Pct Recovery = 73% Analysis Date = 03/18/16 Pct Recovery = 73% Analysis Date = 03/18/16 Pct Recovery = 73% Analysis Date = 03/15/16 Pct Recovery = 73% Analysis Date = 03/15/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/13/16 Pct Recovery = 73% Analysis Date = 03/11/16 Pct Recovery = 74% Analysis Date = 03/11/16 Pct Recovery = 74% Analysis Date = 03/09/16 Pct Recovery = 74% Analysis Date = 03/09/16 Pct Recovery = 74% Analysis Date = 03/06/16 Pct Recovery = 74% Analysis Date = 03/06/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/04/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 03/02/16 Pct Recovery = 74% Analysis Date = 02/29/16 Pct Recovery = 74% Analysis Date = 02/29/16 Pct Recovery = 74% Analysis Date = 02/26/16 Pct Recovery = 75% Analysis Date = 02/26/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/24/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/22/16 Pct Recovery = 75% Analysis Date = 02/20/16 Pct Recovery = 75% Analysis Date = 02/20/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/17/16 Pct Recovery = 75% Analysis Date = 02/15/16 Pct Recovery = 75% Analysis Date = 02/15/16 Pct Recovery = 75% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/13/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 76% Analysis Date = 02/11/16 Pct Recovery = 76% Analysis Date = 02/09/16 Pct Recovery = 76% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 71% 10% 68% 9%
Total 19 71% 10% 68% 9%

Sample Statistics
TRIBUFOS (S,S,S-TRIBUTYLPHOSPHOROTRITHIOATE (DEF))

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 19 100% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9

OBSP Determination:
TRIFLURALIN
METHOD: 2033 , TESTIDCODE: 82661GCM35

Analysis Date = 02/22/17 SpikeMix = ChemService 5054800: 100 µl & Abs 060916: 100 µl Pct Recovery = 73% Analysis Date = 09/09/16 SpikeMix = Crescent 03FF076: 100 µl & ChemService 5054800: 100 µl Pct Recovery = 93% Analysis Date = 02/22/17 SpikeMix = Phenova B20160331: 100 µl & Supelco LC20138V: 100 µl Pct Recovery = 79% Analysis Date = 05/11/17 SpikeMix = ChemService 5054800: 80 µl & Crescent 03FF076: 80 µl Pct Recovery = 70% Analysis Date = 08/27/16 SpikeMix = ChemService 5054800: 80 µl & NSI 041816: 80 µl Pct Recovery = 61% Analysis Date = 03/21/17 SpikeMix = Supelco LC20138V: 80 µl & NSI 041816: 80 µl Pct Recovery = 82% Analysis Date = 08/19/16 SpikeMix = Supelco LC20138V: 80 µl & Pheonva B20160331: 80 µl Pct Recovery = 78% Analysis Date = 05/19/16 SpikeMix = ChemService 3851600: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 79% Analysis Date = 04/19/16 SpikeMix = ERA 0406-15-01: 40 µl & Spex Organics EN150513008: 40 µl Pct Recovery = 82% Analysis Date = 04/24/17 SpikeMix = Crescent 03FF076: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 78% Analysis Date = 02/27/17 SpikeMix = ChemService 5054800: 40 µl & Abs 060916: 40 µl Pct Recovery = 87% Analysis Date = 09/20/16 SpikeMix = Phenova B20160331: 40 µl & ChemService 5054800: 40 µl Pct Recovery = 103% Analysis Date = 03/16/17 SpikeMix = Supelco LC20138V: 40 µl & Abs 060916: 40 µl Pct Recovery = 107% Analysis Date = 01/18/17 SpikeMix = Crescent 03FF076: 40 µl & Supelco LC20138V: 40 µl Pct Recovery = 89% Analysis Date = 09/14/16 SpikeMix = Supelco LC20138V: 40 µl & NSI 041816: 40 µl Pct Recovery = 69% Analysis Date = 05/04/16 SpikeMix = Abs 041415: 20 µl & Abs 040615: 20 µl Pct Recovery = 89% Analysis Date = 04/14/16 SpikeMix = ChemService 3851600: 20 µl & Abs 040615: 20 µl Pct Recovery = 99% Analysis Date = 04/06/16 SpikeMix = Spex Organics EN150513008: 20 µl & Abs 041415: 20 µl Pct Recovery = 92% Analysis Date = 02/09/16 SpikeMix = Abs 040615: 20 µl & Spex Organics EN150514012: 20 µl Pct Recovery = 69% Analysis Date = 05/10/17 Pct Recovery = 76% Analysis Date = 05/08/17 Pct Recovery = 77% Analysis Date = 05/08/17 Pct Recovery = 77% Analysis Date = 05/06/17 Pct Recovery = 77% Analysis Date = 05/06/17 Pct Recovery = 77% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/04/17 Pct Recovery = 77% Analysis Date = 05/01/17 Pct Recovery = 78% Analysis Date = 05/01/17 Pct Recovery = 78% Analysis Date = 04/29/17 Pct Recovery = 78% Analysis Date = 04/29/17 Pct Recovery = 78% Analysis Date = 04/27/17 Pct Recovery = 78% Analysis Date = 04/27/17 Pct Recovery = 78% Analysis Date = 04/25/17 Pct Recovery = 78% Analysis Date = 04/25/17 Pct Recovery = 78% Analysis Date = 04/22/17 Pct Recovery = 79% Analysis Date = 04/22/17 Pct Recovery = 79% Analysis Date = 04/20/17 Pct Recovery = 79% Analysis Date = 04/20/17 Pct Recovery = 79% Analysis Date = 04/18/17 Pct Recovery = 79% Analysis Date = 04/18/17 Pct Recovery = 79% Analysis Date = 04/15/17 Pct Recovery = 79% Analysis Date = 04/15/17 Pct Recovery = 79% Analysis Date = 04/13/17 Pct Recovery = 80% Analysis Date = 04/13/17 Pct Recovery = 80% Analysis Date = 04/11/17 Pct Recovery = 80% Analysis Date = 04/11/17 Pct Recovery = 80% Analysis Date = 04/09/17 Pct Recovery = 80% Analysis Date = 04/09/17 Pct Recovery = 80% Analysis Date = 04/06/17 Pct Recovery = 81% Analysis Date = 04/06/17 Pct Recovery = 81% Analysis Date = 04/04/17 Pct Recovery = 81% Analysis Date = 04/04/17 Pct Recovery = 81% Analysis Date = 04/02/17 Pct Recovery = 81% Analysis Date = 04/02/17 Pct Recovery = 81% Analysis Date = 03/30/17 Pct Recovery = 81% Analysis Date = 03/30/17 Pct Recovery = 81% Analysis Date = 03/28/17 Pct Recovery = 82% Analysis Date = 03/28/17 Pct Recovery = 82% Analysis Date = 03/26/17 Pct Recovery = 82% Analysis Date = 03/26/17 Pct Recovery = 82% Analysis Date = 03/24/17 Pct Recovery = 82% Analysis Date = 03/24/17 Pct Recovery = 82% Analysis Date = 03/21/17 Pct Recovery = 82% Analysis Date = 03/21/17 Pct Recovery = 82% Analysis Date = 03/19/17 Pct Recovery = 83% Analysis Date = 03/19/17 Pct Recovery = 83% Analysis Date = 03/17/17 Pct Recovery = 83% Analysis Date = 03/17/17 Pct Recovery = 83% Analysis Date = 03/14/17 Pct Recovery = 83% Analysis Date = 03/14/17 Pct Recovery = 83% Analysis Date = 03/12/17 Pct Recovery = 83% Analysis Date = 03/12/17 Pct Recovery = 83% Analysis Date = 03/10/17 Pct Recovery = 84% Analysis Date = 03/10/17 Pct Recovery = 84% Analysis Date = 03/08/17 Pct Recovery = 84% Analysis Date = 03/08/17 Pct Recovery = 84% Analysis Date = 03/05/17 Pct Recovery = 84% Analysis Date = 03/05/17 Pct Recovery = 84% Analysis Date = 03/03/17 Pct Recovery = 84% Analysis Date = 03/03/17 Pct Recovery = 84% Analysis Date = 03/01/17 Pct Recovery = 85% Analysis Date = 03/01/17 Pct Recovery = 85% Analysis Date = 02/26/17 Pct Recovery = 85% Analysis Date = 02/26/17 Pct Recovery = 85% Analysis Date = 02/24/17 Pct Recovery = 85% Analysis Date = 02/24/17 Pct Recovery = 85% Analysis Date = 02/22/17 Pct Recovery = 85% Analysis Date = 02/22/17 Pct Recovery = 85% Analysis Date = 02/20/17 Pct Recovery = 85% Analysis Date = 02/20/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/17/17 Pct Recovery = 85% Analysis Date = 02/15/17 Pct Recovery = 85% Analysis Date = 02/15/17 Pct Recovery = 85% Analysis Date = 02/13/17 Pct Recovery = 85% Analysis Date = 02/13/17 Pct Recovery = 85% Analysis Date = 02/10/17 Pct Recovery = 85% Analysis Date = 02/10/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 85% Analysis Date = 02/08/17 Pct Recovery = 85% Analysis Date = 02/06/17 Pct Recovery = 85% Analysis Date = 02/06/17 Pct Recovery = 85% Analysis Date = 02/04/17 Pct Recovery = 85% Analysis Date = 02/04/17 Pct Recovery = 85% Analysis Date = 02/01/17 Pct Recovery = 85% Analysis Date = 02/01/17 Pct Recovery = 85% Analysis Date = 01/30/17 Pct Recovery = 85% Analysis Date = 01/30/17 Pct Recovery = 85% Analysis Date = 01/28/17 Pct Recovery = 85% Analysis Date = 01/28/17 Pct Recovery = 85% Analysis Date = 01/25/17 Pct Recovery = 85% Analysis Date = 01/25/17 Pct Recovery = 85% Analysis Date = 01/23/17 Pct Recovery = 85% Analysis Date = 01/23/17 Pct Recovery = 85% Analysis Date = 01/21/17 Pct Recovery = 85% Analysis Date = 01/21/17 Pct Recovery = 85% Analysis Date = 01/19/17 Pct Recovery = 85% Analysis Date = 01/19/17 Pct Recovery = 85% Analysis Date = 01/16/17 Pct Recovery = 85% Analysis Date = 01/16/17 Pct Recovery = 85% Analysis Date = 01/14/17 Pct Recovery = 85% Analysis Date = 01/14/17 Pct Recovery = 85% Analysis Date = 01/12/17 Pct Recovery = 85% Analysis Date = 01/12/17 Pct Recovery = 85% Analysis Date = 01/09/17 Pct Recovery = 85% Analysis Date = 01/09/17 Pct Recovery = 85% Analysis Date = 01/07/17 Pct Recovery = 85% Analysis Date = 01/07/17 Pct Recovery = 85% Analysis Date = 01/05/17 Pct Recovery = 85% Analysis Date = 01/05/17 Pct Recovery = 85% Analysis Date = 01/03/17 Pct Recovery = 85% Analysis Date = 01/03/17 Pct Recovery = 85% Analysis Date = 12/31/16 Pct Recovery = 85% Analysis Date = 12/31/16 Pct Recovery = 85% Analysis Date = 12/29/16 Pct Recovery = 85% Analysis Date = 12/29/16 Pct Recovery = 85% Analysis Date = 12/27/16 Pct Recovery = 85% Analysis Date = 12/27/16 Pct Recovery = 85% Analysis Date = 12/24/16 Pct Recovery = 85% Analysis Date = 12/24/16 Pct Recovery = 85% Analysis Date = 12/22/16 Pct Recovery = 85% Analysis Date = 12/22/16 Pct Recovery = 85% Analysis Date = 12/20/16 Pct Recovery = 85% Analysis Date = 12/20/16 Pct Recovery = 85% Analysis Date = 12/18/16 Pct Recovery = 85% Analysis Date = 12/18/16 Pct Recovery = 85% Analysis Date = 12/15/16 Pct Recovery = 85% Analysis Date = 12/15/16 Pct Recovery = 85% Analysis Date = 12/13/16 Pct Recovery = 85% Analysis Date = 12/13/16 Pct Recovery = 85% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/11/16 Pct Recovery = 84% Analysis Date = 12/08/16 Pct Recovery = 84% Analysis Date = 12/08/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 84% Analysis Date = 12/06/16 Pct Recovery = 84% Analysis Date = 12/04/16 Pct Recovery = 84% Analysis Date = 12/04/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 12/02/16 Pct Recovery = 84% Analysis Date = 11/29/16 Pct Recovery = 84% Analysis Date = 11/29/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/27/16 Pct Recovery = 84% Analysis Date = 11/25/16 Pct Recovery = 84% Analysis Date = 11/25/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/22/16 Pct Recovery = 84% Analysis Date = 11/20/16 Pct Recovery = 84% Analysis Date = 11/20/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/18/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/16/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/13/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/11/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 84% Analysis Date = 11/09/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/06/16 Pct Recovery = 84% Analysis Date = 11/04/16 Pct Recovery = 84% Analysis Date = 11/04/16 Pct Recovery = 84% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 11/02/16 Pct Recovery = 83% Analysis Date = 10/31/16 Pct Recovery = 83% Analysis Date = 10/31/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/28/16 Pct Recovery = 83% Analysis Date = 10/26/16 Pct Recovery = 83% Analysis Date = 10/26/16 Pct Recovery = 83% Analysis Date = 10/24/16 Pct Recovery = 83% Analysis Date = 10/24/16 Pct Recovery = 83% Analysis Date = 10/21/16 Pct Recovery = 83% Analysis Date = 10/21/16 Pct Recovery = 83% Analysis Date = 10/19/16 Pct Recovery = 83% Analysis Date = 10/19/16 Pct Recovery = 83% Analysis Date = 10/17/16 Pct Recovery = 83% Analysis Date = 10/17/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/15/16 Pct Recovery = 83% Analysis Date = 10/12/16 Pct Recovery = 83% Analysis Date = 10/12/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/10/16 Pct Recovery = 83% Analysis Date = 10/08/16 Pct Recovery = 83% Analysis Date = 10/08/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/05/16 Pct Recovery = 83% Analysis Date = 10/03/16 Pct Recovery = 83% Analysis Date = 10/03/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 10/01/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/29/16 Pct Recovery = 83% Analysis Date = 09/26/16 Pct Recovery = 82% Analysis Date = 09/26/16 Pct Recovery = 82% Analysis Date = 09/24/16 Pct Recovery = 82% Analysis Date = 09/24/16 Pct Recovery = 82% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/22/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/19/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 82% Analysis Date = 09/17/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/15/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/13/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/10/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 82% Analysis Date = 09/08/16 Pct Recovery = 82% Analysis Date = 09/06/16 Pct Recovery = 82% Analysis Date = 09/06/16 Pct Recovery = 82% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/03/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 09/01/16 Pct Recovery = 81% Analysis Date = 08/30/16 Pct Recovery = 81% Analysis Date = 08/30/16 Pct Recovery = 81% Analysis Date = 08/28/16 Pct Recovery = 81% Analysis Date = 08/28/16 Pct Recovery = 81% Analysis Date = 08/25/16 Pct Recovery = 81% Analysis Date = 08/25/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 81% Analysis Date = 08/23/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/21/16 Pct Recovery = 81% Analysis Date = 08/18/16 Pct Recovery = 81% Analysis Date = 08/18/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/16/16 Pct Recovery = 81% Analysis Date = 08/14/16 Pct Recovery = 82% Analysis Date = 08/14/16 Pct Recovery = 82% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/12/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/09/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 08/07/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 82% Analysis Date = 08/05/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 08/02/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/31/16 Pct Recovery = 82% Analysis Date = 07/29/16 Pct Recovery = 82% Analysis Date = 07/29/16 Pct Recovery = 82% Analysis Date = 07/27/16 Pct Recovery = 82% Analysis Date = 07/27/16 Pct Recovery = 82% Analysis Date = 07/24/16 Pct Recovery = 82% Analysis Date = 07/24/16 Pct Recovery = 82% Analysis Date = 07/22/16 Pct Recovery = 82% Analysis Date = 07/22/16 Pct Recovery = 82% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/20/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 83% Analysis Date = 07/17/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/15/16 Pct Recovery = 83% Analysis Date = 07/13/16 Pct Recovery = 83% Analysis Date = 07/13/16 Pct Recovery = 83% Analysis Date = 07/11/16 Pct Recovery = 83% Analysis Date = 07/11/16 Pct Recovery = 83% Analysis Date = 07/08/16 Pct Recovery = 83% Analysis Date = 07/08/16 Pct Recovery = 83% Analysis Date = 07/06/16 Pct Recovery = 83% Analysis Date = 07/06/16 Pct Recovery = 83% Analysis Date = 07/04/16 Pct Recovery = 83% Analysis Date = 07/04/16 Pct Recovery = 83% Analysis Date = 07/01/16 Pct Recovery = 83% Analysis Date = 07/01/16 Pct Recovery = 83% Analysis Date = 06/29/16 Pct Recovery = 83% Analysis Date = 06/29/16 Pct Recovery = 83% Analysis Date = 06/27/16 Pct Recovery = 83% Analysis Date = 06/27/16 Pct Recovery = 83% Analysis Date = 06/25/16 Pct Recovery = 84% Analysis Date = 06/25/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/22/16 Pct Recovery = 84% Analysis Date = 06/20/16 Pct Recovery = 84% Analysis Date = 06/20/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/18/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/15/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/13/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/11/16 Pct Recovery = 84% Analysis Date = 06/09/16 Pct Recovery = 84% Analysis Date = 06/09/16 Pct Recovery = 84% Analysis Date = 06/06/16 Pct Recovery = 84% Analysis Date = 06/06/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 06/04/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 06/02/16 Pct Recovery = 84% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/30/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/28/16 Pct Recovery = 85% Analysis Date = 05/26/16 Pct Recovery = 85% Analysis Date = 05/26/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/24/16 Pct Recovery = 85% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/21/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/19/16 Pct Recovery = 85% Analysis Date = 05/17/16 Pct Recovery = 85% Analysis Date = 05/17/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/14/16 Pct Recovery = 85% Analysis Date = 05/12/16 Pct Recovery = 85% Analysis Date = 05/12/16 Pct Recovery = 85% Analysis Date = 05/10/16 Pct Recovery = 85% Analysis Date = 05/10/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/08/16 Pct Recovery = 85% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/05/16 Pct Recovery = 86% Analysis Date = 05/03/16 Pct Recovery = 86% Analysis Date = 05/03/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 05/01/16 Pct Recovery = 86% Analysis Date = 04/28/16 Pct Recovery = 85% Analysis Date = 04/28/16 Pct Recovery = 85% Analysis Date = 04/26/16 Pct Recovery = 85% Analysis Date = 04/26/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/24/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/22/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/19/16 Pct Recovery = 85% Analysis Date = 04/17/16 Pct Recovery = 85% Analysis Date = 04/17/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/15/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/12/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/10/16 Pct Recovery = 85% Analysis Date = 04/08/16 Pct Recovery = 85% Analysis Date = 04/08/16 Pct Recovery = 85% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/06/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 84% Analysis Date = 04/03/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 04/01/16 Pct Recovery = 84% Analysis Date = 03/30/16 Pct Recovery = 84% Analysis Date = 03/30/16 Pct Recovery = 84% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/27/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/25/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/23/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/21/16 Pct Recovery = 83% Analysis Date = 03/18/16 Pct Recovery = 82% Analysis Date = 03/18/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/16/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/14/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 82% Analysis Date = 03/11/16 Pct Recovery = 82% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/09/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/07/16 Pct Recovery = 81% Analysis Date = 03/05/16 Pct Recovery = 81% Analysis Date = 03/05/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 03/02/16 Pct Recovery = 81% Analysis Date = 02/29/16 Pct Recovery = 80% Analysis Date = 02/29/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 80% Analysis Date = 02/27/16 Pct Recovery = 80% Analysis Date = 02/24/16 Pct Recovery = 80% Analysis Date = 02/24/16 Pct Recovery = 80% Analysis Date = 02/22/16 Pct Recovery = 79% Analysis Date = 02/22/16 Pct Recovery = 79% Analysis Date = 02/20/16 Pct Recovery = 79% Analysis Date = 02/20/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/18/16 Pct Recovery = 79% Analysis Date = 02/15/16 Pct Recovery = 79% Analysis Date = 02/15/16 Pct Recovery = 79% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/13/16 Pct Recovery = 78% Analysis Date = 02/11/16 Pct Recovery = 78% Analysis Date = 02/11/16 Pct Recovery = 78% Analysis Date = 02/09/16 Pct Recovery = 78% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
TRIFLURALIN

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 19 83% 12% 82% 14%
Total 19 83% 12% 82% 14%

Sample Statistics
TRIFLURALIN

Characteristic N % % Basis
Plotted 19 100% Spiked
Estimated Values 1 5% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 19 .  
False Negatives 0 0% 0 out of 19
Not Spiked 9 .  
False Positives 0 0% 0 out of 9