BQS OBSP Determination:
1,1,1,2-TETRACHLOROETHANE
METHOD: 2021 , TESTIDCODE: 77562GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1,1,2-TETRACHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 199 101% 13% 101% 11%
Total 199 101% 13% 101% 11%

Sample Statistics
1,1,1,2-TETRACHLOROETHANE

Characteristic N % % Basis
Plotted 199 100% Spiked
Estimated Values 32 16% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 226 .  
False Negatives 0 0% 0 out of 199
Not Spiked 282 .  
False Positives 1 0% 1 out of 276

BQS OBSP Determination:
1,1,1-TRICHLOROETHANE
METHOD: 2021 , TESTIDCODE: 34506GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1,1-TRICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 219 104% 15% 103% 12%
Total 219 104% 15% 103% 12%

Sample Statistics
1,1,1-TRICHLOROETHANE

Characteristic N % % Basis
Plotted 219 100% Spiked
Estimated Values 58 26% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 246 .  
False Negatives 0 0% 0 out of 219
Not Spiked 262 .  
False Positives 0 0% 0 out of 256

BQS OBSP Determination:
1,1,2,2-TETRACHLOROETHANE
METHOD: 2021 , TESTIDCODE: 34516GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1,2,2-TETRACHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 18 106% 19% 103% 21%
>= Reporting Level 153 102% 15% 101% 13%
Total 171 102% 15% 101% 13%

Sample Statistics
1,1,2,2-TETRACHLOROETHANE

Characteristic N % % Basis
Plotted 171 98% Spiked
Estimated Values 16 9% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 2 1% Spiked
Spiked 197 .  
False Negatives 2 1% 2 out of 175
Not Spiked 311 .  
False Positives 0 0% 0 out of 300

BQS OBSP Determination:
1,1,2-TRICHLOROETHANE
METHOD: 2021 , TESTIDCODE: 34511GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1,2-TRICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 114% 7% 115% 6%
>= Reporting Level 154 106% 14% 105% 12%
Total 158 106% 14% 105% 12%

Sample Statistics
1,1,2-TRICHLOROETHANE

Characteristic N % % Basis
Plotted 158 100% Spiked
Estimated Values 24 15% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 186 .  
False Negatives 0 0% 0 out of 158
Not Spiked 322 .  
False Positives 1 0% 1 out of 317

BQS OBSP Determination:
1,1,2-TRICHLOROTRIFLUOROETHANE
METHOD: 2021 , TESTIDCODE: 77652GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1,2-TRICHLOROTRIFLUOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 102% 7% 104% 8%
>= Reporting Level 141 119% 164% 102% 16%
Total 145 118% 162% 102% 16%

Sample Statistics
1,1,2-TRICHLOROTRIFLUOROETHANE

Characteristic N % % Basis
Plotted 145 100% Spiked
Estimated Values 34 23% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 150 .  
False Negatives 0 0% 0 out of 145
Not Spiked 358 .  
False Positives 2 1% 2 out of 330

BQS OBSP Determination:
1,1-DICHLOROETHANE
METHOD: 2021 , TESTIDCODE: 34496GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 8 109% 25% 119% 19%
>= Reporting Level 150 107% 12% 107% 10%
Total 158 107% 13% 108% 11%

Sample Statistics
1,1-DICHLOROETHANE

Characteristic N % % Basis
Plotted 158 100% Spiked
Estimated Values 22 14% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 186 .  
False Negatives 0 0% 0 out of 158
Not Spiked 322 .  
False Positives 1 0% 1 out of 317

BQS OBSP Determination:
1,1-DICHLOROETHYLENE
METHOD: 2021 , TESTIDCODE: 34501GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 206 107% 82% 100% 15%
Total 206 107% 82% 100% 15%

Sample Statistics
1,1-DICHLOROETHYLENE

Characteristic N % % Basis
Plotted 206 100% Spiked
Estimated Values 52 25% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 234 .  
False Negatives 1 0% 1 out of 207
Not Spiked 274 .  
False Positives 0 0% 0 out of 268

BQS OBSP Determination:
1,1-DICHLOROPROPENE
METHOD: 2021 , TESTIDCODE: 77168GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,1-DICHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 145 91% 13% 88% 10%
Total 145 91% 13% 88% 10%

Sample Statistics
1,1-DICHLOROPROPENE

Characteristic N % % Basis
Plotted 145 100% Spiked
Estimated Values 35 24% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 173 .  
False Negatives 0 0% 0 out of 145
Not Spiked 335 .  
False Positives 0 0% 0 out of 330

BQS OBSP Determination:
1,2,3,4-TETRAMETHYLBENZENE
METHOD: 2021 , TESTIDCODE: 49999GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,3,4-TETRAMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 105% 47% 108% 33%
>= Reporting Level 109 86% 13% 84% 12%
Total 114 87% 16% 84% 12%

Sample Statistics
1,2,3,4-TETRAMETHYLBENZENE

Characteristic N % % Basis
Plotted 114 100% Spiked
Estimated Values 5 4% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 119 .  
False Negatives 0 0% 0 out of 114
Not Spiked 383 .  
False Positives 0 0% 0 out of 355

BQS OBSP Determination:
1,2,3,5-TETRAMETHYLBENZENE
METHOD: 2021 , TESTIDCODE: 50000GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,3,5-TETRAMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 89% 26% 78% 24%
>= Reporting Level 116 86% 16% 85% 13%
Total 120 86% 16% 85% 13%

Sample Statistics
1,2,3,5-TETRAMETHYLBENZENE

Characteristic N % % Basis
Plotted 120 100% Spiked
Estimated Values 7 6% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 125 .  
False Negatives 0 0% 0 out of 120
Not Spiked 383 .  
False Positives 2 1% 2 out of 355

BQS OBSP Determination:
1,2,3-TRICHLOROBENZENE
METHOD: 2021 , TESTIDCODE: 77613GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 92% 28% 87% 28%
>= Reporting Level 125 89% 10% 88% 9%
Total 139 90% 13% 88% 10%

Sample Statistics
1,2,3-TRICHLOROBENZENE

Characteristic N % % Basis
Plotted 139 95% Spiked
Estimated Values 18 12% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 7 5% Spiked
Spiked 168 .  
False Negatives 0 0% 0 out of 146
Not Spiked 340 .  
False Positives 1 0% 1 out of 329

BQS OBSP Determination:
1,2,3-TRICHLOROPROPANE
METHOD: 2021 , TESTIDCODE: 77443GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 23 102% 13% 103% 14%
>= Reporting Level 178 100% 13% 99% 10%
Total 201 100% 13% 99% 10%

Sample Statistics
1,2,3-TRICHLOROPROPANE

Characteristic N % % Basis
Plotted 201 88% Spiked
Estimated Values 24 11% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 24 11% Spiked
Spiked 261 .  
False Negatives 3 1% 3 out of 228
Not Spiked 247 .  
False Positives 0 0% 0 out of 247

BQS OBSP Determination:
1,2,3-TRIMETHYLBENZENE
METHOD: 2021 , TESTIDCODE: 77221GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,3-TRIMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 95% 20% 84% 19%
>= Reporting Level 118 87% 18% 85% 15%
Total 123 88% 18% 85% 15%

Sample Statistics
1,2,3-TRIMETHYLBENZENE

Characteristic N % % Basis
Plotted 123 100% Spiked
Estimated Values 14 11% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 128 .  
False Negatives 0 0% 0 out of 123
Not Spiked 380 .  
False Positives 1 0% 1 out of 352

BQS OBSP Determination:
1,2,4-TRICHLOROBENZENE
METHOD: 2021 , TESTIDCODE: 34551GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,4-TRICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 94% 29% 95% 34%
>= Reporting Level 118 88% 10% 89% 11%
Total 132 89% 13% 89% 11%

Sample Statistics
1,2,4-TRICHLOROBENZENE

Characteristic N % % Basis
Plotted 132 98% Spiked
Estimated Values 20 15% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 3 2% Spiked
Spiked 163 .  
False Negatives 0 0% 0 out of 135
Not Spiked 345 .  
False Positives 1 0% 1 out of 340

BQS OBSP Determination:
1,2,4-TRIMETHYLBENZENE
METHOD: 2021 , TESTIDCODE: 77222GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2,4-TRIMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 102% 42% 85% 39%
>= Reporting Level 135 87% 14% 85% 14%
Total 144 88% 17% 85% 14%

Sample Statistics
1,2,4-TRIMETHYLBENZENE

Characteristic N % % Basis
Plotted 144 99% Spiked
Estimated Values 33 23% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 167 .  
False Negatives 0 0% 0 out of 145
Not Spiked 341 .  
False Positives 1 0% 1 out of 330

BQS OBSP Determination:
1,2-DIBROMO-3-CHLOROPROPANE
METHOD: 2021 , TESTIDCODE: 82625GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2-DIBROMO-3-CHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 23 91% 14% 94% 13%
>= Reporting Level 158 90% 14% 90% 14%
Total 181 90% 14% 90% 13%

Sample Statistics
1,2-DIBROMO-3-CHLOROPROPANE

Characteristic N % % Basis
Plotted 181 84% Spiked
Estimated Values 33 15% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 33 15% Spiked
Spiked 248 .  
False Negatives 1 0% 1 out of 215
Not Spiked 260 .  
False Positives 0 0% 0 out of 260

BQS OBSP Determination:
1,2-DIBROMOETHANE
METHOD: 2021 , TESTIDCODE: 77651GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2-DIBROMOETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 103% 15% 104% 20%
>= Reporting Level 179 97% 15% 97% 11%
Total 188 97% 15% 97% 12%

Sample Statistics
1,2-DIBROMOETHANE

Characteristic N % % Basis
Plotted 188 98% Spiked
Estimated Values 65 34% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 2 1% Spiked
Spiked 218 .  
False Negatives 1 1% 1 out of 191
Not Spiked 290 .  
False Positives 0 0% 0 out of 284

BQS OBSP Determination:
1,2-DICHLOROBENZENE
METHOD: 2021 , TESTIDCODE: 34536GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 106% 5% 104% 6%
>= Reporting Level 210 96% 12% 95% 9%
Total 214 96% 12% 95% 9%

Sample Statistics
1,2-DICHLOROBENZENE

Characteristic N % % Basis
Plotted 214 100% Spiked
Estimated Values 61 29% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 236 .  
False Negatives 0 0% 0 out of 214
Not Spiked 272 .  
False Positives 0 0% 0 out of 261

BQS OBSP Determination:
1,2-DICHLOROETHANE
METHOD: 2021 , TESTIDCODE: 32103GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 28 104% 18% 107% 18%
>= Reporting Level 182 110% 13% 108% 14%
Total 210 109% 14% 108% 13%

Sample Statistics
1,2-DICHLOROETHANE

Characteristic N % % Basis
Plotted 210 93% Spiked
Estimated Values 27 12% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 14 6% Spiked
Spiked 258 .  
False Negatives 1 0% 1 out of 225
Not Spiked 250 .  
False Positives 1 0% 1 out of 250

BQS OBSP Determination:
1,2-DICHLOROPROPANE
METHOD: 2021 , TESTIDCODE: 34541GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,2-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 102% 7% 101% 10%
>= Reporting Level 236 103% 13% 103% 12%
Total 243 103% 13% 103% 12%

Sample Statistics
1,2-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 243 100% Spiked
Estimated Values 65 27% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 270 .  
False Negatives 0 0% 0 out of 243
Not Spiked 238 .  
False Positives 0 0% 0 out of 232

BQS OBSP Determination:
1,3,5-TRIMETHYLBENZENE
METHOD: 2021 , TESTIDCODE: 77226GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,3,5-TRIMETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 90% 23% 85% 28%
>= Reporting Level 137 88% 15% 88% 13%
Total 141 88% 15% 88% 14%

Sample Statistics
1,3,5-TRIMETHYLBENZENE

Characteristic N % % Basis
Plotted 141 99% Spiked
Estimated Values 35 24% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 2 1% Spiked
Spiked 171 .  
False Negatives 0 0% 0 out of 143
Not Spiked 337 .  
False Positives 0 0% 0 out of 332

BQS OBSP Determination:
1,3-DICHLOROBENZENE
METHOD: 2021 , TESTIDCODE: 34566GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,3-DICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 82% 26% 92% 22%
>= Reporting Level 169 94% 11% 92% 9%
Total 173 93% 12% 92% 9%

Sample Statistics
1,3-DICHLOROBENZENE

Characteristic N % % Basis
Plotted 173 100% Spiked
Estimated Values 47 27% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 201 .  
False Negatives 0 0% 0 out of 173
Not Spiked 307 .  
False Positives 0 0% 0 out of 302

BQS OBSP Determination:
1,3-DICHLOROPROPANE
METHOD: 2021 , TESTIDCODE: 77173GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,3-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 12 100% 8% 98% 7%
>= Reporting Level 146 103% 13% 103% 11%
Total 158 103% 12% 102% 10%

Sample Statistics
1,3-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 158 96% Spiked
Estimated Values 23 14% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 6 4% Spiked
Spiked 192 .  
False Negatives 0 0% 0 out of 164
Not Spiked 315 .  
False Positives 1 0% 1 out of 310

BQS OBSP Determination:
1,4-DICHLOROBENZENE
METHOD: 2021 , TESTIDCODE: 34571GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
1,4-DICHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 83% 20% 91% 2%
>= Reporting Level 216 89% 14% 90% 12%
Total 221 89% 14% 90% 12%

Sample Statistics
1,4-DICHLOROBENZENE

Characteristic N % % Basis
Plotted 221 100% Spiked
Estimated Values 56 25% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 248 .  
False Negatives 0 0% 0 out of 221
Not Spiked 260 .  
False Positives 2 1% 2 out of 254

BQS OBSP Determination:
2,2-DICHLOROPROPANE
METHOD: 2021 , TESTIDCODE: 77170GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
2,2-DICHLOROPROPANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 37% . 37% 0%
>= Reporting Level 130 86% 13% 84% 12%
Total 131 85% 13% 84% 12%

Sample Statistics
2,2-DICHLOROPROPANE

Characteristic N % % Basis
Plotted 131 100% Spiked
Estimated Values 26 20% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 159 .  
False Negatives 0 0% 0 out of 131
Not Spiked 349 .  
False Positives 1 0% 1 out of 344

BQS OBSP Determination:
2-BUTANONE
METHOD: 2021 , TESTIDCODE: 81595GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
2-BUTANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 122% 22% 122% 27%
>= Reporting Level 132 106% 24% 104% 10%
Total 137 106% 24% 104% 10%

Sample Statistics
2-BUTANONE

Characteristic N % % Basis
Plotted 137 85% Spiked
Estimated Values 4 2% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 24 15% Spiked
Spiked 178 .  
False Negatives 0 0% 0 out of 161
Not Spiked 329 .  
False Positives 3 1% 3 out of 313

BQS OBSP Determination:
2-CHLOROTOLUENE
METHOD: 2021 , TESTIDCODE: 77275GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
2-CHLOROTOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 13 106% 24% 102% 23%
>= Reporting Level 225 94% 15% 94% 14%
Total 238 94% 16% 94% 14%

Sample Statistics
2-CHLOROTOLUENE

Characteristic N % % Basis
Plotted 238 100% Spiked
Estimated Values 68 29% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 265 .  
False Negatives 0 0% 0 out of 238
Not Spiked 243 .  
False Positives 1 0% 1 out of 237

BQS OBSP Determination:
2-HEXANONE
METHOD: 2021 , TESTIDCODE: 77103GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
2-HEXANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 8 122% 38% 129% 31%
>= Reporting Level 132 97% 13% 98% 11%
Total 140 99% 16% 98% 13%

Sample Statistics
2-HEXANONE

Characteristic N % % Basis
Plotted 140 89% Spiked
Estimated Values 44 28% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 16 10% Spiked
Spiked 164 .  
False Negatives 2 1% 2 out of 158
Not Spiked 344 .  
False Positives 0 0% 0 out of 317

BQS OBSP Determination:
3-CHLOROPROPENE
METHOD: 2021 , TESTIDCODE: 78109GCM66
Open Data Set

 Analysis Date = 05/02/06 
 SpikeMix = NSI 080405-01VOC: 20 µl & Ultra CB-1578: 50 µl 
 Pct Recovery = 109%  Analysis Date = 01/27/06 
 SpikeMix = NSI 080405-01VOC: 20 µl & Supelco LB31918: 30 µl 
 Pct Recovery = 131%  Analysis Date = 04/07/06 
 SpikeMix = Accu B5070191: 30 µl & NSI 080405-01VOC: 20 µl 
 Pct Recovery = 122%  Analysis Date = 08/12/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 102%  Analysis Date = 07/14/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 96%  Analysis Date = 05/20/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 106%  Analysis Date = 12/22/12 
 SpikeMix = NSI 062112-01VOA: 40 µl & Supelco LB92787: 40 µl 
 Pct Recovery = 100%  Analysis Date = 01/19/13 
 SpikeMix = Accu 212051193: 40 µl & Abs 051712: 40 µl 
 Pct Recovery = 115%  Analysis Date = 09/19/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 101%  Analysis Date = 07/27/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 121%  Analysis Date = 05/31/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 117%  Analysis Date = 04/03/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 101%  Analysis Date = 01/09/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 103%  Analysis Date = 10/14/06 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 108%  Analysis Date = 02/26/99 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 106%  Analysis Date = 11/20/98 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 104%  Analysis Date = 09/11/12 
 SpikeMix = NSI 062112-01VOA: 20 µl & Supelco LB92787: 20 µl 
 Pct Recovery = 91%  Analysis Date = 07/30/12 
 SpikeMix = Supelco LB92787: 20 µl & Abs 051712: 20 µl 
 Pct Recovery = 101%  Analysis Date = 11/08/12 
 SpikeMix = Crescent 05BB048: 20 µl & Accu 212051193: 20 µl 
 Pct Recovery = 102%  Analysis Date = 11/02/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 107%  Analysis Date = 09/20/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 109%  Analysis Date = 06/09/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 93%  Analysis Date = 03/14/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 97%  Analysis Date = 08/25/05 
 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 99%  Analysis Date = 06/27/05 
 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 100%  Analysis Date = 07/26/05 
 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 102%  Analysis Date = 03/09/05 
 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 112%  Analysis Date = 04/15/05 
 SpikeMix = Supelco LB22064: 5 µl 
 Pct Recovery = 102%  Analysis Date = 02/11/05 
 SpikeMix = Supelco LB22064: 5 µl 
 Pct Recovery = 99%  Analysis Date = 08/13/06 
 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 101%  Analysis Date = 03/15/06 
 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 109%  Analysis Date = 05/17/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 103%  Analysis Date = 12/08/05 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 101%  Analysis Date = 02/14/06 
 SpikeMix = NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 107%  Analysis Date = 11/15/05 
 SpikeMix = NSI 080405-01VOC: 5 µl & Supelco LB31918: 5 µl 
 Pct Recovery = 100%  Analysis Date = 06/06/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl 
 Pct Recovery = 112%  Analysis Date = 05/03/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 95%  Analysis Date = 03/29/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 113%  Analysis Date = 02/28/13 
 SpikeMix = NSI 062112-01VOA: 10 µl & Accu 212051193: 10 µl 
 Pct Recovery = 105%  Analysis Date = 07/19/12 
 SpikeMix = Crescent 05BB048: 10 µl & Accu 212051193: 10 µl 
 Pct Recovery = 97%  Analysis Date = 05/24/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 104%  Analysis Date = 02/22/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 105%  Analysis Date = 06/17/10 
 SpikeMix = Accu 209081198: 30 µl 
 Pct Recovery = 89%  Analysis Date = 03/26/10 
 SpikeMix = Accu 209081198: 30 µl 
 Pct Recovery = 79%  Analysis Date = 12/24/09 
 SpikeMix = Accu 209081198: 30 µl 
 Pct Recovery = 98%  Analysis Date = 08/11/10 
 SpikeMix = Restek A069860: 30 µl 
 Pct Recovery = 93%  Analysis Date = 05/22/10 
 SpikeMix = Restek A069860: 30 µl 
 Pct Recovery = 83%  Analysis Date = 03/11/10 
 SpikeMix = Restek A069860: 30 µl 
 Pct Recovery = 89%  Analysis Date = 12/04/09 
 SpikeMix = Restek A069860: 30 µl 
 Pct Recovery = 116%  Analysis Date = 03/31/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 126%  Analysis Date = 01/20/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 109%  Analysis Date = 08/24/02 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 97%  Analysis Date = 05/09/02 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 103%  Analysis Date = 12/07/01 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 117%  Analysis Date = 12/20/08 
 SpikeMix = NSI 021408-01: 20 µl 
 Pct Recovery = 92%  Analysis Date = 12/03/08 
 SpikeMix = NSI 021408-01: 20 µl 
 Pct Recovery = 89%  Analysis Date = 08/30/08 
 SpikeMix = NSI 021408-01: 20 µl 
 Pct Recovery = 89%  Analysis Date = 06/25/08 
 SpikeMix = NSI 021408-01: 20 µl 
 Pct Recovery = 113%  Analysis Date = 05/16/08 
 SpikeMix = NSI 021408-01: 20 µl 
 Pct Recovery = 103%  Analysis Date = 07/24/08 
 SpikeMix = ERA 0709-07-04VOC: 20 µl 
 Pct Recovery = 134%  Analysis Date = 07/17/08 
 SpikeMix = ERA 0709-07-04VOC: 20 µl 
 Pct Recovery = 89%  Analysis Date = 06/06/08 
 SpikeMix = ERA 0709-07-04VOC: 20 µl 
 Pct Recovery = 106%  Analysis Date = 04/18/08 
 SpikeMix = ERA 0709-07-04VOC: 20 µl 
 Pct Recovery = 99%  Analysis Date = 01/17/08 
 SpikeMix = ERA 0709-07-04VOC: 20 µl 
 Pct Recovery = 103%  Analysis Date = 11/10/07 
 SpikeMix = ERA 0709-07-04VOC: 20 µl 
 Pct Recovery = 99%  Analysis Date = 04/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 101%  Analysis Date = 01/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 105%  Analysis Date = 05/25/12 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 96%  Analysis Date = 05/08/12 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 87%  Analysis Date = 11/24/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 90%  Analysis Date = 06/10/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 93%  Analysis Date = 04/13/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 86%  Analysis Date = 01/22/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 86%  Analysis Date = 04/21/09 
 SpikeMix = Abs 080408VOC: 40 µl 
 Pct Recovery = 125%  Analysis Date = 01/27/09 
 SpikeMix = Abs 080408VOC: 40 µl 
 Pct Recovery = 94%  Analysis Date = 03/01/14 
 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl 
 Pct Recovery = 83%  Analysis Date = 07/24/13 
 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl 
 Pct Recovery = 96%  Analysis Date = 09/17/13 
 SpikeMix = Crescent 04CC151: 20 µl & Supelco LC00154: 20 µl 
 Pct Recovery = 86%  Analysis Date = 01/29/14 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 97%  Analysis Date = 09/17/13 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 108%  Analysis Date = 08/06/13 
 SpikeMix = Supelco LC00154: 20 µl & Abs 051413: 20 µl 
 Pct Recovery = 91%  Analysis Date = 11/01/13 
 SpikeMix = Accu 213041120: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 83%  Analysis Date = 12/12/13 
 SpikeMix = NSI 053013: 20 µl & Accu 213041120: 20 µl 
 Pct Recovery = 95%  Analysis Date = 06/30/09 
 SpikeMix = Ultra CE-2869: 40 µl 
 Pct Recovery = 93%  Analysis Date = 06/17/09 
 SpikeMix = Ultra CE-2869: 40 µl 
 Pct Recovery = 93%  Analysis Date = 09/01/10 
 SpikeMix = Accu 209081198: 10 µl 
 Pct Recovery = 96%  Analysis Date = 07/16/10 
 SpikeMix = Accu 209081198: 10 µl 
 Pct Recovery = 95%  Analysis Date = 05/05/10 
 SpikeMix = Accu 209081198: 10 µl 
 Pct Recovery = 86%  Analysis Date = 02/19/10 
 SpikeMix = Accu 209081198: 10 µl 
 Pct Recovery = 98%  Analysis Date = 11/10/09 
 SpikeMix = Accu 209081198: 10 µl 
 Pct Recovery = 96%  Analysis Date = 09/21/10 
 SpikeMix = Restek A069860: 10 µl 
 Pct Recovery = 92%  Analysis Date = 07/09/10 
 SpikeMix = Restek A069860: 10 µl 
 Pct Recovery = 99%  Analysis Date = 04/13/10 
 SpikeMix = Restek A069860: 10 µl 
 Pct Recovery = 87%  Analysis Date = 01/26/10 
 SpikeMix = Restek A069860: 10 µl 
 Pct Recovery = 91%  Analysis Date = 10/22/09 
 SpikeMix = Restek A069860: 10 µl 
 Pct Recovery = 108%  Analysis Date = 09/10/02 
 SpikeMix = Ultra S1214: 10 µl 
 Pct Recovery = 93%  Analysis Date = 06/21/02 
 SpikeMix = Ultra S1214: 10 µl 
 Pct Recovery = 93%  Analysis Date = 03/16/02 
 SpikeMix = Ultra S1214: 10 µl 
 Pct Recovery = 122%  Analysis Date = 02/02/02 
 SpikeMix = Ultra S1214: 10 µl 
 Pct Recovery = 127%  Analysis Date = 03/10/12 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 92%  Analysis Date = 10/18/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 93%  Analysis Date = 09/17/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 96%  Analysis Date = 05/03/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 97%  Analysis Date = 03/01/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 103%  Analysis Date = 11/05/10 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 94%  Analysis Date = 08/29/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/17/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 94%  Analysis Date = 06/09/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 94%  Analysis Date = 03/14/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 83%  Analysis Date = 09/17/13 
 SpikeMix = Crescent 04CC151: 10 µl & Supelco LC00154: 10 µl 
 Pct Recovery = 89%  Analysis Date = 12/12/13 
 SpikeMix = Supelco LC00154: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 116%  Analysis Date = 12/31/13 
 SpikeMix = Accu 213041120: 10 µl & ChemService 1530700: 10 µl 
 Pct Recovery = 91%  Analysis Date = 01/15/14 
 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl 
 Pct Recovery = 82%  Analysis Date = 05/22/13 
 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl 
 Pct Recovery = 93%  Analysis Date = 03/19/14 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 101%  Analysis Date = 06/08/13 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 96%  Analysis Date = 08/11/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 112%  Analysis Date = 03/31/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 112%  Analysis Date = 02/18/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 87%  Analysis Date = 11/29/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 97%  Analysis Date = 09/17/06 
 SpikeMix = NSI 080405-01VOC: 2 µl 
 Pct Recovery = 108%  Analysis Date = 03/23/06 
 SpikeMix = NSI 080405-01VOC: 2 µl 
 Pct Recovery = 123%  Analysis Date = 09/19/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 114%  Analysis Date = 08/02/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 103%  Analysis Date = 07/06/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 99%  Analysis Date = 03/18/14 
 Pct Recovery = 96%  Analysis Date = 02/19/14 
 Pct Recovery = 96%  Analysis Date = 02/19/14 
 Pct Recovery = 96%  Analysis Date = 01/22/14 
 Pct Recovery = 96%  Analysis Date = 01/22/14 
 Pct Recovery = 96%  Analysis Date = 12/25/13 
 Pct Recovery = 96%  Analysis Date = 12/25/13 
 Pct Recovery = 96%  Analysis Date = 11/27/13 
 Pct Recovery = 96%  Analysis Date = 11/27/13 
 Pct Recovery = 96%  Analysis Date = 10/30/13 
 Pct Recovery = 96%  Analysis Date = 10/30/13 
 Pct Recovery = 96%  Analysis Date = 10/02/13 
 Pct Recovery = 96%  Analysis Date = 10/02/13 
 Pct Recovery = 96%  Analysis Date = 09/04/13 
 Pct Recovery = 96%  Analysis Date = 09/04/13 
 Pct Recovery = 96%  Analysis Date = 08/07/13 
 Pct Recovery = 96%  Analysis Date = 08/07/13 
 Pct Recovery = 96%  Analysis Date = 07/10/13 
 Pct Recovery = 96%  Analysis Date = 07/10/13 
 Pct Recovery = 96%  Analysis Date = 06/12/13 
 Pct Recovery = 96%  Analysis Date = 06/12/13 
 Pct Recovery = 96%  Analysis Date = 05/15/13 
 Pct Recovery = 96%  Analysis Date = 05/15/13 
 Pct Recovery = 96%  Analysis Date = 04/17/13 
 Pct Recovery = 96%  Analysis Date = 04/17/13 
 Pct Recovery = 96%  Analysis Date = 03/20/13 
 Pct Recovery = 96%  Analysis Date = 03/20/13 
 Pct Recovery = 96%  Analysis Date = 02/20/13 
 Pct Recovery = 96%  Analysis Date = 02/20/13 
 Pct Recovery = 96%  Analysis Date = 01/23/13 
 Pct Recovery = 96%  Analysis Date = 01/23/13 
 Pct Recovery = 96%  Analysis Date = 12/26/12 
 Pct Recovery = 96%  Analysis Date = 12/26/12 
 Pct Recovery = 96%  Analysis Date = 11/28/12 
 Pct Recovery = 96%  Analysis Date = 11/28/12 
 Pct Recovery = 96%  Analysis Date = 10/31/12 
 Pct Recovery = 95%  Analysis Date = 10/31/12 
 Pct Recovery = 95%  Analysis Date = 10/03/12 
 Pct Recovery = 95%  Analysis Date = 10/03/12 
 Pct Recovery = 95%  Analysis Date = 09/05/12 
 Pct Recovery = 95%  Analysis Date = 09/05/12 
 Pct Recovery = 95%  Analysis Date = 08/08/12 
 Pct Recovery = 95%  Analysis Date = 08/08/12 
 Pct Recovery = 95%  Analysis Date = 07/11/12 
 Pct Recovery = 95%  Analysis Date = 07/11/12 
 Pct Recovery = 95%  Analysis Date = 06/13/12 
 Pct Recovery = 95%  Analysis Date = 06/13/12 
 Pct Recovery = 95%  Analysis Date = 05/16/12 
 Pct Recovery = 95%  Analysis Date = 05/16/12 
 Pct Recovery = 95%  Analysis Date = 04/18/12 
 Pct Recovery = 95%  Analysis Date = 04/18/12 
 Pct Recovery = 95%  Analysis Date = 03/21/12 
 Pct Recovery = 95%  Analysis Date = 03/21/12 
 Pct Recovery = 95%  Analysis Date = 02/22/12 
 Pct Recovery = 95%  Analysis Date = 02/22/12 
 Pct Recovery = 95%  Analysis Date = 01/25/12 
 Pct Recovery = 95%  Analysis Date = 01/25/12 
 Pct Recovery = 95%  Analysis Date = 12/28/11 
 Pct Recovery = 95%  Analysis Date = 12/28/11 
 Pct Recovery = 95%  Analysis Date = 11/30/11 
 Pct Recovery = 95%  Analysis Date = 11/30/11 
 Pct Recovery = 95%  Analysis Date = 11/02/11 
 Pct Recovery = 95%  Analysis Date = 11/02/11 
 Pct Recovery = 95%  Analysis Date = 10/05/11 
 Pct Recovery = 95%  Analysis Date = 10/05/11 
 Pct Recovery = 95%  Analysis Date = 09/07/11 
 Pct Recovery = 95%  Analysis Date = 09/07/11 
 Pct Recovery = 95%  Analysis Date = 08/10/11 
 Pct Recovery = 95%  Analysis Date = 08/10/11 
 Pct Recovery = 95%  Analysis Date = 07/13/11 
 Pct Recovery = 95%  Analysis Date = 07/13/11 
 Pct Recovery = 95%  Analysis Date = 06/15/11 
 Pct Recovery = 95%  Analysis Date = 06/15/11 
 Pct Recovery = 95%  Analysis Date = 05/18/11 
 Pct Recovery = 95%  Analysis Date = 05/18/11 
 Pct Recovery = 95%  Analysis Date = 04/20/11 
 Pct Recovery = 96%  Analysis Date = 04/20/11 
 Pct Recovery = 96%  Analysis Date = 03/23/11 
 Pct Recovery = 96%  Analysis Date = 03/23/11 
 Pct Recovery = 96%  Analysis Date = 02/23/11 
 Pct Recovery = 96%  Analysis Date = 02/23/11 
 Pct Recovery = 96%  Analysis Date = 01/26/11 
 Pct Recovery = 96%  Analysis Date = 01/26/11 
 Pct Recovery = 96%  Analysis Date = 12/29/10 
 Pct Recovery = 96%  Analysis Date = 12/29/10 
 Pct Recovery = 96%  Analysis Date = 12/01/10 
 Pct Recovery = 96%  Analysis Date = 12/01/10 
 Pct Recovery = 96%  Analysis Date = 11/03/10 
 Pct Recovery = 96%  Analysis Date = 11/03/10 
 Pct Recovery = 96%  Analysis Date = 10/06/10 
 Pct Recovery = 96%  Analysis Date = 10/06/10 
 Pct Recovery = 96%  Analysis Date = 09/08/10 
 Pct Recovery = 96%  Analysis Date = 09/08/10 
 Pct Recovery = 96%  Analysis Date = 08/11/10 
 Pct Recovery = 96%  Analysis Date = 08/11/10 
 Pct Recovery = 96%  Analysis Date = 07/14/10 
 Pct Recovery = 96%  Analysis Date = 07/14/10 
 Pct Recovery = 96%  Analysis Date = 06/16/10 
 Pct Recovery = 96%  Analysis Date = 06/16/10 
 Pct Recovery = 96%  Analysis Date = 05/19/10 
 Pct Recovery = 96%  Analysis Date = 05/19/10 
 Pct Recovery = 96%  Analysis Date = 04/21/10 
 Pct Recovery = 96%  Analysis Date = 04/21/10 
 Pct Recovery = 96%  Analysis Date = 03/24/10 
 Pct Recovery = 96%  Analysis Date = 03/24/10 
 Pct Recovery = 96%  Analysis Date = 02/24/10 
 Pct Recovery = 96%  Analysis Date = 02/24/10 
 Pct Recovery = 96%  Analysis Date = 01/27/10 
 Pct Recovery = 97%  Analysis Date = 01/27/10 
 Pct Recovery = 97%  Analysis Date = 12/30/09 
 Pct Recovery = 97%  Analysis Date = 12/30/09 
 Pct Recovery = 97%  Analysis Date = 12/02/09 
 Pct Recovery = 97%  Analysis Date = 12/02/09 
 Pct Recovery = 97%  Analysis Date = 11/04/09 
 Pct Recovery = 97%  Analysis Date = 11/04/09 
 Pct Recovery = 97%  Analysis Date = 10/07/09 
 Pct Recovery = 97%  Analysis Date = 10/07/09 
 Pct Recovery = 97%  Analysis Date = 09/09/09 
 Pct Recovery = 98%  Analysis Date = 09/09/09 
 Pct Recovery = 98%  Analysis Date = 08/12/09 
 Pct Recovery = 98%  Analysis Date = 08/12/09 
 Pct Recovery = 98%  Analysis Date = 07/15/09 
 Pct Recovery = 98%  Analysis Date = 07/15/09 
 Pct Recovery = 98%  Analysis Date = 06/17/09 
 Pct Recovery = 98%  Analysis Date = 06/17/09 
 Pct Recovery = 98%  Analysis Date = 05/20/09 
 Pct Recovery = 99%  Analysis Date = 05/20/09 
 Pct Recovery = 99%  Analysis Date = 04/22/09 
 Pct Recovery = 99%  Analysis Date = 04/22/09 
 Pct Recovery = 99%  Analysis Date = 03/25/09 
 Pct Recovery = 99%  Analysis Date = 03/25/09 
 Pct Recovery = 99%  Analysis Date = 02/25/09 
 Pct Recovery = 100%  Analysis Date = 02/25/09 
 Pct Recovery = 100%  Analysis Date = 01/28/09 
 Pct Recovery = 100%  Analysis Date = 01/28/09 
 Pct Recovery = 100%  Analysis Date = 12/31/08 
 Pct Recovery = 100%  Analysis Date = 12/31/08 
 Pct Recovery = 100%  Analysis Date = 12/03/08 
 Pct Recovery = 100%  Analysis Date = 12/03/08 
 Pct Recovery = 100%  Analysis Date = 11/05/08 
 Pct Recovery = 100%  Analysis Date = 11/05/08 
 Pct Recovery = 100%  Analysis Date = 10/08/08 
 Pct Recovery = 101%  Analysis Date = 10/08/08 
 Pct Recovery = 101%  Analysis Date = 09/10/08 
 Pct Recovery = 101%  Analysis Date = 09/10/08 
 Pct Recovery = 101%  Analysis Date = 08/13/08 
 Pct Recovery = 101%  Analysis Date = 08/13/08 
 Pct Recovery = 101%  Analysis Date = 07/16/08 
 Pct Recovery = 101%  Analysis Date = 07/16/08 
 Pct Recovery = 101%  Analysis Date = 06/18/08 
 Pct Recovery = 101%  Analysis Date = 06/18/08 
 Pct Recovery = 101%  Analysis Date = 05/21/08 
 Pct Recovery = 102%  Analysis Date = 05/21/08 
 Pct Recovery = 102%  Analysis Date = 04/23/08 
 Pct Recovery = 102%  Analysis Date = 04/23/08 
 Pct Recovery = 102%  Analysis Date = 03/26/08 
 Pct Recovery = 102%  Analysis Date = 03/26/08 
 Pct Recovery = 102%  Analysis Date = 02/27/08 
 Pct Recovery = 102%  Analysis Date = 02/27/08 
 Pct Recovery = 102%  Analysis Date = 01/30/08 
 Pct Recovery = 102%  Analysis Date = 01/30/08 
 Pct Recovery = 102%  Analysis Date = 01/02/08 
 Pct Recovery = 103%  Analysis Date = 01/02/08 
 Pct Recovery = 103%  Analysis Date = 12/05/07 
 Pct Recovery = 103%  Analysis Date = 12/05/07 
 Pct Recovery = 103%  Analysis Date = 11/07/07 
 Pct Recovery = 103%  Analysis Date = 11/07/07 
 Pct Recovery = 103%  Analysis Date = 10/11/07 
 Pct Recovery = 103%  Analysis Date = 10/11/07 
 Pct Recovery = 103%  Analysis Date = 09/13/07 
 Pct Recovery = 103%  Analysis Date = 09/13/07 
 Pct Recovery = 103%  Analysis Date = 08/16/07 
 Pct Recovery = 104%  Analysis Date = 08/16/07 
 Pct Recovery = 104%  Analysis Date = 07/19/07 
 Pct Recovery = 104%  Analysis Date = 07/19/07 
 Pct Recovery = 104%  Analysis Date = 06/21/07 
 Pct Recovery = 104%  Analysis Date = 06/21/07 
 Pct Recovery = 104%  Analysis Date = 05/24/07 
 Pct Recovery = 104%  Analysis Date = 05/24/07 
 Pct Recovery = 104%  Analysis Date = 04/26/07 
 Pct Recovery = 104%  Analysis Date = 04/26/07 
 Pct Recovery = 104%  Analysis Date = 03/29/07 
 Pct Recovery = 104%  Analysis Date = 03/29/07 
 Pct Recovery = 104%  Analysis Date = 03/01/07 
 Pct Recovery = 105%  Analysis Date = 03/01/07 
 Pct Recovery = 105%  Analysis Date = 02/01/07 
 Pct Recovery = 105%  Analysis Date = 02/01/07 
 Pct Recovery = 105%  Analysis Date = 01/04/07 
 Pct Recovery = 105%  Analysis Date = 01/04/07 
 Pct Recovery = 105%  Analysis Date = 12/07/06 
 Pct Recovery = 105%  Analysis Date = 12/07/06 
 Pct Recovery = 105%  Analysis Date = 11/09/06 
 Pct Recovery = 105%  Analysis Date = 11/09/06 
 Pct Recovery = 105%  Analysis Date = 10/12/06 
 Pct Recovery = 105%  Analysis Date = 10/12/06 
 Pct Recovery = 105%  Analysis Date = 09/14/06 
 Pct Recovery = 105%  Analysis Date = 09/14/06 
 Pct Recovery = 105%  Analysis Date = 08/17/06 
 Pct Recovery = 106%  Analysis Date = 08/17/06 
 Pct Recovery = 106%  Analysis Date = 07/20/06 
 Pct Recovery = 106%  Analysis Date = 07/20/06 
 Pct Recovery = 106%  Analysis Date = 06/22/06 
 Pct Recovery = 106%  Analysis Date = 06/22/06 
 Pct Recovery = 106%  Analysis Date = 05/25/06 
 Pct Recovery = 106%  Analysis Date = 05/25/06 
 Pct Recovery = 106%  Analysis Date = 04/27/06 
 Pct Recovery = 106%  Analysis Date = 04/27/06 
 Pct Recovery = 106%  Analysis Date = 03/30/06 
 Pct Recovery = 106%  Analysis Date = 03/30/06 
 Pct Recovery = 106%  Analysis Date = 03/02/06 
 Pct Recovery = 106%  Analysis Date = 03/02/06 
 Pct Recovery = 106%  Analysis Date = 02/02/06 
 Pct Recovery = 106%  Analysis Date = 02/02/06 
 Pct Recovery = 106%  Analysis Date = 01/05/06 
 Pct Recovery = 106%  Analysis Date = 01/05/06 
 Pct Recovery = 106%  Analysis Date = 12/08/05 
 Pct Recovery = 106%  Analysis Date = 12/08/05 
 Pct Recovery = 106%  Analysis Date = 11/10/05 
 Pct Recovery = 106%  Analysis Date = 11/10/05 
 Pct Recovery = 106%  Analysis Date = 10/13/05 
 Pct Recovery = 106%  Analysis Date = 10/13/05 
 Pct Recovery = 106%  Analysis Date = 09/15/05 
 Pct Recovery = 106%  Analysis Date = 09/15/05 
 Pct Recovery = 106%  Analysis Date = 08/18/05 
 Pct Recovery = 106%  Analysis Date = 08/18/05 
 Pct Recovery = 106%  Analysis Date = 07/21/05 
 Pct Recovery = 106%  Analysis Date = 07/21/05 
 Pct Recovery = 106%  Analysis Date = 06/23/05 
 Pct Recovery = 106%  Analysis Date = 06/23/05 
 Pct Recovery = 106%  Analysis Date = 05/26/05 
 Pct Recovery = 106%  Analysis Date = 05/26/05 
 Pct Recovery = 106%  Analysis Date = 04/28/05 
 Pct Recovery = 106%  Analysis Date = 04/28/05 
 Pct Recovery = 106%  Analysis Date = 03/31/05 
 Pct Recovery = 106%  Analysis Date = 03/31/05 
 Pct Recovery = 106%  Analysis Date = 03/03/05 
 Pct Recovery = 106%  Analysis Date = 03/03/05 
 Pct Recovery = 106%  Analysis Date = 02/03/05 
 Pct Recovery = 106%  Analysis Date = 02/03/05 
 Pct Recovery = 106%  Analysis Date = 01/06/05 
 Pct Recovery = 106%  Analysis Date = 01/06/05 
 Pct Recovery = 106%  Analysis Date = 12/09/04 
 Pct Recovery = 106%  Analysis Date = 12/09/04 
 Pct Recovery = 106%  Analysis Date = 11/11/04 
 Pct Recovery = 106%  Analysis Date = 11/11/04 
 Pct Recovery = 106%  Analysis Date = 10/14/04 
 Pct Recovery = 106%  Analysis Date = 10/14/04 
 Pct Recovery = 106%  Analysis Date = 09/16/04 
 Pct Recovery = 106%  Analysis Date = 09/16/04 
 Pct Recovery = 106%  Analysis Date = 08/19/04 
 Pct Recovery = 106%  Analysis Date = 08/19/04 
 Pct Recovery = 106%  Analysis Date = 07/22/04 
 Pct Recovery = 106%  Analysis Date = 07/22/04 
 Pct Recovery = 106%  Analysis Date = 06/24/04 
 Pct Recovery = 106%  Analysis Date = 06/24/04 
 Pct Recovery = 106%  Analysis Date = 05/27/04 
 Pct Recovery = 106%  Analysis Date = 05/27/04 
 Pct Recovery = 106%  Analysis Date = 04/29/04 
 Pct Recovery = 106%  Analysis Date = 04/29/04 
 Pct Recovery = 106%  Analysis Date = 04/01/04 
 Pct Recovery = 106%  Analysis Date = 04/01/04 
 Pct Recovery = 106%  Analysis Date = 03/04/04 
 Pct Recovery = 106%  Analysis Date = 03/04/04 
 Pct Recovery = 106%  Analysis Date = 02/05/04 
 Pct Recovery = 106%  Analysis Date = 02/05/04 
 Pct Recovery = 106%  Analysis Date = 01/08/04 
 Pct Recovery = 106%  Analysis Date = 01/08/04 
 Pct Recovery = 106%  Analysis Date = 12/11/03 
 Pct Recovery = 106%  Analysis Date = 12/11/03 
 Pct Recovery = 106%  Analysis Date = 11/13/03 
 Pct Recovery = 106%  Analysis Date = 11/13/03 
 Pct Recovery = 106%  Analysis Date = 10/16/03 
 Pct Recovery = 106%  Analysis Date = 10/16/03 
 Pct Recovery = 106%  Analysis Date = 09/18/03 
 Pct Recovery = 106%  Analysis Date = 09/18/03 
 Pct Recovery = 106%  Analysis Date = 08/21/03 
 Pct Recovery = 106%  Analysis Date = 08/21/03 
 Pct Recovery = 106%  Analysis Date = 07/24/03 
 Pct Recovery = 106%  Analysis Date = 07/24/03 
 Pct Recovery = 106%  Analysis Date = 06/26/03 
 Pct Recovery = 106%  Analysis Date = 06/26/03 
 Pct Recovery = 106%  Analysis Date = 05/29/03 
 Pct Recovery = 106%  Analysis Date = 05/29/03 
 Pct Recovery = 106%  Analysis Date = 05/01/03 
 Pct Recovery = 106%  Analysis Date = 05/01/03 
 Pct Recovery = 106%  Analysis Date = 04/03/03 
 Pct Recovery = 106%  Analysis Date = 04/03/03 
 Pct Recovery = 106%  Analysis Date = 03/06/03 
 Pct Recovery = 106%  Analysis Date = 03/06/03 
 Pct Recovery = 106%  Analysis Date = 02/06/03 
 Pct Recovery = 106%  Analysis Date = 02/06/03 
 Pct Recovery = 106%  Analysis Date = 01/09/03 
 Pct Recovery = 106%  Analysis Date = 01/09/03 
 Pct Recovery = 106%  Analysis Date = 12/12/02 
 Pct Recovery = 106%  Analysis Date = 12/12/02 
 Pct Recovery = 106%  Analysis Date = 11/14/02 
 Pct Recovery = 106%  Analysis Date = 11/14/02 
 Pct Recovery = 106%  Analysis Date = 10/17/02 
 Pct Recovery = 106%  Analysis Date = 10/17/02 
 Pct Recovery = 106%  Analysis Date = 09/19/02 
 Pct Recovery = 106%  Analysis Date = 09/19/02 
 Pct Recovery = 106%  Analysis Date = 08/22/02 
 Pct Recovery = 106%  Analysis Date = 08/22/02 
 Pct Recovery = 106%  Analysis Date = 07/25/02 
 Pct Recovery = 106%  Analysis Date = 07/25/02 
 Pct Recovery = 106%  Analysis Date = 06/27/02 
 Pct Recovery = 106%  Analysis Date = 06/27/02 
 Pct Recovery = 106%  Analysis Date = 05/30/02 
 Pct Recovery = 106%  Analysis Date = 05/30/02 
 Pct Recovery = 106%  Analysis Date = 05/02/02 
 Pct Recovery = 106%  Analysis Date = 05/02/02 
 Pct Recovery = 106%  Analysis Date = 04/04/02 
 Pct Recovery = 106%  Analysis Date = 04/04/02 
 Pct Recovery = 106%  Analysis Date = 03/07/02 
 Pct Recovery = 106%  Analysis Date = 03/07/02 
 Pct Recovery = 106%  Analysis Date = 02/07/02 
 Pct Recovery = 106%  Analysis Date = 02/07/02 
 Pct Recovery = 106%  Analysis Date = 01/10/02 
 Pct Recovery = 106%  Analysis Date = 01/10/02 
 Pct Recovery = 106%  Analysis Date = 12/13/01 
 Pct Recovery = 106%  Analysis Date = 12/13/01 
 Pct Recovery = 106%  Analysis Date = 11/15/01 
 Pct Recovery = 106%  Analysis Date = 11/15/01 
 Pct Recovery = 106%  Analysis Date = 10/18/01 
 Pct Recovery = 106%  Analysis Date = 10/18/01 
 Pct Recovery = 106%  Analysis Date = 09/20/01 
 Pct Recovery = 106%  Analysis Date = 09/20/01 
 Pct Recovery = 106%  Analysis Date = 08/23/01 
 Pct Recovery = 106%  Analysis Date = 08/23/01 
 Pct Recovery = 106%  Analysis Date = 07/26/01 
 Pct Recovery = 106%  Analysis Date = 07/26/01 
 Pct Recovery = 106%  Analysis Date = 06/28/01 
 Pct Recovery = 106%  Analysis Date = 06/28/01 
 Pct Recovery = 106%  Analysis Date = 05/31/01 
 Pct Recovery = 106%  Analysis Date = 05/31/01 
 Pct Recovery = 106%  Analysis Date = 05/04/01 
 Pct Recovery = 106%  Analysis Date = 05/04/01 
 Pct Recovery = 106%  Analysis Date = 04/06/01 
 Pct Recovery = 106%  Analysis Date = 04/06/01 
 Pct Recovery = 106%  Analysis Date = 03/09/01 
 Pct Recovery = 106%  Analysis Date = 03/09/01 
 Pct Recovery = 106%  Analysis Date = 02/09/01 
 Pct Recovery = 106%  Analysis Date = 02/09/01 
 Pct Recovery = 106%  Analysis Date = 01/12/01 
 Pct Recovery = 106%  Analysis Date = 01/12/01 
 Pct Recovery = 106%  Analysis Date = 12/15/00 
 Pct Recovery = 106%  Analysis Date = 12/15/00 
 Pct Recovery = 106%  Analysis Date = 11/17/00 
 Pct Recovery = 106%  Analysis Date = 11/17/00 
 Pct Recovery = 106%  Analysis Date = 10/20/00 
 Pct Recovery = 106%  Analysis Date = 10/20/00 
 Pct Recovery = 106%  Analysis Date = 09/22/00 
 Pct Recovery = 106%  Analysis Date = 09/22/00 
 Pct Recovery = 106%  Analysis Date = 08/25/00 
 Pct Recovery = 106%  Analysis Date = 08/25/00 
 Pct Recovery = 106%  Analysis Date = 07/28/00 
 Pct Recovery = 106%  Analysis Date = 07/28/00 
 Pct Recovery = 106%  Analysis Date = 06/30/00 
 Pct Recovery = 106%  Analysis Date = 06/30/00 
 Pct Recovery = 106%  Analysis Date = 06/02/00 
 Pct Recovery = 106%  Analysis Date = 06/02/00 
 Pct Recovery = 106%  Analysis Date = 05/05/00 
 Pct Recovery = 106%  Analysis Date = 05/05/00 
 Pct Recovery = 106%  Analysis Date = 04/07/00 
 Pct Recovery = 106%  Analysis Date = 04/07/00 
 Pct Recovery = 106%  Analysis Date = 03/10/00 
 Pct Recovery = 106%  Analysis Date = 03/10/00 
 Pct Recovery = 106%  Analysis Date = 02/11/00 
 Pct Recovery = 106%  Analysis Date = 02/11/00 
 Pct Recovery = 106%  Analysis Date = 01/14/00 
 Pct Recovery = 106%  Analysis Date = 01/14/00 
 Pct Recovery = 106%  Analysis Date = 12/17/99 
 Pct Recovery = 106%  Analysis Date = 12/17/99 
 Pct Recovery = 106%  Analysis Date = 11/19/99 
 Pct Recovery = 106%  Analysis Date = 11/19/99 
 Pct Recovery = 106%  Analysis Date = 10/22/99 
 Pct Recovery = 106%  Analysis Date = 10/22/99 
 Pct Recovery = 106%  Analysis Date = 09/24/99 
 Pct Recovery = 106%  Analysis Date = 09/24/99 
 Pct Recovery = 106%  Analysis Date = 08/27/99 
 Pct Recovery = 106%  Analysis Date = 08/27/99 
 Pct Recovery = 106%  Analysis Date = 07/30/99 
 Pct Recovery = 106%  Analysis Date = 07/30/99 
 Pct Recovery = 106%  Analysis Date = 07/02/99 
 Pct Recovery = 106%  Analysis Date = 07/02/99 
 Pct Recovery = 106%  Analysis Date = 06/04/99 
 Pct Recovery = 106%  Analysis Date = 06/04/99 
 Pct Recovery = 106%  Analysis Date = 05/07/99 
 Pct Recovery = 106%  Analysis Date = 05/07/99 
 Pct Recovery = 106%  Analysis Date = 04/09/99 
 Pct Recovery = 107%  Analysis Date = 04/09/99 
 Pct Recovery = 107%  Analysis Date = 03/12/99 
 Pct Recovery = 107%  Analysis Date = 03/12/99 
 Pct Recovery = 107%  Analysis Date = 02/12/99 
 Pct Recovery = 107%  Analysis Date = 02/12/99 
 Pct Recovery = 107%  Analysis Date = 01/15/99 
 Pct Recovery = 107%  Analysis Date = 01/15/99 
 Pct Recovery = 107%  Analysis Date = 12/18/98 
 Pct Recovery = 107%  Analysis Date = 12/18/98 
 Pct Recovery = 107%  Analysis Date = 11/20/98 
 Pct Recovery = 107%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
3-CHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 109% 10% 108% 9%
>= Reporting Level 120 100% 11% 99% 10%
Total 125 101% 11% 99% 10%

Sample Statistics
3-CHLOROPROPENE

Characteristic N % % Basis
Plotted 125 98% Spiked
Estimated Values 125 98% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 132 .  
False Negatives 1 1% 1 out of 127
Not Spiked 365 .  
False Positives 1 0% 1 out of 337

BQS OBSP Determination:
4-CHLOROTOLUENE
METHOD: 2021 , TESTIDCODE: 77277GCM66
Open Data Set

 Analysis Date = 07/09/99 
 SpikeMix = ERA 1210-98-04B: 30 µl 
 Pct Recovery = 94%  Analysis Date = 11/29/99 
 SpikeMix = ERA 1210-98-04B: 30 µl 
 Pct Recovery = 99%  Analysis Date = 11/09/99 
 SpikeMix = ERA 1210-98-04B: 30 µl 
 Pct Recovery = 97%  Analysis Date = 09/09/99 
 SpikeMix = ERA 1210-98-04B: 30 µl 
 Pct Recovery = 123%  Analysis Date = 12/22/12 
 SpikeMix = NSI 062112-01VOA: 40 µl & Supelco LB92787: 40 µl 
 Pct Recovery = 99%  Analysis Date = 01/19/13 
 SpikeMix = Accu 212051193: 40 µl & Abs 051712: 40 µl 
 Pct Recovery = 96%  Analysis Date = 05/24/99 
 SpikeMix = ERA 1210-98-04B: 10 µl 
 Pct Recovery = 106%  Analysis Date = 07/20/99 
 SpikeMix = ERA 1210-98-04B: 10 µl 
 Pct Recovery = 130%  Analysis Date = 10/13/99 
 SpikeMix = ERA 1210-98-04B: 10 µl 
 Pct Recovery = 107%  Analysis Date = 09/11/12 
 SpikeMix = NSI 062112-01VOA: 20 µl & Supelco LB92787: 20 µl 
 Pct Recovery = 95%  Analysis Date = 07/30/12 
 SpikeMix = Supelco LB92787: 20 µl & Abs 051712: 20 µl 
 Pct Recovery = 96%  Analysis Date = 11/08/12 
 SpikeMix = Crescent 05BB048: 20 µl & Accu 212051193: 20 µl 
 Pct Recovery = 105%  Analysis Date = 11/20/05 
 SpikeMix = Accu B5070191: 30 µl & Ultra CB-1578: 50 µl 
 Pct Recovery = 94%  Analysis Date = 04/07/06 
 SpikeMix = Accu B5070191: 30 µl & NSI 080405-01VOC: 20 µl 
 Pct Recovery = 112%  Analysis Date = 10/28/05 
 SpikeMix = Supelco LB31918: 30 µl & Accu B5070191: 30 µl 
 Pct Recovery = 108%  Analysis Date = 06/23/05 
 SpikeMix = Crescent 07DD035: 40 µl 
 Pct Recovery = 95%  Analysis Date = 04/06/05 
 SpikeMix = Crescent 07DD035: 40 µl 
 Pct Recovery = 85%  Analysis Date = 10/19/01 
 SpikeMix = ERA 1128-00-06B: 5 µl 
 Pct Recovery = 95%  Analysis Date = 07/31/01 
 SpikeMix = ERA 1128-00-06B: 5 µl 
 Pct Recovery = 89%  Analysis Date = 05/25/01 
 SpikeMix = ERA 1128-00-06B: 5 µl 
 Pct Recovery = 111%  Analysis Date = 05/03/01 
 SpikeMix = ERA 1128-00-06B: 5 µl 
 Pct Recovery = 100%  Analysis Date = 02/07/01 
 SpikeMix = ERA 1128-00-06B: 5 µl 
 Pct Recovery = 101%  Analysis Date = 05/03/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 81%  Analysis Date = 03/29/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 84%  Analysis Date = 02/28/13 
 SpikeMix = NSI 062112-01VOA: 10 µl & Accu 212051193: 10 µl 
 Pct Recovery = 100%  Analysis Date = 07/19/12 
 SpikeMix = Crescent 05BB048: 10 µl & Accu 212051193: 10 µl 
 Pct Recovery = 105%  Analysis Date = 09/25/03 
 SpikeMix = ERA 0828-02-09VOC: 40 µl 
 Pct Recovery = 90%  Analysis Date = 06/20/03 
 SpikeMix = ERA 0828-02-09VOC: 40 µl 
 Pct Recovery = 96%  Analysis Date = 03/06/03 
 SpikeMix = ERA 0828-02-09VOC: 40 µl 
 Pct Recovery = 92%  Analysis Date = 01/16/03 
 SpikeMix = ERA 0828-02-09VOC: 40 µl 
 Pct Recovery = 107%  Analysis Date = 02/26/99 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 91%  Analysis Date = 11/20/98 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 109%  Analysis Date = 05/24/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 102%  Analysis Date = 02/22/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 93%  Analysis Date = 12/16/98 
 SpikeMix = NSI Q-2002: 40 µl 
 Pct Recovery = 101%  Analysis Date = 06/30/09 
 SpikeMix = Ultra CE-2869: 40 µl 
 Pct Recovery = 80%  Analysis Date = 06/17/09 
 SpikeMix = Ultra CE-2869: 40 µl 
 Pct Recovery = 77%  Analysis Date = 04/21/09 
 SpikeMix = Abs 080408VOC: 40 µl 
 Pct Recovery = 82%  Analysis Date = 01/27/09 
 SpikeMix = Abs 080408VOC: 40 µl 
 Pct Recovery = 90%  Analysis Date = 10/04/03 
 SpikeMix = ERA 0828-02-09VOC: 15 µl 
 Pct Recovery = 101%  Analysis Date = 07/19/03 
 SpikeMix = ERA 0828-02-09VOC: 15 µl 
 Pct Recovery = 94%  Analysis Date = 05/12/03 
 SpikeMix = ERA 0828-02-09VOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 02/20/03 
 SpikeMix = ERA 0828-02-09VOC: 15 µl 
 Pct Recovery = 90%  Analysis Date = 09/05/02 
 SpikeMix = ERA 0830-01-06.1VOC: 40 µl 
 Pct Recovery = 96%  Analysis Date = 07/19/02 
 SpikeMix = ERA 0830-01-06.1VOC: 40 µl 
 Pct Recovery = 83%  Analysis Date = 04/26/02 
 SpikeMix = ERA 0830-01-06.1VOC: 40 µl 
 Pct Recovery = 101%  Analysis Date = 01/11/02 
 SpikeMix = ERA 0830-01-06.1VOC: 40 µl 
 Pct Recovery = 90%  Analysis Date = 03/31/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 89%  Analysis Date = 01/20/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 96%  Analysis Date = 11/17/01 
 SpikeMix = NSI 111700VOC: 25 µl 
 Pct Recovery = 94%  Analysis Date = 08/23/01 
 SpikeMix = NSI 111700VOC: 25 µl 
 Pct Recovery = 87%  Analysis Date = 06/01/01 
 SpikeMix = NSI 111700VOC: 25 µl 
 Pct Recovery = 102%  Analysis Date = 03/07/01 
 SpikeMix = NSI 111700VOC: 25 µl 
 Pct Recovery = 103%  Analysis Date = 04/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 104%  Analysis Date = 01/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 94%  Analysis Date = 08/11/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 70%  Analysis Date = 05/13/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 95%  Analysis Date = 03/31/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 90%  Analysis Date = 02/18/09 
 SpikeMix = Ultra CE-2869: 20 µl 
 Pct Recovery = 90%  Analysis Date = 05/17/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 96%  Analysis Date = 12/08/05 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 106%  Analysis Date = 02/15/06 
 SpikeMix = Supelco LB31918: 5 µl & Accu B5070191: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 106%  Analysis Date = 11/29/05 
 SpikeMix = Supelco LB31918: 5 µl & Accu B5070191: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 127%  Analysis Date = 07/28/06 
 SpikeMix = Accu B5070191: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 96%  Analysis Date = 06/06/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl 
 Pct Recovery = 122%  Analysis Date = 01/05/06 
 SpikeMix = Supelco LB31918: 5 µl & Accu B5070191: 5 µl 
 Pct Recovery = 106%  Analysis Date = 05/25/12 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 72%  Analysis Date = 05/08/12 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 72%  Analysis Date = 11/24/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 87%  Analysis Date = 06/10/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 68%  Analysis Date = 04/13/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 58%  Analysis Date = 01/22/11 
 SpikeMix = NSI 062310-01: 40 µl 
 Pct Recovery = 80%  Analysis Date = 08/29/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 76%  Analysis Date = 07/17/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 71%  Analysis Date = 06/09/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 71%  Analysis Date = 03/14/09 
 SpikeMix = Abs 080408VOC: 20 µl 
 Pct Recovery = 82%  Analysis Date = 08/15/05 
 SpikeMix = Protocol R1040726010: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 100%  Analysis Date = 03/04/05 
 SpikeMix = Protocol R1040726010: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 94%  Analysis Date = 05/11/05 
 SpikeMix = Protocol R1040726010: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 106%  Analysis Date = 08/21/10 
 SpikeMix = Spex Organics C1090901006: 30 µl 
 Pct Recovery = 82%  Analysis Date = 06/09/10 
 SpikeMix = Spex Organics C1090901006: 30 µl 
 Pct Recovery = 88%  Analysis Date = 03/17/10 
 SpikeMix = Spex Organics C1090901006: 30 µl 
 Pct Recovery = 85%  Analysis Date = 12/15/09 
 SpikeMix = Spex Organics C1090901006: 30 µl 
 Pct Recovery = 94%  Analysis Date = 06/22/05 
 SpikeMix = Protocol R1040726010: 5 µl 
 Pct Recovery = 106%  Analysis Date = 04/09/05 
 SpikeMix = Protocol R1040726010: 5 µl 
 Pct Recovery = 111%  Analysis Date = 02/01/05 
 SpikeMix = Protocol R1040726010: 5 µl 
 Pct Recovery = 117%  Analysis Date = 08/11/07 
 SpikeMix = Crescent 07FF068: 40 µl 
 Pct Recovery = 81%  Analysis Date = 06/16/07 
 SpikeMix = Crescent 07FF068: 40 µl 
 Pct Recovery = 100%  Analysis Date = 04/20/07 
 SpikeMix = Crescent 07FF068: 40 µl 
 Pct Recovery = 88%  Analysis Date = 03/01/07 
 SpikeMix = Crescent 07FF068: 40 µl 
 Pct Recovery = 88%  Analysis Date = 07/30/05 
 SpikeMix = Crescent 07DD035: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 57%  Analysis Date = 01/27/05 
 SpikeMix = Crescent 07DD035: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 100%  Analysis Date = 05/10/05 
 SpikeMix = Crescent 07DD035: 5 µl 
 Pct Recovery = 71%  Analysis Date = 02/25/05 
 SpikeMix = Crescent 07DD035: 5 µl 
 Pct Recovery = 86%  Analysis Date = 03/01/14 
 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl 
 Pct Recovery = 63%  Analysis Date = 07/24/13 
 SpikeMix = NSI 053013: 20 µl & Supelco LC00154: 20 µl 
 Pct Recovery = 73%  Analysis Date = 09/17/13 
 SpikeMix = Crescent 04CC151: 20 µl & Supelco LC00154: 20 µl 
 Pct Recovery = 73%  Analysis Date = 01/29/14 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 81%  Analysis Date = 09/17/13 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 78%  Analysis Date = 08/06/13 
 SpikeMix = Supelco LC00154: 20 µl & Abs 051413: 20 µl 
 Pct Recovery = 65%  Analysis Date = 11/01/13 
 SpikeMix = Accu 213041120: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 74%  Analysis Date = 12/12/13 
 SpikeMix = NSI 053013: 20 µl & Accu 213041120: 20 µl 
 Pct Recovery = 75%  Analysis Date = 01/03/03 
 SpikeMix = ERA 0830-01-06.1VOC: 15 µl 
 Pct Recovery = 108%  Analysis Date = 11/07/02 
 SpikeMix = ERA 0830-01-06.1VOC: 15 µl 
 Pct Recovery = 93%  Analysis Date = 10/11/02 
 SpikeMix = ERA 0830-01-06.1VOC: 15 µl 
 Pct Recovery = 77%  Analysis Date = 04/16/03 
 SpikeMix = ERA 0828-02-09VOC: 5 µl 
 Pct Recovery = 116%  Analysis Date = 12/13/02 
 SpikeMix = ERA 0828-02-09VOC: 5 µl 
 Pct Recovery = 88%  Analysis Date = 10/25/02 
 SpikeMix = ERA 0828-02-09VOC: 5 µl 
 Pct Recovery = 82%  Analysis Date = 03/10/12 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 74%  Analysis Date = 10/18/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 72%  Analysis Date = 09/17/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 72%  Analysis Date = 05/03/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 66%  Analysis Date = 03/01/11 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 74%  Analysis Date = 11/05/10 
 SpikeMix = NSI 062310-01: 20 µl 
 Pct Recovery = 76%  Analysis Date = 01/23/07 
 SpikeMix = Crescent 07FF068: 20 µl 
 Pct Recovery = 100%  Analysis Date = 11/07/06 
 SpikeMix = Crescent 07FF068: 20 µl 
 Pct Recovery = 88%  Analysis Date = 08/30/06 
 SpikeMix = Accu B5070191: 2 µl 
 Pct Recovery = 89%  Analysis Date = 12/15/05 
 SpikeMix = Accu B5070191: 2 µl 
 Pct Recovery = 114%  Analysis Date = 10/01/02 
 SpikeMix = ERA 0830-01-06.1VOC: 10 µl 
 Pct Recovery = 74%  Analysis Date = 06/11/02 
 SpikeMix = ERA 0830-01-06.1VOC: 10 µl 
 Pct Recovery = 109%  Analysis Date = 03/04/02 
 SpikeMix = ERA 0830-01-06.1VOC: 10 µl 
 Pct Recovery = 111%  Analysis Date = 11/27/01 
 SpikeMix = ERA 0830-01-06.1VOC: 10 µl 
 Pct Recovery = 112%  Analysis Date = 12/27/00 
 SpikeMix = NSI 121699: 5 µl 
 Pct Recovery = 117%  Analysis Date = 12/14/00 
 SpikeMix = NSI 121699: 5 µl 
 Pct Recovery = 74%  Analysis Date = 09/06/00 
 SpikeMix = NSI 121699: 5 µl 
 Pct Recovery = 137%  Analysis Date = 06/27/00 
 SpikeMix = NSI 121699: 5 µl 
 Pct Recovery = 77%  Analysis Date = 04/18/00 
 SpikeMix = NSI 121699: 5 µl 
 Pct Recovery = 79%  Analysis Date = 09/17/13 
 SpikeMix = Crescent 04CC151: 10 µl & Supelco LC00154: 10 µl 
 Pct Recovery = 79%  Analysis Date = 12/12/13 
 SpikeMix = Supelco LC00154: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 78%  Analysis Date = 07/09/10 
 SpikeMix = Spex Organics C1090901006: 10 µl 
 Pct Recovery = 100%  Analysis Date = 04/27/10 
 SpikeMix = Spex Organics C1090901006: 10 µl 
 Pct Recovery = 82%  Analysis Date = 02/09/10 
 SpikeMix = Spex Organics C1090901006: 10 µl 
 Pct Recovery = 77%  Analysis Date = 11/04/09 
 SpikeMix = Spex Organics C1090901006: 10 µl 
 Pct Recovery = 76%  Analysis Date = 12/31/13 
 SpikeMix = Accu 213041120: 10 µl & ChemService 1530700: 10 µl 
 Pct Recovery = 82%  Analysis Date = 01/15/14 
 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl 
 Pct Recovery = 74%  Analysis Date = 05/22/13 
 SpikeMix = Crescent 04CC151: 10 µl & Accu 213041120: 10 µl 
 Pct Recovery = 85%  Analysis Date = 03/19/14 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 78%  Analysis Date = 06/08/13 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 90%  Analysis Date = 12/16/08 
 SpikeMix = Supelco LB55705: 20 µl 
 Pct Recovery = 107%  Analysis Date = 11/18/08 
 SpikeMix = Supelco LB55705: 20 µl 
 Pct Recovery = 89%  Analysis Date = 10/17/08 
 SpikeMix = Supelco LB55705: 20 µl 
 Pct Recovery = 89%  Analysis Date = 08/15/08 
 SpikeMix = Supelco LB55705: 20 µl 
 Pct Recovery = 89%  Analysis Date = 05/09/08 
 SpikeMix = Supelco LB55705: 20 µl 
 Pct Recovery = 107%  Analysis Date = 03/22/08 
 SpikeMix = Supelco LB55705: 20 µl 
 Pct Recovery = 89%  Analysis Date = 09/05/08 
 SpikeMix = Abs 071107VOC: 20 µl 
 Pct Recovery = 89%  Analysis Date = 12/18/07 
 SpikeMix = Abs 071107VOC: 20 µl 
 Pct Recovery = 107%  Analysis Date = 10/19/07 
 SpikeMix = Abs 071107VOC: 20 µl 
 Pct Recovery = 89%  Analysis Date = 09/22/01 
 SpikeMix = NSI 111700VOC: 5 µl 
 Pct Recovery = 94%  Analysis Date = 07/21/01 
 SpikeMix = NSI 111700VOC: 5 µl 
 Pct Recovery = 90%  Analysis Date = 10/14/98 
 SpikeMix = NSI Q-16750-50 101497: 2 µl 
 Pct Recovery = 45%  Analysis Date = 04/11/01 
 SpikeMix = NSI 111700VOC: 5 µl 
 Pct Recovery = 88%  Analysis Date = 01/24/01 
 SpikeMix = NSI 111700VOC: 5 µl 
 Pct Recovery = 80%  Analysis Date = 11/29/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 78%  Analysis Date = 09/19/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 96%  Analysis Date = 08/02/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 100%  Analysis Date = 07/06/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 87%  Analysis Date = 03/19/14 
 Pct Recovery = 79%  Analysis Date = 02/18/14 
 Pct Recovery = 79%  Analysis Date = 02/18/14 
 Pct Recovery = 79%  Analysis Date = 01/21/14 
 Pct Recovery = 79%  Analysis Date = 01/21/14 
 Pct Recovery = 79%  Analysis Date = 12/24/13 
 Pct Recovery = 79%  Analysis Date = 12/24/13 
 Pct Recovery = 79%  Analysis Date = 11/26/13 
 Pct Recovery = 79%  Analysis Date = 11/26/13 
 Pct Recovery = 79%  Analysis Date = 10/29/13 
 Pct Recovery = 79%  Analysis Date = 10/29/13 
 Pct Recovery = 79%  Analysis Date = 09/30/13 
 Pct Recovery = 79%  Analysis Date = 09/30/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 09/02/13 
 Pct Recovery = 79%  Analysis Date = 08/05/13 
 Pct Recovery = 79%  Analysis Date = 08/05/13 
 Pct Recovery = 79%  Analysis Date = 07/08/13 
 Pct Recovery = 80%  Analysis Date = 07/08/13 
 Pct Recovery = 80%  Analysis Date = 06/10/13 
 Pct Recovery = 80%  Analysis Date = 06/10/13 
 Pct Recovery = 80%  Analysis Date = 05/13/13 
 Pct Recovery = 80%  Analysis Date = 05/13/13 
 Pct Recovery = 80%  Analysis Date = 04/14/13 
 Pct Recovery = 80%  Analysis Date = 04/14/13 
 Pct Recovery = 80%  Analysis Date = 03/17/13 
 Pct Recovery = 80%  Analysis Date = 03/17/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 02/17/13 
 Pct Recovery = 80%  Analysis Date = 01/20/13 
 Pct Recovery = 80%  Analysis Date = 01/20/13 
 Pct Recovery = 80%  Analysis Date = 12/23/12 
 Pct Recovery = 80%  Analysis Date = 12/23/12 
 Pct Recovery = 80%  Analysis Date = 11/25/12 
 Pct Recovery = 80%  Analysis Date = 11/25/12 
 Pct Recovery = 80%  Analysis Date = 10/27/12 
 Pct Recovery = 81%  Analysis Date = 10/27/12 
 Pct Recovery = 81%  Analysis Date = 09/29/12 
 Pct Recovery = 81%  Analysis Date = 09/29/12 
 Pct Recovery = 81%  Analysis Date = 09/01/12 
 Pct Recovery = 81%  Analysis Date = 09/01/12 
 Pct Recovery = 81%  Analysis Date = 08/04/12 
 Pct Recovery = 81%  Analysis Date = 08/04/12 
 Pct Recovery = 81%  Analysis Date = 07/07/12 
 Pct Recovery = 81%  Analysis Date = 07/07/12 
 Pct Recovery = 81%  Analysis Date = 06/09/12 
 Pct Recovery = 81%  Analysis Date = 06/09/12 
 Pct Recovery = 81%  Analysis Date = 05/11/12 
 Pct Recovery = 81%  Analysis Date = 05/11/12 
 Pct Recovery = 81%  Analysis Date = 04/13/12 
 Pct Recovery = 81%  Analysis Date = 04/13/12 
 Pct Recovery = 81%  Analysis Date = 03/16/12 
 Pct Recovery = 81%  Analysis Date = 03/16/12 
 Pct Recovery = 81%  Analysis Date = 02/17/12 
 Pct Recovery = 82%  Analysis Date = 02/17/12 
 Pct Recovery = 82%  Analysis Date = 01/20/12 
 Pct Recovery = 82%  Analysis Date = 01/20/12 
 Pct Recovery = 82%  Analysis Date = 12/23/11 
 Pct Recovery = 82%  Analysis Date = 12/23/11 
 Pct Recovery = 82%  Analysis Date = 11/24/11 
 Pct Recovery = 82%  Analysis Date = 11/24/11 
 Pct Recovery = 82%  Analysis Date = 10/27/11 
 Pct Recovery = 82%  Analysis Date = 10/27/11 
 Pct Recovery = 82%  Analysis Date = 09/29/11 
 Pct Recovery = 82%  Analysis Date = 09/29/11 
 Pct Recovery = 82%  Analysis Date = 09/01/11 
 Pct Recovery = 82%  Analysis Date = 09/01/11 
 Pct Recovery = 82%  Analysis Date = 08/04/11 
 Pct Recovery = 82%  Analysis Date = 08/04/11 
 Pct Recovery = 82%  Analysis Date = 07/06/11 
 Pct Recovery = 83%  Analysis Date = 07/06/11 
 Pct Recovery = 83%  Analysis Date = 06/08/11 
 Pct Recovery = 83%  Analysis Date = 06/08/11 
 Pct Recovery = 83%  Analysis Date = 05/11/11 
 Pct Recovery = 83%  Analysis Date = 05/11/11 
 Pct Recovery = 83%  Analysis Date = 04/13/11 
 Pct Recovery = 83%  Analysis Date = 04/13/11 
 Pct Recovery = 83%  Analysis Date = 03/16/11 
 Pct Recovery = 83%  Analysis Date = 03/16/11 
 Pct Recovery = 83%  Analysis Date = 02/16/11 
 Pct Recovery = 83%  Analysis Date = 02/16/11 
 Pct Recovery = 83%  Analysis Date = 01/18/11 
 Pct Recovery = 83%  Analysis Date = 01/18/11 
 Pct Recovery = 83%  Analysis Date = 12/21/10 
 Pct Recovery = 83%  Analysis Date = 12/21/10 
 Pct Recovery = 83%  Analysis Date = 11/23/10 
 Pct Recovery = 84%  Analysis Date = 11/23/10 
 Pct Recovery = 84%  Analysis Date = 10/26/10 
 Pct Recovery = 84%  Analysis Date = 10/26/10 
 Pct Recovery = 84%  Analysis Date = 09/28/10 
 Pct Recovery = 84%  Analysis Date = 09/28/10 
 Pct Recovery = 84%  Analysis Date = 08/31/10 
 Pct Recovery = 84%  Analysis Date = 08/31/10 
 Pct Recovery = 84%  Analysis Date = 08/02/10 
 Pct Recovery = 84%  Analysis Date = 08/02/10 
 Pct Recovery = 84%  Analysis Date = 07/05/10 
 Pct Recovery = 84%  Analysis Date = 07/05/10 
 Pct Recovery = 84%  Analysis Date = 06/07/10 
 Pct Recovery = 84%  Analysis Date = 06/07/10 
 Pct Recovery = 84%  Analysis Date = 05/10/10 
 Pct Recovery = 85%  Analysis Date = 05/10/10 
 Pct Recovery = 85%  Analysis Date = 04/12/10 
 Pct Recovery = 85%  Analysis Date = 04/12/10 
 Pct Recovery = 85%  Analysis Date = 03/15/10 
 Pct Recovery = 85%  Analysis Date = 03/15/10 
 Pct Recovery = 85%  Analysis Date = 02/14/10 
 Pct Recovery = 85%  Analysis Date = 02/14/10 
 Pct Recovery = 85%  Analysis Date = 01/17/10 
 Pct Recovery = 85%  Analysis Date = 01/17/10 
 Pct Recovery = 85%  Analysis Date = 12/20/09 
 Pct Recovery = 85%  Analysis Date = 12/20/09 
 Pct Recovery = 85%  Analysis Date = 11/22/09 
 Pct Recovery = 85%  Analysis Date = 11/22/09 
 Pct Recovery = 85%  Analysis Date = 10/25/09 
 Pct Recovery = 85%  Analysis Date = 10/25/09 
 Pct Recovery = 85%  Analysis Date = 09/27/09 
 Pct Recovery = 86%  Analysis Date = 09/27/09 
 Pct Recovery = 86%  Analysis Date = 08/29/09 
 Pct Recovery = 86%  Analysis Date = 08/29/09 
 Pct Recovery = 86%  Analysis Date = 08/01/09 
 Pct Recovery = 86%  Analysis Date = 08/01/09 
 Pct Recovery = 86%  Analysis Date = 07/04/09 
 Pct Recovery = 86%  Analysis Date = 07/04/09 
 Pct Recovery = 86%  Analysis Date = 06/06/09 
 Pct Recovery = 86%  Analysis Date = 06/06/09 
 Pct Recovery = 86%  Analysis Date = 05/09/09 
 Pct Recovery = 86%  Analysis Date = 05/09/09 
 Pct Recovery = 86%  Analysis Date = 04/10/09 
 Pct Recovery = 87%  Analysis Date = 04/10/09 
 Pct Recovery = 87%  Analysis Date = 03/13/09 
 Pct Recovery = 87%  Analysis Date = 03/13/09 
 Pct Recovery = 87%  Analysis Date = 02/13/09 
 Pct Recovery = 87%  Analysis Date = 02/13/09 
 Pct Recovery = 87%  Analysis Date = 01/16/09 
 Pct Recovery = 88%  Analysis Date = 01/16/09 
 Pct Recovery = 88%  Analysis Date = 12/19/08 
 Pct Recovery = 88%  Analysis Date = 12/19/08 
 Pct Recovery = 88%  Analysis Date = 11/21/08 
 Pct Recovery = 88%  Analysis Date = 11/21/08 
 Pct Recovery = 88%  Analysis Date = 10/23/08 
 Pct Recovery = 88%  Analysis Date = 10/23/08 
 Pct Recovery = 88%  Analysis Date = 09/25/08 
 Pct Recovery = 89%  Analysis Date = 09/25/08 
 Pct Recovery = 89%  Analysis Date = 08/28/08 
 Pct Recovery = 89%  Analysis Date = 08/28/08 
 Pct Recovery = 89%  Analysis Date = 07/31/08 
 Pct Recovery = 89%  Analysis Date = 07/31/08 
 Pct Recovery = 89%  Analysis Date = 07/03/08 
 Pct Recovery = 89%  Analysis Date = 07/03/08 
 Pct Recovery = 89%  Analysis Date = 06/05/08 
 Pct Recovery = 90%  Analysis Date = 06/05/08 
 Pct Recovery = 90%  Analysis Date = 05/07/08 
 Pct Recovery = 90%  Analysis Date = 05/07/08 
 Pct Recovery = 90%  Analysis Date = 04/09/08 
 Pct Recovery = 90%  Analysis Date = 04/09/08 
 Pct Recovery = 90%  Analysis Date = 03/12/08 
 Pct Recovery = 90%  Analysis Date = 03/12/08 
 Pct Recovery = 90%  Analysis Date = 02/13/08 
 Pct Recovery = 91%  Analysis Date = 02/13/08 
 Pct Recovery = 91%  Analysis Date = 01/16/08 
 Pct Recovery = 91%  Analysis Date = 01/16/08 
 Pct Recovery = 91%  Analysis Date = 12/19/07 
 Pct Recovery = 91%  Analysis Date = 12/19/07 
 Pct Recovery = 91%  Analysis Date = 11/20/07 
 Pct Recovery = 91%  Analysis Date = 11/20/07 
 Pct Recovery = 91%  Analysis Date = 10/23/07 
 Pct Recovery = 92%  Analysis Date = 10/23/07 
 Pct Recovery = 92%  Analysis Date = 09/25/07 
 Pct Recovery = 92%  Analysis Date = 09/25/07 
 Pct Recovery = 92%  Analysis Date = 08/28/07 
 Pct Recovery = 92%  Analysis Date = 08/28/07 
 Pct Recovery = 92%  Analysis Date = 07/31/07 
 Pct Recovery = 92%  Analysis Date = 07/31/07 
 Pct Recovery = 92%  Analysis Date = 07/03/07 
 Pct Recovery = 93%  Analysis Date = 07/03/07 
 Pct Recovery = 93%  Analysis Date = 06/04/07 
 Pct Recovery = 93%  Analysis Date = 06/04/07 
 Pct Recovery = 93%  Analysis Date = 05/07/07 
 Pct Recovery = 93%  Analysis Date = 05/07/07 
 Pct Recovery = 93%  Analysis Date = 04/09/07 
 Pct Recovery = 93%  Analysis Date = 04/09/07 
 Pct Recovery = 93%  Analysis Date = 03/12/07 
 Pct Recovery = 94%  Analysis Date = 03/12/07 
 Pct Recovery = 94%  Analysis Date = 02/12/07 
 Pct Recovery = 94%  Analysis Date = 02/12/07 
 Pct Recovery = 94%  Analysis Date = 01/14/07 
 Pct Recovery = 94%  Analysis Date = 01/14/07 
 Pct Recovery = 94%  Analysis Date = 12/17/06 
 Pct Recovery = 94%  Analysis Date = 12/17/06 
 Pct Recovery = 94%  Analysis Date = 11/19/06 
 Pct Recovery = 94%  Analysis Date = 11/19/06 
 Pct Recovery = 94%  Analysis Date = 10/22/06 
 Pct Recovery = 95%  Analysis Date = 10/22/06 
 Pct Recovery = 95%  Analysis Date = 09/24/06 
 Pct Recovery = 95%  Analysis Date = 09/24/06 
 Pct Recovery = 95%  Analysis Date = 08/27/06 
 Pct Recovery = 95%  Analysis Date = 08/27/06 
 Pct Recovery = 95%  Analysis Date = 07/29/06 
 Pct Recovery = 95%  Analysis Date = 07/29/06 
 Pct Recovery = 95%  Analysis Date = 07/01/06 
 Pct Recovery = 95%  Analysis Date = 07/01/06 
 Pct Recovery = 95%  Analysis Date = 06/03/06 
 Pct Recovery = 95%  Analysis Date = 06/03/06 
 Pct Recovery = 95%  Analysis Date = 05/06/06 
 Pct Recovery = 96%  Analysis Date = 05/06/06 
 Pct Recovery = 96%  Analysis Date = 04/08/06 
 Pct Recovery = 96%  Analysis Date = 04/08/06 
 Pct Recovery = 96%  Analysis Date = 03/11/06 
 Pct Recovery = 96%  Analysis Date = 03/11/06 
 Pct Recovery = 96%  Analysis Date = 02/10/06 
 Pct Recovery = 96%  Analysis Date = 02/10/06 
 Pct Recovery = 96%  Analysis Date = 01/13/06 
 Pct Recovery = 96%  Analysis Date = 01/13/06 
 Pct Recovery = 96%  Analysis Date = 12/16/05 
 Pct Recovery = 97%  Analysis Date = 12/16/05 
 Pct Recovery = 97%  Analysis Date = 11/18/05 
 Pct Recovery = 97%  Analysis Date = 11/18/05 
 Pct Recovery = 97%  Analysis Date = 10/21/05 
 Pct Recovery = 97%  Analysis Date = 10/21/05 
 Pct Recovery = 97%  Analysis Date = 09/23/05 
 Pct Recovery = 97%  Analysis Date = 09/23/05 
 Pct Recovery = 97%  Analysis Date = 08/25/05 
 Pct Recovery = 97%  Analysis Date = 08/25/05 
 Pct Recovery = 97%  Analysis Date = 07/28/05 
 Pct Recovery = 97%  Analysis Date = 07/28/05 
 Pct Recovery = 97%  Analysis Date = 06/30/05 
 Pct Recovery = 97%  Analysis Date = 06/30/05 
 Pct Recovery = 97%  Analysis Date = 06/02/05 
 Pct Recovery = 97%  Analysis Date = 06/02/05 
 Pct Recovery = 97%  Analysis Date = 05/05/05 
 Pct Recovery = 97%  Analysis Date = 05/05/05 
 Pct Recovery = 97%  Analysis Date = 04/07/05 
 Pct Recovery = 97%  Analysis Date = 04/07/05 
 Pct Recovery = 97%  Analysis Date = 03/09/05 
 Pct Recovery = 97%  Analysis Date = 03/09/05 
 Pct Recovery = 97%  Analysis Date = 02/09/05 
 Pct Recovery = 97%  Analysis Date = 02/09/05 
 Pct Recovery = 97%  Analysis Date = 01/12/05 
 Pct Recovery = 97%  Analysis Date = 01/12/05 
 Pct Recovery = 97%  Analysis Date = 12/15/04 
 Pct Recovery = 97%  Analysis Date = 12/15/04 
 Pct Recovery = 97%  Analysis Date = 11/17/04 
 Pct Recovery = 97%  Analysis Date = 11/17/04 
 Pct Recovery = 97%  Analysis Date = 10/19/04 
 Pct Recovery = 97%  Analysis Date = 10/19/04 
 Pct Recovery = 97%  Analysis Date = 09/21/04 
 Pct Recovery = 97%  Analysis Date = 09/21/04 
 Pct Recovery = 97%  Analysis Date = 08/24/04 
 Pct Recovery = 97%  Analysis Date = 08/24/04 
 Pct Recovery = 97%  Analysis Date = 07/27/04 
 Pct Recovery = 97%  Analysis Date = 07/27/04 
 Pct Recovery = 97%  Analysis Date = 06/29/04 
 Pct Recovery = 97%  Analysis Date = 06/29/04 
 Pct Recovery = 97%  Analysis Date = 06/01/04 
 Pct Recovery = 97%  Analysis Date = 06/01/04 
 Pct Recovery = 97%  Analysis Date = 05/03/04 
 Pct Recovery = 97%  Analysis Date = 05/03/04 
 Pct Recovery = 97%  Analysis Date = 04/05/04 
 Pct Recovery = 97%  Analysis Date = 04/05/04 
 Pct Recovery = 97%  Analysis Date = 03/08/04 
 Pct Recovery = 97%  Analysis Date = 03/08/04 
 Pct Recovery = 97%  Analysis Date = 02/09/04 
 Pct Recovery = 97%  Analysis Date = 02/09/04 
 Pct Recovery = 97%  Analysis Date = 01/12/04 
 Pct Recovery = 97%  Analysis Date = 01/12/04 
 Pct Recovery = 97%  Analysis Date = 12/15/03 
 Pct Recovery = 97%  Analysis Date = 12/15/03 
 Pct Recovery = 97%  Analysis Date = 11/16/03 
 Pct Recovery = 97%  Analysis Date = 11/16/03 
 Pct Recovery = 97%  Analysis Date = 10/19/03 
 Pct Recovery = 97%  Analysis Date = 10/19/03 
 Pct Recovery = 97%  Analysis Date = 09/21/03 
 Pct Recovery = 97%  Analysis Date = 09/21/03 
 Pct Recovery = 97%  Analysis Date = 08/24/03 
 Pct Recovery = 97%  Analysis Date = 08/24/03 
 Pct Recovery = 97%  Analysis Date = 07/27/03 
 Pct Recovery = 97%  Analysis Date = 07/27/03 
 Pct Recovery = 97%  Analysis Date = 06/29/03 
 Pct Recovery = 97%  Analysis Date = 06/29/03 
 Pct Recovery = 97%  Analysis Date = 05/31/03 
 Pct Recovery = 97%  Analysis Date = 05/31/03 
 Pct Recovery = 97%  Analysis Date = 05/03/03 
 Pct Recovery = 97%  Analysis Date = 05/03/03 
 Pct Recovery = 97%  Analysis Date = 04/05/03 
 Pct Recovery = 97%  Analysis Date = 04/05/03 
 Pct Recovery = 97%  Analysis Date = 03/08/03 
 Pct Recovery = 97%  Analysis Date = 03/08/03 
 Pct Recovery = 97%  Analysis Date = 02/08/03 
 Pct Recovery = 97%  Analysis Date = 02/08/03 
 Pct Recovery = 97%  Analysis Date = 01/11/03 
 Pct Recovery = 97%  Analysis Date = 01/11/03 
 Pct Recovery = 97%  Analysis Date = 12/13/02 
 Pct Recovery = 97%  Analysis Date = 12/13/02 
 Pct Recovery = 97%  Analysis Date = 11/15/02 
 Pct Recovery = 97%  Analysis Date = 11/15/02 
 Pct Recovery = 97%  Analysis Date = 10/18/02 
 Pct Recovery = 97%  Analysis Date = 10/18/02 
 Pct Recovery = 97%  Analysis Date = 09/20/02 
 Pct Recovery = 97%  Analysis Date = 09/20/02 
 Pct Recovery = 97%  Analysis Date = 08/23/02 
 Pct Recovery = 97%  Analysis Date = 08/23/02 
 Pct Recovery = 97%  Analysis Date = 07/25/02 
 Pct Recovery = 97%  Analysis Date = 07/25/02 
 Pct Recovery = 97%  Analysis Date = 06/27/02 
 Pct Recovery = 97%  Analysis Date = 06/27/02 
 Pct Recovery = 97%  Analysis Date = 05/30/02 
 Pct Recovery = 97%  Analysis Date = 05/30/02 
 Pct Recovery = 97%  Analysis Date = 05/02/02 
 Pct Recovery = 97%  Analysis Date = 05/02/02 
 Pct Recovery = 97%  Analysis Date = 04/04/02 
 Pct Recovery = 97%  Analysis Date = 04/04/02 
 Pct Recovery = 97%  Analysis Date = 03/07/02 
 Pct Recovery = 97%  Analysis Date = 03/07/02 
 Pct Recovery = 97%  Analysis Date = 02/06/02 
 Pct Recovery = 97%  Analysis Date = 02/06/02 
 Pct Recovery = 97%  Analysis Date = 01/09/02 
 Pct Recovery = 97%  Analysis Date = 01/09/02 
 Pct Recovery = 97%  Analysis Date = 12/12/01 
 Pct Recovery = 97%  Analysis Date = 12/12/01 
 Pct Recovery = 97%  Analysis Date = 11/14/01 
 Pct Recovery = 96%  Analysis Date = 11/14/01 
 Pct Recovery = 96%  Analysis Date = 10/17/01 
 Pct Recovery = 96%  Analysis Date = 10/17/01 
 Pct Recovery = 96%  Analysis Date = 09/19/01 
 Pct Recovery = 96%  Analysis Date = 09/19/01 
 Pct Recovery = 96%  Analysis Date = 08/21/01 
 Pct Recovery = 96%  Analysis Date = 08/21/01 
 Pct Recovery = 96%  Analysis Date = 07/24/01 
 Pct Recovery = 96%  Analysis Date = 07/24/01 
 Pct Recovery = 96%  Analysis Date = 06/26/01 
 Pct Recovery = 96%  Analysis Date = 06/26/01 
 Pct Recovery = 96%  Analysis Date = 05/29/01 
 Pct Recovery = 96%  Analysis Date = 05/29/01 
 Pct Recovery = 96%  Analysis Date = 05/01/01 
 Pct Recovery = 96%  Analysis Date = 05/01/01 
 Pct Recovery = 96%  Analysis Date = 04/03/01 
 Pct Recovery = 96%  Analysis Date = 04/03/01 
 Pct Recovery = 96%  Analysis Date = 03/05/01 
 Pct Recovery = 96%  Analysis Date = 03/05/01 
 Pct Recovery = 96%  Analysis Date = 02/05/01 
 Pct Recovery = 96%  Analysis Date = 02/05/01 
 Pct Recovery = 96%  Analysis Date = 01/08/01 
 Pct Recovery = 96%  Analysis Date = 01/08/01 
 Pct Recovery = 96%  Analysis Date = 12/11/00 
 Pct Recovery = 96%  Analysis Date = 12/11/00 
 Pct Recovery = 96%  Analysis Date = 11/13/00 
 Pct Recovery = 96%  Analysis Date = 11/13/00 
 Pct Recovery = 96%  Analysis Date = 10/16/00 
 Pct Recovery = 96%  Analysis Date = 10/16/00 
 Pct Recovery = 96%  Analysis Date = 09/17/00 
 Pct Recovery = 96%  Analysis Date = 09/17/00 
 Pct Recovery = 96%  Analysis Date = 08/20/00 
 Pct Recovery = 96%  Analysis Date = 08/20/00 
 Pct Recovery = 96%  Analysis Date = 07/23/00 
 Pct Recovery = 96%  Analysis Date = 07/23/00 
 Pct Recovery = 96%  Analysis Date = 06/25/00 
 Pct Recovery = 96%  Analysis Date = 06/25/00 
 Pct Recovery = 96%  Analysis Date = 05/28/00 
 Pct Recovery = 96%  Analysis Date = 05/28/00 
 Pct Recovery = 96%  Analysis Date = 04/30/00 
 Pct Recovery = 96%  Analysis Date = 04/30/00 
 Pct Recovery = 96%  Analysis Date = 04/01/00 
 Pct Recovery = 96%  Analysis Date = 04/01/00 
 Pct Recovery = 96%  Analysis Date = 03/04/00 
 Pct Recovery = 96%  Analysis Date = 03/04/00 
 Pct Recovery = 96%  Analysis Date = 02/05/00 
 Pct Recovery = 96%  Analysis Date = 02/05/00 
 Pct Recovery = 96%  Analysis Date = 01/08/00 
 Pct Recovery = 96%  Analysis Date = 01/08/00 
 Pct Recovery = 96%  Analysis Date = 12/11/99 
 Pct Recovery = 96%  Analysis Date = 12/11/99 
 Pct Recovery = 96%  Analysis Date = 11/12/99 
 Pct Recovery = 96%  Analysis Date = 11/12/99 
 Pct Recovery = 96%  Analysis Date = 10/15/99 
 Pct Recovery = 96%  Analysis Date = 10/15/99 
 Pct Recovery = 96%  Analysis Date = 09/17/99 
 Pct Recovery = 96%  Analysis Date = 09/17/99 
 Pct Recovery = 96%  Analysis Date = 08/20/99 
 Pct Recovery = 96%  Analysis Date = 08/20/99 
 Pct Recovery = 96%  Analysis Date = 07/23/99 
 Pct Recovery = 96%  Analysis Date = 07/23/99 
 Pct Recovery = 96%  Analysis Date = 06/25/99 
 Pct Recovery = 96%  Analysis Date = 06/25/99 
 Pct Recovery = 96%  Analysis Date = 05/27/99 
 Pct Recovery = 96%  Analysis Date = 05/27/99 
 Pct Recovery = 96%  Analysis Date = 04/29/99 
 Pct Recovery = 96%  Analysis Date = 04/29/99 
 Pct Recovery = 96%  Analysis Date = 04/01/99 
 Pct Recovery = 96%  Analysis Date = 04/01/99 
 Pct Recovery = 96%  Analysis Date = 03/04/99 
 Pct Recovery = 96%  Analysis Date = 03/04/99 
 Pct Recovery = 96%  Analysis Date = 02/04/99 
 Pct Recovery = 96%  Analysis Date = 02/04/99 
 Pct Recovery = 96%  Analysis Date = 01/07/99 
 Pct Recovery = 96%  Analysis Date = 01/07/99 
 Pct Recovery = 96%  Analysis Date = 12/09/98 
 Pct Recovery = 96%  Analysis Date = 12/09/98 
 Pct Recovery = 96%  Analysis Date = 11/11/98 
 Pct Recovery = 96%  Analysis Date = 11/11/98 
 Pct Recovery = 96%  Analysis Date = 10/14/98 
 Pct Recovery = 96%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
4-CHLOROTOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 82% 18% 87% 14%
>= Reporting Level 149 91% 15% 90% 15%
Total 156 91% 15% 90% 15%

Sample Statistics
4-CHLOROTOLUENE

Characteristic N % % Basis
Plotted 156 100% Spiked
Estimated Values 39 25% Spiked
Deleted Values 1 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 157 .  
False Negatives 0 0% 0 out of 156
Not Spiked 319 .  
False Positives 1 0% 1 out of 319

BQS OBSP Determination:
4-ISOPROPYL-1-METHYLBENZENE (CYMENE)
METHOD: 2021 , TESTIDCODE: 77356GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
4-ISOPROPYL-1-METHYLBENZENE (CYMENE)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 79% 31% 77% 22%
>= Reporting Level 132 83% 17% 79% 17%
Total 137 83% 17% 79% 17%

Sample Statistics
4-ISOPROPYL-1-METHYLBENZENE (CYMENE)

Characteristic N % % Basis
Plotted 137 100% Spiked
Estimated Values 16 12% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 165 .  
False Negatives 0 0% 0 out of 137
Not Spiked 343 .  
False Positives 1 0% 1 out of 338

BQS OBSP Determination:
4-METHYL-2-PENTANONE
METHOD: 2021 , TESTIDCODE: 78133GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
4-METHYL-2-PENTANONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 104% 34% 105% 40%
>= Reporting Level 134 99% 13% 98% 13%
Total 143 99% 15% 98% 13%

Sample Statistics
4-METHYL-2-PENTANONE

Characteristic N % % Basis
Plotted 143 93% Spiked
Estimated Values 57 37% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 9 6% Spiked
Spiked 165 .  
False Negatives 2 1% 2 out of 154
Not Spiked 343 .  
False Positives 0 0% 0 out of 321

BQS OBSP Determination:
ACETONE
METHOD: 2021 , TESTIDCODE: 81552GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ACETONE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 90% 16% 97% 22%
>= Reporting Level 156 114% 23% 110% 18%
Total 159 114% 23% 109% 18%

Sample Statistics
ACETONE

Characteristic N % % Basis
Plotted 159 92% Spiked
Estimated Values 4 2% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 13 8% Spiked
Spiked 177 .  
False Negatives 0 0% 0 out of 172
Not Spiked 331 .  
False Positives 7 2% 7 out of 303

BQS OBSP Determination:
ACROLEIN
METHOD: 2021 , TESTIDCODE: 34210GCM66
Open Data Set

The SGPlot Procedure

Sample Statistics
ACROLEIN

Characteristic N % % Basis
Plotted 0 . Spiked
Estimated Values 0 . Spiked
Deleted Values 21 100% Spiked + Not Spiked
Spiked, Censored 0 . Spiked
Spiked 2 .  
False Negatives 0 . 0 out of 0
Not Spiked 19 .  
False Positives 0 . 0 out of 0

BQS OBSP Determination:
ACRYLONITRILE
METHOD: 2021 , TESTIDCODE: 34215GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ACRYLONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 15 111% 19% 116% 20%
>= Reporting Level 132 104% 13% 102% 9%
Total 147 105% 14% 103% 11%

Sample Statistics
ACRYLONITRILE

Characteristic N % % Basis
Plotted 147 91% Spiked
Estimated Values 17 10% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 15 9% Spiked
Spiked 167 .  
False Negatives 0 0% 0 out of 162
Not Spiked 341 .  
False Positives 0 0% 0 out of 313

BQS OBSP Determination:
BENZENE
METHOD: 2021 , TESTIDCODE: 34030GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 90% 29% 107% 38%
>= Reporting Level 245 101% 10% 102% 9%
Total 248 101% 11% 102% 9%

Sample Statistics
BENZENE

Characteristic N % % Basis
Plotted 248 100% Spiked
Estimated Values 75 30% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 276 .  
False Negatives 0 0% 0 out of 248
Not Spiked 232 .  
False Positives 6 3% 6 out of 227

BQS OBSP Determination:
BROMOBENZENE
METHOD: 2021 , TESTIDCODE: 81555GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BROMOBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 139 94% 11% 95% 10%
Total 139 94% 11% 95% 10%

Sample Statistics
BROMOBENZENE

Characteristic N % % Basis
Plotted 139 100% Spiked
Estimated Values 33 24% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 167 .  
False Negatives 0 0% 0 out of 139
Not Spiked 341 .  
False Positives 0 0% 0 out of 336

BQS OBSP Determination:
BROMOCHLOROMETHANE
METHOD: 2021 , TESTIDCODE: 77297GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BROMOCHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 130 105% 13% 105% 12%
Total 130 105% 13% 105% 12%

Sample Statistics
BROMOCHLOROMETHANE

Characteristic N % % Basis
Plotted 130 100% Spiked
Estimated Values 16 12% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 152 .  
False Negatives 0 0% 0 out of 130
Not Spiked 356 .  
False Positives 1 0% 1 out of 345

BQS OBSP Determination:
BROMODICHLOROMETHANE
METHOD: 2021 , TESTIDCODE: 32101GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BROMODICHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 94% 24% 105% 8%
>= Reporting Level 202 103% 15% 103% 14%
Total 207 103% 15% 103% 14%

Sample Statistics
BROMODICHLOROMETHANE

Characteristic N % % Basis
Plotted 207 100% Spiked
Estimated Values 28 14% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 234 .  
False Negatives 0 0% 0 out of 207
Not Spiked 274 .  
False Positives 0 0% 0 out of 268

BQS OBSP Determination:
BROMOETHENE
METHOD: 2021 , TESTIDCODE: 50002GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BROMOETHENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 103% 4% 103% 4%
>= Reporting Level 113 113% 19% 110% 13%
Total 117 113% 19% 109% 13%

Sample Statistics
BROMOETHENE

Characteristic N % % Basis
Plotted 117 99% Spiked
Estimated Values 7 6% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 123 .  
False Negatives 1 1% 1 out of 118
Not Spiked 385 .  
False Positives 0 0% 0 out of 357

BQS OBSP Determination:
BROMOFORM
METHOD: 2021 , TESTIDCODE: 32104GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BROMOFORM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 18 110% 37% 102% 19%
>= Reporting Level 185 104% 19% 101% 15%
Total 203 104% 21% 101% 15%

Sample Statistics
BROMOFORM

Characteristic N % % Basis
Plotted 203 97% Spiked
Estimated Values 33 16% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 2 1% Spiked
Spiked 237 .  
False Negatives 5 2% 5 out of 210
Not Spiked 271 .  
False Positives 1 0% 1 out of 265

BQS OBSP Determination:
BROMOMETHANE
METHOD: 2021 , TESTIDCODE: 34413GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BROMOMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 8 120% 26% 116% 32%
>= Reporting Level 127 114% 29% 115% 23%
Total 135 115% 29% 115% 23%

Sample Statistics
BROMOMETHANE

Characteristic N % % Basis
Plotted 135 92% Spiked
Estimated Values 135 92% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 12 8% Spiked
Spiked 169 .  
False Negatives 0 0% 0 out of 147
Not Spiked 339 .  
False Positives 14 4% 14 out of 328

BQS OBSP Determination:
BUTYLBENZENE
METHOD: 2021 , TESTIDCODE: 77342GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
BUTYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 17 88% 25% 87% 25%
>= Reporting Level 129 81% 15% 79% 14%
Total 146 82% 17% 79% 15%

Sample Statistics
BUTYLBENZENE

Characteristic N % % Basis
Plotted 146 100% Spiked
Estimated Values 21 14% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 174 .  
False Negatives 0 0% 0 out of 146
Not Spiked 334 .  
False Positives 1 0% 1 out of 329

BQS OBSP Determination:
CARBON DISULFIDE
METHOD: 2021 , TESTIDCODE: 77041GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CARBON DISULFIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 7 92% 26% 98% 20%
>= Reporting Level 150 104% 30% 100% 20%
Total 157 103% 30% 100% 20%

Sample Statistics
CARBON DISULFIDE

Characteristic N % % Basis
Plotted 157 100% Spiked
Estimated Values 58 37% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 168 .  
False Negatives 0 0% 0 out of 157
Not Spiked 333 .  
False Positives 13 4% 13 out of 311

BQS OBSP Determination:
CHLOROBENZENE
METHOD: 2021 , TESTIDCODE: 34301GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CHLOROBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 243 98% 11% 97% 9%
Total 243 98% 11% 97% 9%

Sample Statistics
CHLOROBENZENE

Characteristic N % % Basis
Plotted 243 100% Spiked
Estimated Values 74 30% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 276 .  
False Negatives 0 0% 0 out of 243
Not Spiked 232 .  
False Positives 0 0% 0 out of 232

BQS OBSP Determination:
CHLOROETHANE
METHOD: 2021 , TESTIDCODE: 34311GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 11 103% 22% 112% 15%
>= Reporting Level 160 113% 19% 111% 19%
Total 171 112% 19% 111% 19%

Sample Statistics
CHLOROETHANE

Characteristic N % % Basis
Plotted 171 98% Spiked
Estimated Values 14 8% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 3 2% Spiked
Spiked 196 .  
False Negatives 0 0% 0 out of 174
Not Spiked 312 .  
False Positives 1 0% 1 out of 301

BQS OBSP Determination:
CHLOROFORM
METHOD: 2021 , TESTIDCODE: 32106GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CHLOROFORM

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 98% 27% 107% 28%
>= Reporting Level 239 109% 13% 109% 12%
Total 243 109% 14% 109% 12%

Sample Statistics
CHLOROFORM

Characteristic N % % Basis
Plotted 243 100% Spiked
Estimated Values 59 24% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 276 .  
False Negatives 0 0% 0 out of 243
Not Spiked 226 .  
False Positives 2 1% 2 out of 226

BQS OBSP Determination:
CHLOROMETHANE
METHOD: 2021 , TESTIDCODE: 34418GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 16 112% 30% 109% 17%
>= Reporting Level 147 120% 21% 118% 20%
Total 163 119% 22% 118% 20%

Sample Statistics
CHLOROMETHANE

Characteristic N % % Basis
Plotted 163 98% Spiked
Estimated Values 163 98% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 4 2% Spiked
Spiked 189 .  
False Negatives 0 0% 0 out of 167
Not Spiked 319 .  
False Positives 6 2% 6 out of 308

BQS OBSP Determination:
CIS-1,2-DICHLOROETHYLENE
METHOD: 2021 , TESTIDCODE: 77093GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CIS-1,2-DICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 100% 30% 94% 44%
>= Reporting Level 173 100% 13% 100% 11%
Total 176 100% 14% 100% 11%

Sample Statistics
CIS-1,2-DICHLOROETHYLENE

Characteristic N % % Basis
Plotted 176 98% Spiked
Estimated Values 52 29% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 4 2% Spiked
Spiked 207 .  
False Negatives 0 0% 0 out of 180
Not Spiked 301 .  
False Positives 1 0% 1 out of 295

BQS OBSP Determination:
CIS-1,3-DICHLOROPROPENE
METHOD: 2021 , TESTIDCODE: 34704GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
CIS-1,3-DICHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 98% 29% 91% 36%
>= Reporting Level 128 92% 15% 90% 14%
Total 142 93% 17% 90% 14%

Sample Statistics
CIS-1,3-DICHLOROPROPENE

Characteristic N % % Basis
Plotted 142 100% Spiked
Estimated Values 17 12% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 164 .  
False Negatives 0 0% 0 out of 142
Not Spiked 344 .  
False Positives 1 0% 1 out of 333

BQS OBSP Determination:
DIBROMOCHLOROMETHANE
METHOD: 2021 , TESTIDCODE: 32105GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DIBROMOCHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 43 93% 15% 92% 15%
>= Reporting Level 177 101% 13% 101% 12%
Total 220 100% 14% 99% 12%

Sample Statistics
DIBROMOCHLOROMETHANE

Characteristic N % % Basis
Plotted 220 99% Spiked
Estimated Values 43 19% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 2 1% Spiked
Spiked 249 .  
False Negatives 0 0% 0 out of 222
Not Spiked 259 .  
False Positives 0 0% 0 out of 253

BQS OBSP Determination:
DIBROMOMETHANE
METHOD: 2021 , TESTIDCODE: 30217GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DIBROMOMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 108% 24% 112% 14%
>= Reporting Level 120 104% 14% 104% 11%
Total 129 104% 15% 104% 12%

Sample Statistics
DIBROMOMETHANE

Characteristic N % % Basis
Plotted 129 96% Spiked
Estimated Values 19 14% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 5 4% Spiked
Spiked 162 .  
False Negatives 0 0% 0 out of 134
Not Spiked 346 .  
False Positives 1 0% 1 out of 341

BQS OBSP Determination:
DICHLORODIFLUOROMETHANE
METHOD: 2021 , TESTIDCODE: 34668GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DICHLORODIFLUOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 17 128% 30% 126% 24%
>= Reporting Level 124 110% 30% 103% 28%
Total 141 112% 31% 108% 30%

Sample Statistics
DICHLORODIFLUOROMETHANE

Characteristic N % % Basis
Plotted 141 100% Spiked
Estimated Values 141 100% Spiked
Deleted Values 32 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 162 .  
False Negatives 0 0% 0 out of 141
Not Spiked 339 .  
False Positives 0 0% 0 out of 328

BQS OBSP Determination:
DICHLOROMETHANE
METHOD: 2021 , TESTIDCODE: 34423GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DICHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 27 138% 60% 119% 40%
>= Reporting Level 168 148% 113% 115% 24%
Total 195 146% 107% 116% 25%

Sample Statistics
DICHLOROMETHANE

Characteristic N % % Basis
Plotted 195 100% Spiked
Estimated Values 30 15% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 218 .  
False Negatives 0 0% 0 out of 195
Not Spiked 290 .  
False Positives 42 15% 42 out of 280

BQS OBSP Determination:
DIETHYL ETHER
METHOD: 2021 , TESTIDCODE: 81576GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DIETHYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 92% 15% 99% 16%
>= Reporting Level 110 108% 13% 108% 11%
Total 119 107% 14% 107% 11%

Sample Statistics
DIETHYL ETHER

Characteristic N % % Basis
Plotted 119 100% Spiked
Estimated Values 9 8% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 124 .  
False Negatives 0 0% 0 out of 119
Not Spiked 384 .  
False Positives 0 0% 0 out of 356

BQS OBSP Determination:
DIISOPROPYL ETHER
METHOD: 2021 , TESTIDCODE: 81577GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
DIISOPROPYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 101% 27% 114% 21%
>= Reporting Level 114 100% 14% 99% 12%
Total 119 100% 14% 99% 13%

Sample Statistics
DIISOPROPYL ETHER

Characteristic N % % Basis
Plotted 119 100% Spiked
Estimated Values 7 6% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 124 .  
False Negatives 0 0% 0 out of 119
Not Spiked 384 .  
False Positives 1 0% 1 out of 356

BQS OBSP Determination:
ETHYLBENZENE
METHOD: 2021 , TESTIDCODE: 34371GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ETHYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 248 93% 13% 93% 11%
Total 248 93% 13% 93% 11%

Sample Statistics
ETHYLBENZENE

Characteristic N % % Basis
Plotted 248 100% Spiked
Estimated Values 73 29% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 281 .  
False Negatives 0 0% 0 out of 248
Not Spiked 227 .  
False Positives 0 0% 0 out of 227

BQS OBSP Determination:
ETHYL METHACRYLATE
METHOD: 2021 , TESTIDCODE: 73570GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ETHYL METHACRYLATE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 68% 16% 70% 24%
>= Reporting Level 138 92% 12% 90% 10%
Total 141 91% 12% 90% 11%

Sample Statistics
ETHYL METHACRYLATE

Characteristic N % % Basis
Plotted 141 94% Spiked
Estimated Values 11 7% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 5 3% Spiked
Spiked 155 .  
False Negatives 4 3% 4 out of 150
Not Spiked 353 .  
False Positives 0 0% 0 out of 325

BQS OBSP Determination:
ETHYL TERT-BUTYL ETHER
METHOD: 2021 , TESTIDCODE: 50004GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ETHYL TERT-BUTYL ETHER

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 85% 23% 91% 17%
>= Reporting Level 121 97% 11% 96% 10%
Total 126 96% 11% 96% 10%

Sample Statistics
ETHYL TERT-BUTYL ETHER

Characteristic N % % Basis
Plotted 126 100% Spiked
Estimated Values 25 20% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 131 .  
False Negatives 0 0% 0 out of 126
Not Spiked 377 .  
False Positives 0 0% 0 out of 349

BQS OBSP Determination:
HEXACHLOROBUTADIENE
METHOD: 2021 , TESTIDCODE: 39702GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
HEXACHLOROBUTADIENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 13 101% 32% 103% 16%
>= Reporting Level 116 90% 11% 90% 11%
Total 129 92% 15% 90% 12%

Sample Statistics
HEXACHLOROBUTADIENE

Characteristic N % % Basis
Plotted 129 99% Spiked
Estimated Values 14 11% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 1 1% Spiked
Spiked 152 .  
False Negatives 0 0% 0 out of 130
Not Spiked 356 .  
False Positives 1 0% 1 out of 345

BQS OBSP Determination:
HEXACHLOROETHANE
METHOD: 2021 , TESTIDCODE: 34396GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
HEXACHLOROETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 10 97% 18% 96% 15%
>= Reporting Level 121 97% 16% 96% 15%
Total 131 97% 16% 96% 15%

Sample Statistics
HEXACHLOROETHANE

Characteristic N % % Basis
Plotted 131 96% Spiked
Estimated Values 13 10% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 5 4% Spiked
Spiked 141 .  
False Negatives 0 0% 0 out of 136
Not Spiked 367 .  
False Positives 0 0% 0 out of 339

BQS OBSP Determination:
ISOPROPYLBENZENE (CUMENE)
METHOD: 2021 , TESTIDCODE: 77223GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
ISOPROPYLBENZENE (CUMENE)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 100% 27% 102% 10%
>= Reporting Level 168 89% 16% 90% 15%
Total 173 89% 17% 91% 15%

Sample Statistics
ISOPROPYLBENZENE (CUMENE)

Characteristic N % % Basis
Plotted 173 99% Spiked
Estimated Values 57 33% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 2 1% Spiked
Spiked 202 .  
False Negatives 0 0% 0 out of 175
Not Spiked 306 .  
False Positives 0 0% 0 out of 300

BQS OBSP Determination:
M- AND P-XYLENE
METHOD: 2021 , TESTIDCODE: 85795GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
M- AND P-XYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 144 91% 14% 90% 15%
Total 144 91% 14% 90% 15%

Sample Statistics
M- AND P-XYLENE

Characteristic N % % Basis
Plotted 144 100% Spiked
Estimated Values 46 32% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 149 .  
False Negatives 0 0% 0 out of 144
Not Spiked 359 .  
False Positives 52 16% 52 out of 331

BQS OBSP Determination:
METHYL ACRYLATE
METHOD: 2021 , TESTIDCODE: 49991GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
METHYL ACRYLATE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 24 92% 10% 89% 8%
>= Reporting Level 113 95% 9% 95% 9%
Total 137 95% 9% 94% 9%

Sample Statistics
METHYL ACRYLATE

Characteristic N % % Basis
Plotted 137 81% Spiked
Estimated Values 11 6% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 33 19% Spiked
Spiked 192 .  
False Negatives 0 0% 0 out of 170
Not Spiked 310 .  
False Positives 0 0% 0 out of 299

BQS OBSP Determination:
METHYL ACRYLONITRILE
METHOD: 2021 , TESTIDCODE: 81593GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
METHYL ACRYLONITRILE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 11 93% 19% 100% 18%
>= Reporting Level 136 101% 10% 101% 9%
Total 147 100% 11% 100% 9%

Sample Statistics
METHYL ACRYLONITRILE

Characteristic N % % Basis
Plotted 147 93% Spiked
Estimated Values 12 8% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 11 7% Spiked
Spiked 163 .  
False Negatives 0 0% 0 out of 158
Not Spiked 345 .  
False Positives 0 0% 0 out of 317

BQS OBSP Determination:
METHYL IODIDE
METHOD: 2021 , TESTIDCODE: 77424GCM66
Open Data Set

 Analysis Date = 10/23/12 
 SpikeMix = Crescent 05BB048: 40 µl & Abs 051712: 40 µl 
 Pct Recovery = 100%  Analysis Date = 01/19/13 
 SpikeMix = Accu 212051193: 40 µl & Abs 051712: 40 µl 
 Pct Recovery = 103%  Analysis Date = 05/02/06 
 SpikeMix = NSI 080405-01VOC: 20 µl & Ultra CB-1578: 50 µl 
 Pct Recovery = 91%  Analysis Date = 01/27/06 
 SpikeMix = NSI 080405-01VOC: 20 µl & Supelco LB31918: 30 µl 
 Pct Recovery = 44%  Analysis Date = 04/07/06 
 SpikeMix = Accu B5070191: 30 µl & NSI 080405-01VOC: 20 µl 
 Pct Recovery = 114%  Analysis Date = 02/14/13 
 SpikeMix = Crescent 05BB048: 40 µl & ChemService 472200: 40 µl 
 Pct Recovery = 138%  Analysis Date = 08/14/10 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 127%  Analysis Date = 05/29/10 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 123%  Analysis Date = 03/11/10 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 104%  Analysis Date = 12/11/09 
 SpikeMix = NSI 090909-01VOC: 30 µl 
 Pct Recovery = 100%  Analysis Date = 09/08/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 140%  Analysis Date = 06/24/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 142%  Analysis Date = 04/02/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 123%  Analysis Date = 01/26/10 
 SpikeMix = Abs 090809: 30 µl 
 Pct Recovery = 117%  Analysis Date = 08/12/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 86%  Analysis Date = 07/14/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 99%  Analysis Date = 05/20/05 
 SpikeMix = Supelco LB22064: 15 µl 
 Pct Recovery = 97%  Analysis Date = 07/30/12 
 SpikeMix = Supelco LB92787: 20 µl & Abs 051712: 20 µl 
 Pct Recovery = 111%  Analysis Date = 06/12/12 
 SpikeMix = Abs 051712: 20 µl 
 Pct Recovery = 139%  Analysis Date = 08/28/12 
 SpikeMix = NSI 062112-01VOA: 20 µl & ChemService 472200: 20 µl 
 Pct Recovery = 96%  Analysis Date = 09/19/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 47%  Analysis Date = 07/27/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 105%  Analysis Date = 05/31/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 107%  Analysis Date = 04/03/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 84%  Analysis Date = 01/09/07 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 94%  Analysis Date = 10/14/06 
 SpikeMix = Restek A046581: 40 µl 
 Pct Recovery = 75%  Analysis Date = 05/24/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 86%  Analysis Date = 02/22/02 
 SpikeMix = NSI Q-3183: 20 µl 
 Pct Recovery = 86%  Analysis Date = 11/02/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 76%  Analysis Date = 09/20/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 54%  Analysis Date = 06/09/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 64%  Analysis Date = 03/14/01 
 SpikeMix = Ultra S0039: 8 µl 
 Pct Recovery = 116%  Analysis Date = 02/26/99 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 77%  Analysis Date = 11/20/98 
 SpikeMix = NSI Q-16750-50 101497: 25 µl 
 Pct Recovery = 77%  Analysis Date = 07/08/09 
 SpikeMix = Supelco LB60727: 40 µl 
 Pct Recovery = 104%  Analysis Date = 04/08/09 
 SpikeMix = Supelco LB60727: 40 µl 
 Pct Recovery = 112%  Analysis Date = 07/25/09 
 SpikeMix = ERA 0804-08-02VOC: 40 µl 
 Pct Recovery = 99%  Analysis Date = 02/06/09 
 SpikeMix = ERA 0804-08-02VOC: 40 µl 
 Pct Recovery = 83%  Analysis Date = 07/09/10 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 126%  Analysis Date = 04/21/10 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 115%  Analysis Date = 02/03/10 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 116%  Analysis Date = 10/24/09 
 SpikeMix = NSI 090909-01VOC: 10 µl 
 Pct Recovery = 127%  Analysis Date = 07/27/10 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 106%  Analysis Date = 05/11/10 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 108%  Analysis Date = 02/19/10 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 124%  Analysis Date = 11/14/09 
 SpikeMix = Abs 090809: 10 µl 
 Pct Recovery = 122%  Analysis Date = 02/24/12 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 110%  Analysis Date = 11/18/11 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 101%  Analysis Date = 05/28/11 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 111%  Analysis Date = 03/08/11 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 110%  Analysis Date = 11/16/10 
 SpikeMix = Restek A075493: 40 µl 
 Pct Recovery = 113%  Analysis Date = 11/21/12 
 SpikeMix = Abs 051712: 10 µl 
 Pct Recovery = 108%  Analysis Date = 08/13/06 
 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 53%  Analysis Date = 03/15/06 
 SpikeMix = Supelco LB31918: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 116%  Analysis Date = 05/17/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 97%  Analysis Date = 12/08/05 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 116%  Analysis Date = 02/14/06 
 SpikeMix = NSI 080405-01VOC: 5 µl & Ultra CB-1578: 10 µl 
 Pct Recovery = 98%  Analysis Date = 11/15/05 
 SpikeMix = NSI 080405-01VOC: 5 µl & Supelco LB31918: 5 µl 
 Pct Recovery = 86%  Analysis Date = 06/06/06 
 SpikeMix = Accu B5070191: 5 µl & NSI 080405-01VOC: 5 µl 
 Pct Recovery = 109%  Analysis Date = 05/03/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 116%  Analysis Date = 03/29/13 
 SpikeMix = Supelco LB92787: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 104%  Analysis Date = 12/09/12 
 SpikeMix = NSI 062112-01VOA: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 108%  Analysis Date = 10/11/12 
 SpikeMix = Crescent 05BB048: 10 µl & ChemService 472200: 10 µl 
 Pct Recovery = 131%  Analysis Date = 12/17/11 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 100%  Analysis Date = 08/10/11 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 115%  Analysis Date = 05/10/11 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 115%  Analysis Date = 12/03/10 
 SpikeMix = Crescent 06MM148: 40 µl 
 Pct Recovery = 107%  Analysis Date = 04/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 78%  Analysis Date = 01/04/02 
 SpikeMix = NSI Q-3183: 10 µl 
 Pct Recovery = 115%  Analysis Date = 08/25/05 
 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 63%  Analysis Date = 06/27/05 
 SpikeMix = Supelco LB22064: 5 µl & Ultra CA-1229: 10 µl 
 Pct Recovery = 130%  Analysis Date = 07/26/05 
 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 92%  Analysis Date = 03/09/05 
 SpikeMix = Supelco LB22064: 5 µl & NSI 081104-01VOC: 10 µl 
 Pct Recovery = 58%  Analysis Date = 12/31/13 
 SpikeMix = Abs 051413: 20 µl & Crescent 04CC151: 20 µl 
 Pct Recovery = 117%  Analysis Date = 08/06/13 
 SpikeMix = Supelco LC00154: 20 µl & Abs 051413: 20 µl 
 Pct Recovery = 100%  Analysis Date = 04/15/05 
 SpikeMix = Supelco LB22064: 5 µl 
 Pct Recovery = 83%  Analysis Date = 02/11/05 
 SpikeMix = Supelco LB22064: 5 µl 
 Pct Recovery = 111%  Analysis Date = 03/19/14 
 SpikeMix = ChemService 1530700: 20 µl & NSI 053013: 20 µl 
 Pct Recovery = 134%  Analysis Date = 08/22/13 
 SpikeMix = ChemService 1530700: 20 µl & NSI 053013: 20 µl 
 Pct Recovery = 128%  Analysis Date = 01/29/14 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 130%  Analysis Date = 09/17/13 
 SpikeMix = Supelco LC00154: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 114%  Analysis Date = 11/01/13 
 SpikeMix = Accu 213041120: 20 µl & ChemService 1530700: 20 µl 
 Pct Recovery = 114%  Analysis Date = 03/31/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 71%  Analysis Date = 01/20/99 
 SpikeMix = NSI Q-16750-50 101497: 10 µl 
 Pct Recovery = 67%  Analysis Date = 09/16/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 117%  Analysis Date = 06/03/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 142%  Analysis Date = 04/04/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 102%  Analysis Date = 08/12/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/22/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 117%  Analysis Date = 07/03/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 104%  Analysis Date = 07/01/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 119%  Analysis Date = 02/06/08 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 100%  Analysis Date = 10/11/07 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 117%  Analysis Date = 09/19/07 
 SpikeMix = Crescent 07GG012: 20 µl 
 Pct Recovery = 75%  Analysis Date = 04/06/12 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 93%  Analysis Date = 01/26/12 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 108%  Analysis Date = 09/03/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 97%  Analysis Date = 07/20/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 114%  Analysis Date = 04/21/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 102%  Analysis Date = 01/22/11 
 SpikeMix = Restek A075493: 20 µl 
 Pct Recovery = 101%  Analysis Date = 03/24/12 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 96%  Analysis Date = 02/24/12 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 107%  Analysis Date = 10/24/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 115%  Analysis Date = 06/18/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 97%  Analysis Date = 03/26/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 107%  Analysis Date = 02/14/11 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 106%  Analysis Date = 10/23/10 
 SpikeMix = Crescent 06MM148: 20 µl 
 Pct Recovery = 90%  Analysis Date = 09/27/13 
 SpikeMix = Abs 051413: 10 µl & NSI 053013: 10 µl 
 Pct Recovery = 119%  Analysis Date = 11/15/13 
 SpikeMix = Abs 051413: 10 µl & Crescent 04CC151: 10 µl 
 Pct Recovery = 131%  Analysis Date = 12/12/13 
 SpikeMix = Supelco LC00154: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 128%  Analysis Date = 03/19/14 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 132%  Analysis Date = 06/08/13 
 SpikeMix = Accu 213041120: 10 µl & Abs 051413: 10 µl 
 Pct Recovery = 113%  Analysis Date = 02/22/14 
 SpikeMix = ChemService 1530700: 10 µl & NSI 053013: 10 µl 
 Pct Recovery = 104%  Analysis Date = 06/29/13 
 SpikeMix = ChemService 1530700: 10 µl & Crescent 04CC151: 10 µl 
 Pct Recovery = 113%  Analysis Date = 12/31/13 
 SpikeMix = Accu 213041120: 10 µl & ChemService 1530700: 10 µl 
 Pct Recovery = 130%  Analysis Date = 05/09/02 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 42%  Analysis Date = 12/07/01 
 SpikeMix = Ultra S1214: 25 µl 
 Pct Recovery = 56%  Analysis Date = 09/19/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 78%  Analysis Date = 08/02/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 75%  Analysis Date = 07/06/00 
 SpikeMix = NSI 053100-01: 2 µl 
 Pct Recovery = 57%  Analysis Date = 09/26/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 117%  Analysis Date = 08/19/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 117%  Analysis Date = 05/16/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 109%  Analysis Date = 02/27/09 
 SpikeMix = Supelco LB60727: 20 µl 
 Pct Recovery = 114%  Analysis Date = 09/05/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 92%  Analysis Date = 06/17/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 86%  Analysis Date = 04/25/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 90%  Analysis Date = 03/14/09 
 SpikeMix = ERA 0804-08-02VOC: 20 µl 
 Pct Recovery = 86%  Analysis Date = 01/17/09 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 169%  Analysis Date = 12/16/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 98%  Analysis Date = 11/01/08 
 SpikeMix = Ultra CE-0471: 20 µl 
 Pct Recovery = 98%  Analysis Date = 09/17/06 
 SpikeMix = NSI 080405-01VOC: 2 µl 
 Pct Recovery = 116%  Analysis Date = 03/23/06 
 SpikeMix = NSI 080405-01VOC: 2 µl 
 Pct Recovery = 153%  Analysis Date = 02/02/02 
 SpikeMix = Ultra S1214: 10 µl 
 Pct Recovery = 25%  Analysis Date = 03/18/14 
 Pct Recovery = 119%  Analysis Date = 02/19/14 
 Pct Recovery = 118%  Analysis Date = 02/19/14 
 Pct Recovery = 118%  Analysis Date = 01/22/14 
 Pct Recovery = 118%  Analysis Date = 01/22/14 
 Pct Recovery = 118%  Analysis Date = 12/25/13 
 Pct Recovery = 118%  Analysis Date = 12/25/13 
 Pct Recovery = 118%  Analysis Date = 11/27/13 
 Pct Recovery = 118%  Analysis Date = 11/27/13 
 Pct Recovery = 118%  Analysis Date = 10/30/13 
 Pct Recovery = 117%  Analysis Date = 10/30/13 
 Pct Recovery = 117%  Analysis Date = 10/02/13 
 Pct Recovery = 117%  Analysis Date = 10/02/13 
 Pct Recovery = 117%  Analysis Date = 09/04/13 
 Pct Recovery = 117%  Analysis Date = 09/04/13 
 Pct Recovery = 117%  Analysis Date = 08/07/13 
 Pct Recovery = 117%  Analysis Date = 08/07/13 
 Pct Recovery = 117%  Analysis Date = 07/10/13 
 Pct Recovery = 116%  Analysis Date = 07/10/13 
 Pct Recovery = 116%  Analysis Date = 06/12/13 
 Pct Recovery = 116%  Analysis Date = 06/12/13 
 Pct Recovery = 116%  Analysis Date = 05/15/13 
 Pct Recovery = 116%  Analysis Date = 05/15/13 
 Pct Recovery = 116%  Analysis Date = 04/17/13 
 Pct Recovery = 116%  Analysis Date = 04/17/13 
 Pct Recovery = 116%  Analysis Date = 03/20/13 
 Pct Recovery = 115%  Analysis Date = 03/20/13 
 Pct Recovery = 115%  Analysis Date = 02/20/13 
 Pct Recovery = 115%  Analysis Date = 02/20/13 
 Pct Recovery = 115%  Analysis Date = 01/23/13 
 Pct Recovery = 115%  Analysis Date = 01/23/13 
 Pct Recovery = 115%  Analysis Date = 12/26/12 
 Pct Recovery = 115%  Analysis Date = 12/26/12 
 Pct Recovery = 115%  Analysis Date = 11/28/12 
 Pct Recovery = 115%  Analysis Date = 11/28/12 
 Pct Recovery = 115%  Analysis Date = 10/31/12 
 Pct Recovery = 114%  Analysis Date = 10/31/12 
 Pct Recovery = 114%  Analysis Date = 10/03/12 
 Pct Recovery = 114%  Analysis Date = 10/03/12 
 Pct Recovery = 114%  Analysis Date = 09/05/12 
 Pct Recovery = 114%  Analysis Date = 09/05/12 
 Pct Recovery = 114%  Analysis Date = 08/08/12 
 Pct Recovery = 114%  Analysis Date = 08/08/12 
 Pct Recovery = 114%  Analysis Date = 07/11/12 
 Pct Recovery = 114%  Analysis Date = 07/11/12 
 Pct Recovery = 114%  Analysis Date = 06/13/12 
 Pct Recovery = 113%  Analysis Date = 06/13/12 
 Pct Recovery = 113%  Analysis Date = 05/16/12 
 Pct Recovery = 113%  Analysis Date = 05/16/12 
 Pct Recovery = 113%  Analysis Date = 04/18/12 
 Pct Recovery = 113%  Analysis Date = 04/18/12 
 Pct Recovery = 113%  Analysis Date = 03/21/12 
 Pct Recovery = 113%  Analysis Date = 03/21/12 
 Pct Recovery = 113%  Analysis Date = 02/22/12 
 Pct Recovery = 113%  Analysis Date = 02/22/12 
 Pct Recovery = 113%  Analysis Date = 01/25/12 
 Pct Recovery = 112%  Analysis Date = 01/25/12 
 Pct Recovery = 112%  Analysis Date = 12/28/11 
 Pct Recovery = 112%  Analysis Date = 12/28/11 
 Pct Recovery = 112%  Analysis Date = 11/30/11 
 Pct Recovery = 112%  Analysis Date = 11/30/11 
 Pct Recovery = 112%  Analysis Date = 11/02/11 
 Pct Recovery = 112%  Analysis Date = 11/02/11 
 Pct Recovery = 112%  Analysis Date = 10/05/11 
 Pct Recovery = 112%  Analysis Date = 10/05/11 
 Pct Recovery = 112%  Analysis Date = 09/07/11 
 Pct Recovery = 111%  Analysis Date = 09/07/11 
 Pct Recovery = 111%  Analysis Date = 08/10/11 
 Pct Recovery = 111%  Analysis Date = 08/10/11 
 Pct Recovery = 111%  Analysis Date = 07/13/11 
 Pct Recovery = 111%  Analysis Date = 07/13/11 
 Pct Recovery = 111%  Analysis Date = 06/15/11 
 Pct Recovery = 111%  Analysis Date = 06/15/11 
 Pct Recovery = 111%  Analysis Date = 05/18/11 
 Pct Recovery = 111%  Analysis Date = 05/18/11 
 Pct Recovery = 111%  Analysis Date = 04/20/11 
 Pct Recovery = 111%  Analysis Date = 04/20/11 
 Pct Recovery = 111%  Analysis Date = 03/23/11 
 Pct Recovery = 111%  Analysis Date = 03/23/11 
 Pct Recovery = 111%  Analysis Date = 02/23/11 
 Pct Recovery = 111%  Analysis Date = 02/23/11 
 Pct Recovery = 111%  Analysis Date = 01/26/11 
 Pct Recovery = 111%  Analysis Date = 01/26/11 
 Pct Recovery = 111%  Analysis Date = 12/29/10 
 Pct Recovery = 111%  Analysis Date = 12/29/10 
 Pct Recovery = 111%  Analysis Date = 12/01/10 
 Pct Recovery = 111%  Analysis Date = 12/01/10 
 Pct Recovery = 111%  Analysis Date = 11/03/10 
 Pct Recovery = 111%  Analysis Date = 11/03/10 
 Pct Recovery = 111%  Analysis Date = 10/06/10 
 Pct Recovery = 111%  Analysis Date = 10/06/10 
 Pct Recovery = 111%  Analysis Date = 09/08/10 
 Pct Recovery = 111%  Analysis Date = 09/08/10 
 Pct Recovery = 111%  Analysis Date = 08/11/10 
 Pct Recovery = 111%  Analysis Date = 08/11/10 
 Pct Recovery = 111%  Analysis Date = 07/14/10 
 Pct Recovery = 111%  Analysis Date = 07/14/10 
 Pct Recovery = 111%  Analysis Date = 06/16/10 
 Pct Recovery = 110%  Analysis Date = 06/16/10 
 Pct Recovery = 110%  Analysis Date = 05/19/10 
 Pct Recovery = 110%  Analysis Date = 05/19/10 
 Pct Recovery = 110%  Analysis Date = 04/21/10 
 Pct Recovery = 110%  Analysis Date = 04/21/10 
 Pct Recovery = 110%  Analysis Date = 03/24/10 
 Pct Recovery = 110%  Analysis Date = 03/24/10 
 Pct Recovery = 110%  Analysis Date = 02/24/10 
 Pct Recovery = 110%  Analysis Date = 02/24/10 
 Pct Recovery = 110%  Analysis Date = 01/27/10 
 Pct Recovery = 110%  Analysis Date = 01/27/10 
 Pct Recovery = 110%  Analysis Date = 12/30/09 
 Pct Recovery = 110%  Analysis Date = 12/30/09 
 Pct Recovery = 110%  Analysis Date = 12/02/09 
 Pct Recovery = 110%  Analysis Date = 12/02/09 
 Pct Recovery = 110%  Analysis Date = 11/04/09 
 Pct Recovery = 110%  Analysis Date = 11/04/09 
 Pct Recovery = 110%  Analysis Date = 10/07/09 
 Pct Recovery = 110%  Analysis Date = 10/07/09 
 Pct Recovery = 110%  Analysis Date = 09/09/09 
 Pct Recovery = 109%  Analysis Date = 09/09/09 
 Pct Recovery = 109%  Analysis Date = 08/12/09 
 Pct Recovery = 109%  Analysis Date = 08/12/09 
 Pct Recovery = 109%  Analysis Date = 07/15/09 
 Pct Recovery = 109%  Analysis Date = 07/15/09 
 Pct Recovery = 109%  Analysis Date = 06/17/09 
 Pct Recovery = 109%  Analysis Date = 06/17/09 
 Pct Recovery = 109%  Analysis Date = 05/20/09 
 Pct Recovery = 108%  Analysis Date = 05/20/09 
 Pct Recovery = 108%  Analysis Date = 04/22/09 
 Pct Recovery = 108%  Analysis Date = 04/22/09 
 Pct Recovery = 108%  Analysis Date = 03/25/09 
 Pct Recovery = 108%  Analysis Date = 03/25/09 
 Pct Recovery = 108%  Analysis Date = 02/25/09 
 Pct Recovery = 107%  Analysis Date = 02/25/09 
 Pct Recovery = 107%  Analysis Date = 01/28/09 
 Pct Recovery = 107%  Analysis Date = 01/28/09 
 Pct Recovery = 107%  Analysis Date = 12/31/08 
 Pct Recovery = 107%  Analysis Date = 12/31/08 
 Pct Recovery = 107%  Analysis Date = 12/03/08 
 Pct Recovery = 106%  Analysis Date = 12/03/08 
 Pct Recovery = 106%  Analysis Date = 11/05/08 
 Pct Recovery = 106%  Analysis Date = 11/05/08 
 Pct Recovery = 106%  Analysis Date = 10/08/08 
 Pct Recovery = 106%  Analysis Date = 10/08/08 
 Pct Recovery = 106%  Analysis Date = 09/10/08 
 Pct Recovery = 105%  Analysis Date = 09/10/08 
 Pct Recovery = 105%  Analysis Date = 08/13/08 
 Pct Recovery = 105%  Analysis Date = 08/13/08 
 Pct Recovery = 105%  Analysis Date = 07/16/08 
 Pct Recovery = 105%  Analysis Date = 07/16/08 
 Pct Recovery = 105%  Analysis Date = 06/18/08 
 Pct Recovery = 104%  Analysis Date = 06/18/08 
 Pct Recovery = 104%  Analysis Date = 05/21/08 
 Pct Recovery = 104%  Analysis Date = 05/21/08 
 Pct Recovery = 104%  Analysis Date = 04/23/08 
 Pct Recovery = 104%  Analysis Date = 04/23/08 
 Pct Recovery = 104%  Analysis Date = 03/26/08 
 Pct Recovery = 103%  Analysis Date = 03/26/08 
 Pct Recovery = 103%  Analysis Date = 02/27/08 
 Pct Recovery = 103%  Analysis Date = 02/27/08 
 Pct Recovery = 103%  Analysis Date = 01/30/08 
 Pct Recovery = 103%  Analysis Date = 01/30/08 
 Pct Recovery = 103%  Analysis Date = 01/02/08 
 Pct Recovery = 102%  Analysis Date = 01/02/08 
 Pct Recovery = 102%  Analysis Date = 12/05/07 
 Pct Recovery = 102%  Analysis Date = 12/05/07 
 Pct Recovery = 102%  Analysis Date = 11/07/07 
 Pct Recovery = 102%  Analysis Date = 11/07/07 
 Pct Recovery = 102%  Analysis Date = 10/11/07 
 Pct Recovery = 102%  Analysis Date = 10/11/07 
 Pct Recovery = 102%  Analysis Date = 09/13/07 
 Pct Recovery = 101%  Analysis Date = 09/13/07 
 Pct Recovery = 101%  Analysis Date = 08/16/07 
 Pct Recovery = 101%  Analysis Date = 08/16/07 
 Pct Recovery = 101%  Analysis Date = 07/19/07 
 Pct Recovery = 101%  Analysis Date = 07/19/07 
 Pct Recovery = 101%  Analysis Date = 06/21/07 
 Pct Recovery = 100%  Analysis Date = 06/21/07 
 Pct Recovery = 100%  Analysis Date = 05/24/07 
 Pct Recovery = 100%  Analysis Date = 05/24/07 
 Pct Recovery = 100%  Analysis Date = 04/26/07 
 Pct Recovery = 100%  Analysis Date = 04/26/07 
 Pct Recovery = 100%  Analysis Date = 03/29/07 
 Pct Recovery = 99%  Analysis Date = 03/29/07 
 Pct Recovery = 99%  Analysis Date = 03/01/07 
 Pct Recovery = 99%  Analysis Date = 03/01/07 
 Pct Recovery = 99%  Analysis Date = 02/01/07 
 Pct Recovery = 99%  Analysis Date = 02/01/07 
 Pct Recovery = 99%  Analysis Date = 01/04/07 
 Pct Recovery = 98%  Analysis Date = 01/04/07 
 Pct Recovery = 98%  Analysis Date = 12/07/06 
 Pct Recovery = 98%  Analysis Date = 12/07/06 
 Pct Recovery = 98%  Analysis Date = 11/09/06 
 Pct Recovery = 98%  Analysis Date = 11/09/06 
 Pct Recovery = 98%  Analysis Date = 10/12/06 
 Pct Recovery = 97%  Analysis Date = 10/12/06 
 Pct Recovery = 97%  Analysis Date = 09/14/06 
 Pct Recovery = 97%  Analysis Date = 09/14/06 
 Pct Recovery = 97%  Analysis Date = 08/17/06 
 Pct Recovery = 97%  Analysis Date = 08/17/06 
 Pct Recovery = 97%  Analysis Date = 07/20/06 
 Pct Recovery = 96%  Analysis Date = 07/20/06 
 Pct Recovery = 96%  Analysis Date = 06/22/06 
 Pct Recovery = 96%  Analysis Date = 06/22/06 
 Pct Recovery = 96%  Analysis Date = 05/25/06 
 Pct Recovery = 96%  Analysis Date = 05/25/06 
 Pct Recovery = 96%  Analysis Date = 04/27/06 
 Pct Recovery = 95%  Analysis Date = 04/27/06 
 Pct Recovery = 95%  Analysis Date = 03/30/06 
 Pct Recovery = 95%  Analysis Date = 03/30/06 
 Pct Recovery = 95%  Analysis Date = 03/02/06 
 Pct Recovery = 94%  Analysis Date = 03/02/06 
 Pct Recovery = 94%  Analysis Date = 02/02/06 
 Pct Recovery = 94%  Analysis Date = 02/02/06 
 Pct Recovery = 94%  Analysis Date = 01/05/06 
 Pct Recovery = 94%  Analysis Date = 01/05/06 
 Pct Recovery = 94%  Analysis Date = 12/08/05 
 Pct Recovery = 93%  Analysis Date = 12/08/05 
 Pct Recovery = 93%  Analysis Date = 11/10/05 
 Pct Recovery = 93%  Analysis Date = 11/10/05 
 Pct Recovery = 93%  Analysis Date = 10/13/05 
 Pct Recovery = 92%  Analysis Date = 10/13/05 
 Pct Recovery = 92%  Analysis Date = 09/15/05 
 Pct Recovery = 92%  Analysis Date = 09/15/05 
 Pct Recovery = 92%  Analysis Date = 08/18/05 
 Pct Recovery = 91%  Analysis Date = 08/18/05 
 Pct Recovery = 91%  Analysis Date = 07/21/05 
 Pct Recovery = 91%  Analysis Date = 07/21/05 
 Pct Recovery = 91%  Analysis Date = 06/23/05 
 Pct Recovery = 91%  Analysis Date = 06/23/05 
 Pct Recovery = 91%  Analysis Date = 05/26/05 
 Pct Recovery = 90%  Analysis Date = 05/26/05 
 Pct Recovery = 90%  Analysis Date = 04/28/05 
 Pct Recovery = 90%  Analysis Date = 04/28/05 
 Pct Recovery = 90%  Analysis Date = 03/31/05 
 Pct Recovery = 90%  Analysis Date = 03/31/05 
 Pct Recovery = 90%  Analysis Date = 03/03/05 
 Pct Recovery = 89%  Analysis Date = 03/03/05 
 Pct Recovery = 89%  Analysis Date = 02/03/05 
 Pct Recovery = 89%  Analysis Date = 02/03/05 
 Pct Recovery = 89%  Analysis Date = 01/06/05 
 Pct Recovery = 89%  Analysis Date = 01/06/05 
 Pct Recovery = 89%  Analysis Date = 12/09/04 
 Pct Recovery = 89%  Analysis Date = 12/09/04 
 Pct Recovery = 89%  Analysis Date = 11/11/04 
 Pct Recovery = 88%  Analysis Date = 11/11/04 
 Pct Recovery = 88%  Analysis Date = 10/14/04 
 Pct Recovery = 88%  Analysis Date = 10/14/04 
 Pct Recovery = 88%  Analysis Date = 09/16/04 
 Pct Recovery = 88%  Analysis Date = 09/16/04 
 Pct Recovery = 88%  Analysis Date = 08/19/04 
 Pct Recovery = 87%  Analysis Date = 08/19/04 
 Pct Recovery = 87%  Analysis Date = 07/22/04 
 Pct Recovery = 87%  Analysis Date = 07/22/04 
 Pct Recovery = 87%  Analysis Date = 06/24/04 
 Pct Recovery = 87%  Analysis Date = 06/24/04 
 Pct Recovery = 87%  Analysis Date = 05/27/04 
 Pct Recovery = 86%  Analysis Date = 05/27/04 
 Pct Recovery = 86%  Analysis Date = 04/29/04 
 Pct Recovery = 86%  Analysis Date = 04/29/04 
 Pct Recovery = 86%  Analysis Date = 04/01/04 
 Pct Recovery = 86%  Analysis Date = 04/01/04 
 Pct Recovery = 86%  Analysis Date = 03/04/04 
 Pct Recovery = 86%  Analysis Date = 03/04/04 
 Pct Recovery = 86%  Analysis Date = 02/05/04 
 Pct Recovery = 85%  Analysis Date = 02/05/04 
 Pct Recovery = 85%  Analysis Date = 01/08/04 
 Pct Recovery = 85%  Analysis Date = 01/08/04 
 Pct Recovery = 85%  Analysis Date = 12/11/03 
 Pct Recovery = 85%  Analysis Date = 12/11/03 
 Pct Recovery = 85%  Analysis Date = 11/13/03 
 Pct Recovery = 84%  Analysis Date = 11/13/03 
 Pct Recovery = 84%  Analysis Date = 10/16/03 
 Pct Recovery = 84%  Analysis Date = 10/16/03 
 Pct Recovery = 84%  Analysis Date = 09/18/03 
 Pct Recovery = 84%  Analysis Date = 09/18/03 
 Pct Recovery = 84%  Analysis Date = 08/21/03 
 Pct Recovery = 83%  Analysis Date = 08/21/03 
 Pct Recovery = 83%  Analysis Date = 07/24/03 
 Pct Recovery = 83%  Analysis Date = 07/24/03 
 Pct Recovery = 83%  Analysis Date = 06/26/03 
 Pct Recovery = 83%  Analysis Date = 06/26/03 
 Pct Recovery = 83%  Analysis Date = 05/29/03 
 Pct Recovery = 83%  Analysis Date = 05/29/03 
 Pct Recovery = 83%  Analysis Date = 05/01/03 
 Pct Recovery = 82%  Analysis Date = 05/01/03 
 Pct Recovery = 82%  Analysis Date = 04/03/03 
 Pct Recovery = 82%  Analysis Date = 04/03/03 
 Pct Recovery = 82%  Analysis Date = 03/06/03 
 Pct Recovery = 82%  Analysis Date = 03/06/03 
 Pct Recovery = 82%  Analysis Date = 02/06/03 
 Pct Recovery = 81%  Analysis Date = 02/06/03 
 Pct Recovery = 81%  Analysis Date = 01/09/03 
 Pct Recovery = 81%  Analysis Date = 01/09/03 
 Pct Recovery = 81%  Analysis Date = 12/12/02 
 Pct Recovery = 81%  Analysis Date = 12/12/02 
 Pct Recovery = 81%  Analysis Date = 11/14/02 
 Pct Recovery = 80%  Analysis Date = 11/14/02 
 Pct Recovery = 80%  Analysis Date = 10/17/02 
 Pct Recovery = 80%  Analysis Date = 10/17/02 
 Pct Recovery = 80%  Analysis Date = 09/19/02 
 Pct Recovery = 80%  Analysis Date = 09/19/02 
 Pct Recovery = 80%  Analysis Date = 08/22/02 
 Pct Recovery = 80%  Analysis Date = 08/22/02 
 Pct Recovery = 80%  Analysis Date = 07/25/02 
 Pct Recovery = 79%  Analysis Date = 07/25/02 
 Pct Recovery = 79%  Analysis Date = 06/27/02 
 Pct Recovery = 79%  Analysis Date = 06/27/02 
 Pct Recovery = 79%  Analysis Date = 05/30/02 
 Pct Recovery = 79%  Analysis Date = 05/30/02 
 Pct Recovery = 79%  Analysis Date = 05/02/02 
 Pct Recovery = 78%  Analysis Date = 05/02/02 
 Pct Recovery = 78%  Analysis Date = 04/04/02 
 Pct Recovery = 78%  Analysis Date = 04/04/02 
 Pct Recovery = 78%  Analysis Date = 03/07/02 
 Pct Recovery = 78%  Analysis Date = 03/07/02 
 Pct Recovery = 78%  Analysis Date = 02/07/02 
 Pct Recovery = 78%  Analysis Date = 02/07/02 
 Pct Recovery = 78%  Analysis Date = 01/10/02 
 Pct Recovery = 77%  Analysis Date = 01/10/02 
 Pct Recovery = 77%  Analysis Date = 12/13/01 
 Pct Recovery = 77%  Analysis Date = 12/13/01 
 Pct Recovery = 77%  Analysis Date = 11/15/01 
 Pct Recovery = 77%  Analysis Date = 11/15/01 
 Pct Recovery = 77%  Analysis Date = 10/18/01 
 Pct Recovery = 76%  Analysis Date = 10/18/01 
 Pct Recovery = 76%  Analysis Date = 09/20/01 
 Pct Recovery = 76%  Analysis Date = 09/20/01 
 Pct Recovery = 76%  Analysis Date = 08/23/01 
 Pct Recovery = 76%  Analysis Date = 08/23/01 
 Pct Recovery = 76%  Analysis Date = 07/26/01 
 Pct Recovery = 76%  Analysis Date = 07/26/01 
 Pct Recovery = 76%  Analysis Date = 06/28/01 
 Pct Recovery = 75%  Analysis Date = 06/28/01 
 Pct Recovery = 75%  Analysis Date = 05/31/01 
 Pct Recovery = 75%  Analysis Date = 05/31/01 
 Pct Recovery = 75%  Analysis Date = 05/04/01 
 Pct Recovery = 75%  Analysis Date = 05/04/01 
 Pct Recovery = 75%  Analysis Date = 04/06/01 
 Pct Recovery = 74%  Analysis Date = 04/06/01 
 Pct Recovery = 74%  Analysis Date = 03/09/01 
 Pct Recovery = 74%  Analysis Date = 03/09/01 
 Pct Recovery = 74%  Analysis Date = 02/09/01 
 Pct Recovery = 74%  Analysis Date = 02/09/01 
 Pct Recovery = 74%  Analysis Date = 01/12/01 
 Pct Recovery = 74%  Analysis Date = 01/12/01 
 Pct Recovery = 74%  Analysis Date = 12/15/00 
 Pct Recovery = 73%  Analysis Date = 12/15/00 
 Pct Recovery = 73%  Analysis Date = 11/17/00 
 Pct Recovery = 73%  Analysis Date = 11/17/00 
 Pct Recovery = 73%  Analysis Date = 10/20/00 
 Pct Recovery = 73%  Analysis Date = 10/20/00 
 Pct Recovery = 73%  Analysis Date = 09/22/00 
 Pct Recovery = 72%  Analysis Date = 09/22/00 
 Pct Recovery = 72%  Analysis Date = 08/25/00 
 Pct Recovery = 72%  Analysis Date = 08/25/00 
 Pct Recovery = 72%  Analysis Date = 07/28/00 
 Pct Recovery = 72%  Analysis Date = 07/28/00 
 Pct Recovery = 72%  Analysis Date = 06/30/00 
 Pct Recovery = 72%  Analysis Date = 06/30/00 
 Pct Recovery = 72%  Analysis Date = 06/02/00 
 Pct Recovery = 71%  Analysis Date = 06/02/00 
 Pct Recovery = 71%  Analysis Date = 05/05/00 
 Pct Recovery = 71%  Analysis Date = 05/05/00 
 Pct Recovery = 71%  Analysis Date = 04/07/00 
 Pct Recovery = 71%  Analysis Date = 04/07/00 
 Pct Recovery = 71%  Analysis Date = 03/10/00 
 Pct Recovery = 70%  Analysis Date = 03/10/00 
 Pct Recovery = 70%  Analysis Date = 02/11/00 
 Pct Recovery = 70%  Analysis Date = 02/11/00 
 Pct Recovery = 70%  Analysis Date = 01/14/00 
 Pct Recovery = 70%  Analysis Date = 01/14/00 
 Pct Recovery = 70%  Analysis Date = 12/17/99 
 Pct Recovery = 70%  Analysis Date = 12/17/99 
 Pct Recovery = 70%  Analysis Date = 11/19/99 
 Pct Recovery = 69%  Analysis Date = 11/19/99 
 Pct Recovery = 69%  Analysis Date = 10/22/99 
 Pct Recovery = 69%  Analysis Date = 10/22/99 
 Pct Recovery = 69%  Analysis Date = 09/24/99 
 Pct Recovery = 69%  Analysis Date = 09/24/99 
 Pct Recovery = 69%  Analysis Date = 08/27/99 
 Pct Recovery = 68%  Analysis Date = 08/27/99 
 Pct Recovery = 68%  Analysis Date = 07/30/99 
 Pct Recovery = 68%  Analysis Date = 07/30/99 
 Pct Recovery = 68%  Analysis Date = 07/02/99 
 Pct Recovery = 68%  Analysis Date = 07/02/99 
 Pct Recovery = 68%  Analysis Date = 06/04/99 
 Pct Recovery = 68%  Analysis Date = 06/04/99 
 Pct Recovery = 68%  Analysis Date = 05/07/99 
 Pct Recovery = 67%  Analysis Date = 05/07/99 
 Pct Recovery = 67%  Analysis Date = 04/09/99 
 Pct Recovery = 67%  Analysis Date = 04/09/99 
 Pct Recovery = 67%  Analysis Date = 03/12/99 
 Pct Recovery = 67%  Analysis Date = 03/12/99 
 Pct Recovery = 67%  Analysis Date = 02/12/99 
 Pct Recovery = 67%  Analysis Date = 02/12/99 
 Pct Recovery = 67%  Analysis Date = 01/15/99 
 Pct Recovery = 66%  Analysis Date = 01/15/99 
 Pct Recovery = 66%  Analysis Date = 12/18/98 
 Pct Recovery = 66%  Analysis Date = 12/18/98 
 Pct Recovery = 66%  Analysis Date = 11/20/98 
 Pct Recovery = 66%  Y = 1.5  Y = 0.5  Y = 1
The SGPlot Procedure

Plotted Points Statistics
METHYL IODIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 105% 33% 103% 20%
>= Reporting Level 120 103% 22% 106% 17%
Total 134 103% 23% 106% 18%

Sample Statistics
METHYL IODIDE

Characteristic N % % Basis
Plotted 134 96% Spiked
Estimated Values 134 96% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 4 3% Spiked
Spiked 156 .  
False Negatives 2 1% 2 out of 140
Not Spiked 341 .  
False Positives 19 6% 19 out of 324

BQS OBSP Determination:
METHYL METHACRYLATE
METHOD: 2021 , TESTIDCODE: 81597GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
METHYL METHACRYLATE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 97% 8% 98% 9%
>= Reporting Level 125 94% 13% 93% 10%
Total 130 94% 13% 94% 11%

Sample Statistics
METHYL METHACRYLATE

Characteristic N % % Basis
Plotted 130 90% Spiked
Estimated Values 12 8% Spiked
Deleted Values 33 7% Spiked + Not Spiked
Spiked, Censored 13 9% Spiked
Spiked 149 .  
False Negatives 1 1% 1 out of 144
Not Spiked 353 .  
False Positives 0 0% 0 out of 325

BQS OBSP Determination:
N-PROPYLBENZENE
METHOD: 2021 , TESTIDCODE: 77224GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
N-PROPYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 4 84% 15% 83% 19%
>= Reporting Level 177 89% 14% 88% 12%
Total 181 89% 14% 88% 12%

Sample Statistics
N-PROPYLBENZENE

Characteristic N % % Basis
Plotted 181 100% Spiked
Estimated Values 40 22% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 209 .  
False Negatives 0 0% 0 out of 181
Not Spiked 299 .  
False Positives 0 0% 0 out of 294

BQS OBSP Determination:
NAPHTHALENE
METHOD: 2021 , TESTIDCODE: 34696GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
NAPHTHALENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 24 83% 24% 87% 21%
>= Reporting Level 171 81% 14% 79% 13%
Total 195 81% 15% 79% 14%

Sample Statistics
NAPHTHALENE

Characteristic N % % Basis
Plotted 195 86% Spiked
Estimated Values 36 16% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 28 12% Spiked
Spiked 260 .  
False Negatives 4 2% 4 out of 227
Not Spiked 248 .  
False Positives 0 0% 0 out of 248

BQS OBSP Determination:
O-ETHYL TOLUENE
METHOD: 2021 , TESTIDCODE: 77220GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
O-ETHYL TOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 44% . 44% 0%
>= Reporting Level 125 88% 13% 87% 13%
Total 126 87% 13% 87% 13%

Sample Statistics
O-ETHYL TOLUENE

Characteristic N % % Basis
Plotted 126 100% Spiked
Estimated Values 27 21% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 131 .  
False Negatives 0 0% 0 out of 126
Not Spiked 377 .  
False Positives 0 0% 0 out of 349

BQS OBSP Determination:
O-XYLENE
METHOD: 2021 , TESTIDCODE: 77135GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
O-XYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 49% . 49% 0%
>= Reporting Level 245 93% 15% 93% 14%
Total 246 92% 15% 93% 14%

Sample Statistics
O-XYLENE

Characteristic N % % Basis
Plotted 246 99% Spiked
Estimated Values 74 30% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 1 0% Spiked
Spiked 276 .  
False Negatives 2 1% 2 out of 249
Not Spiked 232 .  
False Positives 0 0% 0 out of 226

BQS OBSP Determination:
SEC-BUTYLBENZENE
METHOD: 2021 , TESTIDCODE: 77350GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
SEC-BUTYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 1 41% . 41% 0%
>= Reporting Level 133 86% 12% 86% 10%
Total 134 86% 12% 86% 10%

Sample Statistics
SEC-BUTYLBENZENE

Characteristic N % % Basis
Plotted 134 100% Spiked
Estimated Values 37 28% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 156 .  
False Negatives 0 0% 0 out of 134
Not Spiked 352 .  
False Positives 0 0% 0 out of 341

BQS OBSP Determination:
STYRENE
METHOD: 2021 , TESTIDCODE: 77128GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
STYRENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 99% 23% 101% 20%
>= Reporting Level 193 89% 16% 88% 17%
Total 202 89% 17% 88% 18%

Sample Statistics
STYRENE

Characteristic N % % Basis
Plotted 202 100% Spiked
Estimated Values 47 23% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 235 .  
False Negatives 0 0% 0 out of 202
Not Spiked 273 .  
False Positives 3 1% 3 out of 273

BQS OBSP Determination:
TERT-BUTYLBENZENE
METHOD: 2021 , TESTIDCODE: 77353GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYLBENZENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 81% 28% 80% 9%
>= Reporting Level 126 87% 17% 85% 19%
Total 131 87% 17% 83% 19%

Sample Statistics
TERT-BUTYLBENZENE

Characteristic N % % Basis
Plotted 131 98% Spiked
Estimated Values 32 24% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 155 .  
False Negatives 2 2% 2 out of 133
Not Spiked 353 .  
False Positives 1 0% 1 out of 342

BQS OBSP Determination:
TERT-BUTYL METHYL ETHER (MTBE)
METHOD: 2021 , TESTIDCODE: 78032GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 112% 29% 108% 21%
>= Reporting Level 134 102% 12% 100% 10%
Total 148 103% 15% 100% 11%

Sample Statistics
TERT-BUTYL METHYL ETHER (MTBE)

Characteristic N % % Basis
Plotted 148 97% Spiked
Estimated Values 13 9% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 4 3% Spiked
Spiked 174 .  
False Negatives 0 0% 0 out of 152
Not Spiked 334 .  
False Positives 0 0% 0 out of 323

BQS OBSP Determination:
TERT-PENTYL METHYL ETHER (TAME)
METHOD: 2021 , TESTIDCODE: 50005GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TERT-PENTYL METHYL ETHER (TAME)

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 82% 19% 88% 12%
>= Reporting Level 112 93% 12% 93% 12%
Total 117 92% 12% 92% 13%

Sample Statistics
TERT-PENTYL METHYL ETHER (TAME)

Characteristic N % % Basis
Plotted 117 100% Spiked
Estimated Values 9 8% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 122 .  
False Negatives 0 0% 0 out of 117
Not Spiked 386 .  
False Positives 5 1% 5 out of 358

BQS OBSP Determination:
TETRACHLOROETHYLENE
METHOD: 2021 , TESTIDCODE: 34475GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TETRACHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 35 96% 15% 99% 11%
>= Reporting Level 208 99% 15% 99% 13%
Total 243 99% 15% 99% 13%

Sample Statistics
TETRACHLOROETHYLENE

Characteristic N % % Basis
Plotted 243 100% Spiked
Estimated Values 76 31% Spiked
Deleted Values 32 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 275 .  
False Negatives 0 0% 0 out of 243
Not Spiked 232 .  
False Positives 33 14% 33 out of 232

BQS OBSP Determination:
TETRACHLOROMETHANE
METHOD: 2021 , TESTIDCODE: 32102GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TETRACHLOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 86% 35% 96% 50%
>= Reporting Level 237 99% 19% 100% 15%
Total 240 99% 19% 100% 15%

Sample Statistics
TETRACHLOROMETHANE

Characteristic N % % Basis
Plotted 240 99% Spiked
Estimated Values 45 19% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 275 .  
False Negatives 2 1% 2 out of 242
Not Spiked 233 .  
False Positives 1 0% 1 out of 233

BQS OBSP Determination:
TETRAHYDROFURAN
METHOD: 2021 , TESTIDCODE: 81607GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TETRAHYDROFURAN

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 23 122% 40% 109% 27%
>= Reporting Level 128 97% 10% 98% 10%
Total 151 101% 20% 99% 10%

Sample Statistics
TETRAHYDROFURAN

Characteristic N % % Basis
Plotted 151 86% Spiked
Estimated Values 26 15% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 25 14% Spiked
Spiked 198 .  
False Negatives 0 0% 0 out of 176
Not Spiked 310 .  
False Positives 0 0% 0 out of 299

BQS OBSP Determination:
TOLUENE
METHOD: 2021 , TESTIDCODE: 34010GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TOLUENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 95% 23% 107% 6%
>= Reporting Level 249 102% 12% 100% 9%
Total 254 102% 12% 100% 10%

Sample Statistics
TOLUENE

Characteristic N % % Basis
Plotted 254 100% Spiked
Estimated Values 56 22% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 287 .  
False Negatives 0 0% 0 out of 254
Not Spiked 221 .  
False Positives 17 8% 17 out of 221

BQS OBSP Determination:
TRANS-1,2-DICHLOROETHYLENE
METHOD: 2021 , TESTIDCODE: 34546GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRANS-1,2-DICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 3 100% 7% 99% 11%
>= Reporting Level 173 102% 17% 104% 11%
Total 176 102% 16% 104% 11%

Sample Statistics
TRANS-1,2-DICHLOROETHYLENE

Characteristic N % % Basis
Plotted 176 98% Spiked
Estimated Values 59 33% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 4 2% Spiked
Spiked 207 .  
False Negatives 0 0% 0 out of 180
Not Spiked 301 .  
False Positives 8 3% 8 out of 295

BQS OBSP Determination:
TRANS-1,3-DICHLOROPROPENE
METHOD: 2021 , TESTIDCODE: 34699GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRANS-1,3-DICHLOROPROPENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 5 76% 31% 77% 33%
>= Reporting Level 137 92% 14% 91% 11%
Total 142 92% 15% 91% 12%

Sample Statistics
TRANS-1,3-DICHLOROPROPENE

Characteristic N % % Basis
Plotted 142 96% Spiked
Estimated Values 11 7% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 5 3% Spiked
Spiked 170 .  
False Negatives 1 1% 1 out of 148
Not Spiked 338 .  
False Positives 0 0% 0 out of 327

BQS OBSP Determination:
TRANS-1,4-DICHLORO-2-BUTENE
METHOD: 2021 , TESTIDCODE: 73547GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRANS-1,4-DICHLORO-2-BUTENE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 19 97% 24% 89% 30%
>= Reporting Level 133 90% 18% 88% 18%
Total 152 91% 19% 88% 18%

Sample Statistics
TRANS-1,4-DICHLORO-2-BUTENE

Characteristic N % % Basis
Plotted 152 94% Spiked
Estimated Values 80 49% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 10 6% Spiked
Spiked 167 .  
False Negatives 0 0% 0 out of 162
Not Spiked 341 .  
False Positives 0 0% 0 out of 313

BQS OBSP Determination:
TRICHLOROETHYLENE
METHOD: 2021 , TESTIDCODE: 39180GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRICHLOROETHYLENE

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 224 103% 12% 103% 9%
Total 224 103% 12% 103% 9%

Sample Statistics
TRICHLOROETHYLENE

Characteristic N % % Basis
Plotted 224 100% Spiked
Estimated Values 42 19% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 251 .  
False Negatives 0 0% 0 out of 224
Not Spiked 257 .  
False Positives 9 4% 9 out of 251

BQS OBSP Determination:
TRICHLOROFLUOROMETHANE
METHOD: 2021 , TESTIDCODE: 34488GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
TRICHLOROFLUOROMETHANE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 14 98% 26% 100% 24%
>= Reporting Level 161 114% 18% 113% 17%
Total 175 113% 20% 111% 19%

Sample Statistics
TRICHLOROFLUOROMETHANE

Characteristic N % % Basis
Plotted 175 100% Spiked
Estimated Values 16 9% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 197 .  
False Negatives 0 0% 0 out of 175
Not Spiked 311 .  
False Positives 1 0% 1 out of 300

BQS OBSP Determination:
VINYL CHLORIDE
METHOD: 2021 , TESTIDCODE: 39175GCM66
Open Data Set

The SGPlot Procedure

Plotted Points Statistics
VINYL CHLORIDE

Spike Level N Mean Std-Dev. Median F_Pseudo
< Reporting Level 9 109% 11% 109% 13%
>= Reporting Level 127 109% 25% 106% 25%
Total 136 109% 24% 107% 23%

Sample Statistics
VINYL CHLORIDE

Characteristic N % % Basis
Plotted 136 96% Spiked
Estimated Values 12 9% Spiked
Deleted Values 33 6% Spiked + Not Spiked
Spiked, Censored 5 4% Spiked
Spiked 163 .  
False Negatives 0 0% 0 out of 141
Not Spiked 345 .  
False Positives 2 1% 2 out of 334