OBSP Determination:
BROMOFORM
METHOD: 4440 , TESTIDCODE: 32104GCM66

Analysis Date = 01/26/17 SpikeMix = ChemService 5082900: 40 µl & Accu 216041125: 40 µl Pct Recovery = 89% Analysis Date = 12/16/16 SpikeMix = NSI 041816AVOC: 40 µl & ChemService 5082900: 40 µl Pct Recovery = 91% Analysis Date = 03/16/17 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 69% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 87% Analysis Date = 08/04/16 SpikeMix = Crescent 03FF058: 40 µl & Supelco LC20141V: 40 µl Pct Recovery = 87% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 07/20/16 SpikeMix = Supelco LC20141V: 40 µl & Accu 216041125: 40 µl Pct Recovery = 91% Analysis Date = 06/17/17 SpikeMix = Phenova B20160319: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 90% Analysis Date = 06/09/17 SpikeMix = Phenova B20160319: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 81% Analysis Date = 09/29/16 SpikeMix = ChemService 5082900: 25 µl & Accu 216041125: 25 µl Pct Recovery = 91% Analysis Date = 09/29/16 SpikeMix = ChemService 5082900: 25 µl & Accu 216041125: 25 µl Pct Recovery = 91% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 98% Analysis Date = 08/26/16 SpikeMix = NSI 041816AVOC: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 98% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 08/12/16 SpikeMix = ChemService 5082900: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 90% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = Crescent 03FF058: 25 µl & ChemService 5082900: 25 µl Pct Recovery = 100% Analysis Date = 04/21/17 SpikeMix = NSI 041816AVOC: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 87% Analysis Date = 02/24/17 SpikeMix = Supelco LC20141V: 25 µl & Phenova B20160319: 25 µl Pct Recovery = 63% Analysis Date = 11/21/16 SpikeMix = Crescent 03FF058: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 84% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 99% Analysis Date = 09/08/16 SpikeMix = Supelco LC20141V: 25 µl & Accu 216041125: 25 µl Pct Recovery = 99% Analysis Date = 07/20/16 SpikeMix = NSI 041816AVOC: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 101% Analysis Date = 07/20/16 SpikeMix = NSI 041816AVOC: 25 µl & Supelco LC20141V: 25 µl Pct Recovery = 101% Analysis Date = 01/13/17 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 87% Analysis Date = 11/29/16 SpikeMix = ChemService 5082900: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 83% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 97% Analysis Date = 09/28/16 SpikeMix = Crescent 03FF058: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 97% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 100% Analysis Date = 06/30/16 SpikeMix = ChemService 5082900: 15 µl & Accu 216041125: 15 µl Pct Recovery = 100% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 95% Analysis Date = 06/15/16 SpikeMix = NSI 041816AVOC: 15 µl & ChemService 5082900: 15 µl Pct Recovery = 95% Analysis Date = 07/14/17 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 92% Analysis Date = 06/02/17 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 100% Analysis Date = 02/09/17 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 92% Analysis Date = 12/24/16 SpikeMix = Supelco LC20141V: 15 µl & Accu 216041125: 15 µl Pct Recovery = 80% Analysis Date = 10/29/16 SpikeMix = Supelco LC20141V: 15 µl & Phenova B20160319: 15 µl Pct Recovery = 100% Analysis Date = 10/13/16 SpikeMix = NSI 041816AVOC: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 92% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 91% Analysis Date = 05/27/16 SpikeMix = Phenova B20160319: 15 µl & Supelco LC20141V: 15 µl Pct Recovery = 91% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 04/26/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 107% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 107% Analysis Date = 03/04/16 SpikeMix = Accu 215041380: 15 µl & ERA 0406-15-03: 15 µl Pct Recovery = 107% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 02/05/16 SpikeMix = ERA 0406-15-03: 15 µl & Spex Organics EN150428007: 15 µl Pct Recovery = 81% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 123% Analysis Date = 03/17/16 SpikeMix = NSI 050515AVOC: 10 µl & Supelco LC13545: 10 µl Pct Recovery = 123% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 101% Analysis Date = 01/27/16 SpikeMix = Crescent 04EE008: 10 µl & NSI 050515AVOC: 10 µl Pct Recovery = 101% Analysis Date = 07/13/17 Pct Recovery = 87% Analysis Date = 07/11/17 Pct Recovery = 87% Analysis Date = 07/11/17 Pct Recovery = 87% Analysis Date = 07/08/17 Pct Recovery = 87% Analysis Date = 07/08/17 Pct Recovery = 87% Analysis Date = 07/05/17 Pct Recovery = 87% Analysis Date = 07/05/17 Pct Recovery = 87% Analysis Date = 07/03/17 Pct Recovery = 87% Analysis Date = 07/03/17 Pct Recovery = 87% Analysis Date = 06/30/17 Pct Recovery = 87% Analysis Date = 06/30/17 Pct Recovery = 87% Analysis Date = 06/27/17 Pct Recovery = 87% Analysis Date = 06/27/17 Pct Recovery = 87% Analysis Date = 06/25/17 Pct Recovery = 87% Analysis Date = 06/25/17 Pct Recovery = 87% Analysis Date = 06/22/17 Pct Recovery = 87% Analysis Date = 06/22/17 Pct Recovery = 87% Analysis Date = 06/19/17 Pct Recovery = 87% Analysis Date = 06/19/17 Pct Recovery = 87% Analysis Date = 06/17/17 Pct Recovery = 87% Analysis Date = 06/17/17 Pct Recovery = 87% Analysis Date = 06/14/17 Pct Recovery = 87% Analysis Date = 06/14/17 Pct Recovery = 87% Analysis Date = 06/11/17 Pct Recovery = 87% Analysis Date = 06/11/17 Pct Recovery = 87% Analysis Date = 06/09/17 Pct Recovery = 87% Analysis Date = 06/09/17 Pct Recovery = 87% Analysis Date = 06/06/17 Pct Recovery = 87% Analysis Date = 06/06/17 Pct Recovery = 87% Analysis Date = 06/03/17 Pct Recovery = 87% Analysis Date = 06/03/17 Pct Recovery = 87% Analysis Date = 06/01/17 Pct Recovery = 87% Analysis Date = 06/01/17 Pct Recovery = 87% Analysis Date = 05/29/17 Pct Recovery = 87% Analysis Date = 05/29/17 Pct Recovery = 87% Analysis Date = 05/26/17 Pct Recovery = 87% Analysis Date = 05/26/17 Pct Recovery = 87% Analysis Date = 05/24/17 Pct Recovery = 87% Analysis Date = 05/24/17 Pct Recovery = 87% Analysis Date = 05/21/17 Pct Recovery = 87% Analysis Date = 05/21/17 Pct Recovery = 87% Analysis Date = 05/18/17 Pct Recovery = 87% Analysis Date = 05/18/17 Pct Recovery = 87% Analysis Date = 05/16/17 Pct Recovery = 87% Analysis Date = 05/16/17 Pct Recovery = 87% Analysis Date = 05/13/17 Pct Recovery = 86% Analysis Date = 05/13/17 Pct Recovery = 86% Analysis Date = 05/10/17 Pct Recovery = 86% Analysis Date = 05/10/17 Pct Recovery = 86% Analysis Date = 05/08/17 Pct Recovery = 86% Analysis Date = 05/08/17 Pct Recovery = 86% Analysis Date = 05/05/17 Pct Recovery = 86% Analysis Date = 05/05/17 Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 86% Analysis Date = 05/02/17 Pct Recovery = 86% Analysis Date = 04/30/17 Pct Recovery = 86% Analysis Date = 04/30/17 Pct Recovery = 86% Analysis Date = 04/27/17 Pct Recovery = 86% Analysis Date = 04/27/17 Pct Recovery = 86% Analysis Date = 04/24/17 Pct Recovery = 86% Analysis Date = 04/24/17 Pct Recovery = 86% Analysis Date = 04/22/17 Pct Recovery = 86% Analysis Date = 04/22/17 Pct Recovery = 86% Analysis Date = 04/19/17 Pct Recovery = 86% Analysis Date = 04/19/17 Pct Recovery = 86% Analysis Date = 04/16/17 Pct Recovery = 86% Analysis Date = 04/16/17 Pct Recovery = 86% Analysis Date = 04/14/17 Pct Recovery = 86% Analysis Date = 04/14/17 Pct Recovery = 86% Analysis Date = 04/11/17 Pct Recovery = 86% Analysis Date = 04/11/17 Pct Recovery = 86% Analysis Date = 04/08/17 Pct Recovery = 86% Analysis Date = 04/08/17 Pct Recovery = 86% Analysis Date = 04/06/17 Pct Recovery = 86% Analysis Date = 04/06/17 Pct Recovery = 86% Analysis Date = 04/03/17 Pct Recovery = 86% Analysis Date = 04/03/17 Pct Recovery = 86% Analysis Date = 03/31/17 Pct Recovery = 86% Analysis Date = 03/31/17 Pct Recovery = 86% Analysis Date = 03/29/17 Pct Recovery = 86% Analysis Date = 03/29/17 Pct Recovery = 86% Analysis Date = 03/26/17 Pct Recovery = 86% Analysis Date = 03/26/17 Pct Recovery = 86% Analysis Date = 03/23/17 Pct Recovery = 86% Analysis Date = 03/23/17 Pct Recovery = 86% Analysis Date = 03/21/17 Pct Recovery = 86% Analysis Date = 03/21/17 Pct Recovery = 86% Analysis Date = 03/18/17 Pct Recovery = 86% Analysis Date = 03/18/17 Pct Recovery = 86% Analysis Date = 03/15/17 Pct Recovery = 86% Analysis Date = 03/15/17 Pct Recovery = 86% Analysis Date = 03/13/17 Pct Recovery = 86% Analysis Date = 03/13/17 Pct Recovery = 86% Analysis Date = 03/10/17 Pct Recovery = 86% Analysis Date = 03/10/17 Pct Recovery = 86% Analysis Date = 03/07/17 Pct Recovery = 86% Analysis Date = 03/07/17 Pct Recovery = 86% Analysis Date = 03/05/17 Pct Recovery = 86% Analysis Date = 03/05/17 Pct Recovery = 86% Analysis Date = 03/02/17 Pct Recovery = 86% Analysis Date = 03/02/17 Pct Recovery = 86% Analysis Date = 02/27/17 Pct Recovery = 86% Analysis Date = 02/27/17 Pct Recovery = 86% Analysis Date = 02/25/17 Pct Recovery = 86% Analysis Date = 02/25/17 Pct Recovery = 86% Analysis Date = 02/22/17 Pct Recovery = 86% Analysis Date = 02/22/17 Pct Recovery = 86% Analysis Date = 02/19/17 Pct Recovery = 86% Analysis Date = 02/19/17 Pct Recovery = 86% Analysis Date = 02/17/17 Pct Recovery = 86% Analysis Date = 02/17/17 Pct Recovery = 86% Analysis Date = 02/14/17 Pct Recovery = 86% Analysis Date = 02/14/17 Pct Recovery = 86% Analysis Date = 02/11/17 Pct Recovery = 86% Analysis Date = 02/11/17 Pct Recovery = 86% Analysis Date = 02/09/17 Pct Recovery = 86% Analysis Date = 02/09/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/06/17 Pct Recovery = 86% Analysis Date = 02/03/17 Pct Recovery = 86% Analysis Date = 02/03/17 Pct Recovery = 86% Analysis Date = 02/01/17 Pct Recovery = 86% Analysis Date = 02/01/17 Pct Recovery = 86% Analysis Date = 01/29/17 Pct Recovery = 87% Analysis Date = 01/29/17 Pct Recovery = 87% Analysis Date = 01/26/17 Pct Recovery = 87% Analysis Date = 01/26/17 Pct Recovery = 87% Analysis Date = 01/24/17 Pct Recovery = 87% Analysis Date = 01/24/17 Pct Recovery = 87% Analysis Date = 01/21/17 Pct Recovery = 87% Analysis Date = 01/21/17 Pct Recovery = 87% Analysis Date = 01/18/17 Pct Recovery = 87% Analysis Date = 01/18/17 Pct Recovery = 87% Analysis Date = 01/16/17 Pct Recovery = 87% Analysis Date = 01/16/17 Pct Recovery = 87% Analysis Date = 01/13/17 Pct Recovery = 87% Analysis Date = 01/13/17 Pct Recovery = 87% Analysis Date = 01/10/17 Pct Recovery = 87% Analysis Date = 01/10/17 Pct Recovery = 87% Analysis Date = 01/08/17 Pct Recovery = 87% Analysis Date = 01/08/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/05/17 Pct Recovery = 87% Analysis Date = 01/02/17 Pct Recovery = 87% Analysis Date = 01/02/17 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 87% Analysis Date = 12/31/16 Pct Recovery = 87% Analysis Date = 12/28/16 Pct Recovery = 87% Analysis Date = 12/28/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 87% Analysis Date = 12/25/16 Pct Recovery = 87% Analysis Date = 12/23/16 Pct Recovery = 88% Analysis Date = 12/23/16 Pct Recovery = 88% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/20/16 Pct Recovery = 88% Analysis Date = 12/17/16 Pct Recovery = 88% Analysis Date = 12/17/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/15/16 Pct Recovery = 88% Analysis Date = 12/12/16 Pct Recovery = 88% Analysis Date = 12/12/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/09/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 88% Analysis Date = 12/07/16 Pct Recovery = 88% Analysis Date = 12/04/16 Pct Recovery = 88% Analysis Date = 12/04/16 Pct Recovery = 88% Analysis Date = 12/01/16 Pct Recovery = 88% Analysis Date = 12/01/16 Pct Recovery = 88% Analysis Date = 11/29/16 Pct Recovery = 88% Analysis Date = 11/29/16 Pct Recovery = 88% Analysis Date = 11/26/16 Pct Recovery = 88% Analysis Date = 11/26/16 Pct Recovery = 88% Analysis Date = 11/23/16 Pct Recovery = 89% Analysis Date = 11/23/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/21/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/18/16 Pct Recovery = 89% Analysis Date = 11/15/16 Pct Recovery = 89% Analysis Date = 11/15/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/13/16 Pct Recovery = 89% Analysis Date = 11/10/16 Pct Recovery = 90% Analysis Date = 11/10/16 Pct Recovery = 90% Analysis Date = 11/07/16 Pct Recovery = 90% Analysis Date = 11/07/16 Pct Recovery = 90% Analysis Date = 11/05/16 Pct Recovery = 90% Analysis Date = 11/05/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 11/02/16 Pct Recovery = 90% Analysis Date = 10/30/16 Pct Recovery = 90% Analysis Date = 10/30/16 Pct Recovery = 90% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/28/16 Pct Recovery = 91% Analysis Date = 10/25/16 Pct Recovery = 91% Analysis Date = 10/25/16 Pct Recovery = 91% Analysis Date = 10/22/16 Pct Recovery = 91% Analysis Date = 10/22/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/19/16 Pct Recovery = 91% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/17/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/14/16 Pct Recovery = 92% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/11/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/09/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/06/16 Pct Recovery = 92% Analysis Date = 10/03/16 Pct Recovery = 93% Analysis Date = 10/03/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 10/01/16 Pct Recovery = 93% Analysis Date = 09/28/16 Pct Recovery = 93% Analysis Date = 09/28/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/25/16 Pct Recovery = 93% Analysis Date = 09/23/16 Pct Recovery = 93% Analysis Date = 09/23/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/20/16 Pct Recovery = 93% Analysis Date = 09/17/16 Pct Recovery = 94% Analysis Date = 09/17/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/15/16 Pct Recovery = 94% Analysis Date = 09/12/16 Pct Recovery = 94% Analysis Date = 09/12/16 Pct Recovery = 94% Analysis Date = 09/09/16 Pct Recovery = 94% Analysis Date = 09/09/16 Pct Recovery = 94% Analysis Date = 09/07/16 Pct Recovery = 94% Analysis Date = 09/07/16 Pct Recovery = 94% Analysis Date = 09/04/16 Pct Recovery = 94% Analysis Date = 09/04/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 09/01/16 Pct Recovery = 94% Analysis Date = 08/30/16 Pct Recovery = 95% Analysis Date = 08/30/16 Pct Recovery = 95% Analysis Date = 08/27/16 Pct Recovery = 95% Analysis Date = 08/27/16 Pct Recovery = 95% Analysis Date = 08/24/16 Pct Recovery = 95% Analysis Date = 08/24/16 Pct Recovery = 95% Analysis Date = 08/22/16 Pct Recovery = 95% Analysis Date = 08/22/16 Pct Recovery = 95% Analysis Date = 08/19/16 Pct Recovery = 95% Analysis Date = 08/19/16 Pct Recovery = 95% Analysis Date = 08/16/16 Pct Recovery = 95% Analysis Date = 08/16/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/14/16 Pct Recovery = 95% Analysis Date = 08/11/16 Pct Recovery = 95% Analysis Date = 08/11/16 Pct Recovery = 95% Analysis Date = 08/08/16 Pct Recovery = 95% Analysis Date = 08/08/16 Pct Recovery = 95% Analysis Date = 08/06/16 Pct Recovery = 95% Analysis Date = 08/06/16 Pct Recovery = 95% Analysis Date = 08/03/16 Pct Recovery = 95% Analysis Date = 08/03/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/31/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/29/16 Pct Recovery = 95% Analysis Date = 07/26/16 Pct Recovery = 95% Analysis Date = 07/26/16 Pct Recovery = 95% Analysis Date = 07/23/16 Pct Recovery = 95% Analysis Date = 07/23/16 Pct Recovery = 95% Analysis Date = 07/21/16 Pct Recovery = 95% Analysis Date = 07/21/16 Pct Recovery = 95% Analysis Date = 07/18/16 Pct Recovery = 96% Analysis Date = 07/18/16 Pct Recovery = 96% Analysis Date = 07/15/16 Pct Recovery = 96% Analysis Date = 07/15/16 Pct Recovery = 96% Analysis Date = 07/13/16 Pct Recovery = 96% Analysis Date = 07/13/16 Pct Recovery = 96% Analysis Date = 07/10/16 Pct Recovery = 96% Analysis Date = 07/10/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/07/16 Pct Recovery = 96% Analysis Date = 07/05/16 Pct Recovery = 96% Analysis Date = 07/05/16 Pct Recovery = 96% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 07/02/16 Pct Recovery = 97% Analysis Date = 06/29/16 Pct Recovery = 97% Analysis Date = 06/29/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/27/16 Pct Recovery = 97% Analysis Date = 06/24/16 Pct Recovery = 97% Analysis Date = 06/24/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/21/16 Pct Recovery = 97% Analysis Date = 06/19/16 Pct Recovery = 97% Analysis Date = 06/19/16 Pct Recovery = 97% Analysis Date = 06/16/16 Pct Recovery = 98% Analysis Date = 06/16/16 Pct Recovery = 98% Analysis Date = 06/13/16 Pct Recovery = 98% Analysis Date = 06/13/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/11/16 Pct Recovery = 98% Analysis Date = 06/08/16 Pct Recovery = 98% Analysis Date = 06/08/16 Pct Recovery = 98% Analysis Date = 06/05/16 Pct Recovery = 98% Analysis Date = 06/05/16 Pct Recovery = 98% Analysis Date = 06/03/16 Pct Recovery = 98% Analysis Date = 06/03/16 Pct Recovery = 98% Analysis Date = 05/31/16 Pct Recovery = 98% Analysis Date = 05/31/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/28/16 Pct Recovery = 98% Analysis Date = 05/26/16 Pct Recovery = 98% Analysis Date = 05/26/16 Pct Recovery = 98% Analysis Date = 05/23/16 Pct Recovery = 99% Analysis Date = 05/23/16 Pct Recovery = 99% Analysis Date = 05/20/16 Pct Recovery = 99% Analysis Date = 05/20/16 Pct Recovery = 99% Analysis Date = 05/18/16 Pct Recovery = 99% Analysis Date = 05/18/16 Pct Recovery = 99% Analysis Date = 05/15/16 Pct Recovery = 99% Analysis Date = 05/15/16 Pct Recovery = 99% Analysis Date = 05/12/16 Pct Recovery = 99% Analysis Date = 05/12/16 Pct Recovery = 99% Analysis Date = 05/10/16 Pct Recovery = 99% Analysis Date = 05/10/16 Pct Recovery = 99% Analysis Date = 05/07/16 Pct Recovery = 99% Analysis Date = 05/07/16 Pct Recovery = 99% Analysis Date = 05/04/16 Pct Recovery = 99% Analysis Date = 05/04/16 Pct Recovery = 99% Analysis Date = 05/02/16 Pct Recovery = 99% Analysis Date = 05/02/16 Pct Recovery = 99% Analysis Date = 04/29/16 Pct Recovery = 99% Analysis Date = 04/29/16 Pct Recovery = 99% Analysis Date = 04/26/16 Pct Recovery = 100% Analysis Date = 04/26/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 100% Analysis Date = 04/24/16 Pct Recovery = 100% Analysis Date = 04/21/16 Pct Recovery = 100% Analysis Date = 04/21/16 Pct Recovery = 100% Analysis Date = 04/18/16 Pct Recovery = 100% Analysis Date = 04/18/16 Pct Recovery = 100% Analysis Date = 04/16/16 Pct Recovery = 100% Analysis Date = 04/16/16 Pct Recovery = 100% Analysis Date = 04/13/16 Pct Recovery = 100% Analysis Date = 04/13/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/10/16 Pct Recovery = 100% Analysis Date = 04/08/16 Pct Recovery = 100% Analysis Date = 04/08/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 04/05/16 Pct Recovery = 100% Analysis Date = 04/02/16 Pct Recovery = 100% Analysis Date = 04/02/16 Pct Recovery = 100% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/31/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 101% Analysis Date = 03/28/16 Pct Recovery = 101% Analysis Date = 03/25/16 Pct Recovery = 101% Analysis Date = 03/25/16 Pct Recovery = 101% Analysis Date = 03/23/16 Pct Recovery = 101% Analysis Date = 03/23/16 Pct Recovery = 101% Analysis Date = 03/20/16 Pct Recovery = 101% Analysis Date = 03/20/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/17/16 Pct Recovery = 101% Analysis Date = 03/15/16 Pct Recovery = 101% Analysis Date = 03/15/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/12/16 Pct Recovery = 101% Analysis Date = 03/09/16 Pct Recovery = 101% Analysis Date = 03/09/16 Pct Recovery = 101% Analysis Date = 03/07/16 Pct Recovery = 101% Analysis Date = 03/07/16 Pct Recovery = 101% Analysis Date = 03/04/16 Pct Recovery = 101% Analysis Date = 03/04/16 Pct Recovery = 101% Analysis Date = 03/01/16 Pct Recovery = 101% Analysis Date = 03/01/16 Pct Recovery = 101% Analysis Date = 02/28/16 Pct Recovery = 101% Analysis Date = 02/28/16 Pct Recovery = 101% Analysis Date = 02/25/16 Pct Recovery = 101% Analysis Date = 02/25/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/22/16 Pct Recovery = 101% Analysis Date = 02/20/16 Pct Recovery = 101% Analysis Date = 02/20/16 Pct Recovery = 101% Analysis Date = 02/17/16 Pct Recovery = 101% Analysis Date = 02/17/16 Pct Recovery = 101% Analysis Date = 02/14/16 Pct Recovery = 101% Analysis Date = 02/14/16 Pct Recovery = 101% Analysis Date = 02/12/16 Pct Recovery = 101% Analysis Date = 02/12/16 Pct Recovery = 101% Analysis Date = 02/09/16 Pct Recovery = 101% Analysis Date = 02/09/16 Pct Recovery = 101% Analysis Date = 02/06/16 Pct Recovery = 101% Analysis Date = 02/06/16 Pct Recovery = 101% Analysis Date = 02/04/16 Pct Recovery = 101% Analysis Date = 02/04/16 Pct Recovery = 101% Analysis Date = 02/01/16 Pct Recovery = 101% Analysis Date = 02/01/16 Pct Recovery = 101% Analysis Date = 01/29/16 Pct Recovery = 101% Analysis Date = 01/29/16 Pct Recovery = 101% Analysis Date = 01/27/16 Pct Recovery = 101% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
BROMOFORM

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 50 94% 11% 92% 8%
Total 50 94% 11% 92% 8%

Sample Statistics
BROMOFORM

Characteristic N % % Basis
Plotted 50 100% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 50 .  
False Negatives 0 0% 0 out of 50
Not Spiked 52 .  
False Positives 0 0% 0 out of 52