OBSP Determination:
ACETATE, ETHYL
METHOD: 4437 , TESTIDCODE: 81585GM016

Analysis Date = 07/06/16 SpikeMix = Accu 216041354: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 106% Analysis Date = 07/29/16 SpikeMix = Supelco LC20145V: 40 µl & NSI 041516: 40 µl & NSI 041416HVOC: 40 µl Pct Recovery = 91% Analysis Date = 09/28/16 SpikeMix = Accu 216041354: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl Pct Recovery = 92% Analysis Date = 11/10/16 SpikeMix = NSI 041516: 25 µl & Phenova B20160303: 25 µl & Accu 216041225: 25 µl Pct Recovery = 108% Analysis Date = 06/29/17 SpikeMix = Supelco LC20145V: 25 µl & Abs 060916HVOC: 25 µl & Accu 216041225: 25 µl Pct Recovery = 77% Analysis Date = 05/21/16 SpikeMix = Supelco LC20145V: 25 µl & NSI 041516: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 127% Analysis Date = 08/11/16 SpikeMix = Phenova B20160303: 25 µl & Supelco LC20145V: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 76% Analysis Date = 09/08/16 SpikeMix = Abs 060916HVOC: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 100% Analysis Date = 04/13/17 SpikeMix = Accu 216041354: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 80% Analysis Date = 06/17/17 SpikeMix = Supelco LC20145V: 25 µl & Phenova B20160303: 25 µl & NSI 041416HVOC: 25 µl Pct Recovery = 88% Analysis Date = 08/16/17 SpikeMix = ChemService 6441300: 15 µl & Spex Organics BW170726021: 15 µl & ChemService 6424 Pct Recovery = 108% Analysis Date = 05/20/16 SpikeMix = Accu 216041354: 15 µl & NSI 041516: 15 µl & Accu 216041225: 15 µl Pct Recovery = 144% Analysis Date = 11/02/16 SpikeMix = Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & Accu 216041225: 15 µl Pct Recovery = 86% Analysis Date = 02/02/17 SpikeMix = Accu 216041354: 15 µl & NSI 110916: 15 µl & Accu 216041225: 15 µl Pct Recovery = 82% Analysis Date = 02/24/17 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & Accu 216041225: 15 µl Pct Recovery = 91% Analysis Date = 03/24/17 SpikeMix = Abs 060916HVOC: 15 µl & Phenova B20160303: 15 µl & Accu 216041225: 15 µl Pct Recovery = 108% Analysis Date = 06/01/17 SpikeMix = Accu 216041354: 15 µl & Phenova B20160303: 15 µl & Accu 216041225: 15 µl Pct Recovery = 84% Analysis Date = 06/03/16 SpikeMix = NSI 041516: 15 µl & Phenova B20160303: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 111% Analysis Date = 07/06/16 SpikeMix = Phenova B20160303: 15 µl & Accu 216041354: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 103% Analysis Date = 01/03/17 SpikeMix = Supelco LC20145V: 15 µl & Abs 060916HVOC: 15 µl & NSI 041416HVOC: 15 µl Pct Recovery = 83% Analysis Date = 04/28/16 SpikeMix = ChemService 3818700: 15 µl & Supelco LC13544: 15 µl Pct Recovery = 106% Analysis Date = 08/10/17 SpikeMix = ChemService 6441300: 10 µl & ChemService 6441600: 10 µl & ChemService 6424500: 1 Pct Recovery = 98% Analysis Date = 08/30/17 SpikeMix = ChemService 6441300: 10 µl & ChemService 6424500: 10 µl & Spex Organics BW170725 Pct Recovery = 83% Analysis Date = 03/22/16 SpikeMix = Supelco LC13544: 10 µl & NSI 050515HVOC: 10 µl Pct Recovery = 117% Analysis Date = 02/12/16 SpikeMix = ERA 0601-15-05: 10 µl & Accu 215041338: 10 µl Pct Recovery = 86% Analysis Date = 08/30/17 Pct Recovery = 92% Analysis Date = 08/27/17 Pct Recovery = 92% Analysis Date = 08/27/17 Pct Recovery = 92% Analysis Date = 08/24/17 Pct Recovery = 92% Analysis Date = 08/24/17 Pct Recovery = 92% Analysis Date = 08/21/17 Pct Recovery = 92% Analysis Date = 08/21/17 Pct Recovery = 92% Analysis Date = 08/18/17 Pct Recovery = 91% Analysis Date = 08/18/17 Pct Recovery = 91% Analysis Date = 08/15/17 Pct Recovery = 91% Analysis Date = 08/15/17 Pct Recovery = 91% Analysis Date = 08/13/17 Pct Recovery = 91% Analysis Date = 08/13/17 Pct Recovery = 91% Analysis Date = 08/10/17 Pct Recovery = 91% Analysis Date = 08/10/17 Pct Recovery = 91% Analysis Date = 08/07/17 Pct Recovery = 91% Analysis Date = 08/07/17 Pct Recovery = 91% Analysis Date = 08/04/17 Pct Recovery = 91% Analysis Date = 08/04/17 Pct Recovery = 91% Analysis Date = 08/01/17 Pct Recovery = 91% Analysis Date = 08/01/17 Pct Recovery = 91% Analysis Date = 07/29/17 Pct Recovery = 91% Analysis Date = 07/29/17 Pct Recovery = 91% Analysis Date = 07/27/17 Pct Recovery = 91% Analysis Date = 07/27/17 Pct Recovery = 91% Analysis Date = 07/24/17 Pct Recovery = 91% Analysis Date = 07/24/17 Pct Recovery = 91% Analysis Date = 07/21/17 Pct Recovery = 91% Analysis Date = 07/21/17 Pct Recovery = 91% Analysis Date = 07/18/17 Pct Recovery = 91% Analysis Date = 07/18/17 Pct Recovery = 91% Analysis Date = 07/15/17 Pct Recovery = 91% Analysis Date = 07/15/17 Pct Recovery = 91% Analysis Date = 07/12/17 Pct Recovery = 91% Analysis Date = 07/12/17 Pct Recovery = 91% Analysis Date = 07/10/17 Pct Recovery = 91% Analysis Date = 07/10/17 Pct Recovery = 91% Analysis Date = 07/07/17 Pct Recovery = 91% Analysis Date = 07/07/17 Pct Recovery = 91% Analysis Date = 07/04/17 Pct Recovery = 91% Analysis Date = 07/04/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 07/01/17 Pct Recovery = 91% Analysis Date = 06/28/17 Pct Recovery = 91% Analysis Date = 06/28/17 Pct Recovery = 91% Analysis Date = 06/26/17 Pct Recovery = 91% Analysis Date = 06/26/17 Pct Recovery = 91% Analysis Date = 06/23/17 Pct Recovery = 90% Analysis Date = 06/23/17 Pct Recovery = 90% Analysis Date = 06/20/17 Pct Recovery = 90% Analysis Date = 06/20/17 Pct Recovery = 90% Analysis Date = 06/17/17 Pct Recovery = 90% Analysis Date = 06/17/17 Pct Recovery = 90% Analysis Date = 06/14/17 Pct Recovery = 90% Analysis Date = 06/14/17 Pct Recovery = 90% Analysis Date = 06/11/17 Pct Recovery = 90% Analysis Date = 06/11/17 Pct Recovery = 90% Analysis Date = 06/09/17 Pct Recovery = 90% Analysis Date = 06/09/17 Pct Recovery = 90% Analysis Date = 06/06/17 Pct Recovery = 90% Analysis Date = 06/06/17 Pct Recovery = 90% Analysis Date = 06/03/17 Pct Recovery = 90% Analysis Date = 06/03/17 Pct Recovery = 90% Analysis Date = 05/31/17 Pct Recovery = 90% Analysis Date = 05/31/17 Pct Recovery = 90% Analysis Date = 05/28/17 Pct Recovery = 90% Analysis Date = 05/28/17 Pct Recovery = 90% Analysis Date = 05/25/17 Pct Recovery = 90% Analysis Date = 05/25/17 Pct Recovery = 90% Analysis Date = 05/23/17 Pct Recovery = 90% Analysis Date = 05/23/17 Pct Recovery = 90% Analysis Date = 05/20/17 Pct Recovery = 90% Analysis Date = 05/20/17 Pct Recovery = 90% Analysis Date = 05/17/17 Pct Recovery = 90% Analysis Date = 05/17/17 Pct Recovery = 90% Analysis Date = 05/14/17 Pct Recovery = 90% Analysis Date = 05/14/17 Pct Recovery = 90% Analysis Date = 05/11/17 Pct Recovery = 90% Analysis Date = 05/11/17 Pct Recovery = 90% Analysis Date = 05/09/17 Pct Recovery = 90% Analysis Date = 05/09/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/06/17 Pct Recovery = 90% Analysis Date = 05/03/17 Pct Recovery = 90% Analysis Date = 05/03/17 Pct Recovery = 90% Analysis Date = 04/30/17 Pct Recovery = 90% Analysis Date = 04/30/17 Pct Recovery = 90% Analysis Date = 04/27/17 Pct Recovery = 90% Analysis Date = 04/27/17 Pct Recovery = 90% Analysis Date = 04/24/17 Pct Recovery = 90% Analysis Date = 04/24/17 Pct Recovery = 90% Analysis Date = 04/22/17 Pct Recovery = 89% Analysis Date = 04/22/17 Pct Recovery = 89% Analysis Date = 04/19/17 Pct Recovery = 89% Analysis Date = 04/19/17 Pct Recovery = 89% Analysis Date = 04/16/17 Pct Recovery = 89% Analysis Date = 04/16/17 Pct Recovery = 89% Analysis Date = 04/13/17 Pct Recovery = 89% Analysis Date = 04/13/17 Pct Recovery = 89% Analysis Date = 04/10/17 Pct Recovery = 89% Analysis Date = 04/10/17 Pct Recovery = 89% Analysis Date = 04/07/17 Pct Recovery = 89% Analysis Date = 04/07/17 Pct Recovery = 89% Analysis Date = 04/05/17 Pct Recovery = 89% Analysis Date = 04/05/17 Pct Recovery = 89% Analysis Date = 04/02/17 Pct Recovery = 89% Analysis Date = 04/02/17 Pct Recovery = 89% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/30/17 Pct Recovery = 90% Analysis Date = 03/27/17 Pct Recovery = 90% Analysis Date = 03/27/17 Pct Recovery = 90% Analysis Date = 03/24/17 Pct Recovery = 90% Analysis Date = 03/24/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/21/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/19/17 Pct Recovery = 90% Analysis Date = 03/16/17 Pct Recovery = 90% Analysis Date = 03/16/17 Pct Recovery = 90% Analysis Date = 03/13/17 Pct Recovery = 90% Analysis Date = 03/13/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/10/17 Pct Recovery = 90% Analysis Date = 03/07/17 Pct Recovery = 90% Analysis Date = 03/07/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 90% Analysis Date = 03/05/17 Pct Recovery = 90% Analysis Date = 03/02/17 Pct Recovery = 90% Analysis Date = 03/02/17 Pct Recovery = 90% Analysis Date = 02/27/17 Pct Recovery = 90% Analysis Date = 02/27/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/24/17 Pct Recovery = 90% Analysis Date = 02/21/17 Pct Recovery = 90% Analysis Date = 02/21/17 Pct Recovery = 90% Analysis Date = 02/18/17 Pct Recovery = 90% Analysis Date = 02/18/17 Pct Recovery = 90% Analysis Date = 02/16/17 Pct Recovery = 90% Analysis Date = 02/16/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/13/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 90% Analysis Date = 02/10/17 Pct Recovery = 90% Analysis Date = 02/07/17 Pct Recovery = 90% Analysis Date = 02/07/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/04/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 02/01/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/30/17 Pct Recovery = 90% Analysis Date = 01/27/17 Pct Recovery = 90% Analysis Date = 01/27/17 Pct Recovery = 90% Analysis Date = 01/24/17 Pct Recovery = 91% Analysis Date = 01/24/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/21/17 Pct Recovery = 91% Analysis Date = 01/18/17 Pct Recovery = 91% Analysis Date = 01/18/17 Pct Recovery = 91% Analysis Date = 01/16/17 Pct Recovery = 91% Analysis Date = 01/16/17 Pct Recovery = 91% Analysis Date = 01/13/17 Pct Recovery = 91% Analysis Date = 01/13/17 Pct Recovery = 91% Analysis Date = 01/10/17 Pct Recovery = 91% Analysis Date = 01/10/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/07/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 91% Analysis Date = 01/04/17 Pct Recovery = 91% Analysis Date = 01/01/17 Pct Recovery = 91% Analysis Date = 01/01/17 Pct Recovery = 91% Analysis Date = 12/30/16 Pct Recovery = 91% Analysis Date = 12/30/16 Pct Recovery = 91% Analysis Date = 12/27/16 Pct Recovery = 91% Analysis Date = 12/27/16 Pct Recovery = 91% Analysis Date = 12/24/16 Pct Recovery = 91% Analysis Date = 12/24/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/21/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/18/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/15/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/13/16 Pct Recovery = 91% Analysis Date = 12/10/16 Pct Recovery = 91% Analysis Date = 12/10/16 Pct Recovery = 91% Analysis Date = 12/07/16 Pct Recovery = 91% Analysis Date = 12/07/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/04/16 Pct Recovery = 91% Analysis Date = 12/01/16 Pct Recovery = 91% Analysis Date = 12/01/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 91% Analysis Date = 11/28/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/26/16 Pct Recovery = 91% Analysis Date = 11/23/16 Pct Recovery = 91% Analysis Date = 11/23/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/20/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/17/16 Pct Recovery = 91% Analysis Date = 11/14/16 Pct Recovery = 91% Analysis Date = 11/14/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 91% Analysis Date = 11/12/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 91% Analysis Date = 11/09/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/06/16 Pct Recovery = 91% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 11/03/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/31/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/28/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/26/16 Pct Recovery = 92% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/23/16 Pct Recovery = 93% Analysis Date = 10/20/16 Pct Recovery = 93% Analysis Date = 10/20/16 Pct Recovery = 93% Analysis Date = 10/17/16 Pct Recovery = 93% Analysis Date = 10/17/16 Pct Recovery = 93% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/14/16 Pct Recovery = 94% Analysis Date = 10/11/16 Pct Recovery = 94% Analysis Date = 10/11/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/09/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/06/16 Pct Recovery = 94% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 10/03/16 Pct Recovery = 95% Analysis Date = 09/30/16 Pct Recovery = 95% Analysis Date = 09/30/16 Pct Recovery = 95% Analysis Date = 09/27/16 Pct Recovery = 95% Analysis Date = 09/27/16 Pct Recovery = 95% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/25/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/22/16 Pct Recovery = 96% Analysis Date = 09/19/16 Pct Recovery = 96% Analysis Date = 09/19/16 Pct Recovery = 96% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/16/16 Pct Recovery = 97% Analysis Date = 09/13/16 Pct Recovery = 97% Analysis Date = 09/13/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 97% Analysis Date = 09/10/16 Pct Recovery = 97% Analysis Date = 09/08/16 Pct Recovery = 98% Analysis Date = 09/08/16 Pct Recovery = 98% Analysis Date = 09/05/16 Pct Recovery = 98% Analysis Date = 09/05/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 09/02/16 Pct Recovery = 98% Analysis Date = 08/30/16 Pct Recovery = 99% Analysis Date = 08/30/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/27/16 Pct Recovery = 99% Analysis Date = 08/24/16 Pct Recovery = 99% Analysis Date = 08/24/16 Pct Recovery = 99% Analysis Date = 08/22/16 Pct Recovery = 99% Analysis Date = 08/22/16 Pct Recovery = 99% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/19/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 100% Analysis Date = 08/16/16 Pct Recovery = 100% Analysis Date = 08/13/16 Pct Recovery = 100% Analysis Date = 08/13/16 Pct Recovery = 100% Analysis Date = 08/10/16 Pct Recovery = 101% Analysis Date = 08/10/16 Pct Recovery = 101% Analysis Date = 08/07/16 Pct Recovery = 101% Analysis Date = 08/07/16 Pct Recovery = 101% Analysis Date = 08/05/16 Pct Recovery = 101% Analysis Date = 08/05/16 Pct Recovery = 101% Analysis Date = 08/02/16 Pct Recovery = 102% Analysis Date = 08/02/16 Pct Recovery = 102% Analysis Date = 07/30/16 Pct Recovery = 102% Analysis Date = 07/30/16 Pct Recovery = 102% Analysis Date = 07/27/16 Pct Recovery = 103% Analysis Date = 07/27/16 Pct Recovery = 103% Analysis Date = 07/24/16 Pct Recovery = 103% Analysis Date = 07/24/16 Pct Recovery = 103% Analysis Date = 07/22/16 Pct Recovery = 103% Analysis Date = 07/22/16 Pct Recovery = 103% Analysis Date = 07/19/16 Pct Recovery = 104% Analysis Date = 07/19/16 Pct Recovery = 104% Analysis Date = 07/16/16 Pct Recovery = 104% Analysis Date = 07/16/16 Pct Recovery = 104% Analysis Date = 07/13/16 Pct Recovery = 105% Analysis Date = 07/13/16 Pct Recovery = 105% Analysis Date = 07/10/16 Pct Recovery = 105% Analysis Date = 07/10/16 Pct Recovery = 105% Analysis Date = 07/07/16 Pct Recovery = 105% Analysis Date = 07/07/16 Pct Recovery = 105% Analysis Date = 07/05/16 Pct Recovery = 106% Analysis Date = 07/05/16 Pct Recovery = 106% Analysis Date = 07/02/16 Pct Recovery = 106% Analysis Date = 07/02/16 Pct Recovery = 106% Analysis Date = 06/29/16 Pct Recovery = 106% Analysis Date = 06/29/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/26/16 Pct Recovery = 106% Analysis Date = 06/23/16 Pct Recovery = 106% Analysis Date = 06/23/16 Pct Recovery = 106% Analysis Date = 06/20/16 Pct Recovery = 107% Analysis Date = 06/20/16 Pct Recovery = 107% Analysis Date = 06/18/16 Pct Recovery = 107% Analysis Date = 06/18/16 Pct Recovery = 107% Analysis Date = 06/15/16 Pct Recovery = 107% Analysis Date = 06/15/16 Pct Recovery = 107% Analysis Date = 06/12/16 Pct Recovery = 107% Analysis Date = 06/12/16 Pct Recovery = 107% Analysis Date = 06/09/16 Pct Recovery = 107% Analysis Date = 06/09/16 Pct Recovery = 107% Analysis Date = 06/06/16 Pct Recovery = 107% Analysis Date = 06/06/16 Pct Recovery = 107% Analysis Date = 06/04/16 Pct Recovery = 108% Analysis Date = 06/04/16 Pct Recovery = 108% Analysis Date = 06/01/16 Pct Recovery = 108% Analysis Date = 06/01/16 Pct Recovery = 108% Analysis Date = 05/29/16 Pct Recovery = 108% Analysis Date = 05/29/16 Pct Recovery = 108% Analysis Date = 05/26/16 Pct Recovery = 108% Analysis Date = 05/26/16 Pct Recovery = 108% Analysis Date = 05/23/16 Pct Recovery = 108% Analysis Date = 05/23/16 Pct Recovery = 108% Analysis Date = 05/20/16 Pct Recovery = 108% Analysis Date = 05/20/16 Pct Recovery = 108% Analysis Date = 05/18/16 Pct Recovery = 109% Analysis Date = 05/18/16 Pct Recovery = 109% Analysis Date = 05/15/16 Pct Recovery = 109% Analysis Date = 05/15/16 Pct Recovery = 109% Analysis Date = 05/12/16 Pct Recovery = 109% Analysis Date = 05/12/16 Pct Recovery = 109% Analysis Date = 05/09/16 Pct Recovery = 109% Analysis Date = 05/09/16 Pct Recovery = 109% Analysis Date = 05/06/16 Pct Recovery = 109% Analysis Date = 05/06/16 Pct Recovery = 109% Analysis Date = 05/03/16 Pct Recovery = 109% Analysis Date = 05/03/16 Pct Recovery = 109% Analysis Date = 05/01/16 Pct Recovery = 110% Analysis Date = 05/01/16 Pct Recovery = 110% Analysis Date = 04/28/16 Pct Recovery = 110% Analysis Date = 04/28/16 Pct Recovery = 110% Analysis Date = 04/25/16 Pct Recovery = 110% Analysis Date = 04/25/16 Pct Recovery = 110% Analysis Date = 04/22/16 Pct Recovery = 110% Analysis Date = 04/22/16 Pct Recovery = 110% Analysis Date = 04/19/16 Pct Recovery = 110% Analysis Date = 04/19/16 Pct Recovery = 110% Analysis Date = 04/16/16 Pct Recovery = 110% Analysis Date = 04/16/16 Pct Recovery = 110% Analysis Date = 04/14/16 Pct Recovery = 110% Analysis Date = 04/14/16 Pct Recovery = 110% Analysis Date = 04/11/16 Pct Recovery = 111% Analysis Date = 04/11/16 Pct Recovery = 111% Analysis Date = 04/08/16 Pct Recovery = 111% Analysis Date = 04/08/16 Pct Recovery = 111% Analysis Date = 04/05/16 Pct Recovery = 111% Analysis Date = 04/05/16 Pct Recovery = 111% Analysis Date = 04/02/16 Pct Recovery = 111% Analysis Date = 04/02/16 Pct Recovery = 111% Analysis Date = 03/31/16 Pct Recovery = 111% Analysis Date = 03/31/16 Pct Recovery = 111% Analysis Date = 03/28/16 Pct Recovery = 111% Analysis Date = 03/28/16 Pct Recovery = 111% Analysis Date = 03/25/16 Pct Recovery = 111% Analysis Date = 03/25/16 Pct Recovery = 111% Analysis Date = 03/22/16 Pct Recovery = 112% Analysis Date = 03/22/16 Pct Recovery = 112% Analysis Date = 03/19/16 Pct Recovery = 112% Analysis Date = 03/19/16 Pct Recovery = 112% Analysis Date = 03/16/16 Pct Recovery = 112% Analysis Date = 03/16/16 Pct Recovery = 112% Analysis Date = 03/14/16 Pct Recovery = 112% Analysis Date = 03/14/16 Pct Recovery = 112% Analysis Date = 03/11/16 Pct Recovery = 112% Analysis Date = 03/11/16 Pct Recovery = 112% Analysis Date = 03/08/16 Pct Recovery = 112% Analysis Date = 03/08/16 Pct Recovery = 112% Analysis Date = 03/05/16 Pct Recovery = 112% Analysis Date = 03/05/16 Pct Recovery = 112% Analysis Date = 03/02/16 Pct Recovery = 112% Analysis Date = 03/02/16 Pct Recovery = 112% Analysis Date = 02/28/16 Pct Recovery = 112% Analysis Date = 02/28/16 Pct Recovery = 112% Analysis Date = 02/26/16 Pct Recovery = 113% Analysis Date = 02/26/16 Pct Recovery = 113% Analysis Date = 02/23/16 Pct Recovery = 113% Analysis Date = 02/23/16 Pct Recovery = 113% Analysis Date = 02/20/16 Pct Recovery = 113% Analysis Date = 02/20/16 Pct Recovery = 113% Analysis Date = 02/17/16 Pct Recovery = 113% Analysis Date = 02/17/16 Pct Recovery = 113% Analysis Date = 02/14/16 Pct Recovery = 113% Analysis Date = 02/14/16 Pct Recovery = 113% Analysis Date = 02/12/16 Pct Recovery = 113% Y = 1.5 Y = 0.5 Y = 1
The SGPlot Procedure

Plotted Points Statistics
ACETATE, ETHYL

Spike Level N Mean Std-Dev. Median F_Pseudo
>= Reporting Level 25 97% 17% 92% 17%
Total 25 97% 17% 92% 17%

Sample Statistics
ACETATE, ETHYL

Characteristic N % % Basis
Plotted 25 96% Spiked
Estimated Values 0 0% Spiked
Deleted Values 0 0% Spiked + Not Spiked
Spiked, Censored 0 0% Spiked
Spiked 26 .  
False Negatives 1 4% 1 out of 26
Not Spiked 12 .  
False Positives 1 8% 1 out of 12